Dolan Chemical Laboratory 4001 Bixby Road Groveport, OH 43125 T: 614-836-4221, Audinet 210-4221 F: 614-836-4168, Audinet 210-4168 http://aepenv/labs 

### Water Analysis Form REP-703 Rev. 0, 4/2012



### Location: Mountaineer Plant Report Date: 11/2/2012

Sample Number:124373-001 Date Collected:10/10/2012 09:00Date Received:10/10/2012 

### Plant Outfall #001

Units Parameter Result RL Analysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Arsenic, As 2.93 0.1 DPC EPA 200.8 0.03 10/22/2012 10:31 ug/L Barium, Ba 94.8 0.1 DPC EPA 200.8 0.03 10/22/2012 10:31 ug/L Copper, Cu 4.18 0.05 DPC EPA 200.8 0.02 10/22/2012 10:31 ng/L Mercury, Hg 2.8 2 TLT EPA 1631E 0.8 10/23/2012 ug/L Nickel, Ni 3.94 0.2 DPC EPA 200.8 0.04 10/22/2012 10:31 ug/L Selenium, Se 4.3 0.5 DPC EPA 200.8 0.1 10/22/2012 10:31 mg/L Aluminum, Al 0.212 0.001 DPC EPA 200.8 0.0003 10/22/2012 10:31 mg/L Iron, Fe 0.158 0.01 DAM EPA 200.7 0.002 10/18/2012 16:05 mg/L Chloride, Cl 372 2 TDF EPA 300.1 0.5 10/30/2012 01:21 mg/L Sulfate, SO4 1110 10 TDF EPA 300.1 3 10/30/2012 01:21



### Sample Number:124373-002Date Collected:10/10/2012 09:00Date Received:10/10/2012 

## Trip Blank

Units Parameter Result RL Analysis ByAnalysis Date/TimeMethod MDL Data Qual ng/L Mercury, Hg 0.3 0.5 TLT EPA 1631E 0.2 10/23/2012 J



### Sample Number:124373-003Date Collected:10/10/2012 09:00Date Received:10/10/2012 

## Field Blank

Units Parameter Result RL Analysis ByAnalysis Date/TimeMethod MDL Data Qual ng/L Mercury, Hg 0.3 0.5 TLT EPA 1631E 0.2 10/23/2012 J

Mountaineer Plant, 124373 Page 1 of 5

### Location: Mountaineer Plant Report Date: 11/2/2012

Sample Number:124373-004Date Collected:10/09/2012 13:35Date Received:10/10/2012 

### Leachate Underdrain #001

Units Parameter Result RL Analysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Arsenic, As 96.0 0.1 DPC EPA 200.8 0.03 10/22/2012 10:35 ug/L Barium, Ba 24.1 0.1 DPC EPA 200.8 0.03 10/22/2012 10:35 ug/L Cadmium, Cd 6.42 0.05 DPC EPA 200.8 0.01 10/22/2012 10:35 ug/L Chromium, Cr 0.8 0.2 DPC EPA 200.8 0.03 10/22/2012 10:35 ug/L Lead, Pb 0.188 0.01 DPC EPA 200.8 0.003 10/22/2012 10:35 ug/L Mercury, Hg < 0.3 2 JAB EPA 245.2 0.3 10/31/2012 U ug/L Molybdenum, Mo 10300 0.1 DPC EPA 200.8 0.02 10/22/2012 10:35 ug/L Nickel, Ni 15.7 0.2 DPC EPA 200.8 0.04 10/22/2012 10:35 ug/L Selenium, Se 456 0.5 DPC EPA 200.8 0.1 10/22/2012 10:35 ug/L Vanadium, V 100 2 DAM EPA 200.7 0.5 10/18/2012 16:12 ug/L Zinc, Zn 8.0 0.5 DPC EPA 200.8 0.1 10/22/2012 10:35 mg/L Aluminum, Al 0.0835 0.001 DPC EPA 200.8 0.0003 10/22/2012 10:35 mg/L Boron, B 75.5 0.01 DAM EPA 200.7 0.002 10/18/2012 16:12 mg/L Calcium, Ca 472 0.02 DAM EPA 200.7 0.004 10/18/2012 16:12 mg/L Iron, Fe 0.952 0.01 DAM EPA 200.7 0.002 10/18/2012 16:12 mg/L Magnesium, Mg 564 0.05 DAM EPA 200.7 0.01 10/18/2012 16:12 mg/L Manganese, Mn 2.44 0.0005 DAM EPA 200.7 0.0001 10/18/2012 16:12 mg/L Chloride, Cl 933 10 TDF EPA 300.1 2 10/30/2012 00:21 mg/L Sulfate, SO4 7240 50 TDF EPA 300.1 20 10/30/2012 00:21



### Sample Number:124373-005Date Collected:10/09/2012 13:40 Date Received:10/10/2012 

### Leachate Underdrain #007

Units Parameter Result RL Analysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Arsenic, As 5.83 0.1 DPC EPA 200.8 0.03 10/22/2012 10:40 ug/L Barium, Ba 26.0 0.1 DPC EPA 200.8 0.03 10/22/2012 10:40 ug/L Cadmium, Cd 6.69 0.05 DPC EPA 200.8 0.01 10/22/2012 10:40 ug/L Chromium, Cr 0.03 0.2 DPC EPA 200.8 0.03 10/22/2012 10:40 J ug/L Lead, Pb 0.072 0.01 DPC EPA 200.8 0.003 10/22/2012 10:40 ug/L Mercury, Hg < 0.3 2 JAB EPA 245.2 0.3 10/31/2012 U ug/L Molybdenum, Mo 10800 0.1 DPC EPA 200.8 0.02 10/22/2012 10:40 ug/L Nickel, Ni 24.0 0.2 DPC EPA 200.8 0.04 10/22/2012 10:40 ug/L Selenium, Se 261 0.5 DPC EPA 200.8 0.1 10/22/2012 10:40 ug/L Vanadium, V < 0.5 2 DAM EPA 200.7 0.5 10/18/2012 16:20 U ug/L Zinc, Zn 12.2 0.5 DPC EPA 200.8 0.1 10/22/2012 10:40 mg/L Aluminum, Al 0.0167 0.001 DPC EPA 200.8 0.0003 10/22/2012 10:40 mg/L Boron, B 29.2 0.01 DAM EPA 200.7 0.002 10/18/2012 16:20 mg/L Calcium, Ca 534 0.02 DAM EPA 200.7 0.004 10/18/2012 16:20 mg/L Iron, Fe 2.40 0.01 DAM EPA 200.7 0.002 10/18/2012 16:20 mg/L Magnesium, Mg 141 0.05 DAM EPA 200.7 0.01 10/18/2012 16:20 mg/L Manganese, Mn 3.65 0.0005 DAM EPA 200.7 0.0001 10/18/2012 16:20 mg/L Chloride, Cl 61.5 2 TDF EPA 300.1 0.5 10/30/2012 01:01 mg/L Sulfate, SO4 2160 10 TDF EPA 300.1 3 10/30/2012 01:01

Mountaineer Plant, 124373 Page 2 of 5

### Location: Mountaineer Plant Report Date: 11/2/2012

Sample Number:124373-006Date Collected:10/09/2012 13:45Date Received:10/10/2012 

### Leachate Underdrain #008

Units Parameter Result RL Analysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Arsenic, As 177 0.1 DPC EPA 200.8 0.03 10/22/2012 10:45 ug/L Barium, Ba 23.8 0.1 DPC EPA 200.8 0.03 10/22/2012 10:45 ug/L Cadmium, Cd 6.16 0.05 DPC EPA 200.8 0.01 10/22/2012 10:45 ug/L Chromium, Cr 0.8 0.2 DPC EPA 200.8 0.03 10/22/2012 10:45 ug/L Lead, Pb 0.272 0.01 DPC EPA 200.8 0.003 10/22/2012 10:45 ug/L Mercury, Hg < 0.9 6 JAB EPA 245.2 0.9 10/31/2012 U ug/L Molybdenum, Mo 10600 0.1 DPC EPA 200.8 0.02 10/22/2012 10:45 ug/L Nickel, Ni 7.57 0.2 DPC EPA 200.8 0.04 10/22/2012 10:45 ug/L Selenium, Se 687 0.5 DPC EPA 200.8 0.1 10/22/2012 10:45 ug/L Vanadium, V 211 2 DAM EPA 200.7 0.5 10/18/2012 16:29 ug/L Zinc, Zn 8.2 0.5 DPC EPA 200.8 0.1 10/22/2012 10:45 mg/L Aluminum, Al 0.118 0.001 DPC EPA 200.8 0.0003 10/22/2012 10:45 mg/L Boron, B 123 0.01 DAM EPA 200.7 0.002 10/18/2012 16:29 mg/L Calcium, Ca 447 0.02 DAM EPA 200.7 0.004 10/18/2012 16:29 mg/L Iron, Fe 0.066 0.01 DAM EPA 200.7 0.002 10/18/2012 16:29 mg/L Magnesium, Mg 991 0.05 DAM EPA 200.7 0.01 10/18/2012 16:29 mg/L Manganese, Mn 1.81 0.0005 DAM EPA 200.7 0.0001 10/18/2012 16:29 mg/L Chloride, Cl 1860 10 TDF EPA 300.1 2 10/30/2012 00:41 mg/L Sulfate, SO4 12700 50 TDF EPA 300.1 20 10/30/2012 00:41



### Sample Number:124373-007Date Collected:10/09/2012 13:50 Date Received:10/10/2012 

### Groundwater Interceptor #006

Units Parameter Result RL Analysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Arsenic, As 0.92 0.1 DPC EPA 200.8 0.03 10/22/2012 10:50 ug/L Barium, Ba 71.9 0.1 DPC EPA 200.8 0.03 10/22/2012 10:50 ug/L Cadmium, Cd 0.13 0.05 DPC EPA 200.8 0.01 10/22/2012 10:50 ug/L Chromium, Cr 0.4 0.2 DPC EPA 200.8 0.03 10/22/2012 10:50 ug/L Lead, Pb 0.063 0.01 DPC EPA 200.8 0.003 10/22/2012 10:50 ug/L Mercury, Hg < 0.3 2 JAB EPA 245.2 0.3 10/18/2012 U ug/L Molybdenum, Mo 115 0.1 DPC EPA 200.8 0.02 10/22/2012 10:50 ug/L Nickel, Ni 1.07 0.2 DPC EPA 200.8 0.04 10/22/2012 10:50 ug/L Selenium, Se 5.5 0.5 DPC EPA 200.8 0.1 10/22/2012 10:50 ug/L Vanadium, V < 0.5 2 DAM EPA 200.7 0.5 10/18/2012 16:37 U ug/L Zinc, Zn 5.9 0.5 DPC EPA 200.8 0.1 10/22/2012 10:50 mg/L Aluminum, Al 0.0084 0.001 DPC EPA 200.8 0.0003 10/22/2012 10:50 mg/L Boron, B 1.91 0.01 DAM EPA 200.7 0.002 10/18/2012 16:37 mg/L Calcium, Ca 260 0.02 DAM EPA 200.7 0.004 10/18/2012 16:37 mg/L Iron, Fe 0.020 0.01 DAM EPA 200.7 0.002 10/18/2012 16:38 mg/L Magnesium, Mg 93.1 0.05 DAM EPA 200.7 0.01 10/18/2012 16:37 mg/L Manganese, Mn 0.0081 0.0005 DAM EPA 200.7 0.0001 10/18/2012 16:38 mg/L Chloride, Cl 55.3 1 TDF EPA 300.1 0.2 10/30/2012 01:48 mg/L Sulfate, SO4 739 5 TDF EPA 300.1 2 10/30/2012 01:48

Mountaineer Plant, 124373 Page 3 of 5

### Location: Mountaineer Plant Report Date: 11/2/2012

Sample Number:124373-008Date Collected:10/09/2012 14:05Date Received:10/10/2012 

### Groundwater Interceptor #007

Units Parameter Result RL Analysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Arsenic, As 2.11 0.1 DPC EPA 200.8 0.03 10/22/2012 10:54 ug/L Barium, Ba 77.6 0.1 DPC EPA 200.8 0.03 10/22/2012 10:54 ug/L Cadmium, Cd 0.09 0.05 DPC EPA 200.8 0.01 10/22/2012 10:54 ug/L Chromium, Cr 0.5 0.2 DPC EPA 200.8 0.03 10/22/2012 10:54 ug/L Lead, Pb 0.185 0.01 DPC EPA 200.8 0.003 10/22/2012 10:54 ug/L Mercury, Hg < 0.3 2 JAB EPA 245.2 0.3 10/18/2012 U ug/L Molybdenum, Mo 87.2 0.1 DPC EPA 200.8 0.02 10/22/2012 10:54 ug/L Nickel, Ni 1.17 0.2 DPC EPA 200.8 0.04 10/22/2012 10:54 ug/L Selenium, Se 4.5 0.5 DPC EPA 200.8 0.1 10/22/2012 10:54 ug/L Vanadium, V < 0.5 2 DAM EPA 200.7 0.5 10/18/2012 16:41 U ug/L Zinc, Zn 4.1 0.5 DPC EPA 200.8 0.1 10/22/2012 10:54 mg/L Aluminum, Al 0.0616 0.001 DPC EPA 200.8 0.0003 10/22/2012 10:54 mg/L Boron, B 1.34 0.01 DAM EPA 200.7 0.002 10/18/2012 16:41 mg/L Calcium, Ca 212 0.02 DAM EPA 200.7 0.004 10/18/2012 16:41 mg/L Iron, Fe 0.081 0.01 DAM EPA 200.7 0.002 10/18/2012 16:41 mg/L Magnesium, Mg 68.7 0.05 DAM EPA 200.7 0.01 10/18/2012 16:41 mg/L Manganese, Mn 0.0579 0.0005 DAM EPA 200.7 0.0001 10/18/2012 16:41 mg/L Chloride, Cl 43.0 1 TDF EPA 300.1 0.2 10/30/2012 02:08 mg/L Sulfate, SO4 592 5 TDF EPA 300.1 2 10/30/2012 02:08



### Sample Number:124373-009Date Collected:10/09/2012 14:10 Date Received:10/10/2012 

### Groundwater Interceptor Sump

Units Parameter Result RL Analysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Arsenic, As 4.36 0.1 DPC EPA 200.8 0.03 10/22/2012 11:57 ug/L Barium, Ba 53.5 0.1 DPC EPA 200.8 0.03 10/22/2012 11:57 ug/L Cadmium, Cd 1.14 0.05 DPC EPA 200.8 0.01 10/22/2012 11:57 ug/L Chromium, Cr 3.3 0.2 DPC EPA 200.8 0.03 10/22/2012 11:57 ug/L Lead, Pb 0.392 0.01 DPC EPA 200.8 0.003 10/22/2012 11:57 ug/L Mercury, Hg < 0.3 2 JAB EPA 245.2 0.3 10/18/2012 U ug/L Molybdenum, Mo 1100 0.1 DPC EPA 200.8 0.02 10/22/2012 11:57 ug/L Nickel, Ni 7.92 0.2 DPC EPA 200.8 0.04 10/22/2012 11:57 ug/L Selenium, Se 40.5 0.5 DPC EPA 200.8 0.1 10/22/2012 11:57 ug/L Vanadium, V < 0.5 2 DAM EPA 200.7 0.5 10/18/2012 16:45 U ug/L Zinc, Zn 9.2 0.5 DPC EPA 200.8 0.1 10/22/2012 11:57 mg/L Aluminum, Al 0.0242 0.001 DPC EPA 200.8 0.0003 10/22/2012 11:57 mg/L Boron, B 9.98 0.01 DAM EPA 200.7 0.002 10/18/2012 16:45 mg/L Calcium, Ca 263 0.02 DAM EPA 200.7 0.004 10/18/2012 16:45 mg/L Iron, Fe 0.076 0.01 DAM EPA 200.7 0.002 10/18/2012 16:45 mg/L Magnesium, Mg 109 0.05 DAM EPA 200.7 0.01 10/18/2012 16:45 mg/L Manganese, Mn 0.763 0.0005 DAM EPA 200.7 0.0001 10/18/2012 16:45 mg/L Chloride, Cl 131 1 TDF EPA 300.1 0.2 10/30/2012 02:27 mg/L Sulfate, SO4 1260 5 TDF EPA 300.1 2 10/30/2012 02:27

Mountaineer Plant, 124373 Page 4 of 5

### Location: Mountaineer Plant Report Date: 11/2/2012

Sample Number:124373-010Date Collected:10/08/2012 14:23Date Received:10/10/2012 

### CPS Effluent

Units Parameter Result RL Analysis ByAnalysis Date/TimeMethod MDL Data Qual ng/L Mercury, Hg 36.1 10 TLT EPA 1631E 4 10/23/2012



### Sample Number:124373-011 Date Collected:10/10/2012 08:20Date Received:10/10/2012 

## CPS Effluent

Units Parameter Result RL Analysis ByAnalysis Date/TimeMethod MDL Data Qual ng/L Mercury, Hg 31.0 10 TLT EPA 1631E 4 10/23/2012



### Sample Number:124373-012Date Collected:10/10/2012 08:25Date Received:10/10/2012 

## Bioreactor Effluent

Units Parameter Result RL Analysis ByAnalysis Date/TimeMethod MDL Data Qual ng/L Mercury, Hg 1.8 1 TLT EPA 1631E 0.4 10/23/2012

THIS TEST REPORT RELATES ONLY TO THE ITEMS TESTED AND SHALL NOT BE REPRODUCED EXCEPT IN FULL WITHOUT WRITTEN APPROVAL OF THE LABORATORY. ALL TEST RESULTS MEET ALL OF THE REQUIREMENTS OF THE ACCREDITING AUTHORITY, UNLESS OTHERWISE NOTED. U: Analyte was analyzed and not detected at or above adjusted Method Detection Limit J: Analyte was positively identified, though the quantitation was below Reporting Limit.

Brian Snyder, Chemist II Email bssnyder@aep.comTel. 614-836-4224
Fax 614-836-4168 Audinet 210-4224

Mountaineer Plant, 124373 Page 5 of 5