p. 1 

# OAR Box 

# 1670 Prepped by Charmelle Mathews



### Document

Number: 

# 3< g ^ ) ll-D-17 0 Docket Number: 

# A-98-1 3

Printed 9/24/2008 11:55:14

AM Sheet 39 of 56P. 2 

# L

_PAKTAN KCORPORATIO N Augus t 17 , 199 8

Bruc e C . Jordan , Directo r Emissio n Standard s Divisio n (MD-13 ) Office o f Air Qualit y Plannin g an

d Standard s U.S . Environmenta

l Protectio n Agency Researc h Triangl e Park , N C 2771 1 Attention : Stephe

n Shed d RE : Exxo n Chemica

l Compan y - Lelan dTermina

l O.L.D . Surve

y Dea r Mr . Jordan : 

### A 9 8 1 3 

### II- O 

# - n o 200 0 Wes

t Loo p South , Suit e 220 0 Houston , Texas 77027-359 7 (713)623-000 0 FAX : (713 ) 623-448 0 E-Mail : paktank@pakhoedcorp.co m 

# FIL E COP Y 9t>/e£'G c 

# *

* • '.' V

t PAr.lRUOCKF. T 

### Enclose d pleas e fm

d acomplete d O.L.D . Surve y fo r the Exxon LelandTerminal . Paktan k Corporatio n complete d th e surve y a s w e are th e operato r

o f thi s termina

l fo r Exxo n Chemica

l Company . A s asupplier

to severa l member s o f

the Nationa

l Associatio n o f

Chemica l Distributors , Exxo n believe s tha

t som e o f th e informatio n requeste dby th e EP A i n thi s surve

y shoul db e treate d a s Confidentia

l Busines s Informatio n (CBI) . Th e following numbereditem s are ou r reques t fo r confidentialit

y an d rationale : 1 : Organi c Liqui d Handle d and HAP Conten t III . HJ\ P Constituent : Averag e Liqui dWeigh t % / averag e Vapor

Weight % RE : MSD S onl

y contain s HAP s constituent , no t it s percent

in produc t 2 : Storag e Tan

k Contro l Dat

a (c ) Name(s ) o

f Store d Liquid(s ) RE : Would provide competitor wit h tan k capacit y & throughput

fo r eac h o f our trademarke d an

d sol e suppl

y product s a

t eac h distributor

o r terminal . 3 : Liqui d Transfe

r Operation s (a) Organi c Liqui d Transferre dthroug h Facilit y RE : Sam e rational e as no . 2 , above . Pleas e not e tha t w e hav e enclose d tw o separat e copie s o f the surve y fo r eac h facility . On

e cop y i s complet

e an d stamped Confidential , an dth e secon

dcop y has the confidentia

l informatio n deleted .P. 3

'.»* > ? 

### Bruc e Jordan , Directo r Augus t 17 , 199 8 Pag e 2 Shoul d yo u hav e an

y question s regardin g thi s survey , pleas e contac t Thoma s Lando r

me a t (713 ) 623-0000 . Ver y trul y yours , 

# ~JZ%Z,r/^e<// Quirin o Q . Won

g Manager , Environmenta

l Affairs On behal f of Exxon Chemica

l Compan y - LelandTermina

l QQW/TDL:rm m



# 2 _P. 4



### Bruc e C . Jordan , Directo r Emissio n Standard s Divisio n (MD-13 ) Offic e o f Ai r Qualit y Plannin g an d Standard s U . S . Environmenta l Protectio n Agenc y Researc h Triangl e Park , N C 2771 1 Attention : Stephe n Shed d II . GENERA L INFORMATION A . Name oflega l owne

r (i.e. , paren

t company ) ofplant : Exxon Chemica l Compan y B . I s th e compan

y publicly o

r privately owned ? Publi c C . Nam e oflega l operator ofplant , i f

differen t fromlega l owner : Paktan

k Corporatio n D . Addres s oflega l owner/operato r (pleas e specif

y which) : Paktan

k Corporation . 200 0 Wes t Loop South . Suit

e 2200 . Houston . Texa s 77027 E . Siz e o f company/plant : 1 . Approximat

e numbe r of employee s of

th e busines s enterpris e tha

t owns thi s plant , includin g wher

e applicable , th e paren

t compan y an dall subsidiaries , branches , and unrelate d establishment s ownedby th e paren t company : 80.00 0 2 . Tota l numbe r of employee s ofth e busines s enterpris e tha t operates thi s plant : -0 - 3 . a) Numbe

r o f employee s a

t th e entir e plant site 2 b ) Numbe

r o f employee s associate dwit

h th e organi c liquid s distributio n (non gasoline ) operation s a

t thi s plant : 2 c ) Numbe r o f organi c liquid s distributio n operation s employee s tha t ar e contract employee s 2 F . Name ofplant : Exxon Chemica l Compan y - LelandTermina

l G . Street addres s ofplant : 3500 Moun t Miser y Roa d City , State , Zip code : Leland . N C 2845 1 H . Du n and Bradstreet

number : 00-121-321 4 

# 3P. 5



### 2 I . Latitud e and longitud

e coordinate s o f

plant : 34 ° 15'28 " N 77°22'0 " J . Name o f

contact(s ) abl e to answe

r technica l question s about

th e complete dsurvey : Name Thoma s Lan

d Titl e Environmenta

l Specialis t Telephon e 713-623-000 0 Nam e Jaso n Whichar

d Titl e Safety . Healt

h & Environmenta

l Specialis t Telephon e 910-799-0144



# AP. 6

TABL E 1 . ORGANI C LIQUID S HANDLE D AN D HA P CONTENT(a ) (SURVEYE D LIQUIDS ) I . Organi c Liqui d Name (b ) "CBI " Se e separat e repor t submitta l II . Propertie s (us e th e sam e referenc e temperatur

e fo r a . an d b. , an d indicat e temperature. ) a . Averag e Tru e Vapo

r Pressur e (psia) : b . Densit y (lb/gal) : c . Rei d Vapor

Pressur e (psia) : d . Liqui d Molecula

r Weigh t (lb/lb-mo l @ 70°F) : e . Vapor Molecula r Weigh t (lb/lb-mo l @ 70°F) : 0.1413(g) . 71.37 ° F



### 747 ? 0.319 1 106.1 6 III . HA P Constituent s (ofth e organi c liqui d listed above) : HA P Constituen

t (c ) 1, 4 dimethyibehzen e '-'

- ? > ' " CA

S No . 106-42- 3 Averag e Liquid

Weigh t % 99.7 % Averag e Vapo r Weigh t %

(Note: Insert

lines as required

to list all HAPconstituents in the organic liquid. Make sufficient copies ofthis sheet to list all your organic liquids and

their HAPconstituents.) a) . D o no t

lis t wastewate

r i n thi s tabl e (fo

r wastewater , refe

r t o Table s 4 an

d 5) . b) . Provid e th e complet e nam e fo r the organi c liqui d bein g reported . Ifth e liqui d i s pur e HAP , refe r t o Attachment

A an d us e the nam

e o r CA S numbe

r shown . Fo

r organi c liquid s reference d i n Tabl e 8 , th e famil

y nam e ofth e liqui d ma

y b e used i n lie u of listin g eac h individua

l blend . c) . Lis t

al l th e HA

P constituent s presen

t i n the organi c liqui d identified i n ite mI . Refe r t o Attachment

A fo r acomplet e HA P nam e an d CAS No . listing . 

# 6

### TABL E 2 . STORAG E TAN K CONTRO L DAT A



# G^ Tan

k I D Cod e (a) T-214 9 Tan

k Capacit y (gal ) (b ) CB I Name(s ) o f Store d Liquid(s ) (c ) CB I

• Annua l Throughput (gal/yr) (d ) CB I Roo f

Configuratio n (e ) FX R Floatin g Roo f

Tan k Only : Sea l Typ e 

### ffl Tan

k Roo f Fitting s (g ) Add-o n

Contro l Devic e 

### 0 0 N Applicabl e Ai r

Regulation s 

### ( 0 Pre-k

Se e en dof tabl e fo r footnotes .

T J

### TABLE 3 . LIQUI D TRANSFE ROPERATION S



# - a Organi c Liqui d Transferre d throug h Facilit y (a ) CB I Incomin g Typ e o f Transpor t Vehicl e o r Containe r (b ) P L Loadin g Rac k I D Cod e (c ) Loadin g Ar m

I D Cod e (d ) Outgoin g

Typeo f Transpor t Vehicl e o r Containe r (b ) P L Annua l Volum e

o f Transferre d Liqui d (gal/yr ) CB I Metho d o f

Loadin g o r Unloadin g (e ) BT M Averag e

Loadin g o r Unloadin g Rat e pe r Ar m (gal/min ) CB I Vapo r

Contro l Devic e 

### ( 0 Contro l

Devic e Efficienc y (g )

Se e en do f tabl e fo r footnotes .

T J 0 0TABL E 4 . WASTEWATE RFLO W RATE S AN D DRAI N CONTROL S



# C O Sourc e o f OL D Wastewate r (a ) N/ A Tota l Flo w Rat e (gal/yr ) HA P Nam e

(b ) HA P Concentratio n

i n Wate r (ppmw ) (c ) Numbe r

o f Drain s wit h Emissio n Suppressio n (d ) Numbe r o f Drain s withou t Emissio n Suppressio n (d )

a) . OLD = Organi c Liquid s Distribution . Selec t th e code s that

bes t describ e th e point s o f

wastewate r

generatio n (insert

code s a s require d an d provid e aful

l description) : TC =tan

k cleaning s L R=loadin g rack s (identif y th e specifi c rack s usin g th e sam e rac k code s a s i

n footnot e "a " o f Tabl e 3 . L C = lin e cleaning s L B =liqui dblending/packagin g operation s O T =other , pleas e provide ful l descriptio n (us e extr asheet , if necessary) . b) . Lis t

th e principa

l HAP s typicall y present

i n eac h wastewate

r stream . c) . Estimate d annua

l averag e concentratio n durin g period s o f nomina l flo w i n ppmw . d) . Emissio n suppressio n control s reduc e emission s fromdrai n pipe s an d include , bu t are no t limite d to , water

seal pot s an d p-traps .

T J C O

## TABL E 5 . WASTEWATE R COLLECTIO NAN D TREATMENT CONTRO L (a )



# - 0 OL D Wastewate

r Treatmen t Uni t Tota

l Numbe r o f Unit s o n Sit e (c ) No . o f

Uncovere d Unit s tha t Ven t to th e Atmospher

e (d ) No . o f

Covere d Unit s tha t Ven t t o th e Atmospher

e (d ) No . o f

Unit s tha t Ven t Emission s to a Contro l Devic e Contro l Devic e (e ) Sourc e of Wastewate

r (b) : No t

Applicabl e CatleMonVaH s Manhole s Junctio n Boxe s Sumps/Catc

h Basin s Lif t Station s Storag e Tank

s 

### ( 0 N/

A N/ A N/ A N/ A N/ A Treatmen t Unit s Oil/Wate r Separator s Ai r Flotation System s Coagulation/Precipitatio n Unit s San d Filtratio n Uni

t Equalizatio n Unit s N/ A N/ A N/ A N/ A N/ A See en do f tabl e fo r footnotes .

T J OTABL E 5 . WASTEWATE RCOLLECTIO N AN D TREATMEN T CONTRO L (a ) (Continued )



# 0 OL D Wastewate

r Treatmen t Unit Tota

l Numbe r o f Unit s on Sit

e 

### ( 0 No . o f

Uncovere d Unit s tha t Ven t t o th e Atmospher

e (d ) No . o f

Covere d Unit s tha t Ven t t o th e Atmospher

e (d ) No . o f

Unit s tha t Ven t Emission s t o a Contro l Devic e Contro l Devic e (e ) Sourc e of Wastewate

r (b) : No t Applicabl e Treatment : Units Oxidation Pond s ActivatedSludg e Unit s Trickling Filter s Clarifier s Filte r Presse s Stripper s Effluent/Recycle Pon

d Rotating Biologica

l Contractor s Shi p Of f Sit e 

### G O N/ A N/ A N/ A N/ A N/ A N/ A N/ A N/ A 0 See endof tabl e fo r footnotes .

### TABL E 6 . SEMI-AQUEOU S WAST E COLLECTIONAN D CONTRO L (a )

Type of Wast e (b ) Not Applicabl e Wast

e Generatio n Rat e (tons/year) (c ) Wast

e Collecte d i

n aClose d System ? (Yes/No ) (d ) Metho d o f

On-Sit e Storag e (e ) Wast

e Treate d or Dispose d o f

On Site ? (Yes/No ) 

### ffl Metho d o f

On-Sit e Treatmen t or Disposa l (g ) Contro l Devic e o n

Treatment o r Disposa l Uni t (h )

Se e en do f tabl e fo r foomotes .

T J t oP.1 3

1 0 TABL E 7 . EQUIPMEN T LEA K CONTRO L DAT A 1 . I s ther e aformal , periodi c equipmen t leak detectio n an d repai r

(LDAR ) program ? Ye s • N o X Comments : 2 . Pleas e indicat e whic h Federal/State/loca l rule s requir e an LDA Rprogra ma t thi s facility : a V N/ A b) . c) . 3 . I f aforma l equipmen t

LDA Rprogra mha s bee n implemente d at you r plant , provid e th e followin g information : Definition ofaLeak

* Lea k Detectio n Method b Lea k Respons e Time

0 E

B 5/1 5 a) . Lea k definitio n codes : A = 50 0 ppm v E = Sensor y detectio n D = Bubbl e formatio n b) . Leak detectio n codes : A = EP A Metho d 2 1 (vapo r detector) B = Sigh t (e.g. , drips) , smell , soun d C = Ga s detection/alar msyste m C = 10,00 0 ppm v B = 1,000 ppm v O T = Othe r

(specify )

D = Soap wate r

applicatio n E = Non e O T = Othe r c) . Provid e th e maximu mallowabl e tim e after detectio n t o begi n an d complet e repai r of aleak .



# IJ)

# bz n TABL E 7 . EQUIPMEN T LEA K CONTRO L DAT A (Concluded ) Equipmen t Componen

t Valve s Compressor s Flange s Pump s Samplin g Connection s Pressur e relie f valve s (t o atmosphere ) Inspectio n

Frequenc y (a ) 4 0

- 10 9 1

-

- Tota

l Equipmen t Coun t 4 0

- 10 9 1

—

- Equipmen

t Coun t i n LDA R Progra m 0

- 0 0

-

- Equipmen

t Coun t in LDA Rwit h HA P Servic e 0

- 0 0

-

- Equipmen t Count s wit h Mechanica

l Contro l Device s (b ) 0

- - 0 0

-

- Equipment Count s wit

h a Close d Vent

System (c ) 0

— 0 0

—

— Close d Ven t Syste mContro l Devic e (d ) 0

- 0 0

-

- a) . Inspectio n Frequenc y Codes : M = Monthl y A = Annuall y O T = Othe r

(specify ) T = On e tim e onl y Q = Quarterl y E = Afte r equipmen t

chang e b) . Provid e equipmen t count s fo r

equipmen t

i n HA P servic e wit h mechanica l contro l device s suc h as : seal-les s valves , pump s wit h dua l mechanica l seal s an d abarrie r

fluid , compressor s wit h mechanica l seal s an d abarrie r fluid , an d pressur e relie f valve s wit h ruptur e disks . c) . Provid e equipmen t count s fo r

equipmen t

wit h avapo r

collectio n an d recover y (close d vent ) system . d) . Us e th e sam e contro l devic e code s an d format s a s i n footnot e "h " o f Tabl e 2 .

T JP.1 5

1 2 TABL E 8 . COMPOUNDING/BLENDING/PACKAGIN G OPERATION S Parti . N/A Produc t Nam e (a ) Not Applicabl e Chemica

l Composition (b ) Annua

l Quantit y Produced (gal ) (c ) Doe s achemica l reactio n tak

e place ? (d ) Applicabl e

Regulation s (e )

a) . b) . c) . d) . e) . Provide th e product name s resultin g fro

mblending , compounding , an d packagin g operations . Name s mus t

matc h thos e provide d i

n Tabl e 1 . Fo

r familie s o f

blends , include only th e famil y nam e liste d i n Tabl e 1 . Provide th e name s ofth e ra w material s (mus t

matc h Tabl e 1 ) tha

t ar e use d t o blend/compound th e product . Provide th e annua

l quantitie s ofth e product s produced . Specif y whethe r achemica l reactio n take s plac e during th e compounding o r blendin g of organi c liquid s (i.e. , yes-compounding , no-blending , etc.) . Pleas e identif

y an y regulation s (pertainin g to ai r emissions ) tha

t apply to th e compounding/blendin g operation . PartII . Th e question s belo w ar

e facility-wide , an

d d o not nee d to b e answered o

n aproduct-by-produc t

basis . Pleas e answe

r th e followin

g question s wit

h a s muc h detail a s possible . Inser

t sheet s a s necessary . 1 . Provide adescriptio n ofth e principa l methods/mechanism s use

d fo r blending/compounding . Provide adetaile d descriptio n o f an y mechanism s of

vapo r balancin g o r

othe r vapor emissio n contro l utilize d fo

r thes e processe s (e.g. , submerged fill). 

# ; 4P.1 6



### 1 3 TABLE 9 . AIRPOLLUTION CONTRO L EQUIPMENT PARAMETER S (a) Contro l Device : Scrubbe

r (b ) Identifie r Code(d V N/

A Typ e ofscrubber : ventur i packed bed impingemen

t othe r (specify ) Gas inle t temperature , CF Pressur e drop , in . H, 0 Liquid-to-ga s ratio , gal/10 3 acf m Inle t scrubbing liquor : P H percen t solid s typ e o f alkali added , i

f an y rat e (lb/gal ) Wastewate r generation rate , gal/mi

n HA P composition of

wastewater , mg/

l 1 . 2 . 3 . 4 . 5 . 6 . Emission Source s (c )

Se e en dof tabl e fo r foomotes .



# )SP.1 7



### 14 TABLE 9 . AI

RPOLLUTION CONTRO L EQUIPMENT PARAMETER S (a) (Continued ) Control Device : Incinerato

r (b ) Identifie r Cod e Cdl: N/

A Type : therma

l catalyti c Combustion chambe

r temperature , ° F (pleas e note if

temperamr

e measuremen

t i s not i n chamber ) Exces s air , % Nomina l residenc e time , s Hea t recovery : recuperative , percen

t hea t recover y regenerative , percen

t hea t recover y Emissio n Source s (c ) 1 . 2 . 3 . 4 . 5 . 6 .

Se e en do f tabl e fo r footnotes .



# )bP.1 8



### 1 5 TABL E 9 . AI

RPOLLUTIO

N CONTRO

L EQUIPMEN

T PARAMETER

S (a) (Continued ) Control Device : Flar

e (b ) Identifie r Cod e (d): Not

applicable Type : n o assis t stea massis t ai r assis t pressur e assis t Location : groun d elevate d Hea t conten t ofvente d stream , Btu/scf Flar e ga s exit velocity , ft/s Flar e ti p diameter , in . Flar e height , ft Supplementar

y fue l for : pilot , scf m combustio n purposes , scf

m Stea mrequirement , lb/h

r Emission Source s (c ) 1 . 2 . 3 . 4 . 5 . 6 .

Se e en dof tabl e fo r footaotes .



# nP.1 9



### 1 6 TABL E 9 . AI RPOLLUTION CONTRO L EQUIPMEN

T PARAMETER

S (a) (Continued ) Control Device : Carbo

n Adsorbe r (b ) Identifie r Cod e (d): N/

A Typ e o f carbo n bedan

dnumber : regenerativ e non-regenerativ e fixed fluidized How man y pound s o

f carbon pe r bed Configuration : " paralle l seria l Numbe r o f bed s on-line Numbe r o f bed s desorbing Pressur e drop , in . H, 0 Ga s inlet temperature , ° F Typ e o f regeneratio n Regeneratio n tim

e Adsorptio n tim

e 1 . 2 . 3 . 4 . 5 . 6 . Emissio n Source s (c )

Se e en do f tabl e fo r foomotes .



# / 81 7

TABL E 9 . AI RPOLLUTIO N CONTRO L EQUIPMEN T PARAMETER S (a ) (Continued ) Control Device : Condense

r (b ) Identifie r Cod e (d): >I/

A Typ e o f condenser : surfac e contac t Ti f contact , se

e scrubber l Gas inle t temperature , ° F Ga s outlet temperature , ° F 1 . 2 . 3 . 4 . 5 . 6 . Emission Source s (c )

Se e nex t pag e fp r footnotes .



# /< ?