## Becky Wehrman

Enclosed are the results of analyses for samples received by the laboratory on08/31/10 09:30
.If you have any questions concerning this report, please feel free to contact me at 1-800-858-5227. RE: Waste Sampling Altoona, IA 50009 301 12th Ave SW SmartER 10 January 2011

ANALYTICAL REPORT FOR SAMPLES Client Sample ID Laboratory ID Matrix Date Sampled Date Received 

### N-Gum 01 10I0330-01 Solid 08/30/10 17:18 08/31/10 09:30 N-Gum (T) 02 10I0330-02 Solid 08/30/10 17:20 08/31/10 09:30 N-Patch 01 10I0330-03 Solid 08/30/10 17:22 08/31/10 09:30 N-Patch (T) 02 10I0330-04 Solid 08/30/10 17:24 08/31/10 09:30 War 01 10I0330-05 Solid 08/30/10 17:26 08/31/10 09:30 War 02 (T) 10I0330-06 Solid 08/30/10 17:28 08/31/10 09:30 Physo 01 10I0330-07 Solid 08/30/10 17:30 08/31/10 09:30 Physo 02 (T) 10I0330-08 Solid 08/30/10 17:32 08/31/10 09:30

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in its entirety. 

### Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 Page 1 of 13SmartER

301 12th Ave SW [none] Becky Wehrman Waste Sampling Altoona IA, 50009 Project: Project Number: Project Manager: Reported 01/10/11 14:50

Result Analyte Limit Batch Reporting Prepared AnalyzedMethod Notes Dilution Units 

### N-Gum 01 10I0330-01 (Solid) Date Sampled:8/30/2010 5:18:00PM
Keystone Laboratories, Inc. - Newton Determination of Base/Neutral Extractable Compounds ND EPA 8270B 09/15/1009/15/10 12:28 ug 1I02035

1 Nicotine 0.00005

" " " " 23-114 88.9 % Surrogate: 2-Fluorobiphenyl

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in its entirety. 

### Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 Page 2 of 13SmartER

301 12th Ave SW [none] Becky Wehrman Waste Sampling Altoona IA, 50009 Project: Project Number: Project Manager: Reported 01/10/11 14:50

Result Analyte Limit Batch Reporting Prepared AnalyzedMethod Notes Dilution Units 

### N-Gum (T) 02 10I0330-02 (Solid) Date Sampled:8/30/2010 5:20:00PM
Keystone Laboratories, Inc. - Newton Determination of Base/Neutral Extractable Compounds ND EPA 8270B 09/15/1009/15/10 13:04 ug 1I02035

1 Nicotine 0.00005

" " " " 23-114 99.2 % Surrogate: 2-Fluorobiphenyl

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in its entirety. 

### Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 Page 3 of 13SmartER

301 12th Ave SW [none] Becky Wehrman Waste Sampling Altoona IA, 50009 Project: Project Number: Project Manager: Reported 01/10/11 14:50

Result Analyte Limit Batch Reporting Prepared AnalyzedMethod Notes Dilution Units 

### N-Patch 01 10I0330-03 (Solid) Date Sampled:8/30/2010 5:22:00PM
Keystone Laboratories, Inc. - Newton Determination of Base/Neutral Extractable Compounds EPA 8270B 35.8 1I0203509/15/1009/15/10 13:39 ug 1 Nicotine 0.00005

" " " " 23-114 87.7 % Surrogate: 2-Fluorobiphenyl

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in its entirety. 

### Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 Page 4 of 13SmartER

301 12th Ave SW [none] Becky Wehrman Waste Sampling Altoona IA, 50009 Project: Project Number: Project Manager: Reported 01/10/11 14:50

Result Analyte Limit Batch Reporting Prepared AnalyzedMethod Notes Dilution Units 

### N-Patch (T) 02 10I0330-04 (Solid) Date Sampled:8/30/2010 5:24:00PM
Keystone Laboratories, Inc. - Newton Determination of Base/Neutral Extractable Compounds ND EPA 8270B 09/15/1009/15/10 14:15 ug 1I02035

1 Nicotine 0.00005

" " " " 23-114 91.8 % Surrogate: 2-Fluorobiphenyl

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in its entirety. 

### Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 Page 5 of 13SmartER

301 12th Ave SW [none] Becky Wehrman Waste Sampling Altoona IA, 50009 Project: Project Number: Project Manager: Reported 01/10/11 14:50

Result Analyte Limit Batch Reporting Prepared AnalyzedMethod Notes Dilution Units 

### War 01 10I0330-05 (Solid) Date Sampled:8/30/2010 5:26:00PM
Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids HPLC/UV 6.4 1L0164612/15/1012/15/10 18:05 ug 1 Warfarin Sodium 5.0

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in its entirety. 

### Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 Page 6 of 13SmartER

301 12th Ave SW [none] Becky Wehrman Waste Sampling Altoona IA, 50009 Project: Project Number: Project Manager: Reported 01/10/11 14:50

Result Analyte Limit Batch Reporting Prepared AnalyzedMethod Notes Dilution Units 

### War 02 (T) 10I0330-06 (Solid) Date Sampled:8/30/2010 5:28:00PM
Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids ND HPLC/UV 12/15/1012/15/10 18:22 ug 1L01646

1 Warfarin Sodium 5.0

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in its entirety. 

### Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 Page 7 of 13SmartER

301 12th Ave SW [none] Becky Wehrman Waste Sampling Altoona IA, 50009 Project: Project Number: Project Manager: Reported 01/10/11 14:50

Result Analyte Limit Batch Reporting Prepared AnalyzedMethod Notes Dilution Units 

### Physo 01 10I0330-07 (Solid) Date Sampled:8/30/2010 5:30:00PM
Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids ND HPLC/UV 12/10/1012/13/10 17:50 ug 1L01433

1 Physostigmine Salicylate 100

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in its entirety. 

### Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 Page 8 of 13SmartER

301 12th Ave SW [none] Becky Wehrman Waste Sampling Altoona IA, 50009 Project: Project Number: Project Manager: Reported 01/10/11 14:50

Result Analyte Limit Batch Reporting Prepared AnalyzedMethod Notes Dilution Units 

### Physo 02 (T) 10I0330-08 (Solid) Date Sampled:8/30/2010 5:32:00PM
Keystone Laboratories, Inc. - Newton Determination of Metabolic Acids ND HPLC/UV 12/10/1012/13/10 18:09 ug 1L01433

1 Physostigmine Salicylate 100

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in its entirety. 

### Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 Page 9 of 13SmartER

301 12th Ave SW [none] Becky Wehrman Waste Sampling Altoona IA, 50009 Project: Project Number: Project Manager: Reported 01/10/11 14:50

Result Limit

ReportingUnits Level Spike Result

Source%REC%REC Limits RPD RPD Limit Notes Analyte 

### Determination of Base/Neutral Extractable Compounds - Quality Control 

## Keystone Laboratories, Inc. - Newton

Batch 1I02035 - Solvent Extraction Blank (1I02035-BLK1) Prepared & Analyzed: 09/15/10 Nicotine ug ND 0.00005

" 2020.00 23-114 Surrogate: 2-Fluorobiphenyl 84.7 1710

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in its entirety. 

### Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 Page 10 of 13SmartER

301 12th Ave SW [none] Becky Wehrman Waste Sampling Altoona IA, 50009 Project: Project Number: Project Manager: Reported 01/10/11 14:50

Result Limit

ReportingUnits Level Spike Result

Source%REC%REC Limits RPD RPD Limit Notes Analyte 

### Determination of Metabolic Acids - Quality Control 

## Keystone Laboratories, Inc. - Newton

Batch 1L01433 - PCB Wipe Blank (1L01433-BLK1) Prepared: 12/10/10 Analyzed: 12/13/10 Physostigmine Salicylate ug ND 100 LCS (1L01433-BS1) Prepared: 12/10/10 Analyzed: 12/13/10 Physostigmine Salicylate ug 295.0 100 319.000 70-130 92.5 LCS Dup (1L01433-BSD1) Prepared: 12/10/10 Analyzed: 12/13/10 Physostigmine Salicylate ug 287.6 100 319.000 20 70-130 90.2 2.53 

### Batch 1L01646 - PCB Wipe Blank (1L01646-BLK1) Prepared & Analyzed: 12/15/10 Warfarin Sodium ug ND 5.0 LCS (1L01646-BS1) Prepared & Analyzed: 12/15/10 Warfarin Sodium ug 647.9 5.0 626.000 70-130 104 LCS Dup (1L01646-BSD1) Prepared & Analyzed: 12/15/10 Warfarin Sodium ug 647.2 5.0 626.000 20 70-130 103 0.114 

### Certified Analyses Included in This Report Certifications Analyte Method/Matrix

Certifying Authority Certificate Number Expires Code E-10110

Kansas Department of Health and Environment-KC 04/30/2011 KS-KC E-10287

Kansas Department of Health and Environment 10/30/2011 KS-NT IA001

New Jersey Department of Environmental Protection 06/30/2011 NELAC 95

Iowa Department of Natural Resources 02/01/2012 SIA1X

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in its entirety. 

### Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 Page 11 of 13SmartER

301 12th Ave SW [none] Becky Wehrman Waste Sampling Altoona IA, 50009 Project: Project Number: Project Manager: Reported 01/10/11 14:50 

### Notes and Definitions

Sample results reported on a dry weight basis Relative Percent Difference RPD dry Not Reported NR Analyte NOT DETECTED at or above the reporting limit ND Analyte DETECTED DET

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in its entirety. 

### Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 Page 12 of 13SmartER

301 12th Ave SW [none] Becky Wehrman Waste Sampling Altoona IA, 50009 Project: Project Number: Project Manager: Reported 01/10/11 14:50



### Christine Dawson For Sue Thompson Project Manager I

The results in this report apply to the samples analyzed in accordance with the Chain-of-Custody record. This analytical report must be reproduced in its entirety. 

### Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989 Newton, IA 50208 Page 13 of 13