Docket No:EPA-HQ-RCRA-2012-0072Update VKim Kirkland(703) 308-0490kirkland.kim@epa.epa.govWaste Characterization BranchMaterials Recovery and Waste Management DivisionOffice of Resource Conservation and Recovery**Assem Akram is the Docket Manager, and Lisa Medley the Docket Center's Records Information Manager.** Electronic FileNameDocument TitleAbstractDocumentTypeDocumentSub TypeSource CitationAuthor NameAuthor DateMediaPageCountStart/EndPage**Method 1030 METHOD 1030 IGNITABILITY OF SOLIDS** **This method is suitable for the determination of the ignitability of** **solids and is appropriate for pastes, granular materials, solids that can be** **cut into strips, and powdery substances.** **Method SW-846 06-09 15 1/15** **1030 (1) Test Methods for Readily Combustible Solid s.** **Burning Rate Test. Supports Publication;** **Copyrighted Material** **(14.2.2.5) Recommendations on the Transport of Dangerous Goods** **, Fifth Revised Edition, United Nations, New York,** **1988. 1988** **1030 (2) 49 CFR, Appendix E to Part 173 Supports Publication;** **Copyrighted Material** **12-31-91 Edition. http://ecfr.gpoaccess.gov/cgi/t/text/text** **idx?c=ecfr;sid=75f5fbc866580ef2bc4bc1a8 b340a5ab;rgn=div5;view=text;node=49%3** **A2.1.1.3.9;idno=49;cc=ecfr 12-31-91 2 597/598** **1030 (3) Flammability (Solids). Method A.10. Supports Publication;** **Copyrighted Material** **Official Journal of the European Communities** **, No. L251/63, September 19, 1984.** **http://www.intermed.it/istbiotech/reach/A10 web1992.pdf** **09-19-84 PDF 3 1/3 1030 (4) Validation of Ignitability Method for Soli** **ds Supports Publication;** **Copyrighted Material** **Submitted to the Office of Solid Waste, U.S. EPA, February 1994** **Foster Wheeler Enviresponse, Inc., Edison,** **NJ. 02-94** **1030 (5) Internal Report (AMFA Report) Supports Publication;** **Copyrighted Material** **North Carolina Department of Environmental Health and Natural** **Resources B. Hamner** **Method 3200 METHOD 3200 MERCURY SPECIES FRACTIONATION AND** **QUANTIFICATION BY MICROWAVE ASSISTED EXTRACTION, SELECTIVE SOLVENT** **EXTRACTION AND/OR SOLID PHASE EXTRACTION** **This method contains a sequential extraction and separation procedure** **that may be used in conjunction with a determinative method to differentiate** **mercury species that are present in soils and sediments. This method** **provides information on both total mercury and various mercury species.** **method SW-846 03-12 PDF 34 1/34** **3200 (1) Speciation and Cycling of Mercury in Lavac a Bay,** **Texas, Sediments A time series of sediment depth** **profiles of total mercury (THg) and monomethylmercury (MMHg) showed** **a maximum in both solid phase and porewater MMHg during early spring,** **followed by a decrease throughout the remainder of the year.** **Supports Publication; Copyrighted** **Material Environ. Sci. Technol., 1999, 33(1), 7-13,** **http://pubs.acs.org/doi/abs/10.1021/es9803 79d** **N.S. Bloom, et. al. 01-01-99 Electronic file 7 7/13 3200 (2) Guidelines for terms related to chemical** **speciation and fractionation of elements: Definitions, structural aspects, and methodological** **approaches This document contains guidelines for** **terms related to chemical speciation and fractionation of elements as well** **as definitions, structural aspects, and methodological approaches.** **Supports Publication; Copyrighted** **Material Pure Appl. Chem., 2000, 72(8), 1453-1470,** **http://www.iupac.org/objID/Article/pac7208 x1453** **D. Templeton, et. al. 2000 Electronic file 18 1453/ 1470** **3200 (3) Determination of Artifactual Formation of Monomethylmercury (CH** **3 Hg** **+ ) in Environmental** **Samples Using Stable Hg 2+** **Isotopes with ICP-MS Detection: Calculation of Contents Applying** **Species Specific Isotope Additions This article describes the use of** **different extraction techniques with regard to their potential to form** **monomethylmercury artifact from inorganic Hg during sample prep.** **Supports Publication; Copyrighted** **Material Fresenius J. Anal. Chem., 1997, 358(3),** **363-370, http://www.springerlink.com/content/m7dpx** **89cxqke7fq6/ H. Hintelmann, et. al. 06-97 8 363/370** **3200 (4) Artifact formation of methyl mercury durin g** **aqueous distillation and alternative techniques for the extraction of methyl mercury from** **environmental samples Supports Publication;** **Copyrighted Material** **Fresenius J. Anal. Chem**.**, 1997** ,**358(3), 371-377,** **http://www.springerlink.com/content/35jq2n rwbqn08e3x/** **N. S Bloom, et. al. 06-97 7 371/377 3200 (5) Synthesis and Characterization of Isotopic** **ally Enriched Methylmercury (CH** **3 201** **Hg +** **) Isotopically enriched methylmercury** **was successfully synthesized and can be used in SIDMS and IDMS analysis** **as a standard. Supports Publication;** **Copyrighted Material** **Appl. Organomet. Chem**.**, 2003** ,**17(12), 913-920,** **http://onlinelibrary.wiley.com/doi/10.1002/a oc.551/pdf** **G. M. Rahman, et. al. 11-05-03 8 913/920 3200 (6) Speciation of mercury in soil and sediment** **by selective solvent and acid extraction** **A sequential extraction scheme for mercury in soil was developed to** **classify mercury species based on their environmental mobility and/or** **toxicity for routine lab analysis or on site screening purposes.** **Supports Publication; Copyrighted** **Material Anal. Bioanal** .**Chem**.**, 2003** ,**375(3), 428- 436,** **http://www.springerlink.com/content/m45jm rqf9kac67fw/** **Y. Han, et. al. 01-18-03 9 428/436 3200 (7) Application of Isotope Dilution in Element** **al Speciation: Speciated Isotope Dilution Mass** **Spectrometry (SIDMS) Supports Publication;** **Copyrighted Material** **Comprehensive Analytical Chemistry, Volume 33 (Elemental Speciation: New** **Approaches for Trace Element Analysis), Elsevier, New York, 2000, 277-313,** **http://www.sciencedirect.com/science/articl e/pii/S0166526X00800203** **D. Huo, et. al. 2000 37 277/313 3200 (8) Application of Speciated Isotope Dilution** **Mass Spectrometry to Evaluate Extraction Methods for** **Determining Mercury Speciation in Soils and Sediments** **Common methylmercury( or mercury species from various matrixes)** **extraction techniques were evaluated by applying speciated isotope dilution** **mass spectrometry and EPA RCRA Draft Method 3200 was found to be the** **most efficient. Supports Publication;** **Copyrighted Material** **Anal. Chem**.**, 2004, 76(13), 3548-55,** **http://www.ncbi.nlm.nih.gov/pubmed/15228 324** **G.M. M. Rahman, et. al. 07-01-04 8 3548/3555 3200 (9) Inter-laboratory Validation of EPA Method** **3200 for Mercury Speciation Analysis using Prepared** **Soil Reference Materials This article describes the findings of an** **inter-laboratory validation study of EPA draft method 3200 on two soil** **matrices. Supports Publication;** **Copyrighted Material** **Appl. Organomet. Chem**.**, 19(3), 301-307,** **March 2005, http://onlinelibrary.wiley.com/doi/10.1002/a** **oc.816/abstract G. M. M. Rahman, et. al. 02-04-05 7 301/307** **3200 (10) Occupational Health Guideline for Organo (Alkyl)** **Mercury This article gives general guidelines** **about organo (alkyl) mercury compounds and how to safely handle** **them. Supports Publication;** **Copyrighted Material** **Occupational Safety and Health Adminstration, Washington, D.C., 1978,** **http://www.cdc.gov/niosh/docs/81- 123/pdfs/0384.pdf** **U.S. Department of Labor 09-78 6 1/6 3200 (11) Delayed Cerebellar Disease and Death afte** **r Accidental Exposure to Dimethylmercury** **A case study of an accidental dimethylmercury poisoning illustrates** **the potent toxicity of this material and the need for additional safety** **precautions when used in any scientific research.** **Supports Publication; Copyrighted** **Material New Engl. J. Med** .**, 1998, 338: 1672-1676,** **http://www.nejm.org/doi/full/10.1056/NEJM 199806043382305** **D. W. Nierenberg, et. al. 06-04-98 4 1672/1675 3200 (12) Microwave Enhanced Chemistry: Fundamenta** **ls, Sample Preparation, and Applications** **Supports Publication; Copyrighted** **Material Microwave Enhanced Chemistry:** **Fundamentals, Sample Preparation, and Applications, pub. 10th ed.; American** **Chemical Society, Washington, DC, 1997 H. M. Kingston, et. al. 1997** **3200 (13) Applied Isotope Technologies, Inc 3200 (14) Speciated Isotope Dilution Mass Spectrome** **try of Reactive Species and Related Methods** **Speciated isotope dilution mass spectrometry (SIDMS) permits the** **determination of concentrations of one or more species from a sample even if** **it has been subjected to species conversion prior to species separation** **or degradation or incomplete separation exists.** **Supports Publication; Copyrighted** **Material US Patent 6 790 673 B1** **http://www.findthatpatent.com/Speciated_is otope_dilution_mass_spectrometry_of_rea** **ctive_species_and_related,6790673.html H. M. Kingston 09-14-04 0 0/0** **3200 (15) Rapid Sequential Determination of Inorgan ic** **Mercury and Methylmercury in Natural Waters by Flow-injection - Cold Vapor-Atomic-Fluorescence** **Spectrometry A method with application to river** **waters for the rapid sequential determination of inorganic mercury** **and methylmercury in natural waters at the ng/l level was developed.** **Supports Publication; Copyrighted** **Material Talanta, 1992** ,**39(11), 1537-1542, http://www.sciencedirect.com/science/articl** **e/pii/0039914092801384 W. Jain, et. al. 11-92 6 1537/1542** **3200 (16) Development of Microwave-Assisted Extract ion** **Method and Isotopic Validation of Mercury Species in Soils and Sediments** **Supports Publication; Copyrighted** **Material J. Anal. At. Spectrom., 2005** ,**20, 183-191, Method’s Archive Box 22** **G. M. M. Rahman, et. al. 2005 9 183/191 3200 (17) Development, Research and Validation of** **Environmental Speciation Methods: Evaluation by Speciated Isotope Dilution Mass Spectrometry in** **Mercury and Chromium Speciation Analysis The SIDMS technique was established** **and validated for mercury speciation analysis and an investigation providing** **solutions to difficulties associated with the analysis of mercury and chromium** **species is found in this dissertation. Supports Publication;** **Copyrighted Material** **Ph. D. Dissertation, Duquesne University, Pittsburgh, PA, 2004** **http://digital.library.duq.edu/cdm spiritan/document.php?CISOROOT=/etd&** **CISOPTR=74238&REC=1 G. M. M. Rahman 08-19-04 229 1/229** **3200 (18) Microwave-assisted Solvent Extraction for Quantitative Simultaneous Extraction of Inorganic** **Mercury and Methylmercury from Soils Supports Publication;** **Copyrighted Material** **20 th** **Annual National Environmental Monitoring Conference, Washington, DC,** **July 19-23, 2004 E. Fischer, et. al. 2004** **3200 (19) Field Sampling Technique for Mercury Spec iation** **Supports Publication; Copyrighted** **Material Anal. Proc., 1991, 293-294 W. Jain, et. al. 1991** **2 293/294 3200 (20) Determination of Methylmercury in Natural** **Waters at the Sub-nanograms-per-litre Level by Capillary** **Gas Chromatography after Adsorbent Pre concentration** **Supports Publication; Copyrighted** **Material Anal. Chim. Acta, 1989** ,**221(2), 259-268, http://www.sciencedirect.com/science/articl** **e/pii/S0003267000819625 Y. H. Lee, et. al. 1989 10 259/268** **3200 (21) Mercury Species Immobilized on Sulphydryl Cotton: A New Candidate Reference Material for** **Mercury Speciation This article describes an integrated** **analytical scheme for determination and speciation of Hg in waters as well** **as developing a new class of reference material.** **Supports Publication; Copyrighted** **Material Mikrochim. Acta., 1996** ,**123(1-4), 103-108, http://www.springerlink.com/content/v5261** **u5642445451/fulltext.pdf M. L. Mena, et. al. 1996 6 103/108** **3200 (22) Rapid Analysis for the Field: Method Development and Application to Natural Gas** **Utility Sites Supports Publication;** **Copyrighted Material** **Water Air Soil Poll., 2001**,**127(1-4), 255- 270, Method’s Archive Box 3** **H. M. Boylan, et. al. 2001 16 255/270 3200 (23) The Environmental Geochemistry and** **Bioaccessibility of Mercury in Soils and Sediments-A Review** **This paper examines the current information on mercury bioaccessibility** **and speciation in soils and the ability of speciation methods to approximate** **mercury bioaccessibility. Supports Publication;** **Copyrighted Material** **Risk Anal., 1997, 17(5), 105-113, http://onlinelibrary.wiley.com/doi/10.1111/j.** **1539-6924.1997.tb00897.x/abstract A. Davis, et. al. 10-97 9 105/113** **3200 (24) Distribution of Mercury Species in Soil f rom a** **Mercury-Contaminated Site Supports Publication;** **Copyrighted Material** **Water Air Soil Poll., 1989**,**17(5), 557-569, Method’s Archive Box 3** **N. W. Revis, et. al. 1989 13 557/569 3200 (25) Quantitative Method for Determining the** **Concentration of Mercury (II) Sulphide in Soils and Sediments** **This article describes a method for extracting mercury from soil** **sequentially and that can selectively differentiate mercury(II) sulphide from** **other species and compounds of mercury in soil.** **Supports Publication; Copyrighted** **Material Analyst, 1989, 114, 823-825,** **http://pubs.rsc.org/en/Content/ArticleLandin g/1989/AN/an9891400823** **N. W. Revis, et. al. 1989 4 823/826 3200 (26) Speciation of Mercury in Crude Oil uisng** **Speciated Isotope Dilution Mass Spectrometry This article describes an improved** **sample preparation and detection method that allows for the** **determination of mercury species in crude oil.** **Supports Publication; Copyrighted** **Material Spectroscopy, 2010, 25(1), 36-45,** **http://spectroscopyonline.findanalytichem.c om/spectroscopy/Feature/Speciation-of** **Mercury-in-Crude-Oil-Using Speciated/ArticleStandard/Article/detail/655** **117 G. M. Rahman, et. al. 01-01-10 10 36/45** **3200 (27) Application of Speciated Isotope Dilution Mass** **Spectrometry to Evaluate Methods for Efficiencies, Recoveries, and Quantification of** **Mercury Species Transformation in Human Hair This article describes the use of** **different extraction methods used for mercury speciation in human hair** **samples by providing extraction efficiencies, recoveries and potential of** **species transformations during the process.** **Supports Publication; Copyrighted** **Material J. Anal. At. Spectrom., 2009, 24, 83-92,** **http://pubs.rsc.org/en/Content/ArticleLandin g/2009/JA/b805249b** **G. M. Rahman, et. al. 10-24-08 10 83/92 3200 (28) Comparison of Methods with Respect to** **Efficiencies, Recoveries, and Quantitation of Mercury Species Interconversions in Food** **Demonstrated using Tuna Fish This article describes the efficiencies,** **recoveries, and quantitation of mercury species interconversions in tuna fish** **for total mercury and methylmercury using eight different procedures.** **Supports Publication; Copyrighted** **Material Anal. Bioanal. Chem., 2008, 390(8), 2123-** **32, http://www.ncbi.nlm.nih.gov/pubmed/18317** **738 L. H. Reyes, et. al. 04-08 10 2123/2132** **3511 METHOD 3511 ORGANIC COMPOUNDS IN WATER BY** **MICROEXTRACTION Method 3511 is a procedure for** **extracting selected volatile and semivolatile organic compounds from** **water. The microscale approach minimizes sample size and solvent** **usage, thereby reducing the supply costs, health and safety risks, and** **waste generated. This method was validated for several** **mono- and poly-cyclic aromatic hydrocarbons (MAHs and PAHs) and** **can be applied to any combination of these compounds.** **Supports Publication; Copyrighted** **Material SW-846** **03-12 PDF 13 1/13 3511 (1) Simultaneous Analysis of Monocyclic Aromat** **ic Hydrocarbons in Water by Microextraction** **Supports Publication; Copyrighted** **Material EPRI Report TR-Research Project, April** **1997 04-97** **3511 (2) D. M. Munro. “Simultaneous Determination of** **Volatile and Semivolatile Organic Compounds in Soil.”** Remediation Journal,**10, pp. 65-81, 2000. Supports** **Publication; Copyrighted** **Material http://onlinelibrary.wiley.com/doi/10.1002/re** **m.3440100408/pdf 3572 METHOD 3572** **Extraction of Chemical Agents from Wipe Samples Using Microextraction** **This method describes the extraction of chemical agents from wipe samples** **using a microextraction technique. Supports Publication;** **Copyrighted Material** **SW-846 12/2011 PDF 11 1/11** **3572 (1) Applicable documents to support the occupa tional** **health program when dealing with chemical agents include AR11-34 (The Army Respiratory** **Protection Program; AR 40-5 (Preventive Medicine); DA Pam 40-8 (Occupational Health** **guidelines for the evaluation and Control of Occupational Exposure to Nerve Agents GA, GB,** **GC, and VX.) and DA Pam 40-173 (Occupational Health Guidelines for the Evaluation and Control** **of Occupational Exposure to Mustard Agents H, HD, and HT)** **Supports Publication; Copyrighted** **Material a.** **http://www.apd.army.mil/pdffiles/r11_34.pdf , b.** **http://www.apd.army.mil/pdffiles/p40_8.pdf c.** **http://www.apd.army.mil/pdffiles/p40_173.p df** **03-12 3572 (2) Development and Evaluation of an Analytica** **l Method for Determination of GB, VX, and HD in** **Concrete Supports Publication;** **Copyrighted Material** **William S. Williamson, Jr, et. Al.** **3572 (3) Development and Evaluation of an Analytica l** **Method for Determination of GB, VX, and HD in Coral** **Supports Publication; Copyrighted** **Material William S. Williamson, Jr, et.** **Al. 3572 (4) Development and Evaluation of an Analytica** **l Method for Determination of GB, VX, and HD in** **Charcoal Supports Publication;** **Copyrighted Material** **Michael G. MacNaughton, et. Al.** **3572 (5) Development and Evaluation of an Analytica l** **Method for Determination of GB, VX, and HD on Surfaces** **Supports Publication; Copyrighted** **Material Carter Crigler** **3572 (6) Laboratory Monitoring and Quality Assuranc e** **Plan dated June 2004 Supports Publication;** **Copyrighted Material** **Department of Army, Chemical Material Agency** **Method 3620C METHOD 3620C FLORISIL CLEANUP** **This method includes procedures for cleanup of sample extracts containing** **phthalate esters, nitrosamines, nitroaromatics, haloethers, aniline and** **aniline derivatives, chlorinated hydrocarbons, organochlorine** **pesticides, organophosphates, organophosphorus pesticides, PCBs,** **and other analytes that allow for adequate performace.** **Method SW-846 10-12 28 1/28** **3620C (1) The Chemist’s Companion: A Handbook of Practical Data, Techniques, and References** **Supports Publication; Copyrighted** **Material John Wiley & Sons, Inc., New York. A.J. Gordon, et.** **al. 1972 3 372, 374, 375** **3620C (2) Florisil: Properties, Application, Bibli ography** **Supports Publication; Copyrighted** **Material Pittsburgh, Pennsylvania, 5M381DW. Floridin of ITT** **System 3620C (3) Variation of Florisil Activity; Simple Me** **thod for Measuring Absorbent Capacity and its Use in** **Standardizing Florisil Columns Supports Publication;** **Copyrighted Material** **Journal of the Association of Official Analytical Chemists, 51, 29, 1968.** **P.A. Mills 1968 3620C (4) Pesticides Analytical Manual** **Supports Publication; Copyrighted** **Material Volume 1, July 1985.** **http://www.fda.gov/Food/ScienceResearch/ LaboratoryMethods/PesticideAnalysisManu** **alPAM/ucm111455.htm U.S. Food and Drug** **Association 07-85** **3620C (5) Cleanup of Environmental Sample Extracts Using** **Florisil Solid-Phase Extraction Cartridges Supports Publication;** **Copyrighted Material** **J. Chrom. Sci. 27, 209-215, 1989. http://chromsci.oxfordjournals.org/content/2** **7/5/209.abstract V. Lopez-Avila, et. al. 1989 PDF** **7 209/215 3620C (6) Evaluation of Sample Extract Cleanup usin** **g Solid-Phase Extraction Cartridges** **Supports Publication; Copyrighted** **Material Project Report, December 1989.** **http://nepis.epa.gov/EPA/html/DLwait.htm? url=/Exe/ZyNET.exe/2000AKCX.PDF?ZyA** **ctionP=PDF&Client=EPA&Index=1986 Thru** **1990&File=D%3A%5CZYFILES%5CINDE X%20DATA%5C86THRU90%5CTXT%5C0** **0000003%5C2000AKCX.txt&Query=&Sear chMethod=1&FuzzyDegree=0&User=ANO** **NYMOUS&Password=anonymous&QField =&UseQField=&IntQFieldOp=0&ExtQField** **Op=0&Docs= U.S. EPA 12-89 PDF 124** **3620C (7) Aniline and Selected Substituted Derivati ves** **Supports Publication; Copyrighted** **Material Method 650 U.S. EPA** **3620C (8) Evaluation of SW-846 Method 8060 for Phth alate** **Esters Supports Publication;** **Copyrighted Material** **Proceedings of the Fifth Annual Waste Testing and Quality Assurance** **Symposium, 1989, pp. 144-156. http://nepis.epa.gov/EPA/html/DLwait.htm?** **url=/Exe/ZyNET.exe/9100CUG4.PDF?ZyA ctionP=PDF&Client=EPA&Index=1986** **Thru 1990&File=D%3A%5CZYFILES%5CINDE** **X%20DATA%5C86THRU90%5CTXT%5C0 0000020%5C9100CUG4.txt&Query=&Sear** **chMethod=1&FuzzyDegree=0&User=ANO NYMOUS&Password=anonymous&QField** **=&UseQField=&IntQFieldOp=0&ExtQField Op=0&Docs=** **W.F. Beckert, et. al. 1989 PDF 13 144/156 3620C (9) Organochlorine Pesticides and PCBs** **Supports Publication; Copyrighted** **Material Method 608, 40 CFR 136, October 26,** **1984. http://www.caslab.com/EPA** **Methods/PDF/608.pdf U.S. EPA 10-84 PDF 32 1/32** **4025 METHOD 4025 SCREENING FOR POLYCHLORINATED** **DIBENZODIOXINS AND POLYCHLORINATED DIBENZOFURANS (PCDD/PCDFs) BY** **IMMUNOASSAY This method is a procedure for the** **analysis of polychlorinated dibenzodioxins and polychlorinated** **dibenzofurans (PCDDs/PCDFs) in soil at 500 ppt (pg/g) using a simple one** **step liquid phase oxidative cleanup or, at mid to low ppt levels, using a two** **step coupled column cleanup (oxidation and activated carbon** **binding) adapted from Method 8290. The analysis method uses a** **commercially-available enzyme immunoassay (EIA) test kit containing** **a polyclonal antibody specific for PCDDs/PCDFs.** **method SW-846 03-12 PDF 23 1/23** **4025 (1) DF1 High Performance Dioxin/Furan Immunoassay Kit (CAPE Technologies)** **This Application Note describes a rapid immunoassay specific extraction** **and rapid one step cleanup to prepare soil samples for screening** **analysis using the CAPE Technologies High** **Performance Dioxin/Furan Immunoassay Kit.** **Supports Publication; Copyrighted** **Material DF1 High Performance Dioxin/Furan** **Immunoassay Kit (CAPE Technologies), www.cape-tech.com** **CAPE Technologies 08-28-02 10 1/10 4025 (2) CAPE Technologies Application Notes and re** **lated product literature** **Supports Publication; Copyrighted** **Material http://cape-tech.com/** **4025 (3) Measurement of PCDD/F TEQ by Immunoassay: Concept Development and Validation** **4025 (4) Measurement of PCDD/F TEQ by Immunoassay: Concept Development and Validation** **This presentation discusses the requirements for successful** **development of a PCDD/F Enzyme ImmunoAssay (EIA) and presents data** **demonstrating the determination of PCDD/F toxicity equivalence by EIA.** **Supports Publication; Copyrighted** **Material Organohalogen Compounds, 1998, 35, 97-** **100, http://www.cape-tech.com/TR-001.pdf Robert E. Carlson, et. al. 08-17-98 5 1/5** **4025 (5) Role of Quality Assurance in Immunoassay Methods Used for Field Screening.** **Immunochemical Technology for Environmental Applications** **This paper discusses the problems in environmental immunochemistry** **assays (including kits)by examining current market structure and** **troubleshooting case studies by the manufacturer.** **Supports Publication; Copyrighted** **Material Immunochemical Technology for** **Environmental Applications, American Chemical Society, Chapter 29, 361-372,** **http://pubs.acs.org/doi/abs/10.1021/bk 1997-0657.ch029** **Robert O. Harrison 5/5/97 12 361/372 4025 (6) The 2005 World Health Organization Re** **evaluation of Human and Mammalian Toxic Equivalency Factors (TEFs) of Dioxins and** **Dioxin-like Compounds Supports Publication;** **Copyrighted Material** **Toxicological Sciences, 93(2): 223-241 (2006),** **http://toxsci.oxfordjournals.org/content/93/2 /223.full.pdf+html** **Van den Berg, et. al. 07-07-06 19 223/241 4025 (7) Correlation between EIA Results and GC-MS** **TEQ Supports Publication;** **Copyrighted Material** **Tech reference, www.cape-tech.com 4025 (8) Performance of the CAPE Technologies DF1** **Dioxin/Furan Immunoassy Kit for Soil and Sediment Samples** **Supports Publication; Copyrighted** **Material Tech references,** **www.cape-tech.com 4025 (9) Technologies for Monitoring and Measuremen** **t of Dioxin and Dioxin-like Compounds in Soil and** **Sediment (CAPE Technologies LLC, DF1; Dioxin/Furan Immunoassay Kit; PCB TEQ** **Immunoassy Kit) Supports Publication;** **Copyrighted Material** **www.cape-tech.com 4025 (10) Technical Note TN-005** **Supports Publication; Copyrighted** **Material www.cape-tech.com** **4025 (11) Application Note AN-008 Supports Publication;** **Copyrighted Material** **www.cape-tech.com 4025 (12) An Efficient and Green Cleanup System for** **Analysis of Dioxins/Furans, Dioxin-like PCBs and PBDES** **Supports Publication; Copyrighted** **Material www.cape-tech.com** **4025 (13) Immunoassy Sample Prep Kit SP3-60 Supports Publication;** **Copyrighted Material** **www.cape-tech.com 4025 (14) Sample Prep Starter Kit SP3-ST** **Supports Publication; Copyrighted** **Material www.cape-tech.com** **4430 METHOD 4430 SCREENING FOR POLYCHLORINATED** **DIBENZO-**p**-DIOXINS (PCDDs) AND POLYCHLORINATED DIBENZOFURANS** **(PCDFs) IN SOILS AND SEDIMENTS USING AN ARYL HYDROCARBON RECEPTOR** **BASED PCR ASSAY This method is a screening procedure** **for polychlorinated dibenzo-**p**-dioxins (PCDDs) and polychlorinated** **dibenzofurans (PCDFs) in soils and sediments. This method uses a** **commercially-available aryl hydrocarbon receptor (AhR)-based** **polymerase chain reaction (PCR) assay. The AhR-PCR assay screens** **samples by their toxicity equivalent quotient (TEQ) by responding to** **individual PCDD/PCDF congeners in approximate correlation to their toxicity** **equivalent factors (TEFs). The TEQ measured by the AhR-PCR assay is** **the sum of the response from the individual congeners. See Table 2 for** **a detailed list of response factors for individual PCDD/PCDF congeners.** **method SW-846 03-12 PDF 23 1/23** **4430 (1) Dioxins and Furans in Soil and Sediment 4430 (2) The 2005 World Health Organization** **Reevaluation of Human and Mammalian Toxicity Equivalency Factors for Dioxins and Dioxin-like** **Compounds Supports Publication;** **Copyrighted Material** **Toxicological Sciences, 93(2): 223-241 (2006),** **http://toxsci.oxfordjournals.org/content/93/2 /223.full.pdf+html** **M. Van Den Berg, et. al. 07-07-96 19 223/241 4430 (3) Novel Real-Time PCR Assay for the Detectio** **n of Dioxins and Furans** **Supports Publication; Copyrighted** **Material Organohalogen Compd** .**2002, 58, 341-343 R. L. Allen, et. al. 2002** **3 341/343 4430 (4) Sample Preparation for the Measurement of** **Polychlorinated Dioxins and Furans by the Procept Rapid Dioxin Assay** **This paper investigates several methods for isolating PCDD/F from** **other AhR cross-reactive compounds, with primary focus on PAH.** **Supports Publication; Copyrighted** **Material Organohalogen Compnd** .**2006, 68, 940- 943,** **http://www.dioxin20xx.org/pdfs/2006/06- 138.pdf** **D. R. McAlister, et. al. 2006 4 940/943 4430 (5) The PAS Superfamily: Sensors of Environme** **ntal and Developmental Signals** **This paper provides a detailed description of three signal transduction** **pathways that utilize PAS protein heterodimers to drive their** **transcriptional output in hopes that this information can help in understanding** **the biology of these not well understood superfamily.** **Supports Publication; Copyrighted** **Material Annu. Rev. Pharmacol. Toxicol. 2000, 40,** **519-561, http://mcardle.oncology.wisc.edu/bradfield/** **519.pdf Y. Z. Gu, et. al. 2000 43 519/561** **4430 (6) Soil Screening at 50 pg/g Using a Novel Ar yl** **Hydrocarbon Receptor-based PCR Assay Supports Publication;** **Copyrighted Material** **Organohalogen Compd., 2007, 69, 1230- 1233** **D. R. McAlister, et. al. 2007 4 1230/1233 4430 (7) Cross-reactivity of Compounds on the Proce** **pt Rapid Dioxin Assay** **Supports Publication; Copyrighted** **Material Organohalogen Compd., 2007, 69, 1226-** **1229 D. R. McAlister, et. al. 2007 4 1226/1229** **4430 (8) Role of Heat Shock Protein 90 Dissociation in** **Mediating Agonist-induced Activation of the Aryl Hydrocarbon Receptor** **In this article, authors demonstrate that molybdate inhibits AhR gene activation** **in two types of cells in a concentration dependent manner and protects the** **AhR against agonist-induced proteolysis.** **Supports Publication; Copyrighted** **Material Mol. Pharmacol. 2000, 57(1), 82-92,** **http://molpharm.aspetjournals.org/content/5 7/1/82.full.pdf** **S. Heid, et. al. 2000 11 82/92** **4430 (9) Update to ATSDR Policy Guideline for Dioxi ns** **and Dioxin-Like Compounds in Residential Soil This document seeks public comment** **on a draft revision of its policy that is intended to assist health assessors** **evaluating the public health risks of dioxin and dioxin like compounds in** **residential soils. Supports Publication;** **Copyrighted Material** **Fed. Reg**.**2006, 71, 78441-78442, http://edocket.access.gpo.gov/2006/pdf/E6-** **22388.pdf Fed. Reg. 2006 12-29-06 2 78441/7844** **2 4430 (10) Emerging Homogeneous DNA-based** **Technologies in the Clinical Laboratory This article reviews technologies** **available for performing homogeneous analysis, the clinical applications** **where they are being used, and validation issues that are slowing the** **acceptance of the technologies in the general clinical setting.** **Supports Publication; Copyrighted** **Material Clin. Chem** .**2000, 47(6), http://www.clinchem.org/content/47/6/990.f** **ull.pdf+html C. A. Foy, et. Al. 06-01** **11 990/1000 4430 (11) Rapid Aryl Hydrocarbon Receptor-based** **Polymerase Chain Reaction Screening Assay for Polychlorinated Dibenzo-** p**-Dioxins and Furans in Soil and Sediment** **This article describes a method for the estimation of PCCD/F toxicity** **equivalent quotient of soil and sediment matrices.** **Supports Publication; Copyrighted** **Material Talanta, 2007, 74(4), 992-997,** **http://www.sciencedirect.com/science/articl e/pii/S0039914007005607** **D. R. McAlister, et. Al. 01-15-08 6 992/997 4435 METHOD 4435** **SCREENING FOR DIOXIN-LIKE CHEMICAL ACTIVITY IN SOILS AND SEDIMENTS** **USING THE CALUX® BIOASSAY AND TEQ DETERMINATIONS** **This method is a bio-analytical screening procedure for dioxin-like** **compounds in soils and sediments. This method is** **based on the ability of dioxin and related chemicals to** **activate the aryl hydrocarbon receptor (AhR), a chemical-responsive DNA** **binding protein that is responsible for producing the toxic and biological** **effects of these chemicals. Measurement of the level of activation** **of AhR-dependent gene expression by a chemical or chemical extract** **provides a measure by which to estimate the relative potency and toxic** **potential of these chemicals and/or extracts with resulting values** **expressed as toxic equivalents (TEQs).** **method SW-846 03-12 PDF 59 1/59** **4435 (1) Ah Receptor Mediated Effects of Particulat e** **Organic Extracts from the Paso Del Morte Airshed Along the U.S. - Mexico Border** **Supports Publication; Copyrighted** **Material Environmental Heath Perspectives, 2003,** **111(10), 1299-1305, http://www.ncbi.nlm.nih.gov/pmc/articles/P** **MC1241610/pdf/ehp0111-001299.pdf 2003 7 1299/1305** **4435 (2) Harmonised Quality Criteria for Chemical a nd** **Bioassays Analyses of PCDDs/PCDFs in Feed and Food Part 2: General Considerations,** **Bioassay Methods This article describes proposed** **QA/QC guidelines for bioassays that measure dioxin-like compounds and** **discusses technical questions associated them.** **Supports Publication; Copyrighted** **Material Organohalogen Compounds 2001, 45,** **http://www.dioxins.com/pdf/feedstuffs/feed0 4.pdf** **Peter A. Behnisch, et. al. 2001 5 0/0 4435 (3) Determination of REP Values for the CALUX** **bioassay and comparison to the WHO TEF Values** **In this article relative potency (REP) values are determined for dioxin like** **compounds to understand the relationship between GC/MS results** **and characterize responsiveness of the CALUX® assay.** **Supports Publication; Copyrighted** **Material Organohalogen Compounds 2001, 53, 211-** **214, http://www.dioxins.com/pdf/compounds/co** **mpound02.pdf David J. Brown, et. al.** **2001 4 211/214 4435 (4) Quality control criteria implemented for m** **onitoring the CALUX bioassay** **In this article the authors report the QC criteria that have been developed in** **the lab to monitor the reproducibility and consistency of results from the** **CALUX® assay. Supports Publication;** **Copyrighted Material** **Organohalogen Compounds 2001, 54, 32- 35,** **http://www.dioxins.com/pdf/environment/en vironment01.pdf** **David J. Brown, et. al. 2001 4 32/35 4435 (5) Validation Study for the use of the Dioxin** **Responsive CALUX Assay for Analysis of Japanese Ash and Soil Samples** **In this article the author reports results from a preliminary validation study that** **used blind format to compare the results from the dioxin responsive** **CALUXTM assay with HRGCMS data. Supports Publication;** **Copyrighted Material** **Organohalogen Compounds 2000, 45, 200- 203,** **http://www.dioxins.com/pdf/environment/en vironment10.pdf** **David Brown, et. al. 2000 4 200/203** **4435 (6) Recovery determinations for bioassay analy sis:** **Considerations and results In this article the use of biologically** **inactive congeners as internal spikes is researched and presented along** **with information about HRGC/HRMS recoveries and radiolabeled spike** **experiments. Supports Publication;** **Copyrighted Material** **Organohalogen Compounds, 2002, 58, 357-360,** **http://www.dioxins.com/pdf/compounds/co mpound03.pdf** **David J. Brown, et. al. 2002 4 357/360 4435 (7) Elimination of interfering compounds in** **preparation for analysis by an Ah receptor based bioassay** **In this article various sample prep methods and their efficiency of** **removing environmental contaminants and selected “non-classical” AhR** **ligands are reported. Supports Publication;** **Copyrighted Material** **Organohalogen Compounds 2002, 58, 401- 404,** **http://www.dioxins.com/pdf/compounds/co mpound04.pdf** **David J. Brown, et. al. 2002 4 401/404 4435 (8) Relationships between exposure to dioxin-l** **ike chemicals, testosterone levels, and sex of the** **children of pesticide applicators This article studies the relationships** **between exposure to dioxin-like chemicals, testosterone levels, and** **sex of the children of pesticide applicators with the use of DIPS** **CALUX. Supports Publication;** **Copyrighted Material** **Organohalogen Compounds 2002, 56, 73- 76,** **http://www.dioxins.com/pdf/compounds/co mpound07.pdf** **George Clark, et. al. 2002 4 73/76 4435 (9) Characterization of the CALUX and GRAB** **bioassays for sensitivity and specificity in detection of phamacological agents that activate** **the Ah Receptor signaling system Supports Publication;** **Copyrighted Material** **Organohalogen Compounds, 1999, 42, 309-312,** **http://www.dioxins.com/pdf/compounds/co mpound09.pdf** **George C. Clark, et al. 1999 4 309/312 4435 (10) A Novel Low-Cost Air Sampling Device** **(AmbStack Sampler) and Detection System (CALUX Bioassay) for Measuring Air Emissions of** **Dioxin, Furan, and PCB on a TEQ Basis Tested With a Model Industrial Boiler** **Supports Publication; Copyrighted** **Material Organohalogen Compounds 1999, 40, 79-** **82, http://www.dioxins.com/pdf/environment/en** **vironment09.pdf George C. Clark, et. al. 1999 4 79/82** **4435 (11) Bioanalytical approaches for the Detectio n of** **Dioxin and Related Halogenated Aromatic Hydrocarbons** **Supports Publication; Copyrighted** **Material Biomarkers of Environmentally Associated** **Disease, Chapter 33, 483-494, http://www.crcnetbase.com/doi/abs/10.120** **1/9781420032208.ch33 Bruce D. Hammock, et. al. 2002 12 483/494** **4435 (12) Ah receptor-based bioassays for dioxins a nd** **related chemicals: Applications and limitations Supports Publication;** **Copyrighted Material** **Toxicol. Sci. 2000, 55, 107-115, http://toxsci.oxfordjournals.org/content/55/1** **/107.full.pdf Shawn D. Seidel, et. al. 2000 9 107/115** **4435 (13) Recombinant Cell Bioassay Systems for the Detection and Relative Quantitation of** **Halogenated Dioxins and Related Chemicals Supports Publication;** **Copyrighted Material** **Talanta 63, Issue 5, http://www.sciencedirect.com/science/articl** **e/pii/S0039914004002978 Michael S. Denison, et. al. 08-08-04 11 1123/1133** **4435 (14) Bioanalytical approaches for the detectio n of** **dioxin and related halogenated aromatic hydrocarbons, in: Technology-Driven Biomarkers** **Development and Application in Environmentally Associated Diseases** **Supports Publication; Copyrighted** **Material Technology-Driven Biomarkers** **Development and Application in Environmentally-Associated Diseases 483-** **494, Lewis Press, Boca Raton, FL M. S. Denison, et. al. 2002 12 483/494** **4435 (15) Species-specific recombinant cell lines a s** **bioassay systems for the detection of 2,3,7,8- tetrachlorodibenzo-p-dioxin-like chemicals** **Supports Publication; Copyrighted** **Material Fund. Appl. Toxicol. 1996, 30, 194-203,** **http://toxsci.oxfordjournals.org/content/30/2 /194.full.pdf+html** **P. M. Garrison, et. al. 1996 10 194/203 4435 (16) Comparison of recombinant cell Bioassays** **for the detection of Ah receptor agonists** **Supports Publication; Copyrighted** **Material Biofactors 20 (1/2004), 11-22,** **https://iospress.metapress.com/content/45 8qmdj2gu4mc7ef/resource** **secured/?target=fulltext.pdf D. Han, et. al. 04-19-04 12 11/22** **4435 (17) Recombinant cell lines for the detection of dioxins** **and Ah Receptor ligands- Not all assays are created equal** **Supports Publication; Copyrighted** **Material Organohalogen Compounds 58(2002):** **421-424, http://www.dioxins.com/pdf/compounds/co** **mpound05.pdf D. Han, et. al.** **2002 4 421/424 4435 (18) Determination of Dioxins and Planar PCBs** **in Fish Using the GC/MS and CALUX Bioassay** **Supports Publication; Copyrighted** **Material Organohalogen Compounds 45(2000): 180** **- 184, http://www.dioxin20xx.org/pdfs/2000/00-** **212.pdf R. Hoogenboom, et. al. 2000 4 180/183** **4435 (19) Using the CALUX Assay to select high-TCDD mothers in Southern Kazakhstan and map time** **course of TCDD elimination via breast milk. Supports Publication;** **Copyrighted Material** **Organohalogen Compounds 58(2002): 377-380,** **http://www.dioxin20xx.org/pdfs/2002/02- 467.pdf** **Kim Hooper, et. al. 2002 4 377/380 4435 (20) CALUX results correlate with GC/MS/MS dat** **a from Kazakhstan breast milk samples** **Supports Publication; Copyrighted** **Material Organohalogen Compounds 45(2000):** **236-239, Organohalogen Compounds 45: 236-239** **Kim Hooper, et. al. 2000 4 236/239 4435 (21) CALUX and High Resolution GC/MS Analysis** **of Dioxin-Like Compounds in Chlorophenoxy** **Pesticide Formulations Supports Publication;** **Copyrighted Material** **Organohalogen Compounds 60-65(Dioxin 2003),** **http://www.dioxins.com/pdf/environment/en vironment04.pdf** **Janice K. Huwe, et. al. 4 0/0 4435 (22) CALUX assay is applicable to human** **epidemiological studies Supports Publication;** **Copyrighted Material** **Organohalogen Compounds 54(2001): 48- 50,** **http://www.dioxins.com/pdf/biological/biolog ical02.pdf** **F. Kayama, et. al. 2001 3 48/50 4435 (23) Dioxin and Organochlorine Pesticide** **Concentrations of Breast Milk in China and Japan Supports Publication;** **Copyrighted Material** **Organohalogen Compounds 60 - 65a(2003),** **http://www.dioxins.com/pdf/biological/biolog ical06.pdf** **F. Kayama, et. al. 2003 4 0/0 4435 (24) Regional differences of blood dioxins and** **organchlorine pesticides concentrations of Japanese female farmers.-Application of CALUX** **assay for epidemiological study Supports Publication;** **Copyrighted Material** **Organohalogen Compounds 55(2002): 275-278,** **http://www.dioxins.com/pdf/biological/biolog ical03.pdf** **F. Kayama, et. al. 2002 4 275/278 4435 (25) A COMPARATIVE ANALYSIS OF CERTIFIED** **ENVIRONMENTAL REFERENCE MATERIALS USING CALUXTM ASSAY AND HIGH** **RESOLUTION GC/MS Supports Publication;** **Copyrighted Material** **Organohalogen Compounds 58(2002): 381-384,** **http://www.dioxin20xx.org/pdfs/2002/02- 468.pdf** **T. Nakamura, et. al. 2002 4 381/384 4435 (26) Validation of the CALUX Bioassay: Quantit** **ative Screening Approach** **Supports Publication; Copyrighted** **Material Organohalogen Compounds 58(2002):** **353 - 356, http://www.dioxins.com/pdf/environment/en** **vironment02.pdf I. Van Overmeire, et. al. 2002 4 353/356** **4435 (27) Application of the CALUX Bioassay for the Determination of Low TEQ Values in Milk** **Samples Supports Publication;** **Copyrighted Material** **Organohalogen Compounds 45(2001), http://www.dioxins.com/pdf/biological/biolog** **ical08.pdf Ilse Van Overmeire, et. al. 2001 3 0/0** **4435 (28) A Comparitive Study of GC-HRMS and CALUX TEQ Determinations in Food Samples by the** **Belgian Federal Ministries of Public Health and Agriculture** **Supports Publication; Copyrighted** **Material Organohalogen Compounds 45(2000): 196** **- 200, http://www.dioxins.com/pdf/feedstuffs/feed0** **2.pdf Ilse Van Overmeire, et. al. 2000 4 196/200** **4435 (29) Inter-Laboratory CALUX Comparison Data at Low** **Levels with Traditional GC-HRMS Confirmations Supports Publication;** **Copyrighted Material** **Organohalogen Compounds 60(2003): 255-258,** **http://www.dioxin20xx.org/pdfs/2003/03- 65.pdf** **L. M. Pence, et. al. 2003 4 255/258 4435 (30) Persistent Organic Pollutants (POPs) and** **Immune Function in US Atlantic Coast Harbor Seals** **Supports Publication; Copyrighted** **Material Organohalogen Compounds 60 - 65(2003),** **http://www.dioxins.com/pdf/biological/biolog ical05.pdf** **Susan D. Shaw, et. al. 2003 4 0/0 4435 (31) Comparison of the CALUX Bioassay and ID** **HRGC/HRMS as Measures of Dioxin Toxic Equivalents in Serum** **Supports Publication; Copyrighted** **Material Organohalogen Compounds 60 - 65,** **http://www.dioxins.com/pdf/biological/biolog ical04.pdf** **Marcella Warner, et. al. 2003 4 0/0 4435 (32) Non Additive Interactions in CALUX** **Supports Publication; Copyrighted** **Material Organohalogen Compounds 60 - 65,** **http://www.dioxins.com/pdf/compounds/co mpound06.pdf** **I. Windal, et. al. 2003 4 0/0 4435 (33) Variables that affect TEQ determinations** **by CALUX and GC-HRMS** **Supports Publication; Copyrighted** **Material Organohalogen Compounds 58(2002):** **389-392, http://www.dioxins.com/pdf/environment/en** **vironment03.pdf I. Windal, et. al. 2002 4 389/392** **4435 (34) Application of the luciferase recombinant cell** **culture bioassay system for the analysis of polycyclic aromatic hydrocarbons** **Supports Publication; Copyrighted** **Material Environ. Toxicol. & Chem. 2002, 21(10),** **2027-2033 Michael H. Ziccardi, et. al. 10-02 7 2027-2033** **4435 (35) Chemically Activated Luciferase Gene Expr ession** **(CALUX) Cell Bioassay Analysis for the Estimation of Doxin-Like Activity: Critical** **Parameters of the CALUX Procedure that Impact Assay Results** **Supports Publication; Copyrighted** **Material Environ. Sci. Technol., 2005, 39(19), 7357-** **7364, Isabelle Windal, et. al. 2005 8 7357/7364** **4435 (36) Brominated dioxin-like compounds in vitro assessment in comparison to classical dioxin-like** **compounds and other polyaromatic compounds Supports Publication;** **Copyrighted Material** **Environment International, 2003, 29, 861- 877,** **http://www.pops.int/documents/meetings/p oprc/submissions/AnnexE_2007/Toxicity%** **20studies%20World%20Chlorine%20Coun cil.pdf** **Peter Alexander Behnisch, et. al.** **2003 17 861/877 4435 (37) Study of the interference problems of dio** **xin-like chemicals with the bio-analytical method CALUX** **Supports Publication; Copyrighted** **Material Talanta 63 (2004), 1261-1268,** **http://www.vub.ac.be/ANCH/publications/S chroijen%20et%20al_2004.pdf** **Carmen Schroijen, et. al. 2004 8 1261/1268 4435 (38) The 2005 World Health Organization** **Reevaluation of Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-Like** **Compounds Supports Publication;** **Copyrighted Material** **Toxicological Sciences 93(2):223-241, 2006,** **http://toxsci.oxfordjournals.org/content/93/2 /223.full.pdf+html** **Martin Van den Berg, et. al. 2006 19 223/241 4435 (39) Mathematical Model Developed for Environm** **ental Samples: Prediction of GC/MS Dioxin TEQ from** **XDS-CALUX Bioassay Data This article describes use of the XDS** **CALUX bioassay and GC/MS to create a mathematical model that can be** **useful in risk assessment and management decisions for dioxin-like** **contamination sites. Supports Publication;** **Copyrighted Material** **Environmental Science and Technology 2007, 41(12), 4354-4360,** **http://journals.ohiolink.edu/ejc/article.cgi?is sn=0013936x&issue=v41i0012&article=435** **4_mmdfesdtfxbd D. J. Brown, et. al. 06-15-07 7 4354/4360** **4435 (40) Report on the Comparison of Cell Based As says** **with Mass Spectrometry Methods for the Analysis of PCDDs/PCDFs and PCBs in Biosolids** **Supports Publication; Copyrighted** **Material U.S. EPA Report from the Office of Water** **and Office of Science and Technology, Engineering and Analysis Division on** **Biosolids, June 2002. USEPA 06-02** **4435 (41) U.S. patent # 5,854,010 Supports Publication;** **Copyrighted Material** **Bioassay for detecting 2,3,7,8- tetrachlorodibenzo-para-dioxin and TCDD** **like compounds and novel recombinant cell line useful therefor,** **http://patft.uspto.gov/netacgi/nph Parser?Sect1=PTO1&Sect2=HITOFF&d=P** **ALL&p=1&u=%2Fnetahtml%2FPTO%2Fsr chnum.htm&r=1&f=G&l=50&s1=5,854,010.** **PN.&OS=PN/5,854,010&RS=PN/5,854,010 Michael S. Denison, et. al.** **12-29-98 1 0/0 4435 (42) U.S. Patent # 6,720,431** **Supports Publication; Copyrighted** **Material Methods and apparatus for separating and** **detecting specific polyhalogenated diaromatic hydrocarbons ,** **http://patft.uspto.gov/netacgi/nph Parser?Sect1=PTO1&Sect2=HITOFF&d=P** **ALL&p=1&u=%2Fnetahtml%2FPTO%2Fsr chnum.htm&r=1&f=G&l=50&s1=6,720,431.** **PN.&OS=PN/6,720,431&RS=PN/6,720,431 Michael D. Chu, et. al. 04-13-04 1 0/0** **5021A Method 5021A - VOLATILE ORGANIC COMPOUNDS IN VARIOUS SAMPLE** **MATRICES USING EQUILIBRIUM HEADSPACE ANALYSIS** **method SW-846 03-12 PDF 31 1/31** **5021A (1) Determination of Volatile Organic Compoun ds in** **Soils using Equilibrium Headspace Analysis and Capillary Column Gas Chromatography/Mass** **Spectrometry Supports Publication;** **Copyrighted Material** **U.S. Environmental Protection Agency, Office of Research and Development,** **Environmental Monitoring Systems Laboratory, Cincinnati, OH, December,** **1992. P. Flores, et. al. 12-92** **5021A (2) Headspace Analysis and Related Methods in Gas** **Chromatography Supports Publication;** **Copyrighted Material** **Headspace Analysis and Related Methods in Gas Chromatography," John Wiley and** **Sons, 1984 B. V. Loffe, et. a. 1994** **5021A (3) The Analysis of Selected Components of Reformulated Gasoline in Environmental Samples** **Supports Publication; Copyrighted** **Material from MTBE Handbook, ed. Kostecki, P.** **and Moyer, E. Amherst Scientific Publishers, 2002.** **R. J. Pirkle, et. al. 2002 5021A (4) Environmental Fact Sheet: Analytical Meth** **ods for Fuel Oxygenates** **This fact sheet provides information about EPA’s validated analytical** **methods for common fuel oxygenates. Supports Publication;** **Copyrighted Material** **EPA 510-F-03-001, April, 2003, http://www.epa.gov/oust/mtbe/omethods.pd** **f USEPA OUST 04-03 2 0/0** **5021A (5) Analytical Methods for Fuel Oxygenates Supports Publication;** **Copyrighted Material** **LUSTLine (Bulletin #42), October, 2002, http://www.epa.gov/oust/mtbe/LL42Analytic** **al.pdf H. 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Supports Available in Methods Contract Archive** **03-12 6010D METHOD 6010D** **INDUCTIVELY COUPLED PLASMA—OPTICAL EMISSION SPECTROMETRY** **Inductively coupled plasma—optical emission spectrometry (ICP-OES) is a** **spectrometric technique used to determine trace elements in aqueous** **solutions sample. method SW-846** **03-12 PDF 35 1/35 6010D (1) An Interlaboratory Study of Inductively C** **oupled Plasma Atomic Emission Spectroscopy Method** **6010 and Digestion Method 3050 In this report, the design, execution,** **and results of an interlaboratory study of Method 6010 and Method 3050 are** **discussed. Supports Publication;** **Copyrighted Material** **EPA-600/4-87-032, U.S. Environmental Protection Agency, Las Vegas, NV, 1987,** **http://nepis.epa.gov/Exe/ZyPURL.cgi?Dock ey=91009D89.txt** **C. L. 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Acid digestion** **prior to filtration and analysis is required for groundwater, aqueous samples, industrial** **wastes, soils, sludges, sediments, and other solid wastes for which total (acid** **leachable) elements are required. The analyst should insure that a sample** **digestion method is chosen that is appropriate for each analyte and the** **intended use of the data. method SW-846** **03-12 PDF 31 1/31 6020B (1) The effect of plasma operating parameters** **on analyte signals in inductively coupled plasma** **mass spectrometry Supports Publication;** **Copyrighted Material** **Spectrochim. Acta Part B: Atomic Spec. 40(10-12), 1555-1572 (1985),** **http://www.sciencedirect.com/science/articl e/pii/0584854785801786** **G. Horlick, et. al. 1985 18 1555/1572 6020B (2) The ICP as an ion source-origins, achieve** **ments and prospects/Mass spectrometry with an** **inductively coupled plasma as an ion source: the influence on ultratrace analysis of background and** **matrix response Supports Publication;** **Copyrighted Material** **Spectrochim. Acta Part B, 40(10-12), 1525- 1537 (1985),** **http://www.sciencedirect.com/science/articl e/pii/0584854785801762,** **http://www.sciencedirect.com/science/articl e/pii/0584854786801471** **A. L. Gray 1985 13, 17 1525/1537; 151/167** **6020B (3) Background Spectral Features in Inductive ly** **Coupled Plasma/Mass Spectrometry In this article the basic background** **mass spectra of the inductively coupled plasma are presented.** **Supports Publication; Copyrighted** **Material Appl. Spectrosc. 40, 445 (1986),** **http://www.opticsinfobase.org/as/abstract.cf m?uri=as-40-4-445** **S. H. Tan, et. al. 1986 16 445/460** **6020B (4) Oxide, Hydroxide, and Doubly Charged Analyte** **Species in Inductively Coupled Plasma/Mass Spectrometry** **Supports Publication; Copyrighted** **Material Appl. Spectrosc. 40(4), 434-445 (1986),** **http://www.opticsinfobase.org/abstract.cfm ?URI=as-40-4-434** **M. A. Vaughan, et. al. 1986 12 434/445** **6020B (5) Table of the Isotopes Supports Publication;** **Copyrighted Material** **CRC Handbook of Chemistry and Physics, 74th Ed., CRC Press, Boca Raton, FL,** **1993 N. E. Holden** **6020B (6) Winter Conference on Plasma Spectrochemis try,** **San Diego, California, USA, January 10-15, 1994 Supports Publication;** **Copyrighted Material** **Abstract THP18; p. 237, San Diego, CA (1994),** **http://pubs.rsc.org/en/content/articlelanding /1994/JA/ja994090051n** **T. A. Hinners, et. al. 6020B (7)** **Determination of the rare-earth elements in geological materials by inductively coupled** **plasma mass spectrometry This article describes the development** **of a new method of analysis of geological materials for the** **determination of the rare-earth elements using ICP-MS.** **Supports Publication; Copyrighted** **Material Anal. Chem. 59(8), 1150-1157 (1987),** **http://pubs.acs.org/doi/abs/10.1021/ac0013 5a018** **F. E. Lichte, et. al. 04-87 8 1150/1157 6020B (8) Simple approach to reducing polyatomic io** **n interferences on arsenic and selenium in** **inductively coupled plasma mass spectrometry This article explains how the** **interference by polyatomic ions in the determination of As and Se by ICP MS** **can be substantially reduced by introduction of small amounts of** **propan-2-ol or a molecular gas into the central channel of the ICP.** **Supports Publication; Copyrighted** **Material J. Anal. At. Spectrom, 1989, 4, 299-300,** **http://pubs.rsc.org/en/content/articlelanding /1989/ja/ja9890400299** **E.H. Evans, et. al. 2 299/300 6020B (9) Study of the effects of concomitant eleme** **nts in inductively coupled plasmamass spectrometry** **Supports Publication; Copyrighted** **Material Spectrochim. Acta Part B, 42(3), 1987,** **467-490, http://www.sciencedirect.com/science/articl** **e/pii/0584854787800241 D. Beauchemin, et. al. 24 467/490** **6020B (10) Mass Spectrometry of inductively coupled plasmas** **This article explains the development and use of the ICP-MS.** **Supports Publication; Copyrighted** **Material Anal. Chem. 1986, 58(1), 97A-105A,** **http://pubs.acs.org/doi/pdf/10.1021/ac0029 2a003** **R. S. Houk 01-86 9 97A/105A 6020B (11)** **A Study of Internal Standardization in Inductively Coupled Plasma-Mass Spectrometry** **This article discusses the use of internal standardization to compensate** **for ionization suppression in inductively coupled plasma-mass** **spectrometry (ICP-MS). Supports Publication;** **Copyrighted Material** **Appl. Spectrosc. 41, 5, 801-806 (1987), http://www.opticsinfobase.org/viewmedia.cf** **m?uri=as-41-5-801&seq=0 J. J. Thompson, et. al. 1987 6 801/806** **6020B (12) Final Report of the Multi-Laboratory Eva luation of** **Method 6020 CLP-M Inductively Coupled Plasma Mass Spectrometry** **Supports Publication; Copyrighted** **Material W. R. Newberry, et. al.** **6020B (13) On-Line Solid-phase Chelation for the Determination of Eight Metals in Environmental** **Waters by Inductively Coupled Plasma Mass Spectrometry** **Supports Publication; Copyrighted** **Material Daniel B. Taylor, et. al.** **6020B (14) Patent Number 5,126,272, System for Dete cting** **Transition and Rare Earth Elements in a Matrix Supports Publication;** **Copyrighted Material** **H. M. Kingston, et. al. 6020B (15) A Method and Apparatus for Detecting Tra** **nsition and Rare Earth Elements in a Matrix** **Supports Publication; Copyrighted** **Material H. M. Kingston, et. al.** **6020B (16) Determination of Mercury by ICP-MS Supports Publication;** **Copyrighted Material** **David Dobb, et. al. 6020B (17) Quality Assurance of Chemical Measuremen** **ts Supports Publication;** **Copyrighted Material** **Lewis Publishers (1987) J. K. Taylor 6020B (18) Federal Advisory Committee on Detection** **and Quantitation Approaches and Uses in** **CleanWaterActPrograms,FinalReport Supports Publication;** **Copyrighted Material** **http://water.epa.gov/scitech/methods/cwa/d et/index.cfm** **Federal Advisory Committee on Detection and** **Quantitation Approaches and Uses in** **CleanWaterActPrograms 6800 METHOD 6800** **ELEMENTAL AND MOLECULAR SPECIATED ISOTOPE DILUTION MASS SPECTROMETRY** **This method consists of two approaches: (1) isotope dilution mass** **spectrometry (IDMS) for the determination of the total** **concentrations of elements and molecules and (2) molecular** **speciated isotope dilution mass spectrometry (SIDMS) for the** **determination of elemental and molecular species. IUPAC defines** **speciation analysis as “analyzing chemical compounds that** **differ in isotopic composition, conformation, oxidation or electronic** **state, or in the nature of their complexed or covalently bound** **substituents, which can be regarded as distinct chemical** **species.” method SW-846** **03-12 PDF 68 1/68 6800 Sec 13** **(1) Handbook of Inductively Coupled Plasma Mass** **Spectrometry This book discusses the basics of** **inductively coupled plasma mass spectrometry including general** **technique and practical advice. Supports Publication;** **Copyrighted Material** **Blackie Academic & Professional: London, U.K. 1992, p-315,** **http://www.springerlink.com/content/h6226 4k1r26m4071/** **K. E. Jarvis, et. al. 1992 380 315/315 6800 Sec 13** **(2) Isotopic ratio measurements with an inductively** **coupled plasma source mass spectrometer This article discusses the factors** **controlling accuracy and precision of isotopic ratios when inductively** **coupled plasma source mass spectrometer has been used to** **measure the isotopic composition of U, Pb, Os, and B standards.** **Supports Publication; Copyrighted** **Material Spectrochimica Acta, Part B, Atomic** **Spectroscopy, 1987, 42B, 49- 62, http://www.sciencedirect.com/science/articl** **e/pii/0584854787800496 G. P. Russ III, et. al. 1987 14 49/62** **6800 Sec 13 (3)** **Inductively Coupled Plasma Mass Spectrometry: Practice and Techniques, Academic Press** **This book presents a thorough description of inductively coupled** **plasma-mass spectrometry for the use in trace element analytical chemistry** **issues. Supports Publication;** **Copyrighted Material** **Academic Press: San Diego, CA, USA, 2001, p-48,** **http://www.sciencedirect.com/science/book /9780126838657** **H. E. Taylor 10-00 294 48/48 6800 Sec 13** **(4) Guidelines for Achieving High Accuracy in Isotope** **Dilution Mass Spectrometry This book provides simple robust** **methodology with adequate guidance to allow labs to use IDMS, for** **inorganic and organic mass spectrometry, and obtain reliable data.** **Supports Publication; Copyrighted** **Material The Royal Society of Chemistry:** **Cambridge, UK, 2002, http://books.google.com/books/about/Guide** **lines_for_achieving_high_accuracy_i.html?i d=9wwLS5pcD9sC** **M. Sargent, et. al. 2002 49 0/0 6800 Sec 13** **(5) Characterization of waste – State of the art** **document – Chromium VI specification in solid matrices** **Supports Publication; Copyrighted** **Material PD CEN/TR 14589:2003, British** **Standards, EU publication “International Standards Correspondence Index,** **Technical Report CEN Technical Committee CEN/TC 292, European** **Committee for Standardization, 2003, http://shop.bsigroup.com/ProductDetail/?pi** **d=000000000030095298 06-04-03 42** **6800 Sec 13 (6)** **Supports Publication; Copyrighted** **Material 6800 Sec 16** **(1) Isotope Dilution Mass Spectrometry** **Supports Publication; Copyrighted** **Material Anal. Chem. 1989, 61(10), 643A-649A J. D. Fasset, e** **t. al. 6800 Sec 16** **(2) Method of Speciated Isotope Dilution Mass** **Spectrometry Supports Publication;** **Copyrighted Material** **US Patent Number: 5,414,259, 1995 H. M. Kingston 0 5-09-95 0/0** **6800 Sec 16 (3)** **Correction of Species Transformations in the Analysis of Cr(VI) in Solid Environmental Samples** **Using Speciated Isotope Dilution Mass Spectrometry** **This article describes a method capable of monitoring and correcting** **for such bidirectional species transformations to determine Cr(VI) in** **solid samples. Supports Publication;** **Copyrighted Material** **Anal. Chem. 2000, 72(20), 5047-5054, http://pubs.acs.org/doi/abs/10.1021/ac0000** **08r D. Huo, et. al. 09-09-00 8 5047/5054** **6800 Sec 16 (4)** **Hexavalent Chromium Extraction from Soils: A Comparison of Five Methods** **This article describes the use of five different methods for the determination** **of total Cr(VI) in soil. Supports Publication;** **Copyrighted Material** **Environ. Sci. Tech. 1995, 29(9), 2377- 2381,** **http://cat.inist.fr/?aModele=afficheN&cpsidt =3643033** **B. R. James, et. al. 1995 5 2377/2381 6800 Sec 16** **(5) Accuracy in Species Analysis. Speciated Isotope** **Dilution Mass Spectrometry (SIDMS) Exemplified by the Evaluation of Chromium Species** **Supports Publication; Copyrighted** **Material Spectrochim. Acta, Part B: Atomic** **Spectroscopy, 1998, 53B(2), 299-309, http://www.sciencedirect.com/science/articl** **e/pii/S0584854797001432 H. M. Kingston, et. al. 02-27-98 11 299/309** **6800 Sec 16 (6)** **Application of Isotope Dilution in Elemental Speciation: Speciated Isotope Dilution Mass** **Spectrometry (SIDMS) This chapter discusses the application** **of isotope dilution in elemental speciation using speciated isotope** **dilution mass spectrometry. Supports Publication;** **Copyrighted Material** **Comprehensive Analytical Chemistry, J. A. Caruso, K. L. Sutton and K. L. Ackley** **(eds.), Vol. 33 (Elemental Speciation: New Approaches for Trace Element Analysis),** **Elsevier, New York, USA, 2000, p-277-313, http://www.sciencedirect.com/science/articl** **e/pii/S0166526X00800203 D. Huo, et. al. 2000 37 277/313** **6800 Sec 16 (7)** **The Accurate Determination of Species by Speciated Isotope Dilution Mass Spectrometry:** **Exemplified by the Evaluation of Chromium (VI) in Soil** **Supports Publication; Copyrighted** **Material The Twelfth Annual Waste Testing &** **Quality Assurance Symposium; Washington, DC, July 23-26, 1996, 112-** **119 H. M. Kingston, et. al. 8 112/119** **6800 Sec 16 (8)** **Determination and Correction of Analytical Biases and Study on Chemical Mechanisms in the** **Analysis of Cr(VI) in Soil Samples Using EPA Protocols** **Supports Publication; Copyrighted** **Material Environ. Sci. Tech., 1998, 32(21), 3418-** **3423, http://pubs.acs.org/doi/abs/10.1021/es9710** **29e D. Huo, et. al. 09-12-98 6 3418/3423** **6800 Sec 16 (9)** **IDMS and the National Reference System: Accuracy Transfer in Clinical Chemistry** **This article gives information on the use of IDMS, primarily for assigning** **certified values to human serum reference materials within the SRM** **program a NIST. Supports Publication;** **Copyrighted Material** **Anal. Chem., 1993, 65(12), 475 – 479, http://pubs.acs.org/doi/abs/10.1021/ac0006** **0a620 G. N. Bowers, et. al. 06-93 5 475/479** **6800 Sec 16 (10)** **The Use of Isotope Dilution Mass Spectrometry for the Certification of Standard Reference** **Materials Supports Publication;** **Copyrighted Material** **Environ. Intern., 1984, 10(2), 169-173 L. J. Moore, et. al.** **6800 Sec 16 (11)** **SamplePrep Supports Publication;** **Copyrighted Material** **[Homepage of SamplePrep Web], Available: http://www.sampleprep.duq.edu/,** **referenced 2011 H. M. Kingston, et. al.** **6800 Sec 16 (12)** **The Development of Methods in Speciated Isotope Dilution Mass Spectrometry (SIDMS) for** **Elemental Speciation of Chromium in Environmental Samples Using LC-ICP-MS** **Supports Publication; Copyrighted** **Material Doctoral Dissertation, Duquesne** **University, July 30, 1999 D. Huo 07-30-99** **6800 Sec 16 (13)** **Determination of hexavalent chromium by using speciated isotope-dilution mass spectrometry after** **microwave speciated extraction of environmental and other solid materials** **Supports Publication; Copyrighted** **Material Anal. Bioanal. Chem., 2005, 382(4), 1111-** **1120, http://www.springerlink.com/content/lh1m6** **70w184184rr/ G. M. M. Rahman, et. al. 06-05 10 1111/1120** **6800 Sec 16 (14)** **Determination and evaluation of hexavalent chromium in power plant coal combustion by** **products and cost-effective environmental remediation solutions using acid mine drainage** **Supports Publication; Copyrighted** **Material J. Environ. Monit., 2005, 7, 899-905,** **http://pubs.rsc.org/en/content/articlelanding /2005/em/b504724b** **H. M. "Skip" Kingston, et. al. 07-13-05 7 899/905** **6800 Sec 16 (15)** **Development of a microwave-assisted extraction method and isotopic validation of mercury species** **in soils and sedime Supports Publication;** **Copyrighted Material** **Anal. At. Spectrom., 2005, 20, 183-191, http://pubs.rsc.org/en/Content/ArticleLandin** **g/2005/JA/b404581e G. M. M. Rahman, et. al. 01-01-05 9 183/191** **6800 Sec 16 (16)** **Inter-laboratory Validation of EPA Method 3200 for mercury species analysis using prepared soil** **reference materials Supports Publication;** **Copyrighted Material** **J. Applied Organometallic Chem., 2005, 19, 301-307,** **http://onlinelibrary.wiley.com/doi/10.1002/a oc.816/abstract** **G. M. M. Rahman, et. al. 02-04-05 7 301/307 6800 Sec 16** **(17) Application of Speciated Isotope Dilution Mass** **Spectrometry to Evaluate Extraction Methods for Determining Mercury Speciation in Soils and** **Sediments Supports Publication;** **Copyrighted Material** **Anal. Chem., 2004, 76(13), 3548-3555, http://pubs.acs.org/doi/abs/10.1021/ac0304** **07x G. M. M. Rahman, et. al. 05-11-04 7 3548/3555** **6800 Sec 16 (18)** **Speciated isotope dilution mass spectrometry of reactive species and related methods** **Supports Publication; Copyrighted** **Material US Patent Number 6 790 673 B1, 2004** **and PCT Int. Appl. January 28, 1999, Patent No. WO 9939198** **H. M. Kingston 6800 Sec 16** **(19) Automated In-Process Ratio Mass Spectrometry** **Supports Publication; Copyrighted** **Material U.S. Patent Number 6,974,951 B1 H. M. Skip Kingston** **12-13-05 6800 Sec 16** **(20) Robust microwave-assisted extraction protocol for** **determination of total mercury and methylmercury in fish tissues** **Supports Publication; Copyrighted** **Material Analytica Chemica Acta, 631(2), 121-128,** **2009, http://www.sciencedirect.com/science/articl** **e/pii/S0003267008018229 L. Hinojosa Reyes, et. al. 01-12-09 8 121/128** **6800 Sec 16 (21)** **Application of Speciated Isotope Dilution Mass Spectrometry to Evaluate Methods for** **Efficiencies, Recoveries, and Quantification of Mercury Speciation Transformations in Human** **Hair Supports Publication;** **Copyrighted Material** **J. Anal. At. Spectrom, 2009, 24(1), 83-92, http://pubs.rsc.org/en/Content/ArticleLandin** **g/2009/JA/b805249b G. M. M. Rahman, et. al. 10-24-08 10 83/92** **6800 Sec 16 (22)** **Application of Double Spike Isotope Dilution for the Accurate Determination of Cr(III), Cr(VI) and** **Total Cr in Yeast Supports Publication;** **Copyrighted Material** **Anal. Bioanal. Chem., 2006, 386(6), 1673- 1680,** **http://www.springerlink.com/content/6871v 185q61j2v47/** **Lu Yang, et. al. 09-06-06 8 1673/1680 6800 Sec 16** **(23) Automated, On-Line, Trace Contamination and** **Chemical Species Analysis For the Semiconductor Industry** **Supports Publication; Copyrighted** **Material American Institute of Physics (AIP),** **Conference Proceedings, Proceedings form the 2003 Characterization and** **Metrology for ULSI Technology Conference, Volume 683, Melville, NY,** **2003 H. M. Skip Kingston, et. al.** **6800 Sec 16 (24)** **Development, Research and Validation of Environmental Speciation Methods: Evaluation by** **Speciated Isotope Dilution Mass Spectrometry in Mercury and Chromium Speciation Analysis** **Supports Publication; Copyrighted** **Material G. M. Mizanur Rahman, Duquesne** **University, Pittsburgh, PA USA, 2004 G. M. M. Rahman 08-19-04 229 1/229** **6800 Sec 16 (25)** **Calculations of Double Spike Isotope Dilution Results Revisited** **This article discusses the use of isotope pattern deconvolution analysis** **to simplify the double spiking species specific isotope dilution result** **calculations when inter-conversion might occur.** **Supports Publication; Copyrighted** **Material J. Analytical Atomic Spectrometry, 2006,** **21, 1294-1297, http://www.uc.edu/plasmachem/Documents** **/webpdfs1/Double%20Spike%20for%20Isot ope%20Ratios.pdf** **Juris Meija, et. al. 08-15-06 4 1294/1297 6800 Sec 16** **(26) Testing is an Essential Part of International** **Environmental Regulation and Commerce Compliance** **Supports Publication; Copyrighted** **Material Washington DC, NEMC Presentation 2008 Gonzalo Manch** **ego, et. al. 6800 Sec 16** **(27) 6800 Sec 16** **(28) Explicit Determinations in Speciated Isotope** **Dilution Mass Spectrometry without Calibration Curves** **Supports Publication; Copyrighted** **Material John Kern, et. al.** **6800 Sec 16 (29)** **Sensitivity Analysis for Speciated Isotope Dilution Mass Spectrometry** **Supports Publication; Copyrighted** **Material Journal of Analytical and Atomic** **Spectrometry, 25, 196-200, 2010, http://math.pugetsound.edu/~ctoews/resear** **ch/publications/revision.pdf C. Toews, et. al.** **11-05-09 5 196/200 6800 Sec 16** **(30) Speciation of Mercury in Crude Oil Using** **Speciated Isotope Dilution Mass Spectrometry This article describes the use of** **speciated isotope dilution mass spectrometry for the speciation of** **mercury in crude oil. Supports Publication;** **Copyrighted Material** **Spectroscopy, 25,1, 36-45, 2010, http://spectroscopyonline.findanalytichem.c** **om/spectroscopy/Feature/Speciation-of Mercury-in-Crude-Oil-Using** **Speciated/ArticleStandard/Article/detail/655 117** **G. M. Mizanur Rahman, et. al.** **01-01-10 10 36/45 6800 Sec 16** **(31) Speciation of Mercury in whole human blood by** **SIDMS SPME-GC-ICP-MS with Microwave Assisted Equilibration and Extraction** **Supports Publication; Copyrighted** **Material G. M. Mizanur Rahman, et.** **al. 6800 Sec 16** **(32) Comparison of methods with respect to** **efficiencies, recoveries, and quantitation of mercury species interconversions in food** **demonstrated using tuna fish This article describes the authors’** **evaluation of eight different analytical extraction procedures for mercury from** **biological samples. Supports Publication;** **Copyrighted Material** **Analytical Bioanalytical Chemistry, 390, 2123-2132, 2008,** **http://www.ncbi.nlm.nih.gov/pubmed/18317 738** **Laura H. Reyes, et. al. 04-08 10 2123/2132 6800 Sec 16** **(33) Zinc Dietary Supplement Contamination with** **Toxic Antimony Species Gregory M. Zinn, et. al.** **6800 Sec 16 (34)** **Glyphosate by IDMS and i-Spike IDMS as for Automated and Safe Toxic MS Analysis** **Rebecca L. Wagner, et. al. 6800 Sec 16** **(35) Glutathione analysis as a biomarker for immune** **stress and autism Timothy Fahrenholz, et. al.** **6800 Sec 16 (36)** **Human Gene Therapy Michael Passineau, et. al.** **6800 Sec 16 (37)** **Hexavalent Chromium in Contaminated Soil (High Level)** **This documentation is a certificate of analysis for high level hexavalent** **chromium in contaminated soil. Supports Publication;** **Copyrighted Material** **NIST Certificate of Analysis SRM 2701, 2009, https://www** **s.nist.gov/srmors/view_detail.cfm?srm=270 1** **NIST 03-10-02 1 0/0** **6800 Sec 16 (38)** **Development of a standard reference material for Cr(VI) in contaminated soil** **This article describes the development of a standard reference** **material for hexavalent chromium including the collection, processing,** **preparation, and preliminary physico chemical characterization of the** **material. Supports Publication;** **Copyrighted Material** **Journal of Analytical Atomic Spectroscopy, 23, 1550-1554, 2008,** **http://pubs.rsc.org/en/Content/ArticleLandin g/2008/JA/b808488b** **Stuart Nagourney, et. al. 09-29-08 5 1550/1554 6800 Sec 16** **(39) Characterization of waste – Stat of the art** **document – Chromium VI specification in solid matrices** **Supports Publication; Copyrighted** **Material PD CEN/TR 14589:2003, British** **Standards, EU publication “International Standards Correspondence Index,** **Technical Report CEN Technical Committee CEN/TC 292, European** **Committee for Standardization, 2003 04/03** **6800 Sec 16 (40)** **Sodium Azide Quantification for homeland defense by isotope dilution mass spectrometry** **EPA Method 6800 Gregory M. Zinn, et. al.** **6800 Sec 16 (41)** **Investigation into mercury bound to biothiols: structural identification using ESI-ion-trap MS and** **introduction of a method for their HPLC separation with simultaneous detection by ICP-MS and ESI** **MS In this article, authors describe a** **technique for the separation and molecular identification of mercury and** **methylmercury complexes derived from their reactions with cysteine and** **glutathione. Supports Publication;** **Copyrighted Material** **Analytical Bioanalytical Chemistry, 390, 1753-1764, 2008,** **http://www.springerlink.com/content/y7276 028411l8p53/fulltext.pdf** **Eva Krupp, et. al. 04-08 12 1753/1764 6800 Sec 16** **(42) US AIR FORCE Task Reports for the Homeland** **Security and Homeland Defense: extension of EPA Method 6800 conducted between 2007 and** **2010 with funding from the Headquarters of the US Air Force Surgeon General under the awards** **No.FA7014-07-0014 and No.FA7014-08-C-0029 H. M. Skip Kingston, et. al.** **6800 Sec 16 (43)** **Timothy Fahrenholz, Scott Faber, H. M. Skip Kingston, John Kern, Matt Pamuku,** **Hemasudha Chatragadda, Becky Pekar, “Quantification Glutathione Biomarkers in** **Autism” (in preparation 2012). Supports Publication;** **Copyrighted Material** **Will be available from journal at time of publishing** **6800 Sec 16 (44)** **Rebecca L. Wagner, Stephanie Wetzel, H. M. Skip Kingston“ Direct Speciated Isotope Dilution** **Mass Spectrometry of Analytical Methodology of Illicit Drug in Urine Using Time-of-Flight Mass** **Spectrometry” (in review 2012). Supports Publication;** **Copyrighted Material** **Will be available from journal at time of publishing** **8000D METHOD 8000D DETERMINATIVE CHROMATOGRAPHIC** **SEPARATIONS Method 8000 is not a determinative** **method but instead provides guidance on** **analytical chromatography and describes calibration and QC** **requirements common to all SW-846 chromatographic methods.** **method SW-846 03-12 PDF 56 1/56** **8000D (1) Department of Defense: Appendix G of DoD “Quality Systems Manual for** **Environmental Laboratories”, Version 4.2 Supports** **Publication; Copyrighted** **Material**http://www.denix.osd.mil/edqw/upload/QSM-V4-2-Final-102510.pdf**8000D (2) U.S.E.P.A Contract Laboratory Program SOM 01.2** **Supports Publication;** **Copyrighted Material** http://www.epa.gov/superfund/programs/clp/som1.htm**8000D (3) A list of quantitation limits for poorly- performing** volatile**compounds can be found in Table App D XIII-1** **Supports Publication;** **Copyrighted Material** http://www.epa.gov/region1/oeme/appendc.pdf**8000D (4) A list of quantitation limits for poorly- performing** semivolatile**compounds can be found in Table App E XIII-1** **Supports Publication;** **Copyrighted Material** http://www.epa.gov/region1/oeme/appendd.pdf**8021B METHOD 8021B AROMATIC AND HALOGENATED VOLATILES** **BY GAS CHROMATOGRAPHY USING PHOTOIONIZATION AND/OR ELECTROLYTIC** **CONDUCTIVITY DETECTORS Method 8021B is used to determine** **volatile organic compounds in a variety of solid waste matrices.** **Method SW-846 12-96 PDF 19 1/19** **8021B (1) “Volatile Organic Compounds in Water by P urge** **and-Trap Capillary Column Gas Chromatography with Photoionization and Electrolytic Conductivity** **Detectors in Series, Method 502.2, Rev. 2.0 (1989); Methods for the Detection of Organic** **Compounds in Drinking Water,” U.S. Environmental Protection Agency, Environmental** **Monitoring Systems Laboratory, Cincinnati, OH, EPA/600/4-88/039, December, 1988.** **Supports Publication; Copyrighted** **Material http://www.caslab.com/EPA** **Methods/PDF/502_2.pdf 1995 PDF 35 1/35** **8021B (2) “The Determination of Halogenated Chemica ls in** **Water by the Purge and Trap Method,” Method 502.1; U.S. Environmental Protection Agency,** **Environmental Monitoring and Support Laboratory, Cincinnati, OH 45268, September** **1986. Supports Publication;** **Copyrighted Material** **09-86 8021B (3) “Volatile Aromatic and Unsaturated Organi** **c Compounds in Water by Purge and Trap Gas** **Chromatography, Method 503.1;” U.S. Environmental Protection Agency, Environmental** **Monitoring and Support Laboratory, Cincinnati, OH, September 1986.** **Supports Publication; Copyrighted** **Material 8021B (4) Trace Analyses for Wastewaters** **Supports Publication; Copyrighted** **Material Environ. Sci. Technol., 1981, 15, 1426.** **http://pubs.acs.org/doi/abs/10.1021/es0009 4a002** **J. A. Glaser, et. al. 1981 PDF 10 1426/1435 8021B (5) The Determination of Synthetic Organic** **Compounds in Water by Purge and Sequential Trapping Capillary Column Gas Chromatography** **Supports Publication; Copyrighted** **Material U.S. Environmental Protection Agency,** **Environmental Monitoring and Support Laboratory, Cincinnati, OH 45268.** **http://books.google.com/books/about/The_ Determination_of_Synthetic_Organic_C.ht** **ml?id=Sdr5GwAACAAJ T. A. Bellar, et. al. 1985 70** **8111 METHOD 8111 HALOETHERS BY GAS CHROMATOGRAPHY** **This method is a gas chromatographic method used to determine the** **concentration of haloethers. Method SW-846** **12-1996 PDF 13 1/13 8111 (1) Application of Open-Tubular Columns to SW-** **846 GC Methods** **Supports Publication; Copyrighted** **Material Final Report to the US EPA on Contract** **68-03-3511, Mid-Pacific Environmental Laboratory, Mountain View, CA, 1990.** **V. Lopez-Avila, et. al. 1990 8111 (2) Performance Data for Methods 8041, 8091, 8** **111, and 8121A** **Supports Publication; Copyrighted** **Material Draft Report to US EPA on Contract 68-** **W9-0011, Science Applications International Corp., San Diego, CA, 1992.** **S. Tsang, et. al. 1992 8270D METHOD 8270D** **SEMIVOLATILE ORGANIC COMPOUNDS BY GAS CHROMATOGRAPHY/MASS** **SPECTROMETRY (GC/MS) This method is used to determine the** **concentration of semivolatile organic compounds in extracts prepared from** **many types of solid waste matrices, soils, air sampling media and water** **samples. Method SW-846** **02-07 PDF 68 1/68 8270D (1) Reference Compound to Calibrate Ion Abund** **ance Measurement in Gas Chromatography-Mass** **Spectrometry Systems Supports Publication;** **Copyrighted Material** **Analytical Chemistry, 47, 995-1000, 1975. http://pubs.acs.org/doi/abs/10.1021/ac6035** **7a061 J. W. Eichelberger, et. al. 1975 6 995/1000** **8270D (2) Method Detection Limit for Methods 924 an d 625** **Supports Publication; Copyrighted** **Material Unpublished report, October 1980. P. Olynk, et. al.** **10-80 8270D (3) Interlaboratory Method Study for EPA Meth** **od 625-Base/Neutrals, Acids, and Pesticides** **Supports Publication; Copyrighted** **Material Final Report for EPA Contract 68-03-3102.** **8270D (4) Gas Chromatography for Pesticide Residue Analysis: Some Practical Aspects** **Supports Publication; Copyrighted** **Material Journal of the Association of Official** **Analytical Chemists (AOAC), 48, 1037, 1965.** **J. A. Burke 1965 8270D (5) GC-MS Suitability Testing of RCRA Appendi** **x VIII and Michigan List Analytes** **Supports Publication; Copyrighted** **Material U.S. Environmental Protection Agency,** **Environmental Monitoring and Support Laboratory, Cincinnati, OH 45268,** **February 20, 1987, Contract No. 68-03- 3224.** **http://books.google.com/books/about/GC_ MS_Suitability_Testing_of_RCRA_Append.** **html?id=d6yqSgAACAAJ S. V. Lucas, et. al. 02-87 8** **8270D (6) Screening of Semivolatile Organic Compoun ds for** **Extractability and Aqueous Stability by SW-846, Method 3510** **Supports Publication; Copyrighted** **Material U.S. Environmental Protection Agency,** **Environmental Monitoring and Support Laboratory, Cincinnati, OH 45268, June 5,** **1987, Contract 68-03-3224. http://nepis.epa.gov/Exe/ZyNET.exe/2000T** **MKH.TXT?ZyActionD=ZyDocument&Client =EPA&Index=1986+Thru+1990&Docs=&Q** **uery=&Time=&EndTime=&SearchMethod= 1&TocRestrict=n&Toc=&TocEntry=&QField** **=&QFieldYear=&QFieldMonth=&QFieldDay =&IntQFieldOp=0&ExtQFieldOp=0&XmlQu** **ery=&File=D%3A%5Czyfiles%5CIndex%20 Data%5C86thru90%5CTxt%5C00000011%** **5C2000TMKH.txt&User=ANONYMOUS&P assword=anonymous&SortMethod=h%7C-** **&MaximumDocuments=1&FuzzyDegree=0 &ImageQuality=r75g8/r75g8/x150y150g16/** **i425&Display=p%7Cf&DefSeekPage=x&Se archBack=ZyActionL&Back=ZyActionS&Ba** **ckDesc=Results%20page&MaximumPages =1&ZyEntry=1&SeekPage=x&ZyPURL** **T. M Engel, et. al. 06-87 10 8270D (7) Development of a Soxtec Extraction Proced** **ure for Extraction of Organic Compounds from Soils and** **Sediments Supports Publication;** **Copyrighted Material** **U.S. Environmental Protection Agency, Environmental Monitoring and Support** **Laboratory, Las Vegas, NV, October 1991, EPA 600/X-91/140.** **http://books.google.com/books/about/Devel opment_of_a_Soxtec_Extraction_Proce.ht** **ml?id=SsA8twAACAAJ V. Lopez-Avila 10-91** **8270D (8) Laboratory Validation of VOST and SemiVOS T for** **Halogenated Hydrocarbons from the Clean Air Act Amendments List** **Supports Publication; Copyrighted** **Material Vol. 1 and 2, U.S. Environmental Protection** **Agency, EPA 600/R-93/123a and b, (NTIS PB 93-227163 and 93-27171), Research** **Triangle Park, NC, July 1993. http://nepis.epa.gov/Exe/ZyNET.exe/30003** **WHW.TXT?ZyActionD=ZyDocument&Clien t=EPA&Index=1991+Thru+1994&Docs=&Q** **uery=&Time=&EndTime=&SearchMethod= 1&TocRestrict=n&Toc=&TocEntry=&QField** **=&QFieldYear=&QFieldMonth=&QFieldDay =&IntQFieldOp=0&ExtQFieldOp=0&XmlQu** **ery=&File=D%3A%5Czyfiles%5CIndex%20 Data%5C91thru94%5CTxt%5C00000009%** **5C30003WHW.txt&User=ANONYMOUS&P assword=anonymous&SortMethod=h%7C-** **&MaximumDocuments=1&FuzzyDegree=0 &ImageQuality=r75g8/r75g8/x150y150g16/** **i425&Display=p%7Cf&DefSeekPage=x&Se archBack=ZyActionL&Back=ZyActionS&Ba** **ckDesc=Results%20page&MaximumPages =1&ZyEntry=1&SeekPage=x&ZyPURL** **J. Bursey, et. al. 07-93 8 8270D (9) Single Laboratory Method Validation Repor** **t: Extraction of Target Compound List/Priority** **Pollutant List BNAs and Pesticides Using Accelerated Solvent Extraction (ASE) with** **Analytical Validation by GC/MS and GC/ECD Supports Publication;** **Copyrighted Material** **Document 101124, Dionex Corporation, Salt Lake City, UT, June 16, 1994.** **B. Richter, et. al. 06-94 8270D (10) Supercritical Carbon Dioxide Extraction** **of Polycyclic Aromatic Hydrocarbons from** **Sediments Supports Publication;** **Copyrighted Material** **J. Chromatography A, 653, 83-91, (1993). http://www.sciencedirect.com/science/articl** **e/pii/002196739380394N H. B. Lee, et. al. 1993 9 83/91** **8270D (11) SFE Extraction of PNAs from Solid Matric es Using** **the Dionex 703M SFE Extractor and a Liquid Trap Supports Publication;** **Copyrighted Material** **EPA Region III, Central Regional Laboratory, 839 Bestgate Road, Annapolis,** **MD 21401, December 12, 1994. S. Warner 12-94** **8270D (12) 3M Data Submission to EPA Supports Publication;** **Copyrighted Material** **Letter to B. Lesnik, June 27, 1995. C. Markell 06-9 5** **8270D (13) Determination of Organic Compounds in Dr inking** **Water by Liquid-Solid Extraction and Capillary Column Gas Chromatography/Mass Spectrometry** **Supports Publication; Copyrighted** **Material USEPA Method 525.2, Environmental** **Monitoring Systems Laboratory, Office of Research and Development, US EPA,** **Cincinnati, OH, Revision 2.0, March 1995. http://water.epa.gov/scitech/methods/cwa/u** **pload/525_2-SOCs.pdf 03-95 60 1/60** **8270D (14) Analytical Method for the Analysis of Se mivolatile** **Organic Compounds Supports Publication;** **Copyrighted Material** **USEPA, Superfund Analytical Services/Contract Laboratory Program** **(CLP), Multi-Media, Multi-Concentration Organics Analysis, SOM01.X, Exhibit D -** **Analytical Methods, November 2003. 11-03** **8276 METHOD 8276 TOXAPHENE AND TOXAPHENE CONGENERS** **BY GAS CHROMATOGRAPHY/NEGATIVE ION CHEMICAL IONIZATION MASS** **SPECTROMETRY (GC-NICI/MS) Method 8276 is used to determine the** **concentrations of various toxaphene congeners and technical toxaphene in** **extracts from solid and liquid matrices, using fused-silica, open-tubular** **capillary columns with negative ion chemical ionization mass spectrometry** **(NICI/MS). method SW-846** **09-12 PDF 57 1/57 8276 (1) Chemical Ionization Mass Spectrometry** **Supports Publication; Copyrighted** **Material A. G. Harrison 06-15-92 Book 224 1/224** **8276 (2) Determination of Toxaphene in Soil by Elec tron** **Capture Negative Ion Mass Spectrometry After Fractionation by High-Performance Gel** **Permeation Chromatography Supports Publication;** **Copyrighted Material** **J. Chromatogr., 633, 177- 183, 1993.** **http://www.epa.gov/esd/chemistry/organal/r eports/toxpf/toxpf.htm** **W. C. Brumley, et. al. 02-24-93 7 177/183 8276 (3) Analytical Protocol (GC/NIMS) for OSWER’s** **Response to OIG Report (2005-P-00022) on Toxaphene Analysis** **Supports Publication; Copyrighted** **Material EPA/600/R-08/048 (TIP # 08-069,** **Published Report) U.S. Environmental Protection Agency.** **http://nepis.epa.gov/Adobe/PDF/9100D5NZ .PDF** **W. C. Brumley 02-13-08 17 1/17 8276 (4) Application of Open-Tubular Columns to SW-** **846 GC Methods** **Supports Publication; Copyrighted** **Material Report for the U.S. Environmental** **Protection Agency, Contract 68-03-3511. http://nepis.epa.gov/Exe/ZyNET.exe/30003** **UMO.TXT?ZyActionD=ZyDocument&Client =EPA&Index=1986+Thru+1990&Docs=&Q** **uery=&Time=&EndTime=&SearchMethod= 1&TocRestrict=n&Toc=&TocEntry=&QField** **=&QFieldYear=&QFieldMonth=&QFieldDay =&IntQFieldOp=0&ExtQFieldOp=0&XmlQu** **ery=&File=D%3A%5Czyfiles%5CIndex%20 Data%5C86thru90%5CTxt%5C00000006%** **5C30003UMO.txt&User=ANONYMOUS&P assword=anonymous&SortMethod=h%7C-** **&MaximumDocuments=1&FuzzyDegree=0 &ImageQuality=r75g8/r75g8/x150y150g16/** **i425&Display=p%7Cf&DefSeekPage=x&Se archBack=ZyActionL&Back=ZyActionS&Ba** **ckDesc=Results%20page&MaximumPages =1&ZyEntry=1&SeekPage=x&ZyPURL** **V. Lopez-Avila et. al. 09-90 12 1/12 8276 (5) Development and Application of Test Proced** **ures for Specific Organic Toxic Substances in** **Wastewaters Supports Publication;** **Copyrighted Material** **Category 10, Pesticides and PCB Report for the U.S. Environmental Protection** **Agency, Contract 68-03-2606. http://nepis.epa.gov/Exe/ZyNET.exe/2000V** **0S8.TXT?ZyActionD=ZyDocument&Client= EPA&Index=1976+Thru+1980&Docs=&Qu** **ery=&Time=&EndTime=&SearchMethod=1 &TocRestrict=n&Toc=&TocEntry=&QField=** **&QFieldYear=&QFieldMonth=&QFieldDay= &IntQFieldOp=0&ExtQFieldOp=0&XmlQue** **ry=&File=D%3A%5Czyfiles%5CIndex%20 Data%5C76thru80%5CTxt%5C00000006%** **5C2000V0S8.txt&User=ANONYMOUS&Pa ssword=anonymous&SortMethod=h%7C-** **&MaximumDocuments=1&FuzzyDegree=0 &ImageQuality=r75g8/r75g8/x150y150g16/** **i425&Display=p%7Cf&DefSeekPage=x&Se archBack=ZyActionL&Back=ZyActionS&Ba** **ckDesc=Results%20page&MaximumPages =1&ZyEntry=1&SeekPage=x&ZyPURL** **J. W. Rhoades, et. al. 01-80 89 1/89 8276 (6) Removal of Elemental Sulfur Interferences** **from Sediment Extracts for Pesticide Analysis** **Supports Publication; Copyrighted** **Material Bull. Environ. Contam. Toxicol., 6, 9, 1971.** **http://www.springerlink.com/content/v4u61 74186w55721/** **D. F. Goerlitz, et. al. 1971 2 9/10 8276 (7) Residue Analysis of Sediment and Sewage** **Sludge for Organochlorines in the Presence of Elemental Sulfur** **Supports Publication; Copyrighted** **Material Anal. Chem., 49, 316-318, 1977.** **http://pubs.acs.org/doi/abs/10.1021/ac5001 0a033** **S. Jensen, et. al. 02-77 3 316/318 8276 (8) Gel Permeation Chromatography in the GC/MS** **Analysis of Organics in Sludges Supports Publication;** **Copyrighted Material** **U.S. Environmental Protection Agency. R. H. Wise, et. al. Book 74 1/74** **8276 (9) Extraction of Chlorinated Hydrocarbon Insecticides from Soil** **Supports Publication; Copyrighted** **Material Agron. J., 60, 289, 1968.** **https://www.agronomy.org/publications/aj/a bstracts/60/3/AJ0600030289** **H. B. Pionke, et. al. 05-68 4 289/292 8276 (10) Experiments with Evaporation of Solutions** **of Chlorinated Pesticides** **Supports Publication; Copyrighted** **Material J. Assoc. Off. Anal. Chem., 49, 999, 1966. J. A. Bu** **rke, et. al. 1966 8 999/1006 8276 (11) Trace Analyses for Wastewaters** **Supports Publication; Copyrighted** **Material Environ. Sci. and Technol., 15, 1426, 1981.** **http://pubs.acs.org/doi/abs/10.1021/es0009 4a002** **J. A. Glazer, et. al. 12-81 10 1426/1435 8276 (12) Performance Data for SW-846 Methods 8270,** **8081, and 8141 Supports Publication;** **Copyrighted Material** **U.S. Environmental Protection Agency, EMSL-Las Vegas, EPA/600/4-90/015.** **http://nepis.epa.gov/Exe/ZyNET.exe/9100C V89.txt?ZyActionD=ZyDocument&Client=E** **PA&Index=1986%20Thru%201990&Docs= &Query=&Time=&EndTime=&SearchMeth** **od=1&TocRestrict=n&Toc=&TocEntry=&Q Field=&QFieldYear=&QFieldMonth=&QFiel** **dDay=&UseQField=&IntQFieldOp=0&ExtQ FieldOp=0&XmlQuery=&File=D%3A%5CZ** **YFILES%5CINDEX%20DATA%5C86THR U90%5CTXT%5C00000020%5C9100CV8** **9.txt&User=ANONYMOUS&Password=ano nymous&SortMethod=h%7C** **P. J. Marsden 06-90 102 1/120 8276 (13) Development of a Soxtec Extraction Proced** **ure for Extracting Organic Compounds from Soils and** **Sediments Supports Publication;** **Copyrighted Material** **EPA 600/X-91/140, U.S. Environmental Protection Agency, Environmental** **Monitoring Systems Laboratory V. Lopez-Avila (W. Beckert,** **Project Officer) 10-91 Book** **8276 (14) Solid-Phase Extraction of TCLP Leachates Supports Publication;** **Copyrighted Material** **Proceedings of the Tenth Annual Waste Testing and Quality Assurance** **Symposium, Arlington, VA C. Markell 07-94** **8276 (15) Supercritical Fluid Extraction of Organoc hlorine** **Pesticide Residues from Soils Supports Publication;** **Copyrighted Material** **Proceedings of the Tenth Annual Waste Testing and Quality Assurance** **Symposium, Arlington, VA D. Bennett, et. al. 07-94** **8276 (16) 3M Data Submission to EPA Supports Publication;** **Copyrighted Material** **Letter to B. Lesnik C. Markell 06-27-95 Letter 8276 (17) Single Laboratory Method Validation Repor** **t – Extraction of Organophosphorus Pesticides,** **Herbicides, and Polychlorinated Biphenyls Using Accelerated Solvent Extraction (ASE) with** **Analytical Validation by GC/NPD and GC/ECD Supports Publication;** **Copyrighted Material** **Dionex, Document 101124, Salt Lake City, UT** **B. Richter, et. al. 12-02-94 8276 (18) Evaluation of Rapid Solid Sample Extracti** **on Using the Microwave-Assisted Process (MAP** **TM )** **Under Closed-Vessel Conditions Supports Publication;** **Copyrighted Material** **Spectros. Int. J., 13 (1), 1-14, 1997. http://www.cem.de/documents/pdf/RE/RE0** **36.PDF K. Li, et. al. 1996/1997 PDF 13 1/13** **8276 (19) Pulsed Positive Ion Negative Ion Chemical Ionization Mass Spectrometric Applications to** **Environmental and Hazardous Waste Analysis Supports Publication;** **Copyrighted Material** **Biomed. Mass Spectrom. 10, 369, 1983. L. D. Betowsk i, et. al. 12-12-83 8 369/376** **8276 (20) Interlaboratory Study Plan for Validation of** **Method 8276 Supports Publication;** **Copyrighted Material** **Submitted to U.S. Environmental Protection Agency** **Science Applications International Corporation** **09-08 8276 (21) USEPA Region 4 Modified Method 3545A** **Standard Operating Procedure (SOP) for Pressurized Fluid Extraction (PFE)** **Supports Publication; Copyrighted** **Material Revision 4.1 11-05-10** **8276 (22) USEPA Region 4 Modified Method 3620C, SOP for Florisil® Cleanup** **Supports Publication; Copyrighted** **Material Revision 3.0 08-23-10** **8276 (23) USEPA Region 4 Modified Method 3630C SOP for Silica Gel Cleanup** **Supports Publication; Copyrighted** **Material Revision 3.1 08-10-11** **8276 (24) Inter-laboratory Validation for Fish Tiss ue Study** **Plan Supports Publication;** **Copyrighted Material** **Submitted to U.S. Environmental Protection Agency** **TechLaw Incorporated 09-11 8276 (25) Inter-laboratory Validation for Fish Tiss** **ue Analytical Data Report** **Supports Publication; Copyrighted** **Material Submitted to U.S. Environmental Protection** **Agency TechLaw Incorporated 05-12** **8276 (26) Inter-laboratory Validation for Fish Tiss ue Data** **Validation Report Supports Publication;** **Copyrighted Material** **Submitted to U.S. Environmental Protection Agency** **TechLaw Incorporated 05-12 8276 (27) Inter-laboratory Validation for Fish Tiss** **ue Statistical Analysis Report** **Supports Publication; Copyrighted** **Material Submitted to U.S. Environmental Protection** **Agency TechLaw Incorporated 05-12** **8276 (28) HRGC and HRGC-ECNI Determination of Toxaphene Residues in Fish with a New 22** **Components Standard Supports Publication;** **Copyrighted Material** **Organohalogen Compd., 26, 357, 1995. http://www.dioxin20xx.org/pdfs/1995/95-** **279.pdf H. Parlar, et. al. 1995 PDF 6 357/362** **8410 METHOD 8410 GAS CHROMATOGRAPHY/FOURIER** **TRANSFORM INFRARED (GC/FT-IR) SPECTROMETRY FOR SEMIVOLATILE** **ORGANICS: CAPILLARY COLUMN This method covers the automated** **identification, or compound class assignment of unidentifiable** **compounds, of solvent extractable semivolatile organic compounds which** **are amenable to gas chromatography, by GC/FT-IR.** **Method SW-846 09-94 PDF 17 1/17** **8410 (1) Handbook for Analytical Quality Control in Water** **and Wastewater Laboratories Supports Publication;** **Copyrighted Material** **U.S. Environmental Protection Agency, Environmental Monitoring and Support** **Laboratory. ORD Publication Offices of Center for Environmental Research** **Information: Cincinnati, OH, March 1979; Sec. 4, EPA-600/4-79-019.** **http://nepis.epa.gov/Exe/ZyPURL.cgi?Dock ey=30000PWG.txt** **03-79 164 1/164 8410 (2) Quantitative Analysis Using a Purged Split** **less Injection Technique** **Supports Publication; Copyrighted** **Material Hewlett Packard Application Note, ANGC** **7-79. R. R. Freeman** **8410 (3) Tables of Wavenumbers for the Calibration of** **Infrared Spectrometers Supports Publication;** **Copyrighted Material** **Pergamon: New York, 1977. http://books.google.com/books/about/Table** **s_of_wavenumbers_for_the_calibratio.html ?id=i7_vAAAAMAAJ** **R. H. Cole 1977 219 8410 (4) Criteria for Presentation of Spectra from** **Computerized IR Instruments Supports Publication;** **Copyrighted Material** **Appl. Spectrosc. 1982, 36, 87. http://www.opticsinfobase.org/as/abstract.cf** **m?id=127579 J. G. Grasselli, et. al. 1982 5 87/91** **8410 (5) The Interpretation of Vapor-Phase Infrared Spectra** **Supports Publication; Copyrighted** **Material Group Frequency Data; Volume I. Sadtler** **Laboratories: Philadelphia, PA, 1984. R. A. Nyquist 1984** **8410 (6) Infrared Characteristic Group Frequencies Supports Publication;** **Copyrighted Material** **John Wiley and Sons: New York, NY, 1980.** **http://www.amazon.com/Infrared Characteristic-Group-Frequencies** **Socrates/dp/0471275921 G. Socrates 1980 Book 166** **8410 (7) The infrared Spectra of Complex Organic Molecules** **Supports Publication; Copyrighted** **Material 2** **nd ed.; John Wiley and Sons: New York,** **NY, 1958. http://www.amazon.com/infra-red-spectra** **complex molecules/dp/B007T3ZVP0/ref=sr_1_2?s=** **books&ie=UTF8&qid=1355851489&sr=1- 2&keywords=infra** **red+spectra+complex+molecules L. J. Bellamy 1958** **8410 (8) Infrared Band Handbook Supports Publication;** **Copyrighted Material** **Volumes I and II; Plenum: New York, NY, 1965.** **H. A. Szymanski 1965 8410 (9) Interim Protocol for the Automated Analysi** **s of Semivolatile Organic Compounds by Gas** **Chromatography/Fourier Transform-Infrared Spectrometry** **Supports Publication; Copyrighted** **Material Appl. Spectrosc. 1985, 39, 826.** **http://www.opticsinfobase.org/as/abstract.cf m?uri=as-39-5-827** **D. F. Gurka 1985 7 827/833 8410 (10) Capillary GC/FT-IR** **Supports Publication; Copyrighted** **Material Anal. Chem. 1983, 55, 1361A.** **http://pubs.acs.org/doi/abs/10.1021/ac0026 3a784** **P. R. Griffiths, et. al. 1983 27 1361A/1387 A** **8410 (11) Fourier Transform-Infrared Spectrometry Supports Publication;** **Copyrighted Material** **Wiley-Interscience: New York, NY, 1986. http://onlinelibrary.wiley.com/doi/10.1002/9** **780470106310.fmatter/pdf P. R. Griffiths, et. al. 1986 16** **8410 (12) Quantitation Capability of a Directly Lin ked Gas** **Chromatography/Fourier Transform Infrared/Mass Spectrometry System** **Supports Publication; Copyrighted** **Material Anal. Chem. 1989, 61, 1584.** **http://pubs.acs.org/doi/pdf/10.1021/ac0018 9a022** **D. F. Gurka, et. al. 1989 6 1584/1589 8430 METHOD 8430** **ANALYSIS OF BIS(2-CHLOROETHYL) ETHER AND HYDROLYSIS PRODUCTS BY DIRECT** **AQUEOUS INJECTION GC/FT-IR This method provides procedures for** **the identification and quantitation of bis(2-chloroethyl) ether and its** **hydrolysis compounds in aqueous matrices by direct aqueous injection** **and gas chromatography with detection by a fourier transform** **infrared spectrometer. Method SW-846** **12-96 PDF 11 1/11 8430 (1) Identification of Bis(2-chloroethyl) ether** **Hydrolysis Products by Direct Aqueous Injection GC/FT-IR** **Supports Publication; Copyrighted** **Material J. of High Res. Chrom. 12, 693-696, 1989.** **http://onlinelibrary.wiley.com/doi/10.1002/jh rc.1240121016/abstract** **W. D. Payne, et. al. 1989 4 693/696 9013 METHOD 9013A** **CYANIDE EXTRACTION PROCEDURE FOR SOLIDS AND OILS** **The extraction procedure described in this method is designed for the** **extraction of soluble and insoluble cyanides from solid, oil, and multi** **phase wastes. The resulting extraction solutions may be analyzed for total** **cyanide and/or cyanides amenable to chlorination (e.g., Methods 9010, 9012** **and 9014) as well as analyzed for metal cyanide complexes (e.g.,** **Method 9015). method SW-846** **03-12 PDF 13 1/13 9013 (1)** **American Society for Testing and Materials, "Understanding Cyanide Species," D 6696, ASTM** **International, 2004. Supports** **Publication; Copyrighted** **Material www.astm.org.** **9013 (2) R. S. Ghosh, D. A. Dzombak, R. G. Luthy,** **"Equilibrium Precipitation and Dissolution of Iron Cyanide Solids in Water," Environ. Eng. Sci., Vol.** **16, 293-313, 1999. Supports** **Publication; Copyrighted** **Material 9013 (3)** **J. C. L. Meeussen, M. G. Keizer, W. H. van Riemsdijk, F. A. M. de Haan, "Dissolution** **Behavior of Iron Cyanide (Prussian Blue) in Contaminated Soils," Environ. Sci. Technol., Vol.** **26, 1832-1838, 1992. Supports** **Publication; Copyrighted** **Material 9013 (4)** **J. C. L Meeussen, W. H. Keizer, F. A. M. de Haan, "Chemical Stability and Decomposition** **Rate of Iron Cyanide Complexes in Soil Solutions," Environ. Sci. Technol., Vol. 26, 511-** **516, 1992. Supports** **Publication; Copyrighted** **Material 9013 (5)** **J. T. Bushey, D. A. Dzombak, "Ferrocyanide Adsorption on Aluminum Oxides," J. Coll. Int. Sci.,** **Vol. 272, 46-51, 2004. Supports** **Publication; Copyrighted** **Material 9013 (6)** **T. L. Theis, M. L West, "Effects of Cyanide Complexation on the Adsorption of Trace Metals** **at the Surface of Goethite," Environ. Technol. Letters, Vol. 7, 309-318, 1986.** **Supports Publication;** **Copyrighted Material** **9013 (7) The RETEC Group, Inc., "Metal Cyanide** **Complexes by Anion Exchange Chromatography and UV Detection Method Validation Summary** **Report," March, 2004. Supports** **Publication; Copyrighted** **Material 9014 METHOD 9014** **CYANIDE IN WATERS AND EXTRACTS USING TITRIMETRIC AND MANUAL** **SPECTROPHOTOMETRIC PROCEDURES This method can be used for** **measuring free (non-complexed) cyanide and hydrocyanic acid in** **drinking water, natural surface waters, domestic and industrial wastewaters,** **and in soil extracts. This method may also be used as a determinative step** **for quantifying total and amenable cyanide in the alkaline distillates from** **Method 9010. method SW-846** **03-12 PDF 13 1/13 9015 METHOD 9015** **METAL CYANIDE COMPLEXES IN WATERS AND WASTE EXTRACTS USING** **ANION EXCHANGE CHROMATOGRAPHY AND UV DETECTION** **This method covers the determination of metal cyanide complexes in waters and** **extracts of solid wastes using anion exchange chromatography and UV** **detection (Refs. 1, 2). The following analytes have been determined by this** **method: Analyte** **[Ag(CN) 2** **] -** **[Au(CN) 2** **] -** **[Co(CN) 6** **] 3** **- [Cu(CN)** **3 ]** **2 -** **[Fe(CN) 6** **] 3** **- [Fe(CN)** **6 ]** **4 -** **[Ni(CN) 4** **] 2** **- method SW-846** **03-12 PDF 53 1/53 9015 (1) Standard Test Method for Determination of** **Metal Cyanide Complexes in Wastewater, Surface** **Water, Groundwater and Drinking Water using Anion Exchange Chromatography with UV** **Detection Supports Publication;** **Copyrighted Material** **D 6994, ASTM International, 2004 American Society f or Testing** **and Materials 9015 (2) Determination of Metal Cyanides This appl** **ication note describes a method for determining concentration** **of transition metal cyanides by anion exchange chromatography.** **Supports Publication; Copyrighted** **Material Dionex Application Note No. 55,** **November, 1989, http://www.dionex.com/en** **us/webdocs/4151-AN55_V15.pdf Dionex Corporation 11-89 3 0/0** **9015 (3) Standard Guide for Understanding Cyanide Species** **Supports Publication; Copyrighted** **Material D 6696, ASTM International, 2004 American Society f** **or Testing and Materials** **9015 (4) Equilibrium Precipitation and Dissolution of Iron** **Cyanide Solids in Water In this article the equilibrium solubility** **behavior of iron cyanide solids was studied as a function of pH, pE, and** **other solution conditions. Supports Publication;** **Copyrighted Material** **Environ. Eng. Sci., Vol. 16, 293-313, 1999, http://cat.inist.fr/?aModele=afficheN&cpsidt** **=1890662 R. S. Ghosh, et. al. 07-01-99 21 293/313** **9015 (5) Chemical Stability and Decomposition Rate of Iron** **Cyanide Complexes in Soil Solutions This article investigates the speciation** **of dissolved cyanide under certain conditions relevant to soil and** **groundwater environments. Supports Publication;** **Copyrighted Material** Environ. Sci. Technol.**, Vol. 26, 511-516, 1992,** **http://pubs.acs.org/doi/abs/10.1021/es0002 7a010** **J. C. L. Meeussen, et. al. 03-92 6 511/516 9015 (6) Dissolution Behavior of Iron Cyanide (Prus** **sian Blue) in Contaminated Soils** **Supports Publication; Copyrighted** **Material**Environ. Sci. Technol.**, Vol. 26, 1832-1838, 1992** **J. C. L. Meeussen, et. al. 9015 (7) Cyanide Extraction Procedure for Solids an** **d Oils, Method 9013** **Supports Publication; Copyrighted** **Material U.S. EPA Office of Solid Waste SW-846** **Manual US EPA** **9015 (8) Toxicity to Fish of Cyanides and Related Compounds: A Review** **In this review the toxicity of cyanides and related compounds on fish are** **examined. Supports Publication;** **Copyrighted Material** **EPA Report No. 600/3-76-038, 1976 P. Doudoroff 04-7 6 155 1/155** **9015 (9) Total and Amenable Cyanide: Distillation, Method** **9010 Supports Publication;** **Copyrighted Material** **U.S. EPA Office of Solid Waste SW-846 Manual** **US EPA 9015 (10) "Standard Test Methods for Cyanides in Wa** **ter Supports Publication;** **Copyrighted Material** **D 2036, ASTM International, 2004 9015 (11) Standard Methods for the Examination of W** **ater and Wastewater** **American Public Health Association** **9015 (12) Determination of Trace Level Ions by Ion Chromatography with Concentrator Columns** **In this article ion chromatography techniques used to perform trace** **analysis down to 2 ppb for anions in solution are described.** **Supports Publication; Copyrighted** **Material Analytical Chemistry, Vol. 15, No. 9, 1532-** **1535, 1979, http://pubs.acs.org/doi/abs/10.1021/ac5004** **5a040 R. A. Wetzel, et. al. 08-79 4 1532/1535** **9015 (13) Sunlight-Induced Photochemistry of Aqueou s** **Solutions of Hexacyanoferrate(II) and –(III) Ions This article investigates the** **photochemically induced processes in alkaline aqueous solutions of** **hexacyanoferrate (II) and -(III). Supports Publication;** **Copyrighted Material** **Environ. Sci. Technol., Volume 27, 1875- 1879, 1993,** **http://pubs.acs.org/doi/abs/10.1021/es0004 6a016** **W. S. Rader, et. al. 09-93 5 1875/1879 9015 (14) Photochemistry of Co-ordination Compounds** **_XV This article investigates the photochemical behaviour of some** **cyanide complexes at various wavelenghts.** **Supports Publication; Copyrighted** **Material J. inorg. Nucl. Chem., Vol. 28, 2589-2597,** **1966, http://www.sciencedirect.com/science/articl** **e/pii/0022190266803834 L. Moggi, et. al. 9 2589/2597** **9015 (15) Product Manual IonPacÒ ATC-3 2-mm Anion Trap Column IonPac ATC-3 4-mm Anion Trap** **Column IonPac ATC-HC Anion Trap Column This manual describes how to prepare** **these columns for operation in the laboratory.** **Supports Publication; Copyrighted** **Material Document No. 032697, Revision 08, July** **12, 2002, http://www.dionex.com/en us/webdocs/40850-32697-08_IonPacATC** **HC_3_MAN_V16.pdf Dionex Corporation 7-12-02 12 1/12** **9015 (16) Product Manual IonPac® AG2 Guard Column IonPac® AG3 Guard Column IonPac® AG4** **Guard Column IonPac® AG5 Guard Column IonPac® CG2 Guard Column IonPac® AS2** **Analytical Column IonPac® AS3 Analytical Column IonPac® AS4 Analytical Column IonPac®** **AS5 Analytical Column IonPac® CS2 Analytical Column** **This manual describes how to prepare these columns for operation in the** **laboratory. Supports Publication;** **Copyrighted Material** **Document No. 032226, Revision 14, May 12, 2002, http://www.dionex.com/en** **us/webdocs/4395-32226- 14_AS2345_CS2_V17.pdf** **Dionex Corporation 05-12-02 14 1/14 9015 (17) Product Manual IonPac® AG11 Guard Column** **IonPac® AS11 Analytical Column This manual is for the IonPac®** **AS/AG11 analytical columns designed to resolve a large number of inorganic** **and organic acid ions from a single sample injection in one gradient run.** **Supports Publication; Copyrighted** **Material Document No. 034791, Revision 08, May** **14, 2003, http://www.dionex.com/en us/webdocs/4445-Man-034791-12-IonPac** **AS11-Apr10.pdf Dionex Corporation 05-14-03 44 1/44** **9015 (18) Dionex Installation and Troubleshooting G uide for** **the IonPacÒ MFC-1 Metal-Free Trap Column This manual is for the metal-free trap** **column which is specifically designed for on-line cleanup of eluent ionic** **transition metal impurities in ion chromatography.** **Supports Publication; Copyrighted** **Material Document No. 034990, Revision 02, June** **26, 1998, http://www.dionex.com/en us/webdocs/4463-34990-** **04_IP_MFC_V30.pdf Dionex Corporation 11-06 4 1/4** **9015 (19) Determinative Chromatographic Separations ,** **Method 8000 Supports Publication;** **Copyrighted Material** **U.S. EPA Office of Solid Waste SW-846 Manual** **US EPA 9015 (20) NIST Critically Selected Stability Consta** **nts of Metal Complexes Database, Version 5.0** **Database Software Supports Publication;** **Copyrighted Material** **NIST Standard Reference Database 46, U.S. Department of Commerce,** **Gaithersburg, Maryland, 1998 R. M. Smith, et. al.** **9015 (21) The NBS Tables of Chemical Thermodynamic Properties, Selected Values for Inorganic and C** **1 and C** **2 Organic Substances in SI Units** **Supports Publication; Copyrighted** **Material Journal of Physical and Chemical** **Reference Data, Vol. 11, Supplement 2, 1- 392, 1982** **D. D. Wagman, et. al. 9015 (22) Metal Cyanide Complexes by Anion Exchange** **Chromatography and UV Detection Method Validation Summary Report** **The RETEC Group, Inc. 03-04 9015 (23) Total and Amenable Cyanide (Automated** **Colorimetric, with Off-Line Distillation), Method 9012** **U.S. EPA Office of Solid Waste SW-846 Manual** **US EPA Method 9320** **Radium 228 This method covers the measurement** **of radium-228 in ground water and, if desired, the determination of radium** **226 on the same sample. If the level of radium-226 is above 3 pCi/L, the** **sample must also be measured for radium-228.** **Method 06-12 PDF 13 1/13** **9320 (1) Standard Methods for the Examination of Water and Wastewater, 15th ed.,** **Supports Publication; Copyrighted** **Material Method 707, p. 600, 1980.** **http://www.standardmethods.org/ Greenberg, A.E., J.J.** **Connors, and D.J. Jenkens, eds.** **1980 600 9320 (2) Determination of Radium 228 in Natural Wat** **ers. Radiochemical Analysis of Water. U.S. Govt.** **Printing Office, Washington, D.C., 1971. Supports Publication;** **Copyrighted Material** **U.S. Geol. Surv., Water Supply Paper 1696-G.** **http://pubs.usgs.gov/wsp/1696g/report.pdf Johnson, J.O. 1971 PDF 152 1/152** **9320 (3) Prescribed Procedures for Measurement of Radioactivity in Drinking Water,.** **Supports Publication; Copyrighted** **Material Environmental Monitoring and Support** **Laboratory, U.S. EPA, Cincinnati, OH, EPA-600/4-75-008,** **http://nepis.epa.gov/ Krieger, H.L. 1976 PDF 33 1/33** **Chapter 1 Project Quality Assurance and Quality Control** **The goal of this chapter is to provide an understanding of environmental** **data and the need for quality. Chapter SW-846** **USEPA 03-12 PDF 25 1/25 Chapter 1 (1) Guidance on Systematic Planning Using** **the Data Quality Objectives Process** **Supports Publication; Copyrighted** **Material EPA QA/G-4, Quality Staff, Office of** **Environmental Information, United States Environmental Protection Agency,** **Washington, D.C. February 2006. http://www.epa.gov/quality/qs-docs/g4-** **final.pdf USEPA 02-06 PDF 121 1/111** **Chapter 1 (2) EPA Quality Manual for Environmental Programs** **CIO 2105-P-01-0 Supports Publication;** **Copyrighted Material** **Office of Environmental Information Quality Staff, United States Environmental** **Protection Agency, Washington, D.C. May 5, 2000.** **http://www.epa.gov/irmpoli8/policies/2105P 010.pdf** **USEPA 05-05-00 PDF 63 0/0 Chapter 1 (3) Guidance on Choosing a Sampling Desig** **n for Environmental Data Collection** **Supports Publication; Copyrighted** **Material EPA QA/G-5S, Quality Staff, Office of** **Environmental Information, United States Environmental Protection Agency,** **Washington, D.C. December 2002. http://www.epa.gov/quality/qs-docs/g5s** **final.pdf USEPA 12-02 PDF 178 1/166** **Chapter 1 (4) Guidance on Environmental Data Verifi cation and** **Data Validation Supports Publication;** **Copyrighted Material** **EPA QA/G-8, Quality Staff, Office of Environmental Information, United States** **Environmental Protection Agency, Washington, D.C. November 2002.** **http://www.epa.gov/quality/qs-docs/g8- final.pdf** **USEPA 11-02 PDF 96 1/76 Chapter 1 (5) Data Quality Assessment: A Reviewer’** **s Guide Supports Publication;** **Copyrighted Material** **QA/G-9R, Quality Staff, Office of Environmental Information, United States** **Environmental Protection Agency, Washington, D.C. February 2006.** **http://www.epa.gov/quality/qs-docs/g9r final.pdf** **USEPA 02-06 PDF 61 1/55 Chapter 1 (6) Data Quality Assessment: Statistical** **Tools for Practitioners** **Supports Publication; Copyrighted** **Material QA/G-9S, Quality Staff, Office of** **Environmental Information, United States Environmental Protection Agency,** **Washington, D.C. February 2006. http://www.epa.gov/quality/qs-docs/g9s** **final.pdf USEPA 02-06 PDF 198 1/191** **Chapter 1 (7) Guidance for Preparing Standard Opera ting** **Procedures Supports Publication;** **Copyrighted Material** **EPA QA/G-6, Quality Staff, Office of Environmental Information, United States** **Environmental Protection Agency, Washington, D.C. April 2007.** **http://www.epa.gov/quality/qs-docs/g6- final.pdf** **USEPA 04-07 PDF 60 1/55 Chapter 1 (8) RCRA Waste Sampling Draft Technical G** **uidance Supports Publication;** **Copyrighted Material** **Office of Solid Waste, United States Environmental Protection Agency,** **Washington, D.C. August 2002. http://www.epa.gov/wastes/hazard/testmet** **hods/sw846/pdfs/rwsdtg_a.pdf USEPA 08-02 PDF 61 1/49** **Chapter 1 (9) Guidance for Quality Assurance Projec t Plans** **Supports Publication; Copyrighted** **Material EPA QA/G-5, Quality Staff, Office of** **Environmental Information, United States Environmental Protection Agency,** **Washington, D.C. December 2002. http://www.epa.gov/quality/qs-docs/g5-** **final.pdf USEPA 12-02 PDF 111 1/58** **Chapter 1 (10) EPA Requirements for Quality Assuran ce Project** **Plans Supports Publication;** **Copyrighted Material** **EPA QA/R-5, Office of Environmental Information. United States Environmental** **Protection Agency, Washington, D.C. March 2001.** **http://www.epa.gov/quality/qs docs/r5-final.pdf** **USEPA 03-01 PDF 40 1/24 Chapter 1 (11) RCRA Delisting Program Guidance Manu** **al for the Petitioner** **Supports Publication; Copyrighted** **Material United States Environmental Protection** **Agency, March 23, 2000. http://www.epa.gov/region6/6pd/rcra_c/pd** **o/delist23.pdf USEPA 03-23-00 PDF 61 1/57** **Chapter 1 (12) Waste Analysis at Facilities That Ge nerate, Treat,** **Store and Dispose of Hazardous Wastes, ECDIC 2002-011** **Supports Publication; Copyrighted** **Material Office of Waste Programs Enforcement,** **United States Environmental Protection Agency. April 1994.** **http://www.epa.gov/compliance/resources/ policies/civil/rcra/wasteanalygman-rpt.pdf** **USEPA 04-94 PDF 200 0/0 Chapter 1 (13) Guidance on Technical Audits and Rel** **ated Assessments for Environmental Data Operations** **Supports Publication; Copyrighted** **Material QA/G-7, Quality Staff, Office of** **Environmental Information, United States Environmental Protection Agency,** **Washington, D.C. January 2000. http://www.epa.gov/quality/qs-docs/g7-** **final.pdf USEPA 01-00 PDF 101 1/78** **Chapter 2 CHOOSING THE CORRECT PROCEDURE** **The purpose of this chapter is to aid the analyst in choosing the appropriate** **methods for sample analyses, based upon the sample matrix and the** **analytes to be determined. Chapter SW-846** **USEPA 03-12 PDF 86 1/86 Chapter 2 (1) TOC Determinations in Ground Water Th** **is article describes the evaluation of a modified TOC procedure that permits** **the quantitation of the VOC fraction in ground water samples.** **Supports Publication; Copyrighted** **Material Ground** **Water 1984, 22(1)** **, 18-24, http://info.ngwa.org/gwol/pdf/840629056.P** **DF M. J. Barcelona 01-84 7 18/24** **Chapter 2 (2) Development and Evaluation of Methods for Total** **Organic Halide and Purgeable Organic Halide in Wastewater** **This article describes the laboratory evaluation of two approaches for** **determining total purgeable and nonpurgeable organic halides in** **wastewater. Supports Publication;** **Copyrighted Material** **U.S. Environmental Protection Agency; Office of Research and Development;** **Environmental Monitoring and Support Laboratory; ORD Publication Offices of** **Center for Environmental Research Information; Cincinnati, OH, 1984; EPA** **600/4-84-008, http://nepis.epa.gov/Exe/ZyPURL.cgi?Dock** **ey=500024JK.txt R. Riggin, et. al. 01-84 3 0/0** **Chapter 2 (3) Determination of Inorganic Anions in Water by Ion** **Chromatography Supports Publication;** **Copyrighted Material** **(Technical addition to Methods for Chemical Analysis of Water and** **Wastewater, EPA 600/4-79-020), U.S. Environmental Protection Agency;** **Environmental Monitoring and Support Laboratory; ORD Publication Offices of** **Center for Environmental Research Information; Cincinnati, OH, 1984; EPA** **600/4-84-017 G. McKee, et. al.** **Chapter 3 INORGANIC ANALYTES** **This chapter provides guidance for the analysis of inorganic analytes in a** **variety of matrices. Chapter SW-846** **USEPA 03-12 PDF 29 1/29 Chapter 3 (1) Principles of Instrumental Analysis T** **his text describes the principles and applications of modern analytical** **instruments. Supports Publication;** **Copyrighted Material** **Principles of Instrumental Analysis, 3rd ed, Saunders College Publishing, Philadelphia,** **PA, 1985 D. A. Skoog 1995** **Chapter 3 (2) Sampling Ambient Water for Trace Meta ls at EPA** **Water Quality Criteria Levels, Method 1669 This is a test method for sampling** **ambient water for trace metals to support water quality monitoring** **programs under the Clean Water Act. Supports Publication;** **Copyrighted Material** **U.S. Environmental Protection Agency, Office of Water, Washington, D.C., 1996,** **http://www.ecy.wa.gov/programs/wq/waste water/method_1669.pdf** **US EPA 07-98 38 0/0 Chapter 3 (3) Influence of Laboratory Environment o** **n the Precision and Accuracy of Trace Element** **Analysis In this article, the influence of the** **laboratory air quality on the precision and accuracy of elemental analysis at** **trace and ultratrace levels was investigated.** **Supports Publication; Copyrighted** **Material Anal. Chem., 1985, 57, 1728-1733,** **http://pubs.acs.org/doi/abs/10.1021/ac0028 5a050** **S. B. Adeloju, et. al. 1985 6 1728/1733 Chapter 3 (4) Microwave Enhanced Chemistry: Fundam** **entals, Sample Preparation, and Applications** **Supports Publication; Copyrighted** **Material Microwave Enhanced Chemistry:** **Fundamentals, Sample Preparation, and Applications, American Chemical Society,** **Washington, DC, 1997, p. 257-279. S. H. Kingston, et. al. 1997 23 257/279** **Chapter 3 (5) NBS Clean Laboratories for Trace Elem ent** **Analysis Supports Publication;** **Copyrighted Material** **Anal. Chem., 1982, 54, 1358A-1376A J. R. Moody 198 2 19 1358A/1376** **A Chapter 3 (6) National Bureau of Standards Special** **Publication 422 Accuracy in Trace Analysis: Sampling,** **Sample Handling, and Analysis Supports Publication;** **Copyrighted Material** **National Bureau of Standards Special Publication 422 Accuracy in Trace** **Analysis: Sampling, Sample Handling, and Analysis, National Bureau of Standards,** **Gaithersburg, MD, 1976, p. 509-539 T. Murphy 1976 31 509/539** **Chapter 3 (7) Determination of Trace Elements Supports Publication;** **Copyrighted Material** **Determination of Trace Elements, VCH, New York, NY, 1994, p. 1-38** **G. Tolg, et. al. 1994 38 1/38 Chapter 3 (8) Chemical Analysis, Vol. 47** **Supports Publication; Copyrighted** **Material Chemical Analysis, Vol. 47, John Wiley &** **Sons, New York, NY, 1976 M. Zief, et. al. 1976** **Chapter 3 (9) Production and Analysis of Special Hi gh-Purity** **Acids Purified by Sub-Boiling Distillation This article describes the use of sub** **boiling distillation for the production of high purity inorganic acids and water.** **Supports Publication; Copyrighted** **Material Anal. Chem., 1972, 44, 2050-2056,** **http://pubs.acs.org/doi/abs/10.1021/ac6032 0a016** **E. C. Kuehner, et. al. 1972 7 2050/2056 Chapter 3 (10) Purified Reagents for Trace Metal An** **alysis This article reviews 10 years of experience in the production of** **reagent acids and describes a new lab specifically designed to allow for** **trouble-free operation and production of high quality reagents.** **Supports Publication; Copyrighted** **Material Talanta, 1982, 29(11, Part 2), 1003-1010,** **http://www.sciencedirect.com/science/articl e/pii/0039914082802415** **J. R. Moody, et. al. 11-82 8 1003/1010 Chapter 3 (11) Purification of Inorganic and Organi** **c Materials Supports Publication;** **Copyrighted Material** **Purification of Inorganic and Organic Materials, Marcel Dekker, New York, NY,** **1969, p. 297-306, http://onlinelibrary.wiley.com/doi/10.1002/jp** **s.2600590137/abstract E. C. Kuehner, et. al. 01-70 10 297/306** **Chapter 3 (12) The Sampling, Handling and Storage o f Materials** **for Trace Analysis Supports Publication;** **Copyrighted Material** **Philos. Trans. R. Soc. London, 1982, 305, 669-680, 12.** **http://www.jstor.org/pss/37123 J. R. Moody 07-05-82 12 669/680** **Chapter 3 (13) Selection and Cleaning of Plastic Co ntainers for** **Storage of Trace Element Samples This article describes a study that** **examines the levels of impurities present in different types of plastics** **and the quantities of impurities leached by acid cleaning the plastics** **as well as presenting a method of cleaning containers.** **Supports Publication; Copyrighted** **Material Anal. Chem., 1977, 49, 2264-2267,** **http://chemgroups.northwestern.edu/ohallor an/grouponly/MoodyLindstrom1977.pdf** **J. R. Moody, et. al. 12-77 4 2264/2267 Chapter 3 (14) Clean Chemistry for Trace Analysis** **Supports Publication; Copyrighted** **Material Environmental Testing and Analysis, 1995,** **4, 24-27 F. J. Prevatt 1995 4 24/27** **Chapter 3 (15) Clean Room and Microwave Digestion Techniques: Improvement in Detection Limits for** **Aluminum Determination by GF-AAS This article describes the effects of** **using of a clean room and a closed vessel microwave digestion system on** **a method for ppb concentrations in biological materials using GF-AAS.** **Supports Publication; Copyrighted** **Material Appl. Spectrosc., 1988, 42, 1302-1306,** **http://www.cem.de/documents/pdf/publikati on/digestion/RD006.PDF** **E. M. Skelly, et. al. 01-88 6 1302/1306 Chapter 3 (16) Identifying Sources of Lead Contamin** **ation by Stable Isotope Techniques** **This article describes how investigations were persued to use** **naturally occurring variations in stable lead isotope abundances to find the** **sources of lead in particular environments.** **Supports Publication; Copyrighted** **Material Environ. Sci. Technol., 1972, 6, 705-709,** **http://pubs.acs.org/doi/abs/10.1021/es6006 7a003** **M. B. Rabinowitz, et. al. 08-72 5 705/709 Chapter 3 (17) U.S. National Bureau of Standards Te** **chnical Note 545** **This report describes the research activities and scientific programs of the** **Microchemical Analysis Section of the Analytical Chemistry Division of the** **National Bureau of Standards, Institute for Materials Research during from** **July 1969 to June 1970. Supports Publication;** **Copyrighted Material** **National Bureau of Standards, Gaithersburg, MD, 1970, p. 53-54,** **http://babel.hathitrust.org/cgi/pt?seq=1&vie w=image&size=100&id=mdp.39015001325** **276&page=root&orient=0 E. J. Maienthal 12-70 114 1/114** **Chapter 3 (18) The Coastal Bend Bays Project This p resentation information on the** **Regional Coastal Assessment Program.** **Supports Publication; Copyrighted** **Material 26th Annual Conference on Analysis of** **Pollutants in the Environment, Chicago, IL 2003,** **http://www.epa.gov/emap/html/pubs/docs/g roupdocs/symposia/symp2004/presentation** **s/BrienNicolau.pdf P. N. Boothe, et. al.** **Chapter 3 (19) Living in the Environment This is an environmental science text** **that focuses on prevention of and solutions to environmental problems.** **Supports Publication; Copyrighted** **Material Living in the Environment, Wadsworth Inc.,** **Belmont, CA, 1994, http://www.coursesmart.com/living-in-the** **environment-enhanced homework/miller/dp/9780495387633** **G. T. Miller 1994 Chapter 3 (20)** **Sampling for Analytical Purposes Supports Publication;** **Copyrighted Material** **Wiley, New York, NY, 1998. P. Gy 07-98 Chapter 3 (21) Pierre Gy’s Sampling Theory and Samp** **ling Practice** **Supports Publication; Copyrighted** **Material Second Edition, CRC Press, Inc., Boca** **Raton, FL, 1993. F.F. Pitard 1993** **Chapter 3 (22) Correct Sampling Using the Theories of Pierre Gy** **Supports Publication; Copyrighted** **Material USPEA Office of Research and** **Development, Las Vegas, NV, 1999. http://www.epa.gov/esd/factsheets/csutpg.p** **df USEPA 03-99 2 1/2** **Chapter 3 (23) Guidance for Obtaining Representativ e** **Laboratory Analytical Subsamples from Particulate Laboratory Samples** **Supports Publication; Copyrighted** **Material USEPA Office of Research and** **Development, 2003. http://www.epa.gov/osp/hstl/tsc/Gerlach200** **3.pdf USEPA 2003 156 1/134** **Chapter 4 ORGANIC ANALYTES** **This chapter discusses sampling and analysis methods used for organic** **analytes. Chapter SW-846** **USEPA 03-12 PDF 22 1/22 Chapter 4 (1) Summary Report - Evaluation of the Im** **pact of Post-Holding Time Analyte Degradation on** **Regulatory Decision-Making - VOCs in Water Supports Publication;** **Copyrighted Material** **Oak Ridge National Laboratory. 2001 A. B. Dindal, e t. al. 2001** **Chapter 4 (2) Standard Practice for Estimation of Holding Time** **for Water Samples Containing Organic and Inorganic Constituents** **Supports Publication; Copyrighted** **Material ASTM Standard D4841, 1988 (2008),** **ASTM International, West Conshohocken, PA, 2003, DOI: 10.1520/D4841-88R08,** **www.astm.org ASTM 2008** **Chapter 4 (3) Study Design and Analytical Results U sed to** **Evaluate Stability of Volatile Organic Compounds in Water Matrices** **Supports Publication; Copyrighted** **Material United States Geological Survey Open-File** **Report 98-637. 1999. J. T. Love, et. al. 1999** **Chapter 4 (4) Stability of Volatile Organics in Env ironmental** **Water Samples: Storage and Preservation Supports Publication;** **Copyrighted Material** **Oak Ridge National Laboratory ORNL/TM 11300. 1989.** **http://www.dtic.mil/cgi bin/GetTRDoc?AD=ADA412461** **M. P. Maskarinec, et. al. 1989 Electronic file 144 1/139** **Chapter 4 (5) Stability of VOCs in Water samples Du ring Pre** **analytical Holding. Part 1. Analyses by a Commercial Laboratory** **Supports Publication; Copyrighted** **Material Oak Ridge National Laboratory ORNL/TM** **13240/V1. 1996. O. R. West, et. al. 1996** **Chapter 4 (6) Stability of VOCs in Water samples Du ring Pre** **analytical Holding. Part 2. Analyses by an EPA Regional Laboratory** **Supports Publication; Copyrighted** **Material Oak Ridge National Laboratory ORNL/TM** **13240/V2. 1997. http://www.osti.gov/bridge/servlets/purl/656** **450-6XVR0S/webviewable/656450.pdf O. R. West, et. al. 1997 PDF** **Chapter 4 (7) Practical Reporting Times for Environ mental** **Samples Supports Publication;** **Copyrighted Material** **Environmental Science and Technology, 28: 1430-1436. 1994.** **C. K. Bayne, et. al. 1994 7 1430/1436 Chapter 4 (8) Final Report - Stability of Volatile** **Organics in Environmental Soil samples** **Supports Publication; Copyrighted** **Material Oak Ridge National Laboratory ORNL/TM** **12128. 1992. M. P. Maskarinec, et. al. 1992** **Chapter 4 (9) Preservation and Holding Times Study for Vinyl** **Chloride, Styrene in Industrial Wastewater Supports Publication;** **Copyrighted Material** **Test America, January 2012. Test America, Methods Contract archives** **01-12 Chapter 4 (10) Preservation and Holding Times Study** **for Vinyl Chloride, Styrene in Municipal Wastewater** **Supports Publication; Copyrighted** **Material Hampton Roads Sanitation District in** **Virginia Beach, Virginia, January 2012. Hampton Roads Sanitation** **District in Virginia Beach, Virginia** **01-12 Chapter 4 (11) Standard Guide for Sampling Waste an** **d Soils for Volatile Organic Compounds** **Supports Publication; Copyrighted** **Material ASTM Guide D4547, 1991 (2009), ASTM** **International, West Conshohocken, PA, 2003, DOI: 10.1520/D4547-09,** **www.astm.org ASTM 2009** **Chapter 4 (12) Sample Holding Time Re-evaluation Supports Publication;** **Copyrighted Material** **U.S. Environmental Protection Agency. EPA/600/R-05/124. 2005.** **http://www.epa.gov/esd/cmb/research/bs_0 33cmb06.pdf** **USEPA 2005 329 Chapter 4 (13) Performance of Hydrochloric Acid and** **Trisodium Phosphate as Preservatives for Selected Organic** **Compounds in Ground Water Supports Publication;** **Copyrighted Material** **In: A Guide for Assessing Biodegradation and Source Identification of Organic** **Ground Water Contaminants using Compound Specific Isotope Analysis, EPA** **600/R-08/148. 2008. http://www.epa.gov/nrmrl/pubs/600r08148/** **600r08148.pdf USEPA 12-08 82 1/67** **Chapter 4 (14) Standard Practice for Using the Disp osable En** **Core Sample for Sampling and Storing Soil for Volatile Organic Analysis** **Supports Publication; Copyrighted** **Material ASTM Standard Practice D6418, 2003** **(2009), ASTM International, West Conshohocken, PA, 2003, DOI:** **10.1520/D6418-09, www.astm.org ASTM** **Chapter 4 (15) RCRA Organic Methods Workgroup Meeti ng** **Minutes 01-19-12 RCRA Organic Methods Workgroup** **Meeting Minutes, January 19, 2012. RCRA Organic Methods** **Workgroup Chapter 4 (16) RCRA Organic Methods Workgroup Meeti** **ng Minutes 01-26-12** **RCRA Organic Methods Workgroup Meeting Minutes, January 26, 2012.** **RCRA Organic Methods Workgroup** **Chapter 4 (17) RCRA Organic Methods Workgroup Meeti ng** **Minutes 02-09-12 RCRA Organic Methods Workgroup** **Meeting Minutes, February 9, 2012. RCRA Organic Methods** **Workgroup Chapter 4 (18) Integrity of VOA Vial Seals Support** **s Publication; Copyrighted** **Material EPA/600/R-00/066. 2000.** **http://www.epa.gov/esd/cmb/research/pape rs/bs124.pdf** **USEPA 09-00 PDF 42 1/18 Chapter 5** **MISCELLANEOUS TEST METHODS This chapter covers test methods not** **covered in chapters 2 and 4 Chapter SW-846** **USEPA 03-12 PDF 3 1/3**