Dry Scrubber Blue Goose Combustion Data Septem ber 2010 Fyrite

Location : Dry

Scrubber Date 9/14/10 Time: 9:30

run O2 CO2

1 18 2 2 18 2 3 18 2
Avg 18 2

Molecular wt

1 29.04 2 29.04 3 29.04

AVG 29.04

diff 0

0 0

All diff must be less that 0.3
Analysts: O'Brien&Gere

Page 1Test ID: 9-14-10-POM-BG-Run# 3 

### Value 0

0 0

220.00 150.00 0.001 0.0000 0.0000 200.00 200.00 0.001

310.00 90.00 0.0031 0.0031

1060.00 1000.00 0.0003 0.0001 0.00020



### Value 3.3000 1.0000 4.3000 Total mg of Particulate MCEM **Total mg of MCEM** 

# An **ode Bake Furnace Dry Scrubber Test #3** 

3W B W eight of MCEM From Blank (g) 3WNet of Extracted W ater Adjusted from Blank (g)

Total mg of Gaseous MCEM Volume of Deionized W ater Used 3W(ml) Volume of Deionized W ater Used in Blank (ml) 2M Net MCEM Adjusted from Blank (g)



# 9/14/2010

**MCEM Analysis Data** 1A Filter W eight (g)

3WW eight of Impinger W ater Plus Back Half Rinses Extracted (g). Volume of Acetone Used 3A (ml) Volume of MC Used 3M (ml) 3M W eight of MCEM From Back Glassware Rinses (g) 3M Net of MCEM Adjusted from Blanks (g)



### MCEM Analysis Calculations 1B QC Filter Blank (g) Net MCEM From Filter (g) Volume of Acetone Used 2A (ml) Volume of MC Used 2M (ml) 2M W eight of MCEM From Front Half Glassware Rinses (g) 4A W eight of Acetone Blank (g) 4M W eight of MC Blank (g) Volume of MC Used in Blank (ml) Volume of Acetone Used in Blank (ml)Test ID: 9-14-10-POM-BG-Run# 3



### Value 0.6081 0.84 18 % O 2 in Anode Bake Furnace Gas Stream 2.0000 %CO 2 in Anode Bake Furnace Gas Stream 29.04 28.4695538 0.051670851 543.7 642.1 29.84 70 1.92 1.004 29.84 128 1.26 83.361 94.1 29.82 0.252 0.00034636059



### Value 81.3120207 37.97309 80.4 3.78443 13.7 0.645955 0.051671 0.030405 103.5765 Md = Stack gas dry molecular weight, (lb/lb-mole) 

# An **ode Bake Furnace Dry Scrubber Test #3**  **9/14/2010**

**Method 5 Parameter**  p = Stack gas v elocity pressure (av g. sqrt  p - in. water) Cp = Pitot tube calibration coefficient

Total sampling time required for test (min) Ms = Stack gas (wet) molecular weight (lb/lb-mole) Bws = Stack gas moisture content

Vwc(std) Nozzle diameter (in) Area of Nozzle (ft^2)

Vm (std) = Volume of sample measured by DGM (dscf) Vs = Average stack gas v elocity Total impinger catch (ml) Tm = Absolute average dry gas meter temp (R). Ts = Stack gas absolute average temperature (R) Pm = Pressure at orifice meter (in. Hg) Ta = Sampling site ambient temperature, (°F)  H@ = Orifice meter calibration factor, (in. water) Y = Dry gas meter calibration factor Pbar = Barometric pressure, (in. Hg)

I = % Isokinetic variation



### Air Test Calculations  Hav g= average orifice meter differential Vm = Total sample volume from dry gas meter (dcf) Vlc Volume collected Ps = Absolute stack gas pressure (in Hg)

Vwc (std) = conv erted water v olume Total silica gel catch (ml) Vwsg (std) = conv erted silica gel water v olume Bws = fraction of gas that is moistureTest ID: 9-14-10-POM-BG-Run# 3 LIMS ID#: 2010010514



### Value 3.3000 0.0033 1 0.001 81.31202068 29.84 38.48 10.06 Green Carbon produced tons/hr 0.051670851 68139.46258 4088367.7550 87672.28018 Acfm 71852.12295 Scfm 0.0008 Emission Rate of Total MCEM gr/dscf 0.37 8.77 0.1107 2.66 **0.48**

**0.036 Emission Rate of Gaseious MCEM lb/Ton of Green Carbon produced**  **0.011 Emission Rate of Particulate MCEM lb/Ton of Green Carbon produced**  **0.047 Emission Rate of Total MCEM lb/Ton of Green Carbon produced** 

Start time: 9/14/2010 16:35PM End time: 9/14/2010 18:54PM

Qstd Flow of Anode Bake Furnace Emissions (dscf/hr)

Emission Rate of Gaseous MCEM lb/hr Emission Rate of Gaseous MCEM lb/d Emission Rate of Particulate MCEM lb/hr

**Emission Rate of Total MCEM lb/hr** Emission Rate of Particulate MCEM lb/d Pbar Barometric Pressure During Test (in Hg) Area of Anode Bake Furnace Stack (ft2)

Bws Moisture in Roof Emissions Qstd Flow of Anode Bake Furnace Emissions (dscf/min) Total mg of MCEM in Particulate Sample Total g of MCEM in Particulate Sample Total mg of MCEM in Gaseous Sample

Vm(std) Volume of Air Sampled by DGM (dscf) 

# An **ode Bake Furnace Dry Scrubber Test #3**  **9/14/2010**

**Combined Method 5 Parameter and Analytical**
Total g of MCEM in Gaseous Sample

## Value 1.2

0.0012 81.31202068 29.84 38.48 10.06 Green Carbon produced tons/hr 0.051670851 68185.1631 Qstd Flow of Anode Bake Furnace Emissions (dscf/min) 4091109.786 0.0002 Particulate gr/dscf **0.13 Particulate lb/hr** 

**0.013 Particulate Emissions from Anode Bake Furnace lb/Ton of Green Carbon Baked**  Qstd Flow of Anode Bake Furnace Emissions (dscf/hr) 

## Combined Method 5 Parameter and Analy **tical**

Vm(std) Volume of Air Sampled by DGM (dscf) Pbar Barometric Pressure During Test (in Hg) 

# An **ode Bake Furnace Dry Scrubber Test #3**  **9/14/2010**

Total mg of Particulate Total g of Particulate

Area of Anode Bake Furnace Stack (ft2 )

Bws Moisture in Anode Bake Furnace Emissions