### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

2161 James River 4 

### subbituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte



### 2161 James River 4 As Received Higher Heating Value 

### 2161 James River 4 As Received % Moisture 

### 2161 James River 4 As Received % Ash 

### 2161 James River 4 As Received % Sulfur 

### 2161 James River 4 Dry basis Higher Heating Value 

### 2161 James River 4 Dry basis % Ash 

### 2161 James River 4 Dry basis % Sulfur 

### 2161 James River 4 Dry basis Antim ony 

### 2161 James River 4 Dry basis Arsenic 

### 2161 James River 4 Dry basis Bery llium 

### 2161 James River 4 Dry basis Cadmium 

### 2161 James River 4 Dry basis Chlorine 

### 2161 James River 4 Dry basis Chromium 

### 2161 James River 4 Dry basis Cobalt 

### 2161 James River 4 Dry basis Fluorine 

### 2161 James River 4 Dry basis Lead 

### 2161 James River 4 Dry basis Manganese 

### 2161 James River 4 Dry basis Mercury 

### 2161 James River 4 Dry basis Nickel 

### 2161 James River 4 Dry basis SeleniumAn alysis M ethod for each A nalyte

(example: ASTM D5865-04) 

### ASTM D5865-07a ASTM D3302/D3302M-09 D3173 ASTM D3174-04 ASTM D4239-08 Method B ASTM D5865-07a ASTM D3174-04 ASTM D4239-08 Method B ASTM D6357-04 ASTM D6357-04 ASTM D6357-04 ASTM D6357-04 ASTM D6721-01 ASTM D6357-04 ASTM D6357-04 ASTM D3761-96 ASTM D6357-04 ASTM D6357-04 ASTM D6722-01 ASTM D6357-04 ASTM D4606-03EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 2161 James River 4 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### JRU4-CSR-1 6/22/2010 6/22/2010 8468.00 Btu/lb JRU4-CSR-2 6/23/2010 6/23/2010 8465.00 Btu/lb JRU4-CSR-3 6/23/2010 6/23/2010 8474.00 Btu/lb Fuel Testing Results

### Mercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 29.86 4.95 0.27 12073 Btu/lb 7.06 0.38 29.83 5.05 0.27 12064 Btu/lb 7.20 0.39 29.55 5.08 0.25 12029 Btu/lb 7.21 0.36Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 10 ppm 0.067 ppm 0.13 ppm 1.5 ppm 0.3 7 ppm 0.048 ppm 0.14 ppm 1.1 ppm 0.3 11 ppm 0.058 ppm 0.15 ppm 1.1 ppm 0.3Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### ppm 0.07 ppm 4 ppm 2.5 ppm 22 ppm ppm 0.06 ppm 4 ppm 2.4 ppm 14 ppm ppm 0.05 ppm 4 ppm 2.4 ppm 14 ppmNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 5 ppm 0.8 ppm 42.1 ppm 2.2 ppm 29.86 5 ppm 0.7 ppm 44.3 ppm 2.2 ppm 29.83 5 ppm 0.7 ppm 48.8 ppm 2.2 ppm 29.55 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 

### 44.03 7.06 48.91 70.46 4.80 1.00 0.38 43.73 7.20 49.07 71.53 4.88 1.49 0.39 45.37 7.21 47.42 69.67 4.72 1.00 0.36 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen



### 16.30 14.51 17.04EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 2161 James River 4 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 

### JRU4-CSR-4 6/24/2010 6/24/2010 8443.00 Btu/lb JRU4-CSR-5 6/24/2010 6/24/2010 8436.00 Btu/lb JRU4-CSR-6 6/24/2010 6/24/2010 8461.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 29.54 5.38 0.25 11982 Btu/lb 7.63 0.35 29.64 5.23 0.25 11990 Btu/lb 7.43 0.36 29.78 5.15 0.26 12049 Btu/lb 7.34 0.37Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 11 ppm 0.066 ppm 0.15 ppm 1.2 ppm 0.3 9 ppm 0.069 ppm 0.14 ppm 1.1 ppm 0.3 11 ppm 0.066 ppm 0.14 ppm 1.2 ppm 0.3Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### ppm 0.07 ppm 5 ppm 2.6 ppm 14 ppm ppm 0.07 ppm 5 ppm 2.4 ppm 16 ppm ppm 0.08 ppm 5 ppm 2.4 ppm 13 ppmNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 

### 5 ppm 0.7 ppm 45.3 ppm 2.4 ppm 5 ppm 0.7 ppm 51.0 ppm 2.1 ppm 5 ppm 0.6 ppm 47.3 ppm 2.3 ppmNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur



### 29.54 44.38 7.63 47.99 69.82 4.75 0.99 0.35 29.64 43.94 7.43 48.63 70.41 4.77 0.99 0.36 29.78 44.23 7.34 48.43 71.68 4.83 0.94 0.37 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 

### 16.46 16.04 14.84EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 2161 James River 4 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### JRU4-CSR-7 6/25/2010 6/25/2010 8477.00 Btu/lb JRU4-CSR-8 6/25/2010 6/25/2010 8411.00 Btu/lb JRU4-CSR-9 6/25/2010 6/25/2010 8501.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 29.49 5.25 0.25 12022 Btu/lb 7.45 0.36 29.98 5.1 0.25 12012 Btu/lb 7.28 0.36 29.35 5.22 0.25 12032 Btu/lb 7.39 0.36Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 29.49 29.98 29.35 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 44.71 7.45 47.84 71.13 4.75 1.50 0.36 14.81 44.94 7.28 47.78 70.67 4.73 0.97 0.36 15.99 44.53 7.39 48.08 71.37 4.81 0.93 0.36 15.14 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 2161 James River 4

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /Kg ppmUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm