Liquid Waste Feed Sample Composite Data Sheet 

Project Name Veolia - Sauget, IL Date 10 ta-311) 

Project Number 40942525.20.{)2 Condition No. 1 

Facility Unit4 Run No l! 

Stream Name Uquld Waste Feed (LWF) Start Time 1a.U 

Composite Sample 10 V$4-lWF- 1 18-COMP)& Stop Time li&& 

Operator 

Sample Number Tim e Volume/Mass Sample Number Time Volume/Mass 

1 ta..&s a. eo"'~.., 21 

2 •a.!i} 22 

3 tl() 8 23 

4 tla) 24 

s I'Ut) 25 

6 ibH 26 

7 I 'tO& 27 

8 I 'leU 28 

9 l'tl~ 29 

10 J~t•n 30 

11 I "o t, 31 

12 l.U~) 32 

13 l$'1& ~ 1- 33 

14 ···'IJ-:1 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volume ~,(,OO...,L, 

Comments: Collect appropriately-sized and equal allquots and transfer Immediately Into a 4-liter composite jar. 

Collect a separate 500 ml bottle of sample at each S<Jmpllng time t o be retained in archives. 

ePA ~Ht V~olil:\ s 't • ~ f- -~(,<.. 

SQto'\11'\(ld ~IOI'fl ~~ ~l~ll"' 

.5/)$ .. ()5 $ub.Somp/e C4Nif!X'SIIe 

ReWskm I)IJr~ : June 2012 

Rsvf«•'UI' Juno2013 

E-377 

VESOI3800 
URS 

''"'" Vld ' I I • " 

''"""" w'udt s·tr, .... )•"'1'/, )' 

DAILY .RECORD 

OF EVENTS 

o?co 411 ~~r··' ~.~t( f.• s:k. W"'-lf.tr. c.IJ1 r·"">, h,l ]u'f. 

nrs '"'' Ofl'[.'f, j clrcf, .,..; Por((i -to M•.:I,,M..c( c:f,ly. j¥.)';. J'C'··," 

fu Jn./7 ""'f''·J."'~~v.-/ <r · /f./:1 Tr.•trf· rf •1 /o.f,<f ~J" <A" 

I J""w'f'? of ;,fpl•or. 

IIHS ~!j'~ ~vrt i..A. 

I ''to f/-"'f~ (b;, )Jt. [.(f,.c/ r-4 ,.,..pie~ aT /OJ) fp .. (/ le-tA\ f;. sfr-,-$. 

l:l.':>'J ll~91\ ll.u.l\ a.A, '-ollec~ ~ptlte ~Q"'piP~ 

(...l ~H%J Pb.L-11:n H~.0.'1a.O 

11>'> 1.1!-\ J<...IJ. hrull tl\'h, Lo\\P.d &a"'plf' (v,.,p3.A ll~ lu15' 

l'~b tal\icJ ..,f"IL ;:>01·'~/qs ~4t'IN) m~\4\~ hQ,I\ f"'~ <Ji·rhol' 

C-1 \H'JOI Vb. l--lb~ H~-~Wb 

l'ri'f 1-\\'_jqls lroli\ Qhd; 1 t.oll~-d- ::.o,,.,,l~ (.c~ p). j (n.J.. UApaP.-Il.Jp) Q I J$"0') 

l'i1b i..<:lllet~ c..p 1\ f• r.'l- n~~., 

t..l '. ~ · 'fCl~ fl b L · :,?>() HI) . O.d.{,(, 

tS'1.1 [)~ q .. d I'~ trt~Jn tfld 5 , ~o ii Q<..\- ~;qn~plr C..t''"l'3C. q~ IIJ3f R.I.lt>~!l C..utl\pl~lt'. 

I 'J'f7 Lol\td ~I" b..t ;,Qh•JIIr; 'or Clrth•vt 

U '.1-\-\ UFi fib ,l-toa. \-\(). ~d.~'\ 

U\ !H -l•lL 

t:~~l"!' ,fhtk. r\(l (ft(•l ~U~td ~rJ .~.ll'r\<1 (11-C\J "' -·~l"i ~~~., . 

1/l 

I 

I 

t. ~GJ~Q I 

E·378 

VES01380l 
Fie ld Balance Calibration {;heck 

Project Name __ ...;V:.;C,;O:;:Iia;.:S:::;a~u~ge~t~, I:,;:L __ 

Project Number __ .:4:::094::.::.;2:;5;25~.2;::0.0=2::...-

F;cllltv ___ _;U:::n~lt:.::_ _ _ _ 

Balnnta 10 ____ S.;.'i.:.;¥.=...._ 

Calibration Initials c.t:il C~clcedby Date IOR'tfl) 

-~ We!cbt" 

--- --j -

---- "' --· "' ~~~~ w . 

20 ~Q . ... . 

50 ~.a 

c.-CIMd<of 100 -.:n.; tolonc.o uslnc studt nt 

WelJl!ts 200 ~0() ::, 

SWdent Wolgkt Set 10: 

500 4".1 

\41,,~ 1000 1000-7 

u....a,_oo_.,...,. __ lOJ. 

,.,. _ _ _ towdlj>-lftiU<-l=t.-... IOOOudSO<lg>n~- fw •--- ' "" --... -·-·s0.$11. ....... _'"_ .... ~ Percent OUfetenee • balanoe rudlng- actual mass x 100 

actual mass 

ct>S·08B I f'/o/d l•faltCf (•l•brollon 

,., f.M !!01'·010 

R~llisio" !Jot~ MGI"Cit 10/1 

Rllol,.wd: Uy 1011 

E-379 

VES013802 
< m 

(I) 

0 

w 

00 

0 

w 

Waste Sample Logbook 

Veolia-Sauget, IL - Unit 4 CPT 

Project Number 40942510.20 

P11ge 11 of29 

Sample 10 Code Stream Fraction Cond Run Date run. TW GW Comments ~~~~~B~~~~~~~1~~----~~~~----~-- --~~~~~~~4-~03~,~~~~-7~5~1.~'-+---- ~----~ 

ivs'-as-tv.-GraO e u Solids .wM 1 ~ 

..,.,.,. 12A.Q1b 7 BoAk Solds Alcltie 1 ~ 

ivs'-BS·1~-GI1lb 8 B1tk ~ AttNve 1 2A 

h ... ,,...1~2A USolds ~ 1 2B , IU( 

VS4-8S-12B-Gtsb 4 Bull< Solds AreNvo 1 26 11l) 

tvs4-BS·12B-Gr8b a BIAk ~ Archive 1 2B 'at 1 

128-Gtab 7 Bu1< Solids ArriWe 1 2B 'iO~ 

lvS4-8S-128-<l<tlb 9 Bulk Solids Arc!M 1 28 I'\ 1(. 

i lv~B~12B-Gllll11 8\Ak Solds AttiWe 1 2B I 1 SOf. 

~- • o<- 128-GraO 12 U Sold:s Attti<e I 2B I 'f~\ 

128-G<ID 13 &A Sold:s ArrHre 1 2B - I ot 
< 

m 

Vl 

0 

..... 

00 

~ 

Sample 10 Code 

I'JS4-CS.1~1 

jvS4-CS-12A-Gnb 1 

12A-Gnb2 

jvS4-<:S-12A-Gnb 3 

jvS4-CS-12A.Qab ~ 

jvS4-CS-12A-Qab 5 

~ ... ' ~ 12A-Grab 6 

lvS4-CS-12M>r.lb 7 

jvs.I-CS·12A.Qab 8 

""· ~·1~ 

VS4-CS.12B-Comp28 

lv54-CS·1~2C 

VS4.CS.12S.Grab 1 

VS4·CS·12B-Gtab 2 

V$4-CS-128-Gr«l 3 

VS4·CS·128.(l<ab 4 

jYS4-CS.128-Gnlb 5 

VS4·CS·128-Glab 6 

~CS-128-Gnlb 7 

jvS4-CS-12S-Grlb 8 

~S-128-Gnlb 9 

jvS4-CS-1211-Gqb 10 

jvS4-CS.128-Grab 11 

i'Y:.«:S-1211-Gqb 12 

IVS4-CS-128-Gnlb t3 

~- r><'1~14 

Stream 

Conlaincrlzed SCllds 

Cont;inertzed Solids 

Coo illiuerlzed Sob 

Contalnec12ed Scids 

Cooail-fled 5alds 

CooUinellz.ed 5alds 

Co ICaiobd Solds 

~Solidi 

Contail~ed Solids 

Ccnllhlrized Solids 

Coolaileriled Solkls 

Ccntafnerizcd Solcls 

Conlalneolzed Solds 

Conlaln«im sonds 

Cool~~Wirltcd Solids 

Conl81nerlzed Solids 

Coolailto1led Solds 

Conlaileltled Solids 

Cootafnedzcd Sold$ 

Conllllnlrized Solids 

Containerized Solids 

Cooo:ailoerized Scllds 

~Solids 

Coollaloerbd Solds 

CcniiNized Solds 

Continlrtzed Solds 

Waste Sample Logbook 

Veolla-Sauget, ll - Unit 4 CPT 

Project Number 4094 2510.20 

Fraction Cond Run Date Time TW 

~ 1 1A II) 1~"6'ito 

Alltive 1 2A I:>'Hof 

Alltive 1 2A ()'oro 

Aod1IYe 1 2A IO()fi 

Aod1IYe 1 2A ~~ 

ArciWe 1 2A I · '- 10~6" 

AJd<lve 1 2A 

ArciWe I 2A 

Aldl!Ye 1 2A 

~ 1 28 I'"_, Ill 1!.35 

Phys/Comp, Meta" 1 28 tS'o<J 

Ph~ 1 28 ....s: IS'~$"' 

AodWe 1 28 ~~ 

Aldllve 1 2B ~~o 

AoltiYe f 2B 1~$ 

Ardllvo 1 2B llf-6 

AoltiYe 1 2B ll' f 

Ar<t!Ne 1 2B IU O 

Ardi.e 1 28 l'tOif 

ArdVve 1 2B ·~ Atthlve f 2B 114~ 

MJ:We 1 28 l'tfo 

An:td.e 1 2B lfO,-

A:tiM 1 2B ~O 

Aldllve 1 28 .... IU S' 

Aldllve 1 2B 

Page 19of29 

GW Comments 

~ • •" ' 5" 12. ~ 

'$() '"' · ,,,tl ... ~1 0 (, '"(a.·, •• ~ "'"" ~~~~ -. 1,1~"1 

'-1'\'iq ~() ·, 1, 580~ 

SO't "' .., ·,17-tJ<\ 

.s, ..... 3zi!oo... 

~<; 3 \ 

1~0 "1 ·. 1,8'\bc. 

~~%~ qa,·, a. ·~iq 

~~"ic, '50 ~ a.ou."' '.i~k\ f/l i Q, lt5'(\ 

sn~ 118 ~,~ 

~0~ ~<r, '·~~qo. 

~<tiC~ RS ·, 1,/o?l"\ 

S'l?,e, ~ ~ ' I, (\Oa_t. 

SCI{a \0\ ! ),C\'1'\" 

'j\ ~ «>. I I P> ~ 1,7'\a, "\ 

0~ !a' . • I,")!).(\ t\ 

'" ... ;'34; •.nrq 

1f11{ q ta·. \,')30_'\ 
< 

tTl 

en 

0 

w 

00 

0 

V> 

Sample JD Code Stream 

lvS4-U!W·12A~1 Low BIJ IJqi.WI Waste 

lv<:Lt I>W.12A-Gr.lb 1 Low BIJ ~l.id Wua 

lv<:Lt IN< 12A-G"ab 2 Low BIJ l4ld Wtt#! 

lv<:Lt IIW.12A-Gfab 3 Low Blu l4ld Waste 

~l8W-12A-Gr.lb 4 Low BlJ l4ld Waste 

,..,.~ ""'·12A-Gr.lb 5 Low BIJ l4id w-

~ A11/-12Mllab 6 Low Blu Liquid Wale 

lvS4-LSW-12A-Gr.lb 7 Low Blu Liquid Wasle 

~o.tc:LJ AW.12A-Gr.lb a Low Bar !.quid WISIO 

lvS4-U!W-128-Conll2A Low81U ~uid wasre 

f..IS4-U!W·129-C<rnp28 Low B1u liquid Wasle 

~BW·1~ Low &I Liquid Waste 

ivS4-L9W·12B-G<all 1 Low Bill ~l.id Wasut 

ivS4-LBW· 1 28-G<ab 2 Low B1U l iquid Waste 

f./sw.aw-128-Qab 3 Low Bru Liquid Waste 

jltS4-L91'1-12B-Giab 4 Low Bill ~uld Waste 

fvS4-LBW· 128-G<ab 5 LowBiuliquidWaskl 

!'Js4·lBW-128-Gr.lb 6 Low BIJ Liquid Waslt 

VS4-LSW-128-Gnlb 7 Low Btu liquid Wasle 

!vS4-LBW·128-Grnb 8 Low BIJ liquid Waslle 

~BW 1~9 Low Bal Liquid WatS/e 

!VS+l.BW·128-Grab 10 Low Btu Liquid Waslle 

jv$4·1.8\\'·128-Gnlb 11 Low Btu liQUid Wasle 

....,._, --1 28-(lrlb 1 2 Low Bcu Uqud w .... 

lvS4-U!W-128-Gnb 13 Low Blu Liquid Wasle 

~W-128-Gnb 14 Low lllu l.i!IMII'Iasle 

Waste Sample Logbook Psge11 of16 

Veolia-Sauget, IL - Unit 4 CPT 

Project Number 40942525.20 

Fraction Cond Run Date rnne lW GW Comments 

~ 1 2A Ill ~s a.')OIIl ...... 

.AictiMe 1 2A 0<\l~ SOQ,.L 

~ 1 2A 11,50 

NclliYe 1 2A 00~ 

.wwe 1 2A I <lie) 

~ 1 2A 1-o.. 3~ ·'-

ArdliYe 1 2A 

Archive 1 2A 

ArdWe 1 2A 

~ 1 28 .. lltM ~~~ I~') QO ool 

Pllys/Coo'lp, 1/.elals 1 28 ~II' l)OQ ooL 

~ 1 28 ~ ~~" Arcl\iva 1 28 1.:»'5" O'I l.. 

Arcl\lve 1 28 ~'SO 

ArdWe 1 29 l'fO'f 

Archi'lll 1 28 ·~() 

Arcl'jve 1 28 I~M· 

ArdWe I 28 l)fO 

Arthlw 1 28 ,.115 

Arcl'ive 1 28 l'liO 

Ntll>e 1 28 11115 

Archive 1 28 l'lfO 

ArdiNe 1 29 I S1)f 

Ntll>e 1 28 ... ~ 

ArdWe 1 28 .. t 'BS" ..... 

AlrJwe 1 28 -
< (Tl 

en 

0 

..... 

00 

~ 

Sample 10 Codo 

11M:cq>1 

·12A.Qab 1 

~. - ·12J..Gr31>2 

~BW·12A.Qab 3 

j>'S4-IIBW-12J..Gr31> 4 

12A-Ollb5 

IJS4.HBW·I1A-Gnlb 6 

. '~ -12J..Gr31> 7 

VS4-HBW-12J..Gr31> 8 

VS4-HBW 2~2A 

W-1~28 

VS4-HBW·I28-Cornp2C 

VS4-HBW·I2B.Qab I 

\IS4-HBW-128-Gtab 2 

VS4-HBW·121Hifab 3 

Vs4-liBW-128-Gtab4 

VS4-HBW-128-Grab 5 

VS4-HBW-12B.Qab 6 

VS4-HBW.128-Grab 7 

VS4-HBW-128.(ifab 8 

V$4-HBW· 128-Grab 9 

\154-HBW-128-Grab 10 

VS4-HOW.128-Grab 11 

V$4-HBW-128-Grab 12 

~. •rn -128-Gtab 13 

V$4-HB\'H!li.Qab 14 

Stream 

~ a.I.JQ<.Id w-

~ Btu liQIM Wasle 

Hi!tllllu liqiM w-e 

~B .. i.4*1Waste 

~ lllu I.JQ<.Id Wil51e 

Hi;h lllu I.JQ<.Id Want 

High lllu Uquld Wesle 

~ lllu Ucpj Waste 

High lllu UqiAd Waste 

High Btu UqoM Waste 

~ lllu UqiAd Waste 

High Blu Llqi.id Waste 

H~ BIU LIQUid Wasl& 

Higtl Bill Uqi.id W11$1e 

High Btu Uquld WilSie 

HfGh Btu UqoAd Waste 

High Btu liquid Waste 

High Btu Liquid WISie 

H~ Btu Uquld Waste 

High BIU Uqi.id Waste 

Higlllllu UqiAd Wasil! 

H~ Bill liquid wasm 

Hi;tllllu Uquid Wasle 

H9\lllu l.iquC Wast! 

Higlllllu Uqo.id Wa,i! 

~ a. Uquid WIISt: 

Waste Sample Logbook P~tge3of16 

Veolia-Sauget, IL - Unit 4 CPT 

Project Number 40942525.20 

Fraction Cond Run Data nme TW GW Comments 

~ 1 2A ~'" 1111C. a,')C)o,.\.. 

AtciiYe 1 2A 't}€. -soo., L 

Ndive 1 2A il1'~ \ 

AII:Me I 2A roar. 

AII:Me I 2A ·~' lvti:We 1 2A ~ .. 10~ ~ 

oVc:hiYe 1 2A 

AII:Me I 2A 

ArchNe 1 2A 

Phys/C<lmp I 2B jta,h\ lUi' i,"/fJ~toL 

Metals 1 28 11114 l5Q()IIIL 

Phys/Colre> 1 2B I'IJI> a. c.oo,..~., 

AtdM I 28 ~~~ 'JOO .,.L 

Atcltive 1 28 ~'S\ 

Archive I 28 llO(a 

AtdM 1 2B na\ 

A/chive 1 2B l'n6' 

An:me 1 28 IWI 

An;f1ive 1 2B I"'OC. 

Atetive I 28 lit~ I 

AtdiYe I 2B I 'Of. 

AtrJVve 1 2B l'l~l 

AII:Me 1 2a ICjOC. 

AtrJWe I 28 15'., 

AII:Me 1 2a -... ~ -· 

AtdiYe I 2B 
Waste Sample Logbook Page 3 of29 

Veolia-Sauget, IL - Unit 4 CPT 

Project Number 40942510.20 

Sample 10 Code Stream Fraction Cond Run Date nmo TW GW Comments 

~Wf·12A-Ccmp1 Ucpd Wasle Feed PhysJC<mp 1 2A ~lA to:.r l.,;oo..-l 

lv54-t \\ 'F ·12A-Gnb 1 Liquid W_,. Feed Alf:tive 1 2A '\)? ~ ... l 

lvS4-tWF·12A.Qab 2 UcpdWasleFeed MJWe 1 2A Q"a ~V.'F· 12A.Qab 3 lJqoJd Wasle Feed IJ!1:We 1 2A 1007 

iVSLLWF·12A-Gnb t l4'!WISliiFeed MtWe 1 2A ~ 

~WF-12A-Gnb s UcpdWuFeed Ndive 1 2A -&. 10&7 ,_ 

jvs4.t. WF ·12A-Grnb 6 Liquid Waste Feed An;hive 1 2A 

~Wf.12A.Qab 7 Uquid Waste Feed AtdM 1 2A 

~4-LWF·12A-Gtab8 ~ Wasls Feed Arcllive 1 2A 

!'Js4-LY1f·128-Car92A Uquid Waste Feed Pnys/Cornp 1 2S ~ •• It\ 1'3'>~- zs-~--\ 

jvS4-l WF·12.B.(;anp28 Uquid Wae10 Feed Phys/Canp, Mctlls 1 28 l')o"?- ~3o~-' jvs4-LWF·1~2C Uquld Wasle feed Pl1ys/Con'cl i 2S IS"~1- z '-00.......1 

VS4-tWF·12S..Grab 1 liQuid Waste Feed AleMe 1 28 ,~,., 600111 L 

I'JS4-LWF·12S-Gtab 2 Llqu~ Waelt Feed Atthl'le 1 2B 13- S~ 

VS4-I.WF·128-Grab 3 liQuid WMie Feed AleMe 1 28 110'7 

IVS4-LWF·128-Gtab 4 Liquid Wasle Feed M:l11ve 1 28 li~ 

jv54-t Wf ·128-Gtab 5 llQu1d Was• Feed Nti:M 1 2S II 'US 

jvS4-LWF·12B·Gtab 6 Liquid Wale Feed M:l1ive 1 28 Ill $d. 

jvs4-LWF· 129-Gtab 7 llQu1d Waste Feed Alf:tive 1 2B 07 

VS4-LWF·128-Gtab 8 Uquld Waste Feed Ardlive 1 28 lot~· 

1\'54-t Wf. 128-Gt&O 9 Liquid Wasle Feed NUtie 1 2S 1'1~7 

VSLtWF-128-Grab 10 Uquld Wasta Feed 1\rdiYe 1 28 l't5,} 

.. 

(., 

.. < • 

['I") 

en 

0 

~WF 128-Gtab 11 Uquid W_,. Feed NUtie \ 2S tfOJ 

~WF-129-Gtab 12 Uqu1d Waste feed Alf:tive I 28 ·~ ~WF· 129-Gtab 13 Uqu1d Waele Feed Mme 1 2B ~ lfl7 - ~ 

..., VS4-l.WF·128-Gt3b 14 Uquid w.sle Feed A:dM I 2B 

00 

0 

..... 
Bulk Solids Sample Composite Data Sheet 

Project Name Veolla - Sauget,ll D1te IC!f~l\11'3 

Project Number 4094252S.20.02 Condition No. 1 

Facility Unit 4 Run No -~ Stream Name Bulk Solids (BS) Stannme ()<\at 

Composite Simple 10 VS4-BS-liA_ <OMP_I_ Stop Time ~0% 

Operator 

Sample Number Time Volume/Mass Sample Number n me Volume/Mass 

1 ()q_~E., ~0~(\ 21 

2 o 1

U"I '5'1 a.~ 22 

3 10 0{, 'jla.~ 23 

4 10~ "t<\a' 24 

5 t<n~ 4,~~ 25 

6 26 

7 27 

8 28 

9 29 

10 30 

11 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Flnal Volume/Mass "il~<~. 

Comments: Collett solids In 1000 ml)ar labeled for Archive. Take approp< te y~lzed and equol aliquots rrom each jar to prepare the 

composite sample in a 4 llter jar. Record the volume/mass of each aliquot used to prepare the composite sample on the d•ta snw. 

Retain the remaining sample in the 1000 ml jars and archive. 

SO:J•O!! Sd>-.S.IfiPk CDff!POSile 

- O.tc: ,.,..l(J/2 

R<~ ,_20/J 

E-385 

VES013808 
Bulk Solids Sample Composite Data Sheet 

Project Name Veolia-Sauget, ll Date \01&11/1} 

Project Number 40942525.20.02 Condition No. 1 

F~<lll\Y Unlt4 Run No ~6 

Stream Name Bulk Solids (BS) StatlTime ~~~() 

Composite Sample 10 VS4-8S-li.l:COMP!A Stop Time j~?.~ 

Operator 

Sample Number Time Volume/Mass Sample Number Time Volume/Mass 

1 tal(. 'i06q 21 

2 ~~~I If\(,, 22 

3 I~ t;O~~ 23 

4 ~~~' G"l~c:.. 24 

5 \ ?,"lt 4.1\'\~ 25 

6 26 

7 27 

8 28 

9 29 

10 30 

11 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volume/Mass ~.slq~ 

Comments: CoUect solids In 1000 ml jar labeled for Archive. Take approprlately-slled and equal allquots from each jar to prepare the 

composite sample In a • Uter jar. Record the volume/mass of eadl aliquot used to prepare the composite soomple on tbe data meet. 

Retain the remaining sample In the 1000 mf jars and archive. 

~~~ I~U ~IOrl\ 1\' "lt (. .. IOii.'ll\3 

~-05 S<I/>-S<»op/< C""V»'il< 

RcofsiM (>m; J-!lOll 

Re>f•- J.,.. ZOIJ 

E·386 

VES013809 
Bulk Solids Sample Composite Data Sheet 

Project Name Veolia - Sauget, ll O•t~ IO(a.'tfl3 

Project Number 40942525.20.02 Condition No. 1 

Fac!Rty Unlt4 Run No a.~ 

Stream Name 8ulk Solids (BS) Start Time ~~~(, 

Composite sampleiD VS4·BS.1~;COM~ Stop Time I '60EI 

Operator 

5amplo Number Time Volume/Moss Sample Number Time Volumo/ Mass 

1 I a_% ~ 10 tc 21 

2 13.~1 Q.CI~ 22 

3 t~Ot;. a.q~ '\ 23 

4 tl~\ ~()?! '\ 24 

s ~\~ ~'l~ 25 

6 I'" slit\ 26 

7 I '40 El ?,0"7~ 27 

8 IIU\ &1\1 Clj 28 

9 I "tl'- d.<\{,~ 29 

10 I~ lil --1\~~ 30 

11 \ '\"0{, '30~~ 31 

12 32 

13 33 

14 34 

1S 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volume/ Mass ., ~~~~ 

Comments: Coiled solids in 1000 ml jar labeled for Archive. Take appropriately-sized and equal allquots from ~ach jar to prepare the 

composite sample in a 4 Liter )ilr. Record the volume/mass of each aliquot used to prepare the composite sample on the data sheet. 

Retain the remaining sample In the 1000 ml jars and archive . 

.st>S·o5 Sub-SM¥>/< C""'f"S/r< 

~Dille: JUM Mit 

Revkntl: June 201.1 

E·387 

VES013810 
Bulk Solids Sample Composite Data Sheet 

Project Name Veoh - Savget, ll Oote l()l~'tl 13 

Project Number 40942525.2()-()2 Condition No. 1 

Facility Unlt4 Run No $.~ 

Stream Name Bulk SOlids (BS) Start lime ~% 

Composite Sample 10 VS4-85-I. ~OMP~ Stop Time ~~~ ~ 

Operator 

Sample Number Time Volume/Mass Sample Number llmc Volume/Mass 

1 ·~3E, ~06 "1 21 

2 1~1$1 Sl'i 'I 22 

3 nO E. 0.1\1{ ~ 23 

4 1\~ I i.4\~' 24 

5 ,u, Q.,{,.., 25 

6 I '3's l ~a-a~ 26 

7 I '\04 ~Cl9l~:j 27 

8 II\&\ ~~. 28 

9 \It~~ a.'\IJ\'.o,_ 29 

10 1\.I'SI 30\~ 30 

11 I ~Ot. ~~, 31 

12 I IS~ I 'J-4\7~ 32 

13 'S~ Q.l\&, 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volume/Mass ·a,q\7~ 

Comments: Cohect solids In 1000 ml jar labeled for Archilf<!. Take appropriately-sited and equal allquots from each jar to prepare the 

composite sample In a 4 liter jar. RKOrd the volume/mass of each aliquot used to prepare the c:omposlte sample on the data sheet 

Retain the remalnl"ff sample in the 1000 ml Jars and archive. 

SDS·O!J 5<4>-Sompk Ctxopos/to 

k.-.isio•t>tt~<; J- 21)/2 

-d:J-21)13 

E-388 

VESOI38 ll 
Containerized Solids Sample Composite Data Sheet 

Project Name Vcolia - Sauget, ll Date 1()~~113 

Project Number 40942S25.2CHJ2 Condition No. 1 

fidiiiV Lin it 4 Run No dl'\ 

Stream Nome Containerized Solids (CS) Start Time c~~sComposit e Sample 10 VS4< H iA,<OMP_I_ Stop r.me 5" 

Operator 

Sample Container 10 Time 

Volume/ Somple Container 10 Time 

Volume/ 

Number Mass Number Mass 

1 ~ <:l<\l1 ~0.~ 21 

2 'ill. Q~lO 'SIS ~ 22 

3 ,-o ~00'$ 'SO~~ 23 

4 bO \Oa.Q "1%(\ 24 

5 ~, \Ol' 'tl\ 'c.. 2S 

6 26 

7 27 

8 28 

9 29 

10 30 

11 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Anal Volume/Mass a,5t&~ 

Comments: Take appropriately-sited and equalallquots from each contalnerto prepare the composite sample in o 4·Ut ar jar. 

Record the volume/mass of each aliquot used to prepare the composite sample on the data sheet. 

Collea a representative aliquot of the remaining material In • 500 ml jar to be archived. 

SDS-05~/cc-pnllc 

l&'ffiMft : June. lOll 

Rcl'l<.&aa!V..,. 10/J 

VES01 3812 
Containerized Solids Sample Composite Data Sheet 

Project Name Veoli<~ Sau.get, ll Date lal<i\4/1'3 

Project Number 40942525.20.02 Condition No. 1 

Facility Unlt4 Run No 0.9 

Strum Name Containerlted Solkh (CS) Start Tlme 1a.w 

Compcslte Sample tD VS4.CS-1U ..COMJIU Stop Time ~~~6' 

OporatOf 

Sample ConllllneriD nme Volume/ Sample Container 10 Time Volume/ 

Number Mass Number Mass 

1 'lit). I•U~ -i'()/ ~ 21 

2 ~a 1a '5d!> "'en e. 22 

3 so \~OS ')()'-\!!! 23 

4 60 1UO ()~~ 24 

s 4'6 ~ '5"'00 ell 25 

6 

-_, 

26 

7 27 

8 28 

9 29 

10 30 

11 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Final vot ....... /Mass ~.~1\~ 

ComrMnts: Take appropriately-sized and equal a llquots from each container to prepare the compo$lte sample In a 4-Uter jar. 

Record the volume/mass of each aliquot used to prepare t he compoSite sample on the data sheet. 

Collect a representative aliquot of the ,_alnlng material In • 500 ml Jar to be archived. 

SDS·OIJ5l.<b-s...plc~te 

/&-{)of<.· JIN 2()/i! Re.wr.m .... 2(//] 

VESOI3813 
Containerized Solids Sample Composite Data Sheet 

Project Narne Veolla -Sauge t, II. Date l<l I <l.'\ 113 

Project Number 40942S2S.20.02 Condition No. 1 

Facility Unlt 4 Run No o.B 

Stream Name Containerized Solids {CS) Star! Time 1~)1!) 

Composite Sample 10 VSH:S-lt.1·COMPJ.l Stop Time 1665" 

Opera tO< 

Sample Container ID rrme Volume/ Sample Container ID Tlme Volume/ 

Number Mass Number Mass 

1 ~~ IUS' a~q_~ 21 

2 40. ~~0 ~~~ 22 

3 S'b I '305' i:l''" 23 

4 ~C> ~~0 .1~~ 24 

5 b~ 1335 ~~7~~~ 25 

6 BO l')'iiO ~'~ 26 

7 ~~ 1\iOS &.'\'\~ 27 

8 'I~ 1ttao 3~\1:1, 28 

9 10% 1435 Mi~ 2.9 

10 I I f> 11

HO ~q!iiq 30 

11 a~ I ~0 5" ~cu .... 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 >8 

19 39 

20 flnol Volume/Mass ~%()'\ 

Comments: Take approprtately-5lzod and equal aliquots frO<n each oontainer to prepare the composite sample In a 4-Uter far. 

Record the volume/mass of each aliquot used to prepl!re the composite sample on tho data sheet. 

Coile<1 a repreJenta tlve afiquot of the remaining material in a 500 ml)ar to be archived. 

SDS-D!i.SU.·Sanp/c ~rc 

Rtvf- Oafc' J.,.. 20/l 

R-.~v .... 20tJ 

VESOJ3814 
Containerized Solids Sample Composite Data Sheet 

Project Name Veo1ia-Sauget, IL Date \()I 0.'\ (I 3 

ProjeCt Number 40942525.21).()2 COndition No. 1 

Facility Unit 4 Run No o.t 

Stream Name Containeriztd Solids (CS) Start nme \•l! 

Composite Samp.le 10 VS4-CS.l COM ~ Stopnme I '535' 

Operator 

sample Volume/ S•mple Container to Time Volume/ 

Contalnecr 10 Time Number MW Number Mass 

l ~ 1&.31) 10()~ 21 

2 q. 13.,0 ~~~ .. 22 

3 ~0 1\0S' ~!:){)~ 23 

4 ~0 J'?>a.O ,'\\ 24 

5 b~ ~~5' a~~<\ 25 

6 &(') 1oso 3e~~ 26 

7 \~ I 'lOS' a<l~ 27 

8 <u I 'I ilO ~00~ 28 

9 \~t, , .. ~, 3Q'jj~ 29 

10 \\l tt.t'iO oCIO~ 30 

11 l~b I 'S O~ '30,}_~ 31 

12 l'ab 1r~o ,n~ 32 

13 11( 3 \'S~5 \0~ 33 

14 34 

IS 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volume/Mass ~' ~~ 

Comments: Take appropriately-sited and equalaliquots from each container to prepare the compos~• sample In a 4·Uier jar. 

Record the volume/mass of each aliquot used to pr•pare the composite sample on the data sheet. 

Collett a representative aliquot of the remaining material lrl a 500 ml jar to be archived. 

SD$-«1 SIA>-s-p/e c-,-· .. 

·ISIM Of!~9{""" EOJZ 

fh<o-d; J""" <OIJ 

VESOI3815 
Liquid Waste Feed Sample Composite Data Sheet 

Proj~ Name Veolla-Sauget, ll Date ti~~Jt> 

Project Number 40942S2.5.20-02 Condition No. 1 

FaciUcy Unit Z Run No ~/>.. 

Stream Name Low BTU liquid Waste (LBW) Stan Time <:~'ac Composite Sample 10 VS3-lBIY .(OMP .L Sl.opTlme {)a~ 

Operator 

Sample Number Tlme Volume/Mass Sample Number Time Volume/Mass 

l 0~~0 'S()O toL 21 

2 oq~o 2Z 

3 \()()') 23 

4 I Cla,o 24 

5 1035' 2S 

6 26 

7 27 

8 28 

9 29 

10 30 

u 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volume ~-~0() Ill L. 

Comments: Collect approl)(lately-sized and equ•l allquots and transfer Immediately Into a 4-llter composite Jar. 

Colle<t a separate 500 ml bo!Ue of sample at each samplins time to be retained in archives. 

~"'\)\~!, (,.0\ltc..\od ~rotrl ~-II .. ~.~~ 

SI)S ~ S<lb-$Dmpk Compont• 

flvm;., O.lt' J-20/1 

Rni<o..J:J .... Z0/1 

E·393 

VESOI3816 
Liquid Waste Feed Sample Composite Data Sheet 

ProjeCt Name veona - Sauget, tl Date \01 ~'Ill) 

ProjeCt Number 40942525.2()-02 Condition No. 1 

Fadllty Unlt2 Rim No a.~ 

SueamName Low BTU Uquld Waste (LBW) Start 11me I a.:!!,-

Composlte Sample tO VS34.8\V·1-": 00MP.Mi Stop Tlmo \sls 

Operator 

Sample Number Tlmo Volume/Mass Sample Numbt!r Timet Volume/Man 

1 1~'!. ~ ~00 ""'- 21 

2 1a.'iO 22 

3 tl o 'S 23 

4 1 'l a.o 24 

5 Il lS" ... 25 

6 26 

7 27 

8 28 

9 29 

10 30 

11 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volume a., 'i'00111\... 

Comments: Collect appropriately-sized and equal allquots and transfer Immediately Into a 4·Uter composite Jar. 

Coltea a separate SOO ml bottle of sample at each sampling time to be retained in archives. 

~a ..... ottd hiJI'\ x-1 \~\ tlllf'> 

$ll5 • 06 S..C·SM>pk C""'i'i'Ir• 

~~o-.om.: J- 201~ 

1/o- Jilt¥ 20/3 

E·394 

VES013817 
Liquid Waste Feed Sample Composite Data Sheet 

Project Name VeoHa -Sauget, ll Date 1ora.~113 

Project Number 40942525.20.02 Condition No. 1 

Faclfitv Untt 2 Run No &.B 

Stream Name lOW BTU liquid Waste (l8W) Start Tlmc ~~~S' 

Composite SampltiD VSH8W·J.o!l<OMP~ Stop Tlme \S'O, 

Operator 

sample Number T1me Volume/Mass Sample Numbe< Time Volume/Mass 

1 ~~~lj ~00 ... ~ ll 

2 IUO 22 

3 \606' 23 

4 l \d-o 24 

s 11'36' 25 

6 I ~'SO 26 

7 \'iOS 27 

8 I"\ ~0 28 

9 II%~~ 29 

10 I~ !5() 30 

11 l'fOf -I- 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 36 

19 39 

20 Final Volumo ; ,\OOM._ 

Comments: Collect appropriately-sized and equal allquots and transfer Immediately Into a <~-titer composlte)ar. 

Colle<! a separate 500 ml bottle of sample at each sampling lime to be retained In archives. 

'i>q_""\)1 Q(\ ~UII'I\ \\ ~~..tQII"' 

<.-#/1._.-f A,.o, i c...r £. VS3-J_gW-l:Z..I3- eo ... f'2P. -1::111 P 

SOS.(IfSSub·SM!plo C011Y"'SII• 

l«riskm t:Jtn-.· JU/re 1011 

ll"""""'*J- Z0/3 

VESOI3818 
Liquid Waste Feed Sample Composite Data Sheet 

Project Naill<! Veofla -Sauget, ll Dote ,~, .. ~113 

Project Number 40942525.20.02 Condition No. 1 

Facility Unit l Run No a.& 

Stream Name Low BTIJ llquld waste (l8W) Start Tlme liJ-'3) 

Composite Sample ID VSH8W f.t-COM ~ Stop l imo 1HS" 

Ope<ator 

Sample Number TTme Volumt/Mus sample Number Time Volume/Mass 

1 \;}.~~ ~()() f'l '- 21 

2 l~iO 22 

3 -noS l3 

4 I ~0.0 24 

s ~~~'J 25 

6 ll'lO 26 

7 , cto~ 27 

8 I "16.() 28 

9 ,q·u· 29 

10 14~0 30 

II \ fOG" 31 

12 11 no 32 

13 l'i!i" 1- 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Fmol Volume i,(:.OO "'L 

Comments: CoUect approprlately·slted and equal allquots and transfer Immediately Into a 4·Uter composite jar. 

Collect a separate 500 ml bottle of sample at each sampf111g tlme to be retaiMd In archives. 

f.Q""9 1~ holt\ "t."l\ 5 ~(QQI'I\ 

$()$..()!! Sub..sa.pl< ~;,. 

lll>fliM Drzr .. • J-Mft 

111""-d: ' """ 20/J 

E·396 

VESOJ3819 
Liquid Waste Feed Sample Composite Data Sheet 

Project Name veolla - Sauget, ll Date I() 1~1\1\3 

Project Number 40942525.20-02 Cooditlon No. 1 

Fadllty Unit4 Run No a~ 

Stream Name Hi&h BTU liquid W<Ute (HBW) Start Time C(\S{, 

Composite Sample 10 VS3-HBW-l <OMP .1:_ StOP Time 

Operator 

Sample Number Tlmo Volume/Mass SampleNumbet nme Volume/Mass 

1 01:\~E. ~00 h\1. 21 

2 O~'S I 22 

3 \00& 23 

4 \() ~\ 24 

5 \()-a~ .. 25 

6 26 

7 27 

8 28 

9 29 

10 30 

11 31 

12 32 

13 33 

14 34 

lS 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volume •• 150() .... \... 

Comm~ Colle<! apprOPriately-sized and equal aliquots end transfer immediately into a 4-Uter composite jar. 

Collect a separate SOO ml bottle or sample at each sampling time to be retained In archives. 

!.~c-.o ~~~ ~IOI't\ ~-~ ~\~ft\ 

5().5-05 Sub.s.n,pie ~·· - O.te: J-21>/l 

Rew..-I:J<JM//!()1) 

E-397 

VES013820 
Liquid Waste Feed Sample Composite Data Sheet 

Project Name Vcolla -Sauget, IL Dote ~~ ta.'tl n 

Projecl Number 40942S2S.2D-02 Condition No. 1 

Facility Unit 4 Run No 0.~ 

Strtam Name High BTU Uquld Waste (HBW) Start llme ~~{, 

Composite Somple 10 VS l!.!:COM~ Stop Time ral~ 

()per.! tor 

Sample Number Time Vclume/M•u Sample Number llmo Volume/Mass 

1 1 a ~€. 'l 0() ttl L. 21 

2 'n 1 22 

3 1~0{, 23 

4 I~(} I 24 

s ll ~5' -~ 2S 

6 26 

7 27 

8 28 

9 29 

10 30 

11 31 

' 12 32 

13 33 

14 34 

1S 3S 

16 36 

17 37 

18 38 

19 39 

20 Final Volume .-oo "'\. 

Comments: Collect ap.,ropriately~lzed and equalaOquots and transfer Immediately Into a 4-Uter composite jar. 

Collect a separate 500 ml bottle of sample at each sampling time to be retained in archives. 

sa"'o\ed ~"' -Ia.. ~+r(Qrn 

SDS-O!JSlJb.Sompk C/Jmposlf• 

-·(}Qte: JUM/0/C 

l/o-JUN20JJ 

E·398 

VES013821 
Liquid Waste Feed Sample Composite Data Sheet 

Project Nome VI!OIIa- Sauget, ll Dote \()flit /13 

Project Numb« 40942525.20-02 Condition No. 1 

Fad Illy Unit 4 Run No a.s 

Slteam Name High OTU liquid Waste (HBW) Start llme 1~){, 

Composite Sample 10 VS3 HBW .COM A\_ Stop llme I'SOE. 

Opera tOt 

Sample Number llme Volume/ Mass Sample Number rune Volume/Mess 

l 1~14 -aoo ~>~L 21 

2 Ia,_~ ) 22 

3 \~6b 23 

4 ll~l 24 

5 rns- 25 

6 ll'f I 26 

7 l'lO' 27 

8 l'l~\ 28 

9 I 't~' 29 

10 l't'rl 30 

11 \.;or. -1- 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volume 'i ,100 .,.I. 

Comments: Collect appro riately~lzed and equal allquots and trons!er Immediately into a 4-LHer composite jar. 

Collect a separate 500 ml bottle of sample at each sampling time to be retained In archives. 

qlflp I~ ~1'1\ "1. ~ st~111. 

c.t~wt ,.J. ...t..,. .. .... ~ ~ - .,,ew- roz.B- Gt>"'4f z (} - ~p 

$0$·05 SUb-samp/o CO/IIfN>SII< 

ltz-"lon l>ote: J-l0/2 

-J-lOJJ 

VESOI 3822 
Liquid Waste Feed Sample Composite Data Sheet 

Project Name Veolia -Sauget, tl Date ~1, \113 

Project Number 40942525.20-<12 Condition No. 1 

FadiKy Unlt4 Run No ~! 

Stream Name 1-ilgh BTU Liquid Waste (flOW) Start Time ~~~6 

Composite Sample ID VS3-HBW-1!l_-COMP j&. Stop Time l 'ilEl 

Operator 

Sample Number Time Volumo/Mau Semple Number Time Volume/Mass 

1 ~l{. a o <:> ,. \... 21 

2 \a.,~) 22 

3 I lOE. 23 

4 ll <1.. \ 24 

5 IllS' 25 

6 t\'tl 26 

7 Ill OE. 21 

8 I 'il-l 28 

9 1~\, 29 

10 Itt~ I 30 

11 I ~0(, 31 

12 •"~ I 32 

13 I fl~ -~ 33 

14 34 

1S 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volumo a ,\.oo ... ~ 

Comments: Collect appropriately-sized and equal allquots and transfer Immediately Into a 4-Uter composite jar. 

Collect a separate 500 ml bottle of sample at each sampling tlme to be retained in archives. 

~llfo\Qild f\1 1'1\ ~-"\<1.. b\- ~~ 

SO$ ~ Sub-Somplo Ccmpqsll• 

1/cvfPH 0.10' J""" 20U 

1/c-d: Jllf¥ 2(/JJ 

E·400 

V£8013823 
Liquid Waste Feed Sample Composite Data Sheet 

Projact Name Veoll•-Sauget, ll Date l()j~~"' 

Project Number 40942525.2().02 Condition No. 1 

Facility Unit 4 Run No ~A 

Stream Name liquid Waste Feed (L\VF) Stott Time <:><\37 

Composite Sample ID VSHWF· l!t.·COMP .1_ Stop Time 103J 

Clpe<ator 

Sample Number Time Volume/Mass Somple Number Time Volum9/Mass 

1 C)'\~7 ~()() .... L. 2l 

2 0"~~ 22 

3 \007 23 

4 IOU. 24 

s 10&'7 • 25 

6 26 

7 2? 

8 28 

9 29 

10 30 

11 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 31 

18 38 

19 39 

20 Flnal Volume a ,'ioo "'t. 

Comments: Collect approprlatelv-<fud and equal allquots and transfer Immediately into 1 4-Uter composite jar. 

Collect a separate 500 ml bottle of sample at each sampllns time to be retained in archiVI!s. 

~lt\t;)l9d ~~"' '1. -0.~ ~h~q"' 

SDS-M Sub-s-pie ~tit• 

Rcrtslt:HJ l»Je: JtJM 2012 

l&>i<w<dl J-lOIJ 

E-401 

VES013824 
Liquid Waste Feed Sample Composite Data Sheet 

Project Name Veolla - Sauget, !L Oite 101 a.~ IB 

Project Number 40942525.20.02 Condition No. 1 

Fa dilly Unlt 4 Run No a.~ 

tr~am Name Liquid w aste Feed (LWFI Start lime la-37 

Composite Sample 10 VS4-lWf.1i!-cOM!>M Stop Time IUS' 

Operator 

Sample Numb or Time Volume/Mass Sample Number Time Volume/Mass 

1 ~3"7 ;;oo hll.... 21 

2 \aos~ 22 

3 \\OJ 23 

4 tlU, 24 

5 1~H· .. 25 

6 26 

7 27 

8 28 

9 29 

10 30 

1l 31 

12 32 

13 33 

14 34 

1S 35 

16 36 

17 37 

lll 38 

19 39 

20 l~lvc ume ~.~oo "''-

Comments: Collect appropriately-sized and equal &liquets and transfer Immediately Into a 4-Uter composit e jar. 

Collect a separate SOO mt bottle of sample at eoch samplin& llme to be retained in ardllves. 

SI\10\0I~d ~(1)11\ )(~old. s\~ ~t~ 

SI>S·o551.b-~C-Ito 

/&tii'NM l>ot.: JUM l'OJl 

Ra- !Uf'ClOIJ 

E·402 

VES013825 
Liquid Waste Feed Sample Composite Data Sheet 

Project Name Veolfa- Sauset IL Date \()fa-4113 

Project Number 40942525.2().<)2 Condition No. 1 

Facility Unit4 Run No 0.\\ 

Stream Name Liquid Waste Feed (LWFJ Start Time ~~n 

Composite Sample 10 VS4·LWF-l .COM~ Stopn me \'iO? 

Operator 

Sample Number Time Volume/Man Sample Number Tome Volume/~ 

1 ~S7 l ()() "'L. 21 

2 I~U 22 

3 \l01 23 

4 \'H.~ 24 

s l'U!i 25 

6 1na 26 

7 \~07 27 

8 PI~ 28 

9 I '43'7 29 

10 1 'in 30 

11 l'r07 + 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volume ?11

100 ,..L, 

Comments: Colloo approprlitely-slzed and equal allquots and transfer Immediately Into a 4-Uter composite jar. 

Collect a separate soo ml bottle of ••mple at each samprons time to be retained in archives. 

~IC\gll'd tl'l)tr\ y.~~ s~t(Q"' 

~U...,f-u.4. d·Pi·~f-.. - ,. ... A v<>-4- - r..w F' - -l'2. P. - / "" ::t-~ - t>JP 

SD$-0$51.0-~ CMipMI« 

bWsfwt Ottte: J~~Z 20./1 

fl<y(<w<i/; J.-2013 

E-403 

VES013826 
Liquid Waste Feed Sample Composite Data Sheet 

Project N•me Veoila- SaUGet, tL Date 10(0.'1 fl3 

Project Number 40941525.2<Hl2 CDoortion No. 1 

Facility Unit4 Run No a..s 

Stream Name Uquld Waste Feed (LWF) Start Time ~l/ 

composite Sample 10 IIS4-lWH&l.COMP _!S, Stop Tlme \ 'i?.J 

Operotor 

Sample Number Time Volume/Mass s.tnp!e Number Tlme Volume/Mass 

1 10}.~ 7 a.oo ... L 21 

2 ll'W 22 

3 l'\07 23 

4 l)i).~ 24 

s nH· 25 

6 nu 26 

7 1'\01 27 

8 11tn 28 

9 I'll? 29 

10 \'\\'"~ 30 

11 1,-ol 31 

12 tU4 32 

13 1n1 _ ... 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 final Volume a,c.oo ... ~., 

Comments: Collett approptfately·shed and equal aliquots and transfer Immediately Into a 4·Uie< composite jar. 

Collett a separate SOO ml bottle of sample at each sampling time to be retained In archives. 

~""~\9d ~"' 1- i.~ ~~r@QI'\ 

5()$-05 Sui>-S<IiyM Car.pD$1/o 

fb!g(siotf /)of~ Jlllt Z()Jt 

R.- J- 2013 

E-404 

VESOl3827 
URS DAILY RECORD 

OF EVENTS 

I """\ • I l l. 

) I 

n ~ Otf•tt l, J (., ;! •. 

arl• ~~~ •• , 1, )""" tl'-lfl ..... IUJ. r. Lt.i, I,.HJ..A. J·Ur "''d"J' ~"~'" 

'·•r•-!•Y ~of J'••"Y ~~L-.,,.., SiF· 

r{ .tt~ 'q foft'pl~• j ((. h "'J'• r ff•""J•<•f/,-u!"·{· 

~J~ s-,. p.,,. :r. ·~ •• A t .,,. h ... ,. ,.,. 3 ~ c .. <1•14 

lliO • .,.. 11.,.. ~A - v,. H 

tiS~ ft, ''" f.•• ~A - 1/~ I , A>• ~. 6

,. 1Lll\ ~~.u,.lt( 

11'?1(, C.d lH.I- S l'"l ~ ~"I\~ 

<-1 ~ 't% PV.L ~~--~ II!.J ~~\'\ 

4~'1 t\L\Ill~ hq,,n <.o,.pl~~~·, ( tll''\ <,nl\\vlr Cr.,ropl.A q \ IIJ3'; 

1'1'\ t [..c)llr.c,l ~~>1\,.~ .<llo jl•~ 

c..1 " I"'"St P L> L ~~~~ IJJ a 11.~ 

I~ II kt\11,1~ hq,., I..Oo o\ltk '

1LCJ\1tC.I ':xlmjllt Ct. .pl.~ q\ lbCr) 

t\Ttl IT, a,;d fs ~ l'toh'"'UII'Iplf\l 1.\.1 ll>fi~)J) 

I \'.i LO\lPQ lit •U ~M ~\q_ 

L\ \l-nq7 Ph '- ~) 1 I d I\"' \~'i I [h qrd rs ~{Q If\ I.Ot 'I I l I Cot." \ ~1'11t t Len t ' Q I II.?.') 1114 rt) s .,(f 

llk3o lo ~ ' !.t•- 'Q \1) ~to 0•'1 

c.l 1-1-~11 tl:.'t• I l .,.,,, 

!t,~o Ttttl <•"'rl•1<~ j,.;~ts ~d"'~ S"""' : tr r./..15 

~/~ b:,•" ~ dw· /'{jf~;tr f<i!"fks 

C"'"'('l•i< '[oC~. 

1 ~ 16 ~~'"" •II f"pcr tl• ·~ / Cu(., . ~-"" Cuc.f lo l(iv.,; He-6;,., . ~~5~1 {f,rtd 01\ · w••l .... II ,f lo~'"j dovL c.....,,, ~h/l . .. .t I ul 

(04· 

E-405 

VES013828 
Field Balance Calibration Check 

Project Nome ___ v;;e;;o;.:;li~ai:S;;au~g~e~t,;:';;. l _ _ 

Project Number __ _.::.409=:.;2,52;5::;~40::..()2 _ _ 

Facility ----,,-;.U;,;n:;it;:.3:,.-- -

Balance 10 _ _ ..;. 'i.:....:._:..;;..;--

Callb<otlon lniUals (Itt'> 

Chec)(ed by Date ~2.'5'1~ 

.......... ~ ... ......,,_ l$nce kad1nc ..,..,_. 

w..;po" (!.-- Perc:tnt o~· 

ld 

lei ~MioO!ld ld 

20 tp.o 

50 s:o.o co ~rotloft Cbocl< of 

e•nc. UNna Stvder.t 100 100. 0 

welch~> 200 z_po . 0 

Studtnt Weicht S•t ID: 500 5"00 • l 

Hllr 'g 1000 IODO. "2-. 

"""""-...;p...., .. ..,-~ .. ' • tho bolloc! -used toweiP ....-. .,...., ., .. 10001.-tho IIXlD ond soo..--lor , ,_.,..co«< • Tb kCJ; ttNI! aiWil for PftUI'!I: cflft!lnntl: It .o.s• nw. .. c.ollnMc<l U5i!l&. this ~ 

Percent DUfee a • ba!anoe =:'mass x 100 

&/JS·08D< Fkld 8•'-• C•Hbf'<IIIM 

hr EM SoP·OIO 

ll<wsiolt O.lc.' M....-IJil0/1 

R•"-- JIJ!y 1011 

E-406 

VES013829 
< t'l'1 

Vl 

0 

..... 

00 

w 

0 

m 

.. 

!:l 

Sample 10 Code Stream 

~S4-S$.13A.Qrno1 USc*ls 

~54-BS. t3A.(;rab I USalcl$ 

~S4-8S-13M>rab 2 N:Salcl$ 

IVS4-es-t3M>rab 3 lUI Solds 

lvS4-Bs.t3A.(;rab. fUI:SCllds 

- ~~ 13Mlrab 5 lUI Said$ 

~S4-BS. t3A.(;rab 6 N:Scllds 

- ·· ""13A.(ltab 7 lUI Salcl$ 

lvS4-IlS-13Mlrsb 8 Ill* Sob 

r.-s4-ll$-13~2A MSolds 

>~ ' 00-13!l.Comp28 B~Solds 

-BS-13~2C BUlk Solid$ 

r-s4-I!S·138-Gtab 1 Bt* Solds 

~-8S.I3S.Grab 2 Bulk Solids 

V$4-ll$·138-Grab 3 Bult Solids 

V$4-Bs-138-Grab 4 Bulk Sdids 

VS4-BS·138-Gtab5 Bill Solidi 

lvS4-Bs.13B-Gr.!D 6 B~ ScAlds 

V$4-SS-138-Gtab 7 illlllt Solids 

lvS4-8S.138-Gr.ID 8 MSolids 

V$4-85-138-Gtab ~ illllk Solids 

lvS4-IIs.138-Gr.!D 10 Ill* Solids 

lvS4-BS.138.(ltab 11 9ult Solids 

138-Gr.!D 12 lli*Solds 

,,..., "" 138-Gr.!D 13 9tA1< Solids 

~S.13B-Gr.!D ,. USCllds 

Waste Sample Logbook 

Veolia-Sauget, IL - Unit 4 CPT 

Project Number 40942510.20 

Fraction Cond Run Date nme 

~ 1 3A 0 ~)~ 

An:iWe 1 3A ~'\?.E. 

NdWe 1 3A 0'\<tl 

Nrtitve 1 3A aOO(; 

Attt.iw> 1 3A I ()d.) 

AlrtWe 1 3A 10~ 

NrtM 1 3A 

Atd:ive 1 3A 

AII:Me 1 3A 

l'llysiComp 1 38 ~Yar,JS_ ~ 

Pllys/Corrc>, ~ 1 38 lCM' 

Phys/Canp 1 38 I(,~E, 

Alehl\18 1 38 ll~ 

An:hive 1 38 ll~ 

Atchlve 1 38 ~~ 

Atchiw 1 38 I'll I 

Atchlve 1 38 \'llf 

An:tllve 1 38 1~1 

Atchlve 1 38 

Arthlve I 38 ·~ 1'5~1 

Atd1lve 1 38 16~6 

Ardi .. 1 38 l'iJ 

Atd1lve 1 38 K66 

M:IM 1 38 

Alr1We 1 38 . ·~· ~ 

M:IM 1 38 

Page 13 of 29 

TW GW Comments 

-:l~~ ~ 

ql.\i 

f,~~ t.'t7~ 

~~ 1~ 

5'\ ~ h_~O~ 

106, 1,£> ~ __, 

;1 9-~<1. 

l ,l .. ~ 

~~ q 

'Slli a.Q~ 

~'S8ct 111,~1'& 

-r:\_!1 ~,~~ 

'6Cl \~~t a;~ ~~ 

1:.\h a,s'\~ 

1~ \, \0,~ 

Eo~ ~ 

~'ill, ,(.(\ 8~ 

514~ .!1 8~ 

5'3~ ~~~ 

~~0~ \ ~: .. a4~ I_,! &a~ 

'~~ ~,,~ 
tii 

en 

0 

...., 

00 

w 

-

Sample 10 Code 

"'· ~~ 13A-Comp1 

VS4·CS.13A·Grnb 1 

""' "~ 13A-Grab 2 

VS+CS-13A-G<ab 3 

VS4·CS·13A-Grab 4 

VS+CS-13A-Grlb 5 

VS4-CS.13A·Grab 6 

VS4-CS·13A-G<ab 7 

\J<!A I'< 13A•GraiJ 8 

~S4-CS 138~2A 

'"' ~~ 13S.Comp28 

~S4-CS.138~2C 

VS+CS-138-Gtab 1 

i'fS4-CS.136-Grab 2 

VS4-CS.13B-G<eb3 

~54-CS-138-G<ab 4 

VS4·CS.138-Grnb 5 

VS4-CS-13fi.Giab 6 

~S4-CS.13B-Grab 7 

~S4-CS.13B-Grnb 8 

~54-CS-138-Gtab 9 

VS4·CS·138-Grab 10 

VS4-CS-1JB.Gaob 11 

~CS.13B-Grab 12 

VS4-CS·13B-G<eb 13 

'JS4.CS-138-Grab 14 

Stream 

~Sclids 

Coolalnerized Solids 

C<Jllalnerized Solds 

Coolllinerized Sclids 

Conlalnerlzed S<lllds 

Contamtzed Solds 

Coolalnerized Solids 

Conlalnerized So41ds 

C<Jllainerized &lQds 

Ccnlainelized ScCJds 

Continerized Solds 

Containerized Sefids 

Coolalnerized Solids 

Coollllneriled Soids 

Containerized Solids 

Cootainerized Sold! 

Contalnelized Solids 

Coolailerized Solids 

Contllnerlzed S<lllds 

Ccnlalnerized Solids 

Conlainefized Solids 

Containelized Solids 

Cootanemed Solids 

Contalnelized Solids 

Cootainerized Solids 

C<Jllalneri2ed Solids 

Waste Sample Logbook 

Veolia-Sauget, IL - Unit 4 CPT 

Project Number 40942510.20 

Fraction Cond Run Date Time 

~ 1 3A "'Q,t., 10,.. 

Arc:hiYe 1 3A <J\~ 

AroNve 1 3A ~'50 

Archive 1 3A ~()~ 

Archive 1 3A ~ 

Arr:Hve 1 3A l0\0 

Archive 1 3A 

Ardllve 1 3A 

Arctil-e 1 3A 

PhysiColrll 1 38 '·· I'B'i' 

~.Melals 1 39 I~ 

Phys/Comp 1 3B IUS' 

Arc:l1i'le 1 39 I'U! 

ArchMI 1 3B tl'JO 

Arc:hive 1 3B I 'to'S 

ArrJiole 1 3B tctao 

Archive 1 38 l't~ 

ArohM! 1 3B !It~ 

ArthiYe 1 3B 1'5W 

ArChive 1 38 l'f~ 

ArohiYe 1 38 lflS" 

Arelllvo 1 38 •m 

Archive 1 3B 1&06 

Arthive 1 38 IWO 

ArChive 1 98 ~ \taf 

Arthive 1 38 

TW GW Comments 

TJC\ ~tn-:" ~'- ~ .l,Cl'iO <\ 

~'"' '13. i I ,1.\Ba(\ 

'\~~~ ~.~~ 

'i;)3tA c,c· lpcJ.~ 

5~ ?Oj I.a.~~~ 

as I\~ 

3.~~ 

,~ 

;a ~- '3a. ~ a.<:m' 

'S()fA IQ.. \I no Cll 

ll~a<i l<>:, 1,~3.~~ 

~ •. ,1\~ 

m~:, 10~ '·~~~ 'iOC~ · ~~ 

'SifG 8~; l,'iO'\c:; 

Sl§ <t''t~ ,87·~ 

~ lQq j ·~~~ 

~~ 1!4\ ~ 1,30S~ 

~~<1 ~..,»l~ 

~El!C\ ~'lj 1,1~, 

s~ lq~~ 't'l'l C\ 
< 

m 

(J} 

0 

00 

'-'

'-' N 

Sample 10 Code 

~S4-l8\' ~1 

..... "".t-llMlnb 1 

~ RW.Il,t,-Gr*> 2 

lv<:...o - -13A-Gtab 3 

~v.,..,...,,JMlnb< 

iv<:...o "W·13A-Gr*> 5 

~W·I3A-Grab6 

lv<:...o ""'-~~ 7 

~S4-LBW-13A·Grab8 

iv<:...o "W·138-Ccrrp21\ 

- 13&-Comp28 

lvS4-LBW 13B~2C 

~ RW.1J8.Gtab 1 

~W·13B Grab 2 

lvS4-lBW·130.{;rab 3 

iv<:...o RW. IJB.Grab 4 

VS44..BW-138-Grab 5 

jvs+ulw-138-Grab s 

"""" ' ""'·IJB.Qab 7 

VS4-I.BW·13B-Grab8 

1'1-138-Giab 9 

~ RW.IJB.Qab 10 

VS4-l.BW-138-Grab 11 

""'. • .... 1JB.Gr.lb 12 

b.. RW.1J8.Gtab 13 

~$4-lBW-139-Grab ,. 

Stream 

Low Bw Uquid Wasil 

lDw lll.o Up! Was~& 

lDw BIU Uquid WLow Btl Uquid wLow lll.o Up! Wasllt 

low BIU Uquid Wasllt 

Low BIU Lip! Wasm 

LowBIU~~ 

low BIU ll"'id Wa~ 

Low BIU Uquid Wasll! 

Low BIU UquidWasle 

low Bill Uquid Wasil! 

low Bill Uquid wlow Btu ~ld waste 

l ow Btu l iquid Wasto 

low Btu Liquid Wasla 

low Btu ~id Wasle 

low BIU ll~ Waste 

low lll.o Uquid Waste 

Low BW Liquid WilSie 

low Bill Liquid WLow BIU Uquid Waste 

Low BW ~id W3SI8 

Low BIU Uqud Wasil 

Low lll.l Uquid wLow Bill Uqwl Waste 

Waste Sample Logbook Pege 13of16 

Veolla-Sauget, ll - Unit 4 CPT 

Project Number 40942525.20 

Fraction Cond Run Date Time TW GW Comments 

""~ 1 3A "M. lOlS' .L'S110 ~ 

AldWe 1 3A ~~ '5 foe) _"ll. 

MJWe I 3A oq~ 

MJWe 1 3A II OO'f 

MtfNe I 3A I~ 

AtrJiNe 1 3A ~ 10\$' ... 

Aictive I 3A 

kttive I 3A 

All:hive 1 3A 

PhysK:omp 1 38 ~Ia t'4W il;'500~ 

Mel;als 1 38 IE.Qf 1,lOO .. t. 

""~ 1 38 6~ ~.~ ... ~. 

An:tt;e 1 38 J'Uf' 

61)0 ""' 

Archive 1 38 1»0 

Arcl\lve 1 38 J'tof 

Atthive 1 38 tCfiO 

Arclive I 38 lCI» 

Archive 1 38 N'S() 

MtfNe I 38 ISOS 

Archive 1 38 I~ 

Archive I 38 •mMir-e 1 38 )Sf() 

Archive 1 38 L40r 

.t.'dM I 38 I~ 

.t.'ltliYe I 38 ... ''* ~ .. Arclive 1 33 
Waste Sample Logbook Page 5of16 

Veolia-Sauget, IL - Unit 4 CPT 

Project Number 409-42525.20 

Sample 10 Code Stream Fraction Cond Run Date Time TW GW Comments 

•~ un llA-Ccnlll ~ Ba11.41<1 w.a ~ 1 3A ~. ~ lrl~ '5oO .. l 

IJA.(lQb I ~ Ball.lqiAcl Wasut AAme I 3A j()q,(, 1$00 "'-

~QW.I3Minlb2 ttg~ Bill IJqiAcl w- lvrJWe 1 3A jo<\ fl 

f.ls.uiBW·IJA.(lQbJ ~ Bill UqUd Waste lvrJWe 1 3A oof. 

~8W-13A.(lQb4 ~ 8a.t UqrJd Wasle lvrJWe 1 3A tOi-l 

lvs.uiBW-13A.(lQb 5 High Blu IJqiAcl Wos1e lvrJWe 1 3A .... I~ ....L. 

iv~BW 13A.(lQb S High 8tr Uquid Wasle AltiM 1 3A .... 

~SW I3A-Grall7 H;j>Blu liquid Waste Ald1M! 1 3A 

VS4-HBW·1JA-Gtlb a Hlglllllu Liquid WoJSle AltiM 1 3A 1- - - - --- -... 

·~· ""W.138-<:omp2A High BIU liquid Wos1e PllJSICarll 1 JB I'~J .. l'\3f .~ ... ~... 

VS4-HBW·138-Comp28 Higtl Bill Llqllld Wasle Physl~. Mela!s 1 J8 140b , ,300 .... 1 

~BW·1JB.C4mp2C High BIU llq~ Waste ~ I J8 l&,E. &.,la co ~ 

VS4-M8W·13B-Grlll1 High Bill Llq~ld Wasto An:ll!lle I J8 ,~ .. ~OO ... L. 

jvsol.HBW·138.Qab 2 Higtl BIU llq~ Waste An:ll!lle 1 3B ll'S I 

V$4-HBW-138-Grab 3 High BIU Liquid Waste An:lllve 1 3B \1\0' 

lvS4-HBV1·138·Gtab 4 Hlg1 BIU Liql.id Waste AldlM! 1 38 ,,.., 

VS4-H8W·13S.Gtob 5 High B:u Liquid Wasle Ard1!11e 1 3B 1'4lf 

~BW·I38-Gfab6 tf9\81UL~Was1B An:lwYe 1 38 l't~ I 

f.IS4-HBW-13&<1rlob 7 Hlgilfllu Llql.id Wa51e An:lllve 1 38 ~~ 

lvSoi-HBW-138-Grall& High BIU lkJJ!d Was NciM 1 3B l~\ 

f./$4-HBW-138-Gtat> 9 HlgiiBOJ Llql.id Waste M:lllve 1 3B 

jvs4-HBW-138-Grall10 Hll;tl Bil1.41<1 wage An:lwYe 1 38 \~'1 """' 

Z' lv54-H8W-138-Gtatl 11 High Bill llql.id Wa51e Aldllve 1 3B ~ 

< 0 

ITl 

(/) 

0 

-.... 

~81V 138-Gtatl12 Higll Bill UqrJd Was>e A.'tt.lw 1 38 1~\ 

~BW·138-Gtatl 13 Hlgll BOJ ~Waste AlftiNe 1 3B - IQl. .J: 

·1 J8.Gtab 14 ltgl BIU 1.4111 Wil$111 lvrJWe 1 38 - -· - - 00 

w 

w 
< 

m 

en 

0 

w 

00 

~ 

Sample 10 Codo 

~Wf·1~1 

jvsA.I.WF·1l-'.Qnb 1 

~WF·134-Grab 2 

jvsA.I.WF·1JA.Grlb 3 

VS4-tWF·134-Grab 4 

~Wf·13A-Grab5 

VS4-tWF·13A-Grab 6 

~WF·13A-Grab 7 

jvsA.I.WF·13A-Grab 8 

VS4-LWF·138.ccntp2A 

jvs4.l. WF·138-Colr!>2ll 

VS4·LWF-138.Cctrll2C 

jvs4-LWF-138-Grab 1 

!v*WF·13s.Gtab 2 

jvS4-LWF·138-Grab 3 

~WF·138-GI1b. 

VS4-LWF-138·Grab 5 

jVS4-l. Wf·138-Grab 6 

~54-tWF-13&-Gr.lb 7 

!'JS4-l.Wf·138-Grab 8 

~WF·1J8.G-1b9 

VS4-tWF·138-Grab 10 

~S4tWF·138-Grab 11 

jvs4-l.WF·138.(3rab 12 

~Wf·138-Grab 13 

~WF· 3a-Gnl> 14 

Stream 

l.ll!uld wz:a Feed 

UqUd Was!e F* 

UqUd Wale Feed 

UqUdW-Feed 

UqUdWaslefeed 

UqUd Wasil Feed 

UqiAd Was18 Feed 

UqUd Vlw.e Feed 

UqUdWamF* 

Uquld Wasle Feed 

UqUd W.W Feed 

Uquld Waste Feed 

Uquld Was:a Feed 

LiqUid Waste F* 

LIQuid IVOSUl Feed 

UqUd Wasle Feed 

Uquld Waste Feed 

Uquld Wasta Feed 

Uquld Wasle Feed 

Uquld Wasle Feed 

Uquld Wasle Fted 

Uquld WaS1e Feed 

Liquid Was18 Feed 

Liquid WaslB Feed 

UqUd Wasle Feed 

UqUdWas18Feed 

Wast e Sample Logbook 

Veolia-Sauget, IL - Unit 4 CPT 

Project Number Ml942510.20 

Fraction Cond Run Date Time 

~ 1 :1-' !"" .. ,,, o~J 

An:hM! 1 :1-' I<R!7 

MtM 1 :1-' ~,~ 

AlrHte 1 3A 100? 

Nttive 1 3A ~oM'. 

Nfjtve 1 3A ~ 1017 

AldWe 1 3A 

AldM I 3A - - - A:ciWe 1 3A 

Ph)'S/Conl> I 38 r-,,, I'QS" 

Ph~ ~ 1 38 1(,01 

PhY'fCo<r!> 1 38 ,.,~, 

Archlva 1 38 1~7 

Atehive 1 38 11¥ 

Archive 1 38 11.\0., 

Atr:Nve 1 38 

Arehlve 1 38 ·~ \~ 

Arehlve 1 38 r'lU 

AteiWe 1 3B ,~, 

Archive 1 38 \~ 

MtM 1 3B 1$}7 

Archlva 1 38 1m 

Atdive 1 3B l{t)7 

Mme 1 38 

Mme 1 38 .t- ·~ 1~17 

Aldwe 1 3S -

P~e5of29 

TW GW Comments 

~ ''500 "'I.. 

~00 ..... 

.I-

- • • 10()~ 

~,!00 .. 1.. 

-.~..L 

iO() " '-

I 

f 

I 

I 

I 

.l. 
Waste Sample Logbook Poge 15 of29 

Veolia-Sauget, IL • Unit 4 CPT 

Project Number 40942510.20 

Sample 10 Code Stream Fraction Cond Run Date Time TW GW Comments 

·~· ... 14A-Ccn:c>1 &*Solds ~ 1 4A .... lrl llfl 1.?31"' 

k"' ' "" 14A-Gfab I &*Sdids Atdiw 1 4A l()'f S?a," I I ?,~7"' 

~~ ' eo 14A-Grlll 2 S.Solds Atdiw 1 4A II !~(a , .. 1,\3\o. 

14A-Grlll3 8ult Scllds An:IM I 4A 11 .. \ 1N~o. 1,EM>q 

14A.Gni>4 S.Sclds Nrme 1 4A \\lG E,"J~~ l,Etl'i (11 

,., 14A~5 &*Scllds lvtme 1 4A ..L llfl ~l o. .. .,a, a 

14A.Gnb 6 IliA Scllds AldM 1 4A 1\ / ~BS.14A-Glab 7 ~lk Sdids .Ait:tM 1 4A ."' 7 ""'"'' 1~8 Ill* Solids NdWe 1 4A "' J 

ivs+SS.146-Ccmp2A 81Ak Sdids ~ 1 48 

""" 

7 jvs.t.as-1~28 BUlk Solids Ph~.Me~als 1 48 "' / lv~-Bs. HB-Cornp2C BlAk Sclds Phys.~ 1 48 "' 7 IIS4-8S.1~ 1 Bui~S~ Atehive 1 48 "' / 

IIS4-6S-148-Giill> 2 8'* Soids Archive 1 48 1"".. / 

VSL8S.148-(lra!> 3 Bulk Solid$ ArthNe 1 48 

"""" ~Bs-148-Giab 4 Bulk Solds Arthi'le I 48 7' 

VSL8S.148-(lrab 5 Bulk Solids Arctm 1 48 / 

""" ivs+Bs-148-Giab 8 8'* Solids Ald!ive 1 48 v " VS4-Bs-14B-Grab 1 Bulk Solids Archive 1 48 / "' lvs+es-148-Giab a BIAI<Sclds Arcl'iVe 1 48 / '\ VS4-Bs-1~ 9 l!ullt Solids A«me 1 48 / "'\ 

i'J$o4-Bs.148-Giab 10 BlAkSolds Atti1MI 1 48 / '\.. ~So4-Bs-1~ 11 &*Solds Atti1MI 1 48 / ."" . ... 148-Giab 12 MSolds An:IM 1 48 v "' lvS4-Bs-1~ 13 l!ullt Solds Ndllve 1 48 / \. .... 148-Giab 14 IIUic Solds AtdWa 1 48 1/ 
Waste Sample Logbook Page 23 of 29 

Veolia-Sauget, IL - Unit 4 CPT 

Project Number 40942510.20 

Sample 10 Code Stream Fraction Cond Run Date Tlme lW GW Comments 

lv~1~1 Codao•W>d Sal4s ~ 1 4A " '0 ~ 

iVs4·CS-14A-Gial> 1 COl iCJIII(!ftzed Sal4s AtttM 1 4A 

· ~ 5' ~ 7t, ·. 10~<\ 

VSI-CS-14A-G!al> 2 ~Sdldl NrJ:M 1 4A 005 S"l~ ~~ l,anco 

14A-G!al>3 COialn•lzel Sal4s NritYe 1 4A 110() 7'\ ~ ~ ·, ~~~ (." 

1~4 Ccr1lainellzed S:lllls Mme 1 4A "''" ~ ·. \~1\ .. 

14A-Gral> s COiitaoeized Sclds Atdl.~ 1 4A """ II~ l);l5"1 nct j rJO ~ 

WI~· 14A-G!al>6 Conlainlrlzed Sdldl AldWe 1 "" I'-. -, 

14A-Gral> 7 C<lnlalnerized Solids Arrffle 1 <lA ..... 7 

lvS+CS-14A-Grab 8 CallillnetlzAid ~ Archive 1 "" "' / 

VS4-CS-14B-Comp2A ~Solids Pliys/Comp 1 48 / 

jvs4-CS-148.¢oal>2B Contalnellzed Solids ~,p,Melals 1 48 " / 

lvS4-cS-1 4S.Comp2C Conllonertzed Sclds Phy~ 1 48 '\. 7 

jvS4-CS-148-G!ab 1 Containerized Solids Archive 1 4B / 

lvS4-CS. 148-Grab 2 Con1anertzed Sclds Arci1Ne 1 48 '\. 7 

lvs4-cs-148-Grnb 3 Co"talnerized Solids Archive 1 4B "" / 

lvS4-cS.14B-Grab 4 Coolalncrized Solds Archive 1 48 ' [7 

V$4-CS-148-Grnb 5 Conlalnof1zed Solidi Arclllve 1 48 I "' lvS4-cS-148-Grab 6 Cot1cDinert!ed Sclcls Artlllw 1 48 7 

lvS4-CS-148-Grab 7 Containerized Sclllds An::ilive 1 4B / "' "' ~S-148-Gtab 8 Con!M\ertzed Sdlcls Archive I 48 \.. jvSl-CS-1~b 9 Contafncrized Solkb Archive 1 48 / lu.~ r~ 148-Qal> 10 COIIIIinerized Sc:lcls Archive I 48 ' ' "" rn 

: 

< w 

jvS<-CS-148-G!ab 11 Conllilleriad Sclds Archive 1 48 / ~ 

1~12 COI,._tud Sdlcls Archive I 48 / "' ('1'1 

tl.l ""' "' 1~13 CotltJIMrtzed Sclcls Atc1M I 48 / '\ 0 

-..., •w ~'<'1~14 Contanartzed Sclds Archive 1 48 1/ 

00 ' 

..., 

0> 
< 

m 

en 

0 

Sample 10 Code 

VS4-LBW·14A~1 

VS4-I.BW-14A-Grab 1 

~ - ·1<1A-Grab 2 

lll:L.I R\'1-14A-Grab 3 

VS4-LBW·14A-Grab4 

VS4-LBW-14A-Grab 5 

VS4-LBW·14A-Grab 6 

VS4-LBW-14A·Grat> 7 

VS4UW·14A-Grab 8 

VS4UW·1~ 

VS4-l.SW.1~29 

~AW.1~ 

VS4-LBW·148-Grab 1 

V~LBW-148-Gr.lb 2 

VS4-LBW-148-Grab 3 

VS4-LBW-14B·Grab 4 

VS4-LBW·14B-Grab 5 

VS4UW-146-Grab 6 

vc:.u --148-Grab 7 

iVS4-tBW•148-Gtab 8 

~BW 148-Grab 9 

VS4-tBW·14B·Gr.lb 10 

VS4-LBW·148-Gtab 11 

VS4-LBW·148-Grab 12 

VS4UW·146-Grab 13 

~W-146-Grab 14 

Stream 

Low Bll Uquld Waste 

lowBli UquldWasle 

Low B!U UqlidWasto 

Low Bll Uquid Wasle 

Low Bill Uqlid waste 

Low Bill Liquid Waste 

low Btu Uquia Waste 

Low Bill Uquid Waste 

low Btl Uquid Waste 

Low B!U Uquid Waste 

low Btl Uqlid Wasle 

low Btu Llquld Wasle 

Low B!U UQ\Jllj W.. 

Low ew Uq!MI Waste 

Low Bill Liquid Waste 

Low B!U Uquld Waste 

low Btullquld Waste 

low Btu Uquitl Waste 

Low 8!U Liquid Wasla 

Low 8!U Uquld Wasle 

Low Btu Uquld Waslil 

Low Btu Liquid Waste 

LowBtullquldWaste 

low Btu Liquid Wasle 

Low BW Liquid Waste 

low 8lu l.iquid Wasle 

Waste Sample LogJtook 

Veolia-Sauget, IL - Unit 4 CPT 

Project Number 40942525.20 

Fraction Cond Run Date Time lW 

Phys/Comp 1 4A ''IG \\6'0 

AlrJWe 1 4A 10,0 

An:l1lve 1 4A \1()~ 

AlrJWe 1 4A ~~~~ 

AlrJWe 1 4A IIJS 

Artlllve 1 4A ..... 11'50 

Artllive 1 4A " Ardlive 1 4A 

Artllfve 1 4A " "' Pltys/C<lmp , 4B " 

F'hys/Comp, Metals 1 4B "' PIJ)'SIComp 1 4B ""'-

Arclive 1 4B " 

Archive 1 4B 

Arthive I 4B 

Arclllve 1 4B 

Atthlve 1 48 

Atthlvo 1 4B 

AldM I 4B / 

An:hive 1 48 / 

An:hlve 1 4B I 

AtchiY(l 1 48 / 

Arl:h!ve 1 4B / 

Atchlve 1 48 / 

Atchlve 1 4B / 

Ard1iYe 1 4B / 

{ 

Page 15of16 

GW Comments 

z.5oo ....-\ 

<;()() "L 

... / 

/ 

I 

I 

/ 

/ 

' / 

' / '· ',, v 

L , 

/ " v "' ""'-

" '\ 

\.,_ 

'\ 

\ 

\ 
Waste Sample Logbook PBge 7 of16 

Veolia-Sauget, IL - Unit 4 CPT 

Project Number 40942525.20 

Sample 10 Code Stream Fraction Cond Run Date Time TW GW Comments 

VS4-Ii6W-1.4A.Qln1p1 ~UquidWasle Pl1y!IC<Imp 1 4A J,, liS) 3.,91Q.,.L 

VS4-IiBW-14A-Gmb 1 High ew Uqui! Was1e ~ 1 4A IO'i ~OO"'L 

V$4-liBW· W.-Grab 2 High Btu U11id Was1e Althive 1 4A ll ~ 

VS4-HBW·14A-Gn!b 3 High Btu Liquid Wasle Archive 1 4A II a.+ 

VS4-IiBW-14A.Gnlb 4 Hlgh Bill LqlidW3518 ~ 1 4A ,,~, 

\ls4.HBW-14A-Gnlb 5 High B1u Liquid Wasle Nctr.e 1 4A ... 1151 _..., 

VS4-HBW-14A-Grab 6 High Btu Liquid Wasle Althlve 1 4A 

""" 

/ 

•' 

VS4-HBW-14A.Qab 7 High Btu Liquid Waste Archive 1 4A r-.. / ""· u~ ·14A.Gnlb8 High Btu l.iqoid Wasle AtdWe 1 4A 

". / 

VS4-IfBW-148-Comp2A High Btu Uquid Wa~ Phys/Comp 1 4B / 

VS4-HBW-148-Cort1'2B High Btu Uq\Ad Wasle PhysiCOII'9, Metals 1 48 ""' / 

VS4-HBW-14B.Qln1p2C High Btu Liquid Waste Phys/Comp 1 4B / 

VS4-IfBW-148-Gr.lb 1 High Blu l.iqoid Wasle M:J:Cve 1 4B L 

VS4-IfBW·14B·Gr.lb 2 High B1u Liqlid Wasle An:live ' 48 ' / ' 

V$4-HBW-148-Gmb 3 High Btu U11id Waste Archive 1 4B ', / 

VS4-IfBW·148-Gtab 4 High Btu ~id Waste An:hive 1 4B / . VS4-HSW-t48-Gnlb 5 High B:U liquid Waste ArdiNe 1 48 / ' 

VS4-If8W-148-Grab 6 High Btu Liqlid wa~ An:hi\'8 1 4B / ' 

VS4-IfBW.IA8-Grab 1 High 8lu U1uid WastD Archive 1 48 / 

V$4-liBW-148-Gtab 8 High Blu l.iqoid Waste MJ:r;e 1 4B / ' 

VS4-HSW-14B.Qab 9 High Btu Llqui.d Waste Arel1ive 1 48 / ' ', 

VS4-HBW-14B·Gr.lb 10 High Btu Uqlid Waste Atehive 1 48 /_ '\ 

m 

.... VS4-If8W-14B-Gmb 11 High Btu Uquld Waslll ArtNve 1 48 v '\. 

< 

;;; VS4-Ii8W.148-Grab 12 High Blu l.iqoid W3Sie ArdiNe 1 48 / \. m 

f/} 

0 

-

v.> 

VS4-HBW·14EI-Gtab 13 High Btu Liquid Wasle Archive 1 4B I ' 

VS4-HBW·14B·Grab 14 High Btu liquid Wasla Atehlve 1 48 L 

00 

w 

00 
< 

m 

en 

0 

<.> 

00 

w 

"' 

Sample 10 Code 

jvutWF-~1 

~WF-141.Grab 1 

~WF·1"'.GGII> 2 

jvS4-LWF·14A.()Qb 3 

tvutWF· 14A-Gn!b 4 

~WF-14MlhbS 

~WF-14A-<bb 6 

~Wf-14Minb 7 

~WF-14A-Grab 8 

lvmwF-1411-Con1l2A 

lvS4-t.WF-1~ 

V.'F-1~2C 

ivsH WF ·1 48-Gnlll 1 

VS4-lWF·14B-Gn!b 2 

lvSHWF·14B·Grab 3 

lvS4-lWF·148-Grab 4 

lvS4-t.WF·I48-Grab 5 

~-lWF-148.Q'ab 6 

VS4-lWF-148-Gnlb 7 

VS4-lWF·14B-Grab 8 

i"S4-t.Wf·14B-Grab 9 

~WF-14Grlb 10 

~Wf-148-Grabll 

~WF-14&-Grlll 12 

~WF-148-Grab 13 

~WF-148-Gnlll14 

Stream 

Lt!l*l w- Feed 

UqoJd 'II- Feed 

Liquid Wasle Feed 

Uquld WIISIII Feed 

UqoJd~Feed 

UqoJd was-. Feed 

Liquid was-. Feed 

Uqu'4 Weste Feed 

Liquid WM!e Feed 

Liquid Waste Feed 

Liquid waste Feed 

UqUd W3s1e Feed 

i.lqiAcS Waste Feed 

Uqukl Woste Feed 

Uquld Waste Feed 

Liquid Waste Feed 

l.lquid Wasle Feed 

Liquid Wasle Feed 

l.lquid Wasle Feed 

Uquld Wasle Feed 

Uqllld Wasle Feed 

Uqukl Wasle Feed 

Uqukl waste Feed 

Liquid W3Sie feed 

UquldWastafeed 

Uquld Waste Feed 

Waste Sample Logbook 

Veolia-Sauget, IL- Unit 4 CPT 

Project Number 40942510.20 

Fraction Cond Run Date Time TW 

~ 1 4A "'*'• 110 

Att:hNe 1 4A \}O "J~ 

Ndive 1 4A \107 

Ardive 1 4A lla.o. 

Att:hNe 1 4A \137 

Arri:lft 1 4A '. ~ l><dM 1 4A "'* 

AA:hf.le 1 4A " 

AlrtWe 1 4A 

Ph~ 1 48 

Phys/Cornp, Me!ab 1 48 

~ 1 48 

AtdWe 1 48 

Atctive 1 48 

Atchive 1 48 

Archive 1 49 

AtciWe 1 48 

Att:hNe , 48 

Altl1iVe 1 48 

Atctwve 1 48 

Atcli';e , 48 / 

Atclive I 48 v 

hrtiiO I 48 / 

Atclive I 48 v 

Atclive I 48 / 

Atclive 1 48 

1/ 

Page Tof'Z!J 

GW Comments 

'l5CO..L 

'SOO "'L 

.L. 

/ 

/ 

7 

/ 

/ 

/ 

7 

/ 

/ 

i/ 

7 

/ 

7 

/ 

' , . 

... 

"-.: 

'\. 

\ 
< m 

en 

0 

w 

00 

... 

0 

Sample 10 Code 

M:Lr.t ·11~ I 

118-GIIb 2 

I\IS4-Cl·IIB-Gtab 3 

!Vl:O.t'1.11 8-Gllb 4 

"-roo ·12B.Qab 1 

~· 2&G'Ib2 

tvs..a..I28-GIIb 3 

VS4-Cl·I28-GIIb 4 

jvs4-CL·l J8.Grab I 

VS4-CI. ·138-Grab 2 

VS4.Q.·138-Gnlb 3 

lvS4-Cl·138-Gnl> 4 

jvS4-CL·I48-GIIb 1 

jvS4-Cl·148-Grab 2 

VS4·Cl ·14B-Grab 3 

VS4-Cl·14 9-Grab 4 

Stream 

CNcme~M:I 

CNcme~MI 

atme~M:I 

Ctloc1ne SpiiOOg Mtl 

Cl*xfno ~ ll.ll 

atme~MI 

Cl1larl:le ~ M:f 

atme~Mtl 

Chtome Sp'l$ng Mil 

Clllotlne Splldng Md 

C!Qine~MI 

atme Spldng tAll 

Olloftne Splldng Mil 

Chlorine Splldng Mil 

Chlorine Spll<lng Mil 

Chlorine Spiking MS 

Waste Sa.mple Logbook Poge 25 of 29 

Veolia-Sauget, IL • Unit 4 CPT 

Project Numbe.r 40942510.20 

Fraction Cond Run Date TIII19 TW GW Comments 

AldiYe 1 18 I',B ~ 

hrJiye 1 IS ·~o 

Alrtjye 1 18 l'SI 'J 

AlrJWe 1 18 •"- '" ") 

AI1::IM 1 28 rv'•'1tt ~,, 

MJiNe 1 28 I 1m 

AI1::IM 1 28 l'il7 

tvcme 1 28 ~ 1'5'17 

Archillll 1 38 rc-A l3)' 

Archive 1 38 1'43<. 

Nrfue 1 38 iiWi 

NrJWe I 38 I . 14>'\3 

Ardll"..e 1 48 

Ardlillll 1 49 

Archive 1 48 

AJchi>.., 1 4B 
< 

m 

en 

0 

..... 

~ 

Sample 10 Code 

~B-118-Giab 1 

lvS4-PB-119-Q&b2 

~ .. , "" 118-Giab 3 

118-Giab4 

V~128-Grab 1 

lvS4-1'8-12B-G"ab 2 

~ .... .... 128-Q-ab 3 

12&Giab 4 

\IS4.4'S·IJI!..Grab 1 

~B-13e.Gtab2 

VS4.P8-138-Grab 3 

VS4-f>8.1~4 

lv54-PB-149-Qlll> 1 

VS4-P8-14B-Giab 2 

VS4.PB· 14B·Grab 3 

j\'S4-PB-148-Grab 4 

Stream 

Wd~MI 

lead Sph"og Ml 

Lead spu.g Ml 

Laad Sph"og loa 

Lead Sjtilg .., 

Lead Sjtilg ..., 

Lead Stlldna Mil 

Lead Sjtilg 11.1 

Lead Sjlldng ~ 

Lead Spiklng Ma 

Lead Splkilg MG 

LaadSpi~MII 

Lead Sll«~ Ml1 

Lead Spiking MU 

lead Spiking Mil 

Laad Spllilng Mil 

Waste Sample Logbook Page 26 of29 

Veolia-Sauget, IL - Unit 4 CPT 

Project Number 40942510.20 

Fraction Cond Run Dale Time 1W GW Comments 

An:live 1 18 ~~~,.,, laa{, 

Mtiw 1 18 l"l\(0 

Mtr.e 1 18 1St5 

/~~awe I 16 ~'- 1, 1 

MJWe ' 2B ;o,ol'\', .• ,~ 

AtdWe 1 2a ~ 

Aldivs 1 2B ,,.,7 

Anme 1 28 L.- 7 

NrJiYe I 38 ~ltll ~% 

Archive 1 38 l'Hf> 

Archive 1 38 '"t; AtdlM! I 38 L 

AtdlM! 1 ~ '"~ 

Archive 1 48 

Alchive 1 48 

M:llve 1 49 
Waste Sample Logbook Page 27 of 29 

eo ia~Sau et, ll ~ Unit 4 CPT 

Project Number 40942510.20 

Sample 10 Code Stream Fraction Cond Run Date nme TW GW Comments 

~$4-HG-1 1 e.Grab1 Mercury Spilling Soln MeUis 1 16 .. ,.,,, ~ ! f l\ So\;~t ~~~ -1\~ ~ na· <:mro 

VS4-HG-1 1B-Gtab2 Merary Spiking Soln Metals 1 18 13'40 

VS4-HG-118-Gral>3 t.\era)ry $pkilg Soln Me1als 1 18 If IS" 

~HG-118-Gial4 Menuy Spiking Sdn Mo:ais 1 18 ~ ... ,,,l ~54-HG-128-Giab l Merary Spllng Soln Melals 1 28 "'t;~c ~ l.~sVS4·HG-12B-Giab2 Mercury Spiking Soln Metals 1 28 ~~~~ 

VS4·HG-12B-Go-.b3 Mercury Spii<Wlg Soln MeUis I 28 )'S\7 

~$4-HG-12B-Grab4 Mela.ly SplOOg Soln Mel3s 1 2B ... ,~, 

~HG-IJ8.Grab1 Mercuy Spjl(ing Soln Metas 1 38 Of ,~ 

VS4-HG·I36-Gtab2 Merrury Spiking Soln Metals 1 38 , .. 

~ ~ 

VS4-HG-13B-Grab3 Mercury Splldng Soln Metals 1 38 'biS' 

VS4-HG-138-Giab4 Men:lly Spidng Soln Melals 1 38 . '"eel 

VS4-HG-148-Grab1 Mercury Spll<frlg Soln Mas 1 4B 

VS4-HG-148-Giab2 Memory Spiking Soln Metals 1 4B 

VS4-HG-14B-Grab3 Merc\wy Spiking Soln Metals 1 48 

VS4-HG-14S-G;ab4 Merclly Spiking Soln Meesls 1 46 

l 
Waste Sample Logbook Page 28 of 29 

Veolia-Sauget, IL- Unit 4 CPT 

Project Number 40942510.20 

Sample ID Code Stream Fraction Cond Run Date Time TW GW Comments 

VS+CR-1 18-Grab1 Chromium Spiking Soln Metals 1 18 r"Ju,.J IQ~ 

~S+CR· Hs.GaD2 ammnn Spbg Sc*l Mell!is I 19 ~0 

VS4·CR·1 18-Grnb3 Chromium Spiking Soln Mell!is 1 18 15"15" 

VS4-CR-118-Grab4 Chromilm Spikilg Soln Metals 1 18 • \~!JJ 

~S4-CR-128-Grabl OvaTUn Spiking Sdn Mel3s 1 28 rur.,l. tan 

VS4-CR-12B-Grab2 Chromium Spiking Soln Metals 1 28 ,.j l'r 11 ' 

VS4-CR·128-Giab3 Chronilrn Spikilg Soln Me1a/.s I 28 ~ 1'51\?. 

~S+CR-128-Grab4 Clvcmiml Spiking Soln Metals 1 28 . . m~..-

VS4-CR·13B-Grab1 Cl\romi\Jm Spiking Soln Me1als 1 38 ~19 --.~ ... I'S~ 

~S+CR 13B-Grab2 Chrooil.rn Spiting Soln Metals I 38 1'1 ~, 

~S4-CR·1 38-Grab3 Chroml!m Spo'l<ing Solo Metals 1 38 

'"'~ VS4·CR-138-Grab4 ChromiJm Splkilg Soln Metals 1 38 ,_ ... I f.ct} 

I'S4-CR·1-48-Grab1 Cl1romiiMn Spicing Sc*l Metals I 48 "" / 

VS+CR·148·Grab2 Chromhlm Spiking Soln Metals 1 48 " / 

VS4·CR·14B-Grnb3 Chromium SpiiOOg Soln Melals 1 48 ""' / ~S4-CR 148-Grlb4 Clvomlum Spti1g Soln Metals I 48 " / 

VS4· -,_ 

' / 

VS4- ., 

. v L 

~54- ' / 

VS4- J~ 

VS4· / ~ 

~S+ / ... ~ 

VS+ / '"- ~S+ / ~ 

~54- ./ ... ~ VS+ ---~ 
Bulk Solids Sample Composite Data Sheet 

Project Name Veolla- Sauget, IL Oate \l)l~'t /1} 

Project Number 40942525.2(H)2 Condition No.. 1 

F<>eWity Unlt 4 R:un No 31\ 

Stream Name Bulk Solids (BS) Start Time ()q&(, 

Composite sample 10 \IS4 BS- .COMP ..I:_ Stop Time \IHf. 

Oper.>tor 

Smlple Numbtr Tlmt Volume/Moss Sample Number lime Volume/Mau 

1 cq!.l. 'S \E.~ 21 

2 Oq'J\ 'SO()~ 22 

3 \ OOf. 5"' 1,~ 23 

4 ao-.\ (Clt~ 24 

s \ o'!ll:a ~aGe, 2S 

6 26 

7 27 

8 28 

9 29 

10 30 

11 31 

12 32 

13 33 

14 34 

1S 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volumo/Mass ~%~ts 

Comments: Collect sofids in 1000 ml jar labelod for Ald\lve. Take appropr1at ely-sizod and o.qual aUquots from ead\ Jar to prepare the 

composite sample In a 4 liter jar. Record the volume/mas.s of e ach aliquot used to prepare the composite sample on the data she'll 

Retain the remalnl11g sample In the l OOO ml jars and archive. 

SbS-M SUb-Slnlpk c.,.m. 

-Oatc J.,.Z0/1 

/&t'~c/: JUM 20/J 

E-421 

VESOI3844 
Bulk Solids Sample Composite Data Sheet 

Projecl Nam~ Veolla - S.uge~ ll Date )() 10.,113 

Project Number 40941525.20·02 Condition No. 1 

Facility Unlt4 Run No ~~ 

Stream Name Bulk Solids (BS) Start Time l<l~ I 

Composire Sample ID VS4·BS-1M-COMP j_ Stop Time II S") 

Operator 

Sample Number Tlmo Volume/Mass Sample Number Time Volume/Mass 

1 a~ I ~0~(\ 21 

2 \ \OE. ~~ 22 

3 \\~\ Sl'lao. 23 

4 \I''- 'i\~ 24 

5 \ 1'5 I '50~c; lS 

6 26 

7 27 

8 28 

9 29 

10 30 

11 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volume/Mass ~~':!,\~ 

Comments: CoUe<:t solids In 1000 ml)ar laoolo:d for Archive. Take approprlately·siled and equal aliquots from each jar to prepare the 

composite sample in a 4 Uter jar. Record the volume/mass of eadlaHquot used to prepare the compOSite sample on lhe data sheet. 

Retain tile '""'aining sample in the 1000 ml jars and archive. 

SDS~ Sflb.S ¥k C"""'"'"" 

- o.te: J-Z0/2 

-J-2011 

E-422 

VESOJ3845 
Bulk Solids Sample Composite Data Sheet 

ProjeaName Veollo - ~Uge1. Jl Date 10 li.f/13 

Proje<:t Number 4094252.5.20.02 Condltlon No. 1 

Faclllly Unit 4 Run No ofl 

Stream Name Bulk Solid$ (BS) Start Tlme rnE. 

Composite ~mple 10 VS4..f!S.1Jl. .COM~ Stop Time \'l\5" 

Operator 

Sample Number Tlmo Volume/Mass ~mple Number Time Volume/Mau 

1 \1~ ~I '\ 21 

2 l'?t'5 \ 510 co 22 

3 1~0() ~0~ C\ 23 

4 \If G.\ 5()\t ~ 24 

s l'i\~ ~()\"\ 2S 

6 26 

7 27 

8 28 

9 29 

10 30 

11 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 final Volume/Mass Q,'S-·Cil -

Comments: Collect solids In 1000 ml jar labelitd for Nchlve. Take approprlately.<ized and equal allquots from ead1jar to prepare the 

compo<lte sample In a 4 Uter jar. Record the wlume/mass of ead1allquot used to prepare the composite sample on the data shoel. 

Retain the remaining sample In the 1000 ml jars and archive. 

$()$...()$ Sd> SeiifCI!! C«ffi''U/Ic 

Rovtsioh C.tC' J- MIZ 

R.!M•-.d: Jfll?te Z0/1 

E·423 

VES013846 
Bulk Solids Sample Composite Data Sheet 

Project Name Veolia- S:.uget, ll Date 1() 1~5 13 

Project Number 40942525.2~2 Condition No. 1 

Fad lily Unit 4 Run No 36 

Stream Name Bulk SoHds (BS) Start Time 13'SE. 

Composite Sample 10 VSHIS.11t-eOMPit Stop Time j{,O~ 

Opera !Or 

Sample Numb.,- Time Volume/Mass Sample Number Time Volume/Mass 

1 n~ 3C:l7~ 21 

2 ll'fl ~"G 22 

3 I ~tO<:. ~ll~ 23 

4 I "\ fl.\ ~~~ 24 

5 ll\15'" 30(.9 25 

6 \I{JI ~t)O~ 26 

7 I ~(I() l()() .«<J 27 

8 ,,., l06" 28 

9 \~ fa 907f 29 

10 l'S".f\ ~~, 30 

11 \'(,~ 3:1"7g 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volume/ Mass i,3'ti~ 

Comment£ Coli«t solids In 1000 ml jar labeled for Arcnfve. Take appropriately-sized and equal allquots from eacn jar to prepare the 

composite sample in a 4llter jar. Record the volume/mass of .. th afiquot used to prepare the composite .ample on the data shect 

Retain the remaining sample In the 1000 ml jars and archive. 

SDS-O!J ~te c.,.,-;,. -O.~J-Mli! 

VES013847 
Bulk Solids Sample Composite Data Sheet 

Proje« Name Ve<>!ia - Sauge~ IL Date \() /~'S (I~ 

Project Number 40942525.20.()2 Condition No. 

Facility Unit4 Run No 3& 

Strtam Name eulk Solids (es) Start lime ll" 

Composite S.mple 10 VS4·85-1Jl. -COMP~(. Stop Tlme lb~" 

Operator 

Sample Number Time Volume/Moss Somple Number lime Volume/Mass 

1 13~{. ~()Cq_ 21 

2 ll,.l ~()'\cit 22 

3 I 'l ()(, 300~ 23 

4 I 'till l.OO~ 24 

s ,, .. ~ ~~'\~ 25 

6 1'\H ~()\9 26 

7 'r;o' 'aOI~ 27 

8 \'Si.\ j:X>3 28 

9 I 'Slt ~'\ 29 

10 ,,~, .. ,~ 30 

11 1606 ~l:kJ 31 

12 ,~, ~~s 32 

13 ~~ ~~ 33 

14 34 

15 35 

16 36 . 17 37 

18 38 

19 39 

20 Final Volume/Moss 3.'\~ CI! 

comments: Collect solids In 1000 mljar labellld for Archive. Take appropriately-sized and equal aliquou from each jar to prepare the 

composite sampl•ln a 4 Uter jar. Record the volume/mau of each aliquot used to prepare the composite sample on the data sheet. 

Retain the remirinin& somple in the 1000 ml jars and archive. 

SDS-D!J 5«>-Sc<ttp!. &_.;to 

- 06fa; J- 2012 

R- J-2013 

E·42S 

VES013848 
Containerized Solids Sample Composite Data Sheet 

ProJect Nome Veolla - sauget, IL Date 1:1/~ 511~ 

Project Number 40942S25.2Q-02 Condition No. 1 

Fatllll'/ Unlt4 Run No 3~ 

sueamName Containerize<! Solids (CS) Start Time Oqi!,-

Composite S.mple 10 VS4-CS-13 MP .1_ Stop Time 1 ~'s 

Operator 

Sample Container 10 Time 

Volume/ Sample Container 10 Time Volume/ 

Number Mass Numoor Mass 

1 ~~ I'"'&~ '500_'\ 21 

2 ~d. Qq'{O ~~~ 22 

3 50 I ClO$" ~~ ~ 23 

4 Cl IO<aO 9)~ 24 

s 70 IOt.s- '6~~ 2S 

6 26 

7 27 

8 28 

9 29 

10 30 

11 31 

12 32 

13 33 

14 34 

15 3S 

16 36 

17 37 

18 38 

19 39 

20 Fklol Volume/Mass ol~11c:. 

Comment$! Take approprlately·$l!e<l and equal allquots from each contillner to prepare the composite sample In a 4-llter Jar. 

Reca<d the volume/mass of each aliquot used to prepare the composite sample on the data sheet. 

Collect a representa!M aliquot of the "'malning material in • 500 mljar to oo archived. 

VESO I3849 
Containerized Solids Sample Composite Data Sheet 

Project Name Veolia - Sauget, ll Date \0 ~ s; /13 

Project um~r 40942S2S.:Z0.02 Condition No. 1 

Facility u"lt 4 Run No <tA 

Stream Name conulnerized Solids (CSJ Sl<lrt Time lC~c) 

Composite sample 10 V54.a- .COMP_I Stop Time 1\50 

Operator 

Sample Volume/ Sample COntainer lD Tlme 

Volume/ 

Cont ainer 10 nme Number Mass Numb'er Mass 

1 ?'0 IO'!Q '5'00~ 21 

2 ~~ 110? 5G~~ 22 

3 ~~ ~ 'Stl()_'\ 23 

4 \tl~ \ 1'36"' 1)\'l~ 24 

s \\14 11~0 ~tl 25 

6 - 26 

7 27 

8 28 

9 29 

10 30 

11 31 

12 32 

13 33 

14 34 

1S 35 

16 36 

1J 37 

18 38 

19 39 

20 Final Volume/Moss Cl,{d,)G 

Comments: Take approptlately·sited and equal allquoiS from each conlalner to prepare the composite sample In a 4-Uter jar. 

Re<:Ord the volume/mass of oadt aliquot used lo prepare the composite sample on the data sheet. 

Colloct a representative aliquot ol.tt>e remaining material In a SOO ml jar 10 be archived. 

SD$.Q!15lh-s.mpk C...,.s/fo 

R<.;,ionQ!4'nf"""lOJZ 

1/oW.W<d: ;...., ZOJJ 

VES013850 
Containerized Solids Sample Composite Data Sheet 

Project Name Veolia - Sauget, IL Date to/a.~ /I~ 

Project Number 4094252$.20·02 Condition No. 1 

Facility Unlt4 Run No 38 

Stre!m Name Containerized Solids (CS) Start lime ~~~,. 

Composite Sample 10 VS4-(S..1lt -COMf'iA Stop lime '"asOpmtor 

Sample Volume/ Sample Contalncr 10 Time 

Volume/ 

Container 10 nme Number Mass Number Mass 

1 ~d. ·~~~ 'l('.l)t; 21 

2 '\~ \3'j 0 so~c; 22 

3 \0 I '1()6' I$0C.c:. 23 

4 ~<D 14c).<l 'Sill~ 24 

5 70 l'i~6" ~(1::)~ 25 

6 26 

7 27 

8 28 

9 29 

10 30 

11 31 

12 32 

13 33 

14 34 

IS 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volume/Mass a.~119 

Comments: Take appropriatelv·sltod and equal aliquots from e~ch container to prepare the composite sample In a 4-llter jar. 

Recond the volume/mass of each aliquot used to prepare the composite sample on the data sheet. 

Collect a representative a[(quot of tM remaining material In a SOO ml jar to be archived. 

VES013851 
Containerized Solids Sample Composite Data Sheet 

Proji!CI Name Veolla-saoaet, ll Date 101&.6'/13 

Pro]e<t Number 40942525.2 ~2 Condition No, 1 

Foclllty Unit 4 Run No -a& 

Stream Name Contalnerlud Solids (CS) Start Tune 13'3~ 

Composite SampleiD VS4-CS-1}! <O ~ Stop Time I~S' 

Operat.or 

sampto Container tD Time Volume/ Sample Contolntr ID Time 

Vol.ume/ 

Number Mass Number Man 

1 ~~ lllf li:Rq 21 

2 '\a. \\tO ~'{~ 22 

3 '50 I 'tOt 1100~ 23 

c ~~ '1{)..0 ~1t) 24 

5 70 l'tl6 ~0-' 25 

6 10 1'450 3()(,~ 26 

7 a& '~'" ~qc. 27 

8 <\\ IIJt() '()~ 28 

9 \oq_ ~!i 3\~ 29 

10 1\1\ I 'S"fO a.qo~ 30 

u Ill \E.06' ~ 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 final Volume/Mass '3,3W-c, 

Comments: Take apjl(Opl'iatojy-<lzed and equal allquots from eacll container to prepare tile composite sample In a ._Uter ~r. 

Record tile volome/miS1 of uc:tt aliquot used to prepare tht composite somple on the dota sheet 

Col'.aa representotm af<1uot ol the remolnlnc moter1olln • SOO milo< to be atdlM!dst>S-OS Sd>-samplo C-11• 

ll•vW•n t>t!,.i1f""" 2012 

R.w. ... d: /UM 10/J 

VESOI 3852 
Containerized Solids Sample Composite Data Sheet 

Project Name Veolia -Sauget. IL Date OIU/1~ 

Project Num'* 40942525.20-02 Condition No. l 

Facility Unlt4 RuoNo ~e. 

Stream Name Contalnerlz:ed Solids [CSI Start nme 1~35" 

Composite Sample ID VS4.CHf!.COMP~ Stop r ome 1£.3 ~ 

Operator 

Sample Contaloer 10 r'""' 

Volume/ Sample Contolner 10 11mc 

Volume/ 

Number Mass Number M us 

l -oa... IUS 1ole, 21 

2 ~.ta.. 1~6 "$~(4 22 

3 '5() 1'405' ~ 23 

4 '&fJt~ I 'U-6 ?!O\~ 24 

5 7 () l'i15 l O\q 2S 

6 ?,C) \It 'SCI lO\~ 26 

7 &~ ,~,. ~<teo 27 

8 <\'\ ,,.~() 3~ 2& 

9 ltR l '5~5" 3\ ~ 29 

10 H\ ISSO ~~ 30 

11 1:\.'7 \{,06" ~lq 31 

12 ll7 ~~0 30d~ 32 

u tq) ~~ "l)l '"I 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volumo/Mass ~!{ll>q 

Commeots: Take app<oprlatel~ed and equalaliquots from each container to prepare the composite sample In • 4-Uter )a.r. 

Record the volume/mau of each aliquot used to prej)are the composite sample on t.he data sheet. 

Collect a representative aliquot of the remaining material in a 500 ml jar to be archived. 

5tJS .. M SI.O$'**JtPk eo,.,postt• 

PniHM /Jdr~: JI/IM 2011 

ReW~ IJTit! ZOJ' 

VESOI3853 
Liquid Waste Feed Sample Composite Data Sheet 

Project Name Veolia-sauget, IL Date 10 /.l'i/13 

Project Number 40942525.20-()2 Condition No. 1 

Factrrtv Unit 2 Run No 3A 

Stre.-am Name Low BTU Uquld Waste (UIW) Start Time oq,lr 

Composite Sample 10 VSHSW·l~A COMP L Stop Time 1~'!1~ 

Operata< 

Sample Numbti' Time Volumt/M ... Sample Plumber Time Volume/Miss 

1 0,~~ '5 00 " 1.- 21 

2 0,'\0 22 

3 I OOG" 23 

4 10~ 24 

5 () ~~ . 25 

6 26 

7 27 

8 28 

9 29 

10 30 

11 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volllme & , 'l(lO "'I.. 

Comments: Collect appropria~ed and equal afiquots and tr.lnsfer Immediately Into a 4-Uter composite jar. 

Collect a separate 500 ml bottle of sample at each samplingtlme to be retained in archives. 

Sq "'~ \ed "' ')( -l \ siteQ"" 

$05-115 SdJ..S.,.,S. · P•-• t>m: J.,.. ZQ/2 

llc-.J: Juno ZQIJ 

E-431 

VES013854 
Liquid Waste Feed Sample Composite Data Sheet 

ProjeaName Veolla - Sa1J8et, IL Date I() r ~~ 113 

Project Number 40942525.20.02 condition No. I 

Fac ~tv Unit 2 Run No 'iA. 

Stream Name low BTU Liquid Waste (LBW) Start Time IOSO 

Composite Sample 10 VS3·LBW·@ <OMP j_ Stop Time 1150 

Ope<ator 

Sample Number Time Volume/Mass Sample Humber T1me Volumo/lmss 

1 10 ~0 'iO() " \... 21 

2 \ \0~ 22 

3 \ ta,.O 23 

4 1\35' 24 

5 \150 1- 2S 

6 26 

7 27 

8 28 

9 29 

10 30 

11 31 

12 32 

13 33 

14 34 

15 35 

16 35 

17 37 

18 38 

19 39 

20 Final Volume a..~oo "'L 

Comments: Collect appropriatelv·sil ed and equal allquots and transfer Immediately Into a 4-Uter composite jar. 

COllect a separate soo ml bottle of sample at each sampling lime to be retained in archives • 

.lQ r-.p\t>d tolo'l i--\) 'b \r l'lllr\ 

5DS-06 Sub~ Canpcsite 

R.WI IOII O.t<: J""' 2012 

, ..,.,.., J- 2013 

VES013855 
Liquid Waste Feed Sample Composite Data Sheet 

Project Name veolla-Sauget, IL Date 10la..'O 113 

PrOject Number 40942S2 20~2 Condition No. 1 

Facinty Unit2 Run No ~P> 

Stream Name Low BTU Uquid Waste (LBW) Start Time 13"&5' 

Composite Sample 10 VSHBW·l'U COM~ Stop Time l't~6' 

Operator 

s-pleNumlw Tlme Volume/Ma5$ sample Number Tlme Volume/Mass 

1 113f '500 1'\\.. 21 

2 \~'lO 22 

3 l't() ~ 23 

4 1'\lO 24 

5 '"'3~ ..... 25 

6 26 

7 27 

8 28 

9 29 

10 30 

11 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volume a,~oo ... ~... 

Comments: Collect appropriately-sized and equalaliquot.s and transfer Immediately Into a 4· liter composite jar. 

Collect a separate 500 ml bottle of sample at each sampling time to be retained in archives. 

<..o\lecW ~otn ;.-1\ ~"' 

Sf>S.()$ Sub-Somplo Composite 

R~vlsicm t>Dta: JUM 201.1 

Reviewet/: June 2013 

E-433 

VES013856 
Liquid Waste Feed Sample Composite Data Sheet 

Projec.t Name Veolia - sauget,ll Date 10/tl!i/13 

Project Number 40942525.2G-02 ond~ oo No. 1 

Fadllty Unlt2 Run No 39 

Stream Name low BTU Uquld Waste (LBW) Start Time IllS' 

Composite Samplo iO VSH.BW·1ia-coMI'i.l Stop 11me I~CI-s' 

Operator 

Sample Number Time Volume/Mass sample Number T1me Volume/M•ss 

1 13~S"' <; ()~ "'l. 21 

2 ll~ 22 

3 lit Of 23 

4 \ltlO 24 

5 1'4~~ 25 

6 I '4~ 26 

7 ~~ 27 

8 , no 28 

9 \'U6 29 

10 1no 30 

1J 1{.0f .._ 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 FlnaiVolurM 3 300 1"\L 

Com,.,.,nts: Collect appropriately-sited and equalaliquots and tr~nsfer Immediately into a 4·Uter composite jar. 

Collect a separate 500 ml bottle of sample at each sampling time to be retained in archives. 

&n"" D \ed. ~"' ¥~\\ ~\r-eq,.... 

5DS.(/6~1<C-IO 

l&t'isionl>ate: JUM 2011 

lhodew<tr. , ... 20JJ 

E-434 

VES013857 
Liquid Waste Feed Sample Composite Data Sheet 

Project Name veolia - sauget, IL Date !o l&'S/13 

Proje<:t Number 4094252S.2o-()2 Condition No. 1 

facility Unit 2 Run No 36 

Stream Name Low BTU Uquid Waste (LBW) Start Time r~~5' 

COmpoSite Sample 10 VSHBW COMP•<. Stop Time ~lS" 

Operator 

Sample Number Time Volume/Mass Sample Number Time Volume/Mass 

1 111') '!)()~ "'\... 21 

2 \~'l6 \ 22 

3 11(0'; 2J 

4 \"'oo 24 

5 I 'tl~ 25 

6 1'\C)O 26 

7 t'$'0,. 27 

8 \ "60 28 

9 IUS" 29 

10 "w 30 

11 I tiC)~ 31 

12 1£.6.0 32 

13 lf>U - 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volume a. "oo ,..,L, 

Co""'""'ts: Collect appropriately-sized and equal allquots and transfer immediately into a 4·Liter composite jar. 

Collect a separate 500 ml botUe of sample at each sampling time to be retained In archives. 

~ ... t:.\ed. ~~l'f\ ~~t\ ~\tt<tl'\ 

5D5·0il Svb·Sompl< C«npMite 

Revision !Xtfc: June 2012 

R.-,f, JUfiB20/J 

E-435 

VES013858 
Liquid Waste Feed Sample Composite Data Sheet 

Project Name Veollil - sauae~ ll Date 101&.15 / 13 

Project Number 40942525.20.02 co.Mition No. 1 

f acHity unlt4 Run 111 0 ~~ 

Stream Name High BTU Liquid Waste (HBW) Start Time 01\ ~' 

COmposite sample 10 VS3-HBW-1!t,<OMP_\_ Stop Time I 0~~ 

Operator 

Semple Number Time Volume/Moss Sample Number nme Volume/Mass 

1 OfU'- <; () C) "' L. 21 

l 0,~, 22 

3 I~ 23 

4 to~\ 24 

5 \ 0?.4 25 

6 26 

7 27 

8 28 

9 29 

10 30 

11 31 

12 32 

13 33 

u 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volume a. ,TO() eo.\..-

tomnMnts: COllect appropriately-sized anll equal allquots and transfer immediately into a 4-Uter composite )ar. 

Collect a separate soo ml bottle of sample at each sampling time to be retained in archives. 

Sqh\owd ~()"" "'1--l ~ s ~~ 

S()$.4165~~~~· 

f«,y(tfon """'' JWI< <012 

ltevl•'""" J,_.,. 2013 

E-436 

VES013859 
Liquid Waste Feed Sample Composite Data Sheet 

Project Name v eolla - •ue ~ ll Date lCIIU/13 

Proje(t Number 40942525.20-42 Condition No. I 

Facility Unlt4 Run No 

"'~ Stream Name High BTU liquid Wosto (HBW) Stort Time 10~ I 

Composite Sample ID VS3-HOW·l.!iA.COMP ...\_ Stop Time 1\~) 

Operator 

sample Number nme Volume/Mass Sample Number Tim• volume/Mass 

1 \0'! I ~QC) ML 21 

2 \\()~ 22 

3 l t•' 23 

4 \\~ 24 

5 \ I 'i I .. 25 

6 26 

7 27 

8 28 

9 29 

10 30 

11 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volume ~~001'1\... 

Comments: Collect apprepriately•sized and equal allquots and transfer immediately into a L~er compoSite )ar. 

Collect • separate soo ml bottle of sample at eadl sam pUna Ume to be retained in archives. 

SQ "'~ \fld fi'Qw-, M~ <r.h~WI 

Sl>S ~ Svi>-Sompt. t:.mpcsile 

Rcvis>oo o.t.: Jllfl< i!0/2 

1/evi<wt:d: J..,. i!0/3 

E-437 

VES013860 
Liquid Waste Feed Sample Composite Data Sheet 

Project Name Veolla -Sauget, ll Date ll:l la.StlJ 

Project Number 40942525.20·02 Condition No. 1 

Facility Unit4 Run No ~s 

Stream Name High STU liquid Waste (HBW) Start rrne 11)t 

Composite sample ID VS3+18W-lA. <OMPi! Stop Tome 1~3S" 

Operator 

SampiR Number Time Volume/Mass Sample Number Tlme Volume/Mass 

1 11'3' 1500 fill 21 

2 l'~'il 22 

3 ll{()(. 23 

4 14~\ 24 

5 \'tl5 -~ 25 

6 26 

7 27 

8 28 

9 Z9 

10 30 

lJ 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 FlnoiVolume Q.,'$'00 ,..L 

comments; Collect appropr1atelv·slzed and equal aliquots and transfer Immediately Into a 4-llter composite jar. 

Collect a separate 500 ml bottle of sample at each sampling time to be retained In archives. 

~ ... ~\~ ~ 'J.-Ia. ~\f{lt)W\ 

51>5-05 SobScntp/< ~1'tc 

1/eYisitx; Cot.: J,_ to/2 

R~viewed: June 10/.J 

E-438 

VES013861 
Liquid Waste Feed Sample Composite Data Sheet 

Project Name Veolla - Sauget, ll Date I() ll!i/13 

Project Number 40942525.21).(12 Condition No. 1 

Facility Unh 4 Run No oB 

St.ream Name Hi8h BTU Liquid Waste (HBW) Start Time tnt 

Composite SampieiD VS3·HBW·l ll: COMPai Stop Time 1 ta & 

Operator 

Sample Numbt< Time Volume/Mass Sample Number nme Volume/Mass 

1 Ill ~ "i~ ,..\... 21 

2 \~S I 22 

3 '"~ 23 

4 ~~~ 24 

5 \'ilS 2S 

6 \'t\1 26 

7 I,G~ 27 

8 \UI 28 

9 I 6")4 29 

10 I'S ~I 30 

11 ~~~ ~ ... 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volume 3 • '300 """ 

Comments: Collect appropriately-sized and equal aliquot> and transfer Immediately into a 4-ll\er composite jar. 

Collect a separate SOD ml bottle of sample at each sampling time to be ret<~ln ed in an:hives. 

Socllf\p\~d ~~Of'\ ~-t ~ ~htql"\ 

SlJ.$4 St.b-$1% ¥ ClJtytrdte 

.rsrwoC.rw: J.,.zorz 

11<-J.,..zo/J 

E~39 

VES013862 
Liquid Waste Feed Sample Composite Data Sheet 

Project Name Veotia- sauget, IL oate 1 () 1 tl..S 113 

Project Number 40942525.20-{)2 Condkion No. 1 

Facility Unl14 Run No 36 

Stream Nome High BTU liquid Wute (HBW) Start Time lSl' 

CornpoM!e Sample ID VS3-HBW·l }).-coMpff, Stop Time \ f:,~(. 

OP*rator 

Sample Number Time Volume/Mass Sample Number Tlmo Volume/Mass 

1 l~lf. 'i () 0 "' L 21 

2 ll.,l 22 

3 

·~~ 23 

4 14~1 24 

5 11.\l~ I 

l 2S 

6 II{ 'Sf 26 

7 \,0, 27 

8 , ... ~, 28 

9 ) '$~" 29 

1D l'fS\ 30 

u ~~~ 31 

12 \.HI 32 

13 1{,3~ ... 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volume i ,(,00 .1>1\. 

Comments: Collect opproP<Ialely-sized and equal aliquots and transfer Immediately into • 4.Uter composite jar. 

Collect a separate 500 mt bottle or sample at each sampling time to be retained in ard1ivcs. 

Slcl~\ed ~"' 'f-·1~ $~~1(\ 

.505·05 .5/Jb.Scfopt. ~If• 

Re'lishn D4te.· Jur.c 2012 

Rn'ie~Wd: J~ ZOJJ 

E-440 

VESOL3863 
Liquid Waste Feed Sample Composite Data Sheet 

Project Name Veoll> - Sauge~ ll Date I() J~Ij /\3 

Project Number 40942525.20.02 Condition No. 1 

Facility Unlt4 Run No 31\ 

Stream Name Liquid Waste Feed (LWFI Start 11me Mn 

Composite Sample 10 VS4-LWF-J .COMP _L Stop lime IO'll) 

Operator 

Sample Number nme Volume/Mass Sample Number Time VokJme/Mass 

1 Olt37 'I()() Ml.. 21 

2 oq~t~ I 22 

3 1()(>., 23 

4 \0 .. 24 

5 0~7 25 

6 26 

7 27 

8 28 

9 29 

JO 30 

11 31 

12 32 

13 33 

lA 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Flnal Volume &,too .. ~.. 

Com menu: CoYect appropriately-sized and equal allquots and transfer Immediately Into a 4-l.ller composite jar. 

Collec:la separate 500 ml bottle of sample at each umpf111g lime to be retained in archives. 

~..,p\fd ~IV\ ~.q.~ .1. 

SDS·~ SU....S...,Ie c_.;rc 

lie-(Jotrl: JUM ZO/l 

~d:JUM20fJ 

E·441 

VESOI 3864 
Liquid Waste Feed Sample Composite Data Sheet 

Project Name Veolla - Saugel, ll Date I~ I ~~/13 

Project Nvmber 40942525.20-<12 Condition No. 1 

Facility Unit4 Run No 

Srrnm Name Uqutd Waste Feed (lWI') Start nme 16~ "'"' 

Composit e Sample ID VS4·lWf·1j! ·COMP j_ Stop Tlme 11'5~ 

()pe<ator 

Sample Number Time Volume/Mass Sample Num~r Time Volume/Man 

1 \()~ 'i ()() "'\.. 21 

2 \\(I) 22 

3 Ha.d- 23 

~ \\~J 24 

5 \I ~d.. 25 

6 26 

7 27 

8 28 

9 29 

10 30 

ll 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Anal Volume Q,~OOI'\L. 

Comment.s: Collect appropriately-<lzed and equal aliquots and transfer Immediately Into a 4-litl!f composite jar. 

Collect a separate 500 ml bottle of "mp!e at eadl sampfin& lime to be retained in archives. 

~ .... plt\'1 trOll\ 1. ~ lii~(JI\\ . 

stJS·OIJ ~ c""""";'• - o. .. : J-.1'012 

--.q,J..,.ZOJJ 

E-442 

VES013865 
Liquid Waste Feed Sample Composite Data Sheet 

Projeet Name Veolia - Sauget,ll Date 101 ... ~113 

Projcet Number 40942525.20-02 Cohditlon No. 1 

facility Unit 4 Run No ~& 

Stream Name liquid Waste F..ed (LWF) scart 11me \'3'31 

COmposit e Sample 10 VS4·LWF-lll< oMI'lll Stop 11me \~l~ 

Operator 

Sample Number Time VolurM/Mass Sample Numlar Time Volume/Mass 

1 ~?137 , oa "'\... 21 

2 a~ 22 

3 \1\0) 23 

4 

'"~ 24 

5 'l~ ..... 25 

6 26 

7 27 

8 28 

9 29 

10 30 

11 31 

12 32 

13 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

2D f"...al Volumo a. t 00 "''--

Comments: Colie<t appropriately-sized and equal allquots and transfer Immediately Into a 4·llter composite jar. 

Collect a separate SOD mi bottle of sample at e ach samplins time to be retained in archives. 

'i>~~\~ ~ 1--~ ftQW\ 

$()$.()5~~silo 

ReWsiDI! Dol•: JUtW 2012 

R..,._ J.,..zo/1 

E·«·J 

VES013866 
Liquid Waste Feed Sample Composite Data Sheet 

Project Name Veolla sauge~ IL Date 1 ol~~/l~ 

Proj<ct Number 40942525.20-C2 Conditlon No. 1 

Facility Unit4 Run No ?»& 

SirnmName Uquld Waste Feed (lWF) Start nme l3l1 

Composite Sample 10 VS4·LWF·13._ ..COM~ Stop Time 1~7 

Op•rator 

Sample Number nme Volume/Mass Somple Number nme Volume/Mass 

1 1\~7 SSQ() "'\.. 21 

2 ~~osa. 22 

3 1'\0J 23 

4 

'"~ 24 

5 \l~ 25 

6 ~'t~~ 26 

7 \li<n 27 

8 1$» 23 

9 I'H) 29 

10 ·~56 30 

11 \f:.O) _ .. 31 

12 32 

13 33 

14 34 

1S 35 

16 36 

17 37 

18 38 

19 39 

20 . Final Volume 1)00 "'L 

Comments: Collect appropriately-sized and equal r~quots and transfer Immediately Into a 4-Uier composite jar. 

Collect a separate 500 ml bottle of sample at each sampling time to be retained in archives. 

s,qlt\~ ~ E-tt ... "t-~ 5h~fC'I 

SDS-05 Sub-.$<Nlopk CINI!P"slte 

Rt1isitM (Jote: June 2012 

-J-:t013 

E·444 

VES013867 
Liquid Waste Feed Sample Composite Data Sheet 

Project Name Veolla-Sauget, ll Date l()fa.'i" 113 

Project Number 40942525.20-02 Condition No. 1 

Facility Unlt4 Run No ~8 

Stream Name Uquid Waste Feed (LWFI Stan Time l\a7 

Composite Sample ID VS4·lWF-t:Sl -coMP~ Stop Time 1~7 

Operator 

Sample Number Ttma Volume/MIS$ Sample Number Timt Volume/MIS$ 

1 \'lJ ')<X) "'\.. 21 

2 11~~ 22 

3 \ItO) 23 

4 1'\~~ 24 

s I'll~ 2S 

6 ·~a. 26 

7 \tO) 27 

8 1'1~ 28 

9 \~~7 29 

10 lit~ 30 

11 ,,0, 31 

1.2 l~n 32 

13 l(,l' - 33 

14 34 

15 35 

16 36 

17 37 

18 38 

19 39 

20 Final Volume ~ ,\.00 11\\. 

Comments: Collect appropriately-sited and equalallquots and tr.msfer Immediately Into a 4·Uter composite jar. 

Colle<;! a separote 500 ml bottle of sample at eacfl sampling time to be retained in archives. 

~""1)\~u tto~ j.-?.6. $~1et1ft\ 

SD5·05 Sui>~ID C"""""'re 

flnilitM tJott.• JUM 20tz 

R•vf~d: JUM ZOlJ 

1>-4<15 

VESOI3868 
m 

~ .. 

Pro]~ Name ycol!a- sauss;t. !l/ Unit 4 cpr 

Project Numb Of 40942525.2().()2 

Solution Preparation Log 

SOllltlon Oltt,.,- ~ .... Ill -.I No. 

rl-!~aa. tofu.lt3 .\"t.c ~0 1 

lbl~ z• 

"~ z.. 

, .. ,.~ >OI,ul ~ \\IIU~O I 

~- " .. 

lo 12UIJ \ O"f 0 It, <!Po( •ell<... <\\.~0, 

~ I'L._ 

•61nl~ IO'o~<":,o~ tb\1L 1\Cfo~otO'l VJ.l,/1. 12.* 

ljr,_ ~i' 0-c lof,.\t~ •'>·U-z.~ to~ 

~__ol ft. .. 

IO'o~~ I0~\1!> "'tL~ ~ 

~"ll ... ~.. .... 

• 

~---

E><llhtlon Date 11 30 d"YYIfter "'-""" -"" addle poi3<Wm _ _..,~-..Oiircln ldJtr, 

._ .._ a.-A 2. CZ....'f"'\-'--'l 

•• ~ IM•\- ~ R,.7..t'-Oj 

Mass O< o.w• YolutM 

"l 

50 II \n\•1, 

?.3~ 

'\00 1\\12-1" loo 

Sbo 

~ .... to t!ll~ 

-soo 

"lo'\ tOft'\\t'.. 

Soo 

z..o, lo(rs/ro, 

ctoo 

l oo 11\l>\\1..., 

I 

-

td-l~ 

~"' 

\011'< ... 

~ 

~ 

~ 

oat• I o/ J.J.(, !> 

Pose _1 _ of .i!!(_ 

Redpu t o Make 1 Uter 

Sulfuric~ 

Permanpn.1t• 

IOOmiWam 

100 m1 Corcentnttd H).so .. 

Ollua !D 1 L ...aume 

oiOcKMnO, 

Nitti< Add/Hydrosen 

l'trooddt 

SOOmiWeter 

50 ml conetntratod KNO, 

'33lmllO!IH,o, 

onut.t to ll volume 

0.1 N NlulcAdd 

900mlwater 

G.! ml Conuntratod KNO, 

01tu1e to ll VO:ume 

8N Hydrod110<ic Acid 

250mlwa .. r 690 ml Concentrated HO 

DUuu to ll volume 

~-oh:-_,_,_'-"9 

R.vMo!IDtzl ... • J..-yl0/3 
Project Name yeqtla - Sauget. IL I Unit 4 CPT 

Project Number 4Q942S25.2!H12 

hf Rtaaent No. 

\ Htt.<: ~o 

l- ~0,_ 

3 II. . \ 

-{ tfV(.c_ 11,_0_ 

~ A-.:..\..o~ 

" l.vl't 

Reagent Use Log 

Manufacturer 1 l ot Number 

? '-'~~ -wt4L<-

'3T6 Yt11S 

t--\6£. ., ... ~.,t, 

? Cl~~lo>IHLC. 

~(. S"tc..t8 

Mtv ?.I "~':fDate Optned bplm;on Date 1 

to\U.h!> tolz;t.l N 

rolu.lr3 /O(U/1~ 

... (2~\ r!o Jofz:~l •I(, 

ro 1 'ZJ(( ~ ro r vtt•'t 

to I t.oslt~ t•l 1..s It'( 

(o /1.~ II'!> t<>f~{ I~ 

Date toll~( r~ 

Pilge ...L_ oi a:_ 

lnitialt 

j:Vfu 

(~"' 

~ 

";::.MJ611. 

~ 

\C.cW\ 

'ms GOdt m~ be used: ITB •J.T. B.alcer, Mal • Ma£1W!d:toct1:; A c.Ad'~Jntor; P • Phannc.a, v = VW'R. f = Alhtr, Mat= Mwon 

2 E~ rat n Oate Is 11 prOVIded by manvfacturer or 12 monlhs aft6r openin&. F0$ .. 029 RtMgu/f lise L119 

R«-llisiM Dots: jt.fiiJIY'Y 20/J