EPA Reg. No. 87283-1 
.... ~ , - -

ISB'S Front-end PRlA Completeness Screen 

Draft 3; 10/25/07 

EPA Receipt Date: I/I.? liZ; EPA Reg. Number: j1'?.;<f3-{ 

-----, Checkc-Li~t It,em .• ," ,", " 

Yes No ---

I Has the PRIA Fee been Paid; is a copy of the check or ./ P1.ly.gov receipt included in the Submission Package? L. .. _._ -'-

Is an Application Form (EPA FOlm 8570·1) Included in the ./ 2 SubmiSSion Package, is it completely filled out and signed 

including package type? 

----------

Is a Confidential Statement of Formula (EPA Form 8570~ / 3 29) Included in the Submission Package, is it completely 

filled out and signed (boxes 1·21)? 

4 Is a [<'ormulator's Exemption Statement (EPA Form 8570- ./ 27) Included in the Submission Package? . ,,---_ ... --

5 J:-.; a Certification with Respect to Citation of Data (EPA ./ j:urrn 3570-34) 1ncluded in the Submission Package? ---- -

(, b a nata Matrix (EPA Form 8570-35) Included in the ./ 

Submission Package? 

---_ .. 7 J:.; a Label Included in the Submission Package? ,/ -.-

X Arc Data Included in the Submission Package? v , .. _---- -- I I) Is the Submission an Amendment? V ._,--_. 

N/A 

1
( 

PYXIS REGULATORY CONSULTING, l1'1C 

4110 1361h St. NW 

Gig Harbor, WA 98332 

COURIER DELIVERY 

Kathryn Montague (PM 23) 

Document Processing Desk (FNL LBL) 

Office of Pesticide Programs (7504P) 

U.S. Environmental Protection Agency 

Room 8-4900, One Potomac Yard 

2777 S. Crystal Drive 

Arlington, V A 22202 

November 12, 2010 

Phone: 253-853-7369 

Fax: 253-853-5516 

www.PyxisRC.com 

RE: Willowood Oxytluorfen, LLC - Wi1lowood Oxyfluorfen Technical (EPA Reg. No. 87283-1) 

Submission afFinal Product Labeling 

Dear Ms. Montague, 

On behalf of Willowood Oxyfluorfen, LLC please find the enclosed final product labeling for Willowood 

Oxytluorfen Technical. 

In support ofthis submission, we submit the following documents: 

1. Completed Application for Registration (EPA Form 8570~1) 

2. Two (2) copies of the Willowood Oxyfluorfen Technical final product labeling 

3. Letter of Authorization 

Please feel free to contact me by phone (253) 853~7369 or by email atAnn@PyxisRC.comifyou have 

any questions or need any additional information. 

Sincerely, 

4L1~ 

Ann M. Tillman 

Enclosures 

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Fo~ OMS No. ' ..,'"" 

United Stoto~ Registration opp Identifier Number 

&EPA Environmental Protection Agency r- Amendment 

Wouhington, OC 20460 t:z: Other 

, for , - I 

• ComponylProduct Number 2. EPA Product Menager 3. Proposed Clouillcotion 

, K. o Nene o R"trict&d 

•• (Nomoi PM' 

" LLClWiliowood f), vfll "fp , 

,5. Nome $Ild Addrool of Applicant (Include ZIP Code' 6. Expedited Revelw. In aCCOfdance wi1h FfFRA Section 3(c)(3) 

Willowood Elhofumesate, LLC IbW), my product is similar Ot identical in composition and labeling 

c/o Pyxis RBgul,lIory Consulling, Inc. to: 

4110 1361h SI. NW EPA Reg. No. Gig Harbor, WA 98332 

. D Chllck if this is II new addrl}ss Product Name 

,-II 

D Amendment - Explain below. ~ Final printed labels In ropaonu$ to 111112010 

C- D Agltncv lonllr dated 

RIIHubmlesion in rnponua to Agency lottllr deted "Mo Too" Applicotion. 

:0= Notllicerlon . Explllin below. 0 Orhor - Exploin bolow. 

Explanation: u~o odditionol pegol~1 if nllclluory. tFo, section lond Soctien 11.1 

Submission of final ptinled label. 

-J!!.. 

1. Mo.,'o' Thi. P"d,o' 1'0"", nO' 

U~F:,o,;"g Worer Solublo Pockalling 2. Type of Contoino, 

tf" I By" t;J M"., No No No PlOltiC 

Glan 

I ;~CertifiC8tIOn must ,~;i~'~ No. per II "Yea" No. por Plpar 

wgt. conteiner Pockoge wgt conteino, Oth~r submitted 

I" L"o'," of ; , Ro<o I't: .J :; ~;to' ; 

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6. Manne, In Which Lebel Is Alfixed to Product l J ~i1~~~~:d u Othe, 

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Neme 

:~oent Telephone No. IInclude Aros Codal Ann Tillman (253) 853-7369 

Certification 6. oet~ t<!lp'I~..:~tion 

I cortify thot tho otetomants I heve mede on thi9 form end allettechmonta thereto oro trull. eccumto end completo. Rec'-ivod 

I acknowledge thet eny knowlinOlly lolso 0' mialoooinO IHetomont moy ba punishablo by fine or irTlj:lrilonmont or (';-'t~mgedl both undor oppliceblo low. , 

2. Signoturo 

Jut' r;rJti 3. Titlo " , 

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Agent I " " " ... :' 

4., Typoa Nomo 5.0'"11 

1///,/_/10 , 

Ann Tillman 

EPA F"m 6570-1 'R ... ,·94, , ." Wh ••• EPA '" Cop, , ",.ow 1 Cop, 

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3
WILLOWOOD OXYFLUORFEN TECHNICAL 

FOR USE IN FORMULATING HERBICIDES ONLY 

ACTIVE INGREDIENT: 

Oxyfluorfen: 2-chloro-1-(3-elhoxy-4-nitrophenoxy)-4-

(trifluoromelhyl)benzene .............................................................................. 98.1 % 

OTHER 

INGREDIENTS ............................. h ............................................................... t.9% 

TOT AL. ................. ". " ....................................................... ,,' ..... 100.0% 

EPA Reg. No. 87283-1 EPA Est. No. 86564-CHN-001 

Manufactured for: 

Willowood Oxyfluorfen, LLC 

1600 NW Garden Valley Blvd. 

Roseburg, OR 97471 Net ContentS: Ibs. 

[FON SKIN OR 

CLOTHING: 

IF IN EYES: 

IF 

SWALLOWED 

IF INHALED 

KEEP OUT OF REACH OF CHILDREN 

CAUTION 

FIRST AID 

• Take off contaminated clothing. 

• Rinse skin immediately with plenty of water for t5 -20 minutes. 

• Call a Poison Control Center or doctor for treatment advice. 

• Hold eye open and rinse slowly and genlly with water for 15 -20 

minutes. 

• Remove contact lenses, if present, after the first 5 minutes, then 

continue rinsing. 

• Call a Poison Control Center or doctor for treatment advice. 

• Call a poison control center or doctor immediately for treatment 

advice. 

• Have person S'IP a glass of water'lf able to swallow. 

• Do not induce vomiting unless told to do so by the poison control 

center or doctor. 

• Do not Qive anythinQ by mouth to an unconscious person. 

• Move person to fresh air. 

• If person is not breathing, call 911 oran ambulance, then give 

artificial respiration, preferably by mouth-to-mouth, if possible. 

_. '. S'311 a 120ison control center or doctor for further treatment advice. 

Note to Ph,-:;r.::ian: -Evac'Jation of the stomach might be advisable. 

For MEDICf\.L E:ncrgencies call the National Pesticide Infonnation Center 24-hours a 

day at1-800-858:i3ia.l-lave the product container or label with you when calling a 

Poison Control Center or doctor or QOinQ for treatment. 

PF;.ECA,UTIONARY STATEMENTS 

: HhZARD ';"0 Hl:lMANS AND DOMESTIC ANIMALS 

CAUl·ION. -Flbrmf;.J1 if ab3orbe~:f through skin. Avoid contact with skin, eyes or 

clothing. Wash hands after handling and before eating, drinking, chewing gum, using 

tobacco, or using the toilet. Remove contaminated clothing and wash clothing before 

reuse. 

ENVIRONMENTAL HAZARDS 

This product is toxic to aquatic invertebrates and fISh. Do not discharge effluent 

containing this product directly into lakes, streams, ponds, estuaries, oceans or public 

waters unless this product is specifically identified and addressed in a NDPES permit. 

Do not discharge effluent containing this product to sewer systems without previously 

notifying the sewage treatment plant authority. For guidance, contact your State Water 

Board or Regional Office of the Environmental Protection Agency. 

DIRECTIONS FOR USE 

It is a violation of Federal law to use this product in a manner inconsistent with 

its labeling. 

This product may only be used to formulate end-use products with the following uses: 

(1) artichokes (globe), bananas, blackberry, brOCCOli, cabbage, cauliflower, cacao 

(Hawaii only), citrus (non-bearing), clover grown fur seed, clary sage grown for 

essence, coffee, conifers (seedbeds, transplants, container stock) and selected 

deciduous trees, corn, colton, coltonwood, eucalyptus, fallow bed (colton/soybeans), 

fallow land, garbanzo beans, garlic, grass seeds, guava (Hawaii only), horseradish, 

jojoba, mint, non-crop use on rights of way, nursery stock, onions, onions grown fn"-.. 

seed, ornamentals, papayas (Hawaii only), raspberry, soybeans, taro, and tree fl1 

nuts and vines (which include almond, apple, avocado, beechnut, brazil nut, butternut, 

cashew, cherry, chestnut, chinquapin, crabapple, date, feijoa , fig, filbert, grapes, 

hickory nut, kiwi, loquat, macadamia nut, mayhaw, nectarines, olives, peach, pear, 

pecan, persimmon, pistachio, plum, pomegranates, prune, quince, walnut). 

(2) specific uses not listed on the MP label if the fonnulator, user group or grower has 

complied with U.S. EPA submission requirements regarding support of such uses; and 

(3) uses for experimental purposes that are in compliance with U.S. EPA requirements. 

Each fonnulator is responsible for obtaining EPA registration for his own end use 

products. 

Willowood Oxyfluorfen Technical must be melted by holding at 110QC for 48 hours. Do 

not heat above 200Q

C (product decomposes). 

STORAGE AND DISPDSAL 

Do not contaminate water, food or feed by storage or disposal. 

PESTICIDE STORAGE: Store in original container tightly closed and in a safe place. 

PESTICIDE DISPOSAL: Wastes resulting from the use of this product must be 

disposed of on site or at an approved waste disposal facility. 

CONTAINER HANDLING: Nonrefillable container. Do not reuse or refill this contain 

Completely empty liner by shaking and tapping sides and bottom to loosen clinging 

particles. Empty residue into processing equipment. Then dispose of liner in a 

sanitary landfill or by incineration if allowed by state and local authorities. Offer the 

drum for recycling, if available. 

WARRANTY STATEMENT 

IMPORTANT NOTICE -Seller warrants that this product conforms to the chem'lcal 

description and is reasonably fit for purposes stated on the label when used in 

accordance with the directions and instructions under normal conditions of use. To the 

extent consistent with applicable law, neither this warranty nor any other warranty of 

merchantability or fitness for a particular purpose, express or implied, extends to the 

use contrary to label instructions, or under abnormal conditions, or under conditions 

not reasonably foreseeable to seller, and buyer assumes the risk of any such use. 

EPA approval 11-01-2010 

4
WILLOWOOD OXYFLUORFEN TECHNICAL 

FOR USE IN FORMULATING HERBICIDES ONLY 

ACTIVE INGREDIENT: 

Oxyfluorfen: 2-chloro-1-(3-elhoxY-4-nilrophenoxy)-4-

(trifluoromelhyl)benzene ............................................................................... 98.1 % 

OTHER 

INGREDIENTS .............................................................................................. 1.90/0 

TOTAL ..................................................................................... 100.00/0 

EPA Reg. No. 87283-1 EPA Est. No. 86564-CHN-OO t 

Manufactured for: 

Wdlowood Oxyfluorfen, LLC 

1600 NW Garden Valley Blvd. 

Roseburg, OR 9747 t Net Contents: Ibs. 

IF ON SKIN OR 

CLOTHING: 

IF IN EYES: 

IF 

SWALLOWED 

IF INHALED 

KEEP OUT OF REACH OF CHILDREN 

CAUTION 

FIRST AID 

• Take off contaminated clothing. 

• Rinse skin immediately with plenty of water for 15 -20 minutes. 

• Call a Poison Control Center or doctor for treatment advice. 

• Hold eye open and rinse slowly and gently with water for 15 -20 

minutes. 

• Remove contact lenses, if present, after the first 5 minutes, then 

continue rinsing. 

• Call a Poison Control Center or doctor for treatment advice. 

• Call a poison control center or doctor immediately for treatment 

advice. 

• Have person S'IP a glass of water'lf able to swallow. 

• Do not induce vomiting unless told to do so by the poison control 

center or doctor. 

• Do not Qive anythinQ by mouth to an unconscious person. 

• Move person to fresh air. 

• If person is not breathing, call 911 or an ambulance, then give 

artificial respiration, preferably by mouth-to-mouth, if possible. 

• Call a poison control center or doctor for further treatment advice. 

Note to Ph sician: Evacuation of the stomach mi ht be advisable. 

For MEDICAL Emergencies call the National Pesticide Information Center 24-hours a 

day at 1-800-858-7378. Have the product container or label with you when calling a 

Poison Control Center or doctor or going for treatment. 

PRECAUTIONARY STATEMENTS 

HAZARD TO HUMANS AND DOMESTIC ANIMALS 

CAUTION. Harmful if absorbed through skin. Avoid contact with skin, eyes or 

clothing. Wash hands after handling and before eating, drinking, chewing gum, using 

tobacco, or using the toilet. Remove contaminated clothing and wash clothing before 

reuse. 

ENVIRONMENTAL HAZARDS 

This product is toxic to aquatic invertebrates and fish. Do not discharge effluent 

containing this product directry into lakes, streams, ponds, estuaries, oceans or public 

waters unless this product is specifically identified and addressed in a NDPES permit. 

Do not discharge effluent containing this product to sewer systems without previously 

notifying the sewage treatment plant authority. For guidance, contact your State Water 

Board or Regional Office of the Environmental Protection Agency. 

DIRECTIONS FOR USE 

It is a violation of Federal law to use this product in a manner inconsistent with 

its labeling. 

This product may only be used to fonnulate end-use products with the following uses: 

(1) artichokes (globe), bananas, blackberry, broccoli, cabbage, cauliflower, cacao 

(Hawaii only), citrus (non-bearing), clover grown for seed, clary sage grown for 

essence, coffee, conifers (seedbeds, transplants, container stock) and selected 

deciduous trees, corn, cotton, cottonwood, eucalyptus, fallow bed (cotton/soybeans), 

fallow land, garbanzo beans, garlic, grass seeds, guava (Hawaii only), horseradish, 

jojoba, mint, non-crop use on rights of way, nursery stock, onions, onions grown fn~""", 

seed, ornamentals, papayas (Hawaii only), raspberry, soybeans, taro, and tree fn . 

nuts and vines (which include almond, apple, avocado, beechnut, brazil nut, buttemut, 

cashew, cherry, chestnut, chinquapin, crabapple, date, feijoa , fig, filbert, grapes, 

hickory nut, kiwi, loquat, macadamia nut, mayhaw, nectarines, olives, peach, pear, 

pecan, persimmon, pistachio, plum, pomegranates, prune, quince, walnut). 

(2) speCific uses not listed on the MP label if the formulator, user group or grower has 

complied with U.S. EPA submission requirements regarding support of such uses; and 

(3) uses for experimental purposes that are in compliance with U.S. EPA requirements. 

Each formulator is responsible for obtaining EPA registration for his own end use 

products. 

Willowood Oxyfluorfen Technical must be melted by holding at 110°C for 48 hours. Do 

not heat above 200"C (product decomposes). 

STORAGE AND DISPOSAL 

Do not contaminate water, food or feed by storage or disposal. 

PESTICIDE STORAGE: Store in Original container tightry closed and in a safe place. 

PESTICIDE DISPOSAL: Wastes resulting from the use of this product must be 

disposed of on site or at an approved waste disposal facility. ~ 

CONTAINER HANDLING: Nonrefillable container. Do not reuse or refill this contain 

Completely empty liner by shaking and tapping sides and bottom to loosen clinging 

particles. Empty residue into processing equipment. Then dispose of liner in a 

sanitary landfdl or by incineration if allowed by state and local authorities. Offer the 

drum for recycling, if available. 

WARRANTY STATEMENT 

IMPORTANT NOTICE -Seller warrants that this product conforms to the chem'lCal 

description and is reasonably fit for purposes stated on the label when used in 

accordance with the directions and instructions under normal conditions of use. To the 

extent consistent with applicable law, neither this warranty nor any other warranty of 

merchantability or fitness for a particular purpose, express or implied, extends to the 

use contrary to label instructions, or under abnonnal conditions, or under conditions 

not reasonably foreseeable to seller, and buyer assumes the risk of any such use. 

EPA approval 11-01-2010 

5
41\0136 .. St NW 

WILLOWOOD OXYFLUORFEN, LLC 

Phone: 253-853-7369 

Gig Harbor, WA 98332 

November 9, 2009 

Document Processing Desk (COADR) 

Office of Pesticide Programs (7504P) 

U.S. Environmental Protection Agency 

Room 8A900, One Potomac Yard 

2777 S. Crystal Drive 

Arlington, VA 22202 

To Whom It May Concern: 

RE: Letter of Authorization 

Fax: 253-853-5516 

Please let this letter serve to notify you that Pyxis Regulatory Consulting, Inc. (contact 

information below) is authorized to represent WiIIowood Oxyfluorfen, LLC (Co. No. pending) 

as authorized agent before the U.S. Environmental Protection Agency in all matters regarding 

our pesticide registrations and applications for registrations pursuant to the Federal Insecticide, 

Fungicide and Rodenticide Act (FIFRA), 7 USC Section 136 et seq. Direct all official 

correspondence from EPA to: 

Agent: 

Pyxis Regulatory Consulting, Inc. 

41\0136" St. NW 

Gig Harbor, W A 98332 

T: (253) 853-7369 

F: (253) 853-5516 

info@PyxisRC.com 

If you have any questions, please do not hesitate to contact me. 

Sincerely, 

~~ , 

Brian Heinze ~ 

President 

Willowood Oxyfluorfen, LLC 

cc: Pyxis Regulatory Consulting, Inc. 

6
( ,NITED STATES ENVIRONMENTAL rl . ":CTION AGENCY 

WASHINGTON, D.C. 20460 

February 3, 2010 

OPP Decision Number: D-426039 

EPA File Symbol or Registration Number: 87283-R 

Product Name: WlLLOWWOOD OXYFLUORFEN TECHNICAL 

EPA Application Receipt Date: I 2-Jan-20 I 0 

EPA Waiver Request Receipt Date: 12-Jan-2010 

EPA Company Number: 87283 

Company Name: WILLOWOOD OXYFLUORFEN, LLC 

JANELLE KAY 

PYXIS REGULATORY CONSULTING, INC. 

WILLOWOOD OXYFLUORFEN, LLC 

4110 1136TH STREET, NW 

GIG HARBOR, W A 98332-

SUBJECT: Approval of 50% Small Business Waiver Request 

Dear Registrant: 

OFFlCEOF 

PREVENTION, PESTICIDES AND 

TOXIC SUBSTANCES 

The Office of Pesticide Programs has approved your request for 50% waiver of the 

pesticide registration fee associated with the action referenced above. The decision review 

period for this action will begin on the date of this letter. 

The Action has been identified as Action Code: R31 0 

NEW PRODUCT;NON-F AST TRACK (INCLUDES REVIEWS OF PRODUCT 

CHEMISTRY;ACUTE TOXICITY;PUBLIC HEALTH PEST EFFICACy); 

If you have any questions, please contact the Pesticide Registration Service Fee 

Ombudsman, at (703) 305-6249. 

Sincerely, 

Infonnation 

os~~~~ Teclmology & Resources Management Division 

Office of Pesticide Programs 

7
I ( 

~taril:®lJital~it© ft»® taldd®d tt© talO'1l ~-Jtal©jg~il:IJta1c~rett 

. 

Reg. ~Ol" 01~1/2- l Dec it '--f2~o3q 

DeSClrilPtion:~~_-,-N'""-Q\;Jtt;Al,l-l-\'VmL!· .4<. :wdut""",-~"",: _____ -_ 

1. : Q---iP'lacement within the e-Jac!(eiljacket: 

«Default (chronological, top "':newest) 

o Fils Location: (PDf page number,i,e" "before page 

46") 

2. 9(Send to Data IEllirlllcition contractors this materia!: 

'5r Newly stamped accepted label 

o Notification ( 

K NewCSf ~ +oidiA· *' 

o Other: __________ ~-

3. AUacl'n tl'nis coversileet: to the top of the material 01' jacflet. It 

must be well organized aOld clipped together, NOT STAPLED. 

Then give the material with this coversl'neet to staff in the 

iOlfonnation Services Center (Room 8-4900). 

R e 'liD ewer's N a m IS: ~&b"'--tha"""--i\"",Jcxu:..'t\Q .\'\-1 ~B~e;;t.l!()-I'w,"",",,!::{,D.4----

DivisooW!J: RD \ H6 

Date: ~ ________ ~l~\~\_L\_\_O ________ ~ __ __ 

Created August14. 2008 

8
U.S. ENVIRONMENTAL PROTECTION 

AGENCY EPA Reg. Number: Date oflssuance: 

~"',,€O ST"'T~ ... Office of Pesticide Programs 87283-1 .i ~ "i 

'~-a' Registration Division (7505P) : 1 ClIJ -

\'=.;' Ariel Rios Building 

+""'(PR~ 1200 Pennsylvania Ave., NW 

Washington, D.C. 20460 

NOTICE OF PESTICIDE, Term of Jssuancc: conditional 

L.. Registration Name ofPestieide Product: 

_ Reregistration 

(undcr FIFRA, as amended) Willowood Oxyfluorfen 

Technical 

Name and Address of Registrant (include ZIP Code): 

Willowood Oxyfluorfen, LLC 

8690 Lookingglass Road 

Roseburg, OR 97470 

Note: Changes in labeling differing in subslanee from that acceplcd in connel:tion with this registration must be submitted to and accepted by the 

Registration Division prior 10 usc of the label in commerce. In any correspondcnce on this product always refer 10 the above EPA registralion number. 

On the basis ofinfonnation furnished by the registrant, the above named pesticide is hereby registered/reregisJered under Jhe Federal Insecticide, 

Fungicide and Rodenticide Act. Registration is in no way to be construed as an endorsement or recommendation ofthis product by the Agency. In order 

to project health and the environment, the Administrator, on his motion, may at any time suspend or eanec1the registration of a pesticide in accordance 

with the Act. The acceptance of any name in connection with the registration ofa product under this Act is not to be construed as giving the registrant a 

right to exclusive usc of the name or to its usc if it has bccn covered by othcrs. 

This product is registered in accordance with FIFRA provided that you: 

I. Submit and/or cite all data required for registration review/reregistration of your product when the 

Agency requires all registrants of similar products to submit data. 

2. Submit the data listed below: 

a. Within one year of the date on this registration notice, Storage Stability (830.6317) and 

Corrosion Characteristics (830.6320) studies must be submitted. It is recommended that the 

observations be made at 0, 3, 6, 9, and 12 month intervals. 

3. Make the following label revisi.ons: 

a. Revise the EPA Reg. No. to read, "EPA Reg. No. 87283-1" 

b. Revise the First Aid section so that 'If on Skin or Clothing' instructions are listed first 

c. Per the acute toxicity review, revise the 'Hazards to Humans and Domestic Animals' 

section to read as follows: 

"CAUTION: Harmful if absorbed through skin. A void contact with skin, eyes or 

clothing. Wash hands after handling and before eating, drinking, chewing gum, using 

tobacco, or using the toilet Remove contaminated clothing and wash clothing before 

reuse." 

d. Add, "(Hawaii only)" after "cacao" in the list of use sites. 

Continued on page 2 

S;","ore of App,"';o, Offid'~ 

)1 lYlonb Date: 

Kathryn V. Montag'fjl' i/1l(D Project Manager 23 Z ~.I(l\f .. - i 

Herbicide Branch 

Registration Division (7505P) 

EPA Fonn 8570 6 . 

9
Page 2 of2 

EPA Reg. No. 87283-1 

Notice of Registration 

Submit one (l) copy of the revised final printed label for the record. 

If these conditions are not complied with, the registration will be subject to cancellation in accordance 

with FIFRA sec. 6(e). Your release for shipment of the product constitutes acceptance of these 

conditions. A stamped copy of the label is enclosed for your records. 

10
( 

WILLOWOOD OXYFLUORFEN TECHNICAL 

FOR USE IN FORMULATING HERBICIDES ONLY 

ACTIVE INGREDIENT: 

Oxyfluorfen: 2-ch loro-1-(3-ethoxy-4-n itrop henoxy)-4-( trifluoromelhyObenzene ................. 98.1 % 

OTHER INGREDIENTS ........................................................................................................ 1.9% 

TOTAL .......................................................................................................... 100.0% 

KEEP OUT OF REACH OF CHILDREN 

CAUTION 

FIRST AID 

ACCEPTED 

with COMMENTS 

In EPA Letter Dated: 

Under the Federal 1m ·.,(icide, 

Fungicide, and RodcrlilCldeAct 

as aml!flded, for the peslil::ide 

registered under EPA Reg. No. 

IF IN EYES: • Hold eye open and rinse slowly and gently with water for 15 -20 minutes. 

• Remove contact lenses, if present, after the first 5 minutes, then continue 

rinsing. 

• Call a Poison Control Center or doctor for treatment advice. 

IFON SKIN OR • Take off contaminated clothing. 

CLOTHING: • Rinse skin immediately with plenty of water for 15 -20 minutes. 

• Call a Poison Control Center or doctor for trealment advice. 

IF SWALLOWED • Call a poison control center or doctor immediately for treatment advice. 

• Have person sip a glass of water if able to swallow. 

• Do not induce vomiting unless told to do so by the poison control center or 

doctor. 

• Do not give anything by mouth to an unconscious oerson. 

IF INHALED • Move person to fresh air. 

• If person is not breathing, call 911 or an ambulance, then give artificial 

respiration, preferably by mouth-to-mouth, if possible. 

• Call a poison control center or doctor for further treatment advice. 

Note to Physician: Evacualion of the stomach might be advisable. 

For MEDICAL Emergencies call the National Pesticide Information Center 24-hours a day at 1-800-858-

7378. Have the product container or label with you when calling a Poison Control Center or doctor or 

I going for treatment. 

EPA Reg. No. 87283-

Manufactured for. 

Willowood Oxyfluorfen, LLC 

8690 Lookingglass Road 

Roseburg, OR 97470 

EPA Est. No. 

.,' ( 

,(, . , , 

Net Contents: xx Ibs. 

, " ( " , 

, " " . 

Willowood Oxyfluorfen Technical Label 1 

11
( I I 

PRECAUTIONARY STATEMENTS 

HAZARD TO HUMANS AND DOMESTIC ANIMALS 

CAUTION 

May cause moderate eye irritation. Harmful if swallowed, inhaled or absorbed through skin. Do not get in 

eyes or on clothing. Avoid contact with skin, eyes or clothing. Avoid breathing vapors or dust. Wash 

hands after handling and before eating, drinking, chewing gum, using tobacco, or using the toilet. 

Remove contaminated clothing and was clothing before reuse. 

ENVIRONMENTAL HAZARDS 

This product is toxic to aquatic invertebrates and fish. Do not discharge effluent containing this product 

directty into lakes, streams, ponds, estuaries, oceans or public waters unless this product is specifically 

identified and addressed in a NDPES permit. Do not discharge effluent containing this product to sewer 

systems without previously notifying the sewage treatment plant authority. For guidance, contact your 

State Water Board or Regional Office of the Environmental Protection Agency. 

DIRECTIONS FOR USE 

It is a viotation of Federat taw to use this product in a manner inconsistent with its tabeting. 

This product may only be used to formulate endwuse products with the following uses: 

(1) artichokes (globe), bananas, blackberry, broccoli, cabbage, cautiflower, cacao, citrus (non-bearing), 

ctover grown for seed, ctary sage grown for essence, coffee, conifers (seedbeds, transplants, container 

stock) and setected deciduous trees, corn, cotton, cottonwood, eucalyptus, fatlow bed (cotton/soybeans), 

faltow land, garbanzo beans, garlic, grass seeds, guava (Hawaii onty), horseradish, jojoba, mint, non-crop 

use on rights of way, nursery stock, onions, onions grown for seed, ornamentals, papayas (Hawaii onty), 

raspberry, soybeans, taro, and tree fruit, nuts and vines (which inctude almond, apple, avocado, 

beechnut, brazil nut, butternut, cashew, cheny, chestnut, chinquapin, crabapple, date, feijoa , fig, filbert, 

grapes, hickory nut, kiwi, loquat, macadamia nut, mayhaw, nectarines, olives, peach, pear, pecan, 

persimmon, pistachio, plum, pomegranates, prune, quince, walnut). 

(2) specific uses not listed on the MP labet if the formulator, user group or grower has complied with U.S. 

EPA submission requirements regarding support of such uses; and 

(3) uses for experimental purposes that are in compliance with U.S. EPA requirements. 

Each formulator is responsible for obtaining EPA registration for his own end use products. 

Willowood Oxyfluorien Technical must be melted by holding at 110°C for 48 hours. Do not heat above 

200°C (product decomposes). 

STORAGE AND DISPOSAL 

Do not contaminate water, food or feed by storage or disposal. 

PESTICIDE STORAGE: Store in original container tightly closed and in a safe place. 

PESTICIDE DISPOSAL: Wastes resulting from the use of this product must be disposed of on site or at 

an approved waste disposat facility. 

CONTAtNER HANDLING: Nonrefiltabte container. Do not reuse or refill this container. Completely (,', 

empty tiner by shaking and tapping sides and bottom to loosen clinging particles. Empty residue into' , , ' 

processing equipment. Then dispose oftiner in a sanitary landfill or by incineration if allowed by st<?t!,!(~I"j~ 

tocal authorities. Offer the drum for recycting, if available. ' 

" " , , , , 

, WARRANTY STATEMENT " " " , " " , tMPORTANT NOTtCE -Seiter warrants that this product conforms to the chemical d~scliption and is 

reasonably fit for purposes stated on the labet when used in accordance with ,tj1,e: ,clirectioi.s,~~c! 

instructions under normal conditions of use. To the extent consistent with apptical?~e; lay .. , neither ~his 

warranty nor any other warranty of merchantability or fitness for a particular purpose, express or i,mpliEld, 

extends to the use contrary to tabet instructions, or under abnormat conditions, or under conditi~JI,~ ',lJ~ 

reasonably foreseeable to seller, and buyer assumes the risk of any such use. 

Willowood Oxyfluorfen Technical Label 2 

12
! 

, 

NOTE TO FILE 

Date: September 27, 2010 

EPA File Symbol: 87283-R 

Product Name: Willowood Oxyfluorfen Technical 

Original Application Dated: January 12, 2010 

Renegotiated Date: November 2, 20 I 0 

Action Description: New Manufacturing Use Product (Oxyfluorfen) for several crop use sites 

Comments: 

PRODUCT CHEMISTRY: 

- Basic CSF dated Dec, 28, 2009 was found acceptable by TRB 

- Group A and Group B product chemistry data submitted were fOWld acceptable with the 

exception of Storage Stability and Corrosion Characteristics 

- TRB also noted an impurity of unknown toxicity in the review dated June 21, 2010 

-HED was then consulted for an impurity review and the impurity identified is not 

thought to be of toxicological concern (memo dated September 23, 2010) 

ACUTE TOXICITY REVIEW: 

Signal Word: CAUTION 

TRB found this product to be substantially similar to EPA Reg. No. 11603-29 

DATA COMPENSATION: 

Cite-all with offer to pay companies on the Data Submitter's list for Oxyfluorfen generic 

data and acute toxicity data. Product specific studies were submitted and found 

acceptable. 

LABEL REVIEW: 

revisions per the acute toxicity review 

add "(Hawaii only)" after "cacao" to match label of the cited substantially similar product 

13
#87283-R 

P.C. Codell1601 

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY 

WASHINGTON, D.C. 20460 

OFFICE OF CHEMICAL SAFETY 

AND POLLUTION PREVENTION 

TECHNICAL REVIEW BRANCH 

SIMILARITY CLINIC DETERMINATION 

MEMORANDUM 

221 APRILl2010 

Subject: 

From: 

To: 

Applicant: 

EPA Reg. No.: 87283-R Willowood Oxyfluorfen Technical 

DP Barcode: 373547 

Decision: 426039 

P.c. Code 11601 

Action Code: II 160 I 

Masih Hashim, Toxicology Team Leader fo{i~ 0 / 

Technical Review Branch ~ 0....-JL--::. 

Registration Division (7505P) 1\ ""'-- \ . V/o -1 .... l«:> 

Bethany Benbow, RM T earn 23 't - Herbicide Branch 

Registration Division (7505P) 

Willowood OxyfIuorfen, LLC 

Roseburg, OR 97470 

'L-(,.. - ~ 

FORMULATION FROM LABEL: 

Active Ingredient(s): 

OxyfIuorfen 

Inert Ingredient(s)/impurity: 

1 

Total: 

% bywt. 

98.1 

~ 

100.0 

14
#87283-R 

p.e. Code 111601 

ACTION REQUIRED; To determine if the cited and proposed products (#11603-29 and 

#87283-R) are similar. 

RECOMMENDATIONS: The cited and proposed products are substantially similar. 

The acute toxicity profile for EPA Reg. No. #87283-R is as follows: 

acute oral toxicity IV cited 44712010 

acute dermal toxicity 1lI cited 44712011 

acute inhalation toxicity IV cited 44712012 

primary eye irritation IV cited 44712013 

primary skin irritation IV cited 44712014 

dermal sensitization neg cited 44712015 

LABEL REVIEW SYSTEM 

ID #87283-1 Willowood Oxyfluorfen Technical 

SIGNAL WORD: CAUTION 

PRECAUTIONARY STATEMENTS: 

Harmful if absorbed through skin. Avoid contact with eyes, skin or clothing. 

STATEMENT OF PRACTICAL TREATMENT (SOPT): 

IF ON SKIN: Wash with plenty of soap and water. Get medical attention. 

The following statement should occur under the heading USER SAFETY 

RECOMMENDATIONS: 

Wash hands before eating, drinking, chewing gum, using tobacco 

or using the toilet. 

The Registrant has the option of using Toxicity Category III precautionary and first aid 

statements to address other exposure routes. 

2 

15
( 

PYXIS REGULATORY CONSULTING, INC. 

4110 136th St. NW 

Gig Harbor, WA 98332 

OVERNIGHT DELIVERY 

Katherine Montague (PM 23) 

Document Processing Desk (REGFEE) 

Office of Pesticide Programs (7504P) 

U.S, Environmental Protection Agency 

Room S-490D, One Potomac Yard 

2777 S. Crystal Drive 

Arlington, VA 22202 

RE: Willowood Oxyfluorfen, LLC 

January 12, 2010 

Willowood Oxyfluorfen Technical (EPA File Symbol 87283- ) 

Application for New Pesticide Registration 

Dear Ms. Montague, 

479606-00 

Phone: 253·853-7369 

Fax: 253-853-5516 

www.PyxisRC.com 

On behalf of Willowood Oxyfluorfen, LLC, we are submitting an application for registration of 

Willowood Oxyfluorfen Technical, a technical containing the active ingredient Qxyfluorfen. In support of 

this application, we submit the following documents: 

.,' ( 

1. Application for a New Pesticide Registration (EPA Form 8570-1) ,., , 

2. Confidential Statement of Formula (EPA Form 8570-4) " , 

3. Three (3) Copies of the Proposed Labeling 

4. A CD containing an electronic version of the proposed labeling 

5. Certification with Respect to Label Integrity 

6. Certification with Respect to Citation of Data (EPA Form 8570-34) 

7. Agency Internal Use Copy of the Data Matrix 

8. Public File Copy of the Data Matrix 

9. Documentation of Small Business for PRlA fee reduction 

10. Copy ofPRIA payment 

11. Letter of Authorization 

12. Product Specific Data (3 copies of each report): 

Volume 1 830.1550,830.1600, Tillman, A. M. Product Identity and Composition, Description of 

830.1620,830.1670, th, Materials Used, Description of the· Production Process, 

47960601 830.1750,830.1800 Discussion of the Fonnation of Impurities, Certified Limits, and 

Enforcement Analytical Method for Willowood Oxyfluorfen 

Technical. COlliaillS Confidential Business Information, 

16
47960602 Volume 2 830.1700,830.1800 

Volume 3 830.6302,830.6303, 

830.6304,830.6313, 

47950603 830.6314,830.7000, 

830.7050,830.7200, 

830.7300 

Volume 4 830.6313,830.6315, 

830.6316,830.6317, 

830.6319,830.6320, 

830.6321,830.7100, 

830.7220,830.7370, 47960504 

830.7520,830.7550-

7570,830.7840-

7860, 830.7950 

( 

K. Montague 

Jan. 12,2010 

Page 2 of2 

Lawrence, Q. A. Group A Product Chemistry Analysis of 

Oxyfluorfen 

Information. 

Technical. Contains COlljidellfial Business 

Lawrence, Q. A. Group B - Physical and Chemical Properties 

Testing ofOxyfluorfen Technical. 

Tillman, A. M. Willowood Oxyfluorfen Technical Waiver Request 

for Physical and Chemical Properties. 

We would like to note that Willowood Oxyfluorfen, LLC is using the cite-all within the selective method 

of support. As per EPA's interpretations of 40 CFR Parts 152.86(b)(2)(i) and 152.93(b)(2)(i), Willowood 

Oxyfluorfen, LLC submitted notices of intent to apply and offers to pay to all companies on the 

September 30, 2009 Data Submitter'S List. This action falls under PRIA category R310 (46: New 

manufacturing use product) because it is an application for registration for a technical product identical to 

a currently registered product. The fee for this action is $4,578, but Willowood Oxyfluorfen, LLC is 

requesting a 50% PRIA fee reduction to $2,289. Documentation to support eligibility as a small business 

is enclosed. The PRIA fee has been paid. The decision tirneline is 6 months. 

We trust you will find this application complete. However, please feel free to contact me «253) 853~ 

7369, Ann@PyxisRC.com) if you have any questions or need any additional information. 

Sincerely, 

Ann M. Tillman 

Enclosures 

17
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY 

WASHINGTON, D.C. 20460 

MEMORANDUM 

Date: September 23, 2010 

OFfiCE OF 

CHEMICAL SAFETY AND 

POllUTION PREVENTIDN 

Subject: Oxyfluorfen. EPA Reg. No. 87283-R. Impurities Discussion for New 

Formulation. 

PC Code: 111601 

"Decision No.: 426039 

Petition No.: N/A 

Risk Assessment Type: N/A 

TXRNo.:N/A 

MRID No.: N/A 

From: Christine Olinger, Chemist 

Risk Assessment Branch VII / 

Health Effects Division (750 P 

DP Barcode: D379653 

Registration No.: 87283-R 

Regulatory Action: New Registration 

Case No.: N/A 

CAS No.: 42874-03-3 

40 CFR: 180.381 

Through: Richard Loranger 1<, / rfUf /lA-I11!J'U 

Health Effects Qivision (7509P) L---V ~"if ' 

/ 

And 

Michael 

Risk Assessment 

S. Metzger, 

Branch 

Chief 

VII 

i/uJ {,,~~ 0 

((.. 

P 

( 

~ "'" 

Health Effects Division (750 P) 

To: Bethany BenbowlKathryn Montague 

Herbicide Branch 

Registration Division (7505P) 

I. Action Requested 

Willowwood has proposed registration of a teclmical grade (TGAI) product of oxyfluorfen that 

has a different impurity profile from the currently registered TGAI. The Registration Division 

Page I of2 

18
(RD) has requested HED comment on an impurity and its potential effects on the toxicity of the 

TGAI. 

II. HED Conclusions 

Based on a review of the toxicity data for the parent compound, and a structure activity 

relationship analysis (SAR) of the parent and the impurity, HED does not believe that the new 

TGAI would have a different toxicity profile than the currently-registered TGAI. Considering 

the level of the impurity that would be present, HED has no further concerns. A detailed 

discussion of the toxicity and analysis may be found in the Confidential Appendix to this 

memorandum. The confidential statement offormuIa should be amended to correct a 

typographical error, also noted in the confidential appendix to this review. 

Attachments: 

Confidential Appendix 

Page 2 of2 

19
Confidential Appendix to D379653 

Impurity Description 

The Registration Division inquired about one impurity in the proposed confidential statement of 

formula for EPA reg. no. 87283-R at an upper certified limit of The chemical structure of 

the parent compound and the impurity may be found in Table 1 below. 

Table 1. Oxyfluorfen Nomenclature. 

Chemical structure 

, 

fro ~ ~o w ..... , II 

( ° 

Common name Oxyfluorfen 

CAS Name 42874-03-3 

CAS registry number 2 -Chl oro-l-(3 -ethoxy -4-nitrophenoxy )-4-trifl uoromethy 1 benzene 

Impurity No.1 

Hazard Characterization 

Reference: F. Fort, DP Barcode D281831, 4/29/02 

Oxyfluorfen is of low acute toxicity and is in toxicity category IV for acute oral, dermal, and 

inhalation toxicity. It is a slight eye and dermal irritant and is not a dermal sensitizer. 

Toxicity was similar for subchronic and chronic rat, mouse, and dog studies in both sexes. 

Although oxyfluorfen inhibits heme synthesis, the resulting anemia was generally mild. A 

microcytic anemia with a decreased hematocrit, small erythrocytes, and nonnal red blood cell 

count was described in the 1997 subchronic rat study with the current 98% registration. In other 

words, the red blood cell count was nonnal in this study, but the red blood cell mass was 

decreased because of the small size of the red blood cells, presumably because of inhibition of 

the protoporphyrinogen oxidase enzyme. The anemia was generally mild in other studies, with 

varying hematologic abnonnalities described in the rat, mouse, and dog studies. 

Pagelof2 ~ 

20 *Manufacturing process information may be entitled to confidential treatment*
Confidential Appendix to D37~653 

Mild liver toxicity was observed in the 1997 subchronic rat study. Increased liver weight was 

accompanied by very slight increases in liver enzyme activities and minimal microscopic 

changes. Similar effects also occurred in the other subchronic and chronic rat, mouse, and dog 

studies. There were typically few histopathological lesions seen in the liver, although hepatocyte 

necrosis did occur in the mouse and dog studies. Renal toxicity was most severe in the 2-

generation reproduction study in rats, in which pelvic mineralization occurred. Other subchronic 

and chronic rat studies had other indications of renal toxicity, increases in organ weight and 

occasional histopathological observations. Treatment related mortality occurred in the 

subchronic mouse study, the reproduction study, and developmental studies in rats and rabbits. 

Other toxicological changes included excessive lacrimation in the chronic dog study and 

increases in urine volume and water consumption in the subchronic rat study. 

Developmental studies with the current 98% technical material found no developmental toxicity 

in rats whereas an increase in late resorptions occurred in the rabbit study (principally in 1 litter). 

All genotoxicity assays were negative, except for one Ames assay which was positive only at 

high, insoluble levels. A subsequent Ames assay with 96% material was negative. 

Oxyfluorfen is classified as a category C, possible human carcinogen based upon combined 

hepatocellular adenomas/carcinomas in the mouse carcinogenicity study. The Cancer Peer 

Review Committee recommended a linear, low dose extrapolation for human risk assessments, 

with a Q1 * of7.32 x 10.2 (mglkg/day)"l in human equivalents. 

HED Conclusions 

In review the toxicity for the impurities identified, a qualitative toxicity prediction tool (DEREK 

V. 11) was used to screen for potential hazards not included in the parent compound. As a 

positive control, the DEREK model was run for the parent oxyfluorfen. A summary of the alerts 

found for oxyfluorfen and its impurity may be found in Table 2. Based on the DEREK analysis, 

plausible carcinogenicity and hepatotoxicity alerts were reported for the parent and the impurity. 

These alerts are consistent with the effects noted in the toxicity database. Given the structural 

similarity to the parent and the relatively low amount of the impurity in the formulation, it is 

unlikely that the impurity would have an appreciable effect on the toxicity. 

YES 

Note: The registrant should amend the confidential statement of formula to correct the chemical 

name of the impurity; the chemical name for the impurity is missing a designation of the 

nitrophenoxy group. According to the discussion of the formation of impurities on page 19 of 

the product chemistry review of the technical (H. Mukhoty, D373545, 6/2111 0), the nitrophenoxy 

is 

21 *Manufacturing process information may be entitled to confidential treatment*
DATE OUT: 

SUBJECT: 

FROM: 

TO: 

( 

fEE 

211 JUNE 12010 

PRODUCT CHEMISTRY REVIEW OF MP [X 1 EP [ 1 

DP BARCODE No.: 0373545 EPA File Symbol No.: 87283-R 

PRODUCT NAME: Willowwood Oxyfluorfen Technical 

COMPANY: Willowwood Oxyfluorfen, LLC 

FOOD USE [X 1 INTEGRATED FORMULATION [Xl 

pee: 111601 Decision No. 426039 

ACTION CODE: R310 ~ ~ j 0 

() .. 0 \ '2- ~I ) Har; Mukholy • (21 \01"~ 

Product Chemistry Team • "j 

Technical Review Branch I RD (7505P) 

Bethany Benbow I Kathryn Montague, RM 23 

Herbicide Branch I RD (7505P) 

INTRODUCTION: 

The Registrant has submitted a CSF (dated 12/28/2009) for a proposed MUP, and has also proposed a product 

specific proposed label (dated 01/12/2010) for registration of the aforesaid product under EPA File symbol 

87283-R. The product chemistry data have been submitted under MRIOs: 479505-01 through -04. 

The aforesaid MUP is manufactured by Zhejiang Chemical Company in China. 

Label text indicates that this proposed MUP is intended to be formulated into end-use products with food uses. 

The applicant claims that the proposed product is substantially similar to another registered product EPA Reg. 

No. 11603-29 (Product name: Oxyfluorfen Technical). The cited product was conditionally registered on 

10/15/1999. The product chemistry data for the cited product were reviewed and were found to be acceptable 

on 04/04/2005. The product specific label was accepted on 06/28/2006. 

TRB has been requested to evaluate the product chemistry data required for the registration of the proposed 

MUP and to determine if the proposed product is substantially similar to the cited product. 

SUMMARY OF FINDINGS: 

1. The proposed MUP contains the active ingredient: Oxyfluorfen (98.1%). 

2. The overall mean of the active ingredient from the five batch analysis is 98.08 [MRID: 479505-02, Page 13]. 

3. The proposed nominal concentration of the active ingredient in the MUP is 98.1 %. The nominal 

concentration of the active ingredient matches with the label claim. This is in compliance with PR Notice 91-2. 

The certified limits of the active and inert ingredients comply with 40 CFR § 158.350 (b) (2). 

4. The CSF of the proposed MUP is filled out completely and correctly. This CSF has been reviewed by I.I.A. 

Branch on 06/21/201 O. 

1 

22
• 

DP BARCODE No.: 373545 EPA File Symbol No.: 87283~R PRODUCT NAME: Willowwood Oxyfluorfen 

Technical 

5. The product chemistry data submitted for Group A corresponding to guidelines 830.1550 (product identity and 

composition), 830.1600 (description of materials used to produce the product), 830.1620 (description of 

production process), 830.1670 (discussion of formation of impurities), 830.1750 (certified limits) satisfy the 

product chemistry data requirements of 40 CFR §158.320, 158.325, 158.330, 158.340, and 158.350 

respectively for the proposed formulation [MRID: 479505~01 [. 

6. The active ingredient and the associated impurities were quantified by GC/MS method using both the EI and 

+CI modes. NMR was used to qualify the commercial standard of oxyfluorfen used. A Karl Fischer titration was 

performed to determine the amount of water in each batch of the five batch analysis. The method validation 

was achieved by generating specificity, accuracy, linearity and precision data under the specified analytical 

conditions [MRID: 479505~02J. 

Similar analytical techniques can also be applied for Enforcement Analytical Method. 

7. The product chemistry Group A and Group B data, with the exception of one year storage stability (830.6317) 

and corrosion characteristics (830.6320) studies are satisfied [MRID: 479505~01 through ~04J. 

8. The registrant did not certify the toxicological significance of the associated impurities present in the 

proposed MUP. The proposed MUP contains a new possible isomeric associated impurity compared to the 

associated impurities contained by the cited product (see table of impurities comparison of this review in, pages 

21-22 of this review). 

CONCLUSIONS: 

1. TRB has reviewed the CSF for the proposed MUP and has found it to be acceptable. 

2. Product chemistry data requirements for Group A and Group B, with the exception of one year storage 

stability (830.6317) and corrosion characteristics (830.6320) studies are satisfied and acceptable. 

3. HED shall evaluate the toxicological significance of the new impurities present in the proposed MUP. TRB 

will make decision regarding substantial similarity following HED's decision . 

2 

23
( ( 

DP BARCODE No.: 373545 EPA File Symbol No.: 87283-R PRODUCT NAME: Willowwood Oxyfluorfen 

Technical 

PRODUCT CHEMISTRY DATA (SERIES 830 Group A) 

Group A Data Required MRID No. 

Fulfilled 

830.1550. Chemical Identity (same as in Product CSF A 479505-01 

dated 12/28/2009) 

830.1600. Beginning Materials A 479505-01 

830.1620. Production process A 479505-01 

830.1650. Formulation process N/A 

830.1670. Discussion of Impurities A 479505-01 

830.1700. Preliminary Analysis A 479505-01 

830.1750. Certified Limits (same as in Product CSF dated A 479505-01 

12128/2009) 

830.1800. Enforcement Analytical Method A 479505-01 

A = Acceptable N/A = Not applicable 

3 

24
( ( 

DP BARCODE No.: 373545 EPA File Symbol No.: 87283-R PRODUCT NAME: Willowwood Oxyfluorfen 

Technical 

Group - B 

Data Value or Qualitat. MRID No. 

Reguire Descrip. 

Q 

Fulfilled 

830.6302. Color A Light yellow 479505-03, -

04 

830.6303. Physical State A Solid Powder " 

830.6304. Odor A Odorless " 

830.6313. Stability to normal and elevated A Stable at normal & " 

temp, metals and metal ions. (requesting elevated temp. 

waiver because test substance will not be in temp. 

contact with metal & metal ions) 

830-6314. Oxidation/Reduction action- A No apparent " 

Chemical incompatibility reaction 

830.6315. Flammability N/A Solid " 

830.6316. Explodability A Not explosive " 

chemicals. 

830.6317. Storage stability G " 

830.6319. Miscibility N/A Solid " 

830.6320. Corrosion Characteristics G Not corrosive " 

830.7200. Melting point A 84.9 to 85.8 0 C " 

830.7220. Boiling point N/A " 

830.7050. UV/visible light absorption A The molar " 

absorption 

coefficient in neutral 

solution was 6164.5 

@ 54 nm, in basic 

solution was 6369.2 

@75nm & in 

aCidic solution was 

6369.2 @54 nm 

respectively. 

830.7100 Viscosity N/A " 

4 

25
( 

830.7370. Dissociation Constant A No functional group " 

to dissociate 

830.7550. Partition Coefficient A Log Kow = 4.47 " 

830.7950. Vapor Pressure A 0.0267 mPa 250 C " 

830.7840. Solubility A In water = 0.116 " 

mg/L, , In acetone = 

72.5 g/1 00 g, In 

isophoron = 61.5 

g/100 g, In 

dimethylformamide 

> 50 g/100 g 

830.7000. pH A 5.70 " 

830.7300. Density A Bulk density = " 

0.5795 g/mL 

Explanations: A = Acceptable, N/A;::; Not applicable, G = Data gap 

5 

26
( ( 

DP BARCODE No.: 373545 EPA File Symbol No.: 87283-R PRODUCT NAME: Willowwood Oxyfluorfen 

Technical 

CONFIDENTIAL APPENDIX 

Product identity & composition (830.1550) 

OPPTS GUIDELINE No. 830.1550: PRODUCT IDENTITY AND COMPOSITION 

Willowood Oxyfluorfen Technical contains 98.1% oxyfluorfen. Chemical Code 111601 (CAS No. 

42874-03-3). The CAS nomenclature is 2-chloro-l-(3-eth9xy-4-nitrophenoxy)-4-

(trifluoromethyl)benzene. The lUPAC name is 2-chloro-a,ct,ct-trifluoro-p-tolyl ~--ethoxy-4-nitrophenyl 

ether. Willowood Oxyfluorfen Technical is substantially similar to Agan Chef. Mfg., Ltd. Galigan 

Oxyfluonen Technical (EPA Reg. No. 11603-29). i 

I 

The molecular formula for oxyfluorfen is ClsHIICIF)N04 and it has a molE~culaT weight of 361.7. Its 

structural formula is shown below: 

c 

° '\ CF, 

I '\ 

NO, 

Oxyfluorfen 

Oxyfluorfen is a diphenyl ether herbicide. It is selective contact herbicide which is absorbed by the 

foliate. Oxyfluorfen inhibits photoporphyrinogen oxidase and controls annL:al broad leaved weeds and 

grasses in a wide variety of crops by pre- or post-emergence application. . 

The detailed composition of Willowood Oxyfluorfen Technical is presented on a 'Confidential Statement 

of Formula, EPA Form 8570-4, which has been removed to the Confidential Attachment at Cross 

Reference Number I. 

6 

27
Pages 28-43 - *Manufacturing process information may be entitled to confidential treatment*
Bethany, 

RE: 87283-R (Willowood Oxyfluorfen Technical) 

Ann Tillman to; Bethany Benbow 

willowood Oxyfluorfen LLC agreed to the PRIA extension. 

Ann 

Ann M. Tillman 

Pyxis Regulatory Consulting, Inc. 

4110 136th St. NW 

Gig Harbor, wA 98332 

Office: (253) 853-7369 

Fax; (253) 853-5516 

Ann@PyxisRC.com 

-----Original Message-----

06/30/2010 06:54 AM 

From: Benbow.Bethany@epamail.epa.gov (mailto:Benbow.Bethany@epamail.epa.gov] 

Sent: Tuesday, June 29, 2010 8:30 AM 

To: Ann Tillman 

Subject: 87283-R (Willowood Oxyfluorfen Technical) 

Dear Ms. Tillman, 

It has come to my attention that this proposed MUP (Willowood 

Oxyfluorfen Technical) contains a new impurity in which the 

toxicological significance is unknown. In cases such as this, the Health 

Effects Division will need to evaluate the impurity profile to 

determine if the unknowns are of toxicological concern. As such, the 

PRIA date will need to be extended to 90 days beyond the original due 

date to allow for HED's review. The new due date would be November 2, 

2010 (90 days beyond Aug. 2, 2010). Please let me know if you agree to 

this renegotiation. 

Regards, 

Bethany R. Benbow, M.S. 

Biologist 

Herbicide Branch 

Registration Division, Pesticide Programs 

office of Chemical Safety and Pollution Prevention 

u.s. Environmental Protection Agency 

office: (703) 347-8072 

44
( 

• Form Approved OMB No. 2070~060 

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY 

401 M Street, S.W. 

WASHINGTON, D.C. 20460 

PIlPOI'Wllri< RoducUon Act NotlclI: The public reporttng bl.l"d!lo for this collection of information is estimated to averoge 1.25 hours peffesponse for registraUon 

and 025 hou(1; per response for reregislfllUon 3I1d special review activitieS. induding time for reading the i-lstructions and almpteting the neoess~ry forms. Send 

commenls regarding b.mleneslimale or any other asped of this colledion oflnfolmatlon, including suggestions for reducing tie bll"den 10: Diredor, OPPE 

InfOlmation Man:gement Division (2 f37), U.S. Environmentat Prolection f./JenC)', ~Ot M St~t. S.w., Washington. DC 20400. 

Do not send lhe completed form to ttis address. 

Certification with Respect to Citation of Data 

Adplicanl'sJRegislranfs Name. Mdress, and Te1edhone Number EPA Regil;!lation Number/File Symbol 

Willowood OXyfIuorlen,llC r)o Pyxis Rll\lulatory 4 t10 t36th SI. NW Gig Harbor, WA 98332,253J:i 87283 

AdiVe Indredionifsl an&orrepresentative lest comooundfsl 

Oxyfluorlen 

,,>I, 

Genir.ll Use Pa~em'sl (list al those dalmed forthls drodud usind 40 CFR Part 1581 

TOAt 

Produd t>tIme 

Willowood Oxyfluorlen TecmtCilI 

NOTE: If your produd is a 100% re~cka!ling of another purchased EPA·registered prodtd labeled for a~ the same uses on your label. you do nOl reed to 

submitlhl!: fonn. You must submil tlla FOlmulalO(S Exemption Slatel1l!!rt1 (EPA FOIm 8570·27). 

o 

o 

t am responding to a Dala·Call·ln Notice. and ha;e induded With thi~ tOIm a list of companios senl offers otcompensation 'the Data MaLrix ~Im shoul:;! 

be used for this dUrpose). 

SEcnON t: METHOO OF OATA SUPPORrIChec.k one method onlyl 

I am using Iho dlo·ell method of support, andnewlnduded with this fOIm 

a fist of companies sent otrelS ofcompens.aUon (the Data Malti~ folm 

shoul:;! be lSed ilrthls pUIpOliel. 

t am using the seledive method of support (or rna-all oplton 

under the seieclivo methodl, and hiM! lnduck!dwith this form a 

CQmpleled lisl of data requiremenls (the Data Matrix folm musl be 

used). 

SECTION tI: GENERAL OFFER TO PAY 

\Required ifusi"ng Ihedte·ell method or when UIlIng the dte-aH optJon under the selediw method to satisfy ooe ormore data requirements] 

121 thereby offer and agree to pay compensation. to other persons. wilh regard to the approvat ot lI1is application, to the extent requ~d by FIFRA. 

SECTION til: CERTlFtCATION 

t certify that this appUcation fOf registration, this form for roregl5tralion, or thi.<! DlIla-Call·ln reSf)oose is supported by an data swmilled or cited n the 

application Iorreglstration.ihe form for reregistration, orille Dilta-Call·tn response. In addition, if the c~e-aU option ordle-all option under thc seledive IIl!lthod is 

indicated h Sedien t, this appicafion is supported by aU data In the Agen::y's files thai (1) amcem Ihe drlJderties oreffeds of this produdor an klenV;;zi (..( 

substantially similar product. or ooe ormore of the ngredicnts In this produd; and (2] is a type Of data that would be required to bc subnitted under\~~t.~ , 

requirements In elfed on the date ofapP"Olilltofthis application if the apdlicaiion sought the niHal regislratlon 01 a produd ofidentlcator slmnar compoEi~on and 

uses. i",:, 

t certify that fcreach cXdusive use study c~od in support of this registration or rnregislnltion, thai t am the original dal1l,liUl!<lIittll[ or that I haw rblained 

the written permission OfthB aiginat data subrnitterlo cit8 thBt study. : < .; , t , { , 

" ; t ' , 

t ccclify that for each study dted Vl support of this registration or reregistration that Is not anexdusive usa study, oilher«~)J(lathe origln~ data 

subm/lter; [b) thave obtained the pelmission of the onglnol data submitter to use thesludy in support otitis ~pp~Calion; (c) all pt!rlod"P\e:..gib~il)' fo'~. t. 

compensation haw oXP.l"ed forthe study; (d) the study Is In the public ~ternture: or (e) I hall\! notified In wriling the company Ihat submitted the study;lnd haw: 

offered (I) to pay compenSiltion tothe extent requircd by seetiooo 3(c)(1)(F) and/or 3{clf2I(B) ofFtFRA; and (ill to commence ncgJ(.a'.iGn"~ to delelm',ne Ih',,' 

amourt and t!lllTlS ot compeosatlon. if all)', to be paid for the use ot the study. , , ; , , ' t 

, , I oectify that in aU Instances where ano/f{!rofcompensatlon Is requroo, aJpies ofal olfers to pay compensation end elOdeJ'lCe oflhllirdi!tit'!!.'Y.l!: { { 

accordance with sections 3(c]( t)(F) and/or 3(0)(2)(8) ofFIFRA all) :lVililalte and will be submitted to the AQen:;y upon mque~. ShDukll hilt to IJ"Od;,ce sud! 

eVideoc:e to the Agency upOnrequllSl t uooerstilnd thilt the Agency may initiate actfon to der\)'. cancel orsuspood the registration ormy product In coQ'Il.:rrit'with 

FIFRA. ' , . '." 

t coJ1lfy that1ho statonwnts t havo mado on thts tom and at! atachrnonts to it arn trun, accurab, and comploto. I ackmlwtodgo that any 

knowingly fatn or mlritoadlng 'IIllI1omom may bo pmJshablo by fino or Imprisonmortl or both undor appltcllbto taw. 

Signature 

EPA FOIm 8570 34 (9-97} E!ectronlC and Papervelllions ava~able. Subm,t only Paper vers,on. 

Typed or Printed Name ~nd TrUe 

Ann M. Tillman, Agent 

45
( i ( 

Pf_6.,.. di , .IH"',.. ,,,, .. , "'~. " A //lvell. OMR N " "(l10.fV'l~ - .. • .. S·< 

United St .. lO. a Registration opp Id/lntifilr Number 

aEPA Environmental Protection Agency Amendment 

W.uhingtlln, DC 20460 Other 

Application for Pesticide ~ Section I 

,. CllmpanviProduet Number 2. EPA Product Mllnege, 3. P//lpIlS&d Clllillificililln 

87283 - A' K. Montague ~N/lr>fI o R/lstnct\KI 

4. CllmpanV/Plllduct INllm1l1 'M' Willowood Oxyfluorfen, LLClWillowood Oxyfluorfen Technical 23 

5, NIIffiO and Add/III IIf Applicllnt (Inc/lid" ZIP Cod.} 6. E)Cpedited Reveiw. In accordance with FIFRA Section 31cll3) 

Wlllowood Oxyflugrien, llC fbW). mV product is similat or IdentIcal in composi1ign and labeling 

clo Pyxls Regulatory Consulting, Inc. to: 

4110136thSI.NW 11603-29 EPA Reg. No. Gig Harbor, WA 98332 o Chllck if this f$ II mlw .ddtU$ Product Name Galigan Oxyfluorfen Technical 

Section ~ II 

0 Amendment - Explein belew. U Finol printed I~bels in rep~onse te 

Agency lottel dated 

0 Ruubmlulon In respense to Agency lettel doted 0 "Me Tee" Applicatien. 

0 Netificatien· Explein belew. 0 Othel' Explain below. 

EXplanation: US" additlenal pagelsl if necessory. IFor seetlen I end Sectlen 11.1 

This application fans under Category R310 (46: New manufacturing use product) because it is an app5cation for registration for 

a new technical product identical in composition to a currently registered p/oduct. The fee which is due is $4.578.00 but 

Wiflowood Oxyfluorfen. LLC is requesting a small business fee reduction of 50% to $2,289. The decision timeline is 6 months. 

Section - III 

1. Mltlrill! thill Product Will Be PeebOld In: 

Child·Resi'lIlnt P4e\.:eging Unit Pac\.:eg.ing Water Soluble Pec\.:eging 2. Type 01 Containar 

t?Jv .. t?Jv .. [?J V .. QM'" .f ., .f ., ., Plutic 

Glen 

II Certification must If "Yes· No. per If "Yes· No. per Pepel lined fiberboald 

Unit Packoging wgt. conteiner Pac\.:agl Wilt contalnel .t Other !Spoci/Vl «~r.'rum 

btl submitted , , , ( < < 

3. Lecetien ef Not Centente Information 4. Sizelel RatoQ Contelnor 15. Locetien of Lobel Oi,oction. , , 

11,1' U Contoiner 

~OnL.lb.1 ,«<" 

Labal 25 kg .. On La!Hlill\l.eo:omp.nyl~g prodU<l ' 

U ' < I , « , 6. Manner In Which Lebel is AHlxad te Product ~UthOglaPh Other , , , Plpel Piued . , , Stlnei lid ' , ,-, < , 

...... ""-'. 

Section ~ IV , , 

" " , 

I. Centect Point (Comp(et. ir(lms dfracrly b,/ow tor idl1nrificatien et individual to b. ccnracted, if Ilocasury, ro proctI'.J!. IN.$' appffcatid(l.J --<, 

Name Title I Telephene ",,' No.llnclude A,ea ' Code! 

Pyxis Regulatory Consulting, Inc. Agent (253)-853-7369: ' , , ~ < 

Certification 6. Dete AF,,:;,.-jen 

I cenify thet the stetements I he~ ml!de en this felm and aU ettochmentll therato ere true, Iccurate end cempletl. RICei~~, , , ' 

lec\.:no ..... ledge thllt eny \.:newlinglly fekle or miole&ding stetament may be pUNlheble by line er impriuolVTlent or (Stamped) 

beth under eppllcable law. 

2. Signetule 

~ A ,--f,o 

3. Title 

;.i\. [......7:"· Consultant 

4. TypBd Neme 5.00to 

Ann M. rmman 1/ J d-./..20JO 

. . PA Form 8610·' !R,v. 3·541 PreVieus edmen. ere ob.olete • WhIte - EPA Fa. Copy torigln.J1 Velow _ AppIk:.n1 Copv 

46
Form Approved OMB No. 2070·0060 

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY 

401 M Street, S.W. 

WASHINGTON, D.C. 20460 

Paperwork Reduction Act Notice: The public reporting burden for this collection of information is estimated to average 0.25 hours per response for registration 

activities and 0.25 hours per response for reregistration and special review activities, including time for reading the instructions and completing the necessary 

forms. Send comments regarding the burden estimate or any other aspect of this collection of information, including suggestions for reducing the burden to: 

Director, OPPE Information Management Division (2137), U.S. Environmental Protection Agency, 401 M street, S.W., Washington, DC 20460. Do not send the 

form to this address. 

DATA MATRIX 

Date Jan. 5, 2010 EPA Reg. No.lFile Symbol 87283· I Page 1 of6 

Applicant's/Registrant's Name & Address Product 

Willowood Oxyfluorfen, LLC Willowood Oxyfluorfen Technical 

8690 Lookingglass Road 

Rosebura, OR 97470 

Ingredient Oxyfluorfen (CAS No. 42874-03-3) 

Guideline Reference Number Guideline Study Name MRIO Number Submitter Status Note 

Product Specific Data Requirements 

830.1550 Product Identity and Composition Volume 1 Willowood Oxyfluorfen, LLC OWN 

830.1600 Description of Materials Used to Produce the Volume 1 Willowood Oxyfluorfen, LLC OWN 

Product 

830.1620 Description of Production Process Volume 1 Willowood Oxyfluorfen, LLC OWN 

830.1650 Description of Formulation Process Not Required1 

830.1670 Discussion of Formation of Impurities Volume 1 Willowood Oxyfluorfen, LLC OWN 

830.1700 Preliminarv Analvsis 

830.1750 Certified Limits Volume 1 Willowood Oxvfluorfen, LLC OWN 

830.1800 Enforcement Analytical Method Volume 1 Willowood Oxyfluorfen, LLC OWN 

830.6302 Color · . ,. ~""~ Volume 2 Willowood Oxyfluorfen, LLC OWN · . Physical State " . .. . 830.6303 Volume 2 Willowood Oxyfluorfen, LLC OWN ,. ,. ,. ~ 

" 

830.6304 Odor . ,. ~ ~ "" Volume 2 Willowood Oxyfluorfen, LLC OWN 

830.6313 Stability to Normal and Elevated Temperatures, Volume 2 Willowood Oxytluorfen, LLC OWN Data 

Metals and M~'i:all({~'ls ~ ~: "",, ~ " " " ',.,. .. "" ~,.~ Volume 3 Willowood Oxytluorfen, LLC OWN Waive~ " ~ . · . . .. Si9nature • • " . . . .. • . . Name and Tille Oate . . . ~,. ,. " 

rL)l<<JdL • • . Ann M. Tillman, Consultant Jan. 5,2010 

EPA Form 8570-35 (9·97) Electronic and Paper versions available. Submit only Paper version. Agency Internal Use Copy 

47
Form Approved OMB No. 2070-0060 

UNITED STATES ENVIRDNMENTAL PROTECTIDN AGENCY 

401 M Street, S.W. 

WASHINGTDN, D.C. 20460 

Paperwork Reduction Act Notice: The public reporting burden for this collection of information is estimated to average 0.25 hours per response for registration 

activities and 0.25 hours per response for reregistration and special review activities, including time for reading the instructions and completing the necessary 

forms. Send comments regarding the burden estimate or any other aspect of this collection of information, including suggestions for reducing the burden to: 

Director, OPPE Information Management Division (2137), U.S. Environmental Protection Agency, 401 M Street, S.W., Washington, DC 20460. Do not send the 

form to this address. 

DATA MATRIX 

Date Jan. 5, 2010 EPA Re . No.lFile S mbol 87283- Pa e2.of6 

Applicant's/Registrant's Name & Address Product 

Willowood Oxyfluorfen, LLC 

8690 Lookingglass Road 

Willowood Oxyfluorfen Technical 

Roseb~ OR 97470 

Ingredient Oxyfluorfen (CAS No. 42874-03-3) 

Guideline Reference Number Guideline Stu2.Y.,Name MRID Number Submitter Status Note 

830.6314 I Oxidation/Reduction: Chemical Incompatibility Volume 2 Willowood Oxyfluorfen. LLC OWN 

830.6315 I Flammability Volume 3 Willowood Oxyfluorfen, LLC OWN Waiver 

830.6316 I Explodability Volume 3 Willowood Oxyfluorfen, LLC OWN Waiver4 

830.6317 I Storage Stability PRN 92_55 

830.6319 I Miscibility Not R~!:lired6 

830.6320 I Corrosion Characteristics PRN 92-5' 

830.6321 I Dielectric Breakdown Voltaqe Not Required6 

830.7000 I pH Volume 2 Willowood Oxytluorfen, LLC OWN 

830.7050 I UVNisible Absorption Volume 2 Willowood Oxyfluorfen, LLC OWN 

830.7100 I Viscosity Not Required6 

830.7200 I Melting Point/Melting Range ~ Volume 2 Willowood Oxyfluorfen, LLC OWN 

830.7220 I Boiling Point/Boiling Rapgr::' ; ~ ~::: - Not Required7 

830.7300 I Density/Relative DensityiS-ulk b"ensity I Volume 2 I Willowood Oxyfluorfen. LLC I OWN 

I 830.7370 Dissociation ~onstants in ~ter Volume 3 Willowood Ox fluorfen. LLC OWN Waiver" 

Signature ~ ~ ~; Name and Tille Date 

;: ~ : ; Ann M. Tillman, Consultant Jan. 5, 2010 

a..1.~ -

-- - , 

EPA Fonn 8570-35 (9-97) Electronic and Paper versions available. Submil only Paper version. Agency Internal Use Copy 

48
Form Approved OMS No. 2070-0060 

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY 

401 M Street, S.W. 

WASHINGTON, D.C. 20460 

, 

I Paperwork Reduction Act Notice: The public reporting burden for this collection of information IS estimated to average 0.25 hours per response for registration 

activities and 0.25 hours per response for reregistration and special review activities, including time for reading the instructions and completing the necessary 

forms. Send comments regarding the burden estimate or any other aspect of this collection of information, including suggestions for reducing the burden to: 

Director, OPPE Information Management Division (2137), U.S. Environmental Protection Agency, 401 M Street, S.W., Washington, DC 20460. Do not send the 

form to this address. 

DATA MATRIX 

Date Jan. 5, 2010 EPA Reg. No.lFile Svmbol 87283- I Page3016 

Applicant'sfRegistrant's Name & Address Product 

Willowood Oxyfluorien, LLC Willowood Oxyfluorien Technical 

8690 Lookingglass Road 

Roseburg, OR 97470 

InQredient Oxyfluorfen (CAS No. 42874-03-3) 

Guideline Reference Number Guideline Studv Name MRIO Number Submitter Status Note 

830.7520 Particle Size, Fiber Length, and Diameter Not Required6 

Distribution 

830.7550 Partition Coefficient (n-octanol/water), Shake Volume 3 Willowood Oxyfluorfen, LLC PL 

Flask Method 

830.7560 Partition Coefficient (n-octanol/water), See 830.7550 

Generator Column Method 

830.7570 Partition Coefficient (n-octanol/water), See 830.7550 

Estimation by Liquid Chromatography 

830.7840 Water Solubility: Column Elution Method; Volume 3 Willowood Oxyfluorfen, LLC PL 

Shake Flask Method 

830.7860 Water Solubility, Generator Column Method See 830.7840 

830.7950 Vapor Pressure · . ~ ,,~~ Volume 3 Willowood Oxy~uorfen, LLC PL · ... . . . . ~ ~ ~ ~ ,. 

870.1100 Acute Oral Toxicity: Rat ~ ~.., ,,~~ Cite-All PAY 

870.1200 Acute Dermal Toxicity: Rat Cite-All PAY 

Acute Inhalati9n:;.-ro~icity: R~1 ~; ~ . "" 870.1300 • . 

. . Cite-All PAY 

· . • • • . . Signature .. . .. . . .. ~~ ~ ~ Name and Title 0,. . . .. • 

a..1,~ • .. Ann M. Tillman, Consultant Jan. 5,2010 

EPA Fonn 8570·35 (9·97) Electronic and Paper versions available. Submit only Paper version. Agency Internal Use Copy 

49
Form Approved OMS No. 2070-0060 

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY 

401 M Street, S.W. 

WASHINGTON, D.C. 20460 

Paperwork Reduction Act Notice: The public reporting burden for this collection of information is estimated to average 0.25 hours per response for registration 

activities and 0.25 hours per response for reregistration and special review activities, including time for reading the instructions and completing the necessary 

forms. Send comments regarding the burden estimate or any other aspect of this collection of information, including suggestions for reducing the burden to: 

Director, OPPE Information Management Division (2137), U.S. Environmental Protection Agency, 401 M Street, S.W., Washington, DC 20460. Do not send the 

form to this address. 

DATA MATRIX 

Date Jan. 5, 2010 EPA Reo. No.lFile Symbol 87283- I Paoe'1016 

Applicant's/Registrant's Name & Address Product 

Willowood Oxyfluorfen, LLC Willowood Oxyfluorfen Technical 

8690 Lookingglass Road 

Roseb~r~, OR 97470 

Inaredient Oxvfluorfen (CAS No. 42874-03-3) 

Guideline Reference Number Guideline Studu Name MRID Number Submitter Status Note 

870.2400 Primarv Eve Irritation: Rabbit Cite-All PAY 

870.2500 Primarv Dermal Irritation Cite-All PAY 

870.2600 Dermal Sensitization Cite-All PAY 

Oxvfluorfen Product Soecific and Generic Data ReQuirements 

Willowood Oxyfluorfen, LLC will make offers-to-pay to the following companies on the oxyfluorfen 

data submitters list of Seotember 30, 2009. 

Cite-All The Scotts Company PAY 

Ctte-AII Monsanto Company PAY 

Cite-All Chemisco PAY 

- - , ~,,~ Cite-An Aaan Chem MIa. Ltd. PAY - - --- -- 0 

- - - " 0_ Cite-All Loveland Products, Inc. PAY 

- ~ - , _ 0 Cite-AII Albauah, Inc. PAY 

Cite-All Harrell's LLC PAY --- --- o 0 0 0 · - - Dow AaroSciences LLC 0 0 0 Cite-All PAY , - - - o 0 

Signalure · - - - - 0 0 0 · - -- o _ 

- 0 Name and Tille Oale 0 -- - 0 "- , ~ 

d.-~~ 0 • 0 Ann M. Tillman, Consultant Jan. 5,2010 

EPA Form 8570-35 (9-97) ElectroniC and Paper versions available. Submit only Paper version. Agency Internal Use Copy 

50
Form Approved OMB No. 2070-0060 

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY 

401 M Street, S,W. 

WASHINGTON, D.C. 20460 

Paperwork Reduction Act Notice: The public reporting burden for this collection of information is estimated to average 0.25 hours per response for registration 

activities and 0.25 hours per response for reregistration and special review activities, including time for reading the instructions and completing the necessary 

forms. Send comments regarding the burden estimate or any other aspect of this collection of information, including suggestions for reducing the burden to: 

Director, OPPE Information Management Division (2137), U.S. Environmental Protection Agency, 401 M Street, S.W., Washington, DC 20460. Do not send the 

form to this address. 

DATA MATRIX 

Date Jan. 5, 2010 EPA Reo. No.lFile Symbol 87283- I Paoe::; 016 ~ 

~. 

Applicant'sJRegistrant's Name & Address Product 

Willowood Oxyfluorfen, LLC Willowood Oxyfluorfen Technical 

8690 Lookingglass Road 

RoseburQ, OR 97470 

Inaredient Oxvfluorfen (CAS No. 42874-03-3) 

Guideline Reference Number Guideline Study Name MRID Number Submitter Status Note 

Cite-All Makhteshim Agan of North PAY 

America, Inc. 

Cite-All Spray Drift Task Force PAY 

Cite-All Outdoor Residential Exposure PAY 

Task Force 

Cite-All Agricultural Reentry Task PAY 

Force 

Cite-All Nations Aq II, LLC PAY ~ 

Cite-All FIFRA Endangered Species PAY 

Task Force LLC 

Cite-All Residential Exposure Joint PAY - - - --~ Venture - - - --- " . - - - - " Cite-All Agricultural Handlers PAY " - " ~ - Exposure Task Force . 0_ _ _ ~ 

Cite-All Gro-Pro LLC PAY - --- _A, __ ~ 

- . - . " • Cite-All Source DynamiCS LLC PAY - .. - · - - - . .. Signature . - - - . • • • Name and Tille Dale • • -- . - .. - .. - • - - -~ ~ ~ 

4L1,~ • . Ann M. Tillman, Consultant Jan. 5, 2010 

EPA Form 8570·35 (9-97) Electronic and Paper versions available. Submit only Paper version. Agency Internal Use Copy 

51
Form Approved OMS No. 2070-0060 

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY 

401 M Street, S.W. 

WASHINGTON, D.C. 20460 

Paperwork Reduction Act Notice: The public reporting burden for this collection of information is estimated to average 0.25 hours per response for registration 

activities and 0.25 hours per response for reregistration and special review activities, including time for reading the instructions and completing the necessary 

forms. Send comments regarding the burden estimate or any other aspect of this collection of information, including suggestions for reducing the burden to: 

Director, OPPE Information Management Division (2137), U.S. Environmental Protection Agency, 401 M Street, S.W., Washington, DC 20460. Do not send the 

form to this address. 

Date Jan. 5,2010 

Applicant'slRegistrant's Name & Address 

Willowood Oxyfluorfen, LLC 

8690 Lookingglass Road 

Roseburo, OR 97470 

Inaredient Oxvfluorfen (CAS No. 42874-03-3) 

GuideGne Reference Number 

Signature 

tL~~ 

Guideline Studu Name 

o 

o 

• 

o 

•• ~ - ~,." 

"' . 

0 

0 

DATA MATRIX 

MRID Number 

Cite-All 

0'0 

• 0 

0 

• • 0 

EPA Form 8570-35 (9-97) Electronic and Paper versions available. Submit only Paper version. 

EPA Reo. No.lFile Svmbol 87283· I Pace(" 016 

Product 

Willowood Oxyfluorfen Technical 

Submitter Status Note 

Generic Endangered Species PAY 

Task Force 

Name and Title Date 

Ann M. Tillman, Consultant Jan. 5, 2010 

Agency Internal Uso Copy 

. 

-

52
( ( 

Endnotes for Data Matrix for Willowood Oxyfluorfen Technical 

1 830.1650 ~ These data are not required for the registration of a technical grade active ingredient 

product. See 830.1620 for production process information. 

2 830.6313 ~ Willowood Oxyfluorien, LLC does not package Willowood Oxyfluorien Technical in metal 

containers, nor is Willowood Oxyfluorfen Technical expected to come into contact with metals or metal 

ions during its storage or use. Therefore, a waiver from the requirement of these data is requested. 

Willowcod Oxyfluorien Technical was found to be stable at normal and elevated temperatures. 

3830.6315 _ Willowood Oxyfluorien, LLC requests a waiver from the requirement of this data requirement 

since Willowood Oxyfluorien Technical is a solid and is not expected to be flammable. Please refer to 

the Confidential Statement of Formula for Willowood Oxyfluorien Technical. 

4 830.6316 ~ Willowood Oxyfluorien, LLC requests a waiver from this data requirement because 

oxyfluorien does not have the chemical bonds or functional groups associated with explosive 

chemicals. Please refer to the Confidential Statement of Formula for Willowood Oxyfluorien Technical. 

5830.6317, 830.6320 - Per PR Notice 92-5, storage stability and corrosion characteristics data are not 

required to be submitted unless specificaJly requested by the Agency. Willowood Oxyfluorien, LLC 

agrees to conduct this study if required and requests that the study be made a condition of registration. 

s 830.6319, 830.6321, 830.7100, 830.7520 _ WiJlowood Oxyfluorien Technical is a solid and not an 

emulsifiable concentrate and is not to be diluted with petroleum solvents. Therefore, miscibility data 

are not required for this technical. Willowood Oxyfluorien Technical is not to be used around electrical 

equipment and data for dielectric breakdown constant are not required. WilJowood Oxyfluorien 

Technical is a solid and not a liquid, therefore, viscosity data are not required for this product. 

Willowood Oxyfluorien, LLC is seeking a waiver for particle size, fiber length and diameter distribution 

because Willowood Oxyfluorien Technical is not water insoluble nor is it a fibrous material. 

7 830.7220 _ Willowood Oxyfluorien Technical is a solid and boiling point data are not required for solids. 

Data for melting point are required for solids. See Guideline 830.7200. ~ e e C e e ~ < c 

8 830.7370 _ Willowood OxyfJuorien, LLC is seeking a waiver for this data requirement for V'£iJlp:«,.opd 

Oxyfluorien Technical because the product does not have any fUnctional groups that would dissociate. "e~,,~< 

c c c. , , 

" , 

, , <Ie", 

, 

e C , " 

Page 10f3 

53
PROCFlSING ELECTRONIC' l..ABELS 

(rev, 1f5{09, Ich) 

If e-Iabel submitted via XML e-submission (not on CD-ROM), you may wish to find e-Iabel in 

Documentum, save e-Iabel to "My Documents", add e-Iabel to ELL, start below at step 5. 

Initial E-Label per application (on CD-ROM with paper via ITRMD) 

1 ITRMO receives 

paper submission 

wI a-label on CD 

ij Save copy of e· 

label from ELL to 

My Documents 

,U Send annotated 

e-label to registrant 

via email 

lollo.~nd "How To Pronl"l 

:J. Tracking 

record added to 

OPPIN 

I Review label 

(01 aCCllptllblO •• kJp la .tap 201 

11 File print of 

annotated e-Jabel 

and email in jackal 

a lTRMD adds 

a-label to ELL 

in-process 

~ Add comments 

to e-Iabel 

(GaV1l; add"wi1l1 

commonls" 10 lilofWl'lll 

review 

I~ Add annotated elabel to ELL 

out-process 

4 lTRMD sends 

paper submission 

to AD/BPPDIRO 

t> Connect ELL 

record with 

OPPIN S# 

\I Print annotated elabel 

lu,a "Print with Flianamo'l 

I~ Close 

submission in 

OPPIN 

Resubmission (via ema!! to staffer or PM) 

14 Receive email 

submission wI elabel attached 

1!> Add tracking 

record to 

OPPIN 

It,; Add e-Iabel 

to ELL 

in-process 

lU Save copy of elabels (old & new) from 

ELL to My Documents 

W Compare old and 

new labels with 

Acrobat 

~11 Print e-Iabel, " Mail stamped 

stamp, write cover label & cover 

letter letter to registrant 

!u.a "Prlnl with F,lonamll") 

process - big picture 

1- create OPPIN tracking 

2- put label in ELL; link to S# 

3- save ELL label to MyDocuments 

4- compare I comment 

5- outprocess 

review 

:a File stamped 

label & cover letter 

in jacket 

out-process 

t I Connect ELL 

record with 

OPPIN S# 

(if revisions needed repeat steps 8-19) 

~~ Add cover 

letter to ELL 

!marldala!)l ~ aCCilptad 

with CIlmmontsl 

14 Close 

submission in 

OPPIN 

techniques to know 

- filename for e-Iabels 

- "print with filename" 

- compare I comment 

- printing with comments 

54
( ( 

Certification with Respect to Label Integrity 

version: 9/11/02 

I certify that the information (including, but not limited to, text, tables, and graphics) 

contained in the electronic file identified below by file name and submitted with this 

certification is the same information as that on the paper copies of these documents 

included with this submission. 

# file name 

12,2010 10)~~11:~~~~~X;~~~; 00105.Willowood Ie Technical label v1.pdf 

I certify that the statements that I have made on this form are true, accurate, and 

complete. I acknowledge that any knowingly false or misleading statements may be 

punishable by fine or imprisonment or both under applicable law. 

Signature 

Ann M. Tillman 

Consultant, Willowood Oxyfluorfen, LLC 

Jan. 12,2010 

Date 

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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY 

WASHINGTON, D.C. 20460 

January IS, 2010 

PYXIS REGULATORY CONSULTING, INC. 

WILLOWOOD OXYFLUORFEN, LLC 

4110 1136TH STREET, NW 

GIG HARBOR, WA 98332-

Report of Analysis for Compliance with PR Notice 86-5 

OFFICE OF 

PREVENTION, PESTICIDES AND 

TOXIC SUBSTANCES 

Thank you for your submittal of 12-JAN-l O. Our staff has completed a preliminary 

analysis of the material. The results are provided as follows: 

Your submittal was found to be in full compliance with the standards for submission of 

data contained in PRNotice 86-5. A copy of your bibliography is enclosed, annotated with 

Master Record ID's (MRIDs) assigned to each document submitted. Please use these numbers in 

all future references to these documents. Thank you for your cooperation. If you have any 

questions concerning this data submission, please raise them with the cognizant Product 

Manager, to whom the data have been released. 

56
PRIA 2 - 21 Day Content Screen Review Worksheet 

(EPA/OPP Use Only) 

3/23/09 

21 Day Screen Start Date: I - 1'1. -/0 / 

Experts In-Processing Signature: fYI F HAM,ri67otJ Date 1- II.{~ 10 Fee Paid: Yes_v 

Division management contacted on issues No Yes Date 

EPA Reg. Number: 6 1'2. 'i(~ - EPA Receipt Date: l-I~-IO 

1 

2 

3 

4 

5 

6 

Application Form (EPA Form 8570-1)(link to form) signed & complete 

including package type 

Confidential Statement of Formula all boxes completed, form signed, and 

a) All inerts (link to http://www.epa.gov/opprdOOI/inerts/), 

including fragrances, approved for the proposed uses (see 

Footnote A) 

Certification with Respect to Citation of Data (EPA Form 8570-34) (Link to 

form) completed and signed (N/A if 100% repack) )( 

Certificate and data matrix consistent 

If applicant is relying on data that are compensable, is the offer 

to pay statement included. (see Footnote B) 

is there a letter of Authorization for exclusive use 

completed and sigJ1ed CN/A if source is umegistered or aplllicant 

yes no 

Data Matrix (EPA Form 8570-35) (Link to fOlID) both internal and external X 

copies (PR 98-5) (Link to PR 98-5) completed and signed (N/A if 100% 

Selective Method 

b) Cite-All (Fee category experts use) 

c) Applicant owns all data (Fee category experts use) 

5 Copies of Label (link to http://www.epa.gov/oppfeadl/labeling/IrmD 

(Electronic labels on CD are encouraged and guidance is available)( link to X 

http://www.epa.gov/pesticides/regulating/registering/submissions/index.htm#labels 

I 

57
( 

7 Is the data package consistent with PR Notice 86-5 (link to PRN 86-5) A 

Notice of Filing (link to 

8 httl1://www.el1a.gov/l1esticides/regulating/toierance 12etitions.htm) included \- with petitions (link to 

http://www.epa.gov/pesticides/reouIatingltolerances.h tm) 

9 If applicable for conventional applications, reduced risk rationale (link to 

http://www.epa.gov/opprdOOl/workpJan/reducedrisk.htmI) ?( 

Required Data (link to 

httl1:i /www.el1a.govil1esticides/reguIating/data reguirements.htm) and/or 

data waivers. See Footnote C. 

a) List study (or studies) not included with application 

10 

2 

58
( 

Comments: 

IAJ/ \u..c\t.e~ U-<'(R. iD q::r-q 50_T) \"'{A\)e. 

"" 

* N/A - Not Applicable 

Footnotes 

A. During the 21 day initial content review, all CSFs will be reviewed to determine 

whether all inerts listed, including fragrances, are approved for the proposed uses. Ifan 

unapproved inert is identified, the applicant must either 1) resolve the inert issue by, for 

example, removing the inert, substituting it with an approved inert, submitting 

documentation that EPA approved the inert for the proposed pesticidal uses, correcting 

mistakes on the CSF, etc. or 2) provide the data to support OPP approval of the inert or 3) 

withdraw the application. Removing or substituting an inert ingredient will require a new 

CSF and may require submission of data. All infonnation, forms. data and 

documentation resolving-the inert issue must have been received by the Agency or the 

application withdrawn within the 21 day period. otherwise, the Agency will reject the 

application as described below. 

To successfully complete this aspect of the 21 day initial content screen, applicants are 

strongly encouraged to verify that all inert ingredients have been approved for the 

application's uses even if a prod uct is currently registered by consulting the inert Web 

3 

59
( 

site [link to http://www.epa.gov/opprdOOllinerts/lists.html] and if the inert is not 

approved, to obtain the necessary inert approval prior to submitting an application 

to register a pesticide product containing that inert ingredient. Some inert 

ingredients are no longer approved for food uses or certain types of uses. The name 

and/or CAS number on a CSF must match the name and CAS number on this web site. 

Simple typographical errors in the name or CAS number have resulted in processing 

delays. 

If an inert is not listed on the inert ingredient web site and the applicant believes that the 

inert has been approved, the applicant should contact the Inert Ingredient Assessment 

Branch (IIAB) at inertsbranch@epa.gov and resolve the issue. Gopies of the 

correspondence with lIAB resolving the issue should accompany the application. All 

new inerts except PIP inerts are reviewed by IIAB. The lIAB should also be contacted 

for any questions on what supporting data needs to be submitted for and the Agency's 

inert review process. Questions on PIP inerts should be directed to the Chief of 

Microbial Pesticides Branch [Link to 

http://www.epa.gov/oppbppdl/biopesticides/contactsbppd.htm]. 

When a brand, trade, or proprietary name of an inert ingredient is listed on a CSF, 

additional information such as an alternate name of the inert, CAS number or other 

infonnation [link to http://WVvw.epa.gov/opprdOOl/inelts/tips.pdfJ must also be included 

to enable the Agency to detennine if it has been approved. Each component of an inert 

mixture (including a fragrance) must be identified. In some cases, the suppiier of the 

mixture or fragrance may need to provide this information to the Agency. Prior to the 

Agency's receipt of an application, applicants must arrange with a proprietary mixture or 

fragrance supplier to provide the component information to the Agency or promptly upon 

EPA's request. If the inert ingredients in a proprietary blend (including :fragrances) 

cannot or are not identified or provided within the 21~day content review period, the 

Agency will reject the application. 

During the 21 day content review, applicants should submit information to the individual 

identified by the Agency when the applicant is informed of an unapproved inert. 

Unapproved Inerts Identified on CSFs 

All applications except conventional new products and PIPs 

Once an unapproved inert is identified on a CSF, the Agency will contact the 

applicant with the following options: 

1. Correct the application by, for instance, correcting the inert's identity or CAS 

number, providing documentation that the inert has been approved, or 

removing the unapproved inert from the CSF or replacing it with one that is 

approved for the application's uses; or 

2. Submit the infonnation and data needed for the Agency to approve the 

unapproved inert If this option is selected and implemented, the Agency may 

request an extension in the PRlA decision review tirnefrarne to acconunodate 

the inert review/approval process; 

4 

60
i 

, ( 

3. Withdraw the application (the Agency retains 25% of the full fee for the fee 

category estimated); or 

If none of these options is selected and implemented by the applicant within the 

21 day content review period, the Agency will reject the application and retain 

25% of the full fee of the category identified. 

C~nventional New Product Applications 

When the Registration Division identifies an unapproved inert on a CSF with an 

application for a new product that the applicant has not identified as requiring an 

inert approval (R311, R3l2 or R313), it will contact the applicant with the 

following options: 

1. Correct the application by, for instance, correcting the inert's identity or CAS 

number, providing documentation that the inert has been approved, or 

removing the unapproved inert from the CSF or replacing it with one that is 

approved for the application's uses; or 

2. Submit the infonnation and data needed for the Agency to approve the 

unapproved inert, including any required petition to establish or amend a 

tolerance or exemption from a tolerance. (This option may change the PRIA 

category for the application, which could require a longer decision review 

time and a larger fee. If additional fees are due, they must be received by the 

Agency within the 21 day content review period.) 

3. Withdraw the application (the Agency retains 25% of the full fee for the fee 

category estimated); or 

Ifnone of the above options is selected and implemented during the 21-day 

content-review period, the Agency will reject the application and retain 25% of 

the appropriate fee for the new product-inert approval category. 

PIP Applications 

"When the Biopesticide and Pollution Prevention Division identifies an 

unapproved inert on a PIP CSF and a request to approve the inert does not 

accompany the application, it will contact the applicant with the following 

options: 

I. Correct the application by, for instance, correcting the spelling or name of the 

inert to that in 40 CFR 174, or providing documentation that the inert has been 

approved; or 

2. Submit the infonnation and data needed for the Agency to approve the 

unapproved inert. If an inert ingredient tolerance exemption petition is 

required, the petition must be received by the Agency and the B903 fee paid 

within the 21 day period. If this option is selected and implemented, the 

Agency will discuss harmonizing the timeframe for both actions. 

5 

61
I 

3. Withdraw the application (the Agency retains 25% of the full fee for the fee 

category estimated); or 

lfnone of the above options is selected and implemented during the 21 day 

content review period, the Agency will reject the application and retain 25% of 

the fee. 

B. A policy on documentation of offers to pay is still being developed, however, for a 

me-too or fast track (similar/identical) new product, R300 or A530, an application 

without the necessary authorizations of offers to pay will be placed into either R301 or 

AS31. The Agency recommends that authorizations of offers to pay be submitted with 

other PRIA applicaHons to avoid delays in the Agency's decision. 

C. Biopesticide applicants are advised to contact the Agency and discuss study waivers 

prior to sUbmitting their application to the Agency. Documentation of such discussions 

should be submitted with the study waiver. 

6 

62
( ( 

UNITeD STATES ENVIRONMENTAL PROTECTluN AGENCY 

WASHINGTON, D.C. 20460 

January 13, 2010 

OPP Decision Nwnber: D-426039 

EPA File Symbol or Registration Nwnber: 87283-R 

Product Name: WILLOWWOOD OXYFLUORFEN TECHNICAL 

EPA Receipt Date: 12-Jan-2010 

EPA Company Nwnber: 87283 

Company Name: WILLOWOOD OXYFLUORFEN, LLC 

JANELLE KAY 

PYXlS REGULATORY CONSULTING, INC. 

WlLLOWOOD OXYFLUORFEN, LLC 

4110 I 136TH STREET, NW 

GIG HARBOR, WA 98332-

OffiCE OF 

PREVENTION, PESTICIDES AND 

TOXIC SUBSTANCES 

SUBJECT: Receipt of Application and 50% Small Business Waiver Request 

Dear Registrant: 

The Office of Pesticide Programs has received your application, 50% small business 

waiver request, and cerification of payment. If you submitted data with this application, the 

results of the PRN-86-5 screen will be communicated separately. During the administrative 

screen, the Office of Pesticide Programs has detennined that this Action is subject to a Pesticide 

Registration Service Fee as defined in the Pesticide Registration Improvement Act. 

The Action has been identified as Action Code: R31 0 

NEW PRODUCT;NON-F AST TRACK (INCLUDES REVIEWS OF PRODUCT 

CHEMISTRY;ACUTE TOXICITY;PUBLlC HEALTH PEST EFFICACy); 

Your request for waiver has been forvvarded for review. You will be notified in writing when a 

detennination is made regarding your request. If your waiver request is approved, the decision 

review time period will start on the date of approval. If your waiver request is denied, you will 

receive an invoice for the outstanding balance. 

If you have any questions, please contact the Pesticide Registration Service Fee 

Ombudsman at (703) 305-6249. 

Sincerely, 

Front 

~D~ End Processing Staff 

Infonnation Technology & Resources Management Division 

63
i 

IFee for Servicel {865465C-

,------------------

This package includes the following 

@ New Registration 

oAmendment 

Ii'l Stud,s? 0 Fee Waiver? 

o volpay % Reduction: __ '--------------- -------------------------------------------------------------- -----

for Division 

OAD 

OBPPD 

@RD 

Risk Mgr. 

Receipt No. s-I 865465 

EPA File Symbol/Reg. No. 1 87283-R 

Pin-Punch Date: 1 1/12/2010 

_-' This item is NOT subject to FFS action. 

-- ------- -- j 

--------- -------- ------------- ----------------------- -------------------

Requested: I ~31D 

Granted: I IZ3lo 

Amount Due: $ 4,51C6 

Parent/Child Decisions: 

D Inert Cleared for Intended Use 0 Uncleared Inert in Product 

Reviewer: 

Remarks: 

~~ Date: 'U2 Iro 

/ I 

64
alliable; r.' Yes r No 

2-Jan-2010 

Tracking 

I 

I 

View/Edit 

65
FEE FOR SERVICE 

66
( 

Mike Kellogg 

From: 

Sent: 

To: 

paygovadmin@maiLdoc.twai.gov 

Monday, January 11, 2010 1:22 PM 

Mike Kellogg 

Subject: Pay.Gov Payment Confirmation 

THIS IS AN AUTOMATED MESSAGE. PLEASE DO NOT REPLY. 

Your transaction has been successfully completed. 

Transaction Summary 

Application Name: PRIA Service Fees 

Pay.gov Tracking ID: 2507TF3J 

Agency Tracking 10: 74896491636 

Account Holder Name: Brian Heinze 

Transaction Type: Sale 

Transaction Amount: $2)289.80 

Billing Address: 8698 Lookingglass Road 

City: Roseburg 

State/Province: DR 

Zip/Postal Code: 97471 

Country: USA 

Card Type: Master Card 

Card Number: ************6885 

Transaction Date: Jan 11) 2810 4:22:08 PM 

Decision Number: 

Registration Number: 87283-xx 

Company Name: Willowood Oxyfluorfen) LL 

Company Number: 87283 

Action Code: R310 

1 

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/ld4y(.. ~ i""P"",,'/IGO ~ )J U -1').1//7) 199&-366-620120414 

68

*Confidential Statement of Formula may be entitled to confidential treatment*