### Instructions for filling in the Emission Test Template

This Information Collection Request (ICR) spreadsheet is intended to collect information about emission data from fossil fuel burning power plants and which test methods were used to do so for cases where the test methods are not currently supported by the Electronic Reporting Tool (ERT). This spreadsheet should only be used if the method is not in the ERT or if you do not have access to a lab which performs methods that are in the ERT. You must complete at least 3 separate runs or sampling events for each of the requested constituents. This spreadsheet is intended to be used for one boiler of one facility. Data for multiple boilers should be handled by using separate copies of this spreadsheet. yellow are required. All cells that are shaded in green are populated using drop

-down lists. You do not need to populate cells shaded in gray, as they are automatically populated from the Boiler Information worksheet. resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_EmisTestMethods.xls (example: 8100_Unit_2_EmisTestMethods.xls).

Please refer to the following steps when using these spreadsheets.

Boiler Information Worksheet

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the control device configuration.

Emission Data Worksheets

The emission data worksheets are provided for each constituent or constituent family required for this analysis. On each spreadsheet, you must enter boiler operating information during sampling, fuel input information, and emission test results. There are generally 1 to 3 emission test results records to be entered depending on the constituent or constituent family. For example, CO only requires 1 record with 3 sample events, while Mercury requires that you enter both Hg Hg+2

### , or if the Ontario

- Hydro Method was used, you would need to enter Hg0

### , HgP, and Hg Volatile Organic HAP and Speciated Semi

-Volatile Organic HAP worksheets allow you to use a drop

Constituent field to define as many records as needed to record each HAP that you have results for. General instructions follow for these worksheets:

Boiler Operation Information

1. Please provide the values of all requested parameters for each of test run/sample. 2. Please provide any other supporting information or comments in the Other Supporting Information field.

Fuel Information

1. Please enter what types of fuel are being used in your boiler using the drop

-downs in the Fuel Type Selection field. You may enter up to 4 fuel types. If you are not burning one or more of the fuel types entered in one or more samples, then enter an input rate of zero. 2. Please enter the unit of measure using the drop down provided. 3. Please enter the test method used to determine the fuel input rate. 4. Please provide any other information that you feel may be important in the Other Supporting Information field.

Emission Data

### 1. Some constituents ask for the emission rate results of each run in two different units of measure, while others do not. If emission rate results are requested in two different units of measure (ex. lb/MMBtu (Pounds per million BTU) and ppmvd @ 7% O 2 

### (parts per million by volume dry basis at 7 percent oxygen)), you are required to provide both. 2. Please provide the test method used. This may or may not match the example given in the Test Method Used field. Please ensure that the name includes the owning organization of the test method (ex. U.S. EPA Method 0010). 3. Please provide any other information that you feel may be important in the Other Supporting Information field. 4. If data sheets and QA/QC documentation tables are provided for the test method you are entering data for please also enter these data.

### This Information Collection Request (ICR) spreadsheet is intended to collect information about emission data from fossil fuel burning power plants and which test methods were used to do so for cases where the test methods are not currently supported by the Electronic Reporting Tool (ERT). This spreadsheet should only be used if the method is not in the ERT or if you do not have access to a lab which performs methods that are in the ERT. You must complete at least 3 separate This spreadsheet is intended to be used for one boiler of one facility. Data for multiple boilers should be handled by using separate copies of this spreadsheet. Fields shaded in down lists. You do not need to populate cells shaded in gray, as they are automatically populated from the Boiler Information worksheet. Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_EmisTestMethods.xls

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

The emission data worksheets are provided for each constituent or constituent family required for this analysis. On each spreadsheet, you must enter boiler operating information during sampling, fuel input information, and emission test results. There are generally 1 to 3 emission test results records to be entered depending on the constituent or constituent family. For example, CO only requires 1 record with 3 sample events, while Mercury requires that you enter both Hg0 

### and , HgP, and Hg+2 

### . However, both the Speciated Volatile Organic HAP worksheets allow you to use a drop

-down provided in the

Constituent field to define as many records as needed to record each HAP that you have results for. General instructions

2. Please provide any other supporting information or comments in the Other Supporting Information field.

downs in the Fuel Type Selection field. You may enter up to 4 fuel types. If you are not burning one or more of the fuel types entered in one or more samples,

4. Please provide any other information that you feel may be important in the Other Supporting Information field.

### 1. Some constituents ask for the emission rate results of each run in two different units of measure, while others do not. If emission rate results are requested in two different units of measure (ex. lb/MMBtu (Pounds per million BTU) and

(parts per million by volume dry basis at 7 percent oxygen)), you are required to provide both. 2. Please provide the test method used. This may or may not match the example given in the Test Method Used field. Please ensure that the name includes the owning organization of the test method (ex. U.S. EPA Method 0010). 3. Please provide any other information that you feel may be important in the Other Supporting Information field. 4. If data sheets and QA/QC documentation tables are provided for the test method you are entering data for please alsoEIA

Facility Code Facility Name Boiler ID NC_Riverbend Station Riverbend SteamStation Unit 4, Boiler 7, Exhaust 7AControl Device Configuraton Unit 4, Boiler 7, Exhaust 7AEIA

Facility Code Facility Name Boiler ID NC_Riverbend Station Riverbend SteamStation Unit 4, Boiler 7, Exhaust 7A

Run Number Test Start Date Test Start TimeMeasured Value (ppm) Test End Time Test End DateBasis (Wet or Dry) Test Method Used Data Flag (ADL, BDL, DDL) CO Emission Test ResultsTest Method Comments lb/mmBtu ppmdv @ 7% O2 Calculated Emission RateSteam Output (1000 lb/hr) Total Heat Input (mmBtu/hr) Flue Gas Moisture (%)Flue Gas CO2(%) Flue Gas O2(%) Flue Gas Flow Rate (dscfm)Fuel Input Rate Fuel Type

Flue Gas Temperature (F) Fuel #1Units of Measure Measurement Method Fuel Input Rate Fuel #1Fuel Type Units of Measure Measurement Method Fuel #2Fuel Input Rate Fuel Type Units of Measure Fuel #3Measurement Method Fuel Input Rate Fuel Type Fuel #4Units of Measure Measurement Method Fuel #4 Other Supporting InformationEIA

Facility Code Facility Name Boiler ID NC_Riverbend Station Riverbend SteamStation Unit 4, Boiler 7, Exhaust 7A

1 4/7/2010 14:33 4/7/2010 2 4/8/2010 8:57 4/8/2010 3 4/8/2010 11:52 4/8/2010 Run Number Test Start Date Test Start Time Test End DateMeasured Value (ppm) Basis (Wet or Dry) Test Method Used Data Flag (ADL, BDL, DDL) 16:49 0.0013 Dry U.S. EPA Method 316 ADL 11:07 0.0010 Dry U.S. EPA Method 316 ADL 14:08 0.0011 Dry U.S. EPA Method 316 ADL Test End Time Formaldehyde Emission Test ResultsTest Method

Comments lb/mmBtu ppmdv @ 7% O2

1.47E-06 0.00128 1270 1.14E-06 0.00100 1270 1.25E-06 0.00109 1270 Calculated Emission Rate Steam Output (1000 lb/hr) Total Heat Input

(mmBtu/hr)Fuel Input Rate Fuel Type Units of Measure 7.7 12.74 6.92 126,095 324 8.1 12.87 6.91 130,255 315 7.9 12.81 6.92 132,176 317 Flue Gas Moisture (%) Flue Gas

CO2(%) Flue Gas

O2(%) Flue Gas Flow

Rate (dscfm) Flue Gas

Temperature (F) Fuel #1Measurement

Method Fuel Input

Rate Fuel Type Units of Measure Measurement

Method Fuel Input

Rate Fuel Type Units of

Measure Fuel #2 Fuel #3Measurement

Method Fuel Input

Rate Fuel Type Units of

Measure Measurement

Method Fuel #4 Other Supporting InformationEIA

Facility Code Facility Name Boiler ID NC_Riverbend Station Riverbend SteamStation Unit 4, Boiler 7, Exhaust 7A

1 4/7/2010 14:33 2 4/8/2010 8:57 3 4/8/2010 11:52 Run Number Test Start Date Test Start TimeMeasured Value (ppm) Basis (Wet or Dry)

4/7/2010 17:15 0.5 Dry 4/8/2010 11:07 0.32 Dry 4/8/2010 14:08 0.31 Dry Methane Emission Test Results

Test End Time Test End DateTest Method Used Data Flag (ADL, BDL, DDL) Test Method Comments lb/mmBtu

U.S. EPA Method 18 ADL Methane Non-Methane THC Analy zer 0.00030 U.S. EPA Method 18 ADL Methane Non-Methane THC Analy zer 0.00019 U.S. EPA Method 18 ADL Methane Non-Methane THC Analy zer 0.00019 Methane Emission Test Results Calculated Emission Rateppmdv @ 7% O2

0.497 12.74 6.92 0.318 12.87 6.91 0.308 12.81 6.92 Flue Gas O2(%) Flue Gas

Flow Rate (dscfm) Calculated Emission Rate Steam Output (1000 lb/hr) Total Heat

Input (mmBtu/hr) Flue Gas

Moisture (%) Flue Gas CO2(%)Fuel Input Rate Fuel Type Units of

Measure Measurement

Method Fuel

Input Rate Fuel Type Units of

Measure Flue Gas Temperat ure (F) Fuel #1 Fuel #2Measurement

Method Fuel

Input Rate Fuel Type Units of

Measure Measurement

Method Fuel

Input Rate Fuel Type Units of

Measure Fuel #4 Fuel #3Measurement

Method Other Supporting InformationEIA

Facility Code Facility Name Boiler ID NC_Riverbend Station Riverbend SteamStation Unit 4, Boiler 7, Exhaust 7A

Run Number Test Start Date Test Start Time Test End DateMeasured Value (ppm) Basis (Wet or Dry) Test Method Used SO2Emission Test Results Test End TimeData Flag (ADL,

BDL, DDL) Test Method

Comments lb/mmBtu ppmdv @ 7% O2 Calculated Emission Rate Steam Output (1000 lb/hr)Fuel Input Rate Fuel Type Flue Gas Temperature (F) Fuel #1 Flue Gas O2(%) Flue Gas

Flow Rate (dscfm) Total Heat Input (mmBtu/hr) Flue Gas

Moisture (%) Flue Gas

CO2(%)Units of

Measure Measurement

Method Fuel Input

Rate Fuel Type Units of

Measure Measurement

Method Fuel Input

Rate Fuel Type Fuel #1 Fuel #2 Fuel #3Units of

Measure Measurement

Method Fuel Input

Rate Fuel Type Units of Measure Measurement

Method Fuel #4 Fuel #3Other Supporting InformationEIA

Facility Code Facility Name Boiler ID NC_Riverbend Station Riverbend SteamStation Unit 4, Boiler 7, Exhaust 7A

1 4/9/2010 10:34 2 4/12/2010 9:32 3 4/13/2010 11:07 Run Number Test Start Date Test Start TimePlease note QA/QC documentation starting in Column "AI"

Measured Value (μg/dscm) Basis (Wet or Dry)

4/9/2010 12:18 [<7.73] Dry 4/12/2010 11:00 [<9.19] Dry 4/13/2010 12:49 9.34 Dry Test End Date Test End Time Total Vapor Phase Mercury Emission Test ResultsPlease note QA/QC documentation starting in Column "AI"

Test Method Used Data Flag (ADL, BDL, DDL) Test Method

Comments (lb/mmBtu)

U.S. EPA Method 30B DLL DL based on the MDL [<7.03E-06] U.S. EPA Method 30B DLL DL based on the MDL [<8.37E-06] U.S. EPA Method 30B ADL DL based on the MDL 8.52E-06 Steam Output (1000 lb/hr) Total Vapor Phase Mercury Emission Test ResultsFuel Input Rate

1270 6.88 127,312 318 1270 6.9 129,420 318 1270 6.91 128,052 318 Total Heat Input (mmBtu/hr) Flue Gas CO2(%) Flue Gas Moisture (%) Flue Gas

O2(%) Flue Gas

Flow Rate (dscfm) Flue Gas

Temperature (F)Fuel Type Units of Measure Measurement

Method Fuel Input

Rate Fuel Type Units of

Measure Measurement

Method Fuel Input

Rate Fuel #1 Fuel #2Fuel Type Units of Measure Measurement

Method Fuel Input

Rate Fuel Type Units of Measure Measurement

Method Fuel #3 Fuel #4QA /QC Documentation

Trap ID Section 1

Mass (ng) Section 2

Mass (ng) Total

Mass (ng) Initial

Spike (ng) Total NonSpike (ng)

68518 230 1.2 231.2 100 131.2 65448 253 3 256 100 156 65347 259 0.7 259.7 100 159.7 Other Supporting InformationSample

Volume (dscm) Volume

Difference (%) Volume Diff. Limit Breaktrough

(%) Breaktrough

Limit Concentration

(μg/dscm) Trap ID

0.016475 0.52173913 7.963581927 68681 0.016294 1.185770751 9.573806261 68678 0.016713 0.27027027 9.555329455 68165 ≤20% of field

recovery test ≤10% of Section 1 Hg

mass for Hg conc. >1

μg/dscm: or ≤ 20% of Section Trap #1Section 1

Mass Section 2

Mass Total

Mass Initial

Spike Total NonSpike Sample

Volume Volume

Difference (%) Volume Diff. Limit

130 0 130 130 0.016353 0.740 152 0.6 152.6 152.6 0.016067 1.393 159 1.7 160.7 160.7 0.016624 0.536 ≤20% of field

recovery test Trap #2Breaktrough (%) Breaktrough Limit Concentration

(μg/dscm) Abs. diff. RD (%) Limit C rec

0 7.949540751 0.014041 0.088236 6.0838 0.394736842 9.497479153 0.076327 0.40022 6.2134 1.06918239 9.666944369 0.111615 0.580654 5.8717 ≥ 10 % RD mass for Hg conc. >1 μg/dscm: or

≤20% RD or ≤0.2 μg/dscm abs.diff. for Hg conc. ≤1 ≤10% of Section 1 Hg mass for Hg conc. >1

μg/dscm: or ≤ 20% of Section 1 for Hg conc. ≤1 Measured Spike Recovery ( R ) Paired Trap Agreement (RD)R (%) by

Run Ravg(%) Limit

100.23 101.24 98.13 Average Recovery

, between 85 and 115% Measured Spike Recovery ( R )

99.8698655EIA

Facility Code Facility Name Boiler ID NC_Riverbend Station Riverbend SteamStation Unit 4, Boiler 7, Exhaust 7A

Run Number Test Start Date Test Start TimeMeasured Hg 0Value (μg/dscm) Measured Hg +2Value (μg/dscm) Test End Time Test End DateMeasured Hg PValue

(μg/dscm) Basis (Wet or Dry) Test Method Used Data Flag (ADL, BDL, DDL) Total Vapor Phase Mercury Emission Test ResultsTest Method

Comments Total Mercury (lb/mmBtu) Flue Gas CO2(%) Steam Output (1000 lb/hr) Total Heat

Input (mmBtu/hr) Flue Gas

Moisture (%)Fuel Input Rate Fuel Type Units of Measure Measurement

Method Fuel #1 Flue Gas O2(%) Flue Gas

Flow Rate (dscfm) Flue Gas

Temperature (F)Fuel Input Rate Fuel Type Units of Measure Measurement

Method Fuel Input

Rate Fuel Type Units of Measure Measurement

Method Fuel #2 Fuel #3Fuel Input

Rate Fuel Type Units of Measure Measurement

Method Other Supporting Information Fuel #4EIA Facility Code Facility Name Boiler ID Footnotes: NC_Riverbend Station Riverbend Steam Station Unit 4, Boiler 7, Exhaust 7A * Front half fraction contains filter, cyclone, and cartridge ** Back half fraction contains condensate, solvent, impingers

Speciated Volatile Organic HAP Emission Data

Measured Value (μg/m3) Basis Test Method Used Data Flag (ADL, BDL, DDL) 1,1,1,2-Tetrachloroethane 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.14] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,1,1,2-Tetrachloroethane 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.132] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,1,1,2-Tetrachloroethane 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.139] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,1,1-Trichloroethane 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.138] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,1,1-Trichloroethane 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.13] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,1,1-Trichloroethane 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.137] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,1,2,2-Tetrachloroethane 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.338] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,1,2,2-Tetrachloroethane 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.319] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,1,2,2-Tetrachloroethane 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.336] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,1,2-Trichloroethane 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 1.063] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,1,2-Trichloroethane 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 1.003] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,1,2-Trichloroethane 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 1.055] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,1-Dichloroethane 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.12] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,1-Dichloroethane 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.113] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,1-Dichloroethane 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.119] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,1-Dichloroethene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.187] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,1-Dichloroethene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.177] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,1-Dichloroethene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.186] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,1-Dichloropropene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.124] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,1-Dichloropropene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.117] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,1-Dichloropropene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.123] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2,3-Trichlorobenzene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.174] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2,3-Trichlorobenzene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.164] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2,3-Trichlorobenzene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.173] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2,3-Trichloropropane 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 2.647] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2,3-Trichloropropane 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 2.499] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2,3-Trichloropropane 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 2.629] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2,4-Trichlorobenzene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.215] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2,4-Trichlorobenzene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.203] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2,4-Trichlorobenzene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.213] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2,4-Trimethylbenzene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.174] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL 1,2,4-Trimethylbenzene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.17] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL 1,2,4-Trimethylbenzene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.177] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL 1,2-Dibromo-3-chloropropane 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 1.498] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2-Dibromo-3-chloropropane 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 1.414] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2-Dibromo-3-chloropropane 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 1.487] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2-Dibromoethane 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.191] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2-Dibromoethane 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.18] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2-Dibromoethane 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.19] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2-Dichlorobenzene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.202] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2-Dichlorobenzene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.191] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2-Dichlorobenzene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.201] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2-Dichloroethane 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 1.967] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL 1,2-Dichloroethane 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.31] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2-Dichloroethane 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.196] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2-Dichloropropane 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.225] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL 1,2-Dichloropropane 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.187] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,2-Dichloropropane 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.197] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,3,5-Trimethylbenzene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.193] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,3,5-Trimethylbenzene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.182] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,3,5-Trimethylbenzene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.191] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,3-Dichlorobenzene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.165] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,3-Dichlorobenzene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.156] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,3-Dichlorobenzene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.164] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,3-Dichloropropane 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.162] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,3-Dichloropropane 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.152] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,3-Dichloropropane 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.16] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,4-Dichlorobenzene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.18] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,4-Dichlorobenzene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.168] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 1,4-Dichlorobenzene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.177] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 2,2-Dichloropropane 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.129] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 2,2-Dichloropropane 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.122] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 2,2-Dichloropropane 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.128] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 2-Butanone 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 10.886] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 2-Butanone 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 10.278] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 2-Butanone 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 10.812] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 2-Chlorotoluene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.148] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 2-Chlorotoluene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.14] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 2-Chlorotoluene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.147] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 2-Hexanone 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.823] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 2-Hexanone 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.777] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 2-Hexanone 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.817] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Compound (use drop down to define for as many rows as

needed) Run Number Test Start Date Test Start Time Test End Date Test End Time4-Chlorotoluene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.169] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 4-Chlorotoluene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.159] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 4-Chlorotoluene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.168] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 4-Methyl-2-pentanone 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 10.886] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 4-Methyl-2-pentanone 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 10.278] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL 4-Methyl-2-pentanone 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 10.812] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Acetone 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM 23130.1 Dry U.S. EPA Method 0031 with SW-846 Method 8260B ADL Acetone 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM 4095.985 Dry U.S. EPA Method 0031 with SW-846 Method 8260B ADL Acetone 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM 4638.721 Dry U.S. EPA Method 0031 with SW-846 Method 8260B ADL Benzene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 1.776] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Benzene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 1.185] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Benzene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 1.789] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Bromobenzene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.231] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Bromobenzene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.218] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Bromobenzene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.229] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Bromochloromethane 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.336] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Bromochloromethane 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.317] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Bromochloromethane 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.334] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Bromodichloromethane 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.166] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Bromodichloromethane 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.157] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Bromodichloromethane 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.165] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Bromoform 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 1.278] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Bromoform 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 1.206] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Bromoform 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 1.269] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Bromomethane 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 25.358] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Bromomethane 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 2.464] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Bromomethane 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 1.846] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Carbon disulfide 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 1.326] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Carbon disulfide 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.991] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Carbon disulfide 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.596] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Carbon tetrachloride 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.176] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Carbon tetrachloride 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.182] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Carbon tetrachloride 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.331] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Chlorobenzene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.319] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Chlorobenzene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.212] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Chlorobenzene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.158] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Chlorodibromomethane 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.261] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Chlorodibromomethane 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.246] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Chlorodibromomethane 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.259] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Chloroethane 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.804] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Chloroethane 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.661] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Chloroethane 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.695] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Chloroform 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.136] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Chloroform 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.124] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Chloroform 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.13] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Chloromethane 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 24.668] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Chloromethane 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 12.956] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Chloromethane 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 9.208] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL cis-1,2-Dichloroethene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.13] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL cis-1,2-Dichloroethene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.123] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL cis-1,2-Dichloroethene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.129] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL cis-1,3-Dichloropropene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.204] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL cis-1,3-Dichloropropene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.193] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL cis-1,3-Dichloropropene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.203] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Dibromomethane 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.264] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Dibromomethane 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.249] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Dibromomethane 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.262] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Dichlorodifluoromethane 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.982] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Dichlorodifluoromethane 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.586] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Dichlorodifluoromethane 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 1.166] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Ethylbenzene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.411] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Ethylbenzene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.464] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Ethylbenzene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.467] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Hexachlorobutadiene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.353] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Hexachlorobutadiene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.333] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Hexachlorobutadiene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.35] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Isopropylbenzene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.121] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Isopropylbenzene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.114] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Isopropylbenzene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.12] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Methylene chloride 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM 42.817 Dry U.S. EPA Method 0031 with SW-846 Method 8260B ADL Methylene chloride 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM 36.097 Dry U.S. EPA Method 0031 with SW-846 Method 8260B ADL Methylene chloride 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM 39.927 Dry U.S. EPA Method 0031 with SW-846 Method 8260B ADL m-Xylene & p-Xylene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 1.515] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL m-Xylene & p-Xylene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 1.846] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL m-Xylene & p-Xylene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 1.731] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Naphthalene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 1.084] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Naphthalene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 1.023] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Naphthalene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 1.076] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL n-Butylbenzene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.122] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL n-Butylbenzene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.115] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDLn-Butylbenzene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.121] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL n-Propylbenzene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.111] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL n-Propylbenzene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.105] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL n-Propylbenzene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.11] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL o-Xylene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.716] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL o-Xylene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.829] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL o-Xylene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.765] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL p-Isopropyltoluene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.12] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL p-Isopropyltoluene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.115] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL p-Isopropyltoluene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.119] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL sec-Butylbenzene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.12] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL sec-Butylbenzene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.113] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL sec-Butylbenzene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.119] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Styrene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.199] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Styrene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.191] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Styrene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.203] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL tert-Butylbenzene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.13] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL tert-Butylbenzene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.123] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL tert-Butylbenzene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.129] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Tetrachloroethene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.353] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Tetrachloroethene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.382] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Tetrachloroethene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.416] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Toluene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM 1.026 Dry U.S. EPA Method 0031 with SW-846 Method 8260B ADL Toluene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.958] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Toluene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 1.017] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL trans-1,2-Dichloroethene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.223] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, Reporting limit based on MDL trans-1,2-Dichloroethene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.21] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL trans-1,2-Dichloroethene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.221] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL trans-1,3-Dichloropropene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.151] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL trans-1,3-Dichloropropene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.143] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL trans-1,3-Dichloropropene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.15] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Trichloroethene 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.252] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Trichloroethene 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.238] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Trichloroethene 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.251] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Trichlorofluoromethane 1 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.603] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Trichlorofluoromethane 2 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.502] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Trichlorofluoromethane 3 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.787] Dry U.S. EPA Method 0031 with SW-846 Method 8260B DLL, DL based on MDL Vinyl chloride 4 4/7/2010 3:10 PM 4/7/2010 5:01 PM [< 0.26] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Vinyl chloride 5 4/8/2010 8:57 AM 4/8/2010 10:44 AM [< 0.245] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDL Vinyl chloride 6 4/8/2010 11:52 AM 4/8/2010 1:45 PM [< 0.258] Dry U.S. EPA Method 0031 with SW-846 Method 8260B BDL, DL based on MDLFront Half Mass (ng) Back Half Mass (ng) Total Mass (ng) Test Method Comments lb/mmBtu ppmdv @ 7% O2 [< 8.8] [< 2.16] [< 10.96] [< 0.0000001278] [< 8.8] [< 2.16] [< 10.96] [< 0.0000001206] [< 8.8] [< 2.16] [< 10.96] [< 0.0000001019] [< 8] [< 2.8] [< 10.8] [< 0.0000001259] [< 8] [< 2.8] [< 10.8] [< 0.0000001189] [< 8] [< 2.8] [< 10.8] [< 0.0000000926] [< 23.2] [< 3.28] [< 26.48] [< 0.0000003087] [< 23.2] [< 3.28] [< 26.48] [< 0.0000002914] [< 23.2] [< 3.28] [< 26.48] [< 0.0000002686] [< 80] [< 3.16] [< 83.16] [< 0.0000009695] [< 80] [< 3.16] [< 83.16] [< 0.0000009152] [< 80] [< 3.16] [< 83.16] [< 0.0000009263] [< 8] [< 1.36] [< 9.36] [< 0.0000001091] [< 8] [< 1.36] [< 9.36] [< 0.000000103] [< 8] [< 1.36] [< 9.36] [< 0.0000000926] [< 12] [< 2.64] [< 14.64] [< 0.0000001707] [< 12] [< 2.64] [< 14.64] [< 0.0000001611] [< 12] [< 2.64] [< 14.64] [< 0.0000001389] [< 8] [< 1.68] [< 9.68] [< 0.0000001128] [< 8] [< 1.68] [< 9.68] [< 0.0000001065] [< 8] [< 1.68] [< 9.68] [< 0.0000000926] [< 8] [< 5.6] [< 13.6] [< 0.0000001585] [< 8] [< 5.6] [< 13.6] [< 0.0000001497] [< 8] [< 5.6] [< 13.6] [< 0.0000000926] [< 200] [< 7.2] [< 207.2] [< 0.0000024155] [< 200] [< 7.2] [< 207.2] [< 0.0000022804] [< 200] [< 7.2] [< 207.2] [< 0.0000023157] [< 12.8] [< 4] [< 16.8] [< 0.0000001958] [< 12.8] [< 4] [< 16.8] [< 0.0000001849] [< 12.8] [< 4] [< 16.8] [< 0.0000001482] [< 12] 1.6 [< 13.6] [< 0.0000001585] [< 12.3] 1.8 [< 14.1] [< 0.0000001552] [< 12] 1.96 [< 13.96] [< 0.0000001389] [< 104] [< 13.2] [< 117.2] [< 0.0000013663] [< 104] [< 13.2] [< 117.2] [< 0.0000012899] [< 104] [< 13.2] [< 117.2] [< 0.0000012041] [< 11.2] [< 3.76] [< 14.96] [< 0.0000001744] [< 11.2] [< 3.76] [< 14.96] [< 0.0000001646] [< 11.2] [< 3.76] [< 14.96] [< 0.0000001297] [< 14.4] [< 1.4] [< 15.8] [< 0.0000001842] [< 14.4] [< 1.4] [< 15.8] [< 0.0000001739] [< 14.4] [< 1.4] [< 15.8] [< 0.0000001667] [< 13.6] [< 1.84] [< 15.44] [< 0.0000017946] [< 23.9] [< 1.84] [< 25.74] [< 0.0000002833] [< 13.6] [< 1.84] [< 15.44] [< 0.0000001575] [< 13.6] [< 1.92] [< 15.52] [< 0.0000002054] [< 13.6] [< 1.92] [< 15.52] [< 0.0000001708] [< 13.6] [< 1.92] [< 15.52] [< 0.0000001575] [< 14.4] [< 0.68] [< 15.08] [< 0.0000001758] [< 14.4] [< 0.68] [< 15.08] [< 0.000000166] [< 14.4] [< 0.68] [< 15.08] [< 0.0000001667] [< 11.2] [< 1.72] [< 12.92] [< 0.0000001506] [< 11.2] [< 1.72] [< 12.92] [< 0.0000001422] [< 11.2] [< 1.72] [< 12.92] [< 0.0000001297] [< 11.2] [< 1.44] [< 12.64] [< 0.0000001474] [< 11.2] [< 1.44] [< 12.64] [< 0.0000001391] [< 11.2] [< 1.44] [< 12.64] [< 0.0000001297] [< 12] [< 1.96] [< 13.96] [< 0.0000001639] [< 12] [< 1.96] [< 13.96] [< 0.0000001536] [< 12] [< 1.96] [< 13.96] [< 0.0000001389] [< 8] [< 2.12] [< 10.12] [< 0.000000118] [< 8] [< 2.12] [< 10.12] [< 0.0000001114] [< 8] [< 2.12] [< 10.12] [< 0.0000000926] [< 800] [< 52] [< 852] [< 0.0000099324] [< 800] [< 52] [< 852] [< 0.0000093769] [< 800] [< 52] [< 852] [< 0.0000092626] [< 9.6] [< 2] [< 11.6] [< 0.0000001352] [< 9.6] [< 2] [< 11.6] [< 0.0000001277] [< 9.6] [< 2] [< 11.6] [< 0.0000001112] [< 54.4] [< 10] [< 64.4] [< 0.0000007508] [< 54.4] [< 10] [< 64.4] [< 0.0000007088] [< 54.4] [< 10] [< 64.4] [< 0.0000006299] Calculated Emission Rate Steam Output (1000 lb/hr) Total Heat Input (mmBtu/hr) Flue Gas Moisture (%) Flue Gas CO2(%) Flue Gas O2(%)[< 11.2] [< 2] [< 13.2] [< 0.0000001539] [< 11.2] [< 2] [< 13.2] [< 0.0000001453] [< 11.2] [< 2] [< 13.2] [< 0.0000001297] [< 800] [< 52] [< 852] [< 0.0000099324] [< 800] [< 52] [< 852] [< 0.0000093769] [< 800] [< 52] [< 852] [< 0.0000092626]

790 1800000 1800790 High condenstae Method Blank Contamination for all runs. 0.021103167 3555 336000 339555 High condenstae Method Blank Contamination for all runs. 0.003737039 1530 364000 365530 High condenstae Method Blank Contamination for all runs. 1.77148E-05 [< 62] [< 1] [< 63] Method Blank Contamination [< 0.0000016204] [< 97] [< 1.2] [< 98.2] [< 0.0000010808] [< 140] [< 1] [< 141] [< 0.000001621] [< 16] [< 2.04] [< 18.04] [< 0.0000002103] [< 16] [< 2.04] [< 18.04] [< 0.0000001985] [< 16] [< 2.04] [< 18.04] [< 0.0000001853] [< 22.4] [< 3.88] [< 26.28] [< 0.0000003064] [< 22.4] [< 3.88] [< 26.28] [< 0.0000002892] [< 22.4] [< 3.88] [< 26.28] [< 0.0000002594] [< 10.4] [< 2.6] [< 13] [< 0.0000001516] [< 10.4] [< 2.6] [< 13] [< 0.0000001431] [< 10.4] [< 2.6] [< 13] [< 0.0000001204] [< 80] [< 20] [< 100] [< 0.0000011658] [< 80] [< 20] [< 100] [< 0.0000011006] [< 80] [< 20] [< 100] [< 0.0000009263]

90.4 [< 5.6] [< 96] Method Blank Contamination [< 0.0000231359] 198.7 [< 5.6] [< 204.3] [< 0.0000022485] [< 139.9] [< 5.6] [< 145.5] [< 0.0000016198]

1125 [< 1.56] [< 1126.56] [< 0.0000012096] [< 80.6] [< 1.56] [< 82.16] [< 0.0000009042] [< 45.4] [< 1.56] [< 46.96] [< 0.0000005257] [< 12.4] [< 2.16] [< 14.56] [< 0.0000001604] [< 12.9] [< 2.16] [< 15.06] [< 0.0000001657] [< 23.9] [< 2.16] [< 26.06] [< 0.0000002767] [< 11] [< 1.64] [< 12.64] [< 0.0000002907] [< 15.9] [< 1.64] [< 17.54] [< 0.000000193] [< 10.8] [< 1.64] [< 12.44] [< 0.000000125] [< 16] [< 4.4] [< 20.4] [< 0.0000002378] [< 16] [< 4.4] [< 20.4] [< 0.0000002245] [< 16] [< 4.4] [< 20.4] [< 0.0000001853] [< 49.6] [< 5.2] [< 54.8] [< 0.0000007333] [< 49.6] [< 5.2] [< 54.8] [< 0.0000006031] [< 49.6] [< 5.2] [< 54.8] [< 0.0000005743] [< 8.8] [< 1.44] [< 10.24] [< 0.000000124] [< 8.8] [< 1.44] [< 10.24] [< 0.0000001127] [< 8.8] [< 1.44] [< 10.24] [< 0.0000001019]

2139.4 [< 2.56] [< 2141.96] [< 0.0000225059] [< 1071.5] [< 2.56] [< 1074.06] Method Blank Contamination [< 0.0000118208] 723 [< 2.56] [< 725.56] Method Blank Contamination [< 0.0000083711] [< 8] [< 2.16] [< 10.16] [< 0.0000001184] [< 8] [< 2.16] [< 10.16] [< 0.0000001118] [< 8] [< 2.16] [< 10.16] [< 0.0000000926] [< 13.6] [< 2.36] [< 15.96] [< 0.0000001861] [< 13.6] [< 2.36] [< 15.96] [< 0.0000001757] [< 13.6] [< 2.36] [< 15.96] [< 0.0000001575] [< 16.8] [< 3.88] [< 20.68] [< 0.0000002411] [< 16.8] [< 3.88] [< 20.68] [< 0.0000002276] [< 16.8] [< 3.88] [< 20.68] [< 0.0000001945] [< 220.6] [< 3.28] [< 223.88] [< 0.0000008962] [< 45.3] [< 3.28] [< 48.58] [< 0.0000005347] [< 88.6] [< 3.28] [< 91.88] [< 0.0000010258] [< 10.6] 24 [< 34.6] [< 0.0000003754] [< 13.3] 25.2 [< 38.5] [< 0.0000004237] [< 8.8] 28 [< 36.8] [< 0.0000001019] [< 20] [< 7.6] [< 27.6] [< 0.0000003218] [< 20] [< 7.6] [< 27.6] [< 0.0000003038] [< 20] [< 7.6] [< 27.6] [< 0.0000002316] [< 8] [< 1.44] [< 9.44] [< 0.00000011] [< 8] [< 1.44] [< 9.44] [< 0.0000001039] [< 8] [< 1.44] [< 9.44] [< 0.0000000926]

207 3200 3407 Method Blank Contamination 3.91E-05 152.4 2840 2992.4 Method Blank Contamination 3.29E-05 146.2 3000 3146.2 Method Blank Contamination 1.69E-06 [< 18.4] 100 [< 118.4] [< 0.0000013826] [< 49] 104 [< 153] [< 0.0000016839] [< 20.4] 116 [< 136.4] [< 0.0000002362] [< 80] [< 4.8] [< 84.8] [< 0.0000009886] [< 80] [< 4.8] [< 84.8] [< 0.0000009333] [< 80] [< 4.8] [< 84.8] [< 0.0000009263] [< 8] [< 1.52] [< 9.52] [< 0.000000111] [< 8] [< 1.52] [< 9.52] [< 0.0000001048][< 8] [< 1.52] [< 9.52] [< 0.0000000926] [< 8] [< 0.68] [< 8.68] [< 0.0000001012] [< 8] [< 0.68] [< 8.68] [< 0.0000000955] [< 8] [< 0.68] [< 8.68] [< 0.0000000926] [< 8] 48 [< 56] [< 0.0000006528] [< 20.7] 48 [< 68.7] [< 0.0000007561] [< 8.3] 52 [< 60.3] [< 0.0000000961] [< 8] [< 1.36] [< 9.36] [< 0.0000001091] [< 8.2] [< 1.36] [< 9.56] [< 0.0000001052] [< 8] [< 1.36] [< 9.36] [< 0.0000000926] [< 8] [< 1.36] [< 9.36] [< 0.0000001091] [< 8] [< 1.36] [< 9.36] [< 0.000000103] [< 8] [< 1.36] [< 9.36] [< 0.0000000926] [< 11.7] 5.2 [< 16.9] [< 0.0000001819] [< 11] 4.8 [< 15.8] [< 0.0000001739] [< 10.4] 5.6 [< 16] [< 0.0000001204] [< 8.8] [< 1.4] [< 10.2] [< 0.0000001189] [< 8.8] [< 1.4] [< 10.2] [< 0.0000001123] [< 8.8] [< 1.4] [< 10.2] [< 0.0000001019] [< 8.8] 18 [< 26.8] [< 0.0000003218] [< 10.5] 21.2 [< 31.7] [< 0.0000003489] [< 8.8] 24 [< 32.8] [< 0.0000001019]

69.1 52 121.1 Method Blank Contamination 9.361E-07 [< 23.4] 56 [< 79.4] [< 0.0000008739] [< 20.1] 60 [< 80.1] [< 0.0000002327] [< 16] [< 1.44] [< 17.44] [< 0.0000002033] [< 16] [< 1.44] [< 17.44] [< 0.0000001919] [< 16] [< 1.44] [< 17.44] [< 0.0000001853] [< 9.6] [< 2.24] [< 11.84] [< 0.000000138] [< 9.6] [< 2.24] [< 11.84] [< 0.0000001303] [< 9.6] [< 2.24] [< 11.84] [< 0.0000001112] [< 17.6] [< 2.16] [< 19.76] [< 0.0000002304] [< 17.6] [< 2.16] [< 19.76] [< 0.0000002175] [< 17.6] [< 2.16] [< 19.76] [< 0.0000002038] 21 [< 1.52] [< 22.52] [< 0.0000005505] [< 40.1] [< 1.52] [< 41.62] [< 0.0000004581] [< 60.5] [< 1.52] [< 62.02] [< 0.0000007005] [< 21] [< 3.52] [< 24.52] [< 0.0000002369] [< 16.8] [< 3.52] [< 20.32] [< 0.0000002236] [< 16.8] [< 3.52] [< 20.32] [< 0.0000001945]Fuel Input Rate Fuel Type Units of Measure Measurement Method Fuel Input Rate Fuel Type Units of Measure Measurement Method Fuel Input Rate Flue Gas Flow Rate (scfm) Flue Gas Temperature (F) Fuel #1 Fuel #2Fuel Type Units of Measure Measurement Method Fuel Input Rate Fuel Type Units of Measure Measurement Method Fuel #4 Other Supporting Information Fuel #3EIA

Facility Code Facility Name NC_Riverbend Station Riverbend SteamStation

Speciated Semi-Volatile Organic HAP Emission Data

Acenaphthene 1 Acenaphthene 2 Acenaphthene 3 Acenaphthylene 1 Acenaphthylene 2 Acenaphthylene 3 Anthracene 1 Anthracene 2 Anthracene 3 Benzo(a)anthracene 1 Benzo(a)anthracene 2 Benzo(a)anthracene 3 Benzo(b)fluoranthene 1 Benzo(b)fluoranthene 2 Benzo(b)fluoranthene 3 Benzo(k)fluoranthene 1 Benzo(k)fluoranthene 2 Benzo(k)fluoranthene 3 Benzo(g,h,i)perylene 1 Benzo(g,h,i)perylene 2 Benzo(g,h,i)perylene 3 Benzo(a)pyrene 1 Benzo(a)pyrene 2 Benzo(a)pyrene 3 Benzo(e)pyrene 1 Benzo(e)pyrene 2 Benzo(e)pyrene 3 Chrysene 1 Chrysene 2 Chrysene 3 Dibenzo(a,h)anthracene 1 Dibenzo(a,h)anthracene 2 Dibenzo(a,h)anthracene 3 Fluoranthene 1 Fluoranthene 2 Fluoranthene 3 Fluorene 1 Fluorene 2 Fluorene 3 Indeno(1,2,3-cd)pyrene 1 Indeno(1,2,3-cd)pyrene 2 Indeno(1,2,3-cd)pyrene 3 2-Methylnaphthalene 1 2-Methylnaphthalene 2 2-Methylnaphthalene 3 Naphthalene 1 Naphthalene 2

Compound (use drop down to define for as many rows as

needed) Run NumberNaphthalene 3

Perylene 1 Perylene 2 Perylene 3 Phenanthrene 1 Phenanthrene 2 Phenanthrene 3 Pyrene 1 Pyrene 2 Pyrene 3 1,2,4-Trichlorobenzene 1 1,2,4-Trichlorobenzene 2 1,2,4-Trichlorobenzene 3 1,2-Dichlorobenzene 1 1,2-Dichlorobenzene 2 1,2-Dichlorobenzene 3 1,2-Diphenylhydrazine 1 1,2-Diphenylhydrazine 2 1,2-Diphenylhydrazine 3 1,3-Dichlorobenzene 1 1,3-Dichlorobenzene 2 1,3-Dichlorobenzene 3 1,4-Dichlorobenzene 1 1,4-Dichlorobenzene 2 1,4-Dichlorobenzene 3 Bis(2-chloroisopropyl) ether 1 Bis(2-chloroisopropyl) ether 2 Bis(2-chloroisopropyl) ether 3 2,4,5-Trichlorophenol 1 2,4,5-Trichlorophenol 2 2,4,5-Trichlorophenol 3 2,4,6-Trichlorophenol 1 2,4,6-Trichlorophenol 2 2,4,6-Trichlorophenol 3 2,4-Dichlorophenol 1 2,4-Dichlorophenol 2 2,4-Dichlorophenol 3 2,4-Dimethylphenol 1 2,4-Dimethylphenol 2 2,4-Dimethylphenol 3 2,4-Dinitrophenol 1 2,4-Dinitrophenol 2 2,4-Dinitrophenol 3 2,4-Dinitrotoluene 1 2,4-Dinitrotoluene 2 2,4-Dinitrotoluene 3 2,6-Dinitrotoluene 1 2,6-Dinitrotoluene 2 2,6-Dinitrotoluene 3 2-Chloronaphthalene 1 2-Chloronaphthalene 2 2-Chloronaphthalene 3 2-Chlorophenol 1 2-Chlorophenol 2 2-Chlorophenol 32-Methylphenol 1

2-Methylphenol 2 2-Methylphenol 3 2-Nitroaniline 1 2-Nitroaniline 2 2-Nitroaniline 3 2-Nitrophenol 1 2-Nitrophenol 2 2-Nitrophenol 3 3,3'-Dichlorobenzidine 1 3,3'-Dichlorobenzidine 2 3,3'-Dichlorobenzidine 3 3-Methylphenol 1 3-Methylphenol 2 3-Methylphenol 3 3-Nitroaniline 1 3-Nitroaniline 2 3-Nitroaniline 3 4,6-Dinitro-2-methylphenol 1 4,6-Dinitro-2-methylphenol 2 4,6-Dinitro-2-methylphenol 3 4-Bromophenyl phenyl ether 1 4-Bromophenyl phenyl ether 2 4-Bromophenyl phenyl ether 3 4-Chloro-3-methylphenol 1 4-Chloro-3-methylphenol 2 4-Chloro-3-methylphenol 3 4-Chloroaniline 1 4-Chloroaniline 2 4-Chloroaniline 3 4-Chlorophenyl phenyl ether 1 4-Chlorophenyl phenyl ether 2 4-Chlorophenyl phenyl ether 3 4-Nitroaniline 1 4-Nitroaniline 2 4-Nitroaniline 3 4-Nitrophenol 1 4-Nitrophenol 2 4-Nitrophenol 3 Acetophenone 1 Acetophenone 2 Acetophenone 3 Aniline 1 Aniline 2 Aniline 3 Benzidine 1 Benzidine 2 Benzidine 3 Benzoic acid 1 Benzoic acid 2 Benzoic acid 3 Benzyl alcohol 1 Benzyl alcohol 2 Benzyl alcohol 3 Bis(2-chloroethoxy)methane 1Bis(2-chloroethoxy)methane 2

Bis(2-chloroethoxy)methane 3 Bis(2-chloroethyl) ether 1 Bis(2-chloroethyl) ether 2 Bis(2-chloroethyl) ether 3 Bis(2-ethylhexyl) phthalate 1 Bis(2-ethylhexyl) phthalate 2 Bis(2-ethylhexyl) phthalate 3 Butyl benzyl phthalate 1 Butyl benzyl phthalate 2 Butyl benzyl phthalate 3 Carbazole 1 Carbazole 2 Carbazole 3 Dibenzofuran 1 Dibenzofuran 2 Dibenzofuran 3 Diethyl phthalate 1 Diethyl phthalate 2 Diethyl phthalate 3 Dim ethyl phthalate 1 Dim ethyl phthalate 2 Dim ethyl phthalate 3 Di-n-butyl phthalate 1 Di-n-butyl phthalate 2 Di-n-butyl phthalate 3 Di-n-octyl phthalate 1 Di-n-octyl phthalate 2 Di-n-octyl phthalate 3 Hexachlorobenzene 1 Hexachlorobenzene 2 Hexachlorobenzene 3 Hexachlorobutadiene 1 Hexachlorobutadiene 2 Hexachlorobutadiene 3 Hexachlorocyclopentadiene 1 Hexachlorocyclopentadiene 2 Hexachlorocyclopentadiene 3 Hexachloroethane 1 Hexachloroethane 2 Hexachloroethane 3 Isophorone 1 Isophorone 2 Isophorone 3 Nitrobenzene 1 Nitrobenzene 2 Nitrobenzene 3 N-Nitrosodimethylam ine 1 N-Nitrosodimethylam ine 2 N-Nitrosodimethylam ine 3 N-Nitrosodi-n-propylam ine 1 N-Nitrosodi-n-propylam ine 2 N-Nitrosodi-n-propylam ine 3 N-Nitrosodiphenylam ine 1 N-Nitrosodiphenylam ine 2N-Nitrosodiphenylam ine 3

Pentachlorobenzene 1 Pentachlorobenzene 2 Pentachlorobenzene 3 Pentachloronitrobenzene 1 Pentachloronitrobenzene 2 Pentachloronitrobenzene 3 Pentachlorophenol 1 Pentachlorophenol 2 Pentachlorophenol 3 Phenol 1 Phenol 2 Phenol 3 Pyridine 1 Pyridine 2 Pyridine 3Boiler ID

Unit 4, Boiler 7, Exhaust 7A

4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 Test Start Date Test Start Time Test End Date4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/20104/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/20104/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/20104/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010 4/7/2010 2:33 PM 4/7/2010 4/8/2010 8:57 AM 4/8/2010 4/8/2010 11:52 AM 4/8/2010Footnotes: * Front Half Composite contains particulate filter, front half of the filter holder, and probe solvent rinses ** Back Half Composite contains XAD-2 resin tube, back half of the filter holder, and coil condenser solvent rinses *** Condensate Composite contains condensate and Impinger contents and the glassware solvent rinses

Measured Value (μg/m3) Basis (Wet or Dry)

4:49 PM [< 0.0184] Dry 11:07 AM [< 0.0155] Dry 2:08 PM [< 0.0206] Dry 4:49 PM [< 0.0046] Dry 11:07 AM [< 0.0024] Dry 2:08 PM [< 0.0039] Dry 4:49 PM [< 0.004] Dry 11:07 AM [< 0.0038] Dry 2:08 PM [< 0.0038] Dry 4:49 PM [< 0.0038] Dry 11:07 AM [< 0.0037] Dry 2:08 PM [< 0.0037] Dry 4:49 PM [< 0.0093] Dry 11:07 AM [< 0.0076] Dry 2:08 PM [< 0.0107] Dry 4:49 PM [< 0.0437] Dry 11:07 AM [< 0.0423] Dry 2:08 PM [< 0.0426] Dry 4:49 PM [< 0.0052] Dry 11:07 AM [< 0.005] Dry 2:08 PM [< 0.0051] Dry 4:49 PM [< 0.006] Dry 11:07 AM [< 0.0052] Dry 2:08 PM [< 0.0086] Dry 4:49 PM [< 0.0057] Dry 11:07 AM [< 0.0055] Dry 2:08 PM [< 0.0056] Dry 4:49 PM [< 0.0028] Dry 11:07 AM [< 0.0024] Dry 2:08 PM [< 0.0025] Dry 4:49 PM [< 0.004] Dry 11:07 AM [< 0.0039] Dry 2:08 PM [< 0.0039] Dry 4:49 PM [< 0.0335] Dry 11:07 AM [< 0.0112] Dry 2:08 PM [< 0.0089] Dry 4:49 PM [< 0.0163] Dry 11:07 AM [< 0.0122] Dry 2:08 PM [< 0.0234] Dry 4:49 PM [< 0.0027] Dry 11:07 AM [< 0.0026] Dry 2:08 PM [< 0.0026] Dry 4:49 PM [< 0.0928] Dry 11:07 AM [< 0.077] Dry 2:08 PM [< 0.1374] Dry 4:49 PM [< 0.3019] Dry 11:07 AM [< 0.2864] Dry Test End Time2:08 PM [< 0.2906] Dry 4:49 PM [< 0.0031] Dry 11:07 AM [< 0.003] Dry 2:08 PM [< 0.003] Dry 4:49 PM [< 0.104] Dry 11:07 AM [< 0.0607] Dry 2:08 PM [< 0.0766] Dry 4:49 PM [< 0.0471] Dry 11:07 AM [< 0.0355] Dry 2:08 PM [< 0.0357] Dry 4:49 PM [< 3.3656] Dry 11:07 AM [< 3.2592] Dry 2:08 PM [< 3.2845] Dry 4:49 PM [< 3.4676] Dry 11:07 AM [< 3.3579] Dry 2:08 PM [< 3.3841] Dry 4:49 PM [< 2.8557] Dry 11:07 AM [< 2.7653] Dry 2:08 PM [< 2.7869] Dry 4:49 PM [< 3.3656] Dry 11:07 AM [< 3.2592] Dry 2:08 PM [< 3.2845] Dry 4:49 PM [< 3.2127] Dry 11:07 AM [< 3.111] Dry 2:08 PM [< 3.1352] Dry 4:49 PM [< 3.4676] Dry 11:07 AM [< 3.3579] Dry 2:08 PM [< 3.3841] Dry 4:49 PM [< 2.7537] Dry 11:07 AM [< 2.6666] Dry 2:08 PM [< 2.6873] Dry 4:49 PM [< 2.9067] Dry 11:07 AM [< 2.8147] Dry 2:08 PM [< 2.8366] Dry 4:49 PM [< 3.0087] Dry 11:07 AM [< 2.9135] Dry 2:08 PM [< 2.9362] Dry 4:49 PM [< 6.7313] Dry 11:07 AM [< 6.5183] Dry 2:08 PM [< 6.5691] Dry 4:49 PM [< 43.8553] Dry 11:07 AM [< 42.4678] Dry 2:08 PM [< 42.7984] Dry 4:49 PM [< 6.6293] Dry 11:07 AM [< 6.4195] Dry 2:08 PM [< 6.4695] Dry 4:49 PM [< 6.7313] Dry 11:07 AM [< 6.5183] Dry 2:08 PM [< 6.5691] Dry 4:49 PM [< 3.1617] Dry 11:07 AM [< 3.0616] Dry 2:08 PM [< 3.0855] Dry 4:49 PM [< 3.1107] Dry 11:07 AM [< 3.0122] Dry 2:08 PM [< 3.0357] Dry4:49 PM [< 2.7027] Dry 11:07 AM [< 2.6172] Dry 2:08 PM [< 2.6376] Dry 4:49 PM [< 4.1815] Dry 11:07 AM [< 4.0493] Dry 2:08 PM [< 4.0808] Dry 4:49 PM [< 4.1815] Dry 11:07 AM [< 4.0493] Dry 2:08 PM [< 4.0808] Dry 4:49 PM [< 8.4651] Dry 11:07 AM [< 8.1973] Dry 2:08 PM [< 8.2611] Dry 4:49 PM [< 5.6094] Dry 11:07 AM [< 5.4319] Dry 2:08 PM [< 5.4742] Dry 4:49 PM [< 16.0123] Dry 11:07 AM [< 15.5057] Dry 2:08 PM [< 15.6264] Dry 4:49 PM [< 9.9949] Dry 11:07 AM [< 9.6787] Dry 2:08 PM [< 9.7541] Dry 4:49 PM [< 3.9776] Dry 11:07 AM [< 3.8517] Dry 2:08 PM [< 3.8817] Dry 4:49 PM [< 4.0796] Dry 11:07 AM [< 3.9505] Dry 2:08 PM [< 3.9812] Dry 4:49 PM [< 7.4452] Dry 11:07 AM [< 7.2096] Dry 2:08 PM [< 7.2658] Dry 4:49 PM [< 3.2127] Dry 11:07 AM [< 3.111] Dry 2:08 PM [< 3.1352] Dry 4:49 PM [< 10.5049] Dry 11:07 AM [< 10.1725] Dry 2:08 PM [< 10.2517] Dry 4:49 PM [< 18.358] Dry 11:07 AM [< 17.7772] Dry 2:08 PM [< 17.9156] Dry 4:49 PM [< 4.0796] Dry 11:07 AM [< 4.5431] Dry 2:08 PM [< 3.6827] Dry 4:49 PM [< 8.7711] Dry 11:07 AM [< 8.4936] Dry 2:08 PM [< 8.5597] Dry 4:49 PM [< 60.5815] Dry 11:07 AM [< 58.6648] Dry 2:08 PM [< 59.1216] Dry 4:49 PM [< 107.0884] Dry 11:07 AM [< 98.7623] Dry 2:08 PM [< 89.5781] Dry 4:49 PM [< 5.7114] Dry 11:07 AM [< 5.5307] Dry 2:08 PM [< 5.5737] Dry 4:49 PM [< 2.5497] Dry11:07 AM [< 2.4691] Dry 2:08 PM [< 2.4883] Dry 4:49 PM [< 3.3146] Dry 11:07 AM [< 3.2098] Dry 2:08 PM [< 3.2348] Dry 4:49 PM [< 11.0148] Dry 11:07 AM [< 10.6663] Dry 2:08 PM [< 10.7494] Dry 4:49 PM [< 4.5895] Dry 11:07 AM [< 4.4443] Dry 2:08 PM [< 4.4789] Dry 4:49 PM [< 3.0597] Dry 11:07 AM [< 2.9629] Dry 2:08 PM [< 2.9859] Dry 4:49 PM [< 2.8047] Dry 11:07 AM [< 2.716] Dry 2:08 PM [< 2.7371] Dry 4:49 PM [< 3.3146] Dry 11:07 AM [< 3.2098] Dry 2:08 PM [< 3.2348] Dry 4:49 PM [< 3.0087] Dry 11:07 AM [< 2.9135] Dry 2:08 PM [< 2.9362] Dry 4:49 PM [< 4.7935] Dry 11:07 AM [< 4.6418] Dry 2:08 PM [< 4.678] Dry 4:49 PM [< 4.6915] Dry 11:07 AM [< 4.5431] Dry 2:08 PM [< 4.5784] Dry 4:49 PM [< 3.3656] Dry 11:07 AM [< 3.2592] Dry 2:08 PM [< 3.2845] Dry 4:49 PM [< 2.8047] Dry 11:07 AM [< 2.716] Dry 2:08 PM [< 2.7371] Dry 4:49 PM [< 24.4774] Dry 11:07 AM [< 23.703] Dry 2:08 PM [< 23.8875] Dry 4:49 PM [< 3.0087] Dry 11:07 AM [< 2.9135] Dry 2:08 PM [< 2.9362] Dry 4:49 PM [< 2.9067] Dry 11:07 AM [< 2.8147] Dry 2:08 PM [< 2.8366] Dry 4:49 PM [< 2.9067] Dry 11:07 AM [< 2.8147] Dry 2:08 PM [< 2.8366] Dry 4:49 PM [< 3.2127] Dry 11:07 AM [< 3.111] Dry 2:08 PM [< 3.1352] Dry 4:49 PM [< 3.2127] Dry 11:07 AM [< 3.111] Dry 2:08 PM [< 3.1352] Dry 4:49 PM [< 3.6206] Dry 11:07 AM [< 3.5061] Dry2:08 PM [< 3.5334] Dry 4:49 PM [< 3.2127] Dry 11:07 AM [< 3.111] Dry 2:08 PM [< 3.1352] Dry 4:49 PM [< 6.8333] Dry 11:07 AM [< 6.6171] Dry 2:08 PM [< 6.6686] Dry 4:49 PM [< 8.6691] Dry 11:07 AM [< 8.3948] Dry 2:08 PM [< 8.4602] Dry 4:49 PM [< 3.9776] Dry 11:07 AM [< 4.2468] Dry 2:08 PM [< 3.7324] Dry 4:49 PM [< 8.7711] Dry 11:07 AM [< 8.4936] Dry 2:08 PM [< 8.5597] Dry* Front Half Composite contains particulate filter, front half of the filter holder, and probe solvent rinses ** Back Half Composite contains XAD-2 resin tube, back half of the filter holder, and coil condenser solvent rinses *** Condensate Composite contains condensate and Impinger contents and the glassware solvent rinses

Test Method Used Data Flag (ADL, BDL, DLL) Front Half mass* (ng)

U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 24 U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 20 U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 27 U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 2.2 U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 1.6 U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 1.8 U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL [< 1.8] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1.8] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1.8] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1.5] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1.5] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1.5] U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 8.6 U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 5.8 U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 12 U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1.7] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1.7] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1.7] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 5.6] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 5.6] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 5.6] U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 7 U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 4.1 U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 12 U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2.8] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2.8] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2.8] U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL [< 1.5] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1.5] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1.5] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2.6] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2.6] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2.6] U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 4.8 U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 3.9 U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL [< 3] U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 17 U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 14 U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 12 U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1.5] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1.5] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1.5] U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 84 U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 72 U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 79 U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 100 U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 88

Semi-Volatile Organic HAP Emission Test ResultsU.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 92 U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1.5] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1.5] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1.5] U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 42 U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 31 U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL 22 U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL [< 60] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 60] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 60] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 14000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 14000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 14000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2800] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2800] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2800] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2800] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2800] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2800] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2200] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2200] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2200]U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2200] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2200] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2200] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2200] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2200] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2200] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2200] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2200] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2200] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2800] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2800] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2800] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 4400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 4400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 4400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 10000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 10000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 10000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 10000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 10000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 10000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3200] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3200] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3200] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2800] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2800] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2800] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 15000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 15000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 15000] U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL [< 1100] U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL [< 1100] U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL [< 1100] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3200] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3200] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3200] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 5800] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 5800] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 5800] U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL [< 30000] U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL [< 30000] U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL [< 30000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 4600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 4600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 4600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1900]U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1900] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1900] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2800] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2800] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2800] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 20000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 20000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 20000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1900] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1900] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1900] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2200] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2200] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2200] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2600] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3000]U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 3000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1500] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1500] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 1500] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2000] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2800] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2800] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 2800] U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C DLL, DL based on MDL [< 2400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 5400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 5400] U.S. EPA Method 0010 with SW-846 Method 8270C BDL, DL based on MDL [< 5400]Back Half mass* (ng) Condensate Mass*** (ng) Total Composite (ng)

7.3 [< 4.8] [< 36.1] 6.6 [< 4.8] [< 31.4] 9.5 [< 4.8] [< 41.3] 6.3 0.47 [< 8.97] 3 0.3 [< 4.9] 5.8 0.31 [< 7.91] 4.7 [< 1.4] [< 7.9] [< 4.4] [< 1.4] [< 7.6] [< 4.4] [< 1.4] [< 7.6] [< 3] [< 3] [< 7.5] [< 3] [< 3] [< 7.5] [< 3] [< 3] [< 7.5] [< 6.6] [< 3] [< 18.2] 6.6 [< 3] [< 15.4] [< 6.6] [< 3] [< 21.6] [< 82] [< 2] [< 85.7] [< 82] [< 2] [< 85.7] [< 82] [< 2] [< 85.7] [< 3.6] [< 1] [< 10.2] [< 3.6] [< 1] [< 10.2] [< 3.6] [< 1] [< 10.2] 3.9 [< 0.8] [< 11.7] 5.6 [< 0.8] [< 10.5] 4.5 [< 0.8] [< 17.3] [< 5.6] [< 2.8] [< 11.2] [< 5.6] [< 2.8] [< 11.2] [< 5.6] [< 2.8] [< 11.2] [< 3] 0.92 [< 5.42] [< 3] [< 0.44] [< 4.94] [< 3] [< 0.44] [< 4.94] [< 3.6] [< 1.6] [< 7.8] [< 3.6] [< 1.6] [< 7.8] [< 3.6] [< 1.6] [< 7.8] 56 [< 4.8] [< 65.6] 14 [< 4.8] [< 22.7] 10 [< 4.8] [< 17.8] 12 [< 3] [< 32] 7.8 [< 3] [< 24.8] 32 [< 3] [< 47] [< 1.8] [< 2] [< 5.3] [< 1.8] [< 2] [< 5.3] [< 1.8] [< 2] [< 5.3] 81 [< 17] [< 182] 67 [< 17] [< 156] 180 [< 17] [< 276] [< 460] [< 32] [< 592] [< 460] [< 32] [< 580] Semi-Volatile Organic HAP Emission Test Results[< 460] [< 32] [< 584]

[< 3] [< 1.6] [< 6.1] [< 3] [< 1.6] [< 6.1] [< 3] [< 1.6] [< 6.1] 140 [< 22] [< 204] 70 [< 22] [< 123] 110 [< 22] [< 154] 29 [< 3.4] [< 92.4] [< 8.4] [< 3.4] [< 71.8] [< 8.4] [< 3.4] [< 71.8] [< 2000] [< 2200] [< 6600] [< 2000] [< 2200] [< 6600] [< 2000] [< 2200] [< 6600] [< 2200] [< 2200] [< 6800] [< 2200] [< 2200] [< 6800] [< 2200] [< 2200] [< 6800] [< 1700] [< 1900] [< 5600] [< 1700] [< 1900] [< 5600] [< 1700] [< 1900] [< 5600] [< 1800] [< 2400] [< 6600] [< 1800] [< 2400] [< 6600] [< 1800] [< 2400] [< 6600] [< 1900] [< 2000] [< 6300] [< 1900] [< 2000] [< 6300] [< 1900] [< 2000] [< 6300] [< 2000] [< 2200] [< 6800] [< 2000] [< 2200] [< 6800] [< 2000] [< 2200] [< 6800] [< 1400] [< 1400] [< 5400] [< 1400] [< 1400] [< 5400] [< 1400] [< 1400] [< 5400] [< 1900] [< 1400] [< 5700] [< 1900] [< 1400] [< 5700] [< 1900] [< 1400] [< 5700] [< 1700] [< 1600] [< 5900] [< 1700] [< 1600] [< 5900] [< 1700] [< 1600] [< 5900] [< 7000] [< 2800] [< 13200] [< 7000] [< 2800] [< 13200] [< 7000] [< 2800] [< 13200] [< 22000] [< 50000] [< 86000] [< 22000] [< 50000] [< 86000] [< 22000] [< 50000] [< 86000] [< 2200] [< 8000] [< 13000] [< 2200] [< 8000] [< 13000] [< 2200] [< 8000] [< 13000] [< 2400] [< 8000] [< 13200] [< 2400] [< 8000] [< 13200] [< 2400] [< 8000] [< 13200] [< 1800] [< 2000] [< 6200] [< 1800] [< 2000] [< 6200] [< 1800] [< 2000] [< 6200] [< 1900] [< 2000] [< 6100] [< 1900] [< 2000] [< 6100] [< 1900] [< 2000] [< 6100][< 1700] [< 1400] [< 5300]

[< 1700] [< 1400] [< 5300] [< 1700] [< 1400] [< 5300] [< 2000] [< 4000] [< 8200] [< 2000] [< 4000] [< 8200] [< 2000] [< 4000] [< 8200] [< 2000] [< 4000] [< 8200] [< 2000] [< 4000] [< 8200] [< 2000] [< 4000] [< 8200] [< 12000] [< 1800] [< 16600] [< 12000] [< 1800] [< 16600] [< 12000] [< 1800] [< 16600] [< 3400] [< 3200] [< 11000] [< 3400] [< 3200] [< 11000] [< 3400] [< 3200] [< 11000] [< 20000] [< 1400] [< 31400] [< 20000] [< 1400] [< 31400] [< 20000] [< 1400] [< 31400] [< 2200] [< 7400] [< 19600] [< 2200] [< 7400] [< 19600] [< 2200] [< 7400] [< 19600] [< 2200] [< 2400] [< 7800] [< 2200] [< 2400] [< 7800] [< 2200] [< 2400] [< 7800] [< 1400] [< 4000] [< 8000] [< 1400] [< 4000] [< 8000] [< 1400] [< 4000] [< 8000] [< 8600] [< 3400] [< 14600] [< 8600] [< 3400] [< 14600] [< 8600] [< 3400] [< 14600] [< 1800] [< 1700] [< 6300] [< 1800] [< 1700] [< 6300] [< 1800] [< 1700] [< 6300] [< 10000] [< 8000] [< 20600] [< 10000] [< 8000] [< 20600] [< 10000] [< 8000] [< 20600] [< 10000] [< 11000] [< 36000] [< 10000] [< 11000] [< 36000] [< 10000] [< 11000] [< 36000] 4900 [< 2000] [< 8000] 6100 [< 2000] [< 9200] 4300 [< 2000] [< 7400] [< 10000] [< 4000] [< 17200] [< 10000] [< 4000] [< 17200] [< 10000] [< 4000] [< 17200] [< 100000] [< 13000] [< 118800] [< 100000] [< 13000] [< 118800] [< 100000] [< 13000] [< 118800] 130000 [< 50000] [< 210000] 120000 [< 50000] [< 200000] 100000 [< 50000] [< 180000] [< 4400] [< 2200] [< 11200] [< 4400] [< 2200] [< 11200] [< 4400] [< 2200] [< 11200] [< 1500] [< 1600] [< 5000][< 1500] [< 1600] [< 5000]

[< 1500] [< 1600] [< 5000] [< 1900] [< 2200] [< 6500] [< 1900] [< 2200] [< 6500] [< 1900] [< 2200] [< 6500] [< 15000] [< 3200] [< 21600] [< 15000] [< 3200] [< 21600] [< 15000] [< 3200] [< 21600] [< 2600] [< 3000] [< 9000] [< 2600] [< 3000] [< 9000] [< 2600] [< 3000] [< 9000] [< 1000] [< 2600] [< 6000] [< 1000] [< 2600] [< 6000] [< 1000] [< 2600] [< 6000] [< 1600] [< 1500] [< 5500] [< 1600] [< 1500] [< 5500] [< 1600] [< 1500] [< 5500] [< 1500] [< 2000] [< 6500] [< 1500] [< 2000] [< 6500] [< 1500] [< 2000] [< 6500] [< 1400] [< 1700] [< 5900] [< 1400] [< 1700] [< 5900] [< 1400] [< 1700] [< 5900] [< 2200] [< 3800] [< 9400] [< 2200] [< 3800] [< 9400] [< 2200] [< 3800] [< 9400] [< 3600] [< 2200] [< 9200] [< 3600] [< 2200] [< 9200] [< 3600] [< 2200] [< 9200] [< 2000] [< 2000] [< 6600] [< 2000] [< 2000] [< 6600] [< 2000] [< 2000] [< 6600] [< 1600] [< 1900] [< 5500] [< 1600] [< 1900] [< 5500] [< 1600] [< 1900] [< 5500] [< 20000] [< 8000] [< 48000] [< 20000] [< 8000] [< 48000] [< 20000] [< 8000] [< 48000] [< 2000] [< 2000] [< 5900] [< 2000] [< 2000] [< 5900] [< 2000] [< 2000] [< 5900] [< 1500] [< 1600] [< 5700] [< 1500] [< 1600] [< 5700] [< 1500] [< 1600] [< 5700] [< 1700] [< 2000] [< 5700] [< 1700] [< 2000] [< 5700] [< 1700] [< 2000] [< 5700] [< 1900] [< 2200] [< 6300] [< 1900] [< 2200] [< 6300] [< 1900] [< 2200] [< 6300] [< 1800] [< 1900] [< 6300] [< 1800] [< 1900] [< 6300] [< 1800] [< 1900] [< 6300] [< 1700] [< 2400] [< 7100] [< 1700] [< 2400] [< 7100][< 1700] [< 2400] [< 7100]

[< 2600] [< 2200] [< 6300] [< 2600] [< 2200] [< 6300] [< 2600] [< 2200] [< 6300] [< 3400] [< 8000] [< 13400] [< 3400] [< 8000] [< 13400] [< 3400] [< 8000] [< 13400] [< 3200] [< 11000] [< 17000] [< 3200] [< 11000] [< 17000] [< 3200] [< 11000] [< 17000] 3400 [< 2000] [< 7800] 4200 [< 2000] [< 8600] 3100 [< 2000] [< 7500] [< 3800] [< 8000] [< 17200] [< 3800] [< 8000] [< 17200] [< 3800] [< 8000] [< 17200]Test Method Comments lb/mmBtu ppmdv @ 7% O2 [< 0.0000000169] [< 0.0000000142] [< 0.0000000189] [< 0.0000000042] [< 0.0000000022] [< 0.0000000036] [< 0.0000000037] [< 0.0000000034] [< 0.0000000035] [< 0.0000000035] [< 0.0000000034] [< 0.0000000034] [< 0.0000000085] [< 0.000000007] [< 0.0000000099] [< 0.0000000401] [< 0.0000000389] [< 0.0000000392] [< 0.0000000048] [< 0.0000000046] [< 0.0000000047] [< 0.0000000055] [< 0.0000000048] [< 0.0000000079] [< 0.0000000052] [< 0.0000000051] [< 0.0000000051] [< 0.0000000025] [< 0.0000000022] [< 0.0000000023] [< 0.0000000037] [< 0.0000000035] [< 0.0000000036] [< 0.0000000307] [< 0.0000000103] [< 0.0000000081] [< 0.000000015] [< 0.0000000112] [< 0.0000000215] [< 0.0000000025] [< 0.0000000024] [< 0.0000000024] [< 0.0000000852] [< 0.0000000707] [< 0.0000001261] [< 0.0000002771] [< 0.0000002629]

Calculated Emission Rate[< 0.0000002668] [< 0.0000000029] [< 0.0000000028] [< 0.0000000028] [< 0.0000000955] [< 0.0000000558] [< 0.0000000704] [< 0.0000000433] [< 0.0000000325] [< 0.0000000328] [< 0.0000030897] [< 0.000002992] [< 0.0000030153] [< 0.0000031833] [< 0.0000030826] [< 0.0000031066] [< 0.0000026216] [< 0.0000025386] [< 0.0000025584] [< 0.0000030897] [< 0.000002992] [< 0.0000030153] [< 0.0000029493] [< 0.000002856] [< 0.0000028782] [< 0.0000031833] [< 0.0000030826] [< 0.0000031066] [< 0.0000025279] [< 0.000002448] [< 0.000002467] [< 0.0000026684] [< 0.000002584] [< 0.0000026041] [< 0.000002762] [< 0.0000026746] [< 0.0000026955] [< 0.0000061794] [< 0.0000059839] [< 0.0000060305] [< 0.0000402598] [< 0.0000389861] [< 0.0000392897] [< 0.0000060858] [< 0.0000058933] [< 0.0000059391] [< 0.0000061794] [< 0.0000059839] [< 0.0000060305] [< 0.0000029025] [< 0.0000028106] [< 0.0000028325] [< 0.0000028556] [< 0.0000027653] [< 0.0000027868][< 0.0000024811] [< 0.0000024026] [< 0.0000024213] [< 0.0000038387] [< 0.0000037173] [< 0.0000037462] [< 0.0000038387] [< 0.0000037173] [< 0.0000037462] [< 0.0000077711] [< 0.0000075252] [< 0.0000075838] [< 0.0000051495] [< 0.0000049866] [< 0.0000050254] [< 0.0000146995] [< 0.0000142345] [< 0.0000143453] [< 0.0000091755] [< 0.0000088852] [< 0.0000089544] [< 0.0000036515] [< 0.000003536] [< 0.0000035635] [< 0.0000037451] [< 0.0000036266] [< 0.0000036549] [< 0.0000068348] [< 0.0000066186] [< 0.0000066701] [< 0.0000029493] [< 0.000002856] [< 0.0000028782] [< 0.0000096436] [< 0.0000093385] [< 0.0000094112] [< 0.000016853] [< 0.0000163198] [< 0.0000164468] [< 0.0000037451] [< 0.0000041706] [< 0.0000033807] [< 0.000008052] [< 0.0000077972] [< 0.0000078579] [< 0.0000556148] [< 0.0000538552] [< 0.0000542745] [< 0.0000983089] [< 0.0000906654] [< 0.0000822342] [< 0.0000052431] [< 0.0000050773] [< 0.0000051168] [< 0.0000023407][< 0.0000022666] [< 0.0000022843] [< 0.0000030429] [< 0.0000029466] [< 0.0000029696] [< 0.0000101118] [< 0.0000097919] [< 0.0000098681] [< 0.0000042132] [< 0.0000040799] [< 0.0000041117] [< 0.0000028088] [< 0.00000272] [< 0.0000027411] [< 0.0000025748] [< 0.0000024933] [< 0.0000025127] [< 0.0000030429] [< 0.0000029466] [< 0.0000029696] [< 0.000002762] [< 0.0000026746] [< 0.0000026955] [< 0.0000044005] [< 0.0000042613] [< 0.0000042945] [< 0.0000043069] [< 0.0000041706] [< 0.0000042031] [< 0.0000030897] [< 0.000002992] [< 0.0000030153] [< 0.0000025748] [< 0.0000024933] [< 0.0000025127] [< 0.0000224706] [< 0.0000217597] [< 0.0000219291] [< 0.000002762] [< 0.0000026746] [< 0.0000026955] [< 0.0000026684] [< 0.000002584] [< 0.0000026041] [< 0.0000026684] [< 0.000002584] [< 0.0000026041] [< 0.0000029493] [< 0.000002856] [< 0.0000028782] [< 0.0000029493] [< 0.000002856] [< 0.0000028782] [< 0.0000033238] [< 0.0000032186][< 0.0000032437] [< 0.0000029493] [< 0.000002856] [< 0.0000028782] [< 0.000006273] [< 0.0000060746] [< 0.0000061219] [< 0.0000079583] [< 0.0000077066] [< 0.0000077666] [< 0.0000036515] [< 0.0000038986] [< 0.0000034264] [< 0.000008052] [< 0.0000077972] [< 0.0000078579]7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 Steam Output (1000 lb/hr) Total Heat Input (mmBtu/hr) Flue Gas Moisture (%)8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.87.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.87.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.98.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.8 7.8 7.9 8.812.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 Flue Gas CO2(%) Flue Gas O2(%) Flue Gas Flow Rate (scfm)12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,05212.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,31212.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,42012.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052 12.74 6.92 127,312 12.87 6.91 129,420 12.81 6.92 128,052Fuel Input Rate Fuel Type

323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 Flue Gas Temperature (F) Fuel #1316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8 323.5 315.3 316.8Units of Measure Measurement Method Fuel Input Rate Fuel #1Fuel Type Units of Measure Measurement Method Fuel #2Fuel Input Rate Fuel Type Units of Measure Fuel #3Measurement Method Fuel Input Rate Fuel Type Fuel #4Units of Measure Measurement Method Fuel #4 Other Supporting InformationEIA

Facility Code Facility Name Boiler ID NC_Riverbend Station Riverbend SteamStation Unit 4, Boiler 7, Exhaust 7A

1 4/7/2010 9:08 4/7/2010 2 4/7/2010 10:42 4/7/2010 3 4/7/2010 12:25 4/7/2010

At the tim e this testing was conducted, EPA was allowing the use of a combined M26A/CTM033 sampling train for collection of HCl, HF and HCN Run Number Test Start Date Test Start Time Test End DateMeasured Value (ppm) Basis (Wet or Dry) Test Method Used

10:15 [< 0.002] Dry U.S. EPA Conditional Test Method 033 (CTM-033) 11:51 [< 0.002] Dry U.S. EPA Conditional Test Method 033 (CTM-033) 13:31 [< 0.002] Dry U.S. EPA Conditional Test Method 033 (CTM-033)

At the tim e this testing was conducted, EPA was allowing the use of a combined M26A/CTM033 sampling train for collection of HCl, HF and HCN Hydrogen Cyanide Emission Test Results Test End TimeData Flag (ADL,

BDL, DDL) Test Method

Comments DLL DL based on the MDL [< 2.26263531480886E-06] 9.4 12.83 DLL DL based on the MDL [< 2.12837144312058E-06] 9.6 12.87 DLL DL based on the MDL [< 2.31875208481173E-06] 9.1 12.82 Calculated Emission Rate (lb/mmBtu) Flue Gas Moisture (%) Flue Gas CO2(%) Steam Output (1000 lb/hr) Total Heat

Input (mmBtu/hr)Fuel Input Rate Fuel Type Units of Measure Measurement

Method Fuel Input

Rate 6.99 124,851 321 6.94 125,233 323 6.95 124,826 325 Flue Gas Temperature (F) Fuel #1 Flue Gas O2(%) Flue Gas

Flow Rate (dscfm)Fuel Type Units of Measure Measurement

Method Fuel Input Rate Fuel Type Units of Measure Measurement

Method Fuel Input

Rate Fuel #2 Fuel #3Fuel Type Units of Measure Measurement

Method Matrix spike recoveries for HCN reported at 48% and 52% indicated that the reported values may be biased low. Matrix spike recoveries for HCN reported at 48% and 52% indicated that the reported values may be biased low. Matrix spike recoveries for HCN reported at 48% and 52% indicated that the reported values may be biased low. Fuel #4 Other Supporting InformationMatrix spike recoveries for HCN reported at 48% and 52% indicated that the reported values may be biased low. Matrix spike recoveries for HCN reported at 48% and 52% indicated that the reported values may be biased low. Matrix spike recoveries for HCN reported at 48% and 52% indicated that the reported values may be biased low.EIA

Facility Code Facility Name Boiler ID NC_Riverbend Station Riverbend SteamStation Unit 4, Boiler 7, Exhaust 7A

Run Number Test Start Date Test Start Time Test End DateMeasured Value (ppm) Basis (Wet or Dry) Test Method Used Test End Time Hydrogen Chloride Emission Test ResultsData Flag (ADL,

BDL, DDL) Test Method

Comments Hydrogen Chloride Emission Test Results Steam Output (1000 lb/hr) Total Heat

Input (mmBtu/hr) Calculated Emission Rate (lb/mmBtu) Flue Gas Moisture (%) Flue Gas CO2(%)Fuel Input Rate Fuel Type Units of Measure Measurement

Method Fuel Input

Rate Flue Gas Flow Rate (dscfm) Flue Gas

Temperature (F) Fuel #1 Flue Gas O2(%)Fuel Type Units of Measure Measurement

Method Fuel Input Rate Fuel Type Units of Measure Measurement

Method Fuel Input

Rate Fuel #2 Fuel #3Fuel Type Units of Measure Measurement

Method Fuel #4 Other Supporting InformationEIA

Facility Code Facility Name Boiler ID NC_Riverbend Station Riverbend SteamStation Unit 4, Boiler 7, Exhaust 7A

Run Number Test Start Date Test Start Time Test End DateMeasured Value (ppm) Basis (Wet or Dry) Test Method Used Hydrogen Flouride Emission Test Results Test End TimeData Flag (ADL,

BDL, DDL) Test Method

Comments Calculated

Emission Rate (lb/mmBtu) Flue Gas Moisture (%) Hydrogen Flouride Emission Test Results Steam Output (1000 lb/hr) Total Heat

Input (mmBtu/hr)Fuel Input Rate Fuel Type Units of Measure Measurement

Method Flue Gas Temperature (F) Fuel #1 Flue Gas CO2(%) Flue Gas

O2(%) Flue Gas

Flow Rate (dscfm)Fuel Input

Rate Fuel Type Units of Measure Measurement

Method Fuel Input Rate Fuel Type Units of Measure Measurement

Method Fuel #2 Fuel #3Fuel Input

Rate Fuel Type Units of Measure Measurement

Method Fuel #4 Other Supporting InformationEIA

Facility Code Facility Name Boiler ID NC_Riverbend Station Riverbend SteamStation Unit 4, Boiler 7, Exhaust 7A

Run Number Test Start Date Test Start TimeMeasured NO (ppm) Test End Time Test End DateMeasured NO2(ppm) Basis (Wet or Dry) Test Method Used NOXEmission Test ResultsData Flag (ADL, BDL, DDL) Test Method Comments (lb/mmBtu) Total NOXCalculated Emission Rateppmdv @ 7% O2 Flue Gas O2(%) Calculated Emission Rate Steam Output (1000 lb/hr) Total Heat Input

(mmBtu/hr) Flue Gas

Moisture (%) Flue Gas

CO2(%)Fuel Input Rate Fuel Type Units of Measure Measurement

Method Fuel Input

Rate Flue Gas Temperature (F) Fuel #1 Flue Gas Flow Rate (dscfm)Fuel Type Units of Measure Measurement

Method Fuel Input

Rate Fuel Type Units of Measure Measurement

Method Fuel Input

Rate Fuel #2 Fuel #3Fuel Type Units of Measure Measurement

Method Fuel #4 Other Supporting InformationEIA

Facility Code Facility Name Boiler ID NC_Riverbend Station Riverbend SteamStation Unit 4, Boiler 7, Exhaust 7A

Run Number Test Start Date Test Start TimeTotal Dissolved Solids (mg solids/liter) Total Suspended Solids (mg solids/liter) Test End Time Test End DateTest Method Used Data Flag (ADL, BDL, DDL) Constisuent Emission Test ResultsTest Method Comments Fuel Input Rate Flue Gas Temperat ure (F) Flue Gas Flow Rate (dscfm) Steam Output (1000 lb/hr) Total Heat Input

(mmBtu/hr)Fuel Type Units of Measure Measurement

Method Fuel Input Rate Fuel Type Units of Measure Measurement

Method Fuel Input Rate Fuel #1 Fuel #2Fuel Type Units of Measure Measurement

Method Fuel Input

Rate Fuel Type Units of

Measure Measurement

Method Fuel #4 Fuel #3Other Supporting Information