Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.
1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected
more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of
measure.Information
This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

130 Santee Cooper-Cross Unit 4 bituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte An alysis M ethod for each Analyte (example: ASTM D5865-04) 130 Santee Cooper-Cross Unit 4 As Received Higher Heating Value ASTM D 240 130 Santee Cooper-Cross Unit 4 As Received % Moisture ASTM D 2216 130 Santee Cooper-Cross Unit 4 As Received Antim ony SW846 3050B/6020A 130 Santee Cooper-Cross Unit 4 As Received Arsenic SW846 3050B/6020A 130 Santee Cooper-Cross Unit 4 As Received Beryllium SW846 3050B/6020A 130 Santee Cooper-Cross Unit 4 As Received Cadmium SW846 3050B/6020A 130 Santee Cooper-Cross Unit 4 As Received Chlorine SW846 5050/9056A 130 Santee Cooper-Cross Unit 4 As Received Chromium SW846 3050B/6020A 130 Santee Cooper-Cross Unit 4 As Received Cobalt SW846 3050B/6020A 130 Santee Cooper-Cross Unit 4 As Received Fluorine SW846 5050/9056A 130 Santee Cooper-Cross Unit 4 As Received Lead SW846 3050B/6020A 130 Santee Cooper-Cross Unit 4 As Received Manganese SW846 3050B/6020A 130 Santee Cooper-Cross Unit 4 As Received Mercury SW846 7471B 130 Santee Cooper-Cross Unit 4 As Received Nickel SW846 3050B/6020A 130 Santee Cooper-Cross Unit 4 As Received Selenium SW846 3050B/6020AEIA

Facility Code Facility

Name Boiler ID 130 Santee Cooper-Cross Unit 4

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units % Moisture (as received) Chlorine

(Dry Basis) RUN 1 5/25/2010 5/25/2010 12400.00 Btu/lb 7.74 1270000 RUN 2 5/25/2010 5/25/2010 12200.00 Btu/lb 6.56 1140000 RUN 3 5/25/2010 5/25/2010 12200.00 Btu/lb 7.12 1610000 Mercury and non-mercury metalic HAPs HAPs Test Group

Fuel Testing ResultsChlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units μg/Kg 14.8 μg/Kg <588 μg/Kg 8060 μg/Kg 607 μg/Kg μg/Kg 17.9 μg/Kg <589 μg/Kg 5860 μg/Kg 507 μg/Kg μg/Kg 9.76 μg/Kg 135 μg/Kg 7880 μg/Kg 1000 μg/KgCadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel

(Dry Basis) 61.4 μg/Kg 4110 μg/Kg 3990 μg/Kg 10700 μg/Kg 7170 43.2 μg/Kg 3580 μg/Kg 2760 μg/Kg 8630 μg/Kg 5970 106 μg/Kg 4800 μg/Kg 4450 μg/Kg 15400 μg/Kg 7870Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units μg/Kg 1510 μg/Kg 105000 μg/Kg 2660 μg/Kg μg/Kg 1850 μg/Kg 91700 μg/Kg 2040 μg/Kg μg/Kg 2870 μg/Kg 85300 μg/Kg 2870 μg/KgEIA

Facility Code Facility

Name Boiler ID 130 Santee Cooper-Cross Unit 4

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) Chlorine

(Dry Basis) RUN 1 5/26/2010 5/26/2010 12100 Btu/lb 7.18 1570000 RUN 2 5/26/2010 5/26/2010 12600 Btu/lb 7.33 1860000 RUN 3 5/26/2010 5/26/2010 11500 Btu/lb 6.84 1290000 Fuel Testing Results HAPs Test Group Acid gas HAPsChlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units μg/Kg 8.26 μg/Kg 151 μg/Kg 7130 μg/Kg 1070 μg/Kg μg/Kg 10.7 μg/Kg <599 μg/Kg 7680 μg/Kg 1160 μg/Kg μg/Kg 14.7 μg/Kg 112 μg/Kg 11800 μg/Kg 962 μg/KgCadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) 66.3 μg/Kg 4920 μg/Kg 5510 μg/Kg 18400 μg/Kg 9340 80.4 μg/Kg 4740 μg/Kg 4060 μg/Kg 47600 μg/Kg 8060 96.3 μg/Kg 5690 μg/Kg 5940 μg/Kg 17200 μg/Kg 10100Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units μg/Kg 3050 μg/Kg 90500 μg/Kg 3450 μg/Kg μg/Kg 2970 μg/Kg 75500 μg/Kg 3030 μg/Kg μg/Kg 3400 μg/Kg 81800 μg/Kg 3850 μg/KgEIA

Facility Code Facility

Name Boiler ID 130 Santee Cooper-Cross Unit 4

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) Chlorine

(Dry Basis) RUN 1 5/24/2010 5/24/2010 12000.00 Btu/lb 7.13 1210000 RUN 2 5/24/2010 5/24/2010 12500.00 Btu/lb 6.99 1090000 RUN 3 5/24/2010 5/24/2010 11700.00 Btu/lb 6.74 1030000 HAPs Test Group Non-dioxin/furan organic HAPs

Fuel Testing ResultsChlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units μg/Kg 13.7 μg/Kg <592 μg/Kg 4140 μg/Kg 568 μg/Kg μg/Kg 16.1 μg/Kg 111 μg/Kg 7230 μg/Kg 672 μg/Kg μg/Kg 15.5 μg/Kg <594 μg/Kg 8800 μg/Kg 649 μg/KgCadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) 36.7 μg/Kg 2740 μg/Kg 1790 μg/Kg 7030 μg/Kg 4370 68.5 μg/Kg 5330 μg/Kg 3050 μg/Kg 12000 μg/Kg 8380 68.3 μg/Kg 5360 μg/Kg 3380 μg/Kg 10800 μg/Kg 7500Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units μg/Kg 1300 μg/Kg 110000 μg/Kg 1310 μg/Kg μg/Kg 1470 μg/Kg 80000 μg/Kg 2610 μg/Kg μg/Kg 1430 μg/Kg 116000 μg/Kg 2310 μg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/Kg μg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm μg/Kg