P. 1

Appendi xI

XVolatil e Organic s

Metho d824 0

CIien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r America nPetroleum Institut e STOC KTANKBOTTOM S 007531-0002-S A

Ensec o ID : WAS~ E Sampled : 1 7 NO V 8 9 Prepared :

Aceton e Acetonitril e Acrolei n Acrylonitril e Ally l chlorid e Benzen e Bromo di chloromethan e Bromoform Bromomethan e Carbo ndisulfide

. Carbo ntetrachlorid e Chlorobenzen e Chloropren e Chloroethan e Chlorod i bromomethan e Chlorofor m Chloromethan e DBC P (1,2-Dibromo

3-chlorop-opane ) EDB (1,2-Dibr^.iioethane ) Dibromomethan e trans-1,4-Dichloro

2-buten e Dichlorod i fluoromethan e 1,1-Dichloroethan e 1,2-Dichloroethan e trans-1,2-Dichloroethen e 1,1-Dichloroethen e Dichloromethan e 1,2-Dichloropropan e cis-1,3-Dich1oropropen e trans-1,3-Dichloropropen e 1,4-Dioxan e Ethy l benzen e Ethy l cyanid e 2-Hexanon e Iodomethan e Isobuty l alcoho l Methacrylonitril e Methy l ethy l keton e 4-Methyl-2-pentanon e 106034 9 IF NO V 8 9 2 0 NO V 8 9

esul t



### N D N D N D N D N D N D N D N D N D N D N D N D N D N D N D N D N D

N D N D N D

N D N D N D N D N D N D N D N O N D N D N D N D N D N D N D N D N D N D N D Re

c -.eived : 1 7 NO

V Analyzed : 2 8 NO

V

Unit s
mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/kg mg/kg mg/kg mg/kg < mg/k g mg/k g mg/k g
mg/k g mg/kg mg/k g
mg/k g mg/k g mg/k g mg/k g mg/k g mg/kg mg/k g mg/k g mg/k g mg/kg mg/k g mg/k g mg/k g mg/kg mg/k g mg/kg mg/k g mg/kg mg/k g Reportin g

Limi t

100 0 1000 0 1000 0 1000 0 

### 50 0 50 0 50 0 50 0 100 0 

### 50 0 50 0 50 0 50 0 100 0 

### 50 0 50 0 100 0


### 50 0 50 0 50 0
50 0 100 0 

### 50 0 50 0 50 0 50 0 50 0 50 0 50 0 50 0 1000 0 

### 50 0 50 0 100 0 

### 50 0 1000 0 

### 50 0 100 0 100 0 

### 8 9

89

(continue do

nfollowin g page )

Reporte dBy : Terr y

Riddl e Approve dBy : Jef f Lowr y ND= No t detecte d N A « No t applicabl eP. 2

Rock y Mountai n Ensec 0[ ncorpora[e d Analytica l Laborator

y



### ANALYTICA L RESULT S

FO R

AMERICANPETROLEUMINSTITUT E

ENSECO-RMA L NO
. 00753 1

FEBRUAR Y 6 , 199 0

Reviewe d by : ^k-LSCO^(
, lAUSTi

- . Susa

nC

. Wyat t 

# Enseco

/


### Mauree nA . McDevit t

•4955 Yarro w Street Arvada

. Colorad o 8000 2 303/421-661 1
Facsimile : 303/431-717 1P. 3

Genera l Inorganic s

Clien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r America nPetroleu m Institut e Sit e # 2 Bottom

Solid s 007314-00 1 WAST E 0 1 NO V 8 9

Chlorid e Cyanide , Reactiv e Ignitabilit y Non-Volatil e Oi l Volatil e Oi l Oi l Wate r Solid s pH Sulfide , Reactiv e S A Ensec o ID :

Resul t

850 0 

### N D 8 2 19. 6 

### 0. 5 20. 1 20. 8 57. 6 

### 8. 6 N D Sampled : Prepared :

Unit s mg/k g mg/k g deg
. F % % % % % unit s mg/k g 105866 4 3 1 OC T 8 9 Se e Below Reportin g Limi t 

### 1 5 0. 1

- - 

### 0. 1 0. 1 0. 1 0. 1 0. 1

- - 

### 0. 5 Received :

Analyzed : Analytica l Metho d

300. 0 Mod
. EPA/OS W 1010/102 0 Chevro n Chevro n Chevro n Chevro n. Chevro n 9045/AST M EPA/OS W 

### 0

1 Se e NO V Be l 8 9 o w
Prepare d Dat e 

### 2 8 N A N A N A N A N A N A N A N A N A NO V 8 9 Analyze d Dat e
2 8 NO V 89
. 0 9 NO V 8 9 1 0 NO V 8 9 o i 1 7 NO V 8 9 1 7 NO V 8 9 1 7 NO " 8 9 1 7 r 3 9 1 7 3 9 0 8 8 9 2 2 rtu V 8 9

Not e o : Thi s tes t i s unreliabl e fo r an y sampl e othe r tha na -on-aqueou s liquid

.
Not e z : Sampl e exhibit s a characteristi c o f hazardou s waste .
ND- No t detecte d N A - No t applicabl e
Reporte dBy : Jennife r Franze n Approve dBy : Harol dBorque zP. 4

Clien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r
Osmiu m(189 ) ICP/M S Metal s

Tota l Metal s
America n Petroleu m

Institut e Sit e # 2 Botto m

Solid s 007314-0004-S AEnsec o ID : 105866 4 WAST E Sampled : 3 1 OC T 8 9 0 1 NOV 8 9 Prepared : Se e Belo w Received : 0 1 NOV 8 9 Analyzed : Se e Belo w

Resul t

ND Reportin g Analytica l

Unit s Limi t Metho d Prepare d Dat e Analyze d

Dat e mg/k g 

### 2 RMA L 0 7 NOV 8 9 0 8 NO

V 8 9

ND - No t detecte d N A= No t applicabl e
Reporte dBy : Scot t Heidema n Approve dBy : Ton i Tallaric oP. 5

Metal s

TCL P Leachat e
Clien t Name : America n PetroleumInstitut e Clien t ID : Sit e # 2 Botto mSolid s La bID : 007314-0004-S AEnsec o ID : 105866 4 Matrix : WAST E Sampled : 3 1 OC T 8 9 Received : 0 1 NOV 8 9 Authorized : 0 1 NOV

8 9 Prepare i : Se e Belo wAnalyzed : Se e Belo w Repo r qAnalytica l Prepare d Analyze d Paramete r Resul t Unit s Limi t ' Metho d Dat e Dat e
Arseni c ND mg/ L 0. 5 200. 7 0 8 NO V 8 9 1 3 DE C 8 9 Barium3. 7 mg/ L 0. 3 200. 7 0 8 NOV 8 9 1 3 DE C 8 9 Cadmiu mN D mg/ L 0.0 3 200. 7 0 8 NOV 8 9 1 3 DE C 8 9 Chromiu mND mg/ L 0.0 5 200. 7 0 8 NOV 8 9 1 3 DE C 8 9 

### N D 

### 3. 7 N D N D N D N D N D N D mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L Lea d ND mg/ L 0. 3 200. 7 0 8 NOV 8 9 1 3 DE C 8 9 Silve r ND mg/ L 0.0 5 200. 7 0 8 NOV 8 9 1 3 DE C 89

- Mercur yND mg/ L 0.00 2 747 1 1 0 NOV 8 9 1 3 NO

V 8 9 Seleniu mND mg/ L 0.0 5 270. 2 0 8 NOV 8 9 1 3 NO

V 8 9

ND - No t detecte d N A« No t applicabl e
Reporte d By : Fre dVelasque z Approve dBy : Kimberl y Conro yP. 6

.

•

Clien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r

Aluminum Antimon y Arseni c Bariu m Bery l 1 i ur

n Cadmium Calcium Chromium Cobal t Coppe r
i

__J Lea d Mercur y • Nicke l Potassium Selenium Silve r Sodium Thallium

T 2

_ 

### Ti n Vanadium

— * Zin c America nPetroleum

Sit e # 2 Bottom

So l 007314

- WAST E 0 1 NO V

ND= No t detecte d N A - No t app l

Reporte dBy : 

## 1 i

! 

# 1 icabl e

Davi d •0004-S A



### 89

Resul t

118 0 

### N D 3 540 0 

### N D N O 442 0 

### 35 N D 28 5 4 1. 4 7 N D N D N D 610 0 

### N D N D 2 40 0

Patterso n Metal s

Tota l Metal s

Institut e 

### id s •nsec o ID : Sampled : Prepared :

Unit s
mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

/ 105866 4

3 1 OC T 8 9 Se e Below
Reportin g Limi t


### 1 0 5 1 1 0. 2 0. 5 20 1 1 1 5 0. 3 4 50 0 0. 5 1 50 0 0. 5 5 1 1 Received :

Analyzed : Analytica l Metho d

601 0 601 0 706 0 601 0 601 0 601 0 601 0 601 0 601 0 601 0 601 0 747 1 601 0 601 0 774 0 601 0 601 0 784 1 601 0 601 0 601 0 

### 0

1 NO V Se e Be l 

### 89 o w

Prepare d Dat e 

### 0 7 0 7 0 7 0 7 0 7 0 7 0 7 0 7 0 7 0 7 0 7 1 7 0 7 0 7 0 7 0 7 0 7 0 7 0 7 0 7 0 7

Approve dBy : Kimberl y Conro y 

### DE

C DE C DE C DE C DE C DE C DE C DE C DE C DE C DE C NO V DE C DE C DE C DE C DE C DE C DE C DE C DE C 89 89 89 89 89 89 89 89 89 89 8 9 89 89 89 89 89 8 9 8 9 89 8 9 89 t

Analyze d Dat e

0 7 DE C 0 7 DE C 1 2 DE C 0 7 DE C 0 7 DE C 0 7 DE C 0 7 DE C 0 7 DE C 0 7 DE C 0 7 DE C 0 7 DE C 1 7 NO V 0 7 DE C 0 7 DE C 1 2 DE C 0 7 DE C 0 7 DE C 1 1 DE C 0 7 DE C 0 7 DE C 0 7 DE C 

### 89 89 89 89 89 89 89 89 •8 9 89 89 89 89 89 89 89 89 89 89 89 89P. 7

OT C Sem i volatil e Organic s TCL P Leachat e Metho d 827 0

Clien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r America n Petroleum Institut e Sit e # 2 Botto mSolid s 007314-0004-S AEnsec o ID : WAST E Sampled : 0 1 NO V 8 9 Prepared :

Pyridin e Pheno l bis(2-Chloroethyl ) ethe r 1,4-Dichlorobenzen e 1,2-Dichlorobenzen e o-Creso l
m& p-Cresol(s ) Hexachloroethan e Nitrobenzen e Hexachlorobutadien e 2,4,6-Trichloropheno l 2,4,5-Trichloropheno l 2,4-Dinitrotoluen e Hexachlorobenzen e 2,3,4,6-Tetrachloropheno l Pentachloropheno l

Nitrobenzene-d 5 2-Fluorobipheny l Terphenyl-dl 4 Phenol-d 5 2-Fluoropheno l 2,4,6-Tr i bromopheno l 105866 4 3 1 OC T 8 9 0 9 NO V 8 9

esul t


### N D N D N D N D N D N D N D N D N D N D N D N D N D N D N D N D
N D N O N D N D N D N D Unit s mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L

% % % % % % Received : 0 1 NOV 8 9 Analyzed : 2 7 NOV

8 9 Reportin g Limi t

- - • 0.4 0 0.4 0 0.4 0 0.4 0 0.4 0 0.4 0 0.4 0 0.4 0 0.4 0 0.4 0 

### 2. 0 0.4 0 0.4 0 0.4 0 

### 2. 0

- -

- -

- -

- -

- -

ND - No t detecte d N A - No t applicabl e
Reporte dBy : Philli p Tallaric o Approve dBy : Jef f LowryP. 8

Clien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r Refiner y Hazardou s Constituen t Semivolatile s

Metho d827 0

America nPetroleu

m Institut e Sit e # 2 Botto

m Solid s 007314-0004-S A

Ensec o ID : WAST E Sampled : 0 1 NO V 8 9 Prepared :

Anthracen e Benzo(a)anthracen e Benzo(b)f1uoranthen e Benzo(k)f1uoranthen e Benzo(a)pyren e bis(2-Ethylhexyl ) phthalat e Buty l benzy l phthalat e Chrysen e Di benz(a,h)anthracen e Di-n-buty l phthalat e 1,2-D i ch1orobenzen e 1,3-D i chlorobenzen e 1,4-Dichlorobenzen e Diethy l phthalat e 7,12-Dimethylbenz

anthracen e Dimethy l phthalat e Di-n-octy l phthalat e FIuoranthen e Inden e 1-Methylnaphthalen e Naphthalen e Phenanthren e Pyren e Pyridin e Quinolin e Benzenethio l o-Creso l
m & p-Cresol(s ) 2,4-Dimethylpheno l 2,4-Dinitropneno l 4-Nitropheno l Pheno l

Nitrobenzene-d 5 2-Fluorobipheny l Terphenyl-dl 4 Phenol-d 5 2-Fluoropheno l 2,4,6-Tribromopheno l

N D- No t detecte d N A - No t applicabl e 105866 4 3 1 OC T 8 9 0 6 NO V 8 9

esul t


### N D N D N D N D N D
N D N D N D N D N D N D N D N D N D
N D N D N D N D N D 24 0 270 N D N D N D N D N D N D N D N D N D N D N D

49. 3 67. 5 70. 8 38. 2 48. 0 62. 0 Received : 0 1 NO V 8 9 

### A n

Unit s mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/kg
. mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

% % % % % % alyzed : 1 6 NO V 8 9
Reportin g Limi t 

### 3 7 37 3 7 3 7 37 37 37 3 7 3 7 3 7 37 37 3 7 37 37 37 3 7 37 37 37 37 3 7 37

- - 

### 37

- - 

### 37 37 3 7 18 0 18 0 37

- -

- -

- -

- -

- -

- -

Reporte dBy : Belind a Guerr a Approve dBy : Jef f Lowr yOT C Volatil e Organic s TCL P Leachat e Metho d824 0 P. 9

Clien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r America nPetroleu m Institut e Sit e # 2 Botto

m Solid s 007314-0004-S A

Ensec o ID : 105866 4 WAST E Sampled : 3 1 OC T 8 9 0 1 NO V 8 9 Prepared : 1 0 NO V 8 9

Viny l chlorid e Acrylonitril e Methylen e chlorid e Carbo ndisulfid e 1,1-Dichloroethen e Isobuty l alcoho l Chloroform 1,2-Dichloroethan e 2-Butanon e 1,1,1-Tr i chloroethan e Carbo ntetrachlorid e Trichloroethen e 1,1,2-Trichloroethan e Benzen e 1,1,1,2-Tetrachloroethan e 1,1,2,2-Tetrachloroethan e Tetrachloroethen e Toluen e Chlorobenzen e Toluene-d 8 4-Brombfluorobenzen e 1,2-Dichloroethane-d 4 Resul t

ND ND ND ND N D ND ND ND ND ND ND ND ND 5. 2 ND ND ND 4. 8 ND

10 1 10 0 10 5 Unit s

mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L

% % % Received : 0 1 NO V Analyzed : 1 3 NO

V Reportin g Limi t

0.5 0 5. 0 0.2 5 0.2 5 0.2 5 5. 0 0.2 5 0.2 5 0.5 0 0.2 5 0.2 5 0.2 5 0.2 5 0.2 5 0.2 5 0.2 5 0.2 5 0.2 5 0.2 5 8 9

8 9

ND- No t detecte d N A * No t applicabl e
Reporte dBy : Dian e Pag e Approve dBy : Jef f Lowr yP.1 0

c

J Appendi xI X Volatil e Organic s (CONT. )

Metho d 824 0

Clien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r America n PetroleumInstitut e

Sit e # 2 Botto m

Solid s 007314-0004-S AEnsec o ID : 105866 4 WAST E Sampled : 3 1 OC T 8 9 0 1 NOV 8 9 Prepared : 0 3 NOV 8 9 Received :

Analyzed : 0 1

0 7 NO V NOV 8 9 8 9

Resul t Unit s
Styren e 1,1,1,2-Tetrachloroethan e 1,1,2,2-Tetrachloroethan e Tetrach l oroethen e Toluen e 1,1,1-Trichloroethan e 1,1,2-Trichloroethan e Trichloroethen e Tr i chlorof1uoromethan e 1,2,3-Tr i chloropropan e Viny l acetat e Viny l chlorid e Xylene s (total )

Toluene-d 8 4-Bromofluorobenzen e l,2-Dichloroethane-d 4 

### N D N D N D N D 

### 35 0 N D N D N D N D N D N D N D 

### 46 0
10 9 91. 1 88. 6 mg/k g

mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

% % % Reportin g

Limi t

5 0 5 0 5 0 5 0 5 0 5 0 5 0 5 0 5 0 5 0 10 0 10 0 5 0

ND = » No t detecte d N A« No t applicabl e
Reporte d By : Ti mMille r Approve dBy : Jef f LowryP.1 1

Appendi xI

XVolatil e Organic s

Metho d824 0

Clien t Name : America nPetroleu m Institut e Clien t ID : Sit e # 2 Bottom Solid s La bID : 007314-0004-S A Ensec o ID : 105866 4 Matrix : WAST E Sampled : 3 1 OC T 8 9 Authorized : 0 1 NO

V 8 9 Prepared : 0 3 NO V 8 9

Paramete r Resul t

Aceton e ND Acetonitril e ND Acrolei nND Acrylonitril e ND Ally l chlorid e ND Benzen e 10 0 Bromodichloromethan e ND Bromoform

ND Bromomethan e N D Carbo ndisulfide

- N D Carbo ntetrachlorid e ND Chlorobenzen e ND Chloropren e ND Chloroethan e ND Chlorodibromomethan e ND Chloroform

ND Chloromethan e ND DBC P (1,2-Dibromo

3-chloropropane ) ND ED B (1,2-Dibromoethane ) ND Dibromomethan e ND trans-1,4-Dichloro

2-buten e ND Dichlorodif1uoromethan e ND 1,1-01chloroethan e ND 1,2-Dichloroethan e ND trans-1,2-Dichloroethen e N D 1,1-Dichloroethen e N D Dichloromethan e ND 1,2-Dichloropropan e NO cis-1,3-Dichloropropen e ND trans-1,3-Dichloropropen e NO i,4-Dioxan e ND Ethy l benzen e 9 4 Ethy l cyanid e N D 2-Hexanon e ND Iodomethan e ND Isobuty l alcoho l ND Methacrylonitril e NO Methy l ethy l keton e NO 4-Methyl-2-pentanon e ND Received : 0 1 NO V Analyzed : 0 7 NO

V

Unit s mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mgA g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g Reportin g

Limi t 

### 10 0 100 0 100 0 100 0 

### 5 0 5 0 5 0 5 0 10 0 5 0 5 0 5 0 5 0 10 0 5 0 5 0 10 0
5 0 5 0 5 0
5 0 10 0 5 0 5 0 5 0 5 0 5 0 5 0 5 0 5 0 100 0 

### 5 0 5 0 10 0 5 0 100 0 

### 5 0 10 0 10 0 8 9 8 9

ND* No t detecte d N A - No t applicabl e
Reporte dBy : Ti m

Mille r (continue donfollowin g page )

Approve dBy : Jef f Lowr yP.1 2



### ANALYTICAL RESULT S

FO R

B P AMERICA

INC
.
ENSECO-RMAL NO
. 00731 4

JANUARY5 , 199 0

Reviewe dby : Suda nC
. Wyft t

Par r

Ensec o Incorporated 495 5 Yarro

wStree t• Arvada

. Colorad o 8000 2 303/421-661 1 Fax : 303/431-717 1 Rock y Mountain Analytica l Laborator

y



# Ensec oP.1 3

71 3 > •O V 3 < .OV s -

## 1
J
Genera l Inorganic s P.1 4

Clien t Name ; Clien t ID : La bID : Matrix : Authorized :

Paramete r America n PetroleumInstitut e

Sit e # 3 Crud e Oi l Botto mSt r 006299-0004-S AEnsec o ID : WAST E Sameled : 2 8 AU G 8 9 Prepared :

Chlorid e Cyanide
, Reactiv e Ignitabilit y Non-Volatil e Oi l Volatil e Oi l Oi l Wate r Solid s pH Sulfide
, Reactiv e Resul t Unit s
2510 0 N D 12 7 1 9 0 2 0 2 5 105076 8

2 4 AU G 8 9 Se e Belo w Received :

Analyzed :

54. 8 8. 4 5 0 Reportin g Analytica l

Limi t Metho d
mg/k g mg/k g deg

. F 

## r . % % % % unit s mg/k g 1 5

0. 1

0. 1 0. 1 0. 1 0. 1 0. 1

0. 5 300. 0 Mod

. EPA-OS W 1010/102 0 Chevro n Chevro n Chevro n Chevro n Chevro n 9045/AST M EPA/OS W 2 5 AU G 8 9

Se e Belo w
Prepare d Dat e
0 7 SE P 8 9 N A N A N A N A N A N A N A N A N A Analyze d

Dat e

1 3 SE P 8 9 0 8 SE P 8 9 1 1 0CT8 9 o l i 9 OC T 8 9 1 9 OC T 8 9 1 9 OC T 8 9 1 9 OC T 8 9 1 9 OC T 8 9 1 1 SE P 8 9 0 8 SE P 8 9

Not e o : Thi s tes t i s unreliabl e fo r an ysampl e othe r tha n a non-aqueou s liquid

.
J Not e 1 : Sampl e 4 i s hazardou s du e t o ignitabilit yfo r flashpoint

. 

# 1 1 ] ND - No t detecte d N A - No t applicabl e
Reporte dBy : Blak e Besse r Approve dBy : Tammy.Bai le yP.1 5

Jien t Name : Clien t ID :

' a bID : atrix : Authorized :

'aramete r Appendi xI XVolatil e Organic s (CONT. )

Metho d824 0

America nPetroleu

m Institut e Ramsey-Crud e Tan kBottom s 011425-0001-S A WAST E Sampl < 2 1 SE P 9 0 Prepa n

Styren e 1,1,1,2-Tetrachloroethan e i,1,2,2-Tetrachloroethan e Tetrachloroethen e Toluen e 1,1, 1 -Tr i chloroethan e 1,1,2-Tr i chloroethan e Trich l oroethen e Tr i ch l orof1uoromethan e 1,2,3-Trichloropropan e Viny l acetat e Viny l chlorid e Xylene s (total )
Surrogat e

Toluene-d 8 4-Bromofluorobenzen e 1,2-D i chloroethane-d 4 2 0 SE P 9 0 2 5 SE P 9 0

Resul t



### N D N D N D N D 240 0 

### N D N D N D N D N D N D N D 430 0

Recover y


### 105 9 7 9 9 Unit s

mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

% % % Received : 2 1 SE P 9 0 Analyzed : 2 7 SE P 9 0
Reportin g Limi t


### 250 250 250 250 250 250 250 250 250 250 500 50 0 250

- -

- -

ND» No t detecte d N A - No t applicabl e
Reporte dBy : Michae l Blade s Approve dBy : Jef f LowryP.1 6



### OT C

Clien t Name : America nPetroleu m Clien t ID : Ramsey-Crud e Tan kE LabID : 011425-0001-S A Matrix : WAST E Authorized : 2 1 SE P 9 0

Paramete r Viny l chlorid e 1,1-Dichloroethen e Chloroform 1,2-Dichloroethan e 2-But*npn e Carbon-tetrachlorid e Trichlbroethen e Benzege * Tetrachloroethen e Chlorobenzen e
Surrogat e

Toluene-d 8 4-Bromofluorobenzen e l,2-Dichloroethane-d 4 Volatil e Organic s TCL P Leachat e Metho d824 0
nstitut e ttom s Sampled : 2 0 SE P 9 0 repared : 2 7 SE P 9 0

Resul t


### N D N D N D N D N D N D N D 2 7 N D N O

Recover y 

### 10 3 10 4 10 1 Unit s mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L

% % % Received : 2 1 SE P 9 0 Analyzed : 1 1 OC T 9 0
Reportin g Limi t


### 2 6 1 3 1 3 1 3 2 6 1 3 1 3 1 3 1 3 1 3

- -

- -

N D« No t detecte d N A • No t applicabl e
Reporte dBy : Terr y

Riddl e Approve dBy : Jef f Lowr yP.1 7

Metal s

TCL P Leachat e
Clien t Name : America nPetroleu m Institut e Clien t ID : Ramsey-crud e tan kbottom s LabID : 011425-0001-S A Matrix : WAST E Sampled : 1 8 SE P 9 0 Received:,2 1 SE P 9 0 Authorized : 2 1 SE P 9 0 Prepared : Se e Belo w Analyzed:'Se e Below

Paramete r
Arseni c Bariu m Cadmiu m Chromium Lea d Silve r Mercur y Selenium

. Resul t



### N D 1. 6 0.3 2 

### N D N D N D N D N D Unit s

mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L Reportin g

Limi t 

### 1. 3 0.1 3 0.06 2 0.1 3 0.6 2 0.1 3 0.007 5 0.06 2 Analytica l

Metho d

601 0 601 0 601 0 601 0 601 0 601 0 747 0 774 0



# 1

] Prepare dAnalyze d Dat e Dat e

2 8 SE P 9 0 2 3 OC T 9 0 2 8 SE P 9 0 2 3 OC T 9 0 2 8 SE P 9 0 2 3 OC T 9 0 2 8 SE P 9 0 2 3 OC T 9 0 2 8 SE P 9 0 2 3 OC T 9 0 2 8 SE P 9 0 2 3 OC T 9 0 2 3 OC T 9 0 2 3 OC T 9 0 2 8 SE P 9 0 2 3 OC T 9 0

ND- No t detecte d N A - No t applicabl e
Reporte dBy : Fre dVelasque z Approve dBy : Ton i Lus kP.1 8

Genera l Inorganic s

Clien t Name : Clien t ID : LabID Matrix : Authorized :

Paramete r America nPetroleu m Institut e Ramsey-Crud e Tan kBottom s 011425-0001-S A WAST E Sampled : 2 1 SE P 9 0 Prepared : 2 0 SE P 9 0 Se e Below Received :

Analyzed : Reportin g Analytica l Resul t Unit s Limi t Metho d 2 1 SE P 9 0 Se e Below
Prepare d Dat e Analyze d

Dat e Cyanide , Reactiv e Ignitabilit y Non-Volatil e Oi l Volatil e Oi l Oi l G Wate r Solids

. 

### P H Sulfide , Reactiv e 

### N

D 79. 0 29. 0 63. 0 92. 0 

### 4. 8 3. 2 6. 7 N D mg/k g

deg
. F % % % % % unit s mg/k g 0.1 0



### 0. 1 0. 9 0. 9 0. 9 0. 1

- - 0.5 0 EPA/OS W

101 0 Chevro n Cherro n Cherro n Chevro n Chevro n 9045/AST M EPA/OS W 

### N

A N A N A N A N A N A N A N A N A 2 5 SE P 9 0

2 6 SE P 9 0 o z 2 0 OC T 9 0 2 0 OC T 9 0 2 0 OC T 9 0 2 0 OC T 9 0 2 0 OC T 90
. 2 2 SE P 9 0 0 2 OC T 9 0

Not e o : Thi s tes t i s unreliabl e fo r an y sampl e othe r tha na non-aqueou s liquid

.
Not e z : Sampl e ejc^ibit s a characteristi c o f hazardou s waste .
ND» No t detecte d N A * No t applicabl e
Reporte dBy : Ro nMaioran a Approve dBy : Joh nLafert yP.1 9



### Appendi xIXVolatil e Organic s

Metho d 824 0

Clien t Name : America nPetroleu m Clien t ID : Prairi e Dale-Crud e LabID : 011425-0005-S A Matrix : WAST E Authorized : 2 1 SE P 9 0

Paramete r

Aceton e Acetonitril e Acrolei n Acrylonitril e Ally l chlorid e Benzen e Bromodichloromethan e Bromoform Bromomethan e Carbo ndisulfid e Carbo ntetrachlorid e Chlorobenzen e Chloropren e Chloroethan e Di bromochloromethan e Chloroform Chloromethan e DBC P (1,2-Dibromo

3-chloropropane ) ED B (1,2-Dibromoethane ) Dibromomethan e trans-l,4-0ichloro

2-buten e Dichlorodifluoromethan e 1,1-Dichloroethan e 1,2-Dichloroethan e trans-1,2-D i chloroethen e 1,1-Dichloroethen e Dichloromethan e 1,2-Dichlbropropan e cis-1,3-Dichloropropen e

• trans-1,3-Dichloropropen e 1,4-Dioxan e Ethy l benzen e Ethy l cyanid e 2-Hexanon e j Iodomethan e Isobuty l alcoho l

4 Methacrylonitril e 2-Butanon e (MEK )

- J4-Methyl-2-pentanon e Institut e TankBtm . Sampled : Prepared : 2 0 SE P

2 5 SE P

Resul t


### N D N D N D N D N D N D N D N D N D N D N D N O N O N D N D N O N O

N D N D N D
N O N O N O N D N D N D N D N D N O N D N D 260 N O N D N O N O N D N D N D 9 0 Received : 2 1 SE P 9 0 A

n

Unit s mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g alyzed : 2 7 SE P

Reportin g Limi t 

### 10 0 100 0 100 0 100 0 

### 5 0 5 0 5 0 5 0 10 0 5 0 5 0 5 0 5 0 10 0 5 0 5 0 10 0

5 0 5 0 5 0
5 0 10 0 5 0 5 0
. 

### 5 0 5 0 5 0 5 0 5 0 5 0 100 0 

### 5 0 5 0 10 0 5 0 100 0 

### 5 0 10 0 10 0 9 0 9 0

(continue d o n followin g page ) N D- No t detecte d N A - No t applicabl e Reporte dBy : Michae l Blade s Approve dBy : Jef f LowryP.2 0



### Appendi xI

XVolatil e Organic s (CONT. )
Metho d824 0
Clien t Name : America n Petroleu m Institut e Clien t ID : Prairi e Dale-Crud e Tan k Btm

. 

### La bID : 011425-0005-S A Matrix : WAST E Sampled : 2 0 SE P 9 0 R e . ved : 2 1 S r 

### P 9 0 Authorized : . 2 1 SE P 9 0 Prepared : 2 5 SE P 9 0 An a zed : 2 7 SE P 9 0 Reportin g Paramete r Resul t Unit s Limi t Styren e N Dmg/k g5 0 1,1,1,2-Tetrachloroethan e NDmg/k g5 0 1,1,2,2-Tetrachloroethan e N Dmg/k g5 0 Tetrachloroethen e NDmg/k g5 0 Toluen e 49 0 mg/k g5 0 1,1,1-Trichloroethan e NDmg/k g5 0 1,1,2-Trichloroethan e NDmg/k g5 0 Trichloroethen e NDmg/k g5 0 Trichlorofluoromethan e NDmg/k g5 0 1,2,3-Trichloropropan e N Dmg/kg
. 5 0 Viny l acetat e NDmg/k g10 0 Viny l chlorid e NDmg/k g10 0 Xylene s (total ) 120 0 mg/k g5 0
Surrogat e Recover y Toluene-d 8 11 0 % 4-Bromofluorobenzen e 9 2 % l,2-Dichloroethane-d 4 10 5 %

N D- No t detecte d N A »No t applicabl e Reporte dBy : Michae l Blade s Approve dBy : Jef f LowryP.2 1

OT C Volatil e Organic s TCL P Leachat e Metho d824 0

Clien t Name : America nPetroleu m Clien t ID : Prairi e Dal e LabID : 011425-0005

- Matrix : WAST E Authorized : 2 1 SE P 9 0

Paramete r
Viny l chlorid e 1,1-Dichloroethen e Chlorofor m 1,2-Dichloroethan e 2-Butanon e Carbo ntetrachlorid e Trichloroethen e Benzen e Tetrachloroethen e Chlorobenzen e

Surrogat e

Toluene-d 8 4-Bromofluorobenzen e 1,2-Dichloroethane-d 4 '-Crude 

### S A Inst 1 Tank tut e Btm . Sampled : 2 0 SE P Prepared : 2 9 SE P

Resul t



### N D N D N D N D N D N D N D 0.3 7 

### N D N D 90 9 0

.

Recover y


### 102 9 7 9 5 Unit s

mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L

% % % Received : 2 1 SE P 9 0 Analyzed : 0 5 OC T 9 0
Reportin g Limi t

0.5 0 0.2 5 0.2 5 0.2 5 0.5 0 0.2 5 0.2 5 0.2 5 0.2 5 0.2 5

- -

- -

ND» No t detecte d N A - No t applicabl e
Reporte dBy : Denee nMille r , Approve dBy : Jef f Lowr yP.2 2



### Metal s

Clien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r

Arseni c Bariu m Cadmiu m Chromiu m Lead
. Silve r Mercur y Seleniu m America nPetro l Prairi e 011425

- WAST E 2 1 SE P TCL P

eu m Inst i

: dale-crud e tan k 0005-S A



### 9 0

Resul t



### N D 2. 3 N D N D N D N D N D N O Leachat e

tut e bottom s
Sampled : Prepared :

Unit s
mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L 2 0 SE P 9 0 Receive d

Se e Belo

w Analyze d
Reportin g Limi t


### 1. 0 0.1 0 0.05 0 0.1 0 0.5 0 0.1 0 0.002 0 0.05 0 Analytica l

Metho d

601 0 601 0 601 0 601 0 601 0 601 0 747 0 774 0 : 2 1 SE P 9 0

: Se e Below

Prepare dAnalyze d Dat e Dat e

2 8 SE P 9 0 0 9 OC T 9 0 2 8 SE P 9 0 0 9 OC T 9 0 2 8 SE P 9 0 0 9 OC T 9 0 2 8 SE P 9 0 0 9 OC T 9 0 2 8 SE P 9 0 0 9 OCT.9 0 2 8 SE P 9 0 0 9 OCT:9 0 0 5 OC T 9 0 1 0 OCT'9 0 2 8 SE P 9 0 0 1 OC T 9 0



## ] 

# 1

J ND« No t detecte d N A • No t applicabl e Reporte dBy : Mar kBrundeg e Approve dBy : Ton i Lus kP.2 3

Genera l Inorganic s

CIien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r America n Petroleu mInstitut e

Prairi e Dale-Crud e Tan k Btm

. 011425

- WAST E 2 1 SE P

Cyanide
, Reactiv e Ignitabilit y Non-Volatil e Volatil e Oi l 

### Oil Wate r Solid s 

### p H 

### Oil

Sulfide
, Reactiv e •0005-S A Sampled : 9 0 Prepared : 2 0 SE P Se e Be l
Reportin g Resul t Unit s

ND mg/k g 81. 0 deg

. F 15. 2 % 13. 5 % 28. 7 % 45. 9 7

. 25. 4 % 6. 1 unit s N D mg/k g Limi t

0.1 0

- - 

### 0. 1 0. 5 0. 5 0. 5 0. 1

- - 0.5 0 9 0 Rec « o wAn a Analytica l Metho d

EPA/OS W 101 0 Chevro n Chevro n Chevro n Chevro n Chevro n 9045/AST M EPA/OS W jive d

yze d : 2 1 SE P
: Se e Be l

Prepare d Dat e


### N A N A N A N A N A N A N A N A N A 9 0 o w
Analyze d Dat e

2 5 SE P 9 0 2 6 SE P 9 0 o z 2 0 OC T 9 0 2 0 OC T 9 0 2 0 OC T 9 0 2 0 OC T 9 0 2 0 OC T 9 0 2 2 SE P 9 0 0 2 OC T 9 0

Not e o : Thi s tes t i s unreliabl e fo r an ysampl e othe r tha n a non-aqueou s liquid

.

Not e z : Sampl e exhibit s a characteristi c o f hazardou s waste .

ND= No t detecte d N A - No t applicabl e

Reporte dBy : RonMaioran a Approve dBy : JohnLafert yP.2 4 

# 1

Appendi xI

XVolatil e Organic s '

Metho d824 0

Clien t Name : America nPetroleu m Institut e Clien t ID : Count y

Line-FW

KBottom s LabID : 011425-0004-S A Matrix : WAST E Sampled : Authorized : 2 1 SE P 9 0 Prepared :

Paramete r

Aceton e Acetonitril e Acrolei n Acrylonitril e Ally l chlorid e Benzen e 3romod i chloromethan e Bromoform Bromomethan e Carbo ndisulfid e Carbo ntetrachlorid e Chlorobenzen e Chloropren e Chloroethan e Dibromochloromethan e Chloroform Chloromethan e DBC P (1,2-Dibromo

3-chloropropane ) ED B (1,2-Dibromoethane ) Dibromomethan e trans-1,4-Dichloro

2-buten e Dichlorodifluoromethan e 1,1-Dichloroethan e 1,2-Dichloroethan e trans-1,2-Dichloroethen e 1,1-Dichloroethen e Dich l oromethan e 1,2-Dichloropropan e cis-l,3-Dichioropropen e trans-1,3-Dichloropropen e 1,4-Dioxan e Ethy l benzen e Ethy l cyanid e 2-Hexanon e Iodomethan e Isobuty l alcoho l Methacrylonitril e 2-Butanon e (MEK ) 4-Methyl-2-pentanon e
(continue do nfollowin g page ) ND- No t detecte d N A - No t applicabl e
Reporte dBy : Stephani e Boehnk e Approve dBy : Jef f Lowr y 2 0 SE P 2 5 SE P

esul t


### N D N D ND . N D N D N D N D N D N D N D N D N D N D N D N D N D N O
N D N D N D
N O N D N D N O N O N D N D N O N O N D N O N O N D N O "N D N D N O N O N D 9 0 Received : 2 1 SE P 9 0 .9 0 A

n

Unit s mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g alyzed : 2 6 SE P 9 0

Reportin g Limi t


### 5 0 50 0 50 0 500 2 5 2 5 2 5 2 5 5 0 2 5 2 5 2 5 2 5 5 0 2 5 2 5 5 0
2 5 2 5 2 5 2 5 5 0 2 5 2 5 2 5 2 5 2 5 2 5 2 5 2 5 500 2 5 2 5 5 0 2 5 500 2 5 5 0 5 01

- Appendi x 

### I X Volatil e Organic s (CONT. )

Metho d824 0

Clien t Name : America nPetroleum Institut e Clien t ID : Count y Line-FWKBottom s LabID : 011425-0004-S A Matrix : WAST E Sampled : 2 0 SE P Authorized : 2 1 SE P 9 0 Prepared : 2 5 SE P

Paramete r

Styren e 1,1,1,2-Tetrachloroethan e 1,1,2,2-Tetrachloroethan e Tetraehloroethen e Toluen e 1,1,1-Tr i chloroethan e 1,1,2-Trichloroethan e Triehloroethen e Resul t

ND ND ND ND 3 5 ND ND ND 9 0 9 0

Unit s
mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g Received : 2 1 Analyzed : 2 6
Reportin g Limi t

2 5 2 5 2 5 2 5 2 5 2 5 2 5 2 5 SE P 9 0 SE P 9 0

• P.2 5

Tr i ch l orofluoromethan e 1,2,3-Trichloropropan e Viny l acetat e Viny l chlorid e Xylenes , (total )

Surrogat e

Toluene-d 8 4-Bromofluorobenzen e 1,2-Dichloroethane-d 4 Recover y


### 10 5 102 99 %

% %

ND- No t detecte d N A - No t applicabl e

Reporte dBy : Stephani e Boehnk e Approve dBy : Jef f Lowr yP.2 6



### OT C Volatil e Organic s TCL P Leachat e Metho d 824 0
Clien t Name : America n PetroleumInstitut e Clien t ID : Count yLine-FW K Bottom s La bID : 011425-0004-S A Matrix : WAST E Sampled : 2 0 SE P 9 0 Received : 2 1 SE P 9 0 Authorized: 2 1 SE P 9 0 Prepared : 2 9 SE P 9 0 Analyzed : 0 4 OC T 9 0 Reportin g Paramete r Resul t Unit s Limi t Viny l chlorid e ND mg/ L 0.1 0 1,1-Dichloroethen e ND mg/ L 0.05 0 Chlorofor mN D mg/ L 0.05 0 1,2-Dichloroethan e ND mg/ L 0.05 0 2-Butanon e ND mg/ L 0.1 0 Carbo n tetrachlorid e ND mg/ L 0.05 0 Trich l -oethen e NO mg/ L 0.05 0 Benzen e 0.2 1 mg/ L 0.05 0 Tetraehloroethen e ND mg/ L 0.05 0 Chlorobenzen e ND mg/ L 0.05 0 Surrogat e Recover y

' 0 

### Toluene-d 8 9 8 % 4-Bromofluorobenzen e 9 6 % l,2-Dichloroethane-d 4 10 1 %

ND » No t detecte d N A* No t applicabl e Reporte d By : Stephani e Boehnk e Approve d By : Jef f LowryP.2 7



### Metal s
TCL P Leachat e Clien t Name : America n PetroleumInstitut e Clien t ID : Count yline-fre e wate r knockou t bottom s La bID : 011425-0004-S A Matrix : WAST E Sampled : 2 0 SE P 9 0 Received : 2 1 SE P 9 0 Authorized : 2 1 SE P 9 0 Prepared : Se e Belo wAnalyzed : Se e Belo w Reportin g Analytica l Prepare d Analyze d
Paramete r Resul t Unit s Limi t Metho d Dat e Dat e Arseni c ND mg/ L 1. 0 601 0 2 8 SE P 9 0 0 9 OC T 9 0 Barium3. 4 mg/ L 0.1 0 601 0 2 8 SE P 9 0 0 9 OC T 9 0 Cadmiu mND mg/ L 0.05 0 601 0 2 8 SE P 9 0 0 9 OC T 9 0 Chromiu mND mg/ L 0.1 0 601 0 2 8 SE P 9 0 0 9 OC T 9 0 Lea d 1. 0 mg/ L 0.5 0 601 0 2 8 SE P 9 0 0 9 OC T 9 0 Silve r ND mg/ L 0.1 0 601 0 2 8 SE P 9 0 0 9 OC T 9 0 Mercur yND mg/ L 0.002 0 747 0 0 5 OC T 9 0 1 0 OC T 9 0 Selenium ND mg/ L 0.05 0 774 0 2 8 SE P 9 0 0 1 OC T 9 0

) ND = No t detecte d
J N A* No t applicabl e Reporte dBy : Mar kBrundeg e Approve dBy : Ton i Lus k 

# IGenera l Inorganic s P.2 8

CIien t Name : Clien t ID : La bID : Matrix : Authorized : America n PetroleumInstitut e

Count yLine-FW K Bottom s 011425-0004-S A WAST E Sampled : 2 1 SE P 9 0 Prepared : 2 0 SE P 9 0 Received : 2 1 SE P 9 0 Se e Belo wAnalyzed : Se e Belo w

Paramete r Cyanide
, Reactiv e Ignitabilit y Non-Volatil e Oi l Volatil e Oi l 

### Oi l Wate r Solid s

. 

### p H Sulfide
, Reactiv e Result

.



### N D >16 0 21. 3 18. 0 39. 3 45. 5 15. 2 

### 7. 8 N D Unit s mg/k g deg

. F % % % % % unit s mg/k g Reportin g

Limi t
0.1 0

- - 

### 0. 1 0. 5 0. 5 0. 5 0. 1

- - 0.5 0 Analytic a

Metho d
EPA/OS W 101 0 Chevro n Chevro n Chevro n Chevro n Chevro n 9045/AST M EPA/OS W Prepare d

Dat e

N A N A N A N A N A N A N A N A N A Analyze d

Dat e

2 5 SE P 9 0 2 6 SE P 9 0 2 0 OC T 9 0 2 0 OC T 9 0 2 0 OC T 9 0 2 0 OC T 9 0 2 0 OC T 9 0 2 2 SE P 9 0 0 2 OC T 90

.

Not e o : Thi s tes t i s unreliabl e fo r an ysampl e othe r tha n a non-aqu&ou s liquid

.
ND - No t detecte d N A- No t applicabl e
Reporte dBy : RonMaioran a Approve dBy : JohnLafert yP.2 9

Appendi xI

XVolatil e Organic s

Metho d824 0

Clien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r America nPetroleu m Institut e Semivole-Crud e Tan kBottom s 011425-0003-S A WAST E Sampled : 2 1 SE P 9 0 Prepared : 2 0 2 5 SE P SE P 9 0 9 0

Aceton e Acetonitril e Acrolei n Acrylonitril e Ally l chlorid e Benzen e Bromod i chloromethan e Bromoform Bromomethan e Carbo ndisulfid e Carbo ntetrachlorid e Chlorobenzen e Chloropren e Chloroethan e Dibromochloromethan e Chlorofor m Ch l oromethan e DBC P (1,2-Dibromo

3-chloropropane ) EDB (1,2-Dibromoethane ) Dibromomethan e trans-1,4-Dichloro

2-buten e Di ch l orod i f1uoromethan e 1,1-Dichloroethan e 1,2-Dichloroethan e trans-1,2-Dichloroethen e 1,1-Oichloroethen e Dichloromethan e 1,2-Dichloropropan e cis-l,3-Dichioropropen e trans-1,3-D i chloropropen e 1,4-Dioxan e Ethy l benzen e Ethy l cyanid e 2-Hexanon e Iodomethan e Isobuty l alcoho l Methacrylonitril e 2-Butanon e (MEK ) 4-Methyl-2-pentanon e Resul t

ND ND ND ND ND 550 0 ND ND ND ND ND ND ND N O ND ND ND

NO NO ND

ND ND ND ND ND ND ND ND ND ND ND 740 0 ND ND ND ND ND ND ND Received : 2 1 SE P 9 0

Analyzed : 2 8 SE P 9 0
Reportin g Unit s Limi t
mg/k g 500 0 mg/k g 5000 0 mg/k g 5000 0 mg/k g 5000 0 mg/k g 250 0 mg/k g 250 0 mg/k g 250 0 mg/k g 250 0 mg/k g 500 0 mg/k g 250 0 mg/k g 250 0 mg/k g 250 0 mg/k g 250 0 mg/k g 500 0 mg/k g 250 0 mg/k g 250 0 mg/k g 500 0
mg/k g 250 0 mg/k g 250 0 mg/k g 250 0

mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g 250 0

500 0 250 0 250 0 250 0 250 0 250 0 250 0 250 0 250 0 5000 0 250 0 250 0 500 0 250 0 5000 0 250 0 500 0 500 0

ND N A No t No t detecte d applicabl e (continue donfollowin g page )

Reporte dBy : Michae l Blade s Approve dBy : Jef f Lowr yP.3 0

CIien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r Appendi xI XVolatil e Organic s (CONT. )

Metho d824 0

America nPetroleu

m Institut e Semi vole-Crud e Tan kBottom s 011425-0003-S A WAST E Sampled : 2 1 SE P 9 0 Prepared :

Styren e 1,1,1,2-Tetrachloroethan e 1,1,2,2-Tetrachloroethan e Tetraehloroethen e Toluen e . 1,1,1-Trichloroethan e 1,1,2-Trichloroethan e Triehloroethen e Trichlorof1uoromethan e 1,2,3-Tr i chloropropan e Viny l acetat e Viny l chlorid e Xylene s (total )

Surrogat e

Toluene-d 8 4-Bromof1uorobenzen e l,2-Dichloroethane-d 4 , 0 SE P 2 5 SE P

Resul t


### N D N D N D N D 3200 0 

### N D N D N D N D N O N D N O 5200 0 

### 9 0 90

Recover y 

### 10 9 96 100 Unit s

^g/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

% % % Received : 2 1 Analyzed : 2 8
Reportin g Limi t

250 0 250 0 250 0 250 0 250 0 250 0 250 0 250 0 250 0 250 0 500 0 500 0 250 0

- -

- - SE P 9 0 SE P 9 0

N D- No t detecte d N A - No t applicabl e
Reporte dBy : Michae l Blade s Approve dBy : Jef f Lowr yP.3 1

OTC Volatil e Organic s TCL P Leachat e Method 824 0

Clien t Name : American Petroleu mInstitut e Clien t ID : Semivole-Crud e Tan k Bottoms La b ID : 011425-0003-S A Matrix : WAST E Sampled : Authorized : 2 1 SE P 9 0 Prepared :

Paramete r Viny l chlorid e 1,1-Dichloroethen e Chlorofor

m 1,2-Dichloroethan e 2-Butanohe Carbo n tetrachlorid e Triehloroethen e Benzen e Tetrachloroethen e Chlorobenzen e
Surrogate '

Toluene-d 8 4 -Bromof1uorobenzen e 1,2-Dichloroethane-d 4 2 0 SE P 2 9 SE P

esu l t



### N D N D N D N D N O N D N D 

### 3. 0 N D N D

kCtUVC ^
9 9 

### 9 7 9 6 9 0 9 0

7 Unit s
mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L

% % % Received : 2 1 SE P 9 0 Analyzed : 0 5 OC T 9 0
Reporting Limi t


### 1. 0 0.5 0 0.5 0 0.5 0 

### 1. 0 0.5 0 0.5 0 0.5 0 0.5 0 0.5 0

- -

- -

N D- Not detecte

d N A - Not applicabl e
Reporte dBy : Denee

nMille r Approve dBy : Jef f Lowr

yP.3 2

Metal s

TCL P Leachat e
Clien t Name : America n PetroleumInstitut e Clien t ID : Semivole-crud e tan k bottom s LabID : 011425-0003-S A Matrix : WAST E Sampled : 1 7 SE P 9 0 Received : 2 1 SE P 9 0 Authorized : 2 1 SE P 9 0 Prepared : Se e Belo wAnalyzed : Se e Belo w Reportin g Analytica l Prepare d Analyze d Paramete r Resul t Unit s Limi t Metho d Dat e Dat e
Arseni c ND mn/ L 1. 0 601 0 2 8 SE P 9 0 0 2 OC T 9 0 Barium 2. 6 r L 0.3 8 601 0 2 8 SE P 9 0 0 2 OC T 9 0 Cadmium N D m^/ L 0.05 0 601 0 2 8 SE P 9 0 0 2 OC T 9 0 Chromium0.4 7 mg/ L 0.1 0 601 0 2 8 SE P 9 0 0 2 OC T 9 0 Lea d ND mg/ L Silve r N D mg/ L Mercur yND mg/ L SeleniumN D mg/ L 0.05 0 774 0 2 8 SE P 9 0 0 1 OC T 9 0 

### 1. 0 0.3 8 0.05 0 0.1 0 0.5 0 0.1 0 0.002 0 0.05 0 601 0

601 0 601 0 601 0 601 0 601 0 747 0 774 0 

### 2 8

2 8 0 5 

### SE P SEP OC T 9 0 9 0 9 0 0 2 0 2 

### OC T OC T 1 0 OC T 

### 9 0 9 0 9 0

ND - No t detecte d N A- No t applicabl e
Reporte dBy : Mar kBrundeg e Approve dBy : Ton i Lus kGenera l Inorganic s P.3 3

CIien t Name : Clien t ID : La b ID : Matrix : Authorized :

Paramete r American Petro l

Semivo l 011425

- WAST E 2 1 SE P

Cyanide
, Reactiv e Ignitabilit y Nonvolatil e Volatil e Oi l 

### Oil Water

. Solid s 

### p H 

### Oil

Sulfide
, Reactiv e e-Crud e -0003-S A


### 9 0

Resul t



### N D 64. 0 22. 5 36. 0 58. 5 33. 7 

### 7. 8 8. 4 0.6 3 eu mInstitut e Tan k Bottom s
Sampled : 2 0 SE P Prepared : Se e Be l

Reporting Unit s Limi t
mg/kg 0.1 0 deg

. F % 0. 1 % 0. 9 % 0. 9 %0. 9 % 0. 1 unit s mg/kg 0.5 0 9 0 Receive d

o wAnalyze d
Analytica l Metho d

EPA/OSW 101 0 Chevro n Chevro n

. Chevro n Chevro n Chevro n 9045/AST

M EPA/OSW : 2 1

: Se e 

### SE P Be l

Prepare d Dat e


### N A N A N A N A N A N A N A N A N A 9 0 o w
Analyze d Dat e

2 5 SE P 9 0 2 6 SE P 9 0 2 0 OC T 9 0 2 0 OC T 9 0 2 0 OC T 9 0 2 0 OC T 9 0 2 0 OC T 9 0 2 2 SE P 9 0 0 2 OC T 9 0 

### o

z

Not e o : Thi s tes t i s unreliabl e fo r anysampl e othe r tha n a

non-aqueou s liquid

.
Not e z : Sampl e exhibit s a characteristi c o f hazardou s waste .

ND- No t detecte d N A * No t applicabl e

Reporte dBy : RonMaiorana * Approve dBy : JohnLafert yP.3 4

Appendi xI

XVolatil e Organic s

Metho d824 0

CIien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r America nPetroleum Institut e Midbloc kHeate r Treate r Btm . 011425-0007-S A WAST E Sampled : 2 1 SE P 9 0 Prepared :

Aceton e Acetonitril e Acrolei n Acrylonitril e Ally l chlorid e Benzen e Bromod i chloromethan e Bromofor m Bromomethan e Carbo ndisulfid e Carbo ntetrachlorid e Chlorobenzen e Chloropren e Chloroethan e D i bromochloromethan e Chlorofor m Chloromethan e DBC P (1,2-Dibromo

3-chloropropane ) ED B (1,2-Dibromoethane ) Dibromomethan e trans-1,4-Dichloro

2-buten e D i chlorod i f1uoromethan e 1,1-Dichloroethan e 1,2-Dichloroethan e trans-1,2-Dichloroethen e 1,1-Dichloroethen e Dichloromethan e 1,2-Dichloropropan e cis-1,3-Dichloropropen e tran s -1,3-D i chloropropen e 1,4-Dioxan e Ethy l benzen e Ethy l cyanid e 2-Hexanon e Iodomethan e Isobuty l alcoho l Methacrylonitril e 2-Butanon e (MEK) ~ 4-Methyl-2-pentanon e 2 0 SE P 2 5 SE P

esul t


### N D N D N D N D N D 14 0 N O N O N D N D N D N D N D• 

### N D N D N D N O
N D N O N D
N O N O N D N D N D N D N D N D N D N D N D 320 N O N D N D N D N D N D N D 9 0 Received : 2 1 SE P 9 0 9 0 A

n

Unit s mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g alyzed : 2 7 SE P 9 0

Reportin g Limi t 

### 25 0 250 0 250 0 250 0 

### 12 0 12 0 12 0 12 0 25 0 12 0 12 0 12 0 12 0 25 0 12 0 12 0 250
12 0 12 0 12 0
12 0 250 12 0 12 0 12 0 12 0 12 0 12 0 120 12 0 250 0 

### 12 0 12 0 25 0 12 0 250 0 

### 12 0 25 0 250
(continue donfollowin g page )

Reporte dBy : Michae l Blade s Approve dBy : Jef f Lowr y N D- No t detected 6 ' N A * No t applicabl eP.3 5

CIien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r Appendi xI X Volatil e Organic s (CONT. )

Metho d 824 0

America n Petroleu m

Institut e Midbloc k Heate r Treate r Btm

. 011425-0007-S A WAST E Sampled : 2 1 SE P 9 0 Prepared :

Styren e 1,1,1,2-Tetrachloroethan e 1,1,2,2-Tetraehloroethan e Tetraehloroethen e Toluen e 1,1,1-Trichloroethan e •1,1,2-Trichloroethan e Triehloroethen e Trichlorofluoromethan e 1,2,3-Tr i chloropropan e Viny l acetat e Viny l chlorid e Xylene s (total )

Surrogat e

Toluene-d 8 4 -Bromof1 uorobenzen e 1, 2-D i chl oroethane-d 4 2 0 SE P 2 5 SE P

tesult



### N D N D N D N D 

### 69 0 N D N D N D N D N D N D N D 100 0

Uflrftuov

* ^ctUVc i
10 3 

### 9 8 9 7 9 0 9 0

w y Unit s mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/kg

- .mg/kg

% % % Received : 2 1 SE P 9 0 Analyzed : 2 7 SE P 9 0
Reportin g Limi t


### 12 0 12 0 12 0 12 0 12 0 12 0 12 0 12 0 12 0 120

. 

### 25 0 25 0 12 0

- -

- -

N D- No t detecte d N A - No t applicabl e

Reporte dBy : Michae l Blade s Approve dBy : Jef f Lowr yP.3 6 

# 1

OT C Volatil e Organic s TCL P Leachat e Metho d 824 0

Name : ID :

ized

. America r PetroleumInstitut e Miablcc k Heate r Treate r Btm

. 0U42S-0007-S A WAjT E Sampled :
: P 9 C Prepared : ^ i

-.ete r

1

. • ."I

. chlorid e

'

. Oichloroetnen e

• ; • *o f or m :.'

. "nchlcroethan e '-.-': .anon e '. V r> n tetrachlorid e

•• • V i oroethen e :»?• • r-n e '•- •.•-•.chl oroethen e '..-.'

- ooenzen e
•j v -ogat a

Tr

. uene-d 8 •*• r.-omo f 1 uorobenzen e 1.I-Oichloroethane-d 4 2 0 SE P 2 9 SE P

esul t


### N D N D N D N D 

### N D N O N D 0.9 4 

### N D N D



### 10 2 

### 96 9 8 9 C 9 0

y Unit s mg/ L mg/ L mg/ L mq/ L mq/ L mg/ L mg/ L mg/ L mg/ L mg/ L

% % % 

### R e A n :eived : 2 i SE P 9 0 alyzed : 0 5 OC T 9 0
Reportin g Limi t
0.5 0 0.2 5 0.2 5 0.2 5 0.5 0 0.2 5 0.2 5 0.2 5 0.2 5 0.2 5

- -

- -

ND * No t detecte d N A - No t applicabl e
Reporte dBy : Denee nMille r Approve dBy : Jef f Lowry



# 1P.3 7

Metal s

TCL P Leachat e

Clien t Name : American Petroleu mInstitut e Clien t ID : Midbloc k heate r treate r bottom s La b I D Matri x 011425-0007-S A

WAST E Sampled : 2 0 SE P 9 0 Received : 2 1 SE P 9 0 Authorized : 2 1 SE P 9 0 Prepared : Se e BelowAnalyzed : Se e Below Reportin

g Analytica l Prepare d Analyze d
Paramete r Resul t Unit s Limi t Metho d Dat e Dat e
Arseni c N D mg/ L 1. 0 601 0 2 8 SE P 9 0 0 9 OC T 9 0 Bariu m1. 6 mg/ L 0.1 0 601 0 2 8 SE P 9 0 0 9 OC T 9 0 Cadmiu mN

D mg/ L 0.05 0 601 0 2 8 SE P 9 0 0 9 OC T 9 0 Chromiu m0.1 4 mg/ L 0.1 0 601 0 2 8 SE P 9 0 0 9 OC T 9 0 Lea d 9. 6 mg/ L 0.5 0 601 0 2 8 SE P 9 0 0 9 OC T 9 0 Silve r N D mg/ L 0.1 0 601 0 2 8 SE P 9 0 0 9 OC T 9 0 MercuryN D mg/ L 0.002 0 747 0 0 5 OC T 9 0 1 0 OC T 9 0 Seleniu mN

D mg/ L 0.05 0 774 0 2 8 SE P 9 0 0 1 OC T 9 0

N D = No t detecte d j N A • Not applicabl e
Reporte dBy : Mar

kBrundege Approve dBy : Ton i Lus kGenera l Inorganic s P.3 8

Clien t Name : America nPetro l Clien t ID : Midbloc kHeate r LabID : 01142 5 Matrix : WAST E Authorized : 2 1 SE P

Paramete r Cyanide , Reactiv e Ignitabilit y Non-Volatil e Oi l Volatil e Oi l 

### Oi l Wate r Solid s pH. Sulfide , Reactiv e -0007-S A



### 9 0

Resul t


### N D 77. 0 58. 2 13. 5 71. 7 14. 4 13. 9 

### 8. 9 N D eu m Institut e Treate r Btm . Sampled : Prepared : 2 0 SE P

Se e Be l Reportin g Unit s mg/k g deg
. F % % % % % unit s mg/k g Limi t

0.1 0

- - 

### 0. 1 0. 5 0. 5 0. 5 0. 1

- - 0.5 0 9 0 Receive d
o w Analyze d Analytica l Metho d
EPA/OS W 101 0 Chevro n Chevro n Chevro n Chevro n Chevro n 9045/AST M EPA/OS W : 2 1

: Se e 

### SE P Be l
Prepare d Dat e


### N A N A N A N A N A N A N A N A N A 9 0 o w Analyze d Dat e

2 5 SE P 9 0 2 7 SE P 9 0 o z 2 0 OC T 9 0 2 0 OC T 9 0 2 0 OC T 9 0 2 0 OC T 9 0 2 0 OC T 9 0 2 2 SE P 9 0 0 2 OC T 9 0

Not e o : Thi s tes t i s unreliabl e fo r an y sampl e othe r tha na non-aqueou s liquid

.
Not e z : Sampl e exhibit s a characteristi c o f hazardou s waste .

ND- No t detecte d N A - No t applicabl e
Reporte dBy : Ro nMaioran a Approve dBy : Joh nLafert y


# 1P.3 9

ANALYTICAL RESULT S

FO R

AMERICA N PETROLEU

M INSTITUT E

ENSECO-RMAL NO
. 01168 6

NOVEMBE R21 , 199 0



### Reviewe dby : •zrrfL'OA.^Li/l/t/kZ / 

## .STSusa n «C

. wyat t

a

i Rock y Mountain Analytica l Laborator

y



# Ensec o

Enseco Incorporated 4 W Yarro

wStree t Arvada. Colorad o 8000 2 303/421-OOI 1 Fax : 503/431-717 1P.4 0

Appendi xI

XVolatil e Organic s

Metho d824 0

CIien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r America nPetroleu m Institut e Chickasha-Crud e Tan kBottom s 011686-0001-S A WAST E Sampled : 0 5 OC T 9 0 Prepared :

Aceton e Acetonitril e Acrolei n Acrylonitril e Ally l chlorid e Benzen e Bromodichloromethan e Bromoform Bromomethan e Carbo ndisulfid e Carbo ntetrachlorid e Chlorobenzen e Chloropren e Chloroethan e Dibromochloromethan e Chloroform Chloromethan e DBC P (1,2-Dibromo

3-chloropropane ) ED B (1,2-Dibromoethane ) Dibromomethan e trans-1,4-Dichloro

2-buten e Di chlorod i fluoromethan e 1,1-Dichloroethan e 1,2-Dichloroethan e trans-1,2-Dichloroethen e 1,1-Dichloroethen e Dichloromethan e 1,2-Oichloropropan e cis-1,3-Dichloropropen e trans-1,3-Dichloropropen e 1,4-Dioxan e Ethy l benzen e Ethy l cyanid e 2-Hexanon e Iodomethan e Isobuty l alcoho l Methacrylonitril e 2-Butanon e (MEK ) 4-Methyl-2-pentanon e 0 " OC T lu JC T

iesul t


### N D N O N O N D N O 720 N D N D N D N O N O N D N D N D N D N D N O
N O N O N O
N D N O N O N D N O N D N D N D N D N D N D 620 N D N D N D N O N D N D N D 9 0 Received : 0 5 OC T 9 0 9 0 A

n

Unit s mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g 

### mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g alyzed : 1 5 OC T 9 0 Reportin g Limi t 

### 330 330 0 330 0 330 0 

### 16 0 16 0 16 0 160 330
. 

### 16 0 16 0 16 0 16 0 330 16 0 16 0 330 16 0 16 0 16 0 16 0 330 16 0 16 0 16 0 16 0 16 0 16 0 16 0 16 0 330 0 

### 160 16 0 330 16 0 330 0 

### 16 0 330 330
(continue donfollowin g page )

Reporte dBy : Terr y

Riddl e Approve dBy : Jef f Lowr y ND- No t detecte d N A « No t applicabl eP.4 1

CIien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r Appendi xI XVolatil e Organic s (CONT. )

Metho d824 0

America nPetroleu

m Institut e Chickasha-Crud e Tan kBottom s 011686-0001-S A WAST E Sampled : 0 5 OC T 9 0 Prepared :

Styren e 1,1,1,2-Tetrachloroethan e 1,1,2,2-Tetrachloroethan e Tetraehloroethen e Toluen e 1,1,1-Tr i chloroethan e 1,1,2-Trichloroethan e Triehloroethen e Tr i chlorofluoromethan e 1,2,3-Trichloropropan e Viny l acetat e Viny l chlorid e Xylene s (total )

Surrogat e

Toluene-d 8 4-Bromof1uorobenzen e 1,2-Dichloroethane-d 4 0 3 OC T 9 0 1 2 OC T 9 0

Resul t



### N D N D N D N D 290 0 

### N D N D N D N D N D N D N D 310

Recover y


### 104 9 7 104 Unit s

mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

% % % Received : 0 5 OC T 9 0 Analyzed : 1 5 OC T 9 0
Reportin g Limi t


### 160 160 160 160 160 160 160 160 160 160 33 0 33 0 160

. _

- -

- -

ND- No t detecte d N A - No t applicabl e

Reporte dBy : Terr y Riddl e Approve dBy : Jef f Lowr yP.4 2

Clien t Name : Clien t ID : LabID : Matrix :

Paramete r 011686-0001-S A

WAST E

1,1,1-Tr i chloroethan e Isobuty l alcoho l Viny l chlorid e Acrylonitril e Methylen e chlorid e Carbo ndisulfid e 1,1-Dichloroethen e 

### Chlorofor m . 1,2-Dichloroethan e 2-Butanon e Carbo ntetrachlorid e Triehloroethen e Benzen e 1,1,2,2-Tetrachloroethan e Tetraehloroethen e Chlorobenzen e 1,1,2-Trichloroethan e 1,1,1,2-Tetrachloroethan e Toluen e
Surrogat e

Toluene-d 8 4-Bromof1uorobenzen e 1,2-Dichloroethane-d 4 OT C Volatil e Organic s TCL P Leachat e Metho d824 0

ur nInstitut e Tan kBottom s Sampled : 0 3 OC T Received : 0 5 OC T Authorized : 0 5 OC T

Resul t


### N D N D N D N D N D N O N D N D N D N O N O N O 3. 7 N O N D N O N D N D 5. 2

Recover y 

### 9 8 100 92 90 90 90

Unit s mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L

% % % Leached : 1 8 Prepared : 1 8 Analyzed : 2 3
Reportin g Limi t 

### 1. 2 5 0 2. 5 2 5 1. 2 1. 2 1. 2 1. 2 1. 2 2. 5 1. 2 1. 2 1. 2 1. 2 1. 2 1. 2 1. 2

- 1. 2 

### 1. 2

. .

- -

- - OC T 9 0 OC T 9 0 OC T 9 0

N D* No t detecte d N A - No t applicabl e
Reporte dBy : Brya nAnderso n Approve dBy : Jef f Lowr yP.4 3

Metal s

TCL P Leachat e
Clien t Name : America n Petroleu mInstitut e Clien t ID : La b ID : Matrix : Authorized :

Paramete r
Arseni c Bariu m Cadmiu m Chromiu m Lea d Silve r Mercury Seleniu m 

### C h icka : 011686

- WAST E 

### 0 5 

### OC T »ha-Crud e -0001-S A



### 9 0

Resul t



### N D 

### 5. 7 N D N D N D N D N D N D Tan

k Bottom s
Sampled : Prepared : 0 3 OC T <

Se e Bel t
Reporting Unit s
mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L 

### mg/ L mg/ L Limi t



### 1. 0 0.5 1 0.05 0 0.1 0 0.5 0 0.1 0 0.002 0 0.05 0 

### 3 0 3 W
Analy t Rect Ana '

ica l Metho d

601 0 601 0 601 0 601 0 601 0 601 0 747 0 774 0 ;ive

d Iyze d : 0 5 OC T 9 0

: Se e Below
Prepare d Analyze d Dat e Dat e

1 8 OC T 9 0 2 1 OC T 9 0 1 8 OC T 9 0 2 1 OC T 9 0 1 8 OC T 9 0 2 1 OC T 9 0 1 8 OC T 9 0 2 1 OC T 9 0 1 8 OC T 9 0 2 1 OC T 9 0 1 8 OC T 9 0 2 1 OC T 9 0 2 4 OC T 9 0 2 5 OC T 9 0 1 8 OC T 9 0 0 7 NO

V 9 0

ND = No t detecte d N A- No t applicabl e

Reporte d By : Thoma s Cas e Approve dBy : Roxann e Sulliva nGenera l Inorganic s P.4 4

Clien t Name : America nPetroleu m Institut e Clien t ID : Chickasha-Crud e Tan kBottom s LabID : 011 c 8 6 Matrix : WA S E Authorized : 0 5 OC T

Paramete r Cyanide , Reactiv e Ianitabilit y Non-Volatil e Oi l Volatil e Oi l 

### Oi l Wate r Solid s 

### P H Sulfide , Reactiv e -0001-S A Sampled : 9 0 Prepared : 0 3 OC T Se e Be l Reportin g Resul t Unit s

NDmg/k g 10 2 deg
. F 6. 2 % 22. 5 % 28. 7 % 37. 7 % 33. 6 % 6. 3 unit s N Dmg/k g Limi t

0.1 0

- - 

### •o. i 

### 0. 5 0. 5 0. 5 0. 1

- - 0.5 0 9 0 Received : 0 5
o w Analyzed : Se e 

### OC

T Be l Analytica l Prepare d Metho dDat e EPA/OS W N

A

. 101 0 N

A Chevro nN

A Chevro nN

A Chevro nN

A Chevro nN

A Chevro nN

A 9045/AST M

N

A EPA/OS W N

A 

### 9 0 o w Analyze d Dat e
2 3 OC T 9 0 1 8 OC T 9 0 o z 2 3 OC T 9 0 2 3 OC T 9 0 2 3 OC T 9 0 2 3 OC T 9 0 2 3 OC T 9 0 2 7 OC T 9 0 2 3 OC T 9 0

Not e o : Thi s tes t i s unreliabl e fo r an y sampl e othe r tha na non-aqueou s liquid

.
Not e z : Sampl e exhibit s a characteristi c o f hazardou s waste .

ND= No t detecte d N A - No t applicabl e
Reporte dBy : Eilee nBurk e Approve dBy : Ton i Stoval l


# 1ANALYTICAL RESULT S

FO R

AMERICA N PETROLEU

M INSTITUT E

ENSECO-RMAL NO
. 01177 2

NOVEMBE R27 , 199 0

Reviewe d by : ^.LOdM LW6\&\ Susa nC^Wyat t P.4 5 i

- Rock y Mountai n Analytical Laboratory



# Enseco

Ensec o Incorporate d 495 5 Yarro w Stree t Arvada

. Colorad o 3000 2 303/421-o6l l Fax : 303/431-717 1f Appendi xI XVolatil e Organic s

1 Metho d824 0

' Clien t Name : America nPetroleu m Institut e Clien t ID : O.W
. WARDCRUD E TAN KBOTTOM S La bID : 011772-0001-S A Matrix : WAST E Sampled : 0 9 OC T 9 0 Received : 1 1 OC T 9 0
: Authorized : 1 1 OC T 9 0 Prepared : 1 2 OC T 9 0 Analyzed : 1 9 OC T 9 0 Reportin g

, Paramete r Resul t Unit s Limi t

JAceton e N D Acetonitril e ND i Acrolei nND JAcrylonitril e ND Ally l chlorid e ND Benzen e 120 0 ] Bromodich l oromethan e ND ! Bromoform

ND Bromomethan e N D

, Carbo ndisulfid e ND Carbo ntetrachlorid e ND Chlorobenzen e N D Chloropren e ND Chloroethan e ND Dibromochloromethan e ND Chloroform

ND Chloromethan e ND DBC P (1,2-Dibromo

3-chloropropane ) ND EDB (1,2-Dibromoethane ) N O Dibromomethan e NO trans-1,4-Dichloro

2-buten e ND Dichlorodifluoromethan e ND 1,1-01chloroethan e ND 1,2-Dichloroethan e ND trans-1,2-Dichloroethen e N D 1,1-Dichloroethen e ND Dichloromethan e ND 1,2-Dichloropropan e N O cis-1,3-Oichloropropen e ND trans-1,3-Dichloropropen e ND 1,4-Dioxan e ND Ethy l benzen e 35 0 Ethy l cyanid e . N D

, 2-Hexanon e ND Iodomethan e ND JIsobuty l alcoho l ND Methacrylonitril e ND 2-Butanrn e (MEK ) ND 4-Methyl-2-pentanon e ND 

# 1 ] ] ] mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g 

### 10

0 100 0 100 0 100 0 

### 5 0 5 0 5 0 5 0 10 0 5 0 5 0 5 0 5 0 10 0 5 0 5 0 10 0
5 0 5 0 5 0
5 0 10 0 5 0 5 0 5 0 5 0 5 0 5 0 5 0 5 0 100 0 

### 5 0 5 0 10 0 5 0 100 0 

### 5 0 10 0 100
(continue do

nfollowin g page ) N D- No t detecte d N A • No t applicabl e
Reporte dBy : Michae l Blade s Approve dBy : Jef f Lowr yP.4 7

Clien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r Appendi xI XVolatil e Organic s (CONT. )

Metho d824 0

America nPetroleu

m Institut e O.W
. WAR DCRUD E TAN

KBOTTOM S 011772-0001-S A WAST E Sampled : 1 1 OC T 9 0 Prepared :

Styren e 1,1,1,2-Tetraehloroethan e 1,1,2,2-Tetrachloroethan e Tetraehloroethen e Toluen e 1,1,1-Trichloroethan e 1,1,2-Trichloroethan e Triehloroethen e Tr i ch l orofluoromethan e 1,2,3-Trichloropropan e Viny l acetat e Viny l chlorid e Xylene s (total )
Surrogat e
Toluene-d 8 4-Bromof1uorobenzen e l,2-0ichloroethane-d 4 0 9 OC T 9 0 1 2 OC T 9 0

Resul t



### N D N D N D N D 150 0 

### N D N D N D N D N D N D N D 160 0

Recover y


### 10 5 9 7 93 Unit s

mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g mg/k g

% % % Received : 1 1 OC T 9 0 Analyzed : 1 9 OC T 9 0
Reportin g Limi t


### 5 0 50 5 0 5 0 5 0 5 0 5 0 5 0 5 0 50 100 100 5 0

- -

- -

ND» No t detecte d N A * No t applicabl e
Reporte dBy : Michae l Blade s Approve dBy : Jef f Lowr yP.4 8

Clien t Name : Clien t ID : LabID : Matrix : OT C Volatil e Organic s TCL P Leachat e Metho d824 0

America nPetroleu

m Institut e O.W
. WARDCRUD E TAN

KBOTTOM S 011772-0001-S A

Sampled : 0 9 OC T 9 0 WAST E " ' Received : 1 1 OC T 9 0

Authorized : 1 1 OC T 9 0 Leached : 2 1 OC T 9 0 Prepared : 2 3 OC T 9 0 Analyzed : 2 5 OC T 9 0

Paramete r
1,1, 1 -Tr i eh 1 -"-oethan e Isdbuty l a .a

l Viny l chlo r .a Acrylonitrii e Methylen e chlorid e Carbo ndisulfid e 1,1-Dichloroethen e Chlorofor m 1,2-Dichloroethan e 2-Butanon e Carbo ntetrachlorid e Triehloroethen e Benzen e 1,1,2,2-Tetrachloroethan e Tetraehloroethen e Chlorobenzen e 1,1,2-Trichloroethan e 1,1,1,2-Tetrachloroethan e Toluen e
Surrogat e

Toluene-d 8 4-Bromofluorobenzen e l,2-Dichloroethane-d 4 esul t


### N D N O N O N D N D N D N D N D N D N D N D N D 420 N D N D N D N D N O 560

eCOVerj r 10 7 

### 10 0 10 4 Unit s mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L 

### mg/ L mg/ L mg/ L

% ' % % Reportin g

Limi t 

### 15 0 610 0 

### 31 0 310 0 

### 15 0 15 0 150 15 0 15 0 31 0 15 0 15 0 15 0 15 0 15 0 15 0 15 0 15 0 15 0

- -

- -



# 1 ND- No t detecte d N A * No t applicabl e
Reporte dBy : Michae l Blade s Approve dBy : Jef f Lowr y



# 1P.4 9



### Metal s

Clien t Name : Clien t ID : LabID : Matrix : Authorized :

Paramete r TCL P Leachat e

America nPetroleum

Institut e O.W

. WAR D CRUD E TANK BOTTOM S 011772-0001-S A, j nn nry 

### . . WAST E Sampled : 0 9 OC T 9 0 1 1 OC T 9 0

Resul t Prepared : Se e Belo w Received : 1 1 OC T 9 0 Analyzed : Se e Belo w

Unit s Reportin g Analytica l

Limi t Metho d Prepare d Analyze d Dat e Dat e Arseni c Barium Cadmiu m Chromiu m Lea d Silve r Mercur y Selenium ND

45. 6 0.2 8 0.4 1 N D ND 0.03 3 ND mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L mg/ L 1

.

0

. 0

. 0 , 0 , 0 , 0 , 

### 0 , 5 

### .60 .07 2 

### .1 5 .72 .15 .01 3 .09 8 601 0 601 0 601 0 601 0 601 0 601 0 747 0 774 0 

### N

A N A N A N A N A N A 1 6 NOV

9 0 1 6 NO V 9 0 1 6 NOV 9 0 1 6 NO V 9 0 1 6 NOV 9 0 1 6 NOV 9 0 2 4 OC T 9 0 1 6 NOV

9 0 N A 1 6 NOV

9 0

ND * No t detecte d N A- No t applicabl e Reporte dBy : FredVelasque z Approve dBy : JohnLafert yGenera l Inorganic s P.5 0

Clien t Name : Clien t ID : La bID : Matrix : Authorized :

Paramete r America n PetroleumInstitut e

O.W

. WAR D CRUD E TAN K BOTTOM S 011772-0001-S A WAST E Sampled : 1 1 OC T 9 0 Prepared :

Cyanide
, Reactiv e Ignitabilit y Non-Volatil e Oi l Volatil e Oi l Oi l Wate r Solid s P H Sulfide
, Reactiv e Resul t

ND 6 6 2. 5 18. 0 20. 5 73. 7 5. 8 6. 4 5. 5 0 9 OC T 9 0

Se e Belo w Received :

Analyzed :

Unit s mg/k g deg

. F % % % % % unit s mg/k g Reportin g

Limi t

0.10 '

0. 1 0. 9 0. 9 0. 9 0. 1

0.5 0 Analytica l

Metho d
EPA/OSW ' 101 0 Chevro n Chevro n Chevro n Chevro n Chevro n 9045/AST M EPA/OS W -. 1 OC T 9 0

Se e Belo w
Prepare d Dat e

N A N A N A N A N A N A N A N A N A Analyze d

Dat e
0 6 NOV 9 0 2 9 OC T 9 0 o z 0 6 NO V 9 0 0 6 NOV 9 0 0 6 NOV 9 0 0 6 NOV 9 0 0 6 NOV 9 0 1 2 NOV 9 0 0 2 NO V 9 0



# 1 ] Not e o : Thi s tes t i s unreliabl e fo r an y sampl e othe r thana non-aqueou s liquid

.
Not e z : Sampl e exhibit s a characteristi c o f hazardou s waste .

N D- No t detecte d N A - No t applicabl e
Reporte dBy : Mik e Settel l Approve dBy : JohnLafert yP.5 1