# Exploratio n an d Productio n Waste Study

FrequencyDistributio n o fTCL P Dat a

Numbe rofSample s AP I Dat a

0-0. 5 0.5- 5 5-1 0 10-2 0 20-3 0



# Benzene Concentratio n (mg/l ) 42 0

Figur e1P. 5 

# <_f&£c-soo^3rg >

ATTACHMENT 1P. 6

I . OVERVIEW

Thi s repor t present s th e analytica l result s a s wel l a s supportin g informatio nt o ai dinth e evaluatio nan dinterpretatio no f th e dat a an di s
arrange di

nth e followin gorder :

I . Overvie w
II . Sampl e Descriptio nInformation/Analytica l Tes t Request s
III . Analytica l Result s
IV . Qualit y

Contro l Repor t

A . Standar dEnsec o Q C

B . Project-Specifi c Q C

Consisten t wit hdirective s i nth e CL P protoco l i nSW-84 6 an

dothe r EP

A
methods , al l GC/M S analyse s wer e performe ds o tha t th e maximum concentratio n

o f sampl e wa s analyzed
. Some sample s require ddilution s t o avoi dsaturatio n

o f th e detector , t o achiev e linearit y fo r a specifi c targe t compoun do r t o reduc e matri xinterferences

. A s state dinSectio n7.5. 4 o f Metho d8270 , 7.4.1.1 6 o f Metho d824 0 andExhibi t E o f th e CL P protoco l thes e dilution s must
be performed
. Th e reportin glimit s fo r thes e sample s ar e therefor e proportionat e t o th e dilutio nrequired

. Surrogat e compound s ma y no t b e measurabl e insample s whic hhav e bee ndiluted

.

Sample s 011772-000 1 throug h-000 5 fo r tota l volatile s an dsample s 011772

- 000 1 throug h-0004 , -0001M S (matri xspike) , an d-0002M S fo r TCL P volatile s require ddilution s du e t o concentration s o f targe t o r non-targe t compound s
presen t beyon dlinea r range . Th e reportin glimit s wer e increase daccordingly

.

Sample s 011772-000 1 and-0001M S matri xspik e generate dtwo phase s durin g th e TCL P volatil e an dmetal s extractions

. Pe r th e TCL P method , eac hphas e wa s analyze dseparatel y

an dresult s the nmathematicall y recombined

.

Th e reportin glimit s wer e increase dfo r th e barium analyse s b

y IC P fo r
TCL P sample s 011772-000 1 and-000 3 throug h-000 5 du e t o concentration s o f
barium detecte di nth e metho dblank
.P. 7

Th e recoverie s o f cadmiu m wer e irregula r i

nth e leachat e analyse s for sample s 011772-0001M S an d-0002MS
. The spik e recoverie s wer e measure dfo r non requeste delement s an dfoundt o b e correct . Th e irregularit y appear s t o be confine dt o th e cadmiu m result s onl y

an dmay sugges t matri xinterferences

. Pe r Enseco' s QAPP , th e laborator y doe s no t contro l o

nmatri xspik e samples
.

Sample s withi nthi s projec t hav e bee nanalyze dfo r TCL P a s finalize di n the Jun e 29 , 199 0 Federa l Registe r (p
. 2698 6 - 26998)
. TCL P leachate s ar e
prepare dusin gMetho d131 0 an danalyze dusin gMethod s 6010 , 7470 , an d774 0 fo r metals , 824 0 fo r volatiles , 827 0 fo r semivolatiles , 808 0 fo r pesticides , an d
815 0 for
. herbicides

. Ever y effor t wa s mad e t o achiev e reportin glimit s below th e regulate dlimi t oneac hsample
. However , a s wit hal l environmenta l analyses , matri xinterference s o r targe t compound s may . b e presen t insome sample s whic hlimi t th e effectivenes s o f th e analytica l metho dt o achiev e thes e limits

.

Th e fina l TCL P rul e contain s a requiremen t tha t a matri xspik e b e analyze dfo r eac hanalytica l batc han dtha t th e bia s determine dfro m th e matri xspik e b e use dt o correc t th e measure dvalues
. Ensec o disagree s wit h
th e requiremen t t o adjus t sampl e result s usin gspik e recover y dat a an

d
furthermor e believe s tha t i f correctio no f dat a i s t o b e performed , i t shoul d

no t be performe db

y th e laboratory
. Ensec o ha s submitte dforma l comment s t o
EPA concernin grecover y correctio n(copie s ar e availabl e o nrequest)
. Result s

ar e reporte duncorrecte dfo r spik e recoveries

. Th e result s ro m the.Q C sampl e analyse s (surrogates , labcontrol s an dmatri xspikes ) ar e containe dinth e report , shoul dthes e dat a b e of
. interes t inadjustin greporte dvalues
. A s
state di nMetho d1310 , us e o f alternate dmethod s may b e neede dwhe nth e

recover y o f th e matri xspik e i s below th e expecte danalytica l performance
.P. 8

II . SAMPL E DESCRIPTION INFORMATION/ANALYTICAL TES T REQUEST S

Sampl e Descriptio n Informatio n

Th e Sampl e Descriptio n Informatio n list s al l o f th e sample s receive d in thi s projec t togethe r wit hth e interna l laborator yidentificatio n numbe r assigne d fo r eac hsample

. Eac hprojec t receive d a t Ensec o - RMA L i s assigne d

a uniqu e si xdigi t number

. Sample s withi n th e projec t ar e numbere d sequentially

. Th e laborator yidentification.numbe r i s a combinatio n o f th e si xdigi t projec t cod e and th e sampl e sequenc e number

.

Als o give n i n th e Sampl e Descriptio n Informatio n i s th e Sampl e Typ e (matrix)
, Dat e o f Samplin g (i f known ) and Dat e o f Receip t a t th e laboratory

.

Analytica l Tes t Request s

Th e Analytica l Tes t Request s list s th e analyse s tha t wer e performe d o n

eac hsample

. Th e Custo mTes t column indicate s wher e test s hav e bee n modifie d

t o confor mt o th e specifi c requirement s o f thi s project

.P. 9

III . ANALYTICA L RESULT S

Th e analytica l result s fo r thi s projec t ar e presente di nth e followin g dat a tables
. Th e result s ar e presente db y sample , b

y test , wit htest s reporte di

nth e followin gorder : GC/MS , Chromatography , Metal s an d Inorganics

.

Eachdat a tabl e include s sampl e identificatio ninformation , an dwhe n availabl e an

dappropriate , date s sampled , received , authorized , prepare dan d• analyzed
. Th e authorizatio ndat a i s th e dat e whe nth e projec t wa s define db y th e clien t suc htha t laborator y wor kcoul dbegin

. Th e dat e prepare di s typicall y

th e dat e anextractio no r digestio nwa s initiated

. Fo r volatil e organi c compound s i

nwater , th e dat e prepare di s th e dat e th e screenin go f th e sampl e wa s performed
.

Dat a sheet s contai na listin go f th e parameter s measure dineac htest , th e analytica l result s an dth e Ensec o reportin glimit

. Reportin glimit s ar e adjuste dt o reflec t dilutio no f th e sample , whe nappropriate

. Soli dan dwast e sample s ar e reporte donan"a s received " basis , i.e

. n o correctio ni s mad e fo r moistur e content .

Enseco-RMA L i s n o longe r routinel y blank-correctin ganalytica l data
. Uncorrecte danalytica l result s ar e reported , alongwit hassociate dblan k
results , fo r al l organi c an dmetal s analyses
. Analytica l result s an dblan k
result s ar e reporte dfo r conventiona l inorgani c parameter s a s specifie di nth e method
. Thi s polic y i s describe dindetai l inth e Ensec o Incorporate dQualit y
Assuranc e Program

Pla nfo r Environmenta l Chemica l Monitoring , Revisio n3.3 , May , 1989
.

Inaddition , surrogat e recover y dat a i s presente dfo r al l GC/M S analyses
. Th e surrogat e recover y i s anindicatio no f th e affec t o f th e sampl e matri xo n th e performanc e o f th e method
. Th e result s fro m th e Standar dEnsec o QA/Q C Program , whic hgenerate s dat a whic har e independen t o f matri xeffects , i s give ninSectio nIV .

Th e analytica l dat a reporte dar e subjec t t o th e followin glimitation s o f
th e analytica l methodology :P.1 0

GC/M S

Volatil e Organic s

a ) Th e cis

- an

dtrans-isomer s o f dichloroethylen e canno t be distinguishe dusingEP A Metho d624
. Al l dichloroethylen e presen t i s reporte da s trans-dichloroethylene

.

.Metal s

Arsenic , seleniu

m an dthalliu

m ar e customaril y

determine db

y graphit e furnac e atomi c absorptio n(GFAA)
. Al l mercur y determination s ar e b y col d

vapo r atomi c absorption

. Al l othe r metal s ar e determine dusin gInductivel y Couple dPlasma Atomi c Emissio nSpectroscopy (ICP)
.

Al l metal s nomina l reportin glimit s ar e statisticall y determine db

y analyzin ga reagen t blan kseve ntime s onthre e non-consecutiv e days
. Th e standar ddeviation s fro m eac hgrou po f analyse s ar e the nsumme d(reportin g limi t » thre e time s th e standar ddeviatio no f a blank)
. Th e abilit y t o attai n th e quote dreportin glimit s i s verifie deac hquarter . Reportin glimit s abov e nomina l value s ar e ofte nreporte dsinc e sampl e matri xinterference s mus t be compensate dfo r b

y dilution s prio r t o analysi s o r b y th e us e o f Metho do f
Standar dAdditions

. Al l GFA A reportin glimit s an dresult s ar e verifie db y spik e recoverie s andrepresen t th e lowest.attainabl e fo r eac hsampl e matrix

. Th e metal s reportin glimit s reporte dshoul dno t b e viewe da s quantitatio n limits

. A s recommende db y th e America nChemica l Societ y Subcommitte e on Environmenta l Analytica l Chemistr y (Analytica l Chemistr y 1980 , 52 , 2242-49) , th e Limi t o f Quantitatio n(LOQ ) i s equa l t o te ntime s th e standar ddeviatio n

o f a blan ko r 3. 3 time s th e reportin glimit

.P.1 1 ;\l)tn

. Muai..Jll i 1 — Anaivtica i Ljooraio p

ANALYTICAL RESULT S

FO R

AMERICA N PETROLEU

M INSTITUT E

ENSECO-RMAL NO
. 00634 4

OCTOBE R27 , 198 9

Reviewe d by : _v , 

# U&L I /~

V Susa n C

. Wyat 

# •rtf{~

Jeann e B . Howber t

Enscci> Incorporate d -i'-'')* " Yarrow Stree t Arvilila

. r.i>inrj_ o .Mi

l 11) 2 M>v42WiOl l F.ix : ii.ij'J'l-TIT lP.1 2

Appendi xI

XVolatil e Organic s

Metho d824 0

Clien t Name : America nPetroleu m Institut e Clien t ID : Sit e A

Tan kBtms . Col
. Tank LabID : 006344-0001-S A Ensec o ID : Matrix : WAST E Sampled : Authorized : 3 1 AUG8 9 Prepared :

Paramete r

Aceton e Acetonitril e Acrolei n Acrylonitril e Ally l chlorid e Benzen e Bromodichloromethan e Bromoform Bromomethan e • Carbo ndisulfid e Carbo ntetrachlorid e Chlorobenzen e Chloropren e Chloroethan e Chi orodibromomethan e Chloroform Chloromethan e DBC P (1,2-Dibromo

3-chloropropane ) EO B (1,2-Dibromoethane ) Dibromomethan e trans-1,4-Dichloro

2-buten e D i chlorod i f1uoromethan e 1,1-Dichloroethan e 1,2-Dichloroethan e trans-1,2-Dichloroethen e 1,1-Dichloroethen e Dichloromethan e 1,2-Dichloropropan e cis-1,3-Dichioropropen e trans-1,3-Dichloropropen e 1,4-Dioxan e Ethy l benzen e Ethy l cyanid e 2-Hexanon e Iodomethan e Isobuty l alcoho l Methacrylonitril e Methy l ethy l ketr- e 4-Methyl-2-pentanon e 105077 6 3 0 AU G8 9 0 1 SE P 8 9

esul t



### N D N D N D N D N D 5 7 N D N D N D N D N D N D N D N D N D N D N D

N D N D N D

N D N D N O N D N D N O N D N D N D N D N D 5 7 N D N D N D N O N D N D N D /- M

Unit s mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g •ng/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g :eived : 3 1 AU G8 9 ulyzed : 0 7 SE P 8 9
Reportin g Limi t 

### 2 0 20 0 200 200 1 0 1 0 1 0 1 0 2 0 1 0 1 0 1 0 1 0 2 0 1 0 1 0 2 0
1 0 1 0 1 0
1 0 2 0 1 0 1 0 1 0 1 0 1 0 1 0 1 0 1 0 200 1 0 1 0 2 0 1 0 200

. 1 0 

### 2 0 2 0
(continue do

nfollowin q->age ) N D- No t detecte d N A * No t applicabl e
Reporte dBy : Dian e Pag e Approve dBy : Jef f Lowr y



# JP.1 3

Appendi xI

X Volatil e Organic s (CONT. )

Method 824 0

1ien t Name: Clien tID : La b ID : latrix : ,uthorized :

'aramete r American Petroleu mInstitut e Sit e ATank Btms

. Col
. Tan k 006344-0001-S AEnsec o ID : 105077 6 WAST E Sampled : 3 0 AU G8 9 3 1 AU G8 9 Prepared : 0 1 SE P 8 9 Received : Analyzed : 3 1

0 7 AU G SE P 8 9 8 9

Styren e 1,1,1, 2-Tetrachloroethan e 1,1,2 ,2-Tetrachloroethan e Tetrachloroethen e Toluen e 

### 1,1,1-Tr i chloroethan e 1,1,2-Trichloroethan e Trichloroethen e Tr i chlorofluoromethan e 1,2,3-TrichlorOpropan e Viny l acetat e Viny l chlorid e Tota l xylene s
Toluene-d 8 4-Bromofluorobenzen e (BFB 1 1,2-D i chloroethane-d 4 Resul t

N D N D N D N D 

### 210 ND ND N D ND ND N D N D 32 0 

### 10 4
10 5 97. 3 Unit s

mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

%

% t. Reportin

g Limi t

1 0 1 0 1 0 1 0 1 0 1 0 1 0 1 0 1 0 1 0 2 0 2 0 1 0

N D • • No t detecte d N A- No t applicabl e

Reporte d By : Diane Page Approve dBy : Jef f Lowr

yP.1 4

„ i ien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r America nPetroleu m Sit e A Tan kBtms . 006344-0001-S A WAST E 3 1 AU G8 9

Viny l chlorid e Acrylonitril e Methylen e chlorid e Carbo ndisulfid e 1,1-Oichloroethen e Isobuty l alcoho l Chloroform 1,2-Dichloroethan e 2-Butanon e 1,1,1-Tr i chloroethan e Carbo ntetrachlorid e Trichloroethen e 1,1,2-Trichloroethan e Benzen e 1,1,1,2-Tetrachloroethan e 1,1,2,2-Tetrachloroethan e Tetrachloroethen e Toluen e Chlorobenzen e

Toluene-d 8 4-Bromof1uorobenzen e (BFB ) 1,2-0 i chloroethane-d 4 0T C Volatil e Organic s TCL P Leachat e Metho d824 0

ur nInstitut e

. Col
. Tan k Ensec o ID : 105077 6 Sampled : 3 0 AUG8 9 Prepared : 1 3 £'." • 8 9

Resul t



### N D N D N D N D N D N O N D N D N D N D N D N D N D 7. 7 N D N D N D 2 7 N D

98. 8

94. 8 

### 107 Unit s

mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L 

### mg/ L

%

% % Received : 3 1 AUG8 9 Analyzed : 1 9 SE P 8 9
Reportin g Limi t 

### 4. 4 4 4 2. 2 2. 2 2. 2 4 4 2. 2 2. 2 4. 4 2. 2 2. 2 2. 2 2. 2 2. 2 2. 2 2. 2 2. 2 2. 2 2. 2

, - -

- -

N D= No t detecte d N A » No t applicabl e

Reporte dBy : Lis a Trau t Approve dBy : Jef f Lowr yP.1 5

Refiner y

Hazardou s Constituen t Semivolatile s

Metho d827 0

CIien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r America nPetroleu m Institut e Sit e A Tan kBtms . Col
. Tank 006344-0001-S A

Ensec o ID : 105077 6 WAST E Sampled : 3 0 AU G8 9 3 1 AU G8 9 Prepared : 0 6 SE P 8 9 Received : Analyzed : 3 1

1 1 AU G OC T 8 9 8 9

Anthracen e Benzo(a)anthracen e 8enzo(b)f1uoranthen e Benzo(kmuoranthen e Benzo(a)pyren e bis(2-Ethylhexyl ) phthalat e Buty l benzy l phthalat e Chrysen e Dibenz(a,h)anthracen e Di-n-buty l phthalat e 1,2-Dichlorobenzen e 1,3-Dichlorobenzen e 1,4-Dichlorobenzen e Diethy l phthalat e 7,12-Dimethylbenz

anthracen e Dimethy l phthalat e Di-n-octy l phthalat e Fluoranthen e Inden e 1-Methylnaphthalen e Naphthalen e Phenanthren e Pyren e Pyridin e Quinolin e Benzenethio l o-Creso l

m & p-Cresol(s ) 2,4-Dimethylpheno l 2,4-Dinitropneno l 4-Nitropheno l Pheno l

Nitrobenzene-d 5 2-Fluorobipheny l Terphenyl-dl 4 Phenol-d 5 2-Fluoropheno l 2,4,6-Tribromopheno l

N D= No t detecte d N A - No t applicabl e Resul t

N D ND ND ND ND

ND ND ND ND ND ND ND ND ND

ND ND N D ND N D 17 0 7 8 ND ND ND N O ND ND ND ND N D ND ND

54. 9 55. 7 71. 3 39. 6 38. 6 55. 3 Unit s

mg/k g mg/k g mg/k g mg/k g mg/k g
mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

% % % % % % Reportin g

Limi t

3 0 3 0 3 0 3 0 3 0

3 0 3 0 3 0 3 0 3 0 3 0 3 0 3 0 3 0

3 0 3 0 3 0 3 0 3 0 3 0 3 0 3 0 3 0

3 0

3 0 3 0 3 0 15 0 15 0 3 0

Reporte dBy : Marshal l Tilbur y Approve dBy : Jef f Lowr yP.1 6

CIien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r 

### OT C

America nPetroleu

m Sit e A Tan kBtms . 006344-0001-S A WAST E 3 1 AUG8 9

Pyridin e Pheno l bis(2-Chloroethyl)ethe r 1,4-Dichlorobenzen e 1,2-Dichlorobenzen e p-Creso l
m

_ p-Cresol(s ) Hexachloroethan e Nitrobenzen e Hexachlorobutad i en e 2,4. , 6-Tr i chloropheno l 2,4,5-Tr i chloropheno l 2,4-Dinitrotoluen e Hexachlorobenzen e 2,3,4,6-Tetrachloropheno l Pentachloropheno l
Nitrobenzene-d 5 2-Fluorobipheny l Terphenyl-dl 4 Phenol-d 5 2-Fluoropheno l 2,4,6-Tribromopheno l Semivolatil e Organic : TCL P Leachat e Metho d827 0

i Institut e Col
. Tan k Ensec o ID : 105077 6 Sampled : 3 0 AU

G Prepared : 2 1 SE P

Resul t


### N D N D N D N D N D N D N D N D N D N D N D N D N D N D N D N D
N A N A N A N A N A N A 8 9 8 9

Unit s mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L •q/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L 

### mg/ L



## r . % % % % % Received : ~-\ Analyzed : - 2 Reportin g Limi t

0.2 2 0.2 2 0.2 2 0.2 2 0.2 2 0.2 2 0.2 2 0.2 2 0.2 2 0.2 2 

### 1. 1 0.2 2 0.2 2 0.2 2 

### 1. 1

- -

- -

- -
'-

-

- - AUG8 9 OC T 8 9

ND= No t detecte d N A « No t applicabl e
Reporte dBy : Marshal l Tilbur y Approve dBy : Jef f Lowr yP.1 7

CIien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r

Aluminu m Antimon y Arseni c Bariu m Beryl 1iu

m Cadmiu m Calciu m Chromiu m Cobal t Coppe r Lea d Mercury Nicke l Potassiu

m Seleniu m Silve r Sodiu m Thalliu m Ti n Vanadiu m Zin c Metal s

Tota l Metal s

American Petroleu

m Institut e Sit e ATan

k Btms

. Col

. Tan

k 006344-0001-SAEnsec o ID : 105077 6 WAST E Sampled : 3 0 AU G8 9 3 1 AU G8 9 Prepared : Se e Below

Resul t Reportin g Analytica l Unit s Limi t M



### N D N D N D 

### 3 N D N D N O N D N D N D N O N D 

### 5 N D N D N D N D N D N D 2 5 N D mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g 

### 1 0 

### 5 0. 5 

### 1 0. 2 0. 5 3 0 

### 1 1 1 5 0. 1 

### 4 50 0 0. 5 

### 1 500 

### 1 11 

### 1 1 601 0 601 0 706 0 601 0 601 0 601 0 601 0 601 0 601 0 601 0 601 0 747 1 601 0 601 0 774 0 601 0 601 0 784 1 601 0 601 0 601 0 Received : 3 1 AU G8 9 Analyzed : Se e Below

.ica l Prepare d lo d Dat e

0 5 SE P 8 9 0 5 SE P 8 9 0 8 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 1 4 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 8 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 8 SE P 8 9 0 5 SE P 8 9 0 5 SEP 8 9 0 5 SE P 8 9 Analyzed

Dat e

1 8 SE ? 8 9 1 8 SE P 8 9 1 1 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 7 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 1 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 1 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9

t

m

N D » No t detecte

d N A - Not applicabl e

Reporte dBy : Fre

dVelasque z Approve dBy : Toni Lus kP.1 8

Clien t Name : Clien t ID : La bID : Matrix : Authorized : ir.?/M S Metal s

Tota l Metal s

America n Petroleu mInstitut e Sit e ATan k Btms

. Col
. Tan k 006344-0001-S AEnsec o ID : WAST E Sampled : 3 1 AU G8 9 Prepared : 105077 6 3 0 AU G8 9 Se e Belo w Received :

Analyzed :

Paramete r
Osmium(189 ) 

### Resul t

ND Reportin g Analytica l Unit s Limi t Metho d 3 1 AU G8 9 Se e Belo w
Prepare d Dat e Analyze d

Dat e

mg/k g 

### 0. 1 RMA L 0 7 OC T 8 9 1 4 OC T 3 9

N D= No t detecte d N A - No t applicabl e
-ReportedBy : Scot t Heidema n Approve dBy : Ton i Tallaric oP.1 9

Metal s

TCL P Leachat e

Name : ID : CIien t Clien t La bID : Matrix : Authorize d American Petroleu mInstitut e Sit e ATan

k Btms

. Col

. Tan

k 006344-0001-SAEnsec o I D WAST E 3 1 AU G8 9 105077 6

Sampled : 3 0 AU

G8 9 Received : Prepared : Se e BelowAnalyzed :

Paramete r

Arseni c Bariu m Cadmiu m Chromiu m Lea d Silve r Mercury Seleniu m Resul t Unit s Reporting Analytica l Limi t Method



### N D 

### 7. 5 N D 0.0 8 

### N D N D N D N D mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L 0. 6

0.0 6 0.0 3 0.0 6 0. 3 0.0 6 0.00 3 0.0 6 200

. 200

. 200

. 200

. 200
. 200. 7 747 1 270. 2 3 1 AU G8 9 Se e Below

Prepare d Dat e

1 4 SE P 8 9 1 4 SE P 8 9 1 4 SE P 8 9 1 4 SE P 8 9 1 4 SE P 8 9 1 4 SE P 8 9 1 4 SE P 8 9 1 4 SE P 8 9 Analyze d

Dat e

2 0 SE P 8 9 2 0 SE P 8 9 2 0 SE P 8 9 20

. SE P 8 9 20

. SE P 8 9 2 0 SE P 8 9 1 4 SE P 8 9 1 8 SE P 8 9



# 1
1 N D - Not detecte

d N A - Not applicabl e

Reporte dBy : Sandr

a Jone s Approve dBy : Ton

i Lus kP.2 0

Genera l Inorganic s

Clien t Name : America n Pe l Clien t ID :

. Sit e A LabID : 006344

- Matrix : WAST E Authorized : 3 1 AU G

Paramete r

Chlorid e Cyanide
, Reactiv e Ignitabilit y Non-Volatil e Oi l Volatil e Oi l 

### Oil Wate r Solid s 

### p H Sulfide
, Reactiv e Tan k •000 1



### 8 9 iroleu

m Btms

. C •S AE

Resul t

2160 0 

### N D 5 5 16. 8 

### 2. 3 19. 1 71. 1 

### 9. 0 6. 9 1. 9 Institut e ol

. Tan k

nsec o ID : Sampled : Prepared :

Unit s
mg/k g mg/k g deg

. F

e v % %

t v 10 % unit s mg/k g 105077 6 3 0 "J G8 9 Se e ielo w Reportin g Limi t


### 15 

### 0. 1

- - 

### 0. 1 .0. 1 

### 0. 1 0. 1 0. 1

- - 

### 0. 5 Received :

Analyzed :
Analytica l Metho d

300. 0 Mod

. EPA-OS W 1010/102 0 Chevro n Chevro n Chevro n Chevro n Chevro n 9045/AST M EPA/0S W 

### 3 1



### Se eAU G Be l 8 9
o w
Prepare d Dat e


### 1 N A N A N A N A N A N A N A N A N A 

### SE P 8 9 Analvze a

Dat e

1 3 SE P 8 9 0 8 SE P 3 9 1 2 OC T .3 9 0 6 OC T 3 9 0 6 OC T 8 9 0 6 OC T 3 9 0 6 OC T 8 9 0 6 OC T 8 9 2 3 SE P 8 9 0 8 SE P 3 9



# 1 ] Not e o : Thi s tes t i s unreliabl e fo r an y sampl e othe r tha na non-aqueou s liquid

.

Not e 1 : Sampl e hazardou s du e t o ignitability

.

N D= No t detecte d N A = No t applicabl e

Reporte dBy : Blak e Besse r Approve dBy : Tamm y Baile y



# ]P.2 1

'Aient Name : Clien t ID : '.a bID : Matrix : Authorized :

Paramete r Appendi xI XVolatil e Organic s

Metho d824 0

America nPetroleu

m Institut e Sit e C Crud e TankBottom s 006344-0002-S A

Ensec o ID : 105077 7 WAST E Sampled : 3 0 AUG8 9 3 1 AUG8 9 Prepared : 0 1 SE P 8 9 Received : Analyzed : 3 1

0 7 AU G SE P 8 9 8 9

Aceton e Acetonitril e Acrolei n Acrylonitril e Ally l chlorid e Benzen e Bromod i chloromethan e Bromoform 3romomethan e Carbo ndisulfid e Carbo ntetrachlorid e Chlorobenzen e Chloropren e Chloroethan e Chlorod i bromomethan e Chloroform Chloromethan e DBC P (1,2-Dibromo

3-cnloropropane ) EDB (1,2-Dibromoethane ) Dibromomethan e traps-l,4-Dichloro

2-buten e D i chlorod i f1uoromethan e 1,1-Dichloroethan e 1,2-Dichloroethan e trans-1,2-Dichloroethen e 1,1-Dichloroethen e Dichloromethan e 1,2-Dich l oropropan e ci s-1,3-D i ch1oropropen e tran s -1,3-D i chloropropen e 1,4-Dioxan e Ethy l benzen e Ethy l cyanid e 2-Hexanon e Iodomethan e Isdbuty l alcoho l Methacrylonitril e Methy l ethy l keton e 4-Methyl-2-pentanon e Resul t

ND ND ND ND N D 18 0 ND ND ND ND ND ND ND ND ND ND ND

N D ND N D

N D NO N D N D NO NO NO NO NO N O N D 22 0 NO N D ND ND N D NO NO Unit s

mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g * mg/k g mg/k g mg/k g mg/k g
mg/k g mg/k g mg/k g
mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g Reportin g

Limi t

2 0 20 0 20 0 20 0 1 0 1 0 1 0 1 0 2 0 1 0 10
. 1 0 1 0 2 0 1 0 1 0 2 0

1 0 1 0 1 0

1 0 2 0 1 0 1 0 1 0 1 0 1 0 1 0 1 0 1 0 20 0 1 0 1 0 2 0 1 0 20 0 1 0 2 0 2 0

(continue do

nfollowin g page )

Reporte dBy : Dian e Pag e Approve dBy : Jef f Lowry N D- No t detecte d N A * No t applicabl eP.2 2

Appendi x I

XVolatil e Organic s

Metho d824 0

Clien t Name : America nPetroleu m Institut e Clien t ID : Sit e C Crud e Tan kBottom s LabID : 006344-0002-S A Matrix : WAST E Authorized : 3 1 AU

G8 9

Paramete r

Styren e I.1,1,2-Tetrachloroethan e 1,1,2,2-Tetrachloroethan e Tetrachloroethen e Toluen e 1,1,1-Tr i chloroethan e 1,1,2-Trichloroethan e Trichloroethen e Trichlorofluoromethan e 1,2,3-Trichloropropan e Viny l acetat e Viny l chlorid e Tota l xylene s

Toluene-d 8 4-Bromoflucrobenzen e (BFB ) l,2-Dichloroethane-d 4

N D- No t detecte d N A » No t applicabl e

Reporte dBy : Dian e Pag e Ensec o ID : 105077 7 Samol=- : 3 0 AU

G8 9 Prepared : 0 1 SE P 8 9

Resul t



### N D N D ND . N D 530 N D N D N D N D N D N D N D 510
109

107 98. 5 (CONT. )

i

Unit s
mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

%



### 7
. fa

'-. .- " V"

- •

deceived : 3 1 AUG8 9 Analyzed : 0 7 SE P 8 9
Reportin g Limi t


### 1 0 1 0 1 0 1 0 1 0 1 0 1 0 1 0 1 0 1 0 20 20 1 0

- -

Approve dBy : Jef f Lowr yP.2 3

Clien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r America n Petroleum

Sit e C Crud e Tan k 006344-0002-S A WAST E 3 1 AU G8 9

Viny l chlorid e Acrylonitril e Methylen e chlorid e Carbo n disulfid e 1,1-Dichloroethen e Isobuty l alcoho l Chlorofor m 1,2~Dichloroethan e 2-Butanon e

. 1,1, 1 -Tr i chloroethan e Carbo n tetrachlorid e Trichloroethen e 1,1,2-Trichloroethan e Benzen e 1,1,1,2-Tetrachloroethan e 1,1,2,2-Tetrachloroethan e Tetrachloroethen e Toluen e Chlorobenzen e

Toluene-d 8 4-Bromofl uorobenzen e (BFB 1 1,2-D i chloroethane-d 4 OT C Volatil e Organics

. TCL P Leachat e Metho d 824 0

ur n Institut e k Bottom s Ensec o ID : 105077 7 Sampled : 3 0 AU G8 9 Prepared : 1 3 SE P 8 9

Resul t



### N O N D N O N D N D N O N D N O N D N D N D N D N D 

### 4. 6 N D N D N D 13 N O

95. 6

95. 9 

### 10 7 Unit s

mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L 

### mg/ L mg/ L mg/ L

%

% % Received : 3 1 AU G 8 9 Analyzed : 1 9 SE P 8 9 Reportin g Limi t 

### 4. 2 4 2 

### 2. 1 2. 1 2. 1 42 

### 2. 1 2. 1 4. 2 2. 1 2. 1 2. 1 2. 1 2. 1 2. 1 2. 1 2. 1 2. 1 2. 1

- -

- -

- -

ND» No t detecte d N A - No t applicabl e
Reporte dBy : Lis a Trau t Approve dBy : Jef f Lowr y



# ]P.2 4

Refiner yHazardou s Constituen t Semivolatile s

Metho d 827 0

Clien t Name : America n PetroleumInstitut e Clien t ID : Sit e C Crud e Tan k Bottom s LabID : 006344-0002-S AEnsec o ID : Matrix : WAST E Sampled : Authorized : 3 1 AU G8 9 Prepared :

Paramete r
Anthracen e 3enzo(a)anthracen e Benzo(b j f1uoranthen e Benzolkjfluoranthen e 3enzo(a)pyren e b.is(2-EthylhexyT ) phthalat e Buty l benzy l phthalat e Chrysen e Dibenz(a,h)anthracen e Di-n-buty l phthalat e 1,2-Dichl.orobenzen e 1,3-Dichlorobenzen e 1,4-Dichlorobenzen e Diethy l phthalat e 7,12-Dimethylbenz

anthracen e Dimethy l phthalat e Di-n-octy l phthalat e Fluoranthen e Inden e 1-Methy l naphtha ! en e Naphthalen e Phenanthren e Pyren e Pyridin e Quinolin e Benzenethio l o-Creso l
m& p-Cresol(s ) 2,4-Dimethylpheno l 2,4-Dinitropheno l 4-Nitropheno l Pheno l

.
Nitrobenzene-d 5 2-Fluorobipheny l Terphenyl-dl 4 Phenol-d 5 2-Fluoropheno l 2,4,6-Tr i bromopheno l

N D = No t detecte d N A= No t applicabl e
Reporte d By : Marshal l Tilbur yApprove d By : Jef f Lowr y 1 C ..'77 3 0 iU G 8 9 0 6 SE P 8 9

esul t



### N D N D N D N D N D

N D N D N O N O N D N O N D N D N D

N O N O N D N O N D 

### 14 0 4 0 N D N O N D N O N O N D N D N D N O N D N D

71. 6 56. 7 66. 8 51. 1 46. 0 48. 1 

### Re

c An e

Unit s
mg/kg mg/kg mg/kg mg/kg mg/kg
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
mg/kg mg/kg mg/kg mg/k g mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/k g mg/k g mg/k g mg/kg mg/kg mg/kg

t v % % % % % :eived : 3 1 AU G ilyzed : 1 2 OC T
Reporting Limi t


### 4 0 4 0 4 0 4 0 4 0
4 0 4 0 4 0 4 0 4 0 4 0 4 0 4 0 4 0
4 0 4 0 4 0 4 0 4 0 4 0 4 0 4 0 4 0

4 0

- - 

### 4 0 4 0 

### 4 0 20 0 20 0 4 0

- -

- -

- -

- -

- - 

### 8 9

8 9

\P.2 5

! 1 i

I 

# i

1 

# 1 

# 1 1 1 1 OT C Semivolatil e Organic ; TCL P Leachat e Metho d827 0

Clien t Name : America nPetroleu m Institut e Clien t ID : Sit e C Crud e Tan kBottom s LabID : 006344-0002-S A Ensec o ID : 105077 7 Matrix : WAST E Sampled : 3 0 AU G Authorized : 3 1 AU

G8 9 Prepared : 2 1 SE P

Paramete r Resul t
Pyridin e ND Pheno l ND bis(2-Chloroethyl)ethe r ND 1,4-Dichlorobenzen e ND 1,2-Dichlorobenzen e ND o-Creso l ND
m & p-Cresol(s ) ND Hexachloroethan e ND Nitrobenzen e N D Hexachlorobutadien e N O 2,4,6-Trichloropheno l ND 2,4,5-Trichloropheno l ND 2,4-Dinitrotoluen e ND Hexachlorobenzen e ND 2,3,4,6-Tetrachloropheno l ND Pentachloropheno l ND
Nitrobenzene-d 5 N A 2-Fluorobipheny l N A Terphenyl-dl 4 N A PhenoT-d 5 N A 2-Fluoropheno l N A 2,4,6-Tribromopheno l N A

ND» No t detecte d N A - No t applicabl e 

### 8 9 8 9

Unit s mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L

% % % fa fa fa Received : 3 1 AU G8 9 Analyzed : 0 2 OC T 8 9
Reportin g Limi t

- - 

### 2. 0 2. 0 2. 0 2. 0 2. 0 2. 0 2. 0 2. 0 2. 0 2. 0 1 0 2. 0 2. 0 2. 0

1 A 

### 1 0

- -

• "

• * •

* * * •

" * *

Reporte dBy : Marshal l Tilbur y Approve dBy : Jef f Lowr y

.

•
.Metal s
Tota l Metal s P.2 6

CIien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r

Aluminu m Antimon y Arseni c Bariu m Beryl l.i umr Cadmiu m Calciu m : = Chromium* 5 Cobal t Coppe r Lea d Mercury Nicke l Potassiu

m Seleniu m Silve r Sodiu m Thalliu m Ti n Vanadiu m Zin c American Petroleu m Institut e Sit e C Crud e Tan

k Bottom s 006344-0002-S AEnsec o ID : WAST E Sampled : 3 1 AU G8 9 105077 7 3 0 AU G8 9 Prepared : Se e Below Received : Analyzed :

Resul t • Unit s

1 3 N D 

## o. : 7 0 N D N D 134 0 5 N D 3 3 14 0 N D 5 N D N D N D 951 0 N D N D 4 6 3 Reporting Analytica l

Limi t Metho d

mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/k g mg/k g mg/k g mg/k g mg/kg 1 0

5 0. 5

• 10. 2 0. 5 3 0 1 1 1 5 0
, 4 50 0 0 1 50 0 1 1 1 1 1 

### 1 601 0 601 0 706 0 601 0 601 0 601 0 601 0 601 0 601 0 601 0 601 0 •747 1 601 0 601 0 774 0 601 0 601 0 784 1 601 0 601 0 601 0 3 1 AU G8 9 Se e Below

Preoare d Dat e


### 0 5 0 5 0 8 0 5 0 5 0 5 0 5 0 5 0 5 0 5 0 5 1 4 0 5 0 5 0 8 0 5 0 5 0 8 0 5 0 5 0 5 

### SE P SE P SE P SE P SE P SE P SE P SE P SE P SE P SE P SE P SE P SE P SE P SE P SE P SE P 

### SE P SE P SE P 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 Analyze d Dat e

1 8 SE P 39

. 1 8 SE P 8 9 1 1 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 7 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 1 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 1 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9

_ N D= No t detected N A - Not applicabl e

Reporte dBy : Fre

dVelasque z Approve dBy : Toni Lus kP.2 7

ICP/M S Metal s

Tota l Metal s
Clien t Name : America n Petroleu mInstitut e Clien t ID : Sit e C Crud e Tan k Bottom s La bID : 006344-0002-S AEnsec o ID : 1050777
, Matrix : WAST E • Sampled : 3 0 AU G8 9 Authorized : 3 1 AU G8 9 Prepared : Se e Belo w Received : 3 1 AU G8 9 Analyzed : Se e Belo w

Paramete r
Osmiu m(189 ) Resul t

ND Unit s

mg/k g Reportin g Analytica l

Limi t Metho d Prepare d Dat e Analyze d

Dat e


### 0. 1 RMA

L 0 7 OC T 8 9 1 4 OC T 8 9

ND» No t detecte d > N A - No t applicabl e
Reporte dBy : Scot t Heidema n Approve dBy : Ton i Tallaric oP.2 8

Metal s

TCL P Leachat e
Clien t Name : America nPetroleum Institut e Clien t ID : Sit e C Crud e Tan kBottom s LabID : 006344-0002-S A Ensec o ID : 105077 7 Matrix : WAST E Sampled : 3 0 AUG8 9 Received : 3 1 AUG8 9 Authorized : 3 1 AUG8 9 Prepared : Se e Belo w Analyzed : Se e Belo w

Paramete r Resul t Unit s
Arseni c Barium Cadmium Chromium Lead
. Silve r Mercur y Selenium 

### N D 24 N D N D 2 N D N D N D mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L Reportin g

Limi t



### 2 0. 2 0. 1 0. 2 1 0. 2 0.00 8 0.0 8 Analytica l

Metho d

200. 7 200. 7 200. 7 200. 7 200. 7 200. 7 747 1 270. 2 Prepare d

Dat e

1 4 SE P 8 9 1 4 SE P 8 9 1 4 SE P 8 9 1 4 SE P 8 9 1 4 SE P 8 9 1 4 SE P 8 9 1 4 SE P 8 9 1 4 SE P 8 9 Analyze d

Dat e

2 0 SE P 3 9 2 0 SE P 3 9 2 0 SE P 3 9 2 0 SE P 8 9 2 0 SE P 8 9 2 0 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9



# J

J

ND= No t detecte d -\ N A » No t applicabl e
Reporte dBy : Sandr a Jone s Approve dBy : Ton i Lus k



# 1Genera l Inorganic s P.2 9

CIien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r America n Petroleu mInstitut e

Sit e C Crud e Tan k Bottom s 006344-0002-S AEnsec o ID : WAST E Sampled : 3 1 AU G8 9 Prepared : 105077 7 3 0 AU G8 9 Se e Belo w Received :

Analyzed :

Chlorid e Cyanide
, Reactiv e Ignitabilit y Non-Volatil e Oi l Volatil e Oi l Oi l Wate r Solid s OH Sulfide
, Reactiv e Resul t Unit s Reportin g Analytica l Limi t Metho d

1490 0 

### N D 6 6 17. 7 

### 1. 5 19. 2 71. 4 10. 8 

### 6. 9 N D mg/k g mg/k g • deg

. F
0/ 10 0 / /a Of to %

0/ to unit s •ng/k g 

### 15



### 0. 1

- - 

### 0. 1 0. 1 0. 1 0. 1 0. 1

0. 5 300. 0 Mo d EPA-OS W 1010/102 0 Chevro n Chevro n Chevro n Chevro n Chevro n 9045/AST M EPA/OS W '3 1 AU G3 9

Se e Belo w

Prepare d Dat e

0 1 SE P 8 9 N A N A N A N A N A N A N A N A N A Ana i vze o

Dat e

1 3 0 8 3 9 3 9 1 2 OC T 8 9 0 6 OC T 8 9 0 6 OC T 8 9 0 6 OC T 8 9 0 6 OC T 8 9 0 6 OC T 8 9 2 3 SE P 8 9 0 8 SE ? 9 9 o 1

Not e o : Thi s tes t i s unreliabl e fo r an y sampl e othe r tha na non-aqueou s liquid

.

Not e 1 : Sampl e hazardou s du e t o ignitability

.

ND = No t detecte d N A= No t applicabl e

Reporte dBy : Blak e Besse r Approve dBy : Tamm y Baile yP.3 0

FO R

AMERICANPETROLEU M INSTITUT E

ENSECO-RMA L NO

. 00629 9

OCTOBE R27 , 198 9 Rock yMountain Anaivnca i Laborator

v



## ANALYTICA LRESULTS JUTlSCC O

Reviewe d by : 

# ^•^•vJHi^-

ViMjULJ^Jht^C

Jeann e B . Howber t

Ensec o Incorporate d j"-)^* " Yarrow Stree t

^ Arvaua

. (.".oiorad o M>0<> 2 j 303/421-oo UFa:< : 303-4M-717 1P.3 1

Appendi xI

XVolatil e Organic s

Metho d824 0

CIien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r America nPetroleu m Institut e Sit e # 3 Produce dWate r Tan k 006299-0003-S A

Ensec o ID : WAST E Sampled : 2 8 AU G8 9 Prepared :

Aceton e Acetonitril e Acrolei n Acrylonitril e Ally l chlorid e Benzen e Bromodichloromethan e Bromoform Bromomethan e Carbo ndisulfid e Carbo ntetrachlorid e Chlorobenzen e Chloropren e Chloroethan e Chlorodibromomethan e Chloroform Chloromethan e DBC P (1,2-Dibromo

3-chloropropane ) ED B (1,2-Dibromoethane ) Dibromomethan e trans-1,4-Dichloro

2-buten e Di chlorod i f1uoromethan e 1,1-Dichloroethan e 1,2-Dichloroethan e trans-1,2-Dichloroethen e 1,1-Oichloroethen e Dichloromethan e 1,2-Dichloropropan e cis-1,3-Dichloropropen e trans-1,3-Dichloropropen e 1,4-Dioxan e Ethy l benzen e Ethy l cyanid e 2-Hexanon e Iodomethan e Isobuty l alcoho l Methacrylonitr.il e Methy l ethy l keton e 4-Methyl-2-pentanon e 105076 7 2 4 AU G8 9 0 1 SE P 8 9

esul t



### N D N D N O N O N D 270 N D N O N D N D N D N D N O N D N D N D N D

N D N D N D
N D N D N D N O N D N D N O N D N O N O N D 600 N D N O N D N D N D N D N D Received : 2 5 AU G Analyzed : 0 6 SE P

Unit s mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g Reportin g

Limi t 

### 200 200 0 200 0 200 0 

### 10 0 10 0 10 0 10 0 200 10 0 10 0 10 0 10 0 200 10 0 10 0 200
10 0 10 0 100 10 0 200 10 0 10 0 10 0 100 100 100 100 100 200 0 

### 10 0 100 200 100 200 0 

### 100 200 200 8

9 8 9

N O- No t detecte d N A > No t applicabl e
Reporte dBy : Dian e Pag e (continue donfollowin gpage )

Approve dBy : Jef f Lowr yP.3 2

Appendi xI

XVolatil e Organic s

Metho d824 0

Clien t Name : America nPetroleu m Institut e Clien t ID : Sit e # 3 Produce dWate r Tank LabID : 006299-0003-S A Ensec o ID : 105076 7 Matrix : WAST E Sampled : 2 4 AU G8 9 Authorized : 2 8 AUG8 9 Prepared : 0 1 SE P 8 9

Paramete r Resul t
Styren e ND 1,1,1,2-Tetrachloroethan e N D 1,1,2,2-Tetrachloroethan e NO Tetrachloroethen e NO Toluen e 63 0 1,1,1-Trichloroethan e ND 1,1,2-Trichloroethan e NO Trichloroethen e ND Trichlorofluoromethan e N D 1,2,3-Trichloropropan e ND Viny l acetat e ND Viny l chlorid e ND Tota l xylene s 79 0

Toluene-d 8 10 3 4-Bromof1uorobenzen e (BFB ) 95. 6 1,2-Dichloroethane-d 4 94. 1

N D> No t detecte d N A « No t applicabl e (CONT. )

Unit s mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g
f.

% % Received : 2 5 AU G8 9 Analyzed : 0 6 SE P 8 9
Reportin g Limi t 

### 100 10 0 10 0 100 10 0 10 0 10 0 10 0 10 0 10 0 200 200 10 0

. .

- -

'

Reporte dBy : Dian e Pag e Approve dBy : Jef f Lowr yP.3 3

OT C Volatil e Organic s TCL P Leachat e Metho d824 0

Clien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r America nPetroleu m Institut e Sit e # 3 Produce dWate r Tank 006299-0003-S A

Ensec o ID : WAST E Sampled : 2 8 AUG8 9 Prepared : 105076 7 2 4 AUG8 9 1 3 SE P 8 9 Received : 2 5 AU G8 9 Analyzed : 1 9 SE P 8 9

Viny l chlorid e Acrylonitril e Methylen e chlorid e Carbo ndisulfid e 1,1-Dichlbroethen e Isobuty l alcoho l Chloroform 1,2-Dichloroethan e 2-Butanon e 1,1,1-Tr i chloroethan e Carbo ntetrachlorid e Trichloroethen e 1,1,2-Tr i chloroethan e Benzen e 1,1,1,2-Tetrachloroethan e 1,1,2,2-Tetrachloroethan e Tetrachloroethen e Toluen e Chlorobenzen e Toluene-d 8 4-Bromofluorobenzen e (BFB ) 1,2-D i chloroethane-d 4 sui t


### N D N D N D N D N D N O N D N D N O N D N D N D N D 1 2 N D N D N D 20 N D

95. 1

91. 8 

### 10 9 Unit s mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L

%

% % Reportin g

Limi t 

### 3. 2 3 2 1. 6 1. 6 1. 6 3 2 1. 6 1. 6 3. 2 1. 6 1. 6 1. 6 1. 6 1. 6 1. 6 1. 6 1. 6 1. 6 1. 6

-- '

- -

- -

ND- No t detecte d N A - No t applicabl e
Reporte dBy : Lis a Trau t Approve dBy : Jef f Lowr yP.3 4

Refiner y Hazardou s Constituen t Semivolatile s

Metho d827 0

Clien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r America nPetroleu m Institut e Sit e # 3 Produce dWate r Tank 006299-0003-S A

Ensec o ID : WAST E 2 8 AUG8 9 105076 7



# 1 Anthracen e Benzo(a )anthracen e Benzo(b)f1uoranthen e Benzolk)fluoranthen e Benzo(a)pyren e bis(2-Ethylhexyl ) phthalat e Buty l benzy l phthalat e Chrysen e Dibenz(a,h)anthracen e Di-n-buty l phthalat e 1,2-Dichlorobenzen e 1,3-D i chlorobenzen e 1,4-D i chlorobenzen e Diethy l phthalat e 7,12-D1methylbenz

anthracen e Dimethy l phthalat e Di-n-octy i phthalat e Fluoranthen e Inden e 1-Methylnaphthalen e Naphthalen e Phenanthren e Pyren e Pyridin e Quinolin e Benzenethio l o-Creso l
. m & p-Cresol(s ) 2,4-Dimethylpheno l 2,4-Dinitropneno l 4-Nitropheno l Pheno l

Nitrobenzene-d 5 2-Fluorobiphenyl

Terphenyl-dl 4 Phenol-d 5 2-Fluoropheno l 2,4,6-Tr i bromopheno l

N D• No t detecte d N A - No t applicabl e
Reporte dBy : Belind a Guerr a Sampled : 2 4 AUG Prepared : 0 5 SE P

Resul t



### N D N D N O N D N D
N D N O N O N D N D N D N D N O N O
N D N D N D N D N D 11 0 83 N D N D N O N D N D N D N D N O N D N D N D 8 9 F 8 9 /

Unit s mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g Received : Analyzed : 2 5 AU

G 0 2 OC T 8 9 8 9
Reportin g Limi t

4 0 4 0 4 0 4 0 4 0

4 0 4 0 4 0 4 0 4 0 4 0 4 0 4 0 4 0

4 0 4 0 4 0 4 0 4 0 4 0 4 0 4 0 4 0

4 0

4 0 4 0 4 0 20 0 20 0 4 0

79. 4 80. 8 10 0 56. 0 52. 8 50. 0 fa

fa % % fa f.

Approved

- By : Jef f Lowry



# ]P.3 5

OT C Semivolatil e Organic s TCL P Leachat e Metho d 827 0

Clien t Name : America n PetroleumInstitut e Clien t ID : Sit e # 3 Produce d Wate r Tan k LabID : 006299-0003-S AE"?ec o ID : 105076 7 Matrix : WAST E :mp"ed : 2 4 AU G 8 9 Authorized : 2 8 AU G 8 9 -pared : 2 1 SE P 8 9

Paramete r Pyridin e Pheno l bi s(2-Chloroethyl)ethe r 1,4-Dichlorobenzen e 1,2-Dichlorobenzen e o-Creso l
m& p-Cresol(s ) Hexachloroethan e Nitrobenzen e Hexachlo r jtadien e 2,4,6-Tr i
, ; oropheno l 2,4,5-Tr i cnloropheno l 2,4-Dinitrotoluen e Hexachlorobenzen e 2,3,4,6-Tetrachloropheno l Pentachloropheno l

Nitrobenzene-d 5 2-Fluorobipheny l Terpheny l -<11 4 Phenol-d 5 2-Fluoropheno l 2,4,6-Tr i bromopheno l Received : 2 5 AU C 3 9 Analyzed : 0 4 OC T 8 9

•sui t

N D N D N D N O N O N O N D N D N D N D N O N D N D N D N D N O

10 1 68. 4 71. 8 62. 1 62. 8 65. 5 Unit s

mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/L

% % % % % fa Reportin g

L i

- t

0.04 9 0.04 9 0.04 9 0.04 9 0.04 9 0.04 9 0.04 9 0.04 9 0.04 9 0.04 9 0.2 4 0.04 9 0.04 9 0.04 9 0.2 4

- -

- -

- -

- -

- -

- -

ND - No t detecte d N A - No t applicabl e
Reporte dBy : Da nAlbritto n Approve dBy : Jef f LowryP.3 6

Clien t Name : American Petroleu m Clien t ID : Sit e # 3 La bID : 006299

- Matrix : WAST E Authorized : 2 8 AU

G

Paramete r
Aluminu m Antimon y Arseni c Bariu m Berylliu

m Cadmiu m Calciu m Chromiu m Cobal t Coppe r Lea d Mercury

. Nicke l Potassiu

m Seleniu m Silve r Sodiu m Thalliu m 

### Ti n Vanadiu m Zin c

N D - No t detecte

d N A• Not applicabl e Metal s

Tota l Metal s
Institut e Produce d Wate r Tan

k 0003-S A



### 8 9

Resul t


### 97 4 N O 1 0 

### 18 0 N D 

### 3 3550 0 

### 5 4 

### 4 19 0 97 0 N D 6 1 N D N D N D 942 0 

### N D N D 5 37 0

Reporte dBy : Fre

dVelasque z insec o ID :

Sampled : Prepared :

Unit s
mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg ' mg/k g mg/k g mg/k g mg/k g 105076 7 2 4 AU G8 9 Se e Below Reporting Limi t


### 2 0 1 0 

### 1 2 0. 4 

### 1 4 0 

### 2 2 2 1 0 

### 0. 1 

### 8 100 0 

### 5 2 100 0 

### 1 0 1 1 

### 2 2 ,

Received : Analyzed :
Analytica l Metho d

601 0 601 0 706 0 601 0 601 0 601 0 601 0 601 0 601 0 601 0 601 0 747 1 601 0 601 0 774 0 601 0 601 0 784 1 601 0 601 0 601 0

Approve dBy : Tamm

y Baile y 

### 2 5 

### AU G Se e Be l 

### 8 9 o w

Prepare d Dat e


### 0 5 0 5 0 6 0 5 0 5 0 5 0 5 0 5 0 5 0 5 0 5 0 1 0 5 0 5 0 6 0 5 0 5 0 6 0 5 0 5 0 5 

### SE P SE P OC T SEP SE P SE P SE P SE P SE P SE P SE P SE P SE P SEP OC T SEP SE P OC T SEP SE P 

### SE P 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 

### An e ilvze d Dat e


### 1 8 1 8 1 0 1 8 1 8 1 8 1 8 1 8 1 8 1 8 1 8 1 1 1 8 1 8 1 0 1 8 1 8 1 0 1 8 1 8 1 8 

### SE P SE P OC T SEP SE P SE P SE P SE P SE P SE P SEP SE P SE P SEP OC T SEP SE P OC T SEP SE P SEP 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9P.3 7

CIien t Name : Clien t ID : La bID : Matrix : Authorized : ICP/M S Metal s

Tota l Metal s
America n Petroleum

Institut e Sit e # 3 Produce d Wate r Tan k 006299-0003-S AEnsec o ID : WAST E Sampled : .2 8 AU G8 9 Prepared : 105076 7 2 4 AU G3 9 Se e Belo w Received : 2 5 "JG8 9

Analyzed : Se e .elow

Paramete r
Osmiu m(189 ) Resul t Unit s Reportin g Analytica l Limi t Metho d Prepare d Dat e Analyze d

Dat e


### N O mg/k g 

### M RMA L 0 7 OC T 8 9 14.OC T 8 9

N D * No t detecte d N A - No t applicabl e
Reporte dBy : Scot t Heideman Approve dBy : Ton i Tallaric oP.3 8

Metal s

TCL P Leachat e
Clien t Name : America n PetroleumInstitut e Clien t ID : Sit e # 3 Produce d Wate r Tan k
.a bI D Matri x 006299-0003-S AEnsec o ID : 105076 7

WAST E Sampled : 2 4 AU G8 9 Received : 2 5 AUG8 9 Authorized : 2 8 AU G8 9 Prepared : Se e Belo wAnalyzed : Se e Belo w Reportin g Analytica l Prepare d Analyze d
Paramete r Resul t Unit s Limi t Metho d Dat e Dat e Arseni c ND mg/ L 0. 6 200. 7 1 4 SE P 8 9 2 0 SE P 8 9 Barium0.5 1 mg/ L 0.0 6 200. 7 1 4 SE P 8 9 2 0 SE P 8 9 CadmiumND mg/ L 0.0 3 200. 7 1 4 SE P 8 9 2 0 SE P 8 9 ChromiumN O mg/ L 0.0 6 200. 7 1 4 SE P 8 9 2 0 SE P 8 9 Lea d N O mg/ L 0. 3 200. 7 1 4 SE P 8 9 2 0 SE P 8 9 Silve r ND mg/ L 0.0 6 200. 7 1 4 SE P 8 9 2 0 SE P 8 9 Mercur yN O mg/ L 0.00 4 747 1

. 1 4 SE P 8 9 1 4 SE P 8 9 SeleniumND mg/ L 0.0 7 270. 2 1 4 SE P 8 9 1 8 SE P 8 9

ND - No t detecte d N A- No t applicabl e
Reporte dBy : Sandr a Jone s Approve dBy : Tamm y BaileyP.3 9

Genera l Inorganic s

Clien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r
Chlorid e America nP e

Sit e # 3 006299

- WAST E 2 8 AU G

Cyanide , Reactiv e Ignitabilit y Non-Volatil e Volatil e Oi l 

### Oi l Wate r Solid s 

### p H Oi

l

Sulfide , Reactiv e troleu m Institut e Produce dWate r Tank 000 3


### 8 9 -SA Ensec o M .

Resul t

851 0 

### N D 68 22. 1 

### 4. 1 26. 2 33. 0 45. 7 

### 8. 3 3 4 Samp l Prepar
. :

Unit s mg/k g mg/k g deg
. F f. f. fa % fa unit s mg/k g 105076 7 2 4 AU G8 9 Se e Below Reportin g Limi t


### 1 5 0. 1

- - 

### 0. 1 0. 1 0. 1 0. 1 0. 1

- - 

### 0. 5 Received :

Analyzed : Analytica l Metho d

300. 0 Mod
. EPA-OS W 1010/102 0 Chevro n Chevro n Chevro n Chevro n Chevro n 9045/AST M EPA/OS W 

### 2

5 Se e AU G Be l 8 9 o w Prepare d Dat e 

### 0 7 N A N A N A N A N A N A N A N A N A 

### SE P 8 9 Analyze d

Dat e
1 3 SE P 8 9 0 8 SE P 8 9 1 0 OC T 89

- o l 1 9 OC T 8 9 1 9 OC T 8 9 1 9 OC T 8 9 1 9 OC T 8 9 1 9 OC T 8 9 1 1 SE P 8 9 0 8 SE P 8 9

Not e o : Thi s tes t i s unreliabl e fo r an y sampl e othe r tha na non-aqueou s liquid

.
Not e 1 : Sampl e 3 i s hazardou s du e t o ignitabilit y fo r flashpoint

.

NO- No t detecte d N A - No t applicabl e
Reporte dBy : Blak e Besse r Approve dBy : Tamm y Baile yP.4 0

Appendi xI

XVolatil e Organic s

Metho d824 0

CIien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r America nPetroleu m Institut e Sit e # 1 Crud e TankBottom s 006299-0001-S A

Ensec o ID : WAST E Sampled : 2 8 AUG8 9 Prepared :

Aceton e Acetonitril e Acrolei n Acrylonitril e Ally l chlorid e Benzen e Bromodichloromethan e Bromoform Bromomethan e Carbo ndisulfid e Carbo ntetrachlorid e Chlorobenzen e Chlbropren e Chloroethan e Chlorodibromomethan e Chlorofor m Chloromethan e DBC P (1,2-Dibromo

3-chloropropane ) ED B (1,2-Dibromoethane ) Dibromomethan e trans-1,4-Dichloro

2-buten e Di chlorod i f1uoromethan e 1,1-Dichloroethan e 1,2-Dichloroethan e trans-1,2-Dichloroethen e 1,1-Dichloroethen e Dichloromethan e 1,2-Dichloropropan e cis-1,3-Dichloropropen e tran s -1,3-D i chloropropen e 1,4-Dioxan e Ethy l benzen e Ethy l cyanid e 2-Hexanon e Iodomethan e Isobuty l alcoho l Methacrylonitril e Methy l ethy l keton e 4^Methyl-2-pentanon e 105076 5 2 4 AU G8 9 0 1 SE P 8 9

esul t



### N D N O N D N D N D 250 N D N D N O N O N O N D N D N D N D N D N D

N D N O N O

N O N O N D N O N O N D N D N D N D N D N D 240 N D N O N D N D N D N D N D Received : 2 5 AU G8 9 

### A n

Unit s
mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g
mg/k g mg/k g mg/k g
mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g ilyzed : 0 6 SE P 8 9

Reportin g Limi t


### 100 100 0 100 0 100 0 

### 50 50 5 0 50 100
. 

### 5 0 50 50 50 100 50 50 100
5 0 50 50
50 100 50 50 50 50 50 50 50 5 0 100 0 

### 50 50 100 5 0 100 0 

### 50 100 10 0

ND- No t detecte d N A - No t applicabl e

Reporte dBy : Dian e Pag e (continue donfollowin g page )

Approve dBy : Jef f Lowr yP.4 1

Appendi xI

XVolatil e Organic s

Metho d824 0

Clien t Name : America nPetroleu m Institut e Clien t ID : Sit e # 1 Crud e Tan kBottom s La bID : 006299-0001-S A Ensec o ID : 105076 5 Matrix : WAST E Sampled : 2 4 AUG8 9 Authorized : 2 8 AUG8 9 Prepared : 0 1 SE P 8 9

Paramete r Resul t

Styren e N D 1,1,1,2-Tetrachloroethan e ND U1,2,2-Tetrachloroethan e N D Tetrachloroethen e ND Toluen e 47 0 1,1,1-Trichloroethan e ND 1,1,2-Trichloroethan e ND Trichloroethen e ND Trichlorofluoromethan e ND 1,2,3-Trichloropropan e ND Viny l acetat e ND Viny l chlorid e ND Tota l xylene s 57 0

Toluene- c 4-Bromof l 

### (BFB ; 1,2-Dich l 8 10 4

uorobenzen e 

### 10 1 oroethane-d 4 91. 1 (CONT. ) ,

Received : 2 5 AUG8 9 Analyzed : 0 6 SE P 8 9

Unit s mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

%

fa fa Reportin g

Limi t


### 5 0 5 0 5 0 5 0 5 0 5 0 5 0 5 0 5 0 5 0 10 0 10 0 5 0

- -

- - t'



### ND= No t detecte d N A - No t applicabl e
Reporte dBy : Dian e Pag e Approve dBy : Jef f Lowr yP.4 2

OT C Volatil e Organic s TCL P Leachat e Metho d824 0
Clien t Name : America nPetroleu m Institut e Clien t ID : Sit e # 1 Crud e Tan kBottom s LabID : 006299-0001-S A Ensec o ID : 105076 5 Matrix : WAST E Sampled : 2 4 AUG8 9 Authorized : 2 8 AUG8 9 Prepared : 1 3 SE P 8 9

Paramete r Resul t Viny l chlorid e ND Acrylonitril e ND Methylen e chlorid e 3. 2 Carbo ndisulfid e N D 1,1-Dichloroethen e ND Isobuty l alcoho l NO Chlorofor m

N D 1,2-Dichloroethan e ND 2-Butanon e N O 1,1,1-Trichloroethan e ND Carbo ntetrachlorid e N D Trichloroethen e ND 1,1,2-Trichloroethan e ND Benzen e 2 0 1,1,1,2-Tetrachloroethan e NO 1,1,2,2-Tetrachloroethan e N D Tetrachloroethen e N D Toluen e 3 7 Chlorobenzen e N D

Toluene-d 8 10 5 4-Bromof1uorobenzen e (BFB ) 99. 5 l,2-0ichloroethane-d 4 10 0

ND- No t detecte d N A « No t applicabl e Unit s mg/ L mg/ L mg/ L mg/ L mg/ L 

### mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L

fa

fa fa Received : 2 5 AU G3 9 Analyzed : 1 5 SE P 8 9
Reportin g Limi t


### 4. 2 4 2 2. 1 2. 1 2. 1 4 2 2. 1 2. 1 4. 2 2. 1 2. 1 2. 1 2. 1 2. 1 2. 1 2. 1 2. 1 2. 1 2. 1

. .

Reporte dBy : Lis a Trau t Approve dBy : Jef f Lowr y 

# ^ 1

tP.4 3

Clien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r Refiner y Hazardou s Constituen t Semivolatile s

Metho d827 0

America nPetroleu

m Institut e Sit e # 1 Crud e Tan kBottom s 006299-0001-S A

Ensec o ID : WAST E Sampled : 2 8 AUG8 9 Prepared :

Anthracen e Benzo(a)anthracen e Benzo(b)fluoranthen e Benzo(k)fluoranthen e Benzo(a)pyren e bis(2-Ethylhexyl ) phthalat e Buty l benzy l phthalat e Chrysen e Dibenz(a,h)anthracen e Di-n-buty l phthalat e 1,2-Dichlorobenzen e 1,3-Dichlorobenzen e 1,4-Dichlorobenzen e Diethy l phthalat e 7,12-Oimethylbenz

anthracen e Dimethy l phthalat e Di-n-octy l phthalat e Fluoranthen e Inden e 1-Methylnaphthalen e Naphthalen e Phenanthren e Pyren e Pyridin e Quinolin e Benzenethio l o-Creso l
m & p-Cresol(s ) 2,4-Dimethy l pheno l 2,4-Dinitropneno l 4-Nitropheno l Pheno l

Nitrobenzene-d 5 2-Fluorobipheny l Terphenyl-dl 4 Phenol-d 5 2-Fluoropheno l 2,4,6-Tr i bromopheno l

N D- No t detecte d N A - No t applicabl e
Reporte dBy : Belind a Guerr a 105076 5 2 4 AUG8 9 0 5 SE P 8 9

lesul t


### N D N D N D N D N D
N O N O N D N D N D N D N D N O N D

N D N D N D N O N D 18 0 11 0 4 2 N D N D N D N D N D N D N D N D N D N D

65. 6 62. 4 75. 4 67. 4 65. 4 68. 9 

### Re

c An <

Unit s mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

fa fa % %
1 % :eived : 2 5 AU G ilyzed : 0 2 OC T
Reportin g Limi t 

### 4 0 4 0 4 0 4 0 4 0
4 0 4 0 4 0 4 0 4 0 4 0 4 0 40 40
4 0 40 4 0 40 40 4 0 4 0 4 0 4 0

- - 

### 40

- - 

### 40 4 0 40 200 200 4 0

- -

- -

- -

- -

Approve dBy : Jef f Lowr y 

### 8 9 8 9P.4 4 

# 1

OT C

CIien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r Sit e # 1 Crud e 1

006299-0001-S A WAST E 2 8 AU G 8 9

Pyridin e Pheno l bis(2-Chloroethyl)ethe r 1,4-D i chlorobenzen e 1,2-D i chlorobenzen e o-Creso l
m& p-Cresol(s ) Hexachloroethan e Nitrobenzen e Hexachlorobutad i en e 2,4,6-Tr i chloropheno l 2,4,5-Tr i chloropheno l 2,4-Dinitrotoluen e Hexachlorobenzen e 2,3,4,6-Tetrachloropheno l Pentachloropheno l

Nitrobenzene-d 5 2-Fluorobipheny l Terphenyl-dl 4 Phenol-d 5 2-Fluoropheno l 2,4,6-Tr i bromopheno l Semivolatil e Organic s TCL P Leachat e Method 827 0

Institut e Bottoms Enseco.ID : 105076 5 Sampled : 2 4 AU

G 8 9 Prepared : 2 1 SE P 8 9

Resul t



### N D 0.03 5 

### N O N O N O 0.04 0 0.07 5 

### N D N D N D N D N D N D N D N D N D

93. 8 81. 9 83. 4 80. 0 77. 5 82. 0 Unit s

mg/ L mg/ L mg/ L mg/ L mg/ L 

### mg/ L mg/ L mg/ L mg/ L mg/ L 

### mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L

% 

### X % % % fa Received : 2 5 AU G 8 9 Analyzed : 0 4 OC T 8 9
Reporting Limi t

0.02 9 0.02 9 0.02 9 0.02 9 0.02 9 0.02 9 0.02 9 0.02 9 0.02 9 0.02 9 0.1 4 0.02 9 0.02 9 0.02 9 0.1 4

. .

- -

- -

- -

- -

- -

N O- No t detecte d N A - No t applicabl e

Reporte dBy : Da nAlbritto n Approve dBy : Jef f LowryP.4 5

Metal s

Tota l Metal s

Name : ID : Clien t Clien t La bID : Matrix : Authorize d American Petroleu mInstitut e Sit e # 1 Crud e Tan

k Bottom s 006299-0001-S AEnsec o ID : 105076 5 WAST E Samoled : 2 4 AU G8 9 2 8 AU G8 9 Prepared : Se e Below Received : Analyzed :

Paramete r

Aluminu m Antimon y Arseni c Bariu m Berylliu

m Cadmiu m Calciu m Chromiu m Cobal t Coppe r Lea d Mercury Nicke l Potassiu

m Seleniu m Silve r Sodiu m Thalliu m Ti n Vanadiu m Zin c Resul t Reporting Analytica l Unit s Limi t Metho d


### 3 5 N D 

### 2 2 3 N D N O 123 0 

### 5 N D 14 2 7 N D 16 N D N D N D 204 0 

### N D N D 

### 3 3 4 mg/k g

mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g 1 0

5 1 1

. 0

. 0

. 3 0 1 1 1 5 0

. 4 50 0 0
, 1 50 0 1 0 1 1 1 1 601 0 601 0 706 0 601 0 601 0 601 0 601 0 601 0 601 0 601 0 601 0 747 1 601 0 601 0 774 0 601 0 601 0 784 1 601 0 601 0 601 0 2 5 AU G8 9 Se e Belo w

Prepare d Dat e

0 5 SE P 8 9 0 5 SE P 8 9 0 6 OC T 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 1 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 6 OC T 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 6 OCT 8 9 0 5 SEP 8 9 0 5 SE P 8 9 0 5 SE P 8 9 Analyze d

Dat e

.
1 8 SE P 89

- 1 8 SE P 8 9 1 0 OC T 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 ll'SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 0 OC T 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 0 OC T 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9

N D - No t detecte d N A« No t applicabl e

Reporte dBy : Fre

dVelasque z Approve dBy : Tamm

y Baile y

# I P.4 6 

# 1

ICP/M S Metal s

Tota l Metal s Clien t Name : America n PetroleumInstitut e Clien t ID : Sit e # 1 Crud e Tan k Bottom s iff

- ? : 2Sf|f 9 - ° 001

- S A£n sec o ID : 105076 5 Matrix : WAST E SamDled * 2 4 AU G8 9 Authorized : 2 8 AU G8 9 Prepaid

. Se e Belo w Received : 2 5 AU G8 9 Analyzed : Se e Belo w

Paramete r
Osmiu m (189 ) Resul t

. Unit s Reportin g Analytica l Limi t Metho d Prepare d Dat e Analyze d

Dat e 

### N O mg/k g 

### 0. 1 RMA L 0 7 OC T 8 9 1 4 OC T 8 9

ND- No t detecte d N A - No t applicabl e

Reporte dBy : Scot t Heidema n Approve dBy : Ton i Tallaric oP.4 7

Metal s

TCL P Leachat e
Clien t Name : Clien t ID : La bIC

Matri : Authorized :

Paramete r
Arseni c Barium Cadmiu m Chromium Lea d Silve r Mercur y Selenium America n Petroleum

Sit e # 1 Crud e Ta * 006299-0001-S A V ~TE

- ,U G8 9

Resul t Institut e

3ottom s nsec o ID : Sampled : Prepared :

Unit s 105076 5 2 4 AU G8 9 Se e Belo w Reportin g Analytica l Limi t M

< "

ND 0 ND N O 4. 2 NO ND ND 

### 9 9 mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L 

### 0. 6

0.0 6 0.0 3 0.0 6 

### 0. 3 0.0 6 0.00 4 0.0 7 200. 7 200. 7 200. 7 200. 7 200. 7 200. 7 747 1 270. 2 Received : A

. yzed :
ica l


### o d 2 5 AL

. 8 9

Se e Belo w
Prepare d Dat e
1 4 SE P 8 9 1 4 SE P 8 9 1 4 SE P 8 9 1 4 SE P 8 9 1 4 SE P 8 9 1 4 SE P 8 9 1 4 SE P 8 9 1 4 SE P 8 9 Analyze d

Oat e
2 0 SE P 8 9 2 0 SE P 8 9 2 0 SE P 8 9 2 0 SE P 8 9 2 0 SE P 8 9 2 0 SE P 8 9 1 4 SE P 8 9 1 8 SE P 8 9

ND - No t detecte d N A• No t applicabl e
Reporte dBy : Sandr a Jone s Approve dBy : Tamm y Baile yGenera l Inorganic s P.4 8

Clien t Name : America nPetroleum Clien t ID : Sit e # 1 La bID : 006299

- Matrix : WAST E Authorized : 2 8 AUG

Paramete r

Chlorid e Cyanide , Reactiv e Ignitabilit y Non-Volatil e Oi l Volatil e Oi l 

### Oi l Wate r Solid s 

### P H Sulfide , Reactiv e Crud e Tan k 000 1



### 89 •S A E



### Resul t

659 0 

### N D 72 27. 0 

### 8. 3 35. 3 48. 1 18. 0 

### 8. 0 1. 2 Institut e Bottom s nsec o ID : Sampled : Prepared :

Unit s
mg/k g mg/k g deg
. F fa % % % % unit s mg/k g 105076 5 2 4 AUG8 9 Se e Below
Reportin g Limi t


### 1 5 0. 1

- - 

### 0. 1 0. 1 0. 1 0. 1 0. 1

- - 

### 0. 5 Received :

Analyzed : Analytica l Metho d

300. 0 Mod
. EPA-OS W 1010/102 0 Chevro n Chevro n Chevro n Chevro n Chevro n 9045/AST M EPA/0S W 

### 2

5 Se eAU G Be l 89 o w
Prepare d Dat e


### 0 7 N A N A N A N A N A N A N A N A N A SE P 89 Analyze d

Dat e

13

- SE P 8 9 0 8 SE P 8 9 0 9 OC T 8 9 1 9 OC T 8 9 1 9 OC T 8 9 1 9 OC T 8 9 1 9 OC T 8 9 1 9 OC T 8 9 1 1 SE P 8 9 0 8 SE P 8 9 0 1

Not e o : Thi s tes t i s unreliabl e fo r anysampl e othe r tha n a

non-aqueou s liquid

.

Not e 1 : Sampl e 1 i s hazardou s du e t o ignitabilit yfo r flashpoint

.

N O - No t detecte d N A- No t applicabl e

Reporte d By : Blak e Besse r Approve d By : Tamm yBaile yP.4 9

Name : ID : Clien t CIien t La bID Matri x Authorize d Appendi xI XVolatil e Organic s

Metho d824 0

America nPetroleu

m Institut e Sit e # 1 3 S Pi t Skimming s 006299-^05-S A

Ensec o ID : 105076 9 WAST E Sampled : 2 4 AUG8 9 2 8 AUGb 9 Prepared : 0 1 SE P 8 9 Received : Analyzed : 2 5

0 6 AU G SE P

Paramete r

Aceton e Acetonitril e Acrolei n Acrylonitril e Ally l chlorid e Benzene . Bromodi chloromethan e Bromoform Bromomethan e Carbo ndisulfid e Carbo ntetrachlorid e Chlorobenzen e Chloropren e Chloroethan e Chlorod i bromomethan e Chloroform Chloromethan e DBC P (1,2-Dibromo

3-chloropropane ) EDB (1,2-Dibromoethane ) Dibromomethan e trans-1,4-Dichloro

2-buten e D i chlorod i f1uoromethan e 1,1-Dichloroethan e 1,2-Dichloroethan e trans-1,2-Dichloroethen e 1,1-Dichloroethen e Dichloromethan e 1,2-D i chloropropan e c i s-1,3-D i chloropropen e trans-1,3-Dichloropropen e 1,4-Oioxan e Ethy l benzen e Ethy l cyanid e 2-Hexanon e Iodomethan e Isobuty l alcoho l Methacrylonitril e Methy l ethy l keton e 4-Methyl-2 i pentanon e Resul t

ND ND N D NO ND 1 3 ND ND ND ND NO ND ND ND NO ND ND

N D N D N D

ND ND N D ND ND ND N D ND ND N D ND 8. 8 ND N D ND ND N D ND ND Unit s mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g
mg/k g mg/k g mg/k g
mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/kg
. mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g Reportin g

Limi t

1 0 10 0 10 0 10 0 5
. 5
. 5 ,

N D« No t detecte d N A * No t applicabl e
Reporte dBy : Oian e Pag e (continue do nfollowin gpage ) 8 9 3 9

0 0 0 5. 0 1 0 5. 0 5. 0 5. 0 5. 0 1 0 5. 0 5. 0 1 0

5. 0 5. 0 5. 0

5. 0 1 0 5. 0 5. 0 5. 0 5. 0 5. 0 5. 0 5. 0 5. 0 10 0 5. 0 5. 0 1 0 5. 0 10 0 5. 0 1 0

- 1 0

Approve dBy : Jef f LowryP.5 0

Appendi xIXVolatil e Organic s (CONT. )

Metho d 824 0

Clien t Name : America n PetroleumInstitut e Clien t ID : Sit e # 1 B S Pi t Skimming s La bID : 006299-0005-S AEnsec o ID : Matrix : WAST E Sampled : Authorized : 2 8 AU G8 9 Prepared :

Paramete r
Styren e 1,1,1,2-Tetrachloroethan e 1,1,2,2-Tetrachloroethan e Tetrachloroethene

. Toluen e 1,1,1-Trichloroethan e 1,1,2-Tr i chloroethan e Trichloroethen e Tr i chlorof1uoromethan e 1,2,3-Trichloropropan e Viny l acetat e Viny l chlorid e Tota l xylene s

Toluene-d 8 4-Bromof1uorobenzen e (BFB 1 1,2-D i ch1 oroethane-d 4 105076 9 2 4 AU G 0 1 SE P

esul t



### N D N D N D N D 11 N D N D N D N D N D N O N D 2 6


### 10 4

96. 6 94. 0 

### 8 9 8 9

Unit s
mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

%

fa % Received : 2 5 AU G8 9 Analyzed : 0 6 SEP-3 9
Reportin g Limi t


### 5. 0 5. 0 5. 0

. 

### 5. 0 5. 0 5. 0 5. 0 5. 0 5. 0 5. 0 1 0 1 0 

### 5. 0

- -

N D= No t detecte d N A - No t applicabl e

Reporte dBy : Dian e Pag e Approve dBy : Jef f LowryP.5 1



### CIien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r OT C Volatil e Organic s TCL P Leachat e Metho d824 0
America nPetroleu

m Institut e Sit e # 1 B S Pi t Skimming s 006299-0005-S A

Ensec o ID : 105076 9 WA M Sampled : 2 4 AU G8 9 2 8 nJG8 9 Prepared : 1 3 SE P 8 9 Received : Analyzed : 2 5 AU

G8 9 1 5 SE P 8 9

Viny l chlorid e Acrylonitril e Methylen e chlorid e Carbo ndisulfid e 1,1-Dichloroethen e Isobuty l alcoho l Chloroform 1,2-Dichloroethan e 2-Butanon e 1,1,1-Trichloroethan e Carbo ntetrachlorid e Trichloroethen e 1,1,2-Trichloroethan e Benzen e 1,1,1,2-Tetrachloroethan e 1,1,2,2-Tetrachloroethan e Tetrachloroethen e Toluen e Chlorobenzen e
Toluene-d 8 4-Bromofluorobenzen e (BF B 1,2-D i chloroethane-d 4 Resul t

N D N D N O N D N O N O N O N D N D N D N D N D N D 0.08 3 N D N D N D 0.03 3 N D


### 10 9
10 3 10 0 Unit s

mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/L mg/L mg/L



## r

. % 

### Reportin g

Limi t

0.05 0 0.5 0 0.02 5 0.02 5 0.02 5 0.5 0 0.02 5 0.02 5 0.05 0 0.02 5 0.02 5 0.02 5 0.02 5 0.02 5 0.02 5 0.02 5 0.02 5 0.02 5 0.02 5



### ND• No t detecte d N A - No t applicabl e Reporte dBy : Lis a Trau t Approve dBy : Jef f Lowr y



# IP.5 2

CIien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r Refinery Hazardou s Constituen t Semivolatile s

Metho d827 0

America nPetroleu

m Institut e Sit e # 1 B S Pi t Skimming s 006299-0005-S A

Ensec o ID : 105076 9 WAST E Sampled : 2 4 AU G8 9 2 8 AU G8 9 Prepared : 0 5 SE P 8 9



# 1 Anthracen e Benzo(a)anthracen e Benzo(b)fluoranthen e Benzo(k)f1uoranthen e Benzo(a)pyren e bis(2-Ethylhexyl ) phthalat e Buty l benzy l phthalat e Chrysen e Dibenz(a,h)anthracen e Di-n-buty l phthalate 1, 2 -Di ch1orobenzen e 1,3-Dichlorobenzen e 1,4-Dichlorobenzen e Diethy l phthalat e 7,12-Dimethylbenz

anthracen e Dimethy l phthalat e Di-n-octy l phthalat e Fluoranthen e Inden e 1-Methy l naphtha ! en e Naphthalen e Phenanthren e Pyren e Pyridin e Quinoline Benzenethi.o l o-Creso l

m & p-Cresol(s ) 2,4-Dimethylpheno l 2,4-Oinitropneno l 4-Nitropheno l Pheno l

Nitrobenzene-d 5 2-Fluorobipheny l Terphenyl-dl 4 Phenol-d 5 2-Fluoropheno l 2,4,6-Tr i bromopheno l

N D- No t detecte d N A - No t applicabl e

Reporte dBy : Belind a Guerr a Resul t Unit s


### N O N O N D N D N D
N O N O N O N D N D N D N D N D N D
N D N D N D N D N D N D N D 7 1 N D N D N D N D N D N D N D N O N D N O mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

. mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g Received : 2 5 AU G8 9 Analyzed : 0 2 OC T 8 9
Reportin g Limi t

4 0 4 0 4 0 4 0 4 0

4 0 4 0 4 0 4 0 4 0 4 0 4 0 4 0 4 0

4 0 4 0 4 0 4 0 4 0 4 0 4 0 4 0 4 0

4 0

4 0 4 0 4 0 20 0 20 0 4 0

59. 3 64. 3 74. 4 64. 6 66. 3 73. 8 fa

% % fa % fa

Approve dBy : Jef f Lowry


# 1P.5 3

OT C Semivolatil e Organic s TCL P Leachat e Metho d827 0

Clien t Name : America nPetroleu m Institut e Clien t ID : Sit e 1 B S Pi t Skimming s LabID : 006299-0005-S A Ensec o ID* Matrix : WAST E Sample a Authorized : 2 8 AU

G8 9 Prepared
.

Paramete r Pyridin e Pheno l bis(2-Chloroethyl)ethe r 1,4-Dichlorobenzen e 1,2-Dichlorobenzen e o-Creso l m & p-Cresol(s ) Hexachloroethan e Nitrobenzen e Hexachlorobutadien e 2,4,6-Tr i chloropheno l 2,4,5-Tr i chloropheno l 2,4-Dinitrotoluen e Hexachlorobenzen e 2,3,4,6-Tetrachloropheno l Pentachloropheno l

Nitrobenzene-d 5 2-Fluorobipheny l Terphenyl-dl 4 Phenol-d 5 2-Fluoropheno l 2,4,6-Tribromopheno l 105076 9
: 4 AU G 8 9 1 1 SE P 8 9

esul t

N D N D N D N D N D N D N D N O N O N O N D N D N D N D N O N O

10 8 85. 8 82. 1 79. 0 76. 0 77. 0 Unit s

mg/ L mg/ L mg/ L mg/ L nvj/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L

% % % X % % Recei v Analyz

- : 2 5 AU

G 8 9
: 04 OC T8 9 Reportin g L i mi t

0.02 0 0.02 0 0.02 0 0.02 0 0.02 0 0.02 0 0.02 0 0.02 0 0.02 0 0.02 0 0.1 0 0.02 0 0.02 0 0.02 0 0.1 0

- -

- -

- -

- -

- -

- -

N O- No t detecte d N A - No t applicabl e
Reporte dBy : Da nAlbritto nApprove dBy : Jef f Lowr yMetal s

Tota l Metal s
CIien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r

Aluminu m Antimon y Arseni c Bariu m Berylliu

m Cadmiu m Calciu m Chromiu m Cobal t Coppe r Lea d Mercury Nicke l Potassiu

m Seleniu m Silve r Sodiu m Thalliu m Ti n Vanadiu m Zin c American Petroleu m Institut e Sit e # 1 B S Pi t Skimming s 006299-0005-S AEnsec o ID : WAST E Sampled : 2 8 AU G8 9 Prepared :

Resul t Unit s

8 5 N D 1. 1 4 N D N D 213 0 3 N O 1 0 4 4 N D 9 N D N D N D 80 0 N D N D 2 2 2 mg/kg

mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g 105076 9 2 4 AU G8 9 Se e Below Reporting Limi t

1 0 5 0. 5 1 0. 2 0. 5 3 0 1 1 1 5 0. 1 4 50 0 0. 5 1 50 0 1 0 11 1 1 Received :

Analyzed :
Analytica l Metho d

601 0 601 0 706 0 601 0 601 0 601 0 601 0 601 0 601 0 601 0 601 0 747 1 601 0 601 0 774 0 601 0 601 0 784 1 601 0 601 0 601 0 2 5 AU G8 9 Se e Below

Prepare d Dat e

0 5 0 5

0 5 0 1 SE P 8 9 SE P 8 9 0 6 OC T 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 SE P 8 9 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 6 OC T 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 6 OCT 8 9 0 5 SEP 8 9 0 5 SE P 8 9 0 5 SE P 8 9 Analyze d

Dat e

1 8 SE P 8 9 1 8 SE P 8 9 1 0 OC T 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SEP'8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 1 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 0 OC T 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 0 OC T 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9

N D - Not detecte

d N A - No t applicabl e

Reporte dBy : Fre

dVelasque z Approve dBy : Tamm

y BaileyP.5 5

Clien t Name : Clien t ID : La bID : Matrix : Authorized : ICP/M S Metal s

Tota l Metal s
America nPetroleu mInstitut e Sit e # 1 B S Pi t Skimming s 006299-0005-S AEnsec o ID : WAST E Sampled : 2 8 AU G8 9 Prepared : 105076 9 2 4 AU G8 9 Se e Be'o w Received :

Analyzed :

Paramete r
Osmiu m(189 ) Resul t Unit s Reportin g Analytica l Limi t Metho d 2 5 AU G8 9 Se e Belo w
Prepare d Dat e Analyze d

Dat e



### N O mg/k g 

### 0. 1 RMA L 0 7 OC T 8 9 1 4 OC T 8 9

ND - No t detecte d N A -No t applicabl e
Reporte dBy : Scot t Heidema n Approve dBy : Ton i Tallaric oP.5 6

Metal s

TCL P Leachat e
Clien t Name : America n PetroleumInstitut e Clien t ID : Sit e # 1 B S Pi t Skimming s La bI D Matri x 006299-0005-S AEnsec o ID : 105076 9

WAST E Sampled : 2 4 AU G8 9 Received : 2 5 AUG8 9 Authorized : 2 8 AU G8 9 Prepared : Se e Belo wAnalyzed : Se e Belo w Reportin g Analytica l Prepare d Analyze d
Paramete r Resul t Unit s Limi t Metho d Dat e Dat e Arseni c ND mg/ L 0. 2 200. 7 1 4 SE P 8 9 2 0 SE P 8 9 Barium0.1 7 mg/ L 0.0 2 200. 7 1 4 SE P 8 9 2 0 SE P 8 9 CadmiumND mg/ L 0.0 1 200. 7 1 4 SE P 8 9 2 0 SE P 8 9 Chromiu mND mg/ L 0.0 2 200. 7 1 4 SE P 8 9 2 0 SE P 8 9 Lea d ND mg/ L 0. 1 200. 7 1 4 SE P 8 9 2 0 SE P 8 9 Silve r ND mg/ L 0.0 2 200. 7 1 4 SE P 8 9 2 0 SE P 8 9 Mercur yND mg/ L 0.00 2 747 1 1 4 SE P 8 9 1 7 SE P 8 9 SeleniumND mg/ L 0.0 5 270. 2 1 4 SE P 8 9 1 8 SE P 8 9

ND - No t detecte d N A» No t applicabl e
Reporte dBy : Sandr a Jone s Approve dBy : Tamm y Baile yP.5 7

Genera l Inorganic s

CIien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r America n Petroleum Institut e Sit e # 1 B S Pi t Skimming s 006299-0005-S AEnsec o ID : WAST E Sampled : 2 8 AU G8 9 Prepared :

Resul t Unit s Cyanide
, Reactiv e Ignitabilit y Non-Volatil e Oi l Volatil e Oi l 

### Oi l Wate r Solid s 

### P H Sulfide
, Reactiv e 

### N D >16 0 68. 2 

### 0. 1 68. 3 22. 5 " 

### 8. 7 7. 1 1. 2 mg/k g deg

. F fa fa fa fa fa unit s mg/k g 105076 9 2 4 AU G8 9 Se e Belo w Reportin g Limi t

0. 1

0. 1 0. 1 0. 1 0. 1 0. 1

0. 5 Received :

Analyzed : Analytica l Metho d 2 5 AU G8 9

Se e ",-»lo w
Prepare d D?* e Analyzed

Dat e

. EPA-0S W 1010/102 0 Chevro n Chevro n Chevro n Chevro n Chevro n 9045/AST M EPA/0S W 

### N

A N A N A N A N A N A N A N A N A 0 8 SE P 8 9

1 1 OC T 8 9 1 9 OC T 8 9 1 9 OC T 8 9 1 9 OC T 8 9 1 9 OC T 8 9 1 9 OC T 8 9 1 1 SE P 8 9 0 8 SE P 3 9

Not e o * Thi s tes t i s unreli'M e fo r an ysampl e othe r tha n a non-aqueou s liqui d

ND - No

. detecte d N A• No t applicabl e
Reporte dBy : Blak e Besse r Approve dBy : Tamm yBaile yP.5 8

Appendi xI

XVolatil e Or g

Metho d824 0

Clien t Name : America nPetroleu m Institut e Clien t ID : Sit e # 3 Crud e Oi l Botto m Str
. LabID : 006299-0004-S A Ensec o ID : 105076 8 Matrix : WAST E Sampled : 2 4 AU G Authorized : .2 8 AUG8 9 Prepared : 0 1 SE P

Paramete r Resul t

Aceton e ND Acetonitril e ND Acrolei nN O Acrylonitril e N D Ally l chlorid e ND Benzen e . 11 0 Bromodichloromethan e ND Bromoform

NO Bromomethan e N D Carbo ndisulfid e NO Carbo ntetrachlorid e ND Chl orobenzen e ND Chloropren e ND Chloroethan e N D Chl orodibromomethan e ND Chlorofor m

ND Chloromethan e ND DBC P (1,2-Dibromo

3-chloropropane ) N D ED B (1,2-Dibromoethane ) NO Dibromomethan e NO trans-1,4-Dichloro

2-buten e NO Dichlorodifluoromethan e N D 1,1-Dichloroethan e ND 1,2-Dichloroethan e ND trans-1,2-0ichloroethen e ND 1,1-Dichloroethen e N D Dichloromethan e N D 1,2-Dichloropropan e ND cis-1,3-Dichloropropen e ND trans-1,3-Dichloropropen e NO 1,4-Dioxan e ND Ethy l benzen e 51 0 Ethy l cyanid e ND 2-Hexanon e ND Iodomethan e ND Isobuty l alcoho l NO Methacrylonitril e NO Methy l ethy l keton e NO 4-Methyl-2-pentanon e ND
(continue do nfollowin g ND- No t detecte d N A - No t applicabl e anic s

8 9 Received : 2 5 AU G 8 9 An

<

Unit s
mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g
mg/k g mg/k g mg/k g
mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

page )

Reporte dBy : Dian e Pag e Approve dBy : Jef f

j ilyzed : 0 6 SE P
Reportin g Limi t


### 20 0 200 0 200 0 200 0 

### 100 100 100 100 20 0 100 100 100 100 20 0 100 100 20 0

10 0 10 0 100

100 20 0 100 100 10 0 100 10 0 100 100 100 200 0 

### 100 100 20 0 100 200 0 

### 100 20 0 20 0

Lowry 89

89

•

.P.5 9

CIien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r Appendi xI X Volatil e Organic s (CONT

. Metho d 824 0

America n Petroleu mInstitut e Sit e # 3 Crud e Oi l Botto m Str

. 006299-0004-S AEnsec o ID : WAST E Sampled : 2. 8 AU G8 9 Prepared :

Styren e 1,1,1,2-Tetrachloroethan e 1,1,2 ,2-Tetrachloroethan e Tetrachloroethen e Toluen e 1,1,1-Tr i chloroethan e 1,1,2-Trichloroethan e

" -ichloroethen e ichlorofluoromethan e .,2,3-Trichloropropan e Viny l acetat e Viny l chlorid e Tota l xylene s

Toluen e 4-Bromo f (BF B 1,2-Dic h 

### d 8 uorobenzen e

oroethane-d 4 105076 8 2 4 AU G 0 1 SE. >

esul t



### N D N D N D N D 

### 52 0 N D N D N D N D N D N O N D 

### 71 0

10 5

94. 6 98. 1 

### 8 9 8 9

Unit s
mg/kg mg/kg mg/k g mg/k g mg/k g mg/k g mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

%

fa fa Received : 2 5 AU G8 9 Analyzed : 0 6 SE P 8 9
Reporting Limi t


### 10 0 10 0 10 0 10 0 10 0 10 0 10 0 10 0 10 0 10 0 20 0 20 0 10 0

- -

- -

- -

ND• No t detecte d N A - No t applicabl e

Reporte dBy: Oian e Pag e Approve dBy: Jef f LowryP.6 0

Name : ID : CIien t Clien t LabID : Matrix : Authorized : OT C Volatil e Organic s TCL P Leachat e Metho d824 0

America nPetroleu

m Institut e Sit e # 3 Crud e Oi l Botto m Str
. 006299-0004-S A

Ensec o ID : 105076 8 WAST E Sampled : 2 4 AU G8 9 2 8 AU G8 9 Prepared : 1 3 SE P 8 9

Paramete r
Viny l chlorid e Acrylonitril e Methylen e chlorid e Carbo ndisulfid e 1,1-Dichloroethen e Isobuty l alcoho l Chlorofor m 1,2-Dichloroethan e 2-Butanon e 1,1,1-Tr i chloroethan e Carbo ntetrachlorid e Trichloroethen e 1,1,2-Trichloroethan e Benzen e 1,1,1,2-Tetrachloroethan e 1,1,2,2-Tetrachloroethan e Tetrachloroethen e Toluen e Chlorobenzen e

Toluene-d 8 4-Bromof1uorobenzen e (BFB ) 1,2-Dichloroethane-d 4 Resul t

N O NO NO ND ND N D N D ND ND N D NO NO NO 2. 2 NO NO N D 3. 7 N D

10 4

10 3 98. 8 Unit s

mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L

fa fa Received : 2 5 AU G8 9 Analyzed : 15.SE P 8 9
Reportin g Limi t

0.2 5 2. 5 0.1 2 0.1 2 0.1 2 2. 5 0.1 2 0.1 2 0.2 5 0.1 2 0.1 2 0.1 2 0.1 2 0.1 2 0.1 2 0.1 2 0.1 2 0.1 2 0.1 2

ND- No t detecte d N A * No t applicabl e

Reporte dBy : Lis a Trau t Approve dBy : Jef f Lowr yP.6 1

Refiner y Hazardou s Constituen t Semivolatile s

Metho d827 0

Clien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r America nPetroleu m Institut e Sit e # 3 Crud e Oi l Botto m Str
. 006299-0004-S A

Ensec o ID : 105076 8 WAST E Sampled : 2 4 AU G8 9 2 8 AU G8 9 Prepared : 0 5 SE P 8 9

Anthracen e Benzo(a)anthracen e Benzolb)fluoranthen e Benzo(k)f1uoranthen e Benzo(a)pyren e bis(2-Ethylhexyl ) phthalat e Buty l benzy l phthalat e Chrysen e D i benz(a,h)anthracen e Di-n-buty l phthalat e 1,2-Dichlorobenzen e 1,3-Dichlorobenzen e 1,4-Dichlorobenzen e Diethy l r ..:halat e 7,12-Dimethylbenz

anthracen e Dimethy l phthalat e Di-n-octy l phthalat e Fluoranthen e Inden e 1-Methylnaphthalen e Naphthalen e Phenanthren e Pyren e Pyridin e Quinolin e Benzenethio l o-Creso l
m & p-Cresol(s ) 2,4-Dimethylpheno l 2,4-Dinitropneno l 4-Nitropheno l Pheno l

Nitrobenzene-d 5 2-Fluorobipheny l Terphenyl-dl 4 Phenol-d 5 2-Fluoropheno l 2,4,6-Tr i bromopheno l

ND- No t detecte d N A - No t applicabl e

Reporte dBy : Belind a Guerr a Resul t Received : 2 5 AU G Analyzed : 0 2 OC T
Reportin g Unit s Limi t 8 9 8 9



### N D N D N D N D N D
N O N O N O N O N D N D N D N D N D
N D N D N D N D N D 5 9 47 1 4 N D N D N O N D N D N D N D N O N O N D

61. 2 65. 6 78. 8 39. 2 34. 2 43. 2 mg/kg mg/k g mg/k g mg/k g mg/k g mg/k g mg/k r mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

% % % fa % % •

1 3 

### 1 3 1 3 1 3 1 3
1 3 1 3 1 3 1 3 1 3 1 3 1 3 1 3 1 3
1 3 1 3 1 3 1 3 1 3 '. 3 i 3 1 3 1 3

- - 

### 1 3

- - 

### 1 3 1 3 1 3 65 6 5 1 3

- -

- -

- -

- -

- -

Approve dBy : Jef f Lowr yi62

_

Clien t Name : Hien t ID : a b ID : .latrix : Authorized :

Paramete r OT C Semivolatil e Organic s TCL P Leachat e Metho d827 0

America nPetroleu

m Institut e Sit e # 3 Crud e Oi l Botto m Str
. 006299-0004-S A

Ensec o ID : 105076 8 WAST E Sampled : 2 4 AU G8 9 2 8 AUG8 9 Prepared : 2 1 SE P 8 9 Received : 2 5 AU G8 9 Analyzed : 0 4 OC T 8 9

3 yridin e Pheno l bis(2-Chloroethyl)ethe r 1,4-D i chlorobenzen e 1,2-Dichlorobenzen e o-Creso l
m & p-Cresol(s ) Hexachloroethan e Nitrobenzen e Hexachlorobutad i en e 2,4,6-Tr i chloropheno l 2,4,5-Tr i chloropheno l 2,4-Dinitrotoluen e Hexachlorobenzen e 2,3,4,6-Tetrachloropheno l Pentachloropheno l
Nitrobenzene-d 5 2-Fluoroblpheny l Terphenyl-dl 4 Phenol-d 5 2-Fluoropheno l 2,4,6-Tr i bromopheno l sui t



### N D N D N D N D N D N D N D N D N D N D N D N D N D N D N D N D

95. 6 67. 8 68. 4 6.8 8 3.8 2 7.1 3 Unit s mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L

% % % % % % Reporting

Limi t

- - 0.04 0 0.04 0 0.04 0 0.04 0 0.04 0 0.04 0 0.04 0 0.04 0 0.04 0 0.04 0 0.2 0 0.04 0 0.04 0 0.04 0 0.2 0

- -

- -

- -

- -

- -

- -



# i

1 N O- No t detecte d N A - No t applicabl e
Reporte dBy : Da nAlbritto n Approve dBy : Jef f Lowry



# r .P.6 3

Clien t Clien t La bI D Matri x Author i Name :

ID :

zed : Metal s

Tota l Metal s

America n Petroleu

mInstitut e Sit e # 3 Crud e Oi l Botto mStr

. 006299-0004-S AEnsec o ID : 105076 8 WAST E Sample e 2 4 AUG8 9 2 8 AUG8 9 Prepared

. Se e Below Received : Analyzed :

Paramete r

Aluminu m Antimon y Arseni c Bariu m Berylliu

m Cadmiu m Calciu m Chromiu m Cobal t Coppe r Lead Mercury Nicke l Potassiu

m Seleniu m Silve r Sodiu m Thalliu m Ti n Vanadiu m Zin c Resul t Unit s Reporting Limi t


### 32 9 N D 

### 6. 2 5 8 N D N D 11400 0 

### 4 8 

### 5 54 

### 32 0 N D 

### 10 0 N O N D N D 1200 0 

### N O N D N O 5 4 mg/k g

mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g 

### 5 0 3 0 

### 0 5 1 3 10 0 

### 5 5 5 3 0 

### 0 2 0 300 0 

### 5 5 300 0 

### 5 0 3 0 

### 5 5 Analytica l

•etho d

6
, 60 u 706 0 601 0 601 0 601 0 601 0 601 0 601 0 601 0 601 0 747 1 601 0 601 0 774 0 601 0 601 0 784 1 601 0 601 0 601 0 2 5

Se t 3 8 9 ?lo w

Prepare d Dat e

0 5 SE P 8 9 0 5 SE P 8 9 0 6 OC T 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 1 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 6 OC T 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 6 OC T 8 9 0 5 SE P 8 9 0 5 SE P 8 9 0 5 SE P 8 9 Analyze d

Dat e

1 8 SE P 8 9 1 8 SE P 8 9 1 0 OC T 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 1 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 0 OC T 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 0 OC T 8 9 1 8 SE P 8 9 1 8 SE P 8 9 1 8 SE P 8 9

N D « No t detecte d N A» No t applicabl e

Reporte d By : Fre d Velasque z Approve dBy : Tamm

yBaile yP.6 4

CIien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r
Osmiu m (189 ) ICP/M S Metal s

Tota l Metal s
America n Petroleu mInstitut e Sit e # 3 Crud e Oi l Botto mStr

. 006299-0004-S AEnsec o ID : 105076 8 WAST E Sampled : 2 4 AU G8 9 2 8 AU G8 9 Prepared : Se e Belo w Received : Analyzed :

Resul t Unit s Reportin g Analytica l

Limi t Metho d 2 5 AU G8 9 Se e Belo w
Prepare d Dat e Analyze d

Dat e



### N D mg/k g 

### 0. 1 RMA L 0 7 OC T 8 9 1 4 OC T 8 9

N D• » No t detecte d N A - No t applicabl e
Reporte dBy : Scot t Heidema n Approve dBy : Ton i Tallaric oP.6 5

Metal s

TCL P Leachat e

Clien t Name : Clien t ID : La bI D Matri x Authorize d

Paramete r

Arseni c Bariu m Cadmi ur n Chromiu m '.ea d :ilve r Mercury Seleniu m America n Petroleu mInstitut e Sit e # 3 Crud e Oi l BottomStr

. 006299-0004-S AEnsec o ID : ST E Sampled : AU G8 9 Prepared :

Resul t Unit s 105076 8

2 4 AU G8 9 Se e Below Received :

Analyzed :
Reporting Analytica l Limi t Metho d

N D 0.3 3 N O N D N D N D N O N D mg/L mg/L mg/L mg/ L mg/L mg/L mg/ L mg/ L 0. 5 0.0 5 0.0 3 0.0 5 0. 3 0.0 5 0.00 2 0.0 5 200. 7 200. 7 200. 7 200. 7 200. 7 200. 7 747 1 270. 2 2 5 AU G8 9 Se e Below

Prepare d Dat e

SE P 8 9 SE P 8 9 SE P 8 9 SE P 8 9 SE P 8 9 SE P 8 9 SE P 8 9 SE P 8 9 Analyze d

Dat e

2 0 SE P 8 9 2 0 SE P 8 9 2 0 SE P 89

- 2 0 SE P 8 9 2 0 SE P 8 9 2 0 SE P 8 9 1 7 SE P 8 9 1 8 SE P 8 9

N D • » No t detecte d N A• No t applicabl e

Reporte dBy : Sandra Jone s Approve dBy : Tamm

y Baile yP.6 6

Append

Clien t Name : America nPetroleu m Clien t ID : Ramsey-Crud e Tan k LabID : 011425-0001-S A Matrix : WAST E Authorized : 2 1 SEr 9 0

Paramete r

Aceton e Acetonitril e Acrolei n Acrylonitril e Ally l chlorid e Benzen e 3romodichloromethan e jromofor m romomethan e -arbondisulfid e Carbo ntetrachlorid e Chlorobenzen e Chloropren e Chloroethan e Dibromochloromethan e Chloroform Chloromethan e DBC P (1,2-Dibromo

3-cnloropropane ) EDB (1,2-Dibromoethane ) Dibromomethan e trans-1,4-Dichloro

2-buten e Di chl orod i f1uoromethan e 1,1-Dichloroethan e 1,2-Dichloroethan e trans-1,2-Dichloroethen e 1,1-Dichloroethen e Dichloromethan e 1,2-Dichloropropan e cis-1,3-Dichloropropen e trans-1,3-Dichloropropen e 1,4-Dioxan e Ethy l benzen e Ethy l cyanid e 2-Hexanon e Iodomethan e Isobuty l alcoho l Methacrylonitril e 2-Butanon e (MEK ) 4-Methyl-2-pentanon e
(cont i ND- No t detecte d N A « No t applicabl e
Reporte dBy : Michae l Blade s ixI XVolatil e Org

Metho d824 0

Institut e Bottom s
Sampled : 2 0 SE P Prepared : 2 5 SE P

Resul t


### N O N D N D N O N D 360 N D N D N D N D N D N D N D N D N D N D N D

N D N D N D

N D N D N O N O N D N D N D N O N O N D N D 49 0 N D N D N O N O N D N D N D

nue do nfollowin g anic s i

9 0 Received : 2 1 SE P 9 0 9 0 A

n

Unit s mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g
mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

page )

Approve dBy : Jef f alyzed : 2 7 SE P 9 0

Reportin g Limi t


### 500 500 0 500 0 500 0 

### 25 0 25 0 25 0 25 0 500 25 0 25 0 25 0 25 0 500 25 0 25 0 500
25 0 25 0 25 0
25 0 50 0 ! 

### 25 0 25 0 25 0 25 0 250 25 0 25 0 25 0 500 0 

### 25 0 25 0 500 25 0 500 0 

### 25 0 500 500

i

Lowr y

i 

### 1P.6 7
Rock yMountain Analytica l Laborator

y



### ANALYTICAL RESULT S

FOR

AMERICA N PETROLEU

M INSTITUT E

ENSECO-RMAL NO
. 01142 5

NOVEMBE R1 , 199 0 

# Enseco

Reviewe d by : °Susa nCjWyat

Su eDa l l a

Lnsct u Incorporate d -W*5 Yarrow Stree t Arvaua. Colorad o S000 2 .305/421-661 1 Fax : 505/451-717 1P.6 8

Genera l Inorganic s

CIien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r

Chlorid e America nPetroleu m Institut e Crud e 00786 2 WAST E 1 5 DE C

Cyanide , Reactiv e Ignitabilit y Non-Volatil e Volatil e Oi l 

### Oi l Wate r Solid s 

### p H Oi

l

Sulfide , Reactiv e TankBottom s -0001-S A

Ensec o ID : Sampled : 8 9 Prepared : 106291 1 1 4 DE C ! Se e Be l
Reportin g Resul t Unit s

35 0 mg/k g NDmg/k g >16 0 deg
. F .34. 1 f. ND% 34-
. 1 fa 29. 2 % 37. 7 f. 8. 3 unit s NDmg/k g Limi t



### 1 5 0. 1

- - 

### 0. 1 0. 1 0. 1 0. 1 0. 1

- - 

### 0. 5 3 9 Re c 3 w An a
Analytica l Metho d

300. 0 Mod
. EPA/OS W 1010/102 0 Chevro n Chevro n Chevro n Chevro n Chevro n 9045/AST M EPA/OS W eive d

lyze d : 1 5 DE C 8 9

: Se e Below

Prepare d Dat e

1 8 DE C 8 9 

### N A N A N A N A N A N A N A N A N A Analyze d

Dat e

2 0 DE C 8 9 2 1 DE C 8 9 0 9 JA N 9 0 0 5 JA N 9 0 0 5 JA N 9 0 0 5 JA N 9 0 0 5 JA N 9 0 0 5 JA N 9 0 2 8 DE C 8 9 1 9 DE C 8 9

Not e o : Thi s tes t i s unreliabl e fo r an y sampl e othe r tha na non-aqueou s liquid

.

ND= No t detecte d N A = No t applicabl e

Reporte dBy : Pa

m Rosa s Approve dBy : Kimberl y Conro yP.6 9

_ l ICP/M S Metal s

Tota l Metals *

Clien t Name : America n PetroleumInstitut e Clien t ID : Crud e Tan k Bottom s La bID : 007862-0001-S AEnsec o ID : 106291 1 Matrix : WAST E Sampled : 1 4 DE C 8 9 Authorized : 1 5 DE C 8 9 Prepared : Se e Belo w Received : 1 5 DE C 8 9 Analyzed : Se e Belo w

Paramete r
Osmium(189 ) Resul t

ND Unit s

mg/k g Reportin g Analytica l

Limi t Metho d


### 0. 4 RMA L Prepare d Analyze d Dat e Dat e

2 9 DE C 8 9 0 3 JA

N9 0

_ j

ND = No t detecte d N A- No t applicabl e
Reporte d By : Scot t Heidema n Approve dBy : Ton i Tallaric oP.7 0

Clien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r
Arseni c Barium Cadmium Chromium Lea d Silve r Mercury

. Selenium Metal s

TCL P Leachat e
America n Petroleum

Institut e Crud e Tan k Bottom s 007862-0001-S AEnsec o ID : 106291 1 WAST E Sampled : 1 4 DE C 8 9 1 5 DE C 8 9 Prepared : Se e Belo w Received : Analyzed :

Resul t

N D ND ND N D N D ND N O ND Unit s

mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L Reportin g Analytica l

Limi t Metho d ; 1 5 DE C 8 9
: Se e Belo w
Prepare d Dat e Analyze d

Dat e

5 3 0 3 0 5 3 0 5 0.00 2 0.0 5 601 0

601 0 601 0 601 0 601 0 601 0 747 0 774 0 2 8 DE C 8 9 0 3 JA N 9 0 2 8 DE C 8 9 0 3 JA

N 9 0 2 8 DE C 8 9 0 3 JA

N 9 0 2 8 DE C 8 9 0 3 JA

N 9 0 2 8 DE C 8 9 0 3 JA

N 9 0 2 8 DE C 8 9 0 3 JA

N 9 0 2 9 DE C 8 9 0 3 JA

N 9 0 2 8 DE C 8 9 0 2 JA

N 9 0

ND - No t detecte d N A• No t applicabl e
Reporte d By : Fre d Velasque z Approve dBy : Kimberl y ConroyP.7 1 

# 1

J

J Name :

ID : Clien t Clien t LabID Matri x Authorize d Metal s

Tota l Metal s

America nPetroleu

m Institut e Crud e Tan kBottom s 007862-0001-S A

Ensec o ID : 106291 1 WAST E Sampled : 1 4 DE C 8 9 1 5 DE C 8 9 Prepared : Se e Belo w Received :

Analyzed :

Paramete r

Aluminu m Antimony Arseni c Bariu m Berylliu

m Cadmiu m Calciu m Chromiu m Cobal t Coppe r Lead Mercur y Nicke l Potassiu

m Seleniu m Silve r Sodiu m Thalliu m Ti n Vanadiu m Zin c Resul t

120 0 ND 2. 7 2 6 N D N D 280 0 5 1 4 ND N D 2 5 N D N D ND 76 0 N O NO 6 1 0 Unit s

mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g Reportin g Analytica l

Limi t Metho d



### 1 0 5 0. 5 1 0. 2 0. 5 2 0 1 1 1 5 0. 1 4 50 0 1 1 50 0 0. 5 5 1 2 601 0

601 0 706 0 601 0 601 0 601 0 601 0 601 0 601 0 601 0 601 0 747 1 601 0 601 0 774 0 601 0 601 0 784 1 601 0 601 0 601 0 1 5 DE C 8 9

Se e Below

Prepare d Dat e Analyze d

Dat e

0 3 JA N 0 3 JA N 0 2 JA N 0 3 JA N 0 3 JA N 0 3 JA N 0 3 JA N 0 3 JA N 0 3 JA N 0 3 JA N 0 3 JA N 0 3 JA N 0 3 JA N 0 3 JA N 0 2 JA N 0 3 JA N 0 3 JA N 0 2 JA N 0 3 JA N 0 3 JA N 0 3 JA N 9 0 0 8 9 0 0 8 9 0 0 4 9 0 0 8 9 0 0 8 9 0 0 8 9 0 0 8 9 0 0 8 9 0 0 8 9 0 0 8 9 0 0 8 9 0 0 4 9 0 0 8 9 0 0 8 9 0 0 4 9 0 0 8 9 0 0 8 9 0 0 4 9 0 0 8 9 0 0 8 9 0 0 8 JA N 9 0 JA N 9 0 JA N 9 0 JA N 9 0 JA N 9 0 JA N 9 0 JA N 9 0 JA N 9 0 JA N 9 0 JA N 9 0 JA N 9 0 JA N 9 0 JA N 9 0 JA N 9 0 JA N 9 0 JA N 9 0 JA N 9 0 JA N 9 0 JA N 9 0 JA N 9 0 JA N 9 0

ND- No t detecte d N A » No t applicabl e

Reporte dBy : Harol dBorque z Approve dBy : Kimberl y Conro yP.7 2

OT C Semivolatil e Organic s TCL P Leachat e Metho d827 0

Clien t Name : America nPetroleu m Institut e Clien t ID : Crud e TankBottom s LabID : 007862-0001-S A Ensec o ID : 106291 1 Matrix : WAST E Sampled : 1 4 DE C 8 9 Authorized : 1 5 DE C 8 9 Prepared : 0 2 JA N 9 0

Paramete r Resul t Pyridin e N D Pheno l N D bis(2-Chloroethyl ) ethe r N D 1,4-Dichlorobenzen e N D 1,2-Dich l orobenzen e ND o-Creso l ND
m . _p-Cresol(s ) N D Hexachloroethan e N D Nitrobenzen e N D Hexachlorobutadien e N D 2,4,6-Trichloropheno l ND 2,4,5-Trichloropheno l ND 2,4-Dinitrotoluen e N D Hexach l orobenzen e ND 2,3,4,6-Tetrachloropheno l ND Pentachloropheno l N D
Nitrobenzene-d 5 72. 9 2-Fluorobipheny l 68. 7 Terphenyl-dl 4 75. 9 Phenol-d 5 72. 5 2-Fluoropheno l 64. 5 2,4,6-Tribromopheno l 80. 0

ND- No t detecte d N A - No t applicabl e Unit s mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L

% % % % % fa Received : 1 5 DE C 8 9 Analyzed : 1 2 JA

N 9 0
Reportin g Limi t

0.02 0 0.02 0 0.02 0 0.02 0 0.02 0 0.02 0 0.02 0 0.02 0 0.02 0 0.02 0 0.1 0 0.02 0 0.02 0 0.02 0 0.1 0

- -

- -

- T

- -

'

Reporte dBy : Belind a Guerr a Approve dBy : Jef f Lowr y 1P.7 3 

### I

Refiner y Hazardou s Constituen t

Metho d827 0

Clien t Name : America nPetroleu m Inst i Clien t ID : Crud e Tan kBottom s LabID : 007862-0001-S A Ensec c tut e

) ID : 106291 1 Matrix : WAST E Sampled : 1 4 DE C Authorized : 1 5 DE C 8 9 Prepared : 2 1 DE C

Paramete r

Anthracen e Benzo(alanthracen e Benzo(b)fluoranthen e Benzo- ( k ) f 1 uoranthen e Benzo(a)pyren e bis(2-Ethylhexyl ) phthalat e Buty l benzy l phthalat e Chrysen e Dibenz(a,h)anthracen e Di-n-buty l phthalat e 1,2-Dichiorobenzen e 1,3-Dichlorobenzen e 1,4-Dichlorobenzen e Diethy l phthalat e 7,12-Dimethylbenz

anthracen e Dimethy l phthalat e Di-n-octy l phthalat e Fluoranthen e Inden e 1-Methylnaphtha l en e Naphthalen e Phenanthren e Pyren e Pyridin e Quinolin e Benzenethio l o-Creso l

m & p-Cresol(s ) 2,4-Dimethylpheno l 2,4-Dinitropneno l 4-Nitropheno l Pheno l

Nitrobenzene-d 5 2-Fluorobipheny l Terphenyl-dl4
. Phenol-d 5 2-Fluoropheno l 2,4,6-Tribromopheno l

ND» No t detecte d ! N A = No t applicabl e

Reporte dBy : Michae l Blade s 

# 1 

# 1 Resul t



### N D N D N D N D N D

N D N D N D N D N D N D N D N D N D

N D N D N D N D N D N D N D 2 1 N D N O N O N D N D N D N D N D N D N D

76. 0 95. 6 94. 4 46. 2 53. 2 93. 2 Semi volati l



### 89 89 e

s

Received : 1 5 DE C 8 9 

### A n

Unit s
mg/k g mg/k g mg/k g mg/k g mg/k g
mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g
mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

% % % % fa f. alyzed : 1 2 JA N 9 0
Reportin g Limi t


### 20 20 20 20 20

20 20 20

t 2 0 

### 20 20 20 20 20

20 2 0 20 20 20 20 20 2 0 20

- - 

### 20

. _ 

### 20 2 0 20 100 100 2 0

- -

- -

- -

- -

Approve dBy : Jef f Lowr y 

## 1P.7 4



### OT C

Clien t Name : America nPetroleu m Clien t ID : Crud e TankBottom s LabID : 007862-0001-S A E Matrix : WAST E Authorized : 1 5 DE C 8 9

Paramete r Viny l chlorid e Acrylonitril e Methylen e chlorid e Carbo ndisulfid e 1,1-Dichloroethen e Isobuty l alcoho l Chloroform 1,2-Dichloroethan e 2-Butanon e 1,1,1-Trichloroethan e Carbo ntetrachlorid e Trichloroethen e <*

- 1,1,2-Trichloroethan e Benzen e 1,1,1,2-Tetrachloroethan e 1,1,2,2-Tetrachloroethan e Tetrachloroethen e Toluen e Chlorobenzen e

Toluene-d 8 4-Bromof1uorobenzen e 1,2-Dichloroethane-d 4

ND= No t detecte d N A - No t applicabl e
Reporte dBy : Keit hBeauvai s

1 • - >



## 1 j Volatil e TCL P Organic s Leachat e Metho d

Insti l

inseco tut e



### ID : Sampled : Prepared : 824 0

106291 1 1 4 DE C 8 9

. 2 7 DE C 8 9

Resul t


### N D N D N D N D N D N D N D N D N D N D N D N D N D 0.09 2 

### N O N O N D N D N O
10 3 10 5 10 3 Unit s mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L f.
% fa i

Received : 1 5 DE C 8 9 Analyzed : 0 3 JA

N 9 0 Reportin g Limi t
0.05 0 0.5 0 0.02 5 0.02 5 0.02 5 0.5 0 0.02 5 0.02 5 0.05 0 0.02 5 0.02 5 0.02 5 0.02 5 0.02 5 0.02 5 0.02 5 0.02 5 0.02 5 0.02 5

- -

Approve dBy : Jef f LowryClien t Name :

Clien t ID : La bID : Matrix : Authorized :

Paramete r Appendi xI XVolatil e Organic s (CONT. )

Metho d824 0

America nPetroleu

m Institut e Crud e Tan kBottom s 007862

- WAST E 1 5 DE C 0001-S A

8 9

Styren e 1,1,1,2-Tetrachloroethan e 1,1,2,2-Tetrachloroethan e Tetrachloroethen e Toluen e 1,1,1-^Tri ch l oroethan e 1,1,2-Trichloroethan e Trich l oroethen e Trichlorofluoromethan e 1,2,3-Trichloropropan e Viny l acetat e Viny l chlorid e Xylene s (total )

Toluene-d 8 4-Bromofluorobenzen e 1,2-D i chloroethane-d 4 Ensec o ID : Sampled : Prepared : 106291 1

1 4 DE C 2 0 DE C

Resul t


### N D N D N D N D N O N D N D N D N D N D N D N D 1 1 8 9 8 9

Unit s
mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g Received : Analyzed : 1 5

0 4 DE C JA N 8 9 9 0
Reportin g Limi t

1. 0 1. 0 1. 0 1. 0 1. 0 1. 0 1. 0 1. 0 1. 0 1. 0 2. 0 2. 0 1. 0

10 6 10 7 10 3 %

fa fa

ND- No t detecte d i N A » No t applicabl e

Reporte dBy : Michae l Blade s Approve dBy : Jef f LowryP.7 6

Appendi xI

XVolatil e Organic s

Metho d824 0

CIien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r America nPetroleu m Institut e Crud e Tan kBottom s 007862-0001-S A

Ensec o ID : WAST E Snpled : 1 5 DE C 8 9 P r .ared :

Aceton e Acetonitril e Acrolei n Acrylonitril e Ally l chlorid e Benzen e Bromodichloromethan e Bromoform Bromomethan e Carbo ndisulfid e Carbo ntetrachlorid e Chlorobenzen e Chloropren e Chloroethan e Chlorodibromomethan e Chloroform Chloromethan e DBC P (1,2-Dibromo

3-chloropropane ) ED B (1,2-0ibromoethane ) Dibromomethan e trans-1,4-Dichloro

2-buten e Di chlorod i fluoromethan e 1,1-Dichloroethan e 1,2-Dichloroethan e trans-1,2-Dichloroethen e 1,1-Dichloroethen e Dichloromethan e 1, 2 -D i chloropropan e cis-1,3-Dichloropropen e tran s -1,3-D i chloropropen e 1,4-Dioxan e Ethy l benzen e Ethy l cyanid e 2-Hexanon e Iodomethan e Isobuty l alcohol--

- Methacrylonitril e Methy l ethy l keton e 4-Methyl-2-pentanon e 106291 1 1 4 DE C 8 9 2 0 DE C 8 9

esul t



### N D N D N D N D N O 6. 3 N D N D N D N D N D N D N D N D N D N O N D

N D N D N D

N D N D N O N D N D N O N D N D N O N D N D 1 3 N D N O N D N D N D N D N D Received : 1 5 DE C 8 9



### An <

Unit s
mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g
mg/k g mc/k g mg/k g
mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g ilyzed : 0 4 JA N 9 0
Reportin g Limi t


### 2. 0 20 20 2 0 1. 0 1. 0 1. 0 1. 0 2. 0 1.0
. 

### 1. 0 1. 0 1. 0 2. 0 1. 0 1. 0 2. 0
1. 0 1. 0 1. 0
1. 0 2. 0 1. 0 1.0

- 

### 1. 0 1. 0 •1. 0 

### 1. 0 1. 0 1. 0 2 0 1. 0 1. 0 2. 0 1. 0 20 1. 0 2. 0 2. 0

ND= No t detecte d N A » No t applicabl e (continue donfollowin gpage )

Reported.By : Mfchae l Blade s Approve dBy : Jef f Lowr yP.7 7
Rock y Mountai nEnsec o Incoroorate

Analytica l Laborator

y

ANALYTICAL RESULT S

FO R

AMERICA N PETROLEU

M INSTITUT E

ENSECO-RMAL NO
. 00786 2

JANUARY27 , 199 0 

# Enseco

Susa nC

. Wyat

t'


# V JSPtJiit

i&Lb<X?htJJeann e t\. Howber t

495 5 Yarro w Stre p Arvada

. Colorad o 8000 2 303/421-661 1

Facsimile : 303/431-717 1P.7 8Genera l Inorganic s P.7 9

Clien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r
Chlorid e America nPetrol <

TANKBOTTOM S # 2 00753 1 WAST E 1 7 NOV

Cyanide , Reactiv e Ignitabilit y Non-Volatil e Volatil e Oi l 

### Oi l Wate r Solid s 

### p H Oi

l

Sulfide , Reactiv e -0004-S A



### 8 9

Resul t

1090 0 

### N D 66 27. 2 

### 8. 8 36.0

- 20. 3 40. 1 

### 7. 2 0. 7 »u m Institut e

Ensec o Sam p Prepa i

Unit s
mg/k g mg/k g deg
. F

• % % % % % unit s mg/k g 

### ID : ed : -ed : 106035 1 1 5 NOV Se e Be l
Reportin g Limi t


### 1 5 0. 1

- - 

### 0. 1 0. 1 0. 1 0. 1 0. 1

- - 

### 0. 5 3 9 Receive d
o w Analyze d
Analytica l Metho d

300. 0 Mod
. EPA/OS W 1010/102 0 Chevro n Chevro n Chevro n Chevro n Chevro n 9045/AST M EPA/OS W : 1 7 NO V 8 9

: Se e Belo w

Prepare d Dat e

0 6 DE C 8 9 

### N A N A N A N A N A N A N A N A N A Analyze d

Dat e

1 1 DE C 8 9 3 0 NOV 89
. 1 9 DE C 8 9 o z 0 8 DE C 8 9 0 8 DE C 8 9 0 8 DE C 8 9 0 8 DE C 8 9 0 8 DE C 8 9 2 1 NOV 8 9 3 0 NOV 8 9

Not e o : This

. test , i s unreliabl e fo r an y sampl e othe r tha na non-aqueou s liquid

.

Not e z : Sampl e exhibit s a characteristi c o f hazardou s waste .

ND= No t detecte d N A = No t applicabl e

Reporte dBy : Pa

m Rosa s Approve dBy : Ton i Lus kP.8 0

CIien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r

Arseni c Bariu m Cadmiu m Chr -iu m Le e • Sil\

. ir Mercury Seleniu m Metal s

TCL P Oi l Filtrat e

American Petroleu

mInstitut e TAN K BOTTOM S # 2 007531-0004-S AEnsec o ID : 106035 1 WAST E San * ed : 1 5 NO

V 8 9 1 7 NO V 8 9 Prepa.ed : Se e Below Received : 1 7 NO V 8 9 Analyzed : Se e Below

Resul t

N D N D N D 0. 8 N D N D N O N D Unit s

mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L Reporting

Limi t

5 0

. 0

. 0

. 3 0

. 0

. 0
, Analytica l

Metho d

200. 7 200. 7 200. 7 200. 7 200. 7 200. 7 747 1 270. 2 Prepare d Analyze d

Dat e Dat e

2 9 NO V 8 9 1 3 DE C 8 9 2 9 NO V 8 9 1 3 DE C 8 9 2 9 NO V 8 9 1 3 DE C 8 9 2 9 NO V 8 9 1 3 DE C 8 9 2 9 NO V 8 9 1 3 DE C 8 9 Z 9 NO V 8 9 1 3 DE C 8 9 0 6 DE C 8 9 0 8 DE C 8 9 2 9 NO V 8 9 1 2 DE C 8 9

N D = No t detecte d N A- No t applicabl e

Reporte d By : Fre

dVelasque z Approve dBy : Tamm

y Baile yP.8 1

Metal s
Aqueou s Leachat e
Clien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r
Arseni c Bariu m Cadmiu m Chromiu m Lea d Silve r Mercur y Seleniu m America nPetroleu m Institut e TANKBOTTOM S # 2 007531-0004-S A

Ensec o ID WAST E 1 7 NO V 8 9 106035 1

Sampled : 1 5 NO

V 8 9 Prepared : Se e Below Received : 1 7 NO V 8 9 Analyzed : Se e Below

sui t
1. 1 4. 1 0.05 4 0.0 7 9. 2 N D N D N O Unit s

mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L Reportin g

Limi t
0. 1 0. 3 0.00 5 0.0 1 0.0 5 0.0 1 0.00 2 0.0 5 Analytica l

Method

200. 7 200. 7 200. 7 200. 7 200. 7 200. 7 747 1 270. 2 Prepare d

Dat e

2 9 NO V 8 9 2 9 NO V 8 9 2 9 NO V 8 9 2 9 NO V 8 9 2 9 NO V 8 9 2 9 NO V 8 9 0 6 DE C 8 9 2 9 NO V 8 9 Analyze d Dat e

1 3 DE C 8 9 1 3 DE C 8 9 1 3 DE C 8 9 1 3 DE C 8 9 1 3 DE C 8 9 1 3 DE C 8 9 0 8 DE C 8 9 1 2 DE C 8 9

ND» No t detecte d N A - No t applicabl e
Reporte dBy : Fre dVelasque z Approve dBy : Tamm y Baile yP.8 2

Metal s

CIien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r
Arseni c Bariu m Cadmiu m Chromiu m Lea d Silve r Mercur y Seleniu m TCL P

America nPetroleu

m Inst i TANKBOTTOM S # 2 00753 1 WAST E 1 7 NO V -0004-S A


### 8 9

Resul t


### 1. 1 4. 1 0.05 5 0.0 7 

### 9. 2 N D N O N D Ensec o

Sam o Leachat e

tut e



### ID : led : Prepared :

Unit s mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L 106035 1

1 5 NO V 

### Se e Be l
Reportin g Limi t 

### 0. 2 ,0. 4 0.00 7 0.0 2 0.0 7 0.0 2 0.00 3 0.0 6 3 9 Re c D W An a Analytica l Metho d

200. 7 200. 7 200. 7 200. 7 200. 7 200. 7 747 1 270. 2 eive d

lyze d : 1 7 NO V

8 9
: Se e Belo w
Prepare dAnalyze d Dat e Dat e
2 9 NO V 8 9 0 3 JA

N 9 0 1 2 9 NO V 8 9 0 3 JA

N 9 0 1 2 9 NO V 8 9 0 3 JA

N 9 0 1 2 9 NO V 8 9 0 3 JA

N 9 0 1 2 9 NO V 8 9 0 3 JA

N 9 0 1 2 9 NO V 8 9 0 3 JA

N 9 0 1 0 6 DE C 8 9 0 3 JA

N 9 0 1 2 9 NO V 8 9 1 2 DE C 8 9 1

Not e 1 : Result s base donmultiphas e analysi s an dmathematica l recombination

.

ND= No t detecte d N A • No t applicabl e
Reporte dBy : Fre dVelasque z Approve dBy : Tamm y Baile yP.8 3

ICP/M S Metal s

Tota l Metal s
Clien t Name : America nPetroleu m Institut e Clien t ID : TANK-BOTTOM S # 2 La bID : Matrix : Authorized :

Paramete r
Osmiu m (189 ) 007531-0004-S A WAST E 1 7 NO V 8 9

Resul t

ND Ensec o ID : 106035 1

Sampled : 1 5 NO

V 8 9 Prepared : Se e Below Received : 1 7 NO V 8 9 Analyzed : Se e Below

Unit s mg/k g Reportin gAnalytica l

Limi t Metho d



### 0. 4 RMA

L Prepare dAnalyze d

Dat e Dat e

2 9 DE C 8 9 0 3 JA

N 9 0

ND= No t detecte d N A • No t applicabl e
Reporte dBy : Scot t Heidema n Approve dBy : Ton i Tallaric oP.8 4

Metal s

Tota l Metal s

Clien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r

Aluminu m Antimon y Arseni c Bariu m Beryl!iu

m Cadmiu m Calciu m Chromiu m Cobal t Coppe r Lea d Mercury Nicke l Potassiu

m Seleniu m Silve r Sodiu m Thalliu m Ti n

. Vanadiu m Zin c America n Petroleu mInstitut e TAN K BOTTOM S # 2 007531-0004-S AEnsec o ID : WAST E Sampled : 1 7 NO V 8 9 Prepared :

Resul t 106035 1 1 5 NO V 8 9 Se e Below Received :

Analyzed :

Unit s


### 30 0 N D 3 2 

### 43 0 N D 

### 2. 3 340 0 

### 1 0 N O 

### 21 0 94 0 N D 

### 9 N D N D N O 450 0 

### 0. 7 N D 

### 2 19 0 mg/k g

mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g Reporting

Limi t

1 0 5 3 1 0. 2 0. 5 2 0 1 1 1 5 0. 1 4 50 0 1 1 50 0 0. 5 8 1 4 Analytica l

Metho d

601 0 601 0 706 0 601 0 601 0 601 0 601 0 601 0 601 0 601 0 601 0 747 1 601 0 601 0 774 0 601 0 601 0 784 1 601 0 601 0 601 0 1 7 NO V 8 9 Se e Below

Prepare d Analyze d Dat e Dat e

2 1 DE C 8 9 2 1 DE C 8 9 2 1 DE C 8 9 2 1 DE C 8 9 2 1 DE C 8 9 2 1 DE C 8 9 2 1 DE C 8 9 2 1 DE C 8 9 DE C 8 9 DE C 8 9 DE C 8 9 0 6 DE C 8 9 2 1 DE C 8 9 2 1 DE C 8 9 2 1 DE C 8 9 2 1 DE C 8 9 2 1 DE C 8 9 2 1 DE C 8 9 2 1 DE C 8 9 2 1 DE C 8 9 2 1 DE C 8 9 2 1 2 1 2 1 2 7 DE C 8 9

2 7 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 0 8 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 OE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9

N D = No t detecte d N A- No t applicabl e

Reporte d By : Brya

nAnderso

n Approve dBy : Tamm

y BMe yP.8 5



### Clien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r OT C Semivolatil e Organic s TCL P Leachat e Metho d 827 0
America nPetroleumInstitut e TANK BOTTOM S # 2 007531-0004-S AEnsec o ID : 106035 1 WAST E Sampled : 1 5 NO V 8 9 1 7 NOV 8 9 Prepared : 0 7 DE C 8 9 Received : Analyzed : 1 7 NO

V 8 9 1 2 JA N9 0

Pyridin e Pheno l bis(2-Chloroethyl ) ethe r 1,4-Dichlorobenzen e 1,2-Dichlorobenzen e o-Creso l
m

_p-Cresol(s ) Hexachloroethan e Nitrobenzen e Hexachlorobutadien e 2,4,6-Trichloropheno l 2,4,5-Tr i chloropheno l 2,4-Dinitrotoluen e Hexachlorobenzen e 2,3,4,6-Tetrachloropheno l Pentachloropheno l
Nitrobenzene-d 5 2-Fluorobipheny l Terphenyl-dl 4 Phenol-d 5 2-Fluoropheno l 2,4,6-Tr i bromophenol Resul t Unit s
N D mg/ L N D mg/ L N D mg/ L N D mg/ L N D mg/ L N D mg/ L N D mg/ L N D mg/ L N O mg/ L N D mg/ L NO mg/ L N D mg/ L NO mg/ L N D mg/ L N D

. mg/ L N D mg/ L

NDfa 

### 68. 1 % 70. 0 % 48. 1 fa 51. 0 fa 68. 0 % Reportin g

Limi t

4. 4 4. 4 4. 4 4. 4 4. 4 4. 4 4. 4 4. 4 4. 4 4. 4 2 2 4. 4 4. 4 4. 4 2 2

N O ' No t detecte d N A- No t applicabl e
Reporte d By : Belind a Guerr a ApprovedBy : Jef f LowryP.8 6

Refiner y Hazardou s Constituen t Semivolatile s

Metho d827 0

Clien t Name . America nPetroleu m Institut e Clien t ID : TANKBOTTOM S # 2 LabID : 007531-0004-S A Ensec o ID : Matrix : WAST E Sampled : Authorized : 1 7 NO

V 8 9 Prepared :

Paramete r

Anthracen e Berizo(a)anthracen e Benzo(b)fluoranthen e Benzo(k)f1uoranthen e Benzo(a)pyren e bis(2-Ethylhexyl ) phthalat e Buty l benzy l phthalat e Chrysen e Dibenz(a,h)anthracen e Di-n-buty l phthalat e 1,2-Dichlorobenzen e 1,3-Dichlorobenzen e 1,4-Dichlorobenzen e Diethy l phthalat e 7,12-Dimethylbenz

anthracen e Dimethy l phthalat e Di-n-octy l phthalat e Fluoranthen e Inden e 1-Methy l naphthalen e Naphthalen e Phenanthren e Pyren e Pyridin e Quinolin e Benzenethio l o-Creso l
m

_p-Cresol(s ) 2,4-Dimethylpheno l 2,4-Dinitropheno l 4-Nitropheno l Pheno l

Nitrobenzene-d 5 2-Fluorobipheny l Terphenyl-dl 4 Phenol-d 5 2-Fluoropheno l 2,4,6-Tribromopheno l

N D= No t detecte d N A = No t applicabl e 106035 1 1 5 NO V8 9 1 3 DE C 8 9

esul t

N D N D N D N O N O

N D N D N D N D N D N D N D N D N D

N D N D N D N D N D N D N D N D N D N O N O N O N D N D N O N D N D N D

60. 0 72. 6 77. 2 30. 3 40. 7 67. 4 Received : 1 7 NO V8 9 Analyzed : 1 5 DE

C 8 9

Unit s mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

fa

• % fa fa fa fa Reportin g

Limi t

7 0 70 7 0 7 0 7 0

7 0 7 0 7 0 7 0 7 0 7 0 7 0 7 0 7 0

7 0 7 0 7 0 7 0 7 0 7 0 7 0 7 0 7 0

- - 7 0

- - 7 0 7 0 7 0 35 0 35 0 7 0

_ .

- -

- -

- -

- -

- -

Reporte dBy : Da nAlbritto nApprove dBy : Jef f Lowr yP.8 7

Name : ID : Clien t Clien t LabID : Matrix : Authorized : America nPetroleum

TANKBOTTOM S # 2 007531-0004-S A WAST E 1 7 NO V 8 9

Paramete r Viny l chlorid e Acrylonitril e Methylen e chlorid e Carbo ndisulfid e 1,1-Dichloroethen e Isobuty l alcoho l Chloroform 1,2-Dichloroethan e 2-Butanon e 1,1,1-Trichloroethan e Carbo ntetrachlorid e Trichloroethen e 1,1,2-Trichloroethan e Benzen e 1,1,1,2-Tetrachloroethan e 1,1,2,2-Tetrachloroethan e Tetrachloroethen e Toluen e Chlorobenzen e

Toluene-d 8 4-Bromof1uorobenzen e 1,2-Dichloroethane-d 4 OT C Volatil e Organic s TCL P Leachat e Metho d824 0

ur nInstitut e

Ensec o ID : 106035 1 Sampled : 1 5 NO

V 8 9 Prepared : 3 0 NO

V 8 9

Resul t


### N D N D N O N O N D N D N D N D N O N D N D N D N D 7. 1 N D N D N D 8. 9 N D

99. 3 93. 3 89.9
. Unit s

mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L

fa f. % Received : 1 7 NO V 8 9 Analyzed : 1 2 DE C 8 9
Reportin g Limi t

0.9 4 

### 9. 4 0.4 7 0.4 7 0.4 7
. 

### 9. 4 0.4 7 0.4 7 0.9 4 0.4 7 0.4 7 0.4 7 0.4 7 0.4 7 0.4 7 0.4 7 0.4 7 0.4 7 0.4 7

. .

.---

ND- No t detecte d N A » No t applicabl e
Reporte dBy : Ti m

Mille r Approve dBy : Jef f Lowr yP.8 8

Clien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r Appendi xI XVolatil e Organic s (CONT. )

Metho d824 0

America nPetroleu

m Institut e TAN KBOTTOM S # 2 007531-0004-S A

Ensec o ID : WAST E Sampled : 1 7 NO V 8 9 Prepared :

Styren e 1,1,1,2-Tetrachloroethan e 1,1,2,2-Tetrachloroethan e Tetrachloroetnen e Toluen e 1,1,1-Trichloroethan e 1,1,2-Tr i chloroethan e Trichloroethp** ? Trichlorof! i ometnan e 1,2,3-Tr i chloropropan e Viny l acetat e Viny l chlorid e Xylene s (total )

Toluene-d 8 4-Bromofluorobenzen e 1,2-D i chloroethane-d 4 106035 1 1 5 NO V 2 0 NO V

Resul t



### N D N D N O N O 81 0 N D N D N D N D N O N O N O 120 0

96. 9 95. 8 67. 2 

### I 89 89

Unit s
mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

% % %. Received : 1 7 Analyzed : 2 9
Reportin g Limi t


### 100 100 100 100 10 0 100 100 10 0 100 100 20 0 20 0 100

- -

- - 

### NO V NO V 89 89

i

ND = No t detecte d N A* No t applicabl e
Reporte d By : Terr yRiddl e Approve dBy : Jef f Lowr yP.8 9
\

CIien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r Appendi xI XVolatil e Organic s

Metho d824 0

America nPetroleu

m Institut e TANKBOTTOM S # 2 007531-0004-S A

Ensec o ID : 106035 1 WAST E Sampled : 1 5 NO V 8 9 1 7 NO V 8 9 Prepared : 2 0 NO V 8 9 Received : 1 7 NO V 8 9 Analyzed : 2 9 NO

V 8 9

Aceton e Acetonitril e Acrolei n Acrylonitril e Ally l chlorid e Benzen e Bromod i chloromethan e 3romoform Bromomethan e Carbo ndisulfid e Carbo ntetrachlorid e Chlorobenzen e Chloropreh e Chloroethan e Chlorod i bromomethan e Chlorofor m Chloromethan e DBC P (1,2-Dibromo

3-chloropropane ) ED B (1,2-Dibromoethane ) Dibromomethan e trans-1,4rDichloro

2-buten e D i chlorod i fluoromethan e 1,1-Dichloroethan e 1,2-Dichloroethan e trans-1,2-Dichloroethen e 1,1-Dichloroethen e Dich l oromethan e 1,2-Dichloropropan e cis-1,3-Dichloropropen e trans-1,3-Dichloropropen e 1,4-Dioxan e Ethy l benzen e Ethy l cyanid e 2-Hexanon e Iodomethan e Isobuty l alcohol.:-: : Methacrylonitrile " Methy l ethy l keton e 4-Methyl-2-pentanon e esul t


### N D N D N D N O N D 290 N D N D N O N O N O N O N D N D N D N O N D
N D N O N D
N D N D N D N D N O N D N O N O N O N D N D 11 0 N O N O N D N D N O N O N D Unit s

. mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g Reportin g

Limi t 

### 20 0 200 0 200 0 200 0 

### 10 0 10 0 10 0 10 0 20 0 10 0 10 0 10 0 10 0 20 0 10 0 10 0 200 10 0 10 0 

## io o 10 0 200 10 0 10 0 10 0 10 0 10 0 10 0 100 10 0 200 0 

### 10 0 10 0 200 10 0 200 0 

### 10 0 200 200

ND= No t detecte d N A « No t applicabl e
Reporte dBy : Terr y

Riddl e (continue donfollowin gpage )

Approve dBy : Jef f Lowr yGenera l Inorganic s P.9 0

Clien t Name : America n Petroleu mInstitute

. Clien t ID : La bID : Matrix : Authorized :

Paramete r STOC K TAN K BOTTOMS

007531-OO r "-S AEnsec o ID : 106034 9 WAST E Sampled : 1 5 NOV 8 9 1 7 NOV 8 9 Prepared : Se e Belo w

Chlorid e Cyanide
, Reactiv e Ignitabilit y Non-Volatil e Oi l Volatil e Oi l Oi l Wate r ? M id s

- H 5ulfide
, Reactiv e Resul t

808 0 N O 6 6 24. 1 7. 9 32. 0 42. 9 24. 9 7. 3 ND Received : 1 7 NOV 8 9 Analyzed : Se e Belo w

Unit s
mg/k g mg/k g deg

. F % % % % % unit s mg/k g Reportin g

Limi t

1 5 0

.



### 0. 5 Analytica l

Metho d

300. 0 Mod
. EPA/OS W 1010/102 0 Chevro n Chevro n Chevro n Chevro n Chevro n 9045/AST M EPA/OS W Prepare d

Dat e Analyze d

Dat e

0 6 DE C 8 9 1 1 DE C 8 9 N A N A N A N A N A NA N A N A N A 3 0 NOV

8 9 1 9 DE C 8 9 o z 0 4 DE C 8 9 0 4 DE C 8 9 0 4 DE C 8 9 0 4 DE C 8 9 0 4 DE C 8 9 2 1 NOV 8 9 3 0 NOV 8 9

Not e o : Thi s tes t i s unreliabl e fo r anysampl e othe r tha n a

non-aqueou s 1iquid

.

Not e z : Sampl e exhibit s a characteristi c o f hazardou s waste .

ND = No t detecte d N A= No t applicabl e

Reporte dBy : Pa

m Rosa s Approve dBy : Ton i Lus kP.9 1

Metal s

TCL P Oi l Filtrat e
CIien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r
Arseni c Barium Cadmium Chromium Lea d ' Silve r Mercur y Selenium America n PetroleumInstitut e

STOC K TANK BOTTOM S 007531-0002-S AEnsec o I D WAST E Sampled : 1 7 NO V 8 9 Prepared :

Resul t

ND ND ND 1. 5 ND ND ND ND Unit s

mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L : 106034 9

: 1 5 NOV 8 9
: Se e Belo w Reportin g Limi t


### 5 0. 5 0. 3 0. 6 

### 3 0. 5 0. 1 0. 5 Analy t Receive d

Ana '
ica l Metho d

200. 7 200. 7 200. 7 200. 7 200. 7 200. 7 747 1 270. 2 yze d : 1 7 NOV 8 9
: Se e Belo w
Prepare d Analyze d Dat e Dat e
2 9 NOV 8 9 1 3 DE C 8 9 2 9 NO V 8 9 1 3 DE C 8 9 2 9 NO V 8 9 1 3 DE C 8 9 2 9 NOV 8 9 1 3 DE C 8 9 2 9 NOV 8 9 1 3 DE C 8 9 2 9 NOV 8 9 1 3 DE C 8 9 0 6 DE C 8 9 0 8 DE C 8 9 2 9 NOV 8 9 1 2 DE C 8 9

ND = No t detecte d N A» No t applicabl e
Reporte d By : Fre d Velasque z Approve dBy : Tamm y Baile yP.9 2

Metal s

Aqueou s Leachat e

CIien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r

Arseni c Bar i ur n Cadmiu m Chromiu m Lea d Silve r Mercur y Seleniu m America n Petroleu mInstitut e

STOC K TAN K BOTTOM S 007531-0002-S AEnsec o ID : 106034 9 WAST E Sampled : 1 5 NOV i 1 7 NO V 8 9 Prepared : Se e Bel < Reportin g Resul t Unit s Limi t

N D mg/ L 0. 5 1. 8 mg/ L 0. 3 ND mg/ L 0.0 3 N D mg/ L -0.0 5 1. 0 mg/ L 0. 3 N D mg/ L 0.0 5 N D mg/ L 0.00 2 N D mg/ L 0.0 5 3 9 Re c 3 WAn a Analytica l Metho d

200. 7 200. 7 200. 7 200. 7 200. 7 200. 7 747 1 270. 2 

### 1

7 

### NO V 8 9 Se e Be l ov

*

Prepare d Dat e


### 2 9 2 9 2 9 2 9 2 9 2 9 0 6 2 9 

### NO V NO V NO V NO V NO V NO V DE C NO V 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9 i
Analyze d Dat e


### 13 13 13 13 1 3 1 3 0 8 1 2 

### DE C DE C DE C DE C DE C DE C DE C DE C 8 9 8 9 8 9 8 9 8 9 8 9 8 9 8 9

ND = No t detecte d N A= No t applicabl e

Reporte d By : Fre dVelasque z Approve dBy : Tamm y Baile yP.9 3 

# 1

Clien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r
Arseni c Barium Cadmium Chromium Lea d Silve r Mercur y Selenium Metal s

TCL P Leachat e
America n PetroleumInstitut e STOC K TANK BOTTOM S 007531-0002-S AEnsec o ID : 106034 9 WAST E Sampled : 1 5 NOV 8 9 1 7 NO V 8 9 Prepared : Se e Belo w Received : Analyzed : 1 7 NOV

8 9 Se e Belo w

Resul t

N D 1. 4 ND N O 0. 8 ND ND ND Unit s

mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L Reportin g

Limi t

0

. 0

. 0

. 0

. 0

. 0
, 0

. 0
, 5 3 0 3 0 5 3 0 5 00 3 05 ' Analytica l Metho d

200. 7 200. 7 200. 7 200. 7 200. 7 200. 7 747 1 270. 2 Prepare d

Dat e Analyze d

Dat e

2 9 NOV 8 9 0 3 JA

N9 0 1 2 9 NO V 8 9 0 3 JA

N9 0 1 2 9 NOV 8 9 0 3 JA

N9 0 1 2 9 NOV 8 9 0 3 JA

N9 0 1 2 9 NOV 8 9 0 3 JA

N9 0 1 2 9 NOV 8 9 0 3 JA

N9 0 1 0 6 DE C 8 9 0 3 JA

N9 0 1 2 9 NOV 8 9 1 2 DE C 8 9 1

Not e 1 : Result s base d o n multiphas e analysi s and mathematica l

recombination

.
N D = No t detecte d N A• No t applicabl e
Reporte d By : FredVelasque z Approve dBy : Tamm y Baile y


# 1P.9 4

ICP/M S Metal s

Tota l Metal s
Clien t Name : America n PetroleumInstitut e Clien t ID : STOC K TAN K BOTTOM S La bID : 007531-0OO2-S AEnsec o ID : 106034 9 Matrix : WAST E Sampled : 1 5 NOV 8 9 Received : 1 7 NOV 8. 9 Authorized : 1 7 NOV

8 9 Prepared : Se e Belo wAnalyzed : Se e Belo w Reportin g Analytica l Prepare d Analyze d Paramete r Resul t Unit s Limi t Metho d Dat e Dat e
Osmiu m(189 ) N D mg/k g 0. 4 RMA L 2 9 DE C 8 9 0 3 JA N9 0

ND = No t detecte d N A= No t applicabl e
Reporte d By : Scot t Heidema nApprove dBy : Ton i Tallaric o

# 1

Clien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r
Aluminu m Antimon y Arseni c Bariu m Beryl!iu m Cadmiu m Calcium Chromiu m Cobal t Coppe r Lea d Mercur y• Nicke l

. Potassiu m Seleniu m Silve r Sodiu m Thalliu m Ti n Vanadiu m Zin c Metal s

Tota l Metal s
America n Petroleu mInstitut e STOC K TAN K BOTTOM S 007531-0002-S AEnsec o ID : 106034 9 WAST E Sampled : 1 7 NOV 8 9 Prepared :

Resul t

20 0 N D 2 2 3 6 N O N D 260 0 6 1 10 0 14 0 N O 6 N O N D N D 390 0 N D 9 1 12 0 Unit s

mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g : 1 5 NO

V

: Se e Be l
Reportin

g Limi t


### 1 0 

### 5 3 1 0. 2 0. 5 2 0 

### 1 1 1 5 0. 1 

### 4 50 0 

### 1 1 50 0 

### 1 8 1 4 8 9
o w
Analy t Receive d Analyze d

ica l Metho d

601 0 601 0 706 0 601 0 601 0 601 0 601 0 601 0 601 0 601 0 601 0 747 1 601 0 601 0 774 0 601 0 601 0 • 784 1 601 0 601 0 601 0 : 1 7 NO V 8 9

: Se e Belo w

Prepare d Analyze d Dat e Dat e


### 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 21 2 1 0 6 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 OE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 0 8 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 OE C 8 9 2 7 DE C 8 9 2 7 DE C 8 9 2 7 OE C 8 9 2 7 DE C 8 9

DE C 8 9 DE C 8 9 DE C 8 9 DE C 8 9 DE C 8 9 DE C 8 9 DE C 8 9 DE C 8 9 DE C 89

- DE C 8 9 DE C 8 9 DE C 8 9 OE C 8 9 OE C 8 9 DE C 8 9 DE C 8 9 DE C 8 9 DE C 8 9 DE C 8 9 DE C 8 9

ND - No t detecte d N A- No t applicabl e
Reporte d By : Brya nAnderso n Approve dBy : Tamm y Baile yP.9 6

OT C Semivolatil e Organic s TCL P Leachat e Metho d827 0

Name : ID : CIien t CIien t LabID Matri x Authorized : America nPetroleu m Institut e STOC KTAN

KBOTTOM S 007531-0002-S A WAST E 1 7 NO V 8 9

Paramete r Pyridin e Pheno l bis(2-Chloroethyl ) ethe r 1,4-Dichlorobenzen e 1,2-Dichlorobenzen e o-Creso l
m & p-Cresol(s ) Hexachloroethan e Nitrobenzen e Hexachlorobutadien e 2,4,6-Tr i chloropheno l 2,4,5-Tr i chloropheno l 2,4-Dinitrotoluen e Hexachlorobenzen e 2,3,4,6-Tetrachloropheno l Pentachloropheno l

Nitrobenzene-d 5 2-Fluorobipheny l Terphenyl-dl 4 Phenol-d 5 2-Fluoropheno l 2,4,6-Tr i bromopheno l Ensec o ID : Sampled : Prepared : 106034 S

1 5 NO " 0 7 DE C

Resul t


### N D N D N O N O N D N D N D N O N D N O N D N D N D N D N D N D

78. 7 67. 4 68. 4 56. 5 54. 0 58. 5 19



### .9

Unit s mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L
f. fa fa fa fa fa Received : 1 7 NO V 8 9 Analyzed : 2 0 DE C 8 9
Reportin g Limi t

0.8 5 0.8 5 0.8 5 0.8 5 0.8 5 0.8 5 0.8 5 0.8 5 0.8 5 0.8 5 

### 4. 2 0.8 5 0.8 5 0.8 5 

### 4. 2

- -

- -

- -

- -

- -

ND= No t detecte d N A - No t applicabl e
Reporte dBy : Rober t Marti n Approve dBy : Jef f LowryP.9 7

Refiner yHazardou s Constituen t Semivolatile s

Method 827 0

Name : ID : CIien t Clien t La bID : Matrix : Authorize d American Petroleu mInstitut e STOCK TAN

K BOTTOM S 007531-0002-S AEnsec o ID : 106034 9 WAST E Sampled : 1 5 NO V 8 9 1 7 NO V 8 9 Prepared : 2 0 NO V 8 9 Received :

Analyzed : 1 7 NO

V 8 9 0 7 DE C 8 9

Paramete r Resul t Unit s

Anthracen e Benzo(alanthracen e Benzo(b)f1uoranthen e Benzo(klfluoranthen e Benzo(a)pyren e bis(2-Ethylhexyl ) phthalat e Butyl benzy l phthalat e Chrysen e Dibenz(a,h)anthracen e Di-n-buty l phthalat e 1,2-Dichlorobenzen e 1,3-Dichlorobenzen e 1,4-Dichlorobenzen e Diethy l phthalat e 7,12-Dimethylbenz

anthracen e Dimethy l phthalat e Di-n-octy l phthalat e Fluoranthen e Indene 1-Methylnaphthalen e Naphthalen e Phenanthren e Pyren e Pyridin e Quinoline

. Benzenethio l o-Creso l • m& p-Cresol(s ) 2,4-Dimethylpheno l 2,4-Dinitropheno l 4-Nitropheno l Pheno l

Nitrobenzene-d5'- : ; 2--Fluorob

i phenyl/ : Terphenyl-dl 4 Phenol-d 5 2-Fluoropheno l 2,4,6-Tr i bromopheno l

N D = No t detecte d N A= » No t applicabl e

Reporte d By : Bo bMarti n N D N D N O N O N D
N D N D N D N O N D N D N O N D N D
N D N D N D N O N O N D N D N D N D N D N D N D N O N D N D N O N D N D
N D N D N D N D N O N D mg/k

g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

fa fa fa fa fa fa Reporting

Limi t

20 0 20 0 20 0 20 0 20 0

• 20 0 20 0 20 0 20 0 20 0 20 0 20 0 20 0 20 0

20 0 20 0 20 0 20 0 20 0 20 0 20 0 20 0 20 0

20 0

20 0 20 0 20 0 100 0 100 0 20 0

Approve dBy : Jef f Lowr

yP.9 8

OT C Volatil e Organic s TCL P Leachat e Metho d 824 0

Name : ID : CIien t CIien t La bI D Matri x Authorize d American Petroleu mInstitut e STOCK TAN

K BOTTOM S 007531

- WAST E 1 7 NO V 0002-S A

8 9 Ensec o ID :

Sampled : Prepared : 106C "

1 5 N 3 0 Nt

. • 9 Received : 1 7 NO V 8 9

, 9 Analyzed : 1 1 DE C 8 9

Paramete r
Viny l chlorid e Acrylonitril e Methylen e chlorid e Carbo n disulfid e 1,1-Dichloroethen e Isobuty l alcoho l Chloroform 1,2-Dichloroethan e 2-Butanon e 1,1,1-Trichloroethan e Carbo n tetrachlorid e Trichloroethen e 1,1,2-Trichloroethan e Benzen e 1,1,1,2-Tetrachloroethan e 1,1,2 ,2-Tetrachloroethan e Tetrachloroethen e Toluen e Chlorobenzen e

Toluene-d 8 4-Brombf1uorobenzen e 1,2-Dichloroethane-d 4 JSUl t

N D N D N D N D N D N D N D N D N D N D N D N D N D 4. 6 N D N D N D 7. 0 N O

102 99. 0 11 3 Unit s

mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L

% fa fa Reportin g

Limi t

1. 5 1 5 0.7 ' 0.7 5 0.7 5 IS 0.7 5 0.7 5 1. 5 0.7 5 0.7 5 0.7 5 0.7 5 0.7 5 0.7 5 0.7 5 0.7 5 0.7 5 0.7 5

- -

- -

N D = No t detecte d N A= No t applicabl e

Reporte d By : Denee n Mille r Approve dBy : Jeff.Lowr

yP.9 9

Appendi xI

XVolatil e Organic s (CONT. )

Metho d824 0

CIien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r America nPetroleu m Institut e STOC KTAN

KBOTTOM S 007531-0002-S A

Ensec o ID : 106034 9 WAST E Sampled : 1 5 NO V 8 9 1 7 NO V 8 9 Prepared : 2 0 NO V 8 9 Received :

Analyzed : 1 7

2 8 NO V NO V 8 9 8 9

Resul t Unit s

Styren e 1,1,1,2-Tetrachloroethan e 1,1,2,2-Tetrachloroethan e Tetrachloroethen e Toluen e 1,1,1-Trichloroethan e 1,1,2-Trichloroethan e Trichloroethen e Trichlorofluoromethan e 1,2,3-Tr i chloropropan e Viny l acetat e Viny l chlorid e Xylene s (total )

Toluene-d 8 4-Bromofluorobenzen e 1,2-D i chloroethane-d 4 

### N D N D N D N D 150 0 

### N O N D N D N D N D N D N D 210 0

99. 5 

### 10 2 10 7 mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

% % % Reportin g

• Limi t

• 50 0 50 0 50 0 50 0 50 0 50 0 50 0 50 0 50 0 50 0 100 0 100 0 50 0

N D- No t detecte d N A - No t applicabl e

Reporte dBy : Terr y Riddl e Approve dBy : Jef f Lowr y