### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being Fields that are highlighted in down boxes, included. Gray fields are

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1 03140 PPL Brunner Island 031A/032 bitum inousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte 03140 PPL Brunner Island 031A/032 As Received Higher Heating Value 03140 PPL Brunner Island 031A/032 As Received % Moisture 03140 PPL Brunner Island 031A/032 As Received % Ash 03140 PPL Brunner Island 031A/032 As Received % Sulfur 03140 PPL Brunner Island 031A/032 Dry

basis Higher Heating Value 03140 PPL Brunner Island 031A/032 Dry

basis % Ash 03140 PPL Brunner Island 031A/032 Dry

basis % Sulfur 03140 PPL Brunner Island 031A/032 Dry

basis Antim ony 03140 PPL Brunner Island 031A/032 Dry

basis Arsenic 03140 PPL Brunner Island 031A/032 Dry

basis Bery llium 03140 PPL Brunner Island 031A/032 Dry

basis Cadmium 03140 PPL Brunner Island 031A/032 Dry

basis Chlorine 03140 PPL Brunner Island 031A/032 Dry

basis Chromium 03140 PPL Brunner Island 031A/032 Dry

basis Cobalt 03140 PPL Brunner Island 031A/032 Dry

basis Fluorine 03140 PPL Brunner Island 031A/032 Dry

basis Lead 03140 PPL Brunner Island 031A/032 Dry

basis Manganese 03140 PPL Brunner Island 031A/032 Dry

basis Mercury 03140 PPL Brunner Island 031A/032 Dry

basis Nickel 03140 PPL Brunner Island 031A/032 Dry

basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) ASTM D-5865 ASTM D-3173 ASTM D-5142 ASTM D-4239 Method B ASTM D-5865 ASTM D-5142 ASTM D-4239 Method B ASTM D-3683/D-3684/D-4606M ASTM D-3683/D-3684/D-4606M ASTM D-3683/D-3684/D-4606M ASTM D-3683/D-3684/D-4606M ASTM D-3683/D-3684/D-4606M ASTM D-3683/D-3684/D-4606M ASTM D-3683/D-3684/D-4606M ASTM D-3761 ASTM D-3683/D-3684/D-4606M ASTM D-3683/D-3684/D-4606M ASTM D-3683/D-3684/D-4606M ASTM D-3683/D-3684/D-4606M ASTM D-3683/D-3684/D-4606MEIA Facility Code Facility

Name Boiler ID HAPs Test Group 03140 PPL Brunner Island 031A/032 Mercury and non-mercury

metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 1 4/20/2010 4/20/2010 13050.9 Btu/lb 2 4/20/2010 4/20/2010 12879.8 Btu/lb 3 4/21/2010 4/21/2010 13056.4 Btu/lb Fuel Testing ResultsMercury and non-mercury

metalic HAPs

% Moisture (as received) % A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) 5.94 8.48 2.270 13874.5 Btu/lb 9.02 5.79 9.10 2.251 13671.0 Btu/lb 9.66 5.88 8.14 2.406 13871.7 Btu/lb 8.65% Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony (Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic Units 2.413 0.12 % 120.82 ppb 4.94 ppm 2.48 ppm 2.39 0.14 % 123.71 ppb 4.95 ppm 2.57 ppm 2.556 0.12 % 132.3 ppb 4.92 ppm 2.35 ppmBeryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) 0.04 ppm 0.05 ppm 14.8 ppm 5.07 ppm 17.1 0.04 ppm 0.05 ppm 16.3 ppm 5.68 ppm 17.8 0.04 ppm 0.05 ppm 14.2 ppm 5.8 ppm 16.5Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units ppm 10.4 ppm 0.71 ppm 0.25 ppm ppm 11.9 ppm 1.73 ppm 0.25 ppm ppm 10.9 ppm 1.26 ppm 0.25 ppmEIA Facility Code Facility

Name Boiler ID HAPs Test Group 03140 PPL Brunner Island 031A/032 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 2 4/21/2010 4/21/2010 12999.6 Btu/lb 3 4/21/2010 4/21/2010 13092.4 Btu/lb 4 4/21/2010 4/21/2010 13060.8 Btu/lb Fuel Testing Results% Moisture

(as received) % A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) 5.78 8.79 2.383 13797.6 Btu/lb 9.33 5.53 8.68 2.376 13858.3 Btu/lb 9.19 5.64 8.37 2.271 13841.4 Btu/lb 8.87% Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony (Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic Units 2.529 0.1 % 2.61 ppm 2.515 0.11 % 2.37 ppm 2.407 0.11 % 2.12 ppmBeryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) 0.04 ppm 0.05 ppm 13 ppm 4.77 ppm 16.1 0.04 ppm 0.05 ppm 13.1 ppm 4.75 ppm 16.4 0.04 ppm 0.05 ppm 13.9 ppm 5.42 ppm 16.5Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units ppm 9.32 ppm 0.99 ppm ppm 8.55 ppm 1.09 ppm ppm 9.42 ppm 1.04 ppmEIA Facility Code Facility

Name Boiler ID HAPs Test Group 03140 PPL Brunner Island 031A/032

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis)% Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony (Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic UnitsBeryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis)Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsEIA Facility Code Facility

Name Boiler ID HAPs Test Group 03140 PPL Brunner Island 031A/032

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis)% Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony (Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic UnitsBeryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis)Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /Kg ppm ppbUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm