Company: Did you have 4 test runs?

Plant: If yes, Highlight Columns F and H, and right-click and selec

Unit: You will need to adjust the formulas in the Average Column 

1 2 3 Average

Normal Normal Normal P May need to fix row height if text too long.

6/15/2011 6/15/2011 6/16/2011

13:32 16:34 9:32

15:16 18:14 11:14

1.04E-02 6.05E-03 7.04E-03 7.84E-03 P

9.41E-03 5.35E-03 6.37E-03 7.04E-03 P

1.84E-03 3.09E-03 4.57E-03 3.17E-03

1.66E-03 2.73E-03 4.14E-03 2.84E-03

2.46E-03 1.85E-03 1.17E-03 1.83E-03 P

2.21E-03 1.64E-03 1.06E-03 1.64E-03

1.23E-02 1.24E-02 3.40E-02 1.95E-02 P May need to hide rows if one fraction only.

1.11E-02 1.09E-02 3.08E-02 1.76E-02 P

2.70E-02 2.33E-02 4.68E-02 3.24E-02

2.44E-02 2.06E-02 4.23E-02 2.91E-02

145.5 145.3 145.1 145.3

29.224 29.196 29.990 29.470

20.6 21.9 22.5 21.7

Average Flue Pressure, in. Hg 29.51 29.42 29.54

Flue Gas Moisture, percent by volume

Total Hexavalent Chromium Emissions

mg/dscm

lb/hr

Stack Parameters:

Average Gas Temperature, °F

Average Gas Velocity, ft/sec

mg/dscm

lb/hr

M0061-Backhalf Emissions

mg/dscm

lb/hr

M0061-KOH Emissions

lb/hr

M0061-Rinse Cr Emissions

mg/dscm

lb/hr

mg/dscm

HEXAVALENT CHROMIUM (CR 6+) TEST RESULTS SUMMARY

Motiva Enterprises LLC

Norco Refinery

RCCU Stack

Test Run Number

Source Condition

Date

Start Time

End Time

M0061-Filter Emissions
29.52 29.43 29.55

17.1 16.4 17.3 16.9

1.4 1.4 1.6 1.5

30.792 30.680 30.832

57.503 57.181 60.216

Isokinetic Variance 97.4 98.9 101.6

Barometric Pressure, in. Hg

Average %CO

2

 by volume, dry basis

Average %O

2

 by volume, dry basis

Dry Molecular Wt. of Gas, lb/lb-mole

Gas Sample Volume, dscf
 F and H, and right-click and select "Unhide".

e formulas in the Average Column for the runs you want to use.

t if text too long.

one fraction only.
Norco Refinery

RCCU Stack

Test 1 (13:40-16:58)

6/16/11

Sample

Results Concentration Emissions Rate

Parameter (ug) (ug/dsM3

) (lbs/hr) gr/dscf gr/acf Comment

Antimony < 11.80 < 3.40 < 3.26E-03 < 1.48E-06 < 1.00E-06 DLL

Arsenic < 1.20 < 0.35 < 3.31E-04 < 1.51E-07 < 1.02E-07 BDL

Beryllium < 0.30 < 0.09 < 8.28E-05 < 3.77E-08 < 2.54E-08 BDL

Cadmium < 0.30 < 0.09 < 8.28E-05 < 3.77E-08 < 2.54E-08 BDL

Chromium 3.10 0.89 8.56E-04 3.90E-07 2.63E-07 ADL

Cobalt 2.84 0.82 7.83E-04 3.57E-07 2.41E-07 ADL

Lead < 0.60 < 0.17 < 1.66E-04 < 7.55E-08 < 5.09E-08 BDL

Manganese 14.44 4.16 3.98E-03 1.82E-06 1.22E-06 ADL

Nickel 47.79 13.76 1.32E-02 6.01E-06 4.05E-06 ADL

Selenium < 4.00 < 1.15 < 1.10E-03 < 5.03E-07 < 3.39E-07 DLL

Test Support Data

Sample Volume (Vmstd) .................................................................................................................................................................... 122.665

Volumetric Flowrate (acfm) .................................................................................................................................................................... 379,651
Volumetric Flowrate (dscfm) .................................................................................................................................................................... 255,913

%O2 .................................................................................................................................................................... 1.6

%CO2 .................................................................................................................................................................... 17.3
Norco Refinery

RCCU Stack

Test 2 (09:20-12:41)

6/17/11

Sample

Results Concentration Emissions Rate

Parameter (ug) (ug/dsM3

) (lbs/hr) gr/dscf gr/acf Comment

Antimony < 8.13 < 2.37 < 2.25E-03 < 1.04E-06 < 6.98E-07 DLL

Arsenic < 1.20 < 0.35 < 3.32E-04 < 1.53E-07 < 1.03E-07 BDL

Beryllium < 0.30 < 0.09 < 8.31E-05 < 3.82E-08 < 2.58E-08 BDL

Cadmium < 0.30 < 0.09 < 8.31E-05 < 3.82E-08 < 2.58E-08 BDL

Chromium 1.97 0.57 5.46E-04 2.51E-07 1.69E-07 ADL

Cobalt 1.85 0.54 5.12E-04 2.36E-07 1.59E-07 ADL

Lead < 0.60 < 0.17 < 1.66E-04 < 7.64E-08 < 5.15E-08 BDL

Manganese 22.24 6.49 6.16E-03 2.83E-06 1.91E-06 ADL

Nickel 29.78 8.68 8.25E-03 3.79E-06 2.56E-06 ADL

Selenium < 3.90 < 1.14 < 1.08E-03 < 4.97E-07 < 3.35E-07 DLL

Test Support Data

Sample Volume (Vmstd) .................................................................................................................................................................... 121.13

Volumetric Flowrate (acfm) .................................................................................................................................................................... 376,405
Volumetric Flowrate (dscfm) .................................................................................................................................................................... 253,643

%O2 .................................................................................................................................................................... 1.6

%CO2 .................................................................................................................................................................... 17.3
Norco Refinery

RCCU Stack

Test 3 (13:50-17:11)

6/17/11

Sample

Results Concentration Emissions Rate

Parameter (ug) (ug/dsM3

) (lbs/hr) gr/dscf gr/acf Comment

Antimony < 17.70 < 5.20 < 4.90E-03 < 2.27E-06 < 1.53E-06 DLL

Arsenic < 1.20 < 0.35 < 3.33E-04 < 1.54E-07 < 1.04E-07 BDL

Beryllium < 0.30 < 0.09 < 8.31E-05 < 3.85E-08 < 2.59E-08 BDL

Cadmium < 0.30 < 0.09 < 8.31E-05 < 3.85E-08 < 2.59E-08 BDL

Chromium 2.85 0.84 7.90E-04 3.66E-07 2.46E-07 ADL

Cobalt 4.11 1.21 1.14E-03 5.28E-07 3.55E-07 ADL

Lead < 0.60 < 0.18 < 1.66E-04 < 7.71E-08 < 5.19E-08 BDL

Manganese 4.97 1.46 1.38E-03 6.38E-07 4.30E-07 ADL

Nickel 46.57 13.69 1.29E-02 5.98E-06 4.03E-06 ADL

Selenium < 3.20 < 0.94 < 8.87E-04 < 4.11E-07 < 2.77E-07 DLL

Test Support Data

Sample Volume (Vmstd) .................................................................................................................................................................... 120.164

Volumetric Flowrate (acfm) .................................................................................................................................................................... 374,034
Volumetric Flowrate (dscfm) .................................................................................................................................................................... 251,755

%O2 .................................................................................................................................................................... 1.6

%CO2 .................................................................................................................................................................... 17.3
Concentration Emissions Rate

Parameter

Antimony < 3.66 < 3.47E-03 < 1.60E-06 < 1.08E-06

Arsenic < 0.35 < 3.32E-04 < 1.53E-07 < 1.03E-07

Beryllium < 0.09 < 8.30E-05 < 3.82E-08 < 2.57E-08

Cadmium < 0.09 < 8.30E-05 < 3.82E-08 < 2.57E-08

Chromium 0.77 7.30E-04 3.36E-07 2.26E-07

Cobalt 0.85 8.11E-04 3.73E-07 2.52E-07

Lead < 0.17 < 1.66E-04 < 7.63E-08 < 5.14E-08

Manganese 4.03 3.84E-03 1.76E-06 1.19E-06

Nickel 12.04 1.14E-02 5.26E-06 3.54E-06

Selenium < 1.08 < 1.02E-03 < 4.70E-07 < 3.17E-07

Volumetric Flowrate (acfm) .................................................................................. 376,697

Volumetric Flowrate (dscfm) ...................................................................................................................253,770

%O2 ...................................................................................................................1.6

%CO2 ...................................................................................................................17.3

Test Support Data

(mg/dsM3) (lbs/hr) gr/dscf gr/acf

Motiva Enterprises LLC

Norco Refinery

RCCU Stack

Average Results

June 16 and 17, 2011
Company:

Plant:

Unit:

1 2 3 Average

Normal Normal Normal

6/16/2011 6/17/2011 6/17/2011

13:40 9:20 13:50

16:58 12:41 17:11

379,651 376,405 374,034 376,697

255,913 253,643 251,755 253,770

144.6 144.8 144.9 144.8

31.471 31.201 31.005 31.226

21.7 21.9 21.9 21.8

Flue Gas Moisture, percent by

volume

Stack Parameters:

M2 Gas Volumetric Flow Rate, acfm M2 Gas Volumetric Flow Rate, 

dscfm

Average Gas Temperature, °F

Average Gas Velocity, ft/sec

Date

Start Time

End Time

Source Condition

METALS TEST RESULTS SUMMARY"

Motiva Enterprises LLC

Norco Refinery

RCCU Stack

Test Run Number

21.7 21.9 21.9 21.8

29.51 29.57 29.54

29.52 29.58 29.55

17.3 17.3 17.3 17.3

1.6 1.6 1.6 1.6

30.832 30.832 30.832

122.665 121.130 120.164

Isokinetic Variance 97.7 97.3 97.3

Average Flue Pressure, in. Hg

Barometric Pressure, in. Hg

Average %CO2 by volume, dry basis

Average %O2 by volume, dry basis

Dry Molecular Wt. of Gas, lb/lb-mole

Gas Sample Volume, dscf

volume
SEMIVOLATILE TEST RESULTS SUMMARY Page 1 of 1

Company:

Plant:

Unit:

Location:

Test Run Number 1 2 3 Average

Source Condition Normal Normal Normal

Date 6/20/2011 6/20/2011 6/21/2011

Start Time 12:20 16:50 10:00

End Time 15:40 20:17 13:43

Sample Duration (min): 192.0 192.0 192.0 192.0

Average Gas Temp (oF): 144.3 144.1 144.5 144.3

Average Gas Temp (oC): 62.4 62.3 62.5 62.4

Fractional Gas Moisture Content: 0.22 0.22 0.22 0.22

Gas CO2 Content (%vol): 17.7 17.7 17.5 17.6

Gas O2 Content (%vol): 1.6 1.6 1.5 1.6

Excess Air (%): 8.1 8.1 7.5 7.9 Lines denoted by yellow should 

Gas Wet MW (lb/lbmole-mole): 28.06 28.05 28.03 28.05 Lines denoted by purple should 

Average Gas Vel (ft/sec): 31.69 33.15 32.23 32.36

Average Gas Vel (m/sec): 9.66 10.10 9.82 9.86

Measured Volumetric Flow Rate

 Q (actual ft3/min): 382,332 399,933 388,859 390,375

 Q (actual m3/min): 10,827 11,325 11,011 11,054

 Qstd (std ft3/min): 329,103 343,659 333,732 335,498

 Qstd (Nm3/min): 8,682 9,081 8,830 8,864

 Qstd(dry) (dry std ft3/min): 256,772 267,946 260,341 261,686

 Qstd(dry) (dry Nm3/min): 6,774 7,081 6,888 6,914

Sample Volume (dry std ft3): 115.828 118.473 115.407 116.569

Sample Volume (Nm3): 3.056 3.109 3.050 3.072

Isokinetic Variance 96.3 94.4 94.6 95.1

Motiva Enterprises LLC

Norco Refinery

RCCU 

NEVER PUT EQUATIONS IN 

THE CELLS IN THIS TABLE. IF 

A CHANGE IS NEEDED, 

CONSULT WITH THE 

TECHNICAL DIRECTOR.

Stack
Lines denoted by yellow should always be left visible

Lines denoted by purple should be visible if measured

T EQUATIONS IN 

N THIS TABLE. IF 

GE IS NEEDED, 

LT WITH THE 

AL DIRECTOR.
Analytes

N-Nitrosodimethylamine 3.86 ND < 1.18 < 1.13E-03 3.85 ND < 1.17 < 1.15E-03 3.86

Pyridine 52.60 ND < 16.04 < 1.54E-02 52.60 ND < 16.04 < 1.57E-02 52.60

Phenol (CCC) 3.91 J 1.19 1.15E-03 3.25 ND < 0.99 < 9.72E-04 3.25

Aniline 3.47 ND < 1.06 < 1.02E-03 3.47 ND < 1.06 < 1.04E-03 3.47

bis(2-Chloroethyl)ether 3.94 ND < 1.20 < 1.16E-03 3.94 ND < 1.20 < 1.18E-03 3.94

2-Chloropenol 3.12 ND < 0.95 < 9.15E-04 3.12 ND < 0.95 < 9.33E-04 3.12

1,3-Dichlorobenzene 2.79 ND < 0.85 < 8.18E-04 2.79 ND < 0.85 < 8.35E-04 2.79

1,4-Dichlorobenzene (CCC) 2.64 ND < 0.80 < 7.74E-04 2.64 ND < 0.80 < 7.90E-04 2.64

Benzyl alcohol 3.50 ND < 1.07 < 1.03E-03 3.50 ND < 1.07 < 1.05E-03 3.50

1,2-Dichlorobenzene 2.79 ND < 0.85 < 8.18E-04 2.79 ND < 0.85 < 8.35E-04 2.79

2-Methylphenol 3.39 ND < 1.03 < 9.94E-04 3.39 ND < 1.03 < 1.01E-03 3.39

bis(2-Chloroisopropyl) ether 4.91 ND < 1.50 < 1.44E-03 4.91 ND < 1.50 < 1.47E-03 4.91

3/4-Methylphenol 2.95 ND < 0.90 < 8.65E-04 2.95 ND < 0.90 < 8.83E-04 2.95

N-Nitroso-di-n-propylamine (SPCC) 4.16 ND < 1.27 < 1.22E-03 4.16 ND < 1.27 < 1.24E-03 4.16

o-Toluidine 5.00 ND < 1.52 < 1.47E-03 5.00 ND < 1.52 < 1.50E-03 5.00

Hexachloroethane 3.16 ND < 0.96 < 9.27E-04 3.16 ND < 0.96 < 9.45E-04 3.16

Nitrobenzene 4.08 ND < 1.24 < 1.20E-03 4.08 ND < 1.24 < 1.22E-03 4.08

Isophorone 3.74 ND < 1.14 < 1.10E-03 3.74 ND < 1.14 < 1.12E-03 3.74

(ug) (ug/dscm) (lb/hr) (ug) (ug/dscm) (lb/hr) (ug)

Emissions

SEMIVOLATILE AND PAH EMISSIONS SUMMARY

Motiva Enterprises LLC

Norco Refinery

RCCU STACK

Run 1 Run 2

Sample Catch Conc. Emissions Sample Catch Conc. Sample Catch
2,4-Dimethylphenol 3.64 ND < 1.11 < 1.07E-03 3.64 ND < 1.11 < 1.09E-03 3.64

2-Nitrophenol (CCC) 3.35 ND < 1.02 < 9.82E-04 3.35 ND < 1.02 < 1.00E-03 3.35

Benzoic acid 57.80 ND < 17.62 < 1.69E-02 57.80 ND < 17.62 < 1.73E-02 57.80

bis(2-Chloroethoxy)methane 3.66 ND < 1.12 < 1.07E-03 3.66 ND < 1.12 < 1.09E-03 3.66

2,4-Dichlorophenol (CCC) 3.26 ND < 0.99 < 9.56E-04 3.26 ND < 0.99 < 9.75E-04 3.26

a,a-Dimethylphenethylamine 5.00 ND < 1.52 < 1.47E-03 5.00 ND < 1.52 < 1.50E-03 5.00

1,2,4-Trichlorobenzene 3.09 ND < 0.94 < 9.06E-04 3.09 ND < 0.94 < 9.24E-04 3.09

4-Chloroaniline 4.24 ND < 1.29 < 1.24E-03 4.24 ND < 1.29 < 1.27E-03 4.24

Hexachlorobutadiene (CCC) 3.05 ND < 0.93 < 8.94E-04 3.05 ND < 0.93 < 9.12E-04 3.05

Quinoline 5.00 ND < 1.52 < 1.47E-03 5.00 ND < 1.52 < 1.50E-03 5.00

1,4-Phenylenediamine 5.00 ND < 1.52 < 1.47E-03 5.00 ND < 1.52 < 1.50E-03 5.00

4-Chloro-3 methylphenol (CCC) 3.31 ND < 1.01 < 9.71E-04 3.31 ND < 1.01 < 9.90E-04 3.31

Hexachlorocyclopentadiene (SPCC) 40.60 ND < 12.38 < 1.19E-02 40.60 ND < 12.38 < 1.21E-02 40.60

2,4,6-Trichlorophenol (CCC) 3.69 ND < 1.13 < 1.08E-03 3.69 ND < 1.13 < 1.10E-03 3.69

2,4,5-Trichlorophenol 2.70 ND < 0.82 < 7.92E-04 2.70 ND < 0.82 < 8.08E-04 2.70

Biphenyl 5.00 ND < 1.52 < 1.47E-03 5.00 ND < 1.52 < 1.50E-03 5.00

2-Chloronaphthalene 3.26 ND < 0.99 < 9.56E-04 3.26 ND < 0.99 < 9.75E-04 3.26

2-Nitroaniline 4.83 ND < 1.47 < 1.42E-03 4.83 ND < 1.47 < 1.44E-03 4.83

1,4-Dinitrobenzene 3.36 ND < 1.02 < 9.85E-04 3.36 ND < 1.02 < 1.01E-03 3.36

Dimethylphthalate 4.05 ND < 1.23 < 1.19E-03 4.05 ND < 1.23 < 1.21E-03 4.05

1,3-Dinitrobenzene 4.09 ND < 1.25 < 1.20E-03 4.09 ND < 1.25 < 1.22E-03 4.09

2,6-Dinitrotoluene 3.88 ND < 1.18 < 1.14E-03 3.88 ND < 1.18 < 1.16E-03 3.88

1,2-Dinitrobenzene 3.89 ND < 1.19 < 1.14E-03 3.89 ND < 1.19 < 1.16E-03 3.89

3-Nitroaniline 4.08 ND < 1.24 < 1.20E-03 4.08 ND < 1.24 < 1.22E-03 4.08

2,4-Dinitrophenol (SPCC) 25.30 ND < 7.71 < 7.42E-03 25.30 ND < 7.71 < 7.57E-03 25.30

4-Nitrophenol (SPCC) 28.90 ND < 8.81 < 8.47E-03 28.90 ND < 8.81 < 8.65E-03 28.90
2,4-Dinitrotoluene 4.02 ND < 1.23 < 1.18E-03 4.02 ND < 1.23 < 1.20E-03 4.02

Dibenzofuran 3.44 ND < 1.05 < 1.01E-03 3.44 ND < 1.05 < 1.03E-03 3.44

2,3,5,6-Tetrachlorophenol 3.80 ND < 1.16 < 1.11E-03 3.80 ND < 1.16 < 1.14E-03 3.80

2,3,4,6-Tetrachlorophenol 3.50 ND < 1.07 < 1.03E-03 3.50 ND < 1.07 < 1.05E-03 3.50

Diethlyphthalate 5.10 ND < 1.55 < 1.50E-03 5.10 ND < 1.55 < 1.53E-03 5.10

4-Chlorophenyl-phenylether 3.77 ND < 1.15 < 1.11E-03 3.77 ND < 1.15 < 1.13E-03 3.77

4-Nitroaniline 4.72 ND < 1.44 < 1.38E-03 4.72 ND < 1.44 < 1.41E-03 4.72

4,6-Dinitro2-methylphenol 25.80 ND < 7.87 < 7.57E-03 25.80 ND < 7.87 < 7.72E-03 25.80

N-Nitrosodiphenylamine (CCC) 3.58 ND < 1.09 < 1.05E-03 3.58 ND < 1.09 < 1.07E-03 3.58

Azobenzene 4.96 ND < 1.51 < 1.45E-03 4.96 ND < 1.51 < 1.48E-03 4.96

4-Bromophenyl-phenylether 3.35 ND < 1.02 < 9.82E-04 3.35 ND < 1.02 < 1.00E-03 3.35

Hexachlorobenzene 2.73 ND < 0.83 < 8.01E-04 2.73 ND < 0.83 < 8.17E-04 2.73

Pentachlorophenol (CCC) 2.83 ND < 0.86 < 8.30E-04 2.83 ND < 0.86 < 8.47E-04 2.83

Carbazole 3.53 ND < 1.08 < 1.04E-03 3.53 ND < 1.08 < 1.06E-03 3.53

Di-n-butylphthalate 5.19 ND < 1.58 < 1.52E-03 5.19 ND < 1.58 < 1.55E-03 5.19

Benzidine 114.00 ND < 34.76 < 3.34E-02 114.00 ND < 34.76 < 3.41E-02 114.00

4-Dimethylaminoazobenzene 5.00 ND < 1.52 < 1.47E-03 5.00 ND < 1.52 < 1.50E-03 5.00

Butylbenzylphthalate 4.05 ND < 1.23 < 1.19E-03 4.05 ND < 1.23 < 1.21E-03 4.05

3,3-Dimethylbenzidine 53.90 ND < 16.43 < 1.58E-02 53.90 ND < 16.43 < 1.61E-02 53.90

bis(2-Ethylhexyl)adipate 4.37 ND < 1.33 < 1.28E-03 4.37 ND < 1.33 < 1.31E-03 4.37

3,3-Dimethoxybenzidine 5.00 ND < 1.52 < 1.47E-03 5.00 ND < 1.52 < 1.50E-03 5.00

bis(2-Ethylhexyl)phthalate 8.71 ND < 2.66 < 2.55E-03 12.20 J 3.72 3.65E-03 8.71

3,3'-Dichlorobenzidine 46.80 ND < 14.27 < 1.37E-02 46.80 ND < 14.27 < 1.40E-02 46.80

Di-n-octylphthalate (CCC) 3.22 ND < 0.98 < 9.44E-04 3.22 ND < 0.98 < 9.63E-04 3.22

Naphthalene 1.30 0.397 3.82E-04 1.29 0.393 3.86E-04 0.68
2-Methylnaphthalene 0.11 0.034 3.25E-05 0.16 0.050 4.88E-05 0.05

1-Methylnaphthalene 0.06 0.018 1.73E-05 0.08 0.023 2.27E-05 0.05

Acenaphthylene 0.05 ND < 0.015 < 1.47E-05 0.05 ND < 0.015 < 1.50E-05 0.05

Acenaphthene (CCC) 0.05 ND < 0.015 < 1.47E-05 0.05 ND < 0.015 < 1.50E-05 0.05

Fluorene 0.05 0.016 1.52E-05 0.08 0.024 2.32E-05 0.05

Phenanthrene 0.17 0.051 4.87E-05 0.15 0.044 4.34E-05 0.05

Anthracene 0.05 ND < 0.015 < 1.47E-05 0.05 ND < 0.015 < 1.50E-05 0.05

Fluoranthene (CCC) 0.18 0.055 5.28E-05 0.11 0.034 3.38E-05 0.09

Pyrene 0.42 0.128 1.23E-04 0.24 0.073 7.15E-05 0.22

Benzo(b)fluoranthene 0.05 ND < 0.015 < 1.47E-05 0.05 ND < 0.015 < 1.50E-05 0.05

Chrysene 0.05 ND < 0.015 < 1.47E-05 0.05 ND < 0.015 < 1.50E-05 0.05

7,12-Dimethylbenz(a)anthracene 0.05 ND < 0.015 < 1.47E-05 0.05 ND < 0.015 < 1.50E-05 0.05

Benzo(b)fluoranthene 0.05 ND < 0.015 < 1.47E-05 0.05 ND < 0.015 < 1.50E-05 0.05

Benzo(k)fluoranthene 0.05 ND < 0.015 < 1.47E-05 0.05 ND < 0.015 < 1.50E-05 0.05

Benzo(e)pyrene 0.05 ND < 0.015 < 1.47E-05 0.05 ND < 0.015 < 1.50E-05 0.05

Benzo(a)pyrene (CCC) 0.05 ND < 0.015 < 1.47E-05 0.05 ND < 0.015 < 1.50E-05 0.05

Perylene 0.05 ND < 0.015 < 1.47E-05 0.05 ND < 0.015 < 1.50E-05 0.05

3-Methylcholanthrene 0.05 ND < 0.015 < 1.47E-05 0.05 ND < 0.015 < 1.50E-05 0.05

Indeno(1,2,3-cd)pyrene 0.05 ND < 0.015 < 1.47E-05 0.05 ND < 0.015 < 1.50E-05 0.05

Dibenz(a,h)anthracene 0.05 ND < 0.015 < 1.47E-05 0.05 ND < 0.015 < 1.50E-05 0.05

Benzo(g,h,i)perylene 0.05 ND < 0.015 < 1.47E-05 0.05 ND < 0.015 < 1.50E-05 0.05

Dibenzo(a,e)pyrene 0.05 ND < 0.015 < 1.47E-05 0.05 ND < 0.015 < 1.50E-05 0.05

Run 1 Run 2

Sample volume (Vmstd, dscf) 115.83 118.47

Volumetric Air Flow (DSCFM) 256,772 267,946

Average % CO2 by volume, dry 17.70 17.70

Average % O2 by volume, dry 1.60 1.60

ND < 1.18 < 1.15E-03 < 1.18 < 1.15E-03

ND < 16.04 < 1.57E-02 < 16.04 < 1.56E-02

ND < 0.99 < 9.70E-04 < 1.06 < 1.03E-03

ND < 1.06 < 1.04E-03 < 1.06 < 1.03E-03

ND < 1.20 < 1.18E-03 < 1.20 < 1.17E-03

ND < 0.95 < 9.31E-04 < 0.95 < 9.26E-04

ND < 0.85 < 8.33E-04 < 0.85 < 8.28E-04

ND < 0.80 < 7.88E-04 < 0.80 < 7.84E-04

ND < 1.07 < 1.04E-03 < 1.07 < 1.04E-03

ND < 0.85 < 8.33E-04 < 0.85 < 8.28E-04

ND < 1.03 < 1.01E-03 < 1.03 < 1.01E-03

ND < 1.50 < 1.47E-03 < 1.50 < 1.46E-03

ND < 0.90 < 8.80E-04 < 0.90 < 8.76E-04

ND < 1.27 < 1.24E-03 < 1.27 < 1.24E-03

ND < 1.52 < 1.49E-03 < 1.52 < 1.48E-03

ND < 0.96 < 9.43E-04 < 0.96 < 9.38E-04

ND < 1.24 < 1.22E-03 < 1.24 < 1.21E-03

ND < 1.14 < 1.12E-03 < 1.14 < 1.11E-03

Conc. Emissions Conc. Emissions

(ug/dscm) (lb/hr) (ug/dscm) (lb/hr)

Run 3 Average

Sample Catch
ND < 1.11 < 1.09E-03 < 1.11 < 1.08E-03

ND < 1.02 < 1.00E-03 < 1.02 < 9.95E-04

ND < 17.62 < 1.72E-02 < 17.62 < 1.72E-02

ND < 1.12 < 1.09E-03 < 1.12 < 1.09E-03

ND < 0.99 < 9.73E-04 < 0.99 < 9.68E-04

ND < 1.52 < 1.49E-03 < 1.52 < 1.48E-03

ND < 0.94 < 9.22E-04 < 0.94 < 9.18E-04

ND < 1.29 < 1.27E-03 < 1.29 < 1.26E-03

ND < 0.93 < 9.10E-04 < 0.93 < 9.06E-04

ND < 1.52 < 1.49E-03 < 1.52 < 1.48E-03

ND < 1.52 < 1.49E-03 < 1.52 < 1.48E-03

ND < 1.01 < 9.88E-04 < 1.01 < 9.83E-04

ND < 12.38 < 1.21E-02 < 12.38 < 1.21E-02

ND < 1.13 < 1.10E-03 < 1.13 < 1.10E-03

ND < 0.82 < 8.06E-04 < 0.82 < 8.02E-04

ND < 1.52 < 1.49E-03 < 1.52 < 1.48E-03

ND < 0.99 < 9.73E-04 < 0.99 < 9.68E-04

ND < 1.47 < 1.44E-03 < 1.47 < 1.43E-03

ND < 1.02 < 1.00E-03 < 1.02 < 9.98E-04

ND < 1.23 < 1.21E-03 < 1.23 < 1.20E-03

ND < 1.25 < 1.22E-03 < 1.25 < 1.21E-03

ND < 1.18 < 1.16E-03 < 1.18 < 1.15E-03

ND < 1.19 < 1.16E-03 < 1.19 < 1.16E-03

ND < 1.24 < 1.22E-03 < 1.24 < 1.21E-03

ND < 7.71 < 7.55E-03 < 7.71 < 7.51E-03

ND < 8.81 < 8.62E-03 < 8.81 < 8.58E-03
ND < 1.23 < 1.20E-03 < 1.23 < 1.19E-03

ND < 1.05 < 1.03E-03 < 1.05 < 1.02E-03

ND < 1.16 < 1.13E-03 < 1.16 < 1.13E-03

ND < 1.07 < 1.04E-03 < 1.07 < 1.04E-03

ND < 1.55 < 1.52E-03 < 1.55 < 1.51E-03

ND < 1.15 < 1.12E-03 < 1.15 < 1.12E-03

ND < 1.44 < 1.41E-03 < 1.44 < 1.40E-03

ND < 7.87 < 7.70E-03 < 7.87 < 7.66E-03

ND < 1.09 < 1.07E-03 < 1.09 < 1.06E-03

ND < 1.51 < 1.48E-03 < 1.51 < 1.47E-03

ND < 1.02 < 1.00E-03 < 1.02 < 9.95E-04

ND < 0.83 < 8.15E-04 < 0.83 < 8.11E-04

ND < 0.86 < 8.44E-04 < 0.86 < 8.40E-04

ND < 1.08 < 1.05E-03 < 1.08 < 1.05E-03

ND < 1.58 < 1.55E-03 < 1.58 < 1.54E-03

ND < 34.76 < 3.40E-02 < 34.76 < 3.39E-02

ND < 1.52 < 1.49E-03 < 1.52 < 1.48E-03

ND < 1.23 < 1.21E-03 < 1.23 < 1.20E-03

ND < 16.43 < 1.61E-02 < 16.43 < 1.60E-02

ND < 1.33 < 1.30E-03 < 1.33 < 1.30E-03

ND < 1.52 < 1.49E-03 < 1.52 < 1.48E-03

ND < 2.66 < 2.60E-03 < 3.01 < 2.93E-03

ND < 14.27 < 1.40E-02 < 14.27 < 1.39E-02

ND < 0.98 < 9.61E-04 < 0.98 < 9.56E-04

0.209 2.04E-04 0.333 3.24E-04
0.016 1.54E-05 < 0.033 < 3.22E-05

ND < 0.015 < 1.49E-05 < 0.019 < 1.83E-05

ND < 0.015 < 1.49E-05 < 0.015 < 1.48E-05

ND < 0.015 < 1.49E-05 < 0.015 < 1.48E-05

ND < 0.015 < 1.49E-05 < 0.018 < 1.78E-05

0.016 1.61E-05 0.037 3.61E-05

ND < 0.015 < 1.49E-05 < 0.015 < 1.48E-05

0.029 2.80E-05 0.039 3.82E-05

0.066 6.45E-05 0.089 8.65E-05

ND < 0.015 < 1.49E-05 < 0.015 < 1.48E-05

ND < 0.015 < 1.49E-05 < 0.015 < 1.48E-05

ND < 0.015 < 1.49E-05 < 0.015 < 1.48E-05

ND < 0.015 < 1.49E-05 < 0.015 < 1.48E-05

ND < 0.015 < 1.49E-05 < 0.015 < 1.48E-05

ND < 0.015 < 1.49E-05 < 0.015 < 1.48E-05

ND < 0.015 < 1.49E-05 < 0.015 < 1.48E-05

ND < 0.015 < 1.49E-05 < 0.015 < 1.48E-05

ND < 0.015 < 1.49E-05 < 0.015 < 1.48E-05

ND < 0.015 < 1.49E-05 < 0.015 < 1.48E-05

ND < 0.015 < 1.49E-05 < 0.015 < 1.48E-05

ND < 0.015 < 1.49E-05 < 0.015 < 1.48E-05

ND < 0.015 < 1.49E-05 < 0.015 < 1.48E-05

Run 3

115.41

260,341

17.50

1.50

EPA METHOD 308 DATA

DETERMINATION OF METHANOL EMISSIONS FROM STAT

Test Date: 6/20 and 6/21/2011

Project: Number: ZTSO0192

Company: Motiva Enterprises

Plant: Norco

Test Location: RCCU Stack

Test Number: 1

Pressure, Barometric (Hg"):......................... 29.48

Pressure, Static (H2O"):................................

Pressure, Stack (Hg"):................................... 29.48

Initial Volume (liters):.................................. 8849.9

Final Volume (liters):.................................... 8961.2

Meter Temperature (oF):............................... 95.5

Meter Volume (dscM):.................................... 0.1043

Meter Calibration (Y):................................... 0.998

Initial Wt. (grams or mls):......................... 0.0
Final Wt. (grams or mls):........................... 0.0

Average Delta H (H):.................................. 0.976

Dry Standard Flow Rate (dscMm):.............. 6773.7

Test Number: 2

Pressure, Barometric (Hg"):......................... 29.43

Pressure, Static (H2O"):................................

Pressure, Stack (Hg"):................................... 29.43

Initial Volume (liters):.................................. 8962.5

Final Volume (liters):.................................... 9083.3

Meter Temperature (oF):............................... 0.0

Meter Volume (dscM):.................................... 0.1365

Meter Calibration (Y):................................... 0.998

Initial Wt. (grams or mls):......................... 0.0

Final Wt. (grams or mls):........................... 0.0

Average Delta H (H):.................................. 1.024

Dry Standard Flow Rate (dscMm):.............. 7018.0

Test Number: 3

Pressure, Barometric (Hg"):......................... 29.41
Pressure, Static (H2O"):................................

Pressure, Stack (Hg"):................................... 29.41

Initial Volume (liters):.................................. 9083.3

Final Volume (liters):.................................... 9204.0

Meter Temperature (oF):............................... 0.0

Meter Volume (dscM):.................................... 0.1363

Meter Calibration (Y):................................... 0.998

Initial Wt. (grams or mls):......................... 0.0

Final Wt. (grams or mls):........................... 0.0

Average Delta H (H):.................................. 1.036

Dry Standard Flow Rate (dscMm):.............. 6888.0

Average Methanol lbs/hr: 0.06

Average Methanol ppm: 0.07

Average Methanol lbs/MMBtu: #VALUE!

Average Flow Rate (dscfm) 6893

Flowrate, moisture, O2 and CO2 values taken from M0010 train data sampled at the same tim
THOD 308 DATA g 

MISSIONS FROM STATIONARY SOURCES

Condition: Normal

Test Engineer: E. Santibanez

Fuel Factor (Fd): NA

Time: 1530-1730

Carbon Dioxide Content (%):................................. 17.7

Oxygen Content (%):................................................ 1.6

Nitrogen Content (%):.............................................. 80.70

Methanol (mg)........................................................... 0.0181 J

Water Vapor in Flue Gas (Bws):........................... 0.220

Methanol (mg/m3):........................................................ 0.174 J
Methanol (lbs/hr):..................................................... 0.156 J

Methanol (lbs/MMBtu):.............................................#VALUE! J

Time: 1815-2015

Carbon Dioxide Content (%):................................. 17.70

Oxygen Content (%):................................................ 1.60

Nitrogen Content (%):.............................................. 80.70

Methanol (mg)........................................................... 0.00156 J

Water Vapor in Flue Gas (Bws):........................... 0.220

Methanol (mg/m3):........................................................0.0114 J

Methanol (lbs/hr):..................................................... 0.011 J

Methanol (lbs/MMBtu):.............................................#VALUE! J

Time: 1020-1220

Carbon Dioxide Content (%):................................. 17.50
Oxygen Content (%):................................................ 1.50

Nitrogen Content (%):.............................................. 81.00

Methanol (mg)........................................................... 0.00180 J

Water Vapor in Flue Gas (Bws):........................... 0.220

Methanol (mg/m3):........................................................0.0132 J

Methanol (lbs/hr):..................................................... 0.012 J

Methanol (lbs/MMBtu):.............................................#VALUE! J

sampled at the same time.
METHOD 5/202 PARTICULATE TEST RESULTS SUMMARY

Company:

Plant:

Unit:

Location:

Test Run Number 1 2 3 Average

Source Condition Normal Normal Normal

Date 6/16/2011 6/17/2011 6/17/2011

Start Time 13:40 9:20 14:10

End Time 16:20 12:01 16:48

Sample Duration (min): 144.0 144.0 144.0 144.0

Average Gas Temp (oF): 144.2 144.0 144.7 144.3

Fractional Gas Moisture Content: 0.21 0.18 0.22 0.20

Gas CO2 Content (%vol): 17.3 17.1 17.0 17.1

Gas O2 Content (%vol): 1.6 2.0 1.9 1.8

Gas Wet MW (lb/lbmole-mole): 28.11 28.52 27.99 28.21 Lines denoted by purple should 

Average Gas Vel (ft/sec): 31.41 31.15 30.91 31.16

Measured Volumetric Flow Rate

 Q (actual ft3/min): 378,977 375,778 372,882 375,879

 Qstd (std ft3/min): 326,603 324,605 321,422 324,210

 Qstd(dry) (dry std ft3/min): 257,348 266,492 250,906 258,249

Fd (dscf/MMBtu): 8,710 8,710 8,710 8,710

Sample Volume (dry std ft3): 88.427 88.607 86.618 87.884

PM Concentration (gr/dscf):

 Filterable 0.0096 0.0081 0.0118 0.0098

 Aqueous Condensible: 0.0105 0.0090 0.0082 0.0092

 Organic Condensible: 0.0012 0.0004 0.0001 0.0006

 Total: 0.0213 0.0175 0.0201 0.0197

PM Concentration (mg/Nm3):

 Filterable: 23.6 20.2 29.1 24.3

 Aqueous Condensible: 25.85 22.48 20.10 22.81

 Organic Condensible: 2.910 0.948 0.345 1.401

 Total: 52.3 43.6 49.5 48.5

PM Emission Rate (lb/hr based on measured volumetric flow rate):

Motiva Enterprises LLC

Norco Refinery

RCCU

NEVER PUT EQUATIONS IN 

THE CELLS IN THIS TABLE. IF 

A CHANGE IS NEEDED, 

CONSULT WITH THE 

TECHNICAL DIRECTOR.

Stack
 Filterable: 21.16 18.53 25.44 21.71

 Aqueous Condensible: 23.21 20.65 17.59 20.48

 Organic Condensible: 2.61 0.87 0.30 1.26

 Total: 46.99 40.05 43.33 43.46

Isokinetic Variance 97.8 94.6 98.3 96.9
Lines denoted by purple should be visible if measured

T EQUATIONS IN 

N THIS TABLE. IF 

GE IS NEEDED, 

LT WITH THE 

AL DIRECTOR.
PCDD/PCDF TEST RESULTS SUMMARY Page 1 of 1

Company:

Plant:

Unit:

Location:

Test Run Number 1 2 3 Average

Source Condition Normal Normal Normal

Date 6/15-16/2011 6/16/2011 6/16-17/2011

Start Time 21:55 2:45 0:43

End Time 0:44 6:17 0:34

Sample Duration (min): 192.0 192.0 192.0 192.0

Average Gas Temp (oF): 144.6 143.5 144.0 144.0

Fractional Gas Moisture Content: 0.22 0.22 0.22 0.22

Gas CO2 Content (%vol): 16.9 17.3 17.1 17.1

Gas O2 Content (%vol): 1.6 1.6 1.8 1.7

Gas Wet MW (lb/lbmole-mole): 27.94 28.07 28.03 28.02 Lines denoted by purple should 

Average Gas Vel (ft/sec): 30.96 31.34 31.85 31.38

Measured Volumetric Flow Rate

 Q (actual ft3/min): 373,453 378,059 384,212 378,575

 Q (actual m3/min): 10,575 10,705 10,880 10,720

 Qstd (std ft3/min): 320,662 325,840 330,241 325,581

 Qstd (Nm3/min): 8,459 8,563 8,703 8,575

 Qstd(dry) (dry std ft3/min): 249,677 255,734 258,682 254,697

 Qstd(dry) (dry Nm3/min): 6,587 6,721 6,817 6,708

Isokinetic Variance 97.5 97.2 97.3 97.3

Motiva Enterprises LLC

Norco Refinery

RCCU 

NEVER PUT EQUATIONS IN 

THE CELLS IN THIS TABLE. IF 

A CHANGE IS NEEDED, 

CONSULT WITH THE 

TECHNICAL DIRECTOR.

Stack
Lines denoted by purple should be visible if measured

T EQUATIONS IN 

N THIS TABLE. IF 

GE IS NEEDED, 

LT WITH THE 

AL DIRECTOR.
Sample 

Catch Conc. Emissions

Sample 

Catch Conc. Emissions

Sample 

Catch Conc. Emissions Conc.

Analytes (pg) (ng/dscm)

(ng/dscm at 

7% O2) (pg) (ng/dscm)

(ng/dscm 

at 7% O2) (pg) (ng/dscm)

(ng/dscm 

at 7% O2) (ng/dscm)

2378-TCDD 1.1 3.41E-04 2.45E-04 1.1 3.34E-04 2.40E-04 1.1 3.30E-04 2.40E-04 3.35E-04

12378-PeCDD 1.1 3.41E-04 2.45E-04 1.1 3.34E-04 2.40E-04 1.0 3.00E-04 2.18E-04 3.25E-04

123478-HxCDD 1.2 3.72E-04 2.68E-04 1.2 3.64E-04 2.62E-04 1.1 3.30E-04 2.40E-04 3.55E-04

123678-HxCDD 1.2 3.72E-04 2.68E-04 1.2 3.64E-04 2.62E-04 1.1 3.30E-04 2.40E-04 3.55E-04

123789-HxCDD 1.1 3.41E-04 2.45E-04 1.1 3.34E-04 2.40E-04 1.0 3.00E-04 2.18E-04 3.25E-04

1234678-HpCDD 1.6 4.95E-04 3.57E-04 1.6 4.85E-04 3.49E-04 1.2 3.60E-04 2.62E-04 4.47E-04

OCDD 3.6 1.11E-03 8.03E-04 5.3 1.61E-03 1.16E-03 4.0 1.20E-03 8.72E-04 1.31E-03

2378 -TCDF 1.4 4.34E-04 3.12E-04 1.6 4.85E-04 3.49E-04 2.3 6.89E-04 5.01E-04 5.36E-04

12378-PeCDF 1.1 3.41E-04 2.45E-04 1.1 3.34E-04 2.40E-04 1.1 3.30E-04 2.40E-04 3.35E-04

23478-PeCDF 1.8 5.57E-04 4.01E-04 1.9 5.76E-04 4.15E-04 1.6 4.79E-04 3.49E-04 5.38E-04

123478-HxCDF 1.0 3.10E-04 2.23E-04 1.1 3.34E-04 2.40E-04 1.1 3.30E-04 2.40E-04 3.24E-04

123678-HxCDF 0.96 2.97E-04 2.14E-04 1.1 3.34E-04 2.40E-04 0.96 2.88E-04 2.09E-04 3.06E-04

234678-HxCDF 1.2 3.72E-04 2.68E-04 1.4 4.24E-04 3.06E-04 1.3 3.89E-04 2.83E-04 3.95E-04

123789-HxCDF 1.3 4.03E-04 2.90E-04 1.4 4.24E-04 3.06E-04 1.3 3.89E-04 2.83E-04 4.05E-04

1234678-HpCDF 1.0 3.10E-04 2.23E-04 1.3 3.94E-04 2.84E-04 1.3 3.89E-04 2.83E-04 3.64E-04

1234789-HpCDF 1.3 4.03E-04 2.90E-04 1.2 3.64E-04 2.62E-04 1.2 3.60E-04 2.62E-04 3.75E-04

OCDF 2.1 6.50E-04 4.68E-04 2.0 6.06E-04 4.37E-04 2.1 6.29E-04 4.58E-04 6.29E-04

PCDD/PCDF TEST RESULTS SUMMARY

Motiva Enterprises LLC

Norco Refinery

RCCU Stack

June 15 through 17, 2011

Test 1 - June 15 and 16 Test 2 - June 16 Test 3 - June 16 and 17 Average
Total TCDD 1.1 3.41E-04 2.45E-04 1.1 3.34E-04 2.40E-04 1.1 3.30E-04 2.40E-04 3.35E-04

Total PeCDD 1.7 5.26E-04 3.79E-04 2.0 6.06E-04 4.37E-04 2.6 7.79E-04 5.67E-04 6.37E-04

Total HxCDD 1.2 3.72E-04 2.68E-04 1.2 3.64E-04 2.62E-04 1.1 3.30E-04 2.40E-04 3.55E-04

Total HpCDD 1.6 4.95E-04 3.57E-04 1.6 4.85E-04 3.49E-04 1.2 3.60E-04 2.62E-04 4.47E-04

Total TCDF 2.8 8.67E-04 6.24E-04 3.1 9.40E-04 6.77E-04 3.5 1.05E-03 7.63E-04 9.52E-04

Total PeCDF 1.8 5.57E-04 4.01E-04 1.9 5.76E-04 4.15E-04 2.7 8.09E-04 5.89E-04 6.47E-04

Total HxCDF 1.1 3.41E-04 2.45E-04 1.2 3.64E-04 2.62E-04 1.1 3.30E-04 2.40E-04 3.45E-04

Total HpCDF 1.1 3.41E-04 2.45E-04 1.4 4.24E-04 3.06E-04 1.4 4.19E-04 3.05E-04 3.95E-04

Total PCDD/PCDF 18.1 5.60E-03 4.04E-03 20.8 6.31E-03 4.54E-03 20.8 6.23E-03 4.53E-03 6.05E-03

TEQ Adjusted Total

Test 1 Test 2 Test 3

Sample volume (Vmstd, dscf) 114.049 116.474 117.879 *TEQ

Volumetric Air Flow (DSCFM) 249,677 255,734 258,682 **TEF

Average % CO2 by volume, dry 16.9 17.3 17.1 TEF Factors from World 

Average % O2 by volume, dry 1.6 1.6 1.8 2005 Toxicity Equivalency 

40CFR63 Subpart DDDD

1.0142E-09 1.14E-03
Emissions BLANK

(ng/dscm 

at 7% O2) TEF** (ng/dscm)

(ng/dscm at 

7% O2)

2.42E-04 1.0 3.35E-04 2.42E-04 0

2.35E-04 1.0 3.25E-04 2.35E-04 0

2.56E-04 0.1 3.55E-05 2.56E-05 0 <

2.56E-04 0.1 3.55E-05 2.56E-05 0

2.35E-04 0.1 3.25E-05 2.35E-05 0

3.23E-04 0.01 4.47E-06 3.23E-06 0

9.44E-04 0.0003 3.92E-07 2.83E-07 0

3.88E-04 0.1 5.36E-05 3.88E-05 0

2.42E-04 0.03 1.00E-05 7.25E-06 0

3.88E-04 0.3 1.61E-04 1.17E-04 0

2.34E-04 0.1 3.24E-05 2.34E-05 0

2.21E-04 0.1 3.06E-05 2.21E-05 0

2.86E-04 0.1 3.95E-05 2.86E-05 0

2.93E-04 0.1 4.05E-05 2.93E-05 0

2.63E-04 0.01 3.64E-06 2.63E-06 0

2.71E-04 0.01 3.75E-06 2.71E-06 0

4.54E-04 0.0003 1.89E-07 1.36E-07 0

TEQ* Factor Results

Average
2.42E-04 0

4.61E-04 0

2.56E-04 0

3.23E-04 0

6.88E-04 0

4.68E-04 0

2.49E-04 0

2.85E-04 0

4.37E-03

1.14E-03 8.26E-04

Toxicity Equivalents

Toxicity Equivalency Factor

TEF Factors from World Health Organization (WHO)

2005 Toxicity Equivalency Factors and referenced in 

40CFR63 Subpart DDDDD Table 11.

ng 6708 dscm 6.00E+01 lb

dscm min hr 1000000000*453.59
Company: Did you have 4 test runs?

Plant: If yes, Highlight Columns F and H, and right-click and select "Unhide".

Unit: You will need to adjust the formulas in the Average Column for the runs y

1 2 3 Average

Normal Normal Normal P may need to adjust cell height and or width

6/19/2011 6/19/2011 6/19/2011 P

9:45 12:22 14:50

11:54 14:32 16:58

0.248 0.133 0.103 0.162

0.38 0.20 0.16 0.25 P

0.3634 0.1947 0.1497 0.2359 P

P

0.048 0.043 0.045 0.045 P

0.040 0.036 0.038 0.038

0.0382 0.0346 0.0359 0.0363

0.004 0.004 0.004 0.004 P

0.012 0.011 0.013 0.012 P

0.0119 0.0108 0.0123 0.0116 P

P

383,296 382,967 379,432 381,898

257,461 257,197 254,997 256,552

144.3 144.5 144.3 144.4

31.773 31.745 31.452 31.657

22.2* 22.1 22.0 22.1

29.57 29.54 29.51

29.58 29.55 29.52

18.0 17.1 17.0 17.4

1.7 2.0 1.9 1.9

30.948 30.816 30.796

76.660 76.885 75.459

Isokinetic Variance 97.1 97.5 96.5

* Theoretical maximum moisture content of the gas stream.

Average Flue Pressure, in. Hg

Barometric Pressure, in. Hg

Average %CO2 by volume, dry basis

Average %O2 by volume, dry basis

Dry Molecular Wt. of Gas, lb/lb-mole

Gas Sample Volume, dscf

Flue Gas Moisture, percent by

Cl2 Emissions:

ppm

mg/dscm

lb/hr

Stack Parameters:

M2 Gas Volumetric Flow Rate, acfm

M2 Gas Volumetric Flow Rate, 

Average Gas Temperature, °F

Average Gas Velocity, ft/sec

lb/hr

Date

Start Time

End Time

HCl Emissions:

ppm

mg/dscm

lb/hr

HF Emissions:

ppm

mg/dscm

Source Condition

METHOD 26A TEST RESULTS SUMMARY

Motiva Enterprises LLC

Norco Refinery

RCCU Stack

Test Run Number
d right-click and select "Unhide".

 the Average Column for the runs you want to use.
Company: Did you have 4 test runs?

Plant: If yes, Highlight Columns F and H, and r

Unit: You will need to adjust the formulas in th

1 2 3 Average

Normal Normal Normal P May need to fix row height if text too long

6/15/2011 6/15/2011 6/15/2011

10:25 14:15 17:25

12:40 16:30 19:40

< 2.90E-06 < 2.95E-06 < 2.94E-06 < 2.93E-09 P

< 2.57E-06 < 2.58E-06 < 2.57E-06 < 2.57E-06 P

6.44E-05 5.30E-06 1.24E-05 2.73E-07 P

5.70E-05 4.65E-06 1.08E-05 2.42E-05

< 1.16E-05 < 1.18E-05 1.77E-05 < 1.37E-08 P May need to hide rows if one fraction on

< 1.03E-05 < 1.03E-05 1.54E-05 < 1.20E-05 P

< 7.89E-05 < 2.00E-05 3.30E-05 < 4.40E-08

< 6.99E-05 < 1.76E-05 2.88E-05 < 3.87E-05

143.0 143.5 143.6 143.4

31.047 30.968 30.927 30.980

21.5* 21.9* 22.0 21.8

29.51 29.42 29.39

29.52 29.43 29.40

17.2 16.9 16.2 16.8

1.7 1.4 2.0 1.7

Barometric Pressure, in. Hg

Average %CO2 by volume, dry basis

Average %O2 by volume, dry basis

Average Flue Pressure, in. Hg

Total Mercury Emissions

mg/dncm

lb/hr

Stack Parameters:

Average Gas Temperature, °F

Average Gas Velocity, ft/sec

Flue Gas Moisture, % by volume

mg/dncm

lb/hr

Oxidized Mercury Emissions

mg/dncm

lb/hr

Date

Start Time

End Time

Particle Bound Mercury Emissions

mg/dncm

lb/hr

Elemental Mercury Emissions

Source Condition

SPECIATED MERCURY TEST RESULTS SUMMARY

Motiva Enterprises LLC

Norco Refinery

RCCU Stack

Test Run Number
30.820 30.760 30.672

65.351 64.312 64.376

100.9 100.5 100.9

Dry MW of Gas, lb/lb-mole

Gas Sample Volume, dscf

Isokinetic Variance
e 4 test runs?

ght Columns F and H, and right-click and select "Unhide".

d to adjust the formulas in the Average Column for the runs you want to use.

fix row height if text too long.

hide rows if one fraction only.
Company: Did you have 4 test runs?

Plant: If yes, Highlight Columns I and L, and r

Unit: You will need to adjust the formulas in 

P May need to fix row height if text too lo

P Type of Analyte

< 3.83E-02 < 3.68E-02 < 4.00E-02 < 3.84E-05

< 3.71E-02 < 3.54E-02 < 3.85E-02 < 3.70E-02

Isokinetic Variance 101.1 100.6 100.0

* Theoretical maximum moisture content of the gas stream.

Gas Sample Volume, dscf 30.083 29.769 29.566

Average %CO2 by volume, dry basis 11.3 11.0 11.2 11.2

Average %O2 by volume, dry basis 5.9 7.0 6.4 6.4

Average Flue Pressure, in. Hg 29.57 29.54 29.51

Flue Gas Moisture, percent by volume 22.3* 22.2* 22.1* 22.2

Gas Volumetric Flow Rate, dscfm 258,595 257,109 256,902 257,535

Stack Parameters:

Gas Volumetric Flow Rate, acfm 385,586 383,081 382,538 383,735

ug/dscm:

lb/hr:

Fuel factor, dscf/MMBtu 8710 8710 8710

HCN Emissions

Start Time 9:50 12:00 14:05

End Time 11:03 13:15 15:25

Source Condition Normal Normal Normal 

Date 6/19/2011 6/19/2011 6/19/2011

OTM-029 TEST RESULTS SUMMARY

Motiva Enterprises LLC

Norco Refinery

RCCU Stack

Test Run Number 1 2 3 Average
e 4 test runs?

ght Columns I and L, and right-click and select "Unhide".

d to adjust the formulas in the Average Column for the runs you want to use.

fix row height if text too long.

HCN
Company: Date: 6/28/2011 Page 1 of 1

Plant: Norco, LA GE Energy Project ZTSO0201

Unit: RCCU Scrubber Stack

Date 06/28/11 06/30/11 06/30/11

Start Time 16:39 12:00 15:40

End Time 18:51 14:08 17:50

Test Run 1 2 3 Average

Flow Rate Stack Flow Method 2 dscfm 249457 251560 249597 250205

Moisture Moisture Method 320 % 20.1% 20.2% 20.1% 20.1%

Moisture fraction 0.201 0.202 0.201 0.201

Outlet Formaldehyde CH2O ppmvw 0.10 <0.04 0.041 <0.06

ppmvd 0.13 <0.06 0.051 <0.09

MW= 30.03 lb/hr 0.15 <0.061 0.060 <0.103

mg/dscm 125.4 <52 51.1 <88.3

Outlet Acetaldehyde C2H4O ppmvw <0.12 <0.15 <0.14 <0.13

M320 ppmvd <0.15 <0.18 <0.17 <0.18

MW= 44.05 lb/hr <0.26 <0.32 <0.29 <0.32

mg/dscm <221.2 <268.4 <252 <268.4

Outlet Acrolein C3H4O ppmvw <0.19 <0.24 <0.22 <0.22

M320 ppmvd <0.24 <0.3 <0.28 <0.3

MW= 56.06 lb/hr <0.53 <0.65 <0.6 <0.65

mg/dscm <454.4 <551.4 <517.7 <551.4

Outlet Propanal C3H6O ppmvw <0.087 <0.106 <0.099 <0.097

M320 ppmvd <0.11 <0.13 <0.12 <0.13

MW= 58.08 lb/hr <0.25 <0.3 <0.28 <0.3

mg/dscm <211.4 <256.5 <240.9 <256.5

Outlet Hydrogen Chloride HCl ppmvw 0.40 1.2 0.67 0.77

RCCU EMISSIONS TEST RESULTS SUMMARY - EPA METHOD 320 

Motiva
M320 ppmvd 0.50 1.6 0.84 0.97

MW= 36.46 lb/hr 0.71 2.2 #REF! #REF!

mg/dscm 0.61 1.9 #REF! #REF!

Outlet Hydrogen Cyanide HCN ppmvw <0.55 <0.49 <0.46 <0.5

M320 ppmvd <0.69 <0.61 <0.58 <0.61

MW= 27.03 lb/hr <0.72 <0.65 <0.61 <0.65

mg/dscm <620.5 <553.5 <524.1 <553.5

Outlet Hydrogen Fluoride HF ppmvw 2.3 2.0 2.1 2.1

M320 ppmvd 2.8 2.6 2.7 2.7

MW= 20.01 lb/hr 2.2 2.0 2.1 2.09

mg/dscm 1.9 1.7 1.8 1.8

Company: Date: 6/28/2011 Page 2 of 3

Plant: Norco, LA GE Energy Project ZTSO0201

Unit: RCCU Scrubber Stack

Test Run 1 2 3 Average

Outlet Water H2O ppmvw 201448.6 201752.7 200972.1 201391.2

M320 MW = 18.016 ppmvd NA NA NA NA

Outlet Carbon Dioxide CO2 % wet 15.0% 14.9% 15.0% 14.97%

M320 MW = 44.01 % dry 18.8% 18.6% 18.8% 18.74%

Outlet Carbon Monoxide CO ppmvw 1.6 2.2 3.2 2.4

M320 ppmvd 2.0 2.8 4.0 2.9

MW= 28.01 lb/hr 2.2 3.1 4.4 3.2

Outlet Nitric Oxide NO ppmvw 101.8 109.4 114.6 108.6

M320 ppmvd 127.5 137.0 143.4 136.0

MW= 30.01 lb/hr 148.6 161.1 167.3 159.0

Outlet Nitrogen Dioxide NO2 ppmvw <0.45 <0.52 <0.47 <0.48

M320 ppmvd <0.57 <0.65 <0.59 <0.65

RCCU EMISSIONS TEST RESULTS SUMMARY - EPA METHOD 320 

Motiva
MW= 46.01 lb/hr <1.01 <1.16 <1.06 <1.16

Outlet Nitrous Oxide N2O ppmvw 10.9 13.9 12.9 12.6

M320 ppmvd 13.7 17.4 16.1 15.7

MW= 44.01 lb/hr 23.4 29.9 27.6 27.0

Outlet Sulfur Dioxide SO2 ppmvw 13.9 12.7 13.3 13.3

M320 ppmvd 17.4 15.9 16.6 16.6

MW= 64.07 lb/hr 43.3 39.8 41.5 41.5

Outlet Ammonia NH3 ppmvw 0.58 <0.2 <0.2 <0.33

M320 ppmvd 0.73 <0.24 <0.25 <0.73

MW= 17.03 lb/hr 0.48 <0.16 <0.17 <0.48

Outlet Methane CH4 ppmvw <0.13 <0.13 <0.12 <0.13

M320 ppmvd <0.17 <0.16 <0.15 <0.16

MW= 16.04 lb/hr <0.1 <0.1 <0.1 <0.1

Outlet Ethane C2H6 ppmvw <0.19 <0.18 <0.17 <0.18

M320 ppmvd <0.23 <0.22 <0.22 <0.22

MW= 30.069 lb/hr <0.27 <0.26 <0.25 <0.26

Outlet Ethylene C2H4 ppmvw <0.46 <0.44 <0.45 <0.45

M320 ppmvd <0.58 <0.55 <0.56 <0.55

MW= 28.05 lb/hr <0.6 <0.6 <0.6 <0.6

Outlet n-Octane C8H18 ppmvw 0.12 0.08 0.08 0.09

M320 ppmvd 0.15 0.09 0.09 0.11

MW= 56.06 lb/hr 0.33 0.21 0.20 0.25

Company: Date: 6/28/2011 Page 3 of 3

Plant: Norco, LA GE Energy Project ZTSO0201

Unit: RCCU Scrubber Stack

Motiva

RCCU EMISSIONS TEST RESULTS SUMMARY - EPA METHOD 320 
Example ppmvd as HCl = Hydrogen Chloride ppmvw x 1/(1-Water Fraction)

Calculations 0.40 1/(1-0.165) 0.50

Method 320 lb/hr as HCl = ppmvd x dscfm x 60 min/hr x HCl MW x 1/3.853x108

0.50 249457 60 36.46 1/3.853x108 0.71

mg/dscm as HCl = lb/hr HCl x 28.32 ft3/m3 x 1/dcsfm x 1 hr/60 min x 453592.37 mg/lb

0.71 28.3 1/257197 1/60 453592.37 0.61