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e-mail: aal@aal-inc.com  www.aal-inc.com

AMERICAN ANALYTICAL LABORATORIES, INC

 ANALYTICAL SCIENCES  AKRON OPERATIONS 

IMSAMET of Arizona

RE: Subpart RRR 114 Request

Goodyear, AZ 85338

3829 S. Estrella Parkway

Gary C. Barnett

American Analytical Laboratories, Inc received a sample(s) on 19-Aug-10 10:00 for the analyses 

presented in the following report.

Please promptly take the time to carefully review this report and call us if you have any questions or 

additional needs. Delays may make it more difficult for us to answer your questions.

We thank you for using our services.

Sincerely, 

Richard E. Moore

American Analytical Laboratories, Inc.

Work Order: 1008103

01-Sep-10 12:50
AMERICAN ANALYTICAL LABORATORIES, INC

 ANALYTICAL SCIENCES  AKRON OPERATIONS 

Project:

Project Number:

Project Manager:

Reported:

IMSAMET of Arizona

3829 S. Estrella Parkway Subpart RRR 114 Request

Gary C. Barnett

Subpart RRR 114 Request

Goodyear, AZ 85338 01-Sep-10 12:50

Sample ID Laboratory ID Matrix Date Sampled

ANALYTICAL REPORT FOR SAMPLES

Date Received

Rotary Baghouse #1-Particulate 1008103-01 Solid 17-Aug-10 09:15 19-Aug-10 10:00

Clean Lime Sample 1008103-02 Solid 17-Aug-10 09:22 19-Aug-10 10:00

Narrative:

American Analytical Laboratories, Inc. - Akron The results in this report apply to the samples analyzed in accordance with the chain of 

custody document. This analytical report must be reproduced in its entirety.
AMERICAN ANALYTICAL LABORATORIES, INC

 ANALYTICAL SCIENCES  AKRON OPERATIONS 

Project:

Project Number:

Project Manager:

Reported:

IMSAMET of Arizona

3829 S. Estrella Parkway Subpart RRR 114 Request

Gary C. Barnett

Subpart RRR 114 Request

Goodyear, AZ 85338 01-Sep-10 12:50

Analyte Result Limt Batch

Reporting

Units Dilution Prepared Analyzed Method Analyst 

Rotary Baghouse #1-Particulate

1008103-01 (Solid) 17-Aug-10 09:15

Date Sampled

Qualifier

Metals

Arsenic 1.6 0.97 mg/kg 20 A008150 26-Aug-10 31-Aug-10 SW 846 6020 AK

Beryllium 9.8 0.97 " " " " " " AK

Cadmium 69 0.97 " " " " 30-Aug-10 " AK

Cobalt 5.8 0.97 " " " " " " AK

Chromium 540 25 " 500 " " 30-Aug-10 SW846 6020 AK

SW846 

7471A

Mercury 0.03 0.02 " 1 A008163 30-Aug-10 31-Aug-10 AK

Manganese 1100 25 " 500 A008150 26-Aug-10 30-Aug-10 SW846 6020 AK

Nickel 200 2.5 " 50 " " 30-Aug-10 " AK

Lead 23 0.97 " 20 " " 30-Aug-10 SW 846 6020 AK

Antimony 8.2 0.97 " " " " 30-Aug-10 " AK

Selenium BRL 0.97 " " " " " " AK

Wet Chemistry

BRL SW846 

7196A

Hexavalent Chromium 0.50 mg/kg 1 A008147 25-Aug-10 25-Aug-10 RLL

% Solids 98.5 % " A008138 24-Aug-10 24-Aug-10 EPA 160.3 ROZ

American Analytical Laboratories, Inc. - Akron The results in this report apply to the samples analyzed in accordance with the chain of 

custody document. This analytical report must be reproduced in its entirety.
AMERICAN ANALYTICAL LABORATORIES, INC

 ANALYTICAL SCIENCES  AKRON OPERATIONS 

Project:

Project Number:

Project Manager:

Reported:

IMSAMET of Arizona

3829 S. Estrella Parkway Subpart RRR 114 Request

Gary C. Barnett

Subpart RRR 114 Request

Goodyear, AZ 85338 01-Sep-10 12:50

Analyte Result Limt Batch

Reporting

Units Dilution Prepared Analyzed Method Analyst 

Clean Lime Sample

1008103-02 (Solid) 17-Aug-10 09:22

Date Sampled

Qualifier

Metals

Arsenic 6.6 0.93 mg/kg 20 A008150 26-Aug-10 31-Aug-10 SW 846 6020 AK

Beryllium BRL 0.93 " " " " " " AK

Cadmium BRL 0.93 " " " " 30-Aug-10 " AK

Cobalt 1.2 0.93 " " " " " " AK

Chromium 3.0 1.0 " " " " 30-Aug-10 SW846 6020 AK

BRL SW846 

7471A

Mercury 0.02 " 1 A008163 30-Aug-10 31-Aug-10 AK

Manganese 29 2.5 " 50 A008150 26-Aug-10 30-Aug-10 SW846 6020 AK

Nickel 18 1.0 " 20 " " 30-Aug-10 " AK

Lead 1.4 0.93 " " " " 30-Aug-10 SW 846 6020 AK

Antimony BRL 0.93 " " " " 30-Aug-10 " AK

Selenium BRL 0.93 " " " " " " AK

Wet Chemistry

SW846 

7196A

Hexavalent Chromium 0.74 0.50 mg/kg 1 A008147 25-Aug-10 25-Aug-10 RLL

% Solids 101 % " A008138 24-Aug-10 24-Aug-10 EPA 160.3 ROZ

American Analytical Laboratories, Inc. - Akron The results in this report apply to the samples analyzed in accordance with the chain of 

custody document. This analytical report must be reproduced in its entirety.
AMERICAN ANALYTICAL LABORATORIES, INC

 ANALYTICAL SCIENCES  AKRON OPERATIONS 

Project:

Project Number:

Project Manager:

Reported:

IMSAMET of Arizona

3829 S. Estrella Parkway Subpart RRR 114 Request

Gary C. Barnett

Subpart RRR 114 Request

Goodyear, AZ 85338 01-Sep-10 12:50

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

 Analyte Limit Analyst 

Metals - Quality Control

Qualifier

Batch A008150 - EPA 3050 Modified

Blank (A008150-BLK1) Prepared: 26-Aug-10 Analyzed: 30-Aug-10

Antimony BRL 1.0 mg/kg AK

Selenium BRL 1.0 " AK

Nickel BRL 1.0 " AK

Lead BRL 1.0 " AK

Chromium BRL 1.0 " AK

Manganese BRL 2.5 " AK

Cobalt BRL 1.0 " AK

Cadmium BRL 1.0 " AK

Beryllium BRL 1.0 " AK

Arsenic BRL 1.0 " AK

LCS (A008150-BS1) Prepared: 26-Aug-10 Analyzed: 30-Aug-10

Cadmium 47 1.0 mg/kg 50.0 94.3 80-120 AK

Beryllium 46 1.0 " 50.0 91.3 80-120 AK

Selenium 48 1.0 " 50.0 96.4 80-120 AK

Chromium 46 1.0 " 50.0 91.9 80-120 AK

Manganese 50 2.5 " 50.0 99.3 80-120 AK

Arsenic 46 1.0 " 50.0 92.7 0-120 AK

Nickel 46 1.0 " 50.0 92.4 80-120 AK

Cobalt 47 1.0 " 50.0 94.2 80-120 AK

Lead 47 1.0 " 50.0 93.2 80-120 AK

Antimony 49 1.0 " 50.0 98.4 80-120 AK

LCS Dup (A008150-BSD1) Prepared: 26-Aug-10 Analyzed: 30-Aug-10

Cadmium 46 1.0 mg/kg 50.0 92.4 80-120 2.06 20 AK

Arsenic 47 1.0 " 50.0 93.1 0-120 0.353 20 AK

Chromium 46 1.0 " 50.0 91.7 80-120 0.224 20 AK

Manganese 50 2.5 " 50.0 99.3 80-120 0.0302 20 AK

Beryllium 45 1.0 " 50.0 90.7 80-120 0.660 20 AK

Selenium 49 1.0 " 50.0 97.0 80-120 0.612 20 AK

Cobalt 47 1.0 " 50.0 93.1 80-120 1.11 25 AK

Nickel 46 1.0 " 50.0 92.9 80-120 0.507 20 AK

Lead 46 1.0 " 50.0 92.4 80-120 0.851 20 AK

Antimony 50 1.0 " 50.0 99.6 80-120 1.22 20 AK

American Analytical Laboratories, Inc. - Akron The results in this report apply to the samples analyzed in accordance with the chain of 

custody document. This analytical report must be reproduced in its entirety.
AMERICAN ANALYTICAL LABORATORIES, INC

 ANALYTICAL SCIENCES  AKRON OPERATIONS 

Project:

Project Number:

Project Manager:

Reported:

IMSAMET of Arizona

3829 S. Estrella Parkway Subpart RRR 114 Request

Gary C. Barnett

Subpart RRR 114 Request

Goodyear, AZ 85338 01-Sep-10 12:50

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

 Analyte Limit Analyst 

Metals - Quality Control

Qualifier

Batch A008150 - EPA 3050 Modified

Duplicate (A008150-DUP1) Source: 1008099-01 Prepared: 26-Aug-10 Analyzed: 30-Aug-10

Cobalt BRL 0.97 mg/kg BRL 20 AK

Chromium 5.3 1.0 " 4.5 16.4 20 AK

Antimony BRL 0.97 " BRL 20 AK

Beryllium BRL 0.97 " BRL 20 AK

Selenium BRL 0.97 " BRL 20 AK

Arsenic BRL 0.97 " BRL 20 AK

Cadmium 8.8 0.97 " 8.6 2.80 20 AK

Lead 2.1 0.97 " 2.0 5.20 20 AK

Nickel 14 1.0 " 11 26.6 20 AK

Manganese 66 2.5 " 63 4.09 20 AK

Matrix Spike (A008150-MS1) Source: 1008099-01 Prepared: 26-Aug-10 Analyzed: 31-Aug-10

Beryllium 43 0.98 mg/kg 49.0 BRL 88.7 80-120 AK

Lead 51 0.98 " 49.0 2.0 99.7 80-120 AK

Cadmium 57 0.98 " 49.0 8.6 98.8 80-120 AK

Cobalt 49 0.98 " 49.0 BRL 99.5 80-120 AK

Chromium 52 1.0 " 49.0 4.5 97.7 80-120 AK

Manganese 110 2.5 " 49.0 63 91.2 80-120 AK

Antimony 51 0.98 " 49.0 BRL 104 80-120 AK

Selenium 44 0.98 " 49.0 BRL 89.1 80-120 AK

Arsenic 42 0.98 " 49.0 BRL 86.7 80-120 AK

Nickel 58 1.0 " 49.0 11 96.5 80-120 AK

Matrix Spike Dup (A008150-MSD1) Source: 1008099-01 Prepared: 26-Aug-10 Analyzed: 31-Aug-10

Arsenic 42 0.98 mg/kg 49.0 BRL 86.0 80-120 0.879 20 AK

Selenium 42 0.98 " 49.0 BRL 85.0 80-120 4.81 25 AK

Antimony 48 0.98 " 49.0 BRL 97.2 80-120 7.02 20 AK

Nickel 55 1.0 " 49.0 11 90.1 80-120 5.61 20 AK

Cadmium 53 0.98 " 49.0 8.6 91.5 80-120 6.53 20 AK

Chromium 50 1.0 " 49.0 4.5 92.0 80-120 5.59 20 AK

Manganese 110 2.5 " 49.0 63 88.5 80-120 1.29 20 AK

Beryllium 41 0.98 " 49.0 BRL 83.1 80-120 6.59 20 AK

Cobalt 46 0.98 " 49.0 BRL 93.1 80-120 6.65 20 AK

Lead 48 0.98 " 49.0 2.0 93.2 80-120 6.59 20 AK

American Analytical Laboratories, Inc. - Akron The results in this report apply to the samples analyzed in accordance with the chain of 

custody document. This analytical report must be reproduced in its entirety.
AMERICAN ANALYTICAL LABORATORIES, INC

 ANALYTICAL SCIENCES  AKRON OPERATIONS 

Project:

Project Number:

Project Manager:

Reported:

IMSAMET of Arizona

3829 S. Estrella Parkway Subpart RRR 114 Request

Gary C. Barnett

Subpart RRR 114 Request

Goodyear, AZ 85338 01-Sep-10 12:50

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

 Analyte Limit Analyst 

Metals - Quality Control

Qualifier

Batch A008150 - EPA 3050 Modified

Matrix Spike Dup (A008150-MSD1) Source: 1008099-01 Prepared: 26-Aug-10 Analyzed: 30-Aug-10

Batch A008163 - SW846 7471A

Blank (A008163-BLK1) Prepared: 30-Aug-10 Analyzed: 31-Aug-10

Mercury BRL 0.02 mg/kg AK

LCS (A008163-BS1) Prepared: 30-Aug-10 Analyzed: 31-Aug-10

Mercury 0.14 0.02 mg/kg 0.167 85.3 78-122 AK

LCS Dup (A008163-BSD1) Prepared: 30-Aug-10 Analyzed: 31-Aug-10

Mercury 0.14 0.02 mg/kg 0.167 84.0 78-122 1.54 20 AK

Duplicate (A008163-DUP1) Source: 1008100-01 Prepared: 30-Aug-10 Analyzed: 31-Aug-10

Mercury 0.68 0.03 mg/kg 0.63 6.76 20 AK

Post Spike (A008163-PS1) Source: 1008100-01 Prepared: 30-Aug-10 Analyzed: 31-Aug-10

Mercury 0.96 0.03 mg/kg 0.303 0.63 108 70-130 AK

Post Spike (A008163-PS2) Source: 1008100-01 Prepared: 30-Aug-10 Analyzed: 31-Aug-10

Mercury 0.97 0.03 mg/kg 0.303 0.63 109 70-130 AK

American Analytical Laboratories, Inc. - Akron The results in this report apply to the samples analyzed in accordance with the chain of 

custody document. This analytical report must be reproduced in its entirety.
AMERICAN ANALYTICAL LABORATORIES, INC

 ANALYTICAL SCIENCES  AKRON OPERATIONS 

Project:

Project Number:

Project Manager:

Reported:

IMSAMET of Arizona

3829 S. Estrella Parkway Subpart RRR 114 Request

Gary C. Barnett

Subpart RRR 114 Request

Goodyear, AZ 85338 01-Sep-10 12:50

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

 Analyte Limit Analyst 

Wet Chemistry - Quality Control

Qualifier

Batch A008147 - Alkaline Prep

Blank (A008147-BLK1) Prepared & Analyzed: 25-Aug-10

Hexavalent Chromium BRL 0.50 mg/kg RLL

LCS (A008147-BS1) Prepared & Analyzed: 25-Aug-10

Hexavalent Chromium 9.7 0.50 mg/kg 10.0 97.3 90-110 RLL

Duplicate (A008147-DUP1) Source: 1008100-01 Prepared & Analyzed: 25-Aug-10

Hexavalent Chromium BRL 0.50 mg/kg BRL 10 RLL

Matrix Spike (A008147-MS1) Source: 1008102-01 Prepared & Analyzed: 25-Aug-10

Hexavalent Chromium 9.8 0.50 mg/kg 10.0 BRL 98.2 90-110 RLL

American Analytical Laboratories, Inc. - Akron The results in this report apply to the samples analyzed in accordance with the chain of 

custody document. This analytical report must be reproduced in its entirety.
AMERICAN ANALYTICAL LABORATORIES, INC

 ANALYTICAL SCIENCES  AKRON OPERATIONS 

Project:

Project Number:

Project Manager:

Reported:

IMSAMET of Arizona

3829 S. Estrella Parkway Subpart RRR 114 Request

Gary C. Barnett

Subpart RRR 114 Request

Goodyear, AZ 85338 01-Sep-10 12:50

Notes and Definitions 

Sample results reported on a dry weight basis

RPD Relative Percent Difference

dry

NR Not Reported

BRL Analyte NOT DETECTED at or above the reporting limit

DET Analyte DETECTED

Reporting Limit - also the lower limit of quantitation (LLOQ). This value

 changes if the standard dilution or concentration of the sample is deviated from

 during sample preparation/analysis. Often it is the lowest linear standard for 

 applicable methods.

American Analytical Laboratories, Inc. - Akron The results in this report apply to the samples analyzed in accordance with the chain of 

custody document. This analytical report must be reproduced in its entirety.