P.1 

Appendix IX Volatile Organics 

Method 8240 

CIient Name: 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

American Petroleum Institute 

STOCK TANK BOTTOMS 

007531-0002-SA Enseco ID: 

WAS~E Sampled: 

17 NOV 89 Prepared: 

Acetone 

Acetonitrile 

Acrolein 

Acrylonitrile 

Allyl chloride 

Benzene 

Bromod i chloromethane 

Bromoform 

Bromomethane 

Carbon disulfide. 

Carbon tetrachloride 

Chlorobenzene 

Chloroprene 

Chloroethane 

Chlorodi bromomethane 

Chloroform 

Chloromethane 

DBCP (1,2-Dibromo3-chlorop-opane) 

EDB (1,2-Dibr^.iioethane) 

Dibromomethane 

trans-1,4-Dichloro2-butene 

Dichlorodi fluoromethane 

1,1-Dichloroethane 

1,2-Dichloroethane 

trans-1,2-Dichloroethene 

1,1-Dichloroethene 

Dichloromethane 

1,2-Dichloropropane 

cis-1,3-Dich1oropropene 

trans-1,3-Dichloropropene 

1,4-Dioxane 

Ethyl benzene 

Ethyl cyanide 

2-Hexanone 

Iodomethane 

Isobutyl alcohol 

Methacrylonitrile 

Methyl ethyl ketone 

4-Methyl-2-pentanone 

1060349 

IF NOV 89 

20 NOV 89 

esult 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

NO 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

Rec -.eived: 17 NOV 

Analyzed: 28 NOV 

Units 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg < 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

Reporting 

Limit 

1000 

10000 

10000 

10000 

500 

500 

500 

500 

1000 

500 

500 

500 

500 

1000 

500 

500 

1000 

500 

500 

500 

500 

1000 

500 

500 

500 

500 

500 

500 

500 

500 

10000 

500 

500 

1000 

500 

10000 

500 

1000 

1000 

89 

89 

(continued on following page) 

Reported By: Terry Riddle Approved By: Jeff Lowry 

ND = Not detected 

NA « Not applicable 
P.2 

Rocky Mountain Ensec 0 [ncorpora[ed 

Analytical Laboratory 

ANALYTICAL RESULTS 

FOR 

AMERICAN PETROLEUM INSTITUTE 

ENSECO-RMAL NO. 007531 

FEBRUARY 6, 1990 

Reviewed by: ^k-LSCO^ (, lAUSTi 

-. Susan C. Wyatt 

Enseco 

/ 

Maureen A. McDevitt 

•4955 Yarrow Street 

Arvada. Colorado 80002 

303/421-6611 

Facsimile: 303/431-7171 
P.3 

General Inorganics 

Client Name: 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

American Petroleum Institute 

Site #2 Bottom Solids 

007314-001 

WASTE 

01 NOV 89 

Chloride 

Cyanide, Reactive 

Ignitability 

Non-Volatile Oil 

Volatile Oil 

Oil 

Water 

Solids 

pH 

Sulfide, Reactive 

SA Enseco ID: 

Result 

8500 

ND 

82 

19.6 

0.5 

20.1 

20.8 

57.6 

8.6 

ND 

Sampled: 

Prepared: 

Units 

mg/kg 

mg/kg 

deg. F 

% 

% 

% 

% 

% 

units 

mg/kg 

1058664 

31 OCT 89 

See Below 

Reporting 

Limit 

15 

0.1 

--

0.1 

0.1 

0.1 

0.1 

0.1 

--

0.5 

Received: 

Analyzed: 

Analytical 

Method 

300.0 Mod. 

EPA/OSW 

1010/1020 

Chevron 

Chevron 

Chevron 

Chevron . 

Chevron 

9045/ASTM 

EPA/OSW 

01 

See 

NOV 

Bel 

89 

ow 

Prepared 

Date 

28 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NOV 89 

Analyzed 

Date 

28 NOV 89. 

09 NOV 89 

10 NOV 89 o i 

17 NOV 89 

17 NOV 89 

17 NO" 89 

17 r 39 

17 39 

08 89 

22 rtuV 89 

Note o : This test is unreliable for any sample other than a 

-on-aqueous liquid. 

Note z : Sample exhibits a characteristic of hazardous waste. 

ND - Not detected 

NA - Not applicable 

Reported By: Jennifer Franzen Approved By: Harold Borquez 
P.4 

Client Name: 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

Osmium (189) 

ICP/MS Metals 

Total Metals 

American Petroleum Institute 

Site #2 Bottom Solids 

007314-0004-SA Enseco ID: 1058664 

WASTE Sampled: 31 OCT 89 

01 NOV 89 Prepared: See Below 

Received: 01 NOV 89 

Analyzed: See Below 

Result 

ND 

Reporting Analytical 

Units Limit Method 

Prepared 

Date 

Analyzed 

Date 

mg/kg 2 RMAL 07 NOV 89 08 NOV 89 

ND - Not detected 

NA = Not applicable 

Reported By: Scott Heideman Approved By: Toni Tallarico 
P.5 

Metals 

TCLP Leachate 

Client Name: American Petroleum Institute 

Client ID: Site #2 Bottom Solids 

Lab ID: 007314-0004-SA Enseco ID: 1058664 

Matrix: WASTE Sampled: 31 OCT 89 Received: 01 NOV 89 

Authorized: 01 NOV 89 Preparei: See Below Analyzed: See Below 

Repor q Analytical Prepared Analyzed 

Parameter Result Units Limit ' Method Date Date 

Arsenic ND mg/L 0.5 200.7 08 NOV 89 13 DEC 89 

Barium 3.7 mg/L 0.3 200.7 08 NOV 89 13 DEC 89 

Cadmium ND mg/L 0.03 200.7 08 NOV 89 13 DEC 89 

Chromium ND mg/L 0.05 200.7 08 NOV 89 13 DEC 89 

ND 

3.7 

ND 

ND 

ND 

ND 

ND 

ND 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

Lead ND mg/L 0.3 200.7 08 NOV 89 13 DEC 89 

Silver ND mg/L 0.05 200.7 08 NOV 89 13 DEC 89-

Mercury ND mg/L 0.002 7471 10 NOV 89 13 NOV 89 

Selenium ND mg/L 0.05 270.2 08 NOV 89 13 NOV 89 

ND - Not detected 

NA « Not applicable 

Reported By: Fred Velasquez Approved By: Kimberly Conroy 
P.6 

. 

• 

Client Name: 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

Aluminum 

Antimony 

Arsenic 

Barium 

Beryl 1i urn 

Cadmium 

Calcium 

Chromium 

Cobalt 

Copper 

iLea _ _ J d 

Mercury • 

Nickel 

Potassium 

Selenium 

Silver 

Sodium 

Thallium 

T 2 _ Tin 

Vanadium 

—Zin * c 

American Petroleum 

Site #2 Bottom Sol 

007314-

WASTE 

01 NOV 

ND = Not detected 

NA - Not appl 

Reported By: 

1 

i 

! 1 

icable 

David 

•0004-SA 

89 

Result 

1180 

ND 

3 

5400 

ND 

NO 

4420 

35 

ND 

28 

54 

1.4 

7 

ND 

ND 

ND 

6100 

ND 

ND 

2 

400 

Patterson 

Metals 

Total Metals 

Institute 

ids 

•nseco ID: 

Sampled: 

Prepared: 

Units 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

/ 

1058664 

31 OCT 89 

See Below 

Reporting 

Limit 

10 

5 

1 

1 

0.2 

0.5 

20 

1 

1 

1 

5 

0.3 

4 

500 

0.5 

1 

500 

0.5 

5 

1 

1 

Received: 

Analyzed: 

Analytical 

Method 

6010 

6010 

7060 

6010 

6010 

6010 

6010 

6010 

6010 

6010 

6010 

7471 

6010 

6010 

7740 

6010 

6010 

7841 

6010 

6010 

6010 

01 NOV 

See Bel 

89 

ow 

Prepared 

Date 

07 

07 

07 

07 

07 

07 

07 

07 

07 

07 

07 

17 

07 

07 

07 

07 

07 

07 

07 

07 

07 

Approved By: Kimberly Conroy 

DEC 

DEC 

DEC 

DEC 

DEC 

DEC 

DEC 

DEC 

DEC 

DEC 

DEC 

NOV 

DEC 

DEC 

DEC 

DEC 

DEC 

DEC 

DEC 

DEC 

DEC 

89 

89 

89 

89 

89 

89 

89 

89 

89 

89 

89 

89 

89 

89 

89 

89 

89 

89 

89 

89 

89 

t 

Analyzed 

Date 

07 DEC 

07 DEC 

12 DEC 

07 DEC 

07 DEC 

07 DEC 

07 DEC 

07 DEC 

07 DEC 

07 DEC 

07 DEC 

17 NOV 

07 DEC 

07 DEC 

12 DEC 

07 DEC 

07 DEC 

11 DEC 

07 DEC 

07 DEC 

07 DEC 

89 

89 

89 

89 

89 

89 

89 

89 

•89 

89 

89 

89 

89 

89 

89 

89 

89 

89 

89 

89 

89 
P.7 

OTC Semi volatile Organics 

TCLP Leachate 

Method 8270 

Client Name: 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

American Petroleum Institute 

Site #2 Bottom Solids 

007314-0004-SA Enseco ID: 

WASTE Sampled: 

01 NOV 89 Prepared: 

Pyridine 

Phenol 

bis(2-Chloroethyl) ether 

1,4-Dichlorobenzene 

1,2-Dichlorobenzene 

o-Cresol 

m & p-Cresol(s) 

Hexachloroethane 

Nitrobenzene 

Hexachlorobutadiene 

2,4,6-Trichlorophenol 

2,4,5-Trichlorophenol 

2,4-Dinitrotoluene 

Hexachlorobenzene 

2,3,4,6-Tetrachlorophenol 

Pentachlorophenol 

Nitrobenzene-d5 

2-Fluorobiphenyl 

Terphenyl-dl4 

Phenol-d5 

2-Fluorophenol 

2,4,6-Tri bromophenol 

1058664 

31 OCT 89 

09 NOV 89 

esult 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

NO 

ND 

ND 

ND 

ND 

Units 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

% 

% 

% 

% 

% 

% 

Received: 01 NOV 89 

Analyzed: 27 NOV 89 

Reporting 

Limit 

- - • 

0.40 

0.40 

0.40 

0.40 

0.40 

0.40 

0.40 

0.40 

0.40 

0.40 

2.0 

0.40 

0.40 

0.40 

2.0 

--

--

--

--

--

ND - Not detected 

NA - Not applicable 

Reported By: Phillip Tallarico Approved By: Jeff Lowry 
P.8 

Client Name: 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

Refinery Hazardous Constituent Semivolatiles 

Method 8270 

American Petroleum Institute 

Site #2 Bottom Solids 

007314-0004-SA Enseco ID: 

WASTE Sampled: 

01 NOV 89 Prepared: 

Anthracene 

Benzo(a)anthracene 

Benzo(b)f1uoranthene 

Benzo(k)f1uoranthene 

Benzo(a)pyrene 

bis(2-Ethylhexyl) 

phthalate 

Butyl benzyl phthalate 

Chrysene 

Di benz(a,h)anthracene 

Di-n-butyl phthalate 

1,2-Di ch1orobenzene 

1,3-Di chlorobenzene 

1,4-Dichlorobenzene 

Diethyl phthalate 

7,12-Dimethylbenzanthracene 

Dimethyl phthalate 

Di-n-octyl phthalate 

FIuoranthene 

Indene 

1-Methylnaphthalene 

Naphthalene 

Phenanthrene 

Pyrene 

Pyridine 

Quinoline 

Benzenethiol 

o-Cresol 

m & p-Cresol(s) 

2,4-Dimethylphenol 

2,4-Dinitropnenol 

4-Nitrophenol 

Phenol 

Nitrobenzene-d5 

2-Fluorobiphenyl 

Terphenyl-dl4 

Phenol-d5 

2-Fluorophenol 

2,4,6-Tribromophenol 

ND - Not detected 

NA - Not applicable 

1058664 

31 OCT 89 

06 NOV 89 

esult 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

240 

270 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

49.3 

67.5 

70.8 

38.2 

48.0 

62.0 

Received: 01 NOV 89 

An 

Units 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg. 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

% 

% 

% 

% 

% 

% 

alyzed: 16 NOV 89 

Reporting 

Limit 

37 

37 

37 

37 

37 

37 

37 

37 

37 

37 

37 

37 

37 

37 

37 

37 

37 

37 

37 

37 

37 

37 

37 

--

37 

--

37 

37 

37 

180 

180 

37 

--

--

--

--

--

--

Reported By: Belinda Guerra Approved By: Jeff Lowry 
OTC Volatile Organics 

TCLP Leachate 

Method 8240 

P.9 

Client Name: 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

American Petroleum Institute 

Site #2 Bottom Solids 

007314-0004-SA Enseco ID: 1058664 

WASTE Sampled: 31 OCT 89 

01 NOV 89 Prepared: 10 NOV 89 

Vinyl chloride 

Acrylonitrile 

Methylene chloride 

Carbon disulfide 

1,1-Dichloroethene 

Isobutyl alcohol 

Chloroform 

1,2-Dichloroethane 

2-Butanone 

1,1,1-Tri chloroethane 

Carbon tetrachloride 

Trichloroethene 

1,1,2-Trichloroethane 

Benzene 

1,1,1,2-Tetrachloroethane 

1,1,2,2-Tetrachloroethane 

Tetrachloroethene 

Toluene 

Chlorobenzene 

Toluene-d8 

4-Brombfluorobenzene 

1,2-Dichloroethane-d4 

Result 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

5.2 

ND 

ND 

ND 

4.8 

ND 

101 

100 

105 

Units 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

% 

% 

% 

Received: 01 NOV 

Analyzed: 13 NOV 

Reporting 

Limit 

0.50 

5.0 

0.25 

0.25 

0.25 

5.0 

0.25 

0.25 

0.50 

0.25 

0.25 

0.25 

0.25 

0.25 

0.25 

0.25 

0.25 

0.25 

0.25 

89 

89 

ND - Not detected 

NA * Not applicable 

Reported By: Diane Page Approved By: Jeff Lowry 
P.10 

c 

J 

Appendix IX Volatile Organics (CONT.) 

Method 8240 

Client Name: 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

American Petroleum Institute 

Site #2 Bottom Solids 

007314-0004-SA Enseco ID: 1058664 

WASTE Sampled: 31 OCT 89 

01 NOV 89 Prepared: 03 NOV 89 

Received: 

Analyzed: 

01 

07 

NOV 

NOV 

89 

89 

Result Units 

Styrene 

1,1,1,2-Tetrachloroethane 

1,1,2,2-Tetrachloroethane 

Tetrachl oroethene 

Toluene 

1,1,1-Trichloroethane 

1,1,2-Trichloroethane 

Trichloroethene 

Tri chlorof1uoromethane 

1,2,3-Tri chloropropane 

Vinyl acetate 

Vinyl chloride 

Xylenes (total) 

Toluene-d8 

4-Bromofluorobenzene 

l,2-Dichloroethane-d4 

ND 

ND 

ND 

ND 

350 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

460 

109 

91.1 

88.6 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

% 

% 

% 

Reporting 

Limit 

50 

50 

50 

50 

50 

50 

50 

50 

50 

50 

100 

100 

50 

ND =» Not detected 

NA « Not applicable 

Reported By: Tim Miller Approved By: Jeff Lowry 
P.11 

Appendix IX Volatile Organics 

Method 8240 

Client Name: American Petroleum Institute 

Client ID: Site #2 Bottom Solids 

Lab ID: 007314-0004-SA Enseco ID: 1058664 

Matrix: WASTE Sampled: 31 OCT 89 

Authorized: 01 NOV 89 Prepared: 03 NOV 89 

Parameter Result 

Acetone ND 

Acetonitrile ND 

Acrolein ND 

Acrylonitrile ND 

Allyl chloride ND 

Benzene 100 

Bromodichloromethane ND 

Bromoform ND 

Bromomethane ND 

Carbon disulfide- ND 

Carbon tetrachloride ND 

Chlorobenzene ND 

Chloroprene ND 

Chloroethane ND 

Chlorodibromomethane ND 

Chloroform ND 

Chloromethane ND 

DBCP (1,2-Dibromo3-chloropropane) ND 

EDB (1,2-Dibromoethane) ND 

Dibromomethane ND 

trans-1,4-Dichloro2-butene ND 

Dichlorodif1uoromethane ND 

1,1-01chloroethane ND 

1,2-Dichloroethane ND 

trans-1,2-Dichloroethene ND 

1,1-Dichloroethene ND 

Dichloromethane ND 

1,2-Dichloropropane NO 

cis-1,3-Dichloropropene ND 

trans-1,3-Dichloropropene NO 

i,4-Dioxane ND 

Ethyl benzene 94 

Ethyl cyanide ND 

2-Hexanone ND 

Iodomethane ND 

Isobutyl alcohol ND 

Methacrylonitrile NO 

Methyl ethyl ketone NO 

4-Methyl-2-pentanone ND 

Received: 01 NOV 

Analyzed: 07 NOV 

Units 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mgAg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

Reporting 

Limit 

100 

1000 

1000 

1000 

50 

50 

50 

50 

100 

50 

50 

50 

50 

100 

50 

50 

100 

50 

50 

50 

50 

100 

50 

50 

50 

50 

50 

50 

50 

50 

1000 

50 

50 

100 

50 

1000 

50 

100 

100 

89 

89 

ND * Not detected 

NA - Not applicable 

Reported By: Tim Miller 

(continued on following page) 

Approved By: Jeff Lowry 
P.12 

ANALYTICAL RESULTS 

FOR 

BP AMERICA INC. 

ENSECO-RMAL NO. 007314 

JANUARY 5, 1990 

Reviewed by: 

Sudan C. Wyftt 

Parr 

Enseco Incorporated 

4955 Yarrow Street • 

Arvada. Colorado 80002 

303/421-6611 Fax: 303/431-7171 

Rocky Mountain 

Analytical Laboratory 

Enseco 
P.13 

71 3> 

•OV 3< 

.OV s-
1 

J 

General Inorganics 

P.14 

Client Name; 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

American Petroleum Institute 

Site #3 Crude Oil Bottom Str 

006299-0004-SA Enseco ID: 

WASTE Sameled: 

28 AUG 89 Prepared: 

Chloride 

Cyanide, Reactive 

Ignitability 

Non-Volatile Oil 

Volatile Oil 

Oil 

Water 

Solids 

pH 

Sulfide, Reactive 

Result Units 

25100 

ND 

127 

19 

0 

20 

25 

1050768 

24 AUG 89 

See Below 

Received: 

Analyzed: 

54.8 

8.4 

50 

Reporting Analytical 

Limit Method 

mg/kg 

mg/kg 

deg. F 

r. 

% 

% 

% 

% 

units 

mg/kg 

15 

0.1 

0.1 

0.1 

0.1 

0.1 

0.1 

0.5 

300.0 Mod. 

EPA-OSW 

1010/1020 

Chevron 

Chevron 

Chevron 

Chevron 

Chevron 

9045/ASTM 

EPA/OSW 

25 AUG 89 

See Below 

Prepared 

Date 

07 SEP 89 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

Analyzed 

Date 

13 SEP 89 

08 SEP 89 

11 0CT89 ol 

i9 OCT 89 

19 OCT 89 

19 OCT 89 

19 OCT 89 

19 OCT 89 

11 SEP 89 

08 SEP 89 

Note o : This test is unreliable for any sample other than a 

non-aqueous liquid. 

J Note 1 : Sample 4 is hazardous due to ignitability for flashpoint. 

1 

1 

] 

ND - Not detected 

NA - Not applicable 

Reported By: Blake Besser Approved By: Tammy.Bailey 
P.15 

J ient Name: 

Client ID: 

' ab ID: 

atrix: 

Authorized: 

'arameter 

Appendix IX Volatile Organics (CONT.) 

Method 8240 

American Petroleum Institute 

Ramsey-Crude Tank Bottoms 

011425-0001-SA 

WASTE Sampl< 

21 SEP 90 Prepan 

Styrene 

1,1,1,2-Tetrachloroethane 

i,1,2,2-Tetrachloroethane 

Tetrachloroethene 

Toluene 

1,1,1 -Tri chloroethane 

1,1,2-Tri chloroethane 

Trichl oroethene 

Tri chl orof1uoromethane 

1,2,3-Trichloropropane 

Vinyl acetate 

Vinyl chloride 

Xylenes (total) 

Surrogate 

Toluene-d8 

4-Bromofluorobenzene 

1,2-Di chloroethane-d4 

20 SEP 90 

25 SEP 90 

Result 

ND 

ND 

ND 

ND 

2400 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

4300 

Recovery 

105 

97 

99 

Units 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

% 

% 

% 

Received: 21 SEP 90 

Analyzed: 27 SEP 90 

Reporting 

Limit 

250 

250 

250 

250 

250 

250 

250 

250 

250 

250 

500 

500 

250 

--

--

ND » Not detected 

NA - Not applicable 

Reported By: Michael Blades Approved By: Jeff Lowry 
P.16 

OTC 

Client Name: American Petroleum 

Client ID: Ramsey-Crude Tank E 

Lab ID: 011425-0001-SA 

Matrix: WASTE 

Authorized: 21 SEP 90 

Parameter 

Vinyl chloride 

1,1-Dichloroethene 

Chloroform 

1,2-Dichloroethane 

2-But*npne 

Carbon-tetrachloride 

Trichlbroethene 

Benzege* 

Tetrachloroethene 

Chlorobenzene 

Surrogate 

Toluene-d8 

4-Bromofluorobenzene 

l,2-Dichloroethane-d4 

Volatile Organics 

TCLP Leachate 

Method 8240 

nstitute 

ttoms 

Sampled: 20 SEP 90 

repared: 27 SEP 90 

Result 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

27 

ND 

NO 

Recovery 

103 

104 

101 

Units 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

% 

% 

% 

Received: 21 SEP 90 

Analyzed: 11 OCT 90 

Reporting 

Limit 

26 

13 

13 

13 

26 

13 

13 

13 

13 

13 

--

--

ND « Not detected 

NA • Not applicable 

Reported By: Terry Riddle Approved By: Jeff Lowry 
P.17 

Metals 

TCLP Leachate 

Client Name: American Petroleum Institute 

Client ID: Ramsey-crude tank bottoms 

Lab ID: 011425-0001-SA 

Matrix: WASTE Sampled: 18 SEP 90 Received:,21 SEP 90 

Authorized: 21 SEP 90 Prepared: See Below Analyzed:'See Below 

Parameter 

Arsenic 

Barium 

Cadmium 

Chromium 

Lead 

Silver 

Mercury 

Selenium. 

Result 

ND 

1.6 

0.32 

ND 

ND 

ND 

ND 

ND 

Units 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

Reporting 

Limit 

1.3 

0.13 

0.062 

0.13 

0.62 

0.13 

0.0075 

0.062 

Analytical 

Method 

6010 

6010 

6010 

6010 

6010 

6010 

7470 

7740 

1 

] 

Prepared Analyzed 

Date Date 

28 SEP 90 23 OCT 90 

28 SEP 90 23 OCT 90 

28 SEP 90 23 OCT 90 

28 SEP 90 23 OCT 90 

28 SEP 90 23 OCT 90 

28 SEP 90 23 OCT 90 

23 OCT 90 23 OCT 90 

28 SEP 90 23 OCT 90 

ND - Not detected 

NA - Not applicable 

Reported By: Fred Velasquez Approved By: Toni Lusk 
P.18 

General Inorganics 

Client Name: 

Client ID: 

Lab ID 

Matrix: 

Authorized: 

Parameter 

American Petroleum Institute 

Ramsey-Crude Tank Bottoms 

011425-0001-SA 

WASTE Sampled: 

21 SEP 90 Prepared: 

20 SEP 90 

See Below 

Received: 

Analyzed: 

Reporting Analytical 

Result Units Limit Method 

21 SEP 90 

See Below 

Prepared 

Date 

Analyzed 

Date 

Cyanide, Reactive 

Ignitability 

Non-Volatile Oil 

Volatile Oil 

Oil G 

Water 

Solids. 

PH 

Sulfide, Reactive 

ND 

79.0 

29.0 

63.0 

92.0 

4.8 

3.2 

6.7 

ND 

mg/kg 

deg. F 

% 

% 

% 

% 

% 

units 

mg/kg 

0.10 

0.1 

0.9 

0.9 

0.9 

0.1 

--

0.50 

EPA/OSW 

1010 

Chevron 

Cherron 

Cherron 

Chevron 

Chevron 

9045/ASTM 

EPA/OSW 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

25 SEP 90 

26 SEP 90 oz 

20 OCT 90 

20 OCT 90 

20 OCT 90 

20 OCT 90 

20 OCT 90. 

22 SEP 90 

02 OCT 90 

Note o : This test is unreliable for any sample other than a 

non-aqueous liquid. 

Note z : Sample ejc^ibits a characteristic of hazardous waste. 

ND » Not detected 

NA * Not applicable 

Reported By: Ron Maiorana Approved By: John Laferty 
P.19 

Appendix IX Volatile Organics 

Method 8240 

Client Name: American Petroleum 

Client ID: Prairie Dale-Crude 

Lab ID: 011425-0005-SA 

Matrix: WASTE 

Authorized: 21 SEP 90 

Parameter 

Acetone 

Acetonitrile 

Acrolein 

Acrylonitrile 

Allyl chloride 

Benzene 

Bromodichloromethane 

Bromoform 

Bromomethane 

Carbon disulfide 

Carbon tetrachloride 

Chlorobenzene 

Chloroprene 

Chloroethane 

Di bromochloromethane 

Chloroform 

Chloromethane 

DBCP (1,2-Dibromo3-chloropropane) 

EDB (1,2-Dibromoethane) 

Dibromomethane 

trans-l,4-0ichloro2-butene 

Dichlorodifluoromethane 

1,1-Dichloroethane 

1,2-Dichloroethane 

trans-1,2-Di chloroethene 

1,1-Dichloroethene 

Dichloromethane 

1,2-Dichlbropropane 

cis-1,3-Dichloropropene 

• trans-1,3-Dichloropropene 

1,4-Dioxane 

Ethyl benzene 

Ethyl cyanide 

2-Hexanone 

j Iodomethane 

Isobutyl alcohol 

4 Methacrylonitrile 

2-Butanone (MEK) 

-J 4-Methyl-2-pentanone 

Institute 

Tank Btm. 

Sampled: 

Prepared: 

20 SEP 

25 SEP 

Result 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

NO 

NO 

ND 

ND 

NO 

NO 

ND 

ND 

ND 

NO 

NO 

NO 

ND 

ND 

ND 

ND 

ND 

NO 

ND 

ND 

260 

NO 

ND 

NO 

NO 

ND 

ND 

ND 

90 Received: 21 SEP 

90 An 

Units 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

alyzed: 27 SEP 

Reporting 

Limit 

100 

1000 

1000 

1000 

50 

50 

50 

50 

100 

50 

50 

50 

50 

100 

50 

50 

100 

50 

50 

50 

50 

100 

50 

50 . 

50 

50 

50 

50 

50 

50 

1000 

50 

50 

100 

50 

1000 

50 

100 

100 

90 

90 

(continued on following page) 

ND - Not detected 

NA - Not applicable 

Reported By: Michael Blades Approved By: Jeff Lowry 
P.20 

Appendix IX Volatile Organics (CONT.) 

Method 8240 

Client Name: American Petroleum Institute 

Client ID: Prairie Dale-Crude Tank Btm. 

Lab ID: 011425-0005-SA 

Matrix: WASTE Sampled: 20 SEP 90 Re . ved: 21 SrP 90 

Authorized: . 21 SEP 90 Prepared: 25 SEP 90 Ana zed: 27 SEP 90 

Reporting 

Parameter Result Units Limit 

Styrene ND mg/kg 50 

1,1,1,2-Tetrachloroethane ND mg/kg 50 

1,1,2,2-Tetrachloroethane ND mg/kg 50 

Tetrachloroethene ND mg/kg 50 

Toluene 490 mg/kg 50 

1,1,1-Trichloroethane ND mg/kg 50 

1,1,2-Trichloroethane ND mg/kg 50 

Trichloroethene ND mg/kg 50 

Trichlorofluoromethane ND mg/kg 50 

1,2,3-Trichloropropane ND mg/kg. 50 

Vinyl acetate ND mg/kg 100 

Vinyl chloride ND mg/kg 100 

Xylenes (total) 1200 mg/kg 50 

Surrogate Recovery 

Toluene-d8 110 % 

4-Bromofluorobenzene 92 % 

l,2-Dichloroethane-d4 105 % 

ND - Not detected 

NA » Not applicable 

Reported By: Michael Blades Approved By: Jeff Lowry 
P.21 

OTC Volatile Organics 

TCLP Leachate 

Method 8240 

Client Name: American Petroleum 

Client ID: Prairie Dale 

Lab ID: 011425-0005-

Matrix: WASTE 

Authorized: 21 SEP 90 

Parameter 

Vinyl chloride 

1,1-Dichloroethene 

Chloroform 

1,2-Dichloroethane 

2-Butanone 

Carbon tetrachloride 

Trichloroethene 

Benzene 

Tetrachloroethene 

Chlorobenzene 

Surrogate 

Toluene-d8 

4-Bromofluorobenzene 

1,2-Dichloroethane-d4 

'-Crude 

SA 

Inst1 

Tank 

tute 

Btm. 

Sampled: 20 SEP 

Prepared: 29 SEP 

Result 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

0.37 

ND 

ND 

90 

90 

. 

Recovery 

102 

97 

95 

Units 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

% 

% 

% 

Received: 21 SEP 90 

Analyzed: 05 OCT 90 

Reporting 

Limit 

0.50 

0.25 

0.25 

0.25 

0.50 

0.25 

0.25 

0.25 

0.25 

0.25 

--

--

ND » Not detected 

NA - Not applicable 

Reported By: Deneen Miller , Approved By: Jeff Lowry 
P.22 

Metals 

Client Name: 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

Arsenic 

Barium 

Cadmium 

Chromium 

Lead. 

Silver 

Mercury 

Selenium 

American Petrol 

Prairie 

011425-

WASTE 

21 SEP 

TCLP 

eum Insti 

: dale-crude tank 

0005-SA 

90 

Result 

ND 

2.3 

ND 

ND 

ND 

ND 

ND 

NO 

Leachate 

tute 

bottoms 

Sampled: 

Prepared: 

Units 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

20 SEP 90 Received 

See Below Analyzed 

Reporting 

Limit 

1.0 

0.10 

0.050 

0.10 

0.50 

0.10 

0.0020 

0.050 

Analytical 

Method 

6010 

6010 

6010 

6010 

6010 

6010 

7470 

7740 

: 21 SEP 90 

: See Below 

Prepared Analyzed 

Date Date 

28 SEP 90 09 OCT 90 

28 SEP 90 09 OCT 90 

28 SEP 90 09 OCT 90 

28 SEP 90 09 OCT 90 

28 SEP 90 09 OCT.90 

28 SEP 90 09 OCT:90 

05 OCT 90 10 OCT'90 

28 SEP 90 01 OCT 90 

] 

1 

J 

ND « Not detected 

NA • Not applicable 

Reported By: Mark Brundege Approved By: Toni Lusk 
P.23 

General Inorganics 

CIient Name: 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

American Petroleum Institute 

Prairie Dale-Crude Tank Btm. 

011425-

WASTE 

21 SEP 

Cyanide, Reactive 

Ignitability 

Non-Volatile 

Volatile Oil 

Oil 

Water 

Solids 

pH 

Oil 

Sulfide, Reactive 

•0005-SA 

Sampled: 

90 Prepared: 

20 SEP 

See Bel 

Reporting 

Result Units 

ND mg/kg 

81.0 deg. F 

15.2 % 

13.5 % 

28.7 % 

45.9 7. 

25.4 % 

6.1 units 

ND mg/kg 

Limit 

0.10 

--

0.1 

0.5 

0.5 

0.5 

0.1 

--

0.50 

90 Rec« 

ow Ana 

Analytical 

Method 

EPA/OSW 

1010 

Chevron 

Chevron 

Chevron 

Chevron 

Chevron 

9045/ASTM 

EPA/OSW 

jived 

yzed 

: 21 SEP 

: See Bel 

Prepared 

Date 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

90 

ow 

Analyzed 

Date 

25 SEP 90 

26 SEP 90 oz 

20 OCT 90 

20 OCT 90 

20 OCT 90 

20 OCT 90 

20 OCT 90 

22 SEP 90 

02 OCT 90 

Note o : This test is unreliable for any sample other than a 

non-aqueous liquid. 

Note z : Sample exhibits a characteristic of hazardous waste. 

ND = Not detected 

NA - Not applicable 

Reported By: Ron Maiorana Approved By: John Laferty 
P.24 

1 

Appendix IX Volatile Organics ' 

Method 8240 

Client Name: American Petroleum Institute 

Client ID: County Line-FWK Bottoms 

Lab ID: 011425-0004-SA 

Matrix: WASTE Sampled: 

Authorized: 21 SEP 90 Prepared: 

Parameter 

Acetone 

Acetonitrile 

Acrolein 

Acrylonitrile 

Allyl chloride 

Benzene 

3romodi chloromethane 

Bromoform 

Bromomethane 

Carbon disulfide 

Carbon tetrachloride 

Chlorobenzene 

Chloroprene 

Chloroethane 

Dibromochloromethane 

Chloroform 

Chloromethane 

DBCP (1,2-Dibromo3-chloropropane) 

EDB (1,2-Dibromoethane) 

Dibromomethane 

trans-1,4-Dichloro2-butene 

Dichlorodifluoromethane 

1,1-Dichloroethane 

1,2-Dichloroethane 

trans-1,2-Dichloroethene 

1,1-Dichloroethene 

Dichl oromethane 

1,2-Dichloropropane 

cis-l,3-Dichioropropene 

trans-1,3-Dichloropropene 

1,4-Dioxane 

Ethyl benzene 

Ethyl cyanide 

2-Hexanone 

Iodomethane 

Isobutyl alcohol 

Methacrylonitrile 

2-Butanone (MEK) 

4-Methyl-2-pentanone 

(continued on following page) 

ND - Not detected 

NA - Not applicable 

Reported By: Stephanie Boehnke Approved By: Jeff Lowry 

20 SEP 

25 SEP 

esult 

ND 

ND 

ND. 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

NO 

ND 

ND 

ND 

NO 

ND 

ND 

NO 

NO 

ND 

ND 

NO 

NO 

ND 

NO 

NO 

ND 

NO 

"ND 

ND 

NO 

NO 

ND 

90 Received: 21 SEP 90 

.90 An 

Units 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

alyzed: 26 SEP 90 

Reporting 

Limit 

50 

500 

500 

500 

25 

25 

25 

25 

50 

25 

25 

25 

25 

50 

25 

25 

50 

25 

25 

25 

25 

50 

25 

25 

25 

25 

25 

25 

25 

25 

500 

25 

25 

50 

25 

500 

25 

50 

50 
1 

-

Appendix IX Volatile Organics (CONT.) 

Method 8240 

Client Name: American Petroleum Institute 

Client ID: County Line-FWK Bottoms 

Lab ID: 011425-0004-SA 

Matrix: WASTE Sampled: 20 SEP 

Authorized: 21 SEP 90 Prepared: 25 SEP 

Parameter 

Styrene 

1,1,1,2-Tetrachloroethane 

1,1,2,2-Tetrachloroethane 

Tetraehloroethene 

Toluene 

1,1,1-Tri chloroethane 

1,1,2-Trichloroethane 

Triehloroethene 

Result 

ND 

ND 

ND 

ND 

35 

ND 

ND 

ND 

90 

90 

Units 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

Received: 21 

Analyzed: 26 

Reporting 

Limit 

25 

25 

25 

25 

25 

25 

25 

25 

SEP 90 

SEP 90 

• 

P.25 

Tri chl orofluoromethane 

1,2,3-Trichloropropane 

Vinyl acetate 

Vinyl chloride 

Xylenes, (total) 

Surrogate 

Toluene-d8 

4-Bromofluorobenzene 

1,2-Dichloroethane-d4 

Recovery 

105 

102 

99 

% 

% 

% 

ND - Not detected 

NA - Not applicable 

Reported By: Stephanie Boehnke Approved By: Jeff Lowry 
P.26 

OTC Volatile Organics 

TCLP Leachate 

Method 8240 

Client Name: American Petroleum Institute 

Client ID: County Line-FWK Bottoms 

Lab ID: 011425-0004-SA 

Matrix: WASTE Sampled: 20 SEP 90 Received: 21 SEP 90 

Authorized: 21 SEP 90 Prepared: 29 SEP 90 Analyzed: 04 OCT 90 

Reporting 

Parameter Result Units Limit 

Vinyl chloride ND mg/L 0.10 

1,1-Dichloroethene ND mg/L 0.050 

Chloroform ND mg/L 0.050 

1,2-Dichloroethane ND mg/L 0.050 

2-Butanone ND mg/L 0.10 

Carbon tetrachloride ND mg/L 0.050 

Trichl -oethene NO mg/L 0.050 

Benzene 0.21 mg/L 0.050 

Tetraehloroethene ND mg/L 0.050 

Chlorobenzene ND mg/L 0.050 

Surrogate Recovery 

Toluene-d8 98 % '0 

4-Bromofluorobenzene 96 % 

l,2-Dichloroethane-d4 101 % 

ND » Not detected 

NA * Not applicable 

Reported By: Stephanie Boehnke Approved By: Jeff Lowry 
P.27 

Metals 

TCLP Leachate 

Client Name: American Petroleum Institute 

Client ID: County line-free water knockout bottoms 

Lab ID: 011425-0004-SA 

Matrix: WASTE Sampled: 20 SEP 90 Received: 21 SEP 90 

Authorized: 21 SEP 90 Prepared: See Below Analyzed: See Below 

Reporting Analytical Prepared Analyzed 

Parameter Result Units Limit Method Date Date 

Arsenic ND mg/L 1.0 6010 28 SEP 90 09 OCT 90 

Barium 3.4 mg/L 0.10 6010 28 SEP 90 09 OCT 90 

Cadmium ND mg/L 0.050 6010 28 SEP 90 09 OCT 90 

Chromium ND mg/L 0.10 6010 28 SEP 90 09 OCT 90 

Lead 1.0 mg/L 0.50 6010 28 SEP 90 09 OCT 90 

Silver ND mg/L 0.10 6010 28 SEP 90 09 OCT 90 

Mercury ND mg/L 0.0020 7470 05 OCT 90 10 OCT 90 

Selenium ND mg/L 0.050 7740 28 SEP 90 01 OCT 90 

) ND = Not detected 

J NA * Not applicable 

Reported By: Mark Brundege Approved By: Toni Lusk 

I 
General Inorganics 

P.28 

CIient Name: 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

American Petroleum Institute 

County Line-FWK Bottoms 

011425-0004-SA 

WASTE Sampled: 

21 SEP 90 Prepared: 

20 SEP 90 Received: 21 SEP 90 

See Below Analyzed: See Below 

Parameter 

Cyanide, Reactive 

Ignitability 

Non-Volatile Oil 

Volatile Oil 

Oil 

Water 

Solids . 

pH 

Sulfide, Reactive 

Result. 

ND 

>160 

21.3 

18.0 

39.3 

45.5 

15.2 

7.8 

ND 

Units 

mg/kg 

deg. F 

% 

% 

% 

% 

% 

units 

mg/kg 

Reporting 

Limit 

0.10 

--

0.1 

0.5 

0.5 

0.5 

0.1 

--

0.50 

Analytica 

Method 

EPA/OSW 

1010 

Chevron 

Chevron 

Chevron 

Chevron 

Chevron 

9045/ASTM 

EPA/OSW 

Prepared 

Date 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

Analyzed 

Date 

25 SEP 90 

26 SEP 90 

20 OCT 90 

20 OCT 90 

20 OCT 90 

20 OCT 90 

20 OCT 90 

22 SEP 90 

02 OCT 90. 

Note o : This test is unreliable for any sample other than a 

non-aqu&ous liquid. 

ND - Not detected 

NA - Not applicable 

Reported By: Ron Maiorana Approved By: John Laferty 
P.29 

Appendix IX Volatile Organics 

Method 8240 

Client Name: 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

American Petroleum Institute 

Semivole-Crude Tank Bottoms 

011425-0003-SA 

WASTE Sampled: 

21 SEP 90 Prepared: 

20 

25 

SEP 

SEP 

90 

90 

Acetone 

Acetonitrile 

Acrolein 

Acrylonitrile 

Allyl chloride 

Benzene 

Bromodi chloromethane 

Bromoform 

Bromomethane 

Carbon disulfide 

Carbon tetrachloride 

Chlorobenzene 

Chloroprene 

Chloroethane 

Dibromochloromethane 

Chloroform 

Chl oromethane 

DBCP (1,2-Dibromo3-chloropropane) 

EDB (1,2-Dibromoethane) 

Dibromomethane 

trans-1,4-Dichloro2-butene 

Di chl orodi f1uoromethane 

1,1-Dichloroethane 

1,2-Dichloroethane 

trans-1,2-Dichloroethene 

1,1-Oichloroethene 

Dichloromethane 

1,2-Dichloropropane 

cis-l,3-Dichioropropene 

trans-1,3-Di chloropropene 

1,4-Dioxane 

Ethyl benzene 

Ethyl cyanide 

2-Hexanone 

Iodomethane 

Isobutyl alcohol 

Methacrylonitrile 

2-Butanone (MEK) 

4-Methyl-2-pentanone 

Result 

ND 

ND 

ND 

ND 

ND 

5500 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

NO 

ND 

ND 

ND 

NO 

NO 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

7400 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

Received: 21 SEP 90 

Analyzed: 28 SEP 90 

Reporting 

Units Limit 

mg/kg 5000 

mg/kg 50000 

mg/kg 50000 

mg/kg 50000 

mg/kg 2500 

mg/kg 2500 

mg/kg 2500 

mg/kg 2500 

mg/kg 5000 

mg/kg 2500 

mg/kg 2500 

mg/kg 2500 

mg/kg 2500 

mg/kg 5000 

mg/kg 2500 

mg/kg 2500 

mg/kg 5000 

mg/kg 2500 

mg/kg 2500 

mg/kg 2500 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

2500 

5000 

2500 

2500 

2500 

2500 

2500 

2500 

2500 

2500 

50000 

2500 

2500 

5000 

2500 

50000 

2500 

5000 

5000 

ND 

NA 

Not 

Not 

detected 

applicable 

(continued on following page) 

Reported By: Michael Blades Approved By: Jeff Lowry 
P.30 

CIient Name: 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

Appendix IX Volatile Organics (CONT.) 

Method 8240 

American Petroleum Institute 

Semi vole-Crude Tank Bottoms 

011425-0003-SA 

WASTE Sampled: 

21 SEP 90 Prepared: 

Styrene 

1,1,1,2-Tetrachloroethane 

1,1,2,2-Tetrachloroethane 

Tetraehloroethene 

Toluene . 

1,1,1-Trichloroethane 

1,1,2-Trichloroethane 

Triehloroethene 

Trichlorof1uoromethane 

1,2,3-Tri chloropropane 

Vinyl acetate 

Vinyl chloride 

Xylenes (total) 

Surrogate 

Toluene-d8 

4-Bromof1uorobenzene 

l,2-Dichloroethane-d4 

,0 SEP 

25 SEP 

Result 

ND 

ND 

ND 

ND 

32000 

ND 

ND 

ND 

ND 

NO 

ND 

NO 

52000 

90 

90 

Recovery 

109 

96 

100 

Units 

^g/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

% 

% 

% 

Received: 21 

Analyzed: 28 

Reporting 

Limit 

2500 

2500 

2500 

2500 

2500 

2500 

2500 

2500 

2500 

2500 

5000 

5000 

2500 

--

--

SEP 90 

SEP 90 

ND - Not detected 

NA - Not applicable 

Reported By: Michael Blades Approved By: Jeff Lowry 
P.31 

OTC Volatile Organics 

TCLP Leachate 

Method 8240 

Client Name: American Petroleum Institute 

Client ID: Semivole-Crude Tank Bottoms 

Lab ID: 011425-0003-SA 

Matrix: WASTE Sampled: 

Authorized: 21 SEP 90 Prepared: 

Parameter 

Vinyl chloride 

1,1-Dichloroethene 

Chloroform 

1,2-Dichloroethane 

2-Butanohe 

Carbon tetrachloride 

Triehloroethene 

Benzene 

Tetrachloroethene 

Chlorobenzene 

Surrogate' 

Toluene-d8 

4 -Bromof1uorobenzene 

1,2-Dichloroethane-d4 

20 SEP 

29 SEP 

esul t 

ND 

ND 

ND 

ND 

NO 

ND 

ND 

3.0 

ND 

ND 

kCtUVC^ 

99 

97 

96 

90 

90 

7 

Units 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

% 

% 

% 

Received: 21 SEP 90 

Analyzed: 05 OCT 90 

Reporting 

Limit 

1.0 

0.50 

0.50 

0.50 

1.0 

0.50 

0.50 

0.50 

0.50 

0.50 

--

--

ND - Not detected 

NA - Not applicable 

Reported By: Deneen Miller Approved By: Jeff Lowry 
P.32 

Metals 

TCLP Leachate 

Client Name: American Petroleum Institute 

Client ID: Semivole-crude tank bottoms 

Lab ID: 011425-0003-SA 

Matrix: WASTE Sampled: 17 SEP 90 Received: 21 SEP 90 

Authorized: 21 SEP 90 Prepared: See Below Analyzed: See Below 

Reporting Analytical Prepared Analyzed 

Parameter Result Units Limit Method Date Date 

Arsenic ND mn/L 1.0 6010 28 SEP 90 02 OCT 90 

Barium 2.6 r L 0.38 6010 28 SEP 90 02 OCT 90 

Cadmium ND m^/L 0.050 6010 28 SEP 90 02 OCT 90 

Chromium 0.47 mg/L 0.10 6010 28 SEP 90 02 OCT 90 

Lead ND mg/L 

Silver ND mg/L 

Mercury ND mg/L 

Selenium ND mg/L 0.050 7740 28 SEP 90 01 OCT 90 

1.0 

0.38 

0.050 

0.10 

0.50 

0.10 

0.0020 

0.050 

6010 

6010 

6010 

6010 

6010 

6010 

7470 

7740 

28 

28 

05 

SEP 

SEP 

OCT 

90 

90 

90 

02 

02 

OCT 

OCT 

10 OCT 

90 

90 

90 

ND - Not detected 

NA - Not applicable 

Reported By: Mark Brundege Approved By: Toni Lusk 
General Inorganics 

P.33 

CIient Name: 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

American Petrol 

Semivol 

011425-

WASTE 

21 SEP 

Cyanide, Reactive 

Ignitability 

Nonvolatile 

Volatile Oil 

Oil 

Water. 

Solids 

pH 

Oil 

Sulfide, Reactive 

e-Crude 

-0003-SA 

90 

Result 

ND 

64.0 

22.5 

36.0 

58.5 

33.7 

7.8 

8.4 

0.63 

eum Institute 

Tank Bottoms 

Sampled: 20 SEP 

Prepared: See Bel 

Reporting 

Units Limit 

mg/kg 0.10 

deg. F 

% 0.1 

% 0.9 

% 0.9 

% 0.9 

% 0.1 

units 

mg/kg 0.50 

90 Received 

ow Analyzed 

Analytical 

Method 

EPA/OSW 

1010 

Chevron 

Chevron 

. Chevron 

Chevron 

Chevron 

9045/ASTM 

EPA/OSW 

: 21 

: See 

SEP 

Bel 

Prepared 

Date 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

90 

ow 

Analyzed 

Date 

25 SEP 90 

26 SEP 90 

20 OCT 90 

20 OCT 90 

20 OCT 90 

20 OCT 90 

20 OCT 90 

22 SEP 90 

02 OCT 90 

oz 

Note o : This test is unreliable for any sample other than a 

non-aqueous liquid. 

Note z : Sample exhibits a characteristic of hazardous waste. 

ND - Not detected 

NA * Not applicable 

Reported By: Ron Maiorana* Approved By: John Laferty 
P.34 

Appendix IX Volatile Organics 

Method 8240 

CIient Name: 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

American Petroleum Institute 

Midblock Heater Treater Btm. 

011425-0007-SA 

WASTE Sampled: 

21 SEP 90 Prepared: 

Acetone 

Acetonitrile 

Acrolein 

Acrylonitrile 

Allyl chloride 

Benzene 

Bromodi chloromethane 

Bromoform 

Bromomethane 

Carbon disulfide 

Carbon tetrachloride 

Chlorobenzene 

Chloroprene 

Chloroethane 

Di bromochloromethane 

Chloroform 

Chloromethane 

DBCP (1,2-Dibromo3-chloropropane) 

EDB (1,2-Dibromoethane) 

Dibromomethane 

trans-1,4-Dichloro2-butene 

Di chlorodi f1uoromethane 

1,1-Dichloroethane 

1,2-Dichloroethane 

trans-1,2-Dichloroethene 

1,1-Dichloroethene 

Dichloromethane 

1,2-Dichloropropane 

cis-1,3-Dichloropropene 

trans -1,3-Di chloropropene 

1,4-Dioxane 

Ethyl benzene 

Ethyl cyanide 

2-Hexanone 

Iodomethane 

Isobutyl alcohol 

Methacrylonitrile 

2-Butanone (MEK) ~ 

4-Methyl-2-pentanone 

20 SEP 

25 SEP 

esult 

ND 

ND 

ND 

ND 

ND 

140 

NO 

NO 

ND 

ND 

ND 

ND 

ND • 

ND 

ND 

ND 

NO 

ND 

NO 

ND 

NO 

NO 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

320 

NO 

ND 

ND 

ND 

ND 

ND 

ND 

90 Received: 21 SEP 90 

90 An 

Units 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

alyzed: 27 SEP 90 

Reporting 

Limit 

250 

2500 

2500 

2500 

120 

120 

120 

120 

250 

120 

120 

120 

120 

250 

120 

120 

250 

120 

120 

120 

120 

250 

120 

120 

120 

120 

120 

120 

120 

120 

2500 

120 

120 

250 

120 

2500 

120 

250 

250 

(continued on following page) 

Reported By: Michael Blades Approved By: Jeff Lowry 

ND - Not detected6' 

NA * Not applicable 
P.35 

CIient Name: 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

Appendix IX Volatile Organics (CONT.) 

Method 8240 

American Petroleum Institute 

Midblock Heater Treater Btm. 

011425-0007-SA 

WASTE Sampled: 

21 SEP 90 Prepared: 

Styrene 

1,1,1,2-Tetrachloroethane 

1,1,2,2-Tetraehloroethane 

Tetraehloroethene 

Toluene 

1,1,1-Trichloroethane 

•1,1,2-Trichloroethane 

Triehloroethene 

Trichlorofluoromethane 

1,2,3-Tri chloropropane 

Vinyl acetate 

Vinyl chloride 

Xylenes (total) 

Surrogate 

Toluene-d8 

4 -Bromof1uorobenzene 

1,2-Di chloroethane-d4 

20 SEP 

25 SEP 

tesult 

ND 

ND 

ND 

ND 

690 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

1000 

Uflrftuov* 

^ctUVci 

103 

98 

97 

90 

90 

w 

y 

Units 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg-

.mg/kg 

% 

% 

% 

Received: 21 SEP 90 

Analyzed: 27 SEP 90 

Reporting 

Limit 

120 

120 

120 

120 

120 

120 

120 

120 

120 

120. 

250 

250 

120 

--

--

ND - Not detected 

NA - Not applicable 

Reported By: Michael Blades Approved By: Jeff Lowry 
P.36 

1 

OTC Volatile Organics 

TCLP Leachate 

Method 8240 

Name: 

ID: 

ized. 

Americar Petroleum Institute 

Miablcck Heater Treater Btm. 

0U42S-0007-SA 

WAjTE Sampled: 

^i :P 9C Prepared: 

-.eter 

1 . • ."I. chloride 

'. Oichloroetnene 

•; • *of orm 

:.'. "nchlcroethane 

'-.-': .anone 

'.V r>n tetrachloride 

••• Vi oroethene 

:»?•• r-n e 

'•-•.•-•.chl oroethene 

'..-.'- ooenzene 

•jv -ogata 

Tr. uene-d8 

•*• r.-omof 1 uorobenzene 

1.I-Oichloroethane-d4 

20 SEP 

29 SEP 

esult 

ND 

ND 

ND 

ND 

ND 

NO 

ND 

0.94 

ND 

ND 

102 

96 

98 

9C 

90 

y 

Units 

mg/L 

mg/L 

mg/L 

mq/L 

mq/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

% 

% 

% 

Re 

An 

:eived: 2i SEP 90 

alyzed: 05 OCT 90 

Reporting 

Limit 

0.50 

0.25 

0.25 

0.25 

0.50 

0.25 

0.25 

0.25 

0.25 

0.25 

--

--

ND * Not detected 

NA - Not applicable 

Reported By: Deneen Miller Approved By: Jeff Lowry 

1 
P.37 

Metals 

TCLP Leachate 

Client Name: American Petroleum Institute 

Client ID: Midblock heater treater bottoms 

Lab ID 

Matrix 

011425-0007-SA 

WASTE Sampled: 20 SEP 90 Received: 21 SEP 90 

Authorized: 21 SEP 90 Prepared: See Below Analyzed: See Below 

Reporting Analytical Prepared Analyzed 

Parameter Result Units Limit Method Date Date 

Arsenic ND mg/L 1.0 6010 28 SEP 90 09 OCT 90 

Barium 1.6 mg/L 0.10 6010 28 SEP 90 09 OCT 90 

Cadmium ND mg/L 0.050 6010 28 SEP 90 09 OCT 90 

Chromium 0.14 mg/L 0.10 6010 28 SEP 90 09 OCT 90 

Lead 9.6 mg/L 0.50 6010 28 SEP 90 09 OCT 90 

Silver ND mg/L 0.10 6010 28 SEP 90 09 OCT 90 

Mercury ND mg/L 0.0020 7470 05 OCT 90 10 OCT 90 

Selenium ND mg/L 0.050 7740 28 SEP 90 01 OCT 90 

ND = Not detected 

j NA • Not applicable 

Reported By: Mark Brundege Approved By: Toni Lusk 
General Inorganics 

P.38 

Client Name: American Petrol 

Client ID: Midblock Heater 

Lab ID: 011425 

Matrix: WASTE 

Authorized: 21 SEP 

Parameter 

Cyanide, Reactive 

Ignitability 

Non-Volatile Oil 

Volatile Oil 

Oil 

Water 

Solids 

pH . 

Sulfide, Reactive 

-0007-SA 

90 

Result 

ND 

77.0 

58.2 

13.5 

71.7 

14.4 

13.9 

8.9 

ND 

eum Institute 

Treater Btm. 

Sampled: 

Prepared: 

20 SEP 

See Bel 

Reporting 

Units 

mg/kg 

deg. F 

% 

% 

% 

% 

% 

units 

mg/kg 

Limit 

0.10 

--

0.1 

0.5 

0.5 

0.5 

0.1 

--

0.50 

90 Received 

ow Analyzed 

Analytical 

Method 

EPA/OSW 

1010 

Chevron 

Chevron 

Chevron 

Chevron 

Chevron 

9045/ASTM 

EPA/OSW 

: 21 

: See 

SEP 

Bel 

Prepared 

Date 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

90 

ow 

Analyzed 

Date 

25 SEP 90 

27 SEP 90 oz 

20 OCT 90 

20 OCT 90 

20 OCT 90 

20 OCT 90 

20 OCT 90 

22 SEP 90 

02 OCT 90 

Note o : This test is unreliable for any sample other than a 

non-aqueous liquid. 

Note z : Sample exhibits a characteristic of hazardous waste. 

ND - Not detected 

NA - Not applicable 

Reported By: Ron Maiorana Approved By: John Laferty 

1 
P.39 

ANALYTICAL RESULTS 

FOR 

AMERICAN PETROLEUM INSTITUTE 

ENSECO-RMAL NO. 011686 

NOVEMBER 21, 1990 

Reviewed by: •zrrfL'OA.^ Li/l/t/kZ 

/ 

.STSusan «C. wyatt 

a 

i 

Rocky Mountain 

Analytical Laboratory 

Enseco 

Enseco Incorporated 

4 W Yarrow Street 

Arvada. Colorado 80002 

303/421-OOI1 Fax: 503/431-7171 
P.40 

Appendix IX Volatile Organics 

Method 8240 

CIient Name: 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

American Petroleum Institute 

Chickasha-Crude Tank Bottoms 

011686-0001-SA 

WASTE Sampled: 

05 OCT 90 Prepared: 

Acetone 

Acetonitrile 

Acrolein 

Acrylonitrile 

Allyl chloride 

Benzene 

Bromodichloromethane 

Bromoform 

Bromomethane 

Carbon disulfide 

Carbon tetrachloride 

Chlorobenzene 

Chloroprene 

Chloroethane 

Dibromochloromethane 

Chloroform 

Chloromethane 

DBCP (1,2-Dibromo3-chloropropane) 

EDB (1,2-Dibromoethane) 

Dibromomethane 

trans-1,4-Dichloro2-butene 

Di chlorodi fluoromethane 

1,1-Dichloroethane 

1,2-Dichloroethane 

trans-1,2-Dichloroethene 

1,1-Dichloroethene 

Dichloromethane 

1,2-Oichloropropane 

cis-1,3-Dichloropropene 

trans-1,3-Dichloropropene 

1,4-Dioxane 

Ethyl benzene 

Ethyl cyanide 

2-Hexanone 

Iodomethane 

Isobutyl alcohol 

Methacrylonitrile 

2-Butanone (MEK) 

4-Methyl-2-pentanone 

0" OCT 

lu JCT 

iesult 

ND 

NO 

NO 

ND 

NO 

720 

ND 

ND 

ND 

NO 

NO 

ND 

ND 

ND 

ND 

ND 

NO 

NO 

NO 

NO 

ND 

NO 

NO 

ND 

NO 

ND 

ND 

ND 

ND 

ND 

ND 

620 

ND 

ND 

ND 

NO 

ND 

ND 

ND 

90 Received: 05 OCT 90 

90 An 

Units 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

alyzed: 15 OCT 90 

Reporting 

Limit 

330 

3300 

3300 

3300 

160 

160 

160 

160 

330. 

160 

160 

160 

160 

330 

160 

160 

330 

160 

160 

160 

160 

330 

160 

160 

160 

160 

160 

160 

160 

160 

3300 

160 

160 

330 

160 

3300 

160 

330 

330 

(continued on following page) 

Reported By: Terry Riddle Approved By: Jeff Lowry 

ND - Not detected 

NA « Not applicable 
P.41 

CIient Name: 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

Appendix IX Volatile Organics (CONT.) 

Method 8240 

American Petroleum Institute 

Chickasha-Crude Tank Bottoms 

011686-0001-SA 

WASTE Sampled: 

05 OCT 90 Prepared: 

Styrene 

1,1,1,2-Tetrachloroethane 

1,1,2,2-Tetrachloroethane 

Tetraehloroethene 

Toluene 

1,1,1-Tri chloroethane 

1,1,2-Trichloroethane 

Triehloroethene 

Tri chlorofluoromethane 

1,2,3-Trichloropropane 

Vinyl acetate 

Vinyl chloride 

Xylenes (total) 

Surrogate 

Toluene-d8 

4-Bromof1uorobenzene 

1,2-Dichloroethane-d4 

03 OCT 90 

12 OCT 90 

Result 

ND 

ND 

ND 

ND 

2900 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

310 

Recovery 

104 

97 

104 

Units 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

% 

% 

% 

Received: 05 OCT 90 

Analyzed: 15 OCT 90 

Reporting 

Limit 

160 

160 

160 

160 

160 

160 

160 

160 

160 

160 

330 

330 

160 

._ 

--

--

ND - Not detected 

NA - Not applicable 

Reported By: Terry Riddle Approved By: Jeff Lowry 
P.42 

Client Name: 

Client ID: 

Lab ID: 

Matrix: 

Parameter 

011686-0001-SA 

WASTE 

1,1,1-Tri chloroethane 

Isobutyl alcohol 

Vinyl chloride 

Acrylonitrile 

Methylene chloride 

Carbon disulfide 

1,1-Dichloroethene 

Chloroform . 

1,2-Dichloroethane 

2-Butanone 

Carbon tetrachloride 

Triehloroethene 

Benzene 

1,1,2,2-Tetrachloroethane 

Tetraehloroethene 

Chlorobenzene 

1,1,2-Trichloroethane 

1,1,1,2-Tetrachloroethane 

Toluene 

Surrogate 

Toluene-d8 

4-Bromof1uorobenzene 

1,2-Dichloroethane-d4 

OTC Volatile Organics 

TCLP Leachate 

Method 8240 

urn Institute 

Tank Bottoms 

Sampled: 03 OCT 

Received: 05 OCT 

Authorized: 05 OCT 

Result 

ND 

ND 

ND 

ND 

ND 

NO 

ND 

ND 

ND 

NO 

NO 

NO 

3.7 

NO 

ND 

NO 

ND 

ND 

5.2 

Recovery 

98 

100 

92 

90 

90 

90 

Units 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

% 

% 

% 

Leached: 18 

Prepared: 18 

Analyzed: 23 

Reporting 

Limit 

1.2 

50 

2.5 

25 

1.2 

1.2 

1.2 

1.2 

1.2 

2.5 

1.2 

1.2 

1.2 

1.2 

1.2 

1.2 

1.2 

- 1.2 

1.2 

.. 

--

--

OCT 90 

OCT 90 

OCT 90 

ND * Not detected 

NA - Not applicable 

Reported By: Bryan Anderson Approved By: Jeff Lowry 
P.43 

Metals 

TCLP Leachate 

Client Name: American Petroleum Institute 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

Arsenic 

Barium 

Cadmium 

Chromium 

Lead 

Silver 

Mercury 

Selenium 

Ch icka: 

011686-

WASTE 

05 OCT 

»ha-Crude 

-0001-SA 

90 

Result 

ND 

5.7 

ND 

ND 

ND 

ND 

ND 

ND 

Tank Bottoms 

Sampled: 

Prepared: 

03 OCT < 

See Belt 

Reporting 

Units 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

Limit 

1.0 

0.51 

0.050 

0.10 

0.50 

0.10 

0.0020 

0.050 

30 

3W 

Analyt 

Rect 

Ana' 

ical 

Method 

6010 

6010 

6010 

6010 

6010 

6010 

7470 

7740 

;ived 

Iyzed 

: 05 OCT 90 

: See Below 

Prepared Analyzed 

Date Date 

18 OCT 90 21 OCT 90 

18 OCT 90 21 OCT 90 

18 OCT 90 21 OCT 90 

18 OCT 90 21 OCT 90 

18 OCT 90 21 OCT 90 

18 OCT 90 21 OCT 90 

24 OCT 90 25 OCT 90 

18 OCT 90 07 NOV 90 

ND = Not detected 

NA - Not applicable 

Reported By: Thomas Case Approved By: Roxanne Sullivan 
General Inorganics 

P.44 

Client Name: American Petroleum Institute 

Client ID: Chickasha-Crude Tank Bottoms 

Lab ID: 011c86 

Matrix: WAS E 

Authorized: 05 OCT 

Parameter 

Cyanide, Reactive 

Ianitability 

Non-Volatile Oil 

Volatile Oil 

Oil 

Water 

Solids 

PH 

Sulfide, Reactive 

-0001-SA 

Sampled: 

90 Prepared: 

03 OCT 

See Bel 

Reporting 

Result Units 

ND mg/kg 

102 deg. F 

6.2 % 

22.5 % 

28.7 % 

37.7 % 

33.6 % 

6.3 units 

ND mg/kg 

Limit 

0.10 

--

•o.i 

0.5 

0.5 

0.5 

0.1 

--

0.50 

90 Received: 05 

ow Analyzed: See 

OCT 

Bel 

Analytical Prepared 

Method Date 

EPA/OSW NA 

. 1010 NA 

Chevron NA 

Chevron NA 

Chevron NA 

Chevron NA 

Chevron NA 

9045/ASTM NA 

EPA/OSW NA 

90 

ow 

Analyzed 

Date 

23 OCT 90 

18 OCT 90 oz 

23 OCT 90 

23 OCT 90 

23 OCT 90 

23 OCT 90 

23 OCT 90 

27 OCT 90 

23 OCT 90 

Note o : This test is unreliable for any sample other than a 

non-aqueous liquid. 

Note z : Sample exhibits a characteristic of hazardous waste. 

ND = Not detected 

NA - Not applicable 

Reported By: Eileen Burke Approved By: Toni Stovall 

1 
ANALYTICAL RESULTS 

FOR 

AMERICAN PETROLEUM INSTITUTE 

ENSECO-RMAL NO. 011772 

NOVEMBER 27, 1990 

Reviewed by: ^.LOdM LW6\&\ 

Susan C^Wyatt 

P.45 

i -

Rocky Mountain 

Analytical Laboratory 

Enseco 

Enseco Incorporated 

4955 Yarrow Street 

Arvada. Colorado 30002 

303/421-o6ll Fax: 303/431-7171 
f Appendix IX Volatile Organics 

1 Method 8240 

' Client Name: American Petroleum Institute 

Client ID: O.W. WARD CRUDE TANK BOTTOMS 

Lab ID: 011772-0001-SA 

Matrix: WASTE Sampled: 09 OCT 90 Received: 11 OCT 90 

: Authorized: 11 OCT 90 Prepared: 12 OCT 90 Analyzed: 19 OCT 90 

Reporting 

, Parameter Result Units Limit 

J Acetone ND 

Acetonitrile ND 

i Acrolein ND 

J Acrylonitrile ND 

Allyl chloride ND 

Benzene 1200 

] Bromodichl oromethane ND 

! Bromoform ND 

Bromomethane ND 

, Carbon disulfide ND 

Carbon tetrachloride ND 

Chlorobenzene ND 

Chloroprene ND 

Chloroethane ND 

Dibromochloromethane ND 

Chloroform ND 

Chloromethane ND 

DBCP (1,2-Dibromo3-chloropropane) ND 

EDB (1,2-Dibromoethane) NO 

Dibromomethane NO 

trans-1,4-Dichloro2-butene ND 

Dichlorodifluoromethane ND 

1,1-01chloroethane ND 

1,2-Dichloroethane ND 

trans-1,2-Dichloroethene ND 

1,1-Dichloroethene ND 

Dichloromethane ND 

1,2-Dichloropropane NO 

cis-1,3-Oichloropropene ND 

trans-1,3-Dichloropropene ND 

1,4-Dioxane ND 

Ethyl benzene 350 

Ethyl cyanide . ND 

, 2-Hexanone ND 

Iodomethane ND 

J Isobutyl alcohol ND 

Methacrylonitrile ND 

2-Butanrne (MEK) ND 1 4-Methyl-2-pentanone ND 

] 

] 

] 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

100 

1000 

1000 

1000 

50 

50 

50 

50 

100 

50 

50 

50 

50 

100 

50 

50 

100 

50 

50 

50 

50 

100 

50 

50 

50 

50 

50 

50 

50 

50 

1000 

50 

50 

100 

50 

1000 

50 

100 

100 

(continued on following page) 

ND - Not detected 

NA • Not applicable 

Reported By: Michael Blades Approved By: Jeff Lowry 
P.47 

Client Name: 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

Appendix IX Volatile Organics (CONT.) 

Method 8240 

American Petroleum Institute 

O.W. WARD CRUDE TANK BOTTOMS 

011772-0001-SA 

WASTE Sampled: 

11 OCT 90 Prepared: 

Styrene 

1,1,1,2-Tetraehloroethane 

1,1,2,2-Tetrachloroethane 

Tetraehloroethene 

Toluene 

1,1,1-Trichloroethane 

1,1,2-Trichloroethane 

Triehloroethene 

Tri chl orofluoromethane 

1,2,3-Trichloropropane 

Vinyl acetate 

Vinyl chloride 

Xylenes (total) 

Surrogate 

Toluene-d8 

4-Bromof1uorobenzene 

l,2-0ichloroethane-d4 

09 OCT 90 

12 OCT 90 

Result 

ND 

ND 

ND 

ND 

1500 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

1600 

Recovery 

105 

97 

93 

Units 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

mg/kg 

% 

% 

% 

Received: 11 OCT 90 

Analyzed: 19 OCT 90 

Reporting 

Limit 

50 

50 

50 

50 

50 

50 

50 

50 

50 

50 

100 

100 

50 

--

--

ND » Not detected 

NA * Not applicable 

Reported By: Michael Blades Approved By: Jeff Lowry 
P.48 

Client Name: 

Client ID: 

Lab ID: 

Matrix: 

OTC Volatile Organics 

TCLP Leachate 

Method 8240 

American Petroleum Institute 

O.W. WARD CRUDE TANK BOTTOMS 

011772-0001-SA Sampled: 09 OCT 90 

WASTE "' Received: 11 OCT 90 

Authorized: 11 OCT 90 

Leached: 21 OCT 90 

Prepared: 23 OCT 90 

Analyzed: 25 OCT 90 

Parameter 

1,1,1 -Tri eh1 -"-oethane 

Isdbutyl a .al 

Vinyl chlor .a 

Acrylonitriie 

Methylene chloride 

Carbon disulfide 

1,1-Dichloroethene 

Chloroform 

1,2-Dichloroethane 

2-Butanone 

Carbon tetrachloride 

Triehloroethene 

Benzene 

1,1,2,2-Tetrachloroethane 

Tetraehloroethene 

Chlorobenzene 

1,1,2-Trichloroethane 

1,1,1,2-Tetrachloroethane 

Toluene 

Surrogate 

Toluene-d8 

4-Bromofluorobenzene 

l,2-Dichloroethane-d4 

esult 

ND 

NO 

NO 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

ND 

420 

ND 

ND 

ND 

ND 

NO 

560 

eCOVerjr 

107 

100 

104 

Units 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

% ' 

% 

% 

Reporting 

Limit 

150 

6100 

310 

3100 

150 

150 

150 

150 

150 

310 

150 

150 

150 

150 

150 

150 

150 

150 

150 

--

--

1 

ND - Not detected 

NA * Not applicable 

Reported By: Michael Blades Approved By: Jeff Lowry 

1 
P.49 

Metals 

Client Name: 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

TCLP Leachate 

American Petroleum Institute 

O.W. WARD CRUDE TANK BOTTOMS 

011772-0001-SA , j nn nry. . 

WASTE Sampled: 09 OCT 90 

11 OCT 90 

Result 

Prepared: See Below 

Received: 11 OCT 90 

Analyzed: See Below 

Units 

Reporting Analytical 

Limit Method 

Prepared Analyzed 

Date Date 

Arsenic 

Barium 

Cadmium 

Chromium 

Lead 

Silver 

Mercury 

Selenium 

ND 

45.6 

0.28 

0.41 

ND 

ND 

0.033 

ND 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

mg/L 

1. 

0. 

0. 

0, 

0, 

0, 

0, 

0 

,5 

.60 

.072 

.15 

.72 

.15 

.013 

.098 

6010 

6010 

6010 

6010 

6010 

6010 

7470 

7740 

NA 

NA 

NA 

NA 

NA 

NA 

16 NOV 90 

16 NOV 90 

16 NOV 90 

16 NOV 90 

16 NOV 90 

16 NOV 90 

24 OCT 90 16 NOV 90 

NA 16 NOV 90 

ND * Not detected 

NA - Not applicable 

Reported By: Fred Velasquez Approved By: John Laferty 
General Inorganics 

P.50 

Client Name: 

Client ID: 

Lab ID: 

Matrix: 

Authorized: 

Parameter 

American Petroleum Institute 

O.W. WARD CRUDE TANK BOTTOMS 

011772-0001-SA 

WASTE Sampled: 

11 OCT 90 Prepared: 

Cyanide, Reactive 

Ignitability 

Non-Volatile Oil 

Volatile Oil 

Oil 

Water 

Solids 

PH 

Sulfide, Reactive 

Result 

ND 

66 

2.5 

18.0 

20.5 

73.7 

5.8 

6.4 

5.5 

09 OCT 90 

See Below 

Received: 

Analyzed: 

Units 

mg/kg 

deg. F 

% 

% 

% 

% 

% 

units 

mg/kg 

Reporting 

Limit 

0.10' 

0.1 

0.9 

0.9 

0.9 

0.1 

0.50 

Analytical 

Method 

EPA/OSW' 

1010 

Chevron 

Chevron 

Chevron 

Chevron 

Chevron 

9045/ASTM 

EPA/OSW 

-.1 OCT 90 

See Below 

Prepared 

Date 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

Analyzed 

Date 

06 NOV 90 

29 OCT 90 oz 

06 NOV 90 

06 NOV 90 

06 NOV 90 

06 NOV 90 

06 NOV 90 

12 NOV 90 

02 NOV 90 

1 

] 

Note o : This test is unreliable for any sample other than a 

non-aqueous liquid. 

Note z : Sample exhibits a characteristic of hazardous waste. 

ND - Not detected 

NA - Not applicable 

Reported By: Mike Settell Approved By: John Laferty 
P.51