# Exhaust Emissions Sampling Daltile, El Paso, TX Combined Kiln Exhaust, Spray Dryer Exhaust, Crusher and Screening Baghouse Exhaust June 16 - 19, 2008 Armstrong Environmental, Inc. Project W-2559-08

Report Prepared For: Steve Willis Daltile 7834 C. F. Hawn Freeway Da11as, TX 75217

Report Prepared June 30, 2008 By: Armstrong Environmental, Inc. 

# 1748 Hlavek Rd. Decatur, Texas 76234 (214) 631-0021

# TABLE OF CONTENTS

I. l.ntroduction
H. Sumznary

III. Procedures
N. Appendices

A. Calculation Summaries

B. Continuous Emissions Monitor Sununaries

C. Analytical Summaries

D. Field Data Sheets

E. Equipment Calibrations

F. Standard Gas Certifications Page

1

2-6

7-13

14-25

26 - 109

110 - 171

172 - 186

187 - 197

198 - 209

# I. INTRODUCTION

A series of tests was performed on the Combined Kiln exhaust, the Spray Dryer exhaust, and the Crusher and Screening Baghouse exhaust at the Daltile facility in El Paso, TX on June 16 - 19, 2008.
The purpose of this test series was to deterrnine the exhaust emission rate of the following components:

~ i~
, '~ ~ ~ ^r.

. ~~~a

~bs 

# . Y

. ~Y ~ a• 4

~ '."

~~ '' ``j.

~ .:• ts,•c4...,,y xi~~
, '.
~ .' ~
. •1

. a?'; ,'!' ~~~~fi~~ ° h.."_ - .. L r 1nt

~ S,

~ M '

. . ~ 

# ` ,.•+..y

{ a



### _ ~ ' 1 }._ ~, t~r ~,~ •

~ 3
, • ~ j

,, i k~S~ 7''.

~ y

f r.

~ :r t~ 'i

~ ' ? a", ~ ~ r~~ 

# ._. ~ ~ i: ~ t'~~1-1~1~~ {..`tR ~ '.Y 

# Combined Kiln Exhaust PM, S02, NOx, CO, VOC, HF, HCI, Lead Spray Dryer S02, NOx, CO, VOC Crusher and Screening Ba ouse PM
Testing followed procedures detailed in Title 40: Code of Federal Regulations (40:CFR).
Saznpling was performed by Richard Taylor and Tom Armstrong of Armstrong Environmental, Inc. us'ing an Apex Method 5 sampling train, an EcoPhysics 70S continuous NOx analyzer, a ThermoEnvironmenta148C continuous CO analyzer, a Western Research 721 AT continuous S02 monitor, and a ThermoEnvironmental Model 51 continuous FID analyzer.
Present during the test series was Jon Smith of TCEQ.
Sampling was performed according to the following schedule:

~ •.• ~ .+ `r:"..

~~ :A

~ .1r:

. ~ L'"•{

~ ....r ~~.(~~F~'S y

. • ~ • + , °{ -1s

~ X

• .i. ': ~ r~.~ .r.M ~~~~~'- F ~+'~Y~'^~~+a~': 's'

..~ • SXT~ .i~ • u... • 4?

~ .. t 

# 6J16/08 Combined Kiln Ex 

# ., 2:50 PM 3:56 PM

Stiatification 

# 6/17/08 Combined Kiln Ex., PM, 9:20 AM 1:57 PM

CO, VOC, NOx, HF, HCl 

# 6/17/08 - Combined Kiln Ex., 2:20 PM 6:13 PM Lead 

# 6/18/08 Spray Dryer 10:06 AM 1:48 PM 6/19/08 Ba ouse 7:55 AM 2:37 PM

j A 

# Submitted b : rmstr g E onme tal, Inc.



# i m yrm siroi resident

1

# II. SUMMARY

A series of tests was performed on the Combined Kiln exhaust, the Spray Dryer exhaust, and the Crusher and Screening Bagliouse exhaust at the Daltile facility in El Paso, TX on June 16 - 19, 2008.
Sampling was performed following procedures detailed in Title 40: Code of Federal Regulations.

Results of this test series are summarized in Tables 1- 4.
Results indicate the following emission rates for the Combined Kiln Exhaust:

'.- n H. ~ .,t'. ~

. < "

` + ~~ ~ l 1,- M ~~'t w ~ 1 ~

. .. ,1`..,M.,Y. ~ t

. 't : n

` ~ 1. .:.1 ~
. , ' ~
. ~ rdl. : Y ~ 4 7 n! - n

. ~ - h ..i rss. = ~ ..; ~

. ti . n .y ~ •
+ - 'S '.1 ~ :'~'~ y ! a , ` "•

~ .t'
~ . . .';' -.`7 • ~ ,.r"+,'h ~'!~ .nK.-0f' o };' .jT ~~ ois: i ~ y
~ "'
~ J r

M -. n ~ ~ ~~- t '~ . - 1

~
. ~ .:1 ~~'• i . ~~~~u..~i+.~.h~t.~ " c ' 2:. •,.i

~.o ~+ ~~ ~i ~'~. ~l~ t ".~~V~~~ _ ;'

. 

# PM, lbs/hr 7.836 4.521 4.135 5.497 CO, lbslhr 5.072 5.376 6.187 5.545 NOx, lbs/hr 9.080 9.229 9.543 9.284 VOC, lbs/hr 0.529 0.580 0.598 0.569 S02, lbslhr 21.60 16.62 18.01 18.74 

# HF, Ibslhr 22.04 25.06 21.51 22.87 HCI, lbslhr 3.524 3.344 3.145 3.338 Lead, lbs/hr 0.00137 0 0.00042 0.00060
Carbon Monoxide exceeded the CO analyzer range during Run #2. Sampling was stopped until CO was back in range. Jon Smith of TCEQ requested that sampling be performed through such periods, which occurred in Run #3 for about 5.9 minutes.
Results indicate the following emission rates for the Spray Dryer:

.~~i~.~~

j 1 ~ t h ~ 

## , r ; ' , ~:

' a F _C

~ x

/`F

~~ . ,`

~ l ~ * ` ~ . vna

~ ona ; •T. r
~ . , ti {YS''r ~~ r4M;

~~~-~ `•

`te ~yti~ . i~~

_ !'lT.s 1.
~ 11
~ , L.. t' • : ,, w.f+r-: w.z. ss ~c ~ "1 ~{.~'~ lLl:,

~ •i ~ ~~ 1 `F: , w , y { : A Is
, ~ \Y,I 1 'l,~' L~ ~ 4.:. ..T.-:1•,. ~ R. ^t

. . : 

## ,•,

~ A'tsr.i

~ , [~ ye
~ f3 e."n ..i

~ ...~~~ ~~ 'f; 

# CO,1bslhr 0.0965 0.0882 0.0660 0.0836 

# NOx, lbslhr 2.237 2.260 2.250 2.249 VOC, lbs/hr 0.288 0.215 0.169 0.224 S02, lbs/hr 0 0 0 0
ResuIts indicate the following emission rates for the Crusher and Screening Baghouse:

: , • 

# Run # : _l:.

. .:..'
, . , ..



# ,;-2

. : , . .. . ,



# :3 , . 

# Avera e: PM 

# , gldscm (Front 0.0434 0.0442 0.0468 0.0448 Hal PM 

# , lbs/hr (Front 2.409 2.429 2.642 2.493 and Back Hal


# It should be noted that 60 dscf was not pulled on any run during sampling.

2

### SUMMARY OF EMISSIONS TEST DATa

Table : 1 Plant : Daltile, EI Paso, TX Location : Combined Kiln Exhaust Operator : R. Taylor, T. Armstrong - Test Date : 17•Jun•08 Repetition : 1 2 3

STACK GAS Temperature, F 350.6 352.2 354.3 Velocity, fps 51.92 51.65 52.27 Volume Flow, acfm 67431.5 67086.7 67890.9

scfm 35697.2 35417.0 35859.9 

## scfh 2141831 2125019 2151595 Moisture, % 6.75% 6.83% 6.54J o CO2, o 2.50 2.50 3.00 02, % 17.50 17.50 17.00



## SAMPLE Start Time, hrs:min 9:20 AM 11:10 AM 12:55 PM Finish Time, hrs:min 10:23 AM 12:20 PM 1:57 PM Sample Volume, scf 33.745 33.530 33.962 Isokinetic Ratio, aJ

a 101.187 101.3381 101.3757



## PARTICULATE

~ 

## r-orat-Half-- 7 Sample Weight, mg 37.68 24.06 29.50 Concentration, gr/scf 0.017229 0.011072 0.013403 Emissions, Ibs/hr 5.273473 3.362278 4.120962

8ack Haif Sample Weight, mg 18.31 8.29 0.10 Concentration, gr/scf 0.008372 0.003815 4.54E•05 Emissions, Ibs/hr 2.562561 1.158491 0.013969

Total Particulate, Ibs/hr 7.836033 4.520768 4.134931

CARBON MONOXIDE Concentration, ppm 32.58 34.81 39.56 Emissions, Ibs/hr 5.072337 5.376983 6.18712

NITROGEN OXIDE AS NO2 Concentration, ppm 35.5 36.37 37.14 Emissions, Ibs/hr 9.079986 9.229491 9.542759

VOC AS Methane Concentration, ppm 1NET 5.55 6.12 6.25 Concentration, ppm DRY 5.951788 6.568469 6.687445 Emissions, Ibs/hr 0.529501 0.579777 0.59766

SULFUR DIOXIDE Concentration, ppm 60.7 47.06 50.37 Emissions, Ibs/hr 21.60069 16.61531 18.00637

HYDROGEN FLUORIDE Sample Weight, mg 157.51 179.30 154.00 Concentration, ppm 198.228 227.0971 192.572 Emissions, Ibs/hr 22.04418 25.05638 21.51282

HYDROGEN CHLORIDE 

## Sample Weight, mg 25.18 23.93 22.51 Concentration, ppm 17.36399 16.60777 15.42357 Emissions, Ibs/hr 3.524046 3.344111 3.144503



# 3

# STACK GAS

Temperature, F Velocity, fps Volume Flow, acfm

scfm scfh Moisture, % CO2, 0 / 0 02, % 

## 356.0 51.99 67532.3 35010.3 2100617 8.42o'J o 3.00 17.00 357.6 52.67 68409.4 35349.6 2120979 8.54aJ o 3.00 16.50 359.9 51.21 66508.4 35043.9 

# 2102636 6.48% 2.50 17.00



## SAMPLE Start Time, hrs:min Finish Time, hrs:min Sample Volume, scf Isokinetic Ratio, % 

## 2:20 PM 3:23 PM 33.829 103.4298 3:45 P M 4:49 P M 34.063 103.1449 5:10 PM 6:13 PM 33.362 101.9021 SUMMARY OF EMISSIONS TEST DATA



# Table : 2 Plant : Daltile, EI Paso, TX Location : Common Kiln Exhaust Operator : R. Taylor Test Date : 17-Jun-08 Repetition : 1 

## 2 3



# LEAD Sample Weight, ug 10.00 3.00 Concentration, ug/M3 

## 10.43801 ~ 

## 3.175281 Emissions, Ibs/hr 

## 0.001369 ~ 

## 0.000417

El

## SUMMARY OF EMISSIONS TEST DATA

Table : 3 Plant : Daltile, EI Paso, TX Location : Spray Dryer Operator : R. Taylor, T. Armstrong Test Date : 18-Jun-08 Repetition : 1 2 3


# STACK GAS Temperature, F 140.8 140.8 141.9 Velocity, fps 76.55 73.61 69.81 Volume Flow, acfm 44190.8 42494.4 ' 40299.3

scfm 26915.5 25666.0 23848.2 

# scfh 1614930 1539960 1430892 Moisture,

~ 

# ' J o - 20.54% a - 21.22

~ 

## ' J o 22.66% 

# CO2, % 1.00 1.00 1.00 02, % 19.00 19.00 19.00



# SAMPLE Start Time, hrs;min 10:06 AM 11:30 AM 12:45 PM Finish Time, hrs:min 11:11 AM 12:33 PM 1:48 PM Sample Volume, scf 29.546 30.779 30.703



# CARBON MONOXIDE Concentration, ppm 0.822 0.788 0.635 Emissions, Ibs/hr 0.096493 0.088208 0.066047

NITROGEN OXIDE AS NO2 Concentration, ppm 11.6 12.29 13.17 Emissions, Ibs/hr 2.237089 2.260128 2.250424

VOC AS Methane Concentration, ppm WET 3.41 1.95 1.64 Concentration, ppm DRY 4.291701 1.223008 1.031094 Emissions, Ibs/hr 0.287884 0.215132 0.168528

SULFUR DIOXIDE 

# Sample 1Neight, mg 0.00 0.00 0.00 Concentration, ppm 0 0 0 Emissions, Ibs/hr 0 0 0

5

## SUMMARY OF EMISSIONS TEST DATA

Table 

# : 4 Plant 

# : Daltile, EI Paso, TX Location 

# : Baghouse Operator 

# : T. Armstrong, R. Taylor Test Date 

# : 19•Jun-08 Repetition 

# : 1 2 3



## STACK GAS Temperature, F 98.2 101.0 104.9 Velocity, fps 49.06 48.82 48.73 Volume Flow, acfm 

# - 16957.5 16873.6 16845.2

scfm 13821.9 13648.5 13572.3 scfh 829314 818913 814341 Moisture, 

# %

Q 1.19% 1.44% 1.14% CO2, 

# % 0.00 0.00 0.00 02, 

# % 21.00 21.00 21.00



## SAMPLE Start Time, hrs:min 7:55 AM 10:15 AM 12:35 PM Finish Time, hrs:min 9:57 AM 12:17 PM 2:37 PM Sample Volume, scf 59.040 58.050 58.238 Isokinetic Ratio, 

# % 101.3121 100.8789 101.7734



## PARTICULATE Front Half Sample Weight, mg 72.52 72.67 77.19 Concentration, gr/scf 0.018953 0.019316 0.020451 Concentration, g/dscm 0.043373 0.044204 0.046802 Emissions, Ibs/hr 2.246157 2.260471 2.379963

Back Half Sample VUeight, mg 5.28 5.42 8.50 Concentration, gr/scf 0.00138 0.001441 0.002252 Emissions, lbs/hr 0.163537 0.168594 0.262077
Total Particulate, Ibs/hr 2.409694 2.429066 2.64204



# lei

# III. PROCEDURES

The procedure for emissions sampling followed USEPA test methods as detailed in Title 40: Code of Federal Regulations. The following methods were used:

Method Title 1 Sample and Velocity Traverses for Stationary Sources

2 Determination of Stack Gas Velocity and Volumetric Flow Rate (Type S

Pitot Tube)

3 Gas Analysis for CO2, 02, Excess Air and Dry Molecular Weight

4 Determination of Moisture Content in Stack Gas

5 Determination of Particulate Emissions from Stationary Sources

6C Determination of Sulfur Dioxide Emissions from Stationary Sources

(Instrumental Analyzer Procedure)

7E Determination of Nitrogen Oxides Emissions from Stationary Sources

(Instrumental Analyzer Procedure)

10 Determination of Carbon Monoxide Emissions from Stationary Sources

25A Deterrnination of Total Gaseous Organic Concentration using a Flame

Ionization Analyzer

26A Determination of Hydrogen Halides and Halogens Emissions from

Stationary Sources
Determination of Sulfur Dioxide, Sulfur Trioxide, and Sulfuric Acid Mist in Stack Gas Peroxide-Barium Titration Method from the TCEQ 

# Laboratory Methods Manual was used to determine S 02 on the Spray Dryer exhaust.
02 and CO2 were determined using FyRite Analyzers.
PM. HF and HC1 sampling was perfonned on the combined kiln exhaust for 2.5 minutes at each of 24 points, 12 points per traverse, making a total run duration of 60 minutes. A schematic of the sampling location is shown in Figure 1. The sampling train was configured as follows:
Glass Sampling Nozzle Heated Glass Lined Probe Heated teflon filter

7

# Impinger # 1- 100 mis H20 Impinger #2 - 100 mis 0.1 N H2SO4 Impinger #3 - 100 mis 0.1 N H2SO4 Iznpinger 44 - Empty Impinger #5 - 200 grams silica Gel
Analysis for PM was performed on the probe wash, filter, and solution from the first impinger. HF and HCI analysis was performed on an aliquot from the first impinger, and the solution from the 2nd and 3rd impingers. Analysis was performed using a Dionex LC20 IC/HPLC.
S02 and moisture sampling was performed on the Spray Dryer exhaust for 3.75 minutes at each of 16 points, 8 points per traverse, making a total run duration of 60 minutes. Sample was pulled at a constant rate. A schematic of the sampling location is shown in Figure 2. The sampling train was configured as follows:
Stainless Steel Sampling Nozzle Heated Glass Lined Probe Impinger #1 - 200 mis 80% IPA Impinger #2 - 200 mis 3% H2O2 Impinger #3 - 200 mis 3% H2O2 Impinger #4 - Empty Impinger #5 200 grarns silica gel
S03 analysis was perforrned on the solution from the 1 st impinger. S02 analysis was performed on the solution from the 2nd and 3rd impinger by Barium PerchloratelThorin titrations.
CEMs sampling was performed as follows:

F ~ w

~~ 1 , ( y r~ S i.w.

~ * t•r rY

, a; F ~ +~ " 1,' ~~ ~~~a ~ 1,j..V,,., y ~~ sr

. .. s 'r'4 r' ~:;~7~ •rh. i
, , ~ b r. '.{+

~ `'`• ~ ~r .~~t ~ ! :i+ ~ , k".' ° " F,, •,,_ y

, , ~ . ~ ,, . , •

. ..r

~~ . y • t ~ w "SZ"[;-

~ ~ ~ ..,A ~ • 

# Common Kiln BcoPhyics 70S NOx 0- 51 

# .5 ppm 5.133 ppm, 25 pprn, Analyzer SN 8350095 51.5 ppm NOx in N2 

## Common Kiln Teco 48C CO Analyzer 0- 

# 99.1 ppm 24.3 ppm, 50.3 ppm, CA # 201044 and 99.1 ppm CO in N2 

# Common Kiln Westem Research 721 0- 

# 247 ppm 50.1 ppm, 101 ppm, 247 AT SN VV-721M- ppm S02 in N2 8846-1 

## Common Kiln Teco 51 continuous FID 0- 

# 50 ppm 5•142 Ppm, 20•2 PPm, SN 51-30764-261 41 ppm CH4 in Air 

# Spray Dryer Teco 48C CO Analyzer 0- 50 

# .3 ppm 5 .090 ppm, 24.3 ppm, CA # 201044 and 50.3 ppm CO in N2 

# Spray Dryer BcoPhyics 70S NOx 0- 51 

# .5 ppm 5.133 ppm, 25 ppm,

Analyzer SN 8350095 51.5 ppm NOx in N2 

## Spray Dryer Teco 51 continuous FID 0- 

# 50 ppm 5.142 ppm, 20.2 ppm,

SN 51-30764-261 41 ppm CH4 in Air

:

# All standard gases were EPA Protocol 1. Interference checks can be found in Appendix

B. A schematic of the CEMs configuration is shown in Figure 4. A NOx stratification test was performed on the Combined Kiln exhaust on 6/16/08 resulting in a single point being used for sampling. Three traverse points were used for CEMs sampling on the Spray Dryer.

S02 interference results are as follows:

~ 44 1 ~,~•~ ~ 1

~~
. .! ~ , r la .~ i;.. ~ t ; A•°' ~ i'

~ , ,N

~ + :- t- ~±~

~ ! ' ~~W ~ ~ , ~~ k ' " ~ ~~ ~~ , .: ~ ~4~~'~'i

~ 

# 1 55.7 59.28 6.04

2 42.4 43.06 1.53 3 45.5 47.39 3.97


# Sampling was performed on the Baghouse exhaust for 5 minutes at each of 24 points, 12 points per traverse, making a total run duration of 120 minutes. The sampling train was configured as follows:
Stainless Steel Sampling Nozzle Heated Glass Lined Probe Heated Glass Fiber filter Impinger #1 - 100 mis H20 Impinger #2 - 100 mis H20 Impinger #3 - Empty Impinger #4 - Empty Impinger #5 200 grams silica gel
Particulate analysis was performed on the probe wash, filter, and the impinger solutions. A teflon filter was mistakenly used for Run #3.
At the conclusion of Run #3, Jon Smith took a picture of the probe pitot configuration and requested a wind tunnel calibration be performed on the pitot tube. The pitot tube was calibrated using a lOft. 12 inch diameter wind tunnel yeilding a Cp of 0.8351 on the "A" side, and 0.8371 on the `B" side. Wind tunnel is available for inspection by all interested parties. Picture and calibration summary are in Appendix E.

9

## Figure 1- Combined Kiln Exhaust Traverse

40 R.



## Stack Diametar - 63 inches Pbint #1 - 1.3 inches 

## Fbint #2 - 4.2 inches Point #3 - 7.4 inches Fbint #4 - 11.2 inches Point #5 - 15.75 inches Pbint #6 - 22.4 inches Fbint #7 - 40.6 inches Piaint #8 - 47.25 inches Pb int 49 - 51 _8 inchas 

## Point #10 -55.6 inches Pbint 411- 58.8 inches Point #12 - 61.7 inches ~ -A 

### 12 Ft. 0

# Figure 2 - Spray Qryer Exhaust

CEMS Traverse



# n 53

inches

360 inches

~

~ 

### Poin# #1 - 7 inches Popd #2 - 21 inches Poirrt #3 - 35 inches 

## Stack Diameter - 42 inches Point #1 -1.3 inches Poirrt #2 - 4.4 inches Point #3 - 8.1 inches Poirrt #4 -13.6 inches Point #5 - 28.4 inches Point #6 - 33.9 inches Point #7 - 39.6 inches Point #8 - *40.7 inches

# Figure 3- Crusher and Screening Baghouse Traverse



### 108 inches

~ 

### N 

### Stack Diame#er - 32.5 inches Point #1 -1.0 inches 

## 69 inches Poird #2 - 2.2 inchas Point #3 - 3,8 inches Point #4 - 5.75 inches Point #5 - 8.1 inches Poini #6 -11.6 inches Point #7 - 20.9 inches Point #8 - 24.4 inches Point #9 - 26.75 inches Poird #10 - 28.7 inches Point #11 - 30.3 inches Point #12 - 31.5 inches

# Figure 4 - CEMs Configuration

Heated Probe

Hsated Filter
I CO Analyzer Heated 

## Sampfe Line

~ 

## w
B ias CaGbration S pan Line 

### FID Analyzer NOx Analyzer



## Tranfer Line 

# 6
I Vacuma Samplo S02 Analyzer Pump 

## Processor
Sample



## Ri m p Flowmeter
"'aubration Foirrt To Irderfernce train

F Sample processor consists of two short stem impingers fotlowed by a 0.3 pump micron filter

# Appendix A 1

### EMISSION TEST SUMMARY

PLANT : Daltile. EI Paso. TX DATE : 17•Jun•08 PLACE : Canibined Kiln Exhaust RUNtt : 1
TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 51.9 NOZZLE DIAMETER (INCH.) : 0.24867 PARTICULATE WEIGHT (Front half mg) : 37.68 METER COEFFICIENT (Y) : 1.001 PARTICULATE WEIGHT (Back half mg) : 18.31 PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •0.3 GAS METER VOL.(Cu.Ft.) : 41.045 PERCENT CO2 2.5 BAROMETRIC PRESSURE 26.1 PERCENT 02 17.5 PERCENT CO 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 63 STACK LENGTH(inchs) : STACK AREA (Sq.Ft.) : 21.64754 STACK WIDTH(inchs) : NOZZLE AREA (feet): 0.000337 STACK AREA (Sq.Ft.) : 0

~
ENTER THE STACK AREA SHOWN ABOVE: 21.64754


### FLOWS SAMPLED VOLUME (STD. CU .FT.): 33.7449 VOLUME OF WATER VAPOR (STD. CU .FT.): 2.4429 FRACTIONAL MOISTURE CONTENT 0.0675

DRY BASE: 80.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1000 MOLECULAR WT. OF STACK GAS (WET BASE): 28.3507 STACK PRESSURE (inch Hg): 26.0779 STACK GAS VELOCITY (ft/sec.): 51.9162 ACTUAL STACK GAS FLOW RATE (ACFM): 67431.5028 STANDARD STACK GAS FLOW RATE (SCFH): 2141831.46



### PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0172 PARTICULATE CONCENTRATION (LBS/SCF): 2.46E•06 PARTICULATE EMISSION (LBS/HR): 5.2735



### BACK HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0084 PARTICULATE CONCENTRATION (LBS/SCF): 1.20E-06 PARTICULATE EMISSION (LBS/HR): 2.5626 ISOKINETIC RATIO (%): 101.1870

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. Meter Point Point Point Point Iso

deg F INLET OUTLET Volume VMSTD Velocity Moisture mis 1 350 0.40 0.632456 0.83 97 97 755.8 1.3269 47.5389 2.04359 104.2170 2 347 0.41 0.640312 0.85 98 96 757.4 1.2441 48.0402 1.91597 96.3311 3 350 0.44 0.663325 0.92 100 97 758.9 1.4064 49.8592 • 2.16603 105.3206 4 351 0.43 0.655744 0.90 101 97 760.6 1.3225 49.3198 2.03668 100.2377 5 351 0.42 0.648074 0.88 102 97 762.2 1.3212 48.7429 2.03474 101.3277 6 352 0.37 0.608276 0.77 103 98 763.8 1.236 45.7778 1.90358 101.0604 7 352 0.42 0.648074 0.88 103 98 765.3 1.3188 48.7729 2.03111 101.2092 8 353 0.56 0.748331 1.20 103 98 766.9 1.485 56.3528 2.28706 98.7554 9 350 0.68 0.824621 1.40 102 97 768.7 1.7366 61.9831 2.6745 104.6078 10 351 0.70 0.83666 1.50 104 98 770.8 1.65 62.9268 2.54105 98.0183 11 350 0.72 0.848528 1.50 105 100 772.8 1.7278 63.7801 2.66098 301.1467 12 337 0.52 0.72111 1.10 105 99 774.9 1.4897 53.7659 2.29425 101.7889 13 353 0.69 0.830662 1,50 103 100 776.711 1.7218 62.5527 2.65176 103.1544 14 352 0.68 0.824621 1.50 106 301 778.8 1.6426 62.0596 2.52977 99.0691 15 352 0.59 0.768115 1.25 106 101 780.8 1.5594 57.807 2.4016 100.9684 16 352 0.45 0.67082 0.95 107 102 782.7 1.3916 50.4848 2.14319 103.1727 17 352 0.35 0.591608 0.74 107 ] 02 784.4 1.1454 44.5234 1.76394 96.2852 18 351 0.26 0.509902 0.55 107 102 785.8 1.063 38.3507 1.63706 103.6150 19 352 0.28 0.52915 0.59 107 103 787.1 1.0622 39.8229 1.6358 99.8303 20 352 0.31 0.556776 0.66 107 103 788.4 1.1441 41.902 1.76198 102.1952 21 354 0.38 0.616441 0.80 108 103 789.8 1.2252 46.4494 1.88691 98.9701 22 353 0.49 0.7 100 108 103 791.3 1.4711 52.7132 2.26556 104.5818 23 352 057 0.754983 1.20 109 104 793.1 1.4693 56.8188 2.26283 96.7890 24 346 0.55 0.74162 120 108 103 794.9 1.5905 55.6064 2.44944 106.2640 796.845 350.625 0.6904 1.0279 104.4167 99.9583 102.1875



# gl 

# i

### EMISSION TEST SUMMARY

PLANT : Dalliie. EI Paso. Tx DATE : 17-.;un•08 PLACE : Coirbined Kiln Exhaust RUN#: 2 TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 52.2 NOZZLE DIAMETER (INCH.) : 0.24867 PARTICULATE WEIGHT (Front half mg) : 24.06 METER COEFFICIENT (Y) : 1.001 PARTiCULATE WEIGHT (Back half mg) : 8.29 PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •0.31 GAS METER VOL.(Cu.Ft.) : 41.287 PERCENT CO2 2.5 BAROMETRIC PRESSURE : 26.1 PERCENT 02 17.5 PERCENT CO 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 63 STACK LENGTH(inches) : STACK AREA (Sq.Ft.) : 21.64754 STACK WIDTH(inches) : NOZZLE AREA (feet): 0.000337 STACK AREA (Sq.Ft.) : 0

ENTER THE STACK AREA SHOWN ABOVE: 21.64754



### FLOwS SAMPLED VOLUME (STD. CU .FT.): 33.5300 VOLUME OF WATER VAPOR (STD. CU .FT.): 2.4571 FRACTIONAL MOISTURE CONTENT 0.0683.

DRY BASE: 80.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1000 MOLECULAR WT. OF STACK GAS (WET BASE): 28.3421 STACK PRESSURE (inch Hg): 26.0772 STACK GAS VELOCITY (ft/sec.): 51.6507 ACTUAL STACK GAS FLOW RATE (ACFM): 67086.6571 STANDARD STACK GAS FLOW RATE (SCFH): 2125019.33

PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0111 PARTICULATE CONCENTRATION (LBS/SCF): 1.58E•06 PARTICULATE EMISSION (LBS/HR): 3.3623

BACK HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0038 PARTICULATE CONCENTRATION (LBS/SCF): 5.45E•07 PARTICULATE EMISSION (LBS/HR): 1.1585

ISOKINETIC RATIO 101.3381

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. Meter Point Point Point Point Iso

deg F INLET OUTLET Volume VMSTO Velocity Moisture mis 1 350 0.40 0.632456 0.85 105 105 797.4 1.3082 47.5467 2.039398 102.8181 2 349 0.42 0.648074 0.89 107 105 799 1.3061 48.6908 2.036024 100.1123 3 350 0.42 0.648074 0.88 108 105 800.6 1.3049 48.7209 2.03417 100.0829 4 350 0.43 0.655744 0.91 107 105 802.2 1.3061 49.2975 2.036139 99.0080 5 352 0.40 0.632456 0.85 110 106 803.8 1.3013 47.6054 2.028627 102.4012 6 354 0.36 0.6 0.79 111 107 805.4 1.2176 45.218 1.898175 101.1235 7 354 0.41 0.640312 0.90 112 107 806.9 1.2981 48.2561 2.023568 101.0166 8 355 0.57 0.754983 1.20 112 107 808.5 1.5428 56.933 2.405013 101.8858 9 354 0.70 0.83666 1.50 112 107 810.4 1.7066 63.0535 2.660411 101.6405 10 352 0.74 0.860233 1.60 i l l 108 812.5 1.7071 64.7503 2.661158 98.7615 11 350 0.77 0.877496 1.70 i l l 108 814.6 1.8702 65.9684 2.915419 105.9383 12 344 0.59 0.768115 1.30 111 108 816.9 1.5343 57.531 2.391761 98.9178 13 350 0.69 0.830662 1.50 110 108 818.789 1.717 62.4475 2.676697 102.7477 14 354 0.65 0.806226 1.40 109 108 820.9 1.6277 60.7598 2.53747 100.6031 15 354 0.55 0.74162 1.20 110 108 822.9 1.5441 55.8909 2.407126 103.7492 16 353 0.43 0.655744 0.94 110 108 824.8 1.2994 49.3887 2.025574 98.6766 17 352 0.32 0.565685 0.70 110 108 826.4 1.2173 42.5795 1.897695 107.0987 18 353 0.26 0.509902 0.57 112 109 827.9 0.9709 38.4043 1.513611 94.8261 - 19 354 0.27 0.519615 0.59 112 109 829.1 1.1328 39.1599 1.765979 108.6352 20 355 0.31 0.556776 0.67 112 109 830.5 1.1331 41.9863 1.766376 101.4696 21 356 0.43 0.655744 0.94 113 110 831.9 1.2937 49.4797 2.016713 98.4260 22 355 0.51 0.714143 1.10 133 110 833.5 1.456 53.8532 2.269822 101.6577 23 351 0.47 0.685565 1.00 113 110 835.3 1.3748 51.5712 2.143119 99.7385 24 351 0.45 0.67082 0.98 113 110 837 1.3642 50.462 2.126611 101.1456 838.687 352.16667 0.6861 1.0400 110.5833 107.7083 109.1458



# 15

### EMISSION TEST SUMMARY

PLANT : Oaltile. EI Paso, TX OATE : 17•Jun•08 PLACE : Comtained Kiln Exhaust RUN#: 3
TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 50.5 NOZZLE DIAMETER (INCH.) : 0.24867 PARTICULATE WEIGHT (Front half mg) : 29.5 METER COEFFICIENT (Y) : 1.001 PARTICULATE WEIGHT (Back half mg) : 0.1 PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •0.29 GAS METER VOL.(Cu.Ft.) : 42.183 PERCENT CO2 3 BAROMETRIC PRESSURE 26.1 PERCENT 02 17 PERCENT CO 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 63 STACK LENGTH(inches) : STACK AREA (Sq.Ft.) : 21.64754 STACK WIDTH(inches) : NOZZLE AREA (feet): 0.000337 STACK AREA (Sq.Ft.) : 0

ENTER THE STACK AREA SHOWN ABOVE: 21.64754 

## FzowS SAMPLED VOLUME (STD. CU .FT.): 33.9619 VOLUME OF WATER VAPOR (STD. CU .FT.): 2.3770 FRACTIONAL MOISTURE CONTENT 0.0654

DRY BASE: 80.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1600 MOLECULAR WT. OF STACK GAS (WET BASE): 28.4300 STACK PRESSURE (inch Hg): 26.0787 STACK GAS VELOCITY (ft/sec.): 52.2699 ACTUAL STACK GAS FLOW RATE (ACFM): 67890.8934 STANDARO STACK GAS FLOW RATE (SCFH): 2151594.79

PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0134 PARTICULATE CONCENTRATION (LBS/SCF): 1.92E•06 PARTICULATE EMISSION (LBS/HR): 4.1210

BACK HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0000 PARTICULATE CONCENTRATION (LBS/SCF): 6.49E•09 PARTICULATE ENIISSION (LBS/HR): 0.0140 ISOKINETIC RATIO (% v ): 101.3757

POINTS STACK T. DELTA P SQUAR D,P DELTA H METER T. METER T. Meter Point Point Point Point Iso

deg F INLET OUTLET Volume VMSTD Velocity Moisture mis 1 349 0.40 0.632456 0.88 111 111 839.9 1.2946 47.4425 1.927582 101.5256 2 351 0.43 0.655744 0.94 112 111 841.5 1.2937 49.2502 1.92622 97.9717 3 352 0.42 0.648074 0.92 113 111 843.1 1.3733 48.7042 2.044705 105.2937 4 352 0.43 0.655744 0.94 113 111 844.8 1.2925 49.2806 1.924537 97.9464 5 352 0.42 0.648074 0.92 333 111 846.4 1.2925 48.7042 1.924429 99.1000 6 354 0.39 0.6245 0.86 114 111 848 1.2911 46.9903 1.922424 102.8602 7 355 0.42 0.648074 0.93 114 111 849.6 1.2914 48.7941 1.922802 99.1989 8 353 0.61 0.781025 1.35 115 lll 851.2 1.6147 58.7318 2.404239 102.7960 9 355 0.71 0.842615 1.60 116 112 853.2 1.7743 63.4412 2.641908 104.8300 10 357 0.75 0.866025 1.70 116 113 855.4 1.7733 65.2838 2.640349 102.0610 11 355 0.76 0.87178 1.70 116 113 857.6 1.7733 65.6371 2.640349 101.2632 12 350 0.49 0.7 1.10 116 113 859:8 1.4259 52.5417 2.123103 101.0960 13 350 0.70 0.83666 1.55 115 113 861.572 1.716 62.7993 2.555087 101.7929 14 357 0.72 0.848528 1.60 116 113 863.7 1.6922 63.9648 2.519626 99.4029 15 357 0.59 0.768115 1.30 116 113 865.8 1.6103 57.9029 2.397625 104.4924 16 358 0.46 0.678233 1.00 117 113 867.8 1.3664 51.1586 2.034495 100.4784 17 358 0.35 0.591608 0.77 117 114 869.5 1.2038 44.6246 1.792424 101.4849 18 357 0.26 0.509902 0.57 117 114 871 1.0427 38.438 1.552561 101.9275 19 357 0.28 0.52915 0.62 117 114 872.3 1.0429 39.889 1.552779 98.2336 20 358 0.33 0.574456 0.73 117 114 873.6 1.2037 43.3308 1.792222 104.5033 21 359 0.42 0.648074 0.93 118 114 875.1 1.2835 48.9136 1.911118 98.8378 22 358 0.50 0.707107 1.10 118 115 876.7 1.4434 53.3366 2.149169 101.8077 23 357 0.57 0.754983 1.30 119 115 878.5 1.5231 56.9131 2.267875 100.5567 24 342 0.42 0.648074 0.93 119 115 880.4 1.3478 48.4033 2.006773 102.7021 882.083 354.29167 0.6945 1.0933 115.6250 112.7500 114.1875

. 

# ~ ~

### EMISSION TEST SUMMARY

PLANT : Daltile. EI Paso. TX DATE : 17•jun•08 PLACE : Conzmon Kiln Exhaust RUN# : 4 Lead Train TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 66.1 NOZZLE DIAMETER (INCH.) : 0.24867 PARTICULATE WEIGHT (Front half mg) : 0 METER COEFFICIENT (Y) : 1.001 PARTICULATE WEIGHT (Back halt mg) : 0 PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : -0.3 GAS METER VOL.(Cu.Ft.) : 42.091 PERCENT CO2 3 BAROMETRIC PRESSURE : 26.2 PERCENT 02 17 PERCENT CO 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 63 STACK LENGTH(inchs) : STACK AREA (Sq.Ft.) : 21.64754 STACK WIDTH(inchs) : NOZZLE AREA (teet): 0.000337 STACK AREA (Sq.Ft.) : 0

ENTER THE STACK AREA SHOWN ABOVE: 21.64754



### FLOwS SAMPLED VOLUME (STD. CU .FT.): 33.8290 VOLUME OF WATER VAPOR (STD. CU .FT.): 3.1113 FRACTIONAL MOISTURE CONTENT 0.0842

DRY BASE: 80.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1600 MOLECULAR WT. OF STACK GAS (WET BASE): 28.2200 STACK PRESSURE (inch Hg): 26.1779 STACK GAS VELOCITY (ft/sec.): 51.9939 ACTUAL STACK GAS FLOW RATE (ACFM): 67532.3344 STANDARD STACK GAS FLOW RATE (SCFH): 2100617.23

ISOKINETIC RATIO (%): 103.4298

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. Meter Point Point Point Point Iso

deg F iNLET OUTLET Volume VMSTD Velocity Moisture mis 1 350 0.38 0.616441 0.84 114 114 882.4 1.2118 46.3535 2.37099 99.0137 2 350 0.42 0.648074 0.94 114 115 883.9 1.3726 48.7321 2.68554 106.6752 3 355 0.42 0.648074 0.94 116 115 885.6 1.3702 48.8823 2.68087 106.8180 4 357 0.43 0.655744 0.95 117 115 887.3 1.2885 49.5214 2.52105 99.3970 5 358 0.43 0.655744 0.95 117 115 888.9 1.369 49.5517 2.67862 105.6739 6 357 0.40 0.632456 0.89 117 116 890.6 1.2872 47.7627 2.51844 102.9503 7 358 0.42 0.648074 0.94 118 116 892.2 1.2862 48.9722 2.51661 100.4576 8 358 0.62 0.787401 1.40 118 116 893.8 1.6099 59.5005 3.14982 103.4857 9 359 0.69 0.830662 1.50 118 116 895.8 1.6908 62.8079 3.30823 103.0927 10 358 0.71 0.842615 1.60 119 116 897.9 1.7703 63.6728 3.46373 106.3424 11 356 0.73 0.8544 1.60 119 116 900.1 1.7703 64.4844 3.46373 104.7473 12 350 0.45 0.67082 1.00 119 116 902.3 1.348 50.4425 2.63745 101.2129 13 350 0.68 0.824621 1.50 117 116 903.978 1.71 62.0076 3.34579 104.4482 14 357 0.67 0.818535 1.50 118 117 906.1 1.6089 61.8154 3.14797 99.4303 15 358 0.59 0.768115 1.30 119 117 908.1 1.6066 58.0431 3.14349 105.8710 16 358 0.45 0.67082 1.00 119 117 910.1 1.3645 50.691 2.66972 102.9559 17 359 0.35 0.591608 0.78 119 117 911.8 1.2032 44.7326 2.35419 103.0062 18 359 0.26 0.509902 0.58 119 117 913.3 1.0422 38.5546 2.03915 103.5189 19 358 0.27 0.519615 0.60 120 117 914.6 1.0414 39,2651 2.0375 107.4397 20 359 0.32 0.565685 0.72 120 117 915.9 1.202 42.7725 2.35176 107.6153 21 358 0.42 0.648074 0.94 120 118 917.4 1.2818 48.9722 2.50792 100.1106 22 358 0.51 0.714143 1.10 121 118 919 1.4414 53.9647 2.82024 102.1626 23 355 0.56 0.748331 1.25 121 118 920.8 1.6023 56.4444 3.13491 108.1745 24 350 0.44 0.663325 0.98 121 118 922.8 1.3137 49.8789 2.57025 99.7486 924.441 356.04167 0.6889 1.0750 118.3333 116.3750 117.3542



# 4.7

### EMISSION TEST SUMMARY

PLANT : Daltile. EI Pasu. TX DATE : 17-Jun•08 PLACE : Common Kilri Exhaust RUNts : 5 Lead Train
TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 67.6 NOZZLE DIAMETER (INCH.) : 0.24867 PARTICULATE WEIGHT (Front half mg) : 0 METER COEFFICIENT (Y) : 1.001 PARTICULATE WEIGHT (Back half mg) : 0 PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : 0.3 GAS METER VOL.(Cu.Ft.) : 42.465 PERCENT CO2 3 BAROMETRIC PRESSURE 26.2 PERCENT 02 16.5 PERCENT CO 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 63 STACK LENGTH(inches) : STACK AREA (Sq.Ft.) : 21.64754 STACK WIDTH(inches) : NOZZLE AREA (feet): 0.000337 STACK AREA (Sq.Ft.) : 0

ENTER THE STACK AREA SHOWN ABOVE: 21.64754

FLOwS SAMPLED VOLUME (STD. CU .FT.): 34.0628 VOLUME OF WATER VAPOR (STD. CU .FT.): 3.1819 FRACTIONAL MOISTURE CONTENT (aJ o ): 0.0854 ORY BASE: 80.5000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1400 MOLECULAR WT. OF STACK GAS (WET BASE): 28.1883 STACK PRESSURE (inch Hg): 26.1779 STACK GAS VELOCITY (ft/sec.): 52.6691 ACTUAL STACK GAS FLOW RATE (ACFM): 68409.4273 STANDARD STACK GAS FLOW RATE (SCFH): 2120978.88

ISOKINETIC RATIO (gb): 103.1449

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. Meter

deg F INLET OUTLET Volume

1 353 0.38 0.616441 0.85 117 1I7 924.7 2 355 0.43 0.655744 0.96 119 118 926.3 3 357 0.43 0.655744 0.91 119 118 927.9 4 357 0.42 0.648074 0.94 119 118 929.6 5 359 0.40 0.632456 0.89 120 118 931.2 6 359 0.38 0.616441 0.85 120 118 932.8 7 360 0.42 0.648074 0.91 121 118 934.4 8 361 0.61 0.781025 1.40 121 118 936 9 361 0.70 0.83666 1.60 122 119 937.9 10 361 0.74 0.860233 1.70 122 119 940.1 11 358 0.73 0.8544 1.60 122 119 942.3 12 346 0.57 0.754983 1.30 121 120 944.5 13 355 0.70 0.83666 1.60 118 119 946.4 14 360 0.67 0.818535 1.50 120 119 948.5 15 359 0.59 0.768115 1.30 119 119 950.6 16 360 0.45 0.67082 1.00 119 119 952.6 17 360 0.34 0.583095 0.76 118 118 954.3 18 359 0.27 0.519615 0.60 113 118 955.8 19 359 0.30 0.547723 0.67 118 118 957.1 20 360 0.35 0.591608 0.78 117 118 958.5 21 361 0.45 0.67082 1.00 117 117 959.9 22 358 0.55 0.74162 1.20 117 117 961.7 23 355 0.61 0.781025 1.40 116 116 963.6 24 350 0.40 0.632456 0.90 116 116 965.6 967.165 357.625 0.6968 1.1092 119.0000 118.0833 118.5417 Point Point Point Point Iso VMSTD Velocity Moisture mis 1.2859 46.4654 2.555413 105.3426 1.283 49.4887 2.549572 98.9239 1.363 49.5493 2.708541 105.2209 1.2829 48.9698 2.549429 100.2118 1.2816 47.8481 2.546871 102.7090 1.2815 46.6365 2.546586 105.3654 1.2806 49.0596 2.544816 100.2140 1.5228 59.1601 3.026114 98.9422 1.7612 63.3743 3.499841 106.8220 1.7617 65.1598 3.500819 103.9238 1.7612 64.8997 3.499841 104.4127 1.5197 56.6627 3.020056 101.2127 1.6869 63.1423 3.352307 101.9444 1.6835 61.9636 3.345587 104.3113 1.6039 58.1113 3.187243 105.8329 1.3621 50.7815 2.706884 102.9817 1.2032 44.1407 2.390952 104.6473 1.0423 39.3112 2.07123 101.6665 1.1227 41.4377 2.230993 103.8889 1.124 44.7851 2.233612 96.3541 1.4473 50.8125 2.876046 209.4841 1.5285 56.0726 3.037526 304.4011 1.6127 58.9436 3.204739 104.3990 1.2601 47.5845 2.504203 100,4319



# P

### EMISSION TEST SUMMARY

PLANT : Daltite. EI Paso, TX DATE : l 7•Jurn08 PLACE : Cammon Kilri Exhaust RUNx : 6 Laad Train
TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 49.1 NOZZLE DIAMETER (INCH.) : 0.24867 PARTICULATE WEIGHT (Front half mg) : 0 METER COEFFICIENT (Y) : 1.001 PARTICULATE WEIGHT (Back half mg) : 0 PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •0.31 GAS METER VOL.(Cu.Ft.) : 41.393 PERCENT CO2 2.5 BAROMETRIC PRESSURE 26.2 PERCENT 02 17 PERCENT CO 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 63 STACK LENGTH(inches) : STACK AREA (Sq.Ft.) : 21.64754 STACK WIDTH(inches) : NOZZLE AREA (feet): 0.000337 STACK AREA (Sq.Ft.) : 0

ENTER THE STACK AREA SHOWN ABOVE: 21.64754

FLOWS SAMPLED VOLUME (STD. CU .FT.): 33.3615 VOLUME OF WATER VAPOR (STD. CU.FT.): 2.3111 FRACTIONAL MOISTURE CONTENT 0.0648

DRY BASE: 80.5000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.0800 MOLECULAR WT. OF STACK GAS (WET BASE): 28.3622 STACK PRESSURE (inch Hg): 26.1772 STACK GAS VELOCITY (ft/sec.): 51.2055 ACTUAL STACK GAS FtAW RATE (ACFM): 66508.4212 STANDARD STACK GAS FLOW RATE (SCFH): 2102636.36

ISOKINETIC RATIO (%): 101.9021

POtNTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. Meter

deg F INLET OUTLET Volume

1 353 0.39 0.6245 0.87 112 113 967.5 2 355 0.42 0.648074 0.92 112 113 969.1 3 358 0.42 0.648074 0.93 114 113 970.7 4 359 0.41 0.640312 0.91 115 113 972.4 5 361 0.40 0.632456 0.89 115 113 974 6 362 0.38 0.616441 0.84 117 114 975.6 7 362 0.38 0.616441 0.84 117 114 977.2 8 363 0.61 0.781025 1.35 117 114 978.8 9 363 0.68 0.824621 1.50 118 114 980.7 10 362 0.72 0.848528 1.60 117 115 982.8 11 358 0.74 0.860233 1.60 117 115 984.9 12 353 0.49 0.7 1.10 117 115 987.1 13 359 0.69 0.830662 1.50 116 115 988.884 14 361 0.67 0.818535 1.50 118 115 991 15 362 0.58 0.761677 1.30 118 115 993.1 16 363 0.41 0.640312 0.91 118 116 995 17 363 0.32 0.565685 0.71 118 116 996.6 18 363 0.25 0.5 0.56 118 116 998 19 362 0.26 0.509902 0.58 117 116 999.3 20 361 0.31 0.556776 0.69 118 116 1000.6 21 362 0.38 0.616441 0.84 118 116 1002 22 361 0.48 0.69282 1.10 118 116 1003.6 23 359 0.54 0.734847 1.20 117 116 1005.3 24 353 0.38 0.616441 0.84 116 116 1007.2 1008.893 359.91667 0.6785 1.0450 116.5833 114.7917 115.6875 Point Point Point Point Iso VMSTO Velocity Moisture mis 1.2961 46.929 1.93 0094 102.8065 1.2963 48.7603 1.910362 99.2025 1.3749 48.85 2.026277 105.4153 1.2929 48.2944 1.905316 100.3853 1.2928 47.7601 1.905209 101.7507 1.2892 46.5791 1.899978 104.1707 1.2892 46.5791 1.899978 104.1707 1.5331 59.0511 2.259445 97.8340 1.6938 62.3473 2.49616 102.3696 1.6942 64.1159 2.496858 99.4527 1.7749 64.8419 2.615756 102.5205 1.4373 52.6025 2.118177 101.7097 1.7082 62.6513 2.517364 102.2389 1.6923 61.8119 2.493995 102.9160 1.5303 57.5457 2.255211 100.0834 1.2861 48.4122 1.89541 100.1069 1.1247 42.7699 1.657555 99.0936 1.044 37.8036 1.538512 104.0600 1.0449 38.5288 1.539932 102.0713 1.1247 42.0451 1.657462 100.5512 1.2859 46.5791 1.895038 103.8999 1.3672 52.3185 2.014944 98.2351 1.5298 55.4245 2.25458 103.5056 1.363 46.3234 2.008669 109.5254



# 19

## PLANT : Daltile, EI Paso, TX

DATE : 18•Jun•08 PLACE : Spray Dryer RUN# : 1
TEST DURATiON (MINUTES) : NOZZLE DIAMETER (INCH.) : METER CQEFFICIENT (Y) ; PITOT COEFFICIENT (Cp) : GAS METER VOL.(Cu.Ft.) : BAROMETRIC PRESSURE : 

# EMISSION TEST SUMMARY

60 LIQUID COLLECTED (mis) : 

## 0.5 PARTICULATE WEIGHT (Front half mg) : 1.001 PARTiCULATE WEIGHT (Back half mg) : 0.84 STATIC PRESSURE (in. H20) : 35.453 PERCENT CO2 26.15 PERCENT 02

. PERCENT CO : 162.3 0 0 •0.74 1 

## 19 0

C

~ 

## 7 FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 42 STACK LENGTH(inchs) : STACK AREA (Sq.Ft.) : 9.621128 STACK WIDTH(inchs) : NOZZLE AREA (feet): 0.001364 STACK AREA (Sq.Ft.) :

ENTER THE STACK AREA SHOWN ABOVE: 9.621128


# FLOWS SAMPLED VOLUME (STD. CU .FT.): 29.5458 VOLUME OF WATER VAPOR (STD. CU .FT.): 7.6395 FRACTIONAL MOISTURE CONTENT 

## (aJ a ): 0.2054 DRY BASE: 80.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 28.9200 MOLECULAR WT. OF STACK GAS (WET BASE): 26.6766 STACK PRESSURE (inch Hg): 26.0956 STACK GAS VELOCITY (ft/sec.): 76.5517 ACTUAL STACK GAS FLOW RATE (ACFM): 44190.8065 

## STANDARD STACK GAS FLOW RATE (SCFH): 1614930.13

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 142 1.60 1.264911 0.80 91 92 2 143 1.90 1.378405 93 92 3 143 1.50 1.224745 94 92 4 142 1.90 1.378405 95 93 5 142 1.20 1.095445 95 93 6 142 1.40 1.183216 95 94 7 142 1.30 1.140175 95 94 8 142 1.10 1.048809 96 94 9 140 1.60 1.264911 96 94 10 140 1.70 1.30384 96 95 11 1.39 1.80 1.341641 97 94 12 139 1.20 1.095445 98 95 13 140 0.40 0.632456 100 96 14 139 0.92 0.959166 100 96 15 138 1.10 1.048809 100 97 16 139 1.00 1 101 97

140.75 1.1475 0.8000 96.3750 94.2500 95.3125 

# 20

## PLANT

: 

## Dattile. EI Paso. TX

DATE

: 

## 18-Jun•08 PLACE

: 

## Spray Dryer RUN#

: 

## 2
TEST DURATION (MINUTES) : NOZZLE DIAMETER (INCH.) : METER COEFFICIENT (Y) : PITOT COEFFICIENT (Cp) : GAS METER VOL.(Cu.Ft.) : BAROMETRIC PRESSURE :



# EMISSION TEST SU11fIMARY

60 LIQUID COLLECTED (mis)

: 

## 0.5 PARTICULATE WEIGHT (Front half mg) 1.001 PARTICULATE WEIGHT (Back half mg)

: 

## 0.84 STATIC PRESSURE (in. H20)

: 

## 37.352 PERCENT CO2 26.15 PERCENT 

## 02

: 

## PERCENT CO 176.1 0 0 •0.7 1 19 0

X FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 42 STACK LENGTH(inches) : STACK AREA (Sq.Ft.) : 9.621128 STACK WIDTH(inches) : NOZZLE AREA (feet): 0.001364 STACK AREA (Sq.Ft.) :

ENTER THE STACK AREA SHOWN ABOVE: 9.621128


# tteITi'lk SAMPLED VOLUME (STD. CU .FT.): 30.7785 VOLUME OF WATER VAPOR (STD. CU .FT.): 8.2890 FRACTIONAL MOISTURE CONTENT 0.2122

DRY BASE: 80.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 28.9200 MOLECULAR WT. OF STACK GAS (WET BASE): 26.6031 STACK PRESSURE (inch Hg): 26.0985 STACK GAS VELOCITY (ft/sec.): 73.6131 ACTUAL STACK GAS FLOW RATE (ACFM): 42494.441 STANDARD STACK GAS FLOW RATE (SCFH): 1539960.3

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 138 1.70 1.30384 0.80 98 98 2 140 1.70 1.30384 0.80 100 97 3 141 1.90 1.378405 102 98 4 143 1.70 1.30384 103 99 5 142 0.22 0.469042 102 99 6 142 0.89 0.943398 102 99 7 142 1.20 1.095445 103 99 8 139 1.00 1 104 100 9 140 1.70 1.30384 102 101 10 139 1.90 1.378405 104 101 11 139 1.70 1.30384 104 101 12 141 0.48 0.69282 104 101 13 142

- 

## 0.95 0.974679 105 101 14 142 1.20 1.095445 105 102 15 142 1.20 1.095445 106 102 16 14C 0.98 0.989949 107 103

140.75 1.1020 0.8000 103.1875 100.0625 101.6250


# 21

## PLANT

: 

## Daltile, EI Paso, TX

DATE

: 

## 18-Jun-08 PLACE

: 

## Spray Dryer RUN#: 3
TEST DURATION (MINUTES) : NOZZLE DIAMETER (INCH.) : METER COEFFICiENT (Y) : PITOT COEFFICIENT (Cp) : GAS METER VOL.(Cu.Ft.) : BAROMETRIC PRESSURE 

# EMISSION TEST SUMMARY

60 LIQUID COLLECTED (mis)

: 

## 0.5 PARTICULATE WEIGHT (Front half mg) 1.001 PARTICULATE WEIGHT (Back half mg)

: 

## 0.84 STATIC PRESSURE (in. H20)

: 

## 37.545 PERCENT CO2

. 

## 26.15 PERCENT 02 PERCENT CO 191.1 0 0 -0.73 1 19 0

0 FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 42 STACK LENGTH(inchs) : STACK AREA (Sq.Ft.) : 9.621128 STACK WIDTH(inchs) : NOZZLE AREA (feet): 0.001364 STACK AREA (Sq.Ft.) :

ENTER THE STACK AREA SHOWN ABOVE: 9.621128



## FL01NS SAMPLED VOLUME (STD. CU .FT.): 30.7035 VOLUME OF WATER VAPOR (STD. CU .FT.): 8.9951 FRACTIONAL MOISTURE CONTENT 0.2266

DRY BASE: 80.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 28.9200 MOLECULAR WT. OF STACK GAS (WET BASE): 26.4457
STACK PRESSURE (inch Hg): 26.0963 STACK GAS VELOCITY (ft/sec.): 69.8104 ACTUAL STACK GAS FLOW RATE (ACFM): 40299.2931 STANDARD STACK GAS FLOW RATE (SCFH): 1430892.35

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 141 1.50 1.224745 0.80 102 103 2 142 1.70 1.30384 104 103 3 142 1.50 1.224745 105 103 4 142 0.51 0.714143 106 103 5 142 0.85 0.921954 106 103 6 143 1.20 1.095445 107 104 7 143 1.20 1.095445 108 104 8 142 1.00 1 107 104 9 141 1.30 1.140175 106 104 10 142 1.40 1.183216 109 104 11 142 1.50 1.224745 109 105 12 142 1.20 1.095445 109 106 13 142 0.29 0.538516 110 106 14 141 0.73 0.8544 110 106 15 141 1.10 1.048809 110 106 16 142 0.98 0.989949 110 107

141.875 1.0410 0.8000 107.3750 104.4375 105.9063 

# -.2.zPOINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T deg F INLET OUTLET

90 91 92 93 93 94 94 95 95 95 96 96 96 96 96 97 97 97 97 97 97 98 98 98 91 96 98 99 99 l00 l00 100 101 101 101 102 98 100 100 101 101 101 102 102 103 103 103 103

100.2083 95.3333 Meter Point Point Point Volume VMSTD Velocity Moisture mis 124.705 2.5973 52.6455 0.66518 127.8 2.7547 53.7163 0.70548 131.1 2.664 53.7163 0.68225 134.3 2.659 53.3618 0.68098 137.5 2.6588 51.9193 0.68093 140.7 2.5707 50.4356 0.65837 143.8 2.4045 48.5606 0.61581 146.7 2.652 53.4096 0.67919 149.9 2.816 56.5234 0.7212 153.3 2.9825 59.4744 0.76383 156.9 2.9799 58.5072 0.76315 160.5 2.8548 5.6.8588 0.73113 163.953 1.8615 37.5136 0.47673 166.2 1.8192 36.4857 0.4659 168.4 1.902 37.4801 0.4871 170.7 1.8987 37.9491 0.48626 173 1.8987 37.9832 0.48626 175.3 1.9814 39.4187 0.50744 177.7 2.3937 48.0812 0.61302 180.6 2.4767 50.3904 0.63429 183.6 2.7225 52.6455 0.69725 186.9 2.6378 53.3618 0.67555 190.1 2.4721 49.6771 0.63312 193.1 2.3926 47.3288 0.61274 196.004 97.7708 Point Iso

99.6526 103.5821 100.1718 100.6504 103.4381 102.9538 100.1955 100.4751 100.8118 101.4741 103.0591 101.5971 100.4083 100.8910 102.5006 100.8771 100.9677 101.3474 100.3763 99.0986 104.4565 99.8479 100.5166 102.1077 1 98 0.73 0.8544 0.86 2 98 0.76 0.87178 0.90 3 98 0.76 0.87178 0.90 4 98 0.75 0.866025 0.88 5 98 0.71 0.842615 0.85 6 98 0.67 0.818535 0.80 7 99 0.62 0.787401 0.75 8 99 0.75 0.866025 0.90 9 99 0.84 0.916515 1.00 10 99 0.93 0.964365 1.10 11 99 0.90 0.948683 1.10 12 99 0.85 0.921954 1.00 13 99 0.37 0.608276 0.44 14 99 0.35 0.591608 0.42 15 98 0.37 0.608276 0.44 16 97 0.38 0.616441 0.46 17 98 0.38 0.616441 0.L6 18 97 0.41 0.640312 0.49 19 97 0.61 0.781025 0.73 20 97 0.67 0.818535 0.80 21 98 0.73 0.8544 0.88 22 98 0.75 0.866025 0.90 23 98 0.65 0.806226 0.78 24 98 0.59 0.768115 0.71

98.166667 0.7961 0.7729



### EMISSION TEST SUMMARY

PLANT : Daltde, EI Paso. TX DATE : 19-Jun•08 PLACE : Balthouse RUN# : 1
TEST DURATION (N1INUTES) : 120 LIQUID COLLECTED (mis) : NOZZLE DIAMETER (INCH.) : 0.1927 PARTICULATE WEIGHT (Front half mg) : METER COEFFICIENT (Y) : 1.001 PARTICULATE WEIGHT (Back hatf mg) : PITOT COEFFICIENT (Cp) : 0.8351 STATIC PRESSURE (in. H20) : GAS METER VOL.(Cu.Ft.) : 71.299 PERCENT CO2 BAROMETRIC PRESSURE : 26.1 PERCENT 02 PERCENT CO

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 32.5 STACK LENGTH(inchs) : STACK AREA (Sq.Ft.) : 5.76095 STACK WIDTH(inchs) : NOZZLE AREA (feet): 0.000203 STACK AREA (Sq.Ft.) :

ENTER THE STACK AREA SHOWN ABOVE: 5.76095

FLOWS SAMPLED VOLUME (STD. CU .FT.): 59.0399 VOLUME OF WATER VAPOR (STD. CU .FT.): 0.7108 FRACTIONAL MOISTURE CONTENT (Q(,): 0.0119

DRY BASE: 79.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 28.8400 MOLECULAR WT. OF STACK GAS (WET BASE): 28.7111 STACK PRESSURE (inch Hg): 26.0912 STACK GAS VELOCITY (ft/sec.): 49.0589 ACTUAL STACK GAS FLOW RATE (ACFM): 16957.5395 STANDARD STACK GAS FLOW RATE (SCFH): 829314.219

PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0190 PARTICULATE CONCENTRATION (LBS/SCF): 2.71 E•06 PARTICULATE EMISSION (LBS/HR): 2.2462

BACK HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0014 PARTICULATE CONCENTRATION (LBS/SCF): 1.97E•07 PARTICULATE EMISSION (LBS/HR): 0.1635
ISOKINETIC RATIO (%): 101.3121 15.1 72.52 5.28 •0.12 0 21 0

0



# 23

### EMISSION TEST SUMMARY

PLANT : Daltile. EI Paso. TX DATE : 19•Jun•08 PLACE: BaRhouse RUN3s : 2
TEST DURATION (MINUTES) : 120 LlQUID COLLECTED (mis) ; 18 NOZZLE DIAMETER (INCH.) : 0.1927 PARTICULATE WEIGHT (Front half mg) : 72.67 METER COEFFICIENT (Y) : 1.001 PARTICULATE WEIGHT (Back halt mg) : 5.42 PITOT COEFFICIENT (Cp) : 0.8351 STATIC PRESSURE (in. H20) : .0.12 GAS METER VOL.(Cu.Ft.) : 70.695 PERCENT CO2 0 BAROMETRIC PRESSURE 26.1 PERCENT 02 21 PERCENT CO 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DlAMETER (inch): 32.5 

### STACK LENGTH(inches) : STACK AREA (Sq.Ft.) : 5.76095 

### STACK WIDTH(inches) : NOZZLE AREA (feet): 0.000203 STACK AREA (Sq.Ft.) : 0

ENTER THE STACK AREA SHOWN ABOVE: 5.76095

FLOWS SAMPLED VOLUME (STD. CU .FT.): 58.0500 VOLUME OF WATER VAPOR (STD. CU .FT.): 0.8473 FRACTtONAL MOISTURE CONTENT 0.0144

DRY BASE: 79.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 28.8400 MOLECULAR WT. OF STACK GAS (WET BASE): 28.6841 STACK PRESSURE (inch Hg): 26.0912 STACK GAS VELOCITY (ft/sec.): 48.8161 ACTUAL STACK GAS FLOW RATE (ACFM): 16873.6239 STANDARD STACK GAS FLOW RATE (SCFH): 818912.745

PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0193 PARTICULATE CONCENTRATION (LBS/SCF): 2.76E•06 PARTICULATE EMISSION (LBS/HR): 2.2605

BACK HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0014 PARTICULATE CONCENTRATION (LBS/SCF): 2.06E•07 PARTICULATE EMISSION (LBS/HR): 0.1686 ISOKINETIC RATIO (gy): 100.8789

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. Meter Point Point Point Point Iso

deg F INLET OUTLET Volume VMSTD Velocity Moisture mis 1 98 0.68 0.824621 0.82 98 98 196.261 2.5158 50.8345 0.78113 100.2151 2 99 0.72 0.848528 0.87 103 98 199.3 2.6376 52.3551 0.81896 102.1995 3 100 0.69 0.830662 0.83 104 98 202.5 2.5526 51.2986 0.792571 101.1240 4 100 0.68 0.824621 0.82 104 99 205.6 2.5503 50.9255 0.791843 101.7713 5 99 0.65 0.806226 0.78 104 99 208.7 2.4677 49.745 0.766213 100.6342 6 100 0.65 0.806226 0.78 104 99 211.7 2.4677 49.7895 0.766213 100.7242 7 101 0.62 0.787401 0.75 105 99 214.7 2.4653 48.6703 0.765467 103.1238 8 101 0.75 0.866025 0.90 105 100 217.7 2.6285 53.5302 0.816116 99.9654 9 102 0.89 0.943398 1.10 105 100 220.9 2.8765 58.3646 0.893129 100.5158 10 102 0.88 0.938083 1.05 105 100 224.4 2.8761 58.0358 0.893004 101.0711 11 101 0.79 0.888819 0.95 105 100 227.9 2.7931 54.9391 0.867246 103.5039 12 101 0.68 0.824621 0.82 105 100 231.3 2.508 50.9709 0.778706 100.1722 13 97 0.33 0.574456 0.40 102 100 234.354 1.7649 35.3811 0.548 100.8320 14 101 0.37 0.608276 0.44 104 100 236.5 1.8884 37.5984 0.586347 102.2544 15 102 0.38 0.616441 0.46 ] 04 100 238.8 1.8064 38.137 0.560885 96.6044 16 102 0.40 0.632456 0.48 105 100 241 1.969 39.1277 0.611365 102.6326 17 103 0.42 0.648074 0.50 105 101 243.4 2.0493 40.1297 0.636309 104.3384 18 103 0.48 0.69282 0.58 106 101 245.9 2.1299 42.9004 0.661323 101.4364 19 103 0.62 0.787401 0.75 107 101 248.5 2.3747 48.757 0.737328 99.5098 20 103 0.71 0.842615 0.85 107 102 251.4 2.5369 52.1759 0.787701 99.3421 21 102 0.78 0.883176 0.88 107 102 254.5 2.619 54.6389 0.813179 97.7584 22 102 0.74 0.860233 0.89 107 102 257.7 2.6191 53.2195 0.813202 100.3686 23 102 0.68 0.824621 0.82 107 102 260.9 2.5367 51.0163 0.787635 101.4111 24 101 0.63 0.793725 0.76 107 102 264 2.4185 49.0612 0.750921 100.3581 266.956 101.04167 0.7897 0.7617 304.7917 100.1250 102.4583



# 24

### EMISSION TEST SUMMARY

PLANT : Daltile. EI Paso, TX OATE : 19-Jun•08 PLACE: Baqhouse RUN#: 3 TEST DURATION (MINUTES) : 120 LIQUID COLLECTED (mis) : 14.3 NOZZLE DIAMETER (INCH.) : 0.1927 PARTICULATE WEIGHT (Front half mg) : 77.19 METER COEFFICIENT (Y) : 1.001 PARTICULATE WEIGHT (Back half mg) : 8.5 PITOT COEFFICIENT (Cp) : 0.8351 STATIC PRESSURE (in. H20) : •0.13 GAS METER VOL.(Cu.Ft.) : 71.467 PERCENT CO2 0 BAROMETRIC PRESSURE 26.1 PERCENT 02 21 PERCEIVT CO 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 32.5 STACK LENGTH(inches) : STACK AREA (Sq.Ft.) : 5.76095 STACK WIDTH(inches) : NOZZLE AREA (feet): 0.000203 STACK AREA (Sq.Ft.) : 0

ENTER THE STACK AREA SHOWN ABOVE: 5.76095

FLOwS SAMPLED VOLUME (STD. CU .FT.): 58.2379 VOLUME OF WATER VAPOR (STD. CU .FT.): 0.6731 FRACTIONAL MOISTURE CONTENT {%}: 0.0114

ORY BASE: 79.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 28.8400 MOLECULAR WT. OF STACK GAS (WET BASE): 28.7161 STACK PRESSURE (inch Hg): 26.0904 STACK GAS VELOCITY (ft/sec.): 48.7339 ACTUAL STACK GAS FLOW RATE (ACFM): 16845.2006 STANDARD STACK GAS FLOW RATE (SCFH): 814340.639

PARTICU LATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0205 PARTICULATE CONCENTRATION (LBS/SCF): 2.92E•06 PARTICULATE EMISSION (LBS/HR): 2.3800

BACK HALF PARTICULATE CONCENTRATiON (GR./SCF): 0.0023 PARTICULATE CONCENTRATION (LBS/SCF): 3.22E•07 PARTICULATE EMISSION (LBS/HR): 0.2621 iSOKINETIC RATIO (%): 101.7734

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. Meter Point Point Point Point Iso

deg F INLET OUTLET Volume VMSTD Velocity Moisture mlS 1 104 0.66 0.812404 0.80 103 103 267.47 2.4859 50.3224 0.61122 100.8082 2 103 0.71 0.842615 0.85 108 103 270.5 2.5325 52.1475 0.622663 98.9257 3 104 0.72 0.848528 0.88 109 103 273.6 2.6937 52.5601 0.662305 104.5834 4 ] 05 0.74 0.860233 0.90 109 104 276.9 2.6099 53.3323 0.641705 100.0402 5 104 0.64 0.8 0.76 109 104 280.1 2.4458 49.5541 0.601361 100.7201 6 104 0.54 0.734847 0.66 109 104 283.1 2.2006 45.5183 0.541073 98.6574 7 103 0.59 0.768115 0.72 109 104 285.8 2.364 47.5368 0.581251 101.3031 8 104 0.70 0.83666 0.86 109 104 288.7 2.6096 51.8249 0.641633 102.7562 9 105 0.83 0.911043 1.00 110 104 291.9 2.8529 56.4824 0.701443 103.2544 10 105 0.97 0.932738 1.10 110 ' 104 295.4 2.8537 57.8274 0.70164 100.8811 11 106 0.85 0.921954 1.10 110 105 298.9 2.8511 57.2094 0.701021 102.0613 12 106 0.78 0.883176 0.97 110 105 302.4 2.7516 54.8032 0.676539 102.8217 13 104 0.35 0.591608 0.44 106 105 305.779 1.8123 36.6457 0.445594 100.9197 14 105 0.36 0.6 0.45 109 105 308 1.8718 371985 0.460236 102.8690 15 105 0•36 0.6 0.45 108 105 310.3 1.8735 37.1985 0.460642 102.9598 16 105 0.39 0.6245 0.49 109 105 312.6 1.9534 38.7174 0.4803 103.1420 17 106 0.43 0.655744 0.53 109 105 315 2.0351 40.6904 0.500369 102.4225 18 106 0.44 0.663325 0.55 109 105 317.5 2.0352 41.1609 0.500397 101.2576 19 105 0.62 0.787401 0.77 109 105 320 2.4437 48.8169 0.600848 102.3350 20 104 0.72 0.848528 0.90 110 lOS 323 2.6053 52.5601 0.640574 101.1518 21 105 0.76 0.87178 0.95 111 105 326.2 2.6847 54.0482 0.660103 101.5454 22 106 0.75 0.866025 0.93 111 106 329.5 2.6822 53.7389 0.659485 102.2148 23 107 0.68 0.824621 0.84 111 106 332.8 2.6003 51.2149 0.639339 104.1597 24 107 0.61 0.781025 0.76 110 105 336 2.3902 48.5072 0.587695 101.0904 338.937 104.91667 0.7861 0.7775 109.0417 104.5417 106.7917 

# 25,

# Sheetl

Summary of NOx Analyzer Calibrations and Bias

Plant: Daltile, Dallas, TX Source: Combined Kiln Exhaust Date: 6l17/2008

Analyzer Calibratrion Data

Cylinder Analyzer Absolute % Span Vafue Response Difference Zero Gas 0 0 0 0 Low Range 5.133 5.03 -0.103 -0.2 Mid Range 25 24.45 -0.55 -1.06796

~ 

## - High Range 51.5 51.45 -0.05 -0.09709



# System Calibration Bias and Drift Data

Analyzer Initial Values Final Values Drift Average Calibration System System System System Calibration Response Calibration Calibration Calibration Calibration Values

Response Bias Response Bias

Run #1 Zero Gas 0 0 0 0 0 0 0

Upscale 24.45 22.85 -3.1068 22.7 -3.39806 -0.29126 22.775
Average NOx Concentration: 32.34 Corrected NOx Concentration: 35.49945

Run #2 Zero Gas 0 0 0 0.3 0.582524 0.582524 0.15

Upscale 24.45 22.7 -3.39806 22.5 -3.78641 -0.38835 22.6
Average NOx Concentration: 32.81 Corrected NOx Concentration: 36.36971

Run #3 Zero Gas 0 0.3 0.582524 0.23 0.446602 -0.13592 0.265

Upscale 24.45 22.5 -3.78641 22.08 -4.60194 -0.81553 22.29
Average NOx Concentration: 32.99 Corrected NOx Concentration: 37.14529

Page 1 26

## Sheetl

Summary of Suifur Dioxide Anaiyzer Calibrations and Bias

Rlant: 

## Da1tile, EI Paso, TX Source: 

## Combined Kiln Exhaust Date: 

## 6/17/2008

Analyzer Calibratrion Data



## Cylinder Analyzer Absoiute % 

## Span Value Response Difference Zero Gas 0 -0.25 -0.25 -0.10121 Low Range 50.1 49.2 -0.9 -0.36437 Mid Range 101 101.03 0.03 0.012146 High Range 247 247.03 0.03 0.012146

System Calibration Bias and Drift Data



## Analyzer Initial Values Final Values Drift Average Calibration System System System System Calibration Response Caiibration Calibration Calibration Calibration Values

Response Bias Response Bias

Run #1 Zero Gas -0.25 0 0.101215 -0.15 0.040486 -0.06073 -0.075

Upscale 101.03 92.9 -3.2915 90.5 -4.26316 -0.97166 91.7
Average S02 Concentration: 55.08 Corrected S02 Concentration: 60.69905

Run #2 Zero Gas -0.25 0 0.101215 -0.88 -0.25506 -0.35628 -0.44

Upscale 101.03 92.9 -3.2915 91.67 -3.78947 -0.49798 92.285
Average S02 Concentration: 42.76 Corrected S02 Concentration: 47.05527

Run #3 Zero Gas -0.25 0 0.101215 -0.38 -0.05263 -0.15385 -0.19

Upscale 101.03 92.9 -3.2915 90.55 -4.24291 -0.95142 91.725
Average S02 Concentration: 45.65 Corrected S02 Concentration: 50.37089

Page 1 

# 27

# Sheetl

Surnmary of CO Analyzer Calibrations and Bias
Plant; 

# Daltiie, El Paso, T?C Source: Combined Kifn Exhaust Date: 6/17I2008

Analyzer CalibratrRon Data



# Cylinder Analyzer Absolute % 

# Span Value Response Difference Zero Gas 0 0 0 0 Low Range 24.3 24.7 0.4 0.403633 Mid Range 50.3 48.48 -1.82 -1.83653 High Range 99.1 97.2 -1.9 -1.91726

Systern Calibration Bias and Drift Data



# Analyzer Initial Vaiues Final Vaiues Drift Average Calibration System System System System Calibration Response Calibration Calibration Calibration Caiibration Values

Response Bias Response Bias



# Run #1 Zero Gas 0 0.1 0.100908 0.15 0.151362 0.050454 0.125

Upscaie 48.48 46.5 -1.99798 46.35. -2.14934 -0.15136 46.425
Average CO Concentration: 30.11 Corrected CO Concentration: 32.5755

Run #2 Zero Gas 0 0.15 0.151362 0.1 0.100908 -0.05045 0.125

Upscaie 48.48 46.35 -2.14934 46.3 -2.1998 -0.05045 46.325 Average CO Concentration: 32.09 Corrected CO Concentration: 34.80172

Run #3 Zero Gas 0 0.15 0.151362 0.25 0.25227 -0.100908 0.2

Upscale 48.48 46.35 -2.14934 46.45 -2.04844 0.100908 46.4 Average CO Concentration: 36.54 Corrected CO Concentration: 39.56498

Page 1 

# 28

## 9/17/08 Nox Converter Check

Date/Time NOx ( mm/dd/yy hh:mm:ss ppm 06/17/08 08:17:09 -0.00652 06/17/08 08:18:09 26.81592 Start Nox Converter Check 06/17/08 08:19:09 1 33.42775 06/17/08 08:20:09 33.4502 06/17/08 08:21:09 33.28907 06/17/08 08:22:09 33.19141 06117/08 08:23:09 33.20313 06/17/08 08:24:09 33.10157 06/17/08 08:25:09 33.06739 06/17/08 08:26:09 33.06544 06117/08 08:27:09 33.00001 06/17/08 08:28:09 33.01759 06/17/08 08:29:09 32.99415 06/17/08 08:30:09 32.959 06/17/08 08:31:09 i 32.95997 06/17/08 08:32:09 32.96876

_ 06/17/08 08:33:09 32.88575 06/17/08 08:34:09 32.89162 06/17/08 08:35:09 32.90431 06/17108 08:36:09 32.94377 06/17108 08:37:09 32.95548 06/17/08 08:38:09 32.89592

~ 

## 06/17/08 08:39:09 32.94279 06/17108 08:40:09 32.97346

_ 06/1 7/08 08:41:09 32.95002

~ 

## 06/17/08 08:42:09 32.90998 06/17/08 08:43:09 32.885571 06/17108 08:44:09 32.8719 06/17/08 08:45:09 32.89631 06/17/08 08:46:09 32.89991 06/17/08 08:47:09 32.91135 Sto



## Page 1 299117108 Calibrations

DatelTime S02 VOC NOx CO mmldd/yy hh:mrit:ss ppm ppm PPn► pPm 06l17/08 07:22:38 -0.7 0.1 0.0 0.4 06/17/08 07:22:48 -0.6 0.1 0.0 0.3 06l17108 07:22:58 -0.7 0.1 0.0 0.3 06l17/08 07:23:08 -0.5 0.0 0.0 0.3 06117/08 07:23:18 -0.4 0.0 0.0 0.3 06117/08 07:23:28 -0.3 0.0 0.0 0.3 06/17/08 07:23:38 -0.1 0.0 

### 0.0 0.4 06117/08 07:23:48 -0.2 0.0 0.0 0.4 06117/08 07:23:58 -0.3 0.1 0.0 0.4 06117/08 07:24:08 -0.1 0.1 0.0 0.4 06117/08 07:24:18 -0.2 0.1 0.0 0.4 06117/08 0724:28 -0.1 0.0 0.0 0.4 06117/08 07:24:38 -0.1 0.1 7.2 0.4 06117/08 07.24:48 -0.3 0.1 49.3 0.4 06117108 07:24:58 -0.1 0.1 50.5 0.4 06/17/08 07:25:08 -0.5 0.1 50.8 0.3 06/17108 07:25:18 -0.7 0.0 51.0 0.2 06/17/08 07:26:28 -0.5 0.0 51.2 0.2 06/ 17108 07:25:38 -0.4 0.1 51.3 0.1 06117/08 07:25:48 -0.2 0.1 51.4 0.0 06/17/08 07:25:58 -0.2 0.1 

### 51.4 0.0 06/17/08 07:26:08 -0.3 0.1 51.5 0.0 06/17/08 07:26:18 -0.4 0.1 

### 51.5 0.0 06/17/08 07:26:28 -0.3 0.0 

### 51.4 0.0 06117/08 07:26:38 -0.4 0.0 512 0.0 06117/08 07:26:48 -0.3 0.0' 61.2 D.0 06117108 07:26:58 -0.4 0.0 47.5 0.0 06117/08 07:27:08 -0.2 0.1 1.3 0.0 06/17/08 07:27:18 -0.3 0.1 1.2 0.0 06117/08 07:27:28 -0.2 0.1 0.5 0.2 06117f08 07:27:38 0.0 0.1 0.2 0.3 06/17/08 07:27:48 -0.1 0.1 15.5 0.3 06/17/08 07:27:58 -0.1 0.1 24.8 0.3 06/17/08 07:28:08 -0.3 0.0 25.0 0.2 06117108 07:28:18 -0.3 0.0 25.1 0.1 06/17/08 07:2828 -0.5 0.1 25.1 0.1 06/17/08 07:28:38 -0.5 0.1 25.2 0.0 06117108 07:28:48 -0.4 0.1 25.3 0.0 06/17/08 07:28:58 

### -0.4 0.1 

### 26.3 0.0 06/17/08 07:29:08 

### -0.2 0.1 

### 25.5 0.0 06/17/08 07:29:18 

### -0.2 0.1 

### 25.5 0.0 06/17/08 0729:28 

### -0.2 0.1 

### 25.5 0.0 06/17/08 07:29:38 -0.4 0.1 3.2 0.0 06117/08 07:29:48 -0.3 0.0 0.2 0.0 06117108 07:29:58 -0.3 0.0 0.8 0.0 06/17108 07:30:08 -0.3 0.0 6.2 0.1 06117108 07:30:18 -02 0.0 5.0 0.2 06/17/D8 07:30:28 -0.3 0.0 5.0 0.2 06/17108 07:30:38 -0.2 0.1 

### 5.0 0.1 06117/08 07:30:48 -0.2 0.1 

### 5.1 0.0 06/17/08 07:30:58 -0.4 0.1 

### 5.0 0:0 06/17108 07:31:08 -0.5 0.1 5.0 O.o 06117/08 07:31:18 -0.5 0.1 0.5 0.0 06117/08 07:31:28 -0.4 0.1 0.0 0.0 06/17/08 07:31:38 -0.4 0.0 0.0 0.1 06/17/08 07:31:48 8.7 0.0 1.7 0.2 06/17/08 07:31:58 54.2 0.1 1.6 0.3 06117/08 07:32:08 87.1 0.1 1.5 0.2 06117108 07:32:18 99.2 0.1 1.5 0.2 06/17/08 07:32:28 102.9 0.1 1.5 0.1 06117/08 07:32:38 104.3 0.1 1.5 0.1 06/17/08 07:32:48 105.0 0.1 1.5 0.1 06117108 07:32:58 105.3 0.1 1.5 0.1 06/17/08 07:33:08 105.4 0.1 1.5 0.1 06/17/08 07:33:18 105.4 0.1 1.5 0.1 06/17108 07:33:28 105.6 0.1 1.5 0.1 06l17108 07:39:38 105.7 0.1 1.5 0.1 06117108 07:33:48 105.8 0.0 1.5 0.1 Zero NOx

51.5 ppm NOx

25 ppm NOx Zero S02, CO

5.133 ppm NOx



### Page 1 

# 309/17108 Calibratfons

06/17/08 07:33:58 105.9 0.0 1.5 0.1 06/17/08 07:34:08 105.8 0.1 1.5 0.1 06/17/08 07:34:18 106.8 0.1 1.0 -0.5 06117/08 07:34:28 105.9 0.1 1.5 0.1 06117108 07:34:38 104.9 0.1 1.5 0.1 06117108 07:34:48 100.8 0.1 1.5 0.1 06117/08 07:34:58 

### 100.9 0.1 1.5 0.1 06/17/08 07:35:08 100.9 0.1 1.5 0.1 101 ppm S02 06/17/08 07:35:18 

### 101.2 0.1 1.5 0.1 06/17/08 07:35:28 

### 101.1 0.1 1.5 0.1 06117/08 07:35:38 100.9 0.1 1.5 0.1 06117108 07:35:48 86.2 0.1 0.7 0.1 06/17108 07:35:58 44.1 0.2 0.0 0.2 06/17/08 07:36:08 16.7 0.1 0.0 0.2 06117/08 07:36:18 20.5 0.1 0.0 0.2 06/17/08 07:36:28 36.7 0.0 0.0 0.2 06117108 07:36:38 44.6 0.0 0.0 0.1 06/17/08 07:36:48 47.2 0.0 0.0 0.1 06/17108 07:36:58 47.9 0.0 0.0 0.0 06/17/08 07:37:08 48.4 0.0 0.0 0.0 06117108 07:37:18 48.7 0.0 0.0 0.0 06117/08 07:37:28 48.8 0.0 0.0 0.0 06117/08 07:37:38 49.0 0.1 0.0 0.0 06/17/08 07:37:48 49.1 0.1 0.0 0.0 06f17/08 07:37:58 

### 49.2 0.1 0.0 0.0 06117/08 07:38:08 

### 49.2 0.1 0.0 0.0 50.1 ppm S02 06/17/08 07:38:18 

### 49.2 0.1 0.0 0.0 06/17/08 07:38:28 

### 49.2 0.1 0.0 0.0 06/17108 07:38:38 49.1 0.1 0.0 0.0 06/17/08 07:38:48 49.2 0.1 0.0 0.0 06/17108 07:38:58 48.7 0.1 0.0 0.0 06117108 07:39:08 38.1 0.1 0.0 0.0 06/17/08 07:39:18 182 0.1 0.0 0.0 06117/08 07:39:28 6.7 0.1 0.0 0.2 06/17/08 07:39:38 2.3 0.1 0.0 0.3 06117108 07:39:48 0.9 0.0 0.0 0.3 06/17108 07:39:58 40.8 0.0 0.7 0.3 06117/08 07:40:08 151.3 0.1 1.3 0.3 06J17/08 07:40:18 216.5 0.0 1.2 0.2 06117/08 07:40:28 238.1 0.0 12 02 06117108 07:40:38 244.6 0.1 12 0.1 OGl17108 07:40:48 246.3 0.1 12 0.1 06/17108 07:40:58 246.7 0.1 1.1 0.1 06/17108 07:41:08 

### 246.7 0.0 1.1 0.1 06/17/08 07:41:18 

### 247.0 0.0 1.2 0.1 247 ppm S02 06/17/08 07:41:28 

### 247.2 0.1 9.2 0.1 06/17/08 07:41:38 

### 247.2 0.1 1.2 0.1 06/17/08 07:41:48 242.7 0.1 1.1 0.1 06/17108 07:41:58 1603 0.1 0.1 0.1 06/17108 07:42:08 66.4 0.0 0.0 0.1 06117108 07:42:18 23.4 0.0 0.0 0.1 06117108 07:42:28 10.5 0.0 0.0 0.2 06/17/08 07:42:38 6.4 0.0 0.0 0.4 06117/08 07:42:48 4.1 0.0 0.0 0.4 06/17/08 07:42:58 2.8 0.0 0.0 0.8 06/17/08 07:43:08 1.2 0.0 0.0 4.9 06/17/08 07:43:18 0.1 0.1 0.0 16.2 06/17/08 07:43:28 -0.2 0.1 0.0 28.4 06/17/08 07:43:38 -0.3 0.1 0.0 39.6 06/17/08 07:43:48 -0.2 0.1 0.0 46.2 06/17/08 07:43:58 -0.3 0.1 0.0 49.0 06117/08 07:44:08 -0.3 0.1 0.0 49.7 06117/08 07:44:18 -0.3 0.1 0.0 49.8 06/17/08 07:44:28 -0.5 0.1 0.0 49.9 08117108 07:44:38 -0.5 0.2 0.0 49.9 06/17/08 07:44:48 -0.5 0.2 0.0 48.5 06J17/08 07:44:58 -0.5 0.1 0.0 48.4 06117108 07:45:08 -0.4 0.1 0.0 48.4 06/17/08 07:45:18 -0.5 0.1 0.0 

### 48.4 06/17/08 07:45:28 -0.4 0.1 0.0 

### 48.5 50.3 ppm CO 06/17/08 07:45:38 -0.4 0.1 0.0 48.5



### Page 2 

# 319117108 Calibrations

06117J08 07:45:48 -OA 0.9 0.0 

### 48.5 06117108 07:45:58 -0.2 0.1 0.0 48.4 06117108 07:46:08 0.5 0.1 0.0 48.5 06/17108 07:46:18 0.6 0.7 0.0 39.0 06117l08 07:46:28 0.5 0.1 0.0 27.0 06117/08 07:46:38 0.2 0.1 0.0 17.3 06117/08 07:46:48 0.0 0.9 0.0 14.5 06117/08 07:46:58 0.1 0.1 0.0 17.1 0611 7108 07:47:08 0.0 0.1 0.0 21.1 06/17/08 07:47:18 0.0 0.1 0.0 23.6 06/17/08 07:47:28 -0.1 0.9 0.0 24.5 06117i08 07:47:38 -0.2 0.1 0.0 24.7 06/1710807:47:48 -0.1 0.1 o.0 

### 24.7
06t17108 07:47:58 -0.1 0.2 0.0 

### 24.7 06/17108 07:48:08 -0.4 0.1 0.0 

### 24.7
06117108 07:48:18 -0.4 0.1 0.0 

### 24.7 06/17/08 07:48:28 -0.3 0.1 0.0 

### 24.7 06/1 7108 07:48:38 -0.5 0.1 0.0 24.7 06117108 07:48:48 -0.3 0.1 0.0 24.7 06/17108 07:48:58 -0.3 0.1 0.0 24.6 06/17108 07:49:08 -0.2 0.1 0.0 22.8 0611 7108 07:49:'i 8 ,-01 0.1 0.0 18.0 06117/08 07:49:28 -0.1 0.0 0.0 11.6 06/17/08 07:49:38 -0.3 0.4 0.0 10.0 06117108 a7:49:48 -0.3 0.0 0.0 20.5 0611 7108 07:49:58 -0.3 0.1 0.0 42.7 06/1 7108 07:50:08 -0.3 0.2 0.0 67.0 06/17108 07:50:18 -0.3 0.2 0.0 84.9 06/17/08 0750:28 -0.4 0.2 0.0 93.7 06/17108 07:50:38 -0.5 0.2 0.0 96.4 0617 7108 07:50:48 -0.5 0.2 0.0 97.0

06117108 47:55:48 -0.5 0.1 0.0 8.8 06117108 07:55:58 -0.5 0.1 0.0 2.9 06117108 07:56:08 -0.5 0.1 0.0 1.0 06/17108 07:56:18 -0.4 0.1 0.0 0.5 06/17/08 07:56:28 -0.6 46.2 0.1 0.4 06/17108 07:56:38 0.1 0.5 0.0 0.4 061 7108 07:56:48 0.0 0.1 0.0 0.4 06/17/08 07:56:58 0.1 0.0 0.0 0.5 06t47/08 07:57:08 0.2 0.6 0.0 5.8 , 06/17108 07:57:18 0.2 1.5 0.0 22.5 06/17108 07:57:28 0.1 0.8 0.0 47.4 06/17108 07:57:38 0.0 

### 0.2 0.0 71.5 06117/08 07:57:48 0.0 0.9 0.0 87.8 06/17f08 07:57:58 0.1 0.3 0.0 94.8 06/7 7/08 07:58:08 0.1 0.4 0.0 96.7 06117108 07:58:18 

### -0.2 0.3 0.0 97.2 06117/08 07:58:28 -0.3 

### 0.2 0.0 972 06/17/08 07:58:38 -0.3 0.3 0.0 

### 97.2 06117/08 07:58:48 -0.3 0.2 0.0 

### 97.2 06/17/08 07:58:58 -0.2 02 0.0 

### 97.2 06/17108 07:59:08 -0.2 0.2 0.0 

### 97.2 06117/08 07:59:18 -0.3 0.2 0.0 97.2 06117l08 07:59:28 -0.5 0.2 0.0 96.1 06/17/08 07:59:38 -0.3 0.2 0.0 84.5 0619 7108 07:59:48 -0.2 0.2 0.0 60.9 06117/08 07:59:58 -0.3 0.1 0.0 37.0 06/17108 08:00:08 -0.4 0.1 0.0 18.5 06/17108 08:00:18 -0.5 0.1 0.0 7.3 06/17/08 08:00:28 -0.3 0.1 OA 2.4 06/17/08 08:00:38 -0.3 0.1 0.0 0.8 06/17108 08:00:48 -0.3 0.1 0.0 0.4 24.3 ppm CO

99.1 ppm CO



### Page 3 

# 329117/08 Bias Calibrations

DatelTime S02 VOC 

### NOx CO 

### mm/ddlyy hh:mm:ss ppm ppm ppm ppm 06/17J08 08:54:14 -0.7 0.8 0.0 0.1 06/17108 08:54:24 -0.7 0.9 0.0 0.1 08/17/08 08:54:34 -0.7 0.9 0.0 0.2 06117/08 08:54:44 -0.5 0.9 0.0 0.3 06117/08 08:54:54 -0.1 0.3 0.0 0.2 06/17/08 08:55:04 -0.2 0.1 0.9 0.2 06/17J08 08:55:14 -0.2 0.1 8.1 0.2 06/17/08 08:55:24 0.0 0.1 14.6 0.2 06/17108 08:55:34 0.1 0.1 18.8 0.2 06t17108 08:55:44 0.0 0.1 21.1 0.2 06/17/08 08:55:54 -0.3 0.1 221 0.1 06/17108 08:56:04 -0.3 0.0 22.5 0.1 06/17108 08:56:14 -0.4 0.1 22.7 0.1 06/17108 08:56:24 -0.4 0.1 22.7 0.1 06/17108 08:56:34 -0.3 0.1 22.9 0.1 06/17/08 08:56:44 -0.3 0.1 22.7 0.1 06/17/08 08:56:54 

### 0.0 0.1 

### 22.9 0.1 06/17/08 08:57:04 

## 0.1 0.0 

### 22.8 0.1 06/17J08 08:57:14 

### 0.0 0.1 

### 22.8 0.1 06/17/08 08:57:24 

## -0.1 0.1 

### 22.9 0.1 06117/08 08:57:34 -0.2 0.2 22.8 0.1 06117108 08:57:44 -0.2 0.1 22.4 0.1 06117108 08:57:64 -0.6 0.1 15.6 0.2 06/17108 08:58:04 -0.6 0.1 7.5 1.6 06/17108 08:58:14 -0.5 0.1 3.7 6.3 06/17/08 08:58:24 -0.4 0.1 1.5 14.8 06117/08 08:58:34 -0.4 0.1 0.5 24.8 06/17/08 08:58:44 -0.4 0.1 0.1 33.7 06/17/08 08:58:54 -0.5 0.1 0.0 39.8 06/17/08 08:59:04 -0.5 0.1 0.0 43.2 06/17/08 08:59:14 -0.5 0.1 0.0 45.0 06/17/08 08:59:24 -0.5 0.1 0.0 45.8 06117/08 08:59:34 -0.5 0.1 0.0 46.2 06/17/08 08:59:44 -0.5 0.1 0.0 46.4 06117/08 08:59:54 -0.3 0.1 0.0 46.5 06/17108 09:00:04 -0.6 0.1 0.0 46.5 06/17/08 09:0014 -0.5 0.1 0.0 46.6 06117/08 09:00:24 -0.5 0.1 0.0 46.6 06117108 09:00:34 -0.5 0.1 0.0 46.6 06/17108 09:00:44 -0.4 0.1 

### 0.0 46.6 06/17108 09:00:54 -0.3 0.1 

### 0.0 46.5 06/17/08 09:01:04 -0.2 0.1 

### 0.0 46.5 06117108 09:01:14 -0.1 0.1 

### 0.0 46.5

. 06/17/08 09:01:24 -0.2 0.4 0.0 46.5 06/17/08 09:01:34 -0.1 0.1 0.0 46.5 06/17108 09:01:44 3.5 0.1 0.1 45.5 06/17l08 09:01:54 19.7 0.1 0.6 41.7 06117/08 09:02:04 40.5 0.1 0.9 34.0 06/17/08 09:02:14 58.0 0.1 1.1 24.3 06/17/08 09:02:24 70.5 0.1 1.3 15.3 06/17/08 09:02:34 78.7 0.1 1.3 8.5 06/17108 09:02:44 83.7 0.1 1.3 

### 4.4 06/17/08 09:02:54 86.5 0.1 1.3 2.2 06/17/08 09:03:04 88.1 0.1 1.2 1.1 06117J08 09:03:14 89.1 0.1 1.3 0.6 06/17108 09:03:24 89.9 0.1 1.2 0.4 06117108 09:03:34 90.7 0.1 1.3 0.2 06/17/08 09:03a44 91.1 0.0 1.3 0.2 06117/08 09:03:54 91.7 0.1 1.2 0.2 06/17/08 09:04:04 91.7 0.0 1.3 0.2 06/17108 09:04:14 91.8 0.0 1.2 0.2 06117/08 09:04:24 92.0 0.1 1.2 0.2 06/17/08 09:04:34 92.3 0.1 1.3 0.2 06/17/08 09:04:44 92.3 0.1 1.3 0.2 06/17/08 09:04:54 92.2 0.1 1.3 0.2 06/17/08 09:05:04 92.5 0.1 1.3 0.2 06/17/08 09:05:14 92.6 0.1 1.3 0.2 06/17/08 09:05:24 

### 92.8 0.1 1.3 0.2 06117108 09:05:34 

### 92.7 0.1 1.3 0.2 06/17/08 09:05:44 92.8 0.1 1.2 0.2 25 

### ppm NOx Zero S02, CO

50.3 

### ppm CO Bias Zero NOx Bias

101 ppm S02 Bias



### Page 

## 1 

# 1339/17/08 Bies Calibrnaiions

06/17/08 09:05:54 

### 93.3 0.5 1.3 0.2 06117/08 09:06:04 92.8 0.3 1.2 0.2 06/17/08 09:06:14 86.1 0.1 0.9 0.2 06/17108 09:06:24 67.4 0.1 0.3 0.2 06117/08 09:08:34 46.4 0.1 0.0 0.2 06/17/08 09:06:44 30.2 0.1 0.0 0.2 06/17/08 09:06:54 19.8 1.1 0.0 0.2 06117/08 09:07:04 13.5 2.2 0.0 0.2 06117/08 09:07:14 9.0 0.1 0.0 0.1 06/17/08 09-07:24 6.0 0.0 0.0 0.1 06117/08 09:07:34 4.0 0.1 0.0 0.1 06/17/08 09:07:44 2.8 0.1 0.0 0.1 06117/08 09:07:64 2.1 0.1 0.0 0.1 06/17/08 09:08:04 1.5 3.8 0.0 0.1 06117/08 09:08:14 1.2 19.1 0.0 0.1 06117/08 09:08:24 1.1 19.7 0.0 0.1 06117/08 09:08:34 1.0 19.6 0.0 0.2 06/17108 09:08:44 0.7 19.8 0.0 0.2 06/17/08 09:08:54 0.6 19.7 0.0 0.2 06/17108 09:09:04 0.5 19.7 0.0 0.2 06/17108 09:09:14 0.6 19.9 0.0 0.2 06/17/08 09:09:24 0.5 202 0.0 0.2 06117i08 09:09:34 0.5 

### 20.2 0.0 02 06/17/OB 09:09:44 0.5 

### 20.3 0.0 0.2 20.2 ppm CH4 06117/08 09:09:54 0.5 

### 20.3 0.0 0.2 06117/08 09:10:04 0.5 

### 20.3 0.0 02 06/17108 09:10:14 0.5 20.2 0.0 0.2 06/17108 09:10:24 0.5 5.3 0.0 0.2 06/17/08 09:10:34 0.5 2.3 0.0 0.2 06/17/08 09:10:44 0.5 2.3 0.0 0.2 06117108 09:10:54 0.2 2.3 0.0 0.2 06/17/08 09:11:04 0.2 2.4 0.0 0.2 06l17i08 09:11:14 OZ 2.4 0.0 0.2 06/17/08 09:11:24 0.1 2.4 0.0 0.2 06117/08 09:11:34 0.2 2.4 0.0 0.2 06117/08 09:11:44 0.1 2.3 0.0 0.2 06117/08 09:11:54 0.3 2.6 0.0 0.2 06/17/08 09:12:04 0.2 2.3 0.0 0.2 06/17/08 09:12:14 0.1 2.3 0.0 0.2 06117/08 09:12:24 0.0 5.5 0.0 0.2 06/17/08 09:12:34 0.0 5.2 0.0 0.2 06/17/08 09:12:44 0.0 5.1 0.0 0.2 06117/08 09:12:54 0.3 

### 5.9 0.0 0.2 06117/08 09:13:04 0.3 5.1 0.0 0.2 5.142 ppm CH4 06117108 09:13:14 0.2 

### 5.0 0.0 0.1 06/17/08 09:1324 0.3 5.0 0.0 0.1 06117/08 09:13:34 0.4 3.6 0.0 D,1 06/17/08 09:13:44 0.3 2.3 0.0 0.1 06/17/08 D9:13:54 0.3 2.3 0.0 0.1 06/17/08 09:14:04 0.3 2.4 0.0 0.1 06/17/08 09:14:14 0.1 31.4 0.0 0.1 06/17108 09:14:24 0.2 41.6 0.1 0.1 06/17108 09:14:34 0.3 41.7 0.1 0.1 06117/08 0"4:44 02 

### 41.8 0.0 02 06117/08 09:14:54 0.2 

### 41.8 0.0 0.2 41 ppm CH4 06/17108 09:15:04 0.2 

### 41.8 0.0 0.2 06/17108 09:15:14 0.2 

### 42.0 0.0 0.2 06/17/08 09:16:24 0.1 13.1 0.0 0.2 06/17/08 09:16:34 0.1 2.3 0.0 0.2 06/17108 09:15:44 0.1 2.3 0.0 0.2



### Page 2 

# 346117/08 Run 112

DatelTime S02 VOC NOx CO 

### mm/dd/yy hh:mm:ss ppm ppm ppm ppm 06/17/08 09:19:54 55.7 5.6 32.9 42.1

Start Run #1 06/17108 09:20:04 55.3 5.6 32.9 42.2 06117/08 09:20:14 54.6 5.6 32.9 41.8 06117/08 09:2024 54,2 5.7 32.9 41.1 06/17108 09:20:34 53.9 5.7 32.9 40.0 06117108 09:20:44 53.6 5.6 33.0 38.5 06/17/08 09:20:54 53.7 5.8 33.0 37.1 06/17/08 09:21:04 53.6 5.6 33.2 36.6 06117108 09:21:14 53.3 5.6 33.0 36.7 06/17108 09:21:24 53.4 5,6 32.9 37.1 06/17/08 09:21:34 53.3 5.6 32.9 37.7 46/17/08 09:21:44 53.0 5.6 33.0 38.0 06117108 09:21:54 52.9 6.7 33.0 38.3 06/17/08 09:22:04 52.8 5.6 33.1 38.3 06/17/08 09:22:14 52.7 5.6 33.3 38.2 06117/08 09:22:24 52.5 5.6 33.3 38.0 06117/08 09:22:34 52.5 5.5 33.5 37.6 06/17/08 09:22:44 52.5 5.6 33.4 37.0 06117108 09:22:54 52.2 5.6 33.4 36.5 06117108 09:23:04 52.2 5.6 33.5 36.1 06/17/08 09:23:14 52.3 5.7 33.4 35.5 06/17/08 09:2324 53.0 5.7 33.3 35.2 06/17/08 09:23:34 53.6 5.6 33.2 34.9 06117108 0923:44 54.1 5.6 33.2 34,6 06117/08 09:23:54 55.1 5.6 33.4 34.7 06117/08 09:24:04 56.0 5.7 33.5 34.9 06117f08 09:24:14 56.3 5.6 33.6 34.9 06l17/08 09:24:24 55.8 5.7 33.6 34.8 06/17/08 09:24:34 55.2 5.7 33.7 34.5 06/17/08 09:24:44 54.9 5.7 33.5 34.1 06117/08 09:24:54 55.2 5.6 33.3 34.0 06117/08 09:25:04 55.7 5.6 33.2 33.9 06117/08 09:25:14 56.2 5.6 33.1 33.7 06117/08 09:25:24 56.8 5.9 33.2 33.3 08/17/08 09:25:34 57.1 5.6 33.1 32.6 06l17108 09:25:44 57.4 5.8 32.9 32.0 06117108 09:25:54 57.8 5.6 32.6 32.3 06/17108 09:26:04 58.7 5.6 32.5 33.0 06l17/08 09:2614 59.0 5.6 32.5 33.8 06/17/08 09:26:24 59.6 5.7 32.2 34.4 06117/08 09:26:34 60.0 5.7 31.9 34.5 06/17/08 09:26:44 60.8 5.6 31.6 34.1 06117/08 09:26:54 62.1 5.6 31.6 33.6 06/17/08 09:27:04 63.6 5.6 31.4 33.1 06/17/08 09:27:14 64.4 5.7 31.3 32.9 06117/08 09:27:24 65.0 5.6 31.1 32.8 06117/08 09:27:34 65.2 5.7 31.1 32.9 06117/08 09:27:44 65.3 6.0 30.9 33.1 OfiJ17/08 09:27:54 65.0 6.1 30.8 33.3 06117/08 09:28:04 64.6 5.9 30.7 33.9 06117108 09:28:14 64.3 5.9 30.6 35.2 06/17108 09:28:24 64.1 5.9 30.5 37.5 06/17108 09:28:34 64.4 5.9 30.7 39.8 06/17/08 09:28:44 64.1 5.9 30.7 41.2 06/17/08 09:28:54 64.0 5.9 30.7 41.4 06117/08 0929:04 63.9 5.7 30.8 40.7 06/17/08 09:29:14 64.3 5.9 31.0 39.7 06/17/08 09:29:24 64.5 5.9 31.2 38.9 06/17108 09:29:34 63.9 5.9 31.3 38.0 06/17108 09:29:44 63.5 5.7 31.4 36.8 06/17108 09Z9:54 63.2 5.8 31.3 35.6 06/17/08 09:30:04 63.1 5.9 31.3 34.6 06117/08 09:30:14 63.0 5.9 31.4 33.8 06!17/08 09:3024 62.6 5.8 31.3 33.3 06/17/08 09:30:34 62.6 5.7 31.2 33.1 06/17/08 09:30:44 63.1 5.8 31.1 32.8 06/17/08 09:30:54 63.9 5.9 30.9 32.6 06117/08 09:31:04 64.5 5.9 31.0 32.5 06/17108 09:31:14 64.9 5.9 30.9 32.4 06/17/08 09:31:24 64.9 5.6 30.8 32.3



### Page 1 

# 356117/08 Run #2

06/17/08 09:31:34 64.6 5.6 30.7 32.2 06/17/08 09:31:44 64.0 5.6 30.8 31.9 06117/08 09:31:54 63.2 5.6 31.1 31.6 O6/i 7/08 09:32:04 62.3 5.6 31.2 31.3 06/17/08 09:32:14 62.0 5.6 31.3 31.1 06/17/08 09:32:24 61.6 5.6 31.4 30.9 06/17/08 09:32:34 61.3 5.6 31.6 30.7 06117/08 09:32:44 61.1 5.6 31.9 30.6 06117/08 09:32:54 61.3 5.6 32.0 30.3 06/17/08 09:33:04 60.6 5.6 32.1 30.0 06/17/08 09:33:14 60.0 5.6 32.3 29.8 06117/08 09:33:24 59.4 5.6 32.5 29.4 06117108 09:33:34 58.8 5.6 32.5 29.0 06/17/08 09:33:44 58.6 5.6 32.4 28.6 06117/08 09:33:54 58.2 5.6 32.3 28.4 06/17108 09:34:04 58.2 5.6 32.3 28.3 06l17/08 09:34:14 58.8 5.5 32.3 28.1 06/17/08 09:34:24 59.5 5.6 32.2 28.1 06/17/08 09:34:34 60.0 5.6 32.3 28.2 06I17108 09:34:44 60.5 5.4 32.5 28.2 06117/08 09:34:54 60.7 5.6 32.4 28.2 06117108 09:35:04 60.9 5.6 32.2 28.0 06/17/08 09:35:14 60.6 5.6 32.2 27.7 06/17/08 09:35:24 60.3 5.6 32.4 27.5 06117/08 09:35:34 60.0 5.6 32.4 27.2 06/17108 09:35:44 59.9 5.6 32.4 27.1 06117/08 09:35:54 60.7 5.6 32.4 27.1 06117/08 09:36:04 60.5 5.6 32.6 27.3 06/17108 09:36:14 60.3 5.6 32.9 27.5 06117108 09:36:24 60.0 5.6 33.3 27.6 06117108 09:36:34 59.2 5.6 33.4 27.6 06/17108 09:36:44 58.5 5.6 33.5 27.6 06117/08 09:36:54 58.2 5.6 33.7 27.6 06/17/08 09:37:04 58.0 5.6 33.6 27.5 06117/08 09:37:14 58.0 5.4 33.4 27.5 06/17/08 09:37:24 58.3 5.3 33.4 27.4 06/17108 09:37:34 58.4 5.3 33.5 27.4 06/17/08 09:37:44 58.0 5.3 33.5 27.4 06/17108 09:37:54 57.8 5.3 33.6 27.5 06/17/08 09:38:04 57.7 5.3 33.7 27.5 06/17108 09:38:14 57.5 5.3 33.8 27.6 06/17/08 09:38:24 57.3 5.3 33.8 27.5 06f1710809:38:34 57.0 5.3 33.7 27.3 06/17/08 09:38:44 56.8 5.3 33.7 26.9 06/17/08 0938:54 56.8 5.3 33.6 26.5 06/17108 09:39:04 56.9 5.3 33.5 26.2 06117/08 09:39:14 57.0 5.3 33.4 25.9 06/17108 09:3924 57.4 5.3 33.2 25.7 06/17/08 09:39:34 57.2 5.3 33.3 25.6 06/17/08 09:39:44 56.6 5.3 33.2 25.4 06/17/08 09:39:54 55.7 5.3 33.0 25.2 06117/08 09:40:04 55.1 5.3 33.0 25.1 06117/08 09:40:14 54.8 5.3 33.1 25.1 06117/08 09:40:24 54.5 5.3 33.1 25.1 06117/08 09:40:34 54.6 5.2 33.2 25.1 06117/08 09:40:44 54.9 5.2 33.1 25.1 06/17108 09:40:54 55.0 5.2 33.1 25.1 06/17/08 09:41:04 55.4 5.2 33.3 25.1 06/17108 09:41:14 55.7 5.3 33.3 25.0 06/17108 09:41:24 55.3 5.3 33.3 24.9 06/17/08 09:41:34 55.2 5.2 33.2 24.7 06117/08 09:41:44 54.9 5.3 33.0 24.6 06117/08 09:41:54 54.2 5.2 32.8 24.5 06/17/08 09:42:04 54.0 5.3 32.8 24.5 06/17/08 09:42:14 54.1 5.3 32.7 24.4 06117108 09:42:24 54.3 5.2 32.6 24.4 06117/08 09:42:34 54.7 5.3 32.5 24.5 06J17108 09:42:44 55.0 5.3 32.4 24.5 06117/08 09:42:54 55.6 5.3 32.4 24.5 06/17/08 09:43:04 56.0 5.3 32.3 24.7 06117/08 09:43:14 56.6 5.3 32.4 24.9 06/17/08 09:43:24 56.6 5.3 32.5 25.2 06/17i08 09:43:34 56.4 5.3 32.4 25.3 06/17/08 09:43:44 55.8 5.3 32.1 25.5



### Page 2 

# 3 b

~6117/08 Run 92

06/17/08 09:43:54 55.3 5.3 31.8 25.7 06117/08 09:44:04 55.1 5.3 31.5 25.9 06117/08 09:44:14 54.9 5.3 31.5 26.2 06117/08 09:44:24 54.9 5.2 31.6 26.3 06117108 09:44:34 54.7 5.2 31.8 26.5 06/17108 09:44:44 54.6 5.2 31.6 26.6 06/17/08 09:44:54 54.6 5.2 31.4 26.7 06/17/08 09:45:04 54.5 5.2 31.5 26.9 06117/08 09:45:14 54.2 5.3 31.6 27.1 06117/08 09:4S:24 54.0 5.3 31.7 27.2 06117108 09:45:34 53.6 5.3 31.7 27.2 06/17108 09:45:44 53.5 5.3 31.9 27.9 06117108 09:45:54 53.4 5.3 32.0 27.2 06117108 09:46:04 53.1 5.3 32.1 27.3 06117108 09:46:14 52.6 5.3 32.1 27.3 06/17108 09:46:24 52.5 5.3 32.1 27.4 06117108 09:46:34 52.2 5.3 31.9 27.3 06/17/08 09:46:44 51.8 5.3 31.9 27.3 06/17/08 09:46:54 51.5 5.3 31.7 27.1 06117/08 09:47:04 51.4 5.3 31.6 27.1 06117/08 09:47:14 51.5 5.3 31.6 27.2 06117108 09:47:24 51.6 53 31.6 27.3 0611 T108 09:47:34 51.7 5.3 31.5 27.6 06117108 09:47:44 51.3 5.5 31.5 27.7 06/17108 09:47:54 50.8 5.3 31.6 27.8 06117108 09:48:04 50.$ 5.3 31.6 27.8 06117/08 09:48:14 50.3 5.3 31.6 27.9 06117108 09:48:24 50.4 5.3 31.6 27.9 06117108 09:48:34 50.5 5.3 31.5 27.9 06/17108 09:48:44 50.5 5.3 31.5 27.9 06/17/08 09:48:54 50.9 5.3 31.4 28.0 06/17/08 09:49:04 51.3 5.3 31.4 28.0 06/17108 09:49:14 51.4 5.3 31.5 28.0 06117108 09:49:24 51.4 5.3 31.5 28.0 06117/08 09:49:34 51.4 5.3 31.6 28.1 06117108 09:49:44 51.8 5.4 31.6 28.1 06117108 09:49:54 52.1 5.3 31.7 28.1 06117108 09:50:04 52.4 5.3 31.7 28.0 06l17108 09:50:14 52.7 5.3 31.7 28.0 06/17108 09:50:24 53.0 5.3 31.6 28.0 06/17r08 09:60:34 53.2 5.3 31.5 28.1 06117/08 09.

- 50:44 53.2 5.3 31.3 28.3 06/17108 09:50:54 53.3 5.4 31.2 28.3 06117108 09:51:04 53.3 5.4 31.2 28.5 06/17/08 09:51:14 53.0 5.4 31.0 28.6 06/17108 09:51:24 52.8

- 5.6 30.7 28.9 06/1 7/08 09:51:34 53.0 5.5 30.5 29.1 06/17/08 09:51:44 53.3 5.3 30.5 29.3 06117/08 09:51:54 54.0 5.3 30.6 29.5 06/17/08 09:52:04 54.4 5.5 30.8 29.5 06/17/08 09:52:14 55.1 5.5 31.0 29.5 06117108 09:52:24 55.9 5.5 31.0 29.4 06/17108 09:52:34 56.3 5.5 30.8 29.3 061171Q8 09:52:44 56.9 5.5 30.7 29.3 06/17108 09:52:54 56.9 5.6 30.8 29.3 06/17/08 09:53:04 57.3 5.3 31.0 29.3 06/17108 09:53:14 57.3 5.5 31.0 29.4 06/17/08 09:53:24 57.2 5.6 31.0 29.5 06/17/08 09:53:34 56.9 5.6 31.1 29.6 06/17108 09:53:44 56.2 6.4 31.4 29.7 06/17/08 09:53:54 55.9 5.4 31.5 29.7 06117108 09:54:04 56.0 5.4 31.5 29.7 06/17/08 09:54:14 56.0 5.4 31.5 29.7 06117108 09:54:24 56.0 5.6 31.6 29.8 06117108 09:54:34 56.0 5.5 31.7 29.8 06/17/08 09:54:44 56.0 5.5 31.7 29.7 06/17108 09:54:54 56.1 5.4 31.7 29.6 06/17/08 09:55:04 56.3 5.5 31.9 29.5 06117108 09:55:14 56.3 5.4 32.0 29.4 06117108 09:55:24 56.0 5.4 32.1 29.3 06117108 09:55:34 55.6 5.6 32.1 29.2 06/17/08 09:55:44 55.5 5.6 32.1 29.2 06/17/08 09:55:54 $5.5 5.6 32.0 29.2 06117/08 09:56:04 55.6 5.6 32.1 29.2

Page 3 

# 3'7611 7/08 Rurt #2

06/17/08 09:56:14 55.7 5.6 32.2 29.3 06117/08 09:56:24 56.4 5.6 32.2 29.3 06/17/08 09:56:34 57.1 5.6 32.1 29.2 06/17/08 09:56:44 57.7 5.6 32.2 29.0 08117/08 09:56:54 58.4 5.6 32.1 28.9 06117/08 09:57:04 58.9 5.6 32.0 28.8 06117/08 09:57:14 59.1 5.6 31.9 28.8 66/17/08 09:57:24 59.1 5.6 32.0 28.8 06/17/08 09:57:34 59.1 5.6 32.0 28.9 06/17/08 09:57:44 59.3 5.6 32.0 29.0 06/17108 09:57:54 59.3 5.6 32.1 29.0 06/17/08 09:58:04 59.3 5.6 32.0 29.0 06/17/08 09:58:14 59.4 5.6 32.0 29.1 06/17/08 09:58:24 60.2 5.6 32.0 29.1 06/17/08 09:58:34 61.1 5.6 32.0 29.1 06/17/08 0958:44 61.9 5.6 31.9 29.2 06/17/08 09:58:54 62.1 5.6 31.8 29.2 06/17/08 09:59:04 62.4 5.7 31.7 29.1 06/17/08 09:59:14 62.7 5.6 31.6 29.2 06117108 09:59:24 63.0 5.7 31.6 29.3 06117/08 09:59:34 63.3 5.6 31.5 29.6 06117/08 09:59:44 63.4 5.6 31.5 30.0 06/17108 09:59:54 62.9 5 1 7 31.5 30.5 06/17/0810:00:04 62.6 5.8 31.5 30.9 06/1710810:00:14 61.8 5.9 31.4 31.1 06/17/0810:00:24 61.5 5.9 31.3 31.4 06117/0810:00:34 61.6 5.9 31.2 32.0 06/17/0810:00:44 61.5 5.9 31.2 32.9 0619 7/0810:00:54 61.6 5.7 31.4 33.9 06/1710810:01:04 61.6 5.8 31.4 34.7 06i17/0810:01:14 61.6 5.8 31.3 35.2 06/17/0810:01:24 61.6 5.9 31.3 35.7 06/17/0810:01:34 61.8 6.0 312 36.2 06/17/0810:01:44 61.9 6.2 31.3 36.7 06/17/0810:01:54 62.2 5.9 31.3 37.5 06/1 7108 1 0:02:04 62.0 5.9 31.4 38.7 06/1710810:02:14 61.6 5.9 31.4 40.6 06/1710810:02:24 61.0 5.9 31.5 42.4 0611710810:02:34 60.3 6.0 31.5 43.5 06117/0810:02:44 59.7 5.9 31.4 43.3 06/17J0810:02:54 59.2 6.0 31.3 42.4 06117/0810:03:04 58.8 5.9 31.3 41.4 06/17/0810:03:14 58.6 5.7 31.4 40.9 06/17/0810:03:24 58.9 5.6 31.4 41.0 06/1710810:03:34 59.0 5.6 31.6 41.5 06117/0810:03:44 58.7 5.6 31.8 41.4 06/1710810:03:54 57.7 5.7 32.1 39.9 06117/0810:04:04 57.1 5.6 32.4 37.2 06117/0810:04:14 56.5 5.6 32.6 34.4 06117/0810:04:24 56.1 5.6 32.6 32.2 06/17/0810:04:34 55.9 5.6 32.5 30.7 06/17/0810:04:44 55.9 5.5 32.4 29.9 06/1710810:04:54 56.1 5.6 32.4 29.4 06/17/0810:05:04 56.0 5.6 32.5 29.2 0611710810:0514 55.8 5.6 32.7 29.1 0811710810:05:24 55.9 5.6 32.7 28.9 06/17/0810:05:34 55.7 5.6 32.7 28.9 06/17i0810:05:44 55.6 5.6 32.7 28.8 06117/0810:05:54 55.3 5.6 32.8 28.8 0611710810:06:04 55.0 5.6 32.7 28.7 0611 7/08 1 0:06:14 54.7 5.6 32.7 28.7 06/1710810:0624 54.8 5.6 32.7 28.7 06117/0810:06:34 54.8 5.6 32.7 28.8 06/1710810:06:44 55.0 5.6 32.7 28.7 06/1710810:06:54 55.2 5.6 32.6 28.7 06/7710810:07:04 55.5 5.6 32.6 28.7 06/17/0810:07:14 55.7 5.6 32.6 28.7 06117/0810:07:24 55.5 5.6 32.6 28.7 06/17/0810:07:34 55.1 5.6 32.6 28.7 0611 7/08 1 0:07:44 54.7 5.7 32.7 28.7 0611710810:07:54 54.1 5.6 32.7 28.7. 06/1710810:08:04 53.6 5.5 32.7 28.6 06/1710810:08:14 53.1 5.5 32.8 28.7 06/17/0810:08:24 52.6 5.4 33.0 28.7



### Page 4 

# Wei

### 6117108 Run #2

06117/0810:08:34 52.1 5.4 33.1 28.6 06117/0810:08:44 51.5 5.4 33.0 28.5 06/1710810:08:54 50.8 5.6 33.1 28.3 06/17i0810:09:04 50.5 5.6 32.9 28.2 06/1710810:09:14 49.8 5.6 32.7 28.1 06/17/0810:09:24 49.4 5.6 32.6 28.1 06117/0810:09:34 49.2 5.6 32.6 28.0 06117/0810:09:44 49.4 5.6 32.6 28.0 06/1710810:09:54 49.5 5.6 32.7 28.0 06/17/0810:10:04 49.8 5.3 32.9 28.1 06117/0810:10:14 50.3 5.4 32.9 28.2 06117/0810:10:24 50.6 5.5 33.0 28.3 06/17/0810:10:34 50.6 5.6, 33.2 28.2 06117/0810:10:44 50.6 5.6 33.2 28.2 06117/0810:10:54 50.6 5.6 33.2 28.2 06/17/0810:1 1:04 50.6 5.6 33.3 28.2 06117/0810:11:14 50.6 5.6 33.3 28.3 06/1710810:11:24 50.5 5.6 33.3 28.4 06117/0810:11:34 50.2 5.6 33.3 28.5 06/1710810:11:44 49.8 5.6 33.3 28.5 06/17l0810:11:54 49.7 5.6 33.2 28.4 06/1710810:12:04 49.5 5.5 33.1 28.4 06/17/0810:12:14 49.5 5.6 33.1 28.4 06117/0810:12:24 49.3 5.6 33.2 28.4 06/17/0810:12:34 49.1 5.6 33.0 28.4 0611710810:12:44 49.5 5.6 33.1 28.5 0611710810:12:54 49.6 5.5 32.9 28.5 06117/0810:13:04 49.7 5.5 32.9 28.6 06/17/0810:1314 49.4 5.6 32.9 28.6 06/1710810:13:24 49.1 5.6 32.9 28.4 06117/0810:13:34 49.3 5.6 32.8 28.3 06/17/0810:13:44 49.1 5.6 32.8 28.3 06/17/0810:13:54 49.1 5.6 32.8 28.3 06/17/0810:14:04 49.5 5.6 32.9 28.3 06/17/0810:14:14 49.7 5.6 33.1 28.4 06117/0810:14:24 49.8 5.6 33.1 28.5 06117/0810:14:34 49.7 5.6 33.1 28.6 0611710810:14:44 50.0 5.6 33.2 28.5 06/1710810:14:54 49.6 5.6 33.0 28.5 06/1710810:15:04 49.7 5.6 32.8 28.5 0611710810:1514 49.7 5.6 32.6 28.4 0611710810:15:24 50.0 5.6 32.7 28.4 06117/0810:15:34 50.0 5.6 32.8 28.4 06/17l0810:15:44 49.7 5.6 32.9 28.4 06/17/0810:15:54 49.5 5.6 32.9 28.6 06/17/0810:16:04 49.1 5.6 33.0 28.6 06/17/0810:16:14 48.4 5.6 33.0 28.6 06117/0810:16:24 48.1 5.6 33.0 28.6 06/17/0810:16:34 47.8 5.6 33.0 28.6 06/17/0810:16:44 47.8 5.6 33.1 28.6 06/1710810:16:54 48.0 5.6 33.2 28.5 06117/0810:17:04 48.1 5.6 33.2 28.5 06/17/0810:17:14 48.5 5.6 32.9 28.4 0611710810:17:24 48.6 5.6 32.8 28.4 06/17/0810:17:34 48.6 5.6 32.8 28.4 06/1710810:17:44 48.5 5.5 32.8 28.4 06/17/0810:17:54 48.2 5.4 32.7 28.3 0611710810:18:04 48.0 5.6 32.9 28.3 06/17/0810:18:14 47.2 5.5 32.9 28.2 0611710810:18:24 47.0 5.5 33.1 28.2 0611710810:18:34 47.3 5.4 33.2 28.2 0611710810:18:44 47.6 5.5 33.1 28.2 0611710810:18:54 48.0 5.5 33.0 28.2 0611710810:19:04 48.4 5.6 32.8 28.2 0611710810:19:14 48.3 5.6 32.7 28.2 0611 7108 1 0:19:24 48.4 5.5 32.8 28.2 0611710810:19:34 49.0 5.6 33.0 28.1 0611710810:19:44 49.7 5.6 32.9 28.1 06117/08 10:19:54 50.2 5.6 32.9 28.1 S02 Inieriemce Average 06/1710810:20:04 50.2 5.6 33.0 28.0 55.69 06/17/0810:20:14 49.8 5.6 33.0 27.9 06/17/0810:20:24 49.5 5.6 32.9 27.8 06/1710810:20:34 49.1 5.6 32.9 27.8 06/1710810:20:44 49.0 5.6 32.9 27.8



### Page 5 3 

# ~

### 6/17l08 Run #2

06/17/0810:20:54 49.3 5.6 33.0 27.9 06/17/0810:21:04 49.4 5.6 33.2 27.9 06/17/0810:21:14 49.1 5.6 33.2 28.0 06/17/0810:21:24 49.1 5.6 33.1 28.1 08/17l081021:34 491 5.6 33.0 28.1 06/17/0810:21:44 48.7 5.6 33.0 28.3 06117/0810:21:54 48.3 5.6 33.0 28.4 06117/0810:22:04 47.3 5.6 33.0 28.5 0611710810:22:14 46.3 5.6 33.0 28.6 06J17/081022:24 45.9 5.6 33.0 28.5 06/1710810:22:34 45.6 5.6 33.1 28.5 06/17/0810:22:44 45.8 5.6 33.2 28.6 06117/0810:22:54 46.2 5.6 33.2 28.7 06117/0810:23:04 46.4 5.6 33.2 28.7 06117/0810:23:14 46.7 5.6 33.2 28.7 0611 7/08 1 0:23:24 46.9 5.6 33.3 28.7 06117/081023:34 47.0 5.5 33.4 28.7 06/17/0810:23:44 46.9 5.3 33.4 28.7 06/17/0810:23:54 46.6 5.6 33.4 28.6 06/1710810:24:04 46.4 5.6 33 4 28.7 06/17/0810:24:14 46.0 5.6 33.3 28.6 06/17l0810:24:24 46.0 5.6 33.2 28.7 06117/0810:24:34 46.1 5.5 33.1 28.6 06l17/0810:24:44 46.0 5.6 33.0 28.7 06/17/0810:24:54 46.3 5.6 33.1 28.8
Stap Run #1 55.08 5.55 32.34 30.11

06/17/0810:25:04 45.9 5.6 33.1 28.8 06/17/0810:25:14 45.4 5.6 332 28.8 06/171081025:24 45.0 5.6 33.3 28.8 06/17/0810:25:34 44.5 5.6 33.3 28.9 06117/0810:25:44 43.9 5.6 33.3 28.9 06/17/0810:25:54 43.5 5.6 33.4 28.9 06117/0810:26:04 44.1 5.2 33.4 28.9 06/17/0810:26:14 45.1 2.6 33.4 28.8 06117/0810:26:24 46.5 1.9 27.5 28.6 06/17/0810:26:34 50.0 1.7 16.6 27.5 06/17/0810:26:44 55.2 1.5 9.6 24.5 06117/081026:54 60.8 1.5 5.8 19.4 06J17/0810:27:04 65.7 1.2 4.0 13.4 06117/0810:27:14 69.1 1.2 3.1 8.0 06/17/0810:27:24 70.9 1.2 2.6 4.3 06117/0810:27:34 72.3 1.2 2.4 2.2 06117/0810:27:44 73.7 1.2 2.2 1.1 06t17/0810:27:54 74.6 1.2 2.1 0.6 06/17/081028:04 74.8 1.2 2.0 0.4 0611710810:28:14 74.8 1.2 1.9 0.3 06/17/0810:28:24 75.0 1.2 1.8 0.2 06117/0810:28:34 74.9 1.1 1.8 0.2 0611710810:28:44 74.8 0.9 1.7 0.2 06117/0810:28:54 74.7 0.9 1.7 0.2 06117/0810:29:04 74.7 1.1 1.7 0.2 06117/0810:29:14 74.7 2.3 1.6 0.1 06117/0810:29:24 74.7 3.0 1.7 0.2 06117/0810:29:34 73.5 1.6 6.7 0.3 06/1710810:29:44 66.2 1.5 7.6 1.8 06f1 7/0810:29:54 53.0 1.2 4.0 6.8 0611 7/08 1 0:30:04 39.5 1.2 2.1 15.7 06117/0810:30:14 28.1 1.2 1.1 28.6 06/17/0810:30:24 19.1 1.2 0.6 34.2 06717/0810:30:34 13.0 1.3 0.3 40.0 06/17/0810:30:44 8.0 1.2 0.1 43.3 06117/0810:30:54 4.9 1.1 0.1 44.9 06117/0810:31:04 3.1 0.9 0.1 45.7 06/17/0810:31:94 1.6 0.9 0.0 46.0 06117/0810:31:24 0.6 1.0 0.0 46.2 06/1710810:31:34 0.3 1.0 0.0 46.3 06117/0810:31:44 0.1 1.0 0.0 46.3 06l17/08 10:31:54 -0. 

### 1 0 .9 0.0 46.3 50.3 ppm CO 06117/0810:32:04 -0.2 0.9 0.0 46.4 Zero S02, NOx 06/1710810:32:14 -0.4 3.9 0.0 46.4 06117l0810:32:24 -0.3 2.1 1.4 46.4

Page 6 • 4 

# ' ~6/17/08 Run t!2

06/17/0810:32:34 2.0 1.5 11.9 46.0 0611710810:32:44 5.6 1.3 17.6 43.9 06/17/0810:32:54 5.4 1.3 19.9 38.3 06/1710810:33:04 3.9 1.2 21.3 29.4 0811710810:33:14 2.4 1.0 22.1 19.8 06/1710810:33:24 0.9 1.0 22.4 11.7 06/17/0810:33:34 0.3 1.0 22.6 6.3 06117/0810:33:44 -0.1 1.0 22.6 3.2 06117/0810:33:54 0.0 0.9 22.7 1.5 06/1710810:34:04 -0.2 0.9 22.7 0.9 06117/0810:34:14 -0.4 1.0 22.7 0.5 06117/0810:34:24 -0.6 0.9 22.7 0.3 06117/0810:34:34 -0.6 0.9 

### 22.7 

### 0.2 06117/0810:34:44 -0.6 0.9 

### 22.7 0.2 06117/0810:34:54 -0.1 0.9 

### 22.7 0.1 06117/0810:35:04 -0.2 0.9 

### 22.7 0.1 0611710810:35:14 

### -03 4.0 22.7 0.1 06117/0810:35:24 0.1 5.3 23.1 0.1 06/1710810:35:34 3.8 5.3 26.7 0.5 06/17/0810:35:44 13.7 4.7 29.9 2.7 06/17/0810:35:54 24.6 2.1 31.2 7.6 06/17/0810:36:04 34.8 1.6 24.3 14.0 06/1710810:36:14 45.2 1.5 14.4 18.5 06117/0810:36:24 56.1 1.3 7.7 18.8 06117/0810:36:34 66.1 1.2 4.6 16.6 06117/0810:36:44 72.5 1.1 3.0 10.6 06117/0810:36:64 77.4 1.1 2.2 6.2 06/17/0810:37:04 80.2 0.9 1.9 3.3 06117108 10:37:14 81.6 0.9 1.7 1.7 06/1710810:37:24 82.3 0.9 1.6 0.9 06/1710810:37:34 83.1 0.9 1.6 0.5 06/1710810:37:44 83.7 0.9 1.6 0.3 06117/0810:37:54 84.0 0.9 1.5 0.3 06117/0810:38:04 84.5 0.9 1.5 0.2 06/1710810:38:14 85.1 0.9 1.5 0.2 06117/0810:38:24 85.4 0.9 1.5 0.2 06117/0810:38:34 85.7 0.9 1.5 0.2 09/17/0810:38:44 86.1 0.9 1.5 0.2 0611 7/08 1 0:38:54 86.4 0.9 1.4 0.2 0611710810:39:04 86.7 0.9 1.4 0.1 06/1710810:39:14 86.9 0.9 1.4 0.1 0611710810:39:24 87.2 0.9 1.4 0.1 0611710810:39:34 87.4 0.8 1.4 0.1 06/17/081039:44 87.5 0.9 1.3 0.2 06/1710810:39:54 87.6 0.9 1.4 0.2 06/1710810:40:04 87.7 0.7 1.4 0.1 06/1710810:40:14 87.8 0.7 1.3 0.1 06/1710810:40:24 87.8 0.7 1.4 0.2 06/17/0810:40:34 88.0 0.8 1.4 0.2 06/17/0810:40:44 87.9 0.6 1.4 0.1 06117/0810:40:54 88.0 0.8 1.4 0.1 06117/0810:41:04 88.0 0.8 1.3 0.1 0611710810:41:14 88.1 0.9 1.3 0.2 06/1710810:41:24 88.2 0.9 1.3 0.1 08/17/0810:41:34 88.3 0.9 1.3 0.1 06/1 7108 1 0:41:44 88.3 0.8 1.3 0.1 06117/0810:41:54 88.7 0.6 1.4 0.1 06117/0810:42:04 88.9 0.7 1.3 0.1 06117/0810:42:14 88.8 0.7 1.3 0.2 06117/0810:42:24 88.9 0.7 1.3 0.2 06117J0810:42:34 88.7 0.6 1.3 0.1 06117/0810:42:44 88.8 0.6 1.4 0.1 0611710810:42:54 89.9 0.7 1.4 0.1 0611710810:43:04 90.0 0.6 1.4 0.1 0611710810:43:14 90.4 0.9 1.4 0.1 06/17/0810:43:24 90.5 0.8 1.3 0.1 06117/0810:43:34 90.6 0.6 1.4 0.1 06/1710810:43:44 90.7 0.7 1.3 0.1 0611710810:43:54 

### 90.2 0.6 1.3 0.1 06/1710810:44:04 90.3 0.7 1.4 0.1 06/1710810:44:14 90.6 4.2 1.3 0.1 06/1710810:44:24 90.1 5.1 2.9 0.1 25 ppm NOx Zero CO

101 ppm S02



### Page 

### 7 M6117/08 Run 92

0611710810:49:34 55.5 5.4 33.9 28.9 06/17/0810:49:44 55.8 5.4 33.7 28.7 0611710810:49:54 56.2 5.5 33.6 28.4 06/17/0810:5D:04 56.3 4.9 33.4 28.3 08/17lD810:50:14 56.2 1.4 33.6 28.3 06/17/0810:50:24 55.1 0.9 27.9 28.3 06/1710810:50:34 50.2 0.8 15.8 27.6 06117/0810:50:44 39.9 0.7 8.2 24.7 06/17/0810:50:54 30.4 

### 0.6 4.2 19.6 06/1710810:51

- :04 21.1 0.5 2.3 13.5 Zero Afr 06/17/0810:51:14 15.0 

### 0.5 1.5 8.1 06117/08 10:31:24 10.3 

### 0.4 1.1 4.1 06117/0810:51:34 6.8 0.8 0.9 2.1 06117/0810:51:44 4.5 4.8 0.8 1.1 06/17/0810:51:54 3.7 5.2 4.5 0.8 06/1710810:52:04 8.6 5.2 17.1 1.5 06/17/0810:52:14 16.9 5.3 25.2 4.3 06/17/0810:5224 25.4 12.0 29.2 9.7 06/17/0810:52:34 33.3 

### 20.8 30.8 15.8 06/17/0810:52:44 35.5 

### 20.9 21.7 20.7 20.2 ppm CH4 06/17/0810:52:54 32.8 

### 20.9 11.6 22.5 06117/0810:53:04 25.5 

### 20.7 6.0 20.5 06/17/0810:53:14 18.8 20.6 3.1 15.9 46117/0810 :53 : 2 4 13.6 18.6 1.7 10.6



### Page 8 

# 426/17108 Run #2

Date/TEme S02 VOC NOx CO mm/c!d/yy hh:mm:ss ppm ppm ppm ppm 06/17/0811:09:54 50.6 6.9 31.7 59.2

Start Run tl2 06117/0811:10:04 50.4 6.7 31.5 59.7 06117/0811:10:14 50.5 6.3 31.5 61.6 06117/0611:10:24 50.3 6.2 31.4 64.0 06/17/0811:10:34 49.8 6.1 31.3 65.4 06117/0811:10:44 49.4 6.0 31.3 64.7 06117/0811:10:54 48.7 5.7 31.3 62.4 06117/0811:11:04 48.7 5.9 31.3 59.3 06117/0811:11:14 48.8 5.9 31.3 56.3 06/1710811:11:24 49.0 5.6 31.4 53.6 06/1710811:11:34 49.2 5.6 31.5 51.1 06/1710811:11:44 49.3 5.4 31.7 49.1 06/1710811:11:54 49.0 5.4 31.8 47.8 06/17/0811:12:04 48.6 5.3 32.0 46.9 06/1710811:12:14 48.4 5.3 32.1 46.0 06/1710811:12:24 48.3 5.3 32.1 44.8 06117/0811:12:34 47.9 5.3 32.1 43.1 06/17/0811:12:44 47.7 5.3 32.2 41.4 06/17/0811:12:54 47.5 5.3 32.2 40.1 06/17/0811:13:04 47.3 5.6 32.1 39.2 06/1710811:13:14 47.1 5.6 32.1 38.6 06/17/0811:13:24 47.0 5.5 32.1 37.9 06117/0811:13:34 46.3 5.6 31.9 36.9 06/1710811:13:44 45.9 5.5 32.0 35.5 06/1710811:13:54 45.6 5.4 32.2 34.0 06/17/0811:14:04 45.4 5.6 32.4 32.4 06/17/0811:14:14 45.1 5.4 32.6 31.3 06/17/0811:14:24 44.9 5.5 32.6 30.7 06117/0811:14:34 45.0 5.3 32.7 30.6 06117/0811:14:44 45.0 5.3 32.8 30.7 0611710811:14:54 44.9 5.3 32.8 30.5 06/1710811:15:04 44.8 5.5 32.9 30.2 06/1710811:15:14 44.8 5.3 33.2 29.7 06/17/0811:15:24 45.0 5.3 33.2 29.3 06/17/0811:15:34 45.4 5.5 33.3 28.9 06/17/0811:1544 45.5 6.3 33.3 28.9 06/17/0811:15:54 45.6 5.3 33.3 29.0 06/1710811:16:04 45.3 5.3 33.3 29.1 06117/0811:16:14 45.0 5.4 33.2 29.0 06/17/0811:16:24 44.6 5.6 32.9 28.8 06/17/0811:16:34 44.7 5.6 32.8 28.5 06/17/0811:16:44 45.0 5.3 32.9 28.3 06/17/0811:16:54 45.5 5.3 32.9 28.2 06/1710811:17:04 46.0 5.3 33.1 28.2 06117/0811:17:14 45.8 5.3 33.2 28.3 06/1710811:17:24 45.5 5.3 33.3 28.4 06/17/0811:17:34 45.0 5.3 33.1 28.5 06/1710811:17:44 44.7 5.3 33.1 28.5 0611710811:17:54 44.4 5.3 31.2 28.6 0611710811:18:04 42.9 5.3 30.2 28.8 06/17/0811:18:14 42.3 5.3 31.3 28.3 06/1 7108 1 1:18:24 42.4 5.3 32.0 27.9 06/17/0811:18:34 42.7 5.3 32.4 27.6 06/17/0811:18:44 43.1 5.3 32.7 27.6 0611710811:18:54 43.9 5.3 32.7 27.7 0611710811:19:04 44.9 5.3 32.8 27.8 06/1710811:19:14 45.7 5.3 32.9 27.9 06117/0811:19:24 46.1 5.3 33.0 28.0 0611710811:19:34 46.3 5.3 33.1 28.1 06117/0811:19:44 46.0 5.3 33.2 28.2 0611710811:19:54 45.4 5.3 33.2 28.3 06117/0811:20:04 44.6 5.3 33.1 28.4 06117/0811:20:14 44.1 5.3 33.2 28.5 06117/0811:20:24 43.7 5.3 33.0 28.6 06/17/0811:20:34 43.5 5.3 33.0 28.6 06117/0811:20:44 43.8 5.3 32.9 28.7 06/17/0811:20:54 44.5 5.3 33.1 28.8 06117/0811:21:04 45.0 5.3 33.2 28.8 06117/0811:21:14

. 44.9 5.3 33.2 28.8 06/17/0811:21:24 44.9 5.5 33.2 28.8



### Page 1 

# 4-36/17108 aun #2

06/17/0811:21:34 45.3 5.4 33.3 28.7 06117/0811:21:44 45.5 5.4 33.3 28.6 06/17/0811:21:54 45.6 5.4 33.3 28.5 06117/0811:22:04 45.6 5.3 33.3 28.5 06117/0811:22:14 45.6 5.5 33.3 28.4 06117/0811:22:24 45.6 5.3 33.3 28.4 06/17/0811:22:34 45.6 5.3 33.3 28.6 06/17/0811:22:44 45.8 5.3 33.4 28.6 06/17/0811:22:54 45.5 5.3 33.4 28.7 06/17/0811:23:04 45.1 5.3 33.4 28.8 06/17/0811:23:14 44.8 5.3 33.3 28.8 06/17/0811:23:24 44.7 5.3 33.3 28.6 06/1710811:23:34 44.8 5.3 33.2 28.6 06/17/0811:23:44 44.8 5.3 33.1 28.6 06/1710811:23:54. 45.0 5.3 33.2 28.5 06/17/0811:24:04 44.9 5.3 33.2 28.5 06/17/0811:24:14 44.8 5.3 33.2 28.4 06117/0811:24:24 44.7 5.2 33.3 28.3 06/17/0811:24:34 44.8 5.3 33.3 28.3 06/17/0811:24:44 45.0 5.3 33.3 28.2 06/17/0611:24:54 44.7 5.2 33.1 28.1 06117/0811:25:04 44.6 5.3 33.0 28.1 06/1710811:25:14 44.7 5.3 32.9 27.9 06/17/0811:25:24 45.1 5.3 32.7 27.8 06/ 17/08 11:25:34 45.0 5.3 32.9 27.7 0611 7/08 1 1:25:44 44.8 5.3 33.0 27.5 06/17/0811:25:54 45.2 5.3 32.9 27.4 06/17/0811:26:04 45.3 5.3 32.8 27.1 06/17/0811:26:14 45.2 5.6 32.9 27.0 06/1710811:26:24 45.0 5.6 32.9 26.8 06117/0811:26:34 45.0 5.6 32.8 26.5 06117/0811:26:44 44.8 5.6 32.5 26.5 0611710811:26:54 44.7 5.4 32.4 26.6 06/17/0811:27:04 44.9 5.3 32.3 26.8 06117/0811:27:14 44.8 5.3 32.3 27.0 06/1710811:27:24 44.2 5.3 32.6 27.2 06/1710811:27:34 43.4 5.4 32.9 27.4 06/1710811:27:44 42.7 5.3 33.0 27.6 06/1710811:27:54 42.6 5.3 33.0 27.8 06/1710811:28:04 42.5 5.3 32.9 28.1 06/17/0811:28:14 42.7 5.3 32.9 28.3 06117/0811:28:24 42.7 5.3 33.0 28.6 06/17/0811:28:34 42.5 5.4 33.3 28.8 06117/0811:28:44 42.4 5.3 33.4 28.7 06/1710811:28:54 41.8 5.5 33.4 28.6 06/17/0811:29:04 41.7 5.5 33.3 28.4 06/17/0811:29:14 41.8 5.6 33.3 28.4 06117/0811:29:24 41.9 5.6 33.2 28.4 06117/0811:29:34 42.0 5.4 33.3 28.5 06117/0811:29:44 42.0 5.3 33.3 28.5 0611710811:29:54 42.1 5.3 33.3 28.5 06117/0811:30:04 41.8 5.3 33.1 28.5 06/17/0811:30:14 41.9 5.3 33.0 28.5 06/1710811:30:24 41.6 5.3 32.7 28.5 06117J0811:30:34 41.4 5.3 32.6 28.6 06/1710811:30:44 41.2 5.3 32.5 28.6 0611710811:30:54 41.3 5.3 32.7 28.6 06/17/0811:31:04 41.0 5.3 32.8 28.6 06/17/0811:31:14 40.8 5.3 32.9 28.7 06117/0811:31:24 40.9 5.3 32.9 28.5 06117/0811:31:34 40.9 5.3 33.1 28.4 06117/0811:31:44 40.7 5.3 33.2 28.3 06117/0811:31:54 40.6 5.3 33.5 28.3 06117/0811:32:04 40.6 5.3 33.7 28.3 06117/0811:32:14 40.7 5.3 33.7 28.3 0611710811:32:24 40.9 5.3 33.8 28.4 06/1710811:32:34 41.1 5.3 33.8 28.4 0611710811:32:44 41.3 5.3 33.8 28.4 06/17/0811:32:54 41.5 5.3 33.8 28.4 06/17/0811:33:04 41.8 5.3 33.6 28.4 06/17/0811:33:14 42.2 5.3 33.7 28.5 06117/0811:33:24 42.5 5.3 33.6 28.5 0611710811;33:34 42.8 5.3 33.6 28.5 0611710811:33:44 42.7 5.3 33.7 28.5



### Page 2 

# 446/17/08 Run t12

0611710811:33:54 42.6 5.3 33.7 28.4 0611710811:34:04 42.9 5.3 33.4 28.5 0811 7108 1 1:34:14 43.1 5.3 33.5 28.5 0611710811:34:24 43.4 5.3 33.6 28.5 0611710811:34:34 43.4 5.3 33.5 28.5 06/17/0811:34:44 43.7 5.3 33.4 28.5 06/17/0811:34:54 44.0 5.3 33.3 28.6 06117/0811:35:04 44.1 5.3 33.3 28.6 06/17/0811:35:14 44.6 5.3 33.3 28.6 06/17/0811:35:24 44.9 5.3 33.3 28.7 06117/0811:35:34 45.0 5.3 33.4 28.7 06117/0811:35:44 44.9 5.3 33.4 28.7 06/17/0811:35:54 44.6 5.3 33.4 28.7 06/1710811:36:04 44.6 5.3 33.3 28.7 06/17/0811:36:14 44.3 5.3 33.2 28.7 06/17/0811:36:24 44.1 5.3 33.2 28.7 06/17/0811:36:34 44.0 5.3 33.4 28.8 06/17/0811:36:44 44.0 5.2 33.4 28.8 06/17/0811:36:54 44.0 5.3 33.6 28.8 06/17/0811:37:04 44.1 5.3 33.6 28.9 06/1710811:37:14 44.0 5.3 33.5 28.8 06117/0811:37:24 43.9 5.3 33.4 28.7 06/17/0811:37:34 43.7 5.3 33.3 28.7 06117/0811:37:44 43.5 5.3 33.3 28.8 0611710811:37:54 43.7 5.3 33.2 28.8 06/1710811:38:04 43.8 5.3 32.9 28.8 0611710811:38:14 44.4 5.5 32.6 29.0 06/1710811:38:24 44.6 8.4 32.6 29.3 06/1710811:38:34 44.9 18.5 32.5 30.2 06/17/0811:38:44 45.0 30.4 32.4 33.0 06/17/0811:38:54 44.8 37.3 32.3 40.8 06/17/0811:39:04 44.8 42.5 32.1 57.8 06/17/0811:39:14 44.7 47.5 32.0 63.3 06/17/0811:39:24 44.6 41.6 31.9 59.8 06117/0811:39:34 44.7 33.8 31.9 49.8 06117/0811:39:44 44.7 30.6 31.9 54.6 0611710811:39:54 44.9 25.7 32.0 72.8

Pause

- CO Off Scale 06117/0811:40:04 44.8 21.1 31.9 78.8 06/1710811:40:14 44.7 18.3 31.9 79.8 06117/0811:40:24 44.0 21.7 32.2 83.8 06/17/0811:40:34 43.5 29.5 32.1 99.8 06/1710811:40:44 43.1 37.1 32.2 99.8 06117/0811:40:54 43.0 36.4 32.3 99.8 0611 7108 1 1:41:04 43.0 30.7 32.2 99.8 0611 7108 1 1:41:14 43.0 26.2 32.2 99.8 06/1 7108 1 1:41:24 43.2 25.4 32.1 99.7 0611710811:41:34 43.4 25.0 32.3 99.7 0611710811:41:44 43.7 25.4 32.3 99.7 0611710811:41:54 43.0 23.9 32.2 99.8 06/1710811:42:04 42.7 25.7 32.1 99.8 06/1710811:42:14 42.2 34.0 32.0 99.8 06117/0811:42:24 42.2 38.1 31.8 99.8 0611710811:42:34 42.4 34.5 31.8 99.8 06/17/0811:42:44 42.7 30.1 31.9 99.8 06/17/0811:42:54 43.1 26.9 31.9 99.8 06/17/0811:43:04 43.1 24.9 31.9 99.8 06/17/0811:43:14 43.0 24.2 32.0 99.8 06/17/0811:43:24 42.9 20.4 31.9 99.8 06/17/0811:43:34 42.7 11.9 32.0 99.8 06/17/0811:43:44 42.8 8.7 32.0 99.8 06/1710811:43:54 42.8 7.8 32.2 99.8 06/1710811:44:04 42.5 7.9 32.2 99.8 06/17/0811:44:14 42.0 7.7 32.2 99.8 06/17/0811:44:24 41.6 7.3 32.1 99.7 06/17/0811:44:34 41.2 7.0 32.1 99.8 06/1710811:44:44 41.1 6.9 32.1 95.3 06/17/0811:44:54 41.0 7.0 32.3 85.7 06/17/0811:45:04 41.5 8.1 32.1 79.1 06/17/0811:45:14 40.8 11.9 32.1 74.6 06/17/0811:45:24 40.5 11.3 32.3 71.7 06117/0811:45:34 40.3 10.2 32.0 71.4 06/1710811:45:44 40.0 8.7 31.9 75.1 

# 45
Page 36/17/08 Run #2

06/17/0811:45:54 39.9 6.9 32.0 82.0 06/17/0811:46:04 39.8 6.2 32.2 89.3 06117/0811:46:14 37.3 6.1 24.2 92.2 0611 7/08 1 1:46:24 23.3 6.1 0.5 85.1 06117/0811:46:34 11.0 7.3 1.9 67.9 06/17/0811:46:44 5.2 10.5 0.8 45.3 06/1710811:46:54 2.2 10.7 4.7 24.4 06/17/0811:47:04 9.6 7.8 18.8 13.0 0611710811:47:14 21.6 6.3 27.4 14.4 06/17/0811:47:24 30.4 6.9 29.6 28.1 06117/0811:47:34 34.7 8.8 30.3 46.5

06/1710811:48:57 43.5 6.2 32.2 64.5 06/1710811:49:07 43.4 7.9 32.3 61.1 06/1710811:49:17 43.2 6.4 32.2 59.0 06/17/0811:49:27 43.1 5.4 31.9 57.8 06/17/0811:49:37 43.1 5.3 31.7 58.0 0611710811:49:47 43.4 5.3 31.8 58.3 06/1710811:49:57 42.7 5.1 31.8 55.9
Resume Sampting 06/17/0811:50:07 42.4 5.2 32.1 50.4 06/1710811:50:17 42.3 5.3 32.3 43.6 06/17/0811:50:27 42.6 5.3 32.4 37.8 06/17/0811:50:37 42.9 5.3 32.5 33.8 06/17/0811:50:47 42.7 5.3 32.4 31.5 06117/0811:50:57 42.4 5.3 32.5 30.3 06117/0811:51:07 42.3 5.2 32.7 29.8 06117/0811:51:17 42.0 5.3 32.7 29.4 06117/0811:51:27 41.7 5.3 32.7 29.2 06/17/0811:51:37 41.2 5.3 32.6 29.3 06/1710811:51:47 40.9 5.2 32.7 29.4 06/17/0811:51:57 40.3 5.3 32.4 29.3 06/17/0811:52:07 40.1 5.3 31.9 29.2 06/17/0811:52:17 40.1 5.3 31.6 29.0 06/1710811:52:27 40.1 5.6 31.6 28.9 08/1710811:52:37 39.9 6.1 31.7 29.0 06/1710811:52:47 40.1 6.2 31.9 29.9 08/1710811:52:57 39.9 6.2 31.8 32.3 06/17/0811:53:07 39.9 5.6 31.8 36.6 06/17/0811:53:17 39.6 5.3 32.0 42.2 06/17/0811:53:27 39.6 5.3 32.0 47.6 06/17/0811:53:37 39.5 5.3 32.1 50.4 06117/0811:53:47 39.6 5.3 32.2 49.8 08117/0811:53:57 39.6 5.4 32.3 46.5 06117/0811:54:07 39.3 6.7 32.2 42.4 06117/0811:54:17 39.5 7.7 32.1 39.0 06117/0811:54:27 39.8 6.5 32.1 37.7 06/1710811:54:37 40.1 5.7 32.1 39.6 06/17/0811:54:47 39.9 5.6 32.1 45.1 06/1710811:54:57 39.7 5.7 32.1 51.8 06/17/0811:55:07 39.3 5.6 32.3 55.7 06117/0811:55:17 39.0 5.6 32.5 55.1 06117/0811:55:27 39.0 5.4 32.5 51.0 06117/0811:55:37 39.0 5.3 32.5 46.2 06/17/0811:55:47 39.4 5.3 32.4 42.2 0611710811:55:57 40.1 5.3 32.4 39.7 06/1710811:56:07 40.2 5.3 32.4 38.3 06/17/08 11 - 56:17 40.1 5.3 32.4 37.4 06/1710811:56:27 40.4 5.3 32.4 36.9 0611710811:56:37 40.7 5.3 32.4 36.6 06117/0811:56:47 40.7 5.7 32.3 36.3 06/1710811:56:57 40.6 6.3 32.3 35.9 06/17/0811:57:07 40.3 5.8 32.4 35.5 06117/0811:57:17 40.2 5.3 32.2 36.3 06/17/0811:57:27 40.2 5.3 32.2 38.9 06/17/0811:57:37 40.2 5.3 32.4 42.3 06/1710811:57:47 40.7 5.3 32.5 43.9 06/17/0811:57:57 40.9 5.4 32.5 42.6 06/17/08 11:58:07 41,3 5.3 32.5 39.2 06117/0811:58:17 41.5 5.4 32.4 35.9 06117/0811:58:27 42.0 5.4 32.3 34.1 06/17/0811:58:37 42.5 5.3 32.4 33.4 06/17/0811:58:47 42.9 5.3 32.4 32.9


# 4~ Page 46/17/08 Run #2

0611710811:58:57 42.9 5.2 32.1 31.9 06/17/0811:59:07 42.9 5.4 32.1 30.8 06/17/0811:59:17 43.6 5.7 31.8 29.9 06/17/0811:59:27 44.4 5.7 31.6 29.5 06/17/0811:59:37 45.2 5.7 31.4 29.6 06/17/0811:59:47 45.7 5.6 31.3 30.8 06/17/0811:59:57 45.9 5.5 31.3 32.8 06117/0812:00:07 45.5 5.3 31.5 34.9 06/1710812:00:17 45.4 5.3 31.7 36.2 0611710812:00:27 44.9 5.3 31.9 35.9 06/1710812:00:37 44.4 5.3 31.8 34.5 06/1710812:00:47 44.0 5.3 31.8 32.7 06/1710812:00:57 43.7 5.6 31.7 31.2 06/1710812:01:07 43.6 5.6 31.8 30.2 06/1710812:01:17 43.6 5.6 31.6 29.8 06/1710812:01:27 43.5 5.6 31.6 30.2 06/1710812:01:37 43.2 5.6 31.6 31.3 06/1710812:01:47 42.8 5.4 31.8 32.5 06/1710812:01:57 42.4 5.3 31.9 32.9 06/1710812:02:07 42.2 5.5 32.0 32.4 06/17/0812:02:17 42.1 5.3 32.2 31.4 0611710812:02:27 42.0 5.3 32.2 30.4 0611710812:02:37 41.8 5.3 32.3 29.7 06/17/0812:02:47 42.0 5.3 32.6 29.3 06/17/0812:02:57 41.8 5.3 32.8 29.1 06/1710812:03:07 41.6 5.3 32.9 28.9 06/1710812:03:17 41.4 5.3 32.8 28.8 06/17/0812:03:27 41.0 5.3 33.0 28.8 06/17/0812:03:37 40.6 5.3 32.8 28.8 06/1710812:03:47 39.8 5.3 32.7 28.9 06/17/0812:03:57 39.3 5.3 32.7 28.9 06/17/0812:04:07 38.9 5.3 32.8 28.9 06/1710812:04:17 38.4 5.4 32.8 28.9 06117/0812:04:27 38.3 5.6 32.8 28.8 0611710812:04:37 38.4 5.4 32.7 28.7 0611710812:04:47 38.7 5.3 32.8 28.7 06/1710812:04:57 38.6 5.5 32.9 28.7 06/1710812:05:07 38.9 5.3 33.0 28.6 06/1710812:05:17 39.3 5.3 33.0 28.6 06117/0812:05:27 39.7 5.3 33.0 28.5 06117/0812:05:37 40.3 5.3 33.0 28.5 06/17/0812:05:47 40.0 5.3 33.0 28.5 0611710812:05:57 40.2 5.3 33.0 28.4 06/17/0812:06:07 40.3 5.3 33.0 28.4 06/17/0812:06:17 40.5 5.4 32.9 28.5 06/17/0812:06:27 40.7 5.5 32.9 28.5 06/17/0812:06:37 41.4 5.3 32.9 28.5 06117/0812:06:47 42.0 5.3 32.9 28.5 06/17/0812:06:57 42.0 5.3 33.0 28.5 06/17/0812:07:07 41.8 5.3 33.3 28.5 06/17/0812:07:17 41.8 5.3 33.5 28.5 06/17/0812:07:27 41.6 5.3 33.5 28.4 06117/0812:07:37 41.8 5.4 33.4 28.4 06/1710812:07:47 41.8 5.3 33.5 28.3 06117/0812:07:57 42.0 5.4 33.6 28.4 06117/0812:08:07 42.0 5.4 33.6 28.3 06117/0812:08:17 42.1 5.4 33.5 28.3 06117/0812:08:27 42.4 5.6 33.3 28.3 0611710812:08:37 42.4 5.3 33.2 28.3 06117/0812:08:47 42.3 5.3 33.3 28.4 0611710812:08:57 42.3 5.3 33.3 28.5 06117/0812:09:07 42.5 5.3 33.4 28.6 06117/0812:09:17 42.6 5.3 33.4 28.5 06117/0812:09:27 42.8 5.3 33.4 28.4 06117/0812:09:37 43.1 5.5 33.4 28.4 06117/0812:09:47 43.1 5.5 33.6 28.5 06/17/0812:09:57 43.0 5.4 33.8 28.5 06117/0812:10:07 42.9 5.3 33.8 28.6 06/17/0812:10:17 43.0 5.4 33.6 28.6 06/17/0812:10:27 42.8 5.4 33.6 28.6 06/17/0812:10:37 42.3 5.3 33.6 28.5 06/17/0812:10:47 42.3 5.3 33.6 28.5 06/17/0812:10:57 42.2 5.3 33.8 28.5 06/17/0812:11:07 42.0 5.3 33.8 28.5

Page 5 

# 476/17/08 Run #2

06/17/0812:11:17 41.7 5.3 33.6 28.6 06117/0812:11:27 41.0 5.3 33.7 28.6 06117/0812:11:37 40.9 5.3 33.7 28.5 06/17/0812:11:47 40.3 5.3 33.7 28.6 06117/081211:67 40.1 5.5 33.7 28.6 06117/0812:12:07 40.0 5.5 33.7 28.6 06/1710812:12:17 40.2 5.3 33.8 28.6 06/1710812:12:27 40.3 53 33.8 28.6 06/1710812:12:37 40.4 5.3 33.8 28.6 06/17/0812:12:47 40.9 5.3 33.9 28.5 06/1710812:12:57 41.0 5.4 34.1 28.4 06/1710812:13:07 41.2 5.4 34.1 28.4 06/1710812:13:17 41.5 5.3 34.2 28.3 06/1710812:13:27 41.7 5.3 34.1 28.3 06/17/0812:13:37 42.1 6.3 33.9 28.4 06/1710812:13:47 41.9 5.3 33.7 28.3 06/1710812:13:57 42.1 5.3 33.5 28.3 06/17/0812:14:07 42.3 5.3 33.4 28.3 06/17/0812:14:17 42.2 5.3 33.3 28.3 06117/0812:14:27 41.7 5.3 33.0 28.4 0611710812:14:37 41.3 5.3 32.8 28.4 06117/0812:14:47 41.2 5.3 32.8 28.3 06117/081214:57 40.8 5.3 32.8 28.3 06117/0812:15:07 40.9 5.3 32.9 28.3 S021nterFerence 06117/0812:15:17 41.2 5.3 32.9 28.2 42.4 06117/0812:15:27 40.9 5.3 32.9 28.1 06117/0812:15:37 40.8 5.3 32.9 28.0 06/17/0812:15:47 40.7 5.3 32.9 28.0 06/1710812:15:57 40.4 5.3 33.0 27.9 06/1710812:16:07 40.1 5.3 33.0 27.8 06117/0812:16:17 39.7 5.3 33.0 27.7 06117/0812:16:27 39.4 5.3 33.0 27.6 06117/0812:16:37 39.3 5.4 33.0 27.6 0611710812:16:47 39.3 5.4 33.0 27.6 06117/0812:16:57 39.6 5.4 33.0 27.8 06117/0812:17:07 39.4 5.5 33.0 28.0 06117/0612:17:17 39.2 5.4 33.0 28.1 06/1710812:17:27 39.0 5.4 33.1 28.1 0611710812:17:37 38.5 5.3 33.0 28.1 0611710812:17:47 38.4 5.3 33.1 28.2 0611710812:17:57 38.4 5.4 33.2 28.2 06/1710812:18:07 38.2 5.4 33.1 28.2 0611710812:18:17 38.0 5.5 33.1 28.2 0611710812:18:27 37.9 5.6 33.0 28.3 0611710812:18:37 38.1 5.5 33.1 28.3 0611710812:18:47 38.1 5.4 33.2 28.3 06117/0812:18:57 38.2 5.4 33.3 28.3 06117/0812:19:07 38.0 5.3 33.4 28.4 06117/0812:19:17 37.8 5.5 33.3 28.4 06/17/081219:27 37.7 5.4 33.2 28.4 06117/0812:19:37 37.6 5.5 33.1 28.4 06117/0812:19:47 37.8 5.3 33.0 28.4 0611710812:19:57 37.9 5.5 33.0 28.3
Stop Run #2 42.76 6.12 32.81 32.09

06117/0812:20:07 37.9 5.5 33.1 28.2 06117/0812:20:17 37.9 5.3 33.1 28.2 06/17/0812:20:27 38.0 5.3 33.3 28.2 06/1710812:20:37 38.3 5.3 33.3 28.4 06/1710812:20:47 37.9 3.4 33.4 28.4 06117/0812:20:57 37.4 2.4 30.8 28.5 0611710812:21:07 34.2 2.1 18.0 28.7 06/17/0812:21:17 28.3 2.0 10.6 29.8 0611710812:21:27 21.5 1.8 5.5 32.5 06/1710812:21:37 15.8 1.8 3.1 36.0 06/17108 12:21:47 11.1 1.8 1.8 39.6 06/17/0812:21:57 6.9 1.7 1.3 42.5 06/1710812:22:07 4.2 1.7 1.0 44.4 06/1710812:22:17 2.2 1.5 0.8 45.4 06117/0812:22:27 1.1 1.5 0.6 45.8 06117/0812:22:37 0.3 1.5 0.5 46.1 06117/0812:22:47 0.0 1.5 0.5 46.2 06117/0812:22:57 -0.5 1.5 

### 0.4 46.2 

# 48 Page 66/17108 Run 42

06/17/08 12:23:07 

### -0.8 1.5 

### 0.3 46.3 50.3 ppm CO 06/17/08 12:23:17 

### -1.0 2.5 

### 0.2 46.4 Zero NOx, S02 06/17/0812:23:27 

### -1.2 3.3 

### 0.3 46.3 06117/0812:23:37 -0.4 1.9 5.9 46.3 0611710812:23:47 0.9 1.6 16.2 45.4 06/17/0812:23:57 1.8 1.5 19.4 41.4 06/1710812:24:07 0.9 1.5 20.5 33.5 06/17/0812:24:17 0.2 1.5 21.2 23.9 06/17/0812:24:27 -0.2 1.5 21.8 15.1 06117/0812:24:37 -0.7 1.5 22.2 8.7 06117/0812:24:47 -0.9 1.5 22.4 4.9 06117/0812:24:57 -1.1 1.5 22.5 2.6 06117/0812:25:07 -1.4 1.5 22.5 1.5 06117/0812:25:17 -0.5 1.5 22.5 0.8 08/1710812:25:27 -0.4 1.4 22.5 0.5 08/17/0812:25:37 -0.6 1.2 

### 22.5 0.2 06/17/08 12:25:47 -0.9 1.3 

### 22.5 0.1 25 ppm NOx 06/1710812:25:57 -1.0 1.3 

### 22.5 0.1 06/17/0812:26:07 -0.7 1.2 

### 22.5 0.0 06/17/0812:26:17 -0.3 1.2 22.5 0.0 06/1710812:26:27 -0.3 3.7 22.4 0.0 06117/0812:26:37 -0.2 5.2 22.6 0.0 06117/0812:26:47 2.2 5.3 26.2 0.3 06/17/0812:26:57 10.6 5.0 30.3 2.2 06/17/0812:27:07 19.2 2.4 32.0 7.0 06/17/0812:27:17 27.4 1.9 26.2 13.5 06/17/0812:27:27 35.8 1.7 13.8 18.4 06/1710812:27:37 43.3 1.7 8.6 18.9 06/17/0812:27:47 50.5 1.5 5.3 15.6 06/17/0812:27:57 56.7 1.5 3.2 10.6 06/17l0812:28:07 62.4 1.5 2.3 6.0 06/1710812:28:17 66.4 1.5 2.0 3.2 0611710812:28:27 68.9 1.5 1.8 1.6 06117/0812:28:37 73.2 1.5 1.7 0.8 06117/0812:28:47 78.9 1.4 1.6 0.4 06/17/0812:28:57 81.3 1.3 1.6 0.3 06/1710812:29:07 86.8 1.2 1.5 

### 0.2 06/17/0812:29:17 87.2 1.2 1.5 

### 0.2 06117/0812:29:27 88.4 1.2 1.5 0,2 06117/0812:29:37 89.3 1.2 1.5 0.2 06117/08 12:29:47 

### 91.0 1.2 1.5 0,1 06117/08 12:29:57 

### 92.0 1.2 1.5 0.1 101 ppm S02 06117/0812:30:07 

### 91.9 2.1 1.5 0.1 06/17/0812:30:17 

### 91.8 2.7 1.5 0.1 06117/0812:30:27 90.8 0.7 5.9 0.2 06/17/0812:30:37 65.3 

### 0.6 10.2 1.1 06/17/08 12:30:47 52.2 

### 0.6 4.6 3.0 

### Zero Air 06117/0812:30:57 38.5 

### 0.6 1.9 4.6 06/17/0812:31:07 28.5 

### 0.6 0.9 4.8 06117/0812:31:17 20.7 0.8 0.5 3.7 06117/0812:31:27 16.0 7.8 0.3 2.2 0611710812:31:37 12.8 20.7 2.4 1.2 06/1 7108 1 2:31:47 12.5 

### 21.0 9.4 1.3 06117J08 12:31:57 11.8 

### 21.0 5.3 2.6 20.8 ppm CH4 06/17/0812:32:07 9.7 

### 21.0 2.4 4.2 06l17/0812:32:17 7.4 

### 21.0 1.2 4.7 06117/0812:32:27 5.3 21.0 0.7 4.0 06117/0812:32:37 3.7 16.6 0.3 2.8 06117/0812:32:47 2.8 5.2 0.1 1.6 06117/0812:32:57 3.5 5.1 4.7 1.0

Page 7 

# 496/17108 Run #3

Date/Time S02 VOC NOx CO mm/ddlyy hh:mm:ss ppm ppm ppm ppm 06117/0812:54:57 48.5 5.2 33.6 26.6

Start Run #3 06/1710812:55:07 29.9 1.7 30.1 23.0 06/1710812:55:17 48.6 5.3 33.6 26.6 06/17/0812:55:27 48.2 5.3 33.7 26.7 06/17/0812:55:37 47.8 5.3 33.8 26.9 06/1710812:55:47 47.6 5.3 33.7 27.1 06/1710612:55:57 47.4 5.2 33.7 27.3 06/17/0812:56:07 47.1 5.4 33.7 27.5 06/1 7108 1 2:56:17 46.8 5.5 33.6 27.8 06117/0812:56:27 46.9 5.4 33.7 28.0 06/17/0812:56:37 46.8 5.4 33.9 28.2 06/17/0812:56:47 46.6 5.3 34.2 28.6 06117/0812:56:57 46.4 6.5 34.3 28.9 06117/0812:57:07 46.3 5.3 34.1 29.1 06117/0812:57:17 46.2 5.3 34.1 29.2 06/17/0812:57:27 46.2 5.3 34.3 29.2 06/17/0812:57:37 46.2 5.3 34.1 29.4 0611710812:57:47 46.0 5,4 34.0 29.4 06/17/0812:57:57 46.1 5.3 34.1 29.4 06/1710812:58:07 46.3 5.3 33.9 29.3 0611710812:58:17 46.6 5.3 33.7 29.2 06117/0812:58:27 47.1 5.3 33.8 29.2 06/1710812:58:37 47.4 5.3 33.9 29.2 06/1710812:58:47 47.5 5.3 33.9 29.1 06/1710812:58:57 47.8 5.3 34.0 29.1 06/17/0812:59:07 47.9 5.3 34.2 29.1 06/17/0812:59:17 48.1 5.3 34.3 29.1 06117/0812:59:27 47.8 5.3 34.3 29.1 06117/0812:59:37 47.4 6.3 34.6 29.2 06117/0812:59:47 46.5 5.3 34.6 29.2 06/17/0812:59:57 46.2 5.3 34.6 29.2 06/17/0813:00:07 46.2 5.3 34.6 29.1 06117/0813:00:17 46.3 5.3 34.6 28.9 0611710813:00:27 46.3 5.3 34.5 28.7 0611710813:00:37 46.8 5.3 34.6 28.6 06/17/08.13:00:47 47.0 5.3 34.7 28.3 0611710813:00:57 47.2 5.3 34.8 28.1 06117/0813:01:07 47.2 5.2 34.8 27.9 06J17/0813:01:17 47.4 5.3 34.9 27.7 06/17/0813:01:27 47.1 5.3 34.9 27.6 06/17/0813:01:37 46.7 5.3 34.9 27.6 06117/0813:01:47 46.8 5.3 34.9 27.7 0611710813:01:57 47.0 5.3 34.7 27.8 06117/0813:02:07 47.1 5.3 34.6 27.9 06/17/0813:02:17 47.0 5.3 34.4 27.8 06/17/0813:02:27 47.3 5.3 34.2 27.7 0611710813:02:37 47.9 5.3 34.1 27.4 06117/0813:02:47 48.2 5.3 33.8 27.3 06117/0813:02:57 48.5 5.2 33.5 27.3 06117/0813:03:07 48.7 5.3 33.3 27.3 06/17/0813:03:17 49.1 5.3 33.2 27.4 06/17/0813:03:27 49.4 5.3 32.8 27.4 06/17/0813:03:37 49.7 5.2 32.7 27.5 06/1710813:03:47 49.9 5.3 32.6 27.9 06117/0813:03:57 50.2 5.2 32.8 28.1 06/17/0813:04:07 50.1 5.3 33.1 28.5 06117/0813:04:17 80.1 5.3 33.4 28.7 06/17/0813:04:27 50.0 5.3 33.6 26.8 06117/0813:04:37 50.0 5.3 33.9 28.8 06117/0813:04:47 50.1 5.3 34.1 28.7 06117/0813:04:57 49.8 5.3 34.4 28.6 06/17/0813:05:07 49.7 5.3 34.4 28.4 0611710813:05:17 49.7 5.3 34.2 28.3 06/17/0813:05:27 49.8 5.4 34.1 28.2 06/17/0813:05:37 49.9 5.3 34.1 28.2 06117/0813:05:47 49.8 5.3 34.1 28.1 06/1710813:05:57 50.0 5.3 34.0 28.1 06/17/0813:06:07 50.2 5.3 33.9 28.1 06117/0813:06:17 50.3 5.3 33.8 28.1 0611710813:06:27 50.2 5.3 33.5 28.2



### Page 1 

# 506/17/08 Run #l3

0611710813:06:37 50.4 5.3 33.3 28.4 08/1710813:08:47 50.1 5.3 33.1 28.6 06117/0813:06:57 49.7 5.3 33.0 28.7 06/17/0813:07:07 49.8 5.3 33.0 28.8 06117/0813:07:17 49.4 5.3 33.1 28.9 06/17/0813:07:27 49.1 5.3 33.1 29.0 06117/0813:07:37 48.7 5.3 33.2 29.1 06/17/0813:07:47 48.8 5.3 33.0 29.1 06/1710813:07:57 48.8 5.3 33.0 29.0 06/17/0813:08:07 49.1 5.3 33.0 29.0 06/1710813:08:17 49.3 5.3 32.9 29.0 06/17/0813:08:27 49.3 5.3 33.0 28.9 06/17/0813:08:37 49.1 5.3 33.1 28.8 06/17/0813:08:47 49.0 5.3 33.3 28.7 06/17/0813:08:57 49.1 5.3 33.3 28.8 06/17/0813:09:07 49.2 5.2 33.5 28.8 06117/0813:09:17 49.2 5.2 33.6 28.8 06/17/0813:09:27 49.1 5.3 33.8 28.8 06/17/0813:09:37 49.1 5.3 33.9 28.8 06/17/0813:09:47 48.8 5.3 34.0 28.8 06117/0813:09:57 48.9 5.3 34.1 28.8 06/17/0813:10:07 49.3 5.3 34.3 28.7 06/1710813:10:17 49.4 5.3 34.3 28.7 06117/0813:10:27 49.7 5.3 34.1 28.6 0811 7108 1 3:10:37 50.0 5.3 34.1 28.7 08/1710813:10:47 49.9 5.3 34.1 28.7 06117/0813:10:57 49,9 5.3 34.0 28.6 06/17/0813:11:07 50.0 5.3 34.0 28.6 06117/0813:11:17 50.2 5.3 33.9 28.6 06117/0813:11:27 50.2 5.3 33.9 28.6 06/17/0813:11:37 50.2 5.3 34.0 28.7 06/1710813:11:47 50.2 5.3 34.0 28.8 06/1710813:11:57 50.1 5.4 34.1 28.8 0611710813:12:07 49.9 5.6 34.3 28.8 0611710813:12:17 49.7 5.5 34.5 28.7 0611710813:12:27 49.8 5.3 34.5 28.6 06/1710813:12:37 50,4 5.3 34.5 28.6 06/17/0813:12:47 51.0 5.3 34.3 28.5 06/1710813:12:57 51.2 5.3 34.1 28.4 06117/0813:13:07 51.1 5.3 33.9 28.3 0611710813:13:17 50.8 5.3 33.7 28.2 0611710813:13:27 50.3 5.3 33.4 28.0 06/17/0813:13:37 50.0 5.3 33.5 27.8 06/17/0813:13:47 50.0 5.3 33.3 27.4 06/17/081313:57 50.4 5.3 33.0 27.2 06/17/0813:14:07 50.9 5.3 32.8 27.2 06117/0813:14:17 51.8 5.3 32.7 27.2 0611710813:14:27 52.2 5.9 32.6 27.5 0611710813:14:37 52.6 9.2 32.8 27.8 06117/0813:14:47 52.4 12.7 32.7 28.6 0611710813:14:57 52.2 14.9 32.5 32.0 0611710813:15:07 51.9 18.3 32.3 40.5 06/1710813:15:17 51.7 16.2 32.1 56.0 06/1710813:15:27 51.3 12.6 31.7 77.9 06/1710813:15:37 51.3 11.3 31.7 99.8 06/17/0813:15:47 51.5 15.5 31.5 99.8 06/17/0813:15:57 51.6 19.6 31.4 99.8 06/17/0813:16:07 51.7 16.3 31.4 99.8 06/17/0813:16:17 51.6 12.9 31.3 99.8 06/17/0813:16:27 51.6 11.6 31.3 99,7 06/17/0813:16:37 51.8 10.4 31.4 99.8 06/17/0813:16:47 52.0 10.2 31.6 99.9 06/17/0813:16:57 51.9 15.8 31.8 99.9 06/17/0813:17:07 51.7 23.1 31.9 99,9 06/17/0813:17:17 51.1 26.2 31.9 99.9 06/17/0813:17:27 50.6 21.5 31.9 99.9 06/17/0813:17:37 50.2 15.0 31.9 99.9 06/17/0813:17:47 49.7 11.5 32.1 99.7 06/1710813:17:57 49.6 10.1 32.3 99.7 06/17/0813:18:07 49,3 12.6 32.6 99.8 06/17/0813:18:17 48.9 16.2 32.7 99.7 06/17/0813:18:27 48.3 13.1 32.7 99.8 06/17/0813:18:37 47.7 7.7 32.6 99.8 06/17/0813:18:47 47.7 5.9 32.7 99.8



### Page 2 

# 516/17/08 Run #3

06/1710813:18:57 47,4 5.4 32.7 99.8 0611710813:19:07 46.9 5.2 32.9 99.6 06/1710813:19:17 46.5 5.3 33.0 96.6 06/17/0813:19:27 46.1 6.2 33.2 78.5 06/17/0813:19:37 45.8 5.9 33.3 61.3 06117/0813:19:47 45.7 5.2 33.2 49.4 06117/0813:19:57 45.6 5.1 33.3 43.9 06/17/0813:20:07 45.5 4.8 33.4 43.3 06/17/0813:20:17 45.5 4.8 33.7 43.4 06/1710813:20:27 45.4 4.9 33.9 41.4 06/17/0813:20:37 45.2 5.0 33.7 37.1 06/17/0813:20:47 44.8 5.1 33.6 32.3 06/1710813:20:57 44.7 4.9 33.5 28.1 06/1710813:21:07 44.8 5.1 33.4 25.5 0611710813:21:17 44.7 5.1 33.6 23.8 06/1710813:21:27 44.5 5.1 33.9 22.9 06/1710813:21:37 44.4 5.0 34.2 22.5 06/17/0813:21:47 44.5 5.0 34.3 22.2 06/17/0813:21:57 44.4 5.0 34.4 22.2 06/17/0813:22:07 44.1 5.0 34.4 22.4 06/17/0813:22:17 43.9 5.0 34.4 22.8 06/17/0813:22:27 43.7 5.0 34.5 23.2 06/17/0813:22:37 43.7 5.0 34.6 23.8 06/1710813:22:47 43.8 5.0 34.6 24.3 06/1710813:22:57 43.9 5.0 34.5 24.5 0611710813:23:07 44.0 5.0 34.5 24.6 06117/0813:23:17 43.9 5.0 34.5 24.8 06/1710813:23:27 43.7 5.1 34.3 24.9 06/17/0813:23:37 43.4 5.0 34.2 25.1 06/17/0813:23:47 43.0 5.0 34.2 25.3 06/17/0813:23:57 42.6 5.0 34.2 25.5 06/17/0813:24:07 42.3 5.0 34.1 25.7 06117/0813:24:17 42.0 5.0 34.0 25.8 06117/0813:24:27 41.7 4.9 34.1 25.9 06117/0813:24:37 41.2 4.8 33.9 26.0 06117/0813:24:47 40.4 4.8 33.7 26.1 06117/0813:24:57 39.7 4.7 33.5 26.2 06117/0813:25:07 39.0 4.9 33.4 26.2 06117/0813:25:17 38.3 5.0 33.3 26.3 06117/0813:25:27 37.9 4.9 33.2 26.3 06117/0813:25:37 37.6 4.8 33.2 26.3 0611710813:25:47 37.3 4.8 33.2 26.3 06117/0813:25:57 36.8 4.8 33.2 26.2 06117/0813:26:07 36.5 4.9 33.2 26.1 06/17/0813:26:17 36.4 4.9 33.2 26.0 06117/0813:26:27 36.2 5.0 33.2 25.9 06/17/0813:26:37 36.6 4.8 33.3 25.9 06/17/0813:26:47 35.3 5.0 33.4 25.9 06/17/0813:26:57 35.3 6.0 33.3 26.0 06/1710813:27:07 35.4 4.8 33.3 26.1 06/17/0813:27:17 35.5 4.8 33.3 26.1 06/1710813:27:27 35.4 4.9 33.4 26.2 06/1710813:27:37 35.6 4.9 33.5 26.2 06/1710813:27:47 35.7 4.9 33.4 26.4 06/1710813:27:57 35.8 4.9 33.4 26.6 06117/0813:28:07 35.8 4.9 33.4 26.8 06117/0813:28:17 36.1 5.0 33.3 27.1 06/17/0813:28:27 35.8 5.1 33.3 27.2 06117/0813:28:37 35.8 5.0 33.4 27.3 06/17/0813:28:47 36.0 5.0 33.2 27.3 06117/0813:28:57 36,2 5.0 33.1 27.3 06117/0813:29:07 36.7 6.0 32.9 27.4 06/17/0813:29:17 37.2 4.8 32.9 27.4 06117/0813:29:27 38.0 5.0 33.0 27.5 06117/0813:29:37 38.6 5.1 33.0 27.5 06/1710813:29:47 38.6 5.1 33.0 27.5 06/17/0813:29:57 38.6 5.0 32.9 27.5 06/17/0813:30:07 38.8 5.0 32.9 27.5 06117/0813:30:17 39.4 5.0 32.9 27.5 06/17/0813:30:27 40.0 5.0 32.8 27.6 06117/0813:30:37 40.4 5.0 32.9 27.8 06/1710813:30:47 40.9 5.0 32.9 27.9 06/17/0813:30:57 41.1 5.0 32.8 27.9 06/17/0813:31:07 41.5 5.0 32.7 27.9

Page 3 

# 5~6/17108 Run #3

06/17/0813:31:17 41.9 5.0 32.4 27.9 06/1710813:31:27 42.3 5.0 32.2 27.9 06/17/0813:31:37 42.3 5.0 32.1 27.9 06117/0813:31:47 42.5 5.0 31.7 27.9 06117/0813:31:57 42.9 5.0 31.5 27.9 06/1710813:32:07 43.0 5.0 31.5 28.0 06117/0813:32:17 43.0 5.1 31.6 28.1 06117/0813:32:27 42.9 5.1 31.7 28.2 06/17/0813:32:37 43.2 5.5 31.7 28.4 06/1710813:32:47 43.2 7.8 31.5 28.5 06/1710813:32:57 43.4 7.1 31.1 28.9 06/17/0813:33:07 44.0 6.0 30.7 31.0 06/1710813:33:17 44.7 9.6 30.4 36.7 06/1710813:33:27 45.2 16.6 30.0 45.6 06/1710813:33:37 45.7 20.1 30.0 54.8 08/17/0813:33:47 46.1 22.6 30.0 63.6 06/17/0813:33:57 46.5 23.7 30.2. 75.3 08117/0813:34:07 46.7 23.3 30.3 91.2 06117/0813:34:17 47.1 19.3 30.4 99.8 06/1710813:34:27 47.0 14.7 30.5 99.8 06/1710813:34:37 46.9 10.5 30.7 99.8 0611710813:34:47 46.7 10.8 31.0 99.9 06117/0813:34:57 46.5 13.7 31.2 99.9 06117/0813:35:07 46.2 15.2 31.3 99.9 06117/0813:35:17 45.9 14.2 31.3 99.9 06/17/0813:35:27 45.7 11.7 31.3 99.9 06/1710813:35:37 45.7 9.0 31.3 99.9 06/1710813:35:47 45.7 7.4 31.3 99.8 06/1710813:35:57 45.9 6.1 31.2 99.8 06/1710813:36:07 45.8 5.7 31.5 99.8 06117/0813:36:17 46.1 5.6 31.6 97.3 06117/0813:36:27 46.2 5.3 31.7 84.7 06/17/0813:36:37 46.0 5.4 31.9 70.9 06/17/0813:36:47 45.6 5.4 31.9 59.0 06117/0813:36:57 45.6 5.3 31.8 50.1 06/17/0813:37:07 45.8 5.3 31.8 44.0 06117/0813:37:17 46.0 5.3 32.0 39.5 06/1710813:37:27 45.9 5.2 32.2 36.2 06/1710813:37:37 45.9 5:1 32.1 33.9 06/1710813:37:47 45.9 5.2 32.1 32.5 06/17/0813:37:57 45.6 5.2 32.1 32.0 06117/0813:38:07 45.6 5.1 32.1 31.9 06/17/0813:38:17 45.5 5.0 32.1 31.4 06/1710813:38:27 45.5 5.0 32.1 30.6 06/17/0813:38:37 45.5 5.0 32.1 29.6 06/1710813:38:47 45.6 5.1 32.0 28.6 0611710813:38:57 45.4 5.1 32.0 27.9 06/1710813:39:07 45.2 5.2 32.1 27.5 06/17/0813:39:17 45.4 5.0 32.1 27.1 06/17/0813:39:27 45.5 5.1 31.8 26.9 06/17/0813:39:37 45.6 5.1 31.6 26.8 06/1710813:39:47 45.8 5.1 31.6 26.8 06/1710813:39:57 45.7 6.1 31.7 26.7 06/1710813:40:07 45.4 5.0 31.9 26,5 06/1710813:40:17 45.3 5.0 32.0 26,3 0611710813:40:27 45.1 5.0 32.2 26.0 06/17/0813:40:37 44.8 5.0 32.3 25.8 06/17/0813:40:47 44.7 5.1 32.3 25.7 06/17/0813:40:57 44.7 5.0 32.3 25.6 06/17/0813:41:07 45.0 5.1 32.3 25.5 06/1710813:41:17 45.0 5.0 32.3 25.4 06117/0813:41:27 44.8 5.0 32.4 25.3 06117/0813:41:37 44.8 5.1 32.6 25.2 06/17/0813:41:47 44.7 5.1 32.7 25.2 06/17/0813:41:57 44.4 5.0 32.8 25.3 06/17/0813:42:07 44.0 5.0 32.7 25.4 06/1710813:42:17 43.7 5.0 32.7 25.4 06/1710813:42:27 43.7 5.0 32.7 25.5 06/1710813:42:37 43.8 5.0 32.6 25.5 0611710813:42:47 44.4 5.0 32.7 25.5 06/1710813:42:57 44.1 5.0 32.8 25.4 06117/0813:43:07 43.8 5.0 32.8 25.4 06117/0813:43:17 43.5 5.0 32.8 25.4 06/17/0813:43:27 43.1 5.0 32.9 25.4

Page 4 

# 536/17/08 Run #3

06/17/0813:43:37 42.8 5.0 32.8 25.4 06/17/0813:43:47 42.7 5.1 32.6 25.4 06/1710813:43:57 42.5 5.0 32.6 25.6 06/17/0813:44:07 42.4 5.0 32.5 25.7 06/17/0813:44:17 42.8 5.0 32.6 25.9 06/1710813:44:27 43.1 5.0 32.6 26.2 06/17/0813:44:37 43.2 5.1 32.6 26.4 06117/0813:44:47 43.1 5.1 32.8 26.7 08/17/0813:44:57 43.0 5.1 32.9 26.9 06117/0813:45:07 42.9 5.1 32.7 27.2 06/17/0613:45:17 42.8 5.1 32.3 27.4 06/17/0613:45:27 43.2 5.1 32.2 27.6 06/1710813:45:37 43.6 5.1 32.1 27.8 06/1710813:45:47 43.6 5.1 32.2 28.0 0611710813:45:57 43.6 5.1 32.6 28.1 06/17/0813:46:07 43.5 5.2 32.7 28.4 06/17/0813:46:17 43.2 5.3 32.7 28.6 06/1710813:46:27 42.9 5.2 32.7 28.7 06117/0813:46:37 42.7 5.3 32.6 28.8 06/17/0813:46:47 43.0 5.2 32.8 28.9 06/17/0813:46:57 42.8 5.2 32.9 29.0 06/17/0813:47:07 42.8 5.3 33.1 29.1 06/17/0813:47:17 42.7 5.2 33.1 29.2 06117/0813:47:27 42.8 5.2 33.0 29.2 06/17/0813:47:37 42.6 6.2 32.8 29.2 06/17/0813:47:47 41.9 5.3 32.9 29.3 06/17/0813:47:57 41.7 5.2 32.9 29.3 06117/0813:48:07 41.4 5.3 32.8 29.4 06/17/0813:48:17 41.3 5.3 32.6 29.4 06117/0813:48:27 41.3 5.3 32.4 29.4 06/17/0813:48:37 41.4 5.3 32.2 29.5 06117/0813:48:47 41.4 5.2 32.2 29.5 06117/0813:48:57 41.4 5.3 32.5 29.6 06/17/0813:49:07 41.7 5.3 32.6 29.6 08/17/0813:49:17 42.3 5.3 32.7 29.6 06/1710813:49:27 42.8 5.3 32.7 29.6 06/17/0813:49:37 43.2 5.1 32.7 29.6 06/17/0813:49:47 43.7 6.1 32.8 29.7 06117/0813:49:57 43.9 5.2 32.8 29.8 06117/0813:50:07 44.0 5.0 33.1 29.8 06/17/0813:50:17 43.7 5.1 33.3 29.7 06/17/0813:50:27 43.8 5.1 33.3 29.6 06117/0813:50:37 43.6 5.2 33.3 29.5 06/17/0813:50:47 43.5 5.3 33.4 29.4 06/17/0813:50:57 43.4 5.3 33.4 29.4 06/17/0813:51:07 43.5 5.3 33.4 29.3 06/1710813:51:17 43.8 5.2 33.5 29.3 06/17/0813:51:27 44.2 5.3 33.5 29.3 06/1710813:51:37 44.6 5.2 33.5 29.3 06/1710813:51:47 45.0 5.2 33.6 29.2 06/17/0813:51:57 45.0 5.3 33.6 29.2 06/17/0813:52:07 45.0 5.3 33.4 29.2 06117/0813:52:17 45.1 5.3 33.3 29.1 06/17/0813:52:27 45.2 5.3 33.2 29.1 06/17/0813:52:37 45.4 5.3 33.1 29.1 06/17/0813:52:47 45.4 5.3 33.1 29.1 06117/0813:52:57 45.6 5.3 33.1 29.1 06/17/0813:53:07 45.8 5.3 33.0 29.2 06/17/0813:53:17 46.1 5.3 32.8 29.2 06117/0813:53:27 46.8 5.3 32.6 29.2 06117/0813:53:37 47.5 5.3 32.5 29.2 06/17/0613:53:47 48.1 5.3 32.5 29.2 06/1710813:53:57 48.6 5.2 32.6 29.1 06/1710813:54:07 49.1 5.1 32.5 29.1 06/1710813:54:17 49.4 5.3 32.4 28.9 06/17/0813:54:27 49.6 5.1 32.5 28.7 06/17/0813:54:37 49.7 5.1 32.5 28.6 06/17108 13:54:47 50.1 5.3 32.3 285 06/17/0813:54:57 50.3 5.2 32.3 28.4 06/17/0813:55:07 50.3 5.3 32.3 28.3 S021nterference 06/17/0813:55:17 50.4 5.3 32.4 28.2 45.5 06117/0813:55:27 50.4 5.3 32.4 28.1 06/17/0813:55:37 50.1 5.3 32.3 28.1 06/17/0813:55:47 49.8 5.3 32.2 28.1

Page 5 

# 546/17/08 Run #3

06/1710813:55:57 49.9 5.3 32.0 28.1 0611710813:56:07 49.9 5.3 31.9 28.3 06/1710813:56:17 49.6 5.3 32.1 28.5 06/17/0813:56:27 49.3 5.4 32.3 28.7 0611710813:56:37 48.8 5.3 32.2 28.8 0611710813:56:47 45.6 4.8 31.8 28.6 06/17/0813:56:57 48.6 5.3 32.0 29.2
Stop Run #3 45.65 6.25 32.99 38.54

06/1710813:57:07 48.4 4.9 31.9 29.5 06/17/0813:57:17 48.3 3.3 31.8 29.7 06/17/0813:57:27 47.5 3.3 26.4 29.8 08117/0813:57:37 44.0 4.1 13.5 29.2 06117/0813:57:47 27.5 3.5 6.9 26.2 06/17/0813:57:57 20.9 2.1 4.1 20.8 06/1710813:58:07 16.7 1.8 3.1 15.4 06117/0813:58:17 13.0 1.7 2.5 14.2 06117/0813:58:27 9.6 1.7 1.6 18.6 06/17/0813:58:37 6.8 1.8 1.1 26.4 06/1710813:58:47 5.0 1.6 0.9 34.2 06117/0813:58:57 3.4 1.6 0.7 39.8 06/1710813:59:07 2.1 1.5 0.6 43.1 06/17/0813:59:17 1.2 1.5 0.6 44.7 06/17/0813:59:27 0.7 1.5 0.5 45.6 06/17/0813:59:37 0.5 1.5 0.4 45.9 06/17/0813:59:47 0.3 1.5 0.4 46.2 06/17/0813:59:57 0.2 1.5 0.3 46.3 0611710814:00:07 -0.1 1.5 0.3 46.4 06/17/0814:00:17 

### -0.1 1.5 

### 0.3 46.5 06/17/0814:00:27 

### -0.3 1.5 

### 0.2 46.5 06117/0814:00:37 

### -0.4 1.5 

### 0.2 46.4 06117/0814:00:47 

### -0.4 1.8 

### 0.2 46.4 0611710814:00:57 -0.7 1.5 0.2 46.4 06117/0814:01:07 -0.8 1.5 3.6 45.6 06/17/0814:01:17 -0.8 1.5 13.2 42.4 06117/0814:01:27 -0.4 1.4 18.2 35.1 06/1710814:01:37 -0.3 1.5 20.1 25.1 06/17/0814:01:47 -0.6 1.5 20.8 15.7 06117/0814:01:57 -0.6 1.4 21.0 8.8 06117/0814:02:07 -0.4 1.5 21.2 4.8 06117/0814:02:17 -0.5 1.5 21.5 2.9 06/17/0814:02:27 -0.6 1.5 21.6 2.0 06/17/0814:02:37 -0.6 1.3 21.7 1.5 06/17/0814:02:47 -0.4 1.3 21.9 1.2 0611710814:02:57 -0.4 1.4 21.9 0.9 06117/0814:03:07 -0.4 1.4 22.0 0.7 06/17/0814:03:17 -0.6 1.5 22.0 0.5 06117/0814:03:27 -0.6 1.5 

### 22.0 0.4 06/17/0814:03:37 -0.5 1.4 

### 22.1 0.3 06/17/0814:03:47 -0.3 1.4 

### 22.1 0.2 06117/0814:03:57 -0.2 2.6 

### 22.1 0.1 06/17/0814:04:07 -0.2 2.7 18.6 0.1 06/1710814:04:17 -0.3 3.0 8.7 0.1 06/1710814:04:27 -0.4 2.1 3.5 0.1 06117/0814:04:37 -0.3 1.6 1.8 0.1 0611710814:04:47 3.7 1.5 2.1 0.1 06/1710814:04:57 16.2 1.5 2.1 0.1 06117/0814:05:07 30.3 1.5 2.0 0.1 0611710814:05:17 42.3 1.5 2.0 0.1 06117/0814:05:27 51.9 1.4 1.8 0.1 06/17/0814:05:37 59.6 1.4 1.7 0.1 06/1710814:05:47 66.1 1.4 1.6 0.1 06/1710814:05:57 70.3 1.3 1.5 0.1 06/17/0814:06:07 72.8 1.4 1.5 0.1 06/17/0814:06:17 75.4 1.4 1.5 0.1 06/17/0814:06:27 77.2 1.3 1.4 0.1 06/17/0814:06:37 78.8 1.2 1.4 0.1 08/1710814:06:47 80.1 1.2 1.4 0.1 06/17/0814:06:57 81.2 1.4 1.5 0.1 06/17/0814:07:07 82.3 1.3 1.4 0.0 06117/0814:07:17 82.8 1.2 1.4 0.1 06117/0814:07:27 83.4 1.2 1.4 0.1 50.3 ppm CO Zero NOx, S02

25 ppm NOx Zero CO



## Page 6 

# 556117/08 Run #3

0611710814:07:37 84.2 1.2 1.4 0.0 0611710814:07:47 84.3 1.2 1.4 0.0 0611710814:07:57 84.6 1.2 1.4 0.0 06/17f0814:08:07 84.8 1.3 1.4 0.1 06/1710814:08:17 85.1 1.4 1.4 0.1 0611710814:08:27 85.5 1.3 1.4 0.1 0611710814:08:37 85.6 1.2 1.4 0.0 06/17/0814:08:47 86.1 1.2 1.3 0.0 06117/0814:08:57 87.3 1.3 1.3 0.0 0611710814:09:07 87.9 1.2 1.3 0.1 06/17/0814:09:17 87.9 1.2 1.3 0.1 06/1710814:09:27 88.3 1.2 1.4 0.1 06/1710814:09:37 88.4 1.2 1.3 0.0 06/1710814:09:47 88.8 1.2 1.3 0.0 06/1710814:09:57 89.4 1.2 1.3 0.0 0611710814:10:07 89.4 1.2 1.3 0.0 06/17108 14:10:17 89.7 1.2 1.4 0.0 0611710814:10:27 90.2 1.2 1.3 0.0 06117/0814:10:37 90.3 1.2 1.3 0.0 06117/0814:10:47 

### 90.4 1.2 1.3 0.0 06117/0814:10:57 

### 90.5 1.2 1.3 0.0 101 ppm S02 0611710814:11:07 

### 90.5 1.2 1.3 0.1 06/17/06 14:11:17 

### 90.8 1.9 1.3 0.0 06/17/0814:11:27 90.3 2.7 1.2 0.0 06/17/0814:11:37 85.1 2.5 0.7 0.1 06/17/0814:11:47 70.7 0.6 0.1 0.1 06/1710814:11:57 56.6 

### 0.6 0.0 0.1 06/17108 14:12:07 43.7 

### 0.6 0.0 0.1 Zero Air 0611710814:12:17 34.2 

### 0.5 0.0 0.1 0611710814:12:27 26.6 

### 0.5 0.0 0.1 0611710814:12:37 20.7 0.9 0.0 0.1 0611710814:12:47 17.3 7.6 0.0 0.0 0611710814:12:57 14.5 20.9 0.0 0.0 0611710814:13:07 11.6 

### 21.0 0.0 0.0 06117/0814:13:17 9.5 

### 21.0 0.0 0.0 20..2 ppm CH4 06117/0814:13:27 7.7 

### 20.9 0.0 0.0 06117/0814:13:37 6.3 

### 20.9 0.0 0.1 06/17/0814:13:47 5.1 20.9 0.0 0.1

Page 7 

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# 59

## SK25-800.2437-2007 Customer-Armstrong Environmental Sales Order-0030621



## APEX INSTRUMENTS DRY GAS METER CALIBRATION

Dry Gas Meter Information Gas Meter Model SK25 Gas Meter Serial Number 18002437

Calibration Conditions Wet Test Meter ldenification W-NK-0.5A Calibration Technician ISH ICalibration Date 1 

## 17

- 

## Ma -07 Wet Test Meter Calibratioti Factor 11.0000 1 Barometric Pressure I (Pb) 753.7 1 mm Hg

Calibration Data Results 

## Run Time D Gas Meter Wet Test Meter Standardized Volumes Dry Gas Meter

Ela sed Gas



## Pressure Gas



## Volume Gas



## Tem erature Gas



## Volume Gas



## Tem erature Dry Gas



## Meter Wet Test



## Meter Calibration Factor Corrected 

## Flowrate Value Variation

0 (Pm) (" m) (tm) (Vw) (hn) (" s) \" std (') 0 (Q m ) 

## min mm H 2 0 liters °C liters °C std liters std liters slm 

## Run 1- Initial 0.00 69.00 81.90 24.0 314.9142 24.0 Final 5.00 69.00 92.50 25.0 325.0350 25.0 Total/Av 5.00 69.00 10.60 24.5 10.1208 24.5 10.430 9.892 0.948 -0.010 1.98 Run 2- Initial 0.00 27_00 92.50 25.0 325.0350 25.5 Final 9.00 27.00 101.90 25.0 334.1643 25.5 Total/Avg 9.00 27.00 9.40 25.0 9.1293 25.5 9.196 8.893 0.967 0.008 0.99
Run 3 

## - Initial 0.00 15.00 101.90 25.0 334.1643 25.6 Final 15.00 15.00 109.40 25.0 341.3924 25.8 Total/Avg 15.00 15.00 7.50 25.0 7.2281 25.7 7.329 7.036 0.960 0.002 0.47 

# Avera e Meter Calibration Factor Y 0.958

~ Note: For Calibration Factor Y, the ratio of the reading of the catibration meter to the dry gas meter, acceptable tolerance of individual values from the average is +402.

cerlify that the above Dry Gas Meter was calibrated in accordance with USEPA Methods, CFR 40 Part 60, using the Precision Wet Test Meter # 11AE6, 

## vhich in turn was calibrated using the American 13e11 Prover # 3785, ce ificate # F107, which is traceable to the National Bureau of Standards (N.I.S.T.).

Signature
, 

### `~ Date 7 -0 7

~



# ~

~

SK25

- @002437

- 2007 Cusloi»er-Arrnsrrong Environmerila! Sales Order-0030621 Page t o! 1 Pnnred on 51172007.

### iIREF! Calibrafion Dafe: 5-17-2007



# Nteter Correction Factor Y vs Standardized Flowrate 

# Average Meter Calibrafion Factor (Y) = 0.958

0.985

0.980

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0 

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0.500 1.000 1.500 2.000 2.500

Standardized Flowrate Qmstd (slm) uREF! 

# ; i I 0.945 ,

0.940

0.935 0.000



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# 63

# Sulfur Dioxide Barium-Thorin Analysis

Plant: Daltile, EI Paso, TX Location: Common Kiln Exhaust Date: 17•Jun•08 Standardization Ba (C102)4 Titration (mis) Avg. Titration (mis) 

## .;13: . . . . 12.93333 Blank Titration (mis) Avg. Blank (mis) 0.1

Volume of Standard Sulfuric Acid (mis) Normality of Standard Sulfuric Acid Normality: 0.00893 

## AI iquot Average Run # Location Volume Dilution Volume Titration Titration (mis) (mis) (mis) (mis) (mis)

1 Imp 1 •2 4


# . 6

2 Im p 1•2 ~0::~~~:~:~:~ 

## :::::: ~;::~~~ ~:~ 

# 4

~ 

## ::
~ 

## ::
~ 

## :::::
~ 

## :::::.. •. ~ 

## < : ~ 

## . x: :
~~ 

## :: 

# 66 7 3 36 66

3 Im 

## P 1•2 

## Q:

. . , 

# 3

. 

# 7

Run # Location Total Grams Total Mlg



## 1 I mp 1& 2 S02 0.00643 6.43

2 Imp 1 &2 S02 0.004668 4.67

3 Imp 1& 2 S02 0.005144 5.14

. ~ ;

# EMISSION TEST SUMMARY

PLANT

: 

## Daltile, EI Paso, TX DATE

: 

## 17•Jun•08 PLACE

: 

## Combined Kiln Exhaust RUN#

: 

## 1
TEST DURATION (MINUTES)

: 

## 0 LIQUID COLLECTED (mis)

: 

## 0 NOZZLE DIAMETER (INCH.)

: 

## 0 S02 WEIGHT (mg)

. 

## 6.43 METER COEFFICIENT (Y)

; 

## 0.958 0 PITOT COEFFICIENT (Cp)

: 

## 0 STATIC PRESSURE (in. H20)

: 

## 0 GAS METER VOL.(Cu.Ft.)

: 

## 1.723 PERCENT CO2

. 

## 0 BAROMETRIC PRESSURE

. 

## 26.2 PERCENT 02

: 

## 0 PERCENT CO : 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 0 STACK LENGTH(inchs)

: 

## STACK AREA (Sq.Ft.)

: 

## 0 STACK WIDTH(inchs)

: 

## NOZZLE AREA (feet): 0 STACK AREA (Sq.Ft.)

: 

## 0

ENTER THE STACK AREA SHOWN ABOVE: 0


# FLOWS SAMPLED VOLUME (STD. CU .FT.): 1.4394

Sulfur Dioxide, ppm: 59.2847

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 0 0.10 69.8 69.8 2 0 69.8 69.8 3 0 69.8 69.8 4 0 69.8 69.8 5 0 69.9 69.9 6 0 70.1 70.1 7 0 70.2 70.2 8 0 70.3 70.3 9 0 70.3 70.3 10 0 70.3 70.3 11 0 70.4 70.4 12 0 70.5 70.5 13 0 70.6 70.6

#DIV/0! 0.0000 0.1000 70.1385 70.1385 70.1385



# 65

# EMISSION TEST SUIVIMARY

PLANT : Daltile : EI Paso, TX DATE : 17•Jun•08 PLACE : Combined Kiln Exhaust RUN# : 2
TEST DURATION (MINUTES)

: 

## 0 LIQUID COLLECTED (mis)

: 

## 0 NOZZLE DIAMETER (INCH.)

: 

## 0 S02 WEIGHT (mg) 4.67 METER COEFFICIENT (Y)

: 

## 0.958 0 PITOT COEFFICIENT (Cp)

: 

## 0 STATIC PRESSURE (in. H20)

: 

## 0 GAS METER VOL.(Cu.Ft.)

: 

## 1.723 PERCENT CO2

: 

## 0 BAROMETRIC PRESSURE

: 

## 26.2 PERCENT 02

. 

## 0 PERCENT CO

. 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 0 STACK LENGTH(inchs)

: 

## STACK AREA (Sq.Ft.)

: 

## 0 STACK WIDTH(inchs)

: 

## NOZZLE AREA (feet): 0 STACK AREA (Sq.Ft.)

: 

## 0

ENTER THE STACK AREA SHOWN ABOVE: 0


# FLOWS SAMPLED VOLUME (STD. CU .FT.): 1.4394

Su(fur Dioxide, ppm: 43.0575

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 0 0.10 69.8 69.8 2 0 69.8 69.8 3 0 69.8 69.8 4 0 69.8 69.8 5 0 69.9 69.9 6 0 70.1 70.1 7 0 70.2 70.2 8 0 70.3 70.3 9 0 70.3 70.3 10 0 70.3 70.3 11 0 70.4 70.4 12 0 70.5 70.5 13 0 70.6 70.6

#DIV/01 0.0000 0.1000 70.1385 70.1385 70.1385

mw 

# BE

# EMISSION TEST SUMMARY

PLANT

: 

## Daltile, EI Paso, TX DATE

: 

## 17•Jun-08 PLACE

: 

## Combined Kiln Exhaust RUN#: 3
TEST DURATION (MINUTES)

: 

## 0 LIQUID COLLECTED (mis)

: 

## 0 NOZZLE DIAMETER (INCH.)

: 

## 0 S02 WEIGHT (mg)

. 

## 5.14 METER COEFFICIENT (Y)

; 

## 0.958 0 PITOT COEFFICIENT (Cp)

: 

## 0 STATIC PRESSURE (in. H20)

: 

## 0 GAS METER VOL.(Cu.Ft.)

: 

## 1.723 PERCENT CO2

. 

## 0 BAROMETRIC PRESSURE

: 

## 26.2 PERCENT 02

. 

## 0 PERCENT CO

. 

## 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 0 STACK LENGTH(inchs)

: 

## STACK AREA (Sq.Ft.)

: 

## 0 STACK W1DTH(inchs)

: 

## NOZZLE AREA (feet): 0 STACK AREA (Sq.Ft.)

: 

## 0

ENTER TH E STACK AREA SHOWN ABOVE: 0


# FLOWS SAMPLED VOLUME (STD. CU .FT.): 1.4394

Sulfur Dioxide, ppm: 47.3909

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F I N LET OUTLET

1 0 0.10 69.8 69.8 2 0 69.8 69.8 3 0 69.8 69.8 4 0 69.8 69.8 5 0 69.9 69.9 6 0 70.1 70.1 7 0 70.2 70.2 8 0 70.3 70.3 9 0 70.3 70.3 10 0 70.3 70.3 11 0 70.4 70.4 12 0 70.5 70.5 13 0 70.6 70.6

#D1V/01 0.0000 0.1000 70.1385 70.1385 70.1385



# 6-7

### 43



# Table 7E-4 - Interference Response

Date of Test 

# : 5~ 9 4
- 7 

# A.nalyzer Type : i~c~ 

# c('k y ~'~'S ~-~-b - 70 

# 5 

# ~G ~ Model No 

# .:}

~ 

# r-o

~ 

# tiJs %

~ 

# > l'~..~ ~ y S 

# Serial No 

# : $3s 9 s Calibration Span: 

# - `7' ~ 

# , S —



# Test Gas Type Concentration (ppm) Analyzer

Response


# 5-0 Z ~.~ 

# , 5' ~ 

# p 6.00 G, 4 -7 A,%



# 14

~ 

# . S`o P n1

LO ~ E~ o (o 

# Co 2, °r 0 d • a
~



## 1 

# H C,(
C:. o ~o ~~~ ~^ 

# O J Q U

II2-0 010



# Sum of Responses 0 % of Calibration Span o`1 Q



# W

## Sheetl

Summary of NOx Stratification

Plant: Daltiie, EI Paso. TX Location: Combined Ki1n Exhaust Date: 6/16109



## Concentration % of Mean

37.7 0.3809482 37.94 -0.253231 38.08 -0.62317 38.16 "-0.834563 38.27 -1.125228 37.75 0.2488274 38.33 -1.283773 38.48 -1.680136 37.51 0.8830071 37.92 -0.200383 36.71 2.9969392 37.28 1.4907626

37.84416667 Point # 1

2 3 4 5 

## 6 7 8 9 

# 10 11 12
Average

Page 1

t~6116108 Caltbrations

Date/Time S02 VOC NOx CO mm/ddlyy hh:mm:ss ppm ppm ppm ppm 06/1610813:39:14 0.7 3.0 0.0 0.0 0611610813:39:24 0.5 3.0 0.0 0.0 06118/0813:39:34 3.1 3.0 0.0 0.0 06/16/0813:39:44 38.8 3.0 1.3 0.0 06116/0813:39:54 77.3 3.0 1.4 -0.1 06/16/0813:40:04 92.7 3.0 1.4 -0.2 0611610813:40:14 98.0 3.0 1:4 -0.2 06/1610813:40:24 99.6 3.0 1.4 0.0 06/1610813:40:34 100.3 3.0 1.4 0.0 0611610813:40:44 100.7 3.0 1.4 0.0 06/1610813:40:54 

### 101.1 3.0 1.4 

### 0.0
06116/08 13:41:04 

### 101.0 3.0 1 A 

### 0.0
06/16108 13:41:14 

### 101.1 2.9 1.4 0.0 06116/0813:41:24 

### 100.9 3.0 1.4 

### 0.0 06/1 fi/0813:41:34 100.9 3.0 1.4 0.0 06/1610813:41:44 87.0 3.0 0.7 0.0 06/16/0813:41:54 43.7 3.0 0.0 0.0 06/16/0813:42:04 16.0 3.0 0.0 0.1 08116108 13:42:14 18.8 3.1 0.0 0.1 0611610813:42:24 35.8 3.1 0.0 0.2 06/16/0813:42:34 44.3 3.0 0.0 0.1 0611610813:42:44 47.4 3.1 0.0 0.0 0611610813:4254 48.4 3.1 0.0 -0.1 06116/0813:43:04 49.1 3.2 0.0 -0.1 06116/0813:43:14 49.3 3.1 0.0 -0.2 06/16/0813:4324 

### 49.3 3.2 

### 0.0 -0.2 06/16/0813:43:34 

### 49.3 3.1 

### 0.0 -0.2 06/16/0813:43:44 

### 49.6 3.2 

### 0.0 -0.2 06/16/0813:43:54 

### 49.8 3.2 0.0 -0.2 06116/0813:44:04 45.1 3.2 0.0 -0.2 06116/0813:44:14 25.4 3.2 0.0 -0.1 06116/0813:44:24 11.3 3.2 0.0 -0.1 0611610813:44:34 65.2 3.2 0.7 0.0 O6116/0813:44:44 172.0 3.2 1.0 0.0 08116/0813:44:54 224.8 3.1 1.1 0.0 0611 fi/08 13:45:04 241.9 3.2 1.1 0.0 06/16/0813:45:14 246.5 3.2 1.1 0.0 06116/0813:45:24

. 247.5 3.1 1.1 0.0 06116l0813:45:34 248.2 3.1 1.0 0.0 06/16/0813:45:44 248.8 3.2 1.0 0.0 06/16/0813:45:54 249.4 3.2 1.1 -0.1 06/16/0813:46:04 

### 249.4 3.1 1.0 -0.1 06116/0813:46:14 

### 249.4 3.2 1.1 -0.1 06/1610813:46:24 

### 249.7 32 1.0 0.0 06/16/0813:46:34 

### 249.9 3.2 1.1 0.0 06/16/0813:46:44 247.5 3.2 1.0 0.0 06/16/0813:46:54 177.0 3.2 0.2 0.0 06/16/0813:47:04 72.5 3.2 0.0 0.0 06/1610813:47:14 24.6 3.2 9.0 0.1 06116/0813:47:24 15.0 3.2 48.7 0.1 08/16/0813:47:34 6.7 3.2 49.4 0.1 06/16/0813:47:44 2.1 3.1 49.5 0.1 06/1610813:47:54 0.6 3.1 49.5 0.0 06/1610813:48:04 0.3 3.1 49.4 -0.1 06116/0813:48:14 0.2 3.1 50.5 -0.1 06/1610813:48:24 0.2 3.1 50.8 -0.1 06116/0813:48:34 0.2 3.2 50.9 -0.1 06116/0813:48:44 0.1 3.2 50.9 -0.1 0611610813:48:54 0.1 3.1 80.9 -0.1 06116/0813:49:04 0.0 3.2 51.0 -0.1 06/16/0813:49:14 0.0 3.2 51.0 -0.1 06/1610813:49:24 0.0 3.2 51.0 -0.1 06116/0813:49:34 0.0 3.2 32.0 -0.1 06/16/0813:49:44 0.4 3.2 1.3 -0.1 06/1610813:49:54 0.7 3.2 0.6 -0.1 06/1610813:50:04 0.3 3.2 25.7 0.0 06116/0813:50:14 0.0 3.2 24.5 0.0 06/16/0813:50:24 -0.2 3.2 

### 24.6 0.0 101 ppm S02 Zero CO

50.1 ppm S02 Zero NOx

247 ppm S02

51.5 ppm NOx



### Page 1 

# 706116108 Caiibrations

06/16/08 13:50:34 -0.3 3.2 

### 24.6 -0.1 25 ppm NOx 06/1610813:50:44 -0.3 3.2 

### 24.7 -0.1 06116/0813:50:54 -0.3 3.2 

### 24.7 -0.1 0611610813:51:04 0.1 3.2 24.6 -0.2 06/16/0813:51:14 0.0 3.2 24.7 -0.2 06/1610813:51:24 -0.2 3.2 3.4 -0.2 06/1610813:51:34 0.1 3.2 0.1 -0.2 06/16/0813:51:44 0.2 3.2 2.7 -0.1 06/16/0813:51:54 0.2 3.2 4.9 0.0 06/1610813:52:04 0.0 3.2 4.8 0.1 06/1610813:52:14 -0.1 3.2 4.8 0.0 06116/0813:52:24 0.0 3.2 4.7 -0.1 06/1610813:52:34 0.0 3.2 

### 4.7 -0.2 06/16/08 13:52:44 -0.1 3.2 

### 4.8 -0.2 .5.13 ppm NOx 06/1610813:52:54 -0.2 3.2 

### 4.8 -0.2 06/1610813:53:04 -0.5 3.2 

### 4.8 -0.2 06/1610813:53:14 -0.4 3.2 3.9 -0.2 06/16/0813:53:24 -0.3 3.2 0.0 -0.2 06116/0813:53:34 -0.3 3.2 0.1 -0.2 0611610813:53:44 -0.2 3.2 0.0 1.8 06/1610813:53:54 -0.3 3.2 0.0 9.1 06/16f0813:54:04 0.0 3.2 0.0 21.3 0611610813:54:14 -0.2 3.2 0.0 33.7 0611610813:54:24 -0.3 3.2 0.0 42.3 06/1610813:54:34 -0.5 3.2 0.0 46.5 06/16/0813:54:44 -0.4 3.2 0.0 47.9 06/16/0813:54:54 -0.1 3.2 0.0 48.3 06116/0813:55:04 -0.2 3.2 0.0 48.3 06116/0813:55:14 -0.2 3.2 0.0 48.3 0611610813:55:24 -0.2 3.2 0.0 48.3 06116/0813:55:34 -0.1 3.2 0.0 48.3 06l16/0813:55:44 -0.2 3.2 0.0 48.2 06/16/0813:55:54 -0.3 3.2 0.0 49.2 0611610813:56:04 -0.5 3.2 0.0 

### 49.4 06/16/0813:56:14 -0.3 3.2 0.0 

### 49.4 50.3 ppm CO 06116/0813:56:24 -0.5 3.3 0.0 

### 49.3 06/1610813:56:34 -0.5 3.3 0.0 

### 49.3 06116/0813:56:44 -0.5 3.3 0.0 49.3 06/16/0813:56:54 -0.5 3.5 0.0 49.3 06116/0813:57:04 -0.4 3.5 0.0 49.3 0611610813:57:14 -0.3 3.4 0.0 46.7 0611610813:57:24 -0.1 3.4 0.0 38.2 06/16/0813:57:34 0.0 3.3 0.0 26.3 06116/0813:57:44 -0.1 3.4 0.0 18.0 06116/0813:57:54 -0.1 3.4 0.0 16.4 06/16/0813:58:04 -0.1 3.3 0.0 19.0 06/16/0813:58:14 -0.1 3.4 0.0 22.4 06/16/0813:58:24 -0.2 3.2 0.0 24.5 06/1610813:58:34 -0.3 3.3 0.0 26.1 06/16/0813:58:44 -0.3 3.3 0.0 25.2 06/16/0813:58:54 -0.3 3.3 0.0 25.3 06/1610813:59:04 -0.6 3.3 0.0 25.3 06/1610813:59:14 -0.6 3.4 0.0 

### 28.2 06/16/08 13:5924 -0.4 3.4 0.0 

### 25.2 24.3 ppm CO 06116/0813:59:34 -0.4 3.4 0.0 

### 25.2
0611610813:59:44 -0.5 3.4 0.0 

### 25.2 06116/0813:59:54 -0.3 3.3 0.0 25.2 06116/0814:00:04 -0.4 3.4 0.0 24.2 06116/0814:00:14 -0.3 3.4 0.0 20.3 06116/0814:00:24 -0.3 3.4 0.0 13.9 06/1610814:00:34 -02 3.4 0.0 8.4 06/16/0814:00:44 -0.3 3.4 0.0 5.6 06116/0814:00:54 -0.5 3.4 0.0 5.1 06116/0814:01:04 -0.6 3.4 0.0 5.4 0611610814:01:14 -0.7 3.4 0.0 5.6 06116/0814:01:24 -0.6 3.4 0.0 5.6 06116/0814:01:34 -0.6 3.4 0.0 5.6 06116/0814:01:44 -0.6 3.4 0.0 5.6 06/16/0814:01:54 -0.6 3.4 0.0 5.6 06/16108 14:02:04 -0.3 3.4 0.0 5.5 5.090 ppm 

### CO

Page 2 

# 716/16108 Calibrations

06116/0814:02:14 -0.3 3.4 0.0 

### 5.5 06116/0814:02:24 -0.3 3.4 0.0 

### 5.5 06/1610814:02:34 -0.2 3.4 0.0 5.2 06/1 fi/08 14:02:44 -0.1 3.4 0.0 4.1 06/1610814:02:54 -0.3 3.4 0.0 2.7 06/16/0814:03:04 0.0 3.4 0.0 1.5 06/16/0814:03:14 -0.1 3.4 0.0 0.6 06/16/0814:03:24 0.0 4.0 0.0 0.3 06l16/0814:03:34 -0.1 3.2 0.0 0.2 0611 fi108 14:03:44 -0.2 2.5 0.0 0.2 06/16/0814:03:54 -0.1 2.4 0.0 0.1 06116/0814:04:04 -0.1 2.2 0.0 0.1 06/16/0814:04:14 -0.1 2.2 0.0 0.1 0611610814:04:24 -0.2 2.2 0.0 0.1 06/16/0814:04:34 -0.3 2.3 0.0 0.2 0611610814:04:44 -0.2 2.2 0.0 0.2 0611610814:04:54 -0.2 2.2 0.0 0.2 06116/0814:05:04 3.5 2.2 0.1 0.2 06/1610814:05:14 24.5 2.2 0.7 0.2 06/1610814:05:24 49.2 2.2 1.0 0.2 06/1610814:05:34 69.0 2.2 1.2 0.2 06/1610814:05:44 82.8 2.4 1.3 0.2 06/1610814;05:54 89.6 2.4 1.4 0.1 0611610814:06:04 93.0 2.5 1.4 0.1 06116/0814:06:14 94.4 2.5 1.3 0.1 06/16J0814:06:24 95.2 2.4 1.4 0.1 0611610814:06:34 95.9 2.6 1.4 0.1 0611610814:06:44 96.1 2.7 1.4 0.1 06/16/0814:06:54 96.3 2.8 1.4 0.1 06116/0814:07:04 96.5 2.8 1.4 0.1 06/1610814:07:14 96.6 2.8 1.4 0.1 06/1610814:07:24 96.6 2.9 1.4 0.1 06116/0814:07:34 96.7 3.0 1.4 

### 0.1 06/16/08 14:07:44 96.8 3.0 1.4 

### 0.1 101 ppm 502 Btas 06/16/08 14:07:54 96.8 3.0 1.3 

### 0.1 Zero CO Bias 06116/0814:08:04 

### 96.9 3.4 1.4 0.1 06/16/0814:08:14 92.3 3.6 1.1 0.1 06/1610814:08:24 72.8 3.8 0.3 0.1 06/1610814:08:34 48.0 3.8 0.1 0.1 06/16/0814:08:44 30.5 3.6 4.5 0.1 06/1610814:08:54 20.0 3.6 13.3 0.1 06/1610814:09:04 122 3.6 19.1 0.1 06116/0814:09:14 5.7 3.6 22.0 0.1 06116/0814:09:24 2.0 3.6 23.0 0.0 06/1610814:09:34 0.6 3.6 23.5 0.0 06/1610814:09:44 0.3 3.6 23.6 0.0 06/1.610814:09:54 0.2 3.7 23.6 0.0 06/16/0814:10:04 0.1 3.8 23.8 ' -0.1 06116/0814:10:14 0.0 3.9 23.7 -0.1 0611610814:10:24 0.0 3.8 23.8 -0.1 06116/0814:10:34 0.0 3.9 23.8 -0.1 0611610814:10:44 -0.1 3.9 

### 23.8 -0.1 06/16/08 14:10:54 -0.1 3.9 23.9 0.0 25 ppm NOx Bias 06116/0814:11:04 0.0 3.7 

### 23.9 -0.1 06/16/0814:11:14 0.0 4.6 

### 23.8 -0.1 06116/0814:11:24 -0.1 6.1 22.0 -0.1 06116/0814:11:34 0.0 6.3 12.4 0.0 06116/0814:11:44 0.1 6.3 5.8 1.2 06116/0814:11:54 0.1 6.3 2.4 4.4 06/1610814:12:04 0.0 6.4 0.8 9.7 06/16/08 14:12:14 0.0 6.4 0.2 15.4 06/16/0814:12:24 0.0 6.6 0.0 20.0 06116/0814:12:34 0.0 6.6 0.0 22.7 06/16/0814:12:44 -0.1 6.6 0.0 24.2 06/16/0814:12:54 -0.2 6.6 0.0 24.8 0611610814:13:04 -0.3 6.6 0.0 25.0 06116/0814:13:14 -0.4 6.6 0.0 25.1 06/16/0814:13:24 -0.3 6.6 0.0 25.1 06/1610814:13:34 -0.2 6.6 0.0 25.1 06l1610814:13:44 

### -0.4 6.7 0.0 

### 25.2 06/16/08 14:13:54 -0.5 6.7 0.0 

### 25.2 24.3 ppm CO Bias

Page 3 

# 726116108 Cafibrations

06/16/08 14:14:04 -0.5 4.9 

### 0.0 25.2 Zero S02, NOx Bias 06/16/0814:14:14 

### -0.5 4.6 

### 0.0 25.3 06/16/0814:14:24 -0.1 4.7 0.0 25.1 0611610814:14:34 0.2 4.7 0.0 23.7 06116/0814:14:44 0.5 4.9 0.0 20.1 06/16I0814:14:54 0.5 5.0 0.0 14.9 06116/0814:15:04 0.5 5.0 0.0 9.5 06116l0814:15:14 0.5 5.0 0.0 5.4 06l1610814:15:24 0.5 5.0 0.0 219 0611610814:15:34 0.5 5.0 0.0 1.6 06/1610814:15:44 0.4 4.9 0.0 0.9 06/1610814:15:54 0.2 4.9 0.0 0.5 06/1610814:16:04 -0.1 4.9 0.0 0.3 06/1610814:16:14 -0.1 4.9 0.0 0.2 0611610814:16:24 -0.1 5.0 0.0 0.2 0611610814:16:34 -0.2 5.0 0.0 0.2 06/1610814:16:44 -0.3 5.0 0.0 0.2 0611610814:16:54 -0.4 3.8 0.0 0.2 06/1670814:17:04 0.0 3.3 0.0 0.2 06/16/0814:17:14 0.2 3.2 0.0 0.3 06/1610814:17:24 0.0 3.0 0.0 0.5 0611610814:17:34 0.0 3.0 0.0 0.7 06116l0814:17:44 0.0 3.0 0.0 0.7 0611610814:17:54 -0.2 2.9 0.0 0.5 06/16l0814:18:04 -0.5 0.4 0.0 0.3 06116/0814:18:14 -0.5 

### 0.1 0.0 0.2 06116/0814:18:24 -0.5 

### 0.1 0.0 0.1 Zero Air 06/16/0814:18:34 -0.5 

### 0.1 0.0 0.1 06/1610814:18:44 -0.5 

### 0.3 0.0 0.0 0611610814:18:54 -0.5 1.4 0.0 0.0 06/16/0814:19:04 -0.6 1.6 0.0 0.0 06/1610814:19:14 -0.6 1.7 0.0 0.0 06/1610814:19:24 -0.4 1.9 0.0 010 0611610814:19:34 -0.3 1.9 0.0 0.0 06/1610814:19:44 -0.2 1.9 0.0 0.0 06/16108 14:19:54 -0.3 1.9 0.0 ' 0.1 06/1610814:20:04 -0.4 1.9 0.0 0.1 0611610814:20:14 -0.5 2.0 0.0 0.1 0611610814:20:24 -0.4 5.3 0.0 0.1 0611610814:20:34 -0.5 16.8 0.0 0.1 0611610814:20:44 -0.4 16.8 0.0 0.1 06/1610814:20:54 -0.3 16.7 0.0 0.1 06116/0814:21:04 0.0 16.8 0.0 0.1 06/16/0814:21:14 -0.1 16.7 0.0 0.1 06l16l0814:21:24 -0.2 16.7 0.0 0.1 0611610814:21:34 -0.5 20.0 0.0 0.1 06116J0814:21:44 -0.5 

### 20.3 0.0 0.1 06/16/08 14:21:54 -0.4 

### 20.3 0.0 0.1 20.2 ppm CH4 0611610814:22:04 -0.7 

### 20.3 0.0 0.1 06/16J0814:22:14 -0.7 

### 20.3 0.0 0.1 0611610814:22:24 -0.6 20.2 0.0 0.1 06116/0814:22:34 -0.5 5.3 0.0 0.1 06l16/0814:22:44 -0.6 2.0 0.0 0.1 06f16/0814:22:54 -0.7 2.3 0.0 0.1 0611610814:23:04 -0.5 3.1 0.0 0.1 06/1610814:23:14 -0.3 6.8 0.0 0.1 06/1610814:23:24 -0.2 5.4 0.0 0.1 0611610814:23:34 -0.1 

### 5.3 0.0 0.1 06/16108 14:23:44 0.0 

### 5.3 0.0 0.1 5.142 CH4 06/1610814:23:54 -0.3 

### 5.3 0.0 0.1 06116ro814:24:04 -0.4 5.3 0.0 0.0 0611610814:24:14 -0.3 5.1 0.0 0.0 0611610814:24:24 -0.5 5.2 0.0 0.0 06/16l0814:24:34 -0.5 2.5 0.0 0.0 06116/0814:24:44 -0.3 2.1 0.0 -0.1 06116/0814:24:54 -0.2 2.4 0.0 0.0 06/16/0814:25:04 -0.4 24.5 0.1 0.0 06116/0814:25:14 -0.4 41.9 0.1 0.0 06/16/0814:25:24 -0.2 42.0 0.1 0.0 06l1610814:25:34 -0.3 

### 42.0 0.1 0.0

Page 4 

# 736116/08 Calibrations

0611610814:25:44 -0.3 

### 42.0 0.1 0.1 41 ppm CH4 06/16/0814:25:54 -0.4 

### 42.0 0.1 0.1 06116/0814:26:04 -0.7 

### 42.0 0.0 0.1 06116108 44:26:14 -0.8 42.0 0.1 0.1 06H 6/0814:26:24 -0.8 14.0 0.0 0.1 06/1610814:26:34 -0.8 2.2 0.0 0.1

Page 5 

# 746/16/08 Stratification Test

Date/Time S02 VOC NOx CO mmldcllyy hh:mm:ss ppm ppm ppm ppm 06/18l0814:49:54 61.8 7.5 36.1 34.5

Point #1 06/1610814:50:04 63.1 7.7 36.1 36.2 06116/0814:50:14 62.7 8.1 36.1 37.4 06/16/0814:50:24 62.5 9.1 36.0 38.2 06/1610814:50:34 62.4 10.2 35.9 38.8 06/16/0814:50:44 62.2 9.4 35.9 40.6 06/16/0814:50:54 61.8 9.1 35.9 45.1 06116/0814:51:04 61.3 9.1 36.0 52.7 06116/0814:51:14 61.1 9.8 36.2 62.1 06/16/08 14:51:24 61,1 10.5 36.3 69.7 06116/0814:51:34 60.9 10.3 36.5 73.5 06/1610814:51:44 60.5 9.8 36.5 75.0 06/16/0814:51:54 60.2 9.6 36.8 77.3 06/1610814:52:04 59.9 10.0 36.8 81.0 06116/0814:52:14 59.4 10.0 36.9 84.8 06/1610814:52:24 59.1 9.9 36.8 86.7 06/1610814:52:34 58.8 8.7 36.6 86.9 06/16/0814:52:44 59.0 8.0 36.7 87.4 06/1610814:52:54 59.4 7.7 36.8 89.2 06/16/0814:53:04 59.4 7.7 36.9 90.1 06116/0814:53:14 59.1 7.8 37.2 86.2 06116/0814:53:24 58.5 7.7 37.4 76.6 06116/0814:53:34 57.9 7.7 37.5 63.8 06116/0814:53:44 57.6 7.7 37.5 52.4 0611610814:53:54 57.5 7.7 37.6 44.0

Point #2 06/16/0814:54:04 57.5 7.7 37.9 38.8 06/16/0814:54:14 57.4 7.7 37.9 35.5 06116/0814:54:24 57.1 7.7 37.9 33.3 06/16/0814:54:34 56.9 7.7 37.8 31.8 0611610814:54:44 57.0 7.7 37.8 30.9 06/16/0814:54:54 57.7 7.2 37.9 30.2 06116/0814:55:04 57.6 7.7 38.1 30.2 06/16/0814:55:14 57.0 7.9 38.0 30.0 06116/0814:55:24 56.6 7.7 37.9 29.8 06/16/0814:55:34 56.3 7.7 37.8 29.8 06/16/0814:55:44 56.6 7.9 37.7 29.9 06/16/0814:55:54 56.8 7.7 37.8 30.0 06/16/0814:56:04 57.0 7.7 37.9 30.1 08/1610814:56:14 57.2 7.8 37.9 30.1 06/16/0814:56:24 57.1 7.9 37.8 29.9 06/16/0814:56:34 56.9 7.8 38.0 29.8 06/1610814:56:44 57.2 6.0 38.0 29.7 06/16/0814:56:54 57.3 7.8 38.1 29.6 06/16/0814:57:04 57.6 7.8 38.3 29.6 06/16/0814:57:14 57.9 8.0 38.3 29.5 06/16/0814:57:24 57.4 8.0 38.1 29.4 06/16/0814:57:34 57.0 8.0 38.0 29.4 06/16/0814:57:44 56.8 7.9 37.9 29.3 06/16/0814:57:54 56.5 8.0 37.6 29.3
Stop Point #2 57.10 7.79 37.94 30.66 Starl Point #3 0611610814:58:04 56.6 8.0 37.7 29.2 06116/0814:58:14 56.5 7.9 37.8 29.3 06/1610814:58:24 56.1 8.0 37.9 29.3 06116/0814:58:34 56.1 8.0 37.9 29.2 06/16/0814:58:44 56.1 8.0 37.8 29.2 06/16/0814:58:54 55.8 8.0 38.1 29.2 06/16/0814:59:04 55.6 8.0 38.1 29.2 06/16/0814:59:14 55.5 8.0 38.0 29.2 06/16/0814:59:24 55.1 8.0 38.0 29.2 06/16/0814:59:34 55.2 8.0 38.0 29.3 0611610814:59:44 55.3 8.0 38.1 29.4 06116/0814:59:54 55.0 7.9 38.4 29.4 06116/0815:00:04 54.9 7.9 38.4 29.4 06116/0815:00:14 54.5 7.9 38.3 29.3 06116/0815:00:24 54.5 8.0 38.1 29.3

Page 1 

# 756/16/08 Stratification Test

06116/0815:00:34 54.5 8.0 38.2 29.3 06116/0815:00:44 54.8 8.0 38.2 29.2 06/16J0815:00:54 55.4 8.0 37.9 29.2 06J1610815:01:04 56.3 8.0 37.9 29.2 0611610815:01:14 57.3 8.0 37.9 29.3 06116/0815:01:24 57.9 8.0 38.1 29.3 06/16/0815:01:34 58.4 8.1 38.2 29.3 06/16/0815:01:44 58.5 8.2 38.2 29.3 06/16/0815:01:54 58.5 8.0 38.3 29.3
Stop Point 43 56.02 7.99 38.06 29.30 Stari Point #4 06/1610815:02:04 58.3 8.0 38.2 29.4 06/16/0815:02:14 58.5 8.0 38.2 29.4 0611610815:02:24 58.4 8.0 38.2 29.4 0611610815:02:34 58.4 8.0 38.3 29.4 0811610815:02:44 58.4 8.0 38.3 29.4 06/1610815:02:54 58.5 8.0 38.3 29.3 06/16/0815:03:04 58.3 8.0 38.2 29.3 06116/0815:03:14 58.4 8.0 38.1 29.2 0611610815:03:24 58.5 8.0 38.0 29.0 06/16/0815:03:34 58.9 8.0 38.0 28.9 06116/0815:03:44 59.0 8.0 38.0 28.9 06l16/0815:03:64 59.1 8.0 38.2 28.8 0611610815:04:04 59.2 8.0 38.3 28.7 06116/0815:04:14 59.0 7.7 38.3 28.6 06116/0815:04:24 58.7 7.7 38.3 28.5 06116/0815:04:34 58.4 7.7 38.0 28.4 06116/0815:04:44 58.3 7.7 38.0 28.3 06/16/0815:04:54 58.6 7.8 38.0 28.2 06/16/0815:05:04 59.0 7.7 38.1 28.1 06/16/0815:05:14 59.2 7.8 38.3 28.1 06116/0815:05:24 59.1 7.7 38.3 28.0 06/1610815:05:34 58.7 7.7 38.1 27.9 06/1610815:05:44 58.6 7.7 38.1 27.8 06/1610815:05:54 58.6 7.6 38.0 27.7
Stop Point #4 58.68 7.85 38.16 28.69 Starl Point #5 06/16/0815:06:04 58.8 7.6 37.9 27.5 06/16/0815:06:14 58.8 7.6 38.1 27.4 06116/0815:06:24 58.6 7.6 38.4 27.3 06/16/0815:06:34 58.4 7.4 38.4 27.1 06/16/0815:06:44 58.2 7.6 38.3 26.9 06/16/0815:06:54 58.1 7.6 38.2 26.8 06/16/0815:07:04 57.9 7.6 38.1 26.7 06116/0815:07:14 57.7 7.5 38.1 26.6 0611610816:07:24 58.0 7.3 38.2 26.6 06/1610815:07:34 57,9 ' 7.3 36.4 26.5 06/16/0815:07:44 57.6 7.3 38.4 26.5 0611 6108 1 5:07:54 57.4 7.4 38.4 26.5 06/16/0815:08:04 56.8 7.4 38.3 26.5 06/16/0815:08:14 56.2 7.4 38.2 26.5 06/16/0815:08:24 55.9 7.3 38.1 26.5 06116/0815:08:34 55.5 7.3 38.0 26.6 06/16/0815:08:44 55.4 7.3 38.2 26.7 06/16/0815:08:54 55.8 7.3 38.4 26.7 06/1610815:09:04 55.8 7.3 38.5 26.7 06/1610815:09:14 55.3 7.3 38.5 26.7 0611610815:09:24 54.7 7.3 38.5 26.7 06116/0815:09:34 54,4 7.3 38.4 26.8 0611610815:09:44 54.3 7.3 38.4 26.9 06116/0815:09:54 54.3 7.3 38.2 26.9
Stop Point #5 56.74 7.42 38.27 26.77 Start Point sE6 06116/0815:10:04 54.8 7.4 38.0 27.1 06116/0815:10:14 54.9 7.3 38.0 27.3 06/16/0815:10:24 55.0 7.3 38.1 27.5 06/16/0815:10:34 54.8 7.3 38.2 27.6 06116/0815:10:44 54.6 7.3 38.2 27.7 06116/0815:10:54 54.2 7.3 38.3 27.9 06/1610815:11:04 53.7 7.3 38.3 28.0 06/16J0815:11:14 53.4 7.3 38.4 28.1

Page 2 

# 766116/08 Stratification Test

06116/0815:11:24 53.1 7.3 38.4 28.2 06116/0815:11:34 52.8 7.3 38.2 28.4 06/16/0815:11:44 52.9 7.2 37.9 28.5 06/1610815:11:45 52.9 7.3 37.8 28.7 06/16/0815:12:04 53.2 7.3 37.6 29.0 06/1610815:12:14 53.1 7.3 37.3 29.2 06/16/0815:12:24 53.0 7.3 37.4 29.3 06/1610815:12:34 52.8 7.3 37.2 29.6 06/1610815:12:44 52.8 7.4 37.1 29.7 06/1610815:12:54 52.7 7.3 37.1 29.8 06/1610815:13:04 52.6 7.3 37.2 30.0 06/1610815:13:14 52.6 7.3 37.3 30.2 06/16/0815:13:24 52.7 7.3 37.5 30.3 06/16/0815:13:34 52.4 7.3 37.6 30.4 0611610815:13:44 52.4 73 37.7 30.5 06/1610815:13:54 52,4 7.4 37.8 30.5
Stop Point #6 53.33 7.33 37.78 28.89 Start Point #7 06/1610815:14:04 52.3 7.1 38.0 30.5 06/16/0815:14:14 52.4 7.0 38.3 30.4 06/16/0815:14:24 52.4 7.1 38.3 30.3 06/16/0815:14:34 52.4 7.3 38.3 30.2 06/1610815:14:44 52.6 7.2 38.2 30.2 06/16/0815:14:54 52.5 7.1 38.1 30.2 06/16/0815:15:04 52.5 7.0 38.1 30.2 06/16/0815:15:14 52.2 7.0 38.0 30.1 06/16/0815:15:24 51.8 7.2 38.0 29.9 06/1610815:15:34 51.4 7.2 38.0 29.8 06/16/081515:44 51.4 7.4 38.1 29.6 06/16/0815:15:54 51.9 7.3 38.3 29.4 06/16/0815:16:04 50.7 7.1 38.3 29.3 06/16/0815:16:14 50.7 7.3 38.3 29.3 0611610815:16:24 51.0 7.2 38.4 29.3 06/16/0815:16:34 51.2 7.0 36.4 29.2 06/1610815:16:44 51.2 7.0 38.3 29.2 06116/0815:16:54 51.6 7.0 3B.4 29.3

, 0611610815:17:04 51.9 7.0 38.4 29.4 06116/0815:17:14 52.2 7.0 38.5 29.6 06116/0815:17:24 52.3 7.0 38.6 29.7 06116/0815:17:34 52.3 7.0 38.8 29.9 06116/OB 15:17:44 52.4 7.0 39.0 30.0 06116/0815:17:54 52.5 7.0 39.0 30.1
Stop Point #7 51.88 7.11 38.33 29.79 Start Point #8 06116/0815:18:04 52.7 7.0 39.0 30.1 06/16/0815:18:14 52.8 7.0 39.0 30.3 06/16/0815:18:24 53.0 7.0 38.9 30.3 06/16/0815:18:34 53.2 7.0 39.1 30.3 06/16/0815:18:44 53.3 7.0 39.2 30.3 06/1610815:18:54 53.8 7.0 39.1 30.1 06/16/0815:19:04 54.3 7.0 38.9 30.0 06/16J0815:19:14 54.7 7.0 38.6 29.9 0611610815:19:24 55.2 6.9 38.6 29.8 06/1610815:19:34 55.5 6.9 38.7 29.7 06/1610815:19:44 56.0 6.8 38.7 29.6 0611610815:19:54 56.3 6.8 38.6 29.5 06/1610815:20:04 56.8 6.8 38.4 29.5 06116108 15:20:14 57.1 6.8 38.3 29.5 06/161081520:24 56.9 6.8 37.9 29.5 06/1610815:20:34 57.3 6.8 37.6 29.5 06/1610815:20:44 57.4 6.8 37.6 29.5 0611610815:20:54 57.6 6.8 38.0 29.4 06/1610815:21:04 57.7 6.8 38.1 29.3 06/1610815:21:14 57.9 6.8 38.3 29.2 06/16/0815:21:24 57.8 6.8 38.4 29.1 06/16/0815:21:34 57.6 6.8 38.4 29.0 06/16/0815:21:44 57.7 6.8 38.3 28.9 06/16/0815:21:54 57.8 6.8 38.0 29.0
Stop Point #8 55.85 6.88 38.48 29.65

06/1610815:22:04 58.1 6.7 37.9 29.0



### Page 3 

# 7 76/16/08 StratifzcatPon Test

06116/0815:22:14 58.3 6.8 37.9 29.1 06116/0815:22:24 58.5 6.8 37.8 29.2 06116J0815:22:34 58.2 6.8 37.7 29.4 06116/0815:22:44 57.9 6.8 37.6 29.5 06/1610815:22:54 58.0 6.8 37.6 29.6 06/1610815:23:04 57.8 6.8 37.6 29.8 06/1610815:23:14 58.2 7.3 37.5 30.1 06/16/0815:23:24 58.5 11.1 37.4 30.4 06/1610815:23:34 58.7 14.1 37.2 31.1 06/1610815:23:44 59.1 15.2 37.1 33.3 06/1610815:23:54 59.4 15.6 36.9 39.2
Stop Run #9 58.40 9.23 37.51 30.81

06116/0815:24:04 59.8 15.6 36.9 50.1 06116/0815:24:14 60.0 15.1 36.9 65.3 06/16/0815:24:24 60.1 15.0 37.0 82.0 06/16/0815:24:34 60.1 18.0 37.1 95.6 06/16/0815:24:44 60.1 20.5 37.0 99.8 06116/0815:24:54 60.1 22.7 37.0 99.8 06116/0815:25:04 60.0 22.2 36.9 99.8 06116/0816:25:14 59.9 22.4 36.8 99.8 06116/0815:25:24 59.6 23.2 36.8 99.8 06/1610816:25:34 59.4 21.1 36.8 99.8 06/1610815:25:44 59.1 15.8 36.8 99.8 06/1610815:25:54 58.9 10.4 36.8 99.8 06/1 6108 1 5:26:04 59.0 8.1 36.8 99.8 06/1610815:26:14 58.8 7.1 36.9 99.8 06/1610815:26:24 58.3 6.8 37.0 99.8 06/16/0815:26:34 58.1 6.8 37.1 99.8 06/16/0815:26:44 58.0 6.8 37.1 97.6 06/16/0815:26:54 57.6 6.6 37.4 76.4 06/1610815:27:04 57.1 6.5 37.6 59.0 06/16/0815:27:14 56.2 6.5 37.9 47.4 06/1610815:27:24 55.5 6.5 38.2 40.1 06/16/0815:27:34 55.0 6.5 38.0 35.8 06116/0815:27:44 54.9 6.5 37.8 33.2 0611610815:27:54 55.7 6.6 37.6 31.8

Start Point #10 06/16/0815:28:04 56.9 6.4 37.7 30.9 06/1610815:28:14 58.0 6.4 37.8 30.2 06/16/081548:24 58.3 6.3 38.0 29.8 06/16/0815:28:34 58.0 6.3 38.2 29.5 06/16/0815:28:44 57.6 6.2 38.2 29.1 0611610815:28:54 56.9 6.3 38.4 28.9 06/16/0815:29:04 56.8 6.2 38.5 28.8 06/16/0815:29:14 56.6 6.2 38.8 28.7 06/1610815:29:24 56.6 6.4 39.0 28.8 06/16/0815:29:34 57.0 6.3 39.0 28.8 06116/0815:29:44 57.6 6.2 38.8 28.7 06116/0815:29:54 58.4 6.3 38.7 28.6 06/16/0815:30:04 58.8 6.3 38.7 28.6 06116/0815:30:14 59.0 6.2 38.6 28.5 06/16/0815:30:24 59.1 6.3 38.6 28.5 06/16/0815:30:34 59.1 6.3 38.3 28.5 06l16/0815:30:44 59.1 6.6 37.9 28.3 06116/0815:30:54 59.2 7.3 37.4 28.3 06116/08 1 b:31:04 59.9 7.2 37.0 28.4 06116/0815:31:14 61.2 6.7 36.8 29.1 06/16/0815:31:24 62.4 6.5 36.7 31.8 06/16/0815:31:34 62.9 6.6 36.6 36.1 06/16/0815:31:44 62.9 6.6 36.3 40.6 06/16/0815:31:54 62.6 6.6 36.3 42.8
Slop Point #10 58.94 6.45 37.92 30.42 Start Point #11 06/1610815:32:04 62.3 6.6 36.1 42.1 06/16/0815:32:14 61.7 6.6 36.1 39.7 06/16/0815:32:24 61.7 6.6 36.2 37.0 06116/0815:32:34 61.4 6.6 36.3 35.5 06116/0815:32:44 61.0 6.6 36.1 35.1 06/16/0815:32:54 60.9 6.5 36.1 35.2 06/16/0815:33:04 60.8 6.5 36.2 35.5



### Page 46116108 Stratification Test

06/16/0815:33:14 60.6 6.3 36.4 34.8 06116/0815:33:24 60.6 6.5 36.5 33.4 06/16/0815:33:34 60.5 6.5 36.5 31.9 06/16/0815:33:44 60.3 6.2 36.6 30.6 06/16/0815:33:54 60.1 6.2 36.5 29.6 06/16/0815:34:04 59.4' 6.2 36.6 28.9 06/16/0815:34:14 59.1 6.2 36.8 28.5 06/16/0815:34:24 58.6 6.2 36.9 28.4 06/16/0815:34:34 58.3 6.2 36.9 28.3 06116/0815:34:44 58.3 6.2 36.9 28.2 06/16/0815:34:54 58.2 6.2 36.9 28.1 06/16/0815:35:04 57.7 6.1 37.0 28.1 06/16/0815:35:14 57.6 5.9 37.2 28.0 06/1610815:35:24 57.3 6.0 37.6 28.0 06116/0815:35:34 56.8 6.0 37.7 28.0 06116/0815:35:44 56.5 5.9 37.6 27.9 06116/0815:35:54 56.1 5.9 37.3 27.9
Stop Point #11 59.41 6.27 36.71 31.61 Start Point #12 06/16/0815:36:04 56.3 5.9 37.2 27.9 0611610815:36:14 56.4 6.0 37.1 27.9 06/1610815:36:24 56.3 5.9 37.3 27.9 06/16/0815:36:34 56.3 5.9 37.3 27.9 06116/0815:36:44 56.4 5.9 37.3 27.9 06/1610815:36:54 56.6 5.9 37.4 27.9 06116/0815:37:04 56.7 5.9 37.5 27.9 06116/0815:37:14 56.6 5.9 37.7 27.8 0611610815:37:24 56.6 5.9 37.5 27.8 06/16/0815:37:34 56.4 5.9 37.5 27.8 06/16/0815:37:44 56.4 5.9 37.4 27.8 06/16/0815:37:54 56.6 5.9 37.3 27.8 06/16/0815:38:04 56.6 5.9 37.3 27.7 06/16/0815:38:14 56.5 5.9 37.2 27.7 06/16/0815:38:24 56.4 5.9 37.1 27.8 06116/0815:38:34 56.7 6.9 37.0 27.8 06116/0815:38:44 56.9 5.9 36.9 27.9 06/16/0815:38:54 56.8 5.9 36.8 27.9 06/1610815:39:04 56.8 5.9 36.9 27.9 06/16/0815:39:14 56.9 5.9 37.1 27.8 08116J0815:39:24 56.8 5.9 37.3 27.8 06/ 16108 15:39:34 56.5 5.8 37.6 27.7 08/16J0815:39:44 56.7 5.9 37.6 27.6 06116l0815:39:54 57.0 5.8 37.6 27.5
Stop Point #12 56.60 5.90 37.28 27.82 Start Point #1 06/1610815:40:04 57.3 5.9 37.8 27.5 06/16/0815:40:14 57.5 5.9 37.7 27.5 06/16/0815:40:24 57.8 5.9 37.7 27.6 #OIV/01 57.7 5.9 37.6 27.7 06116/0815:40:44 57.8 5.9 37.6 27.7 06116/0815:40:54 58.0 5.9 37.9 27.8 06/16/0815:41:04 58.3 5.9 38.0 27.8 06/16/0815:41:14 58.3 5.9 37.9 27.9 06/1610815:41:24 58.6 5.9 37.9 28.0 06/1610815:41:34 59.0 5.9 37.8 28.1 06/1610815:41:44 59.2 5.9 37.7 28.2 06/1610815:41:54 59.2 5.9 37.8 28.3 06/1610815:42:04 58.9 5.9 37.9 28.4 06/1610815:42:14 58,8 5.9 37.9 28.5 06/18/0815:42:24 58.8 5.9 37.8 28.5 06/16/0815:42:34 59.0 5.9 37.5 28.5 06/16/0815:42:44 59.3 5.8 37.4 28.6 06/7 6/08 15:42:54 59.8 5.9 37.4 28.6 06/16/0815:43:04 60.4 5.9 37.6 28.7 06/16/0815:43:14 60.1 5.9 37.7 28.7 06/16/0815:43:24 59.7 5.9 37.7 28.8 06/16/0815:43:34 59.5 5.9 37.7 28.8 0611610816:43:44 59.6 6.0 37.6 28.8 06116/0815:43:54 59.5 6.0 37.5 28.8
Stop Point #1 58.83 5.91 37.70 28.24


# 7 9

Page 56/16/08 StratifcatfOn Test

06/16/0815:44:04 53.2 5.3 37.0 28.4 06/1610815:44:14 58.0 5.5 37.1 28.6 06/1610815:44:24 59.5 5.9 36.9 28.6 06116/0815:44:34 59.7 4.4 36.6 28.7 06/16/0815:44:44 59.7 8.2 34.7 28.6 06/16/0815:44:54 57.2 3.5 22.1 28.3 06/16/0815:45:04 50.7 2.9 16.2 26.4 06/16/0815:45:14 41.6 2.7 19.7 22.0 06116/0815:45:24 33.0 2.3 22.3 16.0 06/16/0815:45:34 24.8 2.3 23.4 9.9 06116/0815:45:44 18.8 2.1 23.8 5.2 06116/0815:45:54 15.0 2.0 23.9 2.6 06116/0815:46:04 11.5 2.0 23.9 1.2 06116/0815:46:14 8.8 1.9 23.6 0.5 06116/0815:46:24 6.9 1.8 

### 23.8 0.2 06/16108 15:46:34 5.6 2.0 

### 23.7 0.1 25 ppm NOx 06116/08 15:46:44 4.2 1.8 

### 23.8 0.1 Zero CO
06/1610815:46:54 3.2 1.8 

### 23.8 0.0 06/16/0815:47:04 2.4 1.5 23.7 0.0 06/16/0815:47:14 1.6 3.0 23.6 0.0 06116/0815:47:24 1.2 4.9 19.8 0.0 06116/0815:47:34 0.8 5.0 10.1 0.2 06/16/0815:47:44 0.6 5.0 5.1 1.7 06116/0815:47:54 0.5 5.0 2.4 5.3 06116/0815:48:04 0.5 5.0 1.2 10.7 06116/0815:48:14 0.2 5.1 0.6 16.2 06/16/0815:48:24 0.1 5.1 0.4 20.3 06116/0815:48:34 0.0 5.0 0.3 22.9 06/16/0815:48:44 0.0 4.8 0.2 24.1 06/16/0815:48:54 0.0 4.9 0.2 24.7 06/16/0815:49:04 0.0 4.8 0.1 24.9 06/1610815:49:14 -0.1 4.8 0.1 25.0 06/1610815:49:24 

### -0.2 4.7 

### 0.1 25.1 06/16108 15:49:34 

### -0.4 4.7 

### 0.1 25.1 24.3 ppm CO 06/16108 15:49:44 

### -0.5 4.7 

### 0.1 25.1 Zero NOx 06116/0815:49:54 

### -0.5 2.1 

### 0.1 25.1 S02 0611610815:50:04 -0.8 2.1 0.1 25.1 06116/0815:50:14 -0.1 1.8 0.3 24.8 06/1610815:50:24 4.5 1.6 1.0 23.2 06116/08 15:50:34 15.2 1.6 1.4 19.5 06116/0815:50:44 28.7 1.5 1.6 14.3 06/16/0815:50:54 42.4 1.5 1.6 9.0 06/1610815:51:04 54.9 1.5 1.6 4.9 06/16/0815:51:14 65.2 1.5 1.7 2.5 06/1610815:51:24 72.2 1.5 1.7 1.2 0611610815:51:34 78.0 1.5 1.7 0.6 06/16/0815:51:44 82.7 1.5 1.6 0.3 06/16/0815:51:54 86.0 1.5 1.6 0.2 06/16/0815:52:04 88.1 1.5 1.6 0.1 06116/0815:52:14 89.6 1.5 1.6 0.1 06/16/0815:52:24 91.1 1.5 1.6 0.1 06/16/0815:52:34 92.1 1.5 1.6 0.1 06116/0815:52:44 92.9 1.5 1.6 0.1 06/16/0815:52:54 93.6 1.5 1.6 0.1 06/16/0815:53:04 94.0 1.5 1.6 0.1 06/1610815:53:14 94.4 1.5 1.5 01 06/1 fi108 15:53:24 94.9 1.5 1.5 0.1 06/1 6108 1 5:53:34 

### 95.0 1.6 1.5 0.1 06/16/08 15:53:44 

### 95.3 1.5 1.5 0.1 101 ppm S02 06/16/0815:53:54 

### 95.6 1.5 1.5 0.1 06116/0815:54:04 

### 95.9 1.3 1.6 0.1 06116/0815:54:14 95.9 1.8 1.5 0.1 06/16/0815:54:24 93.0 2.0 1.2 0.1 0611610815:54:34 83.2 2.2 0.6 0.1 06/16/0815:54:44 68.5 1.9 0.3 0.1 06/1610815:54:54 54.4 

### 0.4 0.1 0.1 06/16/08 15:55:04 42.9 

### 0.3 0.2 0.1 Zero Air 06/1610815:55:14 34.9 

### 0.2 0.1 0.1 06/16/0815:55:24 28.2 

### 0.1 0.0 0.1 06/16/0615:55:34 21.9 0.1 0.0 0.1 06116/0615:55:44 17.5 0.5 0.0 0.1

Page 6 

# 806116108 Strat'sficatioa Test

06/16/08 15:55:54 14.1 1.8 08/16108 15:56:04 10.9 2.0 06/16/08 15:56:14 8.3 2.3 06/16/0815:56:24 6.5 2.4 06/16/0815:56:34 4.9 2.4 06116/0815:56:44 3.8 2.4 0611610815:56:54 2.9 15.9 06/1610815:57:04 1.8 20.6 06l1610815:57:14 1.2 20.3 06116/0815:57:24 0.8 20.3 06/1610815:57:34 0.4 20.3 06/1610815:57:44 0.3 20.3 06/1610815:57:54 0.3 20.3 06116/0815:58:04 0.3 5.6 0.0 0.1 0.0 0.1 0.0 0.0 0.0 0.1 0.0 0.1 0.0 0.1 0.0 0.1 0.0 0.1 0.0 0.1 

### 0.0 0.1 20.2 ppm CH4
0.0 0.1 0.0 0.1 0,0 0.1 0.0 0.1



## ~ ; Page 7

## Sheet1



# Summary of CO Analyzer Calibratsons and Bias

Plant: Daltile, EI Paso, TX Source: 

## Spray Dryer Date: 6/18I2008

AnaEyzer 

# Calibratrion Data

Cylinder Analyzer Absolute % Span Value Response Diff . erence Zero Gas

. 0 0.2 0.2 0.397614 Low Range 5.133 5.78 0.647 1.286282 Mid Range 24.3 25.3 1 1.988072 High Range 50.3 49.43 -0.87 -1.72962

System Calibration Bias and Drift Data



## Anaiyzer lnitial Values Final Values Drift 

# Average Calibration System Systern System System Calibration Response Calibration Calibration Calibration Calibrat' son Values Response Bias Response Bias

Run #1 Zero Gas 0.2 0.2 0 0.15 -0.0994 -0.0994 0.175

Upscale 25.3 24.6 -1.39165 24.5 -1.59046 -0.19881 24.55 Average CO Concentration: 1 Corrected CO Concentration: 0.822462

Run #2 Zero Gas 0.2 0.15 -0.0994 0.15 -0.0994 0 0.15

Upscale 25.3 24.5 -1.59046 24.5 -1.59046 0 24.5
Average CO Concentration: 0.94 Corrected CO Concentration: 0.788378

Run #3 Zero Gas 0.2 0.15 -0.0994 0.12 -0.15905 -0.05964 0.135

Upscale 25.3 24.5 -1.59046 24.35 -1.88867 -0.29821 24.425
Average CO Concentration: 0.77 Corrected CO Concentration: 0.635261

Page 1 

# 82

## Sheetl



# Summary of NOx Anatyzer Calibrations and Bias

Plant: 

## Daltile, Dallas, TX Source: 

## Spray Dryer Date: 

## 6/18/2008

Analyzer Calibratrion Data



## Cy(inder Analyzer Absolute % 

## Span Value Response Difference Zero Gas 0 0 0 0 Low Range 5.133 5.08 -0.053 -0.10291 Mid Range 25 25 0 0 High Range 51.5 51.45 -0.05 -0.09709

System Calibration Bias and Drift Data



## Analyzer Initial Values Finai Values Drift Average Calibration System System System System Calibration Response Calibration Calibration Calibration Calibration Values

Response Bias Response Bias

Run #'f Zero Gas 0 0 0 0 0 0 0

Upscale 25 23.3 -3.30097 23 -3.8835 -0.58252 23.15
Average NOx Concentration: 10.74 Corrected NOx Concentration: 11.59827

Run #2 Zero Gas 0 0 0 0 0 0 0

Upscale 25 23 -3.8835 22.88 -4.1165 -0.23301 22.94
Average NOx Concentration: 11.28 Corrected NOx Concentration: 12.29294

Run #3 Zero Gas 0 0 0 0 0 0 0

Upscale 25 22.88 -4.1165 22.6 -4.66019 -0.54369 22.74
Average NOx Concentration: 11.98 Corrected NOx Concentration: 13.17062

Page 1 

# 836118/08 Calibrations



### Oate/Time VOC CO NOx 

### mmldd/yy hh:mm:ss 

### ppm ppm ppm 06/18/08 08:45:14 2.1 0.4 0.0 06118/08 08:45:24 2.1 0.4 0.0 06118/08 08:45:34 2.0 0.4 

### 0.0
06/18/08 08:45:44 2.0 0.4 

### 0.0
06118/08 08:45:54 2.0 0.4 

### 0.0
Ofil18/08 08:46:04 2.0 0.4 0.0 06/18/08 08:46:14 2.0 0.4 0.0 06118/08 08:46:24 2.1 0.4 0.0 06J18/08 08:46:34 2.1 0.4 0.0 06118J08 08:46:44 2.1 0.4 4.7 06/18108 08:46:54 2.1 0.5 47.8 06/18108 08:47:04 2.0 0.5 50.7 06/18108 08:4714 2.1 0.4 51.0 06/18108 08:47:24 2.1 0.4 51.2 06/18/08 08:47:34 1.9 0.4 51.4 06/18/08 08:47:44 2.0 0.3 51.6 06118/08 08:47:54 2.0 0.2 51.1 06118/08 08:48:04 2.0 0.3 51.3 06/18/08 08:48:14 2.0 0.3 51.3 06118108 08:4824 1.8 0.3 

### 51.5
06/18/08 08:48:34 1.8 0.3 

### 51.4
06/18/08 08:48:44 1.8 0.3 

### 51.5
06/18/08 08:48:54 1.8 0.3 

### 51.4 06118/08 08:49:t34 1.7 03 41.5 06118/08 08:49:14 1.7 0.2 1.0 06118/08 08:49:24 1.7 0.2 0.3 06118108 08:49:34 1.7 0.2 3.7 06118108 08:49:44 1.7 0.3 24.8 06/18108 08:49:54 1.7 0.3 25.1 06118/08 08:60:04 1.7 0.3 25.0 06/18/08 08:50:14 1.7 0.2 25.0 06l18/08 08:50:24 1.8 

### 0.2 25.0
06/18/08 08:50:34 1.7 

### 0.2 25.0
06118108 08:50:44 1.8 

### 0.2 25.0
06118/08 08:50:54 1.7 

### 0.2 25.0 06118/08 08:51:04 1.7 0.1 1.3 06/18108 08:51:14 1.7 0.1 0.1 06/18108 08:51:24 1.7 0.2 0.1 06/18108 08:51:34 1.6 0.2 4.9 06/18/08 08:51:44 1.5 0.3 5.1 06118108 08:51:54 1.6 0.2 5.0 06/18108 08:52:04 1.6 0.2 

### 5.1
06/18/08 08:52:14 1.5 0.1 

### 5.1
06118/08 08:52:24 1.8 0.1 

### 5.0
06/18/08 08:52:34 1.5 0.1 5.1 06118108 08:52:44 1.6 0.1 5.0 0n"l18/08 08:52:54 1.6 0.1 5.0 06118/08 08:53:04 1.5 0.1 0.4 06118108 08:53:14 1.5 0.1 0.0 06/18/08 08:53:24 1.5 0.3 0.1 06/18/08 08:53:34 1.5 3.6 0.0 06118/08 08:53:44 1.5 12.9 0.0 06118/08 08:53:54 1.5 25.8 0.0 06118108 08:54:04 1.5 37.3 0.0 46/18/08 08:54:14 1.5 44.4 0.0 06/18/08 08:54:24 1.5 47.5 0.0 06/18/08 08:54:34 1.5 48.5 0.0 06/18/08 08:54:44 1.5 48.8 0.0 06118/08 08:64:54 1.5 48.8 0.0 06/18/08 08:55:04 1.5 49.0 0.0 06118108 08:55:14 1.5 49.4 0.0 06118/08 08:55:24 1.5 49.4 0.0 06/18/08 08:55:34 1.5 

### 49.4 0.0 06/18/08 08:55:44 1.5 

### 49.4 0.0 06/18/08 08:55:54 1.5 

### 49.4 0.0 06/18/08 08:56:04 1.5 

### 49.5 0.0 06118108 08:56:14 1.5 49.4 0.0 Zero NOx

51.5 ppm NOx

25.5 ppm NOx Zero CO

5.133 

### ppm NOx

50.3 

### ppm CO

Page 1 

# 846118/08 Calibrations

06118108 08

~ 6:24 1.5 48.5 0.0 06/18108 08:56:34 1.5 42.7 0.0 06/18108 08:56:44 1.5 31.6 0.0 06l18/08 08:56:54 1.5 21.8 0.0 08/18/08 0B:57:04 1.5 17.9 0.0 06/18/08 08:57:14 1.5 19.2 0.0 06/18108 08:57:24 1.5 22.1 0.0 06/18/08 08:57:34 1.5 24.1 0.0 OS11 Bl08 0B:57:44 1.5 25.0 0.0 06/18/08 08:57:54 1.5 25.2 0.0 06/18/08 08:58:04 1.5 25.3 0.0 06118/08 08:58:14 1.5 25.3 0.0 05/18108 08:58:24 1.8 25.3 0.0 06118/08 08:58:34 1.5 25.3 0.0 06/18/08 08:58:44 1.5 25.3 0.0 06118/08 08:58:54 1.5 25.3 0.0 06/18/08 08:59:04 1.5 24.0 0.0 06/18/08 08:59:14 1.5 19.7 0.0 06/18/08 08:59:24 1.5 13.4 0.0 06118/08 08:59:34 1.5 8.2 0.0 06118/08 08:59:44 1.5 5.9 0.0 06/18/08 08:59:54 1.4 5.5 0.0 06/18108 09:00:04 1.5 5.7 0.0 06/18/08 09:00:14 1.5 5.8 0.0 06118108 09:00:24 1.5 5.8 0.0 06/18108 09:00:34 1.5 5.8 0.0 06118108 09:00:44 1.5 5.8 0.0 06/18/08 09:00:54 1.5 5.7 0.0 06118/08 09:01:04 1.5 5.7 0.0 06118/08 09:01:14 1.5 5.7 0.0 06118/08 09:0124 1.3 5.3 0.0 06/18/08 09:01:34 1.3 4.2 0.0 06118/08 09:01:44 1.3 2.8 0.0 06/18/08 09:01:54 1.3 1.6 0.0 06/18108 09:02:04 1.2 0.9 0.0 06/18/08 09:02:14 1.2 0.5 0.0 06/18J08 09:02:24 1.0 0.4 0.0 06118/08 09:02:34 0.0 0.4 010 06118108 09:02:44 0.1 0.4 0.0 06118/08 09:02:54 0.1 0.3 3.8 06J18/08 09:03:04 0.1 0.3 10.0 06/18/08 09:03:14 0.1 0.3 14.1 06/18/08 09:03:24 0.1 0.3 17.0 06/18108 09:03:34 0.1 0.3 18.8 06/18/08 09:03:44 0.1 0.3 20.1 06118108 09:03:54 0.1 0.3 21.0 06118/08 09:04:04 0.1 0.3 21.8 06118/08 09:04:14 0.0 0.3 22.3 06118108 09:04:24 0.1 0.2 22.7 06/18108 09:04:34 0.1 0.2 22.9 06/18J08 09:04:44 0.1 0.3 23.1 06/18/08 09:04:54 0.1 0.2 23.1 06/18/08 09:05:04 0.1 0.2 23.2 06/18/08 09:05:14 0.1 0.2 23.3 06/18/08 09:05:24 0.1 

### 0.2 23.3 06/18/08 09:05:34 0.0 0.2 23.3 06118/08 09:05:44 0.1 0.2 23.3 06118108 09:05:54 0.1 0.2 23.3 06118108 09:06:04 0.7 02 233 06/18108 09:06:14 2.2 0.2 23.4 06118/08 09:06:24 23 0.2 22.8 06118/08 09:06:34 2.3 0.2 18.0 06/18/08 09:06:44 2.3 0.7 10.6 06/18/08 09:06:54 2.4 2.6 6.0 06/18108 09:07:04 2.3 6.3 3.9 06/18/08 09:07:14 2.3 11.1 2.7 06/18/08 09:07:24 2.3 15.5 2.1 06/18/08 09:07:34 2.4 18.7 1.6 06/18/08 09:07:44 2.4 20.7 1.2 06118108 09:07:54 2.3 22.0 0.9 06/18/08 09:08:04 2.4 22.7 0.7 24.3 ppm CO

5.09 ppm CO

25.1 ppm Bias Zero CO Bias

Page 2 

# m6/18/08 Calibrations

06118108 09:08:14 2.4 23.2 0.5 06/18108 09:08:24 2.4 23.6 0.3 06/18/08 09:08:34 2.4 23.9 0.3 06/18108 09:08:44 2.3 24.1 0.2 06/18108 09:08:54 2.3 24.3 0.1 06118/08 09:09:04 2.4 24.4 0.1 06/18/08 09:09:14 2.5 24.5 0.0 06/18108 09:09:24 2.5 24.5 0.1 06118108 09:09:34 2.4 24.5 0.0 06118/08 09:09:44 2.7 24.5 0.0 06/18108 09:09:54 2.5 24.5 0.0 06118/08 09:10:04 1.8 

### 24.6 0.0 06/18108 09:10:14 0.5 

### 24.6 0.0 24.3 ppm CO Bias 06/18/08 09:10:24 0.1 

### 24.6 0.0 Zero NOx Bias 06118108 09:10:34 0.1 

### 24.5 0.0
06l18108 09:10:44 

### 0.1 23.6 0.0 D6118/08 09:10:54 

### 0.1 21.2 0.0 Zero AIr 06118108 09:11:04 

### 0.1 17.5 0.0 06/18108 0911:14 

### 0.1 13.0 0.0 06118/08 09:11:24 0.3 8.8 0.0 06118108 09:11:34 0.3 5.7 0.0 06118/08 09:11:44 0.3 3.7 0.0 06118/08 09:11:54 0.6 2.5 0.0 06118108 09:12:04 5.4 1.8 0.0 06118/08 09:12:14 18.8 1.5 0.0 06/18/08 09:12:24 19.0 1.3 0.0 06/18/08 09:12:34 19.0 1.1 0.0 06118108 09:12:44 19.2 1.0 0.0 06/18108 09:12:54 19.2 1.0 0.0 06/18/08 09:13:04 19.3 0.9 0.0 06118/08 09:13:14 19.7 0.9 0.0 06118/08 09:13:24 

### 20.2 0.8 0.0 06/18/08 09:13:34 

### 20.2 0.9 0.0 20.2 ppm CH4 06l18/08 09:13:44 

### 20.2 0.8 0.0 06118108 D9:13:54 

### 20.1 0.8 0.0 06l18/08 09:14:04 20.2 0.7 0.0 06118/08 09:14:14 11.4 0.7 0.0 06/18/08 09:14:24 2.3 0.6 0.0 06118/08 09:14:34 2.2 0.6 0.0 06118/08 09:14:44 2.1 0.6 0.0 06/18/08 09:14:54 2.0 0.5 0.0 06/18/08 09:15:04 4.1 0.5 0.0 06118/08 09:15:14 5.4 0.5 0.0 06/18/08 09:15:24 5.1 0.5 0.0 06118/08 09:15:34 

### 5.0 0.4 0.0 06/18/06 09:15:44 5.1 0.4 0.0 5.142 ppm CH4 06118108 09:15:54 

### 5.1 0.4 0.0 06118/08 0916:04 

### 5.0 0.4 0.0 06118l08 09:16:14 5.0 0.3 0.0 06/18/08 09:16:24 5.0 0.3 0.0 06/18/08 09:16:34 3.1 0.3 0.0 D6118/08 09:16:44 2.1 0.3 0.0 06l18108 09:16:54 2.0 0.3 0.0 06/18/08 09:17:04 2.0 0.3 0.0 06118/08 09:17:14 27.2 0.3 0.1 06/18108 09:17:24 41.8 0.3 0.1 06/18/08 09:17:34 41.8 0.3 0.1 06/18/08 09:17:44 42.0 0.3 0.1 06/18/08 09:17:54 

### 42.2 0.3 0.1 06/18108 09:18:04 

### 42.1 0.3 0.1 41 ppm CH4 06/18108 09:18:14 

### 42.1 0.3 0.1 06/18108 09:18:24 

### 42.1 0.3 0.1 06118/08 09:18:34 35.1 0.4 0.1 06J18108 09:18:44 2.8 0.4 0.0 06/18/08 09:18:54 2.0 0.4 0.0

Page 3 

# 86

## 6181VOX

DatelTime NOx mmldd/yy hh:mm:ss ppm 06/18/08 09:21:18 -0.01893 06118108 09:22:18 2.104858 06I18108 09:23:18 26.06837 06/18/08 09:24:18 26.15283 06/18/08 09:25:1 8 26.18213 06/18/08 09:26:18 26.24219 06118/08 09:27:18 26.21729 06118/08 09:28:18 26.20899 06/18/08 09:29:18 26.2251 06/18/08 09:30:18 26.20508 06118/08 09:31:18 26.21778 06/9 8/08 09:32:1 8 26.1836 06118/08 09:33:18 26.23145 06l18l08 09:34:18 26.19532 06/18J08 09:35:18 26.22754 06/18/08 09:36:18 26.19581 06/18/08 09:37:18 26.21192 06/18I08 09:38:1 8 26.17091 06118/08 09:39:18 26.17677 06l18/08 09:40:18 26.20313 06118108 09:41:18 26.15089 06/18f08 09:42:18 26.1836 06118/08 09:43:1 8 26.13233 06118108 09:44:18 26.18849 06!1 8108 09:45:18 26.15138 06/18/08 09:46:18 26.14601 06l18/08 09:47:18 26.16114 06/18/08 09:48:18 26.13478 06!1 8108 09:49:18 26.13966 06/18l08 09:50:18 26.12062 06118/08 09:51:18 26.07472 06118/08 09:52:18 26.13527 06/18/08 09:53:18 26.11622 06118/08 09:54:18 5.877933 Start CQnverter Check

Stop Converter Check

Page 1 

# am

### 6118l08 Run #1

Date/Time VOC CO NOx mmldd/yy hh:mm:ss ppm ppm ppm 06/18108 10:05:57 6.2 1.1 11.3

start Run #1 06118108 10:06:07 6.0 1.0 11.3 06118l0810:06:17 6.0 1.1 11.3 06118/08 10:06:27 6.1 1.1 11.2 06118l0810:06:37 5.8 1.1 11.3 06/18/08 10:06:47 5.9 1.0 11.3 0&l1810810:06:57 6.0 1.0 11.3 06118/08 10:07:07 5.9 1.0 11.3 0611810810:07;17 6.2 1.0 11.4 0611810810:07:27 6.4 1.0 11.3 06/1810810:07:37 6.4 0.9 11.2 06/18/08 10:07:47 6.3 1.0 11.2 06/1810810:07:57 6.1 1.0 11.3 06118/0810:08:07 6.6 1.0 11.3 06/18108 10:08:17 6.3 1.0 11.3 06118/08 10:08:27 5.9 1.0 11.3 06118108 10:08:37 5.8 1.1 11.4 06118/0810:08:47 6.0 1.1 11.4 0611810810:08:57 5.6 1.1 11.4 06/18/0810:09:07 5.5 1.1 11.5 06118/0810:09:17 5.4 1.0 11.4 06118/0810:09:27 5.4 11 11.6 06/18/0810:09:37 5.4 1.1 11.4 06118/0810:09:47 5.4 1.1 11.4 06118I0810:09:57 5.5 1.1 11.4 06118/0810:10:07 5.6 1.1 11.4 06118/0810:10:17 5.4 1.1 11.4 06118/0810:10:27 5.5 1.1 11.3 06118/0810:10:37 5.4 1.1 11.3 06/18/0810:10:47 5.5 1.1 11.3 06118/0810:10:57 5.3 1.1 11.2 06118/0810:11:07 5.5 1.1 11.3 06/18/0810:11:17 5.5 1.1 11.3 06118l0810:11:27 5.3 1.1 11.3 00118/08 10:11:37 5.5 1.1 11.3 06118/08 10:11:47 5.5 1.1 11.3 06118f0810:11:57 5.3 1.1 11.3 06/1810810:12:07 • 5.3 1.1 11.3 06118/0810:12:17 5.3 1.1 11.3 0611810810:12:27 5.6 1.1 11.3 0611810810:12:37 5.4 1.1 11.2 06118/0810:12:47 5.3 1.1 11.2 Ofi11810810:12:57 5.2 1.1 11.2 06/18/08 10:13:07 5.3 1.1 11.2 06/18J0810:13:17 5.3 1.1 11.2 06/38/0810:13:27 5.3 1.1 11.2 06118l0810:13:37 5.2 1.1 11.2 06118/0810:13:47 5.1 1.1 11.2 06.'18/0810:13:57 5.1 1.1 11.2 06/18108 10:14:07 5.0 1.1 11.2 06l18/08 10:14:17 5.0 1.1 11.3 08118/0810:14:27 5.0 1.1 11.3 06118/08 10:14:37 5.0 1.2 11.2 06/18/0810:14:47 5.0 1.1 11.2 06l18/0810:14:57 5.0 1.0 11.3 06/18/08 10:15:07 5.1 1.0 11.2 06118/08 10:15:17 5.3 1.0 11.3 06/18/08 10:15:27 5.2 1.0 11.4 06l18/0810:15:37 5.0 0.9 11.4 06/18108 10:15:47 4.9 1.0 11.3 06/18108 10:15:57 5.0 1.0 11.4 06/18/08 10:16:07 5.0 0.9 11.4 06/18/08 10:16:17 4.8 1.0 11.4 06/18/08 10:16:27 4.8 1.0 11.4 06/18/08 10:16:37 4.7 1.0 11.5 06118/08 10:16:47 4.7 1.1 11.4 06118/08 10:16:57 4.7 1.1 11.4 0611810810:17:07 4.8 1.1 11.4 06/18l08 10:17:17 4.6 1.0 11.5 06118/08 10:17:27 4.5 1.0 11.4

Page 1 ~ ~ 

# i E6/18/08 Run #1

06118/08 10:17:37 4.5 1.1 11.4 06/1810810:17:47 4.4 1.0 11.4 06/18108 10:17:57 4.4 1.0 11.4 06/18/08 10:18:07 4.4 1.0 11.3 08118/0810:18:17 4.4 0.9 11.3 06118/0810:1827 4.4 0.9 11.4 06/18/0810:18:37 4.5 1.0 11.3 06118i0810:18:47 4.5 1.0 11.4 06/18/0810:18:67 4.4 1.0 11.3 06/18/0810:19:07 4.4 1.0 11.3 06/18108 10:19:17 4.2 1.1 11.3 06/18/08 10:19:27 4.4 1.1 11.3 06118108 10:19:37 4.4 1.0 11.3 06/18/0810:19:47 4.1 0.9 11.3 06118108 10:79:57 4.1 1.0 11.3 06/18J0810:20:07 4.1 1.0 11.4 06/18/0810:20:17 4.1 1.0 11.3 06/18/0810:20:27 4.1 1.1 11.3 06/18108 10:20:37 4.1 1.1 11.3 0611810810:20:47 4.0 1.1 11.4 06/18/0810:20:57 0.2 -2.5 7.7 0611810810:21:07 2.5 -0.4 9.8 0611810810:21:17 2.5 0.0 10.1 06/18/08 10:21;27 4.4 1.1 11.2 06/1810810:21:37 4.4 1.0 11.3 06118J0810:21:47 4.2 11 11.4 06/18J081021:57 4.4 1.1 11.4 06118/08 10:22:07 4.1 1.1 11.3 06/18/0810:22:17 4.1 1.1 11.3 06/18l0810:2227 4.1 1.1 11.3 06/18/08 10:22:37 4.1 1.1 11.4 06/1810810:22:47 4.1 1.1 11.4 06/18/0810:22:57 3.9 1.1 11.5 06118/0810:23:07 3.8 1.1 11.4 06/18108 10:23:17 4.1 1.1 11.4 06/18108 10:23:27 4.1 1.0 11.4 0611810810:23:37 4.1 1.0 11.4 06/1810810:23:47 4.1 1.1 11.4 O6/1810810:23:57 4.2 1.1 11.4 06/1810810:24:07 4.1 1.1 11.4 06/18/0810:24:17 4.2 1.1 11.5 06/18/08 10:24:27 4.0 • 1.1 11.5 061181081024:37 3.8 1.1 11.6 06118/08 10:24:47 3.8 1.0 11.5 06/18/0810:24:57 3.8 1.0 11.5 06/18/0810:25:07 3.9 1.0 11.6 06/18/0810:25:17 3.8 1.0 11.6 06/1810810:25:27 4.1 1.0 11.6 06/18108 10:25:37 4.0 1.0 11.6 06/18/0810:25:47 3.8 1.1 11.6 06118/0810:25:57 4.0 1.0 11.5 06118/0810:26:07 4.0 1.0 11.5 06118/08 10:26:17 4.0 1.1 11.5 06118/0810:26:27 4.1 1.0 11.5 06/18/0810:26:37 3.9 0.9 11.5 06/18/081026:47 3.8 1.0 11.6 06/1810810:26:57 3.8 1.1 11.5 06/18108 10:27:07 3.8 1.1 11.6 06118108 10:27:17 3.8 1.1 11.6 06118/0810:27:27 4.0 1.1 11.6 06/1810810:27:37 3.8 1.1 11.6 0611810810:27:47 3.8 1.1 11.6 06/18/08 10:27:57 4.0 1.1 11.5 06/1810810:28:07 4.1 1.1 11.5 06/18/0810:28:17 4.0 1.1 11.4 06/18/081028:27 3.8 1.1 11.4 06/18/0810:28:37 3.8 1.1 11.4 06118/08 10:28:47 4.0 1.1 11.4 06/1810810:28:57 3.8 1.1 11.4 06/18/0810:29:07 3.8 1.1 11.4 06/18108 10:29:17 3.8 1.1 11.4 06/1810810:29:27 3.8 1.1 11.4 06/18108 10:29:37 3.8 1.0 11.5 06/18/0810:29:47 3.7 1.0 11.5



### Page 2 

# ~6/18/08 Run #1

06/18/0810:29:57 3.5 0.9 11.5 06/18/0810:30:07 3.6 1.0 11.5 06118/0810:30:17 3.5 1.0 11.5 06118/0810:30:27 3.5 1.0 11.4 08118/0810:30:37 3.5 0.9 11.4 0611810810:30:47 3.5 0.9 11.4 06/1810810:30:57 3.5 0.9 11.5 06/18108 10:31:07 3.5 0.8 11.4 06l1810810:31:17 3.4 0.9 11.4 06/18/0810:31:27 3.5 0.9 11.4 06/1810810:31:37 3.6 0.8 11.4 06/1810810:31:47 3.5 0.9 11.4 06/18108 10:31:57 3.5 0.9 11 A 06/1810810:32:07 3.5 0.9 11 A 06/18108 10:32:17 3.4 0.9 11.4 06/18/08 10:32 :27 3.4 1.0 11.3 06/18/0810:32:37 3.2 0.9 11.3 06118/0810:32:47 3.3 1.0 11.4 06/1810810:32:57 3.2 1.0 11.4 06118108 10:33:07 3.3 1.0 11.4 06/18/0810:33:17 3.3 0.9 11.4 0611810810:33:27 3.3 0.9 11.4 06/18/0810:33:37 3.3 0.9 11.5 0611810810:33:47 3.3 0.8 11.5 0611810810:33:57 3.3 0.8 11.5 0611810810:34:07 3.3 0.9 11.4 06118/0810:34:17 3.2 1.0 11.4 06/1810810:34:27 3.2 1.0 11.4 06/18/08 10:34:37 3.2 1.0 11.4 06/18l0810:34:47 3.2 0.9 11.5 0611810810:34:57 3.2 0.9 11.4 06/1810810:35:07 3.2 0.9 11.5 06118/0810:35:17 3.2 0.9 11.4 06118/0810:35:27 3.2 0.9 11.5 0611810810:35:37 3.3 0.9 11.4 06/18/0810:35:47 3.3 1.0 11.4 06118108 10:35:57 3.4 1.0 11.5
Port Chenge 06/18/0810:36:07 3.3 0.9 11.5 06/18/0810:36:17 3.2 0.9 11.4 06/18/0810:36:27 3.2 0.9 11.4 06/1810810:36:37 3.2 0.9 11.4 06/1810810:36:47 3.3 0.9 11.4 06/18/0810:36:57 3.2 0.9 11.5 06/18108 10:37:07 3.2 1.0 11.5 06118108 10:37:17 3.2 0.9 11.4 06118/0810:37:27 3.3 0.9 11.4 06/18/0810:37:37 3.1 0.9 11.4 06/1810810:37:47 3.2 1.0 11.4 06118/0810:37:57 3.0 0.9 11.4 06/18/0810:38:07 3.1 0.9 11.4 06/18/0810:38:17 3.2 0.9 11.4 06118/0810:38:27 3.0 0.9 11.1 06118/0810:38:37 3.0 0.9 10.2 06/18/0810:38:47 3.0 0.9 10.2 06118/0810:38:57 3.0 0.8 10.6 0611810810:39:07 3.0 0.8 10.9 0611810810:39:17 3.0 0.8 11.0 0611810810:39:27 3.0 0.8 11.1 06/1810810:39:37 3.0 0.9 11.0 0611810810:39:47 3.0 0.9 11.1 0611810810:39:57 3.0 0.9 11.2 06118/08 10:40:07 3.1 0.9 11.2 06118/08 10:40:17 3.0 0.9 11.3 06118/0810:40:27 3.0 1.0 11.3 06118/0810:40:37 3.0 1.0 11.4 06/18f0810:40:47 2.9 0.9 11.3 06/18/0810:40:57 3.0 0.9 11.3


### Resume 06118/08 10:41:07 3.0 0.9 11.2 06118108 10:41:17 2.9 0.9 11.2 06/18/0810:41:27 2.9 0.9 11.2

Page 3 

# 116/18/08 Run #1

06118/08 10:41:37 3.0 0.9 11.2 0611810810:41:47 3.0 0.9 11.2 0611810810:41:57 3.0 1.0 11.2 06/1810810:42:07 3.0 0.9 11.1 06/18/0810:42:17 3.0 1.0 11.0 0611810810:42:27 3.0 1.0 11.0 06118/0810:42:37 2.9 0.9 11.0 06/18J0810:42:47 2.9 0.9 10.9 06118/0810:42:57 2.9 0.9 10.8 06/18/0810:43:07 2.7 0.9 10.8 06/1810810:43:17 2.9 0.9 10.7 06118/0810:43:27 3.0 0.9 10.7 0611810810:43:37 2.8 0.9 10.7 06118/0810:43:47 2.8 0.9 10.7 0611810810:43:57 2.7 1.0 10.7 06/1810810:44:07 3.0 0.9 1016 06/1810810:44:17 3.0 0.8 10.5 06/18/0810:44:27 3.0 0.9 10.5 06118/08 10:44:37 2.9 1.0 10.6 06/18/0810:44:47 2.8 0.9 10.6 06/18/0810:44:57 2.9 0.9 10.6 06/18/08 10:45:07 2.7 0.9 10.6 06/18/0810:45:17 2.6 0.9 10.5 06/18/0810:45:27 2.7 0.9 10.5 06118/0810:45:37 2.7 0.9 10.5 06118/08 10:45:47 2.7 1.0 10,6 06/1810810:45:57 2.7 0.9 10.5 06/1810810:46:07 2.7 0.8 10.6 06/18/0810:46:17 2.8 0.8 10.6 06/1810810:46:27 2.7 0.8 10.6 06/18/0810:46:37 2.7 0.8 10.6 06/18/0810:46:47 2.7 0.9 10.5 06/18/0810:46:57 2.7 0.8 10.4 06/18/0810:47:07 2.7 0.8 10.4 06118/0810:47:17 2.7 0.9 10.4 06118/0810:47:27 2.6 0.9 10.5 0611810810:47:37 2.6 1.0 10.5 0611810810:47:47 2.7 0.9 10.6 06118/0810:47:57 2.6 0.9 10.4 0611810810:48:07 2.6 0.9 10.5 06118/0810:48:17 2.6 0.9 10.4 06/1810810:48:27 2.7 0.9 10.4 0611810810:48:37 2.6 0.9 10.4 06/18l0810:48:47 2.7 1.0 10.4 06/18/0810:48:57 2.7 1.0 10.4 06118/0810:49:07 2.7 1.0 10.4 06/18108 10:49:17. 2.6 1.0 10.4 0611810810:49:27 2.7 1.0 10.4 06/18/08 10:49:37 2.7 1.0 10.4 06118/0810:49:47 2.7 0.9 10.4 06118/0810:49:57 2.7 0.9 10.4 06118/0810:50:07 2.7 1.0 10.4 06/1810810:50:17 2.6 0.9 10.4 06118/0810:50:27 2.6 1.0 10.4 0611810810:50:37 2.6 1.0 .10.4 06118/0810:50:47 2.7 1.0 10.4 06118/0810:50:57 2.6 1.0 10.4 06/18/0810:51:07 2.5 1.0 10.3 06/18/08 10:51:17 2.3 1.0 10.4 06/18108 10:51:27 2.4 1.0 10.4 06118108 10:51:37 2.3 0.9 10.3 06/1810810:51:47 2.4 0.9 10.4 0611810810:51:57 2.6 0.9 10.3 06/1810810:52:07 2.6 1.0 10.3 06/1810810:52:17 2.5 0.9 10.3 06/1810810:52:27 2.5 0.9 10.2 06/18/0810:52:37 2.3 0.9 10.2 0611810810:52:47 2.5 0.9 10.2 06118/0810:52:57 2.4 0.9 10.3 06118108 10:53:07 2.4 1.0 10.3 06/1810810:53:17 2.5 1.0 10.2 06/18108 10:53:27 2.5 1.0 10.2 0611810810:53:37 2.4 1.0 10.2 06/1810810:53:47 2.5 0.9 10.2



### Page 4 

# 916118/08 Run #1

06/1810810:53:57 2.5 0.9 10.1 0611810810:54:07 2.4 4.0 10.1 0611810810:54:17 2.3 1.1 10.0 0611810810:54:27 2.3 1.1 10.1 06/18108 10:54:37 2.3 1.0 10.0 06118/0810:54:47 2.3 1.0 10.0 06118/08 1 0:54:57 2.3 1.1 10.1 06118/08 10:55:07 2.3 1.1 10.1 0611810810:55:17 2.4 1.1 10,0 06/18/08 10:55:27 2.3 1.1 10.0 06/1810810:55:37 2.3 1.1 10.0 06/1810810:55:47 2.3 1.2 10l1 06/18/08 10:55:57 2.3 1.2 101 0611810810:66:07 2.3 1.2 10.0 06118108 10:S6:17 2.3 1.3 10.0 06/181081

- 0:56:27 2.3 1.3 10.1 0611810810:56:37 2.3 1.3 10.0 06118/0810:56:47 2.4 1.3 10.0 06118108 10:56:57 2.3 1.3 10.0 06118/0810:57:07 2A 12 10.0 06118l0810:57:17 2.5 1.2 10.0 0611810810:57:27 2.4 12 10.0 0611810810:57:37 2.4 1.1 10.0 0611810810:57:47 2.4 1.1 10.0 06/18/0810:57:57 2.4 1.1 9.9 06118/08 1058:07 2.4 1.1 10.0 06/18/0810:58:17 2.3 1.1 10.0 06118/0810:58:27 2.3 1.1 10.0 06/1810810:58:37 2.4 1.1 10.0 06/1810810 58:47 2.3 1.1 10.0 06/1810810:58:57 2.2 1.4 9.9 06/1810810:59:07 2.4 1.1 9.9 06/18/0810:59:17 2.3 1.1 10.0 06l18108.10:59:27 2.3 1.1 9.9 06/1810810:59:37 2.3 1.1 9.9 06118/0810:59:47 2.3 1.0 9.9 08/1810810:59:57 2.3 1.1 10.0 06/18/0811:00:07 2.3 1.1 10.0 Ofil1810811:00:17 2.3 1.1 9.9 06/18l0811:00:27 2.3 1.1 9.9 0611810811:00:37 2.3 1.1 9.9 06/1810811:00:47 2.2 1.1 9.9 06/181081 '! :00:57 2.2 1.2 9.9 0611810811:01:07 2.2 1.2 9.8 06/18l081 'I :01:17 2.3 1.2 9.9 0611 8/08 1 1:01:27 2.4 1.2 9.9 06118/0811:01:37 2.4 7.2 9.9 06/18l0811:01:47 2.3 1.2 9.9 06/1810814 :01:57 2.3 1.2 9.9 06/1810811:02:07 2.3 1.2 9.9 06/1810811:02:17 2.3 1,2 10,0 0611810811:02:27 2.3 1.2 9.9 0611810811:02:37 2.3 1.2 9.9 0611810811:02:47 2.3 1.2 9.9 0611 8108 1 1:02:57 2.3 1.2 9.9 06/18108 1 1:03:07 2.3 1.2 9.9 06/1810811:033:17 2.3 1.2 9.9 06/1810811:03:27 2.3 1.1 9.8 06/1810811:03:37 2.2 1.1 9.8 0611810811:03:47 2.0 1.1 9.8 06/1810811:03:57 2.0 1.1 9.8 06l18/0811:04:07 2.0 1.0 9.8 06/18108 11:04:17 2.1 1.0 9.8 06/1810811:04:27 2.3 1.0 9.7 06118/0811:04:37 2.0 1.0 9.7 0611810811:04:47 2.0 1.1 9.8 06118/0817:04:57 2.0 , 1.1 9.8 06118/08 11:05:07 2.1 1.1 9.8 0611 8108 1 1:05:17 2,0 1.1 9.7 0611810811:05:27 2.1 1.1 9.8 06f18/0811:05:37 2.0 1.1 9.7 06118/0811:05:47 2.1 1.1 9.7 0611 8108 1 1:05:57 2.1 1.1 9.7 0611810811:06:07 2.4 1.0 9.7



### Page 5 

# Q ~6/18108 Run 91

06118108 11:06:17 2.2 1.1 9.7 06/1810811:06:27 2.2 1.1 9.7 06/1810811:06:37 2.0 1.1 9.7 06/1810811:06:47 2.1 1.1 9.7 06118/0811:06:57 2.1 1.1 9.6 06118/0811:07:07 2.0 1.1 9.6 06/18/0811:07:17 2.0 1.1 9.6 06/18/0811:07:27 2.0 1.1 9.6 06118/0811:07:37 2.0 1.1 9.6 06118/0811:07:47 2.0 1.1 9.6 06/18/0811:07:57 2.0 1.1 9.6 0611810811:08:07 2.0 1.0 9.6 0611810811:08:17 2.0 0.9 9.6 O6l1810811:08:27 2.0 0.9 9.6 06/1810811:08:37 2.0 1.0 9.6 06/18J0811:08:47 2.0 1.0 9.6 06/1810811:08:57 2.0 1.0 9.6 0611810811:09:07 2.1 1.1 9.6 06/18/0811:09:17 2.1 1.1 9.6 06118/0811:09:27 2.0 1.1 9.6 06/18/0811:09:37 2.0 1.1 9.6 06/18/0811:09:47 2.0 1.0 9.6 06/18/0811:09:57 2.0 1.0 9.6 06/18/0811:10:07 2.1 1.0 9.6 06/18/0811:10:17 2.0 1.0 9.5 0611810811:10:27 2.0 1.0 9.6 0611810811:10:37 2.1 1.0 9.6 06/18/0811:10:47 2.1 1.1 9.6 0611810811:10:57 2.0 1.1 9.6
Stap Run 01 3.41 1.00 10.74

06/18/0811:11:07 2.0 1.1 9.6 06/1810811:11:17 2.1 1.1 9.5 06118/0811:11:27 2.3 1.0 9.5 0611810811:11:37 2.3 0.9 9.5 0611810811:11:47 4.3 0.9 9.1 0611810811:11:57 5.3 0.9 7.0 0611810811:12:07 4.4 0.9 4.8 06118/0811:12:17 4.3 0.8 2.9 06118/0811:12:27 4.1 1.2 1.9 06/1810811:12:37 4.1 2.9 1.3 06/1810811:12:47 4.1 5.9 0.9 06/1810811:12:57 3.8 10.0 0.6 06118/0811:13:07 3.8 14.0 0.5 06/18/0811:13:17 3.8 17.3 0.3 06/1810811:13:27 3.8 19.7 0.2 06/18/0811:13:37 3.8 21.3 0.2 06118/0811:13:47 3.8 22.5 0.1 06/18/0811:13:57 3.8 23.2 0.1 06118/0811:14:07 3.6 23.7 0.1 06/18108 11:14:17 3.6 24.1 0.1 06/1810811:14:27 3.5 24.3 0.1 06/18/0811:14:37 3.5 24.3 0.0 06/18/0811:14:47 3.5 24.4 0.0 06/1810811:14:57 3.5 24.4 0.0 06/18l0811:15:07 3.5 

### 24.5 0.0 06/18/08 11:15:17 3.2 

### 24.5 0.0 24.3 ppm CO 06118/08 11:15:27 1.2 

### 24.5 0.0. Zero NOx 06/18/0811:15:37 0.6 

### 24.5 0.0 06/18/0811:15:47 0.3 24.4 0.9 06118/0811:15:57 0.3 23.7 6.6 06/18/0811:16:07 0.3 21.6 12.7 06/18108 11:16:17 0.3 17.9 16.0 06/18/0811:16:27 0.3 13.6 18.0 06118/08 11:16:37 0.1 9.7 19.8 06/18/08 11:16:47 0.1 6.7 21.2 06/1810811:16:57 0.1 4.5 22.0 06/18/08 11:17:07 0.1 3.1 22.5 06/18/0811:17:17 0.1 2.0 22.7 06/18/0811:17:27 0.1 1.3 22.8 061181081117:37 0.1 0.8 22.8 0611810811:17:47 0.1 0.5 22.9

Page 6 

# 9 3

### 6118/08 Run #1

06118l0811:17:67 0.1 0.3 23.0 0811 8108 1 1:18:07 

### 0.1 0.2 23.0 06118l0811:18:17 

### 0.1 0.2 23.0 25 pprn NOx 061'I 

### al0a 11:18:27 

### 0.1 0.1 23.0 Zero VOC, CO 06118r0811:1 8:37 0.1 

### 0.1 23.0 06/1810811:18:47 0.0 0.1 23.0 06/1810811:18:57 1.5 0.1 23.0 0611 B/0811:19:07 18.0 0.1 23.0 0611 8108 1 1:19:17 20.4 0.1 22.8 0611810811:19:27 

### 20.5 0.1 19.0 0611810a 11:19:37 

### 20.5 0.1 12.0 20.2 ppm CFi4 06118/0811:19:47 20.5 0.1 6.8 0611 8108 1 1:19:57 

### 20.5 0.1 3.9 06/1810811:20:07 20.8 0.2 2.3 0611 8108 11 :20:17 6.5 0.2 1.5



### PagB 7 

# 94.6/18108 Run 92

(7atelTime VOC CO NOx mm/dd/yy 

### hh:mm:ss ppm ppm ppm 0611810811:29:57 3.8 0.7 9.9

Start Run #2 0611810811:30:07 3.3 0.7 9.9 06/1810811:30:17 3.1 0.7 9.9 06/18/0811:30:27 3.0 0.7 10.0 06/18/0811:30:37 2.8 0.7 10.0 06/18/0811:30:47 2.7 0.7 10.0 06118108 '11:30:57 2.7 0.7 10.0 06118/0811:31:07 2.5 0.7 10.0 06/18/0811:31:17 2.4 0.7 10.1 06/1810811:31:27 2.9 0.7 10.1 06/18/0811:31:37 2.8 0.7 10.1 06118/0811:31:47 2.6 0.8 10.2 06/18/0811:31:57 2.4 0.7 10.2 0611810811:32:07 2.5 0.8 10.2 06118/08 11:32:17 2.4 0.7 10.2 0611810811:32:27 2.4 0.7 10.2 06118/0811:32:37 2.3 0.7 10.3 06/1810811:32:47 4.6 0.8 10.3 06/1810811:32:57 5.0 0.8 10.4 06118/0811:33:07 3.6 0.7 10.3 06/1810811:33:17 32 0.7 10.3 06118/0811:33:27 2.9 0.6 10.3 06/1810811:33:37 2.7 0.6 10.3 0611810811:33:47 2.7 0.6 10.4 06/18J0811:33:57 2.5 0.7 10.4 06/18/0811:34:07 2.4 0.7 10.4 06118/0811:34:17 2.3 0.7 10.4 06/1810811:34:27 2.3 0.7 10.3 06/18/0811:34:37 2.3 0.7 10.4 06/1810811:34:47 2.3 0.6 10.4 06/18/0811:34:57 2.4 0.6 10.4 06118/0811:35:07 2.3 0.6 10.3 06118108 11:35:17 2.3 0.7 10.4 06118/0811:35:27 2.6 0.7 10.4 08/1810811:35:37 2.7 0.7 10.4 0611810811:35:47 2.7 0.6 10.4 06/1810811:35:57 2.7 0.7 10.4 0611810811:36:07 2.7 0.7 10.4 06118/0811:36:17 2.6 0.7 10.4 06/18/0811:36:27 23 0.7 10.4 0611810811:36:37 2.4 0.7 10.4 06/18/0811:36:47 2.6 0.7 10.4 06/1810811:36:57 2.3 03 10.4 06/18/0811:37:07 2.3 0.7 10.4 06/18/0811:37:17 2.3 0.7 10.4 06/18/0811:37:27 2.3 0.8 10.5 06118/0811:37:37 2.4 0.7 10.5 06118/0811:37:47 2.4 0.7 10.6 06/18/0811:37:57 2.4 0.7 10.6 06118/0811:38:07 2.4 0.7 10.6 06/18/0811:38:17 2.4 0.8 10.7 06118/0811:38:27 2.4 0.7 10.7 06/18/0811:38:37 2.4 0.6 10.7 06118/0811:38:47 2.5 0.6 10.8 06/1810811:38:57 2.6 0.6 10.8 06118/0811:39:07 2.6 0.6 10.7 0611 8/08 1 1:39:17 3.0 0.6 10.7 0611810811:39:27 2.7 0.6 10.7 0611810811:39:37 2.7 0.6 10.7 0611810811:39:47 2.4 0.6 10.8 06/1810811:39:57 2.4 0.6 10.8 0611810811:40:07 2.4 0.6 10.8 0611 8/08 1 1:40:17 2.3 0.6 10.7 06118/0811:40:27 2.3 0.6 10.8 06118/0811:40:37 2.4 0.5 10.8 06/18/0811:40:47 2.3 0.5 10.8 06/18/0811:40:57 2.3 0.5 10.9 06118/0811:41:07 2.3 0.5 10.9 06118/08 11:41:17 2.3 0.5 1019 06/1810811:41:27 2.5 0.5 10.9

PacJe 1 

# 956/18106 Run #2

0611810811:41:37 2.6 0.5 11.0 06118/08 11:41:47 2.3 0.5 11.0 06/18/08 11:41 :57 2.3 0.5 10.9 0611810811:42:07 2.3 0.5 10.9 0611810811:42:17 2.3 0.5 10.9 06/1810811:42:27 2.3 0.5 10.9 06/1810811:42:37 2.3 0.5 10.9 06/1810811:42:47 2.3 0.5 10.9 0611810811:42:57 2.3 0.5 10.9 06118/0811:43:07 2.3 0.5 10.9 06118/08 11 :43:17 2.1 0.5 10.8 06118/0811:43:27 2.0 0.5 10.8 0611810811:43:37 2.0 0.5 10.9 0611810811:43:47 2.2 0.5 10.8 0611810811:43:57 2.3 0.5 10.8 06118/0811:44:07 2.1 0.5 10.8 06118/08 11:44:17 2.1 0.5 10.8 0611810811:44:27 2.0 0.5 10.8 06/1810811:44:37 2.0 0.5 10.8 0611810811:44:47 2.0 0.5 10.8 06/1810811:44:57 2.0 0.5 10.8 0611810811:45:07 2.0 0.5 10.8 06/18108 11:45:17 2.0 0.5 10.7 06/18/0811:45:27 2.0 0.5 10.8 0611 810811:45:37 2.1 0.5 10.8 06/1810811:45:47 2.0 0.5 10.8 06/1810811:45:57 2.1 0.5 10.8 06/ 1810811:46:07 2.1 0.5 10.8 06/18108 11:46:17 2.3 0.5 10.9 06118108 11:46:27 2.1 0.5 10.8 06118/0811:46:37 2.0 0.5 10.7 06/1810811:46:47 2.0 0.5 10.8 06118/0811:46:57 2.3 0.5 10.9 06/18/08 11:47:07 2.1 0.5 10.9 06118/08 11:47:17 2.0 0.5 10.8 06118/08 11:47:27 2.1 0.5 10.8 06/18/08 11:47:37 2.1 0.5 10.8 06/18/0811:47:47 2.0 0.5 10.8 0611810811:47:57 2.0 0.5 10.8 0611 8108 1 1:48:07 2.0 0.5 10.8 06/18/08 11:48:17 2.0 0.5 10.9 06118/0811:48:27 2.0 0.5 10.9 0611 8108 1 1:48:37 2.1 0.6 10.9 06/18/08 11:48:47 2.1 0.5 10.8 06118/0811:48:57 2.0 0.5 10.8 06/1810811:49:07 2.0 0.5 10.8 06/18108 11:49:17 2.1 0.5 10.8 0611810811:49:27 2.1 0.5 10.8 06118108 11:49:37 2.1 0.5 10.9 06118/08 11:49:47 2.1 0.5 10.8 06/1810811:49:57 2.0 0.5 10.8 06118/0811:50:07 2.0 0.5 10.8 06118/08 11:50:17 2.0 0.5 10.8 0611810811:50:27 2.0 0.5 10.8 0611810811:50:37 2.0 0.5 10.8 0611810811:50:47 2.0 0.5 10.8 06118/0811:50:57 2.0 0.5 10.9 06118/08 11:51:07 2.0 0.5 10.8 06/18108 11:51:17 2.0 0.5 10.8 0611 8108 1 1:51:27 2.1 0.5 10.8 06118/0811:51:37 2.1 0.5 10.8 06118/0811:51:47 2.0 0.5 10.8 06118108 11:81:57 2.0 0.5 10.8 06/18/0811:52:07 2.0 0.5 10.7 0611810811:52:17 2.0 0.5 10.8 06/1810811:52:27 2.0 0.5 10.8 06/1810811:52:37 2.0 0.5 10.7 06118/0811:52:47 2.0 0.5 10.7 06/18/0811:52:57 2.0 0.5 10.7 06/1810811:53:07 2.0 0.5 10.8 0611810811:53:17 2.0 0.5 '10.8 06118/0811:53:27 2.0 0.5 10.8 06118108 11:53:37 2.0 0.5 10.7 06118/08 11:53:47 1.9 0.5 10.8

Page 2 i R6118108 Run #2

06/18/08 11:53:57 1.8 0.5 10.8 0611810811:54:07 1.7 0.5 10.8 061181D811:54:17 2.0 0.5 10.8 06118/0811:54:27 2.0 0.5 10.8 08/18/08 11:54:37 1.9 0.5 10.8 06118108 11:54:47 1.9 0.5 10.8 06/1810811:54:57 2.0 0.5 10.8 06/18/0811:55:07 2,0 0.5 10.7 0611810811:55:17 1.9 0.5 14.7 06/18/08 11 :55:27 1.7 0.5 10.7 06/1810811:55:37 1.9 0.5 10.7 06/18108 11:55:47 2.0 0.5 10.7 06/1810811:5S:57 1.9 0.5 10.7 06/1810811:56:07 1.9 0.5 10.6 06118/0811:56:17 1.9 0.5 10.7 0611810811:56:27 1.9 0.5 10.7 06118/0811:56:37 2.0 0.5 10.7 D611810811:56:47 2.0 0.5 10.7 0611810811:56:57 1.8 0.5 10.7 06118108 11:57:07 1.7 0.5 10.7 06/1810811:57:17 1.9 0.5 1 D.7 0811810811:57:27 2.1 0.5 10.8 06/18/08 11:57:37 1.8 0.5 10.7 06/18/08 11:57:47 1.7 0.5 10.7 06/18/08 11:57:57 1.7 0.5 10.8 O6l1810811:58:07 1.7 0.5 10.8 06/18/08 11:58:17 9.8 0.5 10.8 06118108 11:58:27 1.9 0.5 10.8 06/1810811:58:37 1.6 0.5 10.7 06/18108 11:58:47 1.8 0.5 10.7 06/18J0811:58:57 1.7 0.5 10.7 06/1810811:59:07 1.7 0.4 10.7 06/18108 11:59:17 1.9 0.4 10.7 06118108 11:59:27 1.9 0.5 10.7 06118/0811:59:37 1.7 0.5 10.7 O6l18/0811:59:47 1.7 0.5 10.7 06118/08 11:59:57 1.7 0.5 10.7
Port Change 06118108 12:00:07 1.7 0.5 10.7 06/1810812:00:17 1.7 0.5 10.8 06118J0812:00:27 1.8 0.5 10.8 0611810812:00:37 1.8 0.5 10.8 0611810812:00:47 1.9 0.5 10.8 06/1810812:00:57 2.0 0.5 10.9 06/18/08 12:01:07 1.7 0.5 10.8 06/18/08 12:01:17 1.7 0.5 9.7 06118/0812:01:27 1.7 0.5 8.3 06/18108 12:01:37 1:7 0.4 8.7 06118108 12:01:47 1.7 0.4 9.6 06118108 12:01:57 1.8 0.4 10.2 0611810812:02:07 1.7 0.4 10.5 06/1810812:02:17 1.7 0.4 10.7 06M 8l08 12:02:27 1.7 0.4 10.8 06/18108 12:02:37 1.3 0.0 10.3 06/1810812:02:47 1.7 D.5 10.7 06/18108 12:02:57 1.8 0.4 10.7



### Resume 06/18/08 12:03:07 1.8 0.4 10.8 06118/08 12:03:17 1.7 0.5 10.9 06/18/08 12:03:27 1.7 0.4 10.8 06116/08 12:03:37 1.7 0.5 10.9 06118/0812:03:47 1.7 0.5 10.9 06118108 12:03:57 1.7 0.5 10.9 06118/08 12:04:07 1.7 0.5 10.9 06118/0812:04:17 1.7 0.5 11.0 06/18/0812:04:27 1.8 0.5 10.9 06118/08 12:04:37 1.7 0.5 11.0 06118108 12:04:47 1.7 0.5 10.9 06118/08 12:04:57 1.7 0.5 11.0 06118/0812:05:07 1.7 0.5 11.0 06118/08 12:05:17 1.7 0.5 11.1 06118/08 12:05:27 1.7 0.5 11.1



### Page 3 

# 976118108 Run #2

0611810812:05:37 1.7 0.5 41.2 06118108 12:05:47 1.7 0.5 11.2 0611810812:05:57 1.7 0.5 11.2 0611810812:06:07 1.7 0.5 11.3 0611810812:06:17 1.7 0.5 11.2 06/1810812:06:27 1.7 0.5 11.3 06/1810812:06:37 1.7 0.5 11.3 0611 8108 1 2:06:47 1.7 0.5 11.2 06118108 12:06:57 1.7 0.5 11.2 06118/08 12:07:07 1.7 0.5 11.2 06118/0812:07:17 1.7 0.5 11.2 0611 8108 1 2:07:27 1.7 0.5 11.2 0611810812:07:37 1.7 0.6 11.2 06J18J0812:07:47 1.7 0.5 11.3 06118l0812:07:57 1.7 0.5 11.3 0611 8108 1 2:08:07 1.8 0.5 11.3 06118/0812:08:17 1.7 0.5 11.3 06118/0812:08:27 1.7 0.5 11.3 06118/08 12:08:37 1.7 0.5 11.3 06118/0812:08:47 1.7 0.5 11.4 0611810812:08:57 1.7 0.5 11.4 06118/08 12:09:07 1.8 0.5 11.4 06118/0812:09:17 1.8 0.5 11.4 06118/0812:09:27 1.7 0.5 11.4 06118/0812:09:37 1.7 0.5 11.4 0611810812:09:47 1.7 O.S. 11.3 06118l0812:09:57 1.7 0.5 11.3 06118108 72:10:07 1.8 0.5 11.3 06/1810812:10:17 1.7 0.5 11.3 06/18108 12:10:27 1.7 0.4 11.4 06/98108 42:10:37 1.7 0.5 11.4 06/18108 12:10:47 1.7 0.5 11.4 0611810812:10:57 1.7 0.5 11.4 06/18/0812:11:07 1.7 0.5 11.4 06/18108 12:11:17 1.7 0.5 11.3 06/18108 12:11:27 1.7 0.5 11.4 06118/0812:11:37 1.6 0.5 11.4 06118108 12:11:47 1.7 0.5 11.4 0611810812:11:57 1.7 0.5 11.4 0611810812:12:07 1.6 0.5 11.5 06l1810812:12:17 1.5 0.4 11

- .6 06/1810812:1227 9.7 0.5 11.6 06118108 12:12:37 1.7 0.5 11.7 06/18/08 'l2:12:47 1.6 0.5 11.7 0611810812:12:57 1.6 0.5 11.8 061'18108 12:13:07 1.5 0.5 11.9 06118/08 12:13:17 1.6 0.5 12.0 06l18/0812:13:27 1.5 0.5 12.0 06118J0812:13:37 1.6 0.5 12.1 06118108 12:13:47 1.5 0.5 12.0 06118J0812:13:57 1.5 0.5 12.0 06118l0812:14:07 1.5 0.5 12.1 06118108 12:14:17 1.6 0.5 12.1 06/18108 12:14:27 1.6 0.5 12.1 0611810812:14:37 1.7 0.5 12.2 0611810812:14:47 1.6 0.5 12.3 06/18108 12:14:57 1.5 0.5 12.3 06/18/08 12:15:07 1.6 0.5 12.3 06/1810812:15:17 1.5 0.5 12.4 06J1810812:15:27 1.5 0.5 12.4 06118/0812:15:37 1.7 0.5 12.4 0611810812:15:47 1.7 0.5 12.4 0611810812:15:57 1.7 

# ` 0.5 12.4 06118/08 12:16:07 1.8 0.5 12.4 06/1810812:16:17 1.7 0.5 12.4 0611810812:16:27 1.7 0.5 12.4 06118108 12:16:37 1.7 0.5 12.4 06/18108 12:16:47 1.7 0.5 12.3 06/1810812:16:57 1.7 0.5 12.3 06/18108 12:17:07 1.7 0.5 12.3 06118/0812:17:17 1.7 0.5 12.3 0611810812:17:27 1.7 0.5 12.3 06J1810812:17:37 1.7 0.5 12.3 06118/08 12:17:47 1.8 0.5 12.3

PFage 4 

# W Ti 

# • ,6/18/08 Run #2

06/18/0812:17:57 1.7 0.5 12.4 06118/0812:18:07 1.7 0.5 12.4 06/18/0812:18:17 1.7 0.5 12.4 06/1810812:18:27 1.7 0.5 12.4 08/18/08 12:18:37 1.7 0.5 12.3 06/1810812:18:47 1.7 0.5 12.3 0611810812:18:57 1.7 0.6 12.2 06/18/0812:19:07 1.7 0.5 12.2 0611810812:19:17 1.7 0.6 12.2 06/18/0812:19:27 1.7 0.6 12.2 06/18/0812:19:37 1.7 0.6 12.2 06/18/0812:19:47 1.7 0.6 12.3 06/18108 12:19:57 1.7 0.6 12.2 06/18108 12:20:07 1.7 0.5 12.3 06118/0812:20:17 1.7 0.6 12.3 06/18l0812:20:27 1.7 0.6 12.3 06/18/0812:20:37 1.8 0.5 12.3 06/18/0812:20:47 1.7 0.6 12.2 06/18J0812:20:57 1.7 0.6 12.3 06118/081221:07 1.7 0.6 12.3 06/1810812:21:17 1.7 0.5 12.3 06118108 12 21:27 1.7 0.5 12.3 06/181081221:37 1.7 0.5 12.3 06/18/0812:21:47 1.8 0.5 12.3 06/18l0812:21:57 1.8 0.6 12.3 0611810812:22:07 1.7 0.5 12.3 06/1810812:22:17 1.8 0.5 12.3 06/1810812:22:27 1.8 0.5 12.3 06118/08 12:22:37 1.8 0.5 12.3 06/1810812:22:47 1.8 0.5 12.3 06/18/0812:22:57 1.7 0.5 12.3 06/18/0812:23

- 07 1.7 0.5 12.2 06/18/0812:23:17 1.7 0.5 12.3 06118/0812:23:27 1.8 0.5 12.3 06118/081223:37 1.7 0.5 12.2 06118/0812:23:47 1.7 0.5 12.3 06/1810812:23:57 1.7 0.5 12.3 06/18108 12:24:07 1.6 0.6 12.3 08118/08 12:24:17 1.7 0.6 12.2 06/18/0812:24:27 1.7 0.6 12.2 06/1810812:24:37 1.7 0.7 12.2 06/18/08 12:24:47 1.7 0.8 12.2 06118/0812:24:57 1.6 1.0 12.2 06/18/0812:25:07 1.7 12 12.2 06/18/08 12:25:17 1.6 1.3 12.2 06/18/08 12:25:27 1.6 1.5 12.2 06/1810812:25:37 1.7 1.6 12.2 06118/08 12 :25:4 7 1.7 1.8 12.2 06118/0812:25:57 1.6 2.0 12.2 06/1810812:26:07 1.5 2.1 12.3 06/1810812:26:17 1.6 2.2 12.2 0611810812:26:27 1.5 2.3 12.2 06/18/0812:26:37 1.6 2.5 12.3 0611810812:26:47 1.7 2.6 12.3 06118/0812:26:57 1.5 2.6 12.2 061181081227:07 1.5 2.7 12.2 06/18f0812:27:17 1.5 2.7 12.3 06/1810812:27:27 1.5 2.7 12.2 06118/0812:27:37 1.6 2.8 12.2 06/18108 12:27:47 1.5 2.8 12.2 06/18/0812:27:57 1.6 3.0 12.2 06118/0812:28:07 1.6 3.0 12.2 06/1810812:28:17 1.5 3.0 12.2 06/18/0812:2827 1.5 3.0 12.2 06118/0812:28:37 1.5 3.2 12.2 0611810812:28:47 1.5 3.3 12.2 06/1810812:28:57 1.5 3.4 12.2 06/18/0812:29:07 1.5 3.5 12.2 06118/0812:29:17 1.5 3.6 12.2 06118108 12:29:27. 1.6 3.7 12.2 06/18/0812:29:37 1.5 3.8 12.2 0611810812:29:47 1.5 3.8 12.2 08/18/0812:29:57 1.5 3.9 12.2 06118/0812:30:07 1.5 4.0 12.3



### Page 6 

# gus aAm6l18108 Run #2

06118/0812:30:17 1.5 4.1 12.2 06118/0812:30:27 1.5 4.2 12.2 06/18108 12:30:37 1.5 4.2 12.2 06/18/0812:30:47 1.5 4.3 12.2 08118108 12:30:57 1.5 4.4 12.2 06118/08 12:31:07 1.5 4.4 12.2 06118/0812:31:17 1.5 4.5 12.2 06/18/08 12:31:27 1.5 4.5 12.2 06/18108 12:31:37 1.5 4.6 12.2 06/1810812:31:47 1.5 4.7 12.2 06/1810812:31:57 1.5 4.8 12.2 06/1810812:32:07 1.5 4.7 12.2 06118108 12:32:17 1.5 4.9 12.2 06/1810812:32:27 1.5 4.9 12.2 06118/08 12:32:37 1.5 4.9 12.1 06118/0812:32:47 1.5 4.9 12.1 0611810812:32:57 0.8 4.2 11.4
Stop Run #2 1.95 0.94 11.28

06/1810812:33:07 1.5 5.0 12.1 06118f0812:33:17 1.5 5.0 12.1 08118108 12:33:27 1.5 4.9 12.1 06/1810812:33:37 2.0 5.0 12.1 06/18/0812:33:47 4.1 5.0 12.1 06/18/0812:33:57 3.9 4.9 11.8 06118J08 i 2:34:07 3.7 4.9 9.1 06/1810812:34:17 3.5 4.8 5.7 0611810812:34:27 3.5 4.8 4.5 0611810812:34:37 3.7 6.0 2.7 0611810812:34:47 3.7 8.5 1.5 06/1810812:34:57 3.6 12.2 1.0 06/1810812:35:07 3.5 15.9 0.6 06118/0812:35:17 3.5 18.9 0.4 06118/08 12:35:27 3.6 21.0 0.3 06/18/0812:35:37 3.8 22.5 0.2 06118/0812:35:47 3.5 23.4 0.2 06l18/0812:35:57 3.8 23.8 0.1 06/18/0812:36:07 3.7 24.1 0.1 06/18l0812:36:17 3.7 24.2 0.1 06/1810812:36:27 3.7 24.3 0.1 06/1810812:36:37 3.6 24.4 0.1 0611810812:36:47 3.5 24.4 0.1 0611810812:36:57 3.6 24.4 0.0 0611810812:37:07 3.6 24.4 0.0 06118/0812:37:17 3.5 24.5 0.0 06118/0812:37:27 3.5 24.5 0.0 06/1810812:37:37 1.6 24.5 0.0 06118/0812:37:47 0.8 24.5 0.0 06/18108 12:37:57 0.6 24.4 0.8 06/1810812:38:07 0.6 23.7 6.7 06118/08 12:38:17 0.4 21.4 13.1 0611810812:38:27 0.3 17.4 16.5 06118/0812:38:37 0.3 12.9 18.4 06/18/0812:38:47 0.3 8.9 20.1 0611810812:38:57 0.3 6.0 21.1 06118/0812:39:07 0.3 4.1 21.9 06/1810812:39:17 0.3 2.8 22.3 06118/0812:39:27 0.2 1.8 22.5 0611810812:39:37 0.3 1.2 22.7 06/1810812:39:47 0.1 0.8 22.7 06/1810812:39:57 0.3 0.5 22.8 06/1810812:40:07 0.3 0.3 22.8 0611810812:40:17 0.3 0.3 22.9 0611810812:40:27 0.3 0.2 22.8 06/1810812:40:37 0.3 0.2 22.9 06/1810812:40:47 

### 0.3 4.1 22.9 06/18/0812:40 

### :57 0.3 0.1 22.9 06/1810812:41:07 0.5 0.1 23.0 06118/08 12:41:17 8.4 0.1 22.9 06/18/0812:41:27 20.7 0.1 22.9 06118/0812:41:37 20.8 0.1 21.4 

### 24 .3 ppm CO Zero NOx

25 ppm NOx Zero VOC, CO

Page 6 

## ~ 

# 0 06118108 Run 92

0611810812:41:47 20.8

. 0.'t 15.4 20.2 ppm CH4 08118/08 '12:41:57 • 20.8 0.1 9.0 08148108 92:42:07

- 20.7 0.1 5.1 06118108'12:42:17 20.8 02 3.1 06/'E 8/0812:42:27 9,0 0.2 1.9



# ~~~ F'age 7 •

.6118108 Run #3

DatelTime VOC CO NOx 

### mm/8dlyy hh:mm:ss ppm ppm ppm 06/18108 12:44:57 1.5 1.2 11.7

8tart Run #3 06/1810812:45:07 1.5 1.2 11.9 06/1810812:45:17 1.5 1.2 12.0 06/18108 12:45:27 1.5 1.2 12.0 06/18108 12:45:37 1.5 1.2 12.1 06/18/08 12 :45 :47 1.5 1.2 12.1 06118l0812:45 :57 1.5 1.2 12.1 06/1810812:46:07 1.5 1.2 12.1 06118108 1 2:46:17 1.5 1.1 12.1 0611 8108 1 2:46:27 1.5 1.1 12.1 06/18108 12:46:37 1.5 1.1 12.2 06/18/08 12:46:47 1.5 9.0 12.2 0611810812:46:57 1.6 1.1 12.3 06/1810812 :47 :07 1.6 1.1 12.2 06118108 12:47:17 1.5 1.0 12.3 06/18108 12:47:27 1.6 1.0 12.2 0611810812:47:37 1.6 1.0 12.3 0611 8108 1 2:47:47 1.7 1.0 12.3 06/18/08 12:47:57 1.7 1.0 12.3 0 6/ 18108 12 : 48 :0 7 1.6 1.0 12.3 06/18108 12:48:17 1.5 1.0 12.3 06/18108 12:48:27 1.6 1.0 12.3 06/1810812:48:37 1.5 1.0 12.3 0611810812:48:47 1.5 0.9 12.3 0611810812:48:57 1.6 0.8 12.2 06118108 12:49:07 2.1 0.8 12.3 06/1810812:49:17 2.9 1.0 12.2 06118/0812:49:27 3.0 1.0 12.3 0611810812:49:37 2.6 1.0 12.2 0611810812:49:47 2.1 1.0 12.2 0611810812:49:57 1.9 1.0 12.3 06118l0812:50:07 9.9 1.0 12.2 06118108 12:50:17 1.8 0.9 12.3 06118/0812:50:27 1.8 1.0. 12.3 06118J08 12:50 :37 1.7 1.0 12.3 06/18108 12:50:47 1.7 1.0 12.2 0611810812:50:57 1.7 1.0 12.2 06118/0812:51:07 1.7 1.0 12.3 06118/0812:51:17 1.7 0.9 12.3 06118J0812:51:27 1.7 1.0 12.3 06118/0812:51:37 1.9 0.9 12.2 06/18/0812:51:47 2.0 0.9 12.2 06118108 12:51:57 2.3 1.0 12.3 06/18/0812:52:07 2.1 0.9 12.3 06/18108 42:52:17 2.0 1.0 12.2 06118108 12:52:27 1.9 1.0 12.3 0611810812:52:37 2.0 1.0 12.3 06118108 1 2:52:47 2.1 1.0 12.3 06118/08 12:52:57 2.1 1.0 12.3 0611 8/08 1 2:53:07 2.0 1.0 12.2 0611 8/08 1 2:53:17 1.8 1.0 92.3 0611 8/08 1 2:53:27 2.0 0.9 12.3 06/1 8/0812:53:37 2.0 0.9 12.3 06/18/08 12:53:47 2.1 1.0 12.3 06/18/08 12:53:57 2.0 1.0 12.3 06118108 i 2:54:07 1.9 1.0 12.3 06/1810812:54:17 2.0 1.0 12.3 06/1810812:54:27 2.0 1.1 12.3 06118108 12:54:37 2.1 1.1 12.3 06118108 12:54:47 2.0 12 12.2 06/18108 12:54:57 2.0 1.2 12.2 0611810812:55:07 2.0 1.3 12.2 06118/0812:55:17 2.0 1.4 12.2 0611 8108 1 2:55:27 1.8 1.5 122 06118/08 12:55:37 1.7 1.5 12.2 06/18/08 12:55:A7 1.8 1.6 12.2 06/1810812:55:57 2.0 1.6 12.2 06118/0812:56:07 2.0 1.7 12.2 06/18108 12:56:17 2.0 1.7 12.2 0611810812:56:27 2.0 1.6 12.2 

# 102
Page 16r18ro8 Run tt3

0611810812:56:37 2.0 1.6 12.3 06/18/0812:56:47 2.0 1.5 12.2 06/1810812:56:57 2.0 1.4 12.2 06/1810812:57:07 2.0 1.4 12.3 08118108 12:57:17 1.9 1.3 12.3 06118/0812:57:27 1.8 1.3 12.3 06118/0812:57:37 1.9 1.2 12.3 06/1810812:57:47 1.9 1.2 12.3 0611810812:57:57 1.8 1.2 12.3 06/18/08 12:58:07 1.8 1.1 12.3 06/18/08 12:58:17 2.0 1.1 12.3 06J 18/08.12:58:2 7 1.8 1.1 12.3 06118/08 12:58:37 1.8 1.0 12.2 06118/0812:58:47 1.8 1.0 12.4 0611810812:58:57 1.7 1.0 12.3 06/1810812:59:07 1.7 1.0 12.3 06118108 12:59:17 1.7 1.0 12.4 06/18/0812:59:27 1.7 1.0 12.3 06/18l08 12:5937 1.8 1.0 12.3 06/18/08 12:59:47 1.7 0.9 12.4 06l18l0812:59:57 1.7 0.9 12.3 06/18108 13:00:07 1.8 0.9 12.3 06118/0813:00:17 1.7 0.9 12.2 06118l0813:00:27 1.7 0.9 .12.3 06118/08 13:00:37 1.7 0.9 12.3 06118108 13:00:47 1.7 0.9 12.2 06118/0813:00:57 1.7 0.8 12.2 06/18/0813:01:07 1.7 0.8 12.3 06118/0813:01:17 1.8 0.8 12.2 06/18l0813:01:27 1.8 0.8 12.2 06/18l0813:01:37 1.8 0.8 12.3 06l1810813:01:47 1.7 0.7 12.3 06/18/0813:01:57 1.7 0.7 12.3 O6/18/0813:02:07 1.7 0.7 12.3 06118/0813:02:17 1.7 0.7 12.2 06/18/08 13:02:27 1.7 0.7 12.2 0611810813:02:37 1.7 0.7 12.2 0611810813:02:47 1.8 0.8 12.3 06/18J0813:02:57 1.7 0.8 12.2 06118/08 13:03:07 1.7 0.7 12 9 06118/0813:03:17 1.7 0.6 12.2 06118l0813:03:27 1.8 0.7 12.3 06l1810813:03:37 1.7 0.7 12.2 06118/0813:03:47 1.7 0.7 12.2 06/1810813:03:57 1.7 0.6 12.2 06/18/0813:04:07 1.7 0.7 12.2 06/18108 13:04:17 1.7 0.7 12.2 06/18/08 13:04:27 1.7 0.6 12.2 06/18/0813:04:37 1.7 0.8 12.2 06/18/0813:04:47 1.7 0.7 12.2 06/18/0813:04:57 1.7 0.6 12.2 06118/0813:05:07 1.7 0.7 12.1 06l1810813:05:17 1.7 0.7 12.1 06/1810813:05:27 1.5 0.7 12.1 0611810813:05:37 1.5 0.8 12.1 06118l0813:05:47 1.6 0.7 12.1 0611810813:05:57 1.7 0.8 12.1 06118108 13:06:07 1.7 0.7 12.1 06/1810813:06:17 1.6 0.7 12.1 06118108 13:06:27 1.6 0.7 12.1 06/1810813:06:37 1.8 0.6 12.2 06/1810813:06:47 1.7 0.6 12.1 06/18/08 13:06:57 1.8 0.6 12.2 06/18J0813:07:07 1.8 0.6 12.1 06/18/0813:07:17 1.8 0.6 12.1 06/18I08 13:07:27 1.7 0.6 12.2 06/18/0813:07:37 1.6 0.6 12.1 06118108 13:07:47 1.8 0.6 12.2 06/1810813:07:57 1.7 0.6 12.2 06/18/08 13:08:07 1.7 0.6 12.2 06118/08 13:08:17 1.7 0.6 12.1 0611810813:08:27 1.7 0.6 12.1 0611810813:08:37 1.7 0.6 12.0 06/18108 13:08:47 1.8 0.6 12.0

Page 2 

# 1036/18108 Run 03

06/18108 13:08:57 1.7 0.6 12.0 0611810813:09:07 1.7 0.6 12.0 06118/08 13:09:17 1.5 0.6 11.9 06118/0813:09:27 1.7 0.6 11.8 06118/0813:09:37 1.7 0.6 11.8 06118/0813:09:47 1.7 0.6 11.9 06/18108 13:09:57 1.7 0.6 11.8 06/1810813:10:07 1.8 0.6 11.9 0611810813:10:17 1.7 0.6 11.8 06118/0813:10:27 1.8 0.6 11.7 06118/08 13:10:37 1.8 0.6 11.7 06118/0813:10:47 1.7 0.6 11.8 06118/08 13:10:57 1.8 0.6 11.7 06118/0813:11:07 1.8 0.6 11.6 0611810813:11:17 1.7 0.6 11.7 06118/0813:11:27 1.7 0.6 11.7 06118/0813:11:37 1.7 0.6 11.7 06/18108 13:11:47 1.7 0.6 11.7 0611810813:11:57 1.7 0.6 11.7 06118/0813:12:07 1.7 0.6 11.7 06118/08 13:12:17 1.7 0.6 11.6 0W18/0813:12:27 1.6 0.6 11.7 06118/0813:12:37 1.6 0.6 11.7 06118J0813:12:47 1.7 0.6 11.7 06118/0813:12:57 1.7 0.6 11.8 0611810S 13:13:07 1.7 0.5 11.7 06118108 13:13:17 1.7 0.6 11.7 06118/08 13:13:27 1.7 0.6 11.8 0611810813:13:37 1.6 0.5 11.7 06118/0813:13:47 1.7 0.5 11.7 06118/0813:13:57 1.7 0.5 11.7 06/18/08 13:14:07 1.7 0.5 11.7 06/18/0813:14:17 1.6 0.5 11.7 06118/0813:14:27 1.6 0.5 11.7 06118J0813:14:37 1.5 0.5 11.8 06/18/08 13:14:47 1.6 0.5 11.7 0611810813:14:57 1.7 0.5 11.7
Port Change 06118/0813:15:07 0.6 -0.3 10.7 0611810813:15:17 1.5 0.5 11.7 06118/0813:15:27 1.7 0.5 11.7 0611810813:15:37 1.8 0.5 11.8 06118l0813:15:47 1.9 0.5 11.8 06/18/0813:15:57 1.5 0.5 11.8 06/1810813:16:07 1.5 0.5 11.2 06/1810813:16:17 1.5 0.5 9.1 06/1810813:16:27 1.5 0.5 8.9 06/1810813:16:37 1.5 0.5 9.8 0611810813:16:47 1.5 0.5 10.5 06118/0813:16:57 1.5 0.5 11.0 06/18/0813:17:07 1.5 0.5 11.2 06118/08 13:17:17 1.5 0.5 11.4 06118/0813:17:27 1.6 0.6 11.5 06118/0813:17:37 1.7 0.6 11.6 06/18/0813:17:47 0.5 -0.7 10.4 06118/0813:17:57 1.7 0.5 11.6


### Resucne 06118/0813:18:07 1.7 0.5 11.7 06118/0813:18:17 1.7 0.6 11.7 06118/0813:18:27 1.6 0.6 11.7 06118/0813;18:37 1.6 0.6 11.7 06118/08 13:18:47 1.6 0.6 11.6 06118/0813:18:57 1.5 0.6 11.6 0611810813:19:07 1.5 0.6 11.7 06/1810813:19:17 1.7 0.7 11.6 06/18/0813:19:27 1.7 0.6 11.6 06/18/08 13:19:37 1.7 0.6 11.6 06118/08 13:19:47 1.6 0.5 11.7 0611810813:19:57 1.5 0.6 11.6 06118108 13:20:07 1.5 0.6 11.6 08118108 13:20:17 1.5 0.6 11.8 06118108 13:20:27 1.5 0.6 11.8



### Page 3 

# 1046118108 Run #3

06/18/0813:20:37 1.5 0.6 11.8 06/18/0813:20:47 1.5 0.6 11.7 06/18/081320:57 1.6 0.6 11.7 06/18108 13:21:07 1.6 0.5 11.8 0811810813:21:17 1.5 0.6 11.7 06/18/08 13:21:27 1.7 0.6 11.7 06118/0813:21:37 1.7 0.6 11.7 06118/0813:21:47 1.5 0.6 11.6 06/18/0813:21:57 1.5 0.6 11.7 06118/0813:22:07 1.5 0.6 11.7 06118/0813:22:17 1.5 0.6 11.8 06118/0813:22:27 1.5 0.6 11.7 061181081322:37 1.5 0.6 11.7 06118108 13:22:47 1.5 0.6 11.7 06118/0813:22:57 1.5 0.6 11.7 06l1810813:23:07 1.5 0.6 11.6 06118/08 1323:17 1.5 0.6 11.7 06118/0813:23:27 1.5 0.6 11.7 06118/0813:23:37 1.5 0.6 11.7 06118/0813:23:47 1.5 0.6 11.6 06118/0813:23:57 1.5 0.6 11.6 0511810813:24:07 1.5 0.6 11.6 06/18/0813:24:17 1.5 0.6 11.6 06/1810813:24:27 1.5 0.6 11.7 06/181081324:37 1.5 0.6 11.7 061181081324:47 1.5 0.6 11.7 06/18/0813:24:57 1.5 0.6 11.7 06118/0813:25:07 1.5 0.6 11.7 06/18/0813:25:17 1.5 0.6 11.8 06/18/08 13:25:27 1.5 0.6 11.8 06118/08 13:25:37 1.5 0.5 11.8 06118/0813:25:47 1.5 0.6 11.8 06/18/0813:25:57 1.5 0.6 11.8 06/18/08 13:26:07 1.5 0.5 11.8 0611810813:26:17 1.5 0.6 11.9 06118108 13:26:27 1.5 0.5 11.7 06118108 13:26:37 1.5 0.5 11.7 06/1810813:26:47 1.5 0.5 11.7 06/181081326:57 1.5 0.5 11.7 06/18108 13:27:07 1.5 0.5 11.8 06118/08 1327:17 1.5 0.5 11.7 06118108 13:27:27 1.5 0.5 11.8 06/18/0813:27:37 1.5 0.5 11.7 06118/0813:27:47 1.5 0.5 11.7 06/1810813:27:57 1.5 0.5 11.7 0611810813:28:07 1.5 0.5 11.6 06/1810813:28:17 1.5 0.5 11.7 06118/0813:28:27 1.5 0.5 11.6 06/18/081328:37 1.5 0.5 11.6 06/18/081328:47 1.5 0.5 11.6 06/1810813:28:57 1.5 0.5 11.6 06/18/0813:29:07 1.5 0.5 11.6 06/18/0813:29:17 1.5 0.5 11.6 06118/0813:29:27 1.5 0.5 11.6 06118/0813:29:37 1.5 0.5 11.5 0611810813:29:47 1.5 0.5 11.6 06118J0813:29:57 1.5 0.5 11.6 0611810813:30:07 1.5 0.5 11.7 06/1810813:30:17 1.5 0.5 11.7 06118108 13:30:27 1.5 0.5 11.7 06/18108 13:30:37 1.5 0.5 11.8 06/1810813:30:47 1.5 0.5 11.7 06/18/0813:30:57 1.5 0.5 11.7 06118108 13:31:07 1.5 0.5 11.7 06118108 13:31:17 1.4 0.5 11.7 06118/08 13:31:27 1.5 0.5 11.7 06118/08 13:31:37 1.5 0.5 11.7 06118/0813:31:47 1.5 0.5 11.7 06/1810813:31:57 1.5 0.6 11.6 06118108 13:32:07 1.5 0.5 11.6 06118/0813:32:17 1.5 0.5 11.7 06/1810813:32:27 1.5 0.5 11.7 06/1810813:32:37 1.5 0.6 11.7 06118/08 13:32:47 1.5 0.6 11.7

Page 4 

# 1056118/08 Run #3

06/18/08 13:32:57 1.5 0.6 11.7 06/1810813:33:07 1.5 0.6 11.7 06118/08 13:33:17 1.5 0.6 11.7 06118/0813:33:27 1.5 0.6 11.8 06/18/08 13:33:37 1.5 0.6 11.8 06/18108 13:33:47 1.5 0.7 11.8 06118/0813:33:57 1.5 0.6 11.8 06118/0813:34:07 1.8 0.7 11.8 06118/0813:34:17 1.7 0.8 11.8 06J18/0813:34:27 1.7 0.7 11.8 06/18/0813:34:37 1.6 0.7 11.8 06/18/0813:34:47 1.5 0.7 11.9 06118/0813:34:57 1.5 0.6 11.9 06/1810813:35:07 1.5 0.6 11.9 06118/0813:35:17 1.5 0.7 11.8 06118l0813:35:27 1.5 0.6 11.8 06/18/0813:35:37 1.5 0.6 11.8 06/1810813:35:47 1.5 0.7 11.8 06118/0813:35:57 1.5 0.6 11.7 06118/0813:36:07 1.5 0.6 11.8 06118/0813:36:17 1.5 0.6 11.7 06118108 13:36:27 1.5 0.6 11.8 0611810813:36:37 1.5 0.6 11.7 06/1810813:36:47 1.5 0.6 11.8 06/18/0813:36:57 1.5 0.6 11.8 06/1810813:37:07 1.5 0.6 11.7 0611810813:37:17 1.5 0.6 11.7 0611810813:37:27 1.5 0.6 11.7 06/18/0813:37:37 1.5 0.6 11.6 06/1810813:37:47 1.5 0.6 11.7 06/18/0813:37:57 1.5 0.6 11.7 0611 8/08 1 3:38:07 1.5 0.6 11.7 06118l0813:38:17 1.5 0.6 11.7 06/18l0813:38:27 1.5 0.6 11.7 06/18/0813:38:37 1.5 0.6 11.8 06/18/0813:38:47 1.5 0.6 11.8 06/1810813:38:57 9.4 0.6 11.8 06/1810813:39:07 1.5 0.6 11.9 08/1810813:39:17 1.5 0.6 12.0 06/1810813:39:27 1.4 0.6 12.1 06118/0813:39:37 1.4 0.6 12.1 06/1810813:39:47 1.5 0.6 12.2 0611810813:39:57 1.4 0.6 12.2 0611810813:40:07 1.5 0.6 12.2 06/18/0813:40:17 1.5 0.6 12.2 06/18/08 13:40:27 1.5 0.6 12.2 06118/0813:40:37 1.5 0.6 12.1 06/18/0813:40:47 1.5 0.6 12.2 06/18l0813:40:57 1.5 0.6 12.2 06/18/0813:41:07 1.3 0.5 12.1 06/18108 13:41:17 1.5 0.6 12.1 06118J0813:4127 1.5 0.6 12.1 06118108 13:41:37 1.5 0.6 12.1 06/18/0813:41:47 1.5 0.6 12.1 06118/0813:41:57 1.5 0.6 12.1 0611810813:42:07 1.4 0.6 12.1 06/18/0813:42:17 1.4 0.6 12.1 06118/0813:42:27 1.4 0.6 12.2 06/18/0813:42:37 1.5 0.6 12.2 06/18l0813:42:47 1.5 0.6 12.2 06/1810813:42:57 1.5 0.6 12.2 06/1810813:43:07 1.5 0.7 12.2 06/1810813:43:17 1.5 0.7 12.2 06118108 13:43:2 

## r 1 S 0.7 12.2 06/18/0813:43:37 1.5 0.8 12.1 06118/0813:43:47 1.5 0.8 12.1 06118/0813:43:57 1.5 0.9 12.1 06118/0813:44:07 1.5 0.9 12.1 06118/0813:44:17 1.5 0.9 12.1 0611810813:44:27 1.5 1.0 12.2 06/18/08 13:44:37 1.5 1.1 12.2 06/18108 13:44:47 1.5 1.1 12.2 0 6/ 18108 13 : 44: 57 1.5 1.2 12.1 06118108 13:45:07 1.5 1.2 12.2



### Page 6 

# 1066118/08 Run #3

061 18J0813:45 :17 1.5 1.2 0611810813:45:27 1.5 1.2 061 1810 813 : 45 :37 1.4 1.1 06/1810813:45:47 1.4 1.1 06/ 18108 13:45 :57 1.4 1.0 06/1810813:46:07 1.3 0.9 06/18/0813:46:17 1.4 1.0 06/1810813:4627 1.5 0.9 06118/0813:46:37 1.5 0.9 06118/0813:46:47 1.5 0.9 06118/0813:46:57 1.5 0.9 06J18/0813:47:07 1.5 0.9 06118/0813:47:17 1.5 0.8 06l1810813:47:27 1.5 0.9 06118108 13:47:37 1.5 0.9 06118/0813:47:47 1.4 0.8 06118/0813:47:57 1.5 0.8
Siop Run #3 1.64 0.77 11.98 12.1 12.1 12.1 12.1 12.1 12.1 12.1 12.1 12.1 12.1 12.1 12.1 12.1 12.1 12.1 12.1 12.1

06118/0813:48:07 0611810813:48:17 0811810813:48:27 0611810813:48:37 0611810813:48:47 06118108 13:48:57 06/18J0813:49:07 06/18/08 13:49:17 06118l0813:49:27 06I18/08 13:49:37 06118/08 13:49:47 O6t18/0813:49:57 06118/0813:50:07 06118/0813:50:17 06118/0813:50:27 06J18108 13:50:37 06/18108 13:50:47. 06/18108 13:50:57 06/1810813:51:07 06118/08 13:5117 06118108 13:51:27 06118/08 13:51:37 0611810813:51:47 0611810813:51:57 06/18108 13:52:07 06/18108 13:52:17 06l1810813:52:27 06/1810813:52:37 06I18108 13:52:47 06/18/08 13:52:57 06118108 13:53:07 08118108 13:53:17 06118/08 13:53:27 06118/0813:53:37 06118/0813:53:47 0611810813:53:57 06f18108 13:54:07 06I1810813:54:17 06118108 13:54:27 06/1810813:54:37 06/18108 13:54:47 06/1810813:54:57 06/18l08 13:55:07 06/18108 13:55:17 06/18108 13:55:27 0611810813:55:37 06l18J08 13:55:47 06118I0813:55:57 06118/08 13:56:07 0611810813:56:17 06/18108 13:56:27 06118108 13:56:37 06118108 13:56:47 0.9 0.3 11.6 1.5 0.8 12.1 1.6 0.8 121 1.7 0.8 12.2 1.7 0.8 12.0 4.7 0.8 9.8 3.5 0.7 6.4 3.5 0.6 3.8 3.5 1.0 2.3 3.5 2.4 2.0 3.5 5.4 1.5 3.5 9.3 1.0 3.5 13.3 0.6 3.5 16.7 0.4 3.5 19.3 0.2 3.5 21.1 0.2 3.5 22.4 0.1 3.5 23.1 0.1 3.5 23.6 0.1 3.5 23.9 0.0 3.5 24.0 0.0 3.5 24.1 0.0 3.6 24.2 0.0 3.6 242 0.0 3.5 24.3 0.0 3.5 

### 24.3 0.0 3.5 

### 24.3 0.0 3.5 

### 24.4 0.0 1.3 

### 24.4 0.0 0.7 24.3 0.0 0.4 24.2 1.1 0.3 23.5 7.0 0.3 21.4 13.4 0.3 17.5 17.3 0.3 12.9 19.4 0.3 8.6 20.4 0.3 5.5 20.9 0.3 3.4 21.3 0.3 2.3 21.6 0.2 1.6 21.8 0.2 1.3 21.9 0.3 1.0 22.0 0.2 0.8 22.1 0.1 0.7 22.2 0.1 0.5 22.3 0.1 0.4 22.3 0.1 0.4 22.4 0.1 0.3 22.6 0.1 0.2 22.6 0.1 0.2 22.6 

### 0.1 0.2 22.6 0.1 0.1 22.6 0.1 0.1 22.6 24.3 ppm CO

25 ppm NOx

zero 

### voC, CO



### Page 6 

# 107

### 6118108 Run #3

06/18/08 33:56:57 0.1 0.1 22.8 0611810813:57:07 3.6 0.1 22.6 06/1810813:87:17 20.1 0.1 22.4 0611810813:57:27 20.8 0.0 21.9 06118/0813:57:37 20.8 0.0 18.2 06118/0813:57:47 20.8 0.0 11.7 06/1810813:57:57 20.8 0.0 6.6 06118/0813:58:07 20.8 0.1 3.6 06l18108 'E 3:58:'E 7 14.3 0.1 2.0 06l18/08 13:68:27 2.1 0.1 1.3 

### 20.2 ppm CH4

Page 7 

# I

~ 

# 8

# a

- ~ 

# /tj,



# r 

# oil, 0 0

~~ 

# ? .5, S~ 

# - 133 

# 6 ,(16 iq

56 '' -, ~ 

# S'f - S 

# 0 0. IL 

# 0

----------



# " 7•

~ 

# B~ 

# - 6 ~~~ .~~3r-~ Zy "

. 

# S

f~~3~ .-i2:o 

# ~ ~.~~ % !l, Z 

# ~ 

# 12-133 

# 2 q

, 6 "'



# t 3



# M,r .A

109

# Cormpmny: Om0hm.E]PaooTX Dmtm: 6/ 7/O8 LocaDon: Cmnnb|nmdKQnmExhouet Run1 Rmn2 Run3
Filter |D Number
OmtemfVVmdQhUmg

Tkne GrommPUterVVt.
[JmtmofVVe|gh\ng

Tlme 

# MP {BrommF||tmrVVt.
Ave.C@noomF||terVVt. 0.3891 0.3856 0 .3 90 2
DatemfVVm\gh|ng

T|rnm FUterTmmwVVL
[JmtmmfVVe|gh|ng 

# VO

T|rnm ' FUtmrTareVVt.
Avm.FUba,ToroVVt. 0.3829 ~------- 0.3798

-------- 0 .3 8 52

-------' VVLofPN4onFi|ter(Qnannm) 0.0061 0.0058 0

. 0050 Tota| VVe|gh1 ofPmrt|ou|ate ( rng) 6.1 5.8 5

. 

# 0

~~ i ~~

# PARTICULATE ANALYTICAL DATA FORM
Company: Daltile, 

# El Paso, TX Date: 

# 6/17/08 Location: Combined Kilns Exhaust

Run 

# 1 Run 2 Run 

# 3
Density (Pa)
Blank Concentration (Ca) 

# -14
~ 

## Rinse Volume (Vaw)

........ .. 

## Residue in Rinse (Wa) 

# = Ca*Vaw*Pa 0.0008 0.0005 0.0006



## Date of Weighing

Time ::; ,

7 .7-;: 7 04: 

## Gross Weight 4 

## -8


## Date of Weighing

Time Gross Weight

Date of Weighing

Time

- 

## A 

## Beaker Tare Weight Date of Weighing

Time ER 

## Beaker Tare Weight Average Gross Weight 100.9685 105.8843 106.4838 

## Less Blank Residue (Wa) 0.0008 0.0005

. 0.0006 

## Average Beaker Tare Weight 100.9361 105.8655

. 106.4587


## Weight of Particulate in Rinse (mg) 31.58 18.26 24.50



# ACETONE BLANK ANALYTICAL DATA FORM

Blank Volume (Va) Date of Weighing

Time A 6 

# A . -M.-• Gross Weight 1:52 

## Date of Weighing

Time Gross Weight Average Gross Weight 111.5294 

## Date of Weighing Ti!!!17

- 11/oosi Time Tare Weight
Date of Weighing

Time Tare Weight Average Tare Weight 111.52865 

## Weight of Blank (Ma) 0.00075 

## Ca= Ma/(Va*Pa) 

# = mg/g 0.00382 

## Note: In no case should a blank residue greater than 

# 0.01 mg/g or 

# 0.001% of the blank lweight be subtracted from the sample weight. 

# ill"

# PARTICULATE ANALYTICAL DATA FORM
Company: Daltile, El Paso, TX Date: 6/17/08 Location: Combined Kilns Exhaust

Run 1 Run 2 Run 3
Density (Pa)

~ 

## i i..*. i i-IL9


## Blank Concentration (Ca)

....... 4 

## 46:

Aliqout, mls Rinse Volume (Vaw) Residue in Rinse (Wa) = Ca*Vaw*Pa 0.0018 0.0018 0.0018

Date of Weighing : :::::G. 41U 

## Time Gross Weight LX



## Date of Weighing

Time 7 7 Gross Weight :

Date of Weighing

Time 7-- - 27. A 7:426A 

## Beaker Tare Weight V1. 4::


## Date of Weighing vo

Time 2 

## W P. M Beaker Tare Weight 

## 1 ; 27; Z 

## : . $ I i 

## 10'.1.
Average Gross Weight 127.2313 131.4960 

## 126.8288 Less Blank Residue (Wa) 0.0018 0.0018 0.0018 Average Beaker Tare Weight 127.2115 131.4860 126.8269

. Weight of Particulate in Rinse (mg) 18.00 8.15 0.10 Correction for Aliquot (mg) 18.3051 8.2881 0.1017



# H20 BLANK ANALYTICAL DATA FORM

Blank Volume (Va) Date of Weighing

Time Gross Weight 

## -2


## Date of Weighing

Time a 

# :a 8:: P01A



## .0 3. 01 :



## . . 26 ~ 

## Gross Weight
Average Gross Weight 100.2623
Date of Weighing

Time A Tare Weight
Date of Weighing

Time MW Tare Weight 1: 0 2. 

## 6 0 a.:: 

## Average Tare Weight 100.2608
Weight of Blank (Ma) 0.0015 Ca= Ma/(Va*Pa) = g/g 6E.06
Note: In no case shOLlid a blank residue greater than 0.01 ma/g or 0.0010, of the blank lweight be subtracted from the sample weight. 

# 112

## Sheet1

Summary of HF and HCI Analysis_

-- , - -

.._ . -- --- = - - ---- i--- -



## P Plant: :Daltile, EI aso, TX (-


# - - - - --- ~ 

## - - -- ------------- - --_



# - - - -- -------- ~ ------ --- ---



# _. . -------- 

# _-_.__I__ ---- -



# ----- -- -- Date:6/17108' j

. - . _ ---- - -- - -- - -- ---- - _ - - - --- . --•------------- -------- - - Location: Combined Kiln Exhaust
~



## . _-- -- - ----- -

G ---- - - ` _... - - - ~ 

## ----- - - -_ _ . ---_ _ --_- - --- - ~ 

## ------- - ------ -------- - - -- - Run # Imp # ' Volume j Dilution : 

## FI-, ug/ml

~ 

## H F, 

## m_ g_

~ 

## CI-, ug/ml LHCI, mg - 1' 1~ 

## 3001
- , ----------.___. ~ 

## _.... 2 0 

## : ~ 

## 24.46 ; 154 

## .5383 1

_ _..----. - -. 3.88' 23.93184 .._-_ 1 1 300 L

. . . 20 ; 2 3.57 , 

## 148. 915 

## r- ..___ ------__ 3.89 ._ _ - 23 .993 

## 52

__. L 

## Ave 

## rage ! 151.72

_ . _... - 23.96268

_ - ..

- - ----- _ --- - -_ ~ 

### ~ 

## ---- ~ 

## -- 2 1
~ 3 

## 00



## - - -- _ ._._ _ _ -. - -- -- 201 26.81 1 

## 169.3856

---- ~ 

## ----_-- 3.68



## _ 22.69824

_ 2 1 300 !

_ _ .. - ... 20 27 .821 175.7668 

## _.._ - 3.7 

## 8 23.31504

---

~ 

## er age ; 1 

## 72.5762 23.00664

- - _-- - --

,

- ------ - ~ 

## -- - - ---_ ----- ' 

## ----- -------- - ------ 3 1; 3 00 '



## _ -- 20 ; 

## 2_2 .92 ; 144.8086



## -- 3.3 51 20.662 

## 8

-- - - 3
~ 1 - 

## 00

3

. ---- _. - ---- - - - 201 23.8 ` 150.3 

## 684_

-- ---- ~ 

# _ 3.6► 

## 22.2048

_ -- --:-_ ~ 

## . _- - --- -- - ; 

## : 147 5885 Ave 

## ra e _ ~ 

# . . - --- --- ----- - - ~ 

## ----- - _ - -- - ; 21.4338

------ - ~ 

## -- - --___--

- - -- - - 1 : 2 

## & 3 - - 300 ; 

## --- -

~ 

## 1 ' 

## 18.5 i 

## 5.84415 - - 3.791 

## 1.168836

__ 1 ; 2&3 _~ y
- 

## 300 .

~ 

## ---__._._ - 1 I -_ 18.

~ 

## . 

## 5.71779

1



## . --- -------- 4.08 ; 1.258272



## - 1.2135 

## 54 ;Average_
~ 

## 5.7 

## 8097

,

-------- -- 

# 22 & 3 : -
_ ---- -- - _-- - •--.-- 

# 300
--------------.... -_ L



# 1' 21.3' 6.72867 -_ ~



## _____ _



# - _ 2.89; 0. 

# 8 91276 

# 2, 2& 3

.. _ . 300 1; 21.29 6 .7255 

# 11

..._ 3.09 ! 0.9529 

# 56

.. ~



# _ Avera e 6.727 09 

# 1 g --•-- ~ 

# -- - _. _- 0.922116

~ 

# _. .. . .._ _ ._ _ ~ 

# ._. _ _______.____

- -r---- ' _ _-μ_ --- ---_--- 3 2& 3 ~ 

# 3_

00 

# - ._--- 14 ` 20 .17 6.371703_

~ -- 

# _ - 3.41 ~ 

# - 1.051 64 

# 4 3 2& 3 ; 300 1 1 20.4 

# 6 .44436 1

.~ 

# ---------. ~ 

# . 3.58 1.104072

~ 

# L Averag e 

# 6.408032

~ 

# - - 1.07 

# 7 858 I -- 

# --- - -- -----

~ ~ ~ ~ 

# ' 25.17 623


## -- ----- - -;-- 

## - - -- - 1 -- - Totals Run #1 157.507 

## 7

, . -- - -- - - ------ . _ - - - ------- -------- ~ 

## - . _ ------- ____ .

i Run #2 1 79.3033 

## ' 23.92876

- -- ----------- - - 1 - - - --- --- - _ . . '

~



## __ ~ 

## _ . - - ---- ---- ------ -_ . ` Run #3 ; 153.99651 j 22.51166

Page 1 113

## Fl
# cl1.



# I,53 —102 .4OOmV 

## Camponent Retenti 1 C124 . oOOmV 

## Rrea External

470.80 M 4.94

416.70 M 5.00 

# Conda.tlons = 4 .98 ug/ml F1-- in H20

= 5.0 ug/ml C1-- in H20 Date : 06/21/2048 Time = 12=18-17



## Component


# F.l 

# r

~ 

# .

N 

# Number Rctention

1 1.000 2 1.533 

# Area External Uni.ts

470.80 M 4.94 L1 ct / m 1 416.70 M 5.00 u g/ m J.

8$7 . 5C3 9.94



# 114

# Canditioiis : 4 e98 ug/ml F1-- in H20 : 5 .0 • uglml Cl' -- i r. H20 Date = 06/21/2008 

## Time = 12:22:43

--102 . 4GOmV 

# 1024 .4UC3mV Carlvarlent RetertJ 

# o rr

~ ............. ........... ~ ... ........................... «•».................••......•.............•........ ... .......... .......... .......... ......,........... .......... . .. ............................•...........•.... ». ................•• «...........••................. 1

~ • ~ ~

{ :! 

## 1 ~ •......., ~ i' ....:::::::::

~ tu:::aa:aous::::u:r . !

~ ~ { : I i ~ .. ........•..::::r.:: • 1 

## 3 € 

# ~ •... ;

~ 

## 21 

## ....... f

. 

# : • , .

~~ 

# ......, : i F1- 1.

C1- 1.53 

# Prea External

447.40• M 4.69



# 425.20 M 5.14



# 41 ._....•.

~ ~ I

~ • ~ F

~ 

# i._...... :

~

;ij • 3

~
. {

I 

# ..,...... . 6s 1

fi ................ .......... « ...................... ............•........• .....,.••....••.••....•.«............. ......••...,..«..,................. ..... . ............... ,...... ,,................ ......... ........«........... ,............. .............. .................. ..... ~


# Gomponent

F ,L - 

## r 1 .—



## 2 

# Number Rotention

1 11,000 ? 1.533

. 

# Area External Units

447.40 M 4, 69 ug/ml. 4.25 _ 20 M 5 . 1.4 ug/m 7.

872.60



# 115

# 116 —102 . 4Ot7mV Comgonent Retention------------------------ ---- -- Area External 1024 . OoOmV

2 Component.
F 1 

# ._ c ,t h4umber Retention

1 1.000 2 1.550 Area External Units
841 , 70 IvI 9.8 7 t.). g/ 

# m]. 777,95 M 10.71. u cj / ml

1619.65 20.58 Conditions :9_95 ug/ml F1,— in H20

: 10.0 ug/ml C].-- in H20 Date = 06/21/2008 Time = 12:26=03

841.70 H 9.87

777.95 M 10,71 F1- 1.

C1- 1.55

# 117 2 

# Area External Units

855.50 M 1_0 .05 lia /ml 738..15~ M

~ 

## .c.7.C ~r~ t.~~~ 

## rnl.

1594.25 20.13 

# Gomponent Number Retention

F 1-- 1 1.000 E'.l. ... 2 1.550 

# i.onda.tions = 9. 0 .5 ug/ml F1— in H20 = 10.0 ug/ml Ox-- in H20 Date = 06/21 /2008 Time : 12=29=04



# F1-

C1- 1.024 .OJOmV

10.05



# 10.08 -102 ..FGw=inV 

# ComPolent Retenti



# 1.

1.55 

# Rrea External

855.50 M

738.75 M

## F1-



## C1- 1 024 . 0r)Om`
, l --102 .4OOmV 

# Companent Retent'

1.

1.5 

# Area External

1770.10 M 20.24



## 1462.90 M 21.40 Conditions = 14.5 ug/ml F1— in H20

~ 

## 20.0 ug/m I C]. -- i n H20 Dete = 06/21/2008 

# Time 12=33-32

Component
F1.-- 

# r., i .

K 

# Number Retention

1 3..016 2 1,566 

# Area External Units

1770 .. 10 M 20 . W4 ug/ml 1462.90 M 21.40 ug/mJ.

32:33 _ 00 41.64



# 118

## Conditions : 19.9 ug/ml Fl- in H20 z 20.0 ug/ml Cl- I'n 

## H20 Date : 06/21/2008 Time : 12:39:12

N 

# -1.02. /1 

## (/OmV
PIOMDOnent 

# Re'Lo-ntion 1021-1 , MOITIV Airea 

# r"derul

Fl- 1.

ci- 1.5 

# i ::......».......... .. ............. .............................. . .... .......•................ ..... ......... ............. . ........... . .................. . .. ................ ............................ . . ....... ........... ...



### I *

..........

.............................. . ... 

# 66. 

# 1 - 

# 1

.............................

.......

•



## 3 

# i

5 . ...... : 

# i

6!

...................... . ........................ ................................... ............. ..... ....... .......... ; .... ........ ......... .......... .............•... .......
............ .. ......... ...... ................. ................ 

# 1750.50 M- 20.02

1593.70 M 23.52

Component 

# Number Retention Area External' Units

F.1 - 

# 1. 1...016 .1.750.50 M 20.02 ug/ml ,%-- 1. - 

# 2 1.566 

# 1593.70 M 2:3.52 ug/m1

K' 

# 3344.20 43_54

119

# F1-

C1- 102 4 .0(;Oms,l

37.27



## 40.88 

# ._.I.02 ..40OmV C-omponent Retenti

1.

1.58 Rrea Ekt.ernsl

3352.30

3135,60 Condztions : 39.8 ug/'ml Fl- in H20



# = 40_0 ua/m1 C1- in M20 oate : 06/2112008 

# Tinte - 12 , :44=35

Component Number Retention Area External 

# Units

F1 - 3, 1.033 3352 ,.CO 37 _27 ug/ml Gi- 2 1.5£33 31 J5 ,.8() 40.88 ug/ml.

2 6488 

# _ 10 78.15



# 1-20

## ug/ml Fl— in H20 40.0 Ug/ml CIL— 

## in H20 06/21/2008 12."47:24

02,4OOmV 102/1,... OOOrriV Co nd it io n-,=-_

Date T

colaponent I

; e -L 

## e 11 t I 

## on

................ ...... ........... ....... ......... I 

## ........... ".., 

## ........... . ........ ....... ....... .............. I 

## ......... . I 

## .................. ............... . . ....... ............................

.............

...... . ............... ................ ....... 

## 3 !

.... .. .................... ... ... ................................ . Area ExterRal

3271.75 36.40

3033.50 39.55

6 .......

Component Number Retention Area External Units

1. 1 .033 3271 . 75 36 .40 L19/fAl 

## 2 

# a 3 3033.50 39.55 ug/ml

2 6305.25 75.94



# 1^2 1

# Ga 1 ibration fi l e : Fl- . cal

AMOk3NT I N.7"ECTE't3 

# AREA 0.

~ 

# 0Q

~ ~ ~ 

# ? ( ~ ~ j`~ 

# ;°_ ................ .............................. ........ ........... ...,................... ......._........ ~ 

# :' 9

... 800

... f

2
3

*1 ma

~ 

## 3312 .: 025

Avq s lopr.; of ctarve : 85 . Q4 Y--a:c x s i ntercept : 0.00 

## C; 4e

- f f o

- f 1 i. ri re g r

~ 

## 0.92 I\! 0 . A r

~ 

## a. A- m o t_i nt C F

0 = 0.000 0.,400 0.000 :L " 459.100 4

~ 

## 980 92.189 2 : 8 

## 48.600

9.950

~ 

## 35

~ 

## n 2

~ 

## 3 

# 6 3 • 1 760.300 196900 88.457 4 : '23 31. ? .0 25 39 v 84q 83 H 2 a.7



# 122

## AlI0UNT INJECTED

AREA 0.000 0.000



## 3084.650 40.000

1

7
3

4

5 0~ 

# 1. ibration fi le - -C? -- .cal

F1 v g s 7. o ;

. ~ 

## c c
~ 

## fi o c. ~ r ~.~ ~ " 

## 76.62 Y

~ 

## - a

~ 

## ; i s i. nt e rc e pt

~ 

## 0,. 0 0 (^ o ~ 

## , . ~ 

## . .i"
~~ - 

## I"' .
~ 

## .I. n r ~~ .~ 7~ 

## - 0.91

~ 

# Itilo . Arca. AmaLi. n CF

0~ 0 ~ 

## C300 0.000 0.. 000 1 = 420.950 5.000 84 . 1°0 

# 2' 758.350 1.0.000 75,835 3 : 1528 .

~ 

## 00 20.000 76.415 4 : 3084.650 40.000 77.1.1.6



# 123

# Condil--ions : 

# Daltile, El 

# Paso
: 

# Run #1 

# Imp #1
: 

# Volume 300 

# Dilution 1/20 Date : 06/21/2008 

# Time : 13:01:11



# -102.4OOmV LOMPORent Retenti 

# 1.024-OOOmV ATes External



# Fl- 1.

ci- 1.55 iti nulta I titti III In II is a I ?:I tll III III III Ian I ti tti III III 111131111111:1111 1 It Im ti ri ri insi m I0 

# 2

3

41' 

# i :

~ ~



# 61

. ........... . ..... .......... . ..................... ... . .................. . ........................................ . ........ . ....... . ...................................... 2115.60 H 

## 24.46

326.50 ti 3.88

Componen't 

# Number Retention Area External Units


# F1 1 1.016 

# 2115..60 11 24,46 Li.g/rnl 2 1.550 

# 3,26, 50 rl 3.88 Llg/M.1.

2 2442-10 28-33



# 124

## Fl

# ci- .1. 024 

# .. 0 0 0 m V



# 23.57

3.89 - 

# 102.4.00mV 

# ComponeDt Re'Lention

I .

1.5 Area External

2046.50 H



# 327.20 M 

# Conditions z Daltile, El 

# Paso

: 

# Run #1 

# Imp #1 " 

# Volume 300 Dilution 1/20 

# Date 06/21/.2008 

# Time = 13:03:46



# Component Number Retention Area External Units
Fl- 1 1.033 

## 2046.

~ 

# M I'l 23.57 

# uo/ml c 1. - 2 1.550 327,20 

# M 3-89 ug/gil

2 2373.70 

# 27-46



# 125

# F1-

C1- MP.



# 1.5 -w 1 q,j . 40CimV 

## (:ompanent Peten

iL' 1424. _ 00nmV 

# Area Externai

2298.84 M 26.81



# 309.70 F1 3.68 Con

~ - 

# .itions = Daltile, E1 Paso

: Rti n #2 I mp # 1 n Vlolume 800 Dil.ution 1/20 Date : 06l21l2008 

# Time - 13:16:24



# Component 

# Nurnber Retention Area External Units

Fl. - 

# a

. x . 0 3 1 210 , 

## 2298.80 1 ,1 1 26.81. t.a:tm,l. '? 1.550 3 0 9 . 7 0 M '31 . 6 8

FA 2608.50 30.48



# 1 ~ O

# Cdncitions



# Date Time

eomponeat Retenti 

# on z Daltile, E1. Paso

= Run #?_ IrtP 41 : Voluine 300 Dilution 1J20 : 46/21 /2008

1 t"?? .. 4 C 0m`v' 

## 1.024• .0(J"7mV 

# Area External.

Fl- 1.

Cl- 1.55 

# 2378.00 M 27.82

31$.00 m 3.78 ~ t ••••••••• `

.. r «
~ ..n •• ~ ••• :«:na« .::.::::::....:.....«................«.«....,.,..i

~ 1::rfrII:8:1r1t71r1ttpiSII111:111919a:'.Itt8itt11ut:trlt:atrr.r:t:f11t111911:111:1 p :
){ E i ~ • ~ 

# 4l

~ ,:::... 

# ~ a:aatx:r • 

# ~► 

## ; 2!.... i

~ : !

! 

### ~ ~

~~

......... ~ ~ ~



### ~ • ! 

## j

. I l ' ~



## I

. 5{.. .«. ;

6 . ...... ;

- 

## 1 :

~ 

## ..... «.«._.....:...... ..._

........................... ..... ... ........ _ .«.. ~ 

## «.««.«.. .«.........«...._.._.. .... .................._._ .........«............._.......w. ~



# Component 

# Number Retention Area ExternaI Units

F I . 1 1. « 0 : ~ 

## $ . 2 3 7 8 ,. 0 C) 11 2 7 ,. 8 2 k) ,q ,f m l .:' 1.550 318,00 I1 3,78 Ev t g .1 

## m l

K 2696 - 00 31.60



# 127

# FlCl- { ! ~ 

## % 1 , ~ 

## 1'. ° .) 0 m V



## 22.92



# 3.35 ~

- . ~ . .. 2 r 

## f () O rn V 

# Camponent kel'enti

1.

1.55 

# Area Extei

- nsl

1996.05 M

281•.84 PS 

# Conditions = Daltile, Ei Paso

= Ru.n #3 I'mp #1 = Volusr:e 300 Dilutivn 1/20 Date 06/23 r'24G8 Time . 13=27-06



# Component Number Retention Area Externai Units

Fl-- 1. 1.0:16 19 9 16 .45 M 22 c.jg/m1. Cl.w- :? 1.550 281 ..£30 M 3.35 ua/ml

2 2277.85 26.27



# 128

## 1 02A. .. nr,nmV - 102 . 1i OnmV 

# COmponent Retenti

(unE,nown) 0.46 

# F1

- 

# i.

Cl- 1.55 Area Er,tpl"na?

Z$5.30 h/A


# 2064.45 C1 23.80

303.40 M 3.60

4 

# 1 Conditions = Daltile, El Paso



# = Ru n#3 I mp # 1 : Volume 300 Qi iution 1 /20 Date : 06/21/2008 Ti.r,te `- 13=29=40



# Component
FlC1•-

2 

# hlumber Retentxon
:l 1 ., 0 ; 3 2 1.550 

## Area Externel Units
2064 _

~ 

## -5 11 w 3 _ 80 uo/ml 303 .

~ 

## 1 0 m 6% 0 u m

~ 

## .

2367.85 27.40



# 129

# 'Conditions = Daltile yL

~ 

## " ..l Paso 

# 1-120 Biank 

# Date = 06r21/2008 

# 3ime

- 

## 13= 38:54

_.102 _ 400m41 10, ?f .0r70;n'w 

# Campanent Ratenti Rrea Exfiernal



# Component Number Retention Area External !lriits

0 0.00 0.00



# 130

# 1833.50 

# m 20.84

1553.60 M 20.33 Fl- 1.



# c l• 1.56 Conditions : Daltile, tc-I Paso

: 19..9 ug/ml Fl- in H20
: 20 

# ug/ml Cl- in H20 Date : 06/21/2008 Time • 13."41:4•0

---102.400mV 102/1 .000,mV Componen'L Retention AreiL



# Fl— 

# c 

# l-. Component

K Number Retention

I I ., 016 2 1.566 Ar ea External Units 1833,50 

# m 20.84 ug/rn.1 1553.60 M 20.33 ug/ml.

3387.10 41-16



# 13 1,

6-F A.

## Gampopent



# ( unkDown )

# FlF1- - l n 2

~ 

# r_;. (.)O m V

4ei:enti

0.81 

# 4.


# 1.43 :1.024 .. 0OOmV 

# Area Extprr,u l

104.60 M N/A 417.94 Pi 4.53


# 258.20 m 2,84 Conditions : 4.98 ug/ml F1- in H2SO4



## = 5.0 ug/mi C1- in H2SC34 Date : 06/21/2008 Time = 13:54-50



# Component 

# Number Retention Area Extel - nal Units

F l - 1 0 

## ..9bb 417 . 90 , M 4.53 ug/mJ. 

# F :L - 3_ 1 y 433 258.20 M 2.80 ug/m ].

L 

# 676.10 7.33



# 132

## Area External

120.70•M NA 396.80 M 4.30

254.80 M 2.76 Conditi-ons z 4.98 ug/ml Fl- in H2SO4

: 5.0 uo/ml Cl- in H2SO4 Date : 06/21/2008 Time z 14:07:22

-1.02.400mV OMPOMIL v



## (unknown) 0.7 Fl- 0.
Fl- 1.3 10-71 , .00OMV



## iort



# .................

50 ,

2 

# ....... ; i



# 31

................. ..................... ................ .......................................

Component

Fl— 

## F. 1 —

2 Number Retention Area External Units

1 0.0016 396,80 

## lvi 4.30 ug/ml 1. 1.383 254.80 M 2.76 ug/ml

651.60 7-07*



# 133

## Condx.tions = 9 .95 ug '/rnl F1- in I-E2St34 - 10_0 ug/ml O1-

~ 

## Ln H2504 C a

- t.^ = 46/21 /2008 Tlme -

~ 

## 4 - 16 - 15



# —102 A.00mv , Component Retent i o~ 

# 1.....

~ ~ 

# ....... ......................_..-_......

~ 

# ,... ~~ 

# ... ~ 

# ....._._..... -......._........._._..._......_.-......._.......

~ 

# _......... ~ 

# ......... ~



# F1

- 

# o. F1- 1.4 

# 1 0? 4 .:? 0 C7 mV

.... ..,._............ ~ . 

# .............. ......... M..

~ 

# .........;

~ 

# i

,..::.... .....:::,:, ;

~; ;w ~



# . I 

# b5 ~ 

## .. 

# ' : l .; ........... 

# ~
z
M .... 

# : - t

. ~ 

# 31

. ..... : !

. , i • 3 E ' ] i • J J 1



### ' E 4

; • ~

~~~ 

### ...... : ~ i •

. ~



## 6 .... ; 

# PreaE Ezternal

753.90 M 8.$8
574.45 M 5,81

Cotnponent Nuber Retention

~ 

## " I. — ]. 0.983 

# F 1. ••- 1 1.466

2 

# 4rea External Uni

- L

- s
753 . 90 m 8.88 ug/ml 570.05 M 6.81 k..t g/ rn .!.

1323.95 15.70



# 134

## Conditioiis 

## 9.95 ug/ml Fl- in H25O4 

## 10.0 ug/ml 

## Cl- in H2SO4 Date 

## 06/21/2008 T'ime =14:18:59



# ---I, 02.4-00MV ComponeSt Retent 10'.'->4.O4OmV ATP,3 * 

## External



# Fl• 0.
Fl• 1.4 ............ .



## 33



# 2.

. . .....



# ~ 

# : j 31
...... : 

# ~

4

6

...... . ........ . . ....... . .... ...... ....... 772.45 14 

## 9.09


# 551.84 m 6.61

Component Number Retention Area External Units



## 1. 0.983 772.45 M 

## 9.09 lig/M.1 .1. 1.433 

## 551.80 11 6.,61 

# ug/rn].

2 1324.25 

## 15.70



# 135

# Component

(unknown)

# rlC1- - 1.02 ., f•O0rnV



# Retent'

D : 8

1.5 

# 107,14 M 3193.40 M
2440.10 H 1 02 4 . d00rriV 

# Area L-ExternaJ



# NlA 38.24
33.41 

# Conditions 39.8 ug/ml F1-- in H2SO4

= 40.0 uO/ml C-'a.-- in H2s04 Oate : 0611/21/2008 Ti- me - 14 = 4-9= 18



# Component 

# Number Retention Area Externa.l Units
F l -. C 

# l_ ~ 

## :1. .. OQ0 ? 1 ~:~ . ~ O I~i 

## 2 1.500 2440.10 M 

# :38 . 2f. u

~ 

# /rn1 33.01. ug/. ma.

2 

# 5633.50 71.25



# 13 6

## 1.024. 000mv 

# Area External _.102 , f•Oamkt 

# Component RetAnti

4.8f 

# I.
1.48 N/A



## , 39,i6

28.77 

# ;unkno,n) F1- Fl_ 

# 544.70 M 3253.40 M
2471.30 ri 

# Conditions = 3a.8 ug/ml FI-- in N2SO4

: 40.0 ug/ml Cl-- in H2SO4 Date = 06/21/2008 T i me - 14= 52 ` 23



# Com¢one7t Number Retenta.on Area External Units

Fl— 1 1.000 "' 1 1263 . 4.O Ni :39 . 16 ug/m1. F :I. 1. 1.483 , 2471. .20 ivl 

## 28.77

~ 

## w!q/m:l

2 5734.70 67.94



# I .l 7~~'~ 

## 24 .!3CaOm`J 

## Area External



# 114.10 M Nlk 1648.40 M 18.49
1148.74 M 

# 13.67 — 102 . 4OOmV 

## Companent Retenti

(«nknawn) 0.81 F1- 4.


# F1- 1.46 Conc4xtions I 0 ,.9 L!glmi Fl-- zn H2504

- 20.0 ug/mi C i -- 1n H2_S

~ 

## }4 

## Date 06/21/2008 Time = 15=01.05



## Component Number Retention Area 

# ExternaI Units

F l — a. 0.983 a. 64 8-4a Ni 18.49 u.c/ml F1— 1 1.466 3.1.48.70 M 1:3.57 t.3c;/mI.

2 2797.10 32.16



# 13 . 8

## Conditions 

## 19-9 ug"/Ml Fl- in H2SO4 20-0 ug/ml. 

# CI-

- i-t"; 11412SO4 

# Date 06/2112008 

# T i me 15:03:215 -

-102.. 400mV Pvomponent ReteDti



# (Unhown) 0.81 C 

# l-

4 

# 0.


# Fl- 1.45 1024.000niV



# 01

........................ ........... . ................. *

............. . . . ......... ............ .................. ................................ ...................................... ............................................. ............................... . ..............



# 6 

# 1

'*
.................... ............ .

...........

........................ .... .....

..... ............ 

## 2 

# ~ ~

.., ; •

. .



# 3

~ ~ i 

# 4

61

.................................... . ...................................................... . . . ..... ............................ . . ........... . .......................................................... ..................... .............. ....... 

## Area 

# . External



# 100.95 m N/A 1642.10 M 18.43


## 1191.50 m 14.08



# Component Number Petention 

## Area 

# External Units

F 1. - 1, 

# 0 -0 , 8:3 1 

# 6 

# 42.. 10 M 18.43 ug/rnl F 

# 3, -- 

# J. 1. 

# 450 11. 9 1 . 50 M



# 2 2833.60 

# _32-51

## fiM0LJNT IN.3ECTED



# AREA 0.000 0.000

7,228 - 400 

## 39.800

1

2
3

2

S 

# Cal.zbra

- txon fl i c- - F

~ 

# -- w cal

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~ 

# 80.40 Y-

- a>, is i nt wr ce.pt r 0.00 

# C©eff o•r

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# 0.91

No . Area Amount CF

0 : 0.000

0, OC}0 0.000 l. 4•07 w 35C) 4.980 81 .797 2 : 763 . 1.75 -9 .950 76 .701 3: 1645.250 19 .. 900 82 .. h76 4 ' 3228 . 4-00 1 

## 39.800 81 ., 1. 1.6



# 140

## ANfOUhlT INj ECTED

AhEA 0.000 

## 0.000

2.G-55.?0O 40 .000

~

~

7



## 4

5 

# CallbratlOYi flle = Gl

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# Avg slope of curve = 59.35 Y-ax i. s i nter wc:pt ° 0.00 

# Coe'ff af l i n regr . 0.92
N10 . Are

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# Amou.nfi C1=

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~ 

## 'i6 ,. 500. 5. 0() 0 51 .1

- 3)0 0 2 5 !,

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## 0 . ~ ~ 5 10 

## .000 !;1 6 . 0 % `

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## 1.170..100 20 .. 000 58 .. 5Ca5 4 -' 2455,700 4 0

~ 

## 0 00 61
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## '' g?



# I . 41

# Conditions Daltiale El 

# Pas©, Combined Kiln Exhaust. Run #I 

# Imps 2 & 3 

# VolLime 300 

# Dilution 1/1 

# Datp- = 06/21/2008 

# Time 15:13:10



# -102..4OOmV Compoped - 

# Retenti

Fl 

# - I . cl - 1.50 

# 1024.000m%/



# on

........... . .................... ............... ...... .. .. ......... .. ......................... ......................................................... ................................ ............................ ...... .............................



# 01

.................. . ....... . ............. 

## 2

41,


# 5~ .....•.,. : 1



# 6

........ ................. ............ .. ... .. ........................ ..... ........... ..................... ..... ................. . ............. .... ... ............. 

# Area LEXteTIM)

1521.30 18.50


# 194 .30 

# M 3,79

Component



## F

2 

# Number Retention Area External Units

1 1.000

1 1. 

# Fj 2 1. ., 3 0 .1. 8 1,500 

# 1.94..3() m '79 (.!q/M.I.



## 1715-60 22,29



# 142

# Conditions z 

# Dal'tile El Paso, .Combined Kiln Exhaust 

# .0,un -41 

# Imp-s 2 & 3 

# Volume. 300 

# Dilution 1/1 Date 

## : 06/21/2008 Time 

## : 15:15:27

- 

## 102.4OOmV uomponent KetWl



# Fl- 1. 

# Fl• 1.46 1024.00OmV 011 *

................... ........... . .... ....................... . ..................... ......... .......... .... .......................................... .. ............................................................ . ...... ......

t (( 

# ` i

..... . . . ..... . . 

## .............
6



# 2



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~

....... ......... . ....................................... . ................. . ................. .... .... ..... . .................. .......................... . ............................... ... . ............ ...... . ............ . .......................... 1 

# Ai-ea Exl6ernal

1485.40 18.1(
333.80 H 

# 4.OE

f-'omponen• Number Retention Area External Units


# F.1 - 1.000 1. /1. a 5 Al. 0 1 

# "R 1. 0 k A g o /I m I 

# -F- , I - I « 466 211"T.113'.80 M 0 8 1,



# 2 1819.20 22«18



# 143

## F1-



# FI1.

1. --102 . 4OOmV 

# uomponent Re

~ 

# en

.'' 1024 .00OmV 

# Area Exterral

1756,30 21.34
236.44 M 2.89 Gonditions : Dalt i le E1 Paso , Cambi ned K1 I rE Exhaus't

:Ru n.42 I ntps 2 & 3 = Vvlurne 300 Diluti®n 1/1 Da.te : 06f21f200$ Time : 15:23.

- 58



# Number Retention Area External Units

1 000 1, 7 5 4. .1. . ? C`a ka g / m 1. 1. 2:3 

## r , _ 4 0 11 

## 2 ,. ~ 

## 3 fn 1..

1992.70 24.19 Component



# F.l°_

?



# 144

# Conuitions 7 Da1tilE E1 Paso, Combined Ki.l.n LE-xhaust : Run #2 ImRs 2 & 3 = Volume 300 Da.lution 1/1 Date : 06/21/2008 Time = 15-26= 3.9

--102 . 4GOmW 

## Compcnent Retent'



# F1- 1.


# F1- 1.4 1024 .00DmV 

# Prea Frternal

1756,14 21,25
252.75 M 3,09



# ct.. a= .l, - 

# Component

2 

# Number Retention

1 1 ,. 0 J. Cy 1 1. .. 41. 6 s:.. 

# Ar en Exter r,a 1. Units

'1 Y56, '.l. f 7 ? 1

~ 

## 2 n 2 5 ? _ 7 5 M

2008.85 24 _ 3S

, 

# 145

## Fl

## C1- 

# 1.

1, 20.17
3.41 

# 1666.60
175.a5 P1 -102 .4OOmV Component 4eten

. 1024 .0O(JmV 

# Area Er,ternal Conditions :Daitile Ei Paso, Combined Kiln Enhau,t

= Ru n #? Irnps 2 & 3 = Volume 340 Di lution I.lI [3ats = 06l21f2408 

# Time = a '

~ 

# J : ..s5 = 2'J

Compon2nt

~ ~



# Number Retention Ar2a E>cttirnal Units

~ 

## . :;. ., t)Q ~ ~'~f~~ ,. ~a~ ~?C~ ~ 

## 1.: +. ~~ ~m~. 

## :, . ? .1 . 500 1. :r ~'~ 

## , ( 7 5 M '-I w A. 1. ta g / m .l.



## 1841.65 2?.5H

# Conditions : Dalt.i.le El Paso ; Combined !:i 1n E'xhaust = Qun #3 Imps 2 & 3 

# = Volume 300 Dilution 1/.I Date = 06/21f2008 

# Time : 25=37-38

--'! 0;'> . 440mV Component Rpten' .



# F1- 1.
C1

- 

## 1. 

# 1024 . 00amV Area Exteroa]

1684,95 20.RC


# 183.74 Pf 3.58

~ 

# (: ]. Cocnponent ~ -

~ . 

## 5~ 

# ...._ :

I 

# .. .._... ...... _....:

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:l . :l. . 000 2 1,466 

# Prea Exte*rna.l tJna.ts

1.684. .9S 20 .. 40 ;.tc

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## /m 1 18;' ., 70 M 3 .58 t.),g/m l.



# 2 1868.65 23 .98



# 147

## Compone7t



# (unknot

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# Reten±i

0.81 1 Q2..4 . JOOmV 

# Area

~ 

# xterna ~



## 241.74 N/A 

# Cvnditions = Daltile Eil. ?aao, Cambined Kiln Exhauct

= 112SO4 B lan lc 

## Date = 06/21/2008 Time = 15-48-57

Component NumbeY Retention 

# Area External Units

0 D _ 0O 0 _ 00

1•

~ 

### i

# Concii tions = Daltila El Paso ; Combined Ki ln Exhas:---.t = 19. 0 1 ug7ml F1--- i n 1-12SO4 

# = 20 ug/ml Cl -- i n H2SO4 Date = 06i21 /2^08 

# Time " 15:58-16

~ 

## .102 '' O RI V :f 0?f , ") 00mV 

# compnDent R.:tentiot;_
- 

# Rrea EXterna:

i 1

- 

# 0.


# Ci

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# 1. 1710.74 hi 24.1e
1134.44 M 19.45

F L ... c 1 ,... 

# Component

2 

# Number Retentzan

1 0,983 ;? 1. _ rt:

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# Area Externa]. Units

1710.70 h'I 24.,72 u.I, -Ifml 

# 1.1 : !!

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# . f [ ( ) Ni :l. 9 . fa .l l.,!

2845.10

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## ~ 

# Fluoride:.Standard • : t ,

; _ .. ..Component 'Concentr.a'fion 

# : ~mg/~,~ • 

# • . •Fluoride 995 -4- 2

The concentration value is based on proven , reliable methods of analysis. • The estirnated uncertainties are two standard deviations of the concentration values. T.he concentration value is warranted to be stable for three months from the date of shipment. The preparation and analyses of the Fluoride Standard was performed with eatreme care by DIONEX Corporation Consumables Manufacturing Department.

i:ocumatt N.o. C'34 l E3-; F i-'
, -Dec-G2 

# 150

.rtex Dione: Dione:lntematianal SQtrsidiaries 

### aiorie.

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The concentration value is -based on. proveii- reliable methods- of analysis. The est . i . mated uncertainties -a're -two standard deviatiOns.of the coh. centration values

. . 3'h6 'concentrafion vdlue•'is war-ranted to be stabl.e -for -three months, from the:date of shipment.
The preparation and analyses of the Chloride Standard was perfonned with extreme care by the DIONEX Co *oration Consumables Manufacturip.6 n,- arftnent.

rp c, --p

Document No. 

### 034184-25 20 May 

### 1998

.nex Carpor2tior nionex u.s. negiortal Olfires 7&-:'.1V!: Summels, CA (405) 737-2522 -,603 IL (F•; - SS' _E': "ZM t 84 f_t6ll?

(3" U7 ISII) Diam interitational Subsidiaries •lis"ria (D 1 ; 61 6 51 2 ! Gorinany(025) 9;1,J0 (03' 4134 

## w

- , or. 5 -, 

## so 52
f')7hP (852) 21M 3282 Kow (2) K53-25801 Dmwk (45) ' 13; Y' 90 9.1 Tne 11s,'trianz t Tl 61) 4B 43 03 Frimx(Cf. , 39 30 C-1 10 Swilzarkwd (MI, 205 9" 65

;in W;,;. N 'r M'k w'x a AN M 131 E- 03 1 %-1 31C4 Clz' 

## , 2004 DialiPs CUP01,11jOr,

## Cl.:Lent: Arm.strong Eavironm,er3tal, Inc. Report nate: 06/25/08 174 8 Hlavek Rd. sampl e y:a*.ri,:, __. ters / Yr_r.'es.ra_:r.i r;,IF ;, a . 

## Decatur, TX 76234 Date Col?ected: 06/17/08 Collected By: Client Attn: Mr. Tom Armstrong 

## Date Received: 06/21/08 

## Email: 

## Armst@ix.netcom.com Time Received: 11:40am Phone: 1-214-631-0021 CHEMTEX FILE #: P8060658

--------------------------------------------------------------------------------------



# ~ IHA Laboratory# 1014 

# 7] 

# n e la p certffrcate # T104704239-08-7 RESULTS OF AlqAEY.SIS

ATame of IIai t: Daltile, E3. Paso Combi.aed KiZn Exhaus t


## Sample SamQle Volume Results 2ML Identification Parameter (lit) mg/sample mg/sample 

## R4 Imbs Lead 345 0.010 0.001 P,un 4

~ 

## PU7 210 

## R4 Filter ---
R5 Imps Lead 305 < 0.001 

## O.00i Run 5 PIr7 1~ 

### Q 

## R5 Filter
R6 Imps Lead 280 0.003 0.001 

## Run 6 PW 215 

## P,6 Filter

B1aak: Lead "175 < 0.001 

## 0.001 Filter CHF2STEX 

## # P8060658+ P8060661+ P8060665

P8060659+ P8060662+ 

## P8060666

P8060660+ P8060663+ 

## Pp060667
Pg060664-• 

## P806066g

LABORATORY QUALITY ASSURANCE/QUALITY CONTROL DATA

LAHORATORY CONTROL SAMPLE (LCS) RECOVERY

d:3211° :@r i nit$ • 1'cfl UF3 O • ,.7ta_itF'd Ial Ue •dor''i 1 t
c.tf'aG - Rl j/l 501 . . 4Fi ~

IMETSOD REFERENCES/AIVALYSIS DATES & ANALYSTS



## Parameter Method Reference Date Analyzed/Fr.a? ysts Lead 40 CFR, Part 60, Appendix A, Method 12 06/25/08 KSP./NR

------------------------------- 

## Dr. . C. 2J . t?ecidy, Ph . D, 

## CIH, ASP i;v/ i:m1 I4R. 

## Director

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# 1495

## PARTICULATE ANALYTICAL DATA FORM

Company: Daltile, El Paso, TX 

### Date: 6/19/08 Location: Baghouse Exhaust 

### Run 1
Density (Pa)
Blank Concentration (Ca) Rinse Volume (Vaw) Residue in Rinse (Wa) = Ca*Vaw*Pa 

### 0.0007

Date of Weighing

Time Gross Weight
Date of Weighing

Time Gross Weight 

### Run 2

......... . . 0.0006

5 5 Run 3



## i 0: 0.0006 

## 90 - -.0. 8;:. T*0$ AIO:



## :A? .06

Date of Weighing

Time Beaker Tare Weight
Date of Weighing 

## V9

. 0 Time Beaker Tare Weight
Average Gross Weight 

### 100.3992 94.5054 103.9117 Less Blank Residue (Wa) 

### 0.0006 0.0006 Average Beaker Tare Weight 

### 94.4600
Weight of Particulate in Rinse (mg) A A 

### 51.99



## ACETONE BLANK ANALYTICAL DATA FORM

Blank Volume (Va) Date of Weighing

Time Gross Weight
Date of Weighing

Time 

### P. Gross Weight
Average Gross Weight 

### 111.5294
Date of Weighing

Time 

### A. Tare Weight
Date of Weighing il 

### WOO

Time Ta.re Weight 

## $5

Average Tare Weight 

### 111.52865
Weight of Blank (Ma) 

### 0.00075 Ca= Ma/(Va**Pa) = mg/g 

### 0.00382
Note: In no case should a blank residue greater than 0.01 mg/g or 0.0010/ 1" of the blank 

### lweight be subtracted from the sample weight. 

# 1i.16

## FILTER ANALITICAL DATA

Company: Daltile, EI Paso, TX Date: 6/19108 Location: Baghouse Exhaust Run 1 Run 2 Run 3

Filter ID Number
Date of Weighing

Time Gross Filter Wt.
Date of Weighing

Time Fl


## ~ : 

## Gross Filter Wt.
Ave. Gross Filter Wt, 0.3849 0.3929 

## 0.4050
Date of Weighing



# Time :~ 

# :5v;P

~ 

# l: Fifter Tare Wt.
Date of Weighin0



# Time ''I:1::I

~ 

# fi:

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# 1f

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# : :<( ~ 

## Filter Tare Wt. :Q;~6~~i ;Q;~~~O: ;#~:~~:~$::



## Ave. Filter Tare Wt. 0.3621 0.3650 0.3798


## Wt. of PM on Filter (grams) 0.0228 0.0279 

## 0.0252
Total Weight of Particulate (rng) 22.8 27.9 25.2



# 1 1 5 7

## PARTICULATE ANALYTICAL DATA FORM
Company: Daltile, El Paso, TX Date: 6/19/08 Location: Baghouse Exhaust 

## Run 1 Run 2 Run 3 Density (Pa)
Blank Concentration (Ca) Rinse Volume (Vaw) Residue in Rinse (Wa) = Ca*Vaw*Pa 

### 0.0014

. 0.0015 0.0015

Date of Weighing

Time 

### 5 A' Gross Weight 

### i .'40 

### 7 4-*


### Date of Weighing

Time Gross Weight

Date of Weighing

Time Beaker Tare Weight
Date of Weighing

Time Beaker Tare Weight
Average Gross Weight Less Blank Residue (Wa) Average Beaker Tare Weight
Weight of Particulate in Rinse (mg) 

### -M

96.0088 0.0014 96.0021



### 5.28, 

# w

103.8182

— I 

### 93.4074 0.0015 93.3975

8.50



## H20 BLANK ANALYTICAL DATA FORM
Blank Volume (Va) Date of Weighing

Time Gross Weight
Date of Weighing 

### .2 y

Time Gross Weight
Average Gross Weight 

### 100.2623
Date of Weighing

Time Tare Weight
Date of Weighing

Time Tare Weight
Average Tare Weight 

### 100.2608
Weight of Blank (Ma) 

### 0.0015 Ca= Ma/(Va
, "-Pa) = g/S 

### 6E•06
Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of thp blank 

### lweight be subtracted from the sample weight. 

# 1 9 1t 

# 8

# Armstrong Environmental, Inc.



# 1748 Hlavek Rd Decatur, TX 

# 76234 CHAIN OF,CUSTODY RECORD - - 

# 1

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# Armstrong Environmental, Inc. 1748 Hlavek Rd Decatur, TX 76234 

# _"USTODY RECORD 

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# 1748 Hlavek Rd Decatur l TX 76234 1)[1014E MO. 

# (214) , 631-002 1 cn 

# C-C V-4
CHAIN OF 

# CUS-TODY RECORD



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Copy lo ("holil/Projed Cooldinalof

# FILTEP, ANALITICAL DATA

Company: Date: ~ 

## l

Location: 

# Run ;r: ki i

Filtnr ID hiurnber C) 'LL Date of Weighing &6 

# l a - ~ 

# Z`tIti ~



## Tirne Gross Filter Wt. ' 1 2 '1
Date ot We9ghing 'Lq o 6 17'" o?

Time 

# `Q g fto:b? Gross FiIter Wt. 

# 33q 1 .?,fla ~ Ave. Gross Filter VVt
Date o7 Weighing 7-7/ 0 6 C" t?`a

~ — 

# /2e7/

~ 

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# ,S` 

# l : sr

_ Filter Tare Wt.
Date of Weiahing

~ 

## azSlal

Tirne yi : ar

, ~ 

## ` It: o 6 

## t: d`' d F itter Tare Wt.

. Z-O ' o 0. 3

Ava. Filter Tare Wt.
Wt. ol' PM on F ilter (grams)
V1rt. oT PM in P.inse (grams)
T otal Weight of Parriculate (mg)



# 164

# F IL i CP, f;NALl i ICAL DA i A

Company: Date: Locafion: Run i~: ~1~, 

# R ,~ 

# k, ' l~



# _ Filter ID Nlumher



# Dat e oi W eighing
' 

### ! • . 

## Gross r ilter Vd't. o 

## c~ ~ 3 

# `O ~ ~ 

# _ 6 .3e 7

Da#e o ~ 

## Weigning ~



# Gross Filter Wt.

~ ,T+"'1°

l



## Ave. Gross rliter VNt. 

## Date ot Waighing A . ~

i im-3 

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## %

~ 

## • .3



## Date o ~ V~~ 

## Aighing ~ Z7 0 

# Z eoy 

## Time 5

°
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## : S
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### ~! ~`~

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~ 

# . `

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# [1.

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# S . 3

Ave. Fiit?r ?ara Wt. 

# Wt. of PIJ on F ilter (grams)

Wt. o; PNi ir► 

## P,insa (grams)
i otal l'Veignt o ~ 

## Parzioula e (mg)

1 

# J.

~ 

# 5

# F ILTFR ANIALITICAL DA T A

Company: Date:

Run ' rr: 

# Locafion:

~ ? 7 ~ 6a,S 

## ~ ~~ f~ i ,•1


# Filter ID NumAar 101 , 

# /

Date o

- I lNeighing A Lo

, 

## Time o Gross F ilter Wt.

Date o

- I Weighing 6 2" Q9 

# I N Time 

# 14;0
, 9 +2Z.- Gross Filter Wt.

Ave. Gross Filter Wt.



# Date o ~ W 

# e ighing ZC^ O 

# , 1.~ ~ 

# _.

.3 v 

# T ima ; Fiiter Tare Wt. .37 `7 S
Date os Weighing

-



# 4 2,74 3 L7 o

~ 

# Li

- 

# 7, ~
Filt?r Tare Vdt.
, ' 37' ~


## Ave. Filt?r T are Wt.
Wt of F1JI on Filter (grams)
Vti't. ot PM in P,inse (grams) 

# T otal Vdzight off Farticulaje (mg)



# 196

## PART|C NALYT\C

~ -7 ~R~ 

## RKq



# Nd \ Q / . ,

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B\mnhConnaniration(Co) Rins:»olum* (Vo"4 Reuidyo in Rinse (wa)= Ce°Vaw°pa

Da|e o,»vai0hing

Time Grnss«vo)ght

Dote n

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## ««e

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## h|nQ

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Time ' G'ossv«migh ~



## -

` DaiyofWeighn0 x 

# A /ce
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## Dotecdwmizh>ng 

# /03

Tinne BsaxorTareWyV,gh` Average C-rnosvYmgh't LossB|ankReu>duo(Wa) A'orago 3yoke1-Ta,wvva)ght

. wpighf o| particu|ate in Rinoa<mg> '

'

~ ~~py 

## JL«» K

## P/\RT|CUL/\TE |C ~L[~~~ 15 

## ,FOP,Kq
Cnmpany

: 

## /

Y ~~~|~~^ 

## Dmtwt ^ 82

- 

## Locat i 

## on : 

## ( " nunz Run2 Pun3 Donoity(

~~ 

## ) i
B>ankCononnt,a

- tion(Cm) Rinsw «n } umm(vmw) L/ Residue in Rinxn (wa)= Ca°vaw°pa --- ~^~ 

## ~--- ----- ~-~ 

## --- --- ~-~ 

## —~--

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# toy— Ti'rne GrnuxWe)ght `

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## ghing

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# ko (aq

//rnw lizi o ' GrosoWeight

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# NSS Dn woiWeighing 

# /0 / / c ) /o y 1 

# 1 .

0 //mw ' BsokerTam Ww gh merageGmos»»aight Less8|ankRssidue- (We) 4'nragm Beoke,Torn h

~ 

## waight of Perticu\ato in Rinse (rnQ) '

' '

~~u"~~

## PART|t.

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## ?' 6 , 70 RK4 ~~7 > `/ [1 ~ 

## /f,` Cnnnpany

:

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## "«i' Datm! Locatinn ~ 

## RunI' Run2

B|ankConuentnat\on(Cm) R|n»m«n|umm (Vaw) Rmsidum in Rinse(w3)= Co°Vaw°Pa

Oete oYwe) '

grhin0
nrne Qros»«oight batm nfVve|ghing

Ti,na QrossVYsight

- D

~ 

## '

te /

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## - Weighing

. //rne Beaky, Ta'e vwa\ght Datponweiztin0

Tima Bsmxmr Taro Weight A«ara@mQroauYvmght Less g|onk Rosidum (Na) A,erage 8ymkmrTere vvo\ght 

# OvIa

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F.' u n 3



## 169

# P A 

# P. T.1 C

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# L A 

# Tt - A N A 

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## P, M


# Company: 

# P

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# ._ Dat

~ 

# ! LocBtion: 

# R un 

# 17 i3un 2
Density (Pa)
Blank Concen-kration (Ca) ~ 

# Rinse Volume 

# (V?.W)

~ 

# esldue ir) Rinse (Wa) 

# = Ca*VawF>a

Date of Weighing 

# d24 j~0~ 2~ Od n 

# T i in e 

# L !97 o t 

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# t):2 - Z 

# W2-

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# .3 , q 5r Gross Weight

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# 3 1 /00

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# /a i1g)



# Ti nn e 

# 7 2-'9'

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# ), Zi 7. i q- 1 1 51, Id 55 Date ol Weighing

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# 41- 2 4a 1



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# Welight
Weight o-l' Particulate in Rinse (Mg) 

# T 6

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# C)

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# Ad

121(106 

# 1747



# 1 2 

# ,6. t'17 L)



# 1 70'

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## ion:



## Densit

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volume (Vaw) ;?esi•,

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## Ca`e of Weighing

Ti'i—.ia G-oss Weight a)a-a of Waig7ing

I ii71e 

## Gross Weight

Da e o= Weighing

T Iii1e 3e3k°i a?'e W°ighi
D3te ot vdeighing



## i ime 

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# !

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# 1~ 

# 1~



# PLANT: DATE: 4-1 1

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# T: LOCATION (SOV

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# 2CE n): G a

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# FiELD D A'TA ~



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# STACK DIAMETER: 53 

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# 186APE Armstrong Environmental lnc. CONVERSION FACTORS EPA Method 5 

### 522 Series Meler t3ox Calibration 1 mm Hg = 0.13330 kPa Pre-Test Orifice Melhod 1 cm = 0.39370 inch English Melor Box Units, English IC Faclor 1 mm = 0.03937 inch 1 cu ft = 28.32 liters r Box >t 10 Date: --- ---- ----- ----»--»-> 05/28/08 iI !i: 30272 Baromelric Pressure: •-•-»-•»> 29.40 (in. Hg) Theoretical Critical Vacuum:---> 13.87 (in. Hg)

!I 

### )RTAf\ For valid tesl results, the Actuai Vacuum should be 1 to 2 in. Hg greater than the Theoretical Critical Vacuum shown above. )RTAt` The Critical Orifice Coefrrcient, K', musl be entered in Engiisti units, (ft)"3'(deg R)^0.5/((in.Hg)'(min)). !I

-»---»----•- DRY GAS METER READINGS -------------- -CRITICAL ORIFICE READINGS-
-- Average Temperatures -

Vofume Voiurne Voiume (nitial Temps. Final Temps. Orifice IC Oritice Actual - Ambient Temperature - DGM DGM Ambient 

### H Timo Initial Final Tolai Inlot Outlet Inlet Outlet Serial# Coefficient Vacuum Initial Final Average Oullot Overail Temp 20) (min) (cu tl) (cu (1) (cu fl) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (deg R) 0.24 5.00 407.662 409.232 1.570 75.0 75.0 77.0 76.0 40 0.242 22.0 76.0 76.0 76.0 535.5 535.8 536.0 0.48 5.00 409.321 411.580 2.259 77.0 76.0 77.0 77.0 48 0.344 20.0 76.0 76.0 76.0 536.5 536.8 536.0 0.90 3.00 411.685 414.737 3.052 77.0 77.0 78.0 77.0 55 0.464 18.0 76.0 76.0 76.0 537.0 537.3 536.0 1.50 5.00 414.737 418.644 3.907 78.0 77.0 80.0 78.0 63 0.593 16.0 76.0 76.0 76.0 537.5 538.3 536.0 2.70 5.00 418.644 424.050 5.406 79.0 ' 78.0 82.0 79.0 73 0.824 13.0 76.0 76.0 70.0 538.5 539.6 536.0


## ............................................. RESULTS ..........,............................,...,.......

tY GAS METER --- ---- ---- ORIFICE --------- -- DRY GAS METER -- --------- ORIFICE



### JME VOLUME RECT CORRECTED i(sld) Vm(sld) ;cu (t) (liters) 1.521 0.1 2.185 0.1 2.953 0.1 3.779 0.1 5.232 0.2 

## VOLUME VOLUME VOLUME CORRECT CORRECT NOMiNAL Vcr(std) Vcr(sld) Vcr (cu n) piters) (cu ft) 1.538 0.1 1.590 2.186 0.1 2.259 2.946 0.1 3.044 3.768 0.1 3.894 5.231 0.2 5.406 

# Average Y -------> CALIBRATION FACTOR Y Value Variation (number) (number) 1.012 0.010 1.000 -0.001 0.998 -0.004 0.997 -0.004 1.000 -0.002 

# 1.001 CALIBRATION FACTOR dH@ Vnlue Variation (in H20) (in H20) 1.381 -0.0041 1.366 -0.020 1.409 0.024 1.434 0.049 1.337 -0.049 

# 1.386 <------- Average dH@_,

For Calibrnlion Faclor Y, the ralio or the reading of tlre calibration meler to Ihe dry gas meter, cceptable loierance of individual vaiues from Ihe average is +-0.02.

or Orifit:e Calibration Factor dFJ e 

### ~ c iff 

### ~ ntial pre6sure in inches of H201hat equates to 0.75 cfm of air t 68 F and 29.92 inches , cceptabl oleral



### ~ ce o( in iduat valuas from the average is +-0.2.

SIGNED: 

### ~-!~

~ r ~~ ? Date: / v ~ 

## ./

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## Temperature Meter Calibrations

Meter Box #: 10 Date: 05/28/08 Calibrated By: TA

Emtech Thermo Degrees F Checker Probe Stack Oven Exit Auxillary

Point 1 32 35 35 36 34 34

Point 2 212 214 212 213 212 212

Point 3 752 743 742 743 742 742

Emtech Thermo Degrees R Checker Probe Stack Oven Exit Auxillary

Point 1 492 495 495 496 494 494

Point 2 672 674 672 673 672 672

Point 3 1212 1203 1202 1203 1202 1202

Percent Difference Probe Stack Oven Exit Auxillary

Point 1 0.609756 0.609756 0.813008 0.406504 0.406504

Point 2 0.297619 0 0.14881 0 0

Point 3 -0.74257 -0.82508 -0.74257 -0.82508 -0.82508



# .•. 

# •Armstrong Environmental Inc. CONVERSION FACTORS
EPA Method 5 511 Series Meter Box Calibration 1 mm Hg 0.13330 kPa Post•Test Orifice Mr+thod 1 cm ~ 0.39370 inch 

### English Meter Box Units, English K' Factor t mm

~ 

### 0.03937 inch 1 cu R a 28.32 iiters
3r Box A 10 Date: ------ -------- ---------- > 08/30/08 al #: :30272 Barometric Pressure: ---------> 29.45 (In. Hg) Theoretical Critical Vacuum:---> 13.89 (in. Hg)

!II 

### ORTAh For valid test resutts, the Actual Vacuurn should be 1 to 2 In. Hg greater than the Theoretical Criticai

. Vacuum shown above. ORTAN The Critical Orifice Coefiicient, K', must be entered in English units, (ft)"3'(deg R)"0.5/((in.Hg) 8 (min)). !II

---- -------- -- DRY GAS METER READINGS ------ --- -CRITICAL ORIFICE READINGSTheoretical Critical Vacuum:---> 13.89 (in. Hg) 

### Volume Volume Volume Initial Temps. Final Temps. Oririce K' Oriflce Actual -- Ambient Temperature -- DGM DGM Ambient
iH Time Initial Final Total Inlet Outlet Iniet Outlet Serial# Coefficient Vacuum Initial Finai Average Outlet Overali Temp 

### 120) (niin) (cu ft) (cu ft) (cu ft) (deg F) (deg F) (deg F) (deg F) (number) (see above) (ln Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (deg R)
0.91 5.00 539.136 542.196 3.060 76.0 76.0 77.0 77.0 55 0.464 19.0 75.0 75.0 75.0 536.5 538.5 535.0 0.91 5.00 542.198 545.249 3.053 77.0 77.0 77.0 77.0 55 0.464 19.0 75.0 75.0 75.0 537.0 537.0 535.0 0.90 5.00 545.249 548.298 3.049 77.0 77.0 77.0 77.0 55 0.464 19.0 75.0 75.0 75.0 537.0 537.0 535.0

.............................................. RESULTS ....... .. ........ ....... ...... ...... .....

..........

RY GAS METER --- ----- ---- ORIFICE -- DRY GAS METER --

UME VOLUME VOLUME VOLUME VOLUME CALIBRATION FACTOft RECT CORRECTED CORRECTED CORRECT NOMINAL Y •n(std) Vrn(std) Vcr(std) Vcr(std) Vcr Vatue Variation (cu ft) (liters) (cu ft) (liters) (cu ft) (number) (number) 2.970 0.1 2.953 0.1 3.041 0.994 -0.003 2.960 0.1 2.953 0.1 3.041 0.998 0.001 2.956 0.1 2.953 0.1 3.041 0.999 0.002 

# Average Y -------> 0.997

: For Calibration Factor Y, the ratio of the reading of the caiibration meter to the dry gas meter, acceptable toierance of individual values from the average is +-0.02. ORIFICE

CALIBRATION FACTOR dH@ 

### Vatue Variation (ln 1-120) (in H20) 1.421 0.0061 1.420 0.005 1.404 -0.011 

# 1.415 <------- Average dH a ~

%r Orifice Cafibration Factor dH@, the.orifice, ifferential pressure in inches of H20 that equates to 0.75 cim of air at 68 F and 29.92 inches of 

# ~ g; aC ptabl 

# ~ tole 

# ~ nce of dividual values from the average is +-0.2. /

~ SIGNEO - Date:

~ .r

~ _A 00 QD

## Temperature Meter Calibrations

Meter Box #: 10 

## Date: 06/30/08 

## Cafibrated By: TA

Emtech Thermo Degrees F Checker Probe Stack Oven Exit Auxillary

Point 1 32 34 34 34 34 34

Point 2 212 213 213 213 213 213

Point 3 752 742 743 742 742 742

Emtech Thermo Degrees R Checker Probe Stack Oven Exit Auxillary

Point 1 492 494 494 494 494 494

Point 2 672 673 673 673 673 673

Point 3 1212 1202 1203 1202 1202 1202

Percent Difference Probe Stack Oven Exit Auxiilary

Point 1 0.406504 0.406504 0.406504 0.406504 0.406504

Point 2 0.14881 0.14881 0.14881 

## 0.14881 0.14881



## Point 3 -0.82508 -0.74257 -0.82508 -0.82508 -0.82508



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Pitot tube/probe number meets or exceeds all specifications criteria and/or appl i-cabl'e design features* and is hereby assiqned a pitot tu5e cal ibration : actor ol 0.84.
S i cnat

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# ure

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# Date 

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# I SC-12

# Environmentcsl Protection Agency Pt. 60, App. A, Me#h. 2

~ 

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# CAl1BRAyEC9 SY: 

# 77 -

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# ~ C p (SIDE A) - C p (S10E 8) 1-*--MUST 6E < 0.01



## Figure 2-9. Pitot tube calibration data.

C 1 ,~~ t ~~ ) 

## =Standard pitot tube coefSicient; use

~ 

### P

~ 

### '.I 

## 0.99 if the coefficient is unknown and the 

# C°l '' tube is designed s.ccording to the criteria

~ 

### p, 

## of Sections 2: r.l to 2. r.5 of this m.ethod. l:quntion 2--2 6p, tc 1=V e.loeity hes.d measured by the standW here: ard pi tot tube, crn H,.O lin . H 2 0 ; , n

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# NOZZLE INSPECTIOh A.ND MEASUREMENT DATA SHEET

Cornp3ny ;

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# ame 

# c l~~ ~~ Da te Sampl ed Nozz le Number

t'resampl e I nspect i on I hereby certify that the above ref erenced no

- zzl e appears to be round, sharp-edged, free of nicks and dants and is judged acceptable for use at this time. 

# Last PrDviously Measured l

~ 

# ✓ Nozzl e A-rea ...Wa-4 37 ft 2 

# i graturz
Date Nieasured date

Postsampl e Measurement Measure three di a.-neters as shown; me.asurement i s i n i nches; record bel ovr; perform cal cul at i ons. `
1, j 

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, 

# Cmpany Namp 

# p

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- 55 — .3

Presampi e i nspActi on I hereby certify that. the above referenced nozzl*e appears to be round, shara-edged, free of ni cks and dents and i s• judged accePtahl e for use' at thi*s time. /
Las t Previ ously Measurzd 

# Nozzl e Area t 2 i g. ,a

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. 

# Dai.e Measured date

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# 1q~

# Barometer Calibrations

Reference Barometer - Princo Itistruments Hg in Glass -Model 9453 - Serial #10030
Date Time Temp, F Watch Actual Diff, % Owner

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~ .

t 

# Scott Specialty Gases Dual-Airalyzed Calibi

- C1ti012 

# Stai+idai-d

. 

### -- - ;,1= LICUIDE AMERICA SPECIALTY GASES LLC

~ r 

### 1290 COtOEERMERE STREET, TROY, MI 48083 Phone: 248-589-2950 Fax: 248 585 2134 4
; 

### ;1 t 

# CE_R_T'IFICATE OF ACCURACY: EPA Protocol Gas :,ssay Laboratory Customer 

# 4 P.O No.: 56235-71-65000 CLEAN A1R ENGINEERING

## ► , SCOTT SPECIAL T Y GASES Project No.: 05-61281-001 DON ALLEN i

12 

### 90 r.

- ,OVIBERIVIERE STREET 500 W. WOOD STREET ~

~ 

### F'QY. PJiI 48083 PALATINE IL 60067

A N A LY TICAL INFORMATION •:r:rrthc, ion wrts perfornied according to EPA Traceability Protocol For Assay & Certification of Gaseous Calibration Stanriarrts;
F'r si;r,rtur P. C1 1 

### ; Sentember, 1997. 

### Cylincler Number: ALM057396 Certification Date: 26Dec2007 Exp. Date: 25Dec2010 Cvlinder Pressure* "` : 1900 PSIG ANALYTICAL COMPON ENT 

### CER TI 

### FIED CONCE

_ 

### NTRATIO N ( 

### Moles) _A 

### CCURA _CY* * 

### TRACEABILIT Y !v'I E

- i' i-i,, (`d C .._. 5.142 PPM + + /- 1 % ;:Ir-: BALANCE

.r. wl;teri •,-,hnrlar tlrr•.tisure is belUw 150 psig.

!ti uasrd on tlle requuemNnts ot EPA PrOiacal Procadure G 1. September 1997 

### REFERENCE_STA NDARD TYPEfSRNI N0. EXPIRATION DATE CYLIN DE R NU MBER CONCENTR ATION C OMPONEN T
01Jut1i309 ALM058053 9,920 PPNI METHANE



### iNSTRUM ENTATION INSTRIJMENTIMODEL;SERIALh DATE 

### LA ST CALIBRATED ANALYTICAL PRINCIPLE 

## ..=; ~r~i~ • +.f~.'3~ 

## ; Oii,^.5 25t.)pr.l007 FLAME IONIZAT:ON



## _A_NALYZE 

## R READINGS (Z = Zero G as R= Reference G as T= Test Gas r= Correlation Coeff icient)

First Triad Analysis Second Triad Analysis Calibration Curve



### IVIETHAN E

Concontrntion=AiBx-Cx2+Dx3-Exa 

## ~ I
r d 0.999998 

## ~ Conslants: A--0.0d6151
8 0 0.000429 C- 0.00
, 

# 1 D. 0.00 [ - 0.00 i 

### _1 ' .

~ i • 26r1cc7007 flesp(inscr Unit:AitEA

"1 C 00000 R1 . 115890 0 71 s 12046.00

br,R 7,o 12 = 0.00000 T2 - 17.059.00
:i ZS)t)t,U T3 i 121 .00 R3 - 116316.0
5 142) PPN.

~ ,^.........-.`

F r ' 

## GV
, : r.) EY: 

# ..-_-- ___-----•

~ 

# .i-_-_-----_.

~ 

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# _

.. ....._. w•Aw.nw.1^^L'RsS~n~vl~.•[b.y.•l /.i'~!'

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~ +....'.::.:

~ .:

### ~ .;;;` ; 3106 Pasadena Freeway



# M A"" 

# HE S O N TR I ~~ A c
' 

## Pasadena, TX 77503

~ /`" ~ J 713-534-8217

- 

### ask. ..The Gas Professionals 

## Certificate of Analysis - EPA Protocol Mixtures

Customer: MATHESON-TRIGAS Protocol: Reference # Lot# Cylinder Number: CC2548 G1 36054 Cylinder Pressure: 2000 PSIG DO NOT.USE THIS CYLINDER WHEN THE Last Analysis Date: 3/18/2008 -. PRESSURE FALLS .BELOW 150 PSIG Expiration Date: 3/18/2011

~ 

## REPLICATE RESPONSES
Component: METHANE Date: 3/18/2008 20.19 Mean Conc: 20.2 PPM +/- 1% rel 20.14

................................................................................ 20.14 -----------------------..........--•----............ BALANCE GAS: AIR

REFERENCE STANDARDS:

Component: METHANE
Reference Standard: SRM

Cylinder #: FF23242 Concentration: 49.22 PPM Exp. Date: 7/1 /2011
CERTIFICATION INSTRUMENTS

Component: METHANE Make/Model: HORIBA FIA-510 Serial Number: 41679080101 Measurement Principle: FID Last Calibration: 3/18I2008

Notes:

This Certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous Calibration Standards Septernber 1997, using procedure G 1 andlor G2.

Analyst: GG ~ ~ 

## MICHAEL TANG Date: 3/18/2008

Manufactured By Specialty Gas Products, a Matheson Tri-Gas Company, Pasadena, Texas.



# 1q9

## ~ ~~ ~ ~ ~ ~ ~ `

~ E 3106 Pasadena Freeway
g 

### Pasadena, TX 77503 

## ~.. /~ 

# T ~ ~ `~ /-;1 S ' 713-534-8217 :; t

- 

### ask ... The Gas Professionats 

## Certificate of Analysis - EPA Protocol Mixtures

Customer: MATHESON-TRIGAS Protocol: Reference # Lot# Cylinder Number: CC84260 G1 36482 Cylinder Pressure: 2000 PSIG DO NOT USE'THIS:CYLINDER•WHENTHE 

# Last Analysis Date: 4/9/2008 PRESSURE FALLS BELOW 150:PSIG Expiration DatE: 1/9/2011 - REPLICATE RESPONSES

Component: METHANE Date:41912008 40.9 Mean Conc: 41.0 PPM +/- 1% rel 41.0 40.9 ..---•--------------------------------------------------------•-------•----•----------------._...........---................................
BALANCE GAS: AIR

REFERENCE STANDARDS:

Component: METHANE
Reference Standard: SRM

Cylinder #: FF23134 

## Cnncentration: 98 23 PPM Exp. Date: 7/112011 

## CERTIFICATION INSTRiJMENTS

Component: METHANE Make/Modef: HORIBA FIA-510 Serial Number: 41679080101 Measurement Principle: FID Last Calibration: 4/9/2008

Notes:

This Certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous Calibration Standards September 1997, using procedure G1 and/or G2.

r

— ~ 

## Analyst: Date: 4/9/2008

MICHAEL TANG
Manufactured By Specialty Gas Products, a Matheson Tri-Gas Cornpany, Pasadena, Texas.



# 200

# Iroll

. 

# Scatt Specialty Gases Dreal-Anulyzed Cctltbrutioiz Staiztlard

1290 C,r•'N'tEEFMERE S 7 REET,TR0Y,M1 480E3 Phonc:: 24S-589-2950 FaY 2t8 5_? :-..



# CFR i IFICATE OF ACCURACY: EPA Protocoi Gas

~ 

### ssay __"Loratory

SCOTT SPEClALTY G "-kSES 

### 1290 G01ABERMERE STREE T 'ROY,

~ 

### './I 48083

ANALYTICAL INFORMATION P.O. No.: 55678-71-65000 Project No.: 05-54263-007 Customer CLEAN AIR ENGINEERI!`!G 

### DON ALLEIV 500 YV. WOOD STREET PAL.^,TINE IL 60007

This c:erzi(ir.ation was performNd according to EPA TraceabiliTy ProtoC01 FOr Assay & Certificati0n of Gaseous CF+libratian StnncfardcPruceclur e G-1; Septemoer, 1997. 

### Cylinder Number: AAL11138 Certification Date: 30Apr2007 Exp. Date: 29Apr2003 Cylinder Pressure' " " : 2000 PSIG ANALYTICAL 

### COMPON ENT CER_TIF_IED CONCEN_TRATION (Moles) ACCUR_AC_Y" TRACEABILITY Ni T RIC O XIDE 5.116 PPM

~ ~ 

### !- 1%

~ ~ 

### D rect NIST and NhJo N(TROGErI - OXYGEN F^ nEE BALANCE

TOTAL d XIDES OF NITROGEN 5.133 PPM 

### Ruference Value Cniv

ijo no: usc vMt:n cyiinAnr 13rttssure t5 br.lov: 150 pstg ';.nntyttca accuracy :+ basdd on the requirements ol EPA Proloc:ol Prucudure G1, Septrmbar 1997. 

### REFERENCE STANDARD

~ 

### TYPEISRM NO. EXPIRATION DATE . CYLINDER NUMBER CONCENTRATION COMPONENT i•jTFtM 2E28 020ct2007 AE,1.069697 10.31 PPNt NITRIC OY.IG'c



### IN 

### ST RUM ENTATION INSTRUMENT/MODEU;SERIAL# DATE LAST CALIBRATED ANALYTICAL PRINCIPLE M;?RiESAIOPE 235!563956034 19l,pr2007 CFI

~ PA: UhA.Y

~ C-tv :'_



### A_NALYZER READINGS

wr 

### (Z = ZEro Gas R- Reference Gas T= Test Gas r= Corrnlaiion Coefficienti

~

First Triad Analysis Second Triad Analysis Cilibralion Curve

NITRIC OXIDE

! Date: 30npt2007 Rnsponse Unit: rdV ~ Concemrntion R t. •. ea - Ca i - D 3 < E> ~ I 

# j Uate 1 SApr 2007 Fi..sUonsr Unita
~ IV

% ~ ~ O.CGG•00 R t n 100.0000 71 :<5.600CC ~ 21 + O.00000 R 1- 100.0000 T t a 50.00000 

# I t~ 0.3'i99

~ 13
I R: , 100.100 C 22 - 0.00000 T2 40.60000 ~ R2 - 100.0000

~ I2 E 0.00000 T2 a 50.00000 ConYlattls: A •0.0 1 s8s t

123■ 0.00000 T3 - 49.60000 n3 100.0000 i Z3 - 0.00000 T3 - 50.00000 P.3 - 100.1000 8 A 0.1030e9 C. C



# ~ Avg. Concvn rration: 5.096 l 

# i PPM Avy. Conacnsution: 5.137 PPM 

### i D= 0 E r 0

~

' I 

### PPPO' ✓ c 

# D 2Y: 20 1 ~

....i::.... ~v~ .wv+lw ✓

. ~ +r.r ~~ ..• ~ :.s7rv.

~ a•rr:..-vArV ✓ , na4Ww
~ /Vrr. w ~ a\aM

~ 4uJVAtwrw

~ /v.vYn-K ~'~ '•Atr.w ~iw~.~ asawY4

~ M>• , .'.w - w.aV ~r~ .Y..-wyv.wrwwr••

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- t~ .1{alr ✓ r. 1

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~ r , ','!. ,} 1 0 . 1 —

### M /t T' 

## ~ ~ ~ ~ l!l ! 3106 Pasadena Freeway K I R 

## ~ f Pasadena, TX 77503 

# TRI-GAS' 4~'

~~~ 

### ti•r

~~ 

### ' 713-534-8217



## ask: ..The Gas Profession'ais 

# Certificate of Analysis - EPA Protoco! Mixtures

Customer: Cylinder Number: Cylinder Pressure: Last Analysis Date: Expiration Date: MTG-CALI SX39223 1900 PSIG 10%1612006
10116l2008 Protocol: Reference # Lot# G1 25738-02
DO NOT USE THIS CYLINDER WHEN THE PRESSURE FALLS BELOW 150 PSIG

REPLICATE RESPONSES

Component: Nitric Oxide Date: 10/9/2006 Date: 10/16/2006 

## 24.87 24.84 Mean Conc: 24.9 ppm +/- 1% rel 24.77 24.95 24.85 24.95 BALANCE GAS: Nitrogen NOx: 25.0 ppm REFERENCE STANDARDS: Component: Nitric Oxide
Reference Standard: GMIS

Cyfinder #: ND22477 Concentration: 48.8 ppm Exp. Date: 2/15/2008
CERTIFICATION INSTRUMENTS Component: Nitric Oxide Make/Model: Horiba CLA-510SS Serial Number: 42312910013 ieasurernent Principle: Cherniiuminescence , Last Calibration: 9J2912006

Notes:
This Certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous Calibration Standards September 1997, using procedure G1 and/or G2.
Analyst: Date: 

# Z

~-~/



## Manufactured By Specialty Gas Products, a Matheson Tri-Gas Company, Pasadena, Texas.



# 202

### M A` 

## ~' ~,.~ ~ ~ ~ ~ 3106 Pasadena Freeway



# T g ~ ~^ 

### Pasadena, TX 77503 

## R' * 

## V ~ S ' 713-534-8217 

## a 

## sk. ..T h 

## e Gas Professionals Certifica t 

## e of Analysis - EPA Protocol Mixtures

Custorner: MTG-DALLAS Cylinder Number: CC165300 Cylinder Pressure: 2000 PSIG Last Analysis Date: 6/18/2007 

## Expiraticri Date: 6/18/2009 Protocol: Reference # Lot# G 1 30591

REPLICATE RESPONSES )O NOT USE THIS CYLINDER WHEN THE PRESSURE FALLS BELOM 150 PSIG



## Component: Nitric Oxide Date: 6/11/2007 Date: 6118/2007 51.27 50.89 Mean Conc: 51.1 ppm +!- 1% rel 51.07 51.19 50.96 51.00 BALANCE GAS: Nitrogen

_ NOx: 51.5 ppm 

## REFERENCE STANDARDS: Component: Nitric Oxide Reference Standard: GMIS

Cylinder #: ND22453 Concentration: 95.2 PPM Exp. Date: 02/15/2008 

## CERTIFICATION INSTRUMENTS Component: Nitric Oxide Make/Model: Horiba CLA-510 Serial Number: 42312910013 leasurement Principle: CHEMI Last Calibration: 5/22/2007

Notes:
This Certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous Calibration Standards September 1997, using procedure G1 andlor G2.

i_ . - • —:

~ : ~ c r _.-:1 .• z 

## Anal ys , ~ 

## -•'
~ 

## Date: 6118/2007 

# Ling Wen Manufactured By Speciafty Gas Products, a Matheson Tri-Gas Company, Pasadena, Texas.



# 2 P , 3r 

# ~ AI R L[QU I D E I srotl Specialty Gases RATA CLAsS


# __~ ____ ` Air Liquide America Speciolty Gases 11C
, 

# ® Ihca.l-Artal tzed Calibratrora Staladard J

1290 COMBE-RMERE STREET, TROY, MI 48083 P?lone: 248-589-2950 Fax: 248-589-2134



# CERTIFICATE OF ACCURACY: EPA Protocol Gas Assay Laboratory

SCOTT SPECIALTY GASES 

## 1290 COMBERMERE STREET TROY, MI 48083



## ANALYTICAL lNFORNIATIO N P.O. No.: 56428-73-65000 Project No.: 05-63541-001 

## Customer CLEAN AIR ENGINEERING 

## DON ALLEN 500 W. V1l00D STREET PALATINE IL 60067

This certification was performed according to EPA Traceability Protocol For Assay & Certificatian of Gaseous Calibratitin Standards; Procedure G-1; September, 1997. 

## Cylinder Number: ALM057083 Certification Date: 14Mar2008 Exp. Date: 12Sep2008 Cylinder Pressure*"*: 2000 PSIG ANALYTICAL 

## COMPONENT CERTIFIED CONCENTRATION_ (Moles) ACCURACY** TRACEABILITY_ CARBON MONOXIDE 5.090 PPM +/- 1% Direct NIST and NMi NI T ROGEN BALANCE

Do not use wht:n cylinder pressure is below 150 psig. 

### '• Analytical accuracy is based on the requirements of EPA Protocol Procedure G1, Seplember 1997. 

### REFERENCE STANDARD TYPE/SRM N 0. 

### EXPIRA TION D 

### ATE CYLINDER NUMBER CO 

### NCENTRATION COMPONENT NTRM 1677 020ct2008 Ai,M069705 10.04 PPM CARBON MONOXIDE



## 1NSTRUMENTATION
lN STR U 

### MENT/MODEL/S ER lA L# 

### DATE LAST CALIBRATED ANALYTICAL PRINCIPLE
FiORI B/l!A PM/1-360I422446 70011 

### 07Mar200B NDIR


# ANALYZER READINGS (Z = Zero G as R= Reference Gas T= Test Gas r= Correlation Coefficient)

First Triad Anaiysis Second Triad AnaIysis Calibration Curve

CAHBON MONOXIDE

Oate: 07MHr2008 ttosponso Unit:MV

21 - 0.00000 R1 r 10.04000 T1 a 5.10300
R2 = 10.04000 Z2 r 0.00000 T2 a 5.10600
Z3 n 0.00000 T3 = S.11100 R3 = 10.04000 Avg. Cnncentration: 5.113 PPM Date: l4Mar2008 Rosponso Unit: MV Concontration=A+Dx4•Cx2+Ox3+Ex4

Z1 m 0.00000 R1 a 10.02000 T1 a. r't.04700 r=0.999984
R2°10.02000 22d0.00000 T2=5.05100 Constants: A=0.002452
Z3 - 0.00000 T3- 5.05300 R3 Q 10.02000 B E 0.999841 C- 0 AvO, Concentration: 5.067 PPM D-0 EQO



# APPROVED BY: 

# 2Q4

## =RL A L H 

# E SON



# TRt°GA5'

ask. . .The Gas Professionals



## Customer: Matheson-Trigas Cylinder Number: SX35357 Cylinder Pressure: 1900 PSIG Last Analysis Date: 5/14/2007 Expiration Date: 5/1412010 3106 Pasadena Freeway Pasadena, TX 77503 713-634-8217 

# Certificate of Analysis - EPA Protocol Mixtures

Protocol: Lot# G1 29911

DO NOT USE THIS CYLINDER WHEN THE PRESSURE

FALLS BELOW 150 PSIG



## REPLICATE RESPONSES
Component: Carbon Monoxide Date: 5/7/2007 Date: 5/14/2007
24.31 24.44 

## Mean Conc: 24.3 ppm +/- 1% rel 24.15 24.34 24.09 24.24



## BALANCE GAS: Nitrogen

REFERENCE STANDARDS:

Component: Carbon Monoxide
Reference Standard: GMIS

Cylinder #: CC204398 Conce

. ntration: 98.44ppm Exp. Date: 7/11 /2007
CERTIFICATION INSTRUMENTS

Component: Carbon Monoxide Make/Model: Horiba VIA-510 Serial Number: 42321590022 AAeasurement Principle: NDIR Last Calibration: 5/4/2007

Notes:

This Certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous Calibration Standards September 1997, using procedure G 1 and/or G2.

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## - _.• - . ., . . Analyst Date: 5/1412007

LING WEN
Manufactured By Specialty Gas Products, a Matheson Tri-Gas Company, Pasadena, Texas.


# 2n5

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ask. . .The Gas Professionals



## Custorner: Matheson-Trigas Cylinder Number: CC 179477 Cylinder Pressure: 1900 PSIG Last Analysis Date: 4l3/2007 Expiration Date: 4/3/2010 3106 Pasadena Freeway Pasadena, TX 77503 713-534-8217 

## Certificate of Analysis - EPA Protocol Mixtures

Protocol: Lot# G 1 28957

DO NOT USE THIS CYLINDER WHEN THE PRESSURE

FALLS BELOW 150 PSIG ,



## REPLICATE RESPONSES
Component: Carbon Monoxide Date: 3127l2007 Date: 4!312007
50.21 50.40 Mean Conc: 50.3 ppm +/- 1% rel 50.34 50.34 50.36 50.30

BALANCE GAS: Nitrogen

REFERENCE STANDARDS:

Component: Carbon Monoxide
Reference Standard: GMIS

Cylinder #: CC204398 ConcQntration: 

## 98.44ppm 

# Exp. Date: 7111/2007


## CERTIFICATION INSTRUMENTS

Component: Carbon Monoxide Make/Model: Horiba VIA-510 Serial Nurnber: 42321590022 Measurement Principle: NDIR Last Calibration: 316I2007

Notes:

This Certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous Calibration Standards Szptember 1997, using procedure G1 andlor G2.

Analyst: Date: 413/2007



## LING WEN
Manufactured By Specialty Gas Products, a Matheson Tri-Gas Company, Pasadena, Texas.



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## Certificate of Analysis - EPA Protocol Mixtures ,



## Customer: MTG-CALI CROSSING Protocol: Reference # Lot# Cylinder Number: EB0000352 G1 25738-01 Cylinder Pressure: 1900 PSIG DO NOT USE THIS CYLINDER'WHEN THE PRESSURE Last Analysis Date: 1011612006 FALLS BELOW 150 PSIG 

## Expiration Date: 1 rJ116/2008:h• - REPLICATE RESPONSES

Component: Sulfur Dioxide Date: 10/9/2006 Date: 10/16/2006 50.07 50.16 Mean Conc: 50.1 ppm +/- 1% rel 50.10 50.20 50.18 50.13 BALANCE GAS: Nitrogen

REFERENCE STANDARDS: Component: Sulfur Dioxide
Reference Standard: GMIS

Cylinder #: CC177775 Concentration: 99.6 ppm Exp. Date: 9/2612008 

## CERTIFICATION INSTRUMENTS Component: Sulfur Dioxide Make/Model: Horiba VIA-510 Serial Number: 42321590023 Measurement Principle: NDIR Last Calibration: 9/26/2006

N otes:
This Certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous Calibration Standards September 1997, using procedure G1 and/or G2.
Anaiyst: .— Date:

Manufactured By Specialty Gas Products, a Matheson Tri-Gas Company, Pasadena, Texas.



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# Certificate of Analysis - EPA Protocol Mixtures

Customer: Cylinder Number: Cylinder Pressure: Last Analysis Date: Expiration Date: MTG-DALLAS CC1fi5855 2000 PSIG 3/27/2008 r 3/27%2010 + Protocol: Reference # Lot#
G 1 36052

DO NOT USE. THIS'CYLINDER - WHENTHE : PRESSURE FALLS BELOW,'f 50 P.SIG



## REPLICATE RESPONSES

Component: Sulfur Dioxide Date: 3/20/2008 Date: 3l27/2008 101.3 101.1 - Mean Conc: 101 ppm +/- 1% rel 101.2 100.8 101.3 100.9 BALANCE GAS: Nitrogen

REFERENCE STANDARDS: Component: Sulfur Dioxide
Reference Standard: GMIS

Cylinder #: ND22558 Concentration: 495.5 PPM Exp. Date: 7/18/2009
CERTIFICATION INSTRUMENTS Component: Sulfur Dioxide Make/Model: Horiba VIA-510 Serial Number: 42321590023 asurement Principle: NDIR Last Calibration: 2/28/2008

Notes:
This Certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous Calibration Standards September 1997, using procedure G1 andlor G2.

Analyst •- Date: 3/27/2008 

# Ling Wen
Manufactured By Specialty Gas Produc'ts, a Matheson Tri-Gas Company, Pasadena, Texas.



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## Certificate of Analysis - EPA Protocol Mixtures

Customer: MTG-DALLAS Cylinder Number: CC165827 Cylinder Pressure: 2000 PSIG Last Analysis Date: 312712008 Expiration Date: 312712010

Component: Sulfur Dioxide

Mean Conc: 247 ppm +!- 1% rel

BALANCE GAS: Nitrogen



## REFERENCE STANDARDS: Component: Sulfur Dioxide
Reference Standard: GMIS Protocol: Reference # Lot# 

# G1 36053

DO NOT USE THIS CYLINDER WHEN THE PRESSURE FALLS BELOW 160. PSIG



## REPLICATE RESPONSES

Date: 3/20/2008 Date: 3/27/2008 246.7 247.5 247.6 247.3 248.0 247.4

Cylinder #: ND22558 Concentration: 495.5 PPM Exp. Date: 7/1812009 

## CERTIFICATION INSTRUMENTS Component: Suifur Dioxide Make/Model: Horiba VIA-510 Serial Number: 42321590023 asurement Principle: NDIR Last Calibration: 2/28/2008

Notes:
This Certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous Calibration'Standards September 1997, using procedure G1 andlor G2.

--• , ~ 

## Anal 

## yst Date: 

## 3/27/2008 

# Ling Wen
Manufactured By Specialty Gas Products, a Matheson Tri-Gas Company, Pasadena, Texas.



# 209