Docket No: EPA-HQ-RCRA-2012-0072

Update V 

Kim Kirkland 

(703) 308-0490 

kirkland.kim@epa.epa.gov

Waste Characterization Branch 

Materials Recovery and Waste Management Division 

Office of Resource Conservation and Recovery 

 Assem Akram is the Docket Manager, and Lisa Medley the Docket Center's Records Information Manager.

Electronic File Name 

Document Title Abstract Document 

Type 

Document Sub Type 

Source Citation Author Name Author Date Media Page 

Count 

Start/ End Page 

Method 1030 METHOD 1030 

IGNITABILITY OF SOLIDS 

This method is suitable for the determination of the ignitability of solids and is appropriate for pastes, granular materials, solids that can be cut into strips, and powdery substances. 

Method SW-846 06-09 15 1/15 

1030 (1) Test Methods for Readily Combustible Solids. 

Burning Rate Test. 

Supports Publication; 

Copyrighted Material 

(14.2.2.5) Recommendations on the 

Transport of Dangerous Goods, Fifth 

Revised Edition, United Nations, New York, 1988. 

 1988 

1030 (2) 49 CFR, Appendix E to Part 173 Supports Publication; 

Copyrighted Material 

12-31-91 Edition. http://ecfr.gpoaccess.gov/cgi/t/text/textidx?c=ecfr;sid=75f5fbc866580ef2bc4bc1a8b340a5ab;rgn=div5;view=text;node=49%3

A2.1.1.3.9;idno=49;cc=ecfr 

 12-31-91 2 597/598 

1030 (3) Flammability (Solids). Method A.10. Supports Publication; 

Copyrighted Material 

Official Journal of the European Communities, No. L251/63, September 19, 1984. http://www.intermed.it/istbiotech/reach/A10web1992.pdf

 09-19-84 PDF 3 1/3 

1030 (4) Validation of Ignitability Method for Solids Supports Publication; 

Copyrighted Material 

Submitted to the Office of Solid Waste, U.S. EPA, February 1994 

Foster Wheeler Enviresponse, Inc., Edison, NJ. 

02-94 

1030 (5) Internal Report (AMFA Report) Supports Publication; 

Copyrighted Material 

North Carolina Department of Environmental Health and Natural Resources 

B. Hamner 

Method 3200 METHOD 3200 

MERCURY SPECIES FRACTIONATION AND QUANTIFICATION BY MICROWAVE ASSISTED EXTRACTION, SELECTIVE SOLVENT EXTRACTION 

AND/OR SOLID PHASE EXTRACTION

This method contains a sequential extraction and separation procedure that may be used in conjunction with a determinative method to differentiate mercury species that are present in soils and sediments. This method provides information on both total mercury and various mercury species. 

method SW-846 03-12 PDF 34 1/34 

3200 (1) Speciation and Cycling of Mercury in Lavaca Bay, 

Texas, Sediments 

A time series of sediment depth 

profiles of total mercury (THg) and monomethylmercury (MMHg) showed a maximum in both solid phase and porewater MMHg during early spring, followed by a decrease throughout the remainder of the year. 

Supports Publication; 

Copyrighted Material 

Environ. Sci. Technol., 1999, 33(1), 7-13, 

http://pubs.acs.org/doi/abs/10.1021/es980379d

N.S. Bloom, et. al. 01-01-99 Electronic file 7 7/13
3200 (2) Guidelines for terms related to chemical 

speciation and fractionation of elements: Definitions, structural aspects, and methodological

approaches 

This document contains guidelines for terms related to chemical speciation and fractionation of elements as well as definitions, structural aspects, and methodological approaches. 

Supports Publication; 

Copyrighted Material 

Pure Appl. Chem., 2000, 72(8), 1453-1470, 

http://www.iupac.org/objID/Article/pac7208x1453

D. Templeton, et. al. 2000 Electronic file 18 1453/1470 

3200 (3) Determination of Artifactual Formation of 

Monomethylmercury (CH3Hg+) in Environmental 

Samples Using Stable Hg2+ Isotopes with ICP-MS 

Detection: Calculation of Contents Applying Species Specific Isotope Additions 

This article describes the use of different extraction techniques with regard to their potential to form monomethylmercury artifact from inorganic Hg during sample prep. 

Supports Publication; 

Copyrighted Material 

Fresenius J. Anal. Chem., 1997, 358(3), 363-370, http://www.springerlink.com/content/m7dpx89cxqke7fq6/ 

H. Hintelmann, et. al. 06-97 8 363/370 

3200 (4) Artifact formation of methyl mercury during 

aqueous distillation and alternative techniques forthe extraction of methyl mercury from environmental samples 

Supports Publication; 

Copyrighted Material 

Fresenius J. Anal. Chem., 1997, 358(3), 

371-377, http://www.springerlink.com/content/35jq2nrwbqn08e3x/

N. S Bloom, et. al. 06-97 7 371/377 

3200 (5) Synthesis and Characterization of Isotopically 

Enriched Methylmercury (CH3201Hg+) Isotopically enriched methylmercury was successfully synthesized and can 

be used in SIDMS and IDMS analysis as a standard. 

Supports Publication; 

Copyrighted Material 

Appl. Organomet. Chem., 2003, 17(12), 

913-920, 

http://onlinelibrary.wiley.com/doi/10.1002/aoc.551/pdf

G. M. Rahman, et. al. 11-05-03 8 913/920 

3200 (6) Speciation of mercury in soil and sediment by 

selective solvent and acid extraction 

A sequential extraction scheme for 

mercury in soil was developed to classify mercury species based on their environmental mobility and/or toxicity for routine lab analysis or onsite screening purposes. 

Supports Publication; 

Copyrighted Material 

Anal. Bioanal. Chem., 2003, 375(3), 428-

436, http://www.springerlink.com/content/m45jmrqf9kac67fw/

Y. Han, et. al. 01-18-03 9 428/436 

3200 (7) Application of Isotope Dilution in Elemental 

Speciation: Speciated Isotope Dilution Mass Spectrometry (SIDMS) 

Supports Publication; 

Copyrighted Material 

Comprehensive Analytical Chemistry, Volume 33 (Elemental Speciation: New 

Approaches for Trace Element Analysis), 

Elsevier, New York, 2000, 277-313,

http://www.sciencedirect.com/science/article/pii/S0166526X00800203 

D. Huo, et. al. 2000 37 277/313 

3200 (8) Application of Speciated Isotope Dilution Mass 

Spectrometry to Evaluate Extraction Methods for Determining Mercury Speciation in Soils and Sediments 

Common methylmercury( or mercury species from various matrixes) extraction techniques were evaluated by applying speciated isotope dilution mass spectrometry and EPA RCRA Draft Method 3200 was found to be the most efficient. 

Supports Publication; 

Copyrighted Material 

Anal. Chem., 2004, 76(13), 3548-55, 

http://www.ncbi.nlm.nih.gov/pubmed/15228324

G.M. M. Rahman, et. al. 07-01-04 8 3548/3555 

3200 (9) Inter-laboratory Validation of EPA Method 3200 

for Mercury Speciation Analysis using Prepared Soil Reference Materials 

This article describes the findings of an inter-laboratory validation study of EPA draft method 3200 on two soil matrices. 

Supports Publication; 

Copyrighted Material 

Appl. Organomet. Chem., 19(3), 301-307, 

March 2005, 

http://onlinelibrary.wiley.com/doi/10.1002/aoc.816/abstract

G. M. M. Rahman, et. al. 02-04-05 7 301/307 

3200 (10) Occupational Health Guideline for Organo (Alkyl) 

Mercury 

This article gives general guidelines about organo (alkyl) mercury compounds and how to safely handle them. 

Supports Publication; 

Copyrighted Material 

Occupational Safety and Health 

Adminstration, Washington, D.C., 1978, 

http://www.cdc.gov/niosh/docs/81-123/pdfs/0384.pdf

U.S. Department of Labor 09-78 6 1/6 

3200 (11) Delayed Cerebellar Disease and Death after 

Accidental Exposure to Dimethylmercury 

A case study of an accidental 

dimethylmercury poisoning illustrates the potent toxicity of this material and the need for additional safety precautions when used in any scientific research. 

Supports Publication; 

Copyrighted Material 

New Engl. J. Med., 1998, 338: 1672-1676, 

http://www.nejm.org/doi/full/10.1056/NEJM199806043382305

D. W. Nierenberg, et. al. 06-04-98 4 1672/1675 
3200 (12) Microwave Enhanced Chemistry: Fundamentals, 

Sample Preparation, and Applications 

Supports Publication; 

Copyrighted Material 

Microwave Enhanced Chemistry: Fundamentals, Sample Preparation, and 

Applications, pub. 10th ed.; American 

Chemical Society, Washington, DC, 1997 

H. M. Kingston, et. al. 1997 

3200 (13) Applied Isotope Technologies, Inc 3200 (14) Speciated Isotope Dilution Mass Spectrometry of 

Reactive Species and Related Methods 

Speciated isotope dilution mass spectrometry (SIDMS) permits the determination of concentrations of one or more species from a sample even if it has been subjected to species conversion prior to species separation or degradation or incomplete separation exists. 

Supports Publication; 

Copyrighted Material 

US Patent 6 790 673 B1 http://www.findthatpatent.com/Speciated_isotope_dilution_mass_spectrometry_of_reactive_species_and_related,6790673.html 

H. M. Kingston 09-14-04 0 0/0 

3200 (15) Rapid Sequential Determination of Inorganic 

Mercury and Methylmercury in Natural Waters by Flow-injection - Cold Vapor-Atomic-Fluorescence Spectrometry 

A method with application to river 

waters for the rapid sequential determination of inorganic mercury and methylmercury in natural waters at the ng/l level was developed. 

Supports Publication; 

Copyrighted Material 

Talanta, 1992, 39(11), 1537-1542, 

http://www.sciencedirect.com/science/article/pii/0039914092801384 

W. Jain, et. al. 11-92 6 1537/1542 

3200 (16) Development of Microwave-Assisted Extraction 

Method and Isotopic Validation of Mercury Species in Soils and Sediments 

Supports Publication; 

Copyrighted Material 

J. Anal. At. Spectrom., 2005, 20, 183-191, 

Method’s Archive Box 22 

G. M. M. Rahman, et. al. 2005 9 183/191 

3200 (17) Development, Research and Validation of 

Environmental Speciation Methods: Evaluation by Speciated Isotope Dilution Mass Spectrometry in Mercury and Chromium Speciation Analysis 

The SIDMS technique was established and validated for mercury speciation analysis and an investigation providing solutions to difficulties associated with the analysis of mercury and chromium species is found in this dissertation. 

Supports Publication; 

Copyrighted Material 

Ph. D. Dissertation, Duquesne University, Pittsburgh, PA, 2004 http://digital.library.duq.edu/cdmspiritan/document.php?CISOROOT=/etd&CISOPTR=74238&REC=1 

G. M. M. Rahman 08-19-04 229 1/229 

3200 (18) Microwave-assisted Solvent Extraction for

Quantitative Simultaneous Extraction of Inorganic Mercury and Methylmercury from Soils 

Supports Publication; 

Copyrighted Material 

20th Annual National Environmental 

Monitoring Conference, Washington, DC, July 19-23, 2004 

E. Fischer, et. al. 2004 

3200 (19) Field Sampling Technique for Mercury Speciation Supports Publication; 

Copyrighted Material 

Anal. Proc., 1991, 293-294 W. Jain, et. al. 1991 2 293/294 

3200 (20) Determination of Methylmercury in Natural Waters 

at the Sub-nanograms-per-litre Level by Capillary Gas Chromatography after Adsorbent Preconcentration 

Supports Publication; 

Copyrighted Material 

Anal. Chim. Acta, 1989, 221(2), 259-268, 

http://www.sciencedirect.com/science/article/pii/S0003267000819625 

Y. H. Lee, et. al. 1989 10 259/268 

3200 (21) Mercury Species Immobilized on Sulphydryl

Cotton: A New Candidate Reference Material for Mercury Speciation 

This article describes an integrated analytical scheme for determination and speciation of Hg in waters as well as developing a new class of reference material. 

Supports Publication; 

Copyrighted Material 

Mikrochim. Acta., 1996, 123(1-4), 103-108, 

http://www.springerlink.com/content/v5261u5642445451/fulltext.pdf 

M. L. Mena, et. al. 1996 6 103/108 

3200 (22) Rapid Analysis for the Field: Method 

Development and Application to Natural Gas Utility Sites 

Supports Publication; 

Copyrighted Material 

Water Air Soil Poll., 2001, 127(1-4), 255-

270, Method’s Archive Box 3 

H. M. Boylan, et. al. 2001 16 255/270 

3200 (23) The Environmental Geochemistry and 

Bioaccessibility of Mercury in Soils and Sediments-A Review 

This paper examines the current information on mercury bioaccessibility and speciation in soils and the ability of speciation methods to approximate mercury bioaccessibility. 

Supports Publication; 

Copyrighted Material 

Risk Anal., 1997, 17(5), 105-113, http://onlinelibrary.wiley.com/doi/10.1111/j.1539-6924.1997.tb00897.x/abstract 

A. Davis, et. al. 10-97 9 105/113 

3200 (24) Distribution of Mercury Species in Soil from a 

Mercury-Contaminated Site 

Supports Publication; 

Copyrighted Material 

Water Air Soil Poll., 1989, 17(5), 557-569, 

Method’s Archive Box 3 

 N. W. Revis, et. al. 1989 13 557/569 
3200 (25) Quantitative Method for Determining the 

Concentration of Mercury (II) Sulphide in Soils and Sediments 

This article describes a method for extracting mercury from soil sequentially and that can selectively differentiate mercury(II) sulphide from other species and compounds of mercury in soil. 

Supports Publication; 

Copyrighted Material 

Analyst, 1989, 114, 823-825, 

http://pubs.rsc.org/en/Content/ArticleLanding/1989/AN/an9891400823 

N. W. Revis, et. al. 1989 4 823/826 

3200 (26) Speciation of Mercury in Crude Oil uisng 

Speciated Isotope Dilution Mass Spectrometry 

This article describes an improved sample preparation and detection method that allows for the determination of mercury species in crude oil. 

Supports Publication; 

Copyrighted Material 

Spectroscopy, 2010, 25(1), 36-45, 

http://spectroscopyonline.findanalytichem.com/spectroscopy/Feature/Speciation-ofMercury-in-Crude-Oil-UsingSpeciated/ArticleStandard/Article/detail/655117

G. M. Rahman, et. al. 01-01-10 10 36/45 

3200 (27) Application of Speciated Isotope Dilution Mass 

Spectrometry to Evaluate Methods for Efficiencies, Recoveries, and Quantification of Mercury Species Transformation in Human Hair 

This article describes the use of different extraction methods used for mercury speciation in human hair samples by providing extraction efficiencies, recoveries and potential of species transformations during the process. 

Supports Publication; 

Copyrighted Material 

J. Anal. At. Spectrom., 2009, 24, 83-92, 

http://pubs.rsc.org/en/Content/ArticleLanding/2009/JA/b805249b

G. M. Rahman, et. al. 10-24-08 10 83/92 

3200 (28) Comparison of Methods with Respect to 

Efficiencies, Recoveries, and Quantitation of Mercury Species Interconversions in Food Demonstrated using Tuna Fish 

This article describes the efficiencies, recoveries, and quantitation of mercury species interconversions in tuna fish for total mercury and methylmercury using eight different procedures. 

Supports Publication; 

Copyrighted Material 

Anal. Bioanal. Chem., 2008, 390(8), 2123-

32, 

http://www.ncbi.nlm.nih.gov/pubmed/18317738

L. H. Reyes, et. al. 04-08 10 2123/2132 

3511 METHOD 3511 

ORGANIC COMPOUNDS IN WATER BY MICROEXTRACTION 

Method 3511 is a procedure for extracting selected volatile and semivolatile organic compounds from water. The microscale approach minimizes sample size and solvent usage, thereby reducing the supply costs, health and safety risks, and waste generated. This method was validated for several mono- and poly-cyclic aromatic hydrocarbons (MAHs and PAHs) and can be applied to any combination of these compounds. 

Supports Publication; 

Copyrighted Material 

SW-846 03-12 PDF 13 1/13 

3511 (1) Simultaneous Analysis of Monocyclic Aromatic 

Hydrocarbons in Water by Microextraction 

Supports Publication; 

Copyrighted Material 

EPRI Report TR-Research Project, April 1997 

 04-97 

3511 (2) D. M. Munro. “Simultaneous Determination of 

Volatile and Semivolatile Organic Compounds in Soil.” Remediation Journal, 10, pp. 65-81, 2000. 

Supports Publication; 

Copyrighted Material 

http://onlinelibrary.wiley.com/doi/10.1002/rem.3440100408/pdf

3572 METHOD 3572 

Extraction of Chemical Agents from Wipe Samples Using Microextraction 

This method describes the extraction of chemical agents from wipe samples using a microextraction technique. 

Supports Publication; 

Copyrighted Material 

SW-846 12/2011 PDF 11 1/11 

3572 (1) Applicable documents to support the occupational 

health program when dealing with chemical agents include AR11-34 (The Army Respiratory Protection Program; AR 40-5 (Preventive Medicine); DA Pam 40-8 (Occupational Health guidelines for the evaluation and Control of Occupational Exposure to Nerve Agents GA, GB, GC, and VX.) and DA Pam 40-173 (Occupational Health Guidelines for the Evaluation and Control of Occupational Exposure to Mustard Agents H, HD, and HT) 

Supports Publication; 

Copyrighted Material 

 a. http://www.apd.army.mil/pdffiles/r11_34.pdf, b. http://www.apd.army.mil/pdffiles/p40_8.pdf c. 

http://www.apd.army.mil/pdffiles/p40_173.pdf

 03-12 
3572 (2) Development and Evaluation of an Analytical 

Method for Determination of GB, VX, and HD in Concrete 

Supports Publication; 

Copyrighted Material 

William S. Williamson, Jr, et. 

Al. 

3572 (3) Development and Evaluation of an Analytical 

Method for Determination of GB, VX, and HD in Coral 

Supports Publication; 

Copyrighted Material 

William S. Williamson, Jr, et. 

Al. 

3572 (4) Development and Evaluation of an Analytical 

Method for Determination of GB, VX, and HD in Charcoal 

Supports Publication; 

Copyrighted Material 

Michael G. MacNaughton, et. Al. 

3572 (5) Development and Evaluation of an Analytical 

Method for Determination of GB, VX, and HD on Surfaces 

Supports Publication; 

Copyrighted Material 

Carter Crigler 

3572 (6) Laboratory Monitoring and Quality Assurance 

Plan dated June 2004 

Supports Publication; 

Copyrighted Material 

Department of Army, Chemical Material Agency 

Method 3620C METHOD 3620C 

FLORISIL CLEANUP 

This method includes procedures for cleanup of sample extracts containing phthalate esters, nitrosamines, nitroaromatics, haloethers, aniline and aniline derivatives, chlorinated hydrocarbons, organochlorine pesticides, organophosphates, organophosphorus pesticides, PCBs, and other analytes that allow for adequate performace. 

Method SW-846 10-12 28 1/28 

3620C (1) The Chemist’s Companion: A Handbook of 

Practical Data, Techniques, and References 

Supports Publication; 

Copyrighted Material 

John Wiley & Sons, Inc., New York. A.J. Gordon, et. al. 1972 3 372, 374, 

375 

3620C (2) Florisil: Properties, Application, Bibliography Supports Publication; 

Copyrighted Material 

Pittsburgh, Pennsylvania, 5M381DW. Floridin of ITT System 

3620C (3) Variation of Florisil Activity; Simple Method for 

Measuring Absorbent Capacity and its Use in Standardizing Florisil Columns 

Supports Publication; 

Copyrighted Material 

Journal of the Association of Official 

Analytical Chemists, 51, 29, 1968. 

P.A. Mills 1968 

3620C (4) Pesticides Analytical Manual Supports Publication; 

Copyrighted Material 

Volume 1, July 1985. http://www.fda.gov/Food/ScienceResearch/LaboratoryMethods/PesticideAnalysisManualPAM/ucm111455.htm 

U.S. Food and Drug 

Association 

07-85 

3620C (5) Cleanup of Environmental Sample Extracts Using 

Florisil Solid-Phase Extraction Cartridges 

Supports Publication; 

Copyrighted Material 

J. Chrom. Sci. 27, 209-215, 1989. http://chromsci.oxfordjournals.org/content/27/5/209.abstract

V. Lopez-Avila, et. al. 1989 PDF 7 209/215 

3620C (6) Evaluation of Sample Extract Cleanup using 

Solid-Phase Extraction Cartridges 

Supports Publication; 

Copyrighted Material 

Project Report, December 1989. http://nepis.epa.gov/EPA/html/DLwait.htm?url=/Exe/ZyNET.exe/2000AKCX.PDF?ZyActionP=PDF&Client=EPA&Index=1986 Thru 1990&File=D%3A%5CZYFILES%5CINDEX%20DATA%5C86THRU90%5CTXT%5C00000003%5C2000AKCX.txt&Query=&SearchMethod=1&FuzzyDegree=0&User=ANONYMOUS&Password=anonymous&QField=&UseQField=&IntQFieldOp=0&ExtQFieldOp=0&Docs= 

U.S. EPA 12-89 PDF 124 

3620C (7) Aniline and Selected Substituted Derivatives Supports Publication; 

Copyrighted Material 

Method 650 U.S. EPA 
3620C (8) Evaluation of SW-846 Method 8060 for Phthalate 

Esters 

Supports Publication; 

Copyrighted Material 

Proceedings of the Fifth Annual Waste Testing and Quality Assurance Symposium, 1989, pp. 144-156. http://nepis.epa.gov/EPA/html/DLwait.htm?url=/Exe/ZyNET.exe/9100CUG4.PDF?ZyActionP=PDF&Client=EPA&Index=1986 Thru 1990&File=D%3A%5CZYFILES%5CINDEX%20DATA%5C86THRU90%5CTXT%5C00000020%5C9100CUG4.txt&Query=&SearchMethod=1&FuzzyDegree=0&User=ANONYMOUS&Password=anonymous&QField=&UseQField=&IntQFieldOp=0&ExtQFieldOp=0&Docs= 

W.F. Beckert, et. al. 1989 PDF 13 144/156 

3620C (9) Organochlorine Pesticides and PCBs Supports Publication; 

Copyrighted Material 

Method 608, 40 CFR 136, October 26, 1984. http://www.caslab.com/EPAMethods/PDF/608.pdf 

U.S. EPA 10-84 PDF 32 1/32 

4025 METHOD 4025 

SCREENING FOR POLYCHLORINATED DIBENZODIOXINS AND POLYCHLORINATED DIBENZOFURANS (PCDD/PCDFs) BY IMMUNOASSAY 

This method is a procedure for the analysis of polychlorinated dibenzodioxins and polychlorinated dibenzofurans (PCDDs/PCDFs) in soil at 500 ppt (pg/g) using a simple onestep liquid phase oxidative cleanup or, at mid to low ppt levels, using a two step coupled column cleanup (oxidation and activated carbon binding) adapted from Method 8290. The analysis method uses a commercially-available enzyme immunoassay (EIA) test kit containing a polyclonal antibody specific for PCDDs/PCDFs. 

method SW-846 03-12 PDF 23 1/23 

4025 (1) DF1 High Performance Dioxin/Furan 

Immunoassay Kit (CAPE Technologies) 

This Application Note describes a rapid immunoassay specific extraction and rapid one step cleanup to prepare soil samples for screening analysis using the CAPE Technologies High Performance Dioxin/Furan Immunoassay Kit. 

Supports Publication; 

Copyrighted Material 

DF1 High Performance Dioxin/Furan Immunoassay Kit (CAPE Technologies), 

www.cape-tech.com

CAPE Technologies 08-28-02 10 1/10 

4025 (2) CAPE Technologies Application Notes and related 

product literature 

Supports Publication; 

Copyrighted Material 

http://cape-tech.com/ 

4025 (3) Measurement of PCDD/F TEQ by Immunoassay: 

Concept Development and Validation 

4025 (4) Measurement of PCDD/F TEQ by Immunoassay: 

Concept Development and Validation 

This presentation discusses the requirements for successful development of a PCDD/F Enzyme ImmunoAssay (EIA) and presents data demonstrating the determination of PCDD/F toxicity equivalence by EIA. 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds, 1998, 35, 97-100, http://www.cape-tech.com/TR-001.pdf 

Robert E. Carlson, et. al. 08-17-98 5 1/5 

4025 (5) Role of Quality Assurance in Immunoassay 

Methods Used for Field Screening. Immunochemical Technology for Environmental 

Applications 

This paper discusses the problems in environmental immunochemistry assays (including kits)by examining current market structure and troubleshooting case studies by the manufacturer. 

Supports Publication; 

Copyrighted Material 

Immunochemical Technology for Environmental Applications, American Chemical Society, Chapter 29, 361-372, 

http://pubs.acs.org/doi/abs/10.1021/bk1997-0657.ch029

Robert O. Harrison 5/5/97 12 361/372 
4025 (6) The 2005 World Health Organization Reevaluation of Human and Mammalian Toxic 

Equivalency Factors (TEFs) of Dioxins and Dioxin-like Compounds 

Supports Publication; 

Copyrighted Material 

Toxicological Sciences, 93(2): 223-241 (2006), 

http://toxsci.oxfordjournals.org/content/93/2/223.full.pdf+html

Van den Berg, et. al. 07-07-06 19 223/241 

4025 (7) Correlation between EIA Results and GC-MS 

TEQ 

 Supports Publication; 

Copyrighted Material 

 Tech reference, www.cape-tech.com 

4025 (8) Performance of the CAPE Technologies DF1 

Dioxin/Furan Immunoassy Kit for Soil and Sediment Samples 

Supports Publication; 

Copyrighted Material 

Tech references, www.cape-tech.com

4025 (9) Technologies for Monitoring and Measurement of 

Dioxin and Dioxin-like Compounds in Soil and Sediment (CAPE Technologies LLC, DF1; Dioxin/Furan Immunoassay Kit; PCB TEQ Immunoassy Kit) 

Supports Publication; 

Copyrighted Material 

www.cape-tech.com

4025 (10) Technical Note TN-005 Supports Publication; 

Copyrighted Material 

www.cape-tech.com

4025 (11) Application Note AN-008 Supports Publication; 

Copyrighted Material 

www.cape-tech.com

4025 (12) An Efficient and Green Cleanup System for

Analysis of Dioxins/Furans, Dioxin-like PCBs and 

PBDES 

Supports Publication; 

Copyrighted Material 

www.cape-tech.com

4025 (13) Immunoassy Sample Prep Kit SP3-60 Supports Publication; 

Copyrighted Material 

www.cape-tech.com

4025 (14) Sample Prep Starter Kit SP3-ST Supports Publication; 

Copyrighted Material 

www.cape-tech.com

4430 METHOD 4430 

SCREENING FOR POLYCHLORINATED DIBENZO-p-DIOXINS (PCDDs) AND 

POLYCHLORINATED DIBENZOFURANS (PCDFs) IN SOILS AND SEDIMENTS USING AN ARYL HYDROCARBON RECEPTORBASED PCR ASSAY 

This method is a screening procedure for polychlorinated dibenzo-p-dioxins 

(PCDDs) and polychlorinated dibenzofurans (PCDFs) in soils and sediments. This method uses a commercially-available aryl hydrocarbon receptor (AhR)-based polymerase chain reaction (PCR) assay. The AhR-PCR assay screens samples by their toxicity equivalent quotient (TEQ) by responding to individual PCDD/PCDF congeners in approximate correlation to their toxicity equivalent factors (TEFs). The TEQ measured by the AhR-PCR assay is the sum of the response from the individual congeners. See Table 2 for a detailed list of response factors for individual PCDD/PCDF congeners. 

method SW-846 03-12 PDF 23 1/23 

4430 (1) Dioxins and Furans in Soil and Sediment 4430 (2) The 2005 World Health Organization 

Reevaluation of Human and Mammalian Toxicity Equivalency Factors for Dioxins and Dioxin-like Compounds 

Supports Publication; 

Copyrighted Material 

Toxicological Sciences, 93(2): 223-241 (2006), 

http://toxsci.oxfordjournals.org/content/93/2/223.full.pdf+html

M. Van Den Berg, et. al. 07-07-96 19 223/241 
4430 (3) Novel Real-Time PCR Assay for the Detection of 

Dioxins and Furans 

Supports Publication; 

Copyrighted Material 

Organohalogen Compd. 2002, 58, 341-343 R. L. Allen, et. al. 2002 3 341/343 

4430 (4) Sample Preparation for the Measurement of 

Polychlorinated Dioxins and Furans by the Procept Rapid Dioxin Assay 

This paper investigates several methods for isolating PCDD/F from other AhR cross-reactive compounds, with primary focus on PAH. 

Supports Publication; 

Copyrighted Material 

Organohalogen Compnd. 2006, 68, 940-943, 

http://www.dioxin20xx.org/pdfs/2006/06-138.pdf

D. R. McAlister, et. al. 2006 4 940/943 

4430 (5) The PAS Superfamily: Sensors of Environmental 

and Developmental Signals 

This paper provides a detailed description of three signal transduction pathways that utilize PAS protein heterodimers to drive their transcriptional output in hopes that this information can help in understanding the biology of these not wellunderstood superfamily. 

Supports Publication; 

Copyrighted Material 

Annu. Rev. Pharmacol. Toxicol. 2000, 40, 

519-561, 

http://mcardle.oncology.wisc.edu/bradfield/519.pdf

Y. Z. Gu, et. al. 2000 43 519/561 

4430 (6) Soil Screening at 50 pg/g Using a Novel Aryl 

Hydrocarbon Receptor-based PCR Assay 

Supports Publication; 

Copyrighted Material 

Organohalogen Compd., 2007, 69, 1230-1233

D. R. McAlister, et. al. 2007 4 1230/1233 

4430 (7) Cross-reactivity of Compounds on the Procept 

Rapid Dioxin Assay 

Supports Publication; 

Copyrighted Material 

Organohalogen Compd., 2007, 69, 1226-1229

D. R. McAlister, et. al. 2007 4 1226/1229 

4430 (8) Role of Heat Shock Protein 90 Dissociation in 

Mediating Agonist-induced Activation of the Aryl Hydrocarbon Receptor 

In this article, authors demonstrate that molybdate inhibits AhR gene activation in two types of cells in a concentration dependent manner and protects the 

AhR against agonist-induced 

proteolysis. 

Supports Publication; 

Copyrighted Material 

Mol. Pharmacol. 2000, 57(1), 82-92, http://molpharm.aspetjournals.org/content/57/1/82.full.pdf

S. Heid, et. al. 2000 11 82/92 

4430 (9) Update to ATSDR Policy Guideline for Dioxins 

and Dioxin-Like Compounds in Residential Soil 

This document seeks public comment on a draft revision of its policy that is intended to assist health assessors evaluating the public health risks of dioxin and dioxin like compounds in residential soils. 

Supports Publication; 

Copyrighted Material 

Fed. Reg. 2006, 71, 78441-78442, 

http://edocket.access.gpo.gov/2006/pdf/E6-22388.pdf

Fed. Reg. 2006 12-29-06 2 78441/7844

2 

4430 (10) Emerging Homogeneous DNA-based 

Technologies in the Clinical Laboratory 

This article reviews technologies available for performing homogeneous analysis, the clinical applications where they are being used, and validation issues that are slowing the acceptance of the technologies in the general clinical setting. 

Supports Publication; 

Copyrighted Material 

Clin. Chem. 2000, 47(6), 

http://www.clinchem.org/content/47/6/990.full.pdf+html

C. A. Foy, et. Al. 06-01 11 990/1000 

4430 (11) Rapid Aryl Hydrocarbon Receptor-based 

Polymerase Chain Reaction Screening Assay for Polychlorinated Dibenzo-p-Dioxins and Furans in 

Soil and Sediment 

This article describes a method for the estimation of PCCD/F toxicity equivalent quotient of soil and sediment matrices. 

Supports Publication; 

Copyrighted Material 

Talanta, 2007, 74(4), 992-997, http://www.sciencedirect.com/science/article/pii/S0039914007005607

D. R. McAlister, et. Al. 01-15-08 6 992/997 
4435 METHOD 4435 

SCREENING FOR DIOXIN-LIKE CHEMICAL 

ACTIVITY IN SOILS AND SEDIMENTS 

USING THE CALUX® BIOASSAY AND TEQ DETERMINATIONS 

This method is a bio-analytical screening procedure for dioxin-like compounds in soils and sediments. This method is based on the ability of dioxin and related chemicals to activate the aryl hydrocarbon receptor (AhR), a chemical-responsive DNAbinding protein that is responsible for producing the toxic and biological effects of these chemicals. Measurement of the level of activation of AhR-dependent gene expression by a chemical or chemical extract provides a measure by which to estimate the relative potency and toxic potential of these chemicals and/or extracts with resulting values expressed as toxic equivalents (TEQs). 

method SW-846 03-12 PDF 59 1/59 

4435 (1) Ah Receptor Mediated Effects of Particulate 

Organic Extracts from the Paso Del Morte Airshed 

Along the U.S. - Mexico Border 

Supports Publication; 

Copyrighted Material 

Environmental Heath Perspectives, 2003, 111(10), 1299-1305, http://www.ncbi.nlm.nih.gov/pmc/articles/PMC1241610/pdf/ehp0111-001299.pdf 

2003 7 1299/1305 

4435 (2) Harmonised Quality Criteria for Chemical and 

Bioassays Analyses of PCDDs/PCDFs in Feed and Food Part 2: General Considerations, Bioassay Methods 

This article describes proposed QA/QC guidelines for bioassays that measure dioxin-like compounds and discusses technical questions associated them. 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 2001, 45, 

http://www.dioxins.com/pdf/feedstuffs/feed04.pdf

Peter A. Behnisch, et. al. 2001 5 0/0 

4435 (3) Determination of REP Values for the CALUX 

bioassay and comparison to the WHO TEF Values 

In this article relative potency (REP) values are determined for dioxin like compounds to understand the relationship between GC/MS results and characterize responsiveness of the CALUX® assay. 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 2001, 53, 211-214, 

http://www.dioxins.com/pdf/compounds/compound02.pdf

David J. Brown, et. al. 2001 4 211/214 

4435 (4) Quality control criteria implemented for monitoring 

the CALUX bioassay 

In this article the authors report the QC criteria that have been developed in the lab to monitor the reproducibility and consistency of results from the CALUX® assay. 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 2001, 54, 32-35, 

http://www.dioxins.com/pdf/environment/environment01.pdf

David J. Brown, et. al. 2001 4 32/35 

4435 (5) Validation Study for the use of the Dioxin

Responsive CALUX Assay for Analysis of Japanese Ash and Soil Samples 

In this article the author reports results from a preliminary validation study that used blind format to compare the results from the dioxin responsive CALUXTM assay with HRGCMS data. 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 2000, 45, 200-203, 

http://www.dioxins.com/pdf/environment/environment10.pdf

David Brown, et. al. 2000 4 200/203 

4435 (6) Recovery determinations for bioassay analysis: 

Considerations and results 

In this article the use of biologically inactive congeners as internal spikes is researched and presented along with information about HRGC/HRMS recoveries and radiolabeled spike experiments. 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds, 2002, 58, 357-360, 

http://www.dioxins.com/pdf/compounds/compound03.pdf

David J. Brown, et. al. 2002 4 357/360 

4435 (7) Elimination of interfering compounds in 

preparation for analysis by an Ah receptor based bioassay 

In this article various sample prep methods and their efficiency of removing environmental contaminants and selected “non-classical” AhR ligands are reported. 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 2002, 58, 401-404,

http://www.dioxins.com/pdf/compounds/compound04.pdf 

David J. Brown, et. al. 2002 4 401/404 
4435 (8) Relationships between exposure to dioxin-like 

chemicals, testosterone levels, and sex of the children of pesticide applicators 

This article studies the relationships between exposure to dioxin-like chemicals, testosterone levels, and sex of the children of pesticide applicators with the use of DIPSCALUX. 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 2002, 56, 73-76, 

http://www.dioxins.com/pdf/compounds/compound07.pdf

George Clark, et. al. 2002 4 73/76 

4435 (9) Characterization of the CALUX and GRAB 

bioassays for sensitivity and specificity in detection of phamacological agents that activate the Ah Receptor signaling system 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds, 1999, 42, 309-312, http://www.dioxins.com/pdf/compounds/compound09.pdf 

George C. Clark, et al. 1999 4 309/312 

4435 (10) A Novel Low-Cost Air Sampling Device 

(AmbStack Sampler) and Detection System (CALUX Bioassay) for Measuring Air Emissions of Dioxin, Furan, and PCB on a TEQ Basis Tested With a Model Industrial Boiler 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 1999, 40, 79-82, 

http://www.dioxins.com/pdf/environment/environment09.pdf

George C. Clark, et. al. 1999 4 79/82 

4435 (11) Bioanalytical approaches for the Detection of 

Dioxin and Related Halogenated Aromatic Hydrocarbons 

Supports Publication; 

Copyrighted Material 

Biomarkers of Environmentally Associated Disease, Chapter 33, 483-494, http://www.crcnetbase.com/doi/abs/10.1201/9781420032208.ch33 

Bruce D. Hammock, et. al. 2002 12 483/494 

4435 (12) Ah receptor-based bioassays for dioxins and 

related chemicals: Applications and limitations 

Supports Publication; 

Copyrighted Material 

Toxicol. Sci. 2000, 55, 107-115, 

http://toxsci.oxfordjournals.org/content/55/1/107.full.pdf

Shawn D. Seidel, et. al. 2000 9 107/115 

4435 (13) Recombinant Cell Bioassay Systems for the

Detection and Relative Quantitation of Halogenated Dioxins and Related Chemicals 

Supports Publication; 

Copyrighted Material 

Talanta 63, Issue 5, http://www.sciencedirect.com/science/article/pii/S0039914004002978 

Michael S. Denison, et. al. 08-08-04 11 1123/1133

4435 (14) Bioanalytical approaches for the detection of 

dioxin and related halogenated aromatic hydrocarbons, in: Technology-Driven Biomarkers Development and Application in EnvironmentallyAssociated Diseases 

Supports Publication; 

Copyrighted Material 

Technology-Driven Biomarkers Development and Application in Environmentally-Associated Diseases 483-494, Lewis Press, Boca Raton, FL 

M. S. Denison, et. al. 2002 12 483/494 

4435 (15) Species-specific recombinant cell lines as 

bioassay systems for the detection of 2,3,7,8-tetrachlorodibenzo-p-dioxin-like chemicals 

Supports Publication; 

Copyrighted Material 

Fund. Appl. Toxicol. 1996, 30, 194-203, 

http://toxsci.oxfordjournals.org/content/30/2/194.full.pdf+html

P. M. Garrison, et. al. 1996 10 194/203 

4435 (16) Comparison of recombinant cell Bioassays for the 

detection of Ah receptor agonists 

Supports Publication; 

Copyrighted Material 

Biofactors 20 (1/2004), 11-22, https://iospress.metapress.com/content/458qmdj2gu4mc7ef/resourcesecured/?target=fulltext.pdf 

D. Han, et. al. 04-19-04 12 11/22 

4435 (17) Recombinant cell lines for the detection of dioxins 

and Ah Receptor ligands- Not all assays are created equal 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 58(2002): 421-424, 

http://www.dioxins.com/pdf/compounds/compound05.pdf

D. Han, et. al. 2002 4 421/424 
4435 (18) Determination of Dioxins and Planar PCBs in Fish 

Using the GC/MS and CALUX Bioassay 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 45(2000): 180 - 184, http://www.dioxin20xx.org/pdfs/2000/00-212.pdf

R. Hoogenboom, et. al. 2000 4 180/183 

4435 (19) Using the CALUX Assay to select high-TCDD

mothers in Southern Kazakhstan and map timecourse of TCDD elimination via breast milk. 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 58(2002): 377-380, 

http://www.dioxin20xx.org/pdfs/2002/02-467.pdf

Kim Hooper, et. al. 2002 4 377/380 

4435 (20) CALUX results correlate with GC/MS/MS data 

from Kazakhstan breast milk samples 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 45(2000): 236-239, Organohalogen Compounds 45: 236-239 

Kim Hooper, et. al. 2000 4 236/239 

4435 (21) CALUX and High Resolution GC/MS Analysis of 

Dioxin-Like Compounds in Chlorophenoxy Pesticide Formulations 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 60-65(Dioxin 2003), 

http://www.dioxins.com/pdf/environment/environment04.pdf

Janice K. Huwe, et. al. 4 0/0 

4435 (22) CALUX assay is applicable to human 

epidemiological studies 

Supports Publication; 

Copyrighted Material 

 Organohalogen Compounds 54(2001): 48-50, 

http://www.dioxins.com/pdf/biological/biological02.pdf

F. Kayama, et. al. 2001 3 48/50 

4435 (23) Dioxin and Organochlorine Pesticide 

Concentrations of Breast Milk in China and Japan 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 60 -65a(2003), 

http://www.dioxins.com/pdf/biological/biological06.pdf

F. Kayama, et. al. 2003 4 0/0 

4435 (24) Regional differences of blood dioxins and

organchlorine pesticides concentrations of Japanese female farmers.-Application of CALUX assay for epidemiological study 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 55(2002): 275-278, 

http://www.dioxins.com/pdf/biological/biological03.pdf

F. Kayama, et. al. 2002 4 275/278 

4435 (25) A COMPARATIVE ANALYSIS OF CERTIFIED 

ENVIRONMENTAL REFERENCE MATERIALS USING CALUXTM ASSAY AND HIGH RESOLUTION GC/MS 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 58(2002): 381-384, 

http://www.dioxin20xx.org/pdfs/2002/02-468.pdf

T. Nakamura, et. al. 2002 4 381/384 

4435 (26) Validation of the CALUX Bioassay: Quantitative 

Screening Approach 

Supports Publication; 

Copyrighted Material 

 Organohalogen Compounds 58(2002): 353 - 356, http://www.dioxins.com/pdf/environment/environment02.pdf

I. Van Overmeire, et. al. 2002 4 353/356 

4435 (27) Application of the CALUX Bioassay for the

Determination of Low TEQ Values in Milk Samples 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 45(2001), 

http://www.dioxins.com/pdf/biological/biological08.pdf

Ilse Van Overmeire, et. al. 2001 3 0/0 
4435 (28) A Comparitive Study of GC-HRMS and CALUX 

TEQ Determinations in Food Samples by the Belgian Federal Ministries of Public Health and 

Agriculture 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 45(2000): 196 - 200, 

http://www.dioxins.com/pdf/feedstuffs/feed02.pdf

Ilse Van Overmeire, et. al. 2000 4 196/200 

4435 (29) Inter-Laboratory CALUX Comparison Data at Low 

Levels with Traditional GC-HRMS Confirmations 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 60(2003): 255-258, 

http://www.dioxin20xx.org/pdfs/2003/03-65.pdf

L. M. Pence, et. al. 2003 4 255/258 

4435 (30) Persistent Organic Pollutants (POPs) and Immune 

Function in US Atlantic Coast Harbor Seals 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 60 - 65(2003), 

http://www.dioxins.com/pdf/biological/biological05.pdf

Susan D. Shaw, et. al. 2003 4 0/0 

4435 (31) Comparison of the CALUX Bioassay and IDHRGC/HRMS as Measures of Dioxin Toxic 

Equivalents in Serum 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 60 - 65, 

http://www.dioxins.com/pdf/biological/biological04.pdf

Marcella Warner, et. al. 2003 4 0/0 

4435 (32) Non Additive Interactions in CALUX Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 60 - 65, http://www.dioxins.com/pdf/compounds/compound06.pdf

I. Windal, et. al. 2003 4 0/0 

4435 (33) Variables that affect TEQ determinations by 

CALUX and GC-HRMS 

Supports Publication; 

Copyrighted Material 

Organohalogen Compounds 58(2002): 389-392, 

http://www.dioxins.com/pdf/environment/environment03.pdf

I. Windal, et. al. 2002 4 389/392 

4435 (34) Application of the luciferase recombinant cell 

culture bioassay system for the analysis of polycyclic aromatic hydrocarbons 

Supports Publication; 

Copyrighted Material 

 Environ. Toxicol. & Chem. 2002, 21(10), 2027-2033 

Michael H. Ziccardi, et. al. 10-02 7 2027-2033 

4435 (35) Chemically Activated Luciferase Gene Expression 

(CALUX) Cell Bioassay Analysis for the Estimation of Doxin-Like Activity: Critical Parameters of the CALUX Procedure that Impact 

Assay Results 

Supports Publication; 

Copyrighted Material 

Environ. Sci. Technol., 2005, 39(19), 7357-7364, 

Isabelle Windal, et. al. 2005 8 7357/7364 

4435 (36) Brominated dioxin-like compounds in vitro

assessment in comparison to classical dioxin-like compounds and other polyaromatic compounds 

Supports Publication; 

Copyrighted Material 

Environment International, 2003, 29, 861-877, 

http://www.pops.int/documents/meetings/poprc/submissions/AnnexE_2007/Toxicity%20studies%20World%20Chlorine%20Council.pdf

Peter Alexander Behnisch, et. al. 

2003 17 861/877 

4435 (37) Study of the interference problems of dioxin-like 

chemicals with the bio-analytical method CALUX 

Supports Publication; 

Copyrighted Material 

Talanta 63 (2004), 1261-1268, http://www.vub.ac.be/ANCH/publications/Schroijen%20et%20al_2004.pdf 

Carmen Schroijen, et. al. 2004 8 1261/1268 
4435 (38) The 2005 World Health Organization 

Reevaluation of Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-Like Compounds 

Supports Publication; 

Copyrighted Material 

Toxicological Sciences 93(2):223-241, 2006, 

http://toxsci.oxfordjournals.org/content/93/2/223.full.pdf+html

Martin Van den Berg, et. al. 2006 19 223/241 

4435 (39) Mathematical Model Developed for Environmental 

Samples: Prediction of GC/MS Dioxin TEQ from XDS-CALUX Bioassay Data 

This article describes use of the XDSCALUX bioassay and GC/MS to create a mathematical model that can be useful in risk assessment and management decisions for dioxin-like contamination sites. 

Supports Publication; 

Copyrighted Material 

Environmental Science and Technology 2007, 41(12), 4354-4360, 

http://journals.ohiolink.edu/ejc/article.cgi?issn=0013936x&issue=v41i0012&article=4354_mmdfesdtfxbd

D. J. Brown, et. al. 06-15-07 7 4354/4360 

4435 (40) Report on the Comparison of Cell Based Assays 

with Mass Spectrometry Methods for the Analysis of PCDDs/PCDFs and PCBs in Biosolids 

Supports Publication; 

Copyrighted Material 

U.S. EPA Report from the Office of Water and Office of Science and Technology, Engineering and Analysis Division on Biosolids, June 2002. 

USEPA 06-02 

4435 (41) U.S. patent # 5,854,010 Supports Publication; 

Copyrighted Material 

Bioassay for detecting 2,3,7,8-tetrachlorodibenzo-para-dioxin and TCDDlike compounds and novel recombinant cell line useful therefor, http://patft.uspto.gov/netacgi/nphParser?Sect1=PTO1&Sect2=HITOFF&d=P

ALL&p=1&u=%2Fnetahtml%2FPTO%2Fsr

chnum.htm&r=1&f=G&l=50&s1=5,854,010.PN.&OS=PN/5,854,010&RS=PN/5,854,010 

Michael S. Denison, et. al. 12-29-98 1 0/0 

4435 (42) U.S. Patent # 6,720,431 Supports Publication; 

Copyrighted Material 

Methods and apparatus for separating and detecting specific polyhalogenated diaromatic hydrocarbons , http://patft.uspto.gov/netacgi/nphParser?Sect1=PTO1&Sect2=HITOFF&d=P

ALL&p=1&u=%2Fnetahtml%2FPTO%2Fsr

chnum.htm&r=1&f=G&l=50&s1=6,720,431.PN.&OS=PN/6,720,431&RS=PN/6,720,431 

Michael D. Chu, et. al. 04-13-04 1 0/0 

5021A Method 5021A - VOLATILE ORGANIC 

COMPOUNDS IN VARIOUS SAMPLE MATRICES USING EQUILIBRIUM HEADSPACE 

ANALYSIS 

method SW-846 03-12 PDF 31 1/31 

5021A (1) Determination of Volatile Organic Compounds in 

Soils using Equilibrium Headspace Analysis and Capillary Column Gas Chromatography/Mass Spectrometry 

Supports Publication; 

Copyrighted Material 

U.S. Environmental Protection Agency, Office of Research and Development, Environmental Monitoring Systems Laboratory, Cincinnati, OH, December, 1992. 

P. Flores, et. al. 12-92 
5021A (2) Headspace Analysis and Related Methods in Gas 

Chromatography 

Supports Publication; 

Copyrighted Material 

Headspace Analysis and Related Methods in Gas Chromatography," John Wiley and Sons, 1984 

B. V. Loffe, et. a. 1994 

5021A (3) The Analysis of Selected Components of 

Reformulated Gasoline in Environmental Samples 

Supports Publication; 

Copyrighted Material 

from MTBE Handbook, ed. Kostecki, P. and Moyer, E. Amherst Scientific Publishers, 2002. 

R. J. Pirkle, et. al. 2002 

5021A (4) Environmental Fact Sheet: Analytical Methods for 

Fuel Oxygenates 

This fact sheet provides information about EPA’s validated analytical methods for common fuel oxygenates. 

Supports Publication; 

Copyrighted Material 

EPA 510-F-03-001, April, 2003, 

http://www.epa.gov/oust/mtbe/omethods.pdf

USEPA OUST 04-03 2 0/0 

5021A (5) Analytical Methods for Fuel Oxygenates Supports Publication; 

Copyrighted Material 

LUSTLine (Bulletin #42), October, 2002, http://www.epa.gov/oust/mtbe/LL42Analytical.pdf

H. White, et. al. 10-02 8 1/8 

5021A (6) RCRA Organic Methods Workgroup Meeting 

Minutes, March 20, 2012. 

Supports Available in Methods Contract Archive 03-20-12 

5021A (7) RCRA Organic Methods Workgroup Meeting 

Minutes, March 22, 2012. 

Supports Available in Methods Contract Archive 03-22-12 

5021A (8) RCRA Organic Methods Workgroup Meeting 

presentation describing changes to method 5021, “Proposed Changes to SW-846 method 5021A, VOCs by Static Headspace”, March 1, 2012. 

Supports Available in Methods Contract Archive 03-12 

6010D METHOD 6010D 

INDUCTIVELY COUPLED PLASMA—OPTICAL EMISSION SPECTROMETRY 

Inductively coupled plasma—optical emission spectrometry (ICP-OES) is a spectrometric technique used to determine trace elements in aqueous solutions sample. 

method SW-846 03-12 PDF 35 1/35 

6010D (1) An Interlaboratory Study of Inductively Coupled 

Plasma Atomic Emission Spectroscopy Method 6010 and Digestion Method 3050 

In this report, the design, execution, and results of an interlaboratory study of Method 6010 and Method 3050 are discussed. 

Supports Publication; 

Copyrighted Material 

EPA-600/4-87-032, U.S. Environmental Protection Agency, Las Vegas, NV, 1987, http://nepis.epa.gov/Exe/ZyPURL.cgi?Dock

ey=91009D89.txt

C. L. Jones, et. al. 05-87 19 1/19 

6010D (2) Quality Assurance of Chemical Measurements Supports Publication; 

Copyrighted Material 

Quality Assurance of Chemical Measurements, Lewis Publishers (1987) 

J. K. Taylor, et. al. 1987 

6010D (3) Federal Advisory Committee on Detection and 

Quantitation Approaches and Uses in Clean Water Act Programs, Final Report 

Supports Publication; 

Copyrighted Material 

Federal Advisory Committee, http://water.epa.gov/scitech/methods/cwa/det/index.cfm

Federal Advisory Committee on Detection and Quantitation Approaches and Uses in Clean Water 

Act Programs 

12-28-07 
6020B METHOD 6020B 

INDUCTIVELY COUPLED PLASMA—MASS SPECTROMETRY 

Inductively coupled plasma—mass spectrometry (ICP-MS) is applicable to the determination of sub-μg/L concentrations of a large number of elements in water samples and in waste extracts or digests When dissolved constituents are required, samples must be filtered and acidpreserved prior to analysis. No digestion is required prior to analysis for dissolved elements in water samples. Acid digestion prior to filtration and analysis is required for groundwater, aqueous samples, industrial wastes, soils, sludges, sediments, and other solid wastes for which total (acidleachable) elements are required. The analyst should insure that a sample digestion method is chosen that is appropriate for each analyte and the intended use of the data. 

method SW-846 03-12 PDF 31 1/31 

6020B (1) The effect of plasma operating parameters on 

analyte signals in inductively coupled plasmamass spectrometry 

Supports Publication; 

Copyrighted Material 

Spectrochim. Acta Part B: Atomic Spec. 40(10-12), 1555-1572 (1985), http://www.sciencedirect.com/science/article/pii/0584854785801786 

G. Horlick, et. al. 1985 18 1555/1572 

6020B (2) The ICP as an ion source-origins, achievements 

and prospects/Mass spectrometry with an inductively coupled plasma as an ion source: the influence on ultratrace analysis of background and matrix response 

Supports Publication; 

Copyrighted Material 

Spectrochim. Acta Part B, 40(10-12), 1525-1537 (1985), http://www.sciencedirect.com/science/article/pii/0584854785801762, http://www.sciencedirect.com/science/article/pii/0584854786801471 

A. L. Gray 1985 13, 17 1525/1537; 

151/167 

6020B (3) Background Spectral Features in Inductively 

Coupled Plasma/Mass Spectrometry 

In this article the basic background mass spectra of the inductively coupled plasma are presented. 

Supports Publication; 

Copyrighted Material 

Appl. Spectrosc. 40, 445 (1986), 

http://www.opticsinfobase.org/as/abstract.cfm?uri=as-40-4-445

S. H. Tan, et. al. 1986 16 445/460 

6020B (4) Oxide, Hydroxide, and Doubly Charged Analyte 

Species in Inductively Coupled Plasma/Mass Spectrometry 

Supports Publication; 

Copyrighted Material 

Appl. Spectrosc. 40(4), 434-445 (1986), 

http://www.opticsinfobase.org/abstract.cfm?URI=as-40-4-434

M. A. Vaughan, et. al. 1986 12 434/445 

6020B (5) Table of the Isotopes Supports Publication; 

Copyrighted Material 

CRC Handbook of Chemistry and Physics, 74th Ed., CRC Press, Boca Raton, FL, 1993 

N. E. Holden 

6020B (6) Winter Conference on Plasma Spectrochemistry, 

San Diego, California, USA, January 10-15, 1994 

Supports Publication; 

Copyrighted Material 

Abstract THP18; p. 237, San Diego, CA 

(1994),

http://pubs.rsc.org/en/content/articlelanding/1994/JA/ja994090051n 

T. A. Hinners, et. al. 

6020B (7) Determination of the rare-earth elements in 

geological materials by inductively coupled plasma mass spectrometry 

This article describes the development of a new method of analysis of geological materials for the determination of the rare-earth elements using ICP-MS. 

Supports Publication; 

Copyrighted Material 

Anal. Chem. 59(8), 1150-1157 (1987),

http://pubs.acs.org/doi/abs/10.1021/ac00135a018 

F. E. Lichte, et. al. 04-87 8 1150/1157 

6020B (8) Simple approach to reducing polyatomic ion 

interferences on arsenic and selenium in inductively coupled plasma mass spectrometry 

This article explains how the interference by polyatomic ions in the determination of As and Se by ICP MS can be substantially reduced by introduction of small amounts of propan-2-ol or a molecular gas into the central channel of the ICP. 

Supports Publication; 

Copyrighted Material 

J. Anal. At. Spectrom, 1989, 4, 299-300, http://pubs.rsc.org/en/content/articlelanding/1989/ja/ja9890400299 

E.H. Evans, et. al. 2 299/300 

6020B (9) Study of the effects of concomitant elements in 

inductively coupled plasmamass spectrometry 

Supports Publication; 

Copyrighted Material 

Spectrochim. Acta Part B, 42(3), 1987, 467-490,

http://www.sciencedirect.com/science/article/pii/0584854787800241 

D. Beauchemin, et. al. 24 467/490 
6020B (10) Mass Spectrometry of inductively coupled

plasmas 

This article explains the development and use of the ICP-MS. 

Supports Publication; 

Copyrighted Material 

Anal. Chem. 1986, 58(1), 97A-105A, 

http://pubs.acs.org/doi/pdf/10.1021/ac00292a003 

R. S. Houk 01-86 9 97A/105A 

6020B (11) A Study of Internal Standardization in Inductively 

Coupled Plasma-Mass Spectrometry

This article discusses the use of internal standardization to compensate for ionization suppression in inductively coupled plasma-mass spectrometry (ICP-MS). 

Supports Publication; 

Copyrighted Material 

Appl. Spectrosc. 41, 5, 801-806 (1987), 

http://www.opticsinfobase.org/viewmedia.cfm?uri=as-41-5-801&seq=0 

J. J. Thompson, et. al. 1987 6 801/806 

6020B (12) Final Report of the Multi-Laboratory Evaluation of 

Method 6020 CLP-M Inductively Coupled PlasmaMass Spectrometry 

Supports Publication; 

Copyrighted Material 

W. R. Newberry, et. al. 

6020B (13) On-Line Solid-phase Chelation for the 

Determination of Eight Metals in Environmental Waters by Inductively Coupled Plasma Mass Spectrometry 

Supports Publication; 

Copyrighted Material 

Daniel B. Taylor, et. al. 

6020B (14) Patent Number 5,126,272, System for Detecting 

Transition and Rare Earth Elements in a Matrix 

Supports Publication; 

Copyrighted Material 

H. M. Kingston, et. al. 

6020B (15) A Method and Apparatus for Detecting Transition 

and Rare Earth Elements in a Matrix 

Supports Publication; 

Copyrighted Material 

H. M. Kingston, et. al. 

6020B (16) Determination of Mercury by ICP-MS Supports Publication; 

Copyrighted Material 

David Dobb, et. al. 

6020B (17) Quality Assurance of Chemical Measurements Supports Publication; 

Copyrighted Material 

Lewis Publishers (1987) J. K. Taylor 

6020B (18) Federal Advisory Committee on Detection and 

Quantitation Approaches and Uses in CleanWaterActPrograms,FinalReport 

Supports Publication; 

Copyrighted Material 

http://water.epa.gov/scitech/methods/cwa/det/index.cfm

Federal Advisory Committee on Detection and Quantitation Approaches and Uses in CleanWaterActPrograms 

6800 METHOD 6800 

ELEMENTAL AND MOLECULAR SPECIATED ISOTOPE DILUTION MASS SPECTROMETRY 

This method consists of two approaches: (1) isotope dilution mass spectrometry (IDMS) for the determination of the total concentrations of elements and molecules and (2) molecular speciated isotope dilution mass spectrometry (SIDMS) for the determination of elemental and molecular species. IUPAC defines speciation analysis as “analyzing chemical compounds that differ in isotopic composition, conformation, oxidation or electronic state, or in the nature of their complexed or covalently bound substituents, which can be regarded as distinct chemical species.”

method SW-846 03-12 PDF 68 1/68 

6800 Sec 13 (1) 

Handbook of Inductively Coupled Plasma Mass Spectrometry 

This book discusses the basics of inductively coupled plasma mass spectrometry including general technique and practical advice. 

Supports Publication; 

Copyrighted Material 

Blackie Academic & Professional: London, U.K. 1992, p-315, http://www.springerlink.com/content/h62264k1r26m4071/ 

K. E. Jarvis, et. al. 1992 380 315/315 
6800 Sec 13 

(2) 

Isotopic ratio measurements with an inductively coupled plasma source mass spectrometer 

This article discusses the factors controlling accuracy and precision of isotopic ratios when inductively coupled plasma source mass spectrometer has been used to measure the isotopic composition of U, Pb, Os, and B standards. 

Supports Publication; 

Copyrighted Material 

Spectrochimica Acta, Part B, Atomic Spectroscopy, 1987, 42B, 49- 62, http://www.sciencedirect.com/science/article/pii/0584854787800496 

G. P. Russ III, et. al. 1987 14 49/62 

6800 Sec 13 (3) 

Inductively Coupled Plasma Mass Spectrometry: Practice and Techniques, Academic Press 

This book presents a thorough description of inductively coupled plasma-mass spectrometry for the use in trace element analytical chemistry issues. 

Supports Publication; 

Copyrighted Material 

Academic Press: San Diego, CA, USA, 

2001, p-48, http://www.sciencedirect.com/science/book/9780126838657 

H. E. Taylor 10-00 294 48/48 

6800 Sec 13 (4) 

Guidelines for Achieving High Accuracy in Isotope Dilution Mass Spectrometry 

 This book provides simple robust methodology with adequate guidance to allow labs to use IDMS, for inorganic and organic mass spectrometry, and obtain reliable data. 

Supports Publication; 

Copyrighted Material 

The Royal Society of Chemistry: Cambridge, UK, 2002, http://books.google.com/books/about/Guidelines_for_achieving_high_accuracy_i.html?id=9wwLS5pcD9sC 

M. Sargent, et. al. 2002 49 0/0 

6800 Sec 13 (5) 

Characterization of waste – State of the art document – Chromium VI specification in solid matrices 

Supports Publication; 

Copyrighted Material 

PD CEN/TR 14589:2003, British Standards, EU publication “International Standards Correspondence Index, Technical Report CEN Technical Committee CEN/TC 292, European Committee for Standardization, 2003, http://shop.bsigroup.com/ProductDetail/?pid=000000000030095298 

 06-04-03 42 

6800 Sec 13 (6) 

Supports Publication; 

Copyrighted Material 

6800 Sec 16 (1) 

Isotope Dilution Mass Spectrometry Supports Publication; 

Copyrighted Material 

Anal. Chem. 1989, 61(10), 643A-649A J. D. Fasset, et. al. 

6800 Sec 16 (2) 

Method of Speciated Isotope Dilution Mass Spectrometry 

Supports Publication; 

Copyrighted Material 

US Patent Number: 5,414,259, 1995 H. M. Kingston 05-09-95 0/0 

6800 Sec 16 (3) 

Correction of Species Transformations in the 

Analysis of Cr(VI) in Solid Environmental Samples 

Using Speciated Isotope Dilution Mass Spectrometry 

This article describes a method capable of monitoring and correcting for such bidirectional species transformations to determine Cr(VI) in solid samples. 

Supports Publication; 

Copyrighted Material 

Anal. Chem. 2000, 72(20), 5047-5054, 

http://pubs.acs.org/doi/abs/10.1021/ac000008r 

D. Huo, et. al. 09-09-00 8 5047/5054 

6800 Sec 16 (4) 

Hexavalent Chromium Extraction from Soils: A Comparison of Five Methods 

This article describes the use of five different methods for the determination of total Cr(VI) in soil. 

Supports Publication; 

Copyrighted Material 

Environ. Sci. Tech. 1995, 29(9), 2377-2381, http://cat.inist.fr/?aModele=afficheN&cpsidt=3643033 

B. R. James, et. al. 1995 5 2377/2381 

6800 Sec 16 (5) 

Accuracy in Species Analysis. Speciated Isotope 

Dilution Mass Spectrometry (SIDMS) Exemplified by the Evaluation of Chromium Species 

Supports Publication; 

Copyrighted Material 

Spectrochim. Acta, Part B: Atomic Spectroscopy, 1998, 53B(2), 299-309, 

http://www.sciencedirect.com/science/article/pii/S0584854797001432

H. M. Kingston, et. al. 02-27-98 11 299/309 
6800 Sec 16 

(6) 

Application of Isotope Dilution in Elemental 

Speciation: Speciated Isotope Dilution Mass Spectrometry (SIDMS) 

This chapter discusses the application of isotope dilution in elemental speciation using speciated isotope dilution mass spectrometry. 

Supports Publication; 

Copyrighted Material 

Comprehensive Analytical Chemistry, J. A. Caruso, K. L. Sutton and K. L. Ackley (eds.), Vol. 33 (Elemental Speciation: New 

Approaches for Trace Element Analysis), 

Elsevier, New York, USA, 2000, p-277-313, http://www.sciencedirect.com/science/article/pii/S0166526X00800203 

D. Huo, et. al. 2000 37 277/313 

6800 Sec 16 (7) 

The Accurate Determination of Species by Speciated Isotope Dilution Mass Spectrometry: Exemplified by the Evaluation of Chromium (VI) in Soil 

Supports Publication; 

Copyrighted Material 

The Twelfth Annual Waste Testing & Quality Assurance Symposium; Washington, DC, July 23-26, 1996, 112-119 

H. M. Kingston, et. al. 8 112/119 

6800 Sec 16 (8) 

Determination and Correction of Analytical Biases and Study on Chemical Mechanisms in the 

Analysis of Cr(VI) in Soil Samples Using EPA 

Protocols 

Supports Publication; 

Copyrighted Material 

Environ. Sci. Tech., 1998, 32(21), 3418-3423, http://pubs.acs.org/doi/abs/10.1021/es971029e 

D. Huo, et. al. 09-12-98 6 3418/3423 

6800 Sec 16 (9) 

IDMS and the National Reference System: 

Accuracy Transfer in Clinical Chemistry 

This article gives information on the use of IDMS, primarily for assigning certified values to human serum reference materials within the SRM program a NIST. 

Supports Publication; 

Copyrighted Material 

Anal. Chem., 1993, 65(12), 475 – 479, 

http://pubs.acs.org/doi/abs/10.1021/ac00060a620 

G. N. Bowers, et. al. 06-93 5 475/479 

6800 Sec 16 (10) 

The Use of Isotope Dilution Mass Spectrometry for the Certification of Standard Reference Materials 

Supports Publication; 

Copyrighted Material 

Environ. Intern., 1984, 10(2), 169-173 L. J. Moore, et. al. 

6800 Sec 16 (11) 

SamplePrep Supports Publication; 

Copyrighted Material 

[Homepage of SamplePrep Web], 

Available: http://www.sampleprep.duq.edu/, 

referenced 2011

H. M. Kingston, et. al. 

6800 Sec 16 (12) 

The Development of Methods in Speciated Isotope Dilution Mass Spectrometry (SIDMS) for Elemental Speciation of Chromium in Environmental Samples Using LC-ICP-MS 

Supports Publication; 

Copyrighted Material 

Doctoral Dissertation, Duquesne University, July 30, 1999 

D. Huo 07-30-99 

6800 Sec 16 (13) 

Determination of hexavalent chromium by using speciated isotope-dilution mass spectrometry after microwave speciated extraction of environmental and other solid materials 

Supports Publication; 

Copyrighted Material 

Anal. Bioanal. Chem., 2005, 382(4), 1111-

1120, http://www.springerlink.com/content/lh1m670w184184rr/ 

G. M. M. Rahman, et. al. 06-05 10 1111/1120 

6800 Sec 16 (14) 

Determination and evaluation of hexavalent chromium in power plant coal combustion byproducts and cost-effective environmental remediation solutions using acid mine drainage 

Supports Publication; 

Copyrighted Material 

J. Environ. Monit., 2005, 7, 899-905, http://pubs.rsc.org/en/content/articlelanding/2005/em/b504724b 

H. M. "Skip" Kingston, et. al. 07-13-05 7 899/905 

6800 Sec 16 (15) 

Development of a microwave-assisted extraction method and isotopic validation of mercury species in soils and sedime 

Supports Publication; 

Copyrighted Material 

Anal. At. Spectrom., 2005, 20, 183-191, 

http://pubs.rsc.org/en/Content/ArticleLanding/2005/JA/b404581e 

G. M. M. Rahman, et. al. 01-01-05 9 183/191 

6800 Sec 16 (16) 

Inter-laboratory Validation of EPA Method 3200 for mercury species analysis using prepared soil reference materials 

Supports Publication; 

Copyrighted Material 

J. Applied Organometallic Chem., 2005, 19, 301-307, http://onlinelibrary.wiley.com/doi/10.1002/aoc.816/abstract 

G. M. M. Rahman, et. al. 02-04-05 7 301/307 
6800 Sec 16 

(17) 

Application of Speciated Isotope Dilution Mass 

Spectrometry to Evaluate Extraction Methods for Determining Mercury Speciation in Soils and Sediments 

Supports Publication; 

Copyrighted Material 

Anal. Chem., 2004, 76(13), 3548-3555, 

http://pubs.acs.org/doi/abs/10.1021/ac030407x 

G. M. M. Rahman, et. al. 05-11-04 7 3548/3555 

6800 Sec 16 (18) 

Speciated isotope dilution mass spectrometry of reactive species and related methods 

Supports Publication; 

Copyrighted Material 

US Patent Number 6 790 673 B1, 2004 and PCT Int. Appl. January 28, 1999, Patent No. WO 9939198 

H. M. Kingston 

6800 Sec 16 (19) 

Automated In-Process Ratio Mass Spectrometry Supports Publication; 

Copyrighted Material 

U.S. Patent Number 6,974,951 B1 H. M. Skip Kingston 12-13-05 

6800 Sec 16 (20) 

Robust microwave-assisted extraction protocol for determination of total mercury and methylmercury in fish tissues 

Supports Publication; 

Copyrighted Material 

Analytica Chemica Acta, 631(2), 121-128, 

2009, http://www.sciencedirect.com/science/article/pii/S0003267008018229 

L. Hinojosa Reyes, et. al. 01-12-09 8 121/128 

6800 Sec 16 (21) 

Application of Speciated Isotope Dilution Mass 

Spectrometry to Evaluate Methods for Efficiencies, Recoveries, and Quantification of Mercury Speciation Transformations in Human Hair 

Supports Publication; 

Copyrighted Material 

J. Anal. At. Spectrom, 2009, 24(1), 83-92, http://pubs.rsc.org/en/Content/ArticleLanding/2009/JA/b805249b 

G. M. M. Rahman, et. al. 10-24-08 10 83/92 

6800 Sec 16 (22) 

Application of Double Spike Isotope Dilution for 

the Accurate Determination of Cr(III), Cr(VI) and Total Cr in Yeast 

Supports Publication; 

Copyrighted Material 

Anal. Bioanal. Chem., 2006, 386(6), 1673-

1680, http://www.springerlink.com/content/6871v185q61j2v47/ 

Lu Yang, et. al. 09-06-06 8 1673/1680 

6800 Sec 16 (23) 

Automated, On-Line, Trace Contamination and 

Chemical Species Analysis For the Semiconductor Industry 

Supports Publication; 

Copyrighted Material 

American Institute of Physics (AIP), 

Conference Proceedings, Proceedings form the 2003 Characterization and Metrology for ULSI Technology Conference, Volume 683, Melville, NY, 2003 

H. M. Skip Kingston, et. al. 

6800 Sec 16 (24) 

Development, Research and Validation of Environmental Speciation Methods: Evaluation by Speciated Isotope Dilution Mass Spectrometry in Mercury and Chromium Speciation Analysis 

Supports Publication; 

Copyrighted Material 

G. M. Mizanur Rahman, Duquesne University, Pittsburgh, PA USA, 2004 

G. M. M. Rahman 08-19-04 229 1/229 

6800 Sec 16 (25) 

Calculations of Double Spike Isotope Dilution Results Revisited 

 This article discusses the use of isotope pattern deconvolution analysis to simplify the double spiking speciesspecific isotope dilution result calculations when inter-conversion might occur. 

Supports Publication; 

Copyrighted Material 

J. Analytical Atomic Spectrometry, 2006, 21, 1294-1297, http://www.uc.edu/plasmachem/Documents/webpdfs1/Double%20Spike%20for%20Isotope%20Ratios.pdf 

Juris Meija, et. al. 08-15-06 4 1294/1297 

6800 Sec 16 (26) 

Testing is an Essential Part of International Environmental Regulation and Commerce Compliance 

Supports Publication; 

Copyrighted Material 

Washington DC, NEMC Presentation 2008 Gonzalo Manchego, et. al. 

6800 Sec 16 (27) 6800 Sec 16 (28) 

Explicit Determinations in Speciated Isotope Dilution Mass Spectrometry without Calibration Curves 

Supports Publication; 

Copyrighted Material 

John Kern, et. al. 
6800 Sec 16 

(29) 

Sensitivity Analysis for Speciated Isotope Dilution

Mass Spectrometry 

Supports Publication; 

Copyrighted Material 

Journal of Analytical and Atomic Spectrometry, 25, 196-200, 2010, http://math.pugetsound.edu/~ctoews/research/publications/revision.pdf 

 C. Toews, et. al. 11-05-09 5 196/200 

6800 Sec 16 (30) 

Speciation of Mercury in Crude Oil Using Speciated Isotope Dilution Mass Spectrometry 

This article describes the use of speciated isotope dilution mass spectrometry for the speciation of mercury in crude oil. 

Supports Publication; 

Copyrighted Material 

Spectroscopy, 25,1, 36-45, 2010, http://spectroscopyonline.findanalytichem.com/spectroscopy/Feature/Speciation-ofMercury-in-Crude-Oil-UsingSpeciated/ArticleStandard/Article/detail/655117 

G. M. Mizanur Rahman, et. al. 

 01-01-10 10 36/45 

6800 Sec 16 (31) 

Speciation of Mercury in whole human blood by SIDMS SPME-GC-ICP-MS with Microwave 

Assisted Equilibration and Extraction 

Supports Publication; 

Copyrighted Material 

G. M. Mizanur Rahman, et. al. 

6800 Sec 16 (32) 

Comparison of methods with respect to efficiencies, recoveries, and quantitation of mercury species interconversions in food demonstrated using tuna fish 

 This article describes the authors’ evaluation of eight different analytical extraction procedures for mercury from biological samples. 

Supports Publication; 

Copyrighted Material 

Analytical Bioanalytical Chemistry, 390, 

2123-2132, 2008, http://www.ncbi.nlm.nih.gov/pubmed/18317738 

Laura H. Reyes, et. al. 04-08 10 2123/2132 

6800 Sec 16 (33) 

Zinc Dietary Supplement Contamination with Toxic Antimony Species 

Gregory M. Zinn, et. al. 

6800 Sec 16 (34) 

Glyphosate by IDMS and i-Spike IDMS as for 

Automated and Safe Toxic MS Analysis 

Rebecca L. Wagner, et. al. 

6800 Sec 16 (35) 

Glutathione analysis as a biomarker for immune stress and autism 

Timothy Fahrenholz, et. al. 

6800 Sec 16 (36) 

Human Gene Therapy Michael Passineau, et. al. 

6800 Sec 16 (37) 

Hexavalent Chromium in Contaminated Soil (High Level) 

 This documentation is a certificate of analysis for high level hexavalent chromium in contaminated soil. 

Supports Publication; 

Copyrighted Material 

NIST Certificate of Analysis SRM 2701, 2009, https://wwws.nist.gov/srmors/view_detail.cfm?srm=2701 

NIST 03-10-02 1 0/0 

6800 Sec 16 (38) 

 Development of a standard reference material for Cr(VI) in contaminated soil 

 This article describes the development of a standard reference material for hexavalent chromium including the collection, processing, preparation, and preliminary physicochemical characterization of the material. 

Supports Publication; 

Copyrighted Material 

Journal of Analytical Atomic Spectroscopy, 23, 1550-1554, 2008, http://pubs.rsc.org/en/Content/ArticleLanding/2008/JA/b808488b 

Stuart Nagourney, et. al. 09-29-08 5 1550/1554 

6800 Sec 16 (39) 

Characterization of waste – Stat of the art document – Chromium VI specification in solid matrices 

Supports Publication; 

Copyrighted Material 

PD CEN/TR 14589:2003, British Standards, EU publication “International Standards Correspondence Index, Technical Report CEN Technical Committee CEN/TC 292, European Committee for Standardization, 2003 

 04/03 

6800 Sec 16 (40) 

Sodium Azide Quantification for homeland defense by isotope dilution mass spectrometry EPA Method 6800 

Gregory M. Zinn, et. al. 
6800 Sec 16 

(41) 

Investigation into mercury bound to biothiols: structural identification using ESI-ion-trap MS and

introduction of a method for their HPLC separation with simultaneous detection by ICP-MS and ESIMS 

 In this article, authors describe a technique for the separation and molecular identification of mercury and methylmercury complexes derived from their reactions with cysteine and glutathione. 

Supports Publication; 

Copyrighted Material 

Analytical Bioanalytical Chemistry, 390, 

1753-1764, 2008, http://www.springerlink.com/content/y7276028411l8p53/fulltext.pdf 

Eva Krupp, et. al. 04-08 12 1753/1764 

6800 Sec 16 (42) 

US AIR FORCE Task Reports for the Homeland Security and Homeland Defense: extension of EPA Method 6800 conducted between 2007 and 2010 with funding from the Headquarters of the US Air Force Surgeon General under the awards No.FA7014-07-0014 and No.FA7014-08-C-0029 

H. M. Skip Kingston, et. al. 

6800 Sec 16 (43) 

Timothy Fahrenholz, Scott Faber, H. M. Skip 

Kingston, John Kern, Matt Pamuku, Hemasudha Chatragadda, Becky Pekar, “Quantification Glutathione Biomarkers in 

Autism” (in preparation 2012). 

Supports Publication; 

Copyrighted Material 

Will be available from journal at time of publishing 

6800 Sec 16 (44) 

Rebecca L. Wagner, Stephanie Wetzel, H. M. Skip Kingston“ Direct Speciated Isotope Dilution Mass Spectrometry of Analytical Methodology of Illicit Drug in Urine Using Time-of-Flight Mass Spectrometry” (in review 2012). 

Supports Publication; 

Copyrighted Material 

Will be available from journal at time of publishing 

8000D METHOD 8000D 

DETERMINATIVE CHROMATOGRAPHIC SEPARATIONS 

Method 8000 is not a determinative method but instead provides guidance on analytical chromatography and describes calibration and QC requirements common to all SW-846 chromatographic methods. 

method SW-846 03-12 PDF 56 1/56 

8000D (1) Department of Defense: 

Appendix G of DoD “Quality Systems Manual for 

Environmental Laboratories”, Version 4.2 

Supports Publication; 

Copyrighted Material 

http://www.denix.osd.mil/edqw/upload/QSM-V4-2-Final-102510.pdf

8000D (2) U.S.E.P.A Contract Laboratory Program SOM01.2 Supports Publication; 

Copyrighted Material 

http://www.epa.gov/superfund/programs/clp/som1.htm

8000D (3) A list of quantitation limits for poorly-performing 

volatile compounds can be found in Table App D XIII-1 

Supports Publication; 

Copyrighted Material 

http://www.epa.gov/region1/oeme/appendc.pdf

8000D (4) A list of quantitation limits for poorly-performing 

semivolatile compounds can be found in Table 

App E XIII-1 

Supports Publication; 

Copyrighted Material 

http://www.epa.gov/region1/oeme/appendd.pdf

8021B METHOD 8021B 

AROMATIC AND HALOGENATED VOLATILES 

BY GAS CHROMATOGRAPHY USING PHOTOIONIZATION AND/OR ELECTROLYTIC CONDUCTIVITY DETECTORS 

Method 8021B is used to determine volatile organic compounds in a variety of solid waste matrices. 

Method SW-846 12-96 PDF 19 1/19 

8021B (1) “Volatile Organic Compounds in Water by Purgeand-Trap Capillary Column Gas Chromatography 

with Photoionization and Electrolytic Conductivity Detectors in Series, Method 502.2, Rev. 2.0 (1989); Methods for the Detection of Organic Compounds in Drinking Water,” U.S. Environmental Protection Agency, Environmental Monitoring Systems Laboratory, Cincinnati, OH, EPA/600/4-88/039, December, 1988. 

Supports Publication; 

Copyrighted Material 

http://www.caslab.com/EPAMethods/PDF/502_2.pdf 1995 PDF 35 1/35 
8021B (2) “The Determination of Halogenated Chemicals in 

Water by the Purge and Trap Method,” Method 502.1; U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory, Cincinnati, OH 45268, September 1986. 

Supports Publication; 

Copyrighted Material 

 09-86 

8021B (3) “Volatile Aromatic and Unsaturated Organic 

Compounds in Water by Purge and Trap Gas Chromatography, Method 503.1;” U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory, Cincinnati, OH, September 1986. 

Supports Publication; 

Copyrighted Material 

8021B (4) Trace Analyses for Wastewaters Supports Publication; 

Copyrighted Material 

Environ. Sci. Technol., 1981, 15, 1426. http://pubs.acs.org/doi/abs/10.1021/es00094a002 

J. A. Glaser, et. al. 1981 PDF 10 1426/1435 

8021B (5) The Determination of Synthetic Organic 

Compounds in Water by Purge and Sequential Trapping Capillary Column Gas Chromatography 

Supports Publication; 

Copyrighted Material 

U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory, Cincinnati, OH 45268. http://books.google.com/books/about/The_Determination_of_Synthetic_Organic_C.html?id=Sdr5GwAACAAJ 

T. A. Bellar, et. al. 1985 70 

8111 METHOD 8111 

HALOETHERS BY GAS CHROMATOGRAPHY 

This method is a gas chromatographic method used to determine the concentration of haloethers. 

Method SW-846 12-1996 PDF 13 1/13 

8111 (1) Application of Open-Tubular Columns to SW-846 

GC Methods 

Supports Publication; 

Copyrighted Material 

Final Report to the US EPA on Contract 68-03-3511, Mid-Pacific Environmental Laboratory, Mountain View, CA, 1990. 

V. Lopez-Avila, et. al. 1990 

8111 (2) Performance Data for Methods 8041, 8091, 8111, 

and 8121A 

Supports Publication; 

Copyrighted Material 

Draft Report to US EPA on Contract 68-W9-0011, Science Applications International Corp., San Diego, CA, 1992. 

S. Tsang, et. al. 1992 

8270D METHOD 8270D 

SEMIVOLATILE ORGANIC COMPOUNDS BY GAS CHROMATOGRAPHY/MASS SPECTROMETRY (GC/MS) 

This method is used to determine the concentration of semivolatile organic compounds in extracts prepared from many types of solid waste matrices, soils, air sampling media and water samples. 

Method SW-846 02-07 PDF 68 1/68 

8270D (1) Reference Compound to Calibrate Ion Abundance 

Measurement in Gas Chromatography-Mass Spectrometry Systems 

Supports Publication; 

Copyrighted Material 

Analytical Chemistry, 47, 995-1000, 1975. 

http://pubs.acs.org/doi/abs/10.1021/ac60357a061 

J. W. Eichelberger, et. al. 1975 6 995/1000 

8270D (2) Method Detection Limit for Methods 924 and 625 Supports Publication; 

Copyrighted Material 

Unpublished report, October 1980. P. Olynk, et. al. 10-80 

8270D (3) Interlaboratory Method Study for EPA Method 

625-Base/Neutrals, Acids, and Pesticides 

Supports Publication; 

Copyrighted Material 

Final Report for EPA Contract 68-03-3102. 

8270D (4) Gas Chromatography for Pesticide Residue 

Analysis: Some Practical Aspects 

Supports Publication; 

Copyrighted Material 

Journal of the Association of Official 

Analytical Chemists (AOAC), 48, 1037, 

1965. 

J. A. Burke 1965 

8270D (5) GC-MS Suitability Testing of RCRA Appendix VIII 

and Michigan List Analytes 

Supports Publication; 

Copyrighted Material 

U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory, Cincinnati, OH 45268, February 20, 1987, Contract No. 68-03-3224. http://books.google.com/books/about/GC_MS_Suitability_Testing_of_RCRA_Append.html?id=d6yqSgAACAAJ 

S. V. Lucas, et. al. 02-87 8 
8270D (6) Screening of Semivolatile Organic Compounds for 

Extractability and Aqueous Stability by SW-846, Method 3510 

Supports Publication; 

Copyrighted Material 

U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory, Cincinnati, OH 45268, June 5, 1987, Contract 68-03-3224. http://nepis.epa.gov/Exe/ZyNET.exe/2000TMKH.TXT?ZyActionD=ZyDocument&Client=EPA&Index=1986+Thru+1990&Docs=&Query=&Time=&EndTime=&SearchMethod=1&TocRestrict=n&Toc=&TocEntry=&QField=&QFieldYear=&QFieldMonth=&QFieldDay=&IntQFieldOp=0&ExtQFieldOp=0&XmlQuery=&File=D%3A%5Czyfiles%5CIndex%20Data%5C86thru90%5CTxt%5C00000011%5C2000TMKH.txt&User=ANONYMOUS&Password=anonymous&SortMethod=h%7C-&MaximumDocuments=1&FuzzyDegree=0&ImageQuality=r75g8/r75g8/x150y150g16/i425&Display=p%7Cf&DefSeekPage=x&SearchBack=ZyActionL&Back=ZyActionS&BackDesc=Results%20page&MaximumPages=1&ZyEntry=1&SeekPage=x&ZyPURL 

T. M Engel, et. al. 06-87 10 

8270D (7) Development of a Soxtec Extraction Procedure for 

Extraction of Organic Compounds from Soils and Sediments 

Supports Publication; 

Copyrighted Material 

U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory, Las Vegas, NV, October 1991, EPA 600/X-91/140. http://books.google.com/books/about/Development_of_a_Soxtec_Extraction_Proce.html?id=SsA8twAACAAJ 

V. Lopez-Avila 10-91 

8270D (8) Laboratory Validation of VOST and SemiVOST for 

Halogenated Hydrocarbons from the Clean Air Act 

Amendments List 

Supports Publication; 

Copyrighted Material 

Vol. 1 and 2, U.S. Environmental Protection 

Agency, EPA 600/R-93/123a and b, (NTIS 

PB 93-227163 and 93-27171), Research Triangle Park, NC, July 1993. http://nepis.epa.gov/Exe/ZyNET.exe/30003WHW.TXT?ZyActionD=ZyDocument&Client=EPA&Index=1991+Thru+1994&Docs=&Query=&Time=&EndTime=&SearchMethod=1&TocRestrict=n&Toc=&TocEntry=&QField=&QFieldYear=&QFieldMonth=&QFieldDay=&IntQFieldOp=0&ExtQFieldOp=0&XmlQuery=&File=D%3A%5Czyfiles%5CIndex%20Data%5C91thru94%5CTxt%5C00000009%5C30003WHW.txt&User=ANONYMOUS&Password=anonymous&SortMethod=h%7C-&MaximumDocuments=1&FuzzyDegree=0&ImageQuality=r75g8/r75g8/x150y150g16/i425&Display=p%7Cf&DefSeekPage=x&SearchBack=ZyActionL&Back=ZyActionS&BackDesc=Results%20page&MaximumPages=1&ZyEntry=1&SeekPage=x&ZyPURL 

J. Bursey, et. al. 07-93 8 

8270D (9) Single Laboratory Method Validation Report: 

Extraction of Target Compound List/Priority Pollutant List BNAs and Pesticides Using 

Accelerated Solvent Extraction (ASE) with Analytical Validation by GC/MS and GC/ECD 

Supports Publication; 

Copyrighted Material 

Document 101124, Dionex Corporation, Salt Lake City, UT, June 16, 1994. 

B. Richter, et. al. 06-94 

8270D (10) Supercritical Carbon Dioxide Extraction of 

Polycyclic Aromatic Hydrocarbons from Sediments 

Supports Publication; 

Copyrighted Material 

J. Chromatography A, 653, 83-91, (1993). http://www.sciencedirect.com/science/article/pii/002196739380394N 

H. B. Lee, et. al. 1993 9 83/91 

8270D (11) SFE Extraction of PNAs from Solid Matrices Using 

the Dionex 703M SFE Extractor and a Liquid Trap 

Supports Publication; 

Copyrighted Material 

EPA Region III, Central Regional Laboratory, 839 Bestgate Road, Annapolis, MD 21401, December 12, 1994. 

S. Warner 12-94 

8270D (12) 3M Data Submission to EPA Supports Publication; 

Copyrighted Material 

Letter to B. Lesnik, June 27, 1995. C. Markell 06-95 

8270D (13) Determination of Organic Compounds in Drinking 

Water by Liquid-Solid Extraction and Capillary Column Gas Chromatography/Mass Spectrometry 

Supports Publication; 

Copyrighted Material 

USEPA Method 525.2, Environmental Monitoring Systems Laboratory, Office of Research and Development, US EPA, Cincinnati, OH, Revision 2.0, March 1995. http://water.epa.gov/scitech/methods/cwa/upload/525_2-SOCs.pdf 

 03-95 60 1/60 
8270D (14) Analytical Method for the Analysis of Semivolatile 

Organic Compounds 

Supports Publication; 

Copyrighted Material 

USEPA, Superfund Analytical Services/Contract Laboratory Program (CLP), Multi-Media, Multi-Concentration Organics Analysis, SOM01.X, Exhibit D - 

Analytical Methods, November 2003. 

 11-03 

8276 METHOD 8276 

TOXAPHENE AND TOXAPHENE CONGENERS BY GAS CHROMATOGRAPHY/NEGATIVE ION CHEMICAL IONIZATION MASS SPECTROMETRY (GC-NICI/MS) 

Method 8276 is used to determine the concentrations of various toxaphene congeners and technical toxaphene in extracts from solid and liquid matrices, using fused-silica, open-tubular capillary columns with negative ion chemical ionization mass spectrometry (NICI/MS). 

method SW-846 09-12 PDF 57 1/57 

8276 (1) Chemical Ionization Mass Spectrometry Supports Publication; 

Copyrighted Material 

A. G. Harrison 06-15-92 Book 224 1/224 

8276 (2) Determination of Toxaphene in Soil by ElectronCapture Negative Ion Mass Spectrometry After 

Fractionation by High-Performance Gel Permeation Chromatography 

Supports Publication; 

Copyrighted Material 

J. Chromatogr., 633, 177- 183, 1993. http://www.epa.gov/esd/chemistry/organal/reports/toxpf/toxpf.htm 

W. C. Brumley, et. al. 02-24-93 7 177/183 

8276 (3) Analytical Protocol (GC/NIMS) for OSWER’s 

Response to OIG Report (2005-P-00022) on Toxaphene Analysis 

Supports Publication; 

Copyrighted Material 

EPA/600/R-08/048 (TIP # 08-069, Published Report) U.S. Environmental Protection Agency. http://nepis.epa.gov/Adobe/PDF/9100D5NZ.PDF 

W. C. Brumley 02-13-08 17 1/17 

8276 (4) Application of Open-Tubular Columns to SW-846 

GC Methods 

Supports Publication; 

Copyrighted Material 

Report for the U.S. Environmental Protection Agency, Contract 68-03-3511. http://nepis.epa.gov/Exe/ZyNET.exe/30003UMO.TXT?ZyActionD=ZyDocument&Client=EPA&Index=1986+Thru+1990&Docs=&Query=&Time=&EndTime=&SearchMethod=1&TocRestrict=n&Toc=&TocEntry=&QField=&QFieldYear=&QFieldMonth=&QFieldDay=&IntQFieldOp=0&ExtQFieldOp=0&XmlQuery=&File=D%3A%5Czyfiles%5CIndex%20Data%5C86thru90%5CTxt%5C00000006%5C30003UMO.txt&User=ANONYMOUS&Password=anonymous&SortMethod=h%7C-&MaximumDocuments=1&FuzzyDegree=0&ImageQuality=r75g8/r75g8/x150y150g16/i425&Display=p%7Cf&DefSeekPage=x&SearchBack=ZyActionL&Back=ZyActionS&BackDesc=Results%20page&MaximumPages=1&ZyEntry=1&SeekPage=x&ZyPURL 

V. Lopez-Avila et. al. 09-90 12 1/12 

8276 (5) Development and Application of Test Procedures 

for Specific Organic Toxic Substances in Wastewaters 

Supports Publication; 

Copyrighted Material 

Category 10, Pesticides and PCB Report for the U.S. Environmental Protection 

Agency, Contract 68-03-2606. 

http://nepis.epa.gov/Exe/ZyNET.exe/2000V0S8.TXT?ZyActionD=ZyDocument&Client=EPA&Index=1976+Thru+1980&Docs=&Query=&Time=&EndTime=&SearchMethod=1&TocRestrict=n&Toc=&TocEntry=&QField=&QFieldYear=&QFieldMonth=&QFieldDay=&IntQFieldOp=0&ExtQFieldOp=0&XmlQuery=&File=D%3A%5Czyfiles%5CIndex%20Data%5C76thru80%5CTxt%5C00000006%5C2000V0S8.txt&User=ANONYMOUS&Password=anonymous&SortMethod=h%7C-&MaximumDocuments=1&FuzzyDegree=0&ImageQuality=r75g8/r75g8/x150y150g16/i425&Display=p%7Cf&DefSeekPage=x&SearchBack=ZyActionL&Back=ZyActionS&BackDesc=Results%20page&MaximumPages=1&ZyEntry=1&SeekPage=x&ZyPURL 

J. W. Rhoades, et. al. 01-80 89 1/89 

8276 (6) Removal of Elemental Sulfur Interferences from 

Sediment Extracts for Pesticide Analysis 

Supports Publication; 

Copyrighted Material 

Bull. Environ. Contam. Toxicol., 6, 9, 1971. http://www.springerlink.com/content/v4u6174186w55721/ 

D. F. Goerlitz, et. al. 1971 2 9/10 
8276 (7) Residue Analysis of Sediment and Sewage 

Sludge for Organochlorines in the Presence of Elemental Sulfur 

Supports Publication; 

Copyrighted Material 

Anal. Chem., 49, 316-318, 1977. 

http://pubs.acs.org/doi/abs/10.1021/ac50010a033 

S. Jensen, et. al. 02-77 3 316/318 

8276 (8) Gel Permeation Chromatography in the GC/MS

Analysis of Organics in Sludges 

Supports Publication; 

Copyrighted Material 

U.S. Environmental Protection Agency. R. H. Wise, et. al. Book 74 1/74 

8276 (9) Extraction of Chlorinated Hydrocarbon 

Insecticides from Soil 

Supports Publication; 

Copyrighted Material 

Agron. J., 60, 289, 1968. 

https://www.agronomy.org/publications/aj/abstracts/60/3/AJ0600030289 

H. B. Pionke, et. al. 05-68 4 289/292 

8276 (10) Experiments with Evaporation of Solutions of 

Chlorinated Pesticides 

Supports Publication; 

Copyrighted Material 

J. Assoc. Off. Anal. Chem., 49, 999, 1966. J. A. Burke, et. al. 1966 8 999/1006 

8276 (11) Trace Analyses for Wastewaters Supports Publication; 

Copyrighted Material 

Environ. Sci. and Technol., 15, 1426, 1981. http://pubs.acs.org/doi/abs/10.1021/es00094a002 

J. A. Glazer, et. al. 12-81 10 1426/1435 

8276 (12) Performance Data for SW-846 Methods 8270,

8081, and 8141 

Supports Publication; 

Copyrighted Material 

U.S. Environmental Protection Agency, EMSL-Las Vegas, EPA/600/4-90/015. http://nepis.epa.gov/Exe/ZyNET.exe/9100CV89.txt?ZyActionD=ZyDocument&Client=EPA&Index=1986%20Thru%201990&Docs=&Query=&Time=&EndTime=&SearchMethod=1&TocRestrict=n&Toc=&TocEntry=&QField=&QFieldYear=&QFieldMonth=&QFieldDay=&UseQField=&IntQFieldOp=0&ExtQFieldOp=0&XmlQuery=&File=D%3A%5CZYFILES%5CINDEX%20DATA%5C86THRU90%5CTXT%5C00000020%5C9100CV89.txt&User=ANONYMOUS&Password=anonymous&SortMethod=h%7C 

P. J. Marsden 06-90 102 1/120 

8276 (13) Development of a Soxtec Extraction Procedure for 

Extracting Organic Compounds from Soils and Sediments 

Supports Publication; 

Copyrighted Material 

EPA 600/X-91/140, U.S. Environmental Protection Agency, Environmental Monitoring Systems Laboratory 

V. Lopez-Avila (W. Beckert, Project Officer) 

10-91 Book 

8276 (14) Solid-Phase Extraction of TCLP Leachates Supports Publication; 

Copyrighted Material 

Proceedings of the Tenth Annual Waste Testing and Quality Assurance Symposium, Arlington, VA 

C. Markell 07-94 

8276 (15) Supercritical Fluid Extraction of Organochlorine 

Pesticide Residues from Soils 

Supports Publication; 

Copyrighted Material 

Proceedings of the Tenth Annual Waste Testing and Quality Assurance Symposium, Arlington, VA 

D. Bennett, et. al. 07-94 

8276 (16) 3M Data Submission to EPA Supports Publication; 

Copyrighted Material 

Letter to B. Lesnik C. Markell 06-27-95 Letter 

8276 (17) Single Laboratory Method Validation Report – 

Extraction of Organophosphorus Pesticides, Herbicides, and Polychlorinated Biphenyls Using 

Accelerated Solvent Extraction (ASE) with Analytical Validation by GC/NPD and GC/ECD 

Supports Publication; 

Copyrighted Material 

Dionex, Document 101124, Salt Lake City, UT 

B. Richter, et. al. 12-02-94 

8276 (18) Evaluation of Rapid Solid Sample Extraction 

Using the Microwave-Assisted Process (MAPTM) 

Under Closed-Vessel Conditions 

Supports Publication; 

Copyrighted Material 

Spectros. Int. J., 13 (1), 1-14, 1997. http://www.cem.de/documents/pdf/RE/RE036.PDF 

K. Li, et. al. 1996/1997 PDF 13 1/13 

8276 (19) Pulsed Positive Ion Negative Ion Chemical

Ionization Mass Spectrometric Applications to Environmental and Hazardous Waste Analysis 

Supports Publication; 

Copyrighted Material 

Biomed. Mass Spectrom. 10, 369, 1983. L. D. Betowski, et. al. 12-12-83 8 369/376 

8276 (20) Interlaboratory Study Plan for Validation of 

Method 8276 

Supports Publication; 

Copyrighted Material 

Submitted to U.S. Environmental Protection 

Agency 

Science Applications International Corporation 

09-08 

8276 (21) USEPA Region 4 Modified Method 3545A 

Standard Operating Procedure (SOP) for Pressurized Fluid Extraction (PFE) 

Supports Publication; 

Copyrighted Material 

Revision 4.1 11-05-10 

8276 (22) USEPA Region 4 Modified Method 3620C, SOP

for Florisil® Cleanup 

Supports Publication; 

Copyrighted Material 

Revision 3.0 08-23-10 

8276 (23) USEPA Region 4 Modified Method 3630C SOP 

for Silica Gel Cleanup 

Supports Publication;

Copyrighted Material 

Revision 3.1 08-10-11 

8276 (24) Inter-laboratory Validation for Fish Tissue Study 

Plan 

Supports Publication; 

Copyrighted Material 

Submitted to U.S. Environmental Protection 

Agency 

TechLaw Incorporated 09-11 
8276 (25) Inter-laboratory Validation for Fish Tissue 

Analytical Data Report 

Supports Publication; 

Copyrighted Material 

Submitted to U.S. Environmental Protection 

Agency 

TechLaw Incorporated 05-12 

8276 (26) Inter-laboratory Validation for Fish Tissue Data 

Validation Report 

Supports Publication; 

Copyrighted Material 

Submitted to U.S. Environmental Protection 

Agency 

TechLaw Incorporated 05-12 

8276 (27) Inter-laboratory Validation for Fish Tissue 

Statistical Analysis Report 

Supports Publication; 

Copyrighted Material 

Submitted to U.S. Environmental Protection 

Agency 

TechLaw Incorporated 05-12 

8276 (28) HRGC and HRGC-ECNI Determination of 

Toxaphene Residues in Fish with a New 22 Components Standard 

Supports Publication; 

Copyrighted Material 

Organohalogen Compd., 26, 357, 1995. http://www.dioxin20xx.org/pdfs/1995/95-279.pdf 

H. Parlar, et. al. 1995 PDF 6 357/362 

8410 METHOD 8410 

GAS CHROMATOGRAPHY/FOURIER TRANSFORM INFRARED (GC/FT-IR) SPECTROMETRY FOR SEMIVOLATILE ORGANICS: CAPILLARY COLUMN 

This method covers the automated identification, or compound class assignment of unidentifiable compounds, of solvent extractable semivolatile organic compounds which are amenable to gas chromatography, by GC/FT-IR. 

Method SW-846 09-94 PDF 17 1/17 

8410 (1) Handbook for Analytical Quality Control in Water 

and Wastewater Laboratories 

Supports Publication; 

Copyrighted Material 

U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory. ORD Publication Offices of Center for Environmental Research Information: Cincinnati, OH, March 1979; Sec. 4, EPA-600/4-79-019. http://nepis.epa.gov/Exe/ZyPURL.cgi?Dockey=30000PWG.txt 

 03-79 164 1/164 

8410 (2) Quantitative Analysis Using a Purged Splitless 

Injection Technique 

Supports Publication; 

Copyrighted Material 

Hewlett Packard Application Note, ANGC 7-79. 

R. R. Freeman 

8410 (3) Tables of Wavenumbers for the Calibration of 

Infrared Spectrometers 

Supports Publication; 

Copyrighted Material 

Pergamon: New York, 1977. http://books.google.com/books/about/Tables_of_wavenumbers_for_the_calibratio.html?id=i7_vAAAAMAAJ 

R. H. Cole 1977 219 

8410 (4) Criteria for Presentation of Spectra from 

Computerized IR Instruments 

Supports Publication; 

Copyrighted Material 

Appl. Spectrosc. 1982, 36, 87. 

http://www.opticsinfobase.org/as/abstract.cfm?id=127579 

J. G. Grasselli, et. al. 1982 5 87/91 

8410 (5) The Interpretation of Vapor-Phase Infrared

Spectra 

Supports Publication; 

Copyrighted Material 

Group Frequency Data; Volume I. Sadtler Laboratories: Philadelphia, PA, 1984. 

R. A. Nyquist 1984 

8410 (6) Infrared Characteristic Group Frequencies Supports Publication; 

Copyrighted Material 

John Wiley and Sons: New York, NY, 1980. http://www.amazon.com/InfraredCharacteristic-Group-FrequenciesSocrates/dp/0471275921 

G. Socrates 1980 Book 166 

8410 (7) The infrared Spectra of Complex Organic 

Molecules 

Supports Publication; 

Copyrighted Material 

2nd ed.; John Wiley and Sons: New York, 

NY, 1958. http://www.amazon.com/infra-red-spectracomplexmolecules/dp/B007T3ZVP0/ref=sr_1_2?s=books&ie=UTF8&qid=1355851489&sr=1-2&keywords=infrared+spectra+complex+molecules 

L. J. Bellamy 1958 

8410 (8) Infrared Band Handbook Supports Publication; 

Copyrighted Material 

Volumes I and II; Plenum: New York, NY, 1965. 

H. A. Szymanski 1965 

8410 (9) Interim Protocol for the Automated Analysis of 

Semivolatile Organic Compounds by Gas Chromatography/Fourier Transform-Infrared Spectrometry 

Supports Publication; 

Copyrighted Material 

Appl. Spectrosc. 1985, 39, 826. 

http://www.opticsinfobase.org/as/abstract.cfm?uri=as-39-5-827 

D. F. Gurka 1985 7 827/833 

8410 (10) Capillary GC/FT-IR Supports Publication; 

Copyrighted Material 

Anal. Chem. 1983, 55, 1361A. 

http://pubs.acs.org/doi/abs/10.1021/ac00263a784 

P. R. Griffiths, et. al. 1983 27 1361A/1387

A 

8410 (11) Fourier Transform-Infrared Spectrometry Supports Publication; 

Copyrighted Material 

Wiley-Interscience: New York, NY, 1986. http://onlinelibrary.wiley.com/doi/10.1002/9780470106310.fmatter/pdf 

P. R. Griffiths, et. al. 1986 16 
8410 (12) Quantitation Capability of a Directly Linked Gas 

Chromatography/Fourier Transform Infrared/Mass Spectrometry System 

Supports Publication; 

Copyrighted Material 

Anal. Chem. 1989, 61, 1584. 

http://pubs.acs.org/doi/pdf/10.1021/ac00189a022 

D. F. Gurka, et. al. 1989 6 1584/1589 

8430 METHOD 8430 

ANALYSIS OF BIS(2-CHLOROETHYL) ETHER AND HYDROLYSIS PRODUCTS BY DIRECT AQUEOUS INJECTION GC/FT-IR 

This method provides procedures for the identification and quantitation of bis(2-chloroethyl) ether and its hydrolysis compounds in aqueous matrices by direct aqueous injection and gas chromatography with detection by a fourier transform infrared spectrometer. 

Method SW-846 12-96 PDF 11 1/11 

8430 (1) Identification of Bis(2-chloroethyl) ether Hydrolysis 

Products by Direct Aqueous Injection GC/FT-IR 

Supports Publication; 

Copyrighted Material 

J. of High Res. Chrom. 12, 693-696, 1989. http://onlinelibrary.wiley.com/doi/10.1002/jhrc.1240121016/abstract 

W. D. Payne, et. al. 1989 4 693/696 

9013 METHOD 9013A 

CYANIDE EXTRACTION PROCEDURE FOR SOLIDS AND OILS 

The extraction procedure described in this method is designed for the extraction of soluble and insoluble cyanides from solid, oil, and multiphase wastes. The resulting extraction solutions may be analyzed for total cyanide and/or cyanides amenable to chlorination (e.g., Methods 9010, 9012 and 9014) as well as analyzed for metal cyanide complexes (e.g., Method 9015). 

method SW-846 03-12 PDF 13 1/13 

9013 (1) 

American Society for Testing and Materials, 

"Understanding Cyanide Species," D 6696, ASTM International, 2004. 

Supports Publication; 

Copyrighted Material 

www.astm.org. 

9013 (2) R. S. Ghosh, D. A. Dzombak, R. G. Luthy, 

"Equilibrium Precipitation and Dissolution of Iron Cyanide Solids in Water," Environ. Eng. Sci., Vol. 16, 293-313, 1999. 

Supports Publication; 

Copyrighted Material 

9013 (3) J. C. L. Meeussen, M. G. Keizer, W. H. van 

Riemsdijk, F. A. M. de Haan, "Dissolution Behavior of Iron Cyanide (Prussian Blue) in Contaminated Soils," Environ. Sci. Technol., Vol. 26, 1832-1838, 1992. 

Supports Publication; 

Copyrighted Material 

9013 (4) J. C. L Meeussen, W. H. Keizer, F. A. M. de 

Haan, "Chemical Stability and Decomposition Rate of Iron Cyanide Complexes in Soil Solutions," Environ. Sci. Technol., Vol. 26, 511-516, 1992. 

Supports Publication; 

Copyrighted Material 

9013 (5) J. T. Bushey, D. A. Dzombak, "Ferrocyanide 

Adsorption on Aluminum Oxides," J. Coll. Int. Sci.,

Vol. 272, 46-51, 2004. 

Supports Publication; 

Copyrighted Material 

9013 (6) T. L. Theis, M. L West, "Effects of Cyanide 

Complexation on the Adsorption of Trace Metals at the Surface of Goethite," Environ. Technol. Letters, Vol. 7, 309-318, 1986. 

Supports Publication; 

Copyrighted Material 

9013 (7) The RETEC Group, Inc., "Metal Cyanide 

Complexes by Anion Exchange Chromatography and UV Detection Method Validation Summary Report," March, 2004. 

Supports Publication; 

Copyrighted Material 
9014 METHOD 9014 

CYANIDE IN WATERS AND EXTRACTS USING TITRIMETRIC AND MANUAL SPECTROPHOTOMETRIC PROCEDURES 

This method can be used for 

measuring free (non-complexed) cyanide and hydrocyanic acid in drinking water, natural surface waters, domestic and industrial wastewaters, and in soil extracts. This method may also be used as a determinative step for quantifying total and amenable cyanide in the alkaline distillates from Method 9010. 

method SW-846 03-12 PDF 13 1/13 

9015 METHOD 9015 

METAL CYANIDE COMPLEXES IN WATERS 

AND WASTE EXTRACTS USING ANION EXCHANGE CHROMATOGRAPHY AND 

UV DETECTION 

This method covers the determination of metal cyanide complexes in waters and extracts of solid wastes using anion exchange chromatography and UV detection (Refs. 1, 2). The following analytes have been determined by this method: 

Analyte 

[Ag(CN)2]- [Au(CN)2]- [Co(CN)6]3- [Cu(CN)3]2- [Fe(CN)6]3- [Fe(CN)6]4- [Ni(CN)4]2- method SW-846 03-12 PDF 53 1/53 

9015 (1) Standard Test Method for Determination of Metal 

Cyanide Complexes in Wastewater, Surface Water, Groundwater and Drinking Water using 

Anion Exchange Chromatography with UV 

Detection 

Supports Publication; 

Copyrighted Material 

D 6994, ASTM International, 2004 American Society for Testing 

and Materials 

9015 (2) Determination of Metal Cyanides This application note describes a 

method for determining concentration of transition metal cyanides by anion exchange chromatography. 

Supports Publication; 

Copyrighted Material 

Dionex Application Note No. 55, November, 1989, http://www.dionex.com/enus/webdocs/4151-AN55_V15.pdf 

Dionex Corporation 11-89 3 0/0 

9015 (3) Standard Guide for Understanding Cyanide 

Species 

Supports Publication; 

Copyrighted Material 

D 6696, ASTM International, 2004 American Society for Testing 

and Materials 

9015 (4) Equilibrium Precipitation and Dissolution of Iron 

Cyanide Solids in Water 

 In this article the equilibrium solubility behavior of iron cyanide solids was studied as a function of pH, pE, and other solution conditions. 

Supports Publication; 

Copyrighted Material 

Environ. Eng. Sci., Vol. 16, 293-313, 1999, http://cat.inist.fr/?aModele=afficheN&cpsidt=1890662 

R. S. Ghosh, et. al. 07-01-99 21 293/313 

9015 (5) Chemical Stability and Decomposition Rate of Iron 

Cyanide Complexes in Soil Solutions 

 This article investigates the speciation of dissolved cyanide under certain conditions relevant to soil and groundwater environments. 

Supports Publication; 

Copyrighted Material 

Environ. Sci. Technol., Vol. 26, 511-516, 1992, http://pubs.acs.org/doi/abs/10.1021/es00027a010

J. C. L. Meeussen, et. al. 03-92 6 511/516 

9015 (6) Dissolution Behavior of Iron Cyanide (Prussian 

Blue) in Contaminated Soils 

Supports Publication; 

Copyrighted Material 

Environ. Sci. Technol., Vol. 26, 1832-1838, 1992

J. C. L. Meeussen, et. al. 

9015 (7) Cyanide Extraction Procedure for Solids and Oils, 

Method 9013 

Supports Publication; 

Copyrighted Material 

U.S. EPA Office of Solid Waste SW-846 Manual 

US EPA 
9015 (8) Toxicity to Fish of Cyanides and Related 

Compounds: A Review 

In this review the toxicity of cyanides and related compounds on fish are examined. 

Supports Publication; 

Copyrighted Material 

EPA Report No. 600/3-76-038, 1976 P. Doudoroff 04-76 155 1/155 

9015 (9) Total and Amenable Cyanide: Distillation, Method 

9010 

Supports Publication; 

Copyrighted Material 

U.S. EPA Office of Solid Waste SW-846 Manual 

US EPA 

9015 (10) "Standard Test Methods for Cyanides in Water Supports Publication; 

Copyrighted Material 

D 2036, ASTM International, 2004 

9015 (11) Standard Methods for the Examination of Water 

and Wastewater 

American Public Health Association 

9015 (12) Determination of Trace Level Ions by Ion 

Chromatography with Concentrator Columns 

In this article ion chromatography techniques used to perform trace analysis down to 2 ppb for anions in solution are described. 

Supports Publication; 

Copyrighted Material 

Analytical Chemistry, Vol. 15, No. 9, 1532-

1535, 1979, http://pubs.acs.org/doi/abs/10.1021/ac50045a040 

R. A. Wetzel, et. al. 08-79 4 1532/1535 

9015 (13) Sunlight-Induced Photochemistry of Aqueous 

Solutions of Hexacyanoferrate(II) and –(III) Ions 

This article investigates the photochemically induced processes in alkaline aqueous solutions of hexacyanoferrate (II) and -(III). 

Supports Publication; 

Copyrighted Material 

Environ. Sci. Technol., Volume 27, 1875-1879, 1993, http://pubs.acs.org/doi/abs/10.1021/es00046a016 

W. S. Rader, et. al. 09-93 5 1875/1879 

9015 (14) Photochemistry of Co-ordination Compounds_XV This article investigates the 

photochemical behaviour of some cyanide complexes at various wavelenghts. 

Supports Publication; 

Copyrighted Material 

J. inorg. Nucl. Chem., Vol. 28, 2589-2597, 1966, http://www.sciencedirect.com/science/article/pii/0022190266803834 

L. Moggi, et. al. 9 2589/2597 

9015 (15) Product Manual IonPacÒ ATC-3 2-mm Anion 

Trap Column IonPac ATC-3 4-mm Anion Trap Column IonPac ATC-HC Anion Trap Column 

This manual describes how to prepare these columns for operation in the laboratory. 

Supports Publication; 

Copyrighted Material 

Document No. 032697, Revision 08, July 12, 2002, http://www.dionex.com/enus/webdocs/40850-32697-08_IonPacATCHC_3_MAN_V16.pdf 

Dionex Corporation 7-12-02 12 1/12 

9015 (16) Product Manual IonPac® AG2 Guard Column 

IonPac® AG3 Guard Column IonPac® AG4 Guard Column IonPac® AG5 Guard Column IonPac® CG2 Guard Column IonPac® AS2 

Analytical Column IonPac® AS3 Analytical 

Column IonPac® AS4 Analytical Column IonPac® 

AS5 Analytical Column IonPac® CS2 Analytical 

Column 

This manual describes how to prepare these columns for operation in the laboratory. 

Supports Publication; 

Copyrighted Material 

Document No. 032226, Revision 14, May 12, 2002, http://www.dionex.com/enus/webdocs/4395-32226-14_AS2345_CS2_V17.pdf 

Dionex Corporation 05-12-02 14 1/14 

9015 (17) Product Manual IonPac® AG11 Guard Column 

IonPac® AS11 Analytical Column 

This manual is for the IonPac® 

AS/AG11 analytical columns designed 

to resolve a large number of inorganic and organic acid ions from a single sample injection in one gradient run. 

Supports Publication; 

Copyrighted Material 

Document No. 034791, Revision 08, May 14, 2003, http://www.dionex.com/enus/webdocs/4445-Man-034791-12-IonPacAS11-Apr10.pdf 

Dionex Corporation 05-14-03 44 1/44 

9015 (18) Dionex Installation and Troubleshooting Guide for 

the IonPacÒ MFC-1 Metal-Free Trap Column 

This manual is for the metal-free trap column which is specifically designed for on-line cleanup of eluent ionic transition metal impurities in ion chromatography. 

Supports Publication; 

Copyrighted Material 

Document No. 034990, Revision 02, June 26, 1998, http://www.dionex.com/enus/webdocs/4463-34990-04_IP_MFC_V30.pdf 

Dionex Corporation 11-06 4 1/4 
9015 (19) Determinative Chromatographic Separations, 

Method 8000 

Supports Publication; 

Copyrighted Material 

U.S. EPA Office of Solid Waste SW-846 Manual 

US EPA 

9015 (20) NIST Critically Selected Stability Constants of 

Metal Complexes Database, Version 5.0 Database Software 

Supports Publication; 

Copyrighted Material 

NIST Standard Reference Database 46, U.S. Department of Commerce, Gaithersburg, Maryland, 1998 

R. M. Smith, et. al. 

9015 (21) The NBS Tables of Chemical Thermodynamic 

Properties, Selected Values for Inorganic and C1

and C2 Organic Substances in SI Units 

Supports Publication; 

Copyrighted Material 

Journal of Physical and Chemical Reference Data, Vol. 11, Supplement 2, 1-392, 1982 

D. D. Wagman, et. al. 

9015 (22) Metal Cyanide Complexes by Anion Exchange

Chromatography and UV Detection Method Validation Summary Report 

The RETEC Group, Inc. 03-04 

9015 (23) Total and Amenable Cyanide (Automated 

Colorimetric, with Off-Line Distillation), Method 9012 

 U.S. EPA Office of Solid Waste SW-846 

Manual 

US EPA 

Method 9320 Radium 228 This method covers the measurement 

of radium-228 in ground water and, if desired, the determination of radium226 on the same sample. If the level of radium-226 is above 3 pCi/L, the sample must also be measured for radium-228. 

 Method 06-12 PDF 13 1/13 

9320 (1) Standard Methods for the Examination of 

Water and Wastewater, 15th ed., 

Supports Publication; 

Copyrighted Material 

Method 707, p. 600, 1980. http://www.standardmethods.org/ 

Greenberg, A.E., J.J. Connors, and D.J. Jenkens, eds. 

1980 600 

9320 (2) Determination of Radium 228 in Natural Waters. 

Radiochemical Analysis of Water. U.S. Govt. Printing Office, Washington, D.C., 1971. 

Supports Publication; 

Copyrighted Material 

U.S. Geol. Surv., Water Supply Paper 1696-G. http://pubs.usgs.gov/wsp/1696g/report.pdf 

Johnson, J.O. 1971 PDF 152 1/152 

9320 (3) Prescribed Procedures for Measurement of 

Radioactivity in Drinking Water,. 

Supports Publication; 

Copyrighted Material 

Environmental Monitoring and Support Laboratory, U.S. EPA, Cincinnati, OH, EPA-600/4-75-008, http://nepis.epa.gov/ 

Krieger, H.L. 1976 PDF 33 1/33 

Chapter 1 Project Quality Assurance and Quality Control The goal of this chapter is to provide 

an understanding of environmental data and the need for quality. 

Chapter SW-846 USEPA 03-12 PDF 25 1/25 

Chapter 1 (1) Guidance on Systematic Planning Using the Data 

Quality Objectives Process 

Supports Publication; 

Copyrighted Material 

EPA QA/G-4, Quality Staff, Office of Environmental Information, United States Environmental Protection Agency, Washington, D.C. February 2006. http://www.epa.gov/quality/qs-docs/g4-final.pdf 

 USEPA 02-06 PDF 121 1/111 

Chapter 1 (2) EPA Quality Manual for Environmental Programs 

CIO 2105-P-01-0 

Supports Publication; 

Copyrighted Material 

Office of Environmental Information Quality Staff, United States Environmental Protection Agency, Washington, D.C. May 5, 2000.

http://www.epa.gov/irmpoli8/policies/2105P010.pdf 

USEPA 05-05-00 PDF 63 0/0 

Chapter 1 (3) Guidance on Choosing a Sampling Design for 

Environmental Data Collection 

Supports Publication; 

Copyrighted Material 

EPA QA/G-5S, Quality Staff, Office of Environmental Information, United States Environmental Protection Agency, Washington, D.C. December 2002.

http://www.epa.gov/quality/qs-docs/g5sfinal.pdf 

USEPA 12-02 PDF 178 1/166 

Chapter 1 (4) Guidance on Environmental Data Verification and 

Data Validation 

Supports Publication; 

Copyrighted Material 

EPA QA/G-8, Quality Staff, Office of Environmental Information, United States Environmental Protection Agency, Washington, D.C. November 2002.

http://www.epa.gov/quality/qs-docs/g8-final.pdf 

USEPA 11-02 PDF 96 1/76 
Chapter 1 (5) Data Quality Assessment: A Reviewer’s Guide Supports Publication; 

Copyrighted Material 

QA/G-9R, Quality Staff, Office of Environmental Information, United States Environmental Protection Agency, Washington, D.C. February 2006.http://www.epa.gov/quality/qs-docs/g9rfinal.pdf 

USEPA 02-06 PDF 61 1/55 

Chapter 1 (6) Data Quality Assessment: Statistical Tools for 

Practitioners 

Supports Publication; 

Copyrighted Material 

QA/G-9S, Quality Staff, Office of Environmental Information, United States Environmental Protection Agency, Washington, D.C. February 2006.

http://www.epa.gov/quality/qs-docs/g9sfinal.pdf 

USEPA 02-06 PDF 198 1/191 

Chapter 1 (7) Guidance for Preparing Standard Operating 

Procedures 

Supports Publication; 

Copyrighted Material 

EPA QA/G-6, Quality Staff, Office of Environmental Information, United States Environmental Protection Agency, Washington, D.C. April 2007.

http://www.epa.gov/quality/qs-docs/g6-final.pdf 

USEPA 04-07 PDF 60 1/55 

Chapter 1 (8) RCRA Waste Sampling Draft Technical Guidance Supports Publication; 

Copyrighted Material 

Office of Solid Waste, United States Environmental Protection Agency, Washington, D.C. August 2002. http://www.epa.gov/wastes/hazard/testmethods/sw846/pdfs/rwsdtg_a.pdf 

USEPA 08-02 PDF 61 1/49 

Chapter 1 (9) Guidance for Quality Assurance Project Plans Supports Publication; 

Copyrighted Material 

EPA QA/G-5, Quality Staff, Office of Environmental Information, United States Environmental Protection Agency, Washington, D.C. December 2002.http://www.epa.gov/quality/qs-docs/g5-final.pdf 

USEPA 12-02 PDF 111 1/58 

Chapter 1 (10) EPA Requirements for Quality Assurance Project 

Plans 

Supports Publication; 

Copyrighted Material 

EPA QA/R-5, Office of Environmental Information. United States Environmental Protection Agency, Washington, D.C. March 2001. http://www.epa.gov/quality/qsdocs/r5-final.pdf 

USEPA 03-01 PDF 40 1/24 

Chapter 1 (11) RCRA Delisting Program Guidance Manual for the 

Petitioner 

Supports Publication; 

Copyrighted Material 

United States Environmental Protection 

Agency, March 23, 2000. 

http://www.epa.gov/region6/6pd/rcra_c/pdo/delist23.pdf 

USEPA 03-23-00 PDF 61 1/57 

Chapter 1 (12) Waste Analysis at Facilities That Generate, Treat, 

Store and Dispose of Hazardous Wastes, ECDIC 2002-011 

Supports Publication; 

Copyrighted Material 

Office of Waste Programs Enforcement, United States Environmental Protection 

Agency. April 1994.

http://www.epa.gov/compliance/resources/policies/civil/rcra/wasteanalygman-rpt.pdf 

USEPA 04-94 PDF 200 0/0 

Chapter 1 (13) Guidance on Technical Audits and Related 

Assessments for Environmental Data Operations 

Supports Publication; 

Copyrighted Material 

QA/G-7, Quality Staff, Office of Environmental Information, United States Environmental Protection Agency, Washington, D.C. January 2000.http://www.epa.gov/quality/qs-docs/g7-final.pdf 

USEPA 01-00 PDF 101 1/78 
Chapter 2 CHOOSING THE CORRECT PROCEDURE The purpose of this chapter is to aid 

the analyst in choosing the appropriate methods for sample analyses, based upon the sample matrix and the analytes to be determined. 

Chapter SW-846 USEPA 03-12 PDF 86 1/86 

Chapter 2 (1) TOC Determinations in Ground Water This article describes the evaluation of 

a modified TOC procedure that permits the quantitation of the VOC fraction in ground water samples. 

Supports Publication; 

Copyrighted Material 

Ground Water 1984, 22(1), 18-24, 

http://info.ngwa.org/gwol/pdf/840629056.PDF 

M. J. Barcelona 01-84 7 18/24 

Chapter 2 (2) Development and Evaluation of Methods for Total 

Organic Halide and Purgeable Organic Halide in Wastewater 

This article describes the laboratory evaluation of two approaches for determining total purgeable and nonpurgeable organic halides in wastewater. 

Supports Publication; 

Copyrighted Material 

U.S. Environmental Protection Agency; Office of Research and Development; Environmental Monitoring and Support Laboratory; ORD Publication Offices of Center for Environmental Research Information; Cincinnati, OH, 1984; EPA600/4-84-008, 

http://nepis.epa.gov/Exe/ZyPURL.cgi?Dockey=500024JK.txt

R. Riggin, et. al. 01-84 3 0/0 

Chapter 2 (3) Determination of Inorganic Anions in Water by Ion 

Chromatography 

Supports Publication; 

Copyrighted Material 

(Technical addition to Methods for Chemical Analysis of Water and Wastewater, EPA 600/4-79-020), U.S. Environmental Protection Agency; Environmental Monitoring and Support Laboratory; ORD Publication Offices of Center for Environmental Research Information; Cincinnati, OH, 1984; EPA600/4-84-017 

G. McKee, et. al. 

Chapter 3 INORGANIC ANALYTES This chapter provides guidance for the 

analysis of inorganic analytes in a variety of matrices. 

Chapter SW-846 USEPA 03-12 PDF 29 1/29 

Chapter 3 (1) Principles of Instrumental Analysis This text describes the principles and 

applications of modern analytical instruments. 

Supports Publication; 

Copyrighted Material 

Principles of Instrumental Analysis, 3rd ed, Saunders College Publishing, Philadelphia, PA, 1985 

D. A. Skoog 1995 

Chapter 3 (2) Sampling Ambient Water for Trace Metals at EPA 

Water Quality Criteria Levels, Method 1669 

This is a test method for sampling ambient water for trace metals to support water quality monitoring programs under the Clean Water Act. 

Supports Publication; 

Copyrighted Material 

U.S. Environmental Protection Agency, Office of Water, Washington, D.C., 1996, http://www.ecy.wa.gov/programs/wq/wastewater/method_1669.pdf 

US EPA 07-98 38 0/0 
Chapter 3 (3) Influence of Laboratory Environment on the 

Precision and Accuracy of Trace Element 

Analysis 

In this article, the influence of the laboratory air quality on the precision and accuracy of elemental analysis at trace and ultratrace levels was investigated. 

Supports Publication; 

Copyrighted Material 

Anal. Chem., 1985, 57, 1728-1733, 

http://pubs.acs.org/doi/abs/10.1021/ac00285a050 

S. B. Adeloju, et. al. 1985 6 1728/1733 

Chapter 3 (4) Microwave Enhanced Chemistry: Fundamentals, 

Sample Preparation, and Applications 

Supports Publication; 

Copyrighted Material 

Microwave Enhanced Chemistry: Fundamentals, Sample Preparation, and 

Applications, American Chemical Society, 

Washington, DC, 1997, p. 257-279. 

S. H. Kingston, et. al. 1997 23 257/279 

Chapter 3 (5) NBS Clean Laboratories for Trace Element 

Analysis 

Supports Publication; 

Copyrighted Material 

Anal. Chem., 1982, 54, 1358A-1376A J. R. Moody 1982 19 1358A/1376

A 

Chapter 3 (6) National Bureau of Standards Special Publication 

422 Accuracy in Trace Analysis: Sampling, Sample Handling, and Analysis 

Supports Publication; 

Copyrighted Material 

National Bureau of Standards Special Publication 422 Accuracy in Trace 

Analysis: Sampling, Sample Handling, and Analysis, National Bureau of Standards, 

Gaithersburg, MD, 1976, p. 509-539 

T. Murphy 1976 31 509/539 

Chapter 3 (7) Determination of Trace Elements Supports Publication; 

Copyrighted Material 

Determination of Trace Elements, VCH, New York, NY, 1994, p. 1-38 

G. Tolg, et. al. 1994 38 1/38 

Chapter 3 (8) Chemical Analysis, Vol. 47 Supports Publication; 

Copyrighted Material 

Chemical Analysis, Vol. 47, John Wiley & Sons, New York, NY, 1976 

M. Zief, et. al. 1976 

Chapter 3 (9) Production and Analysis of Special High-Purity 

Acids Purified by Sub-Boiling Distillation 

This article describes the use of subboiling distillation for the production of high purity inorganic acids and water. 

Supports Publication; 

Copyrighted Material 

Anal. Chem., 1972, 44, 2050-2056, 

http://pubs.acs.org/doi/abs/10.1021/ac60320a016 

E. C. Kuehner, et. al. 1972 7 2050/2056 

Chapter 3 (10) Purified Reagents for Trace Metal Analysis This article reviews 10 years of 

experience in the production of reagent acids and describes a new lab specifically designed to allow for trouble-free operation and production of high quality reagents. 

Supports Publication; 

Copyrighted Material 

Talanta, 1982, 29(11, Part 2), 1003-1010, http://www.sciencedirect.com/science/article/pii/0039914082802415 

J. R. Moody, et. al. 11-82 8 1003/1010 

Chapter 3 (11) Purification of Inorganic and Organic Materials Supports Publication; 

Copyrighted Material 

Purification of Inorganic and Organic Materials, Marcel Dekker, New York, NY, 1969, p. 297-306, http://onlinelibrary.wiley.com/doi/10.1002/jps.2600590137/abstract 

E. C. Kuehner, et. al. 01-70 10 297/306 

Chapter 3 (12) The Sampling, Handling and Storage of Materials 

for Trace Analysis 

Supports Publication; 

Copyrighted Material 

Philos. Trans. R. Soc. London, 1982, 305, 669-680, 12. http://www.jstor.org/pss/37123 

J. R. Moody 07-05-82 12 669/680 
Chapter 3 (13) Selection and Cleaning of Plastic Containers for 

Storage of Trace Element Samples 

This article describes a study that examines the levels of impurities present in different types of plastics and the quantities of impurities leached by acid cleaning the plastics as well as presenting a method of cleaning containers. 

Supports Publication; 

Copyrighted Material 

Anal. Chem., 1977, 49, 2264-2267, 

http://chemgroups.northwestern.edu/ohalloran/grouponly/MoodyLindstrom1977.pdf 

J. R. Moody, et. al. 12-77 4 2264/2267 

Chapter 3 (14) Clean Chemistry for Trace Analysis Supports Publication; 

Copyrighted Material 

Environmental Testing and Analysis, 1995, 4, 24-27 

F. J. Prevatt 1995 4 24/27 

Chapter 3 (15) Clean Room and Microwave Digestion 

Techniques: Improvement in Detection Limits for 

Aluminum Determination by GF-AAS 

This article describes the effects of using of a clean room and a closedvessel microwave digestion system on a method for ppb concentrations in biological materials using GF-AAS. 

Supports Publication; 

Copyrighted Material 

Appl. Spectrosc., 1988, 42, 1302-1306, 

http://www.cem.de/documents/pdf/publikation/digestion/RD006.PDF 

E. M. Skelly, et. al. 01-88 6 1302/1306 

Chapter 3 (16) Identifying Sources of Lead Contamination by 

Stable Isotope Techniques 

This article describes how investigations were persued to use naturally occurring variations in stable lead isotope abundances to find the sources of lead in particular environments. 

Supports Publication; 

Copyrighted Material 

Environ. Sci. Technol., 1972, 6, 705-709, http://pubs.acs.org/doi/abs/10.1021/es60067a003 

M. B. Rabinowitz, et. al. 08-72 5 705/709 

Chapter 3 (17) U.S. National Bureau of Standards Technical Note 

545 

This report describes the research activities and scientific programs of the Microchemical Analysis Section of the 

Analytical Chemistry Division of the 

National Bureau of Standards, Institute for Materials Research during from July 1969 to June 1970. 

Supports Publication; 

Copyrighted Material 

National Bureau of Standards, Gaithersburg, MD, 1970, p. 53-54, http://babel.hathitrust.org/cgi/pt?seq=1&view=image&size=100&id=mdp.39015001325276&page=root&orient=0 

E. J. Maienthal 12-70 114 1/114 

Chapter 3 (18) The Coastal Bend Bays Project This presentation information on the 

Regional Coastal Assessment Program. 

Supports Publication; 

Copyrighted Material 

26th Annual Conference on Analysis of Pollutants in the Environment, Chicago, IL 2003, http://www.epa.gov/emap/html/pubs/docs/groupdocs/symposia/symp2004/presentations/BrienNicolau.pdf 

P. N. Boothe, et. al. 

Chapter 3 (19) Living in the Environment This is an environmental science text 

that focuses on prevention of and solutions to environmental problems. 

Supports Publication; 

Copyrighted Material 

Living in the Environment, Wadsworth Inc., Belmont, CA, 1994, http://www.coursesmart.com/living-in-theenvironment-enhancedhomework/miller/dp/9780495387633 

G. T. Miller 1994 

Chapter 3 (20) Sampling for Analytical Purposes Supports Publication; 

Copyrighted Material 

Wiley, New York, NY, 1998. P. Gy 07-98 

Chapter 3 (21) Pierre Gy’s Sampling Theory and Sampling 

Practice 

Supports Publication; 

Copyrighted Material 

Second Edition, CRC Press, Inc., Boca Raton, FL, 1993. 

F.F. Pitard 1993 

Chapter 3 (22) Correct Sampling Using the Theories of Pierre Gy Supports Publication; 

Copyrighted Material 

USPEA Office of Research and Development, Las Vegas, NV, 1999.http://www.epa.gov/esd/factsheets/csutpg.pdf 

USEPA 03-99 2 1/2 
Chapter 3 (23) Guidance for Obtaining Representative 

Laboratory Analytical Subsamples from Particulate Laboratory Samples 

Supports Publication; 

Copyrighted Material 

USEPA Office of Research and Development, 2003.

http://www.epa.gov/osp/hstl/tsc/Gerlach2003.pdf 

USEPA 2003 156 1/134 

Chapter 4 ORGANIC ANALYTES This chapter discusses sampling and 

analysis methods used for organic analytes. 

Chapter SW-846 USEPA 03-12 PDF 22 1/22 

Chapter 4 (1) Summary Report - Evaluation of the Impact of 

Post-Holding Time Analyte Degradation on Regulatory Decision-Making - VOCs in Water 

Supports Publication; 

Copyrighted Material 

Oak Ridge National Laboratory. 2001 A. B. Dindal, et. al. 2001 

Chapter 4 (2) Standard Practice for Estimation of Holding Time 

for Water Samples Containing Organic and Inorganic Constituents 

Supports Publication; 

Copyrighted Material 

ASTM Standard D4841, 1988 (2008), ASTM International, West Conshohocken, 

PA, 2003, DOI: 10.1520/D4841-88R08, www.astm.org 

ASTM 2008 

Chapter 4 (3) Study Design and Analytical Results Used to 

Evaluate Stability of Volatile Organic Compounds in Water Matrices 

Supports Publication; 

Copyrighted Material 

United States Geological Survey Open-File Report 98-637. 1999. 

J. T. Love, et. al. 1999 

Chapter 4 (4) Stability of Volatile Organics in Environmental 

Water Samples: Storage and Preservation 

Supports Publication; 

Copyrighted Material 

Oak Ridge National Laboratory ORNL/TM11300. 1989. http://www.dtic.mil/cgibin/GetTRDoc?AD=ADA412461 M. P. Maskarinec, et. al. 1989 Electronic file 144 1/139 

Chapter 4 (5) Stability of VOCs in Water samples During Preanalytical Holding. Part 1. Analyses by a 

Commercial Laboratory 

Supports Publication; 

Copyrighted Material 

Oak Ridge National Laboratory ORNL/TM13240/V1. 1996. O. R. West, et. al. 1996 

Chapter 4 (6) Stability of VOCs in Water samples During Preanalytical Holding. Part 2. Analyses by an EPA 

Regional Laboratory 

Supports Publication; 

Copyrighted Material 

Oak Ridge National Laboratory ORNL/TM13240/V2. 1997.

http://www.osti.gov/bridge/servlets/purl/656450-6XVR0S/webviewable/656450.pdf 

O. R. West, et. al. 1997 PDF 

Chapter 4 (7) Practical Reporting Times for Environmental 

Samples 

Supports Publication; 

Copyrighted Material 

Environmental Science and Technology, 28: 1430-1436. 1994. 

C. K. Bayne, et. al. 1994 7 1430/1436 

Chapter 4 (8) Final Report - Stability of Volatile Organics in 

Environmental Soil samples 

Supports Publication; 

Copyrighted Material 

Oak Ridge National Laboratory ORNL/TM12128. 1992. M. P. Maskarinec, et. al. 1992 

Chapter 4 (9) Preservation and Holding Times Study for Vinyl 

Chloride, Styrene in Industrial Wastewater 

Supports Publication; 

Copyrighted Material 

Test America, January 2012. Test America, Methods 

Contract archives 

01-12 

Chapter 4 (10) Preservation and Holding Times Study for Vinyl 

Chloride, Styrene in Municipal Wastewater 

Supports Publication; 

Copyrighted Material 

Hampton Roads Sanitation District in Virginia Beach, Virginia, January 2012. 

Hampton Roads Sanitation District in Virginia Beach, Virginia 

01-12 

Chapter 4 (11) Standard Guide for Sampling Waste and Soils for 

Volatile Organic Compounds 

Supports Publication; 

Copyrighted Material 

ASTM Guide D4547, 1991 (2009), ASTM 

International, West Conshohocken, PA, 2003, DOI: 10.1520/D4547-09, www.astm.org 

ASTM 2009 
Chapter 4 (12) Sample Holding Time Re-evaluation Supports Publication; 

Copyrighted Material 

U.S. Environmental Protection Agency. EPA/600/R-05/124. 2005.http://www.epa.gov/esd/cmb/research/bs_033cmb06.pdf 

USEPA 2005 329 

Chapter 4 (13) Performance of Hydrochloric Acid and Trisodium 

Phosphate as Preservatives for Selected Organic Compounds in Ground Water 

Supports Publication; 

Copyrighted Material 

In: A Guide for Assessing Biodegradation and Source Identification of Organic Ground Water Contaminants using Compound Specific Isotope Analysis, EPA 600/R-08/148. 2008.

http://www.epa.gov/nrmrl/pubs/600r08148/600r08148.pdf 

USEPA 12-08 82 1/67 

Chapter 4 (14) Standard Practice for Using the Disposable En 

Core Sample for Sampling and Storing Soil for Volatile Organic Analysis 

Supports Publication; 

Copyrighted Material 

ASTM Standard Practice D6418, 2003 

(2009), ASTM International, West Conshohocken, PA, 2003, DOI: 10.1520/D6418-09, www.astm.org 

ASTM 

Chapter 4 (15) RCRA Organic Methods Workgroup Meeting 

Minutes 01-19-12 

 RCRA Organic Methods Workgroup 

Meeting Minutes, January 19, 2012. 

RCRA Organic Methods Workgroup 

Chapter 4 (16) RCRA Organic Methods Workgroup Meeting 

Minutes 01-26-12 

 RCRA Organic Methods Workgroup 

Meeting Minutes, January 26, 2012. 

RCRA Organic Methods Workgroup 

Chapter 4 (17) RCRA Organic Methods Workgroup Meeting 

Minutes 02-09-12 

 RCRA Organic Methods Workgroup 

Meeting Minutes, February 9, 2012. 

RCRA Organic Methods Workgroup 

Chapter 4 (18) Integrity of VOA Vial Seals Supports Publication; 

Copyrighted Material 

EPA/600/R-00/066. 2000.

http://www.epa.gov/esd/cmb/research/papers/bs124.pdf 

USEPA 09-00 PDF 42 1/18 

Chapter 5 MISCELLANEOUS TEST METHODS This chapter covers test methods not 

covered in chapters 2 and 4 

Chapter SW-846 USEPA 03-12 PDF 3 1/3