Becky Wehrman

Enclosed are the results of analyses for samples received by the laboratory on 08/31/10 09:30. If you have any 

questions concerning this report, please feel free to contact me at 1-800-858-5227.

RE: Waste Sampling

Altoona, IA 50009

301 12th Ave SW

SmartER

10 January 2011

ANALYTICAL REPORT FOR SAMPLES

Client Sample ID Laboratory ID Matrix Date Sampled Date Received

N-Gum 01 10I0330-01 Solid 08/30/10 17:18 08/31/10 09:30

N-Gum (T) 02 10I0330-02 Solid 08/30/10 17:20 08/31/10 09:30

N-Patch 01 10I0330-03 Solid 08/30/10 17:22 08/31/10 09:30

N-Patch (T) 02 10I0330-04 Solid 08/30/10 17:24 08/31/10 09:30

War 01 10I0330-05 Solid 08/30/10 17:26 08/31/10 09:30

War 02 (T) 10I0330-06 Solid 08/30/10 17:28 08/31/10 09:30

Physo 01 10I0330-07 Solid 08/30/10 17:30 08/31/10 09:30

Physo 02 (T) 10I0330-08 Solid 08/30/10 17:32 08/31/10 09:30

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in 

its entirety.

Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989

Newton, IA 50208

Page 1 of 13
SmartER

301 12th Ave SW [none]

Becky Wehrman

Waste Sampling

Altoona IA, 50009

Project:

Project Number:

Project Manager:

Reported

01/10/11 14:50

Analyte Result Limit Batch

Reporting

Units Dilution Prepared Analyzed Method Notes 

N-Gum 01

10I0330-01 (Solid)

Date Sampled:8/30/2010 5:18:00PM

Keystone Laboratories, Inc. - Newton

Determination of Base/Neutral Extractable Compounds

Nicotine ND 0.00005 ug 1 1I02035 09/15/10 09/15/10 12:28 EPA 8270B

88.9 % 23-114 " " " "

Surrogate: 2-Fluorobiphenyl

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in 

its entirety.

Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989

Newton, IA 50208

Page 2 of 13
SmartER

301 12th Ave SW [none]

Becky Wehrman

Waste Sampling

Altoona IA, 50009

Project:

Project Number:

Project Manager:

Reported

01/10/11 14:50

Analyte Result Limit Batch

Reporting

Units Dilution Prepared Analyzed Method Notes 

N-Gum (T) 02

10I0330-02 (Solid)

Date Sampled:8/30/2010 5:20:00PM

Keystone Laboratories, Inc. - Newton

Determination of Base/Neutral Extractable Compounds

Nicotine ND 0.00005 ug 1 1I02035 09/15/10 09/15/10 13:04 EPA 8270B

99.2 % 23-114 " " " "

Surrogate: 2-Fluorobiphenyl

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in 

its entirety.

Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989

Newton, IA 50208

Page 3 of 13
SmartER

301 12th Ave SW [none]

Becky Wehrman

Waste Sampling

Altoona IA, 50009

Project:

Project Number:

Project Manager:

Reported

01/10/11 14:50

Analyte Result Limit Batch

Reporting

Units Dilution Prepared Analyzed Method Notes 

N-Patch 01

10I0330-03 (Solid)

Date Sampled:8/30/2010 5:22:00PM

Keystone Laboratories, Inc. - Newton

Determination of Base/Neutral Extractable Compounds

Nicotine 35.8 0.00005 ug 1 1I02035 09/15/10 09/15/10 13:39 EPA 8270B

87.7 % 23-114 " " " "

Surrogate: 2-Fluorobiphenyl

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in 

its entirety.

Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989

Newton, IA 50208

Page 4 of 13
SmartER

301 12th Ave SW [none]

Becky Wehrman

Waste Sampling

Altoona IA, 50009

Project:

Project Number:

Project Manager:

Reported

01/10/11 14:50

Analyte Result Limit Batch

Reporting

Units Dilution Prepared Analyzed Method Notes 

N-Patch (T) 02

10I0330-04 (Solid)

Date Sampled:8/30/2010 5:24:00PM

Keystone Laboratories, Inc. - Newton

Determination of Base/Neutral Extractable Compounds

Nicotine ND 0.00005 ug 1 1I02035 09/15/10 09/15/10 14:15 EPA 8270B

91.8 % 23-114 " " " "

Surrogate: 2-Fluorobiphenyl

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in 

its entirety.

Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989

Newton, IA 50208

Page 5 of 13
SmartER

301 12th Ave SW [none]

Becky Wehrman

Waste Sampling

Altoona IA, 50009

Project:

Project Number:

Project Manager:

Reported

01/10/11 14:50

Analyte Result Limit Batch

Reporting

Units Dilution Prepared Analyzed Method Notes 

War 01

10I0330-05 (Solid)

Date Sampled:8/30/2010 5:26:00PM

Keystone Laboratories, Inc. - Newton

Determination of Metabolic Acids

Warfarin Sodium 6.4 5.0 ug 1 1L01646 12/15/10 12/15/10 18:05 HPLC/UV

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in 

its entirety.

Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989

Newton, IA 50208

Page 6 of 13
SmartER

301 12th Ave SW [none]

Becky Wehrman

Waste Sampling

Altoona IA, 50009

Project:

Project Number:

Project Manager:

Reported

01/10/11 14:50

Analyte Result Limit Batch

Reporting

Units Dilution Prepared Analyzed Method Notes 

War 02 (T)

10I0330-06 (Solid)

Date Sampled:8/30/2010 5:28:00PM

Keystone Laboratories, Inc. - Newton

Determination of Metabolic Acids

Warfarin Sodium ND 5.0 ug 1 1L01646 12/15/10 12/15/10 18:22 HPLC/UV

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in 

its entirety.

Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989

Newton, IA 50208

Page 7 of 13
SmartER

301 12th Ave SW [none]

Becky Wehrman

Waste Sampling

Altoona IA, 50009

Project:

Project Number:

Project Manager:

Reported

01/10/11 14:50

Analyte Result Limit Batch

Reporting

Units Dilution Prepared Analyzed Method Notes 

Physo 01

10I0330-07 (Solid)

Date Sampled:8/30/2010 5:30:00PM

Keystone Laboratories, Inc. - Newton

Determination of Metabolic Acids

Physostigmine Salicylate ND 100 ug 1 1L01433 12/10/10 12/13/10 17:50 HPLC/UV

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in 

its entirety.

Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989

Newton, IA 50208

Page 8 of 13
SmartER

301 12th Ave SW [none]

Becky Wehrman

Waste Sampling

Altoona IA, 50009

Project:

Project Number:

Project Manager:

Reported

01/10/11 14:50

Analyte Result Limit Batch

Reporting

Units Dilution Prepared Analyzed Method Notes 

Physo 02 (T)

10I0330-08 (Solid)

Date Sampled:8/30/2010 5:32:00PM

Keystone Laboratories, Inc. - Newton

Determination of Metabolic Acids

Physostigmine Salicylate ND 100 ug 1 1L01433 12/10/10 12/13/10 18:09 HPLC/UV

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in 

its entirety.

Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989

Newton, IA 50208

Page 9 of 13
SmartER

301 12th Ave SW [none]

Becky Wehrman

Waste Sampling

Altoona IA, 50009

Project:

Project Number:

Project Manager:

Reported

01/10/11 14:50

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

 Analyte Limit Notes 

Determination of Base/Neutral Extractable Compounds - Quality Control

Keystone Laboratories, Inc. - Newton

Batch 1I02035 - Solvent Extraction

Blank (1I02035-BLK1) Prepared & Analyzed: 09/15/10 

Nicotine ND 0.00005 ug

Surrogate: 2-Fluorobiphenyl 1710 " 2020.00 84.7 23-114

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in 

its entirety.

Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989

Newton, IA 50208

Page 10 of 13
SmartER

301 12th Ave SW [none]

Becky Wehrman

Waste Sampling

Altoona IA, 50009

Project:

Project Number:

Project Manager:

Reported

01/10/11 14:50

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

 Analyte Limit Notes 

Determination of Metabolic Acids - Quality Control

Keystone Laboratories, Inc. - Newton

Batch 1L01433 - PCB Wipe

Blank (1L01433-BLK1) Prepared: 12/10/10 Analyzed: 12/13/10 

Physostigmine Salicylate ND 100 ug

LCS (1L01433-BS1) Prepared: 12/10/10 Analyzed: 12/13/10 

Physostigmine Salicylate 295.0 100 ug 319.000 92.5 70-130

LCS Dup (1L01433-BSD1) Prepared: 12/10/10 Analyzed: 12/13/10 

Physostigmine Salicylate 287.6 100 ug 319.000 90.2 70-130 2.53 20

Batch 1L01646 - PCB Wipe

Blank (1L01646-BLK1) Prepared & Analyzed: 12/15/10 

Warfarin Sodium ND 5.0 ug

LCS (1L01646-BS1) Prepared & Analyzed: 12/15/10 

Warfarin Sodium 647.9 5.0 ug 626.000 104 70-130

LCS Dup (1L01646-BSD1) Prepared & Analyzed: 12/15/10 

Warfarin Sodium 647.2 5.0 ug 626.000 103 70-130 0.114 20

Certified Analyses Included in This Report

Method/Matrix Analyte Certifications

Code Certifying Authority Certificate Number Expires

KS-KC Kansas Department of Health and Environment-KC E-10110 04/30/2011

KS-NT Kansas Department of Health and Environment E-10287 10/30/2011

NELAC New Jersey Department of Environmental Protection IA001 06/30/2011

SIA1X Iowa Department of Natural Resources 95 02/01/2012

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in 

its entirety.

Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989

Newton, IA 50208

Page 11 of 13
SmartER

301 12th Ave SW [none]

Becky Wehrman

Waste Sampling

Altoona IA, 50009

Project:

Project Number:

Project Manager:

Reported

01/10/11 14:50

Notes and Definitions 

Sample results reported on a dry weight basis

RPD Relative Percent Difference

dry

NR Not Reported

ND Analyte NOT DETECTED at or above the reporting limit

DET Analyte DETECTED

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in 

its entirety.

Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989

Newton, IA 50208

Page 12 of 13
SmartER

301 12th Ave SW [none]

Becky Wehrman

Waste Sampling

Altoona IA, 50009

Project:

Project Number:

Project Manager:

Reported

01/10/11 14:50

Christine Dawson For Sue Thompson

Project Manager I

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in 

its entirety.

Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989

Newton, IA 50208

Page 13 of 13