### Name:

Title: Company: Sign Date: Name: Mike Taylor Title: President Company: Catalyst Air Management Sign Date: Permitted Facility Representative / Date Testing Company Representative / Date 

## KY6041 Spurlock Unit 1 Final Test Report for

/ / Based on information and belief formed after reasonable inquiry, I certify that the statements and information in this test report are true, accurate, and complete. I have reviewed all testing details and results in this test report and hereby certify that the test report is authentic and accurate.

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### KY6041 Spurlock Unit 1

Facility Information: Spurlock 1301 West 2nd st.

Maysville KY 41056 Contact: Louis Petrey Phone: 859-745-4157 ext. 204 Fax: Email: louis.petrey@ekpc.coop Testing Company: Catalyst Air Management 2505 Byington-Solway Rd

Knoxville TN 37931 Contact: Mike Taylor Phone: 865-531-0075 Fax: 831-531-0750 Email: mike.taylor@catalystair.com

Air Permit Number: 6041 Permitted Source ID/Name: Hugh L. Spurlock Generating Station 1 Permitted Maximum Process Rate: 3500 mmBtu/hr Max. Normal Operation Process Rate: Target Process Test Rate

Description of the source (including control equipment). Please see the attachments for source or process flow diagram: Industry/SCC/NAIS 221112

Sampling Location Information:

Test Parameter Information: AFS #: 110017429521 FRS #: 110017429521

SCC / Description 10100202 External Combustion Boilers - Electric Generation - Bituminous/Subbituminous Coal - Pulverized Coal: Dry Bottom (Bituminous Coal)

The following state and federal regulations that apply to the proposed testing:

Location Round

Duct Diam. Distance from upstream dist. Distance from

downstream dist. Number of

Traverse Ports Equiv. Diam Min.Travers Points Rect. Duct Length /Width KY6041 Spulock Unit 1 252 2479.2 3600 4 0 20 0 0

Target Parameter Test Method Number of

Test Runs Test Run

Duration Sample

Points Comments Location Arsenic Method 29 3 240 0 KY6041 Spulock Unit 1 Antimony Method 29 3 240 0 KY6041 Spulock Unit 1 Beryllium Method 29 3 240 0 KY6041 Spulock Unit 1



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### KY6041 Spurlock Unit 1

The following describes any modifications and/or deviations to the applicable test methods. If alternative methods were requested, see the attachments for documentation of request AND approval, including dates.

Cadmium Method 29 3 240 0 KY6041 Spulock Unit 1 Chromium Method 29 3 240 0 KY6041 Spulock Unit 1 Cobalt Method 29 3 240 0 KY6041 Spulock Unit 1 Lead Method 29 3 240 0 KY6041 Spulock Unit 1 Manganese Method 29 3 240 0 KY6041 Spulock Unit 1 Nickel Method 29 3 240 0 KY6041 Spulock Unit 1 Selenium Method 29 3 240 0 KY6041 Spulock Unit 1 Inorganic (Aqueous)

Condensible Part. Method 5/OTM-28 3 240 0 KY6041 Spulock Unit 1 Filterable Particulate Method 5/OTM-28 3 240 0 KY6041 Spulock Unit 1 Total Particulate Method 5/OTM-28 3 240 0 KY6041 Spulock Unit 1 Organic Condensible

Particulate Method 5/OTM-28 3 240 0 KY6041 Spulock Unit 1



### Monday, February 21, 2011 Page 3 of 10

### KY6041 Spurlock Unit 1

Sampling / Stack Data Results Summary


### Location KY6041 Spulock Unit 1 - Method 29 Average Run Number M29-1 M29-2 M29-3 Test Date 5/4/2010 5/4/2010 5/5/2010 Run Start Time 6:12:00 AM 11:17:00 AM 5:39:00 AM

Run Finish Time 10:25:00 AM 3:32:00 PM 9:50:00 AM Net Run Time, minutes 240 240 240 Dry Gas Meter Volume Sampled, dscf 117.424 117.115 120.552 118.364 Moisture Content of Stack Gas, % 15.24 12.24 15.19 14.223 Moisture Saturation at Stack Gas Temperature, % 15.58 15.52 15.25 15.450 Carbon Dioxide, % 10.4 10.3 10.2 10.300 Oxygen, % 8.4 8.6 8.7 8.567 Average Stack Gas Temperature, °F 129.95 129.80 129.25 129.667 Dry Volumetric Flow Rate, dry scfm 674,368.7 693,043.7 683,646.4 683,686.267 Actual Wet Volumetric Flue Gas Flow Rate, acfm 918,757.2 911,691.4 926,862.0 919,103.533 Percent Isokinetic of Sampling Rate, % 99.7 96.7 100.9 99.100 F-Factor, dscfm/MMBtu @ %O2 9780 9780 9780 9,780.000 Fw 10640 10640 10640 10,640.000 Fc 1800 1800 1800 1,800.000



### Monday, February 21, 2011 Page 4 of 10

### KY6041 Spurlock Unit 1

Location KY6041 Spulock Unit 1 - Method 5/OTM-28 Average Run Number Test Date Run Start Time Run Finish Time Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % F-Factor, dscfm/MMBtu @ %O2 Fw Fc



### Monday, February 21, 2011 Page 5 of 10

### KY6041 Spurlock Unit 1

Emissions Summary


### Location: KY6041 Spulock Unit 1 - Method 29 Compound: Antimony Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.0012 0.0012 0.0012 0.001 lb/mmBtuO2 3.68E-07 3.75E-07 3.68E-07 0.000 

### Compound: Arsenic Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.00145 0.00207 0.0012 0.002 lb/mmBtuO2 4.45E-07 6.48E-07 3.68E-07 0.000 

### Compound: Beryllium Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.0003 0.0003 0.0003 0.000 lb/mmBtuO2 9.21E-08 9.38E-08 9.19E-08 0.000 

### Compound: Cadmium Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.00043 0.0003 0.0003 0.000 lb/mmBtuO2 1.32E-07 9.38E-08 9.19E-08 0.000 

### Compound: Chromium Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.01355 0.01205 0.01101 0.012 lb/mmBtuO2 4.16E-06 3.77E-06 3.37E-06 0.000 

### Compound: Cobalt Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.0012 0.00107 0.00044 0.001 lb/mmBtuO2 3.68E-07 3.35E-07 1.35E-07 0.000 

### Compound: Lead Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.01688 0.00856 0.00711 0.011 lb/mmBtuO2 5.18E-06 2.68E-06 2.18E-06 0.000 

### Compound: Manganese Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.00948 0.00881 0.0077 0.009 lb/mmBtuO2 2.91E-06 2.76E-06 2.36E-06 0.000 

### Compound: Nickel Average


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### KY6041 Spurlock Unit 1

Process Run Data RunNumber M29-1 M29-2 M29-3 Mass_mg 0.01307 0.00839 0.01974 0.014 lb/mmBtuO2 4.01E-06 2.62E-06 6.05E-06 0.000 

### Compound: Selenium Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.0669 0.0176 0.0259 0.037 lb/mmBtuO2 2.05E-05 5.51E-06 7.94E-06 0.000


### Location: KY6041 Spulock Unit 1 - Method 5/OTM-28 Compound: Filterable Particulate Average RunNumber M5-28-1 M5-28-2 M5-28-3 Mass_mg 19.9 12.6 12.9 15.133 lb/mmBtuO2 4.76E-03 3.11E-03 3.18E-03 0.004 

### Compound: Inorganic (Aqueous) Condensible Pa Average RunNumber M5-28-1 M5-28-2 M5-28-3 Mass_mg 34 32 34 33.333 lb/mmBtuO2 8.13E-03 7.90E-03 8.39E-03 0.008 

### Compound: Organic Condensible Particulate Average RunNumber M5-28-1 M5-28-2 M5-28-3 Mass_mg 1 1.3 1.4 1.233 lb/mmBtuO2 2.39E-04 3.21E-04 3.45E-04 0.000 

### Compound: Total Particulate Average RunNumber M5-28-1 M5-28-2 M5-28-3 Mass_mg 54.9 45.9 48.3 49.700 lb/mmBtuO2 1.31E-02 1.13E-02 1.19E-02 0.012



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### KY6041 Spurlock Unit 1

Process Run Data

APCD Run Data

Process Lab Run Data 

### Run Name Value UOM Comments Target Value 1 Heat Input 2920.5 Million Btus/million BTU using O2 0 

### 2 Heat Input 2942 Million Btus/million BTU using O2 0 3 Heat Input 2957.8 Million Btus/million BTU using O2 0 1 Unit Load 293 MW 0 

### 2 Unit Load 293 MW 0 3 Unit Load 293 MW 0 1 Steam Rate 2122.3 1000 lbs/hr 0 

### 2 Steam Rate 2169.9 1000 lbs/hr 0 3 Steam Rate 2195.6 1000 lbs/hr 0



### Run Name Value UOM Comments Target Value 1 LOW NOX BURNERS 0 0 

### 4 LOW NOX BURNERS 0 0 5 LOW NOX BURNERS 0 0 

### 1 ELECTROSTATIC PRECIPITATOR 0 Volts 0 4 ELECTROSTATIC PRECIPITATOR 0 Volts 0 5 ELECTROSTATIC PRECIPITATOR 0 Volts 0 

### 1 SCR (SELECTIVE CATALYTIC REDUCTION) 398.11 lb/hr 0 4 SCR (SELECTIVE CATALYTIC REDUCTION) 377.03 lb/hr 0 5 SCR (SELECTIVE CATALYTIC REDUCTION) 386.83 lb/hr 0 

### 1 WET SCRUBBER 147.97 GPM 0 4 WET SCRUBBER 213.39 GPM 0 5 WET SCRUBBER 186.43 GPM 0 

### 1 WET ELECTROSTATIC PRECIPITATOR 0 Volts 0 4 WET ELECTROSTATIC PRECIPITATOR 0 Volts 0 5 WET ELECTROSTATIC PRECIPITATOR 0 Volts 0

Run Name Value UOM Comments 

### 1 0

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### KY6041 Spurlock Unit 1

Sampling / Stack Data Results Detail


### Location KY6041 Spulock Unit 1 - Method 29 Average Run Number M29-1 M29-2 M29-3 Test Date 5/4/2010 5/4/2010 5/5/2010 Run Start Time 6:12:00 AM 11:17:00 AM 5:39:00 AM Run Finish Time 10:25:00 AM 3:32:00 PM 9:50:00 AM Net Traversing Points 20 20 20 Net Run Time, minutes 240 240 240 Nozzle Diameter, inches 0.215 0.215 0.215 0.215 Pitot Tube Coefficient 0.84 0.84 0.84 0.840 Dry Gas Meter Calibration Factor 1 1 1 1.000 Barometric Pressure, inches of Mercury 29.01 29.01 29.1 29.040 Average Orifice Meter Differential, inches H2O 0.84 0.85 0.87 0.853 Dry Gas Meter Volume Sampled, cubic feet 123.180 124.102 125.563 124.282 Average Dry Gas Meter Temperature, °F 78.18 83.65 76.05 79.293 Dry Gas Meter Volume Sampled, dscf 117.424 117.115 120.552 118.364 Total Moisture Liquid collected, g 448.6 347.1 458.6 418.100 Volume of Water Vapor, standard cubic feet 21.12 16.34 21.59 19.683 Moisture Content of Stack Gas, % 15.24 12.24 15.19 14.223 Moisture Saturation at Stack Gas Temperature, % 15.58 15.52 15.25 15.450 Dry Mole Fraction 0.8476 0.8776 0.8481 0.858 Carbon Dioxide, % 10.4 10.3 10.2 10.300 Oxygen, % 8.4 8.6 8.7 8.567 Carbon Monoxide & Nitrogen, % 81.2 81.1 81.1 81.133 Fuel Factor 1.20 1.19 1.20 Dry Molecular Weight, lb/lb-Mole 30.00 29.99 29.98 29.990 Wet Molecular weight, lb/lb-Mole 28.17 28.52 28.16 28.283 Flue Gas Static Pressure, inches of H2O -0.75 -0.75 -0.75 -0.750 Absolute Flue Gas Pressure, inches of Mercury 28.95 28.95 29.04 28.980 Average Stack Gas Temperature, °F 129.95 129.80 129.25 129.667 Average Velocity Head, inches of H2O 0.5239605235 76026 0.522409933

269197 0.535407900

093508 0.527
Average Stack Gas Velocity, feet/second 44.21 43.87 44.60 44.227 Stack Cross-Sectional Area, square feet 346.361 346.361 346.361 346.361 Dry Volumetric Flow Rate, dry scfm 674,368.7 693,043.7 683,646.4 683,686.267 Actual Wet Volumetric Flue Gas Flow Rate, acfm 918,757.2 911,691.4 926,862.0 919,103.533 Percent Isokinetic of Sampling Rate, % 99.7 96.7 100.9 99.100 Percent Excess Air, % 64.4 67.1 68.4 66.633 F-Factor, dscfm/MMBtu @ %O2 9780 9780 9780 9,780.000 Round Duct Diameter, inches 252 252 252 Rectangular Duct Width, inches 0 0 0 Rectangular Duct Length, inches 0 0 0 Fw 10640 10640 10640 10,640.000 Fc 1800 1800 1800 1,800.000



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### KY6041 Spurlock Unit 1

Location KY6041 Spulock Unit 1 - Method 5/OTM-28 Average Run Number Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches Fw Fc



### Monday, February 21, 2011 Page 10 of 10