### PA DEP TENORM Study Report

– Appendix F Rev. 0

January 2015 

### APPENDIX F

XRF ANALYTICAL ANALYSES RESULTSJanuary 2015

F

- 1 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Solids Analysis

Study ID Date/Time Aluminum

Result (ppm) Aluminum

Error (ppm) Antimony

Result (ppm) Antimony

Error (ppm) Arsenic

Result (ppm) Arsenic

Error (ppm) Barium

Result (ppm) Barium

Error (ppm) Bismuth

Result (ppm) Bismuth

Error (ppm)

BR

- 30

- SL

- 029 07/29/13 71,500 80 .0 15.9 0.8 00 5 .00 0.5 00 12,400 30 .0 28.8 0.6 00

WP

- 02

- SL

- 036 07/24/13 75,800 100 26.8 0.7 00 33.2 0.5 00 29,000 40 .0 1 .00 0 .000

WP

- 03

- SL

- 038 07/26/13 124,000 100 3 .00 0 .000 16.5 0.4 00 1,480 14 .0 1 .00 0 .000

WP

- 03

- SL

- 065 11/08/13 94,400 120 25.5 0.4 00 36.7 0.7 00 74,300 80 .0 0.7 00 0.1 00

WP

- 04

- SL

- 001 06/17/13 231,000 200 5.5 0 0.6 00 16.1 0.5 00 4,000 15 .0 1 .00 0 .000

WP

- 04

- SL

- 002 06/17/13 111,000 100 3 .00 0.000 8 .00 0.3 00 9,620 23 .0 1 .00 0 .000

WP

- 04

- SL

- 003 06/17/13 121,000 100 3 .00 0.000 10.3 0.3 00 5,390 18 .0 1 .00 0 .000

WP

- 04

- SL

- 004 06/17/13 120,000 100 3 .00 0.000 8.7 0 0.4 00 14,200 30 .0 1 .00 0 .000

WP

- 04

- SL

- 005 06/17/13 127,000 100 9.3 0 0.5 00 10.6 0.4 00 12,900 30 .0 1 .00 0 .000

WP

- 04

- SL

- 006 06/17/13 126,000 100 3 .00 0.000 10.3 0.4 00 3,510 15 .0 1 .00 0 .000

WP

- 04

- SL

- 007 06/17/13 111,000 100 3 .00 0.000 7.1 0 0.3 00 2,690 14 .0 1 .00 0 .000

WP

- 04

- SL

- 008 06/17/13 117,000 100 3 .00 0.000 12.5 0.4 00 4,920 17 .0 1 .00 0 .000

WP

- 04

- SL

- 009 06/20/13 42,900 80 3 .00 0.000 11.1 0.5 00 169,000 100 1 .00 0 .000

WP

- 04

- SL

- 010 06/20/13 64,100 120 3 .00 0.000 11.3 0.5 00 149,000 100 1 .00 0 .000

WP

- 04

- SL

- 011 06/20/13 84,200 110 15.4 0.2 00 6.4 0 0.4 00 87,500 90 .0 0.2 00 0.2 00

WP

- 04

- SL

- 012 06/20/13 71,600 110 19.6 0.3 00 20.1 0.5 00 101,000 100 1 .00 0.3 00

WP

- 05

- SL

- 027 07/08/13 150,000 200 22.2 0.7 00 15.2 0.8 00 33,400 50 .0 1 .00 0 .00

WP

- 05

- SL

- 028 07/08/13 191,000 200 4 .00 0 .000 24.6 0.6 00 17,600 30 .0 0.4 00 0.1 00

WP

- 05

- SL

- 029 07/08/13 209,000 300 78.2 1.9 0 9 .00 0.5 00 5,990 21 .0 1 .00 0 .000

WP

- 05

- SL

- 030 07/08/13 117,000 200 25.3 0.5 00 9.8 0 0.5 00 54,400 70 .0 1 .00 0 .000

WP

- 05

- SL

- 031 07/08/13 173,000 200 11.9 0.6 00 21.1 0.5 00 16,200 30 .0 1 .00 0 .000

WP

- 05

- SL

- 032 07/08/13 107,000 200 24.7 0.6 00 13.7 0.9 00 43,200 50 .0 1 .00 0 .000

WP

- 05

- SL

- 033 07/08/13 146,000 200 20.6 0.7 00 11.9 0.6 00 27,600 40 .0 1 .00 0 .000

WP

- 05

- SL

- 034 07/08/13 102,000 100 12.2 0.4 00 15.2 0.7 00 26,400 40 .0 1 .00 0 .000

WP

- 06

- SL

- 014 07/01/13 108,000 100 3 .00 0.000 14.5 0.3 00 6,070 19 .0 1 .00 0 .000

WP

- 06

- SL

- 015 07/01/13 121,000 100 3 .00 0.000 18.6 0.4 00 15,800 30 .0 1 .00 0 .000

WP

- 06

- SL

- 016 07/01/13 122,000 100 3 .00 0.000 10.6 0.3 00 2,060 14 .0 1 .00 0 .000

WP

- 06

- SL

- 017 07/01/13 114,000 100 3 .00 0.000 10.4 0.4 00 1,720 13 .0 1 .00 0 .000

WP

- 06

- SL

- 018 07/01/13 40,100 210 7.9 0 0.9 00 0.5 00 0 .000 1,140 14 .0 1 .00 0 .000

WP

- 06

- SL

- 019 07/01/13 44,500 180 3 .00 0.000 0.9 00 0.3 00 1,370 15 .0 1 .00 0 .000January 2015

F

- 2 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Solids Analysis

Study ID Date/Time Aluminum

Result (ppm) Aluminum

Error (ppm) Antimony

Result (ppm) Antimony

Error (ppm) Arsenic

Result (ppm) Arsenic

Error (ppm) Barium

Result (ppm) Barium

Error (ppm) Bismuth

Result (ppm) Bismuth

Error (ppm)

WP

- 06

- SL

- 020 07/01/13 34,500 100 3 .00 0.000 1.7 0 0.3 00 2,360 14 .0 1 .00 0 .000

WP

- 06

- SL

- 021 07/01/13 89,500 320 13.7 1.7 0 2.2 0 0.4 00 668 15 .0 1 .00 0 .000

WP

- 06

- SL

- 022 07/01/13 168,000 200 4 .00 0 .000 11.2 0.5 00 904 12 .0 1 .00 0 .000

WP

- 06

- SL

- 023 07/01/13 103,000 200 4 .00 0 .000 2 .00 0.3 00 318 11 .0 1 .00 0 .000

WP

- 06

- SL

- 024 07/08/13 59,200 350 4.8 0 0.9 1.9 0 0.3 00 384 12 .0 1 .00 0 .000

WP

- 06

- SL

- 025 07/08/13 138,000 200 4 .00 0 .000 11 .0 0.4 00 809 12 .0 1 .00 0 .000

WP

- 06

- SL

- 026 07/08/13 116,000 400 4 .00 0 .000 2.3 0 0.4 00 1,250 15 .0 1 .00 0 .000

WP

- 06

- SL

- 037 07/25/13 35,100 180 5.1 0 0.1 00 37.7 2.7 0 130,000 100 1 .00 0 .000

WP

- 07

- SL

- 039 08/05/13 127,000 100 3 .00 0.000 14.1 0.3 00 731 11 .0 1 .00 0 .000

WP

- 07

- SL

- 040 08/05/13 128,000 100 3 .00 0.000 16.6 0.4 00 891 12 .0 1 .00 0 .000

WP

- 07

- SL

- 041 08/05/13 118,000 100 3 .00 0.000 12.4 0.4 00 915 12 .0 1 .00 0 .000

WP

- 10

- SL

- 045 08/26/13 52,500 70.0 5.4 0 0.6 00 3.7 0 0.4 00 2,780 15 .0 1 .00 0 .000

WP

- 10

- SL

- 048 08/30/13 67,100 90.0 12.8 0.3 00 31.8 1.4 0 66,000 70 .0 1 .00 0 .000

WP

- 11

- SL

- 047 08/27/13 68,500 250 27.9 1.3 0 0.3 00 0.3 00 5,110 20 .0 1 .00 0 .000

WP

- 11

- SL

- 068 11/14/13 22,000 50 .0 5.1 0 0.1 00 5.6 0 0.5 00 126,000 100 1.1 0.3 00

WP

- 12

- SL

- 052 09/05/13 112,000 100 57.5 0.8 00 16.1 0.6 00 61,200 70 .0 1 .00 0 .000

WP

- 12

- SL

- 053 09/05/13 100,000 100 6.8 00 0.5 00 15.6 0.4 00 11,100 30 .0 0.5 00 0.2 00

WP

- 12

- SL

- 055 09/11/13 49,500 100 3 .00 0.000 6.6 0 1.1 0 341,000 300 1 .00 0 .000

WP

- 12

- SL

- 056 09/11/13 97,600 160 3 .00 0.000 44.8 1.7 0 388,000 300 2.2 0 0.4 00

WP

- 13

- SL

- 059 10/15/13 94,300 100 3 .00 0.000 9.7 0 0.4 00 2,920 15 .0 1 .00 0 .000

WP

- 13

- SL

- 062 10/21/13 65,600 10 .0 61.1 0.9 0 37.9 0.9 00 39,000 50 .0 1 .00 0 .000

WP

- 14

- SL

- 073 01/31/14 75,100 100 3 .00 0.000 16.7 0.4 00 4,130 17 .0 1 .00 0 .000

WP

- 14

- SL

- 074 01/31/14 125,000 100 3 .00 0.000 12.4 0.3 00 1,020 12 .0 1 .00 0 .000

WP

- 14

- SL

- 077 02/07/14 24,600 50 .0 22.9 0.4 0 32.5 0.7 00 76,600 80 .0 1.5 0 0.2 00

WP

- 14

- SL

- 078 02/07/14 43,600 70 .0 23.6 0.4 00 31.1 0.6 00 72,500 70 .0 1 .00 0 .000

WP

- 14

- SL

- 079 02/07/14 23,300 60 .0 30.3 0.4 00 35.4 0.9 00 130,000 100 2 .00 0.3 00

WP

- 15

- SL

- 075 02/06/14 209,000 300 78.2 1.9 0 9 .00 0.5 00 5,990 21 .0 1 .00 0 .000January 2015

F

- 3 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Solids Analysis

Study ID Bromine

Result (ppm) Bromine

Error (ppm) Cadmium

Result (ppm) Cadmium

Error (ppm) Calcium

Result (ppm) Calcium

Error (ppm) Cerium

Result (ppm) Cerium

Error (ppm) Cesium

Result (ppm) Cesium

Error (ppm) Chlorine

Result (ppm) Chlorine

Error (ppm)

BR

- 30

- SL

- 029 61.1 0.4 00 8.3 0 0.8 00 24,400 30 .0 2 .00 0 .000 85.5 6.7 0 1,680 3 .00

WP

- 02

- SL

- 036 30.3 0.3 00 21 .0 1.1 0 26,200 40 .0 2 .00 0 .000 253 8.2 0 14,900 10 .0

WP

- 03

- SL

- 038 25.6 0.3 00 2.1 0 0.5 00 9,820 24 .0 137 13 .0 4 .00 0 .000 8,110 8 .00

WP

- 03

- SL

- 065 21.1 0.3 00 27.8 1.1 0 13,800 30 .0 2 .00 0 .000 431 8.8 0 16,300 10 .0

WP

- 04

- SL

- 001 6.4 0 0.2 00 1.9 0 0.5 00 13,300 30 .0 2 .00 0 .000 90 .0 6.5 0 1,670 3 .00

WP

- 04

- SL

- 002 3.1 0 0.2 00 1.6 0 0.4 00 9,920 23 .0 2 .00 6.4 0 67 .0 6.4 0 1,350 3 .00

WP

- 04

- SL

- 003 3.5 0 0.2 00 0.1 00 0.1 00 8,880 22 .0 2 .00 0 .000 49.7 6.5 0 1,340 3 .00

WP

- 04

- SL

- 004 3 .00 0.2 00 0.7 00 0.2 00 35,200 50 .0 2 .00 0 .000 65.5 5.9 0 3,150 5 .00

WP

- 04

- SL

- 005 4 .00 0.2 00 2.9 0 0.6 00 14,500 30 .0 2 .00 0 .000 99.4 6.5 0 1,980 4 .00

WP

- 04

- SL

- 006 4 .00 0.2 00 3.8 0 0.6 00 6,220 20 .0 149 10 .0 82.4 6.9 0 2,190 4 .00

WP

- 04

- SL

- 007 3.5 0 0.2 00 0.1 00 0.1 00 59,600 60 .0 2 .00 0 .000 4 .00 0 .000 1,600 3 .00

WP

- 04

- SL

- 008 3 .00 0.2 00 0.6 00 0.2 00 18,800 30 .0 2 .00 0 .000 4 .00 0 .000 1,410 3 .00

WP

- 04

- SL

- 009 8.3 0 0.3 00 49.5 1.4 0 12,600 30 .0 2 .00 0 .000 472 10 .0 19,600 10 .0

WP

- 04

- SL

- 010 8.3 0 0.3 00 44.4 1.5 0 31,700 50 .0 2 .00 0 .000 442 10 .0 26,300 20 .0

WP

- 04

- SL

- 011 5.9 0 0.3 00 31.3 1.2 0 52,800 60 .0 2 .00 0 .000 353 8.3 0 12,300 10 .0

WP

- 04

- SL

- 012 9.3 0 0.3 00 41.1 1.3 0 24,100 40 .0 2 .00 0 .000 409 9.4 0 19,600 20 .0

WP

- 05

- SL

- 027 36.2 0.3 00 18.2 1.1 0 56,000 60 .0 2 .00 0 .000 231 8.2 0 12,900 10 .0

WP

- 05

- SL

- 028 43.2 0.3 00 4.7 0 0.8 00 46,100 60 .0 2 .00 0 .000 110 7.1 0 20,200 20 .0

WP

- 05

- SL

- 029 18.9 0.3 00 27.1 1.2 0 12,200 40 .0 2 .00 0 .000 227 8.5 0 59,800 40 .0

WP

- 05

- SL

- 030 17.9 0.3 00 25.9 1.1 0 16,500 30 .0 2 .00 0 .000 318 8.5 0 27,300 20 .0

WP

- 05

- SL

- 031 11.6 0.2 00 5.2 0 0.8 00 16,800 40 .0 2 .00 0 .000 122 7.3 0 19,900 20 .0

WP

- 05

- SL

- 032 11.7 0.3 00 19.6 1.1 0 85,500 80 .0 2 .00 0 .000 283 8.5 0 28,600 20 .0

WP

- 05

- SL

- 033 9.5 0 0.2 00 11.5 1 .00 107,000 100 2 .00 0 .000 197 7.7 0 19,400 20 .0

WP

- 05

- SL

- 034 23.2 0.3 00 11.3 1 .00 46,800 50 .0 2 .00 0 .000 192 7.9 0 17,800 10 .0

WP

- 06

- SL

- 014 8.5 0 0.2 00 5.7 0 0.8 00 10,500 20

. 2 .00 0 .000 55.1 7.1 0 1,560 3 .00

WP

- 06

- SL

- 015 8.4 0 0.2 00 9 .00 0.9 00 8,390 21 .0 2 .00 0 .000 4 .00 0 .000 2,400 4 .00

WP

- 06

- SL

- 016 12.8 0.2 00 1.3 0 0.3 00 15,100 30 .0 23.2 5.3 0 4 .00 0 .000 1,320 3 .00

WP

- 06

- SL

- 017 11.2 0.2 00 6.7 0 0.8 00 19,500 30 .0 40.2 7.5 0 4 .00 0 .000 1,170 3 .00

WP

- 06

- SL

- 018 434 1 .00 2 .00 0 .000 98,400 100 166 16 .0 4 .00 0 .000 149,000 100

WP

- 06

- SL

- 019 559 1.2 0 0.1 0 0.1 00 110,000 100 2 .00 0 .000 4 .00 0 .000 98,800 60 .0January 2015

F

- 4 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Solids Analysis

Study ID Bromine

Result (ppm) Bromine

Error (ppm) Cadmium

Result (ppm) Cadmium

Error (ppm) Calcium

Result (ppm) Calcium

Error (ppm) Cerium

Result (ppm) Cerium

Error (ppm) Cesium

Result (ppm) Cesium

Error (ppm) Chlorine

Result (ppm) Chlorine

Error (ppm)

WP

- 06

- SL

- 020 622 1.2 0 2.5 0 0.5 00 173,000 100 87 .0 10 .0 4 .00 0 .000 27,600 20 .0

WP

- 06

- SL

- 021 537 1.1 0 0.3 00 0.1 00 73,300 100 190 20 .0 94 .0 11 .0 91,900 60 .0

WP

- 06

- SL

- 022 534 1.1 0 2 .00 0 .000 159,000 100 93 .0 11 .0 70.3 7.8 0 24,300 20 .0

WP

- 06

- SL

- 023 165 0.6 00 2 .00 0 .000 201,000 100 2 .00 0 .000 37.1 6.2 0 23,700 20 .0

WP

- 06

- SL

- 024 1,220 2 .00 2 .00 0 .000 90,900 90 .0 169 14 .0 105 9.1 0 165,000 100

WP

- 06

- SL

- 025 712 1.3 0 2 .00 0 .000 194,000 100 123 12 .0 75.4 8 .00 27,900 20 .0

WP

- 06

- SL

- 026 1,530 2 .00 2 .00 0 .000 80,600 100 2 .00 0 .000 4 .00 0 .000 153,000 100

WP

- 06

- SL

- 037 45.8 0.6 00 45.8 1.8 0 48,800 60 .0 2 .00 0 .000 350 11 .0 127,000 100

WP

- 07

- SL

- 039 8.3 0 0.2 00 2 .00 0 .000 6,620 21 .0 94 .0 10 .0 4 .00 0 .000 574 1.9 0

WP

- 07

- SL

- 040 5.4 0 0.2 00 1 .00 0.3 00 12,400 30 .0 2 .00 0 .000 4 .00 0 .000 583 1.9 0

WP

- 07

- SL

- 041 6.1 0 0.2 00 1.6 0 0.4 00 14,200 30 .0 2 .00 0 .000 4 .00 0 .000 468 1.7

WP

- 10

- SL

- 045 15.1 0.3 00 0.1 00 0.1 00 137,000 100 96.4 9.9 0 71.2 7.5 0 1,360 2 .00

WP

- 10

- SL

- 048 125 0.7 00 28.4 1.2 0 50,700 50 .0 2 .00 0 .000 241 7.9 0 10,700 10 .0

WP

- 11

- SL

- 047 143 0.6 00 9.2 0 1.1 0 107,000 100 2 .00 0 .000 137 8.5 0 197,000 100

WP

- 11

- SL

- 068 23.1 0.4 00 40.7 1.4 0 184,000 100 2 .00 0 .000 467 9.7 0 6,920 6 .00

WP

- 12

- SL

- 052 178 0.7 00 43.9 1.5 0 41,200 50 .0 2 .00 0 .000 624 11 .0 21,800 20 .0

WP

- 12

- SL

- 053 144 0.6 00 2.8 0 0.6 00 14,200 30 .0 2 .00 0 .000 124 7.5 0 12,100 10 .0

WP

- 12

- SL

- 055 13 .0 0.5 00 101 2.7 0 19,500 40 .0 2 .00 0 .000 954 19 .0 9,470 9 .00

WP

- 12

- SL

- 056 53.8 0.8 00 108 3.3 0 52,800 80 .0 2 .00 0 .000 822 20 .0 21,100 20 .0

WP

- 13

- SL

- 059 9.9 0 0.2 00 6.6 0 0.8 00 62,300 60 .0 2 .00 0 .000 4 .00 0 .000 1,200 2 .00

WP

- 13

- SL

- 062 81.8 0.5 00 37.4 1.2 0 95,500 80 .0 2 .00 0 .000 383 8.6 0 9,910 10 .0

WP

- 14

- SL

- 073 44.6 0.3 00 8.1 0 0.9 00 31,300 40 .0 79 .0 10 .0 19.8 6.2 0 2,280 3 .00

WP

- 14

- SL

- 074 17.6 0.3 00 3.4 0 0.6 00 16,400 30 .0 138 11 .0 4 .00 0 .000 2,820 4 .00

WP

- 14

- SL

- 077 128 0.6 00 35.8 1.3 0 51,300 50 .0 2 .00 0 .000 473 9.8 0 3,670 4 .00

WP

- 14

- SL

- 078 125 0.6 00 32.1 1.2 0 26,200 30 .0 2 .00 0 .000 412 9.2 0 6,090 5 .00

WP

- 14

- SL

- 079 144 0.7 00 56.9 1.4 0 22,700 30 .0 2 .00 0 .000 545 11 .0 3,650 4 .00

WP

- 15

- SL

- 075 18.9 0.3 00 27.1 1.2 0 12,200 40 .0 2 .00 0 .000 227 8.5 0 59,800 40 .0January 2015

F

- 5 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Solids Analysis

Study ID Chromium

Result (ppm) Chromium

Error (ppm) Cobalt

Result (ppm) Cobalt

Error (ppm) Copper

Result (ppm) Copper

Error (ppm) Gallium

Result (ppm) Gallium

Error (ppm) Germanium

Result (ppm) Germanium

Error (ppm)

BR

- 30

- SL

- 029 62.7 1.1 0 9.1 0 1.5 0 467 1.9 0 14.2 0.5 0 2 .00 0.3 00

WP

- 02

- SL

- 036 69.3 1.6 0 36.9 4.9 0 120 1.2 0 20 .0 0.6 0 0.2 0 0.2 00

WP

- 03

- SL

- 038 81.4 1.1 0 33.3 3.8 0 32.1 0.8 00 26.5 0.6 0 1 .00 0.3 00

WP

- 03

- SL

- 065 101 2.5 0 40.3 6 .00 91.7 1.1 0 27.4 0.6 0 1.2 0 0.3 00

WP

- 04

- SL

- 001 149 1.9 0 23.5 3.7 0 44.8 1 .00 26.4 0.5 0 1.4 0 0.3 00

WP

- 04

- SL

- 002 174 1.6 0 27.5 3.5 0 39.6 0.8 0 24.6 0.5 0 1.5 0 0.3 00

WP

- 04

- SL

- 003 147 1.5 0 31.1 3.6 0 36.5 0.8 0 26.1 0.5 0 1.8 0 0.3 00

WP

- 04

- SL

- 004 603 2.8 0 31.6 3.7 0 44 .0 0.9 0 23 .0 0.5 0 0.5 00 0 .000

WP

- 04

- SL

- 005 195 1.9 0 27.3 3.5 0 37.5 0.8 0 25.1 0.5 0 2.4 0 0.3 00

WP

- 04

- SL

- 006 165 1.5 0 29.9 3.6 0 35.1 0.8 0 28.3 0.5 0 2 .00 0.3 00

WP

- 04

- SL

- 007 198 1.6 0 32.4 3.7 0 35.2 0.8 0 24.6 0.5 0 1.8 0 0.3 00

WP

- 04

- SL

- 008 175 1.6 0 28.7 3.6 0 51.9 0.8 0 27.1 0.5 0 2.3 0 0.3 00

WP

- 04

- SL

- 009 181 3.5 0 23.9 4.3 0 49 .0 1.1 0 18.1 0.6 0 0.5 00 0 .000

WP

- 04

- SL

- 010 210 4.8 0 14 .0 4.3 0 50.6 1.2 0 18.5 0.7 0 0.7 00 0.7 00

WP

- 04

- SL

- 011 189 3.4 0 28.4 3.9 0 59.4 1 .00 22.8 0.6 0 0.1 00 0.1 00

WP

- 04

- SL

- 012 93.2 3.5 0 34.4 4.9 0 67.7 1.1 0 21.4 0.6 0 0.7 00 0.3 00

WP

- 05

- SL

- 027 117 2.5 0 24.9 4 .00 83.6 1.2 0 17.9 0.5 0 0.7 00 0.3 00

WP

- 05

- SL

- 028 161 2.7 0 42.3 4.7 0 61.3 1.1 0 26.7 0.5 0 1.2 0 0.3 00

WP

- 05

- SL

- 029 139 2.1 0 3.9 0 0 .000 38.2 1 .00 20.2 0.5 0 1.7 0 0.3 00

WP

- 05

- SL

- 030 106 3.1 0 28.8 4 .00 51.4 1.1 0 20.1 0.5 0 0.8 00 0.3 00

WP

- 05

- SL

- 031 134 2.1 0 23.9 3.6 0 51 .0 1 .00 22 .0 0.5 0 1.1 0 0.3 00

WP

- 05

- SL

- 032 120 2.9 0 29.7 4.2 0 64.8 1.1 0 15.7 0.5 0 0.9 00 0.3 00

WP

- 05

- SL

- 033 176 3.4 0 38.1 4.5 0 54.8 1.1 0 18.1 0.5 0 1.2 0 0.3 00

WP

- 05

- SL

- 034 118 2.2 0 39.5 4.8 0 72.5 1.00 21.9 0.6 0 1.5 0 0.3 00

WP

- 06

- SL

- 014 94.1 1.3 0 21.9 3.1 0 37.8 0.8 00 23.4 0.5 0 1.7 0 0.2 00

WP

- 06

- SL

- 015 66.2 1.2 0 26.3 3.4 0 36.3 0.8 00 26.3 0.5 00 2.2 0 0.3 00

WP

- 06

- SL

- 016 110 1.3 0 42.8 4.4 0 64.9 0.8 00 27.1 0.5 00 1.5 0 0.2 00

WP

- 06

- SL

- 017 107 1.2 0 23.2 3.4 0 45.6 0.8 00 26.4 0.5 00 1.7 0 0.2 00

WP

- 06

- SL

- 018 7,210 1.2 0 3 .00 0 .000 9.6 0 0.7 00 5.6 0 0.5 00 0.5 00 0 .000

WP

- 06

- SL

- 019 7,210 1.3 0 3 .00 0 .000 12.9 0.8 00 8.5 0 0.5 00 0.7 00 0.3 00January 2015

F

- 6 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Solids Analysis

Study ID Chromium

Result (ppm) Chromium

Error (ppm) Cobalt

Result (ppm) Cobalt

Error (ppm) Copper

Result (ppm) Copper

Error (ppm) Gallium

Result (ppm) Gallium

Error (ppm) Germanium

Result (ppm) Germanium

Error (ppm)

WP

- 06

- SL

- 020 60.9 1.1 0 3 .00 0 .000 21.8 0.8 00 7.9 0 0.5 00 0.5 00 0 .000

WP

- 06

- SL

- 021 25.9 0.8 00 3.9 0 0 .00 16.9 0.9 00 7.8 0 0.5 00 0.5 00 0 .000

WP

- 06

- SL

- 022 119 1.8 0 17.2 3.2 0 46.2 1.1 0 19.6 0.5 00 0.5 00 0 .000

WP

- 06

- SL

- 023 83.3 1.5 0 3.9 0 0 .000 26.3 0.8 00 9.1 0 0.4 00 0.1 00 0.1 00

WP

- 06

- SL

- 024 41.5 1 .00 3.9 0 0 .000 14.5 0.8 00 9.4 0 0.4 00 0.5 00 0 .000

WP

- 06

- SL

- 025 110 1.8 0 23.1 3.8 0 46.4 1 .00 17.1 0.5 00 0.6 00 0.3 00

WP

- 06

- SL

- 026 65.8 1.4 0 15 .0 7 .00 49.4 1.3 0 13.2 0.6 00 0.5 00 0 .000

WP

- 06

- SL

- 037 61.9 3.7 0 3 .00 0 .000 42.9 1.6 0 1.3 0 0.7 00 0.7 00 0.7 00

WP

- 07

- SL

- 039 96.9 1.2 0 30 .0 3.5 0 30.2 0.8 00 26.8 0.5 00 1.8 0 0.3 00

WP

- 07

- SL

- 040 90.1 1.1 0 30.6 3.5 0 24.9 0.7 00 25.5 0.5 00 1.8 0 0.3 00

WP

- 07

- SL

- 041 94.7 1.1 0 25.7 3.2 0 29.1 0.8 00 24.1 0.5 00 1 .00 0.3 00

WP

- 10

- SL

- 045 96.5 1.4 0 15.4 2.8 0 33.2 0.8 00 17.5 0.5 00 0.5 00 0 .000

WP

- 10

- SL

- 048 89.4 2.8 0 41.6 6.5 0 84.1 1.3 0 15.1 0.9 00 0.7 00 0.7 00

WP

- 11

- SL

- 047 20.8 1.1 0 3 .00 0 .000 23.2 0.8 00 7.3 0 0.5 00 0.5 00 0 .000

WP

- 11

- SL

- 068 107 3.8 0 3 .00 0 .000 3,810 1.2 0 14.6 0.6 00 0.5 00 0 .000

WP

- 12

- SL

- 052 100 3 .00 16.1 3.2 0 79.8 1.2 0 24.5 0.8 00 1.4 0 0.3 00

WP

- 12

- SL

- 053 98 .0 1.4 0 39.8 4.2 0 56.7 0.9 00 24.4 0.5 00 1.3 0 0.3 00

WP

- 12

- SL

- 055 281 6.5 0 3 .00 0 .000 51.4 1.7 0 13 .0 1 .00 0.5 00 0 .000

WP

- 12

- SL

- 056 440 11 .0 3 .00 0 .000 145 2.5 0 38 .0 1.5 00 1.5 0 1.5 0

WP

- 13

- SL

- 059 131 1.3 0 30 .0 3.5 0 34.1 0.8 00 23.6 0.5 00 1.1 0 0.3 00

WP

- 13

- SL

- 062 91.7 2.6 0 13.9 3.8 0 103 1.3 0 16.1 0.6 00 0.4 00 0.4 00

WP

- 14

- SL

- 073 69.4 1 .00 34.6 3.6 0 54.6 0.8 0 25.1 0.5 00 1.8 0 0.3 00

WP

- 14

- SL

- 074 101 1.3 0 19.1 2.8 0 36 .0 0.8 0 23.1 0.5 00 1.9 0 0.2 00

WP

- 14

- SL

- 077 121 2.4 0 18.5 3.8 0 92.2 1.1 0 20.3 0.6 00 0.4 00 0.4 00

WP

- 14

- SL

- 078 93 .0 1.9 0 24.6 4.5 0 94.5 1.1 0 20.8 0.6 00 0.6 00 0.6 00

WP

- 14

- SL

- 079 84.5 2.2 0 23.5 4.8 0 103 1.4 0 16.5 0.7 00 0.5 00 0.5 00

WP

- 15

- SL

- 075 139 2.1 0 3.9 0 0 .000 38.2 1 .00 20.2 0.5 00 1.7 0 0.3 00January 2015

F

- 7 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Solids Analysis

Study ID Hafnium

Result (ppm) Hafnium

Error (ppm) Iodine

Result (ppm) Iodine

Error (ppm) Iron

Result (ppm) Iron

Error (ppm) Lanthanum

Result (ppm) Lanthanum

Error (ppm) Lead

Result (ppm) Lead

Error (ppm)

BR

- 30

- SL

- 029 9.6 0 1 .00 470 2.7 0 47,900 40 .0 105 8.2 71.8 0.7 00

WP

- 02

- SL

- 036 5.8 0 0.8 00 3 .00 0 .000 36,300 30 .0 254 11 55 0.9 00

WP

- 03

- SL

- 038 8.4 0 0.7 00 3 .00 0 .000 52,700 40 .0 2 .00 0 .000 26.1 0.7 00

WP

- 03

- SL

- 065 3.1 0 0.5 00 3 .00 0 .000 37,000 30 .0 451 11 .0 108 1.2 0

WP

- 04

- SL

- 001 7.6 0 0.7 00 3 .00 0 .000 72,600 60 .0 201 11 .0 33.2 0.7 00

WP

- 04

- SL

- 002 9 .00 0.8 00 3 .00 0 .000 48,000 40 .0 2 .00 0 .000 24.1 0.6 00

WP

- 04

- SL

- 003 11.2 0.8 00 3 .00 0 .000 52,100 40 .0 101 9.1 0 25.1 0.6 00

WP

- 04

- SL

- 004 10.8 0.9 00 3 .00 0 .000 49,500 40 .0 148 8.7 0 23.1 0.7 00

WP

- 04

- SL

- 005 10.1 0.8 00 3 .00 0 .000 52,000 40 .0 2 .00 0 .000 22.2 0.7 00

WP

- 04

- SL

- 006 8.2 0 0.7 00 3 .00 0 .000 54,900 40 .0 184 11 .0 27 0.7 00

WP

- 04

- SL

- 007 6.3 0 0.7 00 3 .00 0 .000 44,800 40 .0 2 .00 0 .000 23.6 0.6 00

WP

- 04

- SL

- 008 7.6 0 0.7 00 3 .00 0 .000 49,600 40 .0 2 .00 0 .000 27.8 0.7 00

WP

- 04

- SL

- 009 4.7 0 0.7 00 3 .00 0 .000 29,400 30 .0 2 .00 0 .000 27.4 0.8 00

WP

- 04

- SL

- 010 6.2 0 0.9 00 3 .00 0 .000 29,100 30 .0 2 .00 0 .000 28.5 0.9 00

WP

- 04

- SL

- 011 8.1 0 0.9 00 3 .00 0 .000 35,000 30 .0 257 7.3 0 30.4 0.7 00

WP

- 04

- SL

- 012 7.1 0 0.9 00 3 .00 0 .000 32,800 30 .0 272 8 .00 27.6 0.9 00

WP

- 05

- SL

- 027 12 .0 1 .00 3 .00 0 .000 51,500 50 .0 405 13 .0 116 1 .00

WP

- 05

- SL

- 028 4.2 0 0.6 00 3 .00 0 .000 62,300 50 .0 2 .00 0 .000 41 .0 0.8 00

WP

- 05

- SL

- 029 1.8 0 0.7 00 4.3 0 0.2 00 52,000 50 .0 459 15 .0 24 .0 0.6 00

WP

- 05

- SL

- 030 9.7 0 0.9 00 3 .00 0 .000 54,200 50 .0 543 13 .0 32 .0 0.7 00

WP

- 05

- SL

- 031 8.8 0 0.8 00 3 .00 0 .000 63,300 50 .0 202 11 .0 33.2 0.8 00

WP

- 05

- SL

- 032 3.2 0 0.5 00 3 .00 0 .000 37,600 40 .0 246 9.8 0 181 1.1 0

WP

- 05

- SL

- 033 6.8 0 0.8 00 3 .00 0 .000 42,800 40 .0 2 .00 0 .000 49.5 0.8 00

WP

- 05

- SL

- 034 9.9 0 0.9 00 3 .00 0 .000 39,200 30 .0 2 .00 0 .000 145 1 .00

WP

- 06

- SL

- 014 7.5 0 0.7 00 3 .00 0 .000 46,100 40 .0 125 11 .0 27.8 0.7 00

WP

- 06

- SL

- 015 8.7 0 0.8 0 3 .00 0 .000 50,600 40 .0 2 .00 0 .000 27.7 0.8 00

WP

- 06

- SL

- 016 7 .00 0.7 0 3 .00 0 .000 41,000 30 .0 2 .00 0 .000 27.5 0.6 00

WP

- 06

- SL

- 017 9 .00 0.8 0 3 .00 0 .000 47,000 40 .0 30.2 5.8 0 35.8 0.7 00

WP

- 06

- SL

- 018 2 .00 0 .000 4.8 0 0.7 00 8,370 16 .0 2 .00 0 .000 10.3 0.4 00

WP

- 06

- SL

- 019 2 .00 1.2 0 3 .00 0 .000 12,000 20 .0 2 .00 0 .000 11.4 0.5 00January 2015

F

- 8 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Solids Analysis

Study ID Hafnium

Result (ppm) Hafnium

Error (ppm) Iodine

Result (ppm) Iodine

Error (ppm) Iron

Result (ppm) Iron

Error (ppm) Lanthanum

Result (ppm) Lanthanum

Error (ppm) Lead

Result (ppm) Lead

Error (ppm)

WP

- 06

- SL

- 020 1 .00 0 .000 3 .00 0 .000 16,500 20 .0 2 .00 0 .000 17.1 0.5 00

WP

- 06

- SL

- 021 2 .00 1 .00 15.6 2.1 0 19,500 30 .0 2 .00 0 .000 11.7 0.5 00

WP

- 06

- SL

- 022 5.1 0 0.7 00 5.1 0 0.7 00 51,100 50 .0 129 11 .0 22.4 0.7 00

WP

- 06

- SL

- 023 3 .00 0.5 00 3 .00 0 .000 25,800 30 .0 2 .00 0 .000 9.9 0 0.4 00

WP

- 06

- SL

- 024 1.7 0 0 .000 20.5 2 .00 23,700 30 .0 203 15 .0 12.7 0 .000

WP

- 06

- SL

- 025 4.1 0 0.6 00 9.5 0 1.1 0 45,400 40 .0 139 12 .0 20.7 0.7 00

WP

- 06

- SL

- 026 2.6 0 0.5 00 3 .00 0 .000 35,200 40 .0 2 .00 0 .000 14.9 0.5 00

WP

- 06

- SL

- 037 1 .00 0 .000 3 .00 0 .000 18,600 30 .0 2 .00 0 .000 1,310 4 .00

WP

- 07

- SL

- 039 11.4 0.8 00 0.7 00 0.2 00 54,700 40 .0 2 .00 0 .000 20.5 0.7 00

WP

- 07

- SL

- 040 7.5 0 0.7 00 3 .00 0 .000 50,600 40 .0 2 .00 0 .000 29 .0 0.7 00

WP

- 07

- SL

- 041 11.8 0.8 00 8.1 0 0.9 00 50,900 40 .0 2 .00 0 .000 26.5 0.7 00

WP

- 10

- SL

- 045 4.6 0 0.5 00 3 .00 0 .000 34,800 30 .0 136 11 .0 29 .0 0.6 00

WP

- 10

- SL

- 048 7.9 0 1.2 0 3 .00 0 .000 33,200 40 .0 187 6.8 0 536 2.1 0

WP

- 11

- SL

- 047 1 .00 0 .000 3 .00 0 .000 11,000 20 .0 241 14 .0 16 .0 0.5 00

WP

- 11

- SL

- 068 1 .00 0 .000 3 .00 0 .000 12,900 20 .0 323 8.4 0 44.3 0.8 00

WP

- 12

- SL

- 052 3.3 0 0.6 00 3 .00 0 .000 40,200 40 .0 720 17 .0 65.1 1 .00

WP

- 12

- SL

- 053 7.6 0 0.8 00 3 .00 0 .000 46,900 40 .0 220 12 .0 24.9 0.7 00

WP

- 12

- SL

- 055 1 .00 0 .000 3 .00 0 .000 25,600 40 .0 2 .00 0 .000 144 1.6 0

WP

- 12

- SL

- 056 1 .00 0 .000 3 .00 0 .000 52,600 60 .0 2 .00 0 .000 289 2.7 0

WP

- 13

- SL

- 059 4.4 0 0.5 00 3 .00 0 .000 47,500 40 .0 2 .00 0 .000 28.7 0.7 00

WP

- 13

- SL

- 062 2.4 0 0.5 00 3 .00 0 .000 37,800 40 .0 423 12 .0 169 1.4 0

WP

- 14

- SL

- 073 8 .00 0.8 00 3 .00 0 .000 46,200 40 .0 41.5 6.4 0 37.1 0.7 0

WP

- 14

- SL

- 074 7.1 0 0.7 00 3 .00 0 .000 49,300 40 .0 2 .00 0 .00 17.6 0.7 0

WP

- 14

- SL

- 077 6.5 0 0.9 00 3 .00 0 .000 28,400 30 .0 430 12 .0 98.5 1.2 0

WP

- 14

- SL

- 078 8 .00 1 .00 3 .00 0 .000 30,000 30 .0 704 14 .0 98.6 1.1 0

WP

- 14

- SL

- 079 3.4 0 0.7 00 3 .00 0 .000 27,500 30 .0 392 9.8 0 142 1.4 0

WP

- 15

- SL

- 075 1.8 0 0.7 00 4.3 0 0.2 00 52,000 50 .0 459 15 .0 24 .0 0.6 00January 2015

F

- 9 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Solids Analysis

Study ID Magnesium

Result (ppm) Magnesium

Error (ppm) Manganese

Result (ppm) Manganese

Error (ppm) Mercury

Result (ppm) Mercury

Error (ppm) Molybdenum

Result (ppm) Molybdenum

Error (ppm) Nickel

Result (ppm) Nickel

Error (ppm)

BR

- 30

- SL

- 029 14,400 120 630 2.1 0 #N/A #N/A #N/A #N/A 53.6 0.9 00

WP

- 02

- SL

- 036 22,900 170 176 1.7 0 5.9 0 0.3 00 169 1.5 0 206 1.5 0

WP

- 03

- SL

- 038 24,100 170 399 1.8 0 1.9 0 0.3 00 5.7 0.6 00 74.9 1 .00

WP

- 03

- SL

- 065 16,500 150 217 2.6 0 2.2 0 0.4 00 125 1.6 0 248 1.9 0

WP

- 04

- SL

- 001 26,100 250 846 30 .0 0.6 00 0.2 00 2.5 0 0.5 00 70.2 1.2 0

WP

- 04

- SL

- 002 20,400 140 592 2.3 0 1.6 0 0.3 00 2.2 0 0.5 00 67.6 0.9 00

WP

- 04

- SL

- 003 21,100 140 600 2.2 0 0.2 00 0 .000 1.9 0 0.4 00 66.3 1 .00

WP

- 04

- SL

- 004 21,800 160 603 2.8 0 2.5 0 0.3 00 2.7 0 0.5 00 58.3 1.00

WP

- 04

- SL

- 005 21,900 160 616 2.5 0 0.3 00 0.3 00 1 .00 0 .000 61.7 1.00

WP

- 04

- SL

- 006 20,600 140 627 2.2 0 0.4 00 0.2 00 3.2 0 0.5 00 63.3 1.00

WP

- 04

- SL

- 007 22,200 140 569 2.3 0 0.7 00 0.2 00 3.4 0 0.5 00 71 .0 1.00

WP

- 04

- SL

- 008 21,100 140 491 2.1 0 1 .00 0 .000 12.7 0.7 00 81.4 1.00

WP

- 04

- SL

- 009 11,900 140 1 .00 0 .000 2.5 0 0.4 00 42.3 1.5 0 151 1.6 0

WP

- 04

- SL

- 010 20,300 230 1 .00 0 .000 2.5 0 0.5 00 44.9 1.6 0 116 1.6 0

WP

- 04

- SL

- 011 18,700 150 337 3.5 0 4.6 0 0.4 00 17.8 1 .00 70.7 1.2 0

WP

- 04

- SL

- 012 16,400 180 183 3.6 0 2.1 0 0.4 00 76.7 1.5 0 113 1.4 0

WP

- 05

- SL

- 027 32,600 260 374 2.7 0 2.5 0 0.3 00 22 .0 0.9 00 91.5 1.3 0

WP

- 05

- SL

- 028 36,300 290 606 3.1 0 2 .00 0.3 00 3.9 0 0.6 00 60.9 1.2 0

WP

- 05

- SL

- 029 48,500 540 596 2.9 0 1 .00 0 .000 5.2 0 0.6 00 45.8 1.1 0

WP

- 05

- SL

- 030 26,100 270 490 3.3 0 2.2 0 0.3 00 3.4 0 0.7 00 56 .0 1.1 0

WP

- 05

- SL

- 031 29,700 270 607 2.7 0 0.7 00 0.2 00 4 .00 0.6 00 61.1 1.1 0

WP

- 05

- SL

- 032 29,600 300 485 3.2 0 1.7 0 0.3 00 5.6 0 0.7 00 58 .0 1.1 0

WP

- 05

- SL

- 033 31,300 290 586 3.7 0 1.7 0 0.3 00 4.5 0 0.6 00 44.7 1 .00

WP

- 05

- SL

- 034 25,200 190 371 2.6 0 0.9 00 0.3 00 23.1 0.9 00 122 1.3 0

WP

- 06

- SL

- 014 19,700 140 370 1.8 0 0.6 00 0.2 00 16.1 0.7 00 61.2 0.9 00

WP

- 06

- SL

- 015 21,800 150 244 1.6 0 1 .00 0 .000 6.4 0 0.6 00 54.9 0.9 00

WP

- 06

- SL

- 016 21,500 150 302 1.6 0 1 .00 0.3 00 12.8 0.6 00 112 1.1 0

WP

- 06

- SL

- 017 22,400 140 463 1.9 0 1 .00 0.3 00 11.6 0.6 00 87.4 1.1 0

WP

- 06

- SL

- 018 128,000 800 64.8 1.2 0 1 .00 0 .000 3 .00 0.4 00 25.2 0.8 00

WP

- 06

- SL

- 019 138,000 700 107 1.5 0 1 .00 0 .000 5.3 0 0.6 00 32.8 0.9 00January 2015

F

- 10 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Solids Analysis

Study ID Magnesium

Result (ppm) Magnesium

Error (ppm) Manganese

Result (ppm) Manganese

Error (ppm) Mercury

Result (ppm) Mercury

Error (ppm) Molybdenum

Result (ppm) Molybdenum

Error (ppm) Nickel

Result (ppm) Nickel

Error (ppm)

WP

- 06

- SL

- 020 76,100 310 160 1.5 0 1.1 0 0.2 00 8.2 0 0.5 00 73 .0 1.1 00

WP

- 06

- SL

- 021 109,000 900 447 2.6 0 0.8 00 0.2 00 2.6 0 0.4 00 95 .0 1.4 00

WP

- 06

- SL

- 022 41,600 300 539 2.7 0 2 .00 0.3 00 8 .00 0.6 00 65.5 1.2 0

WP

- 06

- SL

- 023 40,200 270 328 2.1 0 1 .00 0 .000 2.9 0 0.4 00 37.3 0.9 00

WP

- 06

- SL

- 024 128,000 1,100 150 1.5 0 1 .00 0 .000 7 .00 0.6 00 24.3 0.9 00

WP

- 06

- SL

- 025 39,800 300 418 2.4 0 0.8 00 0.2 0 10.6 0.6 00 62.1 1.2 0

WP

- 06

- SL

- 026 140,000 1,200 278 2.3 0 2.2 0 0.4 0 7.1 0 0.7 00 126 1.7 0

WP

- 06

- SL

- 037 40,600 540 266 4.2 0 9.7 0 0.9 0 7.9 0 1.2 0 38.7 1.5 0

WP

- 07

- SL

- 039 22,100 150 605 2.2 0 0.8 00 0.3 0 3.6 0 0.6 00 54.1 0.9 00

WP

- 07

- SL

- 040 21,100 150 574 2.1 0 1 .00 0 .000 1 .00 0 .000 47 .0 0.9 00

WP

- 07

- SL

- 041 20,400 140 612 2.2 0 1 .00 0 .000 1 .00 0 .000 51.4 0.9 00

WP

- 10

- SL

- 045 104,000 200 453 2.2 0 1.5 0 0.3 00 8.4 0 0.6 00 72.2 1.1 0

WP

- 10

- SL

- 048 21,600 160 399 3.2 0 6.6 0 0.5 00 55.2 1.3 0 105 1.5 0

WP

- 11

- SL

- 047 129,000 800 174 1.9 0 0.7 00 0.2 00 1.9 0 0.4 00 32.9 0.9 0

WP

- 11

- SL

- 068 13,800 110 315 4.2 0 2.2 0 0.3 00 4.6 0 0.9 00 87 .0 1.5 0

WP

- 12

- SL

- 052 45,900 230 825 4 .00 1.4 0 0.3 00 5 .00 0.9 00 115 1.5 0

WP

- 12

- SL

- 053 19,100 150 585 2.3 0 2.3 0 0.4 00 2.8 0 0.6 00 62.7 1 .00

WP

- 12

- SL

- 055 15,200 190 1 .00 0 .000 2.2 0 0.6 00 7.2 0 1.7 0 359 3.3 0

WP

- 12

- SL

- 056 21,900 260 1 .00 0 .000 5.7 0 1.1 0 84.5 3.4 0 221 3.3 0

WP

- 13

- SL

- 059 17,400 130 499 2 .00 1.7 0 0.3 00 8.4 0 0.6 00 58.4 0.9 00

WP

- 13

- SL

- 062 27,000 230 447 3.3 0 2 .00 0.4 00 107 1.5 0. 292 2.1 0

WP

- 14

- SL

- 073 11,900 130 597 2.1 0 0.9 00 0.3 00 3 .00 0.5 00 53.8 0.9 00

WP

- 14

- SL

- 074 22,200 160 748 2.5 0 0.4 00 0.2 00

00 1 .00 0 .000 52.1 0.9 00

WP

- 14

- SL

- 077 5,170 80 .0 253 2.6 0 2.8 0 0.4 00 88.3 1.4 0 200 1.4 0

WP

- 14

- SL

- 078 9,300 120 151 1.9 0 3.7 0 0.4 00 86.9 1.3 0 137 1.4 0

WP

- 14

- SL

- 079 6,060 90 .0 187 2.4 0 5.3 0 0.6 00 79.5 1.6 0 110 1.6 0

WP

- 15

- SL

- 075 48,500 540 596 2.9 0 1 .00 0 .000 5.2 0 0.6 00 45.8 1.1 0January 2015

F

- 11 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Solids Analysis

Study ID Niobium

Result (ppm) Niobium

Error (ppm) Phosphorus

Result (ppm) Phosphorus

Error (ppm) Potassium

Result (ppm) Potassium

Error (ppm) Rubidium

Result (ppm) Rubidium

Error (ppm) Selenium

Result (ppm) Selenium

Error (ppm)

BR

- 30

- SL

- 029 6.8 0 0.5 00 15,900 20 .0 11,900 20 .0 #N/A #N/A #N/A #N/A

WP

- 02

- SL

- 036 7.8 0 0.7 00 131 9.1 0 24,400 40 .0 124 0.4 00 11.3 0.3 00

WP

- 03

- SL

- 038 17.9 0.6 00 178 8.1 0 32,200 50 .0 194 0.5 00 0.5 00 0 .000

WP

- 03

- SL

- 065 8.7 0 0.9 00 3 .00 0 .000 29,100 50 .0 154 0.5 00 6.4 0 0.3 00

WP

- 04

- SL

- 001 25.3 0.9 00 723 17 .0 39,400 60 .0 175 0.5 00 0.5 00 0 .000

WP

- 04

- SL

- 002 15.8 0.6 00 436 7.1 0 28,800 40 .0 144 0.4 00 0.3 00 0.3 00

WP

- 04

- SL

- 003 15.8 0.6 00 452 7.1 0 29,700 50 .0 25.1 0.6 00 0.5 00 0 .000

WP

- 04

- SL

- 004 14.3 0.7 00 460 8.6 0 27,700 50 .0 128 0.4 00 0.4 00 0.4 00

WP

- 04

- SL

- 005 17.1 0.7 00 395 8 .00 30,000 50 .0 154 0.5 00 0.2 00 0.2 00

WP

- 04

- SL

- 006 17.1 0.6 00 263 7.4 0 33,000 50 .0 174 0.5 00 0.1 00 0.1 00

WP

- 04

- SL

- 007 14.2 0.6 00 194 7 .00 28,000 40 .0 160 0.4 00 0.4 00 0.4 00

WP

- 04

- SL

- 008 14.7 0.6 00 373 7.8 0 31,100 50 .0 170 0.5 00 1.5 0 0.2 00

WP

- 04

- SL

- 009 4.9 0 1.2 0 3 .00 0 .000 9,530 26 .0 86.1 0.4 00 3.6 0 0.3 00

WP

- 04

- SL

- 010 5.7 0 1.2 0 3 .00 0 .000 13,000 40 .0 85.7 0.4 00 4.5 0 0.3 00

WP

- 04

- SL

- 011 8 .00 0.9 00 3 .00 0 .000 20,800 40 .0 120 0.5 00 2.3 0 0.3 00

WP

- 04

- SL

- 012 9.4 0 1 .00 3 .00 0 .000 18,000 40 .0 118 0.5 00 6.3 0 0.3 00

WP

- 05

- SL

- 027 16.6 1 .00 6.9 0 0 .000 26,600 50 .0 147 0.5 00 1.9 0 0.2 00

WP

- 05

- SL

- 028 22.7 1 .00 400 22 .0 33,800 60 .0 174 0.5 00 0.7 00 0.2 00

WP

- 05

- SL

- 029 21.5 0.9 00 6.9 0 0 .000 32,400 60 .0 137 0.5 00 0.5 00 0 .00

WP

- 05

- SL

- 030 20.1 1.2 00 6.9 0 0 .000 19,900 40 .0 123 0.4 00 0.5 00 0 .00

WP

- 05

- SL

- 031 20.6 0.9 00 132 18 .0 31,400 50 .0 172 0.5 00 0.1 00 0.1 00

WP

- 05

- SL

- 032 10.7 1 .00 6.9 0 0 .000 18,800 40 .0 116 0.4 00 1.1 0 0.2 00

WP

- 05

- SL

- 033 14.8 1 .00 517 23 .0 21,300 40 .0 95.1 0.4 00 0.8 00 0.2 00

WP

- 05

- SL

- 034 12.2 0.7 00 67 .0 11 .0 29,100 50 .0 150 0.5 00 2.2 0 0.2 00

WP

- 06

- SL

- 014 17.8 0.6 00 93.3 7 .00 29,100 40 .0 160 0.4 00 0.3 00 0.3 00

WP

- 06

- SL

- 015 15.6 0.7 00 70.1 7.6 0 23,800 40 .0 183 0.5 00 0.3 00 0.3 00

WP

- 06

- SL

- 016 12.7 0.6 00 190 7.3 0 38,300 50 .0 170 0.4 00 2.2 0 0.2 00

WP

- 06

- SL

- 017 14.7 0.6 00 160 6.5 0 32,800 50 .0 169 0.4 00 0.5 00 0.2 00

WP

- 06

- SL

- 018 1 .00 0 .000 3 .00 0 .000 7,980 34 .0 14.9 0.4 00 0.3 00 0.3 00

WP

- 06

- SL

- 019 3 .00 0.6 00 3 .00 0 .000 12,400 40 .0 30.7 0.5 00 0.5 00 0 .000January 2015

F

- 12 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Solids Analysis

Study ID Niobium

Result (ppm) Niobium

Error (ppm) Phosphorus

Result (ppm) Phosphorus

Error (ppm) Potassium

Result (ppm) Potassium

Error (ppm) Rubidium

Result (ppm) Rubidium

Error (ppm) Selenium

Result (ppm) Selenium

Error (ppm)

WP

- 06

- SL

- 020 2.9 0 0.5 00 3 .00 0 .000 12,200 30 .0 46.6 0.5 00 0.9 00 0.2 00

WP

- 06

- SL

- 021 2.3 0 0.8 00 6.9 0 0.000 11,900 40 .0 20.9 0.5 00 0.7 00 0.2 00

WP

- 06

- SL

- 022 14.7 0.8 00 6.9 0 0.000 33,600 60 .0 136 0.6 00 0.7 00 0.2 00

WP

- 06

- SL

- 023 3.6 0 0.6 00 6.9 0 0.000 18,100 40 .0 42 .0 0.3 00 0.2 00 0.2 00

WP

- 06

- SL

- 024 10.1 0.7 00 6.9 0 0.000 17,300 40 .0 58.8 0.6 00 0.5 00 0 .000

WP

- 06

- SL

- 025 13.5 0.8 00 6.9 0 0.000 28,800 50 .0 123 0.6 00 0.7 00 0.2 00

WP

- 06

- SL

- 026 10.6 0.9 00 6.9 0 0.000 25,000 60 .0 81.4 0.8 00 0.4 00 0.4 00

WP

- 06

- SL

- 037 1 .00 0 .000 3 .00 0 .000 7,710 32 .0 52.5 0.6 00 6.4 0 0.5 00

WP

- 07

- SL

- 039 16.5 0.6 00 541 7.5 0 33,100 50 .0 159 0.5 00 0.5 00 0 .000

WP

- 07

- SL

- 040 17.6 0.6 00 366 7.1 0 32,700 50 .0 168 0.5 00 0.5 00 0 .000

WP

- 07

- SL

- 041 16.9 0.6 00 501 7 .00 30,500 50 .0 152 0.4 00 0.5 00 0 .000

WP

- 10

- SL

- 045 10.5 0.6 00 346 4.4 0 14,700 30 .0 110 0.4 00 0.5 00 0 .000

WP

- 10

- SL

- 048 3.2 0 0.9 00 149 9.3 0 17,300 40 .0 106 0.6 00 7.3 0 0.3 00

WP

- 11

- SL

- 047 1 .00 0 .000 3 .00 0 .000 19,300 50 .0 24.1 0.3 00 0.5 00 0 .000

WP

- 11

- SL

- 068 0.3 00 0.3 00 312 5.5 0 5,750 22 .0 32.5 0.3 00 2.5 0 0.3 00

WP

- 12

- SL

- 052 15.2 1 .00 188 11 .0 26,900 50 .0 115 0.5 00 1.1 0 0.3 00

WP

- 12

- SL

- 053 17 .0 0.7 00 334 8 .00 25,900 40 .0 141 0.5 00 0.5 00 0.2 00

WP

- 12

- SL

- 055 3 .00 3 .00 3 .00 0 .000 9,940 36 .0 58.7 0.5 00 1.7 0 0.5 00

WP

- 12

- SL

- 056 5.7 0 2.8 0 3 .00 0 .000 21,100 20 .0 171 1 .00 11.3 0.7 00

WP

- 13

- SL

- 059 17.6 0.6 00 267 5.7 0 23,500 40 .0 141 0.4 00 0.5 00 0.2 00

WP

- 13

- SL

- 062 4.2 0 0.8 00 529 12 .0 13,000 40 .0 61.9 0.4 00 8.9 0 0.3 00

WP

- 14

- SL

- 073 16.7 0.6 00 132 5 .00 21,400 40 .0 135 0.4 00 0.4 00 0.2 0

WP

- 14

- SL

- 074 15.8 0.6 00 485 7.7 0 32,500 50 .0 148 0.4 00 0.5 00 0 .000

WP

- 14

- SL

- 077 6 .00 0.8 00 3 .00 0 .000 14,500 30 .0 103 0.5 00 9.1 0 0.3 00

WP

- 14

- SL

- 078 6.3 0 0.8 00 3 .00 0 .000 11,700 30 .0 113 0.5 00 8.4 0 0.3 00

WP

- 14

- SL

- 079 5.5 0 1 .00 3 .00 0 .000 7,290 23 .0 88.3 0.5 00 9.7 0 0.3 00

WP

- 15

- SL

- 075 21.5 0.9 00 6.9 0 0 .000 32,400 60 .0 137 0.5 00 0.5 00 0 .000January 2015

F

- 13 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Solids Analysis

Study ID Silicon

Result (ppm) Silicon

Error (ppm) Silver

Result (ppm) Silver

Error (ppm) Sodium

Result (ppm) Sodium

Error (ppm) Strontium

Result (ppm) Strontium

Error (ppm) Sulfur

Result (ppm) Sulfur

Error (ppm) Tantulum

Result (ppm) Tantulum

Error (ppm)

BR

- 30

- SL

- 029 154,000 100 #N/A #N/A 0 .000 0 .000 #N/A #N/A 6,560 8 .00 33.7 3.8 0

WP

- 02

- SL

- 036 250,000 200 17.7 1.4 0 0.000 0.000 384 0.6 00 17,200 20 .0 77.2 2.7 0

WP

- 03

- SL

- 038 297,000 200 3.4 0 1.5 0 0.000 0.000 184 0.5 00 9,080 12 .0 1.6 0 0.2 00

WP

- 03

- SL

- 065 259,000 200 26.7 1.4 0 0.000 0.000 615 0.9 00 22,200 20 .0 16.8 2 .00

WP

- 04

- SL

- 001 681,000 500 2 .00 0 .000 0.000 0.000 457 0.8 00 20 .0 14,300 38.2 1.9 0

WP

- 04

- SL

- 002 318,000 200 3.3 1.3 0 0.000 0.000 204 0.5 00 5,300 8 .0 25.1 1.5 0

WP

- 04

- SL

- 003 323,000 200 4 .00 1.3 0 0.000 0.000 178 0.4 00 4,080 7 .0 27.4 1.5 0

WP

- 04

- SL

- 004 343,000 200 2.2 2.2 0 0.000 0.000 312 0.6 00 3,140 11 .0 33 .0 1.7 0

WP

- 04

- SL

- 005 351,000 200 5.2 1.4 0 0.000 0.000 259 0.6 00 5,350 9 .00 34.1 1.6 0

WP

- 04

- SL

- 006 316,000 200 3.2 1.3 0 0.000 0.000 187 0.5 00 4,280 8 .00 28 .0 1.5 0

WP

- 04

- SL

- 007 296,000 200 2 .00 0 .000 0.000 0.000 197 0.5 00 5,490 8 .00 30.2 1.5 0

WP

- 04

- SL

- 008 327,000 200 2 .00 0 .000 0.000 0.000 178 0.4 00 9,150 12 .0 26.2 1.6 0

WP

- 04

- SL

- 009 116,000 100 43.6 1.6 0 0.000 0.000 566 1 .00 14,500 10 .0 31.9 2.1 0

WP

- 04

- SL

- 010 187,000 200 43 .0 1.7 0 0.000 0.000 668 1.1 0 37,300 30 .0 38.8 2.3 0

WP

- 04

- SL

- 011 226,000 200 35.3 1.4 0 0.000 0.000 537 0.9 00 19,200 20 .0 27.7 1.9 0

WP

- 04

- SL

- 012 214,000 200 42.2 1.5 0 0.000 0.000 505 0.9 00 31,000 30 .0 40.2 2.3 0

WP

- 05

- SL

- 027 466,000 300 13.6 1.4 0 0.000 0.000 655 1 .00 25,300 30 .0 44.7 2.3 0

WP

- 05

- SL

- 028 575,000 400 4.9 0 1.4 0 0.000 0.000 379 0.7 00 23,800 30 .0 28.3 2 .00

WP

- 05

- SL

- 029 579,000 500 41.4 1.6 0 0.000 0.000 185 0.5 00 8,340 30 .0 33.3 1.8 0

WP

- 05

- SL

- 030 362,000 300 26.9 1.4 0 0.000 0.000 463 0.8 00 19,600 30 .0 37.4 2 .00

WP

- 05

- SL

- 031 507,000 400 8.7 0 1.4 0 0.000 0.000 283 0.6 00 14,800 20 .0 46.8 2 .00

WP

- 05

- SL

- 032 323,000 300 19.9 1.4 0 0.000 0.000 865 1.1 0 19,700 30 .0 35.6 2.1 0

WP

- 05

- SL

- 033 549,000 400 2 .00 0 .000 0.000 0.000 496 0.8 00 33,900 40 .0 28.7 2 .00

WP

- 05

- SL

- 034 294,000 200 10 .0 1.5 0 0.000 0.000 552 0.8 00 18,200 20 .0 35.5 2.1 0

WP

- 06

- SL

- 014 292,000 200 4.9 0 1.3 0 0.000 0.000 173 0.4 00 9,520 11 .0 30.3 1.5 0

WP

- 06

- SL

- 015 297,000 200 2 .00 0 .000 0.000 0.000 201 0.5 00 11,600 10 .0 28.5 1.5 0

WP

- 06

- SL

- 016 317,000 200 3.1 0 1.3 0 0.000 0.000 172 0.4 00 8,140 11 .0 22.7 1.7 0

WP

- 06

- SL

- 017 300,000 200 2 .00 0 .000 0.000 0.000 171 0.4 00 6,070 9 .00 27 .0 1.6 0

WP

- 06

- SL

- 018 90,600 150 3.5 0 3.4 0 0.000 0.000 650 0.9 00 33,600 40 .0 27.5 1.3 0

WP

- 06

- SL

- 019 111,000 100 7.1 0 2 .00 0.000 0.000 924 1.1 0 33,000 30 .0 38 1.5 0January 2015

F

- 14 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Solids Analysis

Study ID Silicon

Result (ppm) Silicon

Error (ppm) Silver

Result (ppm) Silver

Error (ppm) Sodium

Result (ppm) Sodium

Error (ppm) Strontium

Result (ppm) Strontium

Error (ppm) Sulfur

Result (ppm) Sulfur

Error (ppm) Tantulum

Result (ppm) Tantulum

Error (ppm)

WP

- 06

- SL

- 020 84,400 90 .0 2 .00 0 .000 0.000 0.000 2,170 2 .00 57,800 40 .0 32.2 1.6 0

WP

- 06

- SL

- 021 262,000 300 2 .00 0 .000 0.000 0.000 844 1.1 0 42,100 60 .0 31.1 1.7 0

WP

- 06

- SL

- 022 488,000 400 2.1 2.1 0 0.000 0.000 956 1.2 0 12,500 20 .0 46.1 2.1 0

WP

- 06

- SL

- 023 368,000 300 2 .00 1.9 0 0.000 0.000 427 0.7 00 19,900 30 .0 33.6 1.6 0

WP

- 06

- SL

- 024 209,000 300 2 .00 0 .000 0.000 0.000 1,600 2 .00 11,000 50 .0 45.3 1.6 0

WP

- 06

- SL

- 025 406,000 300 2.7 0 2.6 0 0.000 0.000 1,180 1 .00 12,000 20 .0 41.3 2 .00

WP

- 06

- SL

- 026 408,000 500 9.5 0 2.1 0 0.000 0.000 2,220 2 .00 12,700 60 .0 50.1 2.5 0

WP

- 06

- SL

- 037 129,000 200 50.5 2 .00 0.000 0.000 13,300 10 .0 25,100 30 .0 77.7 3.4 0

WP

- 07

- SL

- 039 354,000 200 6.3 0 1.5 0 0.000 0.000 141 0.4 00 3,910 7 .00 1.3 0 0.2 00

WP

- 07

- SL

- 040 320,000 200 2 .00 0 .000 0.000 0.000 149 0.4 00 6,370 9 .00 29.8 1.1 0

WP

- 07

- SL

- 041 343,000 200 2 .00 0 .000 0.000 0.000 141 0.4 00 2,830 6 .00 31.4 1.4 0

WP

- 10

- SL

- 045 136,000 100 1.2 0 1.2 0 0.000 0.000 489 0.7 00 2,580 5 .00 34.4 1.6 0

WP

- 10

- SL

- 048 198,000 100 30.1 1.5 0 0.000 0.000 7,360 5 .00 26,800 20 .0 58.7 2.9 0

WP

- 11

- SL

- 047 176,000 200 17.2 1.7 0 0.000 0.000 230 0.5 00 46,300 60 .0 30.7 1.6 0

WP

- 11

- SL

- 068 69,700 60 .0 40 .0 1.6 0 0.000 0.000 2,890 3 .00 12,500 10 .0 22.1 2.1 0

WP

- 12

- SL

- 052 300,000 200 40.6 1.7 0 0.000 0.000 1,100 1 .00 14,900 20 .0 28.3 2.3 0

WP

- 12

- SL

- 053 295,000 200 4 .00 1.4 0 0.000 0.000 707 0.9 00 3,560 8 .00 24.9 1.7 0

WP

- 12

- SL

- 055 145,000 100 68.9 2.9 0 0.000 0.000 1,980 2 .00 32,600 30

. 49.9 3.4 0

WP

- 12

- SL

- 056 264,000 200 90.2 3.5 0 0.000 0.000 4,050 4 .00 68,400 50 .0 65 .0 5.1 0

WP

- 13

- SL

- 059 250,000 200 2 .00 0 .000 0.000 0.000 284 0.6 0 3,840 6 .00 20.4 1.4 0

WP

- 13

- SL

- 062 244,000 200 45.8 1.5 0 0.000 0.000 2,150 2 .00 40,300 30 .0 16.6 2.2 0

WP

- 14

- SL

- 073 201,000 100 2 .0 0 .000 0.000 0.000 285 0.5 0 2,010 5 .00 19.2 1.5 0

WP

- 14

- SL

- 074 349,000 200 2 .0 0 .000 0.000 0.000 148 0.4 0 1,930 6 .00 26.4 1.5 0

WP

- 14

- SL

- 077 60,700 50 .0 24.7 1.4 0.000 0.000 2,910 2 .00 6,720 7 .00 4.9 0 0.3 00

WP

- 14

- SL

- 078 105,000 100 21.5 1.4 0.000 0.000 2,780 2 .00 12,300 10 .0 34.6 2.4 0

WP

- 14

- SL

- 079 59,100 50 .0 45.3 1.5 0.000 0.000 5,680 4 .00 9,300 9 .00 39 .0 2.9 0

WP

- 15

- SL

- 075 579,000 500 41.4 1.6 0.000 0.000 185 0.5 00 8,340 30 .0 33.3 0.8 00January 2015

F

- 15 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Solids Analysis

Study ID Tellurium

Result (ppm) Tellurium

Error (ppm) Thallium

Result (ppm) Thallium

Error (ppm) Thorium

Result (ppm) Thorium

Error (ppm) Tin

Result (ppm) Tin

Error (ppm) Titanium

Result (ppm) Titanium

Error (ppm)

BR

- 30

- SL

- 029 22.1 1 .00 1.5 0 0.2 00 3.6 0 0.5 00 85.6 1.3 0 3,680 14 .0

WP

- 02

- SL

- 036 52.3 1.4 0 5.9 0 0.3 00 12.2 0.4 00 42.4 0.8 00 2,710 17 .0

WP

- 03

- SL

- 038 3 .00 0 .000 1.6 0 0.2 00 20.1 0.4 00 6.5 0 0.7 00 5,830 12 .0

WP

- 03

- SL

- 065 101 1.4 0 5.5 0 0.3 00 11.8 0.4 00 74.1 0.7 00 4,030 27 .0

WP

- 04

- SL

- 001 7.4 0 0.6 00 1.6 0 0.3 00 17.9 0.4 00 11.9 0.8 00 11,000 20 .0

WP

- 04

- SL

- 002 0.5 00 0.1 00 1.4 0 0.2 00 16.4 0.4 00 2.4 0 0.1 00 6,390 16 .0

WP

- 04

- SL

- 003 3 .00 0 .000 1.2 0 0.2 00 17.5 0.4 00 6 .00 0.4 00 6,250 14 .0

WP

- 04

- SL

- 004 1.3 0 0.1 00 1.7 0 0.3 00 15.5 0.4 00 15 .0 0.5 00 6,410 23 .0

WP

- 04

- SL

- 005 14.7 0.7 00 1.5 0 0.3 00 16 0.4 00 14.8 0.5 00 6,630 19 .0

WP

- 04

- SL

- 006 10.9 0.7 00 1.5 0 0.2 00 18.3 0.4 00 11.8 0.7 00 6,710 14 .0

WP

- 04

- SL

- 007 3 .00 0 .000 1.6 0 0.3 00 14.5 0.4 00 6.6 0 0.5 00 5,530 13 .0

WP

- 04

- SL

- 008 3 .00 0 .000 1.7 0 0.3 00 16.8 0.4 00 1.1 0 0.1 00 6,330 14 .0

WP

- 04

- SL

- 009 138 1.5 0 2.8 0 0.3 00 12 0.5 00 109 0.8 00 2,870 32 .0

WP

- 04

- SL

- 010 124 1.4 0 3.2 0 0.4 00 10.8 0.5 00 108 0.8 00 5,450 50 .0

WP

- 04

- SL

- 011 105 1.4 0 2.6 0 0.3 00 12.5 0.4 00 77.6 0.7 00 4,150 35 .0

WP

- 04

- SL

- 012 111 1.4 0 40.2 2.3 0 12.4 0.4 00 89.7 0.8 00 5,280 41 .0

WP

- 05

- SL

- 027 55.9 1.4 0 3.5 0 0.3 00 16.2 0.4 00 56.8 1 .00 6,240 33 .0

WP

- 05

- SL

- 028 16.3 0.8 00 1.6 0 0.2 00 17.4 0.4 00 22.6 0.7 00 9,000 36 .0

WP

- 05

- SL

- 029 77 .0 1.8 0 1.3 0 1.2 0 15.5 0.4 00 74.9 1.7 00 8,410 26 .0

WP

- 05

- SL

- 030 89 .0 1.5 0 2.1 0 0.3 00 14.5 0.4 00 81.7 0.9 00 7,310 40 .0

WP

- 05

- SL

- 031 21.1 0.9 00 1.9 0 0.2 00 16.5 0.4 00 30.9 0.9 00 8,530 27 .0

WP

- 05

- SL

- 032 62.1 1.3 0 2.3 0 0.2 00 11.1 0.4 00 61.7 0.9 00 4,260 38 .0

WP

- 05

- SL

- 033 40.7 1.2 0 1.3 0 0.2 00 11.2 0.4 00 44.6 0.9 00 6,580 46 .0

WP

- 05

- SL

- 034 37.9 1.2 0 3.1 0 0.3 00 16.4 0.5 00 32 .0 0.7 00 5,620 25 .0

WP

- 06

- SL

- 014 3 .00 0 .000 1.8 0 0.2 00 16.5 0.4 00 11.7 0.7 00 5,500 14 .0

WP

- 06

- SL

- 015 3 .00 0 .000 1.6 0 0.2 00 17.8 0.4 00 24 .0 0.7 00 4,280 14 .0

WP

- 06

- SL

- 016 3 .00 0 .000 2 .00 0.2 00 15.2 0.4 00 9 .00 0.7 00 5,470 12 .0

WP

- 06

- SL

- 017 3 .00 0 .000 1.9 0 0.2 00 16.3 0.4 00 11.5 0.8 00 5,750 12 .0

WP

- 06

- SL

- 018 3 .00 0 .000 2.3 0 0.3 00 6.5 0 0.4 00 3.2 0 0.4 00 705 7.2 0

WP

- 06

- SL

- 019 3 .00 0 .000 2.5 0 0.3 00 8.6 0 0.4 00 1.7 0 0.2 00 1,080 10 .0January 2015

F

- 16 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Solids Analysis

Study ID Tellurium

Result (ppm) Tellurium

Error (ppm) Thallium

Result (ppm) Thallium

Error (ppm) Thorium

Result (ppm) Thorium

Error (ppm) Tin

Result (ppm) Tin

Error (ppm) Titanium

Result (ppm) Titanium

Error (ppm)

WP

- 06

- SL

- 020 3 .00 0 .000 3.5 0 0.3 00 10.9 0.4 00 8.5 0 0.7 00 1,490 9 .00

WP

- 06

- SL

- 021 4.2 0 0.5 00 31.1 1.7 0 8.5 0 0.4 00 10.7 1.2 0 2,260 13 .0

WP

- 06

- SL

- 022 3 .00 0 .000 2.7 0 0.3 00 15.6 0.4 00 9.5 0 0.9 00 6,740 19 .0

WP

- 06

- SL

- 023 3 .00 0 .000 1.2 0 0.2 00 6.3 0 0.3 00 11.5 1.1 00 3,880 14 .0

WP

- 06

- SL

- 024 3 .00 0 .000 1 .00 0 .000 11.5 0.4 00 3.9 0 0 .000 2,370 11 .0

WP

- 06

- SL

- 025 3 .00 0 .000 2.6 0 0.3 00 16 .0 0.4 00 0.9 00 0.1 00 5,750 18 .0

WP

- 06

- SL

- 026 3 .00 0 .000 14.9 0.6 00 17.7 0.5 00 6.9 0 0.8 00 3,410 16 .0

WP

- 06

- SL

- 037 108 1.5 0 10.4 0.5 00 17.4 1.3 0 102 0.9 00 2,990 48 .0

WP

- 07

- SL

- 039 3 .00 0 .000 1.3 0 0.2 00 17.3 0.4 00 3.8 0 0.5 00 6,780 13 .0

WP

- 07

- SL

- 040 3 .00 0 .000 1.2 0 0.2 00 17.8 0.4 00 11.8 1 .00 6,190 12 .0

WP

- 07

- SL

- 041 3 .00 0 .000 1.3 0 0.2 00 17.7 0.4 00 12 .0 0.9 00 6,760 13 .0

WP

- 10

- SL

- 045 3 .00 0 .000 1.1 0 0.3 00 11.8 0.4 00 5.2 0 0.5 00 3,460 12 .0

WP

- 10

- SL

- 048 71.9 1.2 0 7.4 0 0.4 00 13.8 0.8 00 59.6 0.7 00 3,500 33 .0

WP

- 11

- SL

- 047 37.2 1.5 0 2.5 0 0.3 00 7 .00 0.4 00 26.6 1.1 0 2,350 15 .0

WP

- 11

- SL

- 068 119 1.4 0 3.1 0 0.4 00 7.7 0 0.5 00 91.3 0.7 00 675 43 .0

WP

- 12

- SL

- 052 160 2.1 0 2.6 0 0.3 00 17.7 0.5 00 98.5 1 .00 6,620 35 .0

WP

- 12

- SL

- 053 12 .0 0.7 00 2.1 0 0.2 00 17.9 0.4 00 17.7 0.7 00 6,070 16 .0

WP

- 12

- SL

- 055 219 2.3 0 2.2 0 0.5 00 13 .0 0.8 00 182 1.2 0 4,020 67 .0

WP

- 12

- SL

- 056 234 2.5 0 9.5 0 0.8 00 20.3 1.2 0 211 1.4 0 8,470 110

WP

- 13

- SL

- 059 3 .00 0 .000 1.4 0 0.3 00 16.2 0.4 00 8.2 0 0.6 00 4,980 12 .0

WP

- 13

- SL

- 062 112 1.6 0 4.4 0 0.3 00 9.4 0 0.5 00 87.8 1 .00 2,470 31 .0

WP

- 14

- SL

- 073 3 .00 0 .000 1.5 0 0.2 00 17.1 0.4 00 15.7 0.9 00 4,600 11 .0

WP

- 14

- SL

- 074 3 .00 0 .000 1.4 0 0.2 00 17.3 0.4 00 11.8 0.9 00 6,450 13 .0

WP

- 14

- SL

- 077 103 1.6 0 4.9 0 0.3 00 11 .0 0.5 00 74.3 0.8 00 1,890 26 .0

WP

- 14

- SL

- 078 90.4 1.5 0 4.4 0 0.3 00 13.3 0.5 00 73.7 0.8 00 1,520 20 .0

WP

- 14

- SL

- 079 156 1.7 0 6.4 0 0.4 00 11.7 0.7 00 108 0.8 00 901 24 .0

WP

- 15

- SL

- 075 77 1.8 0 1.3 0 1.2 0 15.5 0.4 00 74.9 1.7 0 8,410 26 .0January 2015

F

- 17 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Solids Analysis

Study ID Tungsten

Result (ppm) Tungsten

Error (ppm) Uranium

Result (ppm) Uranium

Error (ppm) Vanadium

Result (ppm) Vanadium

Error (ppm) Yttrium

Result (ppm) Yttrium

Error (ppm) Zinc

Result (ppm) Zinc

Error (ppm)

BR

- 30

- SL

- 029 11.8 1.2 0 6.2 0 0.4 00 17.6 1.7 0 16.8 0.3 00 1,260 3 .00

WP

- 02

- SL

- 036 4.2 0 0.7 00 28.6 0.5 00 160 4.3 0 36.7 0.3 00 158 1 .00

WP

- 03

- SL

- 038 4.5 0 0.6 00 2.9 0 0.2 00 174 5 .00 36.9 0.3 00 108 0.8 0

WP

- 03

- SL

- 065 3.6 0 0.6 00 20.1 0.6 00 74 .0 2.6 0 28.7 0.4 00 127 1 .00

WP

- 04

- SL

- 001 0.7 00 6.1 0 5.3 0 0.3 00 264 9.1 0 37 .0 0.3 00 138 1.1 0

WP

- 04

- SL

- 002 6.7 0 0.6 00 3 .00 0.2 00 139 5.2 0 35.8 0.3 00 107 0.8 00

WP

- 04

- SL

- 003 6 .00 0.6 00 4 .00 0.3 00 113 5 .00 34.9 0.3 00 106 0.8 00

WP

- 04

- SL

- 004 5.7 0 0.6 00 3.6 0 0.2 00 58.5 4.4 0 34.5 0.3 00 114 0.9 00

WP

- 04

- SL

- 005 6.5 0 0.6 00 2.6 0 0.2 00 141 5.6 0 37.9 0.3 00 119 0.9 00

WP

- 04

- SL

- 006 5.7 0 0.6 00 4.2 0 0.3 00 180 5.3 0 36.9 0.3 00 111 0.8 00

WP

- 04

- SL

- 007 4.9 0 0.6 00 3 .00 0.2 00 198 5.3 0 29.7 0.3 00 107 0.8 00

WP

- 04

- SL

- 008 6.9 0 0.7 00 5.3 0 0.3 00 234 5.5 0 33.6 0.3 00 146 0.9 00

WP

- 04

- SL

- 009 1.9 0 1.2 0 8.7 0 0.4 00 97.9 2.9 0 22.6 0.3 00 146 1.2 0

WP

- 04

- SL

- 010 3.7 0 0.6 00 9.9 0 0.4 00 293 8.6 0 24.5 0.4 00 163 1.3 0

WP

- 04

- SL

- 011 4.3 0 0.6 00 5.9 0 0.3 00 1 .00 0 .000 24.3 0.3 00 193 1.2 0

WP

- 04

- SL

- 012 6.9 0 0.8 00 14.6 0.5 00 203 6.9 0 29.5 0.4 00 181 1.2 0

WP

- 05

- SL

- 027 5.1 0 0.8 00 9.7 0 0.4 00 1.8 0 0 .000 25.6 0.3 00 362 1.7 0

WP

- 05

- SL

- 028 6.5 0 0.7 00 4.5 0 0.3 00 95.3 6.5 0 31.7 0.3 00 134 1.1 0

WP

- 05

- SL

- 029 1.6 0 0.3 00 3.7 0 0.2 00 175 8.7 0 29.4 0.3 00 89.6 0.9 00

WP

- 05

- SL

- 030 6.6 0 0.8 00 3.5 0 0.2 00 18.6 0.9 00 29.9 0.3 00 114 1 .00

WP

- 05

- SL

- 031 8.1 0 0.8 00 2.6 0 0.2 00 104 5.7 0 30.9 0.3 00 138 1 .00

WP

- 05

- SL

- 032 4.5 0 0.6 00 5.2 0 0.3 00 1.8 0 0 .000 23.5 0.3 00 71.8 0.8 00

WP

- 05

- SL

- 033 5.2 0 0.7 00 2.3 0 0.2 00 1.8 0 0 .000 20.9 0.3 00 129 1.1 0

WP

- 05

- SL

- 034 6 .00 0.7 00 6.6 0 0.4 00 95.4 5 .00 25.8 0.3 00 245 1.3 0

WP

- 06

- SL

- 014 5.2 0 0.6 00 6.4 0 0.3 00 90.4 4.4 0 33.8 0.3 00 143 0.9 00

WP

- 06

- SL

- 015 5.5 0 0.6 00 3.8 0 0.3 00 59.8 2.8 0 34.3 0.3 00 129 0.9 00

WP

- 06

- SL

- 016 4.8 0 0.6 00 7.1 0 0.3 00 272 5.3 0 32.2 0.3 00 124 0.8 00

WP

- 06

- SL

- 017 5.2 0 0.6 00 6.1 0 0.3 00 171 4.7 0 31.9 0.3 00 97.3 0.8 00

WP

- 06

- SL

- 018 1.5 0 0.6 00 3 .00 0.2 00 11.7 1.3 0 2.7 0 0.2 00 15.6 0.5 00

WP

- 06

- SL

- 019 2.5 0 0.4 00 2.8 0 0.2 00 35.4 2.8 0 8.3 0 0.3 00 22.9 0.6 00January 2015

F

- 18 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Solids Analysis

Study ID Tungsten

Result (ppm) Tungsten

Error (ppm) Uranium

Result (ppm) Uranium

Error (ppm) Vanadium

Result (ppm) Vanadium

Error (ppm) Yttrium

Result (ppm) Yttrium

Error (ppm) Zinc

Result (ppm) Zinc

Error (ppm)

WP

- 06

- SL

- 020 3 .00 0.5 00 13.4 0 0.5 00 54.5 2.9 0 11 0.2 00 34.7 0.6 00

WP

- 06

- SL

- 021 1 .00 0.6 00 4.4 0 0.2 00 10.6 1.8 0 5.8 0 0.2 00 35.7 0.7 00

WP

- 06

- SL

- 022 4.9 0 0.7 00 5.8 0 0.3 00 235 8.2 0 21.9 0.3 00 104 1 .00

WP

- 06

- SL

- 023 2.7 0 0.4 00 1.5 0 0.1 00 129 6 .00 9.7 0 0.2 00 39.8 0.6 00

WP

- 06

- SL

- 024 2.5 0 0.4 00 4.8 0 0.3 00 53 .0 4 .00 12.8 0.3 00 27.7 0.6 00

WP

- 06

- SL

- 025 8 .00 0.8 00 5.4 0 0.3 00 197 7.5 0 20.8 0.3 00 99.3 1 .00

WP

- 06

- SL

- 026 4.2 0 0.7 00 8.8 0 0.5 00 65.8 1.4 0 19.3 0.3 00 56.3 0.9 00

WP

- 06

- SL

- 037 3.4 0 1.8 0 80.8 1.3 0 1 .00 0 .000 32.8 0.6 00 116 1.4 0

WP

- 07

- SL

- 039 5.7 0 0.6 00 2.5 0 0.2 00 176 5.1 0 36.5 0.3 00 97.4 0.8 00

WP

- 07

- SL

- 040 5.1 0 0.6 00 1.5 0 0.1 00 153 4.8 0 26 .0 0.3 00 108 0.8 00

WP

- 07

- SL

- 041 6.3 0 0.6 00 2.3 0 0.2 00 155 5 .00 37 .0 0.3 00 128 0.9 00

WP

- 10

- SL

- 045 6.6 0 0.7 00 3 .00 0.2 00 110 4.3 0 21.9 0.3 00 83 .0 0.8 00

WP

- 10

- SL

- 048 58.7 2.9 0 49.4 1 .00 51.6 2.6 0 33.6 0.4 00 221 1.4 0

WP

- 11

- SL

- 047 1.7 0 0.3 00 2.4 0 0.1 00 37.6 3.1 0 5.1 0 0.2 00 18.4 0.5 00

WP

- 11

- SL

- 068 1 .00 0 .000 17.6 0.5 00 1 .00 0 .000 15.3 0.3 00 44.3 0.9 00

WP

- 12

- SL

- 052 1.8 0 1.2 0 12.4 0.5 00 1 .00 0 .000 35.4 0.4 00 121 1.1 0

WP

- 12

- SL

- 053 24.9 1.7 0 6.3 0 0.3 00 73.1 4 .00 35.7 0.3 00 112 0.8 00

WP

- 12

- SL

- 055 1 .00 0 .000 11.3 0.5 00 1 .00 0 .000 18.8 0.4 00 205 1.9 0

WP

- 12

- SL

- 056 1 .00 0 .000 36.6 1.2 0 1 .00 0 .000 44.5 0.8 00 384 2.9 0

WP

- 13

- SL

- 059 7.2 0.7 00 2 .00 0.2 00 129 4.4 0 31.2 0.3 00 101 0.8 00

WP

- 13

- SL

- 062 1 .00 0.000 33.1 0.6 00 61.2 3.4 0 36 .0 0.3 00 155 1.2 0

WP

- 14

- SL

- 073 8.6 0 0.7 00 3.1 0 0.2 00 98.7 3.8 0 345 0.3 00 112 0.6 00

WP

- 14

- SL

- 074 2.3 0 0.4 00 3.2 0 0.2 00 153 5.1 0 35.5 0.3 00 99.1 0.8 00

WP

- 14

- SL

- 077 5.4 0 0.8 00 31.4 0.7 00 22.5 1 .00 34.1 0.3 00 215 1.3 0

WP

- 14

- SL

- 078 4.8 0 0.7 00 33.8 0.7 00 1 .00 0 .000 31.3 0.3 00 124 1 .00

WP

- 14

- SL

- 079 3 .00 0.7 00 49.4 0.9 00 1 .00 0 .000 34.4 0.4 00 220 1.5 0

WP

- 15

- SL

- 075 1.6 0 0.3 00 3.7 0 0.2 00 175 8.7 0 29.4 0.3 00 89.6 0.9 00January 2015

F

- 19 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Solids Analysis

Study ID Zirconium

Result (ppm) Zirconium

Error (ppm)

BR

- 30

- SL

- 029 238 3 .00

WP

- 02

- SL

- 036 103 1.9 0

WP

- 03

- SL

- 038 237 2 .00

WP

- 03

- SL

- 065 122 2.6 0

WP

- 04

- SL

- 001 353 3.1 0

WP

- 04

- SL

- 002 260 2 .00

WP

- 04

- SL

- 003 250 2 .00

WP

- 04

- SL

- 004 252 2.3 0

WP

- 04

- SL

- 005 248 2.2 0

WP

- 04

- SL

- 006 230 1.9 0

WP

- 04

- SL

- 007 164 1.8 0

WP

- 04

- SL

- 008 197 1.8 0

WP

- 04

- SL

- 009 101 3 .00

WP

- 04

- SL

- 010 89.5 3.2 0

WP

- 04

- SL

- 011 103 2.5 0

WP

- 04

- SL

- 012 111 2.6 0

WP

- 05

- SL

- 027 227 3.2 0

WP

- 05

- SL

- 028 314 3.1 0

WP

- 05

- SL

- 029 304 2.9 0

WP

- 05

- SL

- 030 328 3.5 0

WP

- 05

- SL

- 031 308 2.8 0

WP

- 05

- SL

- 032 162 3.3 0

WP

- 05

- SL

- 033 252 3.1 0

WP

- 05

- SL

- 034 174 2.4 0

WP

- 06

- SL

- 014 228 1.9 0

WP

- 06

- SL

- 015 195 1.9 0

WP

- 06

- SL

- 016 191 1.7 0

WP

- 06

- SL

- 017 196 1.8 0

WP

- 06

- SL

- 018 13.4 2 .00

WP

- 06

- SL

- 019 42.7 2.5 0January 2015

F

- 20 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Solids Analysis

Study ID Zirconium

Result (ppm) Zirconium

Error (ppm)

WP

- 06

- SL

- 020 28.2 3 .00

WP

- 06

- SL

- 021 39.2 2.9 0

WP

- 06

- SL

- 022 177 3.2 0

WP

- 06

- SL

- 023 52.1 1.9 0

WP

- 06

- SL

- 024 180 3.8 0

WP

- 06

- SL

- 025 158 3.3 0

WP

- 06

- SL

- 026 209 5.2 0

WP

- 06

- SL

- 037 1 .00 0 .00

WP

- 07

- SL

- 039 288 2.2 0

WP

- 07

- SL

- 040 251 2 .00

WP

- 07

- SL

- 041 309 2.2 0

WP

- 10

- SL

- 045 154 2.1 0

WP

- 10

- SL

- 048 1 .00 0 .00

WP

- 11

- SL

- 047 32.4 1.5 0

WP

- 11

- SL

- 068 29.2 4.9 0

WP

- 12

- SL

- 052 311 3.9 0

WP

- 12

- SL

- 053 334 2.7 0

WP

- 12

- SL

- 055 76.3 6.7 0

WP

- 12

- SL

- 056 128 9.7 0

WP

- 13

- SL

- 059 233 2.1 0

WP

- 13

- SL

- 062 58.6 3.8 0

WP

- 14

- SL

- 073 309 2.2 0

WP

- 14

- SL

- 074 319 2.2 0

WP

- 14

- SL

- 077 74.6 3.8 0

WP

- 14

- SL

- 078 81 .0 3.8 0

WP

- 14

- SL

- 079 47.2 5.8 0

WP

- 15

- SL

- 075 304 2.9 0January 2015

F

- 21 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Liquids Analysis

Study ID Date/Time Aluminum

Result (ppm) Aluminum

Error (ppm) Antimony

Result (ppm) Antimony

Error (ppm) Arsenic

Result (ppm) Arsenic

Error (ppm) Barium

Result (ppm) Barium

Error (ppm) Bismuth

Result (ppm) Bismuth

Error (ppm)

WT

- 04

- LQ

- 204 10/07/13 20 .0 0 .000 3 .00 0.000 0.5 00 0.000 2 .00 0.000 1 .00 0.000

WT

- 05

- LQ

- 206 10/07/13 93 .0 14 .0 3.00 0.000 0.500 0.000 2.00 0.000 1.00 0.000

WT

- 13

- LQ

- 212 10/08/13 17 .0 0.4 00 3.00 0.000 0.500 0.000 2.00 0.000 1.00 0.000

WT

- 14

- LQ

- 214 10/08/13 20 .0 0.000 3.00 0.000 0.500 0.000 2.00 0.000 1.00 0.000

WT

- 17

- LQ

- 220 10/09/13 20 .0 0.000 3.00 0.000 0.500 0.000 2.00 0.000 1.00 0.000

WT

- 11

- LQ

- 222 10/09/13 20 .0 0.000 3.00 0.000 0.500 0.000 980 12 .0 1.00 0.000

WT

- 15

- LQ

- 226 10/09/13 20 .0 0.000 3.00 0.000 0.500 0.000 65.1 3.8 0 1.00 0.000

WT

- 09

- LQ

- 228 10/09/13 20 .0 0.000 3.00 0.000 0.500 0.000 99.2 4.8 0 1.00 0.000

WT

- 19

- LW

- 232 10/10/13 3,550 16 .0 3.00 0.000 0.500 0.000 1,250 12 .0 1.00 0.000

WT

- 25

- LQ

- 234 10/10/13 20 .0 0.000 3.00 0.000 0.500 0.000 4,850 18 .0 1.00 0.000

WT

- 06

- LQ

- 248 10/15/13 20 .0 0.000 3.00 0.000 0.500 0.000 4,890 18 .0 1.00 0.000

WT

- 08

- LQ

- 240 10/14/13 20 .0 0.000 3.00 0.000 0.500 0.000 3,810 17 .0 1.00 0.000

WT

- 16

- LQ

- 244 10/15/13 30.3 0.7 00 3.00 0.000 0.500 0.000 2 .00 0 .000 1.00 0.000

WT

- 20

- LQ

- 250 10/16/13 1,900 53 .0 3.00 0.000 0.500 0.000 18,600 30 .0 1.00 0.000

WP

- 04

- LQ

- 014 10/16/13 20 .0 0 .000 3.00 0.000 0.500 0.000 23,300 40 .0 1.00 0.000

WT

- 23

- LQ

- 256 10/24/13 16.6 1 .00 3.00 0.000 0.500 0.000 2 .00 0 .000 1.00 0.000

WT

- 21

- LQ

- 264 11/06/13 1,130 38 .0 3.00 0.000 0.500 0.000 3,620 17 .0 1.00 0.000

WT

- 24

- LQ

- 268 11/07/13 20 .0 0 .000 3.00 0.000 0.500 0.000 301 8.6 0 1.00 0.000

WT

- 22

- LQ

- 272 11/07/13 12.8 0.8 00 3.00 0.000 0.500 0.000 225 7.7 0 1.00 0.000

WP

- 10

- LQ

- 015 11/11/13 20 .0 0.000 3.00 0.000 0.500 0.000 5,040 18 .0 1.00 0.000

WT

- 01

- LQ

- 284 11/21/13 20 .0 0.000 3.00 0.000 0.500 0.000 951 12 .0 1.00 0.000

WT

- 02

- LQ

- 278 11/20/13 20 .0 0.000 3.00 0.000 0.500 0.000 837 12 .0 1.00 0.000

WT

- 07

- LQ

- 276 11/20/13 20 .0 0.000 3.00 0.000 0.500 0.000 573 10 .0 1.00 0.000

WT

- 03

- LQ

- 286 11/21/13 87.9 2.1 0 3.00 0.000 0.500 0.000 2.00 0.000 1.00 0.000

WP

- 06

- LQ

- 016 11/22/13 16.7 0.4 00 3.00 0.000 0.500 0.000 2.00 0.000 1.00 0.000

WT

- 10

- LQ

- 290 12/16/13 134 2.2 0 3.00 0.000 0.500 0.000 2.00 0.000 1.00 0.000

WT

- 12

- LQ

- 294 12/16/13 3.6 0 0.000 3.00 0.000 0.500 0.000 2.00 0.000 1.00 0.000

WP

- 06

- LQ

- 017 12/16/13 20 .0 0.000 3.00 0.000 0.500 0.000 2.00 0.000 1.00 0.000

WP

- 09

- LQ

- 018 12/17/13 20 .0 0 .000 3.00 0.000 0.500 0 .000 133 5.8 0 1 .00 0.000

WP

- 08

- LQ

- 021 12/17/13 20 .0 0.000 3.00 0.000 0.500 0.000 152 6.1 0 1.00 0.000January 2015

F

- 22 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Liquids Analysis

Study ID Date/Time Aluminum

Result (ppm) Aluminum

Error (ppm) Antimony

Result (ppm) Antimony

Error (ppm) Arsenic

Result (ppm) Arsenic

Error (ppm) Barium

Result (ppm) Barium

Error (ppm) Bismuth

Result (ppm) Bismuth

Error (ppm)

WP

- 12

- LQ

- 022 12/18/13 20 .0 0.000 3.00 0.000 0.500 0.000 9,120 23 .0 1.00 0.000

WP

- 18

- LQ

- 024 02/06/14 20 .0 0.000 3.00 0.000 0.500 0.000 2 .00 0.000 1.00 0.000

WP

- 19

- LQ

- 029 02/17/14 141 7 .00 3.00 0.000 0.500 0.000 2 .00 0.000 1.00 0.000

WP

- 20

- LQ

- 031 02/17/14 20 .0 0.000 3.00 0.000 0.500 0.000 2 .00 0.000 1.00 0.000

WP

- 21

- LQ

- 033 02/17/14 20 .0 0.000 3.00 0.000 0.500 0.000 2 .00 0.000 1.00 0.000

WP

- 11

- LQ

- 035 02/18/14 468 17 .0 3.00 0.000 0.500 0.000 948 12 .0 1.00 0.000

WP

- 05

- LQ

- 037 02/26/14 20 .0 0.000 3.00 0.000 0.500 0.000 2 .00 0 .000 1.00 0.000

WP

- 04

- LQ

- 039 02/27/14 20 .0 0.000 3.00 0.000 0.500 0.000 12,700 30 .0 1.00 0.000

WP

- 12

- LQ

- 041 02/27/14 20 .0 0.000 3.00 0.000 0.500 0.000 15,400 30 .0 0.6 00 0.1 00

WP

- 11

- LQ

- 043 03/17/14 20 .0 0.000 3.00 0.000 0.500 0.000 804 11 .0 1.00 0.000

WP

- 10

- LQ

- 045 03/18/14 20 .0 0.000 3.00 0.000 0.500 0.000 10,400 20 .0 1.00 0.000

WP

- 14

- LQ

- 046 04/23/14 20 .0 0.000 3.00 0.000 0.500 0.000 2 .00 0 .000 1.00 0.000

WP

- 01

- LQ

- 048 04/24/14 20 .0 0.000 3.00 0.000 0.500 0.000 5,230 18 .0 1.00 0.000

WP

- 10

- LQ

- 050 04/24/14 20 .0 0.000 3.00 0.000 0.500 0.000 11,500 20 .0 1.00 0.000

WP

- 14

- LQ

- 052 06/11/14 20 .0 0.000 3.00 0.000 0.500 0.000 3,940 17 .0 1.00 0.000January 2015

F

- 23 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Liquids Analysis

Study ID Bromine

Result (ppm) Bromine

Error (ppm) Cadmium

Result (ppm) Cadmium

Error (ppm) Calcium

Result (ppm) Calcium

Error (ppm) Cerium

Result (ppm) Cerium

Error (ppm) Cesium

Result (ppm) Cesium

Error (ppm) Chlorine

Result (ppm) Chlorine

Error (ppm)

WT

- 04

- LQ

- 204 475 0.5 00 2 .00 0.000 5,670 8 .00 52 .0 17 .0 4 .00 0.000 46,500 30 .0

WT

- 05

- LQ

- 206 509 0.6 00 2 .00 0.000 7,220 10 .0 2 .00 0 .000 4.00 0.000 50,100 30 0

WT

- 13

- LQ

- 212 0.8 00 0.1 00 0.4 00 0.1 00 34.7 0.5 00 47 .0 16 .0 4.00 0.000 2 .00 0 .000

WT

- 14

- LQ

- 214 8.5 0 0.1 00 2 .00 0 .000 158 1.1 0 2 .00 0 .000 4.00 0.000 806 0.8 0

WT

- 17

- LQ

- 220 12.4 0.1 00 3.2 0 0.4 00 165 1 .00 70 .0 20 .0 4.00 0.000 1,050 1 .00

WT

- 11

- LQ

- 222 897 0.9 00 2 .00 0.000 13,400 20 .0 2.00 0 .000 4.00 0.000 105,000 100

WT

- 15

- LQ

- 226 236 0.3 00 2 .00 0.000 2,790 5 .00 2.00 0 .000 4.00 0.000 24,700 20 .0

WT

- 09

- LQ

- 228 776 0.8 00 1.5 0 0.2 00 12,800 20 .0 2.00 0.000 4.00 0.000 95,400 60 .0

WT

- 19

- LW

- 232 84.1 0.2 00 2 .00 0 .000 1,650 4 .00 2.00 0.000 4.00 0.000 11,100 10 .0

WT

- 25

- LQ

- 234 181 0.3 00 1.6 0 0.2 00 1,450 3 .00 2.00 0.000 4.00 0.000 17,500 10 .0

WT

- 06

- LQ

- 248 217 0.3 00 0.4 00 0.1 00 1,680 3 .00 2.00 0.000 4.00 0.000 18,600 10 .0

WT

- 08

- LQ

- 240 301 0.5 00 2 .00 0 .000 3,620 6 .00 2.00 0.000 4.00 0.000 36,700 20 .0

WT

- 16

- LQ

- 244 0.4 00 0.1 00 0.1 00 0.1 00 58.6 0.7 0 2.00 0.000 10.2 3.5 0 116 0.2 00

WT

- 20

- LQ

- 250 655 0.9 00 2 .00 0.000 11,200 10 .0 2.00 0.000 4.00 0.000 75,700 50 .0

WP

- 04

- LQ

- 014 922 1.2 0 2 .00 0.000 16,500 20 .0 2.00 0.000 4.00 0.000 109,000 100

WT

- 23

- LQ

- 256 79.4 0.2 00 2 .00 0.000 949 2.8 0 2.00 0.000 4.00 0.000 7,490 5 .0

WT

- 21

- LQ

- 264 534 0.7 00 2 .00 0.000 7,430 11 .0 2.00 0.000 3,620 17 .0 55,200 30 .0

WT

- 24

- LQ

- 268 420 0.5 00 2 .00 0.000 6,240 8 .00 2.00 0.000 4.00 0.000 46,500 30 .0

WT

- 22

- LQ

- 272 54.7 0.1 00 0.9 00 0.2 00 378 1.5 0 2.00 0.000 4.00 0.000 4,150 3 .00

WP

- 10

- LQ

- 015 301 0.5 00 2 .00 0 .000 4,460 9 .00 2.00 0.000 4.00 0.000 50,100 30 .0

WT

- 01

- LQ

- 284 834 0.9 00 1.4 0 0.2 00 12,400 20 .0 2.00 0.000 4.00 0.000 87,500 50 .0

WT

- 02

- LQ

- 278 809 0.9 00 2 .00 0.000 11,700 20 .0 2.00 0.000 4.00 0.000 77,100 50 .0

WT

- 07

- LQ

- 276 97.5 0.2 00 2 .00 0.000 1,570 4 .00 2.00 0.000 4.00 0.000 12,000 10 .0

WT

- 03

- LQ

- 286 0.5 00 0.1 00 2 .00 0.000 218 1.2 0 2.00 0.000 4.00 0.000 2.00 0.000

WP

- 06

- LQ

- 016 0.1 00 0.1 00 1.8 0 0.3 00 33.9 0.6 00 2.00 0.000 4.00 0.000 2.00 0.000

WT

- 10

- LQ

- 290 0.5 00 0.1 00 0.3 00 0.1 00 212 1.2 0 2 .00 0.000 4.00 0.000 443 0.6 0

WT

- 12

- LQ

- 294 0.6 00 0.1 00 2 .00 0.000 266 1.5 0 69 19 .0 4.00 0.000 461 0.6 0

WP

- 06

- LQ

- 017 648 0.7 00 2 .00 0.000 10,300 10 .0 2 .00 0 .000 4.00 0.000 69,300 40 .0

WP

- 09

- LQ

- 018 1,150 1 .00 2 .00 0 .000 18,800 20 .0 2 .00 0 .000 4 .00 0 .000 116,000 100

WP

- 08

- LQ

- 021 1,200 1 .00 2 .00 0 .000 21,900 30 .0 2 .00 0 .000 4 .00 0 .000 136,000 100January 2015

F

- 24 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Liquids Analysis

Study ID Bromine

Result (ppm) Bromine

Error (ppm) Cadmium

Result (ppm) Cadmium

Error (ppm) Calcium

Result (ppm) Calcium

Error (ppm) Cerium

Result (ppm) Cerium

Error (ppm) Cesium

Result (ppm) Cesium

Error (ppm) Chlorine

Result (ppm) Chlorine

Error (ppm)

WP

- 12

- LQ

- 022 365 0.5 00 2 .00 0 .000 4,920 8 .00 2 .00 0 .000 4 .00 0 .000 40,300 30 .0

WP

- 18

- LQ

- 024 624 0.7 00 1.3 0 0.2 00 8,190 11 .0 2 .00 0 .000 4 .00 0 .000 62,600 40 .0

WP

- 19

- LQ

- 029 177 0.3 00 2 .00 0 .000 1,710 4 .00 2 .00 0 .000 4 .00 0 .000 14,500 10 .0

WP

- 20

- LQ

- 031 475 0.5 00 2 .00 0 .000 5,840 9 .00 2 .00 0 .000 4 .00 0 .000 47,100 30 .0

WP

- 21

- LQ

- 033 601 0.6 00 2 .00 0 .000 8,610 12 .0 2 .00 0 .000 4 .00 0 .000 69,800 40 .0

WP

- 11

- LQ

- 035 401 0.5 00 1.4 0 0 .0000 2,360 4 .00 2 .00 0 .000 4 .00 0 .000 26,600 20 .0

WP

- 05

- LQ

- 037 907 1 .00 2 .00 0 .000 21,400 30 .0 2 .00 0 .000 4 .00 0 .000 132,000 100

WP

- 04

- LQ

- 039 828 1.1 0 2 .00 0 .000 20,500 30 .0 2 .00 0 .000 4 .00 0 .000 146,000 100

WP

- 12

- LQ

- 041 785 1.1 0 2 .00 0 .000 14,800 20 .0 2 .00 0 .000 4 .00 0 .000 100,000 100

WP

- 11

- LQ

- 043 429 0.6 00 2 .00 0 .000 2,970 6 .00 2 .00 0 .000 4 .00 0 .000 34,700 20 .0

WP

- 10

- LQ

- 045 367 0.5 00 2 .00 0 .000 4,420 8 .00 2 .00 0 .000 4 .00 0 .000 45,000 30 .0

WP

- 14

- LQ

- 046 318 0.4 00 0.9 00 0.1 00 4,340 7 .00 68 .0 19 .0 4 .00 0 .000 31,200 20 .0

WP

- 01

- LQ

- 048 192 0.3 00 0.2 00 0.1 00 1,480 3 .00 2 .00 0 .000 4 .00 0 .000 19,100 10 .0

WP

- 10

- LQ

- 050 279 0.4 00 2 .00 0 .000 1,770 4 .00 2 .00 0 .000 4 .00 0 .000 25,600 20 .0

WP

- 14

- LQ

- 052 679 0.9 00 2 .00 0 .000 14,600 20 .0 2 .00 0 .000 4 .00 0 .000 93,500 60 .0January 2015

F

- 25 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Liquids Analysis

Study ID Chromium

Result (ppm) Chromium

Error (ppm) Cobalt

Result (ppm) Cobalt

Error (ppm) Copper

Result (ppm) Copper

Error (ppm) Gallium

Result (ppm) Gallium

Error (ppm) Germanium

Result (ppm) Germanium

Error (ppm)

WT

- 04

- LQ

- 204 40.7 0.3 00 3 .00 0 .000 0.6 00 0.2 00 0.1 00 0 .000 0.5 00 0 .000

WT

- 05

- LQ

- 206 32.6 0.3 00 3 .00 0 .000 0.9 00 0.2 00 0.3 00 0.1 00 0.5 00 0 .000

WT

- 13

- LQ

- 212 25.1 0.2 00 3 .00 0 .000 0.9 00 0.1 00 0.1 00 0.1 00 0.5 00 0 .000

WT

- 14

- LQ

- 214 23 .0 0.2 00 3 .00 0 .000 1 .00 0.1 00 0.1 00 0.1 00 0.5 00 0 .000

WT

- 17

- LQ

- 220 19.8 0.1 00 3 .00 0 .000 0.7 0 0.1 00 0.5 00 0 .000 0.5 00 0 .000

WT

- 11

- LQ

- 222 3,450 4 .00 3 .00 0 .000 1 .00 0.4 00 0.5 00 0.2 00 0.5 00 0 .000

WT

- 15

- LQ

- 226 36.7 0.2 00 2.2 0 1 .00 1.1 0 0.1 00 0.3 00 0.1 00 0.5 00 0 .000

WT

- 09

- LQ

- 228 233 1 .00 3 .00 0 .000 2.4 0 0.3 00 1 .00 0.2 00 0.2 00 0.2 00

WT

- 19

- LW

- 232 1,270 2 .00 3 .00 0 .000 1.7 0 0.2 00 0.7 00 0.1 00 0.5 00 0 .000

WT

- 25

- LQ

- 234 24.8 0.2 00 3 .00 0 .000 1.2 0 0.2 00 0.4 00 0.1 00 0.5 00 0 .000

WT

- 06

- LQ

- 248 29.2 0.3 00 3 .00 0 .000 0.5 00 0.2 00 0.2 00 0.2 00 0.5 00 0 .000

WT

- 08

- LQ

- 240 42.3 0.4 00 3 .00 0 .000 1.7 0 0.2 00 0.7 00 0.1 00 0.5 00 0 .000

WT

- 16

- LQ

- 244 23.4 0.2 00 3 .00 0 .000 0.6 00 0.1 00 0.5 00 0 .000 0.5 00 0 .000

WT

- 20

- LQ

- 250 118 1.1 0 3 .00 0 .000 3.5 0 0.5 00 1.6 0 0.3 00 0.5 00 0 .000

WP

- 04

- LQ

- 014 115 1.1 0 3 .00 0 .000 0.5 00 0 .000 0.3 00 0.3 00 0.5 00 0 .000

WT

- 23

- LQ

- 256 26 .0 0.2 00 3 .00 0 .000 0.8 00 0.1 00 0.5 00 0 .000 0.5 00 0 .000

WT

- 21

- LQ

- 264 72.1 0.6 00 3 .00 0 .000 3.2 0 0.4 00 1.5 0 0.2 00 0.5 00 0 .000

WT

- 24

- LQ

- 268 67.1 0.4 00 3 .00 0 .000 3 .00 0.3 00 0.1 0 0.1 00 0.5 00 0 .000

WT

- 22

- LQ

- 272 29.8 0.2 00 3 .00 0 .000 0.3 00 0.1 00 0.5 00 0 .000 0.5 00 0 .000

WP

- 10

- LQ

- 015 79.5 0.7 00 3 .00 0 .000 1 .00 0.3 00 0.6 00 0.2 00 0.5 00 0 .000

WT

- 01

- LQ

- 284 118 0.7 00 3 .00 0 .000 1.2 0 0.4 00 0.5 00 0 .000 0.5 00 0 .000

WT

- 02

- LQ

- 278 145 0.8 00 3 .00 0 .000 3.8 0 0.3 00 1.7 0 0.2 00 0.5 00 0 .000

WT

- 07

- LQ

- 276 32.5 0.2 00 3 .00 0 .000 0.7 00 0.2 00 0.2 00 0.1 00 0.5 00 0 .000

WT

- 03

- LQ

- 286 45.9 0.2 00 3 .00 0 .000 0.9 00 0.1 00 0.5 00

0 0 .000 0.5 00 0 .000

WP

- 06

- LQ

- 016 44.2 0.2 00 3 .00 0 .000 0.8 00 0.1 00 0.5 00 0 .000 0.1 00 0.1 00

WT

- 10

- LQ

- 290 26.4 0.2 00 3 .00 0 .000 12.1 0.2 00 0.5 00 0 .000 0.5 00 0 .000

WT

- 12

- LQ

- 294 83.5 0.3 00 3 .00 0 .000 0.6 00 0.1 00 0.5 00 0 .000 0.5 00 0 .000

WP

- 06

- LQ

- 017 93.1 0.6 00 3 .00 0 .000 0.4 00 0.3 00 0.5 00 0 .000 0.5 00 0 .000

WP

- 09

- LQ

- 018 179 0.9 00 3 .00 0 .000 0.1 00 0.1 00 0.4 00 0.4 00 0.5 00 0 .000

WP

- 08

- LQ

- 021 198 1 .00 3 .00 0 .000 2.4 0 0.5 00 2 .00 0.3 00 0.5 00 0 .000January 2015

F

- 26 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Liquids Analysis

Study ID Chromium

Result (ppm) Chromium

Error (ppm) Cobalt

Result (ppm) Cobalt

Error (ppm) Copper

Result (ppm) Copper

Error (ppm) Gallium

Result (ppm) Gallium

Error (ppm) Germanium

Result (ppm) Germanium

Error (ppm)

WP

- 12

- LQ

- 022 119 0.7 00 3 .00 0 .000 0.1 00 0.1 00 0.5 00 0 .000 0.5 00 0 .000

WP

- 18

- LQ

- 024 40.7 0.3 00 3 .00 0 .000 2.4 0 0.2 00 1.1 0 0.1 00 0.5 00 0 .000

WP

- 19

- LQ

- 029 20.3 0.2 00 3 .00 0 .000 1.2 0 0.1 00 0.5 00 0 .000 0.5 00 0 .000

WP

- 20

- LQ

- 031 33.9 0.3 00 3 .00 0 .000 1.4 0 0.2 00 0.6 00 0.1 00 0.5 00 0 .000

WP

- 21

- LQ

- 033 71 .0 0.5 00 3 .00 0 .000 1.1 0 0.3 00 0.8 00 0.2 00 0.5 00 0 .000

WP

- 11

- LQ

- 035 30.2 0.2 00 3 .00 0 .000 0.6 00 0.2 00 0.5 00 0.000 0.5 00 0 .000

WP

- 05

- LQ

- 037 78.9 0.7 00 3 .00 0 .000 1.8 0 0.5 00 0.8 00 0.3 00 0.5 00 0 .000

WP

- 04

- LQ

- 039 86.7 1.2 0 3 .00 0 .000 3.7 0 0.6 00 1.3 0 0.4 00 0.5 00 0 .000

WP

- 12

- LQ

- 041 87.5 0.9 00 3 .00 0 .000 2.8 0 0.6 00 1.6 0 0.4 00 0.5 00 0 .000

WP

- 11

- LQ

- 043 47.8 0.4 00 3 .00 0 .000 0.5 00 0.5 00 0.5 00 0 .000 0.2 00 0.1 00

WP

- 10

- LQ

- 045 50 .0 0.5 00 3 .00 0 .000 2.3 0 0.3 00 0.7 00 0.2 00 0.5 00 0 .000

WP

- 14

- LQ

- 046 28.7 0.2 00 3 .00 0 .000 0.7 00 0.2 00 0.2 00 0.2 00 0.5 00 0 .000

WP

- 01

- LQ

- 048 91.1 0.4 00 3 .00 0 .000 0.7 00 0.2 00 0.5 00 0 .000 0.5 00 0 .000

WP

- 10

- LQ

- 050 1,360 2 .00 3 .00 0 .000 0.8 00 0.2 00 0.4 00 0.1 00 0.5 00 0 .000

WP

- 14

- LQ

- 052 267 1.1 0 3 .00 0 .000 1.3 0 0.5 00 0.5 00 0 .000 0.5 00 0 .000January 2015

F

- 27 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Liquids Analysis

Study ID Hafnium

Result (ppm) Hafnium

Error (ppm) Iodine

Result (ppm) Iodine

Error (ppm) Iron

Result (ppm) Iron

Error (ppm) Lanthanum

Result (ppm) Lanthanum

Error (ppm) Lead

Result (ppm) Lead

Error (ppm)

WT

- 04

- LQ

- 204 2.1 0 0.4 00 3 .00 0.000 90.5 0.8 00 2 .00 0 .000 1.5 0 0.1 00

WT

- 05

- LQ

- 206 1.3 0 0.4 00 3 .00 0.000 127 1 .00 2 .00 0 .000 1.6 0 0.100

WT

- 13

- LQ

- 212 1 .00 0.2 00 3 .00 0.000 102 0.7 00 2 .00 0 .000 0.4 00 0.100

WT

- 14

- LQ

- 214 0.9 0 0.2 00 3 .00 0.000 29.5 0.4 00 2 .00 0 .000 0.1 00 0.100

WT

- 17

- LQ

- 220 1 .00 0 .000 3 .00 0.000 35.3 0.4 00 2 .00 0 .000 0.4 00 0.100

WT

- 11

- LQ

- 222 1.7 0 0.6 00 24.3 4.3 0 179 1.9 0 2 .00 0 .000 3.1 0 0.100

WT

- 15

- LQ

- 226 1.2 0 0.3 00 3 .00 0.000 184 0.9 00 2 .00 0 .000 1 .00 0.100

WT

- 09

- LQ

- 228 1 .00 1 .00 35.8 4.3 0 332 2 .00 2 .00 0 .000 2.2 0 0.100

WT

- 19

- LW

- 232 2 .00 0.3 00 3 .00 0.000 1,110 2 .00 2 .00 0 .000 2 .00 0.100

WT

- 25

- LQ

- 234 1 .00 0 .000 3 .00 0.000 35 0.5 00 2 .00 0 .000 1.4 0 0.100

WT

- 06

- LQ

- 248 0.8 0 0.3 00 3 .00 0.000 113 0.8 00 2 .00 0 .000 1.5 0 0.100

WT

- 08

- LQ

- 240 1 .00 0 .000 3 .00 0.000 112 1 .00 2 .00 0 .000 2.1 0 0.100

WT

- 16

- LQ

- 244 1.2 0 0.2 00 3 .00 0.000 36.8 0.4 0 2 .00 0 .000 0.3 00 0.100

WT

- 20

- LQ

- 250 0.7 00 0.7 00 3 .00 0.000 1,710 5 .00 2 .00 0 .000 18.7 0.3 00

WP

- 04

- LQ

- 014 3.8 0 1.1 0 3 .00 0.000 209 2.3 0 2 .00 0 .000 6.5 00 0.3 00

WT

- 23

- LQ

- 256 1.3 0 0.3 00 3 .00 0.000 35.4 0.5 00 2 .00 0 .000 1.4 0 0.1 00

WT

- 21

- LQ

- 264 0.1 00 0.1 00 3 .00 0.000 988 3.6 0 2 .00 0 .000 12.2 0.3 00

WT

- 24

- LQ

- 268 1.7 0 0.4 00 24 .0 4.4 0 2,520 4 .00 2 .00 0 .000 2 .00 0.1 00

WT

- 22

- LQ

- 272 1.3 0 0.2 00 3 .00 0.000 1,460 2 .00 2 .00 0 .000 0.9 00 0.1 000

WP

- 10

- LQ

- 015 3 .00 0.6 00 8.4 0 8.3 0 880 3.1 0 2 .00 0 .000 3.2 0 0.2 00

WT

- 01

- LQ

- 284 1 .00 0 .00 35 .0 4.4 0 388 2.2 0 2 .00 0 .000 2.7 0 0.1 00

WT

- 02

- LQ

- 278 1.7 0 0.6 00 45.2 4.4 0 910 3.2 0 2 .00 0 .000 5.2 0 0.2 00

WT

- 07

- LQ

- 276 1 .00 0.3 00 3 .00 0.000 36.9 0.5 00 2 .00 0 .000 1.1 0 0.1 00

WT

- 03

- LQ

- 286 1 .00 0 .000 3 .00 0.000 821 1.8 0 2 .00 0 .000 0.5 00 0.1 00

WP

- 06

- LQ

- 016 1.2 0 0.2 00 3 .00 0.000 39.3 0.5 00 2 .00 0 .000 0.5 00 0.1 00

WT

- 10

- LQ

- 290 1.2 0 0.3 00 16.6 4.3 0 128 0.7 00 2 .00 0 .000 0.3 00 0.1 00

WT

- 12

- LQ

- 294 1.7 0 0.3 00 8.2 0 8.1 0 48.5 0.5 00 2 .00 0 .000 0.5 00 0.1 00

WP

- 06

- LQ

- 017 2.7 0 0.6 00 3 .00 0.000 129 1.3 0 2 .00 0 .000 2 .00 0.1 00

WP

- 09

- LQ

- 018 2.6 0 0.8 00 36.8 4.4 0 238 2.1 0 2 .00 0 .000 3.8 0 0.2 00

WP

- 08

- LQ

- 021 1.2 0 1.2 0 15.5 4.3 0 252 2.2 0 2 .00 0 .000 3.7 0 0.2 00January 2015

F

- 28 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Liquids Analysis

Study ID Hafnium

Result (ppm) Hafnium

Error (ppm) Iodine

Result (ppm) Iodine

Error (ppm) Iron

Result (ppm) Iron

Error (ppm) Lanthanum

Result (ppm) Lanthanum

Error (ppm) Lead

Result (ppm) Lead

Error (ppm)

WP

- 12

- LQ

- 022 2.7 0 0.6 00 3 .00 0 .00 122 1.2 0 2 .00 0 .000 3.1 0 0.2 00

WP

- 18

- LQ

- 024 0.5 00 0.5 00 34.5 4.5 0 198 1.3 0 2 .00 0 .000 1.4 0 0.1 00

WP

- 19

- LQ

- 029 0.9 00 0 .000 12.1 4.4 0 116 0.7 00 2 .00 0 .000 0.8 00 0.1 00

WP

- 20

- LQ

- 031 1.3 0 0.4 00 32.5 4.3 0 303 1.4 0 2 .00 0 .000 1.4 0 0.1 00

WP

- 21

- LQ

- 033 2 .00 0.5 00 26.2 4.1 0 375 1.8 0 2 .00 0 .000 1.6 0 0.1 00

WP

- 11

- LQ

- 035 1.1 0 0.4 00 19.4 4.5 0 143 1 .00 2 .00 0 .000 1.9 0 0.1 00

WP

- 05

- LQ

- 037 2.8 0 0.8 00 3 .00 0 .00 437 2.7 0 2 .00 0 .000 4 .00 0.2 00

WP

- 04

- LQ

- 039 0.5 00 0.5 00 2.9 0 2.8 0 525 3.5 0 2 .00 0 .000 5.9 0 0.3 00

WP

- 12

- LQ

- 041 0.9 00 0.9 00 5.9 0 5.9 0 486 3.3 0 2 .00 0 .000 5.6 0 0.3 00

WP

- 11

- LQ

- 043 2.1 0 0.5 00 3 .00 0 .00 245 1.5 0 2 .00 0 .000 2.8 0 0.1 00

WP

- 10

- LQ

- 045 2.1 0 0.5 00 26.4 4.6 0 95.5 1.1 0 2 .00 0 .000 2.7 0 0.1 00

WP

- 14

- LQ

- 046 1.3 0 0.3 00 10.3 4.3 0 42.2 0.6 00 2 .00 0 .000 1.2 0 0.1 00

WP

- 01

- LQ

- 048 1.2 0 0.3 00 3 .00 0 .00 144 0.9 00 2 .00 0 .000 1.7 0 0.1 00

WP

- 10

- LQ

- 050 1 .00 0.4 00 3 .00 0 .00 110 1 .00 2 .00 0 .000 1.9 0 0.1 00

WP

- 14

- LQ

- 052 1 .00 0 .00 3 .00 0 .00 304 2.4 0 2 .00 0 .000 4.5 0 0.2 00January 2015

F

- 29 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Liquids Analysis

Study ID Magnesium

Result (ppm) Magnesium

Error (ppm) Manganese

Result (ppm) Manganese

Error (ppm) Mercury

Result (ppm) Mercury

Error (ppm) Molybdenum

Result (ppm) Molybdenum

Error (ppm) Nickel

Result (ppm) Nickel

Error (ppm)

WT

- 04

- LQ

- 204 4,480 80 .0 17 .0 0.2 00 0.3 00 0 .000 1 .00 0 .000 0.5 00 0.1 00

WT

- 05

- LQ

- 206 4,810 84 .0 14.4 0.2 00 1 .00 0 .000 1.4 0 0.3 00 0.5 00 0.1 00

WT

- 13

- LQ

- 212 150 6.2 0 3.5 0 0.1 00 1 .00 0 .000 1.3 0 0.3 00 2.3 0 0.1 00

WT

- 14

- LQ

- 214 247 8.5 0 3.1 0 0.1 00 1 .00 0 .000 1.2 0 0.3 00 0.6 0 0.1 00

WT

- 17

- LQ

- 220 179 7.6 0 2.7 0 0.1 00 0.4 00 0.1 00 1.4 0 0.3 00 1 .00 0.1 00

WT

- 11

- LQ

- 222 10,900 140 330 1.8 0 1 .00 0 .000 1.1 0 0.3 00 1 .00 0.1 00

WT

- 15

- LQ

- 226 3,870 49 .0 13.6 0.1 00 1 .00 0 .000 1 .00 0 .000 34.4 0.3 00

WT

- 09

- LQ

- 228 9,610 140 31.1 0.5 00 1 .00 0 .000 1 .00 0.3 00 7.9 0 0.3 00

WT

- 19

- LW

- 232 1,480 26 .0 125 0.6 00 0.2 00 0.1 00 0.6 00 0.3 00 1.7 0 0.1 00

WT

- 25

- LQ

- 234 1,760 35 .0 7.9 0 0.1 00 0.3 00 0.1 00 1 .00 0 .000 1.4 0 0.1 00

WT

- 06

- LQ

- 248 2,080 38 .0 9 .00 0.2 00 0.3 00 0.1 00 1 .00 0 .000 17.4 0.3 00

WT

- 08

- LQ

- 240 3,430 63 .0 12.3 0.2 00 1 .00 0 .000 1 .00 0 .000 5 .00 0.2 00

WT

- 16

- LQ

- 244 105 5.4 0 3 .00 0.1 00 1 .00 0 .000 1.4 0 0.3 00 5.6 0 0.1 00

WT

- 20

- LQ

- 250 8,790 120 31.3 0.8 00 1.2 0 0.2 00 1 .00 0 .000 19.3 0.5 00

WP

- 04

- LQ

- 014 7,810 140 20.3 0.8 00 1.2 0 0.2 00 0.1 00 0.1 00 0.9 00 0.1 00

WT

- 23

- LQ

- 256 827 19 .0 2.5 0 0.1 00 1 .00 0 .000 1 .00 0 .000 14.8 0.2 00

WT

- 21

- LQ

- 264 5,190 86 .0 21.8 0.4 00 0.4 00 0.1 00 1 .00 0 .000 30.8 0.5 00

WT

- 24

- LQ

- 268 4,580 81 .0 29 .0 0.3 00 0.3 00 0.2 00 0.6 00 0.6 00 1 .00 0.1 00

WT

- 22

- LQ

- 272 497 14 .0 6.3 0 0.1 00 0.1 00 0.1 00 0.8 00 0.3 00 1.4 0 0.1 00

WP

- 10

- LQ

- 015 4,150 79 .0 18.7 0.4 00 0.4 00 0.1 00 1 .00 0 .000 2.6 0 0.2 00

WT

- 01

- LQ

- 284 9,620 130 48.9 0.5 00 1 .00 0 .000 1 .00 0.3 00 17.3 0.4 00

WT

- 02

- LQ

- 278 6,600 120 79.1 0.6 00 1 .00 0 .000 1.1 0 0.3 00 181 1 .00

WT

- 07

- LQ

- 276 1,390 26 .0 7.3 0 0.1 00 1 .00 0 .000 0.3 00 0 .00 0.7 00 0.1 00

WT

- 03

- LQ

- 286 426 12 .0 25.1 0.2 00 1 .00 0 .000 1.2 0 0.3 00 2.1 0 0.1 00

WP

- 06

- LQ

- 016 184 6.9 0 7.4 0 0.1 00 1 .00 0 .000 1 .00 0 .000 0.8 00 0.1 00

WT

- 10

- LQ

- 290 99.2 5.3 0 3.5 0 0.1 00 1 .00 0 .000 1.4 0 0.3 1.1 0 0.1 00

WT

- 12

- LQ

- 294 176 7.6 0 9.4 0 0.2 00 1 .00 0 .000 1.1 0 0.3 1.4 0 0.1 00

WP

- 06

- LQ

- 017 5,570 110 35.2 0.4 00 0.5 00 0.1 1 .00 0 .000 1 .00 0.1 00

WP

- 09

- LQ

- 018 9,020 150 40.6 0.5 00 0.7 00 0.1 00 1 .00 0.000 0.9 00 0.1 00

WP

- 08

- LQ

- 021 14,100 180 46.4 0.6 00 0.6 00 0.1 00 1 .00 0.000 1.3 0 0.1 00January 2015

F

- 30 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Liquids Analysis

Study ID Magnesium

Result (ppm) Magnesium

Error (ppm) Manganese

Result (ppm) Manganese

Error (ppm) Mercury

Result (ppm) Mercury

Error (ppm) Molybdenum

Result (ppm) Molybdenum

Error (ppm) Nickel

Result (ppm) Nickel

Error (ppm)

WP

- 12

- LQ

- 022 3,500 67 .0 20.4 0.4 00 1 .00 0.2 00 1 .00 0.000 1.2 0 0.1 00

WP

- 18

- LQ

- 024 7,750 98 .0 21.7 0.2 00 1 .00 0 .000 0.8 00 0.3 00 5.5 0 0.2 00

WP

- 19

- LQ

- 029 1,690 31 .0 6.5 0 0.1 00 1 .00 0.000 1 .00 0.3 00 3.1 0 0.1 00

WP

- 20

- LQ

- 031 4,930 83 .0 14 .0 0.2 00 1 .00 0.000 0.6 00 0.3 00 3.2 0 0.1 00

WP

- 21

- LQ

- 033 6,320 100 25.3 0.3 00 1 .00 0.000 1.1 0 0.3 00 5.5 0 0.2 00

WP

- 11

- LQ

- 035 4,950 54 .0 12.7 0.1 00 0.4 00 0.1 00 1 .00 0 .000 3.8 0 0.2 00

WP

- 05

- LQ

- 037 10,400 190 26.4 0.4 00 0.7 00 0.1 00 0.9 00 0.4 00 11.9 0.4 00

WP

- 04

- LQ

- 039 10,600 180 18.7 0.7 00 1.7 0 0.3 00 1 .00 0 .000 11.1 0.5 00

WP

- 12

- LQ

- 041 7,400 140 19.8 0.6 00 1.6 0 0.3 00 0.1 00 0.1 00 8.6 0 0.5 00

WP

- 11

- LQ

- 043 2,980 56 .0 12.4 0.2 00 1 .00 0 .000 1 .00 0.000 4 .00 0.2 00

WP

- 10

- LQ

- 045 3,880 71 .0 13.2 0.4 00 0.7 00 0.1 00 1 .00 0.000 0.8 00 0.1 00

WP

- 14

- LQ

- 046 4,220 59 .0 7.8 0 0.1 00 0.3 00 0 .000 1.3 0 0.3 00 0.3 00 0.1 00

WP

- 01

- LQ

- 048 2,650 38 .0 15.1 0.2 00 0.3 00 0.1 00 12.9 0.4 00 3 .00 0.1 00

WP

- 10

- LQ

- 050 2,210 47 .0 147 0.8 00 0.4 00 0.3 00 13.3 0.4 00 1 .00 0.1 00

WP

- 14

- LQ

- 052 7,050 130 39.2 0.6 00 0.5 00 0.1 00 1 .00 0 .000 6.3 0 0.3 00January 2015

F

- 31 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Liquids Analysis

Study ID Niobium

Result (ppm) Niobium

Error (ppm) Phosphorus

Result (ppm) Phosphorus

Error (ppm) Potassium

Result (ppm) Potassium

Error (ppm) Rubidium

Result (ppm) Rubidium

Error (ppm) Selenium

Result (ppm) Selenium

Error (ppm)

WT

- 04

- LQ

- 204 1 .00 0 .000 3 .00 0 .000 222 2.4 0 0.5 00 0 .000 0.5 00 0.000

WT

- 05

- LQ

- 206 1 .00 0 .000 3 .00 0 .000 363 3.1 0 0.5 00 0 .000 0.5 00 0.000

WT

- 13

- LQ

- 212 1 .00 0 .000 17 .0 0.5 00 25 .0 0.6 00 0.1 00 0.1 00 0.5 00 0.000

WT

- 14

- LQ

- 214 1 .00 0 .000 0.4 00 0.4 00 20.3 0.6 00 0.5 00 0.000 0.5 00 0.000

WT

- 17

- LQ

- 220 0.7 00 0.3 00 9.4 00 0.6 00 16 .0 0.6 00 0.5 00 0.000 0.5 00 0.000

WT

- 11

- LQ

- 222 1 .00 0 .000 3 .00 0 .000 194 3.6 0 0.5 00 0.000 0.5 00 0.000

WT

- 15

- LQ

- 226 1 .00 0 .000 3 .00 0 .000 44.1 1.1 0 0.5 00 0.000 0.5 00 0.000

WT

- 09

- LQ

- 228 1 .00 0 .000 3 .00 0 .000 120 3 .00 0.5 00 0.000 0.5 00 0.000

WT

- 19

- LW

- 232 1 .00 0 .000 3 .00 0 .000 1,180 4 .00 2.3 0 0.1 00 0.5 00 0.000

WT

- 25

- LQ

- 234 1 .00 0 .000 3 .00 0 .000 66.6 1.1 0 0.5 00 0.1 00 0.5 00 0.000

WT

- 06

- LQ

- 248 1 .00 0 .000 3 .00 0 .000 74.6 1.1 0 0.6 00 0.2 00 0.2 00 0.1 00

WT

- 08

- LQ

- 240 1 .00 0 .000 3 .00 0 .000 81.2 1.6 0 0.3 00 0.3 00 0.4 00 0.1 00

WT

- 16

- LQ

- 244 1 .00 0 .000 8.7 0 0.5 00 13.5 0.5 00 0.1 00 0.1 00 0.5 00 0.000

WT

- 20

- LQ

- 250 1 .00 0 .000 3 .00 0 .000 959 5.6 0 0.6 00 0.6 00 0.5 00 0.000

WP

- 04

- LQ

- 014 1 .00 0 .000 3 .00 0 .000 150 3.8 0 0.5 00 0 .000 1.9 0 0.2 00

WT

- 23

- LQ

- 256 1 .00 0 .000 3 .00 0 .000 68.8 1 .00 0.5 00 0.1 00 0.5 00 0 .000

WT

- 21

- LQ

- 264 1 .00 0 .000 3 .00 0 .000 407 3.6 0 0.1 00 0.1 00 0.3 00 0.1 00

WT

- 24

- LQ

- 268 1 .00 0 .000 3 .00 0 .000 295 2.6 0 0.5 00 0 .000 0.5 00 0.000

WT

- 22

- LQ

- 272 1 .00 0 .000 3 .00 0 .000 45.8 0.8 00 0.2 00 0.1 00 0.5 00 0.000

WP

- 10

- LQ

- 015 1 .00 0 .000 3 .00 0 .000 161 2.6 0 0.1 00 0.1 00 0.5 00 0.000

WT

- 01

- LQ

- 284 1 .00 0 .000 3 .00 0 .000 328 3.8 0 0.5 00 0.000 0.5 00 0.000

WT

- 02

- LQ

- 278 0.5 00 0.5 00 3 .00 0 .000 298 3.6 0 0.5 00 0.000 0.5 00 0.000

WT

- 07

- LQ

- 276 1 .00 0 .000 3 .00 0 .000 101 1.3 0 1.5 0 0.1 00 0.5 00 0.000

WT

- 03

- LQ

- 286 0.4 00 0.4 00 3 .00 0 .000 19.8 0.6 00 0.2 00 0.1 00 0.5 00 0.000

WP

- 06

- LQ

- 016 1.1 0 0.3 00 17.3 0.5 00 29.4 0.7 00 0.1 00 0.1 00 0.5 00 0.000

WT

- 10

- LQ

- 290 0.7 00 0.3 00 10.4 0.5 00 27 0.7 00 0.5 00 0 .000 0.5 00 0.000

WT

- 12

- LQ

- 294 0.3 00 0.3 00 15.7 0.6 00 54.1 0.9 00 0.2 00 0.1 00 0.5 00 0.000

WP

- 06

- LQ

- 017 1 .00 0 .000 3 .00 0 .000 294 3.5 0 0.5 00 0 .000 0.5 00 0.000

WP

- 09

- LQ

- 018 1 .00 0 .000 3 .00 0 .000 314 4.4 0 0.5 00 0 .000 0.5 00 0 .000

WP

- 08

- LQ

- 021 1 .00 0 .000 3 .00 0 .000 296 4.8 0 0.5 00 0 .000 5 .00 0 .00January 2015

F

- 32 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Liquids Analysis

Study ID Niobium

Result (ppm) Niobium

Error (ppm) Phosphorus

Result (ppm) Phosphorus

Error (ppm) Potassium

Result (ppm) Potassium

Error (ppm) Rubidium

Result (ppm) Rubidium

Error (ppm) Selenium

Result (ppm) Selenium

Error (ppm)

WP

- 12

- LQ

- 022 1 .00 0 .000 3 .00 0 .000 88.2 1.9 0 0.3 00 0 .000 0.6 00 0.1 00

WP

- 18

- LQ

- 024 1 .00 0 .000 3 .00 0 .000 90.1 2.2 0 0.5 00 0 .000 0.5 00 0 .000

WP

- 19

- LQ

- 029 1 .00 0 .000 3 .00 0 .000 40.7 0.9 00 0.5 00 0 .000 0.5 00 0 .000

WP

- 20

- LQ

- 031 1 .00 0 .000 3 .00 0 .000 68 1.7 0 0.5 00 0 .000 5 .00 0 .000

WP

- 21

- LQ

- 033 0.2 00 0.2 00 3 .00 0 .000 70 2.2 0 0.5 00 0 .000 0.5 00 0 .000

WP

- 11

- LQ

- 035 1 .00 0 .000 3 .00 0 .000 389 2.2 0 2 .00 0.3 00 0.5 00 0 .000

WP

- 05

- LQ

- 037 1 .00 0 .000 3 .00 0 .000 382 5.3 0 0.5 00 0 .000 0.5 00 0 .000

WP

- 04

- LQ

- 039 1 .00 0 .000 3 .00 0 .000 202 4.8 0 0.5 00 0 .000 1.6 0 0.2 00

WP

- 12

- LQ

- 041 1 .00 0 .000 3 .00 0 .000 156 3.5 0 0.5 00 0 .000 1.9 0 0.2 00

WP

- 11

- LQ

- 043 1 .00 0 .000 3 .00 0 .000 484 3.1 0 1.3 0 0.3 00 0.6 00 0.1 00

WP

- 10

- LQ

- 045 1 .00 0 .000 3 .00 0 .000 106 2 .00 0.5 00 0 .000 0.7 00 0.1 00

WP

- 14

- LQ

- 046 1 .00 0 .000 3 .00 0 .000 219 2.1 0 0.5 00 0 .000 0.5 00 0 .000

WP

- 01

- LQ

- 048 1 .00 0 .000 3 .00 0 .000 43.7 1 .00 0.2 00 0.2 00 0.5 00 0 .000

WP

- 10

- LQ

- 050 1 .00 0 .000 3 .00 0 .000 75.1 1.3 0 2 .00 0.2 00 0.5 00 0 .000

WP

- 14

- LQ

- 052 1 .00 0 .000 3 .00 0 .000 301 3.9 0 0.5 00 0 .000 0.7 00 0.2 00January 2015

F

- 33 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Liquids Analysis

Study ID Silicon

Result (ppm) Silicon

Error (ppm) Silver

Result (ppm) Silver

Error (ppm) Sodium

Result (ppm) Sodium

Error (ppm) Strontium

Result (ppm) Strontium

Error (ppm) Sulfur

Result (ppm) Sulfur

Error (ppm) Tanta lum

Result (ppm) Tanta lum

Error (ppm)

WT

- 04

- LQ

- 204 79.4 5.9 0 2 .00 0 .000 9,600 97 .0 294 0.4 00 2 .00 0 .000 14.8 0.4 00

WT

- 05

- LQ

- 206 853 11 .0 2 .00 0 .000 9,840 100 206 0.3 00 131 2.9 0 14.9 0.5 00

WT

- 13

- LQ

- 212 280 1.5 0 2 .00 0 .000 1,010 736 0.2 00 0.1 00 75.5 0.4 00 8.6 0 0.3 00

WT

- 14

- LQ

- 214 25.4 0.6 00 2 .00 0 .000 1,010 843 11.5 0.1 00 58.4 0.4 00 7.6 0 0.3 00

WT

- 17

- LQ

- 220 92.1 1.1 0 2 .00 0 .000 1,010 845 17.8 0.1 00 30.2 0.4 00 9.1 0 0.3 00

WT

- 11

- LQ

- 222 5.1 0 0 .000 2 .00 0 .000 19,600 170 1,160 1 .00 48.3 2.6 0 22.2 0.7 00

WT

- 15

- LQ

- 226 5.1 0 0 .000 2 .00 0 .000 7,370 59 .0 185 0.3 00 48.7 1.3 0 9.3 0 0.3 00

WT

- 09

- LQ

- 228 5.1 0 0 .000 2 .00 0 .000 17,200 170 876 0.8 00 2 .00 0 .000 16.9 0.7 00

WT

- 19

- LW

- 232 8,710 11 .0 2 .00 0 .000 2,920 34 .0 448 0.5 00 155 1.1 0 11.1 0.4 00

WT

- 25

- LQ

- 234 5.1 0 0 .000 2 .00 0 .000 4,210 43 .0 982 0.8 00 2 .00 0 .000 10.7 0.4 00

WT

- 06

- LQ

- 248 5.1 0 0 .000 2 .00 0 .000 4,350 45 .0 1,160 1 .00 2 .00 0 .000 11.2 0.4 00

WT

- 08

- LQ

- 240 5.1 0 0 .000 2 .00 0 .000 7,690 76 .0 1,670 1 .00 2 .00 0 .000 12.1 0.5 00

WT

- 16

- LQ

- 244 10.4 0.2 00 2 .00 0 .000 1,010 740 0.4 00 0.1 00 39.1 0.3 0 9.4 0 0.3 00

WT

- 20

- LQ

- 250 5,320 23 .0 2 .00 0 .000 12,800 130 4,380 3 .00 889 6 .00 27 .0 1 .00

WP

- 04

- LQ

- 014 5.1 0 0 .000 2 .00 0 .000 16,800 160 6,080 4 .00 2 .00 0 .000 40.9 1.3 0

WT

- 23

- LQ

- 256 215 2.4 0 2 .00 0 .000 1,910 28 .0 425 0.4 0 15.5 0.6 00 10.7 0.3 00

WT

- 21

- LQ

- 264 2,160 14 .0 2 .00 0 .000 10,900 110 2,500 2 .00 159 3.2 0 18.6 0.8 00

WT

- 24

- LQ

- 268 0.1 00 0 .000 2 .00 0 .000 9,450 95 .0 733 0.7 00 2 .00 0 .000 16.2 0.5 00

WT

- 22

- LQ

- 272 122 1.7 0 2 .00 0 .000 1,410 21 .0 223 0.3 00 67.1 0.6 00 10.8 0.3 00

WP

- 10

- LQ

- 015 5.1 0 0 .000 2 .00 0 .000 8,780 100 1,800 1 .00 2 .00 0 .000 23 .0 0.7 00

WT

- 01

- LQ

- 284 1,310 18 .0 2 .00 0 .000 15,800 160 1,160 1 .00 759 6.6 0 2.8 0 0.7 00

WT

- 02

- LQ

- 278 209 11 .0 2 .00 0 .000 14,600 140 872 0.8 00 192 4.3 0 13.7 0.7 00

WT

- 07

- LQ

- 276 236 3.1 0 2 .00 0 .000 2,900 35 .0 848 0.7 00 2 .00 0 .000 11.2 0.3 00

WT

- 03

- LQ

- 286 136 1.3 0 2 .00 0 .000 994 17 .0 1.9 0 0.1 00 1,420 1 .00 9.1 0 0.3 00

WP

- 06

- LQ

- 016 112 1 .00 2 .00 0 .000 1,010 720 0.5 00 0 .000 21.4 0.3 00 9.5 0 0.3 00

WT

- 10

- LQ

- 290 343 1.7 0 2 .00 0 .000 1,010 846 0.8 00 0.1 00 77.4 0.4 00 7 .00 0.3 00

WT

- 12

- LQ

- 294 134 1.2 0 2 .00 0 .000 1,140 18 .0 1.1 0 0.1 00 43.9 0.4 00 10.6 0.3 00

WP

- 06

- LQ

- 017 5.1 0 0 .000 2 .00 0 .000 12,800 140 1,090 1 .00 2 .00 0 .000 25.2 0.7 00

WP

- 09

- LQ

- 018 5.1 0 0 .000 2 .00 0 .000 18,400 180 3,350 2 .00 2 .00 0 .000 30.1 0.9 00

WP

- 08

- LQ

- 021 5.1 0 0 .000 2 .00 0 .000 21,600 210 3,380 2 .00 2 .00 0 .000 24.3 1 .00January 2015

F

- 34 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Liquids Analysis

Study ID Silicon

Result (ppm) Silicon

Error (ppm) Silver

Result (ppm) Silver

Error (ppm) Sodium

Result (ppm) Sodium

Error (ppm) Strontium

Result (ppm) Strontium

Error (ppm) Sulfur

Result (ppm) Sulfur

Error (ppm) Tanta lum

Result (ppm) Tanta lum

Error (ppm)

WP

- 12

- LQ

- 022 5.1 0 0 .000 2 .00 0 .000 7,970 80 .0 2,270 2 .00 2 .00 0 .000 22.5 0.7 00

WP

- 18

- LQ

- 024 5.1 0 0 .000 2 .00 0 .000 12,200 120 162 0.3 00 2 .00 0 .000 11.2 0.5 00

WP

- 19

- LQ

- 029 469 4.2 0 2 .00 0 .000 3,360 38 .0 31.3 0.1 00 399 1.4 0 9.4 0 0.3 00

WP

- 20

- LQ

- 031 5.1 0 0 .000 2 .00 0 .000 9,890 98 .0 64.3 0.2 00 2 .00 0 .000 12.1 0.4 00

WP

- 21

- LQ

- 033 5.1 0 0 .000 2 .00 0 .000 13,900 130 118 0.2 00 2 .00 0 .000 15.4 0.5 00

WP

- 11

- LQ

- 035 5,110 12 .0 2 .00 0 .000 8,030 58 .0 1,980 1 .00 2 .00 0 .000 1.1 0 0.1 00

WP

- 05

- LQ

- 037 5.1 0 0 .000 2 .00 0 .000 22,100 220 2,570 2 .00 2 .00 0 .000 28.7 0.9 00

WP

- 04

- LQ

- 039 5.1 0 0 .000 2 .00 0 .000 23,800 220 6,030 4 .00 2 .00 0 .000 31.4 1.2 0

WP

- 12

- LQ

- 041 5.1 0 0 .000 2 .00 0 .000 15,700 160 6,180 4 .00 2 .00 0 .000 29.2 1.2 0

WP

- 11

- LQ

- 043 5.1 0 0 .000 2 .00 0 .000 7,550 77 .0 2,190 2 .00 2 .00 0 .000 19.2 0.6 00

WP

- 10

- LQ

- 045 5.1 0 0 .000 2 .00 0 .000 8,980 89 .0 1,900 1 .00 2 .00 0 .000 16.8 0.6 00

WP

- 14

- LQ

- 046 5.1 0 0 .000 2 .00 0 .000 6,530 70 .0 862 0.7 00 2 .00 0 .000 13.2 0.4 00

WP

- 01

- LQ

- 048 682 6.6 0 2 .00 0 .000 4,570 46 .0 1,240 1 .00 2 .00 0 .000 12.8 0.4 00

WP

- 10

- LQ

- 050 5.1 0 0 .000 2 .00 0 .000 5,520 56 .0 1,450 1 .00 2 .00 0 .000 14.2 0.5 00

WP

- 14

- LQ

- 052 5.1 0 0 .000 2 .00 0 .000 14,700 160 3,780 3 .00 2 .00 0 .000 28.3 1 .00January 2015

F

- 35 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Liquids Analysis

Study ID Tellurium

Result (ppm) Tellurium

Error (ppm) Thallium

Result (ppm) Thallium

Error (ppm) Thorium

Result (ppm) Thorium

Error (ppm) Tin

Result (ppm) Tin

Error (ppm) Titanium

Result (ppm) Titanium

Error (ppm)

WT

- 04

- LQ

- 204 3 .00 0 .000 1.1 0 0.1 00 0.7 00 0.1 00 3 .00 0 .000 33 .0 0.5 00

WT

- 05

- LQ

- 206 3 .00 0 .000 0.9 00 0.1 00 0.6 00 0.1 00 3 .00 0 .000 62 .0 0.7 00

WT

- 13

- LQ

- 212 3 .00 0 .000 0.1 00 0.1 00 0.1 00 0.1 00 3 .00 0 .000 14.2 0.2 00

WT

- 14

- LQ

- 214 3 .00 0 .000 1 .00 0 .000 0.3 00 0.1 00 3 .00 0 .000 3.4 0 0.1 00

WT

- 17

- LQ

- 220 3 .00 0 .000 0.3 00 0.1 00 0.2 00 0.1 00 3 .00 0 .000 6.8 0 0.2 00

WT

- 11

- LQ

- 222 3 .00 0 .000 0.7 00 0.4 00 1 .00 0 .000 3 .00 0 .000 21 .0 2.1 0

WT

- 15

- LQ

- 226 3 .00 0 .000 0.7 0 0.1 00 0.6 0 0.1 00 3 .00 0 .000 5 .00 0.5 00

WT

- 09

- LQ

- 228 3 .00 0 .000 0.4 00 0.2 00 1 .00 0 .000 3 .00 0 .000 6.1 0 1 .00

WT

- 19

- LW

- 232 3 .00 0 .000 0.6 00 0.1 00 0.3 0 0.1 00 3 .00 0 .000 146 1.7 0

WT

- 25

- LQ

- 234 3 .00 0 .000 0.7 00 0.1 00 1 .00 0 .000 3 .00 0 .000 36 .0 1.7 0

WT

- 06

- LQ

- 248 3 .00 0 .000 1 .00 0.1 00 1 .00 0 .000 3 .00 0 .000 34.8 1.6 0

WT

- 08

- LQ

- 240 3 .00 0 .000 1 .00 0.1 00 1 .00 0 .000 3 .00 0 .000 46.8 2.1 0

WT

- 16

- LQ

- 244 3 .00 0 .000 1 .00 0 .000 1 .00 0 .000 3 .00 0 .000 2.7 0 0.1 00

WT

- 20

- LQ

- 250 3 .00 0 .000 1.9 0 0.3 00 1 .00 0 .000 4.2 0 0.1 00 277 8.1 0

WP

- 04

- LQ

- 014 3 .00 0 .000 4.5 0 0.3 00 1 .00 0 .000 7.3 0 0.2 00 78.3 8.2 0

WT

- 23

- LQ

- 256 3 .00 0 .000 0.6 00 0.1 00 0.2 0 0.2 00 3 .00 0 .000 9.7 0 0.2 00

WT

- 21

- LQ

- 264 3 .00 0 .000 1.2 00 0.2 00 1 .00 0 .000 3 .00 0 .000 113 3.2 0

WT

- 24

- LQ

- 268 3 .00 0 .000 0.8 00 0.1 00 0.3 0 0.2 00 3 .00 0 .000 14.9 1 .00

WT

- 22

- LQ

- 272 3 .00 0 .000 0.2 00 0.1 00 0.2 0 0.2 00 3 .00 0 .000 2.9 0 0.4 00

WP

- 10

- LQ

- 015 3 .00 0 .000 2.1 0 0.2 00 1 .00 0 .000 3 .00 0 .000 101 4 .00

WT

- 01

- LQ

- 284 3 .00 0 .000 0.4 00 0.1 00 1 .00 0 .000 3 .00 0 .000 59.6 2 .00

WT

- 02

- LQ

- 278 3 .00 0 .000 0.5 00 0.1 00 1 .00 0 .000 3 .00 0 .000 67.2 1.7 0

WT

- 07

- LQ

- 276 3 .00 0 .000 1.1 0 0.1 00 1 .00 0 .000 3 .00 0 .000 6.5 0 0.8 00

WT

- 03

- LQ

- 286 3 .00 0 .000 1 .00 0 .00 0.4 0 0.1 00 3 .00 0 .000 3.5 0 0.1 00

WP

- 06

- LQ

- 016 3 .00 0 .000 0.3 00 0.1 00 0.4 0 0.1 00 3 .00 0 .000 3 .00 0.1 00

WT

- 10

- LQ

- 290 3 .00 0 .000 0.5 00 0.1 00 1 .00 0 .000 3 .00 0 .000 363 1 .00

WT

- 12

- LQ

- 294 3 .00 0 .000 0.2 00 0.2 00 0.2 00 0.1 00 3 .00 0 .000 3.8 0 0.2 00

WP

- 06

- LQ

- 017 3 .00 0 .000 0.8 00 0.1 00 1 .00 0 .000 3 .00 0 .000 19.1 0.5 00

WP

- 09

- LQ

- 018 3 .00 0 .000 0.7 00 0.1 00 1 .00 0 .000 3 .00 0 .000 5.5 0 1 .00

WP

- 08

- LQ

- 021 3 .00 0 .000 1.7 0 0.2 00 1 .00 0 .000 3 .00 0 .000 5.9 0 1.2 0January 2015

F

- 36 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Liquids Analysis

Study ID Tellurium

Result (ppm) Tellurium

Error (ppm) Thallium

Result (ppm) Thallium

Error (ppm) Thorium

Result (ppm) Thorium

Error (ppm) Tin

Result (ppm) Tin

Error (ppm) Titanium

Result (ppm) Titanium

Error (ppm)

WP

- 12

- LQ

- 022 3 .00 0 .000 1.2 0 0.2 00 1 .00 0 .000 3 .00 0 .000 95.6 3.2 0

WP

- 18

- LQ

- 024 3 .00 0 .000 1 .00 0 .000 0.4 00 0.1 00 3 .00 0 .000 5.7 0 0.2 00

WP

- 19

- LQ

- 029 3 .00 0 .000 0.2 00 0.2 00 0.5 00 0.1 00 3 .00 0 .000 4.6 0 0.1 00

WP

- 20

- LQ

- 031 3 .00 0 .000 0.5 00 0.1 00 0.9 00 0.1 00 3 .00 0 .000 7.4 0 0.2 00

WP

- 21

- LQ

- 033 3 .00 0 .000 0.3 00 0.1 00 0.8 00 0.1 00 3 .00 0 .000 13.1 0.4 00

WP

- 11

- LQ

- 035 3 .00 0 .000 1.1 0 0.1 00 1 .00 0 .000 3 .00 0 .000 11.9 0.7 00

WP

- 05

- LQ

- 037 3 .00 0 .000 1.4 0 0.2 00 1 .00 0 .000 3 .00 0 .000 25.3 0.7 00

WP

- 04

- LQ

- 039 3 .00 0 .000 2.7 0 0.3 00 1 .00 0 .000 3 .00 0 .000 262 8.1 0

WP

- 12

- LQ

- 041 3 .00 0 .000 2.5 0 0.3 00 1 .00 0 .000 3 .00 0 .000 55.9 6.6 0

WP

- 11

- LQ

- 043 3 .00 0 .000 1.2 0 0.1 00 1 .00 0 .000 3 .00 0 .000 10.2 1.3 0

WP

- 10

- LQ

- 045 3 .00 0 .000 1.3 0 0.2 00 1 .00 0 .000 3 .00 0 .000 40.4 4.1 0

WP

- 14

- LQ

- 046 3 .00 0 .000 0.9 00 0.1 00 1 .00 0 .000 3 .00 0 .000 7 .00 0.2 00

WP

- 01

- LQ

- 048 3 .00 0 .000 0.5 00 0.1 00 1 .00 0 .000 3 .00 0 .000 24.6 1.9 0

WP

- 10

- LQ

- 050 3 .00 0 .000 0.9 00 0.1 00 1 .00 0 .000 3 .00 0 .000 97.2 2.8 0

WP

- 14

- LQ

- 052 3 .00 0 .000 2 .00 0.2 00 1 .00 0 .000 3 .00 0 .000 102 3.5 0January 2015

F

- 37 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Liquids Analysis

Study ID Tungsten

Result (ppm) Tungsten

Error (ppm) Uranium

Result (ppm) Uranium

Error (ppm) Vanadium

Result (ppm) Vanadium

Error (ppm) Yttrium

Result (ppm) Yttrium

Error (ppm) Zinc

Result (ppm) Zinc

Error (ppm)

WT

- 04

- LQ

- 204 0.5 00 0.1 00 1 .00 0 .000 2.3 0 0.2 00 0.6 00 0.1 00 1.3 0 0.1 00

WT

- 05

- LQ

- 206 0.5 00 0.2 00 1 .00 0 .000 7.8 0 0.3 00 0.6 00 0.1 00 2.1 0 0.1 00

WT

- 13

- LQ

- 212 1 .00 0 .000 0.1 00 0.1 00 1.1 0 0.1 00 0.3 00 0.1 00 0.6 00 0.1 00

WT

- 14

- LQ

- 214 0.3 00 0.2 00 0.4 00 0.1 00 1 .00 0.1 00 0.4 00 0.1 00 1.2 0 0.1 00

WT

- 17

- LQ

- 220 0 .000 1 .00 1 .00 0 .000 1 .00 0 .000 0.4 00 0.1 00 1.2 0 0.1 00

WT

- 11

- LQ

- 222 1 .00 0 .000 1.5 0 0.1 00 19.4 0.9 00 0.9 00 0.1 00 2.1 0 0.2 00

WT

- 15

- LQ

- 226 1 .00 0 .000 0.6 00 0.1 00 1.4 0 0.2 00 0.3 00 0.1 00 0.7 00 0.1 00

WT

- 09

- LQ

- 228 0.4 00 0.1 00 0.4 00 0.1 00 2.6 0.3 00 0.9 00 0.1 00 1.8 0 0.2 00

WT

- 19

- LW

- 232 0.6 00 0.1 00 5.2 0 0.1 00 13.2 0.7 00 0.6 00 0.1 00 2.8 0 0.1 00

WT

- 25

- LQ

- 234 0.4 00 0.2 00 9.1 0 0.2 00 6.5 0 0.6 00 1.2 0 0.1 00 0.5 00 0.1 00

WT

- 06

- LQ

- 248 1 .00 0 .000 10.7 0.2 00 6.8 0 0.6 00 1.5 0 0.1 00 1.1 0 0.1 00

WT

- 08

- LQ

- 240 1 .00 0 .000 14 .0 0.3 00 8.6 0 0.8 00 1.9 0 0.1 00 1.4 0 0.1 00

WT

- 16

- LQ

- 244 1 .00 0 .000 1 .00 0 .000 0.9 00 0.1 00 0.3 00 0.1 00 1.2 0 0.1 00

WT

- 20

- LQ

- 250 1.2 0 0 .00 25.1 0.5 00 22.4 3 .00 5.4 0 0.2 00 11.2 0.3 00

WP

- 04

- LQ

- 014 1.5 0 0.4 00 21.7 0.6 00 12.6 2.9 0 8.3 0 0.2 00 6.8 0 0.4 00

WT

- 23

- LQ

- 256 1 .00 0 .000 4.9 0 0.1 00 2.1 0 0.1 00 0.4 00 0.1 00 1.2 0 0.1 00

WT

- 21

- LQ

- 264 1 .00 0 .000 17.3 0.3 00 13.6 1.2 0 2.7 0 0.1 00 14.7 0.3 00

WT

- 24

- LQ

- 268 0.5 00 0 .000 4 .00 0.1 00 3.8 0 0.3 00 0.9 00 0.1 00 1.5 0 0.1 00

WT

- 22

- LQ

- 272 1 .00 0 .000 2.8 0 0.1 00 0.8 00 0.1 00 0.3 00 0.1 00 0.8 00 0.1 00

WP

- 10

- LQ

- 015 1.1 0 0.2 00 17.8 0.3 00 14.4 1.4 0 2.3 0 0.1 00 2 .00 0.2 00

WT

- 01

- LQ

- 284 1 .00 0 .000 2.3 0 0.1 00 9.4 0 0.7 00 0.8 00 0.1 00 2.4 0 0.2 00

WT

- 02

- LQ

- 278 1 .00 0 .000 0.7 00 0.1 00 31.9 0.8 00 0.8 00 0.1 00 4.1 0 0.2 00

WT

- 07

- LQ

- 276 0.4 00 0.1 00 9.4 0 0.2 00 1.9 0 0.3 00 0.9 00 0.1 00 0.8 00 0.1 00

WT

- 03

- LQ

- 286 1 .00 0 .000 0.3 00 0.1 00 1.3 0 0.1 00 0.5 00 0.1 00 2.9 0 0.1 00

WP

- 06

- LQ

- 016 1 .00 0 .000 0.4 00 0.1 00 1.7 0 0.1 00 0.4 00 0.1 00 0.4 00 0.1 00

WT

- 10

- LQ

- 290 0.6 00 0.1 00 1 .00 0 .000 0.5 00 0.2 00 0.4 00 0.1 00 2.2 0 0.1 00

WT

- 12

- LQ

- 294 0.3 00 0.1 00 0.3 00 0.1 00 0.5 00 0.1 00 0.4 00 0.1 00 0.8 00 0.1 00

WP

- 06

- LQ

- 017 0.6 00 0.2 00 5.6 0 0.2 00 5.1 0 0.3 00 1 .00 0.1 00 1.8 0 0.2 00

WP

- 09

- LQ

- 018 1 .00 0 .000 10.4 0.3 00 2.9 0 0.3 00 3.3 0 0.1 00 1.8 0 0.3 00

WP

- 08

- LQ

- 021 0.9 0 0.3 00 9.3 0 0.3 00 3 .00 0.4 00 3.4 0 0.1 00 1.8 0 0.3 00January 2015

F

- 38 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Liquids Analysis

Study ID Tungsten

Result (ppm) Tungsten

Error (ppm) Uranium

Result (ppm) Uranium

Error (ppm) Vanadium

Result (ppm) Vanadium

Error (ppm) Yttrium

Result (ppm) Yttrium

Error (ppm) Zinc

Result (ppm) Zinc

Error (ppm)

WP

- 12

- LQ

- 022 1 .00 0 ..000 18 .0 0.3 00 15.1 1.2 0 2.7 0 0.1 00 1.9 0 0.2 00

WP

- 18

- LQ

- 024 0.5 00 0.2 00 1 .00 0 .000 2.3 0 0.1 00 0.6 00 0.1 00 2.4 0 0.1 00

WP

- 19

- LQ

- 029 0.3 00 0.2 00 1 .00 0 .000 1.6 0 0.1 00 0.3 00 0.1 00 1.6 0 0.1 00

WP

- 20

- LQ

- 031 1 .00 0 .000 1 .00 0 .000 2 .00 0.1 00 0.4 00 0.1 00 1.4 0 0.1 00

WP

- 21

- LQ

- 033 0.6 00 0.3 00 1 .00 0 .000 4.2 0 0.2 00 0.6 00 0.1 00 2.9 0 0.1 00

WP

- 11

- LQ

- 035 1 .00 0 .000 17.1 0.3 00 2.8 0 0.3 00 3.2 0 0.1 00 0.8 00 0.1 00

WP

- 05

- LQ

- 037 0.6 00 0.2 00 11.2 0.3 00 5.4 0 0.3 00 2.7 0 0.1 00 2.3 0 0.3 00

WP

- 04

- LQ

- 039 1.4 0 0.6 00 30.7 0.6 00 29.5 2.9 0 7.6 0 0.2 00 1.7 0 0.3 00

WP

- 12

- LQ

- 041 1.4 0 0.5 00 24.3 0.6 00 9.4 0 2.2 0 7.5 0 0.2 00 2.1 0 0.3 00

WP

- 11

- LQ

- 043 0.1 00 0.4 00 19.7 0.3 00 4 .00 0.4 00 2.6 0 0.1 00 1.2 0 0.2 00

WP

- 10

- LQ

- 045 0.6 00 0.2 00 15.1 0.3 00 9.9 0 1.5 0 2 .00 0.1 00 1.3 0 0.2 00

WP

- 14

- LQ

- 046 1 .00 0 .000 6.3 0 0.1 00 0.9 00 0.1 00 0.8 0 0.1 00 0.7 00 0.1 00

WP

- 01

- LQ

- 048 0.4 0 .000 12 .0 0.2 00 6.1 0 0.7 00 1.8 0 0.1 00 1.2 0 0.1 00

WP

- 10

- LQ

- 050 1 .00 0 .000 11.9 0.2 00 25.8 1.2 0 1.8 0 0.1 00 0.8 00 0.1 00

WP

- 14

- LQ

- 052 1.1 0.4 00 21.1 0.4 00 18.7 1.3 0 3.7 0 0.1 00 1.4 0 0.2 00January 2015

F

- 39 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Liquids Analysis

Study ID Zirconium

Result (ppm) Zirconium

Error (ppm)

WT

- 04

- LQ

- 204 1 .00 0 .000

WT

- 05

- LQ

- 206 1 .00 0 .000

WT

- 13

- LQ

- 212 0.4 00 0.4 00

WT

- 14

- LQ

- 214 1 .00 0 .000

WT

- 17

- LQ

- 220 1 .00 0 .000

WT

- 11

- LQ

- 222 1 .00 0 .000

WT

- 15

- LQ

- 226 1 .00 0 .000

WT

- 09

- LQ

- 228 1 .00 0 .000

WT

- 19

- LW

- 232 1 .00 0 .000

WT

- 25

- LQ

- 234 1 .00 0 .000

WT

- 06

- LQ

- 248 1 .00 0 .000

WT

- 08

- LQ

- 240 1 .00 0 .000

WT

- 16

- LQ

- 244 0.6 00 0.2 00

WT

- 20

- LQ

- 250 1 .00 0 .000

WP

- 04

- LQ

- 014 1 .00 0 .000

WT

- 23

- LQ

- 256 1 .00 0 .000

WT

- 21

- LQ

- 264 1 .00 0 .000

WT

- 24

- LQ

- 268 1 .00 0 .000

WT

- 22

- LQ

- 272 1 .00 0 .000

WP

- 10

- LQ

- 015 1 .00 0 .000

WT

- 01

- LQ

- 284 1 .00 0 .000

WT

- 02

- LQ

- 278 1 .00 0 .000

WT

- 07

- LQ

- 276 1 .00 0 .000

WT

- 03

- LQ

- 286 1 .00 0 .000

WP

- 06

- LQ

- 016 0.5 00 0.2 00

WT

- 10

- LQ

- 290 1 .00 0 .000

WT

- 12

- LQ

- 294 1 .00 0 .000

WP

- 06

- LQ

- 017 1 .00 0 .000

WP

- 09

- LQ

- 018 1 .00 0 .000

WP

- 08

- LQ

- 021 1 .00 0 .000January 2015

F

- 40 PA DEP TENORM Study Report

– Appendix

F

Rev. 0 

### Appendix F

– XRF Liquids Analysis

Study ID Zirconium

Result (ppm) Zirconium

Error (ppm)

WP

- 12

- LQ

- 022 1 .00 0 .000

WP

- 18

- LQ

- 024 1 .00 0 .000

WP

- 19

- LQ

- 029 1 .00 0 .000

WP

- 20

- LQ

- 031 1 .00 0 .000

WP

- 21

- LQ

- 033 1 .00 0 .000

WP

- 11

- LQ

- 035 1 .00 0 .000

WP

- 05

- LQ

- 037 1 .00 0 .000

WP

- 04

- LQ

- 039 1 .00 0 .000

WP

- 12

- LQ

- 041 1 .00 0 .000

WP

- 11

- LQ

- 043 1 .00 0 .000

WP

- 10

- LQ

- 045 1 .00 0 .000

WP

- 14

- LQ

- 046 1 .00 0 .000

WP

- 01

- LQ

- 048 1 .00 0 .000

WP

- 10

- LQ

- 050 1 .00 0 .000

WP

- 14

- LQ

- 052 1 .00 0 .000