SANITIZED SUBMISSION 11II1111111111111111111111111111 11111111 PMN2010P1 

### PMN Page 1
,.---------_. Form Approved. O.M.B. Nos. 2070-0012 and 2070·0038 AGENCY USE ONLY ! 

## u.s. ENVIRONMENTAL PROTECTION AGENCY 

# -/0**P~r::MAt.JIII:A("TllgC** Date of receipt: 

# 51110000128 P·11·01 

# Ep, 111111111111111111111111111 111111111111111111111111111111111111111111111111 51110000 1 281$ 

### Submission

....onl"\'" 

### Number

K944HX
must I this form to the extent that it IS known i by you. Make reasonable estimates Ifyou 00 nothaye actual data. • Before you complete thisform. you should read the "Instructions Manual for Premanufacture Notification" (the Instructions Manual is availablefrom the Toxic Substances Control Act (,:,SCA) Information Sef'llce by calling 202-554-1404. orfaxing 202-554-5603) If a user fee has been remitted for this nollce (40 CFR 700.45). indicate in Iheboxes aboye Ihe TS-userfee**ident~lca!ion** numberyou have generated Remember. your user fee ID number must also appear on your corresponding fee remittance For mailing address information see the Help instructions In the e-PMN tool. Part 1- GENERAL INFORMATION You must provide the currently correct Chemical Abstracts (CA) Name ofthe new chemical substance, even if you claim the identity as confidentiaL You may authorize another person to submit chemical identity information for you, butyour submission will not be complete and the review will not begin until EPA receives this information. A letter in support of your submission should reference your TS userfee identification number. For all Section 5 Notice submissions (paper or electronic) you must submit an original notice including all test data; ifyou claimed any information as confidential. an original sanitized copy must also be submitted. Part 11- HUMAN EXPOSURE AND ENVIRONMENTAL RELEASE If there are several manufacture, processing, or use operationsto be d"scribed in Part II, sections A and B ofthis notice, reproduce the sections as needed. Part 111- LIST OF ATTACHMENTS For paper submissions. attach additional sheets ifthere is not enough space to answera questionfully. Label each continuation sheet with tlhe corrt!sponding section heading. In Part III, listthese attachments, anytest data orother data and any optional information included in the notice. OPTIONAL INFORMATION You may include any information that you want EPAto conSider in evaluating the newsubstance. On page 11 ofthis form, space has been provided for you to describe pollution prevention and recycling information you may have reg:;!rding the new substance. "Binding" boxes are included throughout this form for you to indicate your willingness to be bound to cenain statements you make in this section, such as use. production volume, protective equipment.
.The intention is to reduce delays tlhat routinely accompany the development of consent orders or :>ignificant New Use Rules. Checking a "binding" box in a PMN does not by itself prohibit the submitterfrom later deviatIng from the infor,nation (except chemical identity) reported in the form; however, In tlhe case of exemption applications (such as TMEA, LVE, LOREX) certain information provided in such notifications IS binding on**:~e** submitterwhen the Agency approves the exemption application, especially ifthe production volume "binding" box is chosen in a LVE. CONFIDENTIALITY CLAIMS You may claim any information In this notice as confidential. To assert a claim on the form, mark (X) the confidential box next to the Information that you claim as confidentiaL To assert a claim in an attachment circle or bracket the information you claim as confidential. Ifyou claim information in the notices as confidential you must also provide a sanitized version ofthe notice (including attachments) For additional instructions on claiming information as confidential. read the Instructions Manual. TEST DATAAND OTHER DATA You are required to submit all test data in your possession orcontrol and to provide a description ofall otherdata known toor reasonably ascertainable by you. if these data are related tothe health and environmental effects on the manufacture, processing. distribution in commerce, use, ordisposal of the new chemical SUbstance. Standard literature citations may be submitted fordata in the open scientific literature. Complete test data (wrillen in English) not summaries ofdata, must be submitted ifthey do not appear in the open literature. You should clearly identify whethertest data is on the substance oron an analog. Also. tlhe chemical composition ofthe tested material shOuld be characterized. Following are examples oftest data and other data. Data should be submitted according to the requirements of §720.50 ofthe Premanufacture Notnication Rule (40 CFR Part 720). Test Data (Check Belowany included in this notice) Environmental fate data Other Data 

# W Health effects data Risk Assessments 

# D EnVIronmental effects data Structure/activity relationships 

# o 0 Physical/Chemical Properties (A physical and chemical properties worksheet is 

# o located on the last page ofthis form.) 

# D Test data not in the possession or control mthe submitter TYPE OF NOTICE (Check Only One) PMN (Premanufacture Notice) 

# D SNUN (Significant New Use Notice) TMEA (Test Marketing Exemption Application)**'.,~** 

# D 

# . D LVE (Low Volume Exemption)@40CFR 723.50(c)(1) 

# D LOREX (Low Release/Low Exposure Exemption)@ 40 CFR 723.50(c)(2) 

# D LVE Modification 

# D LOREX Modification Mock Submission Mark (X) ifpending LetterofSupport :S THIS A CONSOLIDATED PMN (Y/N)?

/I ofchemicals or polymers (Prenotice Communication # required. enter # on p. J) information in this notice is claimed asconfidential. EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions of EPA Form 7710-25 Page 1 

# P·II-OU8SANITIZED SUBMISSION 1111111111111111111111111111111111111111111111111111111 PMN2010P2 

### PMN Page 2

Include the OMB The public reporting and recordkeeping burden for this collection of information is estimated to average 93 hours pe comments on the Agency's need for this information, the accuracy ofthe provided burden estimates, and any sugg minimizing respondent burden, including through the use ofautomated collection techniques to the Director, Collect Division, U.S. Environmental Protection Agency (2822T), 1200 Pennsylvania Ave., NW, Washington, D.C. 20460. control number in any correspondence. Do not send the completed EPA Form 7710-25 to this address. 

### CERTIFICATION -- A printed copy ofthis signature page, with original signature, must be sub with CD or paper submission. ested methods for r response. Send ion Strategies


### mitted I certify thatto the best of my knowledge and belief: 1. The company named in Part I, section A, subsection 1a ofthis noticeform intends to

manufacture, import or process for a commercial purpose, other than in small quantities sole research and development, the substance identified in Part I, Section B. 2. All information provided in this notice is complete and truthful as ofthe date ofsubmission. 3. 1

### am submitting with this notice all test data in my possession or control and a description of

otherdata known to or reasonably ascertainable by me as required by §720.50 ofthe Premanufacture Notification Rule. Additional Certification Statements: Ifyou are submitting a PMN, Intermediate PMN, Consolidated PMN, or SNUN, check the following userfee ly for

all

• certification statementthat applies: f-------------------------------- ------..--..-- ..-----j 

## [Xl The Company named in Part I, Section A has remitted the fee of$2500 specified in 40 CFR 700.45(b), or The Company named in Part I, Section A has remitted the fee of$1000 for an Intermediate PMN (defined @40 CFR 700.43) in accordance with 40 CFR 700.45(b), or The Company named in Part I Section A is a small business concem under 40 CFR 700.43 and has remitted a fee of $100 in 

# o accordance with 40 CFR 700.45(b). 

### Ifyou are submitting a LowVolume Exemption (LVE) application in accordance with 40 CFR 723.50(c)(1) or a Low Release and Low Exposure Exemption (LoRex) application in accordance with 40 CFR 723.50(c)(2), check the following certification statements: The manufacturer submitting this notice intends to manufacture or importthe newchemical substancefor commercial purposes, 

# o otherthan in small quantities solely for research and development, underthe terms of40 CFR 723.50. The manufacturer is familiarwith the terms ofthis section and will comply with those terms: and 

# o The newchemical substanceforwhich the notice is submitted meets all applicable exemption conditions. Ifthis application is for an LVE in accordance with 40 CFR 723.50(c)(1), the manufacturer intends to commence manufacture of 

# o the exempted substance for commercial purposes within 1 year ofthe date ofthe expiration ofthe 30 day review period.

EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions of EPA Form 7710-25 Page 2SANITIZED SUBMISSION 1111111111111111111III1111111111111111111111IIII11I1111 PMN2010P3



# D

D

Mailing Address (number & street) City Postal Code

(last) Van Norstrand 

# D Peveler

Position Company Eastman Kodak Mailing Address (number & street) City Rochester e-mail judith.vannorstrand@kodak.com 

### 3. Ifyou have had a prenotice communication (PC this notice and EPAassigned a PC Numberto


### 4. enterthe number. the notice, ) concerning
the 

## xxx

Ifyou have submitted a notice of Bona fide intent to 

### 5. manufacture orimport for the chemical substance covered by this notice, enterthe notice number assigned by EPA. 

# D
Manufacture Only 

# D i 3. Both 1. Binding Option 

# D EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions of EPA Form 7710-25 Page 3SANITIZED SUBMISSION 1111111111111111111111111111111111111111111111111111111
You must provide a currently correct Chemical MlJ:>"<''''l> based on current CA index nomenclature ,..n,w"nli/,n<:. Mark (X) the "Confidential" box next to any item you claim as confidential 

### r-···

. Complete either item 1 (Class 1 or 2 substances) or2 (Polymers) as appropriate. Complete all other items.

Ifanother person will submit chemical identity information for you (for either Item 1 or 2), mark (X) the box at the right. Identify 

# D I the name, com an ,and address ofthat erson in a continuation sheet. 1. Class 1 or2 chemical substances (for definitions ofclass 1 and class Class 1 Class 2 2 substances, seethe Instructions Manual) a. Class ofsubstance - Mark (X) 

# D 

# D b. Chemical name (Currently correct Chemical Abstracts (CA) Name that is consistent with TSCA Inventory listings for similar substances. ForClass 1 substances a CA Index Name must be provided. For Class 2 substances either a CA Index Name or CA Preferred Name must bEl providEld, which ever is appropriate based on current CA index nomenclature rules and conventions). 3H-lndolium, 2-[2-r3-[2-(1 ,3-dihydro-1 ,3,3-trimethyl-2H-indol-2-ylidene)ethylidene]-2-[1-(phenyl-1Htetrazol-5-yl)thio]-

### f-cyclohexen-1-yl]ethenyl]-1,3,3-trimethyl-. cflloride 

# D

I CAS Registry Number (if a number already exists for the substance) 440102-72-7 I c. Please identiJ}' which method you used to devE!lop or obtain the specified chemical identity information reported in this notice: (check one). Method 1 (CAS Inventory Expert Service - a copy ofthe 

# [X] IES Order 

### I Method 2 

# D I Identification report obtained from the CAS Inventory Expert Number ' (Other 

# I**~rvices** must be submitted as an attachmentto this notice) 102995-2 , Source) EnterAttachment filename for Part I, Section B, 1. c. 

# D d. Molecular formula 

# IC39 H41 N6 S . CI 

# D e. For a class 1 substance. provide a complete and correct chemical structure diagram. Fora class 2 substance, provide a correct 

# D representa!ive or partial chemical structure diagram,as complete as canbe known, ifone can be reasonably ascertained. 

### I i 

### i

EPA FORM 7710-25 (Rev. 6-09) Replaces previOUS editions of EPA Form 7710-25 Page 4SANITIZED SUBMISSION 1111111111111111111111111111111111111111111111111111111II111 PMN2010P4A

_________**~P_M_N_Page** 

### 4a i For a class 2 substance (1) listthe immediate precursor substances with their respective CAS Registry Numbers. (2) Describe

. the nature ofthe reaction orprocess. (3) Indicate the range ofcomposition and the typical composition (where appropriate). Confidential 

# I

__. ____'---

___-1 e. (1) listthe immediate precursor substance names with their respective CAS Registry Numbers.

EnterAttachment filename for Part I. Section B. 1. e. (1) 

# I 

# [ 

# ]
e. (2) Describe the nature ofthe reaction or process. 

# D

EnterAttachment filename for Part I. Section B. 1. e. (2) 

# I 

# D
e. (3) Indicate the range ofcomposition and the typical composition (where appropriate). 

# D

Attachmentfilename for Part I. Section B.
EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions of EPA Form 7710-25 Page 5SANITIZED SUBMISSION 1111111111111111111111111111111111111111111111111111111 PMN2010P5 

## PMN Pag;;;t.!l-=-::5
_______ _____**~_---, ·---P-a-rt-I----G~E=N~E=RA=--:c-L** 

## INFORMATION - Continu=-=e-=d

_______**~** Section B -- CHEMICAL IDENTITY INFORMATION -- Continued 2. Eolymerl) (For a definition of polymer, see the Instructions Manual.)
. ..___•.

__... 

## I Confidential a. Indicate the number-average weight ofthe lowest molecularweight composition ofthe polymeryou intend to manufacture.**~.** Indicate maximum weight percent of lowmOlec.ularweight species (not including residua.I monomers, reactants, orsolvents) I 

# 0 i below 500 and below 1,000absolute molecularweight ofthat composition.
. ..._______ . Describe the methods of measurement orthe basis foryourestimates: 

### t-G-PC------=O==---rl-O-t-he-r-(-SP-e- 

# 0
---------.. cify Below) 

# I Specify Other:

(i) lowest number average molecular 

# I (ii) maximum weight % below 500 molecular (iii) maximum weight % below 1000 molecular I weight: weight: weight: i I ! EnterAttachment filename for Part I, Section B, 2. a. 

### I 

## [ I b. You must make separate confidentiality claims for monomer or other reactant identity, composition information, and residual information. Mark (X) the "Confidential" box nextto any item you claim as confidential

(1) Provide the specific chemical name and CAS Registry Number (ifa numberexists) ofeach monomer or other reactant used in the manufacture ofthe polymer. (2) - Mark (X) this column ifentry in column (1) is confidential. (3) - Indicate the typical weight percent ofeach monomeror other reactant in the polymer. (4) - Choose "yes"from dropdown menu ifyou want a monomer orother reactant used at two weight percent or less to be listed as part of the polymerdescription on the TSCAChemical Substance Inventory. (5) - Mark (X) this column ifentries in columns (3) and (4) are confidential. I (6) Indicate the maximum weight percentofeach monomerorother reactant that may be present as a residual in the polymeras manufactured for commercial purposes. (7) - Mark (X) this column ifentry in column(6} is confidential. Monomer or other reactant specific chemical name I Typical Include in Max CBI composition identity CBI residual CBI (2) '(3) (4) (5) (6) _(7) 

## I

CAS Registry Number (1) 

## I I I 

# I I I

CAS Registry Number (1) 

# I i 

# I 

# 1 

# 1

CAS Registry Number(1) I

CAS Registry Number (1)

the next page. EPA FORM 7710-25 (Rev, 6-09) Replaces previous editions of EPA Form 7710-25 Page 6SANITIZED SUBMISSION PMN2010P5A

# 111111111111111111111111111111111111I111111111I11~1I11111**II PMNPag~e~5_a~~~~~.**  

# __**~~~~** 

# ______--, i c. Please identify which method you used to develop or obtain the specified chemical identity information reported in this notice I· CBI

(check one). 

### Method 1 (CAS Inventory Expert Service 

# I I 

# I
.. 

# I • a copy ofthe identification report obtained 

# 0 IES Order 

# I Method 2 

# D· from CAS Inventory Expert Service must be
. Number (other source) 

# I**~ubmitted** as an attachment to this notice) L-

__________L._-;===;---',

. EnterAttachment filename for Part I, Section B, 2. c. 

# I 0 I d. The currently correct Chemical Abstracts (CAl name for the polymerthat is consistent with TSCA Inventory listings for similar ",VIY" ''''',. 

# o

I CAS Registry Number (ifa number already exists for the substance) 

# I I
! e. Provide a correct representative or partial chemical structure diagram, as complete as can be known, ifone can be reasonably ascertained. 

# o

EPA FORM 7710·25 (Rev. 6·09) Replaces previous editions of EPA Form 7710·25 Page 7

# ------------------------------- SANITIZED SUBMISSION 1111111111111111111111111111111111111111111111111111111 PMN2010P6 

### PMN Page 6**-~-P-a-rt-'I---- -=:G-=E-:-:N=E~=RA-::-::-L~IN~FO=-=R~M~A--:::T;:-:IO::-:N:-;-----::C=-o-n~ti-;-n-u-ed-;;-** **r--------------------~~--~=** 

### Section B -- CHEMICAL IDENTITY INFORMATION -- Continued 3. Impurities (a) (b) - Identify each impuritythat may be reasonably anticipated to be present inthe chemical substance as manufactured for commercial purpose. Provide the CAS Registry Number ifavailable. Ifthere are unidentified impurities, enter "unidentified." Estimate the maximumweight % ofeach impurity. Ifthere are unidentified impurities, estimate their total weight %. . ..-;---,-------1

. Impurity (a) i CAS Registry 

## I Maximum

. Number Percent % b 

## xxx xxx xxx

I Mark (X) this box ifthe data continues on the next page. 

# 0 '---. 

### .----_. Enter Attachment filename for Part I, Section B, 3. 

# D I 4. Synonyms - Enter any chemical synonyms for the newchemical identified in subsection 1or 2. None 

# D

EnterAttachmentfilename for Part I, Section B, 4. 

# I 

# D 5. Trade identification - List trade names forthe newchemical substance identified in subsection 1or 2. S 0507 

# I Cyanine dye 

# D ORM1835 i 

### I Enter Attachment filename for Part I, Section B, 5. I 

# D 6. Generic chemical name - Ifyou claim chemical identify as confidential, you must provide a generic name for your substance that reveals the specific chemical identity ofthe newchemical substance to the maximum extent possible. Refer to the TSCA Chemical Substance Inventory, 1985 Edition, Appendix Bfor guidance on developing generic names. Substituted aromatictetrazol halide

EnterAttachment filename for Part I, Section B, 6. , 

## I 7. Byproducts - Describe any byproducts resulting from the manufacture, processing, use, ordisposal ofthe new chemical substance. Provide the CAS Registry Number ifavailable. CAS Registry Number Confi­ _(2) dential

103-84-4 64-19-7 '"''''''''''""C. fI.-flh,,, ,yl·

I

i (X) data continues on the next page. 

# I ] EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions ofEPA Form 7710-25 Page 8SANITIZED SUBMISSION I1I1I1111111111111111111111111111111111111111111111111I PMN2010P7 

### PMN Page 7 Part 1-- GENERAL INFORMATION -- Continued Section C -- 

### PRODUCTION, IMPORT, AND USE INFORMATION: The information

# o~ this page refers to consolidated chemical number(s): 

# 0 1

m 

# 0 2 

# 0 304 

# 0 5 

# 0 6**.~~~~~~--~~-----** Mark (Xl the "Confidential" box nextto any item you claim as confidential. 1.**Produc-t-io-n-v-o-'-Iu-m·-e---~E-s-tim-at-e:c.;the** maximum production volume during the first 12 months ofproduction. Also estimate the maximum production volume for any consecutive 12-month period during the first three years ofproduction. Estimates should be on 100% new chemical substance basis. Fora LowVolume Exemption application, ifyou chooseto have your notice reviewed at a lower production VOlume than 10,000 kg/yr, specifythe volume and mark (x) in the binding box. Ifgranted, you are bound to this volume. Maximum first 12-month production (kg/yr) Maximum 12-month production (kg/yr) Confidential Binding Option 

# I

I· (100% newchemical substance basis) • (100% new chemical substance basis) Mark (X)

### --~--~-~--~--O--~I 

## ixxx xxx**~--------~----- ~==,---~** **~.------------------------------------~------~------------------------** EnterAttachment filename for Part I, Section C, 1. CBI 

# o 2. Use Information -- You must make separate confidentiality claims for the description ofthe category of use, the percent ofproduction volume devoted to each category, the formulation ofthe new substance, and other use information. Mark (X) the "Confidential" Box nextto any item you claim as confidential. a. (1) --Describe each intended category ofuse ofthe newchemical substance by function and application. (2) --Mark (X) this column ifentry column (1) is confidential business information (CBI). (3) --Indicate your willingness to havethe information provided in column (1) binding. (4) --Estimate the percent oftotal production for the first three years devoted to each category ofuse. (5) --Mark (X) this column ifentry in column (4) is confidential business information (CBI). (6) --Estimatethe percent ofthe newsubstance as formulated in mixtures, suspensions, emulsions, solutions, orgels as manufactured for commercial purposes at sites underyour control associated with each category of use. (7) --Mark (X) this column ifentry in column (6) is confidential business information (CBI). (8) --Indicate % of productvolume expected for the listed "use" sectors. Mark more than one box ifappropriate. Mark (X) to indicate your willingness to havethe use type provided in (8) binding. (9) --MarklX) this column ifentrv(ies) in column (8) is (are) confidential business information (CB!). I Category of use (1) Binding Prod ' % in 

# I • (by function and application Le. a dispersivedyefor 

### I CBI Option uction CBI i· Form- 

# I finishing polyesterfibers) !Mark (X) • % ulation (2) (3) (4) (5) (6) 

### XXX

XXX 

## x XXX CBI (7) 

# x

x

i 

### I 

# l I 

# 1 T % ofsubstance expected per use Ii I, (8) CBI Com­ Bioding !

### Si~e. I Con- ! Industrial 1imited i**$Umer~** rner<:ial Option (9) 

### XXX XXX

# IXXX

# T XXX 

# I x

i 

### XXX IXXX XXX XXX X i i 

# I i

i 

# I i 

### I 

# I t-----.---..------ 

### ·----+-----r----+--.J--,----,----I--+---+I---+---...L-+---I 

# I I !

# ~___:__:_:_~_o",,--:-----":-:-i --l...-....I. :

... 

# I

. i I 

### I 

# I * Ifyou have identified a "consumer" use, please provide on a continuation sheet a detailed description ofthe use(s) ofthis chemical substance in consumer products. In addition include estimates ofthe concentration ofthe new chemical substance as expected in consumer products and describe 

### I • the chemical reactions bywhich this substance loses its identity in the consumer product. i Mark (X) this box ifthe data continues on the next page. 

# o b. Generic use Ifyou claim any category of use description in subsection 2a as confidential, enter a genericdescription ofthat category. 

# I description Read the Instruction Manual for examples ofgeneric use descriptions. i Contained use in an article 

### I Export. EnterAttachment filename for Part I, Section C, 2. b. 

# I I CBI 

# D

3. Hazard Information -- Include in the notice a copy of reasonable facsimile of any hazard warning statement, label, material safety

data sheet, or other information which will be provided to any person who is reasonably likely to be exposed to this substance Binding Option regarding protective eqUipment or practices for the safe handing, transport, use, ordisposal ofthe newsubstance. List in part III Mark (X) hazard information you include. 

### i Mark (X) this box ifyou attach hazard information. 

# 1X1 D EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions of EPA Form 7710-25 Page9 i



### iSANITIZED SUBMISSION 11111111111111111111111111111111 11111111111 PMN2010P8 

### PMN Page 8 Part 11-- HUMAN EXPOSURE AND ENVIRONMENTAL RELEASE

. Section A -- INDUSTRIAL SITES CONTROLLED BY THE SUBMITTER

The information on pages 8and 8a referto consolidated chemical number(s): 

### 1 

# D2 Complete section A for each type of manufacture, processing, or use operation involving the new chemical substance at industrial sites • you control Importers do not have to complete this section for operations outside the US' however you may still have reporting ., ,

i requirements ifthere are further industrial processing or use operations after import. You mustdescribe these operations. See

instructions manual 1. Operation description Confia.ldentity -­ Enterthe identity ofthe site atwhich the operation will occur. dential Name 

# IEastman Business Park Site address (number and 11669 Lake Avenue street) 

# D City 

### IRochester County IMonroe State INY ZIP code 114652 Ifthe same operation will occur at more than one site, enterthe numberofsites. Identifythe additional sites on a continuation sheet, and ifany ofthe sites have significantly different production rates or 

### I 

### 1 -pperations, include all the information reguested in thissection for those sites as attachments.**~** Mark (X) this box ifthe data continues on the next page. 

# D b. Type-­ Manufacturing 

# D Processing 

# D Use 

# D [K] Mark (X) c. Amount and Duration Complete 1 or 2 as appropriate Confidential Maximum kg/batch (100% new chemical Hours/batch Batches/year 

# [K] 1. Batch substance) XXX XXX XXX Maximum kg/day Hours/day Days/year (100% new chemical substance) 

# D Mark (X) to indicate your willingness to 

# D d. Process description have your process description binding.**~** 

# I I

(1 ) Diagram the major unit operation steps and chemical conversions. Include interim storage ancitransport containers (specify- e.g. 5 gallon i palls, 55 gallon drum, rail car, tank truck, etc.). (2) Provide the identity, the approximate weight (by kg/day or kg/batch on a 100% new chemical substance basis), and entry point ofall starting materials and feedstocks (including reactants, solvents, catalysts, etc.), and of all products, recycle streams, and wastes. Include cleaning chemicals (note frequency ifnot used daily or per batch.). (3) Identify by numberthe points of release, including small or intermittent releases, to the environment ofthe new chemical substance. If releasin to tW0rTledia at the same step, assign a second release numberforthe second medium
...-----------;==.---I 

# [Xl XXX

EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions of EPA Form 7710-25 Page 10SANITIZED SUBMISSION

# IIIIIIIIIIIIIIIIIIIIIIIIIIIII~IIIIIIIIIIIIIIIIIIIIIIIIII**III** PMN2010P8A 

### PMN Page 8a Diagram ofthe major unit operation steps.

EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions of EPA Form 7710-25 Page 11SANITIZED SUBMISSION 1111111111111111111111111111111111111111111111111111111 PMN2010P9 

## PMN Pa e 9 k=.Part 11-- HUMAN EXPOSURE AND ENVIRONMENTAL RELEASE - Continued • Section A -- INDUSTRIAL SITES CONTROLLED BY THE SUBMITTER -- Continued 

### :==----­

The information on pages 9 and 9a referto consolidated chemical number(s): 

# 0 1 

# 0 2 

# 0 3 

# 0 4
...... 

# 0=,-5

__=0=--_6
__ 2. Occupational Exposure -- You must make separate confidentiality claims forthe description ofworker activity. physical form of the newchemical

substance, number ofworkers exposed, and duration of activity. Mark (X) the ·Confidential" box nextto any item you claim as confidential.

(1) -- Describe the activities (Le. bag dumping, tote filling. unloading drums. sampling, cleaning, etc.) in which workers may be exposed to the substance. (2) Mark (X) this column ifentry in column (1) is confidential business information (CSI). (3) -- Describe any protective equipment and engineering controls used to protectworkers. (4) and (6) -- Indicate yourwillingness to have the information provided in column (3) or (5) binding. (5) -- Indicate the physical form(s) ofthe newchemical substance (e.g., solid: crystal, granule. powder, or dust) and % new chemical substance (if 

# I part ofa mixture) at the time ofexposure. (7) -- Mark (X) this column ifentries in columns (3) and (5) are confidential business information (CSI). • (8) -- Estimate the maximum number ofworkers involved in each activity for all sites combined. (9) Mark (X) this column ifentry in column (8) is confidential business information (CBI). ) f (10) and (11 Estimatethe maximum duration 0 the activityfor any worker in hours per day and days peryear. (12) -­ Mark (Xlthis column ifentries in columns (10) and (11) are confidential business information (CBI). Workeractivity Protective Equipment! Binding Physical Binding #of Maximum Duration (i.e., bag dumping, filling CBI Option form(s) Option CBI Workers CBI CBI drums) Engineering Controls Mark (X) &%new Mark (X) Exposed

(i) (2) (3) (4) substance (6) (7) (8) (9) Hrs/Day DaysNr (12) i (6) (10) (11) Addition ofseed crystal to see MSDS ·Solid, 100% 1 0.04 13 reaclor ! i 

# I Handling and cleaning of 

### I Isee MSDS •Paste, -50% 

# I 1 

### I 0.5 

### I 13 • filter i i i i 

### i

Treatment ofwaterllPA see MSDS Liquid 1 

### I 0.5 i 13 

# I liquors from reaction with i sodium hypochlorite i 

# I I i 

### I I 

### I ! Collection ofcrude see MSDS •Paste. -50% 1 i 2 13
, product i i 

### i

---­ 

### i Addition ofdamp crude i see MSDS Paste, -50% i 1 1 0.5 13 i productto reactor 

### I i 

### I I i i i 

### I 

# I I i 

# , 'see I 

# I I ! i ; to trays i

Transfer to dried product see MSDS Solid,100% i 13 from trays to grinder Grinding of final product see MSDS Solid,100% 13 

# I Packaging ofground see MSDS Solid, 100% 0.5 13

product

Attachmentfilename for Part II, SectionA on the bottom ofpage 9a.

EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions of EPA Form 7710-25 Page 12SANITIZED SUBMISSION 111111111111111111111111111111111111111111111111111111111111 PMN2010P9A 

### PMN Paae Sa 3. Environmental Release and Disposal You must make separate confidentiality claims for the release number and the amount ofthe new chemical substance released and other release and disposal information. Mark (X) the "Confidential" box next to each item you claim as confidential. (1) -­ Enterthe number ofeach release point identified in the process description. part II. section A, subsection ld(3). (2) Estimate the amountofthe new substance released (a) directly to the environment or (b) into control technology (in kg/day or kg/batch). (3) -­ Mark (X) this column ifentries in columns (1) and (2) are confidential business information (CBI). (4) -­ Identify the media (stack air. fugitive air (optional-see Instruction Manual). surface water. on-site or off-site land or incineration. POTW. or other (specify» to which the newsubstance will be released from that release pOint. (5) -­ a. Describe control technology. ifany. and control efficiency that will be used to limitthe release ofthe newsubstance to the environment. For releases disposed of on land. characterize the disposal method and state whether it is approved for disposal of RCRA hazardous waste. On a continuation sheet. for each site describe any additional disposal methods that will be used and whetherthe waste is subject to secondary ortertiary on-site treatment. b. Estimate the amount released to the environment after control technology (in kg/day). (6) Mark (X) this column ifentries in columns (4) and (5) are confidential business information (CBI). (7) Identify the destination(s) of releases to water. Please supply NPDES (National Pollutant Discharge Elimination System) numbers for direct discharges or NPDES numbers ofthe POTW (Publicly Owned Treatment Works). Mark (X) ifthe POTW name or NPDES# is confidential business information (CBI). Release Amount of New Medium ofrelease Controltechnology and efficiency (you maywish to Number Substance Released CBI e.g. Stackair optionally attach efficiency data) CBI Binding (1) (2a) (2b) (3) (4) (Sa) Mark (5b) (6) I (Xl ! 

# I i 1 0.05 :Other: Landfill I I 0.1 Other: Landfill i i I 

### I < 1 kg Other: Wastewatertreatment See continuation page. id: I <0.1 kg i
I 

### I plant :<P9ASA3(5a)C1R3> 

# I i Other: Wastewatertreatment 4 < 1 kg See continuation page. id: 

### I < 0.1 kg plant <P9ASA3(5a)C1 R4> i 5 < 1 kg 

### I IOther: Landfill 

# I !

# Iincineratio~ 6 

# I I < 10 kg
.Off-site Incineration 0

7 

# I < 1 kg Other: Landfill 

# I I 8 i < 2 kg Other: Wastewatertreatment See continuation page. id: < 2 kg 

### I plant <P9ASA3(5a)ClR8> 

### I 9 IOff-,'to I"

# 'c."boo Incineration 0 i

I I 

### I I ! Mark (X) this box ifthe data continues on the next page. 

# [R] i 

### (7) Mark (X) the destination(s of releases to water. 

## I NPDES# CBI ! i 

# 0 POTW·-provide i name(s) 

# I i I 

### I Genesee River after wastewater treatment plant : 

### I 

# [R] Navigable waterway- NY-000-1643 

# 0

- provide name(s) 

### I I 

# 0 Enter Attachment filename for Part II, SectionA. 

# I 

# 0 EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions of EPA Form 7710-25 Page 13SANITIZED SUBMISSION 11111111111111111111111111111111 11111111111111111111111111 PMN2010P9A-1 3. Environmental Releaseand Disposal - You must make separate confidentiality claims for the release number and the amount ofthe newchemical substance released and other release and disposal information. Mark (X) the "Confidential" box next to each item you claim as confidential. (1) Enterthe numberofeach release point identified in the process description, part II, section A, subsection 1d(3). (2) Estimate the amount ofthe newsubstance released (a) directly to the environment or (b) into control technology (in kg/day or kg/batch). (3) -­ Mark (X) this column ifentries in columns (1) and (2) are confidential business information (CBI). (4) Identifythe media (stack air fugitive air (optional-see Instruction Manual) surfacewater on-site or off-site land or incineration POTW or other (specify)} to which the new substance will be released from that release point. (5) -­ a. Describe control technology, if any, and control efficiencythat will be used to limitthe release ofthe newsubstance to the environment. For releases disposed ofon land, characterize the disposal method and statewhether it is approved for disposal of RCRA hazardous waste. On a continuation sheet. for each site describe any additional disposal methods that will be used and whetherthe waste is subjectto secondary ortertiary on-sitetreatment. b. Estimatethe amount released to the environment after control technology (in kg/day). (6) Mark (X) this column ifentries in columns (4) and (5) are confidential business information (CBI). (7) Identifythe destination(s) of releases to water. Please supply NPDES (National Pollutant Discharge Elimination System) numbers for direct discharges or NPDES numbers ofthe POTW (Publicly Owned TreatmentWorks). Mark (X) ifthe POTWname or NPDES# is confidential business information (CB!). Release Amount of New Medium of release Controltechnology and efficiency (you maywishto Number Substance Released CBI e.g, Stack air optionally attach efficiency data) CBI Binding (1) (2a) (2b) (3) (4) (Sa) Mark (5b) (6) (Xl 1a 0.05 kg Off-site Incineration Incineration 0
2a 0.1 kg Off-site Incineration Incineration 0
Sa < 1 kg Off-site Incineration Incineration 0
7a < 1 kg Off-site Incineration Incineration 0

Mark (X) this box ifthe data continues on the next page. 

# D (7) Mark (X) the destination(s of releases towater. NPDES# 

### eBI



# D POTW--provide 

# D name(s) 

# D Navigable waterwayprovide name(s)

• 

# D 

# D Other--Specify 

# D I

• EnterAttachment filename for Part II. Section A. 

### 1 

# D EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions of EPA Form 7710-25 Page 141111111111111111111111111111111111111111111111111111111111111111111111 SANITIZED SUBMISSION PMN2010P9A-2 

## Continuation Sheet ID

# I P9ASA3(5a)C1R3 

# I Field

# I Part II. Section A. B.(5a) Control Technology & Efficiency. Row 3 Reaction with sodium hypochlorite to decompose PMN substance. The treated solution is sent to an on-site wastewater treatment plant and then to an industrial sewer.

EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions of EPA Form 7710-25 Page 1511111111111111111111111111111111 11111111111111111111111111 SANITIZED SUBMISSION PMN2010P9A-3 

## Continuation Sheet In

# I P9ASA3(5a)C1 R4 

# I Field

# I Part II, Section A, B.(5a) Control Technology & Efficiency, Row 4 Reaction with sodium hypochlorite to decompose PMN substance. The treated solution is sent to an on-site wastewatertreatment plant and then to an industrial sewer.

EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions of EPA Form 7710-25 Page 1611111111111111111111111111111111111111111111111111111111I1111111111111 SANITIZED SUBMISSION PMN2010P9A-4 

## Continuation Sheet ID

# I P9ASA3(5a)C1R8 

# I Field

# I Part II, Section A, B.(5a) Control Technology & Efficiency, Row 8 Aqueous streams generated from manufacturing operations orfinal equipment rinsing operations that may contain small amounts ofthe PMN substance will undergo on-site biological wastewater treatment, and sludge will be disposed of in compliance with applicable regulations; Treated process streams will be released via plant sewer lines

EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions of EPA Form 7710-25 Page 17SANITIZED SUBMISSION 11111111111111111111111111111111 111111111111111111111 PMN2010P8X1 

### PMN Page 

## 8 Part 11-- HUMAN EXPOSURE AND ENVIRONMENTAL RELEASE Section A -- INDUSTRIAL SITES CONTROLLED BY THE SUBMITTER 

### I Mark (X) the "Confidential" box nex1 to any item you claim as confidential The information on pages 8 and 8a referto consolidated chemical number(s): 

# 01 02 03 04 Os 

# 06 Complete section A for each type of manufacture, processing, or use operation involving the new chemical substance at industrial sites you control. Importers do not have to complete this section for operations outside the U.S.; however, you may still have reporting requirements ifthere are further industrial processing or use operations after import. You must describe these operations. See instructions manual 1. Operation description Confia. Identity -­ Enterthe identity ofthe site atwhich the operation will occur. dential Name Graphics Communications Group of Eastman Kodak Company Site address (number and street) One Polychrome Park, Corporate Ridge Industrial Park 

# 0 City Columbus County Muscogee State GA ZIP code 31907 Ifthe same operation will occur at more than one site, enter the number ofsites. Identify the additional 

# 0 sites on a continuation sheet, and if any ofthe sites have significantly different production rates or 

### 1 operations, include all the information requested in this section for those sites as attachments. -7 Mark (X) this box ifthe data continues on the next page. 

# 0 b. Type-­ Manufacturing 

# 0 Processing 

# [XJ Use 

# 0 0 Mark (X) c. Amount and Duration -­ Complete 1 or 2 as appropriate Confidential Maximum kg/batch (100% new chemical Hours/batch Batches/year 

# 0 1. Batch substance) Maximum kg/day Hours/day Days/year 2. Continuous (100% new chemical substance) 

# [XJ XXX XXX XXX Mark (X) to indicate your willingness to 

# 0 d. Process description have your process description binding. -7 (1) Diagram the major unit operation steps and chemical conversions. Include interim storage and transport containers (specify- e.g. 5 gallon pails, 55 gallon drum, rail car, tank truck, etc.). (2) Provide the identity, the approximate weight (by kg/day or kg/batch on a 100% new chemical substance basis), and entry point of all starting materials and feedstocks (including reactants, solvents, catalysts, etc.), and of all products, recycle streams, and wastes. Include cleaning chemicals (note frequency ifnot used daily or per batch.). (3) Identify by numberthe points of release, including small or intermittent releases, to the environment ofthe new chemical substance. If releasing to two media at the same step, assign a second release numberfor the second medium. 

# 0 See Processing Diagram Attachment

EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions of EPA Form 7710-25 Page 18SANITIZED SUBMISSION 1111111111111111111111111111111111111111111111111111111111111111111111 PMN2010P8AX1 

### PMN ofthe major unit operation steps.

Attachmentfilename for Part II,
EPA FORM 7710-25 (Rev 6-09) Replaces previous editions ofEPA Form 7710-25 Page 19SANITIZED SUBMISSION II1II111I1111II11111111111111111I11111111111 PMN2010P9X1
.. 

### PMN Page 9
... . ..**~--~---~----c** 

### 6 ,------ Part II·· HUMAN EXPOSURE AND ENVIRONMENTAL RELEASE •• Continued

Section A -- INDUSTRIAL SITES CONTROLLED BY THE SUBMIITER _.**Con~t==-in=u=ed=-===--** 

### __ 

# .­ 

# 01 02 03 The information on pages 9 and 9a refer to consolidated chemical number(s): 2. Occupational Exposure -- You must make separate confidentiality claims for the description ofworker activity. physical form ofthe new chemical

substance. numberofworkers exposed, and duration of activity, Mark (X) the "Confidential" box nextto any item you claim as confidential.

(1) Describethe activities (I.e, bag dumping, tote filling. unloading drums, sampling, cleaning, etc,) in which workers may be exposed to the substance, (2) Mark (X) this column ifentry in column (1) is confidential business information (CBI), (3) -- Describe any protective equipment and engineering controls used to protect workers, (4) and (6) -- Indicate your willingness to have the information provided in column (3) or (5) binding, (5) -- Indicate the physical formes) ofthe new chemical substance (e,g" solid: crystal, granule, powder, or dust) and % new chemical substance (if part ofa mixture) at the time ofexposure, (7) -- Mark (X) this column ifentries in columns (3) and (5) are confidential business information (CBI), (8) Estimate the maximum number ofworkers involved in each activity for all sites combined, (9) Mark (X) this column ifentry in column (8) is confidential business information (CBI), (10) and (11) -- Estimate the maximum duration ofthe activityfor any worker in hours per day and days peryear. (12) -- Mark(X) this column ifentries in columns (10) and (11) are confidential business information (CBI), 

### I ! Workeractivity Protective Equipment/ Binding Physical Binding # of Maximum Duration (i.e" bag dumping, filling CBI Option form(s) Option CBI Workers CBI eBI drums) Engineering Controls Mark (X) &%new Mark (X) Exposed

(1) (2) (3) (4)**sUb~ltance** (6) (7) (8) (9) Hrs/Day DayslYr (12) 5) (10) (11) 

# iW.;gh;09 PMNoh.m;,,' See MSDS Dry solid 99­ 6 0.7 60

and discarding waste 

### i 100% from empty container 

### I

, Loading the mix vessel See MSDS Dry solid 99­ 6 0,4 60 100% Overseeing solution See MSDS Solution 6 0,7 I 60 preparation and sampling -0,12% 

# I I Discarding waste from See MSDS Solution 9 I 2 

### I 60 i filtering equipment 

# I -0.12% 

### I I I I 

### I I I I I 

### I I 

### I

: I I I I


### I I I
I I 

### I I Mark (X) this box ifthe

# data continues on the next page 

## I I AnCl(;runem ,Section I the bottom ofpage 9a 

# [ ] !

I

EPA FORM 7710-25 (Rev, 6-09) Replaces previous editions of EPA Form 7710-25 Page 20SANITIZED SUBMISSION 11111111111111111111111111111111 11111111111111111111111111 PMN2010P9AX1 

## PMN P 9

## a

Navigable waterway- 

### I 

### age You must make separate confidentiality claims for the release number and the amount ofthe new chemical 3. Environmental Releaseand Disposal substance released and other release and disposal information. Mark (X) the "Confidential" box nextto each item you claim as confidential. (1) -- Enterthe number ofeach release point identified in the processdescription. part II, section A, subsection 1d(3). (2) -- Estimate the amount ofthe newsubstance released (a) directlyto the environment or (b) into control technology (in kg/day or kg/batch). (3) -- Mark (X) this column ifentries in columns (1) and (2) are confidential business information (CBI). (4) Identifythe media (stack air, fugitive air (optional-see Instruction Manual), surface water. on-site or off-site land or incineration, POTW, or other (specify)) to which the new substance will be released from that release point (5) a. Describe control technology, if any, and control efficiencythatwill be used to limitthe release ofthe newsubstance to the environment. For releases disposed of on land. characterize the disposal method and statewhether it is approved for disposal of RCRA hazardous waste, On a continuation sheet, for each site describe any additional disposal methods that will be used and whetherthe waste is subjectto secondary ortertiary on-site treatment. b. Estimatethe amount released to the environment after control technology (in kg/day), (6) -- Mark (X) this column ifentries in columns (4) and (5) are confidential business information (CBI). (7) -- Identify the destination(s) of releases to water. Please supply NPDES (National Pollutant Discharge Elimination System) numbers fordirect discharges or NPDES numbers ofthe POTW (Publicly Owned Treatment Works). Mark (X) ifthe POTW name or NPDES# is confidential business information (CBI), Release Amount of New Medium of release Control technology and efficiency (you maywish to Number Substance Released CBI e.g. Stack air optionally attach efficiency data) CBI (1) (2a) (2b) (3) (4) Binding (Sa) Mark (5b) (6) {X} 

# I i 1 <0.1 kg i Other: Landfill

i 2 < 0.1 kg i Recoverywith disposal of non- < 0.1 kg 

### I recoverables in compliancewith i regulations 3 < 0.1 kg
I 

### I i Incineration 0


### I i ,..--... 

### I

i I 

### I ! 

### I I ! 

### I 

# I

! i i Mark (X) this box ifthe data continues on the next page. ! 

# D (7) Mark (X) the destination(s of releases to water. NPDES# CBI POTW--provide 

### I 

# D name(s)

. . 

# D Other--Specify 

# D
EnterAttachment filename for Part II, Section A. 

# D EPA FORM 7710-25 (Rev. 6-09) Replaces previOUS editions ofEPA Form 7710-25 Page 21i 

# ISection A -- INDUSTRIAL SITES CONTROLLED BY THE SUBMITT=E=;R_
.........__

# --.!~z....:=~~~~F-"-'-'~~---i 11111111111111111111111111111111111111111111111111111111111111111 SANITIZEDSUBMISSION PMN2010P8X2 

### PMN**pa~** -,,--==-c=-:c-::--=-::::-:-:=----=--::-=::---

____---, 

### 1--- 

### Part 11-- HUMAN EXPOSURE AND ENVIRONMENTAL RELEASE I The information on pages 8and 8a referto consolidated chemica':;;.I.::.:n.=u:;;.m:;:b..:;.9;:.,!r(.:,;S)C'-:

### -::--=0=:"'-..:;1--:-:--"0""""'_2.----"=:='.....::..,,.--:1==;'-_:----'=="'-:--:----:'7=:'--::----\

Complete section A for each type of manufacture, processing, or use operation involving the new chemical substance at industrial sites

, you control. Importers do not have to complete this section for operations outside the U.S.; however, you may still have reporting 

### I requirements ifthere are further industrial processing or use operations after import, You mustdescribe these operations. See lJDstructions manual--:-

_____________________________________--,_,.---::-----i

, 1, Operation description Confia. Identlt Enterthe identity ofthe site atwhich the operation will occur, .___. ____________

## +

__ d..:..en_t_ia_1-1 Name Graphics Communications Group of Eastman Kodak Company**:-------------+-~---** Site address (number a street) One Polychrome Park, Corporate Ridge Industrial Park 

# o**~------------~ -~--~--------------------i**  C;ly C,"oly 

# IM,,,ogoo 

# Em,",

State
... GA.. ZIP code l31907 Ifthe same operation will occur at more than one site, enterthe numberof sites, Identifythe additional sites on a continuation sheet, and ifany ofthe sites have significantly different production rates or 

## 1 o erations, include all the information re uested in this section forthose sites as attachments, -7 Mark (Xl this box ifthe data continues on the next page. b. Type-­ Mark (X) Manufacturing 

# 0 Processing 

## Use 

# o

# o o 

# o c, Amount and Duration -- Complete 1 or2 as appropriate Maximum kg/batch (100% new chemical Hours/batch Batches/year 1, Batch**substanc~)** 

### 0 Maximum kg/day Hours/day Days/year (100% new chemical substance) 2. Continuous 

# [R] XXX XXX XXX 

# I Mark (X) to indicate your willingness to d, Process description have your process description binding, 

### 0 -7 

### I i ,.---' (1) Diagram the major unit operation steps and chemical conversions, Include interim storage and transport containers (specify- e,g. 5gallon pails, 55 gallon drum, rail car, tank truck, etc.), (2) Provide the identity, the approximate weight (by kg/day or kg/batch on a 100% new chemical substance basis), and entry point ofall starting materials and feedstocks (including reactants, solvents, catalysts, etc,), and ofall products, recycle streams, and wastes, Include cleaning chemicals (note frequency if not used daily or per batCh,), (3) Identify by numberthe points of release, including small or intermittent releases, to the environment of the new chemical substance. If

m releasing to two media at the same**stEl~s:sign** a second release number for the second medium, 

### 0 See Coating Operation Diagram Attachment

EPA FORM 7710-25 (Rev, 6-09) Replaces previous editions of EPA Form 7710-25 Page 22

### I

# ~ 11111111111111111111111111111111 11111111111111111111111 SANITIZED SUBMISSION PMN2010PBAX2 

### PMN Page 8a Confidential

# ~. I Diagram ofthe major unit operation steps. 

# D

EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions of EPA Form 7710-25 Page 23SANITIZED SUBMISSION 11111111111111111111111111111111111111111111 PMN2010P9X2 

### PMN 

### Page 9 

# I Part 11·- HUMAN EXPOSURE AND ENVIRONMENTAL RELEASE - Continued I



### Section A _. INDUSTRIAL SITES CONTROLLED BYTHE SUBMITIER_. Continued The infonnation on pages 9 and 9a referto consolidated chemical number(s): 

# 01 [ 2 

# 03 04 05 06 2. Occupational Exposure -- You must make separate confidentiality claims for the description ofworker activity, physical form ofthe newchemical

substance, number ofworkers exposed, and duration ofactivity. Mark (X) the "Confidential" box nextto any item you claim as confidential.

(1) Describe the activities (Le. bag dumping, tote filling, unloading drums, sampling, cleaning, etc.) in which workers may be exposed to the substance. (2) -­ Mark (X) this column if entry in column (1) is confidential business information (CBI). (3) -­ Describe any protective equipment and engineering controls used to protect workers. (4) and (6) -­ Indicate your willingness 10 have the information provided in column (3) or (5) binding. (5) Indicate Ihe physical formes) ofthe newchemical substance (e.g., solid: crystal, granule, powder, or dust) and % newchemical substance (if part of a mixture) at the time ofexposure. (7) -­ Mark (X) this column ifentries in columns (3) and (5) are confidential business information (CBI). I (8) Estimate the maximum number ofworkers involved in each activity for all sites combined. (9) Mark (X) this column ifentry in column (8) is confidential business information (CBI). (10) and (11) -- Estimatethe maximum duration ofthe activity for any worker in hours per day and days per year. (12) -­ Mark (X) this column ifentries in columns (10) and (11} are confidential business information (CBI). Workeractivity Protective Equipment! Binding Physical Binding #of Maximum Duration (i.e., bag dumping,filling CBI Option form(s) Option CBI Workers CBI CBI 

## I drums) Engineering Controls Mark (X) &%new Mark (X) Exposed (1) (2) (3) (4) substance (6) (7) (8) (9) Hrs/Day DaysNr (12)
. (5) (10) (11) 

# i Discarding waste from .See MSDS Solution i 10 2 35 !

filtering equipment ! :-0.12% 

# I i ! 

### I I I 

### I 

### I I 

### i i Overseeing coating ! See MSDS Solution - ! 10 4 35 • operation and i 0.12% i 

# I maintenance ofthe

equipment 

### I 

# I ! 

### 1 : i 

### I 

# J 

# J I 

### i i i I I i 

# I I I 

### I
I i 

### I I I 

## I i I I 

# I i 

# I I 

# I I I i 

### I i 

### I i I I i 

# i I 

### I i 

# I i i 

# i I I 

### i i 

# I I I : I i 

# j i ! 

### I 

### . 

# i I I i i I i 

# I Mark (X) this box ifthe data continues on the next page. 

## I I EnterAttachment filename for Part II. Section A on the bottom of page 9a. 

## [ ]
EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions of EPA Form 7710-25 Page 2411111111111111111111111111111111111/11111111/11111111111111111111/1111 SANITIZED SUBMISSION PMN2010P9AX2 

### PMN Page 9a



# I
I 

# I 3. Environmental Release and Disposal -­ You must make separate confidentiality claims forthe release numberand the amount ofthe new chemical

substance released and other release and disposal information. Mark (X) the "Confidential" box nextto each itemyou claim as confidential. (1) -­ Enterthe number ofeach release point identified in the process description, part II. section A. subsection 1d(3). (2) -­ Estimate the amount ofthe newsubstance released (a) directlyto the environment or (b) into control technology (in kg/day or kg/batch). (3) -­ Mark (X) this column ifentries in columns (1) and (2) are confidential business information (CBI). (4) Identifythe media (stack air, fugitive air (optional-see Instruction Manual). surfacewater, on-site or off-site land or incineration, POTW, or other (specify)) towhichthe new substance will be released from that release point. (5) -­ a. Describe control technology, ifany. and control efficiency that will be used to limit the release ofthe newsubstance to the environment. For releases disposed ofon land, characterize the disposal method and state whether it is approved for disposal of RCRA hazardous waste. On a continuation sheet, for each site describe any additional disposal methods that will be used and whetherthe waste is subjectto secondary ortertiary on-sitetreatment. b. Estimate the amount released to the environment after control technology (in kg/day). (6) -­ Mark (X) this column ifentries in columns (4) and (5) are confidential business information (CBI). (7) Identifythe destination(s) of releases to water. Please supply NPDES (National Pollutant Discharge Elimination System) numbers for direct discharges or NPDES numbers ofthe POTW(Publicly Owned Treatment Works). Mark (X) ifthe POTW name or NPDES# is confidential business information (CBI). Release Amount of New Substance Released Medium of release Controltechnology and efficiency (you may wish to optionally attach efficiency data) Number CBI e.g. Stack air (1) (2a) (2b) (3) (4) 1 < 0.01 kg Other: Landfill
2 < 0.01 kg 

### I 3 (Sa) 

# I Recovery with disposal ofnon­ , recoverables in compliance with I' :regulations Incineration Binding Mark (X) CBI (5b) (6)

I

" I < 0.01 kg 

### I



### o 

# I <001 kg 

# I 

# i I 

# I 

# I ! 

## I I 

### i I 

# I I 

# i I
I 

# I
Mark (Xl this box ifthe data continues on the next page. 

### I (7) Mark (X) the destination(s) of releases towater. POTW--provide name(s) Navigable waterway­

- provide name(s) 

# C Other--Specify I i 

### I ! 

# I 

# I I I



### I ,



# I I 

# o NPDES# 

## I eBI 

# !o

0

1 Enter Attachmentfilename for Part II, Section A, 

# 0' EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions of EPA Form 7710-25 Page 251111111111111111111111111111111111111111111111111111111111II SANITIZED SUBMISSION PMN2010P10 

### PMN 

## Pa e 10 Part 11-- HUMAN EXPOSURE AND ENVIRONMENTAL RELEASE - Continued Section B -- INDUSTRIAL SITES CONTROLLED BY OTHERS -" The information on pages 10 and 10a referto consolidated chemical number(s): 

# D 1 

# [12 

# D 3 

# D 4 

# D 5 

# D 6 I Complete section B fortypical processing or use operations involving the new chemical substance at sites you do not control. Importersdo not have to i complete this section for operations outside the U.S; however, you must report any processing or use activities after import. See the Instructions Manual.

Complete a separate section B foreach type ofprocessing, oruse operation involving the newchemicalsubstance. Ifthe same operation is performed at 

### I more than one site describethe typical operation common to these sites. Identify additional sites on a continuation sheet.

1(a). Operation Description -- To claim information in this section as confidential, bracket (e.g.

# m the specific information thatyou claim as confidential. (1) -- Diagram the major unit operation steps and chemical conversions, including interim storage and transport containers (specify - e.g. 5 gallon pails, 55 gallon drums, rail cars, tank trucks, etc). On the diagram, identify by leiter and briefly describe each worker activity. (2) -- Either in the diagram or in the textfield 1(b) below, provide the identity, the approximate weight (by kg/day or kg/batch. on an 100% new chemical substance basis), and entry point of all feedstocks (including reactants, solvents and catalysts, etc) and all products, recycle streams, and wastes. Include cleaning chemicals (note frequency ifnot used daily or per batch). (3) -- Either in the diagram or in the text field 1(b) below, identify by numberthe points ofrelease, including small or intermittent releases, to the 

### I environment ofthe new chemical substance. i (4) -- Please enterthe# ofsites (remember to identifythe locations ofthese sites on a continuation sheet): 

### I 

# I Number ofSites 

# I 0 

# I Confidential 

# D

1(b). (Optional) This space is for a text description to clarify the diagram above. Confidential 

# D

EnterAttachment filename for Part II, Section B on the bottom ofpage 10a. 

# I D

EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions of EPA Form 7710-25 Page 26 

# I11111111111111111111111111111111 11111111111111111111111 SANITIZED SUBMISSION PMN2010P10·1 

## Continuation Sheet .' ID

# I P10SB1(a)(4)1 

# I Field

# I Part II, Section B, 1(a)(4). Operation Site Locations Not applicable

EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions of EPA Form 7710-25 Page 2711111111111111111111111111111111111111111111111111111111111111111 SANITIZED SUBMISSION PMN2010P10A 

## PMN Pa e 10a 2. Worker Exposure/Environmental Release (1) From the diagram above, provide the lelter for each worker activity. Complete 2-8 for each worker activity described. (2) Estimate the number ofworkers exposed for all sites combined. (4) -- Estimate the typical duration ofexposure perworker in (a) hours perday and (b) days peryear. (6) -- Describe physical form ofexposure and % newchemical substance (if in mixture), and any protective equipment and engineering controls, if any, used to protectworkers. (7) Estimate the percent ofthe newsubstance as formulated when packaged or used as a final product. (9) -­ From the process diagram above, enter the number of each release pOint. Complete 9-13 for each release point identified. (10) -- Estimate the amount ofthe newsubstance released (a) directlyto the environment or (b) into control technology to the environment (in kg/day or kg/batch). (12) -- Describe media of release Le. stack air, fugitive air (optional-see Instructions Manual). surface water, on-site or off-site land or incineration, POTW, or other (specify) and control technology, ifany, that will be used to limit the release ofthe newsubstance to the environment. 

# I (14) -- Identify byproducts which may result from the operation. (3), (5), (8), (11), (13) and (15) -- Mark (X) this column if any ofthe proceeding entries are confidential business information (CBI).

(14) Byproducts: 

# o !



### I I 

### I I

I
: 

# I
I Letter # of of Workers CBI Duration of CBI Protective Equlp.fEngineering Controls/Physical % new %in CBI


# I ! Activity Exposed Exposure Form substance Formulation

(1) (2) (3) (4a) (4b) (5) (6) (6) (7) (8) I 

### I ! i i I 

### I I 

# J i ! 

### I ! I 

# I i I I 

# I i 

# I I ! 

### I 

# i I I ! ! I 

### I i ! 

### I 

### I I 

### I i 

## I Release Amount of New Substance Released CBI Media of Release & ControlTechnology CBI Number

(9) (10a) 

## I (10b) (11) (12) (13)
i i

Mark (X) this box ifthe data continues on the next page. 

# I
I

Enter Attachment filename for Part II, Section B. 

# o
EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions of EPA Form 7710-25 Page 28111111111111111111111111111111111111111111111111111111111111 SANITIZED SUBMISSION PMN2010P11 

## PMN Pa e 11 

## OPTIONALPOLLUTION PREVENTION INFORMATION To claim information in the follOwing section as confidential, bracket (e,g, {}) the specific information that you claim as confidential, In this section you may provide information not reported elsewhere in this form regarding your efforts to reduce or minimize potential risks associated with activities surrounding manufacturing, processing, use and disposal ofthe PMN substance, Please include new information pertinentto pollution prevention, including source reduction, recycling activities and safer processes or products available due tothe newchemical substance, Source reduction includes the reduction in the amount ortoxicity ofchemical wastes by technological modification, process and procedure modification, product reformulation, and/or raw materials substitution, Recycling refers to the reclamation ofuseful chemical components from wastes that would otherwise betreated or released as airemissions or waterdischarges, or land disposal. Quantitative orqualitative descriptions ofpollution prevention, source reduction and recycling should emphasize potential risk reduction in addition to compliance with existing regulatory requirements, The EPA is interested in the information to assess overall net reductions in toxiCity or environmental releases and exposures, notthe shifting of risks to other media (e,g" air towater) or nonenvironmental areas (e,g" occupational or consumer exposure), To the extent known, information about the technology being replaced will assist EPA in its relative risk determination, In addition, information on the relative cost or performance characteristics ofthe PMN substance to potential alternatives may be provided, Describe the expected net benefits, such as

(1) an overall reduction in risk to human health orthe environment; (2) a reduction in the generation ofwaste materials through recycling, source reduction or other means; (3) a reduction in the use ofhazardous starting materials, reagents, or feedstocks; (4) a reduction in potential toxicity, human exposure and/orenvironmental release; or (5) the extentto which the new chemical substance may be a substitute for an existing substance that poses a greater overall risk to human health orthe environment. Information provided in this section will betaken into consideration during the review ofthis substance. See PMN Instructions Manual and Pollution Prevention Guidance manual for uidance and exam les.

EPA FORM 7710-25 (Rev, 6-09) Replaces previous editions of EPA Form 7710-25 Page 291111111111111111111111111111111111111111111111 SANITIZED SUBMISSION PMN2010P12 

### PMN Page 12 Part III -- LIST OF ATTACHMENTS Attach continuation sheets for sections ofthe form, test data and other data (including physical/chemical properties and structure/activity information), and optional information afterthis page. Clearly identifythe attachment and the section ofthe form to which it relates, ifappropriate. Number consecutively the pages ofany paper attachments. In the Number of Pages column below, enterthe inclusive page numbers ofeach attachment for paper submissions orenterthe total number ofpages for each attachment for electronic submissions. Electronic attachments can be identified by filename. Mark (X) the "Confidential" box nextto any attachment name orfilename you claim as confidential. Read the Instructions Manual for guidance on how to claim any information in an attachment as confidential. You must include with the sanitized copy ofthe f fi' I notice form a sanitized version ofany attachment in which you claim in ormation as con Identla
. 

# 1-1.. INumber Associated ICBI i Attachment Name Attachment Filename of Pages PMN Section Number 001 IES Report 

# i 1 Pt.!. Sec.B, k I i 1 002 IKodak PMN Substance Structure 11 PLI, Sec.B, 1e. 1 1003 Process Diagram 3 Pt.2, Sec.A. 1d. 1 

### I i 

### I iProcessing Diagram 

### I 1 Pt.2, SecA 1d. (#2) 

### I I

1005 

### ICoating Operation Diagram 1 Pt.2, Sec.A, 1d. (#3) 

### I i 006 1Material Safety Data Sheet 7 I 

# I 007 

### IStudy 16 

# I i 

### I 008 Analysis 3
1 

### I 009 FT-IR Analysis 1 

## I I

1010 Proton NMR Analysis 2 i 1011 

### IParticle Size Analysis 6 

### I I 1012 

### IDSC Analysis 11 i ,013 1Chemical Safety Data Sheet 12 

### I 1014 Acute Toxicity to Zebra Fish S0507 ! 28 

### I 

## I 1015 ,Ready Biodegradation Test S0507 i 1 16 i 

# I ! 

### IPMN Fee PaymentAcknowledgement 016 i 1 i 

### I • 1 1 

### i 1 

### I i 1 

### I 1 

### I I Mark (X) this box ifthe data continues on the next page. 

# l 

# J EPA FORM 7710-25 (Rev. 6-09) Replaces previous editions of EPA Form 7710-25 Page 30111111111111111111111111111111111111111111111111111111111111 SANITIZED SUBMISSION PMN2010P13 

### PMN P age 

### 13 PHYSICALAND CHEMICAL PROPERTIESWORKSHEET The information on this page refers to chern 

# I Is 

# r 

# 16 To assist EPA's review of physical and chemical properties data, please complete the following worksheet for data you provide and include it in the notice. Identifythe property measured. thevalue ofthe property, the units in which the property is measured (as necessary). and whether ornotthe property is claimed as confidential. Give the attachment number (found on page 12) in column (b). The physical state ofthe neat substance should be provided. These measured properties should be forthe neat (100% pure) chemical substance. Propertiesthat are measured for mixtures or formulations should be so noted (% PMN substance In _I. You are not required to submitthis worksheet; however, EPA strongly recommends that you do so. as itwill simplifythe review and ensure that confidential information is properly protected. You should submitthis worksheet as a supplement to your submission oftest data. This worksheet is not a substitute for submission oftest data. Property Unit 

# I Mark X if Altac Value Measured CBI Nu or Estimate Mark (X) (a) Provided (e) (M or E) (d) 

# D (solid) 

# I (liquid) (gas) Physical state of neat substance 

# [X] 

# D D Measured Vapor Pressure @ 25 

# D 5,01 E-021 Torr Estimate Temperature 

## ·c Density/relative density 

# D g1em3 Solubility @ Temperature 

## ·c 

# D gIL Solvent 0.00009 Solubility in Water @ 

# D gIL Temperature 

## ·c Melting Temperature 

# D j4l:l 

## ·c I Boiling 1Sublimation 898 : Estimate 

# D I temperature @ Torr 

## ! ·C 

# D H1 NMR Spectra Dissociation constant 

# D Octanoll water partition coefficient 

# D I 6,02 Estimate Henry's Law constant 

# D Volatilization from water 

# D Volatilization from soil 

# D pH@ concentration 

# D Flammability 

# D Explodability 

# D Adsorption I Coefficient 

# D Particle Size Distribution 

# D Measured

I Other Specify HPLC purity 

# D 99 area % 

### I Measured
Page 31

### ATTACHMENT HEADER SHEET


### Attachment Number 001 Attachment Name IES Report 

### Associated PMN 

### Section Number Pt.l, Sec.B, 1c. Does not contain CBI



### Report Number KODA101220491061974

Page 32

### Sanitized Version 

# Inventory

# ExpertService
A division oftheAmerican Chemical Society**Phone:~631-1884,61~7-3870** 

### Fax:

### 614-447-3747 E-mail:answers@cas.org Web:www.cas.orglproducts/dientl



### INVENTORY EXPERT SERVICE REPORT

:ES-ORDER NUMBER: 

### REGISTRY NUMBER: 4010**2=-7T'::~f-l**

""""" ..**-"'~,~'''~**
CA INDEX NAME 

### 2-[2-[3-[2-(1,3-dihydro-l,3,3-trimethyl-2H-indol-2-ylidene)ethylidene]­ 2-[ (1-phenyl-1H-tetrazol-5-yl)thio]-1-cyclohexen-1-yl]ethenyl]-1,3,3­ trimethyl-,

.. 

### chloride 1:1

-- ,.,.-,.....**,."""""'''~**



### Please print the above CA Index Name on the appropriate page of your PMN. 

# o If this box is checked, CAS has made correction(s) marked in red to your IES order. Please make the same correction(s) to your PMN before submitting it to the EPA.

CAS**'lS~** O\entlJngy I\i'ver I\oad P.O.Sox:n":l Columbus.Ohio'\:l'l11)..l):l:l4 

### Attachment 1, Page 33

### ATTACHMENT HEADER SHEET
Attachment Number 002 Attachment Name Kodak PMN Substance Structure 

### Associated PMN Section Number Pt.!, Sec.B, 1e. Does not contain CBI



### Report Number KODA101220491061974



### Page 34

### Sanitized Version 

# PMN Substance Structure

CASRN440102-72-7 3H-Indolium, 2-[2-[3-[2-(I,3-dihydro-1,3,3-trimethyl-2H-indol-2-ylidene)ethylidene]-2­ [I-(phenyl-IH-tetrazol-5-yl)thio]-l-cyclohexen-l-yl]ethenyl]-l,3,3-trimethyl-. chloride

Attachment2, Page 35

### ATTACHMENT HEADER SHEET
Attachment Number003 Attachment Name Process Diagram 

### Associated PMN Section Number Pt.2, Sec.A, 1d. Does not contain CBI



### Report Number KODA101220491061974

Page 36

## Manufacturing Process Diagram Sanitized Version

Attachment 3, Page 37

### Sanitized Version



## REACTION CHEMICALS AMOUNT MOLES

Attachment 3, Page 38

### Chemistry Flow Diagram Sanitized Version

CASRN 440102-72-7 3H-1ndolium, 2-[2-[3-[2-(1.3-dihydro-1,3,3-trimethyl-2H-indol-2-ylidene)ethylidene]-2-[(phenyl-1 Htetrazol-5-yl)thio]-1-cyclohexen-1-yl]-1.3,3-trimethyl-. chloride

Attachment 3, Page 39

### ATTACHMENT HEADER SHEET
Attachment Number004 Attachment Name Processing Diagram 

### Associated PMN Section Number Pt.2, Sec.A, 1 d. (#2) Does not contain CBI



### Report Number KODA101220491061974

Page 40Sanitized Version 

### Processing Diagram

Weighing PMN chemical 440102-72-7 0.8 kg/batch 1to 2 batches perday equipment
Resid al PMN chemical from container liner
Water [7732-18-5J**42.~,-,k=-Q_----;1101** 

### Otheraddenda Release Mixed solvent cleaninO"'--

___.....-...I 

### Mix vessel 

# I Mixed solvent cleaning liquors 

### 2 or 

### 3 Release 3

! 

### I Release Cleaning (Le. residue) Filtration 1 equipment or 

### 3

Coating operation

0.12% Solution Key Release 1 

### = Landfill Release 2 

### = Recovery Release 3 

### = Incineration Mixed solvent: 2-Butanone (78-93-3) 45% Water (7732-18-5) 10% 1-Methoxy-2-Propanol (CAS 107-98-2) 35% 4-Butrolactone (CAS 96-48-0) 10%

Attachment 4, Page41

### ATTACHMENT HEADER SHEET
Attachment Number 005 Attachment Name Coating Operation Diagram 

### Associated PMN Section Number Pt.2. Sec.A. 1d. (#3) Does not contain CBI



### Report Number KODA101220491061974

Page42

### coating ontinous 24 hour operation. There re rovide

. oating machine. It takes 12 hours . 0 

### ollowing

aterial ill be captured xhaust and incinerated or will be we t u Sanitized 

### Version 

### Coating Operation

PMN chemical [440102-72-7] 0.8 k /batch as a 0.12% solution of PMN chemical 1to 2 batches per day Holding vessel Mixed solvent**clean",in~** 

### __**~..,** 

### r-M=ix=e:..:::dc...:s::.;:o:.:.;lv:..,:e:..:.,n:.:..t**-=.c,-",Ie=a"-,n~i** 

### n""'g--'-l=i9c=u-"-o'-=rs'--_.... Release 3

Filtration equipment Release Cleaning (i.e. residue) 1 or 

### 3

Solution from coatin 0 

### eration Release 3 Coating Mixed solvent cleaning equipment Release 1_--,-,-M=ix=e""d:...;s::.:o:..:.lv.:...:e:..:.n:.::.t-=c:.:.=le:.:a:.:..;n""in"",gL.;l=iqL::u:.=o.:..:rs"----)100-" 2 or 

### 3

Article operation is a multiple holding tanks used to Key coating solution to one Release 1 = Landfill Release 2

# =Recovery coat one batch. Dust emissions Release 3 

### = Incineration unloading of solid from transport container in filters of local Mixed solvent: 2-Butanone (78-93-3) 45% and incinerated. Water (7732-18-5) 10% 1-Methoxy-2-Propanol (CAS 107-98-2) 35%, 4-Butrolactone (CAS 96-48-0) 10%

Attachment 5, Page 43

### ATTACHMENT HEADER SHEET
Attachment Number006 Attachment Name Material Safety Data Sheet 

### Associated PMN Section Number N/A
Does not contain CBI



### Report Number KODA101220491061974

Page44Sanitized Version 

## Material Safety Data Sheet Revision Date: 

### 11/15/2010 000000033729Nersion: 1.1 

# Kodak Print Date: 

### 12/01/2010



### • 1. Identification ofthe substance/mixture and ofthe company/undertaking

Product name: ORM1835 Productcode: 10091357 Supplier: EASTMAN KODAK COMPANY, 343 State Street, Rochester, New York 14650 For Emergency Health, Safety & Environmental Information, call (585) 722-5151 (USA) Forfurther information about this product, call (800) 242-2424. Synonyms: None. Product Use: Plate manufacturing chemical, For industrial use only.

CONTAINS: S 0507 IR Dye (proprietary) WARNING! POWDERED MATERIAL MAY FORM EXPLOSIVE DUST-AIR MIXTURES HEAT SENSITIVE - CAN DECOMPOSE IF HEATED MAY BE HARMFUL IF SWALLOWED MAY CAUSE SKIN AND EYE IRRITATION DUST MAY BE IRRITATING TOTHE EYES AND RESPIRATORY TRACT THE PHYSICAL-CHEMICALAND TOXICOLOGICAL PROPERTIES OF THIS MATERIAL HAVE NOT BEEN FULLY INVESTIGATED HMIS III Hazard Ratings: Health - 1, Flammability - 

### 1, Reactivity (Stability) - 2 NFPA Hazard Ratings: Health - 3, Flammability - 1, Instability - 2 NOTE: HMIS III and NFPA 704 (2007) hazard indexes involve data review and interpretation that may vary among companies. They are intended only for rapid, general identification ofthe magnitude ofthe potential hazards. To adequately address safe handling, ALL information in this MSDS must be considered. 

# I 3. Composition/information on ingredients Weight Components - (CAS-No.) percent

100 S 0507 IR Dye (proprietary)

Inhalation: Ifinhaled, remove to fresh air. Get medical attention ifsymptoms occur.

Attachment 6, Page45

### Sanitized Version 

### Material Safety Data Sheet Revision Date: 

### 11/15/2010 000000033729Nersion: 1.1 

# Kodak Print Date: 

### 12/01/2010 Eyes: 

### Any material that contacts the eye should bewashed out immediatelywith water. Get medical attention if symptoms occur. Skin: Wash offwith soap and water. Get medical attention ifsymptoms occur. Ingestion: If swallowed, only induce vomiting as directed by medical personnel. Never give anything by mouth to an unconscious person. Nevergive anything by mouth to an unconscious person. Call a physician or poison control centre immediately.
Extinguishing Media: Water spray, Carbon dioxide (C02), Dry chemical. Use water spray to cool unopened containers. Special Fire-Fighting Procedures: Wear self-contained breathing apparatus and protective clothing. Fire or excessive heat may produce hazardous decomposition products. Hazardous Combustion Products: Carbon oxides, Sulphur oxides, nitrogen oxides (NOx), (see also Hazardous Decomposition Products sections.) Unusual Fire and Explosion Hazards: Elevated temperature can cause decomposition. Dust may form explosive mixture in air.

Shovel into suitable containerfor disposal. Avoid dust formation. Clean surface thoroughly to remove residual contamination. 

## 7. Personal precautions: Avoid breathing dust. Avoid contact with eyes, skin, and clothing. Use only with adequate ventilation. Wash thoroughly after handling. Prevention of Fire and Explosion: Keep away from heat and sources of ignition. Exercise caution if heating, especially in a closed container. Dust may form explosive mixture in air. Minimize dust generation and accumulation. Use only with adequate ventilation. Referto NFPA 654, "Standard for the Prevention of Fire and Dust Explosions from the Manufacturing, Processing, and Handling ofCombustible Particulate Solids." Keep from contact with oxidizing materials. Storage: Keep containertightly closed. Keep away from incompatible substances (see Incompatibility section.) 

### •8. ExpC?sure controls/personal protection

Occupational exposure controls: Not established Ventilation: Good general ventilation should be used. Ventilation should be sufficient so that applicable occupational exposure limits are not exceeded. Ventilation rates should be matched to conditions. Supplementary local exhaust ventilation, closed systems, or respiratory protection may be needed in special circumstances.

Attachment6, Page 46

### Sanitized Version 

## Material Safety Data Sheet Revision Date: 11/15/2010 000000033729Nersion: 1.1 

# Kodak Print Date: 12/01/2010 Respiratory protection: None should be needed. Eye protection: Wear safety glasseswith side shields (or goggles). Hand protection: For operations where prolonged or repeated skin contact may occur, impervious gloves should be worn. 

### I 

### 9. Physical and chemical properties

Physical form: solid (crystalline) Colour: green Odour: odourless Specific gravity: 0.15 - 0.27 Vapour pressure: no data available Vapourdensity: no data available Volatile fraction by weight: not applicable Melting point/range: no data available Watersolubility: insoluble pH: not applicable Flash point: not applicable Stability: Not fully evaluated. Materials containing similar structural groups can decompose if heated. Incompatibility: Strong acids, Bases, light. Hazardous decomposition products: nitrogen oxides (NOx), Sulphur oxides, hydrogen chloride Hazardous Polymerization: Hazardous polymerisation does not occur. 

### information Effects of Exposure General advice: The toxicological properties ofthis chemical have not been fully investigated. Inhalation: Airborne dust/mist/vapor may be irritating. Eyes: May cause eye irritation. Airborne dust/mist/vapor may be irritating.

Attachment6, Page 47

### Sanitized Version 

### Material Safety Data Sheet Revision Date: 

### 11/15/2010 000000033729Nersion: 1.1 

# Kodak Print Date: 

### 12/01/2010
Skin: May cause skin irritation. Ingestion: May be harmful ifswallowed.

The following properties are ESTIMATED from the components ofthe preparations. PotentialToxicity: Toxicity to fish (LC50): > 

### 100 mgtl Toxicity to daphnia (EC50): > 

### 100 mgtl Persistenceand degradability: Not readily biodegradable. 

### 13. considerations Discharge, treatment, ordisposal may be subject to federal, state, commonwealth, provincial, or local laws. Since emptied containers retain product residue, follow label warnings even aftercontainer is emptied.

Not regulated for all modes oftransportation. For more trans ortation information, go to: www.kodak.com{9
.___ ots--.h--.-ip_.

____________--. 

### 15. Regulatory information**------------------------------------~** 

### Notification status Regulatory List Notification status TSCA Not all listed DSL Not all listed NDSL None listed EINECS Not all listed ELiNCS None listed NLP None listed AICS Not all listed IECS Not all listed ENCS Not all listed ECI Not all listed NZloC Not all listed

Attachment 6, Page 48Sanitized Version 

### Material Safety Data Sheet Revision Date: 

### 11/15/2010 000000033729Nersion: 1.1 

# Koda Print Date: 

### 12/01/2010

PICCS Not all listed "Not all listed" indicates one or more component is either not on the public Inventory or is subject to exemption requirements. Ifadditional information is needed contact Kodak. Other regulations American Conference of Governmental Industrial Hygienists (ACGIH):
International Agency for Research on Cancer (IARC):

U.S. National Toxicology Program (NTP):

U.S. Occupational Safety and Health Administration (OSHA):
California Prop. 65

U.S. - CERCLAISARA (40 CFR 

### § 302.4 Designation of hazardous substances):
U.S. - CERCLA/SARA - Section 302 (40 CFR 

### § 355 AppendicesA and B - The List of Extremely Hazardous Substances and Their Threshold Planning Quantities): U.S. - CERCLAISARA - Section 313 (40 CFR 

### § 372.65 Toxic Chemical Release Reporting):
U.S. - California - 8 CCR Section 339 - Director's List of Hazardous Substances: U.S. - California - 8 CCR Section 5200-5220 - Specifically Regulated Carcinogens: Nocomponent ofthis product present at levels greaterthan orequal to 0.1% is identified as a carcinogen orpotential carcinogen by ACGIH. No component ofthis product present at levels greaterthan orequal to 0.1% is identified as probable, possible orconfirmed human carcinogen by IARC. No component ofthis product present at levels greaterthan orequal to 0.1% is identified as a known or anticipated carcinogen by NTP. No component ofthis product present at levels greaterthan or equal to 0.1

### % is identified as a carcinogen orpotential carcinogen by OSHA. This product does not contain any chemicals known to State of California to cause cancer, birth defects, or any other reproductive harm. No components ofthis product are subject to the SARA Section 302 (40 CFR 302.4) reporting requirements. No components ofthis product are subjecttothe SARA Section 302 (40 CFR 355) reporting requirements. No components ofthis product are subjecttothe SARA Section 313 (40 CFR 372.65) reporting requirements. No components found on the California Director's List of Hazardous Substances. No components found on the California Specifically Regulated

Attachment 6, Page 49

### Sanitized Version 

### Material Safety Data Sheet Revision Date: 

### 11/15/2010 000000033729Nersion: 1.1 

# Kodak Print Date: 

### 12/01/2010



## u.s. - California - 8 CCR Section 5203 Carcinogens: U.S. - California - 8 CCR Section 5209 Carcinogens: U.S. - Massachusetts - General Law Chapter 111F (MGL c 111 F) - Hazardous Substances Disclosure by Employers (a.k.a. Right to Know Law): U.S. - Minnesota Employee Right-to-Know (5206.0400, Subpart 5. List of Hazardous Substances):
U.S. - New Jersey - Worker and Community Right to Know Act (N.J.S.A. 34:5A-1): U.S. - Pennsylvania - Part XIII. Worker and Community Right-to-Know Act (Chapters 301-323): U.S. - Rhode Island - Title 28 Labor and Labor Relations (Chapters 28-21 Hazardous Substance Right-to-Know Act): Carcinogens List. No components found on the California Section 5203 Carcinogens List. No components found on the California Section 5209 Carcinogens List. No components regulated under the Massachusetts Hazardous Substances Disclosure by Employers Law. No componentsfound on the Minnesota Employee Right-toKnow List of Hazardous Substances. No components regulated underthe New Jersey Worker and Community Right-to-KnowAct. S 05071R Dye No components regulated underthe Rhode Island Hazardous Substance Right-to-Know Act.

The data below reflects current legislative requirements whereas the product in your possession may carry a different version ofthe label depending on the date of manufacture. US/Canadian Label Statements: ORM1835 CONTAINS: S 05071R Dye (notapplicable). WARNING! POWDERED MATERIAL MAY FORM EXPLOSIVE OUST-AIR MIXTURES. HEAT SENSITIVE - CAN DECOMPOSE IF HEATED. MAY BE HARMFUL IF SWALLOWED. MAY CAUSE SKIN AND EYE IRRITATION. OUST MAY BE IRRITATING TO THE EYES AND RESPIRATORY TRACT. THE PHYSICAL-CHEMICALAND TOXICOLOGICAL PROPERTIES OF THIS MATERIAL HAVE NOT BEEN FULLY INVESTIGATED. Store in cool place. Keep away from heat and sources of ignition. Avoid breathing dust. Avoid contact with eyes, skin, and clothing. Use only with adequate ventilation. Wash thoroughly after handling. FIRST AID: If inhaled, remove to fresh air. Any material that contacts the eye should be washed out immediately with water. Wash offwith soap and water. Get medical attention ifsymptoms occur. Keep out of reach of children. Do not handle or use until safety precautions in Material Safety Data Sheet (MSDS) have been read and understood. Since emptied containers retain product residue, follow label warnings even after container is emptied. IN CASE OF FIRE: Water spray, Carbon dioxide (C02), Dry chemical. Use water spray to cool unopened containers. IN CASE OF SPILL: Shovel into suitable containerfor disposal. Avoid dust formation. Clean surface thoroughly to remove residual contamination.

Attachment 6, Page 50Sanitized Version 

### Material Safety Data Sheet Revision Date: 

### 11/15/2010 000000033729Nersion: 1.1 

# Koda Print Date: 

### 12/01/2010 The information contained herein is furnished without warranty ofany kind. Users should considerthese data only as a supplementto other information gathered by them and must make independent determinations of suitability and completeness ofinformation from all sources to assure proper use and disposal ofthese materials and the safety and health ofemployees and customers and the protection of the environment. The information relating to the working solution is for guidance purposes only, and is based on correct mixing and use ofthe product according to instructions.

Attachment 6, Page 51

### ATTACHMENT HEADER SHEET
Attachment Number007 Attachment Name Study 

### Associated PMN Section Number N/A
Does notcontain CBI



### Report Number KODA101220491061974



### Page 52

### Sanitized Version

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### ATTACHMENT HEADER SHEET
Attachment Number008 Attachment Name Analysis 

### Associated PMN Section Number N/A Does not contain CBI



### Report Number KODA101220491061974



### Page 69Sanitized Version 

### EASTMANKODAKCOMPANY RESTRICTEDINFORMATION 

### LC/MS ANALYSIS REPORT MATERIALS SEPARATION AND STRUCTURE CHEMICAL CHARACTERIZAnON LABORATORY LC/MS Analyst: Robert Saccente 

### TECHNICAL SOLUTIONS DIVISION/ANALYTICAL SCIENCE DIVISION 8-82 ROOM 232C Sample Description OneLims

### # MS-12B11.



## CJNI0091357WK (mw

## =625 Oa) One sample labeled CIN10091357WK DEV91357 R3. Information Desired: Characterize sample by mass spectrometry. Experimental The sample was dissolved in 1:1 v:v acetonitrile:HPLC-grade water and analyzed on a SciexAP300 triple quadrupole mass spectrometer using electrospray (Turbolon Spray) LC/MS in positive ionization mode. The primary 

### "N solvent was 0.1 M ammonium acetate 

### + 0.1 M acetic acid buffer, pH 4.7 in HPLC-grade water. The secondary "S" solventwas a 1:1 v:v mixture of acetonitrile:2-propanol. The analyses were generated using gradient conditions 

### (75/25-0/100 in 20 minutes) at aflow rate of 0.25 mUmin. The reversed-phase HPLC column used was a Zorbax Eclipse XDS C-18 [2.1 mm X 150 mm]; 5um particle size. UV detection was performed using a diode array detector set at 254 nm. Results The sample responded favorably in positive ion electrospray. The LC/MS chromatogram ofthe sample is shown in Figure 1. The molecular weights ofthe components that responded tothe mass spectrometer are listed in the attached sample peaktable. The MS/MS spectrum ofthe major component is shown in Figure 2.

HSE-Chemical & EquIpment Regulatory Intonnation
v 4.0 Attachment 8, Page 70 10115101

### Sanitized Version EASTMANKODAKCOMPANY RESTRICTEDINFORMATION Figure 1, LC/MS Chromatogram of Sample Labeled CIN10091357WK DEV91357 R3 at 254 nm. 

### LC/MS Chromatogram ofCIN10091357WK DEV91357 R3 at 254 

## nm. aNov 2010**!o~rectoT C~~m.nt·**  UV signal] 10091357w1< dev91357·r3.esp 

# [ 

# J /

1 3596 6601 W W 4830.89 1327 57.21 I......J U '--..J j " iii " , 'I ' " , I I " j I • , , i I •• Ii I • I , i i ••• 'I • Ii iii " I Iii i ) I I • Ii I • , i , I " " I " i , I " i , I " " I • , " I " , • i •• Ii o 2 4 6 8 10 12 14 16 18 Retention Time (min)

HSE·Chemical & EquIpment Regulatory Information 10115iO I v4.0 

### Attachment 8, Page 71

### Sanitized Version EASTMANKODAKCOMPANY RESTRICTEDINFORMATION Figure 2. Positive Ion Electrospray MS/MS Spectrum of Major Component (mw 625 Da) 

### Positive Ion Electrospray MS/MS Spectrum ofthe MajorComponent (mw 

### =625 Da). 8NO'Y:i:J1Q

P , " , ., i ! , ! 321" I

, 1 I 1 , r • ,I Ii, I , I ,. j , ! ii, I j" i I I I" iii 

## Ii' ij' 

## ,ii ii, j 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440 460 480 500 520 540 560 580 600 62C rM.



### Analyst: Robert Saccente x-79577 Name: F. Debellis Bldg: 

### 337/2 KP Phone: x-83450 Reported

________ Date: 11-08-10 Charge No.


### This report is intended for internal Kodak unrestricted use. This report may not be duplicated except in its entiretyto preserve data integrity. The analysis isforthe sample received and may not represent population from which thesamplewastaken.

lISE-Chemical & Equipment Regulatory Information IOil5/01 v 4.0 

### Attachment 8, Page 72

### ATTACHMENT HEADER SHEET
Attachment Number009 Attachment Name FT-IRAnalysis 

### Associated PMN Section Number N/A Does not contain CBI



### Report Number KODA101220491061974

Page 73

### Sanitized Version EASTMANKODAKCOMPANY RESTRICTEDINFORMATION 

# FT-IRSpectra 2 mg oftest substance added to KBr Spectraacquired using a NicoletNexus470 spectrometer (EPP: ICAL-SOP-0190 and SOP: lCALSOP-O 130)


## FT-IRSpectrum
- Full Scale**44~ 42~** **40~** 

# II**38~ 36~** **34~** 32:**30~ 28~** 

.... ;Ii**26~** 24: 

## 22:**20~ 18~**  16:**14~ 12~**  1&10 1000 800 600 3000 2000 w.venlJTtJ9($(cm-1)

HSE-Chemical & Equipment Regulatory Information 10/15/0I v4.0 

### Attachment 9, Page 74

### ATTACHMENT HEADER SHEET
Attachment Number010 Attachment Name Proton NMR Analysis 

### Associated PMN Section Number N/A Does not contain CSI



### Report Number KODA101220491061974

Page 75

### Sanitized Version EASTMANKODAKCOMPANY RESTRICTEDINFORMATION 

# HI

# NMRSpectra 30 mgoftest substance addedto ImL ofOMSO-d6 in a 5mm 

### 1.0. tube. Spectraacquired using a Varian Mercury-Vx 300 MHz spectrometer (QOO# A

### TO/EP-OP-OO 1) 

### Spectra:



# I Number Type Full Expanded I 

### Temperature Chemical 

## eH,IH/IH, 13

### C,DzO exchange) ! 

### COC) Shifts I 

### 1 HI 

## X 

# I RJT i 

### 2 HI 

## X 

# I RJT 

## j FT-IR 2.1. Results The spectraare consistentwith structure for 

# eIN 10091357.

Analyst Signature: 

## BillLewis Oate: November 9, 2010 FPEG WW IC ROCH QUALITY/ANALYTICAL

HSE-Chemical & Equipment Regulatory Information
v4.0 

### Attachment 10, Page 76 10/15/01Sanitized Version EASTMANKODAKCOMPANY RESTRICTEDINFORMATION 

### HI NMR- Full Scale 

# :1 PHASEFIL.1R 0.1 0.09

## 1 0.08 0.07

0.04-:: 

## :: ·DMSO-d6

..... 0.03 0.02 0.01

0 6.03 3.69 14.20 L.........J W L...---I 10 9 8 7 654 Olerricai Shift (ppm) 3 2 

### o 

### HI NMRExpanded Scale

0050

# lPHASEFlU R 0.045 0.040

0.005

o 2.02 1.99 9.0 8.5 8.0 7.0 6.5 6.0
HSE-Chemical & Equipment Regulatory Information 10115101 v4.0 13.37 7.5 Chemical Shift (ppm)

Attachment 10, Page 77

### ATTACHMENT HEADER SHEET
Attachment Number 011 Attachment Name Particle Size Analysis 

### Associated PMN Section Number N/A Does not contain CBI



### Report Number KODA101220491061974

Page 78

### Sanitized Version EASTMANKODAKCOMPANY RESTRICTEDINFORMATION 

## ParticleSizeAnalysis Particle Size (Horiba) Analyst: Gary Slater/Valerie Turner 

# --+- tJ09t357R3_ns 11/09/2010 -+-1J09t357R3_nsr 1lO9t357R3_s

6 5 4



### 0.1 10 100 1000 um



### ns=nosonicl s=sonicl r=replicate Filename Median 10091357R3_ns 59.259 10091357R3_nsr 57.677

10091357R3_s 44.980 10091357R3_sr 45.2054 Filename 10091357R3_ns 10091357R3_nsr 10091357R3_s 10091357R3_sr 10# 2.01E+14 2.01E+14 2.01E+14 2.01E+14 Circulation Speed 3 3 3 3 Ultra sonic OFF OFF 01 :00 (7) 01:00 (7) LaserT% 76.8(%) 76.9(%) 73.0(%) 73.5(%) Lamp T% 83.0(%) 82.6(%) 79.7(%) 80.0(%) Form of Distribution Standard Standard Standard Standard Distribution Base Volume Volume Volume Volume R.R.lndex 120a0101 120a0101 120a0101 120a0101 HSE-Chemical & Equipment Regulatory Information v4.0 

### Attachment 11, Page 79 10115101Sanitized Version 

### EASTMANKODAKCOMPANY RESTRICTEDINFORMATION S.P. Area 1317.6(cm2/cm3) 1359.8(cm2/cm3) 1800.5(cm2/cm3) 1775.0(cm2/cm3) Median 59.2589(\-Im) 57.6774(\-Im) 44.9804(\-Im) 45.2054(\-Im) Mean 74.0556(\-Im) 72.2779(\-Im) 58.6210(\-Im) 58.5128(l..Im) Variance 3229.5(l..Im2) 3160.5(l..Im2) 2609.7(l..Im2) 2530.1(I..Im2) S.D. 56.8287(l..Im) 56.2182(l..Im) 51.0849(l..Im) 50.3003(l..Im) CV 76.7378 77.7807 87.1442 85.9646 Mode 62.9943(\-Im) 55.2492(l..Im) 48.0797(l..Im) 48.0906(l..Im) Diameter Frequency (%) Frequency (%) Frequency (%) Frequency (%) 0.022 0 0 0 0 0.026 0 0 0 0 0.029 0 0 

# a 0 0.034 

# a a a a 0.039 0 0 

# a a 0.044 0 

# a 0 

# a 0.051 

# a a a a 0.058 

## a a 0 

## a 0.067 0 

# a a a 0.076 

## a a 

# a a 0.087 

## a 

# a a 

# a 0.100 

## a 0 

# a a 0.115 

## a a a a 0.131 

## a 0 0 0 0.150 0 0 0 0 0.172 0 0 0 

## a 0.197 0 0 

## a 0 0.226 0 

# a 0 0 0.259 0 0 0 0 0.296 0 0 0 0 0.339 0 0 0 

## a 0.389 

## a a 0 0 0.445 

# a a 0 0 0.510 

# a 0 

## a 0 0.584 0 0 

# a 0 0.669 

## a 0 0 0 0.766 

## a 0 

# a 0 0.877 

# a 0 0 

## a 1.005 0 0 0 

# a 1.151 0 0 0 

# a 1.318 0 0 0 0

1.51 0 0 0 0 1.729 0 0 0 

# a 1.981 0 

## a 0 0 2.269 

# a 0 0 0 2.599 0 

## a 0 0 2.976 0 0 

## a 0 3.409 0 0 

# a 0 3.905 0 

# a 0 0 4.472 0 0 0 0 5.122 0 0 0.102 

## a 5.867 0 0 0.156 0.141 HSE-Chemical & Equipment Regulatory Information v4.0 Attachment 11, Page 80 10115101

### 6.720 0 7.697 0 8.816 0.188 10.097 0.364 11.565 0.617 13.246 0.932 15.172 1.282 17.377 1.653 19.904 2.064 22.797 2.556 26.111 3.175 29.907 3.949 34.255 4.864 39.234 5.844 44.938 6.769 51.471 7.502 58.953 7.935 67.523 8.016 77.339 7.75 88.583 7.171 101.460 6.342 116.210 5.356 133.103 4.352 152.453 3.352 174.616 2.503 200.000 1.822 229.075 1.286 262.376 0.867 300.518 0.563 344.206 0.364 394.244 0.245 451.556 0.177 517.200 0.138 592.387 0 678.504 0 777.141 0 890.116 0 1019.515 0 1167.725 0 1337.481 0 1531.914 0 1754.613 0 2000.000 0 0 0.156 0.273 0.456 0.7 0.99 1.308 1.653 2.049 2.543 3.185 4.007 4.992

6.05 7.031 7.771 8.149 8.128 7.737 7.039 6.119 5.083 4.063 3.088 2.291 1.669 1.188 0.814 0.541 0.359 0.246

0.18 0.141 0 0 0 0 0 0 0 0 0 0 0.246 0.399 0.636 0.981 1.437

1.97 2.525 3.069 3.608 4.177 4.811

5.51 6.219

6.84 7.261 7.4 7.23 6.781 6.114 5.294 4.393 3.494 2.673 1.954 1.412 1.017

0.73 0.515 0.358

0.25 0.182 0.141 0.115 0 0 0 0 0 0 0 0 0 0 Sanitized Version 

### EASTMANKODAKCOMPANY RESTRICTEDINFORMATION 

### 0.226 0.371 0.6 0.941 1.395 1.932 2.494 3.045 3.588 4.162 4.803 5.514 6.242 6.887 7.332

7.49 7.326 6.869 6.184 5.343 4.422 3.506 2.675 1.948 1.397 0.994 0.703 0.488 0.335 0.234 0.171 0.134

0.11 0 0 0 0 0 0 0 0 0 0

HSE-Chemical&EquipmentRegulatory Infonnation
v 4.0 Attachment 11, Page 81 10115101

### Sanitized Version EASTMANKODAKCOMPANY RESTRICTEDINFORMATION 

# 165634 ::!010-1070
Sample: 2010-1070 155634 F....: 20101070.001 Size: 1.0000 mg 

### DSC Operator: M. Spacher Memo<!: 25-420C GI 1DC/mIn N2 Run Dale: 28-Sep-2010 08:24**7~------------------------------------------------------------------------~**

4

2

328. t'e

Temperature ('C)

Total**En~l"IY**(J/I;) 545 Rate(WtV J.lili dT!dt(Clmio.) 261 

### R*E 

### IH!: Slope ofMaximmn Peak (\\iIg/C) 

### Wulih al Hilf He1ghl(C) 

### DSCCel1 850 EndoExtrapolatM OnsetTemp (C) EmOnsetTemp (C) EmEitrapolatM OnsetTemp (C) THDp atMaximu.**P~ak(Tmhr.** C) Residue DeSaiptiOll 94 132 185 198 black CellSase 2920

10119:2010

HSE-Chemical & Equipment Regulatory Information 1011510I v4.0 

### Attachment 11, 

### Page 82i Sanitized Version



### · PART IV -- Certification

## Summa~ryL...- 

## __**-----~------~--~----___1**

The iriformationprovidedis accurate to the bestof ourabilities andknowledge. The sample analyzedanddiscussedis representative of whatwillbe manufactured/importedforcommercial purposes. The analyticalmethodsdiscussedare appropriatefor the type and form of the chemical substance andthe analyticaldata hasbeen interpretedandconfirms the composition. The components that function asthe intendeduse have allbeen identified

Date completed:

## 11-09-2010

: Commercialization team members involvedwith completingthe Certificate of Composition rJiSErepresentative:Judy VanNorstrand ..--------4
m •• 

### i 

### Commercialization Team Leader:JamesMatz

Process chemist:Stephen Wark :Developmentchemist:JohnHarder/FranDebellis I

### Polymerchemist:
------------­ i-­ 

### chemist:W. . G. 

### Sl-a-te-r-IV.-.-r,-u-r-n-er-------------------j

HSE-Chemical & EquipmentRegulatory Information
v 4.0 Attachment 

### ii, Page 83 10/15101

### Sanitized Version


## Instructionsfor CertificateofComposition Forthepurposeofdocumentingthecorrectidentityofa chemical when HSEtestingand/ora new chemical notification is needed. Thisform is to be completed duringRTDP/KMCP by appropriatecommercialization team members. It

### is intendedthat members ofa commercializationteam completethis form after, );­ a representative sampleofthechemical is selected );­ the representative sampleis analyzed withtheappropriatemethodsto determinethecomposition );­ the analyticaldata areinterpreted );­ thecomponentsthatfunction as theintended use havebeen identified Thecompleted form is returnedto theHSE representativeon thecommercializationteam. Instructions: 1) Chemical Substance: IdentifY the chemical using the internal name and/orthe CIN ifa mixture. For an intermediate identifY the final (i.e. intermediate forthe dye ...). 2) Part I: For anon-polymer, a. List the componentsthat are present in a representative sample ofthe chemical. Include isomers, tautomers, stereoisomers, analogs, impurities, and solvents. For each componcntprovide, i. KAN and/or ClN ii. Name (Attach Structure) iii. Range ofpercent inrepresentative sample iv. A chemical is notified with a commercial purpose. (i.e. dye, sensitizer, antifoggant, intermediate...) All components inthe sample that functions as the intended purpose mustbe identified. Provide yes or no under the column, Functions as IntendedUse? b. Forimportedchemicals, use the Certificate ofAnalysis, MSDS, and/orany other data providedby the vendorto list the components in Part I. IfKodak analyzed the imported chemical, confirm Kodak's analytical datais consistent with the information providedby the vendor. 3) Part II: For a polymer, a. List the monomers and reactants thatmake up the polymer. Foreach monomer and reactant provide: i. KAN/CIN ii. Name (Attach Structure) iii. Weight percentinthe polymer iv. Maximum weight percent asresidual b. Give the lowest number average molecular weight c. Maximum weight percentbelow 500 molecularweight d. Maximum weightpercentbelow 1000 molecularweight e. Attach structure ofpolymer and synthetic pathway (include initiators andnon-isolated intermediates). f. For imported chemicals use the CertificateofAnalysis, MSDS, and/or any other data providedby the vendorto complete PartII. IfKodakanalyzedthe imported polymer, confirm Kodak's analytical data is consistent withthe information provided by the vendor. 4) Part III: Analytical Methods a. Briefly summarizethe analytical methods andresults used to confirm the composition oftherepresentative sample. (Analytical methods may include, literature examples, vendorinformation, professional interpretation when necessary) b. Provide the name and organization ofthe person who providedthe analytical summary. c. IfKodak analyzedthe imported chemical, confirm Kodak's analytical data is consistent with the information provided by the vendor. d. When achemical is notified all physico-chemical data inour possession must be submitted. Please attach one example for each type ofanalytical methodobtained. (i.e. If4 NMR'swere done onthe representative samplejust provide one ofthe four) Please include all Vendor information pertainingto an imported chemical. 5) Part IV: Certification Summary a. Provide the datetheteam members agree that the Certificate ofComposition is complete and "The information provided is accurate to the best ofourabilities and knowledge. The sample analyzed and discussed is representative ofwhat will be manufactured/imported for commercial purposes. The analytical methods discussed are appropriate for the type andform ofthe chemical substance andthe analytical data has been interpreted and confirmsthe composition. The componentsthat function asthe intended use have all beenidentified." b. The commercializationteam members involved with the completion ofthe Certificate ofComposition signpart IV.

HSE-Chemical & EqUipment Regulatory Information v 4.0 

### Attachment 11, Page 

### 84 10/15/01

### ATTACHMENT HEADER SHEET
Attachment Number 012 Attachment Name DSC Analysis 

### Associated PMN Section Number N/A Does not contain CBI



### Report Number KODA101220491061974

Page 85

### Sanitized Version EASTMANKODAKCOMPANY RESTRICTEDINFORMATION 

## DSCAnalysis 

# 165634 1010-1070
Sample: 2010-11)70 165634 File: 20101070.001 Size: 1.0000 II'Ii:I DSC Operator; M. Spacher Method: 25-420C 01 1OClmln N2 Run OablO 28-Sep-20 1 0 06:24**7~---------------------------------------------------------------------,** 6 5 4



### o -1 -2
Temperatu
.... ("C)

TotalEnergy (JIll 545 

### RatelWig5 Hili dT/dt(Clmin) 261 Ri;E 

### I!JJ!: SlopeofMaximum Pe"u (WigIC) 

### Wulih at

### BBlf Height(C) DSCCell 850 EndoExtrapolated OnsetTemp(C) Exo OnsetTemp(C) ExoExtrapolated OnsetTemp(C) Tt'1Dp atMasiJmuJl Peak(TDibr.C) 94 132 185 198 Residue DeScripriOll black CeJIBase 2920

10/19/2010

HSE-Chemical & Equipment Regulatory Information 10/15/0] v4.0 

### Attachment 12, Page 86

### ATTACHMENT HEADER SHEET
Attachment Number013 Attachment Name Chemical Safety Data Sheet 

### Associated PMN Section Number N/A Does not contain CSt



### Report Number KODA101220491061974

Page 87TSL }'ILE ID 165634 

# Chemical SafetyData Sheet (CSDS) EmptyDataFieldsIndicate ThatNOData WereAvailable Date Printed: ]]/]2/2010 Technical Safety Laboratory,B-320 Room 2103 Phone Ext. 26604 for Inquiries PAGE 1 OF 2 Release Versioll9 OIS\\1NT12032004



# . TESTING IN PROGRESS MolecularWeight: Mol. Weight: 661 Approval Date 06/1512010 Solubility



### FLAMMABILITY 

# i o 

### =r 

### 3 CD ::I 

# .... ...10**~** 

### FLAMMABLE LIMITS (EXPLOSIVE LIMITS) "'0 I» CO CD C» C» 

### THERMAL STABILITY Test Atmosphere Pan Type Tcst Pressure (psia) Exo To (C) Tmpr dP/dt Total Energy (JIg) Heating Rate Sample Weight Tmhr Rate dTfdt ROE Max Scan Temp (C) IARITsoage llItrogen Hastelloy-C 3.00 91.00 STABLE AT 90(' FOR 72 fl( (IRS. IDse SCTeen* llItTogen glass capillary I)u j4'J 10 C/min 100 200 3.28 234 1145 IIJSC Screen mtmgen gtass capillary U2**)4~** 10 e/min 1.00 198 3.66 261 1995 IResidue DSC !ARC ISOAG mtTogen AT90C FOR7 glass capillary HOURS 159 498 10 C/min LaO 197 2.99 214 1489 IVSP llItrogcn Upen vent, 114, s 170 196 27 40.00 225 1388 

## en I» ::I ;::;: N' CD Q.

### ~ U1 

## O· HAZARD RATINGS HeatSensitivityCode (H) Y ImpactSensitivityCode (I) 0 'lnermal EnergyCode (T) 2 PeroxideFonnerCode (El 

### o OtherReactivity Code (0) 0 Water ReactivityCode(W) 0 PolymerizabilityCode (Z) 0 Oxidi7.er Code(X) 

### o PyrophoricCode (Al N ::ITSL FILE ID 165634 

# Chemical Safety Data Sheet (CSDS) RmptyDataFieldsIndicate ThatNOData WereAvailable DatePrinted: 11112/2010 Technical Safety Laboratory, B-320 Room 2103 PhoneExt. 26604 for Inquiries 

# TESTINGIN PROGRESS

REACTIVITY Incompatibility Strong oxidiz€'r IncompatibilityOther Polymerization' Process ReviewComment" Heat ofPoly (JIg): Peroxide #: Peroxide Statement: Miscellaneous Infol]!!1!!;<:lIl: 

## » 

# 6f (") Incident: :T 

### 3**~** IncidentComment: :::I


### .....**~** References:**~**

### ~ CO Summary:**~** CO <0 OtherComments: Peroxide Hrs: Peroxide Temp:

Deflagration and Detonation Potential: 

## en Dl :::I ;::;: ii:j' 

## &**~** iil 

## O· :::I

### ATTACHMENT HEADER SHEET
Attachment Number 014 Attachment Name Acute Toxicity to Zebra Fish S0507 

### Associated PMN Section Number N/A Does not contain CBI



### Report Number KODA101220491061974

Page 90

### Sanitized Version
No.: R2010NC037·01 Environmental Assessment and Pollution



## SPONSOR Intertek(Tianjin)TestingServiceLtd ShanghaiBranch



## REPORTFOR REPORT OFACUTETOXICITYTOZEBRAFISH

## (BRACHYDANIORERIO)
TEST SUBSTANCE: S0507 StudyNo.: S2010NC037-01 

### Report No.: R2010NC037-01


## Study Director: Liu Jining

DateofReportCompletion Dec. 7, 2010

# {~\ Key Lab ofPesticide Environmental Assessmentand Pollution Control,MEP Address: 8Jiang-wang-miaoStreet, Nan/jing210042, China Tel: (+86)2585287074 Fax: (+86) 25 85474630 Page I of28 

### Attachment 14, Page 91Sanitized Version No, R2010NC037-01 Lab ofPesticide Environmental and Pollution


### CONTENTS SPONSORANDTESTFACILITY.........................................................................................................4 STATEMENTOFGLP COMPLIANCE.................................................................................................5 QUALITY ASSURANCE STATEMENT...............................................................................................6 STUDY DETAILS PAGE.........................................................................................................................7 I SUMMARy............................................................................................................................................8 2 INTRODUCTION................................................................................................................................ 10 3 EQUIPMENT& MATERIALS........................................................................................................... 11 3.1 Date ofTest ......................................................................................................................... II 3.2 Test Organism ..................................................................................................................... 11 3.3 Dilution Medium ................................................................................................................. 11 3.4 Apparatus............................................................................................................................. 12 3.5 Reference Substance............................................................................................................ 12 4 TEST DESIGN ..................................................................................................................................... 12 4.1 Preparation ofthe Test Solutions......................................................................................... 12 4.2 Observations and Evaluations ............................................................................................. 13 4.3 Range-finding Test.............................................................................................................. 13 4.4 Definitive Test..................................................................................................................... 14 4.5 Validity ofTest.................................................................................................................... 15 4.6 Stability ofTest Solution and Chemical Analysis............................................................... 15 5 DATA PROCESSING ......................................................................................................................... 17 6 RESULTS ............................................................................................................................................. 18 6.1 Analytical Method for Determination ofS0507 in Water................................................... 18 6.2 Analysis ofS0507 in Test Solutions.................................................................................... 18 6.3 Test Condition ..................................................................................................................... 18 6.4 Mortality and Effects........................................................................................................... 

### 19 6.5 Conclusions ......................................................................................................................... 19 7 HEALTH & SAFETY.......................................................................................................................... 19 8 MAINTENANCE OF RECORDS & DOCUMENTATION .............................................................20 Page 2of28 Attachment 14, Page 92Sanitized Version
No.: R2010NC037-01 Lab ofPesticide Environmental Assessment and Pollution


### 9 REFERENCE ................................_ ......................................................................................................20 TABLES...................................................................................................................................................21 Table I Recovery ofS0507 in Test Medium.............................................................................21 Table 2 Stability Test Results ofS0507 in Test Medium (Definitive Test)..............................21 Table 3 WaterQuality Parameters ofTest Solutions duringthe Definitive Test......................22 Table 4 Toxicity ofPotassium Dichromateto 

### Brachydanio rerio ............................................23 Table 5 Mortality during the Range-finding Test......................................................................23 Table 6 Mortality duringthe Definitive Test.............................................................................24 Table 7 Visual Observations during Definitive Test.................................................................25 Table 8 Characteristics ofthe Dilution Water...........................................................................26 FIGURE ...................................................................................................................................................27 Figure I Calibration Curve for the Test Item ............................................................................27 Figure 2 Standard UPLC-MS/MS Chromatogram ofthe Test Item (lmg/L)............................27 Figure 3 UPLC-MS/MS Chromatogram ofthe Recovery Test Sample (0.1 mg/L)
..................27 

### Figure 4 UPLC-MS/MS Chromatogram ofthe Control Sample (Definitive Test) ...................27 Figure 5 UPLC-MS/MS Chromatograms ofthe Test Item in Definitive Test (1.6 mg/L)
........28

Page 3 of28 Attachment 14, Page 93Sanitized Version
No.: R201ONC037·01 Lab ofPesticide Environmental


### SPONSORAND TEST FACILITY Sponsor: Intertek(Tianjin) Testing Service Ltd Shanghai Branch Address: 2F,BuildingNo.4 Shanghai ComalongIndustrial Park, 889 Yi Shan Road, Shanghai, China, 200233 Contactperson: 

### Li Xangjun Tel: 02160915013 

### Test Substance: S0507

TestFacility: Key Laboratory ofPesticide Environmental Assessment and Pollution Control, MEP (PEAPC) Address: 8 liang-wang-miao Street, Nanjing 210042, China Tel.: (+86) 25 85287074 Fax: (+86) 2585474630



### Legal Representative Person: Gao Zhenning, Director-general, professor Laboratory Management: Shan Zhengjun, professor Head ofDepartment: Shi Lili, professor Study Director: Liu Jining Study Personnel: Wang Lei,TianJing, Wu Guanqun QualityAssurance: Ge Feng

Page 4 of28 Attachment 14, Page 94Sanitized Version
No.: R2010NC037-0J Lab ofPesticide Environmental Assessmenl and Pollution


### STATEMENT OF GLP COMPLIANCE
Study No.: S2010NC037-01 Report No.: R20 1 ONC037-01
According to "OECD Guidelines for testing of chemicals", "The guidelines for the testing of chemical (HJ/T 

### 153-2004)"and "The guidelines of chemical testing good laboratory practices (HJ/T 

### 155-2004)" issued by State Environmental Protection Administration (SEPA) of the People's Republic of China, this experiment was conducted under CMA (China Metrology Accreditation) and CNAS (China National Accreditation Service for Conformity Assessment) experimental conditions at our laboratory. The experimental protocol was strictly carried out in the process of the experiment, and the present report has reflected the experimental results truly and correctly.

(Study Director) Date:

(Laboratory Management) Date:

Page Sof28 Attachment 14, Page 95Sanitized Version
Lab ofPesticide Environmental Assessment and Pollution No.: R20IONC037-0I 

### QUALITYASSURANCE STATEMENT
Study No.: S2010NC037-01 Report No.: R20IONC037-01

This experiment was carried out in accordance with the experimental protocol. It is hereby certified that what the present report describes has accurately reflected the raw data ofthe experiment. Duringthe on-site process, QAU Inspections were perfonned for this study. The dates of Quality Assurance inspection are givenbelow. inspections Phase/Process Inspection Reporting Protocol Sept 10, 2010 Sept 10, 2010 Study Draft Report Dec. 2, 2010 Dec. 2, 2010 Test solutions preparation Oct. 4, 2010 Oct. 4, 2010 Process Observation/Determination Oct. 8,20

(Person responsible for QAU) Date:

Page 6 of28 Attachment 14. Page 96Sanitized Version
Lab ofPesticide Assessment and Pollution Control. MEP No. R2010NC037-0I


### STUDY DETAILSPAGE Study number: Report number: Study title: Test substance: Identity: Chemical Name:
Molecular formula: Molecular weight: Appearance: Storage conditions: Management: Head ofDepartment: Study Director: Person attendingto routine duties and technical queries in the temporary absence ofthe Study Director: Study Directorcontact details:

Location ofstudy:
Study dates Start: Completion: Draft report:

------ ..-- .. 

### S20lONC037-01 R201ONC037-01 Acute Toxicity to Zebra fish 

### (Brachydanio rerio) S0507

S0507 3H-lndolium, 2-[2-[3-[(I,3-dihydro-I,3,3-trimethyl-2H-indol-2­ ylidene)ethyIidene]-2-[(1 -phenyl-IH-tetrazol-5-yl)thio]-1 cyclohexen-I-yl]ethenyl]-l,3,3-trimethyl-, chloride C39H4IN6S'CI 661.31 Solid Room temperature Shan Zhengjun Shi Lili Liu lining Wang Lei

Liu lining Telephone: +862585287091 Facsimile: +8625 85474630 Email:lin@nies.org Key LabofPesticide Environmental Assessment and Pollution Control, MEP 8liang-wang-miao Street Nanjing 210042, liangsu, China Oct. 4, 2010 Nov. 19,2010 Dec. 2, 2010

Page 7of28 Attachment 14, Page 97Sanitized Version
No.: R20IONC037-0I Lab ofPesticide Environmental and Pollution 

### 1SUMMARY Under Semi-static conditions (24h-renewal), the acute toxicity oftest item (S0507) to zebra fish 

### (Brachydanio rerio) was conducted according to the following guidelines: "The guidelines for the testing ofchemicals", SEPA (HJ/T 

### 153-2004); Procedure 203 of the "Guidelines for Testing of Chemicals" ofthe OECO: "Fish, Acute Toxicity Test" (1992) etc. During the whole test period, the pH values ofthe control mediums and test mediums were between 7_36 and 756, and the Dissolved Oxygen**(~O)** 

### values varied from 101% to 108% ofthe air saturation at the test temperature, and the total hardness was in the range of 119 mg (CaCO])/L to 125 mg (CaC03

### )/L. During the test, the temperature of the test mediums were maintained in the range of23.2°C to 23SC, and all fishes in the control group were normal. With the same conditions, K2Cr207 was used as the negative control substance, and the resulting 24 h-LCso 

### was 282 mglL. So the study met the acceptability criteria prescribed by the protocol (pH:**6.0~8.5;** 

### dissolved oxygen concentration: > 

### 60% ofthe air saturation value; total hardness:**1O~250** 

### mg (CaCO])/L; temperature: (23 :::2) DC; 24 h-LCso 

### of K2

### Cr Z

### 07 in the range of 200 to 400 mg/L). 

### Thereforethe test was considered valid. In 

### order to confirm the stability ofthe test item in the test medium, concentrations ofthe test samples during the Definitive Test were analyzed by UPLC-MS/MS. A linear regression equation was obtained with the peak area response (A) vs. the concentration ofthe test item (c, mg/L): A 

### =30811 c -344.13, with good linearity of rJ=0.9992. 

### The results show that linearity for the concentration range of0.01 mg/L 

### to 2 mglL is good. Besides, the minimum detection amount ofUPLC-MS/MSfor S0507 is 5x IO-"g, andthe minimum detection concentration for water sample is 0.01 mglL. The analytical results showed that the concentration ofthe test item is consistent in the test medium throughout the 96-hour test period (deviation within 20%). Thus a Semi-static procedure (24h-renewal) was reasonable. The results showed that under valid Semi-static test conditions (24 h-renewal), the 96 h-LCso 

### ofthe test item to zebra fish is 0.78 mglL (analysed concentration 0.71 mglL), with 95% confidence limit of 0.71 mg/L 

### to 0.85 mg/L. 

### The maximum tested concentration causing no mortality (NOEC) is 0.2 mglL (analysed concentration 

### O. 191 mglL). The lowest tested concentration at which the substance is observed to have a lethal effect (LOEC) is 0.4 mglL (analysed concentration 0.389 mg/L). The minimum concentration causing 100% mortality was 1.6 mglL (analysedconcentration 1.37 mglL).

Page 8of28 Attachment 14. Page 98Sanitized Version


### According to "The guidelines for the hazard evaluation of new chemical substances (HJ/T 154-2004)", S0507 belongs to the category ofvery toxic chemical for zebra fish (Brachydanio redo).

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### Sanitized Version No.. R2010NC031-01 Lab ofPesticide Environmental Assessment and Pollution 

## 2INTRODUCTION This test was designed to determine the acute toxicity oftest item (S0507) to zebra fish 

### (Brachydanio rerio). The test fishes were exposed for 96 hours to the test solution. The study comprised at least one range-findingtest followed by a definitive test to determine, where possible, the 96-hour median lethal concentration (LCso) 

### ofthe test item, with 95% confidence limits. Where no toxicity was seen in the range-finding test, it would be followed by a Limit Test at a single concentration. The study met the requirements of: 

### [1] "Theguidelines for the testing ofchemicals", SEPA (HJ/T 153-2004). [2] HJ/T 

### 154-2004.The guidelines for the hazard evaluation ofnew chemical substances. SEPA. [3] "The guidelines for the testing of chemicals", Beijing: China Environmental Sciences Publishing House. 2004. SEPA. [4] Part C.l (Acute Toxicity for Fish) of EC Methods for the Determination of Ecotoxicity;
- Annex to Council Regulation (EC), L142 (2008). [5] Procedure 203 ofthe 'Guidelines for Testing of Chemicals' ofthe OECD: "Fish, Acute Toxicity Test" (1992). [6] Ecological Effects Test Guidelines, OPPTS 850.1075, Fish Acute Toxicity Test, Freshwater and Marine. EPA 712-C-96-118, April 1996. 

### TheGuide for Careand lise ofLaboratory Animals (1988) The in-life experimental procedures undertaken during the course of this study were subject to the provisions ofthe Guide for Care and Use ofLaboratory Animals (1988) in China. The Guide, administered by the Ministry of Science and Technology of the People's Republic ofChina, regulates all scientific procedures in living animals which may cause pain, suffering, distress or lasting harm and provides for the designation of establishments where procedures may 

### be undertaken, the licensing oftrained individuals who perform the practical techniques and the issue of project licences for specified programmes ofwork. This study complied with all applicable sections ofthe Guide and the associated Codes ofPractice for the Housing and Care ofAnimals used in Scientific Procedures. The number of animals used was the minimum that was consistent with scientific integrity and regulatory acceptability, consideration having been given to the welfare of individual animals in terms ofthe number and extent ofprocedures to be carried out on each animal.
Page ]0 of28 

### Attachment 14, Page 

### 100

### Sanitized Version No. R2010NC037-01 LabofPesttclde Environmental Assessment and Pollution 

## 3EQUIPMENT & 

## MATERIALS 3.1 Date ofTest Oct. 4, 2010**~**

### Nov. 19,2010 

### 3.2 Test Organism The test species of Zebra fish, 

### Brachydanio rerio, were obtained as fry from a commercial fish supplier ofGuangzhou Hongfa Aquatic Animals Culture Company in China. Details concerning the source ofthe fish were recorded in the raw data. Feeding fry were held for 14 days in holding tanks supplied with a continuous flow of aerated waterbeforebeing used for testing. Fish to be used in thetest was held for 7 days in water ofthe quality andtemperature to be used in thetest. A photoperiod of 16 hours light, provided by overhead fluorescent tubes, and 8 hours dark was maintained. The oxygen concentration was about 98% of the air saturation value. The fish was fed daily during the holding period on proprietary fish food. They were held without food for approximately 24 hours before being placed into the test vessels. The ingredients ofthe fish food are given as follows: Crude Protein >49.0% Crude Fat> 5.0% Crude Fibre < 

### 3.0% Crude Ash < 

### 12.0% Moisture 

### < 10.0% During the holding period the tanks was inspected daily and any debris or unhealthy or dead fish removed. After the 48 hour settling-in period, no mortality was observed in the following 7 days. So this batch offish was accepted (Batch No. F2010091 I). The wet-weight ofthe fish used to the test was 0.19 g in average, with an average length of2.3 cm. 

### 3.3 Dilution Medium Good quality tap waterwhich had been dechlorinated for at least 24 hours was used. The total hardness ofthe test water was 122.2 mg (CaC03

### )/L, oxygen concentration was Page 11 of28 

### Attachment 14, Page 101

### Sanitized Version
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### about 98% of the air saturation value and pH was 7.55 at room temperature. Characteristics of the dilution water are measured at least twice a year by Jiangsu Provincial Center for Disease Prevention and Control. The latest measuring result is showed in Table 8. 

### 3.4 Apparatus Normal laboratory apparatus and: (a) Oxygen meter (HACH HQ30d. The Dissolved Oxygen can be directly read by immersing the probe in the water sample when the reading is stable.); (b) Thermometer; (HACH HQ30d. The Temperature can be directly read by immersing the probe in the water sample when the reading is stable.); (c) Equipment for determinationofhardness ofwater (Model: 16900, made by HACH company, the hardness can be directly read by immersing the probe in the water sample when the reading is stable.); (d) Tanks made of chemically inert material, with a sealable inert lid, and with a capacity ofapproximately 8 L(Sanhe Zuping Glass Instrument Factory, Haimen); (e) Thermostatic waterbath (Chang Yuan Medical Instrument Factory,Jiangsu); 

### 3.5 Reference Substance Reference substance: Potassium dichromate, K2Cr207, CAS: 7778-50-9; purity: 2':99.8%; Lot number: 10011460037; NanjingChemical Reagent Co.Ltd. The test with the reference substance is performed at least once a year as a means of assuring that the laboratory test conditions are adequate and have not changed significantly. The most recent test was performed in July 2010. The results ofthis study (archivedunder Project numberS20IONCOI2) are shown in Table4. 

### 4 TESTDESIGN 4.] Preparationofthe Test Solutions In the range-finding test, the test solutions ofS0507 were prepared by directly dissolving appropriate amount ofS0507 in dilution medium and then facilitating its dispersion by ultrasonication for 30 min. In the definitive test, stock solution ofthe test substance (1000 mg/L) 

### was prepared by dissolving 0.1006 g S0507 into 100 mL test water. The test solutions were prepared by dilutingthe stocksolution. Details about the Preparations are showed as follows: Nominal The Amountof Dilution Medium Test Type Concentration The Test Volume (L) Page 12 of28 

### Attachment 14, Page 102Sanitized Version

. R20IONC037·0I 

### (mglL) Substance Added (g) Range-finding Test 0 0 5 0.005 5 10 

### 0.051 5 100 0.502 5 Nominal The volume of Dilution Medium Test Type Concentration The stock Solution Volume (L) (mglL) Added (mL) Definitive Test 0 0 5 0 0 5 0 0 5 0.1 0.5 5 0.1 0.5 5 0.1 0.5 5 0.2 5 0.2 5 0.2 I 

### 5 0.4 

### 2 5 0.4 2 5 0.4 

### 2 5 0.8 4 5 0.8 4 5 0.8 4 

### 5 

### 1.6 8 

### 5 

### 1.6 8 5 

### 1.6 8 5 

### 4.2 Observations and Evaluations During the test, 

### all kinds ofabnormal responses ofthe fish observed would have been recorded, such as mortality, inactivity, strange swimming pattern, other abnormal behaviour, etc.. Fish would have been considered dead ifthere is no visible movement (e.g. gill movements) and iftouching ofthe caudal peduncle produces no reaction. 

### 4.3 Range-finding Test The range-finding test, carried out under static conditions, was regularly conducted to determine the range ofconcentrations for the subsequent test. In the range-finding test, groups offish (5 pergroup) were exposed to the test solutions with nominal concentration of 1 mglL, 10 mglL and 100 mglL. Synchronously one control group was conducted in test water without the test item. For each test tank (Total Page 13 of28 Attachment 14, Page 103Sanitized Version
Lab ofPesticide Environmental 

### volume: 8 L) 5 Ltest solution was filled in. No replicates were used. The test fish were be randomly chosen and put in different test solutions after the temperature has been adjusted to the required value. This was done in 30 min. Duringthe test, the following conditions were maintained:

-Light: 16 hours photoperiod daily (light intensity: 1000to 1500 lux); -Temperature: 23.2 °C 

### to 23.5 DC; 

### -Oxygen concentration: 90%to 102% ofthe airsaturation; -Feeding: none. Test duration was 96 hours. Dead fish was removed at least once daily and discarded. The mortalities of the fish were recorded at 24-h, 48-h, 72-h and 96-h, and then the maximum concentration causing no mortality (NOEC) and the minimum concentration causing 100% mortality were determined. 

### 4.4 Definitive Test Semi-static method (24h-renewal) was adopted in Definitive Test according to the stability of the test solution indicated by Table 2. Based on the results of the range-findingtest, test concentrations of0.1 mglL, 0.2 mglL, 0.4 

### mg/L, 0.8 

### mg/L and 1.6 

### mg/L were assigned in Definitive Test. Synchronously one control group was used in the test. Three replicates were assigned for each treatment group and control group, while the initial number oftesting fish was 10 for each replicate. The test fish were be randomly chosen and put in different test solutions after the temperature has been adjusted to the required value. This was done in 30 min. Duringthetest, the following conditions were maintained:

-Light: 16 hours photoperiod daily (light intensity: 1000 to 1500 lux); -Temperature: 23.2 °C 

### to 23.5 DC; 

### -Oxygen concentration: 101 % to 108% ofthe air saturation; -Feeding: none. At24-h, 48-h, 72-h and 96-h, the mortalities ofthe fish were recorded, and observations on individual behaviour were performed. Meanwhile, measurements of pH, dissolved oxygen and temperature were carried outand recorded daily.

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### Sanitized Version R201OJ-:C037-0I 

### 4.5 Validity ofTest 4.5.1 Control group A control group, comprising the same number of fish as that exposed at each test concentration, was placed into test water alone. 4.5.2 Reference substance test With the conditions maintained as before, K2Cr207 was be used as the test substance and the resulting 24 h-LCso

### was 282 mgiL The results ofthis study are shown in Table 4. 4.5.3 Fish loading 0.2 g to 0.6 g fish (wet weight) per litre oftest medium. 4.5.4 Validity oftest result During the whole test period, the pH values ofthe control mediums and test mediums were between 7.36 and 7.56, and the Dissolved Oxygen (DO) values varied from 101% to 108% ofthe air saturation at the test temperature, and the total hardness was in the range of 119 mg (CaCO})/L 

### to 125 mg (CaCO})/L During the test, the temperature of the test mediums were maintained in the range of23.2°C to 23.5°C, and all fishes in the control group were normal. With the same conditions, K2Cr207 was used as the negative control substance, and the resulting 24 h-LCso 

### was 282 mgiL So the study met the acceptability criteria prescribed by the protocol (pH: 6.0-8.5; dissolved oxygen concentration: > 

### 60% ofthe air saturation value; total hardness: 10-250 mg (CaCOJ)/L; temperature: (23 ±2) 24 h-LCso 

### of K2Cr207 in the range of 200 to 400 mg/L). 

### Therefore the test was considered valid. 4.6 Stability ofTest Solution and Chemical Analysis 4.6.1 Preparation ofstandard stock solution Storage solution I ofthe test substance (1000 mgiL) was prepared by dissolving 0.05 g S0507 into 50 mL methanol. The standard stock solution II oftest substance (10 mgiL) for the calibration curve was prepared by diluting 1mL ofsolution Iwith methanol to atotal volume of 100 mL. The standard stock solution III oftest substance (0.1 mgiL) for the calibration curve was prepared by diluting 1mL ofsolution II with methanol toa total volume of 100 mL. 4.6.2 Working solution

Page 

### is of28 

### Attachment 14, Page 105Sanitized Version
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### Prepare the standard working solution of 0.0I to 2 mg/L by drawing and diluting the above storage solutions with Mobile phase (Methanol: water 80:20 (v:v)). Details of the working solutions are showed as follows: The Concentration TheVolume ofthe Final Volume after Concentration ofthe Storage Storage Solution Dilution (mglL) Solution Added Added (mL) (mglL) (mL) 0.01 0.1 I ]0 0.02 0.1 2 10 0.05 0.1 5 10 0.1 10 0.1 10 0.2 10 0.2 JO 0.5 JO 0.5 10 10 I 10 2 JO 2 10 4.6.3 UPLC-MS/MS conditions Apparatus: ACQUITY RTM ultra Perfonnance LC (Waters, USA) Column: ACQUITY UPLC® BEH CI8 i.7!lm, 2.1 mmx50 mm (Waters, USA) Detector: Quattro PremierXE MS-MS (Waters, USA) Mobile phase: Methanol: water = 

### 80:20 (v:v) (containing0.1

### % Fonnie acid) Column Temperature: 30°C Flow rate: 0.3 mLimin Injection volume: 5 ilL MS/MS detection parameters are as follows: Data type: MRM data Ionisation mode: Electrospray Polarity: Positive Capillary: 3.0 kV, Extractor: 2.0V, RF Lens: 0.3 V Source Temperature: I10°C,Desolvation Temperature: 380°C Cone Gas Flow: 50 Llh, Desolvation Gas Flow: 500 Lih LM Resolution I: 13.0, LM Resolution 2: 13.0 HM Resolution I: 13.0, HM Resolution 2: 13.0 Ion Energy 1: 0.4, Ion Energy 2: 2.0Page 16 of28 Attachment 14, Page 106Sanitized Version Lab ofPesticide 

### Collision Gas (Pressure): 3.58e·3 

### mbar Parent (m/z) 

### Daughter (m/z) 

### Dwell (s) Cone Volt. (V) Col. Energy (eV) 625.9 479.44 0.100 35 20 Under the above conditions, the retention time ofS0507 was about 0.64 min (see Fig. 2). 4.6.4 Sampling and analysis ofthe test solution Samples were taken (at least in duplicate) from each concentration at the beginning and for each renewal during the Definitive Test (at 0 h, 24 h(before/after renewal), 48 h(before/after renewal), 72 h(before/after renewal) and 96 h). On each occasion, one sample was analysed after certain pre-treatments; the remaining samples were retained in casefurther analysis would be required. 4.6.5 Pre-treatment method ofthe sample Water samples collected were filtrated by 0.22 j..lm millipore membrane and then the filtrates were analysed by UPLC-MS/MS. 

### 5 DATAPROCESSING Korbor processing method should be used to calculate the LCso 

### and LC50 

### confidence limits. (1) 

### LCso calculate formula Formula (I) 

### Where, LCso-the concentration leadingto 50% mortality ofthe fish (mg/L); 

### Xm--Iogarithm ofhighest concentration; i-logarithm oftwo concentration that is next; I;P-sum ofall treatment mortality (expressed as decimal). (2) LCso Calculate confidence limits (P=0.95) formula Formula(2) Where, p--mortality in one treatment; q-l-p; i-logarithm oftwo concentration that is next; n-numberoffishes in every treatment. Confidence 

### limits (P

## =0.95) of log(LCso

## )= log(LCso

## )± 1.96Slog(LCso ) Page 17 of28 Attachment 14, Page 107

### Sanitized Version No,: R2010NC037·0I Lab ofPesticide 

## 6RESULTS 6.1 Analytical Method for Determination ofS0507 in Water (I) Calibration curve A series ofstandard solutions with concentration at 0.01 mglL, 0.02 mglL, O.OS mg/L, 0.1 mglL, 0.2 mglL, O.S mglL, I mg/L and 2 mglL were measured under the UPLC-MS/MS conditions mentioned above, Based on the test result, a linear regression equation was obtained between the concentration and the area ofthe peak emerged at 0.64 min: 

### A =30811 c -344,13, with good linearity of 

### r 2

### =0.9992, where 

### A represents peak area; and c is the concentration ofthe test item (mglL) (See Figure 1). The results showthat I inearity for concentration range of0.0I mg/L to 2 mg/L is good. (2) Recovery & 

### Precision The recovery samples with concentrations at 0.1 mglL and 2 mglL were prepared by adding 0.1 mL and 2 mL ofstandard stock solution (10 mglL in methanol) to test water (IOmL) and then the solutions obtained were filtrated by 0.22 f.lm millipore membrane and then the filtrates were analysed by UPLC-MS/MS. Measurements obtained from the recovery test were shown in Table I. Figure 3 showed the chromatograph ofthe recovery sample from the recovery test. The recovery rate was 1**02~** 

### I04% among the concentration range from 0.1 to 2 

### mgiL. The relative standard deviation was between**4.81~S.S2 %.**  

### (3) Detection limit The minimum detection amount of UPLC-MS/MS for SOS07 is SxIO· ll

### g, and the minimum detection concentration for water sample is 0.01 

### mgiL. 6.2 Analysis ofS0507 in Test Solutions The analyzed results for the test samples from the Definitive Test are given in Table 2. Figure 4 and Figure S showed the chromatographs ofthe control sample and the treated sample from the Definitive Test. The results indicated that concentration of SOS07 was stable (within 80% ofthe initial concentration) in the water during the test period. Thus Semi-static method (24h-renewal) used in the Definitive Test was reasonable. 

### 6.3 TestCondition During the Definitive Test, the pH, dissolved oxygen concentration, total hardness and temperature ofthe control and treatmentgroups were showed in Table 3. During the whole test period, the pH values ofthe control mediums and test mediums were between 7.36 and 

### 7.S6, and the Dissolved Oxygen (DO) values varied from 101% Page 18 of28 

### Attachment 14, Page 108Sanitized Version Lab ofPesticide**Fnvim""n~nl,"1 A<"~""nent**  No.: R20!ONC037·01


### to 108% ofthe air saturation at the test temperature, and the total hardness was in the range of 119 mg (CaCO])/L to 125 mg (CaCO])/L During the test, the temperature of the test mediums was maintained in the range of23.2°C to 23.5°C. 6.4 Mortality and Effects 

### Table 5 and Table 6 show the mortality data during the range-finding test and Definitive Test respectively. Table 7 showedthe observations duringthe Definitive Test. All fish in the control were alive and appeared normal. The treated fishes were observed to be lying on side orback, orabnormally swift swimming and Tumbling with the test concentration no less than 0.4 mglL No fish died in treatments of0.1mglL and 0.2 mglL All Fishes were dead after96h-exposure in treatments of 1.6 mglL. 6.5 Conclusions The results showed that under valid Semi-static test conditions (24 h-renewal), the 96 ofthe test item to zebra fish is 0.78 mglL (analysed concentration 0.71 mglL), with 95% confidence limit of 0.71 mglL to 0.85 mglL The maximum tested concentration causing no mortality (NOEC) is 0.2 mglL (analysed concentration 0.191 mg/L). The lowest tested concentration at which the substance is observed to have a lethal effect (LOEC) is 0.4 mglL (analysed concentration 0.389 mglL). The minimum concentration causing 100% mortality was 1.6 mglL (analysed concentration 1.37 mglL). LC50 

### 0.78 mg/L (analysed concentration0.71 mglL); NOEC 0.2 mglL (analysed concentration 0.191 mglL); LOEC 0.4 mg/L (analysed concentration 0.389 mg/L); The minimum concentration causing 100% mortality = 

### 1.6 mg/L (analysed concentration 1.37 mg/L). 

### According to "The guidelines for the hazard evaluation of new chemical substances (HJ/T 

### 154-2004)", S0507 belongs to the category ofvery toxic chemical for zebra fish 

### (Brachydanio rerio). 7 

### HEALTH & 

### SAFETY (n order for PEAPC to comply with Law of the People's Republic of China on the Prevention and Treatment of Occupational Diseases 200I, and the current Control of Substances Hazardous to Health Regulations, it is a condition ofundertaking the study that the Sponsor provide PEAPC with all information available to it regarding known or potential hazards associated with the handling and use ofany substance supplied by the Sponsor to PEAPC. The Sponsor also complied with all current legislation and Page 190f28 Attachment 14, Page 109Sanitized Version No.. R201ONC037·01 Lab ofPesticide Assessment and Pollution 

### regulationsconcerning shipmentofsubstancesby road, rail, seaorair. Such information in the form of a completed PEAPC test item data sheet must be received at PEAPC before the test item can be handled in the laboratory. 

### 8 MAINTENANCE OFRECORDS & DOCUMENTATION All raw data arising from the performance ofthis study will remain the property ofthe Sponsor. Records and documentation relating to 

### this study (including electronic records) will be maintained in the archives ofPEAPC for a period offive year from the date on whichthe Study Director signs the final report. This includes the Study Protocol, raw data, a copy ofthefinal report. Types of sample which are unsuitable, by reason of instability, for long term retention and archiving will be disposed ofafter the periods stated in PEAPC Standard Operating Procedures. Test item remaining will be retained by PEAPC in its archive for a period of one year from the date on which the Study Director signs the final report. After such time, the Sponsor will be contacted and his advice sought on the return, disposal or further retention ofthe materials. 

### Ifrequested, PEAPC will continue to retain the materials subject to a reasonable fee as agreeableto the Sponsor. PEAPC will retain the Quality Assurance records relevant to this study and a copy ofthe final report in its archive indefinitely. 

### 9 REFERENCE [I]OECD. 203 Fish, Acute Toxicity Test. Paris: 17 July 1992. [2] SEPA. The guidelines for thetesting ofchemicals. HJ/T 

### 153-2004.2004. [3] SEPA. The guidelines for the hazard evaluationof new chemical substances. HJ/T 

### 154-2004. 2004. [4]SEPA. The guidelines for the testingof chemicals. Beijing: China Environmental Sciences Publishing House. 2004. [5]Part C.I (Acute Toxicity for Fish) of EC Methods for the Determination of Ecotoxicity;
- Annex to Council Regulation (EC), L142 (2008). [6] Ecological Effects Test Guidelines, OPPTS 850.1075, Fish Acute Toxicity Test, Freshwater and Marine. EPA 712-C-96-118, April 1996.

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### TABLES Table 1 Recovery ofS0507 in Test Medium Mean Recovery RSO Nominal Measured Recovery rate (%) (%) 

### Concentration (mg/L) 

### Concentration (mg/L) Rate (%)


### 102



### Table 2 Stability Test Results ofS0507 in Test Medium (Definitive Test) -------, 

### AnalysedConcentration (mg/L) 

### Nominal 24 h 48 h 72 h Concentration (mglL) Oh (beforelafter renewal) (before/after renewal) (before/after renewal) 96 h
0 NO.G.l NO. ND. NO. NO. ! 

### 0.1 0.103 0.094/0.096 0.089/0.103 0.0910.100 0.089 I 

### 0.2 0.4 i 

### 0.185 0.410 0.186/0.184 0.380/0.379 0.184/0.208 0.378/0.440 

### 0.185/0.215 0.378/0.368 0.184 0.376 0.8 ! 

### 0.790 0.753/0.685 0.736/0.859 0.739/0.664 0.730 I 1.6 I 

### 1.61 1.40/1.31 1.384/1.29 

### 1.34311.33 i 

### 1.31 G.lNO: not detected, since belowthe sensitivity ofthe analytical method.

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### Table 3 Water Quality Parameters ofTest Solutions duringthe Definitive Test Nominal I 

# I ,Dissolved 

### I
...----, , Concentration 

# I : Temperature i Hardness Duration(h) pH CC) oxygen i (mg/LCaC03) (mglL) 

### (%) 0 I 7.46 23.5 102 125 24(expired/fresh) 

### 7.4417.45 23.5/23.4 1011105 

### 120/121 

### I 0 i

### 48(eXPired/fre~ 7.5017.48 23.2123.3 1041102 

### 120/120 

### I 72(expired/fres 

### 7.5117.46 23.4123.3 101/103 1211122 i 96 7.48 23.5 101 119 

### I 0 7.51 

# t: 23.5 1031104 120 24(expired/fresh) 

### 7.4817.50 23.5/23.4 1061103 i 120/121 0.1 48(expired/fresh) 

### 7.5217.52 23.2/23.3 1041102 

### 121/120 I**~?2(** expired/fresh) 

### 7.5517.52 23.4123.3 101/103 1221121 

### I 96 7.53 23.5 01 121 0 7.53 23.5 

### 1021104 120 ,-­ 24(expired/fresh) 

### 7.5617.50 23.5/23.4 1051103 121/120 0.2 48(expired/fresh) 

### 7.5317.52 23.2/23.3 1041105 1191120 72( expired/fresh) 

### 7.5517.55 23.4123.3 1011104 1201121 -" 96 7.36 23.5 102 121 0 7.52 23.5 104 120 24(expired/fresh) 

### 7.5517.50 23.5123.4 1011102 1211120 0.4 

# I 48(expired/fresh) 

### 7.4817.52 23.2/23.3 101/103 1191121 • 72(expired/fresh) 

### 7.5217.54 23.4/23.3 1021105 

### 120/122 

# r 96 7.48 23.5 102 121 0 7.55 23.5 106 119 24(expired/fresh) 

### , 7.5317.52 23.5/23.4 104/103 1201121 0.8 48(expired/fresh) 7.46/7.50 

### 23.2/23.3 1011103 121/120 72(expired/fresh) 

### 7.5017.52 23.4/23.3 101/102 122/120


### _ .... 96 7.49 23.5 108 121 0 7.56 23.5 104 119 24(expired/fresh) 

### 7.5517.54 23.5/23.4 101/102 

### 120/121 

### 1.6 48(expired/fresh) 

### 7.4517.53 23.2/23.3 1011103 1211122 

# I 72(expired/fresh) 

### 7.5217.55 23.4/23.3 1001102 

### 122/121 96 7.50 23.5 101 121

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### Table4 ToxicityofPotassium Dichromateto Brachydanio rerio
! ! ! 

### TheNumberofthe Dead Concentration Number 

### I I (mg/L) 

### ofFish 6h 12 h 18 h 24 h i I 

### 10 0 0 0 0 0 

### I 

### 10 0 0 0 0 l

, 

### 10 0 0 0 0 I 

### 10 0 0 0 0 

# =J 100 10 0 0 0 0 

### 10 0 0 0 0 I 

### 10 0 1 2 2 200 10 0 2 3 3
i 

### 10 0 0 1 2 i I 

### 10 0 2 3 4 300 

### 10 1 3 3 4 

### 10 I 3 4 5 

### I 10 1 3 6 

### I 7 

### 400 

### 10 2 4 6 7
i 

### 10 2 4 7 

### 8 i 

### \0 3 6 9 10 500 

### 10 3 6 10 10 

### \0 2 4 

### \0 10 LCso 

### (mglL) >500 480 311 282 95%confidence limit (mgiL) 

## - 427**~** 

### 538 292
- 331 265
- 300 i



### Table 5 Mortalityduringthe Range-findingTest TheNumberofthe Dead Fish Nominal Concentration Initial Number (mg/L) 

### ofFish 24h 48h 72h 96 h 0 5 0 0 0 0 I 5 0 4 5 5 10 5 5 5 5 5 100 5 5 i 

### 5 5 5

Page 23 of28 

### Attachment 14, Page 113Sanitized Version
No. R2010NC037·01 Lab ofPesticide Environmental



### Table6 Mortality during the Definitive Test Nominal Analysed Initial The Numberofthe Dead Fish Concentration Concentration• Number (mglL) (mglL) ofFish 24 h 48 h 72h 96 h 10 

### 0 0 0 0 0 ND i 

### 10 0 0 0 0 10 0 0 0 0 10 0 0 0 0 0.1 0.0955 10 

### 0 0 0 0 10 0 0 0 0 10 0 

### I 0 

# D 0 0.2 0.191 10 0 A 

### 0 0 I 

### 10 0 0 0 0 10 0 0 ) 

### 2 0.4 0.389 10 0 0 1 2 ! 10 

### 0 0 0 I 

### IO 0 1 2 4 0.8 

### i 0.745 10 

### 0 0 I 

### 3 I 10 0 0 I 

### 2 4 I 10 

### 0 9 

### IO 10 1.6 1.37 10 

### 0 9 10 10 10 

### 0 10 

### 10 10 LCso 

### (mg/L)(nominal) > 1.6 1.15 0.96 0.78 95% confidence limit (mglL) (nominal) 

# - 1.12-1.18 0.90-1.02 0.71-0.85 I LCso 

### (mglL)(analysed) >1.37 1.02 0.87 0.71 

# I 95%confidence limit (mglL) (analysed) 

## - 1.00-1.05 0.82-0.92 0.66-0.771 The average ofthe analysed concentrations at O-h, 24-h, 48-h, 72-h, 96-h. ND: notdetected, sincebelow the sensitivity ofthe analytical method.

Page 24 of28 Attachment 14, Page 114Sanitized Version
Lab "fP"o,i,·iAe Envlfomnental Assessment and Pollution No.: R2010NC037·01



### Table 7 Visual 

### Observations during Definitive

### Test

! 

### Nominal Visual Observations I 

# I Conceot'"tjon 

# I No. i i (mg/L) 

### 24 h 48 h 72h 96 h 

### I #1 NB NB NB NB 

# ° #2 NB NB NB NB

• 

### #3 NB NB NB NB #1 NB NB NB NB I 

### 0,1 ! 

### #2 NB NB NB NB #3 NB NB NB NB #1 NB NB NB NB 0.2 I 

### #2 NB NB NB NB #3 NB NB NB NB #1 NB AS SR&AS SR&AS 0.4 #2 NB AS SR&AS SR&AS #3 NB AS SR&AS SR&AS i I 

### #1 TS TS&AS SR&AS i 

### SR&AS 0.8 #2 TS TS&AS SR&AS SR&AS I 

### #3 TS TS&AS SR&AS SR&AS #1 TS TS&AS Dead Dead I 

### 1.6 #2 TS TS&AS Dead Dead 

### i #3 TS Dead Dead Dead Note: Abbreviations ofsymptoms ofintoxication described in the table: AK-Strongextended gills OB-Fish mainly atthe water surface AP-Apathy SA-Mucous secretion BA-Distendedabdomen SR-Fish lying on side or back FV-Finsfrayed out at the border SV-Strongventilation GA-Exophthalmus TS-Tumbling during swimming KR-Convulsions CC-Colorchanging NB-Normal behaviours AS-Abnormally swift swimming

Page 25 of28 Attachment 14, Page 115Sanitized Version Lab ofPesticideEnvironmental and Pollution No
.. R2010NC037-01



### Table 8 Characteristics ofthe Dilution Water Items Analyzed value Acceptable value As 

### Cd <0.001 

### mg 

### IL :::;0.01 

### mg 

### IL :::;0.005 

### mg 

### IL Cr6+ 

### Pb <0.000 I 

### mg

### IL :::;0.05 

### mg 

### IL :::;0.01 

### mg 

### IL Hg AI <0.004 

### mg

### IL :::;0.001 

### mg 

### IL :::;0.2 

### mg

### IL Fe 

### Mn <0.001 

### mg 

### IL :::;0.3 

### mg 

### IL :::;0.1 

### mg 

### IL Cu 

### Zn <0.0002 

### mg

### IL :::;1.0 

### mg

### IL :::;1.0 

### mg 

### IL Ni 0.01 

### mg 

### IL :::;0.02 

### mg 

### IL Ag 

### pH <0.03 

### mg 

### IL :::;0.1 

### mg 

### IL 6.5-8.5 

### mg 

### IL The total hardness Visible substance <0.001 

### mg 

### IL :::;450 

### mg (CaC03)/L None methyl parathion 0.002 

### mg

### IL :::;0.02 

### mg 

### IL malathion 0.25 

### mg

### IL :::;0.25 

### mg 

### IL Parathion 0.001 

### mg 

### IL :::;0.003 

### mg 

### IL Co Total organic carbon (TOC) < 0.001 

### mg 

### IL 7.55 

### mg 

### IL 122.2 

### mg 

### IL None < 0.001 

### mg 

### IL
<0.0005 

### mg

### IL
< 0.001 

### mg 

### IL
< 0.001 

### mg 

### IL 1.91 

### mg 

### IL 

# - :::;5 

### mg 

### IL

Page 26 of28 Attachment 14, Page 116Sanitized Version

No., R20IONC037·0I Lab ofPesticide Environmental Assessment and Pollution 

### FIGURE

u.s 15 2.5 Coocentrauon (fIlY1.) 

### Figure 1Calibration Curve for the Test Item**""'=~-~~---.......,----m(r.** 1.50 

### Figure 2 Standard UPLC-MS/MS Chromatogram ofthe Test Item (1

### mglL)

Figure 3 UPLC-MS/MS Chromatogram ofthe Recovery Test Sample (0.1 mg/L)

'0-**5~O~~-l,O""'O~~~1.5ri O-~-2** **0~O~""-~2.""50-'-'--** mir 

### Figure 4 UPLC-MS/MS Chromatogram ofthe Control Sample (Definitive Test) Page 27 of28 Attachment 14, Page 117Sanitized Version

No.: R2010NC'037-01 Lab ofPeslieide Environmental Assessment and Pollution

1(J[J

# i

oh(fresh) 24 h(expired)

100 1.50 2.00 0.50 

### 24 h(fresh) 96 h(expired) Figure 5 UPLC-MS/MS Chromatograms ofthe Test Item in DefinitiveTest (1.6 mglL)

Page 28 of28 Attachment 14, Page 118

### ATTACHMENT HEADER SHEET
Attachment Number 015 Attachment Name Ready Biodegradation Test S0507 

### Associated PMN Section Number N/A Does not contain CBI



### Report Number KODA101220491061974



### Page 119

### Sanitized Version Lab ofPesticide Environmental and



## SPONSOR Intertek(Tianjin)Testing ServiceLtd ShanghaiBranch

Reportfor Ready Biodegradation Test ( Closed Bottle Method)

TestSubstance: S0507 Study No.: S2010NC037-02 Report No.: R2010NC037-02


## Study Director: Liu Jining

DateofReportCompletion Dec. 7,2010

,:;0

### " 

## g Key LabofPesticideEnvironmentalAssessment andPollution Control,MEP Address: 8Jiang-wang-miaoStreet, Nanjing210042, China Tel: (+86)2585287074 Fax: (+86) 25 85474630 Page 1of 16 

### Attachment 15, Page 120Sanitized Version
No.: R201ONC037·02 Assessment 

### CONTENTS SPONSOR AND TEST FACILITy.............................................................................................................3 STATEMENTOF GLP COMPLIANCE ....................................................................................................4 QUALITY ASSURANCE STATEMENT ..................................................................................................5 STUDY DETAILS PAGE............................................................................................................................6 I SUMMARY...............................................................................................................................................7 2 INTRODUCTION .....................................................................................................................................8 3 SAFETY PRECAUTIONS........................................................................................................................9 4 EQUIPMENT & 

### MATERIALS................................................................................................................9 4.1 Date ofTest..............................................................................................................................9 4.2 Inoculum................................................................................................................................... 9 4.3 Apparatus .................................................................................................................................9 4.4 Preparation ofthe Test Solutions .............................................................................................9 4.5 Preparation ofthe Test Medium............................................................................................. 10 

### 5 TEST DESIGN......................................................................................................................................... 10 

### 5.1 Test Methods.......................................................................................................................... 10 

### 5.2 Validity ofTest....................................................................................................................... 11 6 DATA PROCESSING............................................................................................................................. II 6.1 Calculation ofTheoretical Oxygen Demand.......................................................................... 11 6.2 Calculation ofOxygen Consumption..................................................................................... 12 6.3 Calculation ofPercentage Biodegradability........................................................................... 12 7 RESULTS................................................................................................................................................. ]2 7.1 Test Conditions....................................................................................................................... 12 7.2 Conclusions............................................................................................................................ 12 8 HEALTH & 

### SAFETY ............................................................................................................................. 13 9 MAINTENANCE OF RECORDS & DOCUMENTATION................................................................. 13 10 

### REFERENCES....................................................................................................................................... 13 Table 1Concentrations ofDissolved Oxygen (DO) .................................................................... 15 Table 2 Biodegradation ................................................................................................................ 15 Figure 1Biodegradation curve..................................................................................................... 16

Page 2 of 16 Attachment 15, Page 121Sanitized Version No: R2010NC037-02 Lab. ofPesticide Environmental Assessment and Pollution 

### SPONSOR AND TEST FACILITY Sponsor: Intertek(Tianjin) Testing ServiceLtd Shanghai Branch Address: 2F,BuildingNo.4 Shanghai Comalong Industrial Park, 889 Yi Shan Road, Shanghai, China, 200233 Contactperson: Li

### Xangjun Tel: 02160915013


### TestSubstance: S0507

TestFacility: Key Laboratory ofPesticide Environmental Assessment and Pollution Control, MEP (PEAPC) Address: 8Jiangwangmiao Street, Nanjing 210042, China Tel.: (+86) 2585287074 Fax: (+86) 25 85474630


### Legal Representative Person: Gao Zhenning, Director-general, professor Laboratory Management: Shan Zhengjun, professor Head ofDepartment: ShiLiIi, professor Study Director: Liu Jining Study Personnel: Wu Guanqun, TianJing Quality Assurance: GeFeng, assistant professor

PageJ of 16 Attachment 15, Page 122Sanitized Version
No.: R201ONC037-02 Lab. ofPesticide Environmental Assessment and Pollution



### STATEMENT OF GLP COMPLIANCE
Study No.: S2010NC037-02 Report No.: R2010NC037-02 According to "OECD Guidelines for testing of chemicals", "The guidelines for the testing of chemical (HJ/T 153-2004)"and "The guidelines of chemical testing good laboratory practices ( (HJ/T 

### 155-2004) " issued by State Environmental Protection Administration (SEPA) ofthe People's Republic of China, this experiment was conducted under CMA (China Metrology Accreditation) and CNAS (China National Accreditation Service for Conformity Assessment, CNAS) experimental conditions at our laboratory. The experimental protocol was strictly carried out in the process ofthe experiment, and the present report has reflected the experimental results truly and correctly.

(Study Director) Date:

(Laboratory Management) Date:

Page4 of 16 Attachment 15, Page 123Sanitized Version
No.: R2010NC037·02 Lab. ofPesticide Assessment and Pollution 

### QUALITY ASSURANCE STATEMENT
Study No.: S2010NC037-02 Report No.: R20IONC037-02

This experiment was carried out strictly in accordance with the experimental protocol. It 

### is hereby certified that what the present report describes has accurately reflected the raw data ofthe experiment.

Type of Phase/Process inspections Start inspection date Date i 

### End 

### inspection date Reportingdate Protocol Study Draft Report i 

### Process Measure Sept. 6 2010 Dec. 1,2010 Oct. 8,2010 Sept. 62010 Sept. 6 2010 Dec. 1,2010 Dec. 1,2010 Oct. 8,2010 I 

### Oct. 8, 2010 i



### (Person responsible for QAU) Date:

Page 5ofl6 Attachment 15, Page 124Sanitized Version
No.: R2010NC037-02 Lab. ofPestic,de Environmental Assessment and Pollution 

### STUDY DETAILSPAGE Study number: Report number: Study title: Test substance: Identity: SubstanceName:
Chemical formula: Molecular weight: Appearance: Storage conditions: Management: Head ofDepartment: Study Director: Person attending to routine duties and technical queries in the temporary absence of the Study Director: Study Directorcontactdetails:

Location ofstudy: Study dates: Start: Completion: S201ONC037-02 R20IONC037-02 Ready biodegradation S0507

S0507 3H-lndolium, 2-[2-[3-[(I,3-dihydro-1,3,3-trimethyl-2H-indol-2­ ylidene)ethylidene]-2-[(I-phenyl-IH-tetrazol-5-yl)thio]-1­ cyclohexen-l-yl]ethenyl]-I,3,3-trimethyl-, chloride C39H4IN6S'CI 

### 661.31 Solid Room temperature ShanZhengjun Shi Lili Liu Jining Shi Lili. Formal GLP responsibilities will be assumed by Management. Liu Jining Telephone: +862585287091 Facsimile: +862585474630 Email:lin@nies.org Key Lab of Pesticide Environmental Assessment and Pollution Control, MEP(PEAPC) 8 liwang-wang-miao Street, Nanjing 210042 Jiangsu, China Sept. 9, 2010 Oct. 8, 2010

Page 6of 16 Attachment 15, Page 125Sanitized Version**~o.:** R2010NC037-02 Lab.ofPesttcide


### 1 SUMMARY The study was conducted according to the guidelines ofSEPA HJ/T 

### 153-2004, "the guidelines for the testing of chemicals"; Part CA-E (Closed Bottle Test) of EC Methods for the Determination of Ecotoxicity; Annex to Council Regulation (Eq, L142 (2008); OECD Procedure 3010; Closed Bottle test and US Environmental Protection Agency (EPA), Office of Prevention, Pesticides and Toxic Substances, (OPPTS) Method 835.3110 (0), 

### adopted January 

### 1998; GB/T 21831-2008, Chemicals-Ready biodegradability: Closed bottle test. Under valid conditions, the ready biodegradability of S0507 was determined in a 28-day dissolve oxygen depletion using secondary effluentfrom a domestic waste water treatment plant. During the test, the temperature was kept at 20D

### C ± 

### 2°e. The test is valid because the level of biodegradation ofthe reference substance reaches 68.1% within 14 days. Oxygen consumption in inoculum blanks is 1.04 mg Oilitre after 28-day test. Thus the study met the acceptability criteria prescribed by the protocol and was considered valid. Finally the results showed that under valid conditions, 28-day biodegradation ofthe and S0507 reach 0%, 14 day of reference substance (sodium benzoate) reach 68.1%, which indicated that S0507 has no ready biodegradability.

Page 7 of 16 Attachment 15, Page 126Sanitized Version
/',;0 R201ONC037-02 Lab. ofPesticide Environmental Assessment


### 2 INTRODUCTION The purpose of this test is to determine the ready biodegradability of water-soluble organic chemicals in an aerobic, aqueous medium by monitoring the consumption ofoxygen in closed bottles, containingthe test substance and an inoculum ofsewage micro-organisms, over a 28-day period. The test may also be used to assess the biodegradability of insoluble and volatile substances. It 

### is designed to meet the requirements ofSEPA HJ/T 

### 153-2004, "the guidelines for the testing ofchemicals", Part CA-E 

### (Closed Bottle Test) ofEC Methods for the Determination ofEcotoxicity; Annex to Council Regulation (EC), L142 (2008), OECD Procedure 

### 3010, Closed Bottle test and US Environmental Protection Agency (EPA), Office ofPrevention, Pesticides and Toxic Substances, (OPPTS) Method 835.3110 (0), 

### adopted January 1998. The method is not applicable to test substances that are inhibitory to aerobic sewage micro-organisms at the test concentration. Degradation is expressed as the ratio ofthe biochemical oxygen demand (BOD) and either the theoretical oxygen demand (ThaD) orthe chemical oxygen demand (COD) ofthe test substance. Information on the relative proportions ofthe major components ofthe test substance together with theirempirical formulae or COOs are therefore necessary prerequisitesto this test. Substances are considered to be "readily biodegradable" ifthe BOD is equal to or greater than 60% ofthe ThaD (or COD) within ten days ofdegradation exceeding 10% during the 28-day test period. Because ofthe stringency ofthis type oftest, a BOD equivalent to less than 60% of the ThaD or COD within 28-days does not necessarily mean that the substance is not biodegradable under environmental conditions. Conditions more favourable to degradation, such as a higher concentration of sewage micro-organisms or a longer exposure period, may be necessary toestablish biodegradation. In this test, test solutions will be prepared in an inorganic salts medium, inoculated with a small number ofmicro-organisms from a mixed popUlation, and kept in closed bottles in the dark at a temperature of 20 ± 

### 2°C. Controls will comprise vessels containing inoculated mineral salts medium together with inoculated mineral salts medium with a measured quantity ofa reference substance. Further inoculated bottles will contain the reference substance and the test substance (inhibition ofthe degradation ofthe reference will indicate that the test substance is toxic to the bacterial inoculums). The progress ofdegradation will be followed by the determination ofthe concentration ofdissolved oxygen in test and control bottles. Results will be expressed as mg O2 

### consumed per mgtest substance divided by the ThaD ortheCOD. Where a test substance is known to have a low ThaD or is expectedto be poorly degradable, the inclusion of at least one higher test concentration is recommended to ensure that measurable reductions in oxygen concentration are obtained duringthe test. Page 8ofl6 Attachment 15, Page 127

### Sanitized Version
Environmental Assessment andPollution


### The test is valid ifthe level ofbiodegradation ofthe reference substance achieves 60% or more within 14 days after the start ofthe test and, following biodegradation ofthe test substance, the level ofdissolved oxygen does notfall below 0.5 mg 02llitre. Oxygen consumption in inoculated blanks must not exceed 1.5 mg 02/L 

### after28 days ofincubation. 

## 3 SAFETYPRECAUTIONS Sewage effluents may contain potentially pathogenic micro-organisms. Appropriate protective clothing was therefore worn when collecting and handling sewage. Test substance (S0507) was treated as hazardous substances and appropriate precautions were taken to avoid breathing dust orvapour, and any contactwith skin orclothing. 

## 4EQUIPMENT& MATERIALS 4.1 Date ofTest Sept. 9. 2010**~** 

### Oct. 8, 2010. 4.2 Inoculum Samples ofsecondary effluent were obtained as the test inoculum from a sewage plant treating predominantly domestic sewage (Nanjing Chengdong Sewage Treatment Plant). Aerobic conditions were maintained in the effluent by aeration from a laboratory supply of oil-free compressed air. On the day ofthe test, the test inoculum was prepared by filtering the sample ofsewage effluent through a coarse filter, (discarding the first 200 mL) and collecting the remaining filtrates. This inoculum was maintained under aerobic conditions in the test area until use. 4.3 Apparatus Incubator(MIR-253, Sanyo, Japan) pH-meter (HQ40d, HACH, American) BOD-Bottle (250 mL, blown, Jintan Jingbo Experiment Instrument Factory) Dissolved oxygen (HQ40d, HACH, American) 4.4 Preparation ofthe Test Solutions Stock solution for the reference substance (1000 mglL): Dissolved 0.50I g of the reference substance (sodium benzoate)was prepared in 500 mL ultra-pure water. Stock solution for the test substance (1000 mglL): Dissolved 0.50 g ofthe test substance was prepared in 500 mL ultra-pure water. Page9 of 16 

### Attachment 15, Page 128

### Sanitized Version
No.: R201ONC037-02 Lab. ofPesticide Environmental Assessment and Pollution


### In line with nonnal practice in this type of study, an assessment of the stability of the test substanceformulation and achieved concentration were notconducted. 

### 4.5 Preparation oftheTest Medium The dilution medium was prepared by adding I mL ofeach ofthe following stock solutions, prepared in pre-aerated purewaterto each I itre ofpure water. 

### Stock solution A KH2

### P04 

### (potassium dihydrogen phosphate) K2

### HP04 

### (dipotassium hydrogen phosphate) Na

### z HP04

### .2H2

### 0 (disodium monohydrogen phosphatedihydrate) NH4

### CI (ammonium chloride) 

### giL 8.50 21.75 33-40

0.50 Dissolved the above reagents in water, and set the volume I liter, the pH of this solution should be 7.4 

### Stock solution B CaCh(calcium chloride) 27.50 

### Stock solution C MgS04

### .7Hz 

### O (magnesium sulphate heptahydrate) 22.50 

### Stock solution D FeCb.6H2

### 0 (iron (lll)chloride hexahydrate) 0.25 

## 5 TESTDESIGN 5.1 Test Methods Four groups of "inoculum control", "test", "reference control" and "toxicity control" were assigned in this test, with 2 replicates each. Firstly appropriate 0.6 mL stock solution oftest substance, then added to "test" and "toxicity control" BOD-bottle. Secondly, appropriate 0.6 mL ofstock solution of sodium benzoate was added to BOD-bottles of"reference control" and "toxicity control"; then 0.3 mL inoculum was added to all BOD-bottles. a) Inoculum control: containing inoculum only (1 

### mLlL); b) Test: containingtest substance (2 mg/L)

### and inoculum (I 

### mLlL); c) Reference control: containing reference substance (2 mg/L) 

### and inoculum (\ mULl; d) Toxicity control: containing test substance (2 mg/L), 

### reference substance (2 mg/L) 

### and inoculum (\ mULl; The BOD bottles would be full filled (Total Volume: 300 mL) with the test medium that had been aerated for 20 minutes and allowed to stand at the test temperature for at least 20 h. The Page 10 of 16 

### Attachment 15, Page 129

### Sanitized Version
Lab" ofPesticide Environmental Assessmentand Pollution No": R2010NC037-02


### concentrations of dissolved oxygen in duplicate vessels of each "test", "inoculum control", "reference control" and "toxicity control" group were determined after addition ofthe prepared solutions to the BOD bottles (0 d) and the remaining bottles were incubated at 20°C 

### ± 2°C in darkness. Subsequent determinations of the concentration of dissolved oxygen in duplicate vesselstaken from each group were made on 5 d, 7 d, 11 d, 14 d, 18 d, 21 d, 25 d and 28 d. The pH and temperature ofthe contents ofeach bottle were measured after the concentration of dissolved oxygen had been determined. Determinations ofthe dissolved oxygen (DO) in the "toxicity control" group were made at the start and after five days. Ifthe DO in "toxicity control" after 5 days was more than 60% or the test substance is toxic to the inoculum, the experiment should be stopped. Otherwise the experiment would not be broken offuntil it ends. 

### 5.2 Validity ofTest The test is considered valid if a)The level ofbiodegradation ofthe reference substance achieves 60% or more within 14 days afterthe test starts, and b)Following biodegradation of the test substance, the level of dissolved oxygen does not fall below 0.5 mg Oz/L, and c)Oxygen consumption in inoculated blanks must not exceed 1.5 mg O/L after 28 days of incubation. 

### 6 DATA PROCESSING 6.1 Calculation ofTheoretical Oxygen Demand The theoretical oxygen demand (ThOD) of the test or reference substance with a molecular formula of

is calculated in the following way assuming that carbon is mineralised to COz , hydrogen to H2

### 0, phosphorus to P205 and sodium to Na2

### 0. Halogens are presumed to be eliminated as hydrogen halides and nitrogen as ammonia. ThODNH3 

### 16 [2c 

### + 1/2 

### (h-cl-3n) 

### + 3s 

### + 5/2p 

### + lI2na
- 

### 01 mg02/mg MW 

### Nitrogen in a test substance may be eliminated as ammonia, nitrite or nitrate. The higher oxidation states give aconsequent increase in the ThOD of

### + 3/2n (nitrite)and 

### + 5/2n 

### (nitrate). Page II 01'16 

### Attachment 15, Page 130

### Sanitized Version
No.: R201Ol\C037-02 Lab. OfPcsficide Environmental Assessmenf andPollution


### The ThODNH3 

### oftest substance and reference substance are 2.20 mg 02/mg and 1.67 mg02/mg. 

### 6.2 Calculation ofOxygen Consumption On each measurement occasion the oxygen content (mg02!L) ofappropriate control, reference and test bottles is determined. The blank-corrected level ofoxygen consumption 

### (mg02/L) by test or reference mixtures is calculated by subtracting the mean levels ofoxygen consumed by the inoculum blanks. The BOD (mg02/mg) of test and reference substance is calculated by dividing the blank-corrected level ofoxygen consumption in the test orreference mixtures by the appropriate test concentration. BOD (mg 02/mg test or reference substance) mg (test or reference substance) /L Where: T(o) mean mg02/L content in the bottles containing test orreference substance on Day 0; T(n) = 

### mg02/L content in the test orreference substance bottles on Day n; C(o) = 

### mean mg02/L content in the control bottles on Day 0; C(n) mean mg02/L contentin the control bottles on Day n; n = 

### Day numbersample measured. 

### 6.3 Calculation ofPercentage Biodegradability The percentage degradation after n days ofthe test were calculated by dividing the amount of oxygen consumed per mg oftestsubstance by the ThOD orCOD in the following way: mg02 

### consumed/mgtestsubstance 0 Degradability(%)**----~--------~----------xl** 

### 0 ThO0 

## 7RESULTS 7.1 TestConditions During the test, the temperature was kept at 20°C 

### ± 2°C. The test is valid because the level of biodegradation ofthe reference substance achieves 68.1% 

### within 14 days. Oxygen consumption in inoculated blanks must is 1.04 mg 0211itre after 28 days of incubation. Therefore the test would be considered valid. 

### 7.2 Conclusions Table 1 and Table 2 showed the biodegradation data during the 28-d test. The result indicated Pagel2ofl6 

### Attachment 15, Page 131Sanitized Version No,: R20IONC037·02 Lab, ofPestie.d. Environmental 

### 14-day biodegradation of the reference substance (sodium benzoate) reached 68.1%. 28 d biodegradation oftest substance reached 0%, which indicated that test substance has no ready biodegradability. 

### 8 HEALTH & SAFETY In order for PEAPC to comply with Law ofthe People's Republic ofChina on the Prevention and Treatment ofOccupational Diseases 200I, and the current Control ofSubstances Hazardous to Health Regulations, it is a condition ofundertaking the study that the Sponsor provide PEAPC with all information available to it regarding known or potential hazards associated with the handling and use of any substance supplied by the Sponsor to PEAPC. The Sponsor also complied with all current legislation and regulations concerning shipment ofsubstances by road, rail, seaor air. Such information in the form ofa completed PEAPC test substance data sheet must be received at PEAPC before the test substance can be handled in the laboratory. 

### 9 MAINTENANCE OFRECORDS & 

### DOCUMENTATION All raw data arising from the performance ofthis study will remain the property ofthe Sponsor. Records and documentation relating to this study (including electronic records) will be maintained in the archives ofPEAPC for a period offive year from the date on which the Study Director signs the final report. This includes the Study Protocol, raw data, a copy ofthe final report. Types of sample which are unsuitable, by reason of instability, for long term retention and archiving were disposed ofafter the periods stated in PEAPC Standard Operating Procedures. Test substance remained will be retained by PEAPC in 

### its archive for a period ofone year from the date on which the Study Director signs the final report. After such time, the Sponsor will be contacted and his advice soughton the return, disposal orfurther retention ofthe materials. Ifrequested, PEAPC will continuetoretain the materials subjectto a reasonable fee being agreed with the Sponsor. PEAPC will retain the Quality Assurance records relevant to this study and a copy ofthe final report in its archive indefinitely. 

### 10 REFERENCES [I] SEPA. The guidelines for the testing ofchemicals. HJ/T 

### 153-2004. 2004. [2] SEPA. The guidelines for the hazard evaluation of new chemical substances. HJ/T 

### 154-2004.2004. Page 13 of 16 Attachment 15, Page 132Sanitized Version Lab. ofPesticide Environmental Assessment and Pollution No.: R2010NC037-02 

### [3] SEPA. The guidelines ofchemical testing good laboratory practices. H1IT 

### 155-2004.2004. [4] SEPA. The guidelines for the testing ofchemicals. Beijing: China Environmental Sciences Publishing House. 2004. [5] OBIT

### 21831-2008, Chemicals-Ready biodegradability: Closedbottle test. [6] OECD. 3010 Closed Bottle Test. Paris: 1992. [7] Part C.4-E (Closed Bottle Test) ofEC Methods for the Determination ofEcotoxicity; Annex to Council Regulation (EC), Ll42 (2008). [8] US Environmental Protection Agency (EPA). Closed Bottle Test. Office of Prevention, Pesticides and Toxic Substances, (OPPTS) Method 835.3110 (0), 

### adopted January 1998.

Page 14 of 16 Attachment 15, Page 133

### Sanitized Version
Lab ofPesticide Environmental Assessment and Pollution No,: R2010NC037-02



### Table 1Concentrations ofDissolved Oxygen (DO) Samples Od Inoculum 8.61

control 8.58 8.63 Test 8.59 Reference 8.60

control 5d 8.52 8.54 8.59 8.57 8.57 Toxicity control 7d 8.36 8.39 8.47 8.44 8.60 DO after ndays (mglL) lid 8.23 8.24 8.34 8.31 14 d 8.14 8.18 8.22 8.25 8.60 7.69 18 d 8.04 8.05 8.16 8.14 8.57 7.69 21d 7.83 7.94 7.64 8.03 7.90 8.03 7.91 7.86 8.60 8.57 8.60 7.69 7.69 7.69



### Table2 Biodegradation Sample Biodegradation after n days (%) 5d 7d 11 d 14d 18 d 21 d 25 d 28 d Test 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Reference 25.3 51.8 62.0 67.5 71.6 73.4 77.5 79.9

control 24.4 50.0 62.0 68.7 69.8 74.3 77.5 80.2

Page 15 of 16 

### Attachment 15, Page 134Sanitized Version Lab, ofPesticide Environmental Assessment and Pollution No" R20IONC037·02



### Figure I Biodegradation curve

Page 16 of 16 Attachment 15. Page 135

### ATTACHMENT HEADER SHEET
Attachment Number016 Attachment Name PMN Fee PaymentAcknowledgement 

### Associated PMN Section Number N/A Does not contain CSI



### Report Number KODA101220491061974

Page 136Sanitized Version


### From: paygovadmin@mail.doc.twai.gov To: R. David Peveler, Ph.D. Subject: Pay.Gov Payment Confirmation THIS IS AN AUTOMATED MESSAGE. PLEASE DO NOT REPLY. Your transaction has been successfully completed. Transaction Summary Application Name: TSCA User Fees Pay.gov Tracking 10: 2522HOCQ Agency Tracking 10: 74157949339 Account Holder Name: Lynn L. Bergeson Transaction Type: Sale Transaction Amount: $2,500.00 Billing Address: 1203 19th Street, NW Bill Address 2: Suite 300 City: washington State/Province: DC Zip/Postal Code: 20036 Country: USA Card Type: American Express Card NUlT'.ber: ***********8008 Transaction Date: Dec 7, 2010 2:17:00 PM

Attachment 16, Page 137