# NOTICE This technical report does not necessarily represent final EPA decisions or positions. It is intended to present technical analysis of issues using data that are currently available. The purpose in the release of such reports is to facilitate the exchange of technical information and to inform the public of technical developments. 

# Assessment and Standards Division Office of Transportation and Air Quality U.S. Environmental Protection Agency National Renewable Energy Laboratory U.S. Department of Energy Coordinating Research Council 

# EPAct/V2/E-89: Assessing the Effect of Five Gasoline Properties on Exhaust Emissions from Light-Duty Vehicles Certified to Tier 2 Standards Final Report on Program Design and Data Collection Appendix E Spreadsheets of Detailed Round Robin Fuel Inspection Data

EPA-420-R-13-004 April 2013

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :1 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60oF g/cm3 D4052 0.72080.7212 - 0.72130.7211 - - - - - - - - - 0.7211 API Gravity, 60oF oAPI D4052 64.6 64.5 - 64.5 64.6 - - - - - - - - - 64.6 Ethanol vol. % D5599 - - 11.46 10.21 - 

### - - 9.59 

### - - - 10.13 10.09 10.14 10.03 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.10 - - <0.10 Distillation IBP oF 92.6 91.9 - - - 93.0 - - 93.0 92.3 94.6 - - 93.8 92.9

5% evapoF 112.0 112.7 - - - 111.6 - - 111.9 112.4 113.6 - - 112.5 112.5 10% evapoF 117.2 117.6 - - - 116.7 - - 116.7117.1 118.0 - - 117.2 117.3 20% evapoF 124.0124.1 - - - 120.0 - - 123.4124.0 124.1 - - 123.9 123.9 30% evapoF 130.8 131.6 - - - 130.9 - - 130.8 131.3 131.5 - - 130.9 131.2 40% evapoF 139.9 140.1 - - - 139.5 - - 139.5 139.8 140.0 - - 139.5 139.9 50% evapoF 148.8 149.4 - - - 148.7 - - 148.1 149.3 149.1 - - 148.6 148.9 60% evapoF 172.0 171.2 - - - 170.5 - - 171.8 173.9 172.7 - - 177.3 172.3 70% evapoF 223.9223.3 - - - 223.9 - - 224.2225.0224.3 - - 225.7224.1 80% evapoF 254.7253.1 - - - 252.8 - - 254.5255.5255.2 - - 256.0254.6 90% evapoF 300.0300.7 - - - 298.5 - - 299.6300.3300.5 - - 302.5300.2 95% evapoF 334.2334.6 - - - 333.6 - - 334.1 334.6335.1 - - 338.0334.5 FBPoF 367.8368.0 - - - 366.3 - - 366.3365.1 372.6 - - 367.7368.0 Recovery vol. % 98.4 98.2 - - - 98.5 - - 97.8 98.5 98.4 - - 98.4 98.4 Residue vol. % 1.0 1.1 - - - 1.0 - - 1.1 1.0 1.0 - - 1.1 1.0 Loss vol. % 0.6 0.7 - - - 0.5 - - 1.1 0.5 0.6 - - 0.5 0.6 Corrected Recovery vol. % 98.4 98.2 - - - - - - - 98.5 98.4 - - - 98.4 Corrected Loss vol. % 0.6 0.7 - - - - - - - 0.5 0.6 - - - 0.6 DVPE (EPA equation) psi D5191 10.11 10.16 10.02 10.11 9.28 10.09 - 10.00 - - 10.05 9.88 - 10.05 10.07 Aromatics vol. % D1319 - 15.8 - 15.0 15.4 16.2 - 15.8 - - - - 14.2 15.5 15.4 Olefins vol. % D1319 - 8.5 - 7.7 8.0 7.2 - 6.5 - - - - 7.7 7.5 7.6 Saturates vol. % * - - - - - - - - - - - - - - 67.0 Benzene vol. % D3606 - - - 0.64 - - - 0.59 - - - 0.62 0.56 0.71 0.62 S mg/kg D5453 29 33 28 28 - - - 32 - - - - - 30 30 RON - D2699 94.7 - 94.9 - - - - 94.8 - - - - - 94.9 94.8 MON - D2700 85.4 - 85.8 - - - - 87.3 - - - - - 86.7 86.3 (RON+MON)/2 - - 90.1 - 90.4 - - - - 91.1 - - - - - 90.8 90.6 C mass %D5291 mod.**82.40 - - - 80.50 - - - - - - - 81.7282.1681.70 H mass %D5291 mod.**14.01 - - - 14.12 - - - - - - - 14.36 13.60 14.02 O mass % D5599 - - 4.4 3.9 - - - 3.7 - - - 3.9 3.9 3.9 3.9 Net Heat of Combustion MJ/kg D4809 42.042 - - - - - - 41.848 - - - - - 41.95841.950 Water mass % E-1064 - - - - - - - 0.052 - - - 0.089 - - 0.0705 Lead g/l D3237 - - - - - - - - - - - - - - - Copper Strip Corrosion - D130 - - - - - - - 1A - - - - - - 1A Solvent Washed Gum Content mg/100ml D381 - - - - - - - <0.5 - - - - - - <0.5 Oxidation Stability min. D525 - - - - - - - >240 - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 (**OptiDist** or equivalent) **PROPERTY UNIT**  **Laboratory Average**  **TEST METHOD** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :2 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60o

### F g/cm3 

### D4052 0.72170.7221 - 0.72220.7221 - - - - - - - - - 0.7220 API Gravity, 60 o

### F o

### API D4052 64.3 64.3 - 64.2 64.3 - - - - - - - - - 64.3 Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.10<0.05<0.10<0.10 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.10 - <0.10<0.10 Distillation IBP oF 75.6 80.0 91.6 86.1 85.3 79.3 82 - - 80.9 85.4 85.8 87.4 83 83.5

5% evapoF 106.2 106.0 112.1 104.6 103.1 99.2 97 - - 104.8 105.5 106.1 115.6 105 105.4 10% evapoF 122.5 122.4126.3119.4120.2116.4 117 - - 121.5 121.3122.0 130.8 121 121.7 20% evapoF 156.4155.9 156.9 151.0 151.5150.9 152 - - 154.7153.0 153.9 163.0 153 154.4 30% evapoF 192.2 192.1 191.3188.0 187.5189.0 190 - - 191.1 189.3189.9 197.2 190 190.6 40% evapoF 218.9219.6219.0216.9216.7217.8 218 - - 218.8217.7217.9222.2 218 218.5 50% evapoF 237.0237.6237.7235.1 235.2236.6 237 - - 236.9236.4236.0238.9 236 236.7 60% evapoF 252.6253.2253.2254.5250.0251.8 253 - - 252.5252.0251.8257.0 251 252.7 70% evapoF 271.4271.9272.7270.4270.1 271.0 271 - - 271.7271.4271.2275.8 272 271.7 80% evapoF 305.8305.7305.6304.0305.1 304.6 306 - - 304.7305.4305.0313.4 305 305.9 90% evapoF 340.0340.7341.2339.7339.4337.5 342 - - 337.2337.4340.6344.0 341 340.1 95% evapoF 351.8352.5353.8351.6352.2351.0 356 - - 351.1 350.9352.1 359.5 353 353.0 FBPoF 374.7376.3376.3370.0375.8375.2 373 - - 371.3377.8380.8377.9 375 375.3 Recovery vol. % 97.9 97.1 97.5 97 96.2 97.3 97 - - 97.1 96.5 97.1 97.4 96.8 97.2 Residue vol. % 1.1 1.1 1.0 0.5 1.3 1.1 1.2 - - 1.1 1.0 0.9 1.2 0.9 1.0 Loss vol. % 1.0 1.8 1.3 2.5 2.6 1.6 1.8 - - 1.8 2.5 2.0 1.4 2.3 1.8 Corrected Recovery vol. % 98 97.2 97.7 97.7 - - - - - 97.1 97.2 97.5 97.3 - 97.5 Corrected Loss vol. % 0.9 1.7 1.5 1.8 - - - - - 1.8 1.8 1.6 1.5 - 1.6 DVPE (EPA equation) psi D5191 10.1410.28 10.01 10.30 9.43 10.08 10.25 - - - 10.20 10.14 - 10.38 10.20 Aromatics vol. % D1319 - 13.8 - 13.7 14.1 14.2 14.1 - - - - - 14.4 14.1 14.1 Olefins vol. % D1319 - 7.2 - 6.8 7.8 6.3 5.7 - - - - - 6.9 7.2 6.8 Saturates vol. % * - - - - - - - - - - - - - - 79.1 Benzene vol. % D3606 - - - 0.55 - - 0.46 - - - - 0.52 - 0.50 0.51 S mg/kg D5453 22 26 22 22 - - 25 - - - - - - 23 23 RON - D2699 96.0 - 96.2 - - - 96.1 - - - - - - 95.7 96.0 MON - D2700 88.3 - 88.7 - - - 88.4 - - - - - - 89.1 88.6 (RON+MON)/2 - - 92.2 - 92.5 - - - 92.3 - - - - - - 92.4 92.3 C mass %D5291 mod.**84.88 - - - 84.77 - - - - - - - 85.4485.3985.12 H mass %D5291 mod.**14.22 - - - 14.63 - - - - - - - 14.61 14.25 14.43 O mass % D5599 - - - - - 

### - <0.1 

### - - - - <0.1 <0.01 - <0.1 Net Heat of Combustion MJ/kg D4809 44.320 - - - - - 43.600 - - - - - - 43.96043.960 Water mass % E-1064 - - - - - - 0.005 - - - - 0.014 - - 0.0095 Lead g/l D3237 - - - - - - <0.001 - - - - - - - <0.001 Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - <0.5 - - - - - - - <0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :3 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60oF g/cm3 D4052 0.73470.7351 - 0.73500.7350 - - - - - - - - - 0.7350 API Gravity, 60oF oAPI D4052 60.8 60.8 - 60.8 60.8 - - - - - - - - - 60.8 Ethanol vol. % D5599 - - 11.4410.47 - 

### - 10.15 - 

### - - - 10.3810.3610.42 10.36 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 - 

### - - - <0.10 - - <0.10 Distillation IBP oF 104.6104.6 - - - 106.7 - - - 107.4 105.9 - - 109.2 106.4

5% evapoF 135.5 136.3 - - - 135.6 - - - 135.6 136.2 - - 137.0136.0 10% evapoF 141.6141.6 - - - 141.4 - - - 141.6 141.4 - - 142.3141.7 20% evapoF 149.1 149.4 - - - 148.7 - - - 148.9 148.6 - - 148.6148.9 30% evapoF 155.3155.3 - - - 154.7 - - - 154.8 154.9 - - 155.1 155.0 40% evapoF 174.5 174.3 - - - 174.8 - - - 175.3 171.8 - - 180.1 175.1 50% evapoF 217.4218.5 - - - 216.8 - - - 217.3216.8 - - 218.3217.5 60% evapoF 231.7230.9 - - - 231.1 - - - 231.1 231.5 - - 224.6230.2 70% evapoF 243.5244.9 - - - 242.9 - - - 242.1 243.3 - - 244.6243.6 80% evapoF 258.1 259.6 - - - 247.7 - - - 259.4257.1 - - 260.4257.1 90% evapoF 295.5295.7 - - - 293.7 - - - 296.8293.2 - - 300.3295.9 95% evapoF 334.4332.9 - - - 332.7 - - - 334.1 332.0 - - 340.2334.4 FBPoF 372.2370.2 - - - 366.4 - - - 368.5364.5 - - 371.8368.9 Recovery vol. % 98.6 98.6 - - - 98.9 - - - 98.4 98.0 - - 98.2 98.4 Residue vol. % 1.0 1.0 - - - 1.0 - - - 1.1 1.0 - - 1.0 1.0 Loss vol. % 0.4 0.4 - - - 0.1 - - - 0.5 1.0 - - 0.8 0.6 Corrected Recovery vol. % 98.6 98.6 - - - - - - - 98.4 98.1 - - - 98.4 Corrected Loss vol. % 0.4 0.4 - - - - - - - 0.5 0.9 - - - 0.6 DVPE (EPA equation) psi D5191 6.99 7.04 6.85 7.04 6.33 - 6.89 - - - 6.99 6.88 - 6.78 6.93 Aromatics vol. % D1319 - 15.1 - 14.6 14.3 15.7 - 14.6 - - - - 15.0 15.9 15.0 Olefins vol. % D1319 - 8.1 - 7.5 7.5 7.8 - 6.8 - - - - 8.0 7.3 7.6 Saturates vol. % * - - - - - - - - - - - - - - 67.0 Benzene vol. % D3606 - - - 0.58 - - 0.54 - - - - 0.57 0.63 0.75 0.61 S mg/kg D5453 20 23 19 21 - - 23 - - - - - - 26 22 RON - D2699 98.1 - 98.3 - - - 97.7 - - - - - - 97.8 98.0 MON - D2700 87.6 - 88.2 - - - 86.9 - - - - - - 87.6 87.6 (RON+MON)/2 - - 92.9 - 93.3 - - - 92.3 - - - - - - 92.7 92.8 C mass %D5291 mod.**81.69 - - - 80.50 - - - - - - - 81.8082.4481.61 H mass %D5291 mod.**14.13 - - - 14.12 - - - - - - - 14.39 14.0414.17 O mass % D5599 - - 4.3 3.9 - 

### - 3.8 - 

### - - - 3.9 3.9 3.9 3.9 Net Heat of Combustion MJ/kg D4809 41.996 - - - - - 40.860 - - - - - - 41.75041.536 Water mass % E-1064 - - - - - - 0.051 - - - - 0.067 - - 0.059 Lead g/l D3237 - - - - - - - - - - - - - - - Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - <0.5 - - - - - - - <0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 (**OptiDist** or equivalent) **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :4 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60oF g/cm3 D4052 0.73430.7349 - 0.73470.7346 - - - - - - - - - 0.7346 API Gravity, 60oF oAPI D4052 60.9 60.8 - 60.9 60.9 - - - - - - - - - 60.9 Ethanol vol. % D5599 - - 10.74 9.96 - 

### - - - 10.02 

### - - 10.05 9.85 9.83 9.94 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - 

### - - <0.10 0.06 - <0.10 Distillation IBP oF 87.9 90.8 - - - 90.7 - - 87.8 89.3 91.7 - - 90.8 89.9

5% evapoF 114.8115.2 - - - 112.8 - - 118.6114.5 117.4 - - 118.0115.9 10% evapoF 125.4126.1 - - - 124.0 - - 127.9 125.2 128.1 - - 127.1 126.3 20% evapoF 140.6140.8 - - - 139.0 - - 141.9 140.3 142.3 - - 141.3140.9 30% evapoF 151.7151.8 - - - 150.6 - - 152.4151.2 152.4 - - 152.1 151.7 40% evapoF 158.9 162.3 - - - 157.8 - - 162.9 160.7 160.4 - - 165.1 161.2 50% evapoF 220.2220.5 - - - 218.6 - - 225.1 220.9224.2 - - 223.8221.9 60% evapoF 245.1 246.2 - - - 239.2 - - 248.2246.5248.0 - - 247.9245.9 70% evapoF 269.5270.1 - - - 266.5 - - 272.4269.0269.9 - - 272.3270.0 80% evapoF 302.2302.3 - - - 301.8 - - 308.3300.8302.5 - - 306.6303.5 90% evapoF 336.5335.7 - - - 336.2 - - 340.5336.5337.3 - - 339.8337.5 95% evapoF 350.6351.0 - - - 350.4 - - 355.2350.3350.7 - - 355.7352.0 FBPoF 370.5370.8 - - - 368.8 - - 368.7368.0371.1 - - 370.7369.8 Recovery vol. % 97.5 97.3 - - - 97.0 - - 97.3 97.5 97.2 - - 97.5 97.4 Residue vol. % 1.1 1.1 - - - 1.1 - - 1.1 1.1 1.1 - - 1.0 1.1 Loss vol. % 1.4 1.6 - - - 1.9 - - 1.6 1.4 1.7 - - 1.5 1.5 Corrected Recovery vol. % 97.7 97.3 - - - - - - - 97.4 97.5 - - - 97.5 Corrected Loss vol. % 1.2 1.6 - - - - - - - 1.5 1.4 - - - 1.4 DVPE (EPA equation) psi D5191 10.0310.11 9.70 10.11 9.28 10.0310.10 - 10.05 - 9.32 9.93 - 10.0010.01 Aromatics vol. % D1319 - 15.7 - 15.7 15.6 16.0 - - 15.1 - - - 14.7 15.6 15.5 Olefins vol. % D1319 - 7.4 - 6.4 8.0 6.1 - - 6.1 - - - 6.7 6.9 6.8 Saturates vol. % * - - - - - - - - - - - - - - 67.8 Benzene vol. % D3606 - - - 0.54 - - - - 0.51 - - 0.52 0.57 0.57 0.54 S mg/kg D5453 20 24 19 20 - - - - 30 - - - - 21 21 RON - D2699 96.9 - 97.3 - - - 97.2 - - - - - - 97.1 97.1 MON - D2700 87.0 - 87.8 - - - 87.5 - - - - - - 87.9 87.6 (RON+MON)/2 - - 92.0 - 92.6 - - - 92.4 - - - - - - 92.5 92.4 C mass %D5291 mod.**82.18 - - - 81.35 - - - - - - - 82.21 82.2382.21 H mass %D5291 mod.**14.18 - - - 14.11 - - - - - - - 14.2713.9014.12 O mass % D5599 - - 4.0 3.7 - - - - 3.8 - - 3.8 3.7 3.7 3.7 Net Heat of Combustion MJ/kg D4809 42.256 - - - - - 41.678 - - - - - - 41.92441.952 Water mass % E-1064 - - - - - - - - 0.063 - - 0.090 - - 0.077 Lead g/l D3237 - - - - - - - - - - - - - - - Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - 1.5 - - - - - - - 1.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 (**OptiDist** or equivalent) **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :5 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60oF g/cm3 D4052 0.75710.7575 - 0.75740.7573 - - - - - - - - - 0.7573 API Gravity, 60oF oAPI D4052 55.2 55.1 - 55.1 55.2 - - - - - - - - - 55.2 Ethanol vol. % D5599 - - - - - 

### - <0.10 

### - - - - <0.10<0.05<0.10<0.10 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.10 - - <0.10 Distillation IBP oF 91.3 92.6 100.4 93.9 99.7 93.5 - - 89.9 92.0 92.3 95.1 94.8 94 94.1

5% evapoF 127.2 129.8134.6122.4127.6126.7 - - 125.3129.2 131.2 128.7135.3 125 128.6 10% evapoF 144.7146.8149.4140.1 145.2 143.5 - - 142.4145.9 147.4145.5 150.5 143 145.4 20% evapoF 172.8174.3175.1 168.2 171.9 170.3 - - 170.4173.9 174.2 172.7176.4 171 172.6 30% evapoF 199.9200.9200.1 196.6198.3198.2 - - 197.7200.5200.8199.6202.3 198 199.4 40% evapoF 222.0223.6222.3221.6 221 221.2 - - 220.3223.4222.5222.7223.3 221 222.1 50% evapoF 237.0238.0237.2237.0236.1 236.4 - - 235.4237.7237.2237.8237.9 236 237.0 60% evapoF 247.6248.2248.0241.1 246.9247.2 - - 247.2248.2247.9247.8248.1 248 247.2 70% evapoF 258.6258.6258.3258.5257.5258.0 - - 257.8258.5258.4258.5258.7 260 258.5 80% evapoF 273.3273.8273.6272.6272.1 272.3 - - 271.8273.3273.1 273.2274.0 274 273.1 90% evapoF 300.9300.6301.1 298.0298.8298.1 - - 299.7300.7300.4299.7300.6 301 300.0 95% evapoF 324.3323.4325.2320.5321.6323.1 - - 322.0325.5323.8323.8324.5 324 323.5 FBPoF 357.2358.9356.4351.3358.7356.6 - - 354.3363.5360.5358.2358.5 360 357.8 Recovery vol. % 98.0 98.0 98.8 97.2 98 98.1 - - 98.5 98.4 98.3 98.1 98.7 97.3 98.2 Residue vol. % 1.0 1.0 0.8 0.6 1.1 1.0 - - 1.0 1.0 1.0 0.8 1.0 1.0 0.9 Loss vol. % 1.0 1.0 0.4 2.2 0.9 0.9 - - 0.5 0.6 0.7 1.1 0.3 1.7 0.9 Corrected Recovery vol. % 98.1 98.0 98.8 97.8 - - - - - 98.4 98.3 98.3 98.7 - 98.3 Corrected Loss vol. % 0.9 1.0 0.4 1.6 - - - - - 0.6 0.7 0.9 0.3 - 0.8 DVPE (EPA equation) psi D5191 6.98 7.04 6.90 7.01 6.34 6.89 7.05 - - - 6.99 6.85 - 6.86 6.95 Aromatics vol. % D1319 - 35.2 - 35.6 33.4 34.8 - 34.0 - - - - 34.3 35.8 34.7 Olefins vol. % D1319 - 7.4 - 6.2 7.3 7.1 - 5.7 - - - - 7.5 7.0 6.9 Saturates vol. % * - - - - - - - - - - - - - - 58.4 Benzene vol. % D3606 - - - 0.55 - - 0.48 - - - - 0.52 - 0.49 0.51 S mg/kg D5453 22 27 22 24 - - 26 - - - - - - 25 24 RON - D2699 96.6 - 96.6 - - - 97.2 - - - - - - 96.2 96.7 MON - D2700 86.2 - 86.6 - - - 86.1 - - - - - - 86.4 86.3 (RON+MON)/2 - - 91.4 - 91.6 - - - 91.7 - - - - - - 91.3 91.5 C mass %D5291 mod.**86.25 - - - 86.08 - - - - - - - 86.9986.9886.58 H mass %D5291 mod.**12.70 - - - 12.92 - - - - - - - 13.02 13.0412.92 O mass % D5599 - - - - - - <0.1 - - - - <0.1 <0.01 - <0.1 Net Heat of Combustion MJ/kg D4809 43.260 - - - - - 42.672 - - - - - - 42.91442.948 Water mass % E-1064 - - - - - - 0.004 - - - - 0.024 - - 0.014 Lead g/l D3237 - - - - - - <0.003 - - - - - - - <0.003 Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - <0.5 - - - - - - - <0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :6 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60oF g/cm3 D4052 0.73400.7343 - 0.73420.7341 - - - - - - - - - 0.7342 API Gravity, 60oF oAPI D4052 61.0 61.0 - 61.1 61.1 - - - - - - - - - 61.1 Ethanol vol. % D5599 - - 11.7410.66 - 

### - 9.97 

### - - - - 10.5810.4410.55 10.56 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - 0.01 

### - - - - <0.10 0.06 - <0.10 Distillation IBP oF 105.6106.3 - - - 106.1 - - 106.4106.9 106.6 - - 108.8106.7

5% evapoF 129.8130.7 - - - 129.3 - - 130.7130.7 129.5 - - 131.9 130.4 10% evapoF 135.8136.3 - - - 135.0 - - 135.7136.4 135.4 - - 136.7135.9 20% evapoF 142.7143.0 - - - 141.9 - - 142.4143.1 142.3 - - 143.1 142.6 30% evapoF 148.4148.7 - - - 147.5 - - 147.9 148.8 147.9 - - 148.6148.3 40% evapoF 153.9 153.4 - - - 152.7 - - 153.0154.2 152.6 - - 154.1 153.4 50% evapoF 186.7187.9 - - - 185.6 - - 189.4189.3 185.1 - - 195.7188.5 60% evapoF 227.4228.0 - - - 225.3 - - 230.3229.1 226.7 - - 230.8228.2 70% evapoF 265.6266.9 - - - 264.8 - - 270.7266.9265.3 - - 273.7267.7 80% evapoF 308.8309.6 - - - 306.8 - - 313.2310.2307.3 - - 314.9310.1 90% evapoF 340.1 340.1 - - - 338.7 - - 342.2340.5336.9 - - 344.3340.4 95% evapoF 351.5351.4 - - - 350.6 - - 354.5352.2350.5 - - 358.0352.7 FBPoF 370.8371.3 - - - 367.4 - - 370.1 363.8371.2 - - 369.9369.2 Recovery vol. % 98 97.7 - - - 98.3 - - 97.6 98.0 97.5 - - 97.1 97.8 Residue vol. % 1.0 1.0 - - - 1.0 - - 1.0 1.0 1.0 - - 1.1 1.0 Loss vol. % 1.0 1.3 - - - 0.7 - - 1.4 1.0 1.5 - - 1.8 1.2 Corrected Recovery vol. % 98.1 97.7 - - - - - - - 98.0 97.7 - - - 97.9 Corrected Loss vol. % 0.9 1.3 - - - - - - - 1.0 1.3 - - - 1.1 DVPE (EPA equation) psi D5191 7.28 7.22 7.19 7.29 6.56 7.27 7.35 - - - 7.14 7.25 - 7.19 7.24 Aromatics vol. % D1319 - 15.1 - 14.7 15.3 - - 15.1 - - - - 14.4 15.4 15.0 Olefins vol. % D1319 - 9.6 - 8.9 8.4 - - 8.1 - - - - 8.8 9.0 8.8 Saturates vol. % * - - - - - - - - - - - - - - 65.6 Benzene vol. % D3606 - - - 0.66 - - 0.61 - - - - 0.64 0.69 0.82 0.68 S mg/kg D5453 23 28 23 24 - - 22 - - - - - - 22 23 RON - D2699 96.3 - 96.5 - - - 95.8 - - - - - - 96.4 96.3 MON - D2700 86.5 - 87.4 - - - 85.6 - - - - - - 86.9 86.6 (RON+MON)/2 - - 91.4 - 92.0 - - - 90.7 - - - - - - 91.7 91.5 C mass %D5291 mod.**81.95 - - - 81.00 - - - - - - - 81.7281.4281.52 H mass %D5291 mod.**14.14 - - - 14.13 - - - - - - - 14.3014.2614.21 O mass % D5599 - - 4.4 4.0 - - 3.8 - - - - 4.0 3.9 4.0 4.0 Net Heat of Combustion MJ/kg D4809 41.980 - - - - - 41.752 - - - - - - 41.62441.785 Water mass % E-1064 - - - - - - 0.058 - - - - 0.087 - - 0.073 Lead g/l D3237 - - - - - - - - - - - - - - - Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - <0.5 - - - - - - - <0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 (**OptiDist** or equivalent) **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :7 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60oF g/cm3 D4052 0.72060.7209 - 0.72080.7208 - - - - - - - - - 0.7208 API Gravity, 60oF oAPI D4052 64.6 64.6 - 64.6 64.6 - - - - - - - - - 64.6 Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.10<0.05<0.10<0.10 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.10 - - <0.10 Distillation IBP oF 96.2 100.7102.7100.2 - 97.5 100 - - 101.4 101.3100.4100.4 100 100.1

5% evapoF 126.9 129.0130.5 122.1 - 124.3 125 - - 128.1 130.2 128.0131.7 128 127.6 10% evapoF 136.1 138.1 138.6133.4 - 134.9 136 - - 136.9 138.6137.1 139.8 137 137.0 20% evapoF 148.7149.3149.9 146.2 - 147.8 148 - - 149.4 150.4149.2 151.1 149 149.0 30% evapoF 161.5 161.8162.5 159.2 - 160.2 161 - - 162.1 163.2 162.3163.7 161 161.7 40% evapoF 176.5 176.8176.7174.4 - 175.6 176 - - 177.1 177.6176.8178.4 177 176.6 50% evapoF 192.9 193.5 193.5 191.7 - 192.3 192 - - 193.3 193.9 193.4194.7 193 193.1 60% evapoF 209.8210.9210.4208.9 - 209.9 209 - - 210.7211.1 210 211.5 210 210.2 70% evapoF 227.8229.7228.7227.3 - 228.6 228 - - 228.7229.5228.6229.2 229 228.6 80% evapoF 248.8252.5251.8249.6 - 250.8 251 - - 252.1 253.0251.6252.9 252 251.5 90% evapoF 296.9298.8299.7293.5 - 299.8 298 - - 299.4302.0297.2300.3 297 298.4 95% evapoF 327.3329.9331.3326.8 - 328.7 329 - - 329.2330.1 329.4331.6 329 329.3 FBPoF 357.0360.4359.4355.4 - 365.5 360 - - 358.3382.5359.6362.8 359 361.8 Recovery vol. % 98.3 97.7 98.7 96.6 - 97.5 98.5 - - 98.4 98.4 97.7 98.6 97.9 98.1 Residue vol. % 1.0 1.1 0.8 0.6 - 1.1 1.0 - - 1.0 1.0 1.1 1.1 0.8 1.0 Loss vol. % 0.7 1.2 0.5 2.8 - 1.4 0.5 - - 0.6 0.6 1.2 0.3 1.3 1.0 Corrected Recovery vol. % 98.4 97.8 98.7 97.4 - - - - - 98.4 98.4 97.9 98.6 - 98.2 Corrected Loss vol. % 0.6 1.1 0.5 2.0 - - - - - 0.6 0.6 1.0 0.3 - 0.8 DVPE (EPA equation) psi D5191 7.19 7.22 7.06 7.17 6.45 7.00 7.22 - - - 7.13 7.07 - 7.32 7.15 Aromatics vol. % D1319 - 17.8 - 16.8 17.9 17.6 15.5 - - - - - 16.5 16.7 17.0 Olefins vol. % D1319 - 8.0 - 7.7 8.3 7.1 6.8 - - - - - 7.4 7.3 7.5 Saturates vol. % * - - - - - - - - - - - - - - 75.5 Benzene vol. % D3606 - - - 0.56 - - 0.51 - - - - 0.54 0.57 0.55 0.55 S mg/kg D5453 22 25 21 22 - - 24 - - - - - - 23 23 RON - D2699 91.2 - 91.3 - - - 91.2 - - - - - - 92.1 91.2 MON - D2700 84.4 - 83.9 - - - 84.2 - - - - - - 84.7 84.2 (RON+MON)/2 - - 87.8 - 87.6 - - - 87.7 - - - - - - 88.4 87.7 C mass %D5291 mod.**85.20 - - - 84.40 - - - - - - - 85.7285.3285.16 H mass %D5291 mod.**14.05 - - - 14.39 - - - - - - - 14.3714.2014.25 O mass % D5599 - - - - - - - - - - - <0.1 <0.01 - <0.1 Net Heat of Combustion MJ/kg D4809 43.872 - - - - - 43.548 - - - - - - 43.78643.735 Water mass % E-1064 - - - - - - 0.005 - - - - 0.033 - - 0.019 Lead g/l D3237 - - - - - - <0.001 - - - - - - - <0.001 Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - <0.5 - - - - - - - <0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :8 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60oF g/cm3 D4052 0.71870.7192 - 0.71920.7191 - - - - - - - - - 0.7191 API Gravity, 60oF oAPI D4052 65.1 65.1 - 65.1 65.1 - - - - - - - - - 65.1 Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.10<0.05<0.10<0.10 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.10 - - <0.10 Distillation IBP oF 79.7 79.8 91.2 85.7 - - 84 - - 82.4 79.9 83.8 86.7 84 83.7

5% evapoF 107.2 109.5 112.6103.1 - - 100 - - 108.3 107.8107.1 116.9 108 108.1 10% evapoF 122.4124.7126.9 118.8 - - 118 - - 123.4 123.2 122.2 130.3 124 123.4 20% evapoF 151.1 153.5 153.0146.9 - - 148 - - 152.0 151.3149.8157.9 152 151.6 30% evapoF 180.9 182.9 180.9 177.9 - - 178 - - 181.7 180.5220.8185.6 182 185.1 40% evapoF 204.1 205.5204.6202.3 - - 203 - - 205.0203.8203.6207.4 205 204.4 50% evapoF 220.6221.7220.6220.3 - - 220 - - 221.3220.5220.8222.7 222 221.1 60% evapoF 233.3234.5233.8229.7 - - 234 - - 233.7233.3233.7234.8 234 233.5 70% evapoF 245.5246.9246.0245.1 - - 245 - - 247.2246.1 245.2248.5 248 246.4 80% evapoF 262.8265.0264.6262.4 - - 263 - - 263.7263.3262.9266.6 266 264.0 90% evapoF 301.3304.2304.3299.2 - - 302 - - 304.3302.1 299.5310.0 304 303.1 95% evapoF 328.9331.3331.3327.0 - - 330 - - 331.2329.1 326.0338.2 332 330.5 FBPoF 357.3364.8364.1 355.7 - - 363 - - 362.1 359.8359.2362.7 360 360.9 Recovery vol. % 97.5 97.9 97.6 96.65 - - 96.7 - - 97.6 97.2 97.7 97.7 96.9 97.5 Residue vol. % 1.0 1.0 0.9 0.1 - - 1.1 - - 1.0 1.0 0.9 1.1 1.1 0.9 Loss vol. % 1.5 1.1 1.5 3.3 - - 2.2 - - 1.4 1.8 1.4 1.2 2.0 1.7 Corrected Recovery vol. % 97.7 97.9 97.8 97.2 - - - - - 97.5 97.5 98.0 97.7 - 97.7 Corrected Loss vol. % 1.3 1.1 1.3 2.3 - - - - - 1.5 1.5 1.1 1.2 - 1.4 DVPE (EPA equation) psi D5191 10.1610.4310.0010.25 9.41 - 10.32 - - - 10.2410.25 - 9.93 10.20 Aromatics vol. % D1319 - 15.8 - 15.5 15.1 - 15.9 - - - - - 15.6 16.2 15.7 Olefins vol. % D1319 - 6.3 - 5.9 6.1 - 6.5 - - - - - 7.2 6.2 6.4 Saturates vol. % * - - - - - - - - - - - - - - 78.0 Benzene vol. % D3606 - - - 0.53 - - 0.48 - - - - 0.50 - 0.48 0.50 S mg/kg D5453 22 25 21 22 - - 26 - - - - - - 22 23 RON - D2699 95.2 - 95.6 - - - 95.5 - - - - - - 95.6 95.5 MON - D2700 87.7 - 87.7 - - - 87.6 - - - - - - 88.1 87.8 (RON+MON)/2 - - 91.5 - 91.7 - - - 91.6 - - - - - - 91.9 91.7 C mass %D5291 mod.**84.69 - - - 84.75 - - - - - - - 85.5685.4985.12 H mass %D5291 mod.**14.15 - - - 14.50 - - - - - - - 14.4814.1614.32 O mass % D5599 - - - - - - <0.1 - - - - <0.1 <0.01 - <0.1 Net Heat of Combustion MJ/kg D4809 44.046 - - - - - 44.098 - - - - - - 43.96644.037 Water mass % E-1064 - - - - - - - - - - - 0.020 - - 0.020 Lead g/l D3237 - - - - - - 0.001 - - - - - - - 0.001 Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - <0.5 - - - - - - - <0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :9 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60oF g/cm3 D4052 0.74500.7453 - 0.74540.7459 - - - - - - - - - 0.7454 API Gravity, 60oF oAPI D4052 58.2 58.1 - 58.2 58.2 - - - - - - - - - 58.2 Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.10<0.05<0.10<0.10 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.10 - - <0.10 Distillation IBP oF 82.2 84.4 91.2 88.3 85.1 - 85 - - 84.1 84.0 84.9 87.1 84 85.3

5% evapoF 105.4106.9 108.1 103.0104.9 - 103 - - 104.6 107.2 105.6111.2 102 105.1 10% evapoF 114.9 116.6117.3112.9 115.3 - 115 - - 114.4 116.0115.1 119.4 113 115.1 20% evapoF 130.3132.1 131.2 128.0131.0 - 131 - - 129.8 130.9 130.1 134.4 129 130.3 30% evapoF 147.3149.0147.2 144.9 147.7 - 149 - - 146.6 147.8146.9 151.4 146 147.2 40% evapoF 168.0170.1 167.9 164.9 167.5 - 169 - - 167.0 168.4168.2 173.1 166 167.7 50% evapoF 193.2 195.3192.6190.2 192.6 - 194 - 192.1 194.2 192.5 199.2 191 192.8 60% evapoF 225.1 224.2225.7222.4224.6 - 227 - - 224.7226.7223.9231.9 223 224.7 70% evapoF 260.7259.2261.0258.9260.2 - 261 - - 260.4261.7259.6265.7 260 260.3 80% evapoF 293.8292.3293.9287.1 294.1 - 290 - - 292.6294.8291.7299.0 292 292.2 90% evapoF 342.2342.5343.0339.7341.8 - 344 - - 341.7341.2340.9349.5 341 341.8 95% evapoF 364.3363.2365.2363.1 362.8 - 365 - - 362.5363.0 363 367.8 363 363.5 FBPoF 381.1 384.4385.0375.9387.7 - 387 - - 380.2394.1 390.3381.2 381 384.7 Recovery vol. % 98 98.0 97.8 96.6 98.1 - 97.8 - - 97.5 97.9 97.7 97.4 97.2 97.6 Residue vol. % 1.1 1.1 0.9 0.6 1.0 - 0.9 - - 1.1 1.1 0.8 1.0 0.5 1.0 Loss vol. % 0.9 0.9 1.3 2.8 1.0 - 1.3 - - 1.4 1.0 1.5 1.6 2.3 1.4 Corrected Recovery vol. % 98.1 97.9 98 97.6 - - - - - 97.4 98.0 98 97.4 - 97.9 Corrected Loss vol. % 0.8 1.0 1.1 1.8 - - - - - 1.5 0.9 1.2 1.6 - 1.2 DVPE (EPA equation) psi D5191 10.2810.4010.19 10.34 9.41 - 10.32 - - - 10.31 10.22 - 10.32 10.30 Aromatics vol. % D1319 - 36.1 - 35.7 35.1 - 35.7 - - - - - 34.6 37.3 35.8 Olefins vol. % D1319 - 7.5 - 6.1 6.4 - 5.5 - - - - - 6.2 6.2 6.2 Saturates vol. % * - - - - - - - - - - - - - - 58.0 Benzene vol. % D3606 - - - 0.57 - - 0.52 - - - - 0.52 - 0.55 0.54 S mg/kg D5453 23 27 22 23 - - 24 - - - - - - 23 23 RON - D2699 94.5 - 94.6 - - - 94.6 - - - - - - 94.3 94.5 MON - D2700 84.4 - 84.7 - - - 85.3 - - - - - - 84.9 84.8 (RON+MON)/2 - - 89.5 - 89.7 - - - 90.0 - - - - - - 89.6 89.7 C mass %D5291 mod.**86.91 - - - 85.50 - - - - - - - 87.0387.1587.03 H mass %D5291 mod.**12.65 - - - 12.84 - - - - - - - 13.02 12.7812.82 O mass % D5599 - - - - - - <0.1 - - - - <0.1 <0.01 <0.1 <0.1 Net Heat of Combustion MJ/kg D4809 43.540 - - - - - 42.854 - - - - - - 43.23443.209 Water mass % E-1064 - - - - - - 0.007 - - - - 0.011 - - 0.009 Lead g/l D3237 - - - - - - <0.001 - - - - - - - <0.001 Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - <0.5 - - - - - - - <0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :10 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60oF g/cm3 D4052 0.76410.7646 - 0.76440.7643 - - - - - - - - - 0.7644 API Gravity, 60oF oAPI D4052 53.4 53.4 - 53.4 53.4 - - - - - - - - - 53.4 Ethanol vol. % D5599 - - 10.35 9.88 - 

### - 9.83 

### - - - - 9.82 9.70 9.87 9.82 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.10 0.06 - <0.10 Distillation IBP oF 103.8103.7 - - - 107.4 - - 104.4104.6 103.0 - - 106.1 104.7

5% evapoF 130.1 130.8 - - - 129.1 - - 130.5 129.2 129.9 - - 130.7130.0 10% evapoF 136.7136.7 - - - 135.9 - - 136.1 136.4 136.1 - - 136.5 136.3 20% evapoF 144.6144.8 - - - 144.1 - - 144.1 144.1 144.2 - - 144.3144.3 30% evapoF 151.1 152.0 - - - 151.1 - - 150.8150.9 150.6 - - 150.7151.0 40% evapoF 161.7163.9 - - - 162.5 - - 160.1 161.8 158.4 - - 162.5 161.6 50% evapoF 215.7217.4 - - - 217.2 - - 217.9216.6216.8 - - 218.4217.1 60% evapoF 260.7262.1 - - - 261.3 - - 261.9260.8261.2 - - 262.8261.5 70% evapoF 285.9292.1 - - - 291.1 - - 292.5291.6290.8 - - 288.6290.4 80% evapoF 317.6318.0 - - - 317.2 - - 317.7316.9316.3 - - 318.8317.5 90% evapoF 340.2340.3 - - - 339.2 - - 340.5340.0338.9 - - 342.2340.2 95% evapoF 353.0354.0 - - - 355.3 - - 353.8354.0353.4 - - 356.8354.3 FBPoF 371.3373.0 - - - 375.7 - - 371.3369.9374.7 - - 371.1 372.4 Recovery vol. % 98.4 98.5 - - - 97.9 - - 98.5 97.8 98.3 - - 98.0 98.3 Residue vol. % 1.0 1.0 - - - 1.0 - - 1.0 1.1 1.0 - - 1.0 1.0 Loss vol. % 0.6 0.5 - - - 1.1 - - 0.5 1.1 0.7 - - 1.0 0.7 Corrected Recovery vol. % 98.4 98.5 - - - - - - - 97.8 98.3 - - - 98.3 Corrected Loss vol. % 0.6 0.5 - - - - - - - 1.1 0.7 - - - 0.7 DVPE (EPA equation) psi D5191 7.19 7.19 7.08 7.16 6.45 7.00 7.19 - - - 7.10 7.08 - 7.02 7.11 Aromatics vol. % D1319 - 33.5 - 34.5 33.5 34.2 - - - - - - 32.7 35.6 34.0 Olefins vol. % D1319 - 7.5 - 6.2 6.1 6.6 - - - - - - 6.1 6.0 6.1 Saturates vol. % * - - - - - - - - - - - - - - 50.1 Benzene vol. % D3606 - - - 0.53 - - 0.50 - - - - 0.51 0.49 0.58 0.52 S mg/kg D5453 23 27 24 25 - - 25 - - - - - - 25 25 RON - D2699 98.5 - 98.6 - - - 99.7 - - - - - - 98.4 98.5 MON - D2700 86.8 - 87.4 - - - 86.7 - - - - - - 87.4 87.2 (RON+MON)/2 - - 92.7 - 93.0 - - - 93.2 - - - - - - 92.9 92.9 C mass %D5291 mod.**83.46 - - - 82.85 - - - - - - - 83.4583.4983.47 H mass %D5291 mod.**12.72 - - - 12.90 - - - - - - - 13.0412.6712.83 O mass % D5599 - - 3.7 3.6 - - 3.6 - - - - 3.5 3.5 3.6 3.6 Net Heat of Combustion MJ/kg D4809 41.486 - - - - - 40.770 - - - - - - 41.37441.210 Water mass % E-1064 - - - - - - 0.058 - - - - 0.076 - - 0.067 Lead g/l D3237 - - - - - - <0.003 - - - - - - - <0.003 Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - <0.5 - - - - - - - <0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 (**OptiDist** or equivalent) **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :11 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60oF g/cm3 D4052 0.75930.7598 - 0.75970.7597 - - - - - - - - - 0.7596 API Gravity, 60oF oAPI D4052 54.6 54.5 - 54.6 54.6 - - - - - - - - - 54.6 Ethanol vol. % D5599 - - 10.81 10.30 - 

### - 9.92 

### - - - - 10.4010.15 10.21 10.30 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.10 - - <0.10 Distillation IBP oF 90.4 92.0 - - - 94.2 - - 92.7 90.5 91.9 - - 92.1 92.0

5% evapoF 115.9 115.9 - - - 114.6 - - 113.7115.6 116.4 - - 117.2 115.4 10% evapoF 124.5 124.9 - - - 123.9 - - 123.4124.8 125.1 - - 125.4124.4 20% evapoF 137.8137.8 - - - 137.6 - - 137.1 137.7 137.6 - - 137.9 137.6 30% evapoF 148.3148.3 - - - 148.2 - - 147.2 148.4 148.2 - - 148.3148.1 40% evapoF 157.5 157.1 - - - 157.0 - - 155.1 156.6 155.6 - - 156.7156.5 50% evapoF 189.6188.4 - - - 190.0 - - 188.6189.7 189.2 - - 196.4189.3 60% evapoF 230.5231.6 - - - 231.0 - - 230.0231.8231.5 - - 233.1 231.1 70% evapoF 251.3252.4 - - - 251.0 - - 250.2251.7251.9 - - 252.9251.4 80% evapoF 270.2270.9 - - - 269.1 - - 269.4269.8270.7 - - 272.8270.0 90% evapoF 297.7 299 - - - 299.0 - - 298.0298.5299.5 - - 302.8298.6 95% evapoF 324.3325.5 - - - 325.5 - - 323.4324.9326.1 - - 336.0325.0 FBPoF 359.5361.6 - - - 358.6 - - 358.0358.9368.0 - - 361.2360.8 Recovery vol. % 98.4 97.6 - - - 97.5 - - 97.2 98.0 97.7 - - 97.9 97.9 Residue vol. % 1.0 1.0 - - - 1.0 - - 1.0 1.0 1.0 - - 1.0 1.0 Loss vol. % 0.6 1.4 - - - 1.5 - - 1.8 1.0 1.3 - - 1.1 1.1 Corrected Recovery vol. % 98.4 97.6 - - - - - - - 98.0 97.9 - - - 98.0 Corrected Loss vol. % 0.6 1.4 - - - - - - - 1.0 1.1 - - - 1.0 DVPE (EPA equation) psi D5191 9.91 10.03 9.76 9.99 9.11 - 10.02 - - - 9.95 9.91 - 9.87 9.93 Aromatics vol. % D1319 - 35.9 - 35.4 34.8 35.7 33.8 34.4 - - - - 17.4 35.1 35.0 Olefins vol. % D1319 - 7.5 - 6.6 7.1 7.0 7.2 6.8 - - - - 8.9 6.3 6.9 Saturates vol. % * - - - - - - - - - - - - - - 47.8 Benzene vol. % D3606 - - - 0.53 - - 0.50 - - - - 0.51 0.57 0.57 0.54 S mg/kg D5453 23 28 22 24 - - 27 - - - - - - 22 24 RON - D2699 97.8 - 98.2 - - - 97.4 - - - - - - 97.8 97.8 MON - D2700 85.6 - 86.3 - - - 85.0 - - - - - - 85.5 85.6 (RON+MON)/2 - - 91.7 - 92.3 - - - 91.2 - - - - - - 91.7 91.7 C mass %D5291 mod.**83.65 - - - 83.10 - - - - - - - 83.6783.71 83.68 H mass %D5291 mod.**12.44 - - - 12.74 - - - - - - - 12.7612.5012.61 O mass % D5599 - - 3.9 3.7 - - 3.6 - - - - 3.8 3.7 3.7 3.7 Net Heat of Combustion MJ/kg D4809 41.462 - - - - - 40.970 - - - - - - 41.09241.175 Water mass % E-1064 - - - - - - 0.055 - - - - 0.076 - - 0.0655 Lead g/l D3237 - - - - - - - - - - - - - - - Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - 0.5 - - - - - - - 0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 (**OptiDist** or equivalent) **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :12 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60oF g/cm3 D4052 0.75140.7518 - 0.75180.7517 - - - - - - - - - 0.7517 API Gravity, 60oF oAPI D4052 56.6 56.5 - 56.5 56.5 - - - - - - - - - 56.5 Ethanol vol. % D5599 - - 10.63 9.91 - 

### - 9.83 

### - - - - 9.89 9.68 9.85 9.83 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.10 - - <0.10 Distillation IBP oF 90.6 89.9 - - - 92.1 - - 92.9 89.4 92.7 - - 91.6 91.3

5% evapoF 110.1 110.5 - - - 110.8 - - 111.9 109.3 111.3 - - 111.4110.7 10% evapoF 116.4116.6 - - - 117.0 - - 117.6116.3 117.5 - - 116.9 116.9 20% evapoF 124.8125.5 - - - 123.8 - - 125.5 125.1 125.5 - - 124.2 125.0 30% evapoF 133.6134.1 - - - 133.2 - - 133.9 133.7 134.1 - - 134.0133.8 40% evapoF 142.4142.8 - - - 142.3 - - 143.0143.1 143.3 - - 143.0142.8 50% evapoF 152.6152.8 - - - 151.3 - - 151.5 152.1 153.0 - - 153.3152.2 60% evapoF 196.0197.6 - - - 200.1 - - 200.8198.0 198.3 - - 210.2 198.5 70% evapoF 273.9275.0 - - - 275.5 - - 276.0274.7275.3 - - 280.4275.1 80% evapoF 307.6308.1 - - - 307.7 - - 308.0307.7308.0 - - 312.2307.9 90% evapoF 339.9340.3 - - - 340.1 - - 339.4339.4339.9 - - 341.7339.8 95% evapoF 357.8357.8 - - - 357.5 - - 357.0358.0358.3 - - 365.0357.7 FBPoF 376.3377.8 - - - 376.3 - - 373.6373.4378.0 - - 379.5375.9 Recovery vol. % 98.0 97.8 - - - 97.8 - - 97.4 97.8 97.8 - - 97.5 97.9 Residue vol. % 1.1 1.1 - - - 1.1 - - 1.1 1.1 1.1 - - 1.1 1.1 Loss vol. % 0.9 1.1 - - - 1.1 - - 1.5 1.1 1.1 - - 1.4 1.1 Corrected Recovery vol. % 98.1 97.8 - - - - - - - 97.8 98.0 - - - 97.9 Corrected Loss vol. % 0.8 1.1 - - - - - - - 1.1 0.9 - - - 1.0 DVPE (EPA equation) psi D5191 10.15 10.18 9.99 10.23 9.35 - 10.20 - - - 10.1310.01 - 10.1410.13 Aromatics vol. % D1319 - 34.3 - 35.4 34.5 - - 34.6 - - - - 38.0 35.1 34.8 Olefins vol. % D1319 - 8.0 - 6.8 6.8 - - 6.4 - - - - 7.5 6.0 6.9 Saturates vol. % * - - - - - - - - - - - - - - 48.5 Benzene vol. % D3606 - - - 0.57 - - 0.52 - - - - 0.55 0.60 0.62 0.57 S mg/kg D5453 19 22 17 18 - - 21 - - - - - - 19 19 RON - D2699 101.2 - 100.4 - - - 99.9 - - - - - - 100.0100.4 MON - D2700 87.4 - 87.9 - - - 88.5 - - - - - - 88.1 88.0 (RON+MON)/2 - - 94.3 - 94.2 - - - 94.2 - - - - - - 94.1 94.2 C mass %D5291 mod.**84.31 - - - 81.80 - - - - - - - 83.4083.7683.32 H mass %D5291 mod.**12.26 - - - 12.72 - - - - - - - 13.0012.7412.68 O mass % D5599 - - 3.9 3.6 - - 3.6 - - - - 3.6 3.6 3.6 3.6 Net Heat of Combustion MJ/kg D4809 41.648 - - - - - 41.084 - - - - - - 41.38841.373 Water mass % E-1064 - - - - - - 0.053 - - - - 0.078 - - 0.066 Lead g/l D3237 - - - - - - <0.003 - - - - - - - <0.003 Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - <0.5 - - - - - - - <0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 (**OptiDist** or equivalent) **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :13 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60oF g/cm3 D4052 0.75370.7541 - 0.75410.7540 - - - - - - - - - 0.7540 API Gravity, 60oF oAPI D4052 56.0 56.0 - 56.0 56.0 - - - - - - - - - 56.0 Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.10<0.05<0.10<0.10 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.10 - - <0.10 Distillation IBP oF 93.5 94.9 100.6 96.0 97.7 93.2 99 - 93.8 93.8 97.2 97.7 102.0 97 96.6

5% evapoF 126.1 129.3131.0123.2 125.2 125.6 123 - 123.8126.6 129.9 129.4135.2 123 127.0 10% evapoF 139.3141.7142.5 135.7138.6137.9 137 - 137.6139.6 141.7142.2 146.3 137 139.8 20% evapoF 158.7160.7160.0154.9 157.6156.8 157 - 157.2158.5 159.4160.9 163.8 157 158.7 30% evapoF 178.7179.6179.4175.0177.1 176.8 177 - 176.6178.1 179.4180.3181.1 177 178.2 40% evapoF 200.4200.6201.0198.1 198.9 198.9 199 - 198.4199.9200.7201.7203.2 198 199.9 50% evapoF 222.8223.4223.0220.8221.7221.0 222 - 221.1 223.0223.3223.6225.0 222 222.5 60% evapoF 245.2245.3245.8242.8244.9244.5 245 - 244.0245.7246.0246.3246.7 245 245.2 70% evapoF 269.9269.5270.5268.2269.4269.2 270 - 268.4269.8270.2270.8271.2 270 269.8 80% evapoF 303.7304.0305.1 301.2302.5302.5 305 - 301.7302.4304.3303.9306.0 303 303.5 90% evapoF 338.2338.5339.3336.8336.6337.2 337 - 336.7337.7338.2338.4339.6 339 337.9 95% evapoF 354.4354.4355.8352.1 353.3353.7 356 - 353.1 354.0353.5354.8356.5 355 354.4 FBPoF 376.6379.0374.9370.3379.0375.6 385 - 373.6375.8384.0376.9379.3 377 377.5 Recovery vol. % 97.9 98.0 98.7 98.0 97.1 97.7 98.5 - 97.5 98.1 98.1 98.3 98.4 96.9 98.2 Residue vol. % 1.1 1.1 0.8 0.4 1.2 1.1 0.9 - 1.1 1.1 1.1 1.0 1.0 1.0 1.0 Loss vol. % 1.0 0.9 0.5 1.6 1.7 1.2 0.6 - 1.4 0.8 0.8 0.7 0.6 2.1 0.9 Corrected Recovery vol. % 98.0 98.0 98.7 98.3 - - - - - 98.1 98.2 98.4 98.4 - 98.3 Corrected Loss vol. % 0.9 0.9 0.5 1.3 - - - - - 0.8 0.7 0.6 0.6 - 0.8 DVPE (EPA equation) psi D5191 6.92 6.98 6.86 6.98 6.28 6.77 6.96 - - - 6.96 6.89 - 6.92 6.9 Aromatics vol. % D1319 - 34.9 - 34.2 33.4 34.7 33.9 - - - - - 34.1 33.5 34.1 Olefins vol. % D1319 - 7.4 - 6.5 6.8 6.5 5.2 - - - - - 6.6 5.1 6.3 Saturates vol. % * - - - - - - - - - - - - - - 59.6 Benzene vol. % D3606 - - - 0.53 - - 0.49 - - - - 0.50 - 0.53 0.51 S mg/kg D5453 21 25 21 22 - - 26 - - - - - - 22 23 RON - D2699 95.7 - 95.9 - - - 95.8 - - - - - - 95.9 95.8 MON - D2700 85.8 - 85.7 - - - 86.1 - - - - - - 85.6 85.8 (RON+MON)/2 - - 90.8 - 90.8 - - - 91.0 - - - - - - 90.8 90.8 C mass %D5291 mod.**87.07 - - - 86.44 - - - - - - - 86.9 86.6386.76 H mass %D5291 mod.**12.74 - - - 13.11 - - - - - - - 13.1613.6013.15 O mass % D5599 - - - - - - <0.1 - - - - <0.1 <0.01 <0.1 <0.1 Net Heat of Combustion MJ/kg D4809 43.230 - - - - - 43.184 - - - - - - 43.09843.171 Water mass % E-1064 - - - - - - - - - - - 0.014 - - 0.014 Lead g/l D3237 - - - - - - <0.001 - - - - - - - <0.001 Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - 1.5 - - - - - - - 1.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :14 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60oF g/cm3 D4052 0.72200.7228 - 0.72230.7222 - - - - - - - - - 0.7223 API Gravity, 60oF oAPI D4052 64.2 64.1 - 64.2 64.2 - - - - - - - - - 64.2 Ethanol vol. % D5599 - - - - - 

### - <0.10 

### - - - - <0.10<0.05<0.10<0.10 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.10 - - <0.10 Distillation IBP oF 98.9 99.6 101.3 99.1 102.9 - 101 - - 99.2 103.1 99.0 100.7 99 100.4

5% evapoF 126.4127.9 129.4122.9 127.2 - 123 - - 126.4 128.3125.7130.4 124 126.5 10% evapoF 135.5 137.0136.9 132.6136.0 - 134 - - 135.4 136.0134.9 137.8 134 135.5 20% evapoF 147.5 148.8148.1 144.7147.0 - 146 - - 147.6 147.7146.8149.4 146 147.3 30% evapoF 160.2 161.4160.5 157.9 159.6 - 159 - - 160.4 160.4159.5 161.8 159 160.0 40% evapoF 175.7176.4175.5 173.2 174.6 - 174 - - 175.7 175.7174.4177.4 174 175.1 50% evapoF 192.7193.7192.9 191.1 192.2 - 193 - - 193.5 193.3192.3195.0 192 192.8 60% evapoF 211.7212.8212.9210.7211.5 - 212 - - 212.6212.9211.5213.8 210 212.0 70% evapoF 237.1 238.4238.6234.5235.8 - 237 - - 238.1 237.9236.6239.5 236 237.3 80% evapoF 280.6281.7280.8275.7279.9 - 281 - - 279.8281.5278.3284.7 277 280.1 90% evapoF 337.8339.0340.0337.5338.5 - 338 - - 337.6339.5337.7340.4 338 338.5 95% evapoF 354.8354.0355.6353.4354.6 - 355 - - 354.4354.2353.8355.7 354 354.5 FBPoF 372.4373.6373.5366.7380.3 - 388 - - 373.2381.5385.9374.2 369 377.5 Recovery vol. % 98.1 97.9 98.6 97.0 98.8 - 98.5 - - 98.0 97.6 98.0 98.7 97.7 98.0 Residue vol. % 1.1 1.1 0.9 0.8 1.0 - 0.9 - - 1.1 1.1 0.7 1.0 0.6 1.0 Loss vol. % 0.8 1.0 0.5 2.2 0.2 - 0.6 - - 0.9 1.3 1.3 0.3 1.7 1.0 Corrected Recovery vol. % 98.2 97.6 98.6 97.6 - - - - - 98.0 97.9 98.2 98.7 - 98.1 Corrected Loss vol. % 0.7 1.0 0.5 1.6 - - - - - 0.9 1.0 1.1 0.3 - 0.9 DVPE (EPA equation) psi D5191 7.25 7.23 6.99 7.24 6.77 - 7.31 - - - 7.17 7.22 - 7.09 7.14 Aromatics vol. % D1319 - 16.9 - 16.2 17.0 - 17.0 - - - - - 17.9 16.6 16.9 Olefins vol. % D1319 - 9.3 - 8.8 9.0 - 7.6 - - - - - 8.5 7.7 8.5 Saturates vol. % * - - - - - - - - - - - - - - 74.6 Benzene vol. % D3606 - - - 0.54 - - 0.49 - - - - 0.51 0.53 0.52 0.52 S mg/kg D5453 23 27 23 23 - - 25 - - - - - - 24 24 RON - D2699 91.1 - 91.7 - - - 91.5 - - - - - - 91.5 91.5 MON - D2700 84.3 - 84.5 - - - 85.1 - - - - - - 84.6 84.6 (RON+MON)/2 - - 87.7 - 88.1 - - - 88.3 - - - - - - 88.1 88.1 C mass %D5291 mod.**84.82 - - - 85.21 - - - - - - - 85.6685.4285.28 H mass %D5291 mod.**13.96 - - - 14.55 - - - - - - - 14.39 14.2414.29 O mass % D5599 - - - - - - - - - - - <0.1 <0.01 - <0.1 Net Heat of Combustion MJ/kg D4809 44.000 - - - - - 42.770 - - - - - - 43.78643.519 Water mass % E-1064 - - - - - - 0.005 - - - - 0.024 - - 0.015 Lead g/l D3237 - - - - - - <0.001 - - - - - - - <0.001 Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - <0.5 - - - - - - - <0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :15 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60oF g/cm3 D4052 0.74240.7428 - 0.74280.7430 - - - - - - - - - 0.7428 API Gravity, 60oF oAPI D4052 58.8 58.8 - 58.8 58.8 - - - - - - - - - 58.8 Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.10<0.05<0.10<0.10 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.10 - - <0.10 Distillation IBP oF 80.8 83.3 92.3 88.3 - 81.1 84 - - 85.5 86.3 85.2 86.8 80 84.7

5% evapoF 105.9 106.2 108.5 103.9 - 104.3 102 - - 105.9 107.2 105.2 111.2 106 105.5 10% evapoF 115.4116.4118.2 113.6 - 114.4 114 - - 116.0 116.5 115.3119.5 116 115.6 20% evapoF 130.9 131.3131.9 128.4 - 129.8 130 - - 131.2 130.6130.2 134.0 131 130.5 30% evapoF 147.2 147.8147.4144.6 - 145.9 146 - - 147.6 146.6146.2 150.8 147 146.6 40% evapoF 167.0167.6166.6164.2 - 165.5 167 - - 167.1 166.0166.0170.6 166 166.3 50% evapoF 190.4190.6189.7188.0 - 189.3 190 - - 190.5 189.4189.0194.0 190 189.7 60% evapoF 216.6217.1 216.5214.4 - 215.4 217 - - 217.6216.2215.3220.2 216 216.2 70% evapoF 243.2 244 243.9241.9 - 241.8 242 - - 243.5242.9242.4245.9 244 243.0 80% evapoF 266.0266.7266.9265.0 - 264.7 265 - - 265.9266.1 265.8268.9 267 265.9 90% evapoF 299.2300.5299.5298.3 - 298.3 300 - - 299.9299.0300.0305.2 299 299.4 95% evapoF 328.2331.2331.3327.2 - 327.3 330 - - 331.4329.8328.4337.6 328 329.3 FBPoF 363.0368.6363.2360.4 - 362.4 366 - - 361.0364.0363.2366.5 365 363.7 Recovery vol. % 98.4 97.6 97.8 96.8 - 98.1 98.0 - - 97.4 97.3 97.1 97.9 97.8 97.5 Residue vol. % 1.0 1.0 0.8 0.5 - 1.0 0.9 - - 1.0 1.0 1.1 1.1 0.8 0.9 Loss vol. % 0.6 1.4 1.4 2.7 - 0.9 1.0 - - 1.6 1.7 1.8 1.0 1.4 1.6 Corrected Recovery vol. % 98.4 97.6 98.0 97.7 - - - - - 97.2 97.8 97.4 97.9 - 97.7 Corrected Loss vol. % 0.6 1.4 1.2 1.8 - - - - - 1.8 1.2 1.5 1.0 - 1.4 DVPE (EPA equation) psi D5191 10.3310.37 9.92 10.36 9.45 10.12 10.26 - - - 10.31 10.30 - 10.0610.23 Aromatics vol. % D1319 - 36.1 - 35.6 34.6 35.4 33.4 - - - - - 35.4 36.7 35.3 Olefins vol. % D1319 - 7.6 - 7.2 7.2 7.0 6.3 - - - - - 8.2 7.2 7.2 Saturates vol. % * - - - - - - - - - - - - - - 57.4 Benzene vol. % D3606 - - - 0.54 - - 0.49 - - - - 0.51 0.61 0.53 0.54 S mg/kg D5453 22 27 22 23 - - 25 - - - - - - 23 24 RON - D2699 95.1 - 95.1 - - - 94.9 - - - - - - 94.7 95.0 MON - D2700 84.6 - 84.7 - - - 85.2 - - - - - - 84.9 84.9 (RON+MON)/2 - - 89.9 - 89.9 - - - 90.1 - - - - - - 89.8 90.0 C mass %D5291 mod.**87.36 - - - 85.93 - - - - - - - 87.1787.0686.88 H mass %D5291 mod.**12.34 - - - 13.00 - - - - - - - 12.89 12.91 12.79 O mass % D5599 - - - - - - <0.1 - - - - <0.1 <0.01 - <0.1 Net Heat of Combustion MJ/kg D4809 43.442 - - - - - 42.750 - - - - - - 43.13243.108 Water mass % E-1064 - - - - - - 0.007 - - - - 0.016 - - 0.012 Lead g/l D3237 - - - - - - <0.001 - - - - - - - <0.001 Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - 0.5 - - - - - - - 0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :16 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60oF g/cm3 D4052 0.76330.7638 - 0.76360.7635 - - - - - - - - - 0.7636 API Gravity, 60oF oAPI D4052 53.6 53.6 - 53.6 53.6 - - - - - - - - - 53.6 Ethanol vol. % D5599 - - 11.2010.65 - 

### - 10.69 

### - - - - 10.5710.8410.62 10.76 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.10 - - <0.10 Distillation IBP oF 102.4103.8 - - - 107.2 - - 104.7101.9 106.1 - - 105.6104.5

5% evapoF 131.7132.0 - - - 134.0 - - 134.8131.3 133.6 - - 133.9 133.0 10% evapoF 138.7138.4 - - - 139.5 - - 140.0138.5 139.5 - - 139.5 139.2 20% evapoF 147.5 147.6 - - - 147.6 - - 148.5 147.5 148.1 - - 148.1 147.8 30% evapoF 155.3155.3 - - - 154.8 - - 153.5 155.0 155.8 - - 156.0155.1 40% evapoF 168.5 165.7 - - - 177.2 - - 180.0169.6 169.1 - - 174.7172.1 50% evapoF 217.4215.9 - - - 220.6 - - 220.6218.5217.7 - - 220.9218.8 60% evapoF 237.5236.3 - - - 238.0 - - 238.6237.6236.5 - - 238.1 237.5 70% evapoF 250.8250.2 - - - 252.1 - - 253.0251.4252.0 - - 253.5251.9 80% evapoF 267.8268.0 - - - 268.1 - - 269.8267.8267.7 - - 271.0268.6 90% evapoF 299.6297.8 - - - 300.0 - - 302.0298.8299.8 - - 306.1 300.6 95% evapoF 329.0326.7 - - - 329.0 - - 333.3326.2329.3 - - 342.2330.8 FBPoF 362.7366.4 - - - 367.8 - - 364.5358.8369.1 - - 369.8365.6 Recovery vol. % 98.4 97.8 - - - 98.5 - - 98.3 97.7 98.5 - - 97.6 98.1 Residue vol. % 1.0 1.0 - - - 1.0 - - 1.0 1.0 1.0 - - 1.0 1.0 Loss vol. % 0.6 1.2 - - - 0.5 - - 0.7 1.3 0.5 - - 1.4 0.9 Corrected Recovery vol. % 98.4 97.8 - - - - - - - 97.6 98.5 - - - 98.1 Corrected Loss vol. % 0.6 1.2 - - - - - - - 1.4 0.5 - - - 0.9 DVPE (EPA equation) psi D5191 7.18 7.22 7.02 7.19 6.46 - 7.08 - - - 7.14 7.16 - 7.00 7.12 Aromatics vol. % D1319 - 35.2 - 35.2 34.5 36.2 34.6 35.6 - - - - 37.1 36.7 35.6 Olefins vol. % D1319 - 7.9 - 6.7 6.1 5.5 6.6 5.9 - - - - 8.6 6.7 6.8 Saturates vol. % * - - - - - - - - - - - - - - 46.9 Benzene vol. % D3606 - - - 0.63 - - 0.60 - - - - 0.61 0.60 0.65 0.62 S mg/kg D5453 21 25 20 23 - - 26 - - - - - - 22 23 RON - D2699 101.5 - 101.0 - - - 100.8 - - - - - - 100.8101.0 MON - D2700 87.9 - 88.6 - - - 88.1 - - - - - - 88.4 88.3 (RON+MON)/2 - - 94.7 - 94.8 - - - 94.5 - - - - - - 94.6 94.7 C mass %D5291 mod.**83.45 - - - 81.99 - - - - - - - 83.4283.3283.40 H mass %D5291 mod.**12.44 - - - 12.68 - - - - - - - 12.8712.6412.66 O mass % D5599 - - 4.0 3.9 - - 3.9 - - - - 3.8 3.9 3.8 3.9 Net Heat of Combustion MJ/kg D4809 41.210 - - - - - 40.860 - - - - - - 40.97041.013 Water mass % E-1064 - - - - - - 0.057 - - - - 0.074 - - 0.066 Lead g/l D3237 - - - - - - - - - - - - - - - Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - 1.0 - - - - - - - 1.0 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 (**OptiDist** or equivalent) **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :20 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60o

### F g/cm3 

### D4052 0.74230.7427 - 0.74250.7424 - - - - - - - - - 0.7425 API Gravity, 60 o

### F o

### API D4052 58.9 58.8 - 58.9 58.9 - - - - - - - - - 58.9 Ethanol vol. % D5599 - - 22.0320.90 - 

### - 20.33 

### - - - - 18.50 - 19.7720.31 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - 0.03 

### - - - - <0.1 - - <0.10 Distillation IBP oF 109.7108.1 - - - 107.6 - - 106.3107.8 108.6 - - 107.4107.9

5% evapoF 137.6 138.7 - - - 135.6 - - 137.7137.0 137.4 - - 137.4137.3 10% evapoF 142.9 143.2 - - - 141.7 - - 142.7142.6 142.8 - - 142.5 142.6 20% evapoF 150.0 150.2 - - - 149.1 - - 149.7149.8 149.8 - - 149.4149.7 30% evapoF 155.6 155.5 - - - 155.0 - - 155.3155.4 155.2 - - 154.9 155.3 40% evapoF 159.9 159.8 - - - 159.3 - - 159.4160.0 159.9 - - 159.1 159.6 50% evapoF 162.9 162.6 - - - 162.2 - - 162.7163.7 163.0 - - 162.0 162.7 60% evapoF 178.3 181 - - - 176.8 - - 186.3177.7 176.5 - - 182.4179.9 70% evapoF 233.2234.7 - - - 235.9 - - 234.0236.1 236.1 - - 233.6234.8 80% evapoF 254.6253.3 - - - 253.7 - - 252.0253.9253.4 - - 251.1 253.1 90% evapoF 299.1 298.8 - - - 297.3 - - 300.9296.1 298.5 - - 300.2298.7 95% evapoF 337.2337.2 - - - 335.2 - - 339.4334.2335.2 - - 338.0336.6 FBPoF 375.0373.5 - - - 373.3 - - 368.1362.6374.2 - - 376.6371.9 Recovery vol. % 98.5 98.9 - - - 98.4 - - 98.597.9 98.4 - - 98.8 98.4 Residue vol. % 1.0 1.0 - - - 1.0 - - 1.01.1 1.0 - - 1.0 1.0 Loss vol. % 0.5 0.1 - - - 0.6 - - 0.51.0 0.6 - - 0.2 0.6 Corrected Recovery vol. % 98.5 98.9 - - - - - - - 97.9 98.4 - - - 98.4 Corrected Loss vol. % 0.5 0.1 - - - - - - - 1.0 0.6 - - - 0.6 DVPE (EPA equation) psi D5191 6.72 6.73 6.59 6.73 6.08 6.70 6.79 - - - 6.71 6.64 - 6.70 6.70 Aromatics vol. % D1319 - 14.9 - 14.7 15.7 14.3 - 15.4 - - - - - 16.3 15.2 Olefins vol. % D1319 - 8.4 - 7.7 7.3 7.2 - 6.0 - - - - - 7.3 7.4 Saturates vol. % * - - - - - - - - - - - - - - 57.1 Benzene vol. % D3606 - - - 0.60 - - 0.57 - - - - 0.59 - 0.69 0.61 S mg/kg D5453 20 23 20 21 - - 22 - - - - - - 23 22 RON - D2699 102.3 - 101.8 - - - 101.6 - - - - - - 101.8 101.9 MON - D2700 88.8 - 89.5 - - - 89.0 - - - - - - 89.8 89.3 (RON+MON)/2 - - 95.6 - 95.7 - - - 95.3 - - - - - - 95.8 95.6 C mass %D5291 mod.**78.13 - - - 77.55 - - - - - - - 78.5778.0078.06 H mass %D5291 mod.**13.85 - - - 13.86 - - - - - - - 14.06 14.26 14.01 O mass % D5599 - - 8.2 7.8 - - 7.6 - - - - 6.9 - 7.4 7.58 Net Heat of Combustion MJ/kg D4809 40.072 - - - - - 40.104 - - - - - - 39.99640.057 Water mass % E-1064 - - - - - - - - - - - 0.138 - - 0.138 Lead g/l D3237 - - - - - - <0.0003 - - - - - - - <0.003 Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - <0.5 - - - - - - - <0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 (**OptiDist** or equivalent) **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :21 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60o

### F g/cm3 

### D4052 0.77510.7756 - 0.77550.7753 - - - - - - - - - 0.7754 API Gravity, 60 o

### F o

### API D4052 50.8 50.8 - 50.8 50.8 - - - - - - - - - 50.8 Ethanol vol. % D5599 - - 20.9520.90 - 

### - 20.32 

### - - - - 18.51 - 20.0420.14 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.1 - - <0.10 Distillation IBP oF 103.4103.7 - - - 111.8 - - 108.6 103.6 103.8 - - 109.3106.3

5% evapoF 133.3133.7 - - - 135.6 - - 137.1 132.7 134.8 - - 135.9 134.7 10% evapoF 140.6 140.8 - - - 141.8 - - 142.6 140.4 141.4 - - 141.7141.3 20% evapoF 150.1 149.9 - - - 150.9 - - 150.9 149.5 150.1 - - 150.4150.3 30% evapoF 157.0 156.7 - - - 157.5 - - 157.6 156.7 157.0 - - 157.4157.1 40% evapoF 162.5 162.4 - - - 162.7 - - 162.7162.7 162.3 - - 162.7162.6 50% evapoF 167.2 167.3 - - - 168.1 - - 167.7167.9 167.0 - - 168.1 167.6 60% evapoF 214.4213.1 - - - 217.5 - - 224.5211.8216.4 - - 223.1 217.3 70% evapoF 255.4255.3 - - - 253.4 - - 256.5255.7254.9 - - 255.2255.2 80% evapoF 276.0275.3 - - - 273.5 - - 274.6274.4275.8 - - 277.2275.3 90% evapoF 305.5304.6 - - - 303.7 - - 305.6302.3305.3 - - 307.8305.0 95% evapoF 330.2330.2 - - - 329.2 - - 334.5329.1 331.3 - - 334.3331.3 FBPoF 360.6363.9 - - - 359.4 - - 361.9354.5363.2 - - 359.8360.5 Recovery vol. % 98.4 97.9 - - - 98.4 - - 98.4 98.0 98.5 - - 98.2 98.2 Residue vol. % 1.0 1.0 - - - 1.0 - - 1.0 1.0 1.0 - - 1.0 1.0 Loss vol. % 0.6 1.1 - - - 0.6 - - 0.6 1.0 0.5 - - 0.8 0.8 Corrected Recovery vol. % 98.4 97.9 - - - - - - - 98.0 98.5 - - - 98.2 Corrected Loss vol. % 0.6 1.1 - - - - - - - 1.0 0.5 - - - 0.8 DVPE (EPA equation) psi D5191 7.14 7.17 7.03 7.12 6.40 - 6.98 - - - 7.11 6.95 - 6.94 7.06 Aromatics vol. % D1319 - 36.7 - 35.0 34.9 37.0 - 35.0 - - - - 35.2 34.5 35.5 Olefins vol. % D1319 - 8.0 - 7.6 7.0 7.3 - 6.6 - - - - 6.3 7.1 7.1 Saturates vol. % * - - - - - - - - - - - - - - 37.3 Benzene vol. % D3606 - - - 0.56 - - 0.52 - - - - 0.53 0.73 0.72 0.61 S mg/kg D5453 20 25 19 22 - - 27 - - - - - - 20 22 RON - D2699 102.2 - 101.3 - - - 101.6 - - - - - - 100.3101.4 MON - D2700 86.8 - 88.2 - - - 86.8 - - - - - - 88.1 87.5 (RON+MON)/2 - - 94.5 - 94.8 - - - 94.2 - - - - - - 94.2 94.5 C mass %D5291 mod.**79.55 - - - 79.15 - - - - - - - 80.2080.7079.90 H mass %D5291 mod.**12.23 - - - 12.70 - - - - - - - 12.5412.2412.43 O mass % D5599 - - 7.4 7.4 - - 7.2 - - - - 6.6 - 7.1 7.1 Net Heat of Combustion MJ/kg D4809 39.392 - - - - - 39.182 - - - - - - 39.28039.285 Water mass % E-1064 - - - - - - - - - - - 0.128 - - 0.128 Lead g/l D3237 - - - - - - 0.009 - - - - - - - 0.009 Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - 0.5 - - - - - - - 0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 (**OptiDist** or equivalent) **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :22 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60o

### F g/cm3 

### D4052 0.73680.7372 - 0.73720.7372 - - - - - - - - - 0.7371 API Gravity, 60 o

### F o

### API D4052 60.3 60.2 - 60.3 60.3 - - - - - - - - - 60.3 Ethanol vol. % D5599 - - 22.1221.22 - 

### - 20.58 

### - - - - 18.57 - 20.0620.51 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.1 - - <0.10 Distillation IBP oF 84.7 90.0 - - - 92.5 - - 91.7 91.3 88.6 - - 93.0 89.8

5% evapoF 119.4118.0 - - - 119.7 - - 119.8 118.1 117.9 - - 120.5 118.8 10% evapoF 129.9 128.8 - - - 130.4 - - 130.1 129.0 129.1 - - 130.1 129.6 20% evapoF 144.8 143.6 - - - 144.5 - - 144.4144.2 144.2 - - 144.7144.3 30% evapoF 154.1 153.7 - - - 153.6 - - 153.5 153.6 153.8 - - 153.8 153.7 40% evapoF 160.0 159.6 - - - 159.2 - - 159.1 159.7 159.6 - - 159.1 159.5 50% evapoF 163.6 163.7 - - - 162.9 - - 162.0 163.6 163.1 - - 162.6 163.2 60% evapoF 168.2 166.3 - - - 168.2 - - 165.5 168.3 166.7 - - 168.2 167.2 70% evapoF 234.5233.4 - - - 234.0 - - 233.7233.7233.9 - - 234.4233.9 80% evapoF 250.4253.0 - - - 254.9 - - 254.4254.8254.0 - - 256.5253.6 90% evapoF 297.4298.1 - - - 296.4 - - 298.3296.3297.5 - - 303.4297.3 95% evapoF 333.9336.2 - - - 333.3 - - 334.6333.9334.8 - - 342.8334.5 FBPoF 372.9374.7 - - - 364.2 - - 371.4362.0374.0 - - 377.2369.9 Recovery vol. % 98.9 97.4 - - - 98.1 - - 97.2 97.3 97.6 - - 97.8 97.8 Residue vol. % 1.0 1.1 - - - 1.0 - - 1.1 1.1 1.1 - - 1.0 1.1 Loss vol. % 0.1 1.5 - - - 0.9 - - 1.7 1.6 1.3 - - 1.2 1.1 Corrected Recovery vol. % 98.8 97.5 - - - - - - - 97.3 97.8 - - - 97.9 Corrected Loss vol. % 0.2 1.4 - - - - - - - 1.6 1.1 - - - 1.1 DVPE (EPA equation) psi D5191 10.05 10.31 9.93 10.27 9.38 10.31 - - - - 10.1710.11 - 10.22 10.21 Aromatics vol. % D1319 - 14.9 - 14.5 15.0 15.3 - 14.6 - - - - - 15.4 15.0 Olefins vol. % D1319 - 7.9 - 6.2 7.3 6.3 - 6.6 - - - - - 7.1 6.9 Saturates vol. % * - - - - - - - - - - - - - - 57.6 Benzene vol. % D3606 - - - 0.59 - 0.56 - - - - - 0.57 - 0.65 0.59 S mg/kg D5453 20 23 20 20 - - 21 - - - - - - 21 21 RON - D2699 102.2 - 101.7 - - - 101.8 - - - - - - 101.3101.8 MON - D2700 88.6 - 89.3 - - - 89.8 - - - - - - 89.6 89.3 (RON+MON)/2 - - 95.4 - 95.5 - - - 95.8 - - - - - - 95.5 95.6 C mass %D5291 mod.**78.34 - - - 77.60 - - - - - - - 78.3778.6478.24 H mass %D5291 mod.**13.76 - - - 13.87 - - - - - - - 14.05 13.71 13.85 O mass % D5599 - - 8.3 7.9 - - 7.7 - - - - 7.0 - 7.5 7.7 Net Heat of Combustion MJ/kg D4809 40.254 - - - - - 39.816 - - - - - - 40.02240.031 Water mass % E-1064 - - - - - - 0.105 - - - - 0.121 - - 0.113 Lead g/l D3237 - - - - - - 0.004 - - - - - - - 0.004 Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - <0.5 - - - - - - - <0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 (**OptiDist** or equivalent) **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :23 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60o

### F g/cm3 

### D4052 0.74730.7477 - 0.74770.7475 - - - - - - - - - 0.7476 API Gravity, 60 o

### F o

### API D4052 57.6 57.5 - 57.6 57.6 - - - - - - - - - 57.6 Ethanol vol. % D5599 - - 21.7721.03 - 

### - 20.26 

### - - - - 18.50 - 20.0420.32 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.1 - - <0.10 Distillation IBP oF 110.0 107.4 - - - 110.0 - - - 108.1 108.5 - - 110.1 109.0

5% evapoF 132.7133.8 - - - 132.8 - - - 133.2 132.7 - - 134.3133.3 10% evapoF 138.8 139.1 - - - 138.6 - - - 139.1 138.8 - - 139.1 138.9 20% evapoF 146.2 146.5 - - - 145.9 - - - 146.4 146.0 - - 146.1 146.2 30% evapoF 152.7152.6 - - - 151.9 - - - 152.7 152.2 - - 151.9 152.3 40% evapoF 158.2 157.8 - - - 157.6 - - - 158.0 157.6 - - 157.4157.8 50% evapoF 162.3162.9 - - - 162.5 - - - 162.9 162.4 - - 162.2 162.5 60% evapoF 170.7165.6 - - - 172.6 - - - 174.1 169.0 - - 177.7171.6 70% evapoF 269.9271.5 - - - 269.5 - - - 271.0271.5 - - 271.9270.9 80% evapoF 311.5312.5 - - - 311.0 - - - 311.4309.3 - - 312.5311.4 90% evapoF 338.6339.1 - - - 338.1 - - - 337.8338.0 - - 337.7338.2 95% evapoF 350.3350.1 - - - 348.7 - - - 350.0350.0 - - 350.8350.0 FBPoF 365.6367.0 - - - 365.2 - - - 359.6365.2 - - 365.0364.6 Recovery vol. % 97.9 98.3 - - - 98.4 - - - 98.0 97.9 - - 98.6 98.0 Residue vol. % 1.0 1.0 - - - 1.0 - - - 1.0 1.0 - - 1.0 1.0 Loss vol. % 1.1 0.7 - - - 0.6 - - - 1.0 1.1 - - 0.4 1.0 Corrected Recovery vol. % 98.1 98.3 - - - - - - - 98.0 98.1 - - - 98.1 Corrected Loss vol. % 0.9 0.7 - - - - - - - 1.0 0.9 - - - 0.9 DVPE (EPA equation) psi D5191 6.93 6.96 6.68 6.92 6.28 - 6.81 - - - 6.90 6.91 - 6.64 6.84 Aromatics vol. % D1319 - 16.3 - 15.4 16.2 16.6 - 15.5 - - - - 14.6 16.5 15.9 Olefins vol. % D1319 - 8.1 - 7.3 8.0 7.9 - 6.8 - - - - 7.1 7.0 7.5 Saturates vol. % * - - - - - - - - - - - - - - 56.4 Benzene vol. % D3606 - - - 0.58 - - 0.68 - - - - 0.55 - 0.70 0.63 S mg/kg D5453 20 23 19 20 - - 22 - - - - - - 22 21 RON - D2699 97.4 - 97.4 - - - 97.2 - - - - - - 97.7 97.4 MON - D2700 86.0 - 87.2 - - - 86.4 - - - - - - 87.4 86.8 (RON+MON)/2 - - 91.7 - 92.3 - - - 91.8 - - - - - - 92.6 92.1 C mass %D5291 mod.**78.82 - - - 77.90 - - - - - - - 78.81 77.8378.34 H mass %D5291 mod.**13.82 - - - 13.79 - - - - - - - 13.9714.88 13.86 O mass % D5599 - - 8.0 7.8 - - 7.5 - - - - 6.8 - 7.4 7.5 Net Heat of Combustion MJ/kg D4809 39.966 - - - - - 39.896 - - - - - - 39.88239.915 Water mass % E-1064 - - - - - - - - - - - 0.112 - - 0.112 Lead g/l D3237 - - - - - - <0.003 - - - - - - - <0.003 Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - 0.5 - - - - - - - 0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 (**OptiDist** or equivalent) **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :24 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60o

### F g/cm3 

### D4052 0.74190.7424 - 0.74230.7422 - - - - - - - - - 0.7422 API Gravity, 60 o

### F o

### API D4052 59.0 58.9 - 58.9 58.9 - - - - - - - - - 58.9 Ethanol vol. % D5599 - - 22.2 21.17 - 

### - 20.44 

### - - - - 18.68 - 20.0820.51 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - 0.03 

### - - - - <0.1 - - <0.10 Distillation IBP oF 87.8 90.4 - - - 89.8 - - 91.2 90.7 89.8 - - 90.5 89.7

5% evapoF 116.8 117.3 - - - 114.0 - - 112.3115.1 116.1 - - 119.5 115.9 10% evapoF 127.3127.9 - - - 125.5 - - 124.1 127.0 127.0 - - 128.7126.9 20% evapoF 143.3143.4 - - - 141.7 - - 141.4142.9 142.7 - - 143.5 142.8 30% evapoF 152.4153.9 - - - 152.3 - - 152.5 153.6 153.7 - - 153.8 153.2 40% evapoF 160.5 160.9 - - - 159.7 - - 159.3160.5 160.5 - - 160.2 160.4 50% evapoF 165.3165.3 - - - 164.4 - - 163.9 165.5 165.1 - - 164.8 165.1 60% evapoF 171.8 171.3 - - - 174.2 - - 169.7174.6 172.6 - - 184.9 172.9 70% evapoF 265.1 265.9 - - - 265.1 - - 262.8267.0267.2 - - 269.7266.1 80% evapoF 305.8306.3 - - - 303.6 - - 302.6305.4306.3 - - 309.6305.5 90% evapoF 338.3338.6 - - - 337.6 - - 336.1 337.9338.1 - - 340.6338.1 95% evapoF 350.6350.3 - - - 349.8 - - 349.1 350.2350.6 - - 353.6350.3 FBPoF 369.5371.7 - - - 366.0 - - 367.7363.8370.1 - - 370.0368.2 Recovery vol. % 98.2 97.6 - - - 97.2 - - 96.4 97.3 97.4 - - 97.6 97.6 Residue vol. % 1.0 1.0 - - - 1.1 - - 1.1 1.0 1.1 - - 1.1 1.0 Loss vol. % 0.8 1.4 - - - 1.7 - - 2.5 1.7 1.5 - - 1.3 1.4 Corrected Recovery vol. % 98.3 97.7 - - - - - - - 97.3 97.6 - - - 97.7 Corrected Loss vol. % 0.7 1.3 - - - - - - - 1.7 1.3 - - - 1.3 DVPE (EPA equation) psi D5191 10.08 10.21 9.76 10.24 9.33 - 10.26 - - - 10.19 10.03 - 10.19 10.12 Aromatics vol. % D1319 - 14.5 - 15.2 15.9 15.9 - 14.6 - - - - - 15.9 15.3 Olefins vol. % D1319 - 7.5 - 6.2 9.0 7.0 - 7.4 - - - - - 6.6 7.3 Saturates vol. % * - - - - - - - - - - - - - - 56.9 Benzene vol. % D3606 - - - 0.62 - - 0.56 - - - - 0.57 - 0.71 0.62 S mg/kg D5453 20 24 20 20 - - 22 - - - - - - 21 21 RON - D2699 101.3 - 100.5 - - - 100.9 - - - - - - 100.5 100.8 MON - D2700 88.0 - 88.4 - - - 89.6 - - - - - - 88.5 88.6 (RON+MON)/2 - - 94.7 - 94.5 - - - 95.3 - - - - - - 94.5 94.7 C mass %D5291 mod.**78.48 - - - 77.60 - - - - - - - 78.5278.4078.47 H mass %D5291 mod.**13.74 - - - 13.76 - - - - - - - 14.00 13.9413.86 O mass % D5599 - - 8.2 7.9 - - 7.6 - - - - 6.9 - 7.5 7.6 Net Heat of Combustion MJ/kg D4809 40.262 - - - - - - - - - - - - 39.96640.114 Water mass % E-1064 - - - - - - 0.103 - - - - 0.113 - - 0.108 Lead g/l D3237 - - - - - - 0.005 - - - - - - - 0.005 Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - 0.5 - - - - - - - 0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 (**OptiDist** or equivalent) **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :25 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60o

### F g/cm3 

### D4052 0.76980.7704 - 0.77020.7705 - - - - - - - - - 0.7702 API Gravity, 60 o

### F o

### API D4052 52.1 52.0 - 52.0 52.0 - - - - - - - - - 52.0 Ethanol vol. % D5599 - - 21.0220.52 - 

### - 20.23 

### - - - - 18.49 - 19.91 20.03 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.1 - - <0.10 Distillation IBP oF 88.5 88.6 - - - 86.8 - - 88.3 90.4 90.7 - - 92.2 89.0

5% evapoF 114.1 115.0 - - - 110.2 - - 115.2 114.7 114.5 - - 119.2 113.7 10% evapoF 125.8 126.6 - - - 122.5 - - 126.3126.5 126.3 - - 129.4125.5 20% evapoF 142.2 142.9 - - - 140.5 - - 143.1 142.5 142.5 - - 145.1 142.1 30% evapoF 153.3153.7 - - - 152.8 - - 154.0 153.5 153.3 - - 154.7153.3 40% evapoF 161.2 161.3 - - - 160.5 - - 161.1 160.6 160.7 - - 161.8 160.9 50% evapoF 167.5 166.5 - - - 166.7 - - 167.5 166.8 166.8 - - 167.2 166.9 60% evapoF 191.1 193.9 - - - 187.3 - - 226.8 193.2 191.2 - - 237.4191.3 70% evapoF 282.1 281.6 - - - 280.0 - - 284.7283.2280.9 - - 288.7281.6 80% evapoF 310.5312.0 - - - 309.9 - - 314.2309.7309.6 - - 316.8310.3 90% evapoF 337.7338.9 - - - 337.3 - - 342.1 337.7337.8 - - 344.1 337.9 95% evapoF 353.5352.9 - - - 352.8 - - 359.8353.1 351.0 - - 362.7352.7 FBPoF 371.7375.0 - - - 371.5 - - 369.7368.0372.7 - - 376.9371.8 Recovery vol. % 97.7 97.4 - - - 97.4 - - 97.1 97.2 97.1 - - 97.1 97.4 Residue vol. % 1.0 1.1 - - - 1.1 - - 1.1 1.1 1.1 - - 1.1 1.1 Loss vol. % 1.3 1.5 - - - 1.5 - - 1.8 1.7 1.8 - - 1.8 1.6 Corrected Recovery vol. % 97.9 97.4 - - - - - - - 97.1 97.4 - - - 97.5 Corrected Loss vol. % 1.1 1.5 - - - - - - - 1.8 1.5 - - - 1.5 DVPE (EPA equation) psi D5191 10.15 10.25 9.99 10.27 9.38 - 10.31 - - - 10.08 10.14 - 10.10 10.16 Aromatics vol. % D1319 - 35.2 - 35.1 35.4 36.0 - 35.4 - - - - 35.0 37.9 35.2 Olefins vol. % D1319 - 7.5 - 6.5 6.7 7.6 - 5.4 - - - - 5.8 6.8 6.6 Saturates vol. % * - - - - - - - - - - - - - - 38.1 Benzene vol. % D3606 - - - 0.63 - - 0.59 - - - - 0.60 0.69 0.75 0.65 S mg/kg D5453 24 29 24 25 - - 27 - - - - - - 25 25.7 RON - D2699 102.6 - 102.3 - - - 102.6 - - - - - - 101.3102.2 MON - D2700 88.1 - 88.6 - - - 88.2 - - - - - - 88.4 88.3 (RON+MON)/2 - - 95.4 - 95.5 - - - 95.4 - - - - - - 94.9 95.3 C mass %D5291 mod.**81.94 - - - 79.47 - - - - - - - 80.1080.9780.62 H mass %D5291 mod.**12.46 - - - 12.55 - - - - - - - 12.66 11.85 12.38 O mass % D5599 - - 7.5 7.4 - - 7.3 - - - - 6.6 - 7.1 7.2 Net Heat of Combustion MJ/kg D4809 39.578 - - - - - 39.352 - - - - - - 37.63438.855 Water mass % E-1064 - - - - - - 0.113 - - - - 0.120 - - 0.117 Lead g/l D3237 - - - - - - 0.001 - - - - - - - 0.001 Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - <0.5 - - - - - - - <0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 (**OptiDist** or equivalent) **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :26 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60o

### F g/cm3 

### D4052 0.75890.7594 - 0.75950.7594 - - - - - - - - - 0.7593 API Gravity, 60 o

### F o

### API D4052 54.7 54.6 - 54.6 54.6 - - - - - - - - - 54.6 Ethanol vol. % D5599 - - 15.9715.85 - 

### - 15.05 

### - - - - 14.19 - 15.1315.24 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.1 - - <0.10 Distillation IBP oF 87.4 90.2 - - - 91.1 - - 85.7 89.0 88.6 - - 92.9 88.7

5% evapoF 110.3110.4 - - - 109.3 - - 107.4109.3 110.8 - - 113.3109.6 10% evapoF 117.4118.0 - - - 116.7 - - 115.6 116.9 117.9 - - 119.4117.1 20% evapoF 128.3128.6 - - - 127.5 - - 126.6 127.3 128.2 - - 129.7127.8 30% evapoF 139.3139.2 - - - 137.9 - - 137.6 138.7 139.0 - - 140.1 138.6 40% evapoF 150.5 150.0 - - - 149.2 - - 149.2 149.8 150.0 - - 151.3149.8 50% evapoF 161.1 160.6 - - - 160.0 - - 159.7159.7 160.4 - - 161.3160.3 60% evapoF 177.5 176.4 - - - 175.6 - - 172.4172.9 173.6 - - 188.0 174.7 70% evapoF 277.9276.7 - - - 277.6 - - 275.7276.5277.3 - - 280.0277.0 80% evapoF 307.4308.3 - - - 307.6 - - 304.5305.4305.5 - - 312.7306.5 90% evapoF 339.4339.6 - - - 338.1 - - 338.1 338.4338.5 - - 344.1 338.7 95% evapoF 357.3357.4 - - - 357.1 - - 354.9356.5357.1 - - 357.1 356.7 FBPoF 376.0378.4 - - - 379.6 - - 373.5378.1 378.3 - - 376.4377.3 Recovery vol. % 98.5 97.7 - - - 98.1 - - 98.0 98.0 98.0 - - 97.4 98.1 Residue vol. % 1.1 1.1 - - - 1.1 - - 1.1 1.1 1.1 - - 1.1 1.1 Loss vol. % 0.4 1.2 - - - 0.8 - - 0.9 0.9 0.9 - - 1.5 0.9 Corrected Recovery vol. % 98.5 97.7 - - - - - - - 98.0 98.1 - - - 98.1 Corrected Loss vol. % 0.4 1.2 - - - - - - - 0.9 0.8 - - - 0.8 DVPE (EPA equation) psi D5191 10.2710.3710.08 10.33 9.50 10.1410.28 - - - 10.29 10.16 - 9.96 10.2 Aromatics vol. % D1319 - 35.1 - 35.6 34.7 37.3 - 35.4 - - - - 34.0 36.9 35.6 Olefins vol. % D1319 - 7.9 - 6.3 6.5 5.7 - 5.6 - - - - 6.5 6.8 6.5 Saturates vol. % * - - - - - - - - - - - - - - 42.7 Benzene vol. % D3606 - - - 0.60 - - 0.56 - - - - 0.59 0.69 0.67 0.62 S mg/kg D5453 22 26 21 22 - 24 22 - - - - - - 23 23 RON - D2699 102.4 - 101.7 - - - 101.6 - - - - - - 101.1 101.7 MON - D2700 88.3 - 88.9 - - - 88.0 - - - - - - 88.8 88.5 (RON+MON)/2 - - 95.4 - 95.3 - - - 94.8 - - - - - - 95.0 95.1 C mass %D5291 mod.**81.6 - - - 80.57 - - - - - - - 81.6682.0981.48 H mass %D5291 mod.**12.35 - - - 12.44 - - - - - - - 12.8312.18 12.45 O mass % D5599 - - 5.8 5.8 - - 5.5 - - - - 5.2 - 5.5 5.6 Net Heat of Combustion MJ/kg D4809 40.586 - - - - - 40.122 - - - - - - 40.44440.384 Water mass % E-1064 - - - - - - 0.084 - - - - 0.091 - - 0.088 Lead g/l D3237 - - - - - - <0.003 - - - - - - - <0.003 Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - <0.5 - - - - - - - <0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 (**OptiDist** or equivalent) **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :27 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60o

### F g/cm3 

### D4052 0.74320.7435 - 0.74350.7433 - - - - - - - - - 0.7434 API Gravity, 60 o

### F o

### API D4052 58.6 58.6 - 58.6 58.7 - - - - - - - - - 58.6 Ethanol vol. % D5599 - - 15.99 15.09 - 

### - 15.15 

### - - - - 14.18 14.31 14.71 14.91 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.1 0.09 - <0.10 Distillation IBP oF 104.5 102.4 - - - 104.7 - - 101.5 105.9 103.7 - - 110.6 104.8

5% evapoF 135.1 136.3 - - - 132.3 - - 134.5 134.7 136.6 - - 137.6 135.3 10% evapoF 142.5 142.5 - - - 141.2 - - 141.7142.3 143.0 - - 143.1 142.3 20% evapoF 152.1 152.4 - - - 151.4 - - 151.5 152.1 151.8 - - 152.7152.0 30% evapoF 158.8 158.5 - - - 158.2 - - 155.0 158.6 158.4 - - 158.7158.0 40% evapoF 164.0 164.6 - - - 163.3 - - 163.0 164.1 163.3 - - 164.1 163.8 50% evapoF 219.7221.6 - - - 218.1 - - 223.6219.7222.4 - - 225.3221.5 60% evapoF 249.9249.9 - - - 351.1 - - 250.5250.8251.6 - - 252.0265.1 70% evapoF 273.5275.2 - - - 274.2 - - 276.6274.4274.6 - - 275.8274.9 80% evapoF 310.5310.4 - - - 309.6 - - 312.5309.6310.8 - - 315.9311.3 90% evapoF 340.1 339.3 - - - 339.3 - - 341.4340.0340.2 - - 342.1 340.3 95% evapoF 351.4352.3 - - - 351.0 - - 354.4350.8351.6 - - 351.8351.9 FBPoF 373.7374.3 - - - 373.7 - - 368.0367.0376.2 - - 372.4372.2 Recovery vol. % 98.3 98.3 - - - 97.6 - - 97.7 97.6 98.3 - - 97.5 98.1 Residue vol. % 1.0 1.0 - - - 1.0 - - 1.0 1.0 1.0 - - 1.0 1.0 Loss vol. % 0.7 0.7 - - - 1.4 - - 1.3 1.4 0.7 - - 1.5 0.9 Corrected Recovery vol. % 98.3 98.3 - - - - - - - 97.6 98.3 - - - 98.1 Corrected Loss vol. % 0.7 0.7 - - - - - - - 1.4 0.7 - - - 0.9 DVPE (EPA equation) psi D5191 7.01 7.03 6.87 6.99 6.35 6.90 7.04 - - - 7.00 7.01 - 6.92 6.97 Aromatics vol. % D1319 - 14.6 - 14.9 15.3 14.6 - 14.1 - - - - 14.3 16.2 14.9 Olefins vol. % D1319 - 8.0 - 7.2 7.2 7.7 - 6.0 - - - - 7.5 8.1 7.4 Saturates vol. % * - - - - - - - - - - - - - - 62.9 Benzene vol. % D3606 - - - 0.57 - - 0.53 - - - - 0.54 0.51 0.66 0.56 S mg/kg D5453 25 28 24 26 - - 26 - - - - - - 26 26 RON - D2699 101.6 - 100.5 - - - 100.7 - - - - - - 100.2 100.8 MON - D2700 88.8 - 89.6 - - - 89.1 - - - - - - 89.4 89.2 (RON+MON)/2 - - 95.2 95.1 - - - 94.9 - - - - - - 94.8 95.0 C mass %D5291 mod.**80.05 - - - 79.54 - - - - - - - 80.41 81.0880.27 H mass %D5291 mod.**13.96 - - - 14.05 - - - - - - - 14.19 13.85 14.01 O mass % D5599 - - 5.9 5.6 - - 5.6 - - - - 5.3 5.3 5.5 5.5 Net Heat of Combustion MJ/kg D4809 41.200 - - - - - 40.830 - - - - - - 41.15641.062 Water mass % E-1064 - - - - - - 0.088 - - - - 0.091 - - 0.090 Lead g/l D3237 - - - - - - <0.003 - - - - - - - <0.003 Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - 0.5 - - - - - - - 0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 (**OptiDist** or equivalent) **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :28 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60o

### F g/cm3 

### D4052 0.76970.7701 - 0.77000.7699 - - - - - - - - - 0.7699 API Gravity, 60 o

### F o

### API D4052 52.1 52.1 - 52.1 52.1 - - - - - - - - - 52.1 Ethanol vol. % D5599 - - 15.50 15.73 - 

### - 14.96 

### - - - - 14.41 14.6714.59 14.98 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.1 0.09 - <0.10 Distillation IBP oF 104.5 104.5 - - - 105.6 - - 100.6 104.8 103.2 - - 107.4103.9

5% evapoF 136.7138.0 - - - 133.8 - - 135.4137.0 137.0 - - 136.1 136.3 10% evapoF 144.6 144.9 - - - 142.9 - - 143.5 144.6 144.8 - - 143.6 144.2 20% evapoF 154.3154.3 - - - 153.3 - - 153.7154.0 154.2 - - 153.0 154.0 30% evapoF 160.6 160.5 - - - 160.0 - - 159.2 160.8 160.0 - - 159.0 160.2 40% evapoF 167.3165.4 - - - 166.5 - - 162.6 167.5 165.7 - - 164.3165.8 50% evapoF 216.7215.8 - - - 215.9 - - 216.9216.6217.7 - - 219.2216.6 60% evapoF 239.7240.2 - - - 240.1 - - 237.8241.2242.0 - - 241.3240.2 70% evapoF 249.0 254 - - - 253.2 - - 247.3253.2252.6 - - 253.9251.6 80% evapoF 269.1 269.1 - - - 268.0 - - 267.7268.2268.3 - - 270.3268.4 90% evapoF 298.9299.4 - - - 298.6 - - 298.4298.0299.5 - - 303.2298.8 95% evapoF 328.4327.3 - - - 327.5 - - 326.0326.5327.8 - - 336.5327.3 FBPoF 363.8366.3 - - - 362.8 - - 362.4359.1 364.5 - - 364.3363.2 Recovery vol. % 98.3 98.2 - - - 97.7 - - 98.5 98.2 98.3 - - 98.2 98.3 Residue vol. % 1.0 1.0 - - - 1.0 - - 1.0 1.0 1.0 - - 1.0 1.0 Loss vol. % 0.7 0.8 - - - 1.3 - - 0.5 0.8 0.7 - - 0.8 0.8 Corrected Recovery vol. % 98.3 98.2 - - - - - - - 98.2 98.4 - - - 98.3 Corrected Loss vol. % 0.7 0.8 - - - - - - - 0.8 0.7 - - - 0.8 DVPE (EPA equation) psi D5191 6.92 6.93 6.77 6.92 6.20 - 6.93 - - - 6.83 6.83 - 6.80 6.87 Aromatics vol. % D1319 - 34.6 - 34.5 34.1 34.6 - 33.7 - - - - 33.4 36.5 34.5 Olefins vol. % D1319 - 8.4 - 6.6 7.3 6.9 - 5.4 - - - - 7.1 7.2 7.0 Saturates vol. % * - - - - - - - - - - - - - - 43.5 Benzene vol. % D3606 - - - 0.57 - - 0.54 - - - - 0.55 0.59 0.69 0.59 S mg/kg D5453 22 26 22 24 - - 24 - - - - - - 24 24 RON - D2699 103.2 - 102.9 - - - 102.8 - - - - - - 101.8 102.7 MON - D2700 89.0 - 89.8 - - - 88.9 - - - - - - 89.8 89.4 (RON+MON)/2 - - 96.1 - 96.4 - - - 95.9 - - - - - - 95.8 96.1 C mass %D5291 mod.**82.17 - - - 81.02 - - - - - - - 81.8682.0581.78 H mass %D5291 mod.**12.58 - - - 12.60 - - - - - - - 12.79 12.50 12.62 O mass % D5599 - - 5.5 5.6 - - 5.4 - - - - 5.2 5.3 5.2 5.4 Net Heat of Combustion MJ/kg D4809 40.442 - - - - - 40.180 - - - - - - 40.52840.383 Water mass % E-1064 - - - - - - 0.088 - - - - 0.094 - - 0.091 Lead g/l D3237 - - - - - - <0.003 - - - - - - - <0.003 Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - <0.5 - - - - - - - <0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 (**OptiDist** or equivalent) **Average TEST**  **METHOD PROPERTY**  **UNIT Laboratory** 

## Phase 3 of EPAct/V2/E-89 Program

Fuel Inspection Data

Fuel :29 **Red fill color indicates an outlier Orange fill color indicates data not included in parameter averages** 

Lab A Lab B Lab C Lab D Lab E F G H I J K L M N O Density, 60oF g/cm3 D4052 0.77970.78000.78180.78290.7788 - - - 0.77980.7798 - - - 0.7799 - 0.7797 API Gravity, 60oF oAPI D4052 49.8 49.7 49.3 49.1 49.8 - - - 49.8 49.8 - - - 49.8 - 49.8 Uncorrected Ethanol mass % D5501 mod.* - - 80.28 - - - - - - - 78.90 - - - - 79.59 Uncorrected Methanol mass % D5501 mod.* - - - - - - - - - - 0.01 - - - - 0.01 Ethanol vol. % D5501 mod.* 75.80 - 78.51 77.39 - - - - - - 76.88 - - 76.24*** - 77.15 Methanol vol. % D5501 mod.* Not detected Not

detected Not

detected Not

detected Not

detected - - - - - <0.01 - - **0.62***** - <0.01 Estimated Hydrocarbon Content vol. %100 - D5501Ethanol - E203Water 23.57 - 20.69 21.91 - - - - - - 22.40 - - 23.04*** - 22.14 Distillation IBP oF 105.1 92.3 109.0 102.1 102.0 - - 105.1 99.5 - 95.3 94.9 90.6 102.6 - 99.0

5% evapoF 123.6 132.1 135.1 135.6 135.5 - - 129.6 127.7 - 132.4 136.3 132.6 143.6 - 132.9 10% evapoF 147.3 153.7 158.0 156.4 154.9 - - 151.3 154.0 - 155.6 156.0 155.1 158.6 - 154.3 20% evapoF 165.6 168.2 170.4 167.6 167.4 - - 167.2 168.7 - 168.7 167.5 167.5 168.0 - 167.6 30% evapoF 169.4 170.8 172.7 170.0 169.9 - - 170.2 171.3 - 171.2 170.0 170.0 170.2 - 170.3 40% evapoF 170.5 171.7 173.8 170.8 170.8 - - 171.3 172.2 - 172.1 170.9 170.9 171.1 - 171.2 50% evapoF 171.2 172.1 174.3 171.3 171.3 - - 171.9 172.6 - 172.7 171.6 171.4 171.4 - 171.8 60% evapoF 171.6 172.5 174.7 171.7 171.7 - - 172.2 173.0 - 173.0 171.9 171.8 171.9 - 172.1 70% evapoF 172.0 172.8 175.1 172.2 172.0 - - 172.6 173.4 - 173.4 172.2 172.2 172.3 - 172.5 80% evapoF 172.5 173.2 175.4 172.4 172.4 - - 172.9 173.7 - 173.6 172.6 172.6 172.7 - 172.9 90% evapoF 173.6 174.1 176.1 173.9 173.3 - - 173.8 174.5 - 174.7 173.6 173.7 173.7 - 173.9 95% evapoF 175.4 176.1 177.9 177.6 175.5 - - 175.8 176.3 - 176.9 175.9 176.0 176.1 - 176.2 FBPoF 180.6 269.9 181.9 180.6 299.1 - - 298.2 263.5 - 294.5 286.9 292.0 292.8 - 265.8 Recovery vol. % 96.3 98.0 95.9 95.6 98.5 - - 98.6 97.6 - 98.3 97.4 97.6 99.1 - 98.1 Residue vol. % 1.6 1.1 1.7 1.6 0.8 - - 0.9 0.6 - 0.6 0.9 0.9 0.9 - 0.8 Loss vol. % 2.2 0.8 2.4 2.8 0.7 - - 0.5 1.8 - 1.1 1.7 1.5 0 - 1.1 Corrected Recovery vol. % - - - - - - - 98.6 98.0 - 98.5 97.3 97.7 99.0 - 98.2 Corrected Loss vol. % - - - - - - - 0.5 1.4 - 0.9 1.8 1.4 0.1 - 1.0 DVPE (EPA equation) psi D5191 9.01 9.04 8.76 7.72 9.02 - - 8.58 9.05 8.12 9.07 - 8.86 - - 8.92 Benzene vol. % D5580 - - - - - - - 0.12 - - - - - - 0.12 S mg/kg D5453 - - - - - - 18 - 16 - - - - 14 - 16 C mass % D5291 mod.** - - - - - 57.88 - - - 57.66 - - - 57.04 58.39 57.74 H mass % D5291 mod.** - - - - - 13.1 - - - 12.08 - - - 13.08 12.92 12.80 O mass % D5501 mod.* 26.76 - 27.65 27.21 - - - - - - 27.15 - - 27.03*** - 27.19 mass % E203 0.81 0.96 1.03 0.90 0.95 - - - - - - - - 0.91 - 0.93 vol. % E203 0.63 0.75 0.80 0.70 0.74 - - - - - - - - 0.71 - 0.72 Net Heat of Combustion MJ/kg D4809 30.058 - - - - - - - - - 30.058 Solvent Washed Gum mg/100 ml D381 - - - - - 2.8 1.0 - - - - - - - - 1.9 Unwashed Gum mg/100 ml D381 - - - - - 0.6 3.0 - - - - - - - - 1.8 Acidity (as acetic acid) mass % D1613 - - - - - - 0.0021 - - - - - - - - 0.0021 pHe - D6423 - - - - - - 7.96 - - - 8.20 - - - - 8.08 Inorganic Chloride mg/kg D7319 - - - - - - Not detected - - - - - - - - Not detected Copper mg/l D1688 modified as outlined in D4806 - - - - - - 0.02 - - - - - - - - 0.02 * Method adapted by individual laboratories to testing of E85 fuels ** Method adapted by individual laboratories to testing of gasolines *** Data not included in parameter averages due to suspected sample contamination with methanol Water **TEST METHOD Average**  **Data From 2008 CRC E85 Class Volatility Program Round Robin Participant**  **PROPERTY UNIT** 

D86 (**non-OptiDist**)

## Phase 3 of EPAct/V2/E-89 Program Fuel Inspection Data

Fuel :30 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60o

### F g/cm3 

### D4052 0.75050.7509 - 0.75090.7508 - - - - - - - - - 0.7508 API Gravity, 60 o

### F o

### API D4052 56.8 56.8 - 56.8 56.8 - - - - - - - - - 56.8 Ethanol vol. % D5599 - - 10.69 9.88 - 

### - 9.74 

### - - - - 9.86 9.67 9.91 9.8 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - 

### - <0.01 

### - - - - <0.1 0.07 - <0.10 Distillation IBP oF 91.9 91.0 - - - 92.4 - - 90.388.2 91.6 - - 92.0 90.9

5% evapoF 110.9 110.4 - - - 109.8 - - 110.8109.7 110.4 - - 108.0 110.3 10% evapoF 117.0 117.1 - - - 116.1 - - 116.6116.4 116.9 - - 115.0 116.7 20% evapoF 125.4126.1 - - - 124.7 - - 125.4125.3 125.2 - - 125.0 125.4 30% evapoF 134.4134.5 - - - 132.2 - - 134.1134.0 133.9 - - 134.0 133.9 40% evapoF 143.4143.6 - - - 142.6 - - 142.9143.2 143.1 - - 143.0 143.1 50% evapoF 153.4153.6 - - - 152.8 - - 151.7152.9 153.0 - - 152.0 152.9 60% evapoF 196.8 197.2 - - - 196.4 - - 200.7196.7 195.5 - - 208.0 197.2 70% evapoF 266.8267.2 - - - 267.9 - - 268.3266.7266.7 - - 270.0267.3 80% evapoF 295.4295.7 - - - 294.1 - - 294.4294.2293.9 - - 298.0294.6 90% evapoF 324.3323.5 - - - 323.9 - - 324.1323.4323.6 - - 329.0323.8 95% evapoF 341.9341.8 - - - 341.4 - - 341.6341.7342.5 - - 333.0341.8 FBPoF 366.5368.7 - - - 366.4 - - 363.6362.7368.6 - - 364.0366.1 Recovery vol. % 98.2 97.7 - - - 98.1 - - 97.998.1 97.8 - - 97.2 98.0 Residue vol. % 1.0 1.0 - - - 1.0 - - 1.01.0 1.0 - - 1.0 1.0 Loss vol. % 0.8 1.3 - - - 0.9 - - 1.10.9 1.2 - - 1.8 1.1 Corrected Recovery vol. % 98.3 97.7 - - - - - - - 98.0 98.0 - - - 98.0 Corrected Loss vol. % 0.7 1.3 - - - - - - - 1.0 1.0 - - - 1.0 DVPE (EPA equation) psi D5191 10.2710.28 10.15 10.33 9.44 10.25 10.37 - - - 10.26 10.08 - 10.0410.23 Aromatics vol. % D1319 - 33.9 - 35.6 34.5 36.0 - 34.1 - - - - 37.4 37.1 35.5 Olefins vol. % D1319 - 6.8 - 5.7 6.7 6.2 - 5.7 - - - - 7.7 6.4 6.5 Saturates vol. % * - - - - - - - - - - - - - - 48.2 Benzene vol. % D3606 - - - 0.58 - - 0.53 - - - - 0.56 0.53 0.70 0.58 S mg/kg D5453 21 25 21 21 - - 24 - - - - - - 25 23 RON - D2699 101.3 - 100.5 - - - 100.5 - - - - - - 100.4100.5 MON - D2700 87.8 - 88.7 - - - 87.6 - - - - - - 88.3 88.1 (RON+MON)/2 - - 94.6 - 94.6 - - - 94.1 - - - - - - 94.4 94.3 C mass %D5291 mod.**83.78 - - - 82.64 - - - - - - - 83.5882.6683.17 H mass %D5291 mod.**12.36 - - - 12.88 - - - - - - - 12.9313.8313.00 O mass % D5599 - - 3.9 3.6 - - 3.6 - - - - 3.6 3.6 3.7 3.6 Net Heat of Combustion MJ/kg D4809 41.474 - - - - - 41.088 - - - - - - 41.35041.304 Water mass % E-1064 - - - - - - - - - - - 0.086 - - 0.086 Lead g/l D3237 - - - - - - - - - - - - - - - Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - <0.5 - - - - - - - <0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines D86 (**OptiDist** or equivalent) **Average PROPERTY**  **UNIT TEST**  **METHOD Laboratory** Phase 3 of EPAct/V2/E-89 Program

Fuel Inspection Data Fuel : 31 **Red fill color indicates an outlier**

1 2 3 4 5 6 7 8 9 10 11 12 13 14 Density, 60 oF g/cm3 D4052 0.7739 0.7744 - 0.7743 0.7742 - - - - - - - - - 0.7742 API Gravity, 60 oF oAPI D4052 51.1 51.0 - 51.1 51.1 - - - - - - - - - 51.1 Ethanol vol. % D5599 - - 20.86 20.95 - - 20.19 - - - - 18.45 - 20.08 20.11 Total Content of Oxygenates Other Than Ethanol vol. % D5599 - - - - - - <0.01 - - - - <0.1 - - <0.10 Distillation IBP oF 104.0 105.9 - - - 109.7 - - - 103.1 106.1 - - 106.3 105.8 5% evap oF 132.3 133.8 - - - 133.3 - - - 131.5 131.7 - - 133.8 132.5 10% evap oF 139.0 139.8 - - - 139.5 - - - 138.7 138.5 - - 139.5 139.1 20% evap oF 147.8 148.2 - - - 147.8 - - - 147.5 147.2 - - 148.6 147.7 30% evap oF 155.3 155.5 - - - 154.9 - - - 154.9 154.7 - - 155.9 155.1 40% evap oF 161.8 161.1 - - - 161.5 - - - 161.2 161.1 - - 162.1 161.3 50% evap oF 167.6 167.9 - - - 167.4 - - - 167.3 166.4 - - 166.8 167.3 60% evap oF 215.4 218.5 - - - 210.8 - - - 214.2 210.9 - - 236.1 214.0 70% evap oF 270.5 273.5 - - - 270.3 - - - 272.3 271.3 - - 274.0 271.6 80% evap oF 297.7 298.7 - - - 297.2 - - - 296.4 294.8 - - 301.8 297.0 90% evap oF 325.6 325.6 - - - 324.6 - - - 325.0 325.1 - - 329.6 325.2 95% evap oF 342.5 343.5 - - - 341.7 - - - 340.8 342.1 - - 349.6 342.1

FBP oF 365.2 366.5 - - - 365.8 - - - 362.9 367.5 - - 366.0 365.6 Recovery vol. % 98.5 98.8 - - - 98.4 - - - 97.9 97.9 - - 97.6 98.3 Residue vol. % 1.0 1.0 - - - 1.0 - - - 1.0 1.0 - - 1.0 1.0 Loss vol. % 0.5 0.2 - - - 0.6 - - - 1.1 1.1 - - 1.4 0.7 Corrected Recovery vol. % 98.5 98.8 - - - - - - - 97.9 98.1 - - - 98.3 Corrected Loss vol. % 0.5 0.2 - - - - - - - 1.1 0.9 - - - 0.7 DVPE (EPA equation) psi D5191 7.05 7.07 6.92 7.05 6.25 - 6.98 - - - 7.00 6.88 - 6.88 6.98 Aromatics vol. % D1319 - 35.6 - 35.4 35.8 37.0 - 35.4 - - - - 35.4 38.0 35.5 Olefins vol. % D1319 - 8.4 - 6.6 6.5 6.8 - 5.8. - - - - 6.7 5.7 6.8 Saturates vol. % * - - - - - - - - - - - - - - 37.6 Benzene vol. % D3606 - - - 0.61 - - 0.60 - - - - 0.60 0.60 0.79 0.60 S mg/kg D5453 24 28 24 26 - - 27 - - - - - - 22 25 RON - D2699 102.4 - 101.8 - - - 101.9 - - - - - - 100.7 101.7 MON - D2700 87.8 - 88.7 - - - 88.0 - - - - - - 88.1 88.2 (RON+MON)/2 - - 95.1 - 95.3 - - - 95.0 - - - - - - 94.4 95.0 C mass %D5291 mod.** 79.94 - - - 79.12 - - - - - - - 80.14 80.41 79.90 H mass %D5291 mod.** 12.36 - - - 12.51 - - - - - - - 12.65 12.45 12.49 O mass % D5599 - - 7.4 7.5 - - 7.2 - - - - 6.6 - 7.2 7.2 Net Heat of Combustion MJ/kg D4809 39.702 - - - - - 39.204 - - - - - - 39.266 39.391 Water mass % E-1064 - - - - - - - - - - - 0.143 - - 0.143 Lead g/l D3237 - - - - - - <0.003 - - - - - - - <0.003 Copper Strip Corrosion - D130 - - - - - - 1A - - - - - - - 1A Solvent Washed Gum mg/100ml D381 - - - - - - 0.5 - - - - - - - 0.5 Oxidation Stability min. D525 - - - - - - >240 - - - - - - - >240 * Calculated using the following equation: Saturates = 100 - D1319Aromatics - D1319Olefins - D5599Ethanol ** Method adapted by individual laboratories to testing of gasolines **Average**

**PROPERTY UNIT**  **Laboratory**

D86 (**OptiDist** or equivalent) **TEST METHOD**