### Name: Patricia Q. West

Title: Manager, Environmental, Energy Supp Company: Progress Energy Florida, Inc. Sign Date: 9/3/2010 Name: Carl Vineyard, P.E. Title: Project Manager Company: Grace Consulting, Inc. Sign Date: 9/3/2010 Permitted Facility Representative / Date Testing Company Representative / Date 

## Crystal River 5 Final Test Report for

/ / Based on information and belief formed after reasonable inquiry, I certify that the statements and information in this test report are true, accurate, and complete. I have reviewed all testing details and results in this test report and hereby certify that the test report is authentic and accurate.

Thursday, February 17, 2011 Page 1 of 14

### Crystal River 5
9/3/2010 Facility Information: Crystal River Power Plant Unit 5
15760 West Power Line Road

Crystal River FL 344286708 Contact: Dave Meyer Phone: 727-820-5229 Fax: 727-820-5229 Email: Dave.Meyer@pgnmail.com Testing Company: Grace Consulting, Inc.
PO Box 58
510 Dickson St. Wellington OH 44090 Contact: Hal Stiles Phone: 440-647-6672 Fax: 440-647-6673 Email: halstiles@gcitest.com

Air Permit Number: 0170004-024-AV Permitted Source ID/Name: Crystal River North Plant 0170004 Permitted Maximum Process Rate: 7200 mmBtu/hr Max. Normal Operation Process Rate: 7200 mmBtu/hr Target Process Test Rate 6480 mmBtu/hr

Description of the source (including control equipment). Please see the attachments for source or process flow diagram: diagram attached

The following describes any modifications and/or deviations to the applicable test methods. If alternative methods were requested, see the attachments for documentation of request AND approval, including dates. Industry/SCC/NAIS 221112

Sampling Location Information:

Test Parameter Information: AFS #: FRS #: 110017431215

SCC / Description 10100202 External Combustion Boilers - Electric Generation - Bituminous/Subbituminous Coal - Pulverized Coal: Dry Bottom (Bituminous Coal)

The following state and federal regulations that apply to the proposed testing:

Location Round

Duct Diam. Distance from upstream dist. Distance from

downstream dist. Number of

Traverse Ports Equiv. Diam Min.Travers Points Rect. Duct Length /Width Stack Unit 5 372 1248 3744 4 0 12 0 0

Target Parameter Test Method Number of

Test Runs Test Run

Duration Sample

Points Comments Location Hydrogen Fluoride Method 26A 3 180 0 Stack Unit 5 Hydrogen Chloride Method 26A 3 180 0 Stack Unit 5 O2 Method 3A O2 3 180 0 Stack Unit 5 Co2 Method 3A CO2 3 180 0 3 points Stack Unit 5 Sulfur Dioxide Method 6C 3 180 0 Stack Unit 5 Nitrogen oxides (NOx) Method 7E 3 180 0 Stack Unit 5



### Thursday, February 17, 2011 Page 2 of 14

### Crystal River 5
9/3/2010 The following describes any modifications and/or deviations to the applicable test methods. If alternative methods were requested, see the attachments for documentation of request AND approval, including dates. HCN will be collected using CTM-033 with 2 N NaOH to help keep the pH of the impingers above 12. The sample time for CTM-033 will be 60 minutes with a target sample volume of 30 cubic ft.



### Thursday, February 17, 2011 Page 3 of 14

### Crystal River 5
9/3/2010 Sampling / Stack Data Results Summary



### Location Stack Unit 5 - Method 26A Average Run Number M26A-1 M26A-2 M26A-3
Test Date 3/29/2010 3/29/2010 3/29/2010 Run Start Time 8:22:30 AM 8:07:30 AM 3:22:30 PM

Run Finish Time 11:30:00 AM 11:15:00 AM 6:30:00 PM

Net Run Time, minutes 180 180 180 Dry Gas Meter Volume Sampled, dscf 113.625 113.706 112.937 113.423 Moisture Content of Stack Gas, % 14.51 12.72 14.07 13.767 Moisture Saturation at Stack Gas Temperature, % 13.41 13.43 13.15 13.330 Carbon Dioxide, % 12.5 12.4 12.3 12.400 Oxygen, % 6.6 6.8 6.9 6.767 Average Stack Gas Temperature, °F 124.75 124.83 124.04 124.540 Dry Volumetric Flow Rate, dry scfm 1,834,924.7 1,854,113.4 1,825,986.5 1,838,341.53 3 Actual Wet Volumetric Flue Gas Flow Rate, acfm 2,400,615.1 2,406,049.4 2,378,877.8 2,395,180.76 7 Percent Isokinetic of Sampling Rate, % 100.2 99.2 100.1 99.833 F-Factor, dscfm/MMBtu @ %O2 9690 9563 9436 9,563.000
Fw 0 0 0 0.000
Fc 0 0 0 0.000



### Location Stack Unit 5 - Method 3A CO2 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Fuel Type
Fw
Fc



### Thursday, February 17, 2011 Page 4 of 14

### Crystal River 5
9/3/2010
Location Stack Unit 5 - Method 3A O2 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Fuel Type
Fw
Fc



### Location Stack Unit 5 - Method 6C Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Fuel Type
Fw
Fc



### Thursday, February 17, 2011 Page 5 of 14

### Crystal River 5
9/3/2010
Location Stack Unit 5 - Method 7E Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Fuel Type
Fw
Fc



### Thursday, February 17, 2011 Page 6 of 14

### Crystal River 5
9/3/2010 Emissions Summary

Process Run Data 

### Location: Stack Unit 5 - Method 26A Compound: Hydrogen Chloride Average RunNumber M26A-1 M26A-2 M26A-3 Mass_mg 0.79 1.602 0.597 0.996 lb/mmBtuO2 2.17E-04 4.40E-04 1.64E-04 0.000 

### Compound: Hydrogen Fluoride Average RunNumber M26A-1 M26A-2 M26A-3 Mass_mg 1.933 0.5272 0.335 0.932 lb/mmBtuO2 5.31E-04 1.45E-04 9.21E-05 0.000



### Location: Stack Unit 5 - Method 6C Compound: Sulfur Dioxide Average Run 1 2 3 lb/mmBtuO2 6.52E-02 6.66E-02 6.39E-02 0.065 ppm 2.77E+01 2.82E+01 2.73E+01 27.733 ppm@7%O2 2.69E+01 2.78E+01 2.71E+01 27.267



### Location: Stack Unit 5 - Method 7E Compound: Nitrogen oxides (NOx) Average Run 1 2 3 lb/mmBtuO2 4.49E-02 4.49E-02 4.70E-02 0.046 ppm 2.65E+01 2.65E+01 2.80E+01 27.000 ppm@7%O2 2.58E+01 2.61E+01 2.78E+01 26.567



### Thursday, February 17, 2011 Page 7 of 14

### Crystal River 5
9/3/2010 Process Run Data

APCD Run Data 

### Run Name Value UOM Comments Target Value 1 Coal Burned 288 Tons/hr 280


### 1 Steam Output 5290 1000 lb steam/hr 5240
1 Flue Gas Carbon Dioxide Content 9.6 % 10.1
1 Flue Gas Sampling Point Temperature 129 Deg F 128


### 1 Flue Gas Sampling Point Pressure 29.2 in. Hg 29.2
1 Unit Gross Electrical Output 770 Mwe 750
1 Unit Net Electric Generation 718 MWh 715


### 1 Scrubber Liquor pH 5.92 pH 5.45
1 Scrubber Liquor Flow Rate 166 gpm 150
1 Heat Input 6690 mmBtu/hr 6500


### 2 Coal Burned 289 Tons/hr 280
2 Steam Output 5300 1000 lb steam/hr 5240
2 Flue Gas Carbon Dioxide Content 10.9 % 10.1


### 2 Flue Gas Sampling Point Temperature 128 Deg F 128
2 Flue Gas Sampling Point Pressure 29.2 in. Hg 29.2
2 Unit Gross Electrical Output 770 Mwe 750


### 2 Unit Net Electric Generation 718 MWh 715
2 Scrubber Liquor pH 5.8 pH 5.45
2 Scrubber Liquor Flow Rate 166 gpm 150


### 2 Heat Input 6723 mmBtu/hr 6500
3 Coal Burned 290 Tons/hr 280
3 Steam Output 5305 1000 lb steam/hr 5240


### 3 Flue Gas Carbon Dioxide Content 10.9 % 10.1
3 Flue Gas Sampling Point Temperature 128 Deg F 128


### 3 Flue Gas Sampling Point Pressure 29.2 in. Hg 29.2
3 Unit Gross Electrical Output 772 Mwe 750
3 Unit Net Electric Generation 720 MWh 715


### 3 Scrubber Liquor pH 5.9 pH 5.45
3 Scrubber Liquor Flow Rate 676 gpm 150
3 Heat Input 6742 mmBtu/hr 6500

Run Name Value UOM Comments Target Value 

### 1 Precipitator 0 Thursday, February 17, 2011 Page 8 of 14

### Crystal River 5
9/3/2010

Process Lab Run Data 1 0


### 1 0

Thursday, February 17, 2011 Page 9 of 14

### Crystal River 5
9/3/2010 Sampling / Stack Data Results Detail



### Location Stack Unit 5 - Method 26A Average Run Number M26A-1 M26A-2 M26A-3 Test Date 3/29/2010 3/29/2010 3/29/2010 Run Start Time 8:22:30 AM 8:07:30 AM 3:22:30 PM Run Finish Time 11:30:00 AM 11:15:00 AM 6:30:00 PM Net Traversing Points 25 25 25 Net Run Time, minutes 180 180 180 Nozzle Diameter, inches 0.218 0.218 0.218 0.218 Pitot Tube Coefficient 0.84 0.84 0.84 0.840 Dry Gas Meter Calibration Factor 1.016 1.016 1.016 1.016 Barometric Pressure, inches of Mercury 29.3 29.3 29.3 29.300 Average Orifice Meter Differential, inches H2O 1.49 1.49 1.48 1.487 Dry Gas Meter Volume Sampled, cubic feet 118.132 118.485 118.088 118.235 Average Dry Gas Meter Temperature, °F 88.21 89.46 91.33 89.667 Dry Gas Meter Volume Sampled, dscf 113.625 113.706 112.937 113.423 Total Moisture Liquid collected, g 409.5 352.1 392.9 384.833 Volume of Water Vapor, standard cubic feet 19.28 16.57 18.49 18.113 Moisture Content of Stack Gas, % 14.51 12.72 14.07 13.767 Moisture Saturation at Stack Gas Temperature, % 13.41 13.43 13.15 13.330 Dry Mole Fraction 0.8659 0.8728 0.8685 0.869 Carbon Dioxide, % 12.5 12.4 12.3 12.400 Oxygen, % 6.6 6.8 6.9 6.767 Carbon Monoxide & Nitrogen, % 80.9 80.8 80.8 80.833 Fuel Factor 1.14 1.14 1.14 Dry Molecular Weight, lb/lb-Mole 30.26 30.26 30.24 30.253 Wet Molecular weight, lb/lb-Mole 28.81 28.70 28.80 28.770 Flue Gas Static Pressure, inches of H2O -0.68 -0.55 -0.66 -0.630 Absolute Flue Gas Pressure, inches of Mercury 29.25 29.26 29.25 29.253 Average Stack Gas Temperature, °F 124.75 124.83 124.04 124.540 Average Velocity Head, inches of H2O 0.7853431111 7961 0.786119188

212873 0.771784683

297989 0.781
Average Stack Gas Velocity, feet/second 53.01 53.13 52.53 52.890 Stack Cross-Sectional Area, square feet 754.768 754.768 754.768 754.768 Dry Volumetric Flow Rate, dry scfm 1,834,924.7 1,854,113.4 1,825,986.5 1,838,341.5 33 Actual Wet Volumetric Flue Gas Flow Rate, acfm 2,400,615.1 2,406,049.4 2,378,877.8 2,395,180.7 67 Percent Isokinetic of Sampling Rate, % 100.2 99.2 100.1 99.833 Percent Excess Air, % 44.7 46.8 47.8 46.433 F-Factor, dscfm/MMBtu @ %O2 9690 9563 9436 9,563.000 Round Duct Diameter, inches 372 372 372 Rectangular Duct Width, inches 0 0 0 Rectangular Duct Length, inches 0 0 0 Fw 0 0 0 0.000 Fc 0 0 0 0.000



### Thursday, February 17, 2011 Page 10 of 14

### Crystal River 5
9/3/2010
Location Stack Unit 5 - Method 3A CO2 Average Run Number Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type Fw Fc Cgasw Cgasw Units



### Thursday, February 17, 2011 Page 11 of 14

### Crystal River 5
9/3/2010
Location Stack Unit 5 - Method 3A O2 Average Run Number Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type Fw Fc Cgasw Cgasw Units



### Thursday, February 17, 2011 Page 12 of 14

### Crystal River 5
9/3/2010
Location Stack Unit 5 - Method 6C Average Run Number Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type Fw Fc Cgasw Cgasw Units



### Thursday, February 17, 2011 Page 13 of 14

### Crystal River 5
9/3/2010
Location Stack Unit 5 - Method 7E Average Run Number Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type Fw Fc Cgasw Cgasw Units



### Thursday, February 17, 2011 Page 14 of 14