### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being Fields that are highlighted in down boxes, included. Gray fields are

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

6085 R M Schahfer 14 subbituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte

6085 R M Schahfer 14 As Received Higher Heating Value 6085 R M Schahfer 14 As Received % Moisture 6085 R M Schahfer 14 As Received % Ash 6085 R M Schahfer 14 As Received % Sulfur 6085 R M Schahfer 14 Dry basis Higher Heating Value 6085 R M Schahfer 14 Dry basis % Ash 6085 R M Schahfer 14 Dry basis % Sulfur 6085 R M Schahfer 14 Dry basis Antim ony 6085 R M Schahfer 14 Dry basis Arsenic 6085 R M Schahfer 14 Dry basis Bery llium 6085 R M Schahfer 14 Dry basis Cadmium 6085 R M Schahfer 14 Dry basis Chlorine 6085 R M Schahfer 14 Dry basis Chromium 6085 R M Schahfer 14 Dry basis Cobalt 6085 R M Schahfer 14 Dry basis Fluorine 6085 R M Schahfer 14 Dry basis Lead 6085 R M Schahfer 14 Dry basis Manganese 6085 R M Schahfer 14 Dry basis Mercury 6085 R M Schahfer 14 Dry basis Nickel 6085 R M Schahfer 14 Dry basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) ASTM D5865 ASTM D3302 ASTM D3174 ASTM D4239 Method B ASTM D5865 ASTM D3174 ASTM D4239 ASTM D3683 ASTM D3683 ASTM D3683 ASTM D3683 ASTMD4208 ASTM D3683 ASTM D3683

ASTM D3683 ASTM D3683 ASTM D6722 ASTM D3683 ASTM D3683EIA Facility Code Facility

Name Boiler ID HAPs Test Group 6085 R M Schahfer 14

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Run 1 4/28/2010 4/28/2010 8976.00 Btu/lb Run 2 4/28/2010 4/28/2010 8907.00 Btu/lb Run 3 4/29/2010 4/29/2010 9178.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) 4.73 0.02 12236.00 Btu/lb 26.64 6.45 4.84 0.02 12200.00 Btu/lb 26.99 6.63 4.79 0.02 12393.00 Btu/lb 25.94 6.46% Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony (Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic Units 0.03 0.03 % 0.06 μg/g <1.0 μg/g <1.0 μg/g 0.02 0.02 % 0.08 μg/g <1.0 μg/g 2 μg/g 0.03 0.03 % 0.08 μg/g <1.0 μg/g 2 μg/gBeryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) 0.3 μg/g <2.0 μg/g 4 μg/g 3 μg/g 8 0.4 μg/g <2.0 μg/g 5 μg/g 2 μg/g 9 0.4 μg/g <2.0 μg/g 5 μg/g 2 μg/g 10Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units μg/g 4 μg/g <1.0 μg/g 2 μg/g μg/g 4 μg/g <1.0 μg/g 2 μg/g μg/g 4 μg/g <1.0 μg/g 2 μg/gEIA Facility Code Facility

Name Boiler ID HAPs Test Group 6085 R M Schahfer 14

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 1 4/27/2010 4/27/2010 8787.00 Btu/lb 2 4/27/2010 4/27/2010 8904.00 Btu/lb 3 4/27/2010 4/27/2010 8976.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) 28.09 4.65 0.33 12220 Btu/lb 6.47 27.18 4.88 0.35 12228 Btu/lb 6.7 26.65 4.74 0.36 12237 Btu/lb 6.46% Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony (Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic Units 0.45 0.02 % 0.49 0.03 % 0.49 0.03 %Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis)Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units 65.3 62.6 62.1EIA Facility Code Facility

Name Boiler ID HAPs Test Group 6085 R M Schahfer 14

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 1 4/6/2010 4/6/2010 9550.00 Btu/lb 2 4/6/2010 4/6/2010 9918.00 Btu/lb 3 4/6/2010 4/6/2010 9867.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) 22.26 5.32 0.43 12285 Btu/lb 6.84 19.52 5.7 0.53 12323 Btu/lb 7.08 19.85 5.22 0.49 12310 Btu/lb 6.51% Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony (Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic Units 0.55 0.66 0.61Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis)Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsEIA Facility Code Facility

Name Boiler ID HAPs Test Group 6085 R M Schahfer 14

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis)% Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony (Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic UnitsBeryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis)Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm