**Instructions for using the Emission Test Reporting Template for the Primary Aluminum Test Program**

This Information Collection Request (ICR) spreadsheet is intended to be used to report emissions data from primary aluminum reduction facilities as an alternative to the Electronic Reporting Tool (ERT), as well as in cases where the test methods arenot currently supported by the ERT.**Data for multiple process units should be reported by using separate copies of the appropriate tabs of this spreadsheet.** **Please Do Not delete rows or columns , addition of rows and columns is appropriate**  **as necessary.**
**Emission Data Worksheets** The emission data worksheets are provided for each test required for this testing program, although all facilities are not required to conduct all of the tests. On each worksheet,please enter process unit operating informationduring sampling and emission test results. The emission test results to be entered depends on the constituent. **Source Operating Information** 1. Please provide the Exhaust Flow Rate (acfm and dscfm) and the Exhaust Temperature (deg F). 2. Please provide the values of all requested parametersfor each of the sample testing periods in the appropriate cells. 3. Please provide any other supporting informationor commentsin the Other Supporting Informationfield.

# Primary Aluminum Testing: Filterable Particulate Matter

**Parent company**

**name:** Noranda Aluminum, Inc. **Facility address:** 391 St. Jude Industrial Park

New Madrid, MO 63869 **Description of source tested:**161 Duct

**Test Method Used (e.g. Method 5)**  **Data Flag**

**(A DL, BDL, DLL)**  **Test Method Comments**

1 4/24/2013 11:08 4/24/2013 15:32 Method 5 ADL 2 4/24/2013 16:48 4/24/2013 20:30 Method 5 ADL 3 4/25/2013 8:48 4/25/2013 12:28 Method 5 ADL

**Moisture (%) CO2 (%)**  **O2 (%) Flow (acfm)**  **Temperature (°F)**
1 0.8 0.9 20.6 315,821 174 2 0.7 0.9 20.6 324,914 183 3 0.6 0.8 20.5 316,789 183

**lb/hr lb/ton of** 

**throughput Ma** **terial Rate (ton/hr)** 

1 0.664 0.105 Aluminum 6.30 2 0.930 0.148 Aluminum 6.30 3 0.552 0.088 Aluminum 6.30 **Run Number**  **Run Number** **Test Start**

**Date Test Start** 

**Time Test End** 

**Date Test End** 

**Time**

**Flow (dscfm)**

261,410 **Filterable Particulate Emission Test Results**
**Concentration (ug/dscm)** 
0.678 0.934 0.572

**Exhaust Gas Other Supporting Information** 

**Run Number** **Calculated Emission Rate Production or Throughput**  257,678 265,504

## Primary Aluminum Testing: HAP Metals

**Parent company name:** Noranda Aluminum, Inc. **Facility address:**391 St. Jude Industrial Park New Madrid, MO 63869 

### Description of source:

**Pollutant Concentration**  **(ug/dscm) Test Method Used** 

**(e.g. Method 29) Data Flag** 

**(A DL, BDL, DLL)**  **Test Method Comments**
1 Antimony 2 Antimony 3 Antimony 1 Arsenic 2 Arsenic 3 Arsenic 1 Beryllium 2 Beryllium 3 Beryllium 1 Cadmium 2 Cadmium 3 Cadmium 1 Chromium 2 Chromium 3 Chromium 1 Cobalt 2 Cobalt 3 Cobalt 1 Lead 2 Lead 3 Lead 1 Manganese 2 Manganese 3 Manganese 1 Nickel 2 Nickel 3 Nickel 1 Selenium 2 Selenium 3 Selenium 1 Mercury 2 Mercury 3 Mercury **Run Number** **Test Start**

**Date Test Start** 

**Time Test End** 

**Date Test End** 

**Time Filterable Particulate Emission Test Results** 

## Primary Aluminum Testing: HAP Metals

**Parent company name:** Noranda Aluminum, Inc. **Facility address:**391 St. Jude Industrial Park New Madrid, MO 63869 

### Description of source:

**lb/hr lb/ton of** 

**throughput Material**  **Rate (tons/hour)** **Moisture**

**(%) CO** **2**

**(%) O** **2**

**(%) Flow** 

**(acfm) Flow** 

**(dscfm) Temp** 

**( °F)**  1 2 3 1 2 3 1 2 3 1 2 3 1 2 3 1 2 3 1 2 3 1 2 3 1 2 3 1 2 3 1 2 3 **Run Number**  **Other Supporting Information**

**Calculated Emission Rate Production or Throughput**  **Exhaust Gas**

# Primary Aluminum Testing: Hexavalent Chromium

**Parent company**

**name:** Noranda Aluminum, Inc. **Facility address:** 391 St. Jude Industrial Park

New Madrid, MO 63869 

### Description of source tested:

**Test Method Used (SW-846 M0061)**  **Data Flag**

**(A DL, BDL, DLL)**  **Test Method Comments**

1 2 3

**Moisture (%) CO2 (%)**  **O2 (%) Flow (acfm)**  **Temperature (°F)**
1 2 3

**lb/hr lb/ton of**  **throughput Ma** **terial Rate**  **(tons/hour)**
1 2 3 **Run Number** **Test Start**

**Date Test Start** 

**Time Test End** 

**Date Test End** 

**Time Hexavalent Chromium Emission Test Results** 

**Concentration (ug/dscm)** 

**Run Number**  **Exhaust Gas Other Supporting Information**  **Flow (dscfm)**

**Run Number** **Calculated Emission Rate Production or Throughput** 

# Primary Aluminum Testing: PM and POM as MCEM
**Parent company**

**name:** Noranda Aluminum, Inc. **Facility address:** 391 St. Jude Industrial Park

New Madrid, MO 63869 

### Description of source tested:

**Rate (tons/hour)** 1 2 3

**Moisture (%) CO2 (%)**  **O2 (%) Flow (acfm)**  **Temperature (°F)** 1 2 3

**lb/hr lb/ton of**  **throughput Pollutant**  **Conc (ug/dscm)**  **Test Method Used (e.g. Method 315)** 
PM POM as MCEM PM POM as MCEM PM POM as MCEM **Run Number** **Test Start**

**Date Test Start** 

**Time Test End** 

**Date Test End** 

**Time Ma** **terial**

**Run Number**  **Exhaust Gas**

**Calculated Emission Rate Other Supporting Information**  **Flow (dscfm)**

**Run Number** 

1

2

3 **Production or Throughput**

**Data Flag (A** **DL, BDL, DLL) Particulate Matter and POM as MCEM Emission Test Results** 
**Test Method Comments**

### Page 1 of 8 

# Primary Aluminum Testing: Polycyclic Aromatic Hydrocarbons

**Parent company**

**name:** Noranda Aluminum, Inc. **Facility address:**  391 St. Jude Industrial Park

New Madrid, MO 63869 **Description of source tested:** 161 Duct

**lb/hr lb/ton**  **Throughput** 1 4/24/2013 11:08 4/24/2013 15:32 5.06E-05 8.04E-06 6.30 2 4/24/2013 16:48 4/24/2013 20:30 2.10E-05 3.33E-06 6.30 3 4/25/2013 8:48 4/25/2013 12:28 4.77E-06 7.57E-07 6.30 1 4/24/2013 11:08 4/24/2013 15:32 7.00E-06 1.11E-06 6.30 2 4/24/2013 16:48 4/24/2013 20:30 7.36E-06 1.17E-06 6.30 3 4/25/2013 8:48 4/25/2013 12:28 4.77E-06 7.57E-07 6.30 1 4/24/2013 11:08 4/24/2013 15:32 1.14E-05 1.82E-06 6.30 2 4/24/2013 16:48 4/24/2013 20:30 5.95E-06 9.44E-07 6.30 3 4/25/2013 8:48 4/25/2013 12:28 2.86E-05 4.54E-06 6.30 1 4/24/2013 11:08 4/24/2013 15:32 1.49E-06 2.36E-07 6.30 2 4/24/2013 16:48 4/24/2013 20:30 9.91E-07 1.57E-07 6.30 3 4/25/2013 8:48 4/25/2013 12:28 1.99E-06 3.16E-07 6.30 1 4/24/2013 11:08 4/24/2013 15:32 1.93E-06 3.06E-07 6.30 2 4/24/2013 16:48 4/24/2013 20:30 1.93E-06 3.06E-07 6.30 3 4/25/2013 8:48 4/25/2013 12:28 1.63E-06 2.58E-07 6.30 1 4/24/2013 11:08 4/24/2013 15:32 2.29E-06 3.64E-07 6.30 2 4/24/2013 16:48 4/24/2013 20:30 2.29E-06 3.64E-07 6.30 3 4/25/2013 8:48 4/25/2013 12:28 3.26E-06 5.17E-07 6.30 1 4/24/2013 11:08 4/24/2013 15:32 1.80E-06 2.86E-07 6.30 2 4/24/2013 16:48 4/24/2013 20:30 1.40E-06 2.22E-07 6.30 3 4/25/2013 8:48 4/25/2013 12:28 5.05E-06 8.02E-07 6.30 1 4/24/2013 11:08 4/24/2013 15:32 1.99E-06 3.15E-07 6.30 2 4/24/2013 16:48 4/24/2013 20:30 1.64E-06 2.61E-07 6.30 3 4/25/2013 8:48 4/25/2013 12:28 2.83E-06 4.50E-07 6.30 Benzo[b]fluoranthene (205-99-2)

Benzo[g,h,i]perylene (191-24-2) Acenaphthylene (208-96-8)

**Compound Run**  **Number Test Start** 

**Date**

Anthracene (120-12-7)

Benz[a]anthracene (56-55-3)

Benzo[a]pyrene (50-32-8)

Benzo(e)pyrene (192-97-2) Acenaphthene (83-32-9) **Test Start Time**  **Test End**

**Date Test End** 

**Time Calculated Emission Rate** **Throughput (ton/hr)** 

### Page 2 of 8

**lb/hr lb/ton** 

**Throughput Compound**  **Run Number** **Test Start**

**Date Test Start** 

**Time Test End** 

**Date Test End** 

**Time Calculated Emission Rate** **Throughput (ton/hr)** 

1 4/24/2013 11:08 4/24/2013 15:32 1.18E-06 1.87E-07 6.30 2 4/24/2013 16:48 4/24/2013 20:30 1.39E-06 2.20E-07 6.30 3 4/25/2013 8:48 4/25/2013 12:28 1.61E-06 2.56E-07 6.30 1 4/24/2013 11:08 4/24/2013 15:32 2.54E-06 4.03E-07 6.30 2 4/24/2013 16:48 4/24/2013 20:30 1.98E-06 3.14E-07 6.30 3 4/25/2013 8:48 4/25/2013 12:28 4.46E-06 7.08E-07 6.30 1 4/24/2013 11:08 4/24/2013 15:32 2.18E-06 3.46E-07 6.30 2 4/24/2013 16:48 4/24/2013 20:30 1.93E-06 3.06E-07 6.30 3 4/25/2013 8:48 4/25/2013 12:28 1.91E-06 3.03E-07 6.30 1 4/24/2013 11:08 4/24/2013 15:32 1.59E-05 2.53E-06 6.30 2 4/24/2013 16:48 4/24/2013 20:30 1.18E-05 1.87E-06 6.30 3 4/25/2013 8:48 4/25/2013 12:28 3.03E-05 4.81E-06 6.30 1 4/24/2013 11:08 4/24/2013 15:32 4.76E-06 7.55E-07 6.30 2 4/24/2013 16:48 4/24/2013 20:30 4.81E-06 7.64E-07 6.30 3 4/25/2013 8:48 4/25/2013 12:28 4.94E-05 7.84E-06 6.30 1 4/24/2013 11:08 4/24/2013 15:32 2.13E-06 3.38E-07 6.30 2 4/24/2013 16:48 4/24/2013 20:30 1.84E-06 2.92E-07 6.30 3 4/25/2013 8:48 4/25/2013 12:28 1.66E-06 2.63E-07 6.30 1 4/24/2013 11:08 4/24/2013 15:32 2.06E-03 3.27E-04 6.30 2 4/24/2013 16:48 4/24/2013 20:30 1.81E-03 2.87E-04 6.30 3 4/25/2013 8:48 4/25/2013 12:28 9.82E-04 1.56E-04 6.30 1 4/24/2013 11:08 4/24/2013 15:32 2.96E-05 4.70E-06 6.30 2 4/24/2013 16:48 4/24/2013 20:30 1.10E-05 1.74E-06 6.30 3 4/25/2013 8:48 4/25/2013 12:28 7.02E-06 1.11E-06 6.30 1 4/24/2013 11:08 4/24/2013 15:32 4.25E-05 6.74E-06 6.30 2 4/24/2013 16:48 4/24/2013 20:30 3.79E-05 6.01E-06 6.30 3 4/25/2013 8:48 4/25/2013 12:28 2.06E-04 3.28E-05 6.30 1 4/24/2013 11:08 4/24/2013 15:32 1.62E-06 2.58E-07 6.30 2 4/24/2013 16:48 4/24/2013 20:30 1.76E-06 2.79E-07 6.30 3 4/25/2013 8:48 4/25/2013 12:28 1.43E-06 2.27E-07 6.30 1 4/24/2013 11:08 4/24/2013 15:32 6.10E-06 9.68E-07 6.30 2 4/24/2013 16:48 4/24/2013 20:30 5.58E-06 8.85E-07 6.30 3 4/25/2013 8:48 4/25/2013 12:28 1.63E-05 2.59E-06 6.30 Pyrene (129-00-0) Fluorene (86-73-7)

Indeno (1,2,3-cd) pyrene (193-39-5)

Naphthalene (91-20-3)

2-Methylnaphthalene (91-57-6)

Phenanthrene (85-01-8)

Perylene (198-55-0) Benzo[k]fluoranthene (207-08-9)

Chrysene (218-01-9)

Dibenz[a,h]anthracene (53-70-3)

Fluoranthene (206-44-0)

### Page 3 of 8



# Primary Aluminum Testing: Polycyclic Aromatic Hydrocarbons

391 St. Jude Industrial Park**Parent company name:**  Noranda Aluminum, Inc. **Facility address:**  New Madrid, MO 63869 **Description of source tested:** 161 Duct

**Me asured**  **Value (n g)** **Wet or Dry**

**Basis Test Method** 

**(e.g.,CA RB 429)**  **Data Flag**

**(A DL, BDL, DLL)** **Front Half**

**Ma****ss* (ng)****Back Half**

**Ma ss**  (ng)****Condensate**

**Ma ss** * (ng)** Aluminum 1 1.81E+02 Dry CARB 429 ADL Aluminum 2 7.40E+01 Dry CARB 429 ADL Aluminum 3 1.70E+01 Dry CARB 429 ADL Aluminum 1 2.50E+01 Dry CARB 429 BDL Aluminum 2 2.60E+01 Dry CARB 429 ADL Aluminum 3 1.70E+01 Dry CARB 429 BDL Aluminum 1 4.09E+01 Dry CARB 429 ADL Aluminum 2 2.10E+01 Dry CARB 429 ADL Aluminum 3 1.02E+02 Dry CARB 429 ADL Aluminum 1 5.32E+00 Dry CARB 429 ADL Aluminum 2 3.50E+00 Dry CARB 429 ADL Aluminum 3 7.09E+00 Dry CARB 429 ADL Aluminum 1 6.90E+00 Dry CARB 429 BDL Aluminum 2 6.80E+00 Dry CARB 429 BDL Aluminum 3 5.80E+00 Dry CARB 429 BDL Aluminum 1 8.20E+00 Dry CARB 429 ADL Aluminum 2 8.10E+00 Dry CARB 429 ADL Aluminum 3 1.16E+01 Dry CARB 429 ADL Aluminum 1 6.43E+00 Dry CARB 429 ADL Aluminum 2 4.95E+00 Dry CARB 429 ADL Aluminum 3 1.80E+01 Dry CARB 429 ADL Aluminum 1 7.10E+00 Dry CARB 429 ADL Aluminum 2 5.80E+00 Dry CARB 429 BDL Aluminum 3 1.01E+01 Dry CARB 429 ADL **Polycyclic A romatic Hydrocarbons Emission Test Results** 

Acenaphthene

Acenaphthylene

Anthracene

Benz[a] anthracene

Benzo[a] pyrene

Benzo[b] fluoranthene
Benzo[g,h,i]peryle ne Benzo(e) pyrene **Compound Run** 

**Number Throughput**  **Ma terial** 

### Page 4 of 8

**Me asured**  **Value (n g)** **Wet or Dry**

**Basis Test Method** 

**(e.g.,CA RB 429)**  **Data Flag**

**(A DL, BDL, DLL)** **Front Half**

**Ma****ss* (ng)****Back Half**

**Ma ss**  (ng)****Condensate**

**Ma ss** * (ng)** **Polycyclic A romatic Hydrocarbons Emission Test Results**  **Compound Run** 

**Number Throughput**  **Ma terial** 

Aluminum 1 4.20E+00 Dry CARB 429 ADL Aluminum 2 4.90E+00 Dry CARB 429 ADL Aluminum 3 5.75E+00 Dry CARB 429 ADL Aluminum 1 9.08E+00 Dry CARB 429 ADL Aluminum 2 6.98E+00 Dry CARB 429 ADL Aluminum 3 1.59E+01 Dry CARB 429 ADL Aluminum 1 7.80E+00 Dry CARB 429 ADL Aluminum 2 6.80E+00 Dry CARB 429 ADL Aluminum 3 6.80E+00 Dry CARB 429 ADL Aluminum 1 5.69E+01 Dry CARB 429 ADL Aluminum 2 4.15E+01 Dry CARB 429 ADL Aluminum 3 1.08E+02 Dry CARB 429 ADL Aluminum 1 1.70E+01 Dry CARB 429 ADL Aluminum 2 1.70E+01 Dry CARB 429 BDL Aluminum 3 1.76E+02 Dry CARB 429 ADL Aluminum 1 7.60E+00 Dry CARB 429 ADL Aluminum 2 6.50E+00 Dry CARB 429 ADL Aluminum 3 5.90E+00 Dry CARB 429 ADL Aluminum 1 7.36E+03 Dry CARB 429 ADL Aluminum 2 6.38E+03 Dry CARB 429 ADL Aluminum 3 3.50E+03 Dry CARB 429 ADL Aluminum 1 1.06E+02 Dry CARB 429 ADL Aluminum 2 3.88E+01 Dry CARB 429 ADL Aluminum 3 2.50E+01 Dry CARB 429 ADL Aluminum 1 1.52E+02 Dry CARB 429 ADL Aluminum 2 1.34E+02 Dry CARB 429 ADL Aluminum 3 7.36E+02 Dry CARB 429 ADL Aluminum 1 5.80E+00 Dry CARB 429 BDL Aluminum 2 6.20E+00 Dry CARB 429 BDL Aluminum 3 5.10E+00 Dry CARB 429 BDL Aluminum 1 2.18E+01 Dry CARB 429 ADL Aluminum 2 1.97E+01 Dry CARB 429 ADL Aluminum 3 5.81E+01 Dry CARB 429 ADL

* Contains particulate filter, front half of filter holder and probe solvent rinses *** Contains condensate, impinger contents and glassware solvent rinses ** Contains XAD-2 resin tube, back half of filter holder and coil condenser solvent rinses Phenan threne

Perylene

Pyrene Dibenz[a,h] anthracene

Fluoranthene

Fluorene

Indeno (1,2,3-cd) pyrene

Naphthalene

2-Methyl naphthalene Benzo[k] fluoranthene

Chrysene

### Page 5 of 8 

# Primary Aluminum Testing: Polycyclic Aromatic Hydrocarbons

391 St. Jude Industrial Park **Parent company name:**  Noranda Aluminum, Inc. **Facility address:**  New Madrid, MO 63869 **Description of source tested:** 161 Duct

**Total (ng) Test Method** 

**Comments Moisture**  **(%) CO** **2 (%)**  **O 2** **(%) Flow**  **(acfm) Flow** 

**(dscfm) Temperature** 

**( °F)**  1.81E+02 1 0.8 0.8 20.6 326,262 268,234 178 7.40E+01 2 0.5 0.9 20.6 328,471 269,883 181 1.70E+01 3 0.5 0.8 20.5 327,274 267,423 181 2.50E+01 1 0.8 0.8 20.6 326,262 268,234 178 2.60E+01 2 0.5 0.9 20.6 328,471 269,883 181 1.70E+01 3 0.5 0.8 20.5 327,274 267,423 181 4.09E+01 1 0.8 0.8 20.6 326,262 268,234 178 2.10E+01 2 0.5 0.9 20.6 328,471 269,883 181 1.02E+02 3 0.5 0.8 20.5 327,274 267,423 181 5.32E+00 1 0.8 0.8 20.6 326,262 268,234 178 3.50E+00 2 0.5 0.9 20.6 328,471 269,883 181 7.09E+00 3 0.5 0.8 20.5 327,274 267,423 181 6.90E+00 1 0.8 0.8 20.6 326,262 268,234 178 6.80E+00 2 0.5 0.9 20.6 328,471 269,883 181 5.80E+00 3 0.5 0.8 20.5 327,274 267,423 181 8.20E+00 1 0.8 0.8 20.6 326,262 268,234 178 8.10E+00 2 0.5 0.9 20.6 328,471 269,883 181 1.16E+01 3 0.5 0.8 20.5 327,274 267,423 181 6.43E+00 1 0.8 0.8 20.6 326,262 268,234 178 4.95E+00 2 0.5 0.9 20.6 328,471 269,883 181 1.80E+01 3 0.5 0.8 20.5 327,274 267,423 181 7.10E+00 1 0.8 0.8 20.6 326,262 268,234 178 5.80E+00 2 0.5 0.9 20.6 328,471 269,883 181 1.01E+01 3 0.5 0.8 20.5 327,274 267,423 181 Benz[a] anthracene

Benzo[a]pyrene

Benzo[b] fluoranthene
Benzo[g,h,i] perylene **Exhaust Gas Compound**  **Run**

**Number**

Acenaphthene

Acenaphthylene

Anthracene

Benzo(e)pyrene

### Page 6 of 8

**Total (ng) Test Method** 

**Comments Moisture**  **(%) CO** **2 (%)**  **O 2** **(%) Flow**  **(acfm) Flow** 

**(dscfm) Temperature** 

**( °F)**  **Exhaust Gas Compound**  **Run**

**Number**

4.20E+00 1 0.8 0.8 20.6 326,262 268,234 178 4.90E+00 2 0.5 0.9 20.6 328,471 269,883 181 5.75E+00 3 0.5 0.8 20.5 327,274 267,423 181 9.08E+00 1 0.8 0.8 20.6 326,262 268,234 178 6.98E+00 2 0.5 0.9 20.6 328,471 269,883 181 1.59E+01 3 0.5 0.8 20.5 327,274 267,423 181 7.80E+00 1 0.8 0.8 20.6 326,262 268,234 178 6.80E+00 2 0.5 0.9 20.6 328,471 269,883 181 6.80E+00 3 0.5 0.8 20.5 327,274 267,423 181 5.69E+01 1 0.8 0.8 20.6 326,262 268,234 178 4.15E+01 2 0.5 0.9 20.6 328,471 269,883 181 1.08E+02 3 0.5 0.8 20.5 327,274 267,423 181 1.70E+01 1 0.8 0.8 20.6 326,262 268,234 178 1.70E+01 2 0.5 0.9 20.6 328,471 269,883 181 1.76E+02 3 0.5 0.8 20.5 327,274 267,423 181 7.60E+00 1 0.8 0.8 20.6 326,262 268,234 178 6.50E+00 2 0.5 0.9 20.6 328,471 269,883 181 5.90E+00 3 0.5 0.8 20.5 327,274 267,423 181 7.36E+03 1 0.8 0.8 20.6 326,262 268,234 178 6.38E+03 2 0.5 0.9 20.6 328,471 269,883 181 3.50E+03 3 0.5 0.8 20.5 327,274 267,423 181 1.06E+02 1 0.8 0.8 20.6 326,262 268,234 178 3.88E+01 2 0.5 0.9 20.6 328,471 269,883 181 2.50E+01 3 0.5 0.8 20.5 327,274 267,423 181 1.52E+02 1 0.8 0.8 20.6 326,262 268,234 178 1.34E+02 2 0.5 0.9 20.6 328,471 269,883 181 7.36E+02 3 0.5 0.8 20.5 327,274 267,423 181 5.80E+00 1 0.8 0.8 20.6 326,262 268,234 178 6.20E+00 2 0.5 0.9 20.6 328,471 269,883 181 5.10E+00 3 0.5 0.8 20.5 327,274 267,423 181 2.18E+01 1 0.8 0.8 20.6 326,262 268,234 178 1.97E+01 2 0.5 0.9 20.6 328,471 269,883 181 5.81E+01 3 0.5 0.8 20.5 327,274 267,423 181 *** Contains condensate, impinger contents and glassware solvent rinses Dibenz[a,h] anthracene

Fluoranthene

Pyrene Fluorene

Indeno (1,2,3-cd) pyrene

Naphthalene

2-Methyl naphthalene

Phenanthrene

Perylene Benzo[k] fluoranthene

Chrysene

### Page 7 of 8



### 391 St. Jude Industrial Park New Madrid, MO 63869

**Other Supporting Information**

### Page 8 of 8

**Other Supporting Information**

### Page 1 of 8 

# Primary Aluminum Testing: Dioxins and Furans

**Parent company**

**name:** Noranda Aluminum, Inc. **Facility address:** 391 St. Jude Industrial Park

New Madrid, MO 63869 **Description of source tested:**161 Duct

**lb/hr lb/ton**  **Throughput** 1 4/24/2013 11:08 4/24/2013 15:32 1.57E-11 2.49E-12 6.30 Aluminum 2 4/24/2013 16:48 4/24/2013 20:30 1.56E-11 2.47E-12 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 1.15E-11 1.83E-12 6.30 Aluminum 1 4/24/2013 11:08 4/24/2013 15:32 1.45E-11 2.31E-12 6.30 Aluminum 2 4/24/2013 16:48 4/24/2013 20:30 7.65E-12 1.21E-12 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 8.78E-12 1.39E-12 6.30 Aluminum 1 4/24/2013 11:08 4/24/2013 15:32 6.16E-12 9.77E-13 6.30 Aluminum 2 4/24/2013 16:48 4/24/2013 20:30 9.34E-12 1.48E-12 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 5.89E-12 9.35E-13 6.30 Aluminum 1 4/24/2013 11:08 4/24/2013 15:32 4.20E-11 6.66E-12 6.30 Aluminum 2 4/24/2013 16:48 4/24/2013 20:30 6.06E-11 9.62E-12 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 3.93E-11 6.24E-12 6.30 Aluminum 1 4/24/2013 11:08 4/24/2013 15:32 7.00E-11 1.11E-11 6.30 Aluminum 2 4/24/2013 16:48 4/24/2013 20:30 4.25E-11 6.74E-12 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 7.32E-11 1.16E-11 6.30 Aluminum 1 4/24/2013 11:08 4/24/2013 15:32 5.04E-11 7.99E-12 6.30 Aluminum 2 4/24/2013 16:48 4/24/2013 20:30 5.38E-11 8.54E-12 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 3.93E-11 6.24E-12 6.30 Aluminum 1 4/24/2013 11:08 4/24/2013 15:32 4.20E-11 6.66E-12 6.30 Aluminum 2 4/24/2013 16:48 4/24/2013 20:30 5.10E-11 8.09E-12 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 4.21E-11 6.68E-12 6.30 Aluminum 1 4/24/2013 11:08 4/24/2013 15:32 8.11E-11 1.29E-11 6.30 Aluminum 2 4/24/2013 16:48 4/24/2013 20:30 1.18E-10 1.87E-11 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 4.77E-11 7.57E-12 6.30 Aluminum **Calculated Emission Rate Throughput**  **Ma terial** 

1,2,3,7,8,9- HxCDD 1,2,3,6,7,8- HxCDD
1,2,3,6,7,8- HxCDF 1,2,3,4,7,8- HxCDD
1,2,3,4,7,8- HxCDF 1,2,3,4,6,7,8- HpCDF
1,2,3,4,7,8,9- HpCDF 1,2,3,4,6,7,8- HpCDD **Throughput (ton/hr)**  **Compound Run** 

**Number Test Start** 

**Date Test Start** 

**Time Test End** 

**Date Test End** 

**Time**

### Page 2 of 8

**lb/hr lb/ton** 

**Throughput Calculated Emission Rate**  **Throughput Ma** **terial Throughput**  **(ton/hr) Compound**  **Run**

**Number Test Start** 

**Date Test Start** 

**Time Test End** 

**Date Test End** 

**Time**

1 4/24/2013 11:08 4/24/2013 15:32 4.76E-11 7.55E-12 6.30 Aluminum 2 4/24/2013 16:48 4/24/2013 20:30 5.66E-11 8.99E-12 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 5.14E-11 8.15E-12 6.30 Aluminum 1 4/24/2013 11:08 4/24/2013 15:32 7.93E-10 1.26E-10 6.30 Aluminum 2 4/24/2013 16:48 4/24/2013 20:30 6.17E-10 9.80E-11 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 6.75E-10 1.07E-10 6.30 Aluminum 1 4/24/2013 11:08 4/24/2013 15:32 4.11E-11 6.53E-12 6.30 Aluminum 2 4/24/2013 16:48 4/24/2013 20:30 2.04E-11 3.24E-12 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 3.68E-11 5.84E-12 6.30 Aluminum 1 4/24/2013 11:08 4/24/2013 15:32 9.23E-11 1.47E-11 6.30 Aluminum 2 4/24/2013 16:48 4/24/2013 20:30 4.53E-11 7.19E-12 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 3.93E-11 6.24E-12 6.30 Aluminum 1 4/24/2013 11:08 4/24/2013 15:32 1.59E-10 2.53E-11 6.30 Aluminum 2 4/24/2013 16:48 4/24/2013 20:30 1.36E-10 2.16E-11 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 1.43E-10 2.27E-11 6.30 Aluminum 1 4/24/2013 11:08 4/24/2013 15:32 4.76E-10 7.55E-11 6.30 Aluminum 2 4/24/2013 16:48 4/24/2013 20:30 8.78E-10 1.39E-10 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 7.02E-10 1.11E-10 6.30 Aluminum 1 4/24/2013 11:08 4/24/2013 15:32 2.74E-10 4.35E-11 6.30 Aluminum 2 4/24/2013 16:48 4/24/2013 20:30 1.28E-10 2.03E-11 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 4.49E-11 7.13E-12 6.30 Aluminum 1 4/24/2013 11:08 4/24/2013 15:32 5.62E-13 8.93E-14 6.30 Aluminum 2 4/24/2013 16:48 4/24/2013 20:30 1.02E-12 1.62E-13 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 4.92E-13 7.80E-14 6.30 Aluminum 1 4/24/2013 11:08 4/24/2013 15:32 1.76E-13 2.80E-14 6.30 Aluminum 2 4/24/2013 16:48 4/24/2013 20:30 2.97E-13 4.72E-14 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 2.36E-13 3.74E-14 6.30 Aluminum OCDF OCDD 2,3,7,8- TCDD

2,3,7,8-TCDF 1,2,3,7,8- PeCDF

2,3,4,7,8- PeCDF 2,3,4,6,7,8- HxCDF 1,2,3,7,8,9- HxCDF
1,2,3,7,8- PeCDD

### Page 3 of 8 

# Primary Aluminum Testing: Dioxins and Furans

391 St. Jude Industrial Park **Parent company name:**  Noranda Aluminum, Inc. **Facility address:** 391 St. Jude Industrial Park New Madrid, MO 63869 New Madrid, MO 63869 **Description of source tested:**161 Duct

**Me asured**  **Value (n g)** **Wet or Dry**

**Basis Test Method** 

**(e.g.,CA RB 429)**  **Data Flag**

**(A DL, BDL, DLL)** **Front Half**

**Ma****ss* (ng)****Back Half**

**Ma ss**  (ng)****Impinger Soln**

**Ma ss** * (ng)** 1 5.60E-03 Dry CARB 428 BDL 2 5.50E-03 Dry CARB 428 BDL 3 4.10E-03 Dry CARB 428 BDL 1 5.19E-03 Dry CARB 428 ADL 2 2.70E-03 Dry CARB 428 BDL 3 3.13E-03 Dry CARB 428 ADL 1 2.20E-03 Dry CARB 428 BDL 2 3.30E-03 Dry CARB 428 BDL 3 2.10E-03 Dry CARB 428 BDL 1 1.50E-03 Dry CARB 428 BDL 2 2.14E-03 Dry CARB 428 ADL 3 1.40E-03 Dry CARB 428 BDL 1 2.50E-03 Dry CARB 428 BDL 2 1.50E-03 Dry CARB 428 BDL 3 2.61E-03 Dry CARB 428 ADL 1 1.80E-03 Dry CARB 428 BDL 2 1.90E-03 Dry CARB 428 BDL 3 1.40E-03 Dry CARB 428 BDL 1 1.50E-03 Dry CARB 428 BDL 2 1.80E-03 Dry CARB 428 BDL 3 1.50E-03 Dry CARB 428 BDL 1 2.90E-03 Dry CARB 428 BDL 2 4.17E-03 Dry CARB 428 ADL 3 1.70E-03 Dry CARB 428 BDL **Separate A nalysis** 

1,2,3,7,8,9- HxCDD 1,2,3,6,7,8- HxCDD
1,2,3,6,7,8- HxCDF 1,2,3,4,7,8- HxCDD
1,2,3,4,7,8- HxCDF 1,2,3,4,6,7,8- HpCDF
1,2,3,4,7,8,9- HpCDF 1,2,3,4,6,7,8- HpCDD **Test Method Comments Compound**  **Run Number**  **Dioxins and Furans Emission Test Results**

### Page 4 of 8

**Me asured**  **Value (n g)** **Wet or Dry**

**Basis Test Method** 

**(e.g.,CA RB 429)**  **Data Flag**

**(A DL, BDL, DLL)** **Front Half**

**Ma****ss* (ng)****Back Half**

**Ma ss**  (ng)****Impinger Soln**

**Ma ss** * (ng)** **Separate A nalysis**  **Test Method Comments Compound**  **Run Number**  **Dioxins and Furans Emission Test Results**

1 1.70E-03 Dry CARB 428 BDL 2 2.00E-03 Dry CARB 428 BDL 3 1.83E-03 Dry CARB 428 ADL 1 2.80E-03 Dry CARB 428 BDL 2 2.20E-03 Dry CARB 428 BDL 3 2.40E-03 Dry CARB 428 BDL 1 4.90E-03 Dry CARB 428 BDL 2 2.40E-03 Dry CARB 428 BDL 3 4.37E-03 Dry CARB 428 ADL 1 3.30E-03 Dry CARB 428 BDL 2 1.60E-03 Dry CARB 428 BDL 3 1.40E-03 Dry CARB 428 BDL 1 1.90E-03 Dry CARB 428 BDL 2 1.60E-03 Dry CARB 428 BDL 3 1.70E-03 Dry CARB 428 BDL 1 1.70E-03 Dry CARB 428 BDL 2 3.10E-03 Dry CARB 428 BDL 3 2.50E-03 Dry CARB 428 BDL 1 9.80E-03 Dry CARB 428 BDL 2 4.51E-03 Dry CARB 428 ADL 3 1.60E-03 Dry CARB 428 BDL 1 6.70E-03 Dry CARB 428 BDL 2 1.20E-02 Dry CARB 428 BDL 3 5.84E-03 Dry CARB 428 ADL 1 2.10E-03 Dry CARB 428 BDL 2 3.50E-03 Dry CARB 428 BDL 3 2.80E-03 Dry CARB 428 BDL * Front Half Composite contains particulate filter, front half of the filter holder, and probe solvent rinses ** Back Half Composite contains XAD-2 resin tube, back half of the filter holder, and coil condenser solvent rinses OCDD 1,2,3,7,8- PeCDD

OCDF 2,3,7,8- TCDD

2,3,7,8-TCDF 1,2,3,7,8- PeCDF

2,3,4,7,8- PeCDF 2,3,4,6,7,8- HxCDF 1,2,3,7,8,9- HxCDF

### Page 5 of 8 

# Primary Aluminum Testing: Dioxins and Furans

391 St. Jude Industrial Park **Parent company name:**  Noranda Aluminum, Inc. **Facility address:**  New Madrid, MO 63869 **Description of source tested:** 161 Duct

**Composite A nalysis** 
**Total (ng) Total (ng)**  **Moisture (%)**  **CO 2** **(%) O** **2 (%)**  **Flow (acfm)**  **Flow**

**(dscfm) Temperature** 

**( °F)**  5.60E-03 5.60E-03 1 0.8 0.8 20.6 326,262 268,234 178 5.50E-03 5.50E-03 2 0.5 0.9 20.6 328,471 269,883 181 4.10E-03 4.10E-03 3 0.5 0.8 20.5 327,274 267,423 181 5.19E-03 5.19E-03 1 0.8 0.8 20.6 326,262 268,234 178 2.70E-03 2.70E-03 2 0.5 0.9 20.6 328,471 269,883 181 3.13E-03 3.13E-03 3 0.5 0.8 20.5 327,274 267,423 181 2.20E-03 2.20E-03 1 0.8 0.8 20.6 326,262 268,234 178 3.30E-03 3.30E-03 2 0.5 0.9 20.6 328,471 269,883 181 2.10E-03 2.10E-03 3 0.5 0.8 20.5 327,274 267,423 181 1.50E-03 1.50E-03 1 0.8 0.8 20.6 326,262 268,234 178 2.14E-03 2.14E-03 2 0.5 0.9 20.6 328,471 269,883 181 1.40E-03 1.40E-03 3 0.5 0.8 20.5 327,274 267,423 181 2.50E-03 2.50E-03 1 0.8 0.8 20.6 326,262 268,234 178 1.50E-03 1.50E-03 2 0.5 0.9 20.6 328,471 269,883 181 2.61E-03 2.61E-03 3 0.5 0.8 20.5 327,274 267,423 181 1.80E-03 1.80E-03 1 0.8 0.8 20.6 326,262 268,234 178 1.90E-03 1.90E-03 2 0.5 0.9 20.6 328,471 269,883 181 1.40E-03 1.40E-03 3 0.5 0.8 20.5 327,274 267,423 181 1.50E-03 1.50E-03 1 0.8 0.8 20.6 326,262 268,234 178 1.80E-03 1.80E-03 2 0.5 0.9 20.6 328,471 269,883 181 1.50E-03 1.50E-03 3 0.5 0.8 20.5 327,274 267,423 181 2.90E-03 2.90E-03 1 0.8 0.8 20.6 326,262 268,234 178 4.17E-03 4.17E-03 2 0.5 0.9 20.6 328,471 269,883 181 1.70E-03 1.70E-03 3 0.5 0.8 20.5 327,274 267,423 181 1,2,3,7,8,9- HxCDD 1,2,3,6,7,8- HxCDD
1,2,3,6,7,8- HxCDF 1,2,3,4,7,8- HxCDD
1,2,3,4,7,8- HxCDF 1,2,3,4,6,7,8- HpCDF
1,2,3,4,7,8,9- HpCDF 1,2,3,4,6,7,8- HpCDD **Compound Run** 

**Number Exhaust Gas** 

### Page 6 of 8

**Composite A nalysis** 
**Total (ng) Total (ng)**  **Moisture (%)**  **CO 2** **(%) O** **2 (%)**  **Flow (acfm)**  **Flow**

**(dscfm) Temperature** 

**( °F)**  **Compound Run** 

**Number Exhaust Gas** 

1.70E-03 1.70E-03 1 0.8 0.8 20.6 326,262 268,234 178 2.00E-03 2.00E-03 2 0.5 0.9 20.6 328,471 269,883 181 1.83E-03 1.83E-03 3 0.5 0.8 20.5 327,274 267,423 181 2.80E-03 2.80E-03 1 0.8 0.8 20.6 326,262 268,234 178 2.20E-03 2.20E-03 2 0.5 0.9 20.6 328,471 269,883 181 2.40E-03 2.40E-03 3 0.5 0.8 20.5 327,274 267,423 181 4.90E-03 4.90E-03 1 0.8 0.8 20.6 326,262 268,234 178 2.40E-03 2.40E-03 2 0.5 0.9 20.6 328,471 269,883 181 4.37E-03 4.37E-03 3 0.5 0.8 20.5 327,274 267,423 181 3.30E-03 3.30E-03 1 0.8 0.8 20.6 326,262 268,234 178 1.60E-03 1.60E-03 2 0.5 0.9 20.6 328,471 269,883 181 1.40E-03 1.40E-03 3 0.5 0.8 20.5 327,274 267,423 181 1.90E-03 1.90E-03 1 0.8 0.8 20.6 326,262 268,234 178 1.60E-03 1.60E-03 2 0.5 0.9 20.6 328,471 269,883 181 1.70E-03 1.70E-03 3 0.5 0.8 20.5 327,274 267,423 181 1.70E-03 1.70E-03 1 0.8 0.8 20.6 326,262 268,234 178 3.10E-03 3.10E-03 2 0.5 0.9 20.6 328,471 269,883 181 2.50E-03 2.50E-03 3 0.5 0.8 20.5 327,274 267,423 181 9.80E-03 9.80E-03 1 0.8 0.8 20.6 326,262 268,234 178 4.51E-03 4.51E-03 2 0.5 0.9 20.6 328,471 269,883 181 1.60E-03 1.60E-03 3 0.5 0.8 20.5 327,274 267,423 181 6.70E-03 6.70E-03 1 0.8 0.8 20.6 326,262 268,234 178 1.20E-02 1.20E-02 2 0.5 0.9 20.6 328,471 269,883 181 5.84E-03 5.84E-03 3 0.5 0.8 20.5 327,274 267,423 181 2.10E-03 2.10E-03 1 0.8 0.8 20.6 326,262 268,234 178 3.50E-03 3.50E-03 2 0.5 0.9 20.6 328,471 269,883 181 2.80E-03 2.80E-03 3 0.5 0.8 20.5 327,274 267,423 181 OCDF OCDD 2,3,7,8-TCDD

2,3,7,8-TCDF 2,3,4,7,8-PeCDF 1,2,3,7,8-PeCDD

1,2,3,7,8-PeCDF

2,3,4,6,7,8- HxCDF 1,2,3,7,8,9- HxCDF

### Page 7 of 8



### 391 St. Jude Industrial Park New Madrid, MO 63869

**Other Supporting Information**

### Page 8 of 8

**Other Supporting Information**Page 1 of 4 

## Primary Aluminum Testing: Polychlorinate Biphenyls (PCB)
**Parent company**

**name:** Noranda Aluminum, Inc. **Facility address:** 391 St. Jude Industrial Park

New Madrid, MO 63869 **Description of source tested:** 161 Duct

**lb/hr lb/ton**  **Throughput** 1 4/24/2013 11:084/24/2013 15:32 1.18E-07 1.87E-08 6.30 Aluminum 2 4/24/2013 16:484/24/201320:30 8.21E-08 1.30E-08 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 9.26E-08 1.47E-08 6.30 Aluminum 1 4/24/2013 11:084/24/2013 15:32 6.44E-07 1.02E-07 6.30 Aluminum 2 4/24/2013 16:484/24/201320:30 5.10E-07 8.09E-08 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 5.61E-07 8.91E-08 6.30 Aluminum 1 4/24/2013 11:084/24/2013 15:32 5.85E-07 9.28E-08 6.30 Aluminum 2 4/24/2013 16:484/24/201320:30 3.94E-07 6.25E-08 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 3.62E-07 5.75E-08 6.30 Aluminum 1 4/24/2013 11:084/24/2013 15:32 4.17E-07 6.62E-08 6.30 Aluminum 2 4/24/2013 16:484/24/201320:30 8.75E-07 1.39E-07 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 4.18E-07 6.64E-08 6.30 Aluminum 1 4/24/2013 11:084/24/2013 15:32 5.88E-08 9.33E-09 6.30 Aluminum 2 4/24/2013 16:484/24/201320:30 1.13E-07 1.80E-08 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 1.09E-07 1.74E-08 6.30 Aluminum 1 4/24/2013 11:084/24/2013 15:32 5.04E-08 7.99E-09 6.30 Aluminum 2 4/24/2013 16:484/24/201320:30 6.80E-08 1.08E-08 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 5.61E-08 8.91E-09 6.30 Aluminum Hexachlorinated biphenyls Tetrachlorinated biphenyls

Pentachlorinated biphenyls Dichlorinated biphenyls

Trichlorinated biphenyls Monochlorinated biphenyls **Throughput Material**  **Test Method Comments Test End**  **Date Test End** 

**Time Calculated Emission** 

**Rate Throughput** 

**(ton/hr) Compound**  **Run**

**Number Test Start** 

**Date Test Start** 

**Time**Page 2 of 4

**lb/hr lb/ton** 

**Throughput Throughput**  **Material Test Method Comments**  **Test End Date**  **Test End**

**Time Calculated Emission** 

**Rate Throughput** 

**(ton/hr) Compound**  **Run**

**Number Test Start** 

**Date Test Start** 

**Time**

1 4/24/2013 11:084/24/2013 15:32 1.01E-08 1.60E-09 6.30 Aluminum 2 4/24/2013 16:484/24/201320:30 5.10E-09 8.09E-10 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 5.61E-09 8.91E-10 6.30 Aluminum 1 4/24/2013 11:084/24/2013 15:32 4.76E-09 7.55E-10 6.30 Aluminum 2 4/24/2013 16:484/24/201320:30 5.10E-09 8.09E-10 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 4.21E-09 6.68E-10 6.30 Aluminum 1 4/24/2013 11:084/24/2013 15:32 3.36E-09 5.33E-10 6.30 Aluminum 2 4/24/2013 16:484/24/201320:30 4.53E-09 7.19E-10 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 3.09E-09 4.90E-10 6.30 Aluminum 1 4/24/2013 11:084/24/2013 15:32 2.66E-09 4.22E-10 6.30 Aluminum 2 4/24/2013 16:484/24/201320:30 4.33E-09 6.88E-10 6.30 Aluminum 3 4/25/2013 8:48 4/25/2013 12:28 1.77E-09 2.81E-10 6.30 Aluminum Octachlorinated biphenyls

Decachlorinated biphenyls Nonachlorinated biphenyls Heptachlorinated biphenylsPage 3 of 4

**Composite Analy**  **sis Compound**  **Total (ng) Total (ng)**  **Moisture (%** **) CO** **2 (%** **) O** **2 (%** **) Flow**  **(acfm) Flow** 

**(dscfm) Temperature** 

**( °F)**  0.42 0.42 1 0.8 0.8 20.6 326,262 268,234 178 0.29 0.29 2 0.5 0.9 20.6 328,471 269,883 181 0.33 0.33 3 0.5 0.8 20.5 327,274 267,423 181 2.3 2.3 1 0.8 0.8 20.6 326,262 268,234 178 1.8 1.8 2 0.5 0.9 20.6 328,471 269,883 181 2 2 3 0.5 0.8 20.5 327,274 267,423 181 2.09 2.09 1 0.8 0.8 20.6 326,262 268,234 178 1.39 1.39 2 0.5 0.9 20.6 328,471 269,883 181 1.29 1.29 3 0.5 0.8 20.5 327,274 267,423 181 1.49 1.49 1 0.8 0.8 20.6 326,262 268,234 178 3.09 3.09 2 0.5 0.9 20.6 328,471 269,883 181 1.49 1.49 3 0.5 0.8 20.5 327,274 267,423 181 0.21 0.21 1 0.8 0.8 20.6 326,262 268,234 178 0.4 0.4 2 0.5 0.9 20.6 328,471 269,883 181 0.39 0.39 3 0.5 0.8 20.5 327,274 267,423 181 0.18 0.18 1 0.8 0.8 20.6 326,262 268,234 178 0.24 0.24 2 0.5 0.9 20.6 328,471 269,883 181 0.2 0.2 3 0.5 0.8 20.5 327,274 267,423 181 Hexachlorinated biphenyls Tetrachlorinated biphenyls

Pentachlorinated biphenyls Tetrachlorinated biphenyls Dichlorinated biphenyls

Trichlorinated biphenyls Trichlorinated biphenyls **Other Supporting Information**

**Separate Analy**

**sis**

Monochlorinated biphenyls **Poly chlorinated Bipheny** **ls Emission Test Results**
**Compound Run**  **Number Exhaust Gas** 

Pentachlorinated biphenyls

Hexachlorinated biphenyls Monochlorinated biphenyls

Dichlorinated biphenylsPage 4 of 4

**Composite Analy**  **sis Compound**  **Total (ng) Total (ng)**  **Moisture (%** **) CO** **2 (%** **) O** **2 (%** **) Flow**  **(acfm) Flow** 

**(dscfm) Temperature** 

**( °F)**  **Other Supporting Information Separate Analy** 

**sis Poly** **chlorinated Bipheny ls Emission Test Results** 
**Compound Run**  **Number Exhaust Gas** 

0.0 0.0 1 0.8 0.8 20.6 326,262 268,234 178 0.0 0.0 2 0.5 0.9 20.6 328,471 269,883 181 0.0 0.0 3 0.5 0.8 20.5 327,274 267,423 181 0.0 0.0 1 0.8 0.8 20.6 326,262 268,234 178 0.0 0.0 2 0.5 0.9 20.6 328,471 269,883 181 0.0 0.0 3 0.5 0.8 20.5 327,274 267,423 181 0.0 0.0 1 0.8 0.8 20.6 326,262 268,234 178 0.0 0.0 2 0.5 0.9 20.6 328,471 269,883 181 0.0 0.0 3 0.5 0.8 20.5 327,274 267,423 181 0.01 0.01 1 0.8 0.8 20.6 326,262 268,234 178 0.0 0.0 2 0.5 0.9 20.6 328,471 269,883 181 0.01 0.01 3 0.5 0.8 20.5 327,274 267,423 181 Octachlorinated biphenyls

Decachlorinated biphenyls Nonachlorinated biphenyls

Decachlorinated biphenyls Heptachlorinated biphenyls

Nonachlorinated biphenyls Heptachlorinated biphenyls

Octachlorinated biphenyls

# Primary Aluminum Testing: Exhaust flow rates, temperatures, and O2/CO2 contents

**Parent company**

**name:** Noranda Aluminum, Inc. **Facility address:** 391 St. Jude Industrial Park

New Madrid, MO 63869 **Description of source tested:**161 Duct

**Moisture (%)**  **CO 2** **(%) O** **2 (%)**  **Flow (acfm)**  **Flow**

**(dscfm)** 1 4/24/13 11:08 4/24/13 15:32 Methods 1-4 Method 5 0.8 0.9 20.6 315,821261,410 2 4/24/13 16:48 4/24/13 20:30 Methods 1-4 Method 5 0.7 0.9 20.6 324,914265,504 3 4/25/13 8:48 4/25/13 12:28 Methods 1-4 Method 5 0.6 0.8 20.5 316,789257,678 1 4/24/13 11:08 4/24/13 15:32 Methods 1-4 CARB 428/429 0.8 0.8 20.6 326,262268,234 2 4/24/13 16:48 4/24/13 20:30 Methods 1-4 CARB 428/429 0.5 0.9 20.6 328,471269,883 3 4/25/13 8:48 4/25/13 12:28 Methods 1-4 CARB 428/429 0.5 0.8 20.5 327,274267,423 **Test Start Date**  **Run Number**  **Exhaust Gas Simultaneous**  **with which pollutant test?**  **Test Method (e.g. Method 5)**  **Test End Time**  **Test End Date**  **Test Start Time** 

### 391 St. Jude Industrial Park

**Temp ( °F)**  174 183 183 178 181 181