CnmpoMnt Dala**~**

1X1o" 1x 1d' -' II 1X1o' 

# _ , 

# ..**~** 7X1o' ..J 3x1o' 0 111.40 21.00 28.80 

### sa 

### no


# ...........

VES 006200

## Calibrati on Update R ep o rt

· S amp le Name : CALm 

### S ml 0 80902

D at a File Nam e : C:\ PF

A KNET\D ATA\AN1 0 N\1 0 -23 _AA SOOJ . DXD Method File Name : c:\peak:net\roethodlmelhod\120anionsmet Schedul e File 

### N an 1 e : c:\peala>ellschedulelschedule\schedule\l20anions\200 8 \l2Qani on0902. s cb Date Time Co ll ecte d : 2008-09.02 4:23 : 48 PM Calibratio n Date : 2008-09.02 4:32:58 P M Sy s1em Operator : LLE 

### Peak lnfonnation : All Components P eat# Co mpon e n t N am e Rete nti on Ti lll e 

### Cal Re sponse Ca l R esponse (Prev ioU$ ) (M ea sure d) 

### 0 (null) 

### 0.00 0 0 C

hloride Ni tri te B

r omi de 

### Nittate Phos p hate Sulphate 

### CALIB STDJ 0809()2

16.0 14.0. 12 . 0 10.0 

# "' 8 . 0 

# "' 6.0 

### 4.0 2.0



# o,

- 2 . o L . 

### ' 0 1.0 2.0 3 . 0 

### 4 .0 5 .0 6.0 7.0 8.0



## . . .

Pa.e;e I o f I 

### Ca l R espo nse (N ew ) 0

' 

### 9.0

O.M'retli D.ltc: 2008-09-Ql

Cu«cilt Time : 1 &.32;59 

### VES 006201

## Cali b r atio n Up date Report Samp l o Nome: CALmSTD2 

### 080902.

. Data Flit 

### Name : C:\l'EAKNE:r\DA TAIANlON\1 0-23

_AAT002..DXD Method File Name: c:\peaknet\methodlmctbodll 2 0unlons.mct Sched u le File 

### Na . = : c : lpe alo.let\scbedule\schcdulc\.wl\cdulc\ J20anionsi2008\J20union0902 .sch Date Time Collected : 2008-09-02 6: 07 :3 8 PM Cali bration Date: 2008-09 - 02 6:16:16 PM Systcan Opcr310r : LLE 

### Peale lnfonnalion : AU Componeots Peak #I Compone.nt Name Reteotioa Tlmt 

### Col Response Cal Rt:sponse**(l'r~us )**  (Musured) I Fluoride 

### 1.02 3572 3816 2 Chloride 1 . 62 4822 3649 3 Nitrite 1.9 8 

### 4899 5334 4 Bromide 3.07 2296 23 92 

# s Nilmle 

### 3.53 6040 6399 

### 6 Phosphate 5 . 8) 21162 23257 7 

### Sulphate 7.82 3 305 2538 

### CALIB STD2 080901 

### 16.0 f 14.0 12.0 

# JO.O t 'i 8.0 6.0 

# ::1 2 3 

### 4 

# s 6 

### I I I 

### I I 

### -2.0 0 

### 1.0 2.0 3 . 0 

### 4.0 5.0 6 .0 7 . 0

:**~kNt:RtE** S . I Od**f'a ~~:s**  1 of l Ca l R .. ponse ( Now) 

### 38 1 6 3649 5334 2392 63 9 9 23257 2538

7 

### I 8.0

C llm nl Dm: 2008.00.02 C

11ncnt 1""- : 1 8 :- 16

: 18 

### VES 006202

## Calibration Update Report

· Samp le Name : CALIB S TD3 081)902

l>ata . File Name: C:\PEAKNEl'ID ATA \AN IO N\10-23

_ AATOOJ.DXD Melhod File Name: c:\peaknet\method\method\120anioos . rnei Schedule File Name : c:\peaknet\scbedule\schedule\scbedulell20anioos\20081 1 20anion0902 . seb Da te Time Collected : 2008-09-02 6: 17 :07 PM Calibnlti on Date : 2008..09-02 6 :25:47 PM System Operator : L LE Peak Information : All Components Pea k # Component N am e R ete nti o n Time Cal Response Cal Respo1 ou (Previous) (Measund) I 

### Fluoride 1.00 33292 35210 2 

### Chloride 1.62 38508 37713 3 Nitrite 1.9 7 31469 33632 4 

### Bro mide 3.05**30~;27** 

### 33099 5 

### Nitrate 3.52 . 60219 64144 6 Phosph ate 

### 5.83 60108 63741 ? 

### Sulphate 

### 1.n 103170 107881



### . 

### CALIB STD3 080902 16.0 14 . 0 12.0 10.0 

# . 

# "' 8 .0 "- 

### 6.0 4 .

0 I 2 3 4 5 

### 6 2.0

## ~

## ~ 

# i I 

## ), I



### 0 

# - .. . -2 .0 0 1.0 2.0 

### 3 .0 4 . 0 5.0 6.0 7 .0



### . ..

# ~~ :Peak.Net-S E S . IOd 

### . Ca l Res p onse (Ne w

) 35210 

### 3n13 33632 33099 64144 63741 1078 81

7 I 

### .----..__ 8. 0

Ottrent Date : 2008 ·09-0:l <.\ttTeM Time.: 1&2.5:49 

### VES 006203

## Calib r ation U p date R e port Somp l e Name : CALIB STD4 080902 Data File Name: C :\PEAKNE'I\DA T A\ANlON\10-23

_AAS004.DX D 

### Method File Name: 

### c:\peaknet\medtod'.notbod\1 2 0anions.met Sc hedule File Name: c:lpeakne1\scbcdu l e\scbcdulc\9<:bedule\120anions\2008\l20anion0902 . . sch Dat e Time Coll ected: 2008 - 09..()2 6:26 :38 PM Ca l ibratio n Date : 2008-09..()2 6:35 : 19 PM SyslO!n 

### Operator : LLB 

### Peak lnfonnaiion : All Components Peok II 

### C omponent Na- !Utflltloo TIJne Col 

### Rospoll$0 Cal 

### R<Spoll$0 2 3 4 

### 5 

### 6 7 

### 8 Fluoride Chlor ide 

### Ni trite B ro. mide 

### Ni lmte Phospha te Sulphate



### 16.0 14.0 

### 12.0 10 . 0 8.(> 

### 0 . 98 1.60 

### 1. 97 3.03 

### 3 .48 5 .7 8 

### 7.73 (l'revions ) (M..uurc:d) 

### 196784 192 132 199137 1926 82 

### 184267 18287 8 1 689 19 164438 340458 328604 

### 35 1 467 3 41755 5782 45 560950 CALJ1J STD4 080902

6 . 0 2 3 4 6 8 

### Co l R<spoJUe (New) 192 1 32 192682 

### 182878 164438 328604 341755 

### 560950

I 

# l S I 7 1

# :~ . . Jl-U_}J\ '----- · ---' I

# '--~~~~~-::-::-- 0 1.0 

### 2.0 3.0 4 .0 

### 5.0 6.0 7.0 8 . 0

h M.elor i C\ltRnt Otoe :**4~9-02** CW'rem. T ime: 18 ;l.S:l0 

### VES 006204

## Calibration Update Report Samp l e Name : CALJB S TDS 080902 D ata File Name : C:\PEAKNE 'I\I) ATA\ANJON\l l l-23



### _AASOOS.D XD 

### M

ethod File N.ame : c :lpeaknet lm ethod\method\120anions.met Schedule F ile Name: c:\peaknet\sch e dule\scltedulclscbedulc\120anionsl200&\120anion0902 .scb 

### Date Time Collected : 2008-09-02 

### 6 : 36 : 08 PM Cahl>ration Date: 

### 2008 - 09-02 6:44:51l'M 

### System Opera tor : LL E Peak lnfonnation : 

### All Components P e ak# Compo n ent Name Rete nti on Tinte 

### Ca l Response (Previous) Ca l 

### Respon se ( M easatred) 

### Cal Response (New) ·**----- -·** **--- ------** **~- --** **--- ---** **----** 2 3 

### 4 5 

### 6 7 

### 3 Fluoride Chloride 

### N i tri t e Bromide N i trate Phospbalc Sul phate 

### 0 . 98 1.60 1.97 

### 3 . 02

. 3.45

5.15 7.68 

### 4 00612 404 1 66 332606 3 40805 

### 690717 71 8726 1163556 

### CALIB SID 5 080902 16.0 1 4 .0 

### 12.0 10 . 0 2 3 6 4 I 

### M 1

# ~

# ~ t

# '--**-.../ ~**  I**~~--.~ 1**  '-- '- . 

# V**!--"7--:-~ --** **--..,.,,.--- ::-** **.** 0 L O 2.0 3 . 0 4.0 

### 5.0 42378 7 426352 

### 406593 358816 

### 723267 756481 1224 3 68

3 I 423787

426352 

### 406593 3 5 8816 72326 7 7 5 6481 1 224368

7 I 

# '---- Jl

6.0 

### 7 . 0 8.0

Cw-rent D a te : lootl -09-02 Cutren t Till'lt' : 18:44 : $1 

### VES 

### 006205

## Calibratio n U pdat e Report S ample Nam e : CALIB STD6 080902 Data File Name: C:IPEAKNE1\DATA\ANION\ 1 0-lJ

_ AAS006.DXD Method File Name:**c:lpeaknet\mel~ od\** **met od** **0anio niel**  Schedule File 

### Name: c:lp eaknetlscbedu l e \s chc dul c\sc hedu.lc\120anions\2008\ 1 20anion090 2 . sc h Dat e Time O> Uec t ed : 2008-09-02 6: 45 : 41 PM Calib<a ti on Dat e : 2008 -0 9-02 6 : 54 : 2 2 PM 

### S}'$\cm Op e ra

toc: LL.E Peak lnformal.ioo : All Components Peak # 

### Co . mp o nes1 t N am e Rete nti o n nmc Cal Response Ca l RespGnse ( P r e vious ) ( Mea s llrtd ) 2 Fl u ori d e () . 98 

### 6S09S6 63839'7 3 Chlori d e 1. 6() 6622 1 5 

### 64799 1 4 N i tri te 1. 9'7 6 1 895 4 609 174 

## s Br o mide 3.02 5 5 1959 54067 0 6 N i trate 3 .4 3 I 1 2 9195 11 0381 2 7 Phosph ate 5.70 1174736 11 5061 2 & Sulphate 7 .6 5 1 89 3428 1 8474 2 3 CA.LIB STD6 080902 1 6 .() 2 1 4 . () I 

### 6 I 1 2.() 4 

### I 10. 0 

# s 7 

### I I 

# "' 8 .0 

# .. 6 . 0 

### 4. 0

# ~ 2 . 0 I 

# \. I 0 \... ·2.0 

### 0 1.0 2 . 0 

### 3 . 0 4 . 0 5 .0 6.0 7.0



## ...

: fl dkNe• · Se s.J o d PD J:l: I of l 8 

### I Gal 

### Respo n se ( N

ew ) 63 8 39'7 

### 64799 1 609 174 5 40 67 0 11 03812 I 150612 1 8474 2 3

8 . 0

O. rt<on l O.c- :**2** Cwre ot Tirnc: 

### t t :.s4 aJ 

### VES 006206

### S amp l e Anal ys i s R e p ort Sample N am e : I CB Data F ile 

### N am . e : C:\PEAl<NE T\DAT A

\A

NI ON\ 1 0-2 3

_ AASU07 . l>XD Detecto r Type : D X- 1 20 Me th od F ile ·Name : c:lpeal<net\method\metbod\120anions . met Schedule Fil e Naine : c:lpe alcnet\..:hedule\•cbedule \scbedul e \l2()anions\2008\120ani on0902 . sch Da t e Time Collec t ed : 2008-09 - 02 

## 6:ss: II PM 

### . Sys t em Operator : LLE Cah'briltion Da t e : 2008-09 - 02 6:54:22 PM Calibration Type : 

### EXTERNAL Component Amount Units : mg/L D i

lution Factor : 1.00 Peak Information : All Peaks P e• k # 

### Co mp o aeut Na m e Amo unt (m g/L } 

### Retenti on Time P eak Area

ICB 16 . 0 14.0 12 . 0 10 . 0 V> 

# s.o :1.. 

### 6 . 0 4.0 2.0

0

- 2 . 0

.**·~ ·**  

### ·· - · ... . 

### 0 !. 0 

### 2.0 3.0 4 .0 

## s.o 6.0 7 .0

. ..

hRelof l 

### P eak H eig ht

8 . 0

OlmM [hte : 2008-09-03

eurrecu fim e: · : 13:23 :02 

### V E S 

### 006207

### S amp le Anal y sis R eport S a m p le Nam e: I CV 

### Data File N ame: C:\P EA KN E 'ru>ATA IANIO N\IG-Z3

_AAR008.DXD**Dc~ tot** **·** 

### Type : DX-120 Me thod File N ru ne : c: lpe akne t lme U!Od\me th odll 2 0•ni o u s.met Sched ul e F i l e Name: c:lpeaknet\scbedulelsched u le \<;c b cdul e\120 ani ons l2008 11 20aru on0902 . s ch D ate Ti m e Co ll ected : 2008 · 0 9-02 7 : 04 : 44 P M S )'l!iem Operato r : L LE Calibrati on Date : 

### 2 0 08-09-02 6:54 : 22 PM 

### Calibration Type : EXTERNAL Com po nen t Amount Units : mg/L Dilution F actor : 1.00 P eak lnfoanatlon :All Peaks P ... t 

### # C o mpoae ot N a me Am o aa t ( m g!L) Reto11 tio D Tim e 

### l 0 . 0000 0 . 80 2 

### F lu oride 3 . 0200 0 .98 3 Chlor i d

e 4 . 5 195 1. 60 4 

### Nitri t e 2 .28 6 9 

### 1. 97 

## s Bromi de 

### 8 . 99

63 3 . 0 3 6 Nitrate 

### 3. 00 23 3 . 47 7 P hosphat e 

### 9 . 0262 

### 5 . 15 8 

### Sulphate 18 . 0669 7:7 0 JC V 

### l 6.0 I 1 4 . 0 1 2.0 10 . 0 8 . 0 2 3 

### 6 V> l 4 I 

# ,. 6 . 0 

# :lc I 

### 5 7 4.0 

# l I 

### 2. 0

0 

### ·2.0 0 1. 0 

### 2.0 

### 3.0 4 . 0 

### 5.0



### . ..**lo ti** 

### ---**--~---- --** **-- --** **-- --** **~--** 

# .

6.0 Pe alc Arta**Peai<U~ lrt** 



# -

-- 1 2 0

5 0 2 03 2 3 0 88 5 9 61128 3

09234 

### 6 29 50 2

98

7 61 486 1 3 

### 2

6061 5 37 66 2 52 64 2 4 60746 

### 5

48 537 393 74 892603 52088

8 I



### 7 . 0 8.0

C\ltrclrt .O..Ie ; 2Q08.09r..02 CUn'en tTi.me : 1 9 : 1;5!'2 6 

### V E S 0062 0 8

### Sample Analysis R eport Sam ple Name : QCS 1CMIX6 o a .. File Name: C:IP£AJOIIE1\DATA\ANION\JQ..l3

_ AAQ009 .D XD 

### Detector Type: OX-120 Method l'ile Name :**c:~et\method\method\1 20an** **ioruo met**  

### Schedule File N ame: c : \pealmet\sehedule\scbedu l elsclledule\120nni o ns 12008\120anion0902.seh Date Time Collected : 2008..09-02 7 : 14:45 PM Sys:em**~ralor :**  

### LLE Calil>.ratioo Date : 2008-09 - 02 6:54:22 PM Calibration Type : EX'l"ERNAL Compontnl Amouol Unl:s : mgiL 

### Dilution Factor : LOO 1' .. 1< 

### Information : All Peaks 

### Peak II Component N ame Amoun t (me/L) Retention T ime



# - .... . . I 

### 0.0000 

### 0.80 2 F luoride 2.0503 ' 

### 0.98 3 Chloride 5 . 0858 1.60 4 

### Nilrite 2.7528 1.97 5 

### Bromide 10.0092 3.03 

### 6 Nitrate 2.4422 3.48 7 

### Pbospb•te 

### 4 . 8332 5 .7 8 8 Sulphate 

### 15 . 1582 

## 1.n QCSTCM!X6 16.0 14.0

. 12.0

10.0 8.0 3 4 

## 'fi I 5 6 

### 6.0 

# :LL I 

### 4 . 0

# '"'r~ 7 2.0 I



### 0

- 2.0 0 1.0 

### 2.0 3.0 

### 4.0 S.O 

### 6 . 0



# .. 

# Ill : PeaJdfa..Se S.IOd Peak Are• PeakJleigbt 

### 11310 1906 

### 205833 37945 350<122 65825 3630SO 57538 29 1 326 4034 1 423616 49110 283356 20368 7

43170 43307

8 I



### 7.0 8 . 0

C\tJ:rCIU I.MU : 1()()3.09.(Jl C'lmetll T"tmc- : 1 9:23:23 

### VES 

### 006209

## Sam pl e Analysis 

## Report Sample Nome : MllLANK Data File Name : C:\PEAJOIIET\DATAIANION\JO-l3

_AA0018.DXD**Dctcct~rType:** 

### DX-120 Method File Name : c :lpeaknet\methodlmeU10d\120unions.met Schedule File Name: c:lpeabwt\scbedulclsehedulelscbedulo\120anionsl2008\120anion0902 .sch Date Time CoUccted : 2008-09-02 8:39:41 PM Sysu:m Operator : LLE Calibra tion 

### Date : 200&-09 -0 2 6:54 : 22 PM GaUbnttion Type : EXTERNAL Compoocot A.moun1 

### Units : mgiL 

### Dilution Factor : 1.00 Peak 

### tnfo1'11)8tioo : All Peaks

Puk # Compo nent Name Amount {mg/L) Retention Tun e Peak Area



# · - - · "- - - · - · - ··



### MBLANK 16.0 1 

# . l<lOf 

# . 12.0 10.0 

# "' 8.0 

# ... 6.0 4.0 2 .0

0 -2 . 0 1- . 0 1.0 2 ,0 3.0 4. 0 

### 5.0 6.0 

### 7.0



## . 

# -**P~w;** I ot l Peak ffeigllt



### 8.0

Clll'lolll DoJc - : 2008..()9...03 Cur;mc Time : 1 6 :

04:29 

### VES 006210

### Sam pl e Ana l ysis R ep ort Sam pJ t Name: MSPIKE Dota F Ut Nam e : C :\P EA KNET\D A T A\ANION\JO..l3

_AA00 19.D XD Detector Type : D X ·l 20 · Met ho d 

### File Na m.

e: 

### c : lpeatnct\method\mcthodl l2 0unions.mct Sehed u le File 

### Name : c:\peaknet\sched\lle lsc hedulc \scho:du le\120anio n s\20 0 8\ 1 2 0anion0902. sch Dat e T ime Collected: 2008 - 09 · 02 8 : 49 : 1 2 

### PM System Operator : LLE Ca l ibratio n 

### Date : 2008 - 09..02 6:54:22 PM Calibratio n Type : 

### EXTERNAL Compoo"" l Amount Units : mgiL Dilution l'aciOr: 1.00 Peak lnfotmalion : All Peaks



### Peak It 

### Compo a ent Nam e Amount (m&IL) 

### Rttenllon Time Peak Arto P e a k Htig;b t



# ------ ---- ---- ------ ---- ----- --- -- -- ------------ ---- - - I 2 3 4 

# s 6 

### 7 

### 8 0.0000 0.80 

### 8185 l'lu oride 

### 2. 0081 0 .98 20 1406 Chlori de 

### 3.1331 1. 60 

### 210535 N ibite 1.4848 1.97 19Q088 Bro;nide 

### 5.9109 3. 05 

### 170328

· N itrate 

### 1.9856 350 3411)57 Phosphate 

### 5 . 9598 5.78 353592 Sulph at e 

### 12 . 01 28 7 . 72 

### 583476 /lfSPIK£ 

### 16

. 0 

### 14.0 12.0 · 10 .

0 8. 0 

### 6. 0 2 3 4 6 8

# :~**rj~U_jj___)L__)\___** ·2.0 .__ __ _ 0 1.0 

### 2.0 0 ...... M '' 

### 3 .0 

## - · · .,-s.::-o ----: 6 :-:: .o,..--"'?."'o----:s::-:.a .-- 1369 37977 . 

### 3 9816 30353 24663 40804 25877 

### 33899



# liJ : PM N tt.SE S.I Od**lo'~lo l**  t\IUC 111 Dcue : 200! • 09 -02 Curtcn t Ti " : 2 0'".S7:A9 

### VES 0062 1 1

### Sample Analysis Report Sample Name : B-BLANK Data File 

### Name: C:IPE AKNET\D AT A \A NIO N\10-23

_AAN020.DXD Detector Type: DX-120 Method File 

### Name: e:lpealmel\methodlmeehod\120aniQns . .met Schedule File Name: c :\pealcnetlscl!edulelsched ule\sche du t e\120anionsl20081!20anion0902 .sch Date Time CoUected · : 2008-09-02 8:58:38 PM System Operator : LLE Calibration Date: 2008-09-02 6:54:22 PM**Calibcati~m** 

### Type : ExTERNAL Component Amount Units : mg!L Dilution Facto . r : 1 .00 Peak Information : All Peaks Peak# Component Name 

### Amount (rng/L) · Retention Time



# ---·· · -··· .. . . I 

### fluoride 0.2742 1.02 2 0.0000 1.13 

### 3 Chl ot'ide 0.3906 1'.62 4 

### Nitrite 0 . 9378 L.97 5 

### 0.0000 3.28 6 

### Sulphate 2.0213 7.77 

### B -BLANK 

### t6oi 

# I 14.0 12 .0 

# I I O

.otl) 

### 8.0 :1. 

### 6.0 4.0 

# • 1

# ':**~** 2.0

# -~ \

0 -2.0 

# - 0 

### 1. 0 2 . 0 3.0 4 .0 5.0

...**I** of I 

### 6.0 Peak Area P eak Height 

### 22911 5522 51871 9269 23390 5186 117368 19051 7394443 645188

88524 5299

6 I**~** 7 . 0 

## .. 8.0

Current J)w: : 1008-09 -Ul Cune ot 'Time: 21 :01:20 

### VES 006212

## S ampl e A n a l ys is R e por t Sample Name : Jl.Sl' IKE D ata F il e**m~:** C :IPEAKNn\DA T A\AN I O NU0-23_AAN 02 1. DXD Detector Type: DX-120 M ethod Fil . e Name : c:'opeaknet\method\m e thod\120anions .met Schedule File Name: c:'l!eaJ<net\schedul e\scbcdule\<ehedule \12 0aniol'ls\2008\120anion0902.sclJ Da t e Time Collected: 2008-09-02 9:08:08 PM Systt111 Operator : LLE Calibration Date : 2008-()9 - 02 6:54:22 P M Calibration Type : BXTERNAL Comp<>net>l Amowi t Units : mgiL Diluti on Factor : 2.00 P eak lnfonnation : 

## Ali Peaks P eak# Co m ponent N ame A mo unt (mg/L) R e tenti on Time Pea k Are a P e ak :Hel gb t



## - -- 

## - I 0.0000 0 . 80 

### 1904 4 91 2 Fluoride 0.6023 1. 02 25629 1066 

### 3 0.0000 1.42 22289 2 782 4 Chlori d e 9 . 9845 1.62 343581 62652 5 Nitri te 1 .6512 1.98 10258 1 1347 1 6 B r omide - 3401.0721 3 . 15 24280884 1 857692 7 Sulphate 4 .6584 7 . 78 103512 601 3 

### B-SPTKE . 16.0 r 

### ' 14.0 

# I 12.0 10.0 8.0 4 

# \ "' I :1. 6.0 

# lJ 4.0 5 

# ( 7 2.0 I I I 

### '"'--- 0 1-- ·**·2.0 ~_** _ _ ,

0 1.0 2.0 3.0 4.0 5 .0 6 . 0 7 .0 8 . 0

. ..

Current OILtc : al08 · 09-01. Pu.e I oft Current Time :**~1 Sl**  

### YES 0 06 2 13

### Sample An a.l y sis Report Sam p le Name · : AH3046 Data File Name: C:\l'EAXNI!;'N>ATA\AN I ON\ 10-23

_AAM022 .0 XO Detec tor 

### Type: DX - 1 20 Melhod F ile Name : c:\peaknet\method\method\120anions .met Schedule File Name: c:\peaknetlscbedulelschedulelschedule\120anions\2008\120anion 0902 .sc h D ate Time Collected: 2008-09.{)2 !) : 1 7: 40 PM System Operator : LLE Calibration Date : 2008.{)!).{)2 · 6:54 :22 PM Calibration Type : EXTERNAL Component Amount Units : mg/L Diluti o n Factor: 25 .00 Peak lnfoml>tion : All Peaks

P ea k # Component Name Amoun t (mg/L ) . R ete n ti on Time 1 

### 0.0000 

### . 0.80 2 

### Fluoride 2.9994 1.00 3 Chloride 133.7 5 99 1.62 4 Nitrite 2.4629 1.98 5 Nitra t e 54.8229 3.48 6 Phosphat e 10 .684 9 5.8 3 7 Sulphate 48 .2226 7.77 AH3046 16.0 14.0 12. 0 10 . 0 

### 3 I t/.1 8 .0 :1. 6 .0 5 I 4.0 

# _A 2.0 I 2 4

___ I 

## _!---.J**~** l 

### 0

- 2.0



## - · -- - - - 

## o · 1.0 2.0 3.0 4 .0 5 .0 

# .. .

• :

# ~~ct.S£S**.1 0c;l**  •**Pa ~lqf** **l** 

### 6 l 

### 6.0 Peak Area PeakHelgbt 2187 46 0 7 3 53 1633 369849 85362

7839 1 387 378405 43746

15 3 14 1152 84033 4931



### .

7 

### )--._ 7.0 8.0

C1lntnO Date: 101)8:..09 - 02 C1lnenl Time : 21:26d 7 

### VES 006214

## Sample Anal ysis Re po r t Samp l e Name : AH3046 Data File Name: C :IPE AKNE'I\DATAIA NION110-23

_ AAQ016 . D XD Detector Ty pe: DX - 120 Method File Name : c:\peaknet\m e1bod\metbod \ 12 0anions . me t Sched ule File N ame : c : \peaknet\s<:bedule\sc b edti le\s c hedul e \120aniOns\2008\1 2 0anion0902.sch Date T ime Collected : 2008 - 09-02 3 :40:48 

### PM Sy s tem Operator: 

### LLB Calibration Date: 2 008-09-02 12:27:39 

### PM Calibration T ype: EXTERNAL 

### Component Amooru Units : mgiL Dilutioo Fac t or: 100.00 Peak Infonnation : All P e aks Peak # 

### Cornpo nent Name Amou nt (mg/l;) Retentio n Ti m

_ e



## .. 

# -

.. 

# ·- - ·-· ·- · I Fluoride 5 . 0157 1. 03 2 Chloride 130 .7067 1.62 3 Nitrate 56 .6328 3 . 55 4 Pbospl1llte 17 .23 20 

### 5.85 5 Sulphate 46.0796 7. 80 AH3046 16.0 1 4 . 0 12. 0 10. 0 

## 'a 8 . 0 6 .0 4 . 0 2 3 2 .0 

### I I I 

# f--__l__j\_ 0 -2.00 

### 1.0 2 . 0 3 . 0 4.0 5.0



### . ..**P~lofl** 4 I 6.0 Peak Area**P~k elght**  4046 

### 396 

### 84m 17770 86706 10494

3004 267 15715 1058

5 I 7.0 

### 8.0

C urrtnt DMt : 2001.00-02 CuneaiT'tme : I M9!3 1 

### VE S 

### 006215

## Sam p le A nalys i s 

## Rep ort Sample Name : AH3047 ·Data File Name: C:IPEAKNET\DATA\ANION\ 1 0-23

_ AAM0 2 3. D XD 

### Detector Type: DX-120 Melhod File N ame: c:lpeaknet\melhod\method\J20aoions.met Schedule File Name: c:lpeaknet\schedule\sclledule\schedule\I20anionsl2008\120anion0902 .scb Date Time Collected :**2008~9-02** 

### 9:27 : 06 PM System Operator : LLE Calibration Dat e :**2008-09~2** 

### 6:54:22 PM Ca

. lib<"ation Type : EXTERNAL Component Amount Units : mg/L Dilu ti on factor: 25.00 Peak Inforination : AU 

### P eaks l'e.alt # Component 

### Na m e Autouu t (mg/L) Retentio n 

### T ime
I 

### 0.0000 0.80 2 

### Fluoride · 4 . 4583 1.00 3 Chloride 17 1. 5442 1.60 4 

### Nitri t e 3.0412 1.97 5 Nitrate 

### 73 . 0 177 3.47 6 

### Phosphate 7.6813 5.83 7 Sulphate 44.8596 

### 7:17 AHJQ47



### . 16 . 0

14.0 12 .

0 3 

### 10.0 

### 8 . 0 5 (/) I :1. 

### 6.0 

# l_.

# ~ 4 .0 2 . 0 I 2 I I 

### 0

· 2.0**--·** 

### 0 1.0 2 . 0 3.0 4.0 

### 5.0

.

# ~~ :

# Pe~k~et·SE S. l(ld 

### 6 I 

### 6 . 0 l'eskArea 

### PeakBeigbt



## - 2458 467 13232 32 25 483162 9%97

10825 1465 511346 60377

8146 597 17493 4573



# .

7 I**~** 

### 7.0 8.0

C\IITMt D :n t: 2008-09 ·01 Curre.""' t Time . : 2: 1 ::OS :

48: 

### V E S 0 06 2 16

# ., S ampl e AJJ aly sis Report Santp l t Name: AH304 8 .. _ __ • • _. . . Data File Name : C:IPEAKNE'ru>ATA\ANION\10.23

_ AAM024.DJCD De!ectorType : DX - 1 20 , Metl10d File Name : c:\peaknet \melbodlmethod\120aoions.met Sched ule File Name: e:\peaknet\sehcclulelschedulc\schedule\ t20anions\2008 \120aoiol10902.sch 

### Dote rune Collected: 2008-09-{)2 9 : .36 :3 8 

### PM System Operator : 

### LLE Ca. l ibnt ion Date : 2008-09-02 6 :54 :22 PM Calibnilion Type : llX1'EJ!NAL Component Amount Uruts : 

### nw'L**lu~on** Fa<:tor : 25 . 00 Puk illformalion : All Peaks

PukN Co mponent Name Amo ..nt (mg!L) Retention Time Peak Area PeakHeigbt



# .. 

# -- L 0.0000 0.80 2707 4 86 2 F luor i de 20.980 1 1.00 80329 15354 3 0 . 0000 1.37 6681 835 4 C hloride 297.81 41 1.62 896549 201154 

# s Nitrite 2.6 801 .2.00 8960 1271 6 Brom i de 5 . 1347 3.07 3 807 580 7 Ni trate 109 .9700 3.45 790604 89 7 82 8 Phosphate 11 . 856 5 5 . 8 3 18 11 2 1378 9 Sulphate 107 . 1758 7.75 199185 11556 

### AH3 1J48 16. 0 14 . 0 12.0 7 10.0 l 

# "' 8 . 0 

### 2

# ~ :::1. 6.0 4 . 0 9 2 . 0 8 I

0 113

# LJ~ I 

# J \. J..... I 

## J**~** -2.0 0 1.0 2.0 3. 0 4 .0



## . 

# -**~l l**  5.0 6.0 7.0 8 . 0

CurTinC O.IC t**200S Ii9~**  Om:n1 Time : 2 1.4 5 : 15 

### VES 006217

### Sa m p le Analysis Re p ort Sample-Name : AH3049 Data File Name : C:\.l'li: AK .NE1\DA TA\A1' HONI10 · 23

_ AAM025.DXD 

### Deteeror Type : 

### OX - 120 

### Method F ile Name : c:\peaknet\rnethod\methodll20anio n s .m et Schedule Fi l e Name : c:\pealmet\schedulelschedule\schedule\120anions\2008\120anion0902.sc h 

### Dale Time Collected: 2008-09-0i 9:46:04 

# PM · Syst e m Opecator: LLE Calibration 

### Date : 2008 - 09-02 6:54:22 

### PM Calibration Type : EXTERNAL Corrponent Amou nt 

### U nits : rog!L Dilution Factor : 1.00 Peak Infoon ation : All Peaks

Peak# Component 

### Name Amount ( mg/L} Retentio n 

### Time · I 0.0000 0.78 2 F luoride 0.3372 1.02 3 0 .0000 1'.13 4 0.0000 1.40 

## s Chloride 1.6101 1.63 6 Ni trite 11.5160 2.00 7 0.0000 2.25 

# s Nitrate 18 . 6776 332 9 P hosp hate 0.3885 5.85 

### t O Sulphate 4.1310 7.75



# Ill : PctkNet ·SE 5.l0d 

# - J>AAe 1 6 f2 . P eak An11 44908 29279 52846 36 156 105352 1803971

80487 5240008 12991 220975 Peak Belglat 6795 5687 8380 ;3857 

### 24596**32~122** 1 1 616 474473 10

28 12834

Cement Date: .2008-<19 -0 2

CWTel'lt TUne : 2 1 :S4:46 

### V E S 

### 0 0 62 1 8

### Sample A n alysis Repo r t S am plt N a m t : A H3 0 4 9 

### Data File 

### Name: C:\PE AKNET\D A TAIANION\ 1 0-23

_AA MO ZS .DXD
AH3049 16 . 0 1 ' 14.0 . 12 .0 1 1 0.0 Cll 8 .0 I :1. 6 . 0 

# ( 4.0 \ 7 

### 2. 0

# ~

0

· 2. 0 0 1.0 2.0 

### 3.0 . 4 .0 5 . 0**P;~ee** 2of2 9 

### I 6.0 10 I



### . _. _A._ 7.0 

### -·· - - - 8 . 0

Oli'Tefll**Oat~:** 200s.o9-0'2

CurretVTime: l•:S4i46 

### VES 

### 0 0 62 1 9

### Sample Analys i s Repo r t Samp l e 

### N ame

_ : A H30 49 Da ta Fi l e Name: C:\PEA.Kl 'I£T\D A T A\AN IO N\10-23

_AAP017.DXD Detector Ty pe : DX - 120 Metllod File Name: c:\peakoetlmethod\method\120anions.met Sc h ehde File Name : e:\peaknet \s chedule\schedule\schedulc \ 120an i ons\2008\120anion0902 . sch Date T i me Collected:**2008~9 02**  3:50:20 PM S ystem Opecator : L LE Calit rari on Date: 2008-09 - 02 12:27:39 P M Calihnlrion Type : EXTERNAL**~onent** Amount Uni ts : mg/L Di luli<>ll Factor : 1 0. 00 Peak Info nnation : All Peaks Peak# Component Name Amount (mg!L) R etentlo ll Time P ea k Area I 0 . 0000 0.80 6867 2 Chloride 1. 5258 1.63 9297 

### 3 Nitrite 10 .4 305 1.98 1363 3 2 4 Nitrate 24 . 1444 3.50 396850 l Sulpha te 4 . 5370 7.80 15397 AH3049 16 . 0 14.0 1 2.0 10 . 0 fl) 8.0 :L 6 . 0 4 I 4 .

0 3 

# n I 

# j 2 .0 I 

# U\ 5 I I

# -~**t** 0 1. 0 2. 0 3 . 0 

### 4 . 0 5. 0 

### 6 . 0 7 . 0 

### 8.0



### . . .**r~e** 1 o f t Peak He ight 1 3 22 217 4 2451 3 46560

1 0 1 2



### c ..,-e ,,,**oa~ ~**  

### : WQ3 . Q9 ..()2 CU:m::nt Time : 15 :..59 :00 

### VES 

### 006220

### S a m pl e Anal y sis R epor t Sample N ame .: AB 3 0 50**Da ta** **F~ e**  

### N am e : C : IP E AKN E1\DATA \A

NJ O N\10-23 _AAR 026 .DXD Dete<torTyp e: DX-120 M etm d File Name: c :lpealcnet\melbod\method\120anio ns. me t 

### Sclled u l

e File Name : c : lpealcnet\scbedu1elscbedule\scbedul e\ 120anions\2008\120anion09Q2.scll Date 'rime Collected : 2008-09-02 9 : 55:34 

### PM Sys t em Op e rnto r : LLE Calilra t ion 

### D a te : 2008 - 09-02 6:54:22 

### P M Calilrat i on Ty pe : EXTERNAL Component Amou n t Units : mg!L Di lu llon Factor : 1.00 Peak In formation : A ll Peaks

Pe ak II Co m ponent N ame A mo u nt ( m g/L ) R e t en ti on T i me l 0.0000 0.78 2 Fluoride 0.2346 1.03 3 0.0000 1.13 

### 4 0. 0 000 1.38 5 Chlori de 0 .5 15 4 1.63 6 N itrite 10.88()4 

### 2.00 1 Nitrate 1 8.5042 3 .33 g Phosphate 0.2268 5.85 

### 9 Sulph ate 33210 7.77 AH305() 16 .0 

# I 1 4 .0 12 .0 10.0 

# I '1 8 . 0 

# ,**~** 

# . , I 6.0 1 4.0

# ~ 2 .0



# _ _ l.)J-J.Jj \.,_ O

f · - Pu k A rea 17826 1 8906 7 8966 21784 31692 1678423 5107 3 40 3347 151893

9 

### 8 I I**ei~ t**  2960 4 553 12543 2708 6568 291208 476336 292 8851

- 2.0y 0 1.0 2.0 3 .0 4.0 5.0**-- s.o** **P~ec** l o f I Cttmn t D

s te : lOOS · 09 .Q2 Cwrem Tune : 22 :04 : 1 2 

### V E S 

### 006221

## Sample Analysis 

## R eport Sampl e Name: AHJOSI**ata Fil** **Nam :**  C : IPEAKNE'f\DATA \ANJO N\10-13

_ AA002 7 . DXD DetectOr Type : DX-120 

### Method file 

### Name: c:\peaknet\rnethod\metbod\120an i ons.met Schedul e File Name : c:lpeaknetlschedule\schedule \<cbedule\12 0ani01\s\2008\12 0anion0902.scb Date T ime Collected : 2008-09-02 10:05:0 1 PM System Operator : LLB Calibration Date: 2008-09-02 6:54 :22 PM Calibration Type: EXTERNAL . Component Amo u nt Units : mg/L Dilut ion Factor: 1 .00

Peak# Component N ame · Peak Information : AU Pe aks Amoun t (mgfL) Retention Time P ea k Area Peak H eig h t



### - · - · · ···- 

# --- - -- ------- -- - - --- -- -- .. 

## - - 1 2 Fluoride 

### 3 4 5 Chloride 

### 6 Nitrite 7 

### 8 Nitrate 

### 9 Sulphate 16.0 14 . 0 12.0 10 . 0 

## 'i 8 . 0 6.0 4 .0 3 1 2 1 4 5 

# 2.oc ,

0 f •.J

- 2.0 0 1.0 2.0

# ~~~ :

# P~et·S**E** S. I Od 7 ! 0. 0000 0.3909 0 . 0000 

### 0.0000 0.6176 12 .9.827 0 . 0000 17.7602 

### 3.8 039 AH3Q51 

# J \ '-- -3:0- - 4.0 5.0 0 . 78 1. 02 

### Ll3 1.38 1.6 3 2.00 2.25 

### 3 .33 

### 7.71 24415 34706 126489 26901 38500 

### 2114353

15 117 6 4634564

1755 13

9 t 3982 

### 7255 1 9419 3077 7442 372244

16566 

### 436918

10323



# _____/'-..,_ 6.0 7 .0 8 .0**C~n~** Otte: 2QOS .()!.l.02**C\l~nl** Time : 22:13;4) 

### VES006 2 22

### Sam pl e Analys i s Report Samp l o Namt: AB3052 D •t• F'lle Name: C:\PEAKN.E'J:\DATA\ANION \ I 0-2J

_ AA0028.DXD Detector Type: DX-120 Method File Name: e:\peaknet'method\method\120unioos.met Schedul e File N ame : c:\peaknet\.schedulc\sehedulc \scbe dule \120anions \2008\120anion0902 . &ch Dou:Time CoUected: 200 8 -09.()2 10 : 14 : 31 PM 

### S y stem Operator : LLE Ca 1 ibralion Dat e : 2008-09-02 6:54 : 22 PM 

### Ca l ibration Type : 

### EXTERNAL**Ol~l** Amount U nits : mg/L D i lulion Focloc: I 0.00 PeU lnfonnation : All Peaks

PHI<# Compo a emName Amo•nt (mg/L) Retention Time



# - •. .. 

# .. 

# . I 0 . 0000 0.78 

### 2 F l uoride 

### 2.0546 1.00 

### 3 Chloride 32.1010 1.60 4 Nitrite 1.3809 1 . 98 5 Nitrate 

### 87 . 1 .3 42 3.42 6 Sulpbgte 120 . 5047 7 . 72 A.ll 3

0S

2 16

. 0 

# I 14 . 0 12 . 0 10.0 

## 'a 8.0 

## . 6.0 · 

### 3 4.0 2.0 12 

# LJ**·2.~ 1**  I I I 

### \ "--



# - 0 1.0 2 .0 

### 3 . 0 4 .0 5 .0



# - 

# II : PclllNct.SIB . IOd Pttc lu f l 

### 6 . 0 J!eak Aru Peak Height 4255 812 15968 3878 215939 42598

12950 2135 1694873 184243 585377 34118



### 6 

# _f\ _ 7. 0 

### 8 . 0

C 1111nt Ott'C. :**2.008 09~**  OJ rtt:rU T i me- : 22:23 : 14 

### VES 006223

# ' Sample Analysis Report Sample Name : AH305l l)a tA Fi l e Name: C:\PEAl{NET\DATA\ANIO N\ 10-23_AA N018.DXD Detec to r Type : DX-120 Meibod File Name : c:lpealm e t\metbod\roethod\120anions .m et Seh<du.te File N ame: c:\pealmetlscbedule\sch<dule\scbedule\120anions\2008\120anion0902 . scll Date Time CoUected : 2008-09-02 3:59:50 PM System Operator: LLE Calibration Date : 2008-09-02 12:27:39 PM Calibration 

### Type: EXtERNAL Component Amount 

### Units : mgiL Dilution Factor: 5.00 Peak loformation : All Peaks

Peak# Component N am e AmoUllt ( m g/L) Retentio n Time Peak Area PeakHelgbt



### - 1 0.0000 0.78 10970 1785 2 Fluoride 3.5292 

### J:OO 68424 9080 

### 3 0.0000 1.35 7133 1057 4 Chloride 35 . 2156 1.62 508697 113417 5 Nitrite 1.2671 1.98 28963 4 537 

### 6 Nitrate 58 . 4445 

### 335 4073577 392033 7 Sulpha te 134.1116 7.70 1330476 77739 

### AR30S2 16 .0 1 4.0 4 12.0

. 10. 0 7

8.0 

# \ I 

## 'a 6 .0, 

# _}\_ 4.0 2.0• 

### I 2 3 

## s

# ~ d I I 0 -2.0 

# -· ·" 0 1. 0 2.0 

### 3 .0 4.0 5.0 6.0 7.0 8 .0


# .. .**C~n ent**  O.. le :**100~2 .**  Pne · I ofl Corn:m**Tit~~e :**  t 6 : oa:27 

### VES 006224

### Sample Analysis Report Sample Name : AH3052D Data FUt Name: C:\PEAKNETIDATAIANIONU0-23_AAN029.DXD Detector Type: DX-120 Method File Name: c:\peaknet\methodlmcdlod\120anioos . mct Schedule File Name: c:\peaknet\schedule\.<Chedule\schedule\120anions\2008\120anion0902.scll Date TUne Collected : 2008-09-{)2 I 0:24:03 PM SY.s t cm Operntor : LLE Cal ibration Date : 2008-09-{)2 6:54:22 PM Calibration Type : EXTERNAL Component Amount Units : mg/L Dilution Factor: 10.00 Peak In formatio n : All Pe aks

Pea k # Component Name Amount (mg/L} Retention 

### Time l 0.0000 0 . 80 2 FIUO(ide 4 .3298 1.00 3 0 . 0000 1.37 4 Chloride 27.5926 1.62 5 Nitrite 1.6432 1. 98 

### 6 Ni trnte 84.5652 3 .4 2 7 Sulphate 119.9763 7.72 

### AH3052D 16.0 14.0 12.0 10.0 rn 

### 8 . 0 

# "" 6.0 

### 4 4.0

# LJL 2.0 I 2 I I 0 -2.0L._ 0 

### J.O 2.0 3.0 4.0 5.0



### ...

PtRe I of1 6.0 Peak Area Peak Height



# - 6344 10 52 38973 4978

5333 

### 665 184413 41051

16339 2668 1636469 175734 582710 33831

7 I 

# _j \__
7 . 0 

### 8.0

Ctinent lhte: : 200l, .()9 .o z CUtrent Tune : 21:31 ; 40 

### VES 006225

### Sample Analysis Report

. '

sam ple Name : A1130S3 Data File Nam e :**C:IPEAKN'E':N>ATA\i ~Nl** **ON\10-23_AAN039.DXD** 

### Detector Type : 

### DX-120 Method File Name: c : lpeaknet\metbodlmethod\120anions.met Schedul e File Name : c:lpeaknetlschedulelscbedulelschedulel 12Qo&n i ons\2008\120anion0902.sch Dare iirne Collected: 2008-09-02 10 : 33:29 PM System Operator : LLE Calibration Date : 2008 · 09-02 6:54:22 PM Calib.rat i on Type: 

### EXTERNAL Component Amount U nits : mg/ L Dilution Factor: 10.00 Peak lnfonnation : All Peaks

.Peak# Co mponent Name Amount (mg/L) Re ten llo a Time



# ·· - ·--- 

# . 1 

### 0 .0000 0 . 78 2 Fluoride 2.4828 1.00 3 0 .0000 1.35 4 

### Chloride 34.6631 1.60 5 

### Nitrire 1.6380 1 . 98 6 Nitrate 124.4844 3.38 

## 1 Sulpha t e 141.4927 7.70 AH30S3 

### 16.0 ' 

# \ 14.

0 12.0 10.0 

# .I 8.0 (I) 4 

# \ :1. 

### 6. 0 4.0 2.0

# ~5 I 

### 0 

## - -**~**



### - 2.0 0 1.0 2.0 3 . 0 4.0 5.0

...

PaJC 1 

### on Peak Ar ea Peak Height



# · -- - - -- · · --------·· - -

6.0 5076 1014 20289 

### 4850

4103 805 233989 45 820

16273 

### 2799 2638790 272150

691734 40 244



### - 7 I 

# /\ _./ '-- 

### 7 .0 8 .0

Cun'tnt ()a.Je ;**1008.()9.()~** Cwrrent 1'imt:: 22: 4 2 : I I 

### VES 

### 006226

### Samp l e Anal ysis Report Samp l e Name : Al130s4 D ata File Name- : C: \PEA KNE'l\DA TA\ANION\10.23_AAN03 l.DXD Detec t or Type : DX - 120 Method File Name :**c:lpeaknet~odlmeth odl120anions.met**  Sc h edul e File N"Jlle . : c:lpeaknetlscbedule\sebedulelschedolc ll20ani<ms\2008\120anio n0902 . scb Daw Time Collected: 2008·09.02 10 : 43:00 PM 

### Sys tem Operator : LLE Calibration Date: 2008-09-02 6:54:22 PM Calib rntioo 

### Type : EXTBRi"'AL Component Amount Units : 

### mg/L Dilution F a ctor: 10.00 Peak Information : All P eaks 

### Peak# Component Name Amount (m g/L)



## - · - - -- --·-- 

# --- ----- I 2 

### Fluoride 3 Cbloride 4 Nitrite 5 Nitrate 6 Sulphate

12.0 10.0 0.0000 2.2132 36 . 8316

1.5643 86.0967 126.6170 

### Rete n tion TilDe 0.80 1.00 1.62 

### 1.98 3.42 

### 7.72 AH3054 P eak Area 4388 17568 249341

15319 167 1 205 616262

# :~: , . \

8.0 3 \ 6

# !:~ 2

# ~ . j\1 2.0, 

# :1 ll_11 ' '

0-;

# ~----~1**-- ----------~-**  

# '-**2.0 i___,;----;;:·** **-;c- ·-** **-:-; ;:--** **--:-::---~-=- --,:-** **--~-;:--**

0 1 . 0 2.0 3.0 4.0 . 5.0 6.0 7.0 8.0 Peak l:lelgllt 852 4262 57161 2531 180311 35913

# ~~ : PnkNec - S E .S.Hid'**Pa~re** I or I Cl.lrrM I [hit(: : 1008-09-02**~~ Ti** **me :**  2.2:Si:37 

### VES 

### 006227

### Sam ple Analysis Report Sample Name : A£1.3055 Data**FU~ ame:**  

### C:IPEAKNET\DATAIANION\l0-23_AAM032.DXD Detector Type: 

### DX-120 Method File Name: c:\peaknet \method\l:nethod\120anions . me t Sc hedu le File 

### Name : c:\peaknet\schedule\sebcdule\schedule\l20anions\2008\120anion0902.sch Date T ime Collected : 2008 - 09-02 10 : 5 2:25 PM System Operator : L LE Calibra ti on Date: 2008-09-02 6:54:22 PM**Calibnu~** 

### Type : EXTERNAL Component Amount**ni~** 

### : mg!L Dilutio n Factor : 1.00 Peak lnfonnation : A.ll Peaks Pcilk # 

### Componen t Name Amount (mg/L ) Retention Time



# --- -- - - I 

### 0.0000 0.80 

### 2 Fluoride 0.4756 1.02 

### 3 0 . 0000 1.15 4 0.0000 1.38 5 

### Chloride 2.2725 1.62 -6 

### Nitrite 1.1624 1.9 8 7 

### Nitrate 19.5531 3.30 ' 8 

### Phosphate 0 .2080 5 . 87 9 

### Sulphate 12 .3411 7.72 

### AH3055 16.0 

# \ 14.0 12.0 10.0 en 

### 8 . 0 :1. 

### 6.0 5 

### 6 

### 4.0 z3 

# u. 2.0 I 1 1 4 .



## o · 

# - . . 0t\..'J \.

- 2.0 

### ,- - -- 

## - 0 1.0 2.0 3 .0 

### 4.0 5.0

... 

# fl : PeUNcc·SE SJOd 

### P l\llk A.rea P eak H eil;bt 5086 892 43292 

### 83"/8 79875 12715 1 0933 14 80 150705 30457 147097 2 4 125 65 1 6306 564837 2227 202 600053 34885

9 ' 

### I

# ~-·-**_}\_** 6.0 7.0 8.0

Currertt DINe : 2003-1)1).02 C

un: en t T i me: 23: 01: 02 

### VES 006228

### Sample Anal ysis Report Sam pl e Name: AHJOSS Data File 

### Name : C:ll'EAKNET\l)ATA\ANION\16--23

_AAN019.DXD DeteetorType: OX- 120 Method File Name: c:\peal<nel\methodlmetbod\120anions.met Sebedule 

### FileName: c:lpeaknet\scbedule\schedulelscbedule\120anionsi2008\120anionQ902 . sch Th!tc 

### Time Collected:**200&-09~2** 

### 4:09: 16 PM Syslem 

### Operator : LLE Calibration Date : 2008..o9-02 · 12:27:39 PM Cahbration 

### Type : EXTERNAL 

### Com p onent Amount Units : mg/L Dilution Factor: 

### 5.00 Peak Information : AU Peaks

Ptak . # 

### Component Name . Amount (mg/L) Re tentio n T ime



### . 1 

### 0.0000 0.80 2 

### Fluoride 0.4400 1.02 3 

### 0.0000 1.15 4 

### Chloride 2 . 3979 1.62 5 

### Nitrite 1. 0889 1.98 6 Nitrate 29 . 0821 3.45 

### 7 Phosphate 0.7968 5.87 

### 8 Sulphate 12.6 1 63 7,78 A.H3055 

### 16 :

0 14.0 6 

### 12.0 I

# ~ 10.0 

# ., 8.0 :i. 

### 6. 0 4.0 2 . 0 1 23 4 5 

# . · ·· - - j L

_ _

._ I ll

### ~ I 

### 0 -2.0 0 1.0 

### 20 3 . 0 4.0 

### 5.0

.. . 

# II ' Puklle ..SE S . IOd**Pt~tt** I of I 

### 7 I**-· ·**  

# . 6.0 Pea k Area PeakHelgbt 9083 

### 1586 7718 1 552 11 057 2281 30256 6047 24231 4203 106 1 467 120070 

### 2i66 212 108906 6484

8 I 

### 7 .

0 8.0

C\><Teot o.<e , 200S-&.>.02 C\ln'ellll Time : 16;17 ; $3 

### VES006229

### · Sample Analysis Report Sample Nam e: CCB D a n File Name: C: \ PEAKNE'l'\DATA\ANION\10-23

_ AAL033.DXD 

### Detector 

### Type : DX-12 0 Method File 

### Name : c:lpeaknet\metbod\rn elh od\ 120anions.mct Schedule File N ame : c : \pealcn et\schedule\scbedule \scbedu le\l20anions\2008\120airloo09 02. sch Date Ti m e Colle ct ed : 2008-09.02 11:01:51 PM · 

### System {)petat o r : LLE calibration Date : 

### 2008 · 09 - 02 6:54:22 PM 

### Calibration T ype : EXTERNAL Component Amount Units : mg/L Dilutio n 

### F actor: 1.00 Peak 

### Information : All Pea k

.- Peak# 

### Co mponent N ame Amount (mg/L) Retentloll Time l , 2

V) ::1. 

# '"I 14 . 0 12.0 

### 10 . 0 8 .0 

### 6.0 4.0 

### 2.0



# or- -2.0 t_

_ _ 0 1.0 2.0 

### 0 . 0000 0.0000

2 I 3.0 

### CC B

4.0

l' ;

• ,ee t of I 5.0 1.35 

### 3.58

6.0 Peak Area 

### 3523 6661



## - · - - ·- · - 

# .. · Peak Ileight 54 1 

### 591

7.0 

# - s:o Current Oa.le ; 2008-o9. o2

ClmcDl T ime: l);J0:)3



### VES 006230I 

### Sa m p le Analysis Repo rt S omple Nome : CCV Data F ile 

### Name: C: \ PEA.KNET\DA IA\AN10N\10-l3_AAL034.DXD 

### Detector Type : DX - 120 Method File Name: 

### c : lpeaknetlmelhod\melhod\ 1 20nniom . met Sched u l e Fi le Name : c:lpeakne!\schedule\sohedulelschodule\12Qanions\20081120nnion0902.sch Dnte Time Co llected : 2008-09-02 II : I I :22 PM System Operator : L L

E Ca libration Dare : 2008-09-02 6:54:22 PM Calibration Ty pe : EXTERNAL CoJ11>ooent Amount 

### Units : mgfL Dilurian Factor : 1 . 00 Peak Information : All Peaks**P~• k**  # 

### Component N o

me Amount (m&fL) R ete ntlou T ime I 

### 0 . 0000 0 . 80 2 

### Fluoride 1.8968 0 . 98 

### 3 Chloride 3 . 0506 1.60 4 

### Nitrite 

### LSOOS 1.97 

## s Bromide 6.0870 3.05 6 Nitrate 2.0273 3.50 1 

### P h

osphate 6.0685 · 5.77 g Sulphate 

### 12 .1 910 7.70 

### CCY 16.0 r 

# '**14 ~**  

# ' 1 2.0i

### 10.0**~** 

# ., 8.0 t ::L 

### 6.0 · f 2 3 

### 6

# :1~ 4 5 I 7 I I I**PeakAr~** ? I SS 

### 1897 38 204 751 192 193 1 73753 348538 360403 592470



### 8 I 

### 1 3 19 38765 39109 30474 24740 41337 26041 

### 34146

0 

### LO 2.0 3.0 4. 0 

## s.o 6 . 0 7.0 8 . 0 

# l!J ; P.nkM: t ..se 

### S, ,Od**Pt~te** s of I C.m: ru DIMe : 1008--09- 0 .l O. nutT i m

c : 23 : 19:$9



### . ·-· 

# - -- -· - -- --- -- -- -- VES 006231

### Samp l e Analysis Report Sample Na . me : AH 3 0

56 Data File Name:**C:\PEAKNETIDATA\A~10Nil0-2J AA** **03S.DXD** 

### Detector Type : DX - 120 Method File Name : c :\ peaknetlmethod\metbod\120anions .met Schedule Fi l e Name: c:lpeaknetlschedulc\scbedule\scbedule\120anions\2008\ 12 0anion0902.sch Dat e Time Collected : 2008-09-02 II :20:47 PM Sy stem Operator : LLE Calibration Date: 2008-09-02 6:54:22 PM Calibration Type : E XTERNAL Compooent Amount Units : mg!L Dilutio n F actor : 1.00 Peak Information : All P eaks P eak# 

### Component Name Amoun t (mg/1,) Re te n tion Ti me



### · - I 

### 0.0000 Q.80 2 

### Flu o ride 0.4 172 1.02 3 

### 0.0000 1.1.5 4 

### Chloride 2 . 0899 1.62 5 

### Nitrite 1. 2 067 !.98 6 0 . 0000 3 . 28 7 Sulphate I 1.3200 7.7 3 

### AH3056 1 6.0 1 14.0 1 2 .0 10 .0 (/) 

### 8.0 • ::1. 

### 6.0 

# \ 4 5 

### 4.0 23 I I 

### 2.0 

# ___**Jj~Ju\ ~** 

() ' 

### ·2 .0



### - 0 1. 0 2.0 3 . 0 4 .0 5 . 0



### . 

### - 

# Iii : P c.kNec-SE S .10d**~ee 1o** **l** 

# · - 6.0 

### . P eak Area**Peakll~ght**

. . 

### 3563 

### 7 os 37375 . 7493 53409 

### 9694 1 38140 28549 

### 152982 25625 8253438 697145

548562 320 1 4

7 I 

# A _ 7 . 0 8.0

C\lrrtnt 011tt : 200$-09
- 0Z Currerd Ti me. : 2 3 :29:24 

### V ES 0 06232

## Sample Analysis 

## Report S•mp le Name : AH3058 Da t a File Name : 

### C : \PEAKNE 1\DATA \ANIONU 0-23

_AAL036 .DXD Oete . : tor Type: 

### DX-120 Metbod F i le Name: c:\peaknet\in ethod\melbod\J20anions.met Schedule File Name : 

### c : \peakJJet\schedule\scbedule\scheduleU20 an ioos\2008\ 1 2 0ani on0902.scll Date Ti m e Collect e d : 2008 ..09.()2 I I :30: 13 P M System Operator : LLE Ca1ilration Date: 

### 2008-09-02 6:54:22 PM 

### Calilrati on Type : EXTERNAL**Co~onent** 

### Amount Units : mg/L Dil u tion Factor : 1. 00 

### pe ak Informa\ioo : All P eaks Pea k 

### # Compone nt N ame Amount (mg!L) R etention Time I 

### 0 . 0000 0.80 2 

### Fluoride 0 . 7671 1. 02 J 

### 0.0000 LIS l 

# o.oooo 1.38 j 

### Chloride 4.3628 1.62 6 Nitrite 

### 1.1397 1.98 1 Nitrate 

### 19.43'29 3.32 & 

### Phosphate 0.2930 5 . 85 

### 9 Sulphate . 25 .885 2 

### 7.68

I 

### A.H30 5

8 16.0 14 .0 12 . 0 1 . 0 . 0 8.0 . 

## s 

# \ 'i 6.0 4 .0 

# "J 2 . 0 I !I 

### 4

# ~

0 I I 

## U \,_

_ , _ , .. 

# \ '----- 

# --

- 2.0 :- -· 

### . . . . . . .. 0 1.0 

### 2 .0 3.0 4 . 0 5 . 0



### - .. 

### 8 I 

### 6

]

__ _ Peak Area . Peak R elg,b t 5156 

### 8 79 

### 72964 14182 91479 14447 12348 1669 297926 57569 

### t440n 23006 6115611 542592 7293 548 13 03 121 760 51

9 I 

# Jl

· 7-:-

o

-· - s.o OJrrer ,t Da1e : 4:000: ·09-0l C

U!Tent T itne : 23 : l8

! SO 

### VES 006233

### Samp le An alysis Re port Saniple Name: AH93Z5 Dab File Name : C:\PEAKII'E1\DATA\ANTON\11)..23_AAL 037.D XD 

### Detector Type: DX - 120 Method File Name : c: lp eaknetlmetbodlmcthod\120aoio,.• . mct Schedule File Name : c:lpeaknet\scbedu l elschedulclso hedule \120anio ns12008\120anion0902 .sch Date T ime Collected: 2008-09-02 II :39:38 PM Syslem Operator : LLE Ol l ibrnlion Date : 2008-09-02 6 :5 4 : 22 PM Cahbrotion Type: EXTERNAL 

### Component Amount Units : mg/L Dil1lion Fac:tor : 10.00 Peale Information c All Peaks



### Pt1k N 

### Component Nam e 

### Amount ( mg/L) Reteation T=e



# - . 1 

### 0 . 0000 0 . 80 2 Fluoride 1. 33 41 1.03 3 0.0000 1.15 4 

### Chloride 54.4485 1.62 5 

### Nitrite 3.4982 1.98 

### 6 Bromide 141.9363 3.05 7 

### Nilnlte 20.8588 3 .50 

### 8 Sulphate 

### 8 . 0387 7.77 9 0.0000 8.30 AH9J1J 

### 16.0 14.0 12.0 10

. 0 4 I 

### 8.0 6 

### 'Q 6 . 0



# _ AA_ 4.0 

### !23 5 

### 2.0 . 

# u_ I I I**o~** 

### -2.0 0 1.0 2 . 0 

# 3: o 4 . 0 5.0



### ...**a~** I O(l 

### . 

### 6 . 0 

# .

PtakArea P ealc Height 12223 

### 2064 8706 2146 13836 2897 3768 12 84493

40382 

## . 

## n04 420927 60916 359090 41147 

### 29434 1871

2639 253



### .

8 9 I



### · 7

-:o- - & :o

C\wrent Oate =**1'003 0~** 

Cu rrcntltmo : ll : ti;IS 

### VES 006234

### Sample Analysis Report Satnple Name : AH932S 

### Data

_ Flle Name: C:IPEAKNE'I\DATA IANI ON\10 -23

_ AAU014.DXl> Octee10rType: DX- 1 20 Method File Name : c:lpcaknetlmethodlmetbod\ 1 20anions . met Schedule 

### File Name: c:\peaknetlschedulelschedule\schedulell20anions\20081120anion0902.scb 

### Date Time 

### Collected: 2008 - 09-02 

### 3:21:51 PM System Operator : LLE 

### Calibration Date: 2008-09·02 12:27:39 

### PM Calibration Type : EXTERNAL 

### Component Amount Units : mg/L Dilution 

### Fac tor: 10.00 Peak 

### Inform ation : All P03ks



### Pe•k # 

### Con1po n ent Name . Amo1111t (mg/L) 

### Retention Tim e I 

### 2 Fluoride 

### 3 4 Chloride 

### 5 Nitrite 6 Bromide 7 

### Nitrate 

### 8 Sulphate

# :::~**!** 4 I 

### 0.0000 1.0009 

### 0.0000 51.9005

3.3447 

### 134 . 7260 2l.l775

7 . 0815



### 6 AH9315 0.78 1.03 1.15 1.62 1.98 3 . 07 

### 3.53 7 .78 PellkArea 

### 12869 8892 

### 13302 

### 360149

39764 407203 345127



### 26822

1 2.0f 10 . 0 8.0 

### 6.0 4.0 2.0



### 0

# ~ 

# i

# f**'-.~J'.f**_ _ _/. 1 

# \1\

___ _______**.--'- --**  Pea k Heigbt 2070 . 2170 

### 2640 79875

6690 

### 56715 39 793



### 1774

## 2.0**!- --.-::** **--;:-.,--~-.----:--:- -:-:----:-~** **-= ---,::-::--**  

# o L O 2.0 3 . 0 4. 0 S .O 

### 6 . 0 7 .0 

### 8.0

# ~~ ; PeakNa.SlH. IOd**Pt~** I of l Cwellt Ihttc : 2003-09.()2 Cl.ll'l'e o t iitne: I S :3 0:J) 

### VES 006235

## Samp l e Analysis Report · Samp l e Nanie : AH937.6 Data File Name: C:IPEAKNE1\DATA\ANJON\l0-23_AAL038.DXD Detector Type: DX-120 Me t hod Fil e Name : c:\peaknetlmethodlmethod\120anioos .met Schedule File Name : c:lpeaknetlscbedule\schedule\schedule\J 20anions\2008\ 120anion0902.scl• D ate T ime Collect ed: 2008-09-0211:49 : 03 PM System Operator : LLE Calibration Date: 2008-09 - 02 6:54:22 PM Calibrat io n Type : llXTE RNAL Component Amount Un its : mg/L Dilution Factor : 10.00 Peak Information :All Peaks

P .. k # COttlpottentNa.me Amount (mg/L) Retention Time Peak Area Peak H elgbl



# --------- · ------------ - - ....,.--- -- - ·-- 0.0000 0 . . 

### 80 2 Fl uoride 1.3643 1.03 3 0.0000 1.1 5 4 0.0000 1.37 

## s Chloride 5 ? .8582 1. 62 

### 6 N i trite 2.3253 1. 98 7 Bromide 138.6178 3.05 g N i!r3te 14.7040 3.52 

### 9 Sulphate 8.1433 7.78 10 0.0000 8.30

Pate I o f2 1 2912

. 9010 i 5141 7949 365096 25166 410482 249157 299 4 1

2587 2084 2078 2737 1063 808 27

4368 

### 59095 29285

1 901 249

C OTTenl O ll tt : 2()08..o9.02

Currtnt Ti:mt : 23:$1:4() 

### VES 0062 . 36

## · Sample Analysis 

## Report SamJ>Ie Name : AH9326 Data File Name: C:\PEAKNET\DATAIANION\10·23_AAL038.DXD 

## 16.or 14 .0t 12.0j 

### IO.O:f 5 

### 8.01 

# ! ' 7 6.0 ' · I 4 . 0; \ I 

### 11H9326



# . _j 8

# 0~**~i J**  6 

# \J\**2-~ c~** **~** 

# ------ 0 1.0 2 .0 3 . 0 4.0 5.0 6.0



# m Ia : PtakN e t .S E S. JOd 

### 7 . 0 9 10 I I 

## 8.o·

0. 11

1' ftt4**[)~ :**  2008-09-02 C

men t Time : 2J!S?!40 

### VES 006237

## Sample Analysis R e po.rt Sample Name : AH9327 Datal'Ue Name: C:ll'EAKNETIDATAIANlON\10-23

_AAL039.DXD Detc:tor!ype: DX· I 20 Method File Name : c:\peaknet\metbodlmethod\ 120anions.met Schedu l e File 

### Name : c:lpealo:let\schedule lscbadule\scbedule\120anions\2008\120anion0902.scb Date T ime Collected : 2008-09·02 11:58:30 PM 

### System Operator : LLE Calibration Date: 2008-09-02 .6 : 54:22 PM Calibration Type : EXTERNAL**Cc~Tponeot** 

### Amount Units : rngiL 

### Dilution Faetor: 10.00 Peak I nformation : AH Peaks

Peak # Component N am<> 

### Amouot {mg/L) Retention Time I 

### 0.0000 0.78 2 Fluoride 

### 1.4534 1.03 3 0.0000 

### 1.15 4 

### 0.0000 1.35 5 Chloride 

### 51.7965 1.62 

### 6 Nitrite 

### 4 .3 1 08 1.98 7 Bromide 

### 135 . 0473 3.03 

### 8 N itrate 

### 23.9498 3.48 9 Sulj>ha t e 

### 9. 1 251 7.77 10 0.0000 8.30 Pe ak Area 13016 9908 1 8397 9949 357299

50949 399277 415031

34697

2705 Peak Height



# - - ----- 1935 2275 3192 1343 83105

8056 55888 47300

2162

253

Ol rTenl**Oa ~**  : 2003-09 · 03**Ct.~tnni imc**  ; 00:07: 12 

### VES 006238

### Sample Analysis Report Sample Name : AH9327 

### Data File Name : C:\PEAKNEl\DATA\ANION\10-:U

_ AAL039.DXD AH9327 16.0 14.0 1 2.0 10 .0 

## s I Cll 8.0 

# uh ' . :1. 6.0 

# fi j 4 . 0

. 123

# _j~ 2.0 I I I .

0**-· --~** 

- 2.0**~-** 0 1.0 2.0 3 .0 . 4.0 

## s.o 6.0 7 . 0 

### 9 10 I I 

# - 8.0

O..rrent**~¢ :**  l008-0!NJ3

Co!Telll**Tiro~ :**  00:07 : 12 

### VES 

### 006239

## Sample Analysis Report Sample Name: AH9 328 Data 

### F i l eName: C :\PEAKNET\DATA\ANION\1 0-:Z3_AAR01S.DXD Detector Type: DX - 120 Method File Name: c:lpeaknet lmethodlmethod\120anion s.met Schedule Fi le Name : c:\peaknetlsched ul e\schedule\-.chedule\l20aruons\2008\l20anioo0902 . sc h Da t e Time Collec ted: 2008 - 09..02 3 : 31:22 PM · · 

### Sy!;tem Operator: LLE Ca l ibration D ate: 2008·09-02 12: 27:39 PM Calibra tion 

### Type : EXTERNAL Component Amo un t Uni t< : mg/L Dilution Fac t (! r : 10 . 00 Peak Womtation : AU 

### Pe aks 

### P

..

l< 

### # Com pon ent Narne Amo u n t (me/L) Retention Time

M OM . .. I 

### 0.0000 0 . 78 2 

### Fluoride 2.0459 1.00 3 0 . 0000 1.3 5 

### 4 Chloride 150.2626 1.63 5 

### Nitrite 2.5327 

### . 2 .00 6 

### Bromide 2.446 8 3 . 08 7 

### Nitrate 11 8. 1004 3 .38 8 Sul phate 

### 4. 3 32 6 7 .80 AH9328 l6 .0f 

# I 

# I 14 . 0 12 . 0 

# :....- 

# "'I . • Vl 

### 8.0 ::1. 

### 6.0 

### 4.01 2 . 0 l 

### 2 3 5 

### 6 

### 1 l l I I 

## \ 0 -2.0 0 1.0 2.0 3 . 0 

### 4.0 5 . 0 

# .. . 

# IIJ :Peal:Ntt·S E S.IOd**a~** J, of l 

### 6.0 P ea k Area Peak 

### H e lgJtt 

### 6909 12 41 19064 304 9 7

4 1 2 1099 14 73170 3 28008

28945 4329



### 5

599 925 371069 3 358551 14480 966



### 8 I 7.0 8 . 0

CunetU OMc : '2008-09 ·02 Cutreot Tirne : I.S:)?:S9 

### VES 006240

## Samp le Analysis Report Samp le Name : 

### AH9328 Data File N ame: C:IPEAKNET\DATA\AN10Nit0 -23

_AAL040.DXll 

### DetectOTType: DX-120 Method File Name: c : lpealcnet\metbod\melbod\J20anions . met Schedule File 

### Name : c : 'q>ealmet\schedulelscbedule\scbedule\ 1 20anioosl20081120anion0902 .sch Da . te T ime 

### Collected: 2008-09-03 12:08:00 

## AM · · System 

### Oper ator : LL B 

### Calibration Date : 2008-09-02 6:54 : 22 PM Calil...-ation Type : EX TERNAL**Co~onent** 

### Amount Un its : mg!L Dilution 

### Factor : 50 . 00 Peak 

### I n formation : All Peaks**Pe~k** 

### # Component Name Amount {mg/L) Retention Time 

### PukArea Peak 

### Helgbt



# _____________ .:.._ 

# __ _ _______ ___ _________ l Fluoride 2 Chloride } Nitrite 

### 4 N itrate


### 16 .0I 14.0 

### 12.0 10.0 4.1589 173.4513



### 3.6028 165.5579

4 8.0 2 I 

### AH9328 

### 1.02 1.62 2.00 3.48

6.0 

### I 

# f\

# t-"--'-**-J U** **~- --** **---·-** 3649 

### 234180

4424 5838 66 

### 594 52088

660 

### 678 15

## 2.0~**--.--~----~-=----- :-c** **=-** 0 1.0 

### 2.0 3.0 

### 4.0 5 . 0 

### 6.0 -- -: 7.0 -- 8.0 - 

# Iii : PeakNet·SE S.IOd ha<: l o( l Cum:11 t Otte: 2(1Q8.(;9.()3 Cllmn.t TllfPe**~** 00:14-.37 

### VES 000241

## Sample Analy sis 

## Re port Sa

mple N am e: AH9329 Da111Flle Name : C:\PEAJ<NEl\DATAIAN10N\10-l3

_AAL041 .DXD De tettor Type : DX-120 Method File N ame: c : lpeaknet\methodlmethod\ 120anions.met Schedule Fi le Name : c:lpeaknet\schedule\scbedule\scbedule\ 120anions\2008\ 120an i on0902 . scb 

### . Da te TIDle Collected : 2008 - 09..03 12:17:26 AM System Operator : L LE Calibr ati on Date : 2008..()9..02 6:54:22 PM Calibrat i on Type : 

### EXTERNAL Component Amount Units : mg/L Dilution Factor: 50 . 00 Peak'Infonnalion : AU 

### Peaks Pea k # Component Name Amount (tng/L) lle tealio n Tim e



### . .._

. 

# ____

I 

### 0.0000 1.15 2 

### 0.0000 1.37 J 

### Chl oride 204 .661 I 

### 1.62 4 

### Nitrnte 1 39 .7288 3.50 5 

### Sulphate 1 2 . 1669 7.78 

### AH9329 

### f6 . 0f 14.0 12 .0l 10.0**8.0 ~**  3 

### 4 

# .., 

# j =!. 

### 6 . 0 t I

### 4.0**~** 

# )L_ ,_ 2.0 t 

### ' 0 ·2. 00 1.0 

### 2. 0 3 . 0 4 . 0 5.0



## ... 

# E : PnkNet.S E S .tOd P-...e I o f l 

### 6.0 

# . Peak Area Peak Height



# · - --· 9979 1323 5659 899 278571 60035 4 88101 57630

2312 182

5 I



### · · ·· · - - 7 . 0 8 . 0

Cn:m1 1 o.te : 2008 .Q9-0) C\ln'«!t T ime : 00 :26;(t) 

### VES 006242

### Sample Analysis Report Samp l e Name: AH9330 Data File Name: C:\PEAKNETIDATAIAN10N\ 1 0-23

_ AAL042.DXD Det e<tO r Type : DX- 120 

### Metl» d File N ame:**c:~ knet\methodlmethod\120anions.met**  Schedu le File N ame : c:lpealrnet\scb edu l e \schedu le lschedule\ 120anions l200 8\l20anion0902 .scb Date T ime C ollecied : 2008-Q9-03 12:26 : 5 1 AM · · 

### S yst 'l'll Operator : LLB Ca l ibration Dat e : 2008-09..02 6:$4 :22 PM Ca lib ration Type: EXTERNAL 

### ComponC<lt Amount Units : 

### mg!L Dilu t ion F actor : 50.00 

### Pe ak Inf ormati o n : All P eak s P ea k# Componen t 

### Name I Fluori de 2 J C hlo ri de 4 Nitrite S 

### Nitrate 6 Sul phate 

### 16.o 

# 1 1 4 . 0 1 

### 12 .01 Amount (mg/L) 3 . 3104 

### 0.0000 219. 94 93

3 .7680 1 70.5 4 76



### 12.4262



## JO.o t 5

## 8~ 

# f I Retention Tiine



### AH9330 1.02 1.35 1.62 

### 2.00 3.48 7 .78 Peak 

### Area
1 9 42 476 5 

### 300536

485 1 602$40

2562 Pe.ok Heigbl 47 6 

### 683 67487



### 720 69480 191

# :~**_: _~** **-~-'\-- ...,.** **1 ===::** **:_J\_,_--: ~-** **·- ,_** **----~ ~=~~~==·~** **~- -"-~==**  0 1.0 2 .0 3. 0 4 . 0 5 .0 6.0 7 .0 8.0 

# IIi : f>e1k N c: 1 .S E $.10d Puc I o fl



# -- ---- ------ ---- Currtn t**~e :**  2QO$.Q9-0J**Cun~t** Time : OO : JS:Z8 

### VES 006243

### Sample Analysis Report Sample Name : B- SPIKED Data File Name : C:\PEAKNETIDATA\ANION\10-23_AAL043.DXD Detettor Type: DX-120 

### . Meth>d File Name : c:lpeakne t\mefuod \metbod\120anions.met Schedule File Name: c:\peaknet\schedule\scbedule\schedule\120anions\2008\J20anion0902.sch Date T ime Collected: 2008-09 - 03 12:36:17 AM Sysl!m Operalor : U.E Calibration Da t e: 2008-09-02 6:54:22 .PM Calibration Type : EXTER NAL 

### . Con"I""''nt Amount Units : mg/L Oiluli on Factor : 2.00 Peak Information : All Peaks

Peak II Com ponent Name Amount (mg/L ) Relelllion T:ime I 

### 0.0000 0 .80 l Fluoride 0.1423 1.02 3 

### . 0.0000 1.40 4 Chloride 8 .3 674 1.62 

### s Nitrite**1. 7~4**  1.98 

### 6 0.0000 3.17 

### 7 Sulphate 3.4120 7.78 

### 8-SPIKED 16 . 0f 

# \ 14 . 0 12.0 1 10.0 

# \ v.> 8.0 4 ::r.. 6.0 I 4.0 I 2 · 3 

# fU_ \ 2.0

0 I I 

## _j_, -2 .0

## o'-· 1.0 2.0 3 .0 4.0 5.0



### . ..

# ~~~ : f'mNet-SE SJOd**~e!otl** 6 . 0 Peak Area PeakHelgbl



## - 1702 433 2440 586 23754 2525 285055 51311

9 1 029 11938 22690100 1699467 731 98 4334

7

. I 

# -- 7.0 

## s.o

Qln-ent**~** : 200S..()c) · Ol Cum.nt Time: 00:44:59 

### VES 006244

## Sa mpl e Analysis Report Sample Name : CCB 

### D att File Nam e : C: \PEAKNETIDATA\AN JON\10-2J

_AAJ044.DXl> Deteotor Type : DX ·120 Metllo d File N ame: c: \pealmet\metbod\method\120anions.rnet 

### . Schedule File N ame: c:'pealmcl\schedole\schedule\schedule\120anionsl2008\120anion0902.sch Date Time CoUected : 2008 -09.03 12 : 45 : 48 AM System Operator: LLE Calilmltion Dat e : 2008-09 - 02 6:54:22 PM Calibration Type : 

### BXTERNAL COI'Jl>Onent Amount Units : mgiL 

### Dituli on Factor : 1.00 Peak Infonnation : All Peaks

Peak II Co mpon ent Name Amoun t (mg/L) Reten tio n Time P eak Area

CCB 

### 16.0 14.0 12.0 10 .0 . <n 8.0 :0. 

### 6 . 0 4.0 2.0

0

- 2.0 0 1.0 2 . 0 3 . 0 4.0 5.0 6.0 

### 7 . 0

. . .**h~** I ofl Peak H eig h t



### 8 .

0

O:lr:rtnl ()ale : 2(10&.{)9-oJ Ctne1\4 T ime : 16:07 : 32 

### VES 006245

### Sample Analysis Report S am p le Name : CCV 

### Data File Name: C:IPEAKNE1\DATAIANION\10-23_AAJ04S.DXD Deteetor 

### Type : DX-120 Meth>d Fi le Name : c : \peaknet\metbod\metbod\129anions. met Schedule Fil e Name : c:\pe aknet\schedule\schedule\schedule\120anions\2008\120an ion0902.scb DateTimeCollected: 

### 2008-09-0312:55:19AM Systtm Operator : LLE Calilt-alion Date : 2008-09-QZ 6:54:22 P M Cali . tcalion Type : EXTERNAL**Co~oncnt** Amount Units : mg/L 

### Dillllion F actor : 1.00 Peak Infonnatiou : All Peaks Peak II 

### Compon . ent N ame Amo•nt (mg/L) R etentlou T lme. . 

### Peak Area Peak 

### Height



# ·-- - · - - -·------------- --- - --- -- ----- I 

### 0 . 0000 0.80 6812 

### 2 Fluoride 1.8226 1.00 

### 181977 

## > Chloride 2 .9 523 1. 62 

### 197875 4 Nitrite 

### 1.4363 1.98 1 83601 

### S Bromide 5 . 86 1 2 3.07 167 093 

### 6 N itrate 

### 1.9580 3 .52 336086 7 Ph osphate 

### 5.7957 5.71 

### 343313 S 

### Sulp hate 11.7117 7.72 568292 CCII 16.0 . 

### 14.0 f 12.0 " 

### IO . Oj 

# s.o j 6 . 0 j 

### 2

### ~ 4 6 8 1254 38 564 4313 1

· 30163 . 23679 39538 24722 32978

4. 0 t I J I

# ~ I ; 1

# ~t-J**J** 

# \JL

_ JV L

_ _ _ _ _!\.

___ 

# 1\ __**h~e** to il Ome nl Dalll ! 2(}03...()JJ.O)

Current Time : 0 1 :OJ ;

s-6 

### VES 

### 006246

## Sample 

## Analysis Report Sample Name : CALIB STDl Data File Name: C:\l'EAKNE1\DA TA\ANlON\10- 23_AAE08S.DXD Detector 

### Type: DX-120 MetllOd Fiie Name : c:\peaknet\rnethod\melhod\120anions.met Schedule 

### File . Name : c:\peaknet\s<:bedulelschedule\schedule\120anions\2008\120.nion0902.scll Date Time Collected : 2008 - 09.03 7:13:58 AM Systtrn Operator : LLE Calibration Date: 

### 2008 - 09.()2 6:54:22 PM Calib ration Type : EXTERNAL 

### Corrponent Amount Units : mg/L Dilution Factor: 1.00 

### P ea k Information : Al.l Peaks Peak# Compone nt Name Amoon t (mg/L) Reteotloo Tlme Peak Area P eakllelgbt



## -- · - - .. 

## - - -· -·----· -------- -- - --- ----·------ ·---· · ·-·

16 .0J 14 .0 12.0i 

### I O

.Of 8 . 0 6.0 4 .0 0 .0000

CALlBSTDl 1.3 7

2.0 . 

# ' l .

0 

## r- --··--- -- - -- - · -- -- - --- - - -· - -- - - ------ 8413

## -2.**·'- --** **-: ---** **.,- -:--** **·---:-- --"7** **-:--~::- ----** **-·--·-------**

0 1.0 2 .0 - -3.0 4.0 5.0 6 . 0 7.0 8.0 1253

### ~ 

## 15 : Po lcNei · SE S. IOd Pa.t. c I o f I Cunenl Date : 2008 .00 ·03 Cuo-ont**im~ :**  0 7 :22: 3S 

### VES 006247

### Samp l e An alysis Report Saltll'le Name: CALIB STD2 Dais File Name: 

### C:IPEAKNETIJ)ATAIANION\J0..23

_AAE086.DXD DetertorType: DX-120 Metllo<l File 

### Name : c:\peaknet\methodlmetbod\120anions.met Schedule F ile Name : c:lpeaknetlschedulelschedule\schedu l e\ 120anionsl20081120anion0902.scb DateTime Collected: 2008-09-03 . 7:23:23 AM Systan 

### Operator: LLE Calibration Da t e: 2008-09;02 6:54:22 PM Calibration Type: EXTERNAL Component Amount Units : mg/L Dihiiion Factor: 1.00 Peak lnformation : All Peaks

Petk # 

### Component Name 

### Amount (mg/L) Retention Time Peak Area 

### PeokHelg)lt**·- --** **·· -·-** **---,- ~-** **----- -···-** **-- ----** **--·** 

### -·-·· · · ·- - ·· -. - ·- I 

### F l uoride l 3 

### Chloride 4 

### N itrite 5 

### 6 Phosphate 7 Sulphate 16 . 0 14 .0 12.0 10 .

0 8.0 

## 6

. ol 0.0874 0.0000 

### 0. 121 0 0. 07 7 6 0 .0000 

### 0.5383 0.2581 CAUBSTD2 

### 1.02 4071 1.37 10509 1.65 5520 2.00 5145 3.58 6144 5 .82 21937 7.78 3026



# 4.0t 2 . 0 · . 1 2 3 4 5 6 7 

### 815 14 28 1 140 849 788 1665 220

I I I I 1 i · l

# -2**L==-= ==** **~-~~~-=~~=~~=~~= ~=~~~-** **:- ~~** **-=··-~ :~**  0 1.0 

### 2.0 3.0 4 .0 5.0 6.0 7.0 8.0

(..'u:Ttnl- Date : l()0$..@.0) Cwm.c. T i otac · ! 07:32:01 

### V E S 00 62 48

### Sa mpl e Ana lysis Report**So~** 

### It N:une : CALIB STD2 

### Dato FUe Nome: C: \PEA.KN'E'I\DAT AIAN 1 0N\10-l3

_AAE086.DXD



### . Detector Type: DX-120 

### Met h od File Name : c :\peakn e tlmetbo<l\methO:CJI 120anious.met S<:h<dule File Name : c: lpeakncrlscbedulelsclladulelsc hcdulell20anionsl20081120anion0902 .s eh Date Tame Collected: 2008.09..03 7:23:23 AM Systm1 Operator: LLE 

### Colibntion Date : 2008-09..02 6:54 : 22 PM Cal 

### il>rotion Type : EXTERNAL**~~Amount** 

### Units: mg/L Dih.tion Factor : 1.00 Peak Information : All Peaks

Peol< # 

### CompoDent Nlllllt Amount (mg/L) Retentioo TilD e



# . I Fluoride 0.0874 1.02 2 

### 0.0000 1.37 l 

### Chloride 0 . 1 210 1.65 <f. 

### Nitrite 0.0776 2.00 

## s 0.0000 3.58 

### 6 Pbospbate 

# o.sm 5.82 

### 7 Sulphate 

### 0 .2544 7.78 

### CAU!JSJ'Dl 16.0 14 .

0 12 . 0 10 .

0 

## 'a 8.0 6.0 4.0 2.0 I 2 3 4 . 5 , I 

## ! I 

## j ! 

# l I 

### I I 

## ! 0 

### ' 

### ' ·2. 0 0 1.0 2.0 3.0 4.0 5 .0



## . 

# -

P altf: J o( l .



### 6 

### I I 

### ' 6 .0 

### PeakArtll Peak flelg)lt**~071** 

### 815 10509 14 28 5520 1140 5145 849 

### 6144 7 88 

### 21937 1665

2847 214



### 7 , 

### I 

### i 7 . 0 

### 8.0

Cvncnt Dille ; 2:008-(;9.0.)**C~o nm.l**  Tinw ! U}:l.l:02 

### VES 006249

# !· Sa mple Analysis Report Sar11ple Name :**CA Ll~**  

### STD3 

### Data File 

### Name: C:\PEAKNETIDATA\ANIO N\10-23_A AE08 7 .DXO

· Detector 

### Type :DX-120 Meth od File N ame: c :\peaknet\method\method \120' .snions . met Scbcd llle file Name : c:\p!:akn&\scbedule\schedulelschedule\120anions\20Q8\ 120anion0902 .scb Oatt1ime Collected: 2008.09-03 7:32: 49 AM System Op erator : LLE Ca

libntion D ate : 2008..()9-02 6:54:22 PM Calibr a ti

o!l Type: EX'l'ERNAL Conponent Amount Units : mg/ L 

### Dih.otion 

### Factor: 1.00 

### P e ak Information : 

### All Peaks Pe a k II 

### Component N a m e Amoun t (mg!L) 

### Retention Tim e I 

### 2 3 4 

## s · 6 

### 7 g 

### Fluoride Chloride Nitrite Bromide Nilrate P h osphate Sulphate



### 16.{) 14.0 12.0 10.0 

### M 4 .0 . 0 . 3 993 1.00 0.0000 1.35 0 . 6437 1.62 0.3004 1. 98 1.2066 3 . 08 0.4044 · 

### 3.57 1.2427 5. 80 2 .4408 7.73 CALifJSTD3 Peak Area 

### 35558

9 92 9 40241 33%6 3223 1 63096 64155 108949 Peak Heigh ( 

### 70 15 1309 7914 55 11 4518 7818 4714 63 31

6.0!

# -~**t**

# ____l _:

_

_



# Lt

_

____ ll .. . _

_ _

_

_ _

___ _l_· ··- ·· - __ _ __ 

# L .**·2.oL· =-=** **-- -~** **-...:,-:** 0 1.0 2.0 3 . 0 --- 4 .0

Pe;te l of I G'UtTent. Oa.te: 2008-09 ·03 Cunel)l T me : 07:4 1:32 

### VES 006250

## Sample A n alysis 

## Report Sa

mp le N ame : CALIB STD4 

### D a b File 

### Name : C:IPEAKNET\DATAIANION\l0-23_AAE088. D XD Dclcctor 

### Type : DX -120 

### Melli()() F il e Name : e:lpeaknetlmetbodl.metbodll20aoions . m et Schtdu l e File Nam e: c:lpeaknetlscbedul elsehedul e\scbedule\120aoions\200 8\120aoion0902.scb Date Time Collected: 2008-09..03 7:42:21 AM**~y Siem**  

### O,rerator : LLE . · Ca lib ration Date: 200 8-09-02 6 :5 4:22 

### PM Cal i\> ration 

### Type : EXTERN AL Component Amoun t !J nits : mgiL Dilut ion Fa c t or : 1. 00 P eak Information : All Peaks Pf2k# Co m p onen t Name . Amo un t (mg/L) Reten tion Time I 2 } 

# • 5 6 7 g Sl Fluoride Chl oride Nitrite Bromide Nill'll t e Phosphate Sulphate



### 16.01 l4 . 0j 12 .0l 

## IO .Oj'

8.0 0.0000 0.80 1.9914 1.00 0.0000 1.3 7 3 . 1075 1.62 1.5030 1.98 !'.0 8 76 3 . 08 2.0298 3 . 53 6.0585 5.77 12 .2 208 7.70 

### G:ALIBSTD4 Peak Area 8983 199650

10422 208741 192532 

# mm 348986 359779 59 39 75 Peak Height 1531 398 8 1

1 264 409 43 30099 2

47n 41008 26276 34397



### 6

· 0 

# 1 

# T j 4 

## s 6

# ~ 8 ; 4.0 1

### ~ I I

### ~ 1 ,

# 2.~**,_** _____ 

# ll\**~** 

# JL_ju**~j\_** _ _ _ _) \_

-2.0 1 

### L

__ _ _ _ _ ... .. . . . .. . .. .. 0 1.0 

### 2 .0 3.0 4 . 0

C.'Ufl"e:lt Oil$e : 2008.c»-03 Curren!**T'm-~** · 07 : $1>:S8 

### VES 0062 5 1

### Sa mple Analysis Report Sample Name : CALIB STDS 

### Dat> File Name: C:\PEAKNET\DATA\ANIO N \ 10..23

_ AAE 0 89.DXD 

### Detector Type: DX - 120 Metbod File Name : c : '4>eak.net\metbodlmethod\120anions . met Schedule File Name: c:'4> ealcnetlscb.edu le\scl"!dnle\scb edule\l20anions\2008\l20anio n0902.sch Datt Time Collected : 2008-(19 - 03 7 : 5 I :47 AM Sysiom Operator : LLE Calil>ration Da te : 2008..09-02 6:54:22 PM Ca l oration Tyl'l': EXTERNAL Component Amount Units : mg!L Dillltion Factor: 1.00 Peak Information : All Peaks

P ea k II Compo n ent Name**mo~tnt** (mg/L) Re tention Time I 0.0000 0.78 2 F l uoride 3.9S38 0.98 

### 3 Chloride 6.2762 . 1.62 4 N itrite 3.0441 1.97 

# s Bromide 12.4953 3.05 6 N itrate 4.1863 3 .48 7 Phosphate 12.5537 . 5.70 

### 8 Sulphate 25 . 1317 7.65 

### CAL!BSTD5



# Ill : Prak.Nc.t ·S E S

. I

Od Pare lo r ! Peal< Area 1 4 675 410354 

### 438n2 403698 367779 749645 7801 58 1262.97 1 Pea k H e i ght 2574 86713 

### 99725 61586 

### 52298 85193 55699 73549

Cum:nt**D;~ -e**  : 2008 · 09 · 03

Current 'T ime: 0$:()0:29 

### VES 006252

### Sample A n alysis Report Sam ple Name : CALIB S TD 6 Data File Name:**C:IPEAKNETIJ)ATA\AN ON\10-~** **AAE090.riXD** 

### Detector Type: DX-120 Melhod file N ame: c:\peak.D<':t\metbodlmethod\120anions.met Schedule 

### File N ame: c:lpealcnet\scb.edulelscbedulelschcd u

l e\120anions\2008\ 120anion0902.sch Date :rim e Collected : 2008-09·03 8:0 I: 18 AM · SyS1em Operat<>r : LLE Calbration Date: 2008-09·02 6:54:22 PM Calib ration Type : EXTERNAL Component Amount .Units : mgiL Diluti on Factor : 

### 1.00 Peak Information ' : All Peaks

P <ak # Contpoutnt Name Amouot ( mg/L) Retention Time I . 0.0000 0.80 2 Fluoride 6 . 3617 0.98 3 Chloride 9 .5 995 1.62 4 Nitrite 4.7237 1.98 5 Bromide 18.9206 3.05 

### 6 Nitrat e 6.3150 3.45 7 Phosphate 18.9026 5.67 

### 8 Sulphate 37.9068 7.62 

### C4L . lBSTD6 Pe.ok Area 24516 683628 699817 645461 573099 1173776 1219751 1962066
16.0 ' 1 2 

### 6

## 1~**0 ~**  I 8 

# :::: I 1 

# i 

# ! ; / A

I

· 2.0 PeakHeigbt 4 259 134582 153465 105871 83600 125573 S6203 113434**-·- ··-** **~- --** **--** 

## - · - --·- - - ··· -· ·- ·----- · - ·· ---·--....- - - - .. 

### - 0 LO 2.0 3.0 4.0 5.0 6 . 0 7 . 0 8.0 

# II**PtakN ~-SBS** **IOd** PaJe 1 of I**OJ~ nt**  ().nc ; 1008-o9-0J**OJrrer~tTunt:** 08: 10: 0 1 

### VES 006253

## Sa mpl e An aly sts .Re port Sa mp l e Nam e : MBLANK D at o**Fi~** 

### Name: C:\PEAKNE 1\DA T AIAN 10N\ 10 -23

_AAE09 1 . D XO**Det~ or**  

### Type : DX-120 Metl>od F ile Name: e:lpeaknet\methodlmelhod\120anions.met Schedule File Name : c:\peaknet\sc hedule\sebedule\schedule\120anions\2008\120anion0902 .sch Da t e

Time Collected: 2008-o9-o3 10: 46:09 AM Sys 1m! 

### Oper• t or : LLE C ali bration Date: 2008-09-02 6:54:22 PM Calibration Type : BXTERNAL Component Amount Units : rngiL 

### DiiUiion Foetor : 1.00 Peak Information : Al l Peaks**e~ k**  It 

### Co mpone n t Name Amo u nt (mg/ L ) R etention Ti m e

MBUNK 

# 1 6.0 1 1 4 . 0 12.0 10 . 0 

# "' 8 . 0



### - "- 

### 6.0 4.0 2.0

0 

### --

- 2 . 00 1.0 

### 2.0 3.0 4.0 5.0



## .. .

# ~~~ : Petk Ne t -SES . I Od P -. e l ofl 

### 6.0 P ea k Area P e al< H eig ht

.. .. 

# _ _ 7.0 8.0

Cum:tlt**~e** ; 201)8.()9 . 03 C\Jrr'QII1'tnle : IO:j4 : 47 

### V E S 006254**a~pl e**  

## A n a l ys is R e

p or t Sample Name : 

### MSPl KE Dato Fi leN a me:**C:IPEAKNET\DA A\AN** **N\ l-23** **AAE09 .DX** **D** 

### Detl>'tor T ype: DX- 1 20 Met!Jod File N ame : c:\peal01et\method\method\120anions.met Schedule File Name: c:\peaknet\scbedulelschedule\w h edu le\12Qanions\2008\J2Qanion0902.sch 

### Date Time Collected: 2008-09-03 10:55:36 AM Sysitm Opera t or : LLE Calibration Date : 2008-09-02 6:54:22 

### PM Calibrati o n Type : 

### EJ{TERNAL Corrpooent Amount Units : mg/L Dilulio n Factor : 1.00 

### Peak Information : 

### All Peaks

P .. k # . C o mpo n e n t N a me Amou n t (mg/L) 

### Rete n tio n T ime I 2 3 4 5 

### 6 

### 7 

### 8 Fluor i de Chloride 

### Nitrite 

### Bromide Nitrate Phosphate Sulphate

16.0 . 14 .0 12 . 0 10.0 8.0 

### - 0.0000 0.80 2.0255 0.98 3.0263 1.62 1.5079 1.98 6.0307 3 . 07 1.9993 3.52 6.02 3 5 5 .77 1 2.1600 

### 7.68 MSPIKE Pe ak A r ea 8919 203228 203049 1 93189 

### 172093 343519 357583 

### 590905

Ill 

### :s. 6.0 2 

# t 4 

# 1 8 Pe ak 

### Height 1490 33083 42374 30135 23579 39413 2'5876 33891

4.0 I

## ~ 

# r 7

. I

# -~+--**~:** uJL_JJL

_ _ _ 

# A_j\_ _

- 2 .0

### ---=**~- -=-:,.---** **--:-:---** 0 - · .....**ro~ -...,** **'"'. ,_--,** **-, .0** **-- --::** **.o ----,.** **-::- .o** **..** - 6.0 7 . 0 8.0**~clo(l** OJrrent**0.~ ;**  l008.()9.0) OJrrcnt Time · : II :04 : 1 9 

### VES 

### 00 6 25 5

## Sampl e 

## A n alysis R e

p o rt Sample Name : AH3048 D

ata F ile Namt: 

### C : \PE AKNE 'J\DATA\ANlON\lO-Z3_AAD097 . DXD Detector Type : OX· I 20 Method File Name : c:\peaknet\method\method\J20anions . met Scbedule File Name : c:\peliknetlsche du le\sclledule\scbed ule\ 120anions\2008\120anion0902 . sch Date Time Collected : 2008-09 - 03 II :43:07 AM 

### Sysr:m Oper ator : LLE Calibration Date : 2008-09-02 6:54:22 P M Cal ib ration 

### Type : EXTERNAL Component Amount Units : mWJ

### Dilu!ion Factor : 50.00 Peak I nformation : Al l Ptaks

P e..k # 

### Co mp o n e n t Nam t 

### A mo u nt (mg!L) Reten ti o n Tim e



### . . 

## ·-. - - ... ....**·** l 

### Fluoride 19.61 75 1.00 2 

### Chloride 280.5242 1.62 3 Nitrate 104.5367 3.50 4 Phosphate 16.0138 

### 5.83 

## s Sulphate 106.8870 7.75 AH3048 

### 16.0 1 4.0 1 2.0 10.0 2 I 

## 'a 8.0 6 .

0 3 I 

### 4.0



# _ A 2.0 1

## ~

0 -2.0 0 1.0 2 . 0 3.0 4 . 0 5.0

Pale I of I



# -- - - -- --- - --·-·- · -· -· · 4 I

### 6.0 Peak Area P eak H e i ght 

### 34857 6225 389060 8626 3 359965 42599



### 8922 . 698 

### 9

4192 5408

5 

### I**~-** 

### 7.0 8.0

Cun'MI Date : 200 $-$..():) CWrcn ltime: 11 :5 1 :44 

### VES 00 6 256

### Sample Ana l ysis Report S anple Name: 

### All305l Dab File Name: C : IPEAKNET\DAT A\ANION\10..2J_AAD098J>XD Detector 

### Type: D X-120 Mc(hod File Name : c:\peaknet\tnetlJod\method\120anions . met S<:hed ulo FileName: c:\pealmt:t\schedule\scbcdulc\schedule\120anions\2008\120anion0902 .s ch Date Time Collected: 2008-09 · 03 11:52:33 AM System Operator : LLB Calibration Date: 2008 - 09·02 ·6::54 : 2.2 PM Calibration Type : llXTERNAL Co mpooent Amount Units : mg/L Dilootioo Factor : I 0.00 Peak Information : AD Peaks

P.,.k • C ompollent Nome Amou nt (mg/L) Retention Tome 1 0.0000 0 . 80 

### 2 Fluori d e 3.8157 1.00 

### 3 0.0000 1.35 4 Chl oride 36.6889 1.62 

# s Nitrite 1.3000 1.98 

### 6 N i trale 96.9567 3.40 7 Sulphate 1 35.1404 7 .70 AH305 2 1 6.0 

# II 14 , () 12.0 10 . 0 V> 8 .0 4 ::1. 6.0 I 4.0 2.0 I 2 3 

# s I ! I I 

## \ 0

· 2 . () 0 1.0 2.0 3.0 4 .0 5.0



## . 

# - 

# II : fCIJcNcc ·SE SJOd P•ac tor I 

### PeskArea P eak He(gllt 2397 

### 460 33766 4266

9104 1209 248329 54180



### 11904 1748 1924826 204233 6S94S2 

### 38133

7 I 

# , __}\_

6 . 0 7. 0 8 . 0 

# c.- · - : l0041-09 · 0J CW'tcA t**Tlt~llt** : ll :Ot: I S 

### VES 006257

### Sa m p l e A n a l ysis Report Sam p le Name: AB3052D Daia File 

### N ame : C:\PEAKNETIDATA\ANION\10-23

_AAD099.DXD DettctorType: DX- 120 

### Me1bod File 

### Name: c:\peaknet\meihodlmetbod\120anions .m et Schedule File Name: c:\peaknetlscbedul e\sclledule\scl.>edule\120ani onsl2008\120onion0902.sch Datt Time 

### Collected : 2008-09-03 12 : 02:04 PM · SyS1Cm 

### Operator : LLE 

### Calibra tion Date : 2008-09-02 6:54:22 PM**Ca~ ration**  

### Type : EXTERNAL Component Amount Units :**~** Dihltion 

### Fa<:tor: 10.00 Peak 

### Information ; All Peaks

P tak # Component 

### Name Amount 

### {mg/L) · Retention Time 1 

### 0.0000 

## o.so 2 

### Fluoride 4 .0923 1.00 3 

### 0.0000 1.35 4 

### Cbloride 27 . 8332 1.62 5 Nitri te 

### 1.3 192 1.9& 6 

### Nitrate 84.8629 3 .40 7 Sulphate 

### 119.7498 7.70 AH30S2D 

### 16.0 

# \ 14;0 i2.0 10.0 

### 4 ' \ 

# "' s.o ::1. 

### 6.0 4. 0

# LJ~ 2.0 1 2 I I 

### 0

- 2 .

00 1.0 2.0 3.0 4.0 5.0



### . 

### - 6 . 0 Peak Area Peak Height 

### 2566 481 36567 4578

8158 1114 186088 40582 12152 187 0 1643204 )7 4478 581567 33352

7 I 

# ·)\_ 7.0 8.0**CWT~nt,Da1e :**  2008-09 · 03 t\lm:nt Ti;m.e : , 1 2.: t 0:4 7 

### VES 006258

### S ample Analysis R e p ort S amp le Name : C Cll Data Fi le 

### Na m e: C:IPEAJ<NE'I\DATA\ANI O N\1 0- 23_ AAD 19 3 . DXD D

etec t or Typ e : DX-120 Method File Nam e : c:\peakne t\method\metbodl 120an i on s . me t Sched u

le File N ame : c:lpeaknet \.

..:bedul e\schedul e\<;ebedule\ 1 20an ions\20 0 8\12funion0902.sch D

ate Ti m e Collected : 2008 - 09-03 3:18:35 PM System O p erat or : LLE Calibration Date : 2008-09-02 6:54:22 PM Calib ration Type : E X

TERNAL Component Amo un t U n i ts : mg/L D ilution Factor : 1.00 Peale lJlf onnation : A UPeaks Peak II C omp oae n t N ame Amo u n t ( mg/L) R eten ti on Time 

### Pellk Area



### ·-··- · · - ·

-



## CCB 1 6.0 1 4 .

0 12.0 10 . 0. 

## '1 & . o 6 . 0 4 . 0 2 . 0



### 0

- 2.0 0 1.0 2 .0 

### 3.0 4 . 0 5.0 

### 6.0 7 . 0



## . . .

# ~~~~ : Peta k Nec · SS 5 .10d P&f!e I o f t 

### P e ak H eight



### .

.



### 8 . 0

Oureot Da le : 2008 · 09 .03 Qlncnt Ti me: I.S :V: l l 

### VES 006259

### S ample Analysis Repo r t Sanple Nam e: CCV Data File Name : C : \PE AKNE1\D AT A \ A

NI O N\10-23

_AA D104.DXD Dettctor Typ e : OX-120

. M ellio d F i l e Name : c:\peaknetlmetbod\rnethod\120aniolls.met Schedule 

### File Name :**c:~laJet \~bedu** **e\sehedule\~edule\120anious\2008\120anion0902.s b**  Date Time Collected: 2008-09-03 3:28:01 P M SySiem Op erator : LLE Calibratiou Date : 2008-09 · 02 6:54:22 PM Calibration Type : 

### EXTERNAL Component Amoun t Units : mg/L Dillltiou Factor : 1.00 Peak I nf

omutiou : All Peaks Peak # Component Name Ao•ount (mg!L) Retention Time 1 0.0000 0.78 2 Fluoride 2.0141 0.98 3 Chloride 3.0343 1. 60 4 Nitrite 1.4935 1.95 

## s Bromide 6.04 89 3 .00 

### 6 Nitrate 2 .0100 3.45 7 Phosphate 6 . 0180 5.77 

### 8 Sulphate 12.0977 7.68 

### CCV 1 6. 0 14 .0 12 .0 10 . 0 tl) 8.0 ::1, 6.0 2 3 

### 6 7 P eak Area 8676 202035 20361 4 

### 1912 51 172628 3 45438 357239 587759

8 Peak H eight 142 5 39609 4

4008 30752 24598 41416 25937 33975



### 4 .0

# ~ 

# ll_**~** 

# j, I 

# _; \_ , _A_**.::~t ·**  

# _ _ lJL ___)\_ \ 0 1.0 2.0 3.0 4.0**h~lo l**  5.0 

### 6.0 7.0 8 . 0

C\Jnent Da l e ; l.OOS-09.0)**Cus:r~n1Time :** **1S }6;-4)**  

### VES 

### 006260

# Method 7471A -M e r c ury In S o l id O r S e mi s olid Wast e

Maxxom Analytics Inc. 6740 Campobello Rd. Mi ssissauga, Ontario, Canada 

## LSN2L8 

## 1- 800-668-0639 

## www . maxxamaoalytics.com

VES 006261

# . .

l.lor<ury In Sea by CVAA • SOil {ug/O)

I . . ' ' '



# . . -.m WO<ka ho« Number: 1602842



### VES 006262

### RUSH R

epo rt Name: Wo i1< S h«t - ( Liqui d s and So li ds} #' 1602842 A

.$ si & o ment Date: Wcxin:esday; September O l. 2008 Ass i g n e

d c

o: H A

SAN B AYDAR Te!t Code: H G-S lnsttument I d ' Tcu Descrip<ion' TO D I!.TE.RMINI! MERCURY BY 

### CO W VAPOURAA . · Job S•mp l e % 'Nu robet Number D 

## s.....te!D F Moist M=SPK 

### lv l CP2 AIDOSS-0 1 REF MA T

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## n ,oo 2 20081081 2 8 2008109 /0 3 17,00 2 2008108128 2008109/03 17, 00 2 2008108128 2008109/03 1 7 ,00 2 20 08108128 2008/091!)3 17, 00 

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### - fJ!11 Remarks · (31 5 ) 4 37-0509 , .. RUS W .. tCP+HG. TOTAL**CHLORIDE.~,** BTU&.% ASH ()()lfi'ENT SUS TO PSC.REPUBUC. Projec< #: 1 000 2 - 022 NATION.$!. : J!IISR INTERN ATI ONAL Metb<XI Snike Sanm l ts



### VE S 0 062 64Maxxam A.Mtyti c-s-l nc CAM**fC0~48/1 P~** **1** of1 Prep 

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# j 

# 6t>J..ftJE_ Vo lume lui\ SurrogatefSplke so l utions Solutio n 10 

### # Cone . B l k·Spk MS Sam ple s



### . · IC PMS

ICAP ICP So il Spk . A(SPK·08.09}&B Variable 1ml./50ml. GFAAS 

### Hg H g Splke( H g Spk·08·10) 0.25ppm 1ml./50ml. 

# ,h'

Solvent Suppli er Lot 

### No. Spiked by:

HN03 Fisher 308172 

# !/Ill!- HCI Fishe r 

### 208051 Spiking Witnoued by : 

### H202 

## HtSQ• . Spike Date (yyyy / mmldcl)

# (j{~il00!/2":> Comments



### · . 

### V ES 0 0 6265

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# -------- M

ethod Name : SOP-0112 Me thod Description: Soi1 -- Caapobello Rd. (500 uL loop] Eltment : Hg Da t 8: 2008 - 09 - 03 Te chnique :FI - MHS**C~libration** 1ype: Hg, terQ Int e tc ept : J .. inear Wa •e longth: 2 5 3.7 nm. Sa o ple I n to Name: 8 - 9-03A.S IF 

### R es ults Data Set Name: 8 - 9 - 03a**~.,- .,.~--**  

# ...**------.-·-·------ ----=** **=== ==** **~-~- ----** **-=- --**  E lern ent: llg Seq. N o. : 9**S~ e**  ID: Calib Blank 

### Repl

f l 2 

### Heon : SampleCo nc 

### ag/L StndConc mg/L Auto - zero per-foread. li S Loc.: 9 Dat e :**00 -0** **~-03** Po ak HeiQht 0.0003 0.0002 Tiae Peak Stored 0 9:08:23 H o 09:09:04 Ho Ele...,nt : llg Seq . N o,: 10 AS Loc.: 10 Do te : 2008 - 09 - 03 So•ple 10: 0.25 ppb



# --- ------ -- - ---- - -- --- ------ 

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ea n: Samp1eCo nc o>q/L Stnd Conc mg/ L Peak H

eig h t 

## o.oon 0.0 017 '\'i me Peak S tored 09: 10 : 0 2 N o 09 : 1 0 : 4 3 N o ( H9l Standard number 1 a PPlied. (0 .0 " 002$) Cor:ce. . la.tion Co eff ici ent: 1 4 00000 Slope: 5. 93 4 94



# ------ ... --- ----=-----· - =-=== ---- ......**=~- -·** **·· ----**  S l eoent: Hg Seq . N o . : 11 Saple 10: 0 . 5 ppb RA!;>l



# ' l 2 M

ean : Satnp le"'....ooc 1119/L Stnd Conc 109/L liS Loc.: 11 Date:**2008 0~** **03** Pe ak Re.!9hl 

## o. 0040 0 . 00 4 0 Title Peak S to red 0 9 :11:41 llo 09:12:23 No (l lg] Ston dar<l nural:>er 2 app lied. ( 0.00050 ) Correlation**Co tf~** **le nt:**  0. 96321 Slo pe: 7 . 207 52 Elon1ent: Hg Seq . No.: 1 2 liS 

### Loc. : 12 Date: 2008 - 09 -03 Sonple l O: 1.0 ppb**---- ---** **--- ---** **---- ----** **-- --~----** **-----** 

# .. 

# --- - -- -- ----- ----- ------ - ...... 

# ------- - -- ---- - 1\op l

I l 2 tia.an: srunp le Conc mg/L St ndConc mg/L P eak 

### He1Qht 0.0080 0.0019 Time Peal< 

### Stor e d 09:13:21 No 09:14:03 !lo [Hg) Stand ard**~r** 3 app lied . (0.00100) Correlation**Coeft~cie nt:**  0.99 4 22 Slope: 1 . 61031 

# =-·---------- Element: P.g Seq. No .: 13 Soaple ID : 2 .0 ppb AS Loc . : 13 Dat e : 2008 - 09-03 

# -·----------------- --- - ----- ------- ---- ---- -- - ---- -- -· - -- -- ·---·-- - ---4-------- - -------- 1\tpl

I I**~** 

### sampleco nc mq/L StndCon c lfl9/L Peak Height 

### O. OlGO 0.0160 T i&e P eak. Stored 09:15:40 No 09:16:2 1 N o P

age - 4 - 

### VES 

### 006267Hem : (H9) Standa rd .nUttber 4 applied. (0.00200) Correlation Coeffi cient: 0.99812**-·---- ·--------~----** **-==** £lm>ent: Hg Se q . No.: 14 liS L oc. : l4 

### Sa•ple IO: S.O ppb Slope.: 7 . 82089 Da te : 2008-09-03**------ ----** **--~- --** **--------- ------------------** **-------- ---------** **--- --** **------- ---** **---~ --** **~---** 

### Repl



# • l 2 f.W!an: SampleConc m

g/L StndConc m

q/L 

### Pn k H

elQ ht 0.0411 0.0406 'l ' lro.e Pea k Stored 09: 18 :00 No 09:16 : 42 No !Hg) Standa r d number 5 applio d. (0.005 00 ) Correl a tio n Co•ffieient: 0.99963 Slo pe : 8 . 07641**&lft~nt:** Hq Seq . No.: 15 AS Loc.: 15 D•te: 2008-09-03**S~le** ID: 10 . 0 ppb Ropl



# ' 1 2 M

om: saapleConc roq/L SmdConc mg/L**Pea ~**  

### Height 0.0768 0 . 0759 Time P eat Store<! 09:20:21 No 09:21:03 No ! Hql Standard ouoooer 6 applied. [ 0.01001 Corre l ation Coefficient: 0.99933 S l ope : 7 . 72409 Calibratio n data fo r Hg**~n ered**  calc ul ated M

e a n Si qn al Conce n txatio n Concen tration Standard S ta n da.rd 1 0 ( Pk H e i ght) (rug/L) (mg/L l l)eviation Calib Blank 0.0002 0 . 25 ppb 0 .0 015 0.00025 0.000 19 0.000030 

### o.s ppb 0. 0037 0.00050 0.00048 0.000010 l.O ppb 0 . 0077 0.00100 0.00100 0 . 000030 2.0 ppb 0.0158 0.00200 0.00204 0 . 000012**~-0** ppb 0.0406 0.00500 0 . 00526 0.000371 10 . 0 ppb 0.0761 0.01000 0.00985 0.000594**Cor~el ~ion**  Co effi cient: 0.99933 Slope: 1. 72409 tRSD 

## z.o 0.3 0.4 0.9 0.8



### - 

# ···- ·-- --- - - - . 

### VES 006268' 

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### VES 006269Perk!n -£Lner AAWinLAb: 2008-09-03, 02:12 : 25 PM SaDple xntor.atioo File C:\AAUSBR\SAMPINI0\8-9-0JA.SIF Descriptl.o · n !latch I D volwue Units !Oe ight Unlts 

### Analyst Sample V ol um e AS SIUOple ID Loo

17 1602S&O: REFMAT 19 ))LANK 19 H TI\X SPK 20 AI269&-01:01 21 AI269&-Ql 22 AH931S-02 23 AI2011-Q3 24 1112013-03 25 AI201S- 03 26 1112681 - 0l 27 AI2691-01 28 1116362-01 29 REFI1A1 30 111687·01 X 2 31 1602721 :**R~ntA:r** 32 llLA NK 33**rrRx** 

## s PK 3 4 1118093-01: Dl 35 AI809l•01 

### 36 Al8091 -0 l 37 AI8095-0l 38 

### AIBO!I&-01 39 

### AI809l-Ol <0 1118098-01 41 1115522-01 4 2 A1636t ·0 1 43 AI6361-0l 44 AJ6363-0l C5 l\l6372-0l 46 1116371-0l 47 11 16375-01 48 AI6371-0l 4 9 1116379 -01 50 1\ 16381-01 

### 51 1\1638 2-01 52 REFMA1 53 CCB 5 4 CCV 55 l602842:REfMAT 56 BLIIIIK 57 MTI\X SPK 58 11113051-0l: Dl 59 IIJ!3051-0l 60 A/!3052-01 61 

### IUI305l·Ol 62 A!130SI - Ol 63 AH305,-0 l 64 Afl3051 -01 6S R£FMA7 66 CCB 67 CCV 8 - 9-0Ja 1602560/2721/1602842 L

ily 0.00 s..,.ple 8.-.ple W

<dqht UDi ta 0.5100 

## o.sooo 0 .5000 0.5100 0 .5 000 0.5000 0 . 5000 0.5100 0.4900 0. 4900 0.5 1 00 0.5000 0.5100 0.5100 0.5100 

## o.s o oo 0.5 1 00 0.5000 0.5100 0.5000 0.5000 0.5100 

## o. 5000 0.5000 0.5100 0.5100 0.5000 0 .5000 0.5100 0.5000 0.5000 0.5000 0 . 5 1 00 0.5000 0. 5000 0 . 5 1 00 

## o. 5100 0. 5000 0.5100 0.5000 0 .49 00 0 . 5000 0.4900 0.5100 0. 49 00 0.5000 0.5100 Uaor Di lution

50.0000 50.0000 50.0000 50.0000 50.0000 50.0000 50.0000 50.0000 50.0000 50.0000 50.0000 50.0000 50.0 0 00 100 .0000

50.0 00 0 50 . 0000 50.0000 50 . . 0000 50.0000 50.0000 50.0000 50.0000 50 . 0000 50 . 0000 .50.0000 50.0000 50.0000 50.0000 50.0000 50 . 0000 50 . 0000 50.0000 50.0 0 00 50. 000 0 50 .000 0 50.0 00 0 50 .000 0 50.0000 50 . 0000 50.0000 50.0000 500 . 0000 500.0000 500.0000

50 . 0000 

## soo.oooo

50.0000 Page -21- Rema r k o



### VES 0062 70

## . (pO '{) .



# tw 

# 7· Y'f E l eDent: Aq Seq. No.: 71 Sunple ID:**602842:RE~'l'** Sampleconc mg/L 0.302 0.298 0 . 300 StndConc mg/L 0 . 0030 8 0.00303 0 . 00306 AS Loc.: 55 Pea k Heig h t 0. 0241 0 .0 237 

### Time 02:14: 32 02:15:13 Date: 2006 - 09 - 03 Peak Stored

No No 

### )M :o•- · - •-'!"--•••**,__rl =a=m=** **~•= ===** **~--- ====** **=- --**  £1ement: Hg Seq. No.: 72 AS Loc . : 56 Date: 2008 -09- 03 S.mple . I D:**B~NK -~---~** **-- --** **----~ ----** **-~ --** **-- ---** **----- --~** **-- ------** **--- ----** **--- ---** **-- ---** **--- --** **-- --** **--** Rep l SampleConc St.ndConc Peak Time Peak

l mg/ L**mg/~** Height St.ored I -0.00078 - 0 . 0000 1 0.0002 02:1 6: 4 7 11o 2 - 0.00 122 - 0.0000 1 0.000 1 0 2 :1 7 :2 9 No Moan: - 0.00100 - 0.00001 

### = =-=-==== -- •-===-- ----= ===-= - --=• -•=-=- •-- -=- • --== == e::o::d!r. == ,.. -•,.-• • •- Ele11ent: Hg Seq. No . : 73 AS Loc.: 57 Date : 2008 - 09 - 03 Sunple ID: MTRX SPK Repl SampleConc StndGonc Peak 

### Time Peak

I mg/ L m g/ 1 Heig h t Stored I 1.02 0. 0104 0.0807 02: 1 8:26 No ! 1. 01 0.010 3 0 . 0799 02: 1 9 : 07 No Mean: 1. 02 0 .0 104 EleDent : Hg Seq. No.: 74 AS Loc. : 58 

### Date: 2008 - 09 -03 Sunp le I D: AH3055-0 1 :Dl Rep l SampleConc StndConc Peak Tira e Peak

I mg/L mg/ L Height Stored 1 0 . 599 0 .0 0599 0 . 0465 02:20:43 No l 0.594 0 . 005 94 0 . 0461 0 2 :2 1:24 No**~an :**  0.591 0. 0 0597 Element: Hg Seq . No.: 75 AS L oc.: 59 o ats: 2008 - 09 - 03 Sample ID : AH3055 -0 l 

# - - ----- -- - - -·y -- -- -------------- -------- - --- - --- -- - - --- - --- -- ------ - - --- - -- --- -- ---- --- !<epl



# ' I 2 Mean: Samp l eConc mg/L 0.693 0 .6 78 0.686 StndConc l>IJ/L 0 . 00679 0.00665 0.00672 Peak Height 0.05 27 0.0516 t ime Peak**S~o:red** 02:23:00 No 02 : 23:42 No

- ,...,.,. ... ""' . - = == =--===--== -- ... ·--- - ........ 

# ----- --=-c==--==== - = - -----· - -- - ELement: Hg Saq . No.: 76 AS Loc.: 6 0 Data: 2 008- 09 -03 

### Sarop l e 

## r o: AH3052 - 0l Repl Samp l eConc St ndConc Peak 'rime Peak

I tllg/L 1ng/L Hei gh t Stored 1 8.35 0. 00835 0.0648 02 : 25:20 N o 2 8 . 20 0.0 0820 0.0636 02:26 : 02 No N aan : 8. 28**0.008~8** El em•nt: Hg Seq. N o. : 77 /\SLoe . : 61 Date: 2008 - 09 - 03 

### sample ID : AH30 5 3-01 Rop l Samp le Conc Stnd Conc P e-ak Time Pea k I mg/L l<lg/ L H e i ght Stored 1 1.41. 0. 00726 0.0563 02: 2 7 : 40 No 2 

### 7. 1 8 0.00704 0. 0 546 0 2 : 28 : 22 No t-:ean: 

### 7.29 

## o. 00 71 5 Page - 23 - 

### VES 00627 1

# G· 'fY

# O·~ 

# (( ;r( Element : llg Seq. No . : 78 l\S Loc.: 62 Date: 20 0 8 - 09 - 03 Sample ID: AH305 4- 01



# - - ------ - - -- - - --- - -- - - - - - -- --- - - --- - - ---- ---- - - - ---- - - - --- - -- -- -- - - - -- -- - - - - - - - - ------ - Rep!. SampleConc StndConc 

### Pea k Time Peak



### # mg/L . 

### mg/L . He i ght Stored 1 6. 4 9 0.00662 0 .05 l3 02:30 : 00 

# No 2 6.36 0 . 00649 0.0503 02:30 : 42 No Met an: 6. 42 0.00655



### - --== =--IW --==,..._.., ==:o: •o::oo==- •••---- - = ==--== =-:--= -·- = -- .c::=:= = Element: Hg Seq. No.: 79 l\S L oc . : 63 Date : 2008-09 - 03 Sample 10: AH305 6- 01

### ----**-- -~-----** **----------~- --** **----- ---** **-- ----** **-- ------** **-- --** **-~ --** **-- ---** **------** Repl Sall\p l eConc StndConc P . eak Time Pea)f 

# • • mg/L mg/t Height stored l 0. 5 89 0.00 577 0. 04 48 02:32:2 1 No 2 0.578 0. 00567 0. 04 40 02 : 33:03 No Mean : 0.584 0.00572



# ----- - ---- - ----- -=--- -........ ····-- -= = -==== ---= --·---- --=**em~nt:** H g Seq. No.: 80**~S** Loc.: 64 Date: 2008 - 09-0 3**SU~ple** ID: l\H3058 - 0 1**tO~** .J. ' · 

### -1.1 .

### --**-- --** **-- --** **----- --** **-- ---~** **---- --** **--- --** **-- ---------** **--- --** **----- --** **-----** Repl Sam ple Conc StndConc · Peale Time Peak

J mg/L mg/L Height Stored l 0.889 0.00089 0.0071 0 2 :34 ; 35 No 2 0.846 0.00085 0.0068 02:3 5:1 7 No Mean: 0.868 0.00087 

# -- --=- ----.. ---- - - --- -- ------ --=- - ......,.====-- -- ... - ....**------** Element: Hg Seq. N o .: 81 sample !0: lU'FMAT R&pl
- SampleConc StndConc



### t mg/L mg/L L 0 . 315 0 . 0 0 322 2 0.312 0.00318 Mean: 0.314 0.00320 Element: Hg Seq. No . : 82**S~ple** Io: AH3058·01 Samp l eCon c m

g / L 0 . 636 0.613 0.624 StndCooc mg/t 0 . 0 0636 0. 0 0613 0 .0 0624 Element: H g Se q . No.: 8 3 S ample ID: CCB AS' Loc . : 65 oat@: 2008 - 09 - 03 Peak time Paak H

e ight Stored 0.0251 02 : 36:49 No 0.0248 02:37:3 1 No AS Lo c . : 66 Date: 2 008 - 09-03 Peak Height 0 . 04 9 3 0.0476 Time Peak·

· stored 02:40:03 No 02:40 : 44 N o AS toe.: 67 Date : 2008 - 09 - 03



## ... -- - -- ... - - ---- ... _ -- .. 00 -00-- - --- - - . -- ------ ......... - ..,_ .. - ...... - - -

. M ___ - - - - - --- - - -- - _ ... --- - ... ... ... _ ... ------ .. - Repl · Sample-Cone StndConc

t mg/L mq/ L l
- 0 . 00003 - 0 . 00003 2 - 0 . 00003 - 0.0000 3 M&an: - 0 . 00003 -0.0 0003 Element: Hg Seq. No.: 84 Sa11ple ID : C CV Rep l

t l 2 M;!an: Samp l eConc mg/L

0 . 0 038 4 0.00386 0 .0 0385 StndConc 

### mg/L 0 .0 0384 0.00386 0.00385 Pea le Tiltte Heiqht 0 . 0000 02:4 2:15 0. 0000 . 02:42:5 6 AS Loc.: 68 Pea k Heigh t 0. 02 99 0. 0 301 

### Time 02: 43 : 53 02 : 44 :34 Pe ak Stored

No No Oate : 2008-09 - 0 3 Pu k Stored

No No Pag e -24 - 

### VES 006272

### Per k in - El m e r AA»inL a b : 2 00 8 - 0 9- 03 , 02 : 4 5:2 1 P H

Pa g e - 2 5 - 

### VES 006273t .

# Wartuho.-t HUmbt r. 1603354 -



# _

_ __ :J __ -

VES 006274• • 0 

# ... 

# 6 Regulation Water - RUSH 

# ,.--- · Repon l;fome: Wo:k Sheet · (Liqu ids ond s<>li d$) 1: 1603)58**Assignmc~t** ))aot: Assi &n ed t o : Tell Code: HG·I.. 1-ruld: Test o..aiption: TodeotnnlneHgby 

### cv..y;_ Nov 16,2000 MOL. <hanged from O . OOipPO>IO O.OOOippm . Job Sornple % N

umber Number D SamoleiD · · F Moist M'ffiXSPK OC23C Al0220o04

SPIJ<E OC23C

· BLANK •A894939 AH.J046'01R HBTU.U4-R1 

## n · f 'A894939 AH3047.01R llllTU·U4·R2 

# " -( 'A894939 AH3048.01R IIBTU · U4 · R3

# ~·'"" ·<' . • A894?39**AH30~9-0IR** LBTU-U4·RI 

### I •A894939 AH.JOlO.OIR LBTU-U4-R2 'A894939 AH.JOS 1.0 I R LBTU-U4-RJ ' A894939 AH30S9.01R MS- U 4-R J 'A 

### •• s •A894939 AH3060.01R MS· U 4-R2 

# ... .n ' 1 • A894939 AH.J061.01R · MSoU4·R3 )< • A89S312 AH4S76.()6R SCHF ..t>ULE 23124 I AS%582 . A!0220-04R 0 . MILES-WELL WATER A896582 A!0220-04R I MILES· WELL WA lER A896696 A10781.()6R DP · Tl · S 108/26108l A896n8 JJ0974-02R FIELDBLANIC A89679S JJ1368·09R SANJT ARY SEWER A89:7040 , JJ2467 .() lR • • ' 0 " 82149 .. JJ2410-02R 821S2 A897040 ' JJ2472-0lR 8215 8 A89'i040 AI 24 7 4.01R . 82168 A897040 AI247S.OIR 82169 A897049 AI2S22.Q2R :W2 . ALWOODSPO 

### 1'- · 

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oo:nOO by: 0 Val i dated by: 

### , . . OF or I Expiry Test AF COni Il3te Deadline Qlrtria 1-

' 0

2 2008108128 2008109/03 17:00 l 1008108123 l008109103 17:00 2 2008108128 2008109/03 17:00

. l 2008108128 2008109/03 17:00 2 2008108123 2008109/03 17:00 2 ' 2008108128 2008109/03 11: 00 I 2008108128 2008109/03 17:00



# ... I 2008108128 2008109/03 17:00 

### 0 I 2008108128 2008109/03 17 : 00 

### [:j · I 2008 / 09 1 02 2008109104 11:00 170 I 200 8 109/03 2008/09104 18:00 I 2008/09 . '03 2008/09/04 18:()0 I 2o0ai09102 2008109104 18 : 00 1 2008/09102 2008109/04 18:00 1 20o8/09104 2008109/08 18 :00

0 • . I 200&'09/03 . 0 2008/09104..18:00 . I 200l!l09/03 2008109104 18:00 . 1 2008109/03 200&'09/04 18 :00 I 2008109/03 2008109104 18 :00 I 2008/09/0) 2008/09/04 18 :00 I 2008109/03 

## :ioosto9I04 18:00 170**~** 0 A-, I _..I

Date: Dat e :

## 01

# -:I~L Date: 

### r Date :



### -

0 ___ 0

_ _ _____ _ 

### VES 006275**~.** 

### Ba Ojmc.Namc OI\894939Ml>CENSR lottmotlonal
MA89 SJ t 3A C h risti'" Horl:<ons 0 A8 965tlC<R Well Wi>e Centre

0AS96'79SA11J Slctlln & Trvd< Moau&c<urinr; MAa97C4alAS Rcsloo ofPcd (VS952) MA897049A . TownofOra.n.g.evi U e**SurrM•t~<IS•Ikcs ~mn** **c l'rcno** **tion** Rtmarks nl 

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# •· IIII IIII I II IIII H IIIU HBTU-U4-R1 AH3047-o1 

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## ~14**.** 111111111111111 1 011111110 MiLE$-WELL WATER AJ022044: D1 1s . 

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# lll lllllltiiiiiiiiiii !II B SA-NI'fARY SEWER AJ2467..()2 19 . 

## 1011 1101 1 1 [ 110 1 1111 1 1 82149 AJ2470-02 

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# IIIIIII U IIIUD I I I Ili i D 82158 AJ24 74-0 1 22. 

# ll ll l ll l llllBII !II IU 82168 Al2475-01 23 . 

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### R eagent Tracking Record W o rb h eai iJ 

# - 1603 358 YlllumeluU SunogUIS4>ikeiO!utioM Solution 10 I**B!~ -$p** **k** 

## MS S a mplu ICPMS 

### ICAP GFAAS 

### Hg**~** 

### 0517. 5m L 0517.5ml 20 '

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### Supplier Lot No . 

### S p i ked by : 

### HNO, 

### F i sh e r 

### 307292 2 008 -08·29 

# /c... - l-J**NH20H~CL** 

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### 7227 6 

## ' 2 0 0-09.02 

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### 67655 200.0S.02 H2S04 

### Fisher 1 08 0 03 

## ' 2008· · 08·29 Splko Oatt (yyyy/mmldd) K2S208 

### Fisher 

### 75812 2008··09.02 2008 · >09.0 3 

## KMN04 F is h e r 

### SC635 44 83 2 00 8·· 0 8·19 Co m m en ts



# - VES 006278

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### VES 006279\ \ 

# CEt A C Hg Analysis Report Analyst: ll:onapath W or ksheet rue: C:\Program Files\QuickTrue\Worbheetsl8 · 9 · 4a.wsz Dat eSta r t <d : 2008/09/04 12 :54 :15 PM Comtnent: 

# Re su lt s S"'"f,)le**N~** Type COOe 

# ..- %RSO Flags WI • Vo l. (ppb) Cll l il>ratiM 8Jod< STO 0 . 000 70 3 . 03 1. 00 1.00**R~s** 67.4 72.$ 70. 1 70.1 S1>1)(13rd " STO 0. 1 00 357 

# .. 0.64 1 .00 1 .00 Rep<Oc:ales 357 . 7 359 . 6 354.9 354.9 St3r.ctarct#2 STO 0.200 $73 1 . 10 1. 00 1 . 00 l'(epJ;cale$ &&2.0 & 7 4.9 679.2 674. 3 Standard 113 ST D 

### o.soo 1$04 0.56 • 1 .00 1.00**R.e pl** **~** 1592.2 1 610 . 0 1$1 1. 4**160 .~**  Ston<t3rd #4 STD 1.000**~36** 0.87 . 1 .00 1 . 00 Rt p li caces 3095.4 3146.8 3158 . 5 3 1 44. 0 Stondard 115 STO 2.000 01207 0.90 1 . 00 1 . 00 Repiiatas 6128 . 1 6225.7 5254.0 

# = · StaOOal'd #6 STD 5.000 1 55n 0. 75 t.OO 1.00 R

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lc<te$ 1 5539 .8 15T3& 1**~.4** 15 627.6 Cll i brolion 15,000. 

# • Equation: A · = :is.876 + 312 t .923C •

### ~ 10 . 000 Cor"*ation : 0.99996 ls SEE: 45.3041 

# t 5 , 000 FlaOf: 0 0 3 4 5 COO<enlratbn ( ppb ) ICV · L OW UN K 0.250 8 17 1 . 32 1 .00 1 . 00**~ce: te** **i** 8 1 0 . $ 62<! . 5 829 . 1 805.6 tCV · A U N

K 0.983 3105 0.3 1 1.00 1 . 00 Reo<lcates 3075.6 3118.3 313<. 1 3094.0 ICV - B IJNK 3 . 000 1 22 1 5 0.8 1 1 . 0 0 t. OO R ep! cates 1 2103.1 12m. • 123 17 .6 12 1 62..4**~008/09/04** 7:23:55 PM 8-9-4a . . wsz Page I


### VES 006280SampltName Type Cone pAl>• %1\S D Flags Wl. Vol. (J>pb) CCV CCV 0 . 992 3132 0.90 

### too 1.00 R&plca!e$ 3092. 6 3 1 31 . 4 3152 . 9 3 152.4 · CCB 

## cce 0.0 12 73 2.16 1 .00 1. 00**Ro ~**  69 , 8 73.9 74.2 72.3 SPI KE WS#16J)3789 liNK 1 .43 0 4505 1. 05 1.00 1 . 00 

### R.-s 4450 . 5 4517.2 4 481l . 6 4563 . 1 B

LANK U N

K 0.001 39 6 . 70 1 .00 1 . 00 ROJ)RcoieS 3 5. 1 4 0 . 5 40.5 39 .7 MTRXSPI< U N

K 1 .a20 $ 732 1 . 0 3 1 . 00 1 . 00 Rep l iCates 5651.6 5725.2 5765.1 5785 . 5 Al866 1- 05;0 1 U N

K 0 . 0 12 74 3 .77. 1 .00 1 . 00 Rep H C3Jes 7 0 . 9 72. 9 72.9 . 77.4 Al 8 66 1 .Q6 UN K 0 . 009 63 4, 1 6 1 . 00 1. 0 0 Replicat.es 85.0 64 . 8 59.7 6 1 .5 MTRX SPK UN K 1.720 53 97 1.79 1 . 00 1.00 Rep ncates 527 8.5 5366.9 5436.9 5504.5 A.J4304- 01 UNK 0.660 173 0. 80 .50 1 . 50



# . fl. epl\eJ t es 17 1.3 174 .5**.o~ o**  1 73.1 SPIKY' WS!f1!038S8 liNK 1 . 310 4128 2.07 1 . 00 1.00 

# qr Reptlcot es 4023 . 0 40 98.3 4 1 7 4 .9 4 216 . 2

BlAN K li N K . 0.02 1 1 01 

### 2m 1 . 00 1. 00

## t-1~ 

# """ 11 "".. 1 0 4 . 1 1 00.3 100.5 99 . • M

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RX .SPK UNI< 1 . 790 s6ia 1.79 1.00 1. 00 

# r-z.-. 'j . R ep Uc:ot .. 54a7. 7 M83 . 3 5661 . 3 5720. 4**~** 

## c·-:r<>! 1\10936-02 : 01 liNK 0 .70 1 2225 3.07 1. 00 1 . 00 I Ropicate s 2284.6 221 8.0 2 192.6 21 43.7


# . -> o-tiJ() 

## 1- Al0936-02 U NK 0 . 766 :1428 2.49 1 . 00 1. 00 Replicates 2493.0 2.446 , 1 2426 . 6 234 7.8 

### -::>o·<C <> C 

### gAH5757·0 1 li N K 0 . 020 97 2 . 1 5 1 . 00 1 . 00 

# N.)> ROQI!c;ate$ 9Q.5 95 . 7 99 . 9 95.4 AH5843 - 11 U N

K 0 . 033 1 38 4 . 35 1 .0 -3 1 .00

## ~R**eplicates** 1 29.2 1 40.4 140.7 \ 4 2 .2 Al0453-07 li N K 0 .091 3 20 5 . 11 1 . 00 1 . 0 0

## ~<O**l<a <$**  297.5 3 1 8, 0 3 29 .8 334 . 1 20011109/ 04 7:23 : 55 P M 8-9- 4 a . wsz Page 2**~---- -----'--** **----- ---·**  .. 

### ·-·- - .. 

## ---· -- - - - - - VES 006281

# . 

# . SaMple Hame Type Cone 

# ...- %RSD Fr..gs Wt. Vol • (ppb)**~** UN!( 1 . 680 $267 4 .A1 1 . 00 1.00**~** 5124.0 5090 . 6**1** 

# -.v 

# _-:;:> 0• 

# c:'o I'=\- UHK 0.081 2M 2 .01 1.00 1 . 00 

## T'/_5) R.-s 2798 2118.8 292.3 2910 AJ078().06 

# ,__ 0.021 100 3.72 1 . 00 1.00 

## f}P Re1)broo 104.3 100JI**~~e.** 

### a 96.5 AIO!IJ4.(J2 UNK 1.010 3182 Z-62 1 .00 1.00 Rcplates l2A50 3229.8 311111.3 30!2.0 

### -? O·eo 

## l A!0937-o2 UNK 0.586 1 86$ 1.25 1 . 00 1.00 Roplcales 1872 . 4 1882.1 1&74.0 1830.2 

### ">0•000" A

l 2U9-06 UNK 0.012 73 2.86 . 1 . 00 1 . 00 

# r5> Roplcaleo TOA 72.8 74.& 75.0 At2100.06 UNK 0.014 81 3 . 07 1.00 1 . 00 

### @> Replicates 

### n.o &3.0 82.4 79.9 Al2153-00 UNK 0.017 89 3.&0 1.00 1 . 00

### ~lea 83 . 8 91.7 81l . O 89.1 A

1 2"l8.06 UNK 0.018 92 3 .30 1.00 1 . 00 

# cj5) Rep l i(ates 91 . 0 95.9 91.8 88 . 7 A12466·02 UNI( 0.021 10 3 3. 03 1.00 1. 00 "'P ' Rop latel 98.1 1 03.5 103.5 105.3

### Al2~.()2 1M< 0.023 107 2JJ6 1.00 1 . 00 

### ('I Ropllca1es 104.6 108.0 108.9 104.9 At247 \-0 1 IJNK 0.023 107 4 . 53 1.00 1.00 

# riS>R ... Icolel 101 . 1 IOU 112.4 109.1 CCV liM< 1.000 3171 t,.ro 1.00 1.00 vR-1es 3115.2 3161.2 3111i.3 .12111.6 

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# 4 ... IJNK 0 . 011 89 1.98 1.QO 1.00 1111. 4 70.0 87.2 87.5

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# "!Y(lfAic>l .. \28. 4 1 33 . 3 13<L. 4 13 1. 8 200810911>4 7 : 2J : Sl PM &-9-4a.wsz Poge3


### VES 006282' Sample- Typo CCno 

# ...- %RSD Fblg$ Wt. Vol, ( ppb )**~~~~78-<16** lH( 0.()24 110 1.88 1.00 1 . 00 

# tfJ Repllr;ateo 112.4 IOU 107 .1 110.8 SPIKE WSI16<»35e 1.0« 1 .340 Q)< 0.88 1.00 1 . 00 

## ft!l/ /-...,. 4158. 9 <193.5 4211.2 4:140.4 l>lanlc**~** 0.()52 191 1.39 1 . 00 1 . 00 

# r'!J> R<t>bleS I GilA 200.7 194 . 1 186.7 """' £Pic UN K 1.350 • 237 1.<06 1.00 1.00 

## I (/ 

# 1'/ RepMat;,. 4158.4 

### •m .e**~rT4.1** 4294 .9

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### ~"'\ oi02-1 · UNK 0 .009 64 C ,Sol 1 . 00 1.00 

# '9 Riplleotos 603 65.2 117.2 8•U oi0220.Q.C UNK 0 . 011 TO 4 . 0 1 1.00 1.00 

## 0) Replicates 156.8 13.0 71 . 8 G9.3**eh~ FIL** **TER EO**  lJNK O<R 1873a 1.11 0 . 50 1.50

### -~"S;~83**8** 1 4700 . 7 1884S . 3 1 8941.5 ah304 7.0 1 FILTERED UNK 15.900 3345 1 . 38 .50 7.60

Rep H cal .. 3262 . 2 3339. 4 3362.8 3377.3 

# Jw.; ;. PL.. !:> D• "0 )..',)" 

### -"> 

## o · 01:S: (' 

# \ -f. • l/t;;;.....J 'u.**-~** 

### .• , 

# •y 3h3048-0 1 OIL Y FilTE RED 

# d"'**~** U NK 78.500 1 1 24 4 , 33 1 .00 225 . 00 RfP II ellll 1100.8 1 073.2 1 138.3 11ti5.6**'\')L-~** 

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# 1?1- e-.s;-**a~9-01** UN!< .0.005 20 30 . 66 1.00 1.00 

# r'-.**~ic:stes** 1 2.2 1 8.2 2U 2U ah3()5Q.01 UNK 0.1'77 590 1.68 1.00 1 . 00 Replcalot S82.3 580.3 004.2 565 . 4 

# --;, "' • .0 <!) 0 2._ ah3051-01 UNK .0 . 001 34 14.28 1 , 00 1 . 00 

## N$> Replta"" %7 . 8 3U JU 39.5 al\30 5!141 UNK O<R c951l6 1. 08 0 1 . 00 5000.CO**~** ... 48764 , 1 48528.2 4 9!1:1.9.8 4aao5.2

### ~~~ BLK UNK .0.053 •t31**~** 1 . 00 100**~,** 

# .. - 120 . • ·129 , 1 ·129.7 ·143.9 ai>3Q60.01 UNX OIR 51¥70 1,1)3 0 '.00 5000 .00 Roplc:l ... 51233. 0 5193JA !12253 . 8 !WOO . 

### a till< LINK 4 . 020 ·21 7.75 1 . 00 1 . 00**R~lcatel:** ·281 · 238 · 28.2 · 26.8 CCV UNK 1.030 3286 0.30 1.00 1 . 00 Replic4te• 3262.3 327 5.2 3274. 1**3~.4**

### ~ 2008/09/04 7:13:55 P ill 8·9-'la . wsz P ogc4


### VES 006283

### : Sample' .Name Type Cone 

# .....,. •!,RS O F l ags: Wl V o l. (ppb) CCB**~NK** 0.1 )1 3 n 3.76 1 . 00 1 . 00 Replb J! e s 78.2 80.6 ni. 73.6

.....**7(>(>6** UNK 0 . 06'7 244 8.95 1 . 00 1.00

# ~ Repl i cai<U 263.1 259 . 5 234.4 2 1 7.4 Al0781.()6 U NK 0 . 01 8 9 1 ' 1 ,72 1 . 00 1 . 00 

# r§:> Rllpl i cat&s 90.0 &1 . 3 90 . 1 93.4 AJ09 7 4·02 UHK 0.01 4 78 3 . 73 1. 00 1.00 

# sl'9 Ro p!ICIIe$ 7 5.8 80 . 3 8 1 .4 75.9 AJ1368-09 UNK 0.080 266 2.n 1 .00 1 .00 opRe pll-. 27 4 . 6 287.2 289.1 292 . 9 Al2467· 02 

### VNK 0.04 2 166 1.95 1 . 00 1 . 00 

# rj5) R.,cic;<eo ' 16

7 .! 161.5 164 . 7 16 9.0 AJ2470.0 2 UNK**0. ~0**  473 1 . 64 1 .00 1 . 00 Rep6c:!es 463.8 471 . 0 48 1 . 6 477.4 

## -::::> "''"'., .o 

# I 1 . 00 1. 00 AI247 2.Q2 

### UNK 0.077 276 2.30 

## (\jt>**R~pl ca!e$**  2 68.3 . 273 . 0 282.6 278.9

. A l 24 7 <IL-0 1 UN K 0 . 1 36 46 1 0.76 1 . 00 1 .00 Re

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ciea 456. 1 461 . 7 463.8 462.9 

## --?:> 0 • D "' 

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I247S.01 UN K ,,130 1 2915 

## uo 1 . 0 0 1 . 00 Rep l i<;al"' 1 2698.7 1 2909.2 13023 . 8 1 3028 .9 

# :.> AJ2522.Q2 

### 0 ' OE>-:+ 

# I UNK ..0.003 25 1 7 .4 2 1.00 1 . 0 0 

# t:JD Rep li cates 28.1 28.6 23.8 1ii .J a h3046-0; · liNk . 1 57 . 000 . 2220 1 .42 1. 00 22MO '**Rel)l C~<eS**  :nn .8 22 18. 3 223 5 .4 2250.7 

## <!:> l-,::, 

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# 1>"1-0 UNK ()IR 1 5769 1 . 1 3 0 1 .00 0000 . 00 Re p1icakJs 15 524.4 1 5759 . 7 15862. 1 15 930.5 a h3 000-01 IJtiK OIR 1 6390 1.30 0 1 . 00 0000 . 00 Re pli cates 16102.9 1 6357.2 1 6524.4 165 78. 4 all806H l1 U NK 0/R 17609 1 . 1 2 0 1 . 00 000 0 . 00**Rep ll** **~es** 11345.7 17577 . 3 1 77 1 8.3 17793. 3 CCV U NK 1. 030 3253 0 . 58 1 . 00 1 . 00 Repllcuo 3226 .4 3252.3 3282.0 3289.7

,/ CC B UN K 0.011 11 3. 1 4 1 . 00 1 . 00

### ~es 74 . 3 71.7 69 .6 ' 6 9 . 6 2008109/04 7:l3 : SS PM 8 · 9 · 4• . ws-t 

### P•s • S
VES 006284

### : Sampat NamC! Type CCnc ,.AI>• %RSD Flags Wl V <A . (ppb) SPIKE W$6110402A UNK 1 . 300 4104 1.4\ 1.00 1 . 00



# . qg--1**~plt;Uet** 4029.0 <1090.0 4 13 7 . 1 4160.4

9lANl< UNK 0 . 003 45 4.23 1 . 00 1.00 

# tN.9 Repbtot 4 4.& 4&.2 48.1 44 . 1 MmXSPk UNK 1.360 4288 1 . 6 1: 1 . 00 1.00 

# roof. Roplcoles 41 9U 

## • ms 4324.5 435 1.8 

### -0·**17'2-~**

AJA82S.08:01 UNl< 0.()31 132 4 ,50 1.00 1.00

### ~ Aepibt .. 136.7 1» .8 133.8 123.2**A~** UNI< 0.027 1 20 3 . 71 1.00 1 . 00 

# <:1> F<epblH 125.A 12 1 .0 11 7 . 7 115 . 1**A~~** UNI( 0.059 219 2.02 1 . 00 1. 00 

# cp Replielt .. 219.3 22 1 .3 223.8 213.4 AG4729-® UN K 0 .00 6 55 6 . 99 1.00 1 . 00 

# fj) Replicab!s**~.8** 51.2 58.3 58 . 9 AH36 1 2.Q6 UNK 0 . 009 5 5 6 . 37 1.00 1 ,00 

## I)P Replcates 63 . 1 1)0,8 70 . 4 64 . 0 AH93 57·13 UNK 0 . 009 64 3.8 0 1 .00 1 .00 

# c:P ReDIIitatca 80.5 63.9 00.2 6< . 9 A H 941g. 11 UNK 0 . 033 155 2.78 1.00 1,00

## ~ Replicates 160.0 154 .6 16 1 . 1 155.5**AIOA~7** UNK O.Q35 1 45 1.99 1. 00 1 . 00 

## -N) Rljlll "'l<s 143 . 3 1 4 6 . 0 149.0 142 .7 AI045648 UNK 0.08< 291 1 . 73 1.00 1.00 

## N;:>**~'"''"** 292.1 302 . 4 301 . I 293.9 CCII 

# ._ 0.995 31 44 0.87 

### t:OO 1 . 00 

# vRcpfi"".. 3104.8 a1 .. . e 3 1 05. 4 3180 . 1 CC8 IH< 0.013 75 2.42 1 , 00 1 . 00 

# /Replb ... 7U 76.8 74 .2 76..2 AI0450-01 UNK 0.014 19 2.05 100 1. 00

### ~ RotlllcaiU 8 1.2 74 .7 

# n .• 71.3 AI0461-08 UNl< 0 .006 5 1 4 . 70 tOO 1 . 00 

# c{) Repltatts :18.2 61.3 64 . 5 58.6**04~-07** UNK 0.036 1 56 2.29 1 . 00 1 . 00

### ~ Rop ll c"IH 154 .9 

### m . o tGO . S 1 52 .0 200 8 109/04 1:2l : lS I'M S -9-4 a. wsz. P•gc6


### VES 006285

# ' 

# . •**S.mpl~** Niltn e Type Cone 

# ..- %RSO Flag; WI. Vol . (Wb ) AI0939 ·02 UNK 4 . 800 15020 4.02 1 .00 1 . 00 •**RGI)Iica~Bcs** 15414.5 1535 4.8**1~185 3**  14 1 28.5

# 0941**~** 0 010\tg-- ON!< 0.784 2485 2.49 1 . 00 >.00

Repjlca»s 2539.8. 2509.9**2492.~** 2 3 98.9

## --~ 

## e v

## o~o · 

## coog--- U NK 0.022 1 05 4 .72 1 .00 1 .00 1110975- 02 

## (\!> Rep l lclres 105 . 2 1 08.7 109.0 98.3 Al2392.Q9 U NK 0.021 1 00 4 . 5 8 1 . 00 1 . 00



## · tp**R~p ll** **cabS** 94.9 9 8.6 1 05.9 99 . 7**AJ 46~** **2** UI!K 0.026 116 0 . 95 1. 00 1 . 00 

# <9**Rep~** 11 5.9 1 1 7 .2 11 4 . 6 1 15 . 3 AJ246S.02 UN K 0.02 4 110 4 . 12 1 .00 1.00 

# 119 ROQ i ca'eS 1 0 5.6 107 .7 113 . 4 115.2 Al4824-06 U N

K 0.040 16 1 1 . 01 1.00 · 1 .0 0 

# t'!/Repll-s 1 5 9.8 1 6 2.9 162 .5 15 9.9 Al5 86S.01 U NK 0.022 100 3.50 1 . 00 1 .0 0 /'f>Reptlc!!c.s 1 02 .1 1 01 . 3 109 . 2 1 06

; 1 !- 15 8 72-0 1 UNK**.1 30**  1 2 937 1 . 29 1.00 1 .00**Re~""** 1 2898.7 1 3010.5 13000.1 12960-4**~** 

## 0 Clf\ AH 3059- 0 1 U N

K 11200000.000 1 0360 1.22 1 . 00 5000 .00 Repllc;O.cs 101 91 . 0 10341.2 10 4 29.9 10477.8

# ~ ll:? q"' UN K 11600000.000 1 0782 1.13 1 . 00 5000 . 0 0 

# t>L :::. Re pr.ates 106Ge..O 10787 .1 10873.3 10660.5**h** t!JPd I .X..

- 7 

## "'/:,•0 3. 3, 

### fS . OP,O AH3061.0 1 ON!< 1250000o . OOO 1162 4 

### r.o> 1.00 5000.00**~licatM** 1 1455 . 1 1 1 632 .3 t 17 1 2.5 1 1 695.8 

## ,.....-- . : 331·5""**~** 

### 12910 SP I KE UNK 1 .320 41119 0.82 1 . 00 1 . 00 Rep!IO>tes 4 11 0 . 2 4 1 73.5 4 168.3 4164. 3 CCV UNl< 0.986 3115 1 . 0 1 1. 00 1.00 ·**Repfl~fes.** 3070.4 3 1'17.3 31 34. 3 3 1 39.6 CCB l iNK 0 . 007 57 3 .8 0 1 . 00 1. 00**Re plical~**  57 .7 59. 7**54 ~** **57.~** 

# , -> lr:rvO 

### (t7VO 

# e::- ;;·r**rJ ·**  

# 33 r!{'ooo 0 

# ·> - ) I 

## J,.....**~**



# ()•"' -;:;::;'f · [ 

# n-- Page 7 Z008109/04 7 : 23; 55 PM 0 .

### ~ --? 

# ?- ::J · · 8·9 - 4a .vm 

### VES 006286

# Method 6010 -Test Method for Total Metals by 

# ICP

Maxxam Analytics Inc. 6740 Campobello Rd. Mississauga, Ontario , Canada LSN2L8 1-800-668-0639 

## www.maxxamanalytics.com

VES 006287

### Unique Calibration Standards 

### I. 

## D . tab le for ICP-5 (Axial) ( S tanda rds prepared in 2% HN03) General J. D . Uniqu e 1.0 . BLA NK /ICB/ CCB ICP-WG-0834 STD · A ICP·WC-0835

. STD • B ICP-WC-Q836

CAL - 1 5KNa ICP-WC-Q833 H i-Kna ICP·W0:0856 ICV /CCV ICP-W Q-0 858 ICS-AB ICP-WQ-0841 CR) ICP-WQ-0852 u Buffer IC P-WQ-0857 .

Analys\ I n i t i alS: 

# kc. Date :

### 'UJ(i~ 

# At /]

. ' Maxxam · Analytics Inc. CAM FCD-00279/1 Page 1 of1



### .



### VES 006288

### A utoSample r Report Ta ble : SEPT03A 09/0 3/06 05:25: 2 1 PH A

ut osamp ler Typ e: TYP E TJA QC 

### Positions : 13/19 # 

### Sets : 1 Tab le Name: S E PT03A Sample Positions : 4 2/1 92 Rins e Statio n loc a t ion is rac k - 1 , p o s . - 1.

-- - Racks --- Rack# Type ua·ag e · IIP os L eft Anal . y ses 

### I Pos



# - - --- -**-------------- --** **~---** 

# -- - - - ----- - - 

# -------- - - ------ . - ---- 1 Aux. 

### (L) Rack STD/QC/BLANK 13 20

· 2 

### Sainple (16mm ) Samples 0 1 3 

### Sample {16mml 

### sample s 0 1 4 Sample ( 1 6 tnm) Samp le s 0 1 5 

### S ample ( 1 6mm) Sam p l e s 4 2 1 

### page 1

Sa mp le S e ts Set# Type Prep a re? Description M ethod IIPos · Rack# St ar tPo s 1 

### Normal No maxx am



### -- - P r e paratio n I n fo -- - Set# Uptake U pt ake#2 F inal No Sa mp l es Prep ared . R

a ck # 1 Pos Row Col Samp le N a me



# - ------ ----- ---- ---- l 1 1 

### N O

NE 2 l 

### 2 knahi 15 3 l 3 

### STO · A4 

### 1 4 

### STD - B 5 

### 1 5 

### CAL - B LK 6 l 

### 6 HCL 

### ( 7 ... 1 9 Not Used ) Rack #2 Pos Row Col Sample Name



# ---- ---- ----- --- ---- 1 1 

### l 1 C VAX 2 1 

### 2 lCB 3 1 

### 3 CRI 4 1 

### 4 ICSABAX 5 1 5 

### H I KNA 6 1 6 1602743:BLANK:l.l1 7 

### 1 7 

### 1 602743:SPIKE:1.1 1 8 l 8**1602743 ITRX**  

### S P K :10 9 1 9 

### 1602743:AH3049:DUP 1 0 1 1 0 l 602743 :AH 30 49: 10 11 

### l 11 

### l6 027 43:AH 30 49:D UP 12 1 1 2 

### 1602743 :AH3049:1 00 13 

### i l 

### l602743 : AH3046:10 1 4 2 2 

### 1602743 : AH3046 : 1 00 1 5 2 

### 3 l602743 : AH30 47: 1 0 PSC34 1 50 2 1 

### Dil . Factor
S et # #Used Type



# --- -- - ---- -- · NA- l 

### S tandard -NA - 1 S t an da rd

· NA- l 

### Standard -NA- 1 Sta nd ard -NA - l 

### Sta nda rd

· N

A- 1 

# Qc Standard Set II #Used Type



# --- -- - - - - --- 1 

### · NA- samp le l -NA - 

### S amp le· l -NA · Samp le 1 

### - NA - Samp l e l 

### - N A- Samp l e l -NA - Sample 1 - NA - Sample 1 - NA - Sam ple l -NA- Sample l - NA - Sample 1 

### - NA- Sample l · NA • 

### Sample 1 

### - NA- Sample 1 - NA - Sample l 

### - NA- Samp l e
VES 006289

# . . AutoSampler Repor t Ta bl e : SEPT03A 09/03/08 05 : 25:21 PM 

### page 2 R ack #2 Po s Ro w Co l Samp le Name set # #Us e d Typ e**-- ---** **~---** 

# -- - - - --- - - .. 

# -

16 2 4 

### l602 7 43 :AH 3 0 47 : 1 00 1 -NA - Samp le 17 2 5 

### 1 602 743 :AH 3048: 10 1 -NA - Sample 18 2 6 

### 1602 74 3 : AH30 4 8:100 1 

### - NA - Sample 1 9 2 7 

### 1602743:AH3050 : 10 1 - N A- Sample 20 2 8 160 2743 :AH30 50 : 1 00 1 

### - NA - Sample 2 1 2 9 1602 7 43 :AH30Si : 10 1 

### · NA- Sample 22 2 10 1602743:AH30S l: l 0 0 l 

### -NA - Sample 23 2 ll 

### 1 602743 : AH30 48: 10 0 0 l -NA · Samp l e 2 4 2 

### 1 2 CCV 1 

### . - NA- Sampl e 2 5 ' 3 

### 1 CCB 1 -NA - Samp le 26 3 

### 2 1 6 0 2838 : BLANK : l00 1 

### -NA - Sample 27 3 

### 3 1 602838:RBFMAT : 98 1 

### · NA - Sa mple 28 3 4 

### 1 602838:RBFMAT:980 1 -NA- Sample 29 3 5 

### 1 602838 : MTRX S P K : 96 1 

### - NA - Sample 30 3 6 160 2 838:AH3058:DUP 1 

### -NA - Sample 3 1 3 ? 

### 160 2838 : AH3058:96 1 

### - NA- S ample 32 3 

### 8 160 2838 : AH3055:98 1 

### · NA- Sample 33 3 

### 9 l602838 : AH3056: 1 0 4 1 -NA · Sample 34 3 

### 10 CCV 1 

### - NA - Sample 35 3 11 

### CCB 1 · NA- Sample 3 6 3 12 1602838:AH3052: 1 04 1 -NA - Sample 37 4 

### 1 1602838 : AH3052 :1 040 1 

### -NA - sample 38 4 ' 

### 2 1602838 : AH3052:10400 1 - NA · Sample · 39 4 

### 3 1602838:AH3053:104 1 -NA - Samp l e 40 4 

### 4 16b2838 : AH3 053 : 1040 1 

### - NA - S amp l e 4 1 4 5 1602838:AH3053 : l0400 1 -NA - sample 42 4 

### 6 1602838 : AH3054:100 l - NA- 

### Sample 43 4 7 1602838 :AH3054 : 1000 l · NA- Sa mple 44 4 

### 8 l602838 : AH3054 :1 0000 1 - NA - 

### Sample 45 4 

### 9 l602838 :RBFMAT :98 1 -NA - 

### Sampl e 4 ' 6 4 

### 10 CCV 1 - NA · Samp l e 47 4 ll 

### CCB 1 -NA- sample 48 4 

### 12**1602946:8~:0.2** 

### 1**NA** 

### · samJ)le Rac k #3 Pos Row Col Sample Name S e t # #Used Typ e



# - ------ - - - - - - -- -- --- 

# ------- - - - -- 1 1 1 

### 1 602946:REFMAT:O.l9 l 

### - NA - sample 2 1 2 1602946 : MTRX S PK : 0. 2 1 · NA - Sa mple 3 

### 1 3 1 6 0 2 946 :AH96 49:D UP 1 -NA - Sample 4 

### 1 4 

### 160 29 46 :AH 9649 :0 .19 1 - NA · Sampl e 5 

### l 5 

### 1 602946:AHJ403:0.2 1 · NA- sa · mple · 6 1 6 

### 160 2946 : AH7404:0.2 1 - NA · Sample 

### 7 1 7 . 1 60294 6 : AH8 3 60 : 0.19 l 

### - NA- Sample 8 

### 1 8 1602946:AH8361:0.2 1 

### · NA- Samp l e 9 1 9 160 2 946 :AH96 48:0 .2 1 

## -NA - Samp l e 10 1 

### 10 1602946:A H 9650:0 . 2 1 

### ' -NA - sampl e 11 1 11 

### 160294 6:AH965 l : 0 .2 1 - NA · Sample 12 l 12 CCV 1 · NA- Sample 13 2 

### l CCB 1 

### - NA · Samp l e 14 2 

### 2 1602946 :AH9652 : . 0 . 2 l 

### -NA - Sample 1 5 2 3 

### 160 2 946 : AH9653 :0 . 1 9 l - NA -**Samp~ e** 


### V E S 0 06290

### AutoS amp l er Repo rt Table: SEPT03 A 09/03/08 05:25:21 P M page 3 Rack # 3 Pos Row Col Samp le Name Set 

### It #Used Type



# ----- - ---- -- ---- ---- 

# - - -- -- ---- -- 16 2 4 

### 1602 94 6:AH9654 : 0 . 2 1 -NA - Sample 17 2 

### 5 160 2946:AH 9655 : 0 . 2 1 - NA - Sample 18 2 

### 6 16029 4 6 :AH9 656:0.19 1 

### - NA - Samp le 19 2 

### 1 1602946 : AH 9 6 57 :0 . 2 1 - NA - Sa mp le 20 2 

### 8 1 6029 46 :Al 619 2 : 0.2 1 

### -NA- Samp l e 2 1 2 

### 9 1 602946:A I 6 "1 93 :0 .19 1 - NA - Samp l e 22 2 

### 1 0 1 6029 4 6:A .I 622l:0.19 1 

### -NA - Sample 23 2 

### 11 160294 6: A.I 62 22:0. 1 9 1 -N A - sample 2 4 2 

### 12 l 6029 4 6: AI622 3:0.19 1 

### -NA- Sample 25 

### 3 l 

### 1602946 :A I6825:0. 1 9 l 

### - NA - Samp l e 26 3 

### 2 CCV l - NA- Samp le 27 3 

### 3 CC B l 

### - NA - Sample 28 3 4 

### 1599 7 04 :B LANK : 50 l - NA - Sample 29 3 5 

### 1 599704:REAGBL : 5 0 l -NA - Sample 30 3 

### 6 1599704 : SPIKE:DUP 1 

### - NA- Sample 3 1 3 

### 7 1599704:SPIKE:50 1 - NA- samp l e 32 3 

### · 8 1 599704:AH2002:SO 1 · · NA - 

### Sample 33 3 

### . 9 159970 4: AH 20 03 : 50 l 

### - NA - Sample 34 3 

### 1 0 l 599704 : AH 2 004 : 50 l -NA - S amp l e 35 3 ll 

### 1 5997 04 : AH2005 : 50 l - N A - Samp l e 36 3 

### 12 1 599704:AH2006:50 1 - NA - S amp l e 37 4 l 

### l599 704:AH20 07:50 1 -NA- Samp l e 38 4 

### 2 1 599704:AH2008:50 1 

### -NA - S amp le 39 4 

### 3 1599704 :AH200 . 9 : 5 0 1 - NA- Sample 40 4 4 

### CCV 1 - NA - Sample 4 1 4 

### 5 CCB 1 

### - NA - S ampl e 42 4 

### 6 1599704:AH 201 0:50 1 -NA - Sample 43 4 

### 7 1 5 9 9704:AH2011:50 1 "
- NA- Sample 44 4 

### 8 1599704:AH20 12: 5 0 1 -N A - Samp le 45 4 

### 9 l 599 7 04: A H20l3:50 1 

### - NA - Sample 46 4 

### 10 1599704 : AH20 14:50 l 

### -NA - Samp le 47 4 

# u**59~7Q4 20l5** **50** 

### 1 

### - NA- SamP,le 4 8 4 

### 12 1599704: AH2 . 0 1 6: 50 l - NA - Samp le Rack #4 P es Row Col Sample N a m e Set # #Used Type



# -- ---- - - ---- - - ----- - ___ _ _____ _

# .. _ l l l 

### 1 599 704: AH2017:50 l 

### - NA - Sample 2 1 2 

### 1599704:AH2018:50 l 

### -NA - Samp l e 3 1 3 

### 1599 704: AH20l9 : 5 0 1 

### - NA - Sample 4 1 

### 4 1 5997 04:AH2 02 0: 50 1 

### - NA - Sample 5 

### 1 5 l5997 04: AH202 1 : 50 1 -NA - 

### sample . 6 1 6 

### CCV l 

### - NA ·- S ample 7 1 

### 7 CCB l - NA - Samp le 8 1 8 

### l59 970 7 :BLANK: 50 1 - N A - S ample 9 1 

### 9 l599707 : REAGBL:50 1 

### - NA - S ample 10 l 

### 10 1 5997 0 7 : S PIKE :D UP l 

### - NA - Sample 11 1 

### 11 l 599707:SPIKE : 50 1 " NA - Samp l e 12 1 

### 12 

### l 59 9707:AH2 022 :50 1 - NA- Sample 1 3 2 

### 1 15 99707:AH2 023 : 50 l. 

### - NA - Sample 14 2 

### 2 1 599707:AH2024 : 50 l - NA - Samp le 1 5 2 3 

### 1 599707: AH2 025:50 l -NA - Sample


### VES 006291

### AutoSampler Report Table: SEPT03A 09/03/08 05:25:21 PM page 4 

### Rack 

## 114 Pos Row Col Sample Name Set: 

### ff #Used Type



# -- - ----- ------- ---- - 

# - ----- -- ·- - - 16 2 4 

### 1599707:AH2 026:50 1 - NA · Sample 17 2 5 l599707 :AH 2027:50 1 · NA · Sample 18 2 6 

### 1 599707:AH2028:50 1 

### -NA - Sample 19 2 

### 7 CCV 1 · NA · sample 20 2 

### 8 CCB l 

### -NA- Sample 21 2 

### 9 1599707 :AH 2029:50 1 

### - NA - Sample 22 2 

### 10 1 599707:AH2030:50 1 

### - NA- Sample 23 2 11 

### l599707:AH2031:50 1 

### -NA· Sample 24 2 

### 12 1599707:AH2032:50 1 

### - NA - Sample 25 3 

### 1 1599 707:AH2 033:50 l 

### - NA - Sample 26 3 

### 2 1599707:AH2034:50 1 - NA - 

### Sample 27 3 

### 3 1599707:A82035:50 1 

### - NA - Sample 

### 28 3 4 

### 1599707:AH2036:50 1 -NA - 

### Sample 29 3 

### 5 l599707:AH2037:50 1 

### - NA - Sample 30 3 

### 6 1599 7 07 :AH2 038:50 1 - NA - 

### Sample 31 3 

### 7 1599707:AH2039:50 1 -NA- 

### sample 32 3 8 

### CCV 1 - . NA - 

### Sample 33 3 9 

### CCB 1 ·NA- Sample 34 3 

### 10 ( emp ty ) l 

### - NA - - NA 

### 35 3 11 ( 

### empty ) 

### 1 -NA- -N A 36 3 . 

### 12 ( empty ) 

### 1 -NA - - NA37 4 l 

### ( empty ) 

### 1 - NA- -NA 38 4 2 ( 

### e mpty ) 

### 1 - NA- - NA39 4 

### 3 ( 

### empty ) 1 

### - NA · 

### -NA40 4 4 

### ( empty ) 

### 1 - NA - - NA 

### 41 4 

### 5 ( empty ) l 

### - NA · 

### -NA 42 4 

### 6 ( empty ) 

### 1 - NA - 

### - NA 43 4 

### 7 ( empty ) 1 

### -NA- 

### - NA 44 4 

### 8 ( empty ) l 

### -NA · - NA45 

# • 9 ( empty ) 

### 1 - NA - 

### · NA46 

# • 10 ( empty ) 

### 1 - t<"A - -NA

### 47 4 11 

### ( empty ) 1 

### - NA - -NA 

### 48 4 

### 12 ( 

### emp ty ) 1 

### -NA .. - NA Rack #5 Pos Ro w Col Sample Name set 

### # # U sed Type



# --- ----- - -- --- -- --- - 

# --- - -- ------ l l 1 ( 

### empt y ) 

### 1 - NA · 

### -NA2 

### 1 2 ( 

### empty ) 1 

### -NA - -NA 3 1 3 ( 

### empty ) 1 

### · NA· - NA4 1 4 ( 

### emp ty ) 1 

### · NA - - NA 5 l 

### 5 { 

### empty ) l 

### -NA - -N A 6 l 

### 6 ( 

### empty ) 1 · NA · 

### - NA- ( 7 ... 48 Not u sed)



### VES 006292

### 1681

0 

### ll 

# " 

# ..**~** 

# • "' c 

# ..

. -31 0 

### Profile line : As**~89. 042/**  

### Peak Position : 

## -.02 9863 Peak In tens i ty: 1534.04 Peak Nidth : 9.52765 

## New**Spe~.** 

### S hift 

## at : 0

31**~pectrUM** 

### Shifter Position I



### VES 

### 006293

### A nalysis R eport · 

## qc Sta n dard 09/03/08 11:2 7 : 0 2 AM page 1**r~ ethod** **:** 

### PSC3 4 Sample N a m e : HCL Operator: gbu Run Ti me: 09 / 0 . 3/08 11 :21: 36 Comme nt : Mode: CCNC C o rr . Factor: 1

Elem A.g Al 

### As B Ba 

### Be 

### Bi Units ppm p pm pp m ppm ppm pp m ppm Avge - . 0 017 . 0 4 78 .0014 . 0 1 85 -.00023 .00 01 7 - . 0079 # 1 - . 0005 . 0653 .0054 .0 1 ( 3 -. 00 0 07 . 00023 - . 00 9 1 #2 -. 0029 . 044 7 - .0047 .0180 - . 00037 . 0 001 4 - . 00 30 #3 - .00 1 6 .0333 . 0035 .0 201 - . 00026 .00016 -. 0 117 Ele m Ca Cd Co 

### Cr Cu 

### Fe K 

### Uni ts ppm p p m ppm ppm ppm ppm p p m Avge .0555 - . 00 0 66 -. 0015 - . 0017 - .00 2 7 . 00 16 - . 0598 # 1 .0569
- . 00005 . 0 0 05
- .0004 . 000 4 .0037 -. 0831 # 2 .0546 -. 0 011 6 - . 001 4 - . 0036 - . 0028 . 0002 -. 08 4 1 #3 .0551 - ,0007 6
- . 0035 - .0 011 - . 0057 .0010 - . 0 1 22 Ele m 

### Mg M n 140 

### Na 

### N i · p 

### 2203/ l U

nits ppm ppm ppm ppm ppm ppm pp m Av ge . 00 1 2
- . 00002 - . 00 1 2 . 0625 . 0 00 3 .0190 - .0027 

### #1 .0167 . 00014 -. 0003 .0660 . 0012 . 0193 - . 0048 

### # 2 -. 0060 -. 00023 - . 0027 .062 6 -. 0004 . 0232 - . 0022 #3 • . 00 71 .0 0003
- .0 007 . 0588 .0003 . 0. 1 46 -. 0011 Slem 22 03/ 2 

## s Sb 1960/1 3: 960/2 Si Pb Uni ts pp m p pm pp m ppm ppm ppm pp m Avge
- . 0009 . 0 1 85
- . 0042 .0064 - · . 0 000 .0 407 - . 00 1 5 

### #1 - . 0003 . 021 9
- . 0045 . 003 4 .0 04 2 

### . .0447 - . 0018 #2 - . 0010 . 0 1 87 - .0078 .0095 ·. 0 047 . 038 1 - . 0 01 4 #3 · .0013 .0149 -.0 002 .0065 . 0 00 4 .0393 - . 0012 Elem Se · S n Sr T i T l 

## u 

## v Un its ppm p pm ppm ppm pp m pp m ppm A

v ge . 00 2 1 .0015 . 000 11 -.0 00 41 . 0010 - .0399 - . 00 15 

### #1 .0040 . 0035 .000 1 7 .00025 . 0020 .0 0 4 0 .0 002 112 .000 0 -. 0005 . 000 11
- . 00046 . 00 1 6 - . 1 004 - . 0030 1#3 .0024 .0 0 1 6 . 000 06 - . 00 1 02 - . 0007**.023~** 

### -. 00 1 7 E lem y 

### 2 13Zn 

### zn 

## Z r Units pprn ppm pp m ppm Avge 49.07 . 0005
- . 0005 - . 0022 #l 48 . 79 .0010 . 0011 - . 000 4 112 

### 49.29 . 0003
- . 00 1 2 - .0024 1! 3 49.15 . 0003 -. 0014 • - . 0038



### V E S 006294S t andardiza t ion Rpt. 09/03/08 11:34: 5 9 AM 

### page 1 Met h od : PSC34 Standa rd : CAL - BLK / Run Time: 09/03/08 11 : 29:30

Elem Ag ·Al 

### As B 

### Ba Be Bi Avge . 0267 .7986
- . 0053 .3 1 82 . 02266 - . 1 0 1 28 .0536 

### lfl .0520 . 8446 - .0 050 . 3568 . 03098 -. 09095 .1 699 #2 . 0430 .7666 - . 0080 . 3 1 38 .0 1.89 9 · - .10495 . 0910 113 - . 0150 .7846
- .0030 .2839 . 01799 - .10795 - .1 000 Ele m 

### Ca Cd Co Cr Cu F e Fe Avge .0366 .09762 - .0243 . 0107 . 2499 .0 340 . 0916 # 1 .0400 . 145.93 .0740 .0 180 . 3378 .0790 . 1149 112 .0340 . 08996 -. 0500 . 0040 .21 59 .0190 . 0730 #3 .0360 . 05697
- . 0970 . 0 1 00 . 1 959 . 0040 .08 70 E l e m K M g Mg Mn M o 

### Na Ni A

v g e - . 6567 . 0210 . 0463 . 00500 - . 0160 34 . 31 .04 1.3 #1. - . 758 6 .0360 .1429 .00700 .0730 35 . 66 . 0780 112 - . 5607 .0290 . ()050 . 00600 - .0520 33.52 . 0430 #3 - . 6507 - . 0020
- .0090 .00200 - . 0690 33.75 . 0030 B l e m p 2203/ 1 2203/2 

## s Sb 1. 96 0 / 1 1 960/2 Avge . .3711 .1003 .061.3 . 3332 .0956
- . 0 4 63 .01.17 

### Ill .39 68 - · . 3118 . 1959 . 324.8 . 1 95 9
- . 1199 .1059 

### lf.2 . 38'1.8 . 6 1 07 .0320 . 3408 . 12 09 .0 450 - . 0940 #3 .3348 . 0020 7. 0440 .3338 - . 0300 - . 0640 . 0230 E l em 

### Si Sn Sr T i T l 

## u 

## v Avg e .1593 .0 330 . 072 6 3 .02 1 99 - . 03 70 .1.039 .0077 #1 . 21 5 9 .05 ' 90 .0 8296 .1 6392 . 0040 . 1 339 . 0 2 90 #12 . . 1 339 . 0390 .06997 - . 03098 - .0210 . 12 1 9 .00 1 0 »3 .1 279 .0010 . 06497 -. 066 . 97 

### - · . o9 " 4o .OS60 - . 007 0 E le m 2l3Zn Zn Zr A.vge - . 003 0 - . 0 3 33 - 1 . 102 U

1 .0 0 20 . 0440 -1.31.6 #2 - . 0050 -. 0650 -1..871. #3 - . 0 0 60 - . 0790
- 1. . 9 18



### VES00629 5

### Standa rdi zat ion Rpt. 09/03 / 08**11 3~:45**  AM 

### page 1 Method: PSC34 Standard: 

### STO·B ./ 

### Run Time: 09/03/08 11:35:03

E lem Ag 

### Pe 

### Mg Ko p 

## s Sb 

### Avg e l3 . 1 4. 4.0.29 5 .232 22.24 20.36 9 . 603 5.658 #1 13.21 4 0.25 5.228 21.87 20.29 9 . 569 5.477 #2 13.19 4 0.41 5.265 22.43 20.52 9. 710 5.821 #3 l3 . 03 40 . 20 5.203 22.42 20. 26 9 .5 30 5.674 El e m Si Sn 

### Ti 213Zn Zr 

### Avge 14.21**12 .6~**  

### 180.0 4 5.695 212. 1



### . Ill 14.22 12.70 180.06 5 .702 212.6

#2 14 .31 12.77 180.60 5 . 714 

### 212.6 lt3 1'1 . 11 

### 12.6 1 179 . 46 5.668 2H.2



### VES 006296

### Standardization Report 09/03/08 11 : 39:45 AM 

### page 1 

### Method: PSC34 Slope s 

### Conc(SIR)/IR Element wave len High std Low 

### std 

### Slope Y - intercept Date Standardized Ag 328.068 

### STD-B CAL-BLK .038308 - . 00102 1 09/03/08 11 : 35 : 03 Al 308.215 

### STD-A CAL-BLK . 2801 75 . -. 223748 09/03/08 11:35:03 

### As 189.042 

### STD - A CAL-BLK .087507 .00 0466 09/03/08 11:35:03 

### B H9.678 

### STD - A CAL-BLK . 040724 - . 012957 09/03/08 11:35:03 

### Ba 455.404 

### STD-A CAL-BLK .026968 -. 000611 09/03/08 11:35:03 

### Be 313.042 

### STD-A CAL-BLK . 006340 .000642 09/03/08 11:3 5:03 

### 8i 223.061 

### STO- A CAL-8LK . 080 459 - .004316 09/03/08 11:35:03 

### Ca 317.933 

### STD - A CAL-BLK .614555 - .022522 09/03/08 11:35:03 

### Cd 126.502 

### STO-A C AL -BLK . 004679 - .000457 09/03/08 11:35:03 

### Co 228.616 

### STO-A CAL-BLK .026438 . 000643 09/03/08 11:35:03 Cr 

### 267.716 

### STD-A CAL-BLK .06 9487 - . 000711 09/03/08 11:35:03 

### Cu 324.753 

### STD-A CAL-BLK .034165 - . 008537 09/03/08 11:35:03 

### Fe 259.940 

### . STD - 8 CAL-BLK .049758 - . 004559 09/03/08 11:35 :0 3 

### Fe 271.441 

### STD-A CAL-BLK . 985811 -. 033501 09/03/08 11:35:03 

### K 766.4 91 knahi 1 5 

### CAL - BLK .784520 . 0 41072 09/03/08 11:35:0 3 

### Mg 279.078 

### STD-B- CAL - BLK . 19284 1 -. 008 9 31 09/03/08 11:35:03 

### Mg 383 .231 

### STD - A CAL-BLK . ?26263 -.015244 09/03/08 11 :3 5:03 Mn 

### 257 . 610 

### STD-A CAL-BLK .037608 - . 0001.88 09/03/08 11:35:03 

### M

o 202.000 

### STD - 8 CAL-BLK . 022 468 .000359 09/03/08 11:35:03 

### Na 588.995 knahi 15 

### C AL- BI ,K . 767437 -37 . 2071 09/03/08 11:35:03 

### Ni 23l.60 4 

### STD-A- C AL- 8 L K . 033002 -. 001363 09/ 03/08 1 1: 35:03 p 

### 1 78.287 

### STO - B CAL - 8LK .250183 - .092855 09/03/08 11 : 35:03 2203/1 220.351 

### STD-A CA!,-8LK .0 1 7987 -.001804 09/ 03 /08 1 1:35:03 2203/2 220.3 52 

### $1'0-A CAL - 8LK . 034151 - . 002094 09/03/08 11:35:03 

## s t82 .0 40 

### STD - 8 CAL-B L K . 215749 -. 071880 09/03/08 11:35:03 

### Sb 206.838 

### STD-B CAL-8 LK . 089113 - . 008521 09/03/08 11:35:03 19 60/1 196.021 

### STD·A CAL-BLK .078576 .003639 09/03/08 11:35:03 196 0/2 t96. 022 

### STO-A CAL-BLK .0 7 530 0 -. o·oo878 09/03/08 11:35 :0 3 

### Si 251.612 

### ST0 - 8 CAL-BLK . 071702 -. 011419 09/03/08 11:35:03 

### Pb 220.353 

### NONS 

### NONE .000000 .000000 

### * NOT STANDARDIZED se 196 . 026 

### NONE NONE .000000 .000000 

### *NOT STANDARDIZED Sn 189 . 989 

### STO-B CAL - BLK .079085 -.002609 09/03/08 11:35:03 

### Sr 407.771 

### STO-A CAL-BLK . 006924**.0()0~03** 

### 09/03/08 11:35:03 

### Ti 334 . 941 

### STD-B CAL-BLK .005555 - . 000122 09/03/08 11:35:03 

### Tl 190 .864 

### STD - A CAL - BLK .162254 .006000 09/03/08 11:35:03 

# u 367.000 

### STD-A CAL-BLK 1. 

### 01504 - .1 05512 09/03/08 11:35:03 

### v 292.402 

### STD-A CAL-8LK .065509 -. 000502 09/03/08 11:35:03 y 

### 371.000 

### NONE NONE 

### 1.00000 .000000 

### *NOT STANDARDIZED 213Zn 213.856 

### STD - B CAL-8LK .087766 .000263 09/03/08 11:35:03 

### Zn 206.200 

### STD - A CAL-BLK .016837 . 000561 09/03/08 11 : 35:03 

### Zr 339.198 

### ST0-8 CAL-8LK .004682 .007968 09/03/08 11:35:03



### V E S 00 6 297

### Sr.andardi.zar.ion R p t. 09/03/08 11: 4 5 : 5 7 AM 

### pag e 1 

### Method : P S C34 

### S t an d ard : STD-A 

# / Run Time : 09/03/08 11 : 40 : 27



### Blem Al As B 

### Ba B e Bi Ca 

### · Avge 6.625 5. 74 8 23.0 7 32 . 329 77.2 2 0 5 . 780 1 6. 4 9

#1 . 6.597 5. ?88 23.06 32 . 279 76 . 978 5 . 776 16.47 112 6.587 5 . 7 8 3 2 3 ' . 0 6 32 .27 4 77 . 104 5 . 704 1 6 ..44 #3 6 . 6 93 5 . 673 23.10 32.435 77 . 577 5 . 8 6 1**1~.** 57 

### Elem Cd .C o 

### C r Cu 

### Fe Mg M n Avge 11 2 .40 38.07 14.32 26.58 10 . 1 4 6 .2 49 25 . 708 # 1 112 . 2 1 3 7 .99 

### 14.31 26.60 10 . 1 4 6 .247 2 5 .683 112 112.20 

### 38.01 14 . 29 26.5 2 10.08 6. 203 25 . 655 #3 112 . 80 38 . 22 1 4 .3 5 26 . 61 10. 1 8 6 .2 96 25.785 

### E

l em Ni 2203/l 2203 / 2 1960/1 1960/2 

### Sr Tl A

v ge 15 .42 .58 . 12 30.70 6 . 3]:1 6 .350 6 4 .874 6 . 128 

### IU 15 . 37 57.65 30.58 6 . 173 6.228 64. 728 6.030 112 15 . 33 58.78 30 . 72 6 .4 81 6.398 6 4.7 71 6.061 

### U3 1 5.54 57.91 30 . 80 6. 278 6.425 6 5.123 6 . 294 

### Elem 

## u v Zn A

v ge 4.537 7 . 353 130.1 11 1 4 . 555 7 . 348 1 2 9. 9 112 4.450 7.333 129 . 8 11 3 4 . 608 ' 7 . 3 7 7 130 . 5 

# h ? 2$, 

# 7 o S · 

# ---- -

Clf 

# .i %. 58



# - f)'

## ?

VES 006298

### Standardization Report 09/03/08 11 : 45:57 AM page l M

eth o d: I? SC34 ' Slope a 

### Conc(SIR)/IR E l ement tolavelen High std Low 

### std Slope ¥ -intercept Da t e Standardized A

g 328 . 068 STD - B CAL - BLK .038308 - .001021 09/03/08 1 1: 40 : 27 A

l 308.2 1 5 STD-A CAL-BLK . 336005 - .268334 09/03/08 11:40:27 As 1 89 . 042 STD-A CAL-BLK . 086904 . 000463 09/03/08 1 1:40 : 27 B 249 . 678 STD - A CAL -BLK . 044071 -.014022 09/03/08 11:40 : 27 Ba 455 ' .404 STD - A CAL-BLK . 030954 - .00070 1 09/03/08 11:40:27 Be 31 3.04 2 STD - A CAL - BLK .006468 . 0 0 0655 09/03/08 11 :4 0 : 27 

### Bi ' 2 23 . 061 STD-A CAL - BLK .087354 - .004686 09/03/08 11:40:27 Ca 317.933 STD - A CAL-BLK . 607898 - .022278 09/03/08 1 1:40 : 27 Cd . 226 . 502 STD-A CAL - BLK .Q04457 - -000 4 35 09/03/08 11 :40:27 C

o 228 . 6 1 6 STD-A CAL - BLK . 026260 .0 0 0639 09/03/08 11 :4 0 : 27 Cr 267.716 STD - A CAL - BLK . 0700 2 9 - .000747 09/0 3 /08 1 1 ; 4 0:27 Cu 324.753 STD - A CAL-B LK . 038153 - .009534 09/03/08 11:40 : 27 Fe 259 . 940 STD - B CAL -BLK .049758 - . 004559 09/03/08 1 1 :40 : 27 F e 271. 4 41 STD - A CAL-BLK .989973 - . 0336 4 2 09/03/08 11 : 40 : 27 K 766 . 491 knahi_15 CAL - B L K .784520 . 041072 - 09/03/08 11:40:27**~lg** 

### 279.078 STD - B CAL - BLK . 1928 4 1 -.008931 09/03/08 11 : 40 : 27 

### Mg 383 . 231 STD - A CAL - BLK . 802884 - -0 1 6852 09/03/08 1 1 : 4 0:27 

### M

n 2 57.6 1 0 STD - A CAL-B LK -038 9 25 - .0001.95 09/03/08 11 : 40 : 27 

### Mo 202.000 STD-B CAL - BLK . 022468 .000359 09/03/08 1 1:40:27 Na 588.995 knahi 15 CAL-BLK . 767 4 37 -37 - 2071 09/03/08**1~:40 27**  

### Ni 231.604 STD - A 

## - CAL - BLK .032462 - . 001341 09/03/08 1 1 : 40 : 27 

### p • 1 78.287 STD - B CAL-BLK . 250183 • -092855 09/03/08 11 :4 0:27 2203/1 220.351 STD - A CAL - B L K .017296 . - .00173 4 09/03/08 11:40: 2 7 2203/2 220.3S2 S TD - A CAL - BLK .0328 1 5 - . 0020 1 2 09/03/08 11: 4 0:27 

## s 1 82.0 4 0 STD - B CAL - BL K . 2 1 57 4 9 - . 071880 09/03/08 1 1 :40:27 

### Sb 2. 06-838 STD - B CAL-BLK .089 11 3

_ . _00852 1 09/03/08 11 :4 0:27 1 960/ 1 196.021 STD-A CAL-BLK . 078514 .003636 09/03/08 11 : 40:27 1960/2 1 96 . 022 STD - A CAL-BLK . 078300 - - 000913 09/03/08 11:40: 2 7 S i 25 1. 612 STD - B CAL-BLK . 071702 -.0114 1 9 09/03/08 11:40:27 

### Pb 220.353 NONE NONE . 000000 .0 0 0000 *NOT STANDARDIZED S e 1 96 . 026 NONE NONE . 000000 . 000000 *NOT STANDARDIZED So 189.989 S'I' D -B CAL-BLK .079085 - .002609 09/03/08 1 1 :40:2 7 Sr 407 . 771 STD -A CAL - BL K . 007716 - .000560 09/03/08 1 1:40:27 Ti )34. 9 ' 41 STD - B " 

## CAL - BLi< :oo55SS**:** 

### oooi:22 o ·9/03/0"8**11:~0 :2** **'** 

### T1 1 90.864 STD - A CAL-BLK .164 5 66 .006066 0 9/03/08 1 1 :40 :2 7 

## u 367.000 STD - A CAL-B L K 1. 1 4083 - .118587 09/03/08 11:40 : 27 

### v 292.402 STD-A CAL - BLK .067981 -. 000521 09/03/08 11:40 : 27 y )71. 

### 000 NONE NONE 1 .00000 .000000 *NOT STANDARDIZED 2 1 3Zn 213.856 STD - B CAL-BLK .087766 -000263 09/03/08 1 1 : 40 : 27 Z

n 206.200 STD - A CAL - BLK .0 1 538 1 . 000512 09/03/08 1 1: 40 : 27 Zr )39.198 STD - B CA):,-BLK .004682 . 007968 09/03/08 11:40 : 27



### VES 006299