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                            Funding & Awards
 Method Development and Validation of Comparative Finished Fiber Analysis Using Nano-Sampling Cryomicrotomy and Time-of-Flight Secondary Ion Mass Spectrometry
Award Information
Awardee
              NC State University
Award #
              2009-DN-BX-K216
Funding Category
              Competitive
Location
                    Raleigh, NC
Congressional District
              4
Status
              Closed
Funding First Awarded
              2009
Total funding (to date)
              $619,141
Original Solicitation
              NIJ FY 09 Research and Development in Forensis Analysis of Trace Evidence:  Invited Full Proposals
Description of original award (Fiscal Year 2009, $619,141)
This proposal is part 1 of a multi-part program. It will focus on method development to establish more rigorous standard methods of analysis for finished fibers with negligible nano- or micro-level destruction of the fiber, thereby essentially having an insignificant negative impact on the preservation of evidence. This will be achieved via sub-micron level sample removal using cryomicrotomy (microscopic cold cutting with a diamond blade) followed by Time-Of-Flight Secondary Ion Mass Spectrometry (TOF-SIMS) analysis of the surface and cross-section of the pre-dyed fibers.
ca/ncf



  
Grant-Funded Publications
        
                      Time-of-flight-secondary ion mass spectrometry method development for high-sensitivity analysis of acid dyes in nylon fibers
                  Advancing the Forensic Analysis of Dyed Fibers by Time-of-Flight Mass Spectrometry
                  Method Development and Validation of Comparative Finished Fiber Analysis Using Nano-Sampling Cryomicrotomy and Time-of-Flight Secondary Ion
                  Liquid Chromatographic and Mass Spectrometric Analysis of Dyes for Forensic Purposes

  
Date Created: September 23, 2009
    
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                  An Examination of the Law Enforcement Role in Implementing Extreme Risk Protection Orders
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