# Exhaust Emissions Sampling DaI-Italia, LLC., Muskogee, OK Spray Dryer, Kiln Scrubber, and Trim Kiln Exhausts

April 11 - 13, 2006 - AYmstr^ong En>>ironmental, 17zc. Project W-2496-06

Report Prepared For: Bob Hurt ' Daltile 7834 C. F. Hawn Freeway Dallas, TX 75217

Report Prepared April 18, 2006 By: 

# Arr7zstrong Envir•onnaental, Inc. 7715 Sovereign Row Dallas, Texas 75247 (214) 631-0021

# TABLE 4F CaNTENTS P age

T. Introduction 1 II. Summary 2-7

III. Procedures 8

- 

# 14

IV. Appendices

A. Calculation Summaries 15

- 

# 31

B. Confiinuous Elnissions Monitor Summaries 32

- 

# 124

C. GCIFID Chromatogram Summaries 125

- 

# 155

D. Analytical Summarnies 156

- 

# 238

E. Field Data Sheets 239

- 

# 259

F. Equipment CaliUrations 260

- 

# 278

G. Standard Gas Certifications 279

- 

# 290

H. S02 Interference 291

- 

# 307

### SUMMARY OF EMISSIONS TEST DATA

Table : 3 Plant : Dal•Italia, Muskogee, OK Location : Kiln Scrubber Exhaust Operator : R. Taylor, G. Salinas, T. Armstrong Test Date : 12•Apr•06 Repetition : 1 1 2 2 3 3


### STACK GAS Temperature, F 137.9 137.7 137.5 137.9 138.1 137.9 Velocity, fps 30.35 29.40 29.95 29.64 27.36 29.01 Volume Ftow, acfm 35167.5 34063.3 34699.0 34343.9 31702.9 33610.8

scfm 23444.6 23352.0 24398.0 24452.2 21705.2 22998.2 

### scfh 1406674 1401122 1463881 1467129 1302311 1379892 Moisture, 0

/ 0 23.92%, 21.78% 19.80% 18.74% 21.84% 21.91% CO2, % 3.50 3.50 3.00 3.00 3.50 3.50 02, % 17.50 17.50 18.00 18.00 17.50 17.50

SAMPLE Start Time, hrs:min 10:20 AM 10:20 AM 12:20 PM 12:20 PM 1:55 PM 1:55 PM Finish Time, hrs:min 11:23 AM 11:23 AM 1:23 PM 1:23 PM 2:58 PM 2:58 PM Sample Volume, scf 37.779 36.649 38.373 37.122 35.414 37.998 Isokinetic Ratio, % 99.19634 95.19177 96.81835 92.0814 100.4374 100.2116

PARTICULATE 

## c=:.. 

## Front Ha

~ 

### Sample Weight, mg 108.89 94.99 78.21 Concentration, gr/sct 0.044474 0.038196 0.034076 Emissions, Ibs/hr 8.940003 7.990267 6.341765

Back Half Sample Weight, mg 11.40 13.20 7.75 Concentration, gr/scf 0.004656 0.005308 0.003377 Emissions, Ibs/hr 0.935954 1.110344 0.628419
Total Particulate, Ibs/hr 9.875957 9.100611 6.970185

CARBON MONOXIDE Concentration, ppm 162.89 155.58 147.09 Emissions. Ibs/hr 16.65558 16.59182 1475357

NITROGEN OXIDE AS NO2 Concentration, ppm 30.76 32.45 33.52 Emissions, Ibs/hr 5.167154 5.685317 5.523581

SULFUR DIOXIDE Concentration, ppm 1.03 0.0054 0.48 Emissions, Ibs/hr 0.240727 0.001316 0110047

VOC AS C3H8 Concentration as CH4. ppm WET 13.92 12.80 14.61 Concentration, as CH4, ppm DRY 18.29571 15.75224 18.70928 Emissions as CH4, Ibs/hr 1.068997 0.959941 1.072349 Emissions as Carbon, Ibs/hr 0.801748 0.719955 0.804261 Emissions as C3H8, Ibs/hr 0.979914 0.879946 0.982986


## HYDROGEN FLUORIDE Sample Weight, mg 0.00 0.24 0.46 Concentration, ppm 0 0.274562 0.514124 Emissions, Ibs/hr 0 0.218559 0.384922


## CHLORINE Sample Weight, mg 0.00 0.00 0.00 Concentration, ppm 0 0 0 Emissions, Ibs/hr 0 0 0

HYDROGEN CHLORIDE Sample Weight, mg 0.00 0.34 0.37 Concentration, ppm 0 0.21313 0.226594 Emissions, Ibs/hr 0 • 0.029629 .0029628

1-i

### 23.4 23.31 .419906 1.413232

61.96 61.86 5.23091 5.217991

48.86 49.08 2.90319 52.63397 .116575 1.10994 

## 837431 0.832455 023527 1.017445

92.01 89.64 72.51438 72.70912 1 : 887641 1.843671

0.41 0.52 0.091688 0.118584 0.008482 0.010675

118.21 108.68 51.0482 48.30297 2.427719 2.235277 SUMMARY OF EMISSIONS TEST DATA 

### T able . Q Plant : Da!•Italia, Muskogee, OK Location : Trim Kiln Exhaust Operator : R. Taylor, G. Salinas. T. Armstrong Test Date : 13•Apr•06 Repetition 1 1 2 2
STACK GAS 

### Temperature. F 456.3 456.6 461.2 Q61.4 Velocity. fps 80.08 80.79 82.15 80.56 Volume Flow, acfm 15730.0 15869.1 16137.2 15824.8

scfm 8309.7 8422.5 8468.8 8364.9 

## scfh 498579 505351 508127 501893 Moisture, % 7.51% 7.06% 7.64% 6.95% CO2, % 3.00 3.00 3.00 3.00 02, % 18.00 18.00 18.00 18.00


### SAMPLE Start Time, hrs:min 9:20 AM 9:20 AM 10:50 AM 10:50 AM 

### Finish Time, hrs:min 10:23 AM 10:23 AM 12:02 PM 12:02 PM Sample Volume, scf 53.237 53,388 53.924 53.886 Isokinetic Ratio, % 103.6873 102.92 103.0525 104.595


### PARTICULATE Front I ~~ 

### mpl ae Weight, mg 47.34 33.71 Concentration, gr/scf 0.013721 0.009646 

### Emissions, Ibs/hr 0.977598 0.700419
6ack Half 

## 3 3

462.7 

### 462.6 81.43 78.41 15995.4 15402.8 8461.5 8139.5 

## 507691 488372 6.75% 6.8696 3.00 3.00 18.00 18.00

12:15 PM 12:15 PM 1:17 PM 1:17 PM 53.173 52.357 101.7038 104.4415

24.79 0.007194 0.521911

Sample Weight, mg 20.20 Concentration, gr/scf 0.005855 0 Emissions, Ibslhr 0.417142 0
Total Particulate, lbs/hr 1.39474 1


### CARBON MONOXIDE Concentration, ppm 100.66 Emissions, Ibs/hr 3.697618 3 

### 18.05 13.70 .005165 0.003976 .375039 0.28843
.075458 0.81034



## 99.81 97.54 .686532 3.5996


### NITROGEN OX1DE AS NO2 Concentration, ppm 23.84 Emissions, Ibs/hr 1.438703 1


### SULFUR D10XIDE Concentration, ppm 62.07 Emissions. lbs/hr 5.211573

VOC AS C31i8 Concentration as CH4, ppm WET 49.88 Concentration, as CH4, ppm DRY 53.66641 5 Emissions as CH4, Ibs/hr 1.126496 1 

### Emissions as Carbon, Ibs/hr 0.844872 0 Emissions as C31-18, Ibs/hr 1.032621 1


### HYDROGEN FLUORIDE Sample Weight, mg 86.71 Concentration, ppm 68.97436 Emissions, Ibs/hr 1.80977,C


### CHLORINE Sample Weight, mg 0.51 Concentration, ppm 0.114053 Emissior+.s, Ebs/hr 0.010624


### HYDROGEN CHLORIDE Sample Weight, mg 113.72 Concentration, ppm 49.56698 

### Emissions, ibs/hr 2.373518

7

# III. PROCEDURES

The procedure for emissions sampling followed USEPA test methods as detailed in Title 40: Code of Federal Regulations. The following methods were used:

Method Title 

# 1 Sample and Velocity Traverses for Stationary Sources

2 Determination of Stack Gas Velocity and Volumetric Flow Rate (Type S

Pitot Tube)

3 Gas Analysis for the Determination of Dry Molecular Weight

5 Detennination of Particulate Emissions from Stationary Sources

6C Determination of Sulfur Dioxide Emissions from Stationary Sources

(Instrumental Analyzer Procedure)

7E Determination of Nitrogen Oxides Emissions from Stationary Sources

(Instrumental Analyzer Procedure)

10 Detennination of Carbon Monoxide Emissions from Stationary Sources

18 Measurement of Gaseous Organic Compound Emissions by Gas

Chromatography

25A Determination of Total Gaseous Organic Concentration using a Flame

Ionization Analyzer

26A Determination of Hydrogen Halides and Halogens Emissions from

Stationary Sources

202 Determination of Condensible Particulate Emissions from Stationary

Sources 02 and CO2 were determined using FyRite Analyzers. PM, HF, and HC1 sampling was perfonned on each source as follows:

Source Number of Traverse Points M nuteslPoint Spray Dryer 24 2•5 Kiln Scrubber 20 3.0 Trim Kiln 12 5•0 

# The PM sampling train was configured as follows:

:

# Glass or Stainless Steel sample nozzle Heated Glass Lined probe Heated Glass Fiber Filter (teflon filter for the Trim Kiln) Impinger #1 - 100 mis H20 Impinger #2 - 100 mis H20 Impinger #3 - 100 mis H20 Impinger #4 - Empty Impinger #5 - 200 grams Silica Gel The probe and prefilter glassware was rinsed with acetone. The irnpingers solutions were recovered and' rinsed with H20 and MeCI. The impinger solution was extracted with the MeCI rinse. All solutions were evaporated in tared glass beakers, with the exception of the impinger solution from the Trim Kiln, which was evaporated in Teflon beakers. The HF/HC1/C12 sampling train was configured as follows: Glass Salnpling Nozzle Heated Glass Lined Probe Heated teflon filter Impinger #1 - 100 mis 0.1 N H2SO4 Inlpinger #2 - 100 mis 0.1 N H2SO4 Impinger #3 - 100 mis 0.1 N NaOH Impinger 94 - 100 mis 0.1 N NaOH Impinger #5 - 200 grams silica Gel HF and HCl analysis was performed on the solution from the 1 st and 2nd impinger. Chlorine analysis was performed the solution from the 3rd and 4th impingers. Analysis was performed using a Dionex LC20 IC/HPLC. Calibrations standards were blended frorn a 1002 mg/Lt certified Chloride standard and a 1011 mg/Lt certified Fluoride standard. Continuous monitoring was performed as follows:



# Source Com onent Monitor Ran e 

# Standards Spay Dryer CO Fuji 3300 0- 100 ppm 49.9ppm, 99.1ppm CO in N2 EPA Protocol 1 

# Trim Kiln, Kiln CO Fuji 3300 0- 500 200ppm, 494ppm, CO 

# Scrubber in N2 EPA Protocol 1 Spray Dryer, Ki1n 

# NOx EcoPhysics 70s 0-60 ppm 25.5ppm, 51 ppm NOx 'I'rim Scrubber, Kiltt in N2 EPA Protocol 1 

# Spray Dryer, Kiln S02 Western Research 0- 100 49 

## • 8 PPm, 100 ppm S02 

# Sci

- ubber 721-AT in N2 EPA Protocol 1 

# Trinl Kiln S02 Western Research 0- 250 140ppm, 250pprn S02 721-AT in N2 Epa Protocol 1 Spray Dryer, Kiln 

# vOC TECO 51 0- 70 19.9ppm, 40.8ppm, Scrubbcr, l'rim Kiln 61.7ppm CI44 in N2 EPA Protocol I



# 9

# Methane vvas detem

- iined. using a Carle 100 GCIFID calibrated witti the abave CH4

starndards. San

- lples were talcen via a peristaltic punlp -and integrated gas bags.

10

# Figure I - Spray Dryer Baghouse Exhaust

roor

I"

mmi

—~

~ 

### 'Ra ck Diemter - 71 inches Poiryl #1 - 1.5 inclhes Point #2 - 4.75 inches Poinl 93 - 8.4 inches f'oint #4 -12.6 inches Point #5 -17.75 iiiclies 

## Poird #6 - 25 ? inches Point #7 - 45.7 inchQs Point #8 - 53.25 incftes 

## F'oirtt #9 - Sa.4 inches Poinl #10 - 62.6 inches 

## Point #11 - 66.25 inches Point #12 - 69.5 inches

# I'igure 2 - Kiln Scrubber

~ 

# xhaust

Sfact: Liameter - 59.5 inches Paint #1 -1.5 inclies 

## Pnint #2 - 4 .9 inches Point #3 - 81 incltes Pt7iflt #il - 13A irt c}Zes Poitit #5 - 203 inches Paint #6 - 39.1 inches Pain! #7 - 46.1 inches Paint #8 - 50.8 inches PoiM #9 - 54.6 inclins Point #10 - 5g inches ~ 

### -j N

# Figure } - Trim Kiln Exhaust

aoil

'i 80"

~ 

# w Stack Diarneter - 24.5 inches Point #i - 1.1 inches 

## Poini #2 - 3.6 inches Point #3 - 7.25 inclZes Poird #4 -1725 inches 

## Poird #5 - 20.91nches Point #6 - 23.9 inches

# Fi gLlro 4- CEt , .,l Confi gurati on

lnstaLl: Fifter, Heated Probe 

## Co Ane1yLer'

Hea#eti Ssmple Line

G as

FID Analyzer @9g

~ 

### hlo:. Anaiyzer

purnla 

# 1 -4 S02 A raalyrZer 

## Heated tt-lanifoki



## `'atnple ~ 

## To Interfernce Train Pr 

## 'ocessor Gaiib:'ation Point Puttnp

Bias Calibratinn Sp-an Line ~ 

## •P

5 

# ~ tiample larocessor cansists of ttivo sl7ort stem impingers followed by a 0_3 PurnP 

## niicron filter

## EfVIISSION TEST SUMMARY

PLAN T : 

### DaI•:ta1,a. Nfoskogee. OP: DATE : 

### I?_-Apr 06 PLACE
: 

### Kiln Scrubber iwxhaus! RUN# : 

### 1 TEST DURATION (MINUTES)
: 

### 60 LIQUID COLLECTED (mis)
: 

### 216.8 NOZZLE DIAMETER (INCH.)
: 

### 0.312 PARTICULATE WEIGHT (Front half mg)
: 

### C METER COEFFICIENT (Y)
: 

### 1 PARTICULATE WEIGHT (Back half mg) : 

### 0 PITOT COEFFICIENT (Cp)
: 

### 0.84 STATIC PRESSURE (in. H20)
: 

### •0.21 GAS METER VOL.(Cu.Ft.)
: 

### 38.2 PERCENT CO2 3.5 BAROMETRIC PRESSURc 29.7 PERCENT 02 17.5 PERCENT CO
: 

### 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 59.5 STACK LENGTH(inchs)
: 

### STACK AREA (Sq.Ft.)
: 

### 19.30907 STACK W1DTH(inchs)
: 

### NOZZLE AREA (feet): 0.000531 STACK AREA (Sq.Ft.)
: 

### 0

ENTER THE S T ACK AREA SHOWN ABOVE: 19.30907


## FLOWS SAMPLED VOLUME (STD. CU .FT.): 36.6495 VOLUME OF WATER VAPOR (STD. CU .FT.): 10.2048 FRACTIONAL MOISTURE CONTENT 0.2178

DRY BASE: 79.0000 MOLECU LAR WT. OF STACK GAS (DRY i3ASE): 29.2600 MOLECU LAR WT. OF STACK GAS (WET BASE): 26.8076 STACK PRESSURE (inch 

## Hg): 29.6846 STACK GAS VELOCITY (ft/sec.): 29.4018 ACTUAL STACK GAS FLOW RATE (ACFM): 34063.27 STANDARD STACK GAS FLOW RATE (SCFH): 1401122.14

ISOKINETIC RATIO 

## (%): 95.1918

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 138 0.30 0.547723 1.30 78 78 2 138 0.30 0.547723 1.30 85 80 3 138 0.26 0.509902 1.20 87 81 4 138 0.24 0.489898 110 88 81 5 138 0.23 0.479583 i.00 89 81 6 138 0.20 0.447214 0.88 90 82 7 138 0.19 0.43589 0.84 90 83 8 138 0.20 0.447214 0.88 94 83 9 138 0.18 0.424264 0.80 91 83 10 137 0.15 0.387298 0.66 92 84 11 136 0.22 0.469042 0.97 87 85 12 136 0.20 0.447214 0.88 92 85 13 137 0.20 0.447214 0.89 93 85 14 137 .0.18 0.424264 0.79 96 85 15 138 0.19 0.43589 0.84 93 86 16 137 0.24 0.489898 1.10 94 86 17 139 0.23 0.479583 1.00 95 87 18 139 0.27 0.519615 1.20 95 87 19 138 0.28 0.52915. 1.30 95 87 20 138 0.24 0.489898 1,07 96 88

137.7 0.4724 1.0000 91.0000 83.8500 87.4250


# 20

### 1 137 0.22 0.469042 0.99 2 138 0.23 0.479583 1,00 3 138 0.20 0.447214 0.80 4 138 0.19 0.43589 0.85 5 13S 0.21 0.458258 0.94 6 138 0.24 0.489898 1.10 7 138 0.27 0.519615 1.20 8 138 0.27 0.519615 1,20 9 138 0.28 0.52915 1.25 10 137 0.24 0.489898 1.10 11 i 35 0.31 0.556776 140 12 138 0.30 0.547723 1.40 13 138 0.25 0.5 1.10 14 138 0.24 0.489898 1.10 15 ! 38 0.23 0.479583 1.05 16 138 0.20 0.447214 0.92 17 138 0.20 0.447214 0.92 18 138 020 0.447214 0.91 19 0.19 0.43589 0.87 20 137 0 15 0.387298 069

137.85 0.4788 1.0395 89 92 95 96 97 97 98 99 99 99 94 100 100 101 101 101 101 101 102 102

98.2000 89 89 90 90 91 91 91 92 92 92 93 94 

## 94 94 94 95 95 U5 95 95

92.5500 95.3750 

# EMISSION TEST SUMNlARY

aLANT : : DATE : :2 A r-;)6 PLACE . Kiln

~ 

### ,; -•ut.ber Exnaust 

## RUN#: 2 TEST DURATION (MINUTES) : -NOZZLE DIAMETER (INCH.) : METER COEFFICIENT (Y) : PITOT COEFFICIENT (Cp) : GAS METER VOL.(Cu.Ft.) : BAROMETRIC PRESSURE : 60 LIQUID COLLECTED (mis) : 

## 0.312 PARTICULATE WEIGHT (Front half mg) 1 PARTICULATE WEIGHT (Back half n

~ 

## ,g) 0.84 STATIC PRESSURE (in. H20) : 39.251 PERCENT CO2 : 293 ' PERCENT 02 PERCENT CO : 18; 9 

# a C 

## -a.22 3 18 0


## FOR CIRCULAR STACK FOR RECTANGULAR- STACK STACK DIAMETER (inch): 59.5 STACK LENGTH(inches) : 

## STACK AREA (Sq.Ft.) : 19.30907 STACK WIDTH(inches) : NOZZLE AREA (feet): 0.000531 STACK AREA (Sq.Ft.) :



## ENTER THE S T ACK AREA SHOWN Ai30VE: 19,30907


# FLOWS SAMPLED VOLUME (STD. CU .FT.): VOLUME OF WATER VAPOR (STD. CU .FT.): FRACTIONAL MOISTURE CONTENT ( o ):

DRY BASE: MOLECULAR WT. OF STACK GAS (DRY i3ASE): MOLECULAR WT. OF STACK GAS (WET BASE): S T ACK PRESSURE (inch Hg): STACK GAS VELOCITY (ft/sec.): 

## ACTUAL STACK GAS FLOW RATE (ACFM): STANDARD STACK GAS FLOW RATE (SCFH):

ISOKINETIC RATIO (%):
POINTS STACK T. DELTA P SQUAR D.P DELTA H



## deg F 37.1224 8.5620 0.1874 79.0000 29.2000 27.1009

29.6838 29.6440 34343.8899 1467129.37

92.0814


## METER T. INLET METER T.



## OUTLET 0



# 21

## EMISSION TEST SUMMARY

PLANT : 

### D::l.itelia. iyt::skoga?. OK. DATE : 

### 12•Apr•06 PLACE
: 

### K,Iri Scrub:

- )er Exhaust RUN#: 3 TEST DURA T ION (MINUTES)
: 

### 60 LIQUID COLLECTED (mis)
: 

## 216 

# r NOZZLE DIAMETER (INCH.)
: 

### 0.312 PARTICULATE WEtGHT (Front half mg)
: 

### G METER COEFFICIENT (Y)
: 

### 1 PARTICULATE WEIGHT (Back half mg)
: 

### 0 PITOT COEFFICIENT (Cp)
: 

### 0.84 STATIC PRESSURE (in. H20)
: 

### .0.2 GAS METER VOL.(Cu.Ft.)
: 

### 40.523 PERCENT CO2 3.5 BAROMETRIC PRESSURE
: 

### 29.7 PERCENT 02 17.5 PERCENT CO 0
FOR CIRCULAR S T ACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 59.5 STACK LENGTH(inchs)
: 

### STACK AREA (Sq.Ft.)
: 

### 19.30907 STACK WIDTH(inchs)
: 

### NOZZLE AREA (feet): 0.000531 STACK AREA (Sq.Ft.)
: 

### 0
ENTER THE STACK AREA SHOWN ABOVE: 19.30907


## FLOWS SAMPLED VOLUME (STD. CU .FT.): 37.9975 VOLUME OF WATER VAPOR (STD. CU .FT.): 10.6614 FRACTIONAL MOISTURE CONTENT 

## (%): 0.2191

DRY BASE: 79.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29,2600 MOLECULAR WT. OF STACK GAS (WET BASE): 26,7929 STACK PRESSURE (inch Hg): 29.6853 STACK GAS VELOCITY (ft/sec.): 29,0113 ACTUAL STACK GAS FLOW RATE (ACFM): 33610.8369 STANDARD STACK GAS FLOW RATE (SCFH): 1379892.29

ISOKINETIC RATIO 

## (%): 100.2116

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 138 0.29 0.538516 1.40 95 95 2 138 0.30 0.547723 1.40 103 96 3 139 0.28 0.52915 1.30 102 97 4 138 0.26 0.509902 1.20 103 97 5 138 0.23 0.479583 1.10 103 97 6 138 0.20 0.447214 0.94 103 98 7 138 0.18 0.424264 0.85 103 98 8 138 0.19 0.43589 0.90 103 98 9 138 0,19 0.43589 0.90 103 98 10 138 0.17 0.412311 0.80 103 98 11 138 0.23 0.479583 1.10 101 98 12 137 0.21 0.458258 0.99 102 99 13 137 0.20 0.447214 0.94 102 99 14 137 0.20 0.447214 0.95 103 99 15 137 0.19 0.43589 0.89 103 99 16 138 0.20 0.447214 0.95 103 99 17 138 0.20 0.447214 0.94 103 99 18 138 0.21 0.458258 0.99 103 99 19 138 0.22 0.469042 1.00 102 99 20 138 0.22 0.469042 100 101 100

137.85 0.4660 1.0270 102.2000 98.1000 100.1500


# ?2

## EMISSION TEST SUMMARY

PLANT : bal-ltal;a. Vw:;kogee. bK DATE : 12-4rn•06 PLACE : l;iEn Scrubbcir Fxiiiust 

## RUNr: ? TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 252.3 

### NOZZLE DIAMETER (lNCH.) : 0.3C97 PARTICULATE WEIGHT (Front half mg) : 108.89 METER COEFFICiENT (Y) : 0.972 PARTICULATE WEIGHT (Back hakf mg) : 11.4 PITOT COEFFICIcNT (Cp) : 0.84 4 STATIC PRESSURE (in. H20) : •D 21 GAS METER VOL.(Cu.Ft.) : 40.433 PERCENT CO2 33 

### BAROMETRIC PRi=SSURE 29.7 PERCENT 02 17.5 

### PERCENT CO 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 59.5 STACK LENGTH('snchs) : STACK AREA (Sq.Ft.) : 19.30907 STACK WIDTH(inchs) : 

### NOZZLE AREA (feet): 0.000523 STACK AREA (Sq.Ft.) : 0

ENTER THE STACK AREA SHOWN ABOVE: 19.30907


## FLOWS SAMPLED VOLUME (STD. CU .FT.): 37.7792 VOLUME OF WATER VAPOR (STD. CU .FT.): 11.8758 

### FRACTIONAL MOIS T URE CONTEN T(

~ 

### J o ): 0.2392 DRY BASE: 79.0000 

### MOLECULAR WT, OF STACK GAS (DRY BASE): 29.2600 M0LECULAR WT. OF S T ACK GAS (WET BASE): 26.5670 STACK PRESSURE (inch Hg): 29.6846 STACK GAS VELOClTY (ft/sec.): 30.3549 

### ACTUAL STACK GAS FLOW RATE (ACFM): 35167.5017 STANDARD S T ACK GAS FLOW RATE (SCFH): 1406674.11

PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0445 PARTlCULAT;. CONCENTRATION (LBS/SCF): 6.36E•06 PARTICULATE EMISSION (LBS/HR): 8.9400


### BACK HALF PARTICULATE CONCENI'RATION (GR./SCF): 0.0047 PARTICULATE CONCENTRATION (LBS/SCF): 6.65E-07 PARTICULATE EMISSION (LBS/HR): 0.9360 iSOKINETIC RA T f0 {q

o ): 99.1963



### POINTS STACK T. D"cL T A P SQUAR D.P DELi A H METER T. METER T.

deg F INLET OUTLET

1 138 0.21 0.458258 1.00 82 80 2 138 0.27 0.519615 1.30 84 80 3 l39 0.29 0.538516 1.40 80" $'J 4 138 0.27 0.519615 1.30 87 80 5 138 0.26 0.509902 1.20 88 81 6 138 0.24 0.489898 1.10 89 81 7 138 023 0.479583 1.10 89 82 8 138 0.25 0.5 1.20 90 82 9 i 38 0.27 0.519615 1.30 90 83 10 138 0.30 0.547723 1.40 91 83 11 137 0.17 0.412311 0.84 85 84 12 137 0.18 0.424264 0.89 85 84 13 137 0.:9 0.43589 0.94 89 84- 14 139 0.20 0.447214 0.99 99 84 15 137 0.2 i 0.458258 1.00 92 84 16 137 017 0.412311 0.84 94 $5 17 ? 3$ 0.20 0.447214 0.99 94 86 18 138 0.21 0.458258 i. 30 95 86 19 138 0.31 0.556776 1.50 95 37 20 138 0.33 0.574456 1.60 95 38

137.85 0.4855 1.1595 89.9500 83.2000 86.5750 

# ?3

### EMISSION TEST SUMMARY

PLANT : DaI-It;:Ita. MuSkngeH. OK 

### DATE : 12-AFsr-06 PLACE : Ki}n 3rru!:!'iEtr Exh

~ ust RUNst : 2 TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 201.3 NOZZLE DIAMETER (INCH.) : 03097 PARTICULATE WEIGHT (Front half mg) : 34.99 METER COEFFICIENT (Y) : 0.972 PARTICULATE WEIGHT (Back half mg) : : 3.2 PITOT COEFFICIENT (Cp) : 0.34 STA T IC PRESSURE (in. H20) : 0.2 GAS METER VOL.(Cu.FI.) : 4; .752 PERCENT CO2 2 BAROMETRIC PRESSURE 29.7 PERCENT 02 18 PERCENT CO 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 59.5 STACK LENGTH(inches) : STACK AREA (Sq.Ft.) : 19.30907 STACK WIDTH(inches) : NOZZLE AREA (feet): 0.000523 STACK AREA (Sq.Ft.) : 0


### ENTER THE STACK AREA SHOWN ABOVE: 19.30907


## FLOWS SAMPLED VOLUME (STD. CU .FT.): 38.3735 VOLUME OF WATER VAPOR (STD. CU .FT.): 9.4752 FRACTIONAL MOISTURE CONTENT 0.1980



### DRY BASE: 79.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.2000 MOLECUL AR WT. OF STACK GAS (WET BASE): 26.9821

STACK PRESSURE (inch Hg): 29.6853 STACK GAS VELOCITY (ft/sec.): 29.9506 ACTUAL STACK GAS FLOW RATE (ACFM): 34699.0433 STANDARD STACK GAS FLOW RATE (SCFH): 1463881.07

PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0382 

### PARTICULATE CONCENTRATION (LBS/SCF): 5.46E•06 PARTICULATE EMISSION (LBS/HR): 7-9903


### BACK HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0053 

### PARTICULATE CONCENTRATION (LBS/SCF): 7.58E•07 PARTICULATE EMISSION (LBS/HR): 1.1103 ISOKINETIC RATIO (%): 96.8184



### POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.



### deg F INLET OUTLET

1 132 0. i 6 0.4 8.00 90 89 2 137 0.19 0.43589 0.95 94 90 3 138 0.20 0.447214 1.00 95 91 4 138 0.19 0.43589 0.95 95 9 i 5 137 0.21 0.458258 1.00 96 92 6 137 0.22 0.469042 1.10 96 92 7 138 0.25 0.5 1.20 97 92 8 133 0.27 0.519615 1.30 99 93 9 138 0.30 0.547723 1.50 101 93 10 138 0,31 0.556776 1.50 102 93 11 138 0.21 0.458258 1.00 99 94 12 138 0.28 0.52915 1.50 10? 94 13 '. 38 027 0.519615 1 40 101 95 14 ] 33 0.2E 0.52915 1.50 102 95 15 138 0.25 0.5 1.30 102 95 16 133 0.2C , 0.447214 1.00 102 95 17 12118 0.19 0.43589 1.00 103 95 18 :36

~ :.21 0.458258 1.10 104 95 19 138 G.25 0.5 1 3;) 102 95 20 137 026 0.509902 1 40 103 95

137.5 0.4829 1.5500 99.2000 93.2000 96.2000

P 4

### EMISSION TEST SUMMARY

PLANT : Caf•!talia. OK. DATE : . z-Aar•06 PLACE "ocrunLvr Eyt

- aus; RUN#: < 

### TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : NOZZLE DIAMETER (INCH.) : 0.3097 PARTICULATE WEIGHT (Front half mg) : METER COEFFICIENT (Y) : 2. 9 72 PARTICULATE WEIGHT (Back hatf mg) : ?ITOT COEF=ICIENT (Cp) 3.8: STA 7 IC PRESSURE (in. H20) : GAS METER VOL.(Cu.Ft.) : 38 78 PERCENT CO2 BAROMETRIC PRESSURE 24.7 ?ERCENT 02 

### PERCENiCO

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAME T ER (inch): 59-5 STACK LENGTH(inchs) : STACK AREA (Sq.Ft.) : I9.30907 STACK WIDTH(inchs) : NOZZLE AREA (feet): 0.000523 STACK AREA (Sq.Ft.) :

ENTER THE STACK AREA SHOWN ABOVE: 19.30907


## FLOWS SAMPLED VOLUME (STD. CU .FT.): 35.4140 VOLUME OF WATER VAPOR (STD. CU .FT.): 9.8941 FRACTIONAL MOISTURE CONTENT {q o ): 0.2184 DRY BASE: 79.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.2600 MOLECULAR WT. OF STACK GAS (WET BASE): 26.8011 ST.4CK PRESSURE (inch Hg): 29.6846 STACK GAS VELOCITY (ft/sec.): 27.3644 ACTUAL STACK GAS FLOW RATE (ACFM): 31702.8871 STANDARD STACK GAS FLOW RATE (SCFH): 1302310,56
PARTICULATE FRONT HALF PARTICULATE CONCEN T RATION (GR./SCF): 0.0341 PARTICULATE CONCENTRATION (LBS/SCF): 4.87E•06 PARTICULATE EMISSION (LBS/HR): 6.3418

BACK HALF PARTICULA T E CONCENTRATION (GR./SCF): 0.0034 PARTICULATE CONCENTRATION (LBS/SCF): 4.83E•07 ,PARTICULATE EMISSION (LBS/HR): 0.6284 ISOKINETIC RATIO (%): 100.4374

POINTS STACK T. DELTA P SQUAR D.P Dc'LTA H METER T. METER T.

deg F INLET OUTLET
1 138 0.20 0.447214 i l C 95 94 2 138 C.24 0.489898 1.30 100 95 3 139 0.25 0.5 1.30 102 95 4 139 0.26 0.509902 1,40 102 95 5 139 0 24 0.489898 30 103 96 6 139 0.20 0.447214 : 00 103 96 7 135 0.21 0.458258 : 1 C 103 96 fi i 39 0.22 0.469042 1.10 103 96 9 136 0.23 0.479583 1.20 103 9-3 10 i 38 0.24 0.489898 1.30 102 96 11 138 0 15 0.387 298 081 10: 97 12 137 0, i 7 0.412311 0.92 l O 1 97 13 138 0. I:; 0.424264 D.97 i 03 97 14 :3S C; 17 0.412311 0,92 103 97 15 138 0 15 0.387298 081 103 97 16 138 0.:8 0.424264 0.97 103 1 

### 96 17 I 3

~ 

### + r?. i 6 0.4 0,£35 1 

### 103 96 18 1 38 0.14 0.374166 0.76 l Os 96 19 :"sL 0.16 04 C.f:b 102 97 20 i 33 ;

~ 

### . :; ~ 

### 0.387298 0 81 103 97
138.05 0.4395 1.0395 102,0500 96.1000 210.2 78.21
-021 

# 3.5 17.5 

## 0

0

99.0750



## ~ 

# v

## 0.81 0.9 1.50 85 80 0.92 0.959166 1.70 85 81 1.30 1.140175 2.40 86 81 1.40 1.183216 2.60 88 82 1.30 1.140175 2.40 87 82 1.20 1.095445 2.30 88 83 0.93 0.964365 1.70 85 83 1.10 1.048809 2.10 86 84 1.30 1.140175 2.40 87 84 1.40 1.183216 2.60 89 84 1.30 1.140175 2.40 91 85 1. ; 0 1.048809 2.10 91 87

1.0786 2.1833 87.3333 83.0000 85.1667 

# 1 2 3 4 5 6 7 8 9 10 11
1 

# 2 434

459 459 458 456 456 452 460 459 460 ^61 465

456.58333 

# EMISSION TEST SUMMARY

PLANT 11%11usl,o;ee. C;i! DATE : 13 Ahr•06 

# PLACE : Trim Kiln Exh,aLas't RUN# :

_ TEST DURATION (MINUTES) : 6C

~ 

## LIQUID COLLECTED (mis) : oh.] NOZZLE DIAMETER (INCH.) : 0.2483 PARTICULATE WEIGHT (r=ront haff mg) : G METER COEFFICIENT (Y) : 1 PARTICULATE WEIGHT (Back half mg) : 0 

## PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : .0.55 GAS METER VOL.(Cu.Ft.) : 55.256 PERCENT CO2 : 3 BAROMETRIC PRESSURE : 29.7 PERCENT 02 : 18 

# PERCENT CO : 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 24.5 STACK LENGTH(inchs) : 

# STACK AREA (Sq.Ft.) : 3.273856 STACK WIDTH(inchs) : NOZZLE AREA (feet): 0.000336 STACK AREA (Sq.Ft.) : 0

ENTER THE STACK AREA SHOWN ABOVE: 3.273856


# FLOVYS SAMPLED VOLUME (STD. CU .FT.): VOLUME OF WATER VAPOR (STD. CU .FT.): FRACTIONAL MOISTURE CONTENT

DRY BASE: MOLECULAR WT. OF STACK GAS (DRY BASE): MOLECULAR WT. OF STACK GAS (WET BASE): STACK PRESSURE (inch Hg): STACK GAS VELOCITY (ft/sec.): ACTUAL STACK GAS FLOW RATE (ACFM): STANDARD STACK GAS FLOW RATE (SCFH):

ISOKINETIC RATIO ( J

o ):
POINTS STACK T. DELTA P SQUAR D.P DELTA H



# deg F 53.3883 4.0527 0.0706 79.0000 29.2000 28.4098

29.6596 80.7872 15869.132 505351.318

102.9200

METER T. METER T. INLET OU T LET



# 26

# EMISSION TEST SUMMARY

PLANT : Dal•I;alia. , Mi.skogee. 0K 

## DATE : i 3 Apr-06 PLACE : T rim Kiln Exhaust ?UN# :

~ 

## ? TLST DURaTION (MINUTES) : 

## IVOZZLE DIAMETER (INCH.) : METER COEFFICIENT (Y) : PITOT COEFFICIENT (Cp) : GAS METER VOL.(Cu.Ft.) : BAROMETRIC PRESSURE : 60 LIQUfD COLLECTED (mis) : 0.2483 PARTICULATE WEIGHT (Fron; half mg) 1 PARTICULATE WEIGHT (Back half mg) 0.84 STATIC PRESSURE (in. H20) : 56.517 PERCENT CO2 : 29.7 PERCENT 02 : PERCENT CO : 0 0 0.53 3 18 

## 0



# C FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 24.5 STACK LENGTH(inches) : STACK AREA (Sq.Ft.) : 3.273856 STACK WIDTH(inches) : NOZZLE AREA (feet): 0.000336 STACK AREA (Sq.Ft.) :

ENTER THE STACK AREA SHOV'JN ABOVE: 3.273856


# FLOWS SAMPLED VOLUME (STD. CU .FT.): 53.8860 VOLUME OF WATER VAPOR (STD. CU .FT.): 4.0245 FRACTIONAL MOISTURE CONTENT (%): 0.0695

DRY BASE: 79.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.2000 MOLECULAR WT. OF STACK GAS (WET BASE}: 28.4217 STACK PRESSURE (inch Hg): 29.6610 STACK GAS VELOCITY (ft/sec.): 80.5616 ACTUAL STACK GAS FLOW RATE (ACFM): 15824.8273 STANDARD STACK GAS FLOW RATE (SCFH): 501893.365

ISOKINETIC RATIO (%): 104.5950
POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 456 0.91 0.953939 1.70 90 87 2 461 1.20 1.095445 2.30 94 88 3 462 1.40 1.183216 2.60 93 88 4 462 -.30 1.140175 2.40 95 89 5 461 1.20 1.095445 2.30 96 89 6 460 0.96 0.979796 1.80 100 91 7 461 1.10 1.048809 2.10 91 89 8 463 1.20 1.095445 2.30 95 91 9 463 1.30 1.140175 2.40 96 91 10 463 1.20 1.095445 2.30 96 92 11 463 1.10 1.048809 2.10 97 92 12 462 1.00 1 1.90 97 92
461.41667 1.0731 2.1833 95.0000 89.9167 92.4583


# 2 

# 7

# EM1SSlON TEST SUMMARY

PLANT : Dai-Italia. tVluskogee, rJK DATE : '_ 3-Apr-06 PLACE : Trirn KiIn Exf;aust RUN#: 3


## TEST DURATION (MINUTES) : 60 NOZZLE DIAMETER (INCH.) : 0.2483 

## METER COEFFICIENT (Y) : 1 PITOT COEFFICIENT (Cp) : 0.84 GAS METER VOL.(Cu.Ft.) : 55.067 BAROMETRIC PRESSURE : 29.7

FOR CIRCULAR STACK STACK DIAMETER (inch): 24.5 STACK AREA (Sq.Ft.) : 3.273856 NOZZLE AREA (feet): 0.000336
ENTER THE STACK AREA SHOWN ABOVE:


# FLOWS SAMPLED VOLUME (STD. CU .FT.): VOLUME OF WATER VAPOR (STD. CU .FT.): FRACTIONAL MOISTURE CONTENT (%):

DRY BASE: MOLECULAR WT, OF STACK GAS (DRY BASE): MOLECULAR WT. OF STACK GAS (WET BASE): STACK PRESSURE (inch Hg): STACK GAS VELOCITY (ft/sec.): ACTUAL STACK GAS FLOW RATE (ACFM): STANDARD STACK GAS FLOW RATE (SCFH):

1SOKINETIC RATIO (%): LIQUID COLLEC T ED (mis) : PARTICULATE 

## WEIGHT (Front half mg) ; 0 PARTICULATE WEIGHT (Back half rng) : 0 STATIC PRESSURE (in. H20) : 0.53 PERCENT CO2 : 3 PERCENT 

# 02 : 18 PERCENT CO 0

FOR RECTANGULAR STACK STACK LENGTH(inchs) : STACK WIDTH(inchs) : STACK AREA (Sq.Ft.) : C

3.273856

52.3574

3.8550 0.0686 79.0000 29.2000 28.4319

29.6610 78.4134 15402.8489 488372.192

104.4415

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 465 0.92 0.959166 1.80 91 91 2 464 1.20 1.095445 2.30 95 90 3 463 1.30 1.140175 2.40 97 91 4 465 1.20 1.095445 2.30 97 91 5 464 1.10 1.048809 2.10 95 91 6 437 0.91 0.953939 1.70 95 92 7 466 1.00 1 1.90 94 92 8 466 1.20 1.095445 2.30 97 92 9 466 1.20 1.095445 2.40 98 93 10 466 1.10 1.048809 2.10 97 93 11 464 1.00 1 1.90 98 93 12 465 0.99 0.994987 1.90 98 92

462.58333 1.0440 2.0917 96.0000 91.7500 93.8750

s

# EMlSSION TEST SUMMARY

PLANT : Dat•1*311, 12. MU-,:eU

~~ 

### _ ei

~ 

### ","'( 

### DATE . : 3

~ 

### .pr Q6 PLACE : 1 rim ±<,Ar. E>;haus; RUN# : 1 TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 91.9 

### NOZZLE DIAMETER (INCH.) : 0.2487 PARTICULATE WEIGHT (Front half mg) : ti.34 

### ME T ER COEFFICIENT (Y) : G.972 PARTICUL ATE WrIGHT (Back nalf mg) : 20.2 r'1TOT COEFFICIENT (Cp) : 0.8M STATIC PRcSSURE (in. H20) : •0 55 GAS METER VOL.(Cu.Ft.) : :;6.16 PERCENT CO2 3 BAROMETRIC PRESSURE 29.7 PERCENT 02 14 PERCENT CO 0
FOR CIRCULAR STACK FOR REC T ANGULAR STACK 

### STACK DIAMETER (inch): 24.5 STACK L"cNGTH(inchs) : STACK AREA (Sq.Ft.) : 3.273856 STACK WIDTH(inchs) : 

### NOZZLE AREA (feet): 0.000337 S T ACK AREA (Sq.Ft.) : 0
ENTER THE STACK AREA SHOWN ABOVE: 3.273856


# FLOWS SAMPLED VOLUME (STD. CU .FT.): 53.2366 VOLUME OF WATER VAPOR (STD. CU .FT.): 4.3257 FRAC T IONAL MOISTURE CONTENT {q o ): 0.0751 DRY BASE: 79.0000 MOLECULAR WT..OF STACK GAS (DRY BASE): 29.2000 MOLECULAR W T. OF S T ACK GAS (WET BASE): 28.3583 STACK PRESSURE (inch Hg): 29.6596 STACK GAS VELOCITY (ft/sec.): 80.0786 ACTUAL STACK GAS FLOW RATE (ACFM): 15729.9538 STANDARD STACK GAS i=LOW RATE (SCFH): 498579.228
PARTICULATE FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0137 PARTICULATE CONCENTRATION (LBS/SCF): 1.96E•06 PARTICULATE EMISSION (LBS/HR): 0.9776


### BACK uALF PARTICULATE CONCENTRATION (GR./SCF): 0.0059 PARTICULATE CONCENTRATION (LBS/SCF): 8.37E•07 PARTICULATE EM1SSi0N (LBS/HR): 0.4171
ISOKINETIC RATIO (aj' o ): 

### 103.6873

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 450 1.10 1.048809 2.20 76 76 2 456 1.30 1.140175 2.60 79 76 3 457 1.30 1.140175 2.60 81 77 4 457 1.30 1.140175 2.60 82 78 5 457 1.10 1.048809 2.20 81 78 6 456 0. 0 32 0.959166 :.80 82 79 7 456 i.20 1.095445 2.40 80 79 8 A- 58 1.30 1.140175 2.60 83 79 gt:r(:) 1.30 1.140175 2.60 83 80 10 460 ;.20 1.095445 2.40 84 gl 11 116: 1.00 1 2.00 84 81 12 4.49 ;,ti.16 0.87178 i.50 86 32
456.33333 1.0684 2.2917 81.6667 78.8333 80.2500


# 2~

## EMISSION TEST SUMMARY

PLANT : r)a; iiylia. h.4,.is

~ oa_e

~ . Oy 

### DATE : 13->'.pr-0h PLACE : i rim <<,iln i:.xtiaust 

### RUN# : 2 TEST DURATION (MINUTES) : oU LIQUID COLLECTED (mis) NOZZLE DIAMETER (lNC'-f.) : ',12=:87 PARTICULATE WEIGHT (Front half mg) : '.3.71 

### iv1ETER COErFICIENT (Y) : 0 9. 2 PARTICULATE WEIGHT (Back half mg) : In'.():5 PI'OT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : r-53 GAS METER VOL.(Cu.Ft.) : 57.4:; PERCENT CO2 3 BAROMETRIC PRESSURE 29.7 PERCENT 02 18 PERCENT CO 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 24.5 STACK LENGTH(inches) : 

### STACK AREA (Sq.Ft.) : 3.273856 STACK WIDTH(inches) : NOZZLE AREA (feet): 0.000337 STACK AREA (Sq.Ft.) : 0

ENTER THE STACK AREA SHOWN ABOVE: 3.27 385-6 

## FLowS SAMPLED VOLUME (STD. CU .FT.): 53.9239 VOLUME OF WATER VAPOR (STD. CU .FT.): 4.4622 FRACTIONAL MOISTURE CONTENT (%): 0.0764

DRY BASE: 79.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.2000 

## MOLECULAR WT. OF STACK GAS (WET BASE): 28.3440 STACK PRESSURE (inch Hg): 29.6610 STACK GAS VELOCITY (ft/sec.): 82.1520 ACTUAL STACK GAS FLOW RATE (ACFM): 16137.2302 

## STANDARD STACK GAS FLOW RATE (SCFH): 50B126.869

PARTICULATE 

## FRONT HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0096 

## PARTICULATE CONCENTRATION (LBS/SCF): 1.38E•06 PARTICULATE EMISSION (LBS/HR): 0.7004


## BACK HALF PARTICULATE CONCENTRATION (GR./SCF): 0.0052 PARTICULATE CONCENTRATION (LBS/SCF): 7.38E•07 PARTICULATE EMISSION (LBS/HR): 0.3750 ISOKINETIC RATIO (%,): 103.0525

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 460 1.20 1.095445 2.40 82 82 2 461 1.30 1.140175 2.60 85 82 3 461 1.30 1.140175 2.60 86 82 4 461 1.30 1.140175 2.60 87 83 5 dC 3 1.20 1.095445 2.40 87 84 6 458 0.87 0.932738 :.70 88 84 7 460 1.20 1.095445 2.40 85 35 8 461 1.30 1.140175 2.60 88 85 9 463 1.30 1.140175 2.6C 89 85 10 464 1.30 1.140175 2.60 90 86 11 462 1.20 1.095445 2.40 90 8 ~ 

### 12 450 0.92 0.959166 1.80 90 37

461.16667 1.0929 2.3917 87.2500 84.2500 85.7500 

# 30

## EMISSION TEST SUMMARY

?LAN T. "`a? I:a? tc . ~,~ • ISf`•'.^ f ~ ~) ~ 

### DATE : 13-Apr.06 PLACE : 7n:-n "'.i?r Exhau,t 

### RUN# : 3 TEST DURATION (MiNUTES) : 60 LIQUiD COLLECTED (mis) : 81.3 

### NOZZLE DIAMETER (INCH.) : 0.2467 PARTICULATE WEIGHT (Front half mg) : 24.79 

## M"c T rR COEFFICIENT (Y) : 0.972 PARTICULATE WE1GHT (Back half mg) : i 3.7 PITOT COEFFICIENT (Cp) : 0.84 STATlC PRESSURE (in. H20) : •0,53 GAS fvlE T ER VOL.(Cu.Ft,) : 56.998 PERCENT CO2 3 BAROMETRIC PRESSURE

. 29.7 PERCENT 02 . 1$ 

## PERCENT CO 0
FOR CIRCULAR STACK FOR RECTANGULAR S i ACK S T ACK DlAMETER (inch): 24.5 STACK LENGTH(inchs) : STACK AREA (Sq.Ft.) : 3.273856 STACK WIDTH(inchs) : NOZZLE AREA (feet): 0.000337 STACK AREA (Sq.Ft.) : 0

ENTER THE STACK AREA SHOVt N ABOVE: 3.273856


## FLOWS SAMPLED VOLUME (STD. CU .FT.): 53.1727 

## VOLUME OF WA T ER VAPOR (S'[D. CU.FT.): 3.8503 FRACTIONAL MOIS T URE CON T ENT {%): 0.0675

DRY BASE: 79.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.2000 MOLECULAR WT. OF STACK GAS (WET BASE): 28.4438 

## S TACK PRESSURE (inch Hg): 29:6610 STACK GAS VELOCiTY (ft/sec.): 81.4302 ACTUAL STACK GAS FLOW RATE (ACFN+): 15995.4449 

## STANDARD STACK GAS FLOW RATE (SCFH): 507691.339
PARTICULATE FRONT HALF PARTtCULATE CONCENTRATION (GR./SCF): 0.0072 PAR i ICULATE CONCENTRATION (LBS/SCF): 1.03E•06 PARTICULATE EMISSION (LBS/HR): 0.5219


## -BACK HALF PARTiCUt.ATE CONCENTRATION (GR./SCF): 0.0040 PARTICULATE CONCENTRATION (LBS/SCF): 5.6$L•07 PARTICULATE EMISSION (LBS/HR): 0.2884 iSOKINETIC RATIO (% a }: 101.7038



## POINTS STACK T. DELTA P SQUAR D.P DELTA H. METER T. METER T.

deg F INLET OUTLET

1 462 1.20 1.095445 ' 2.40 87 87 2 463 :.40 1.183216 2.80 88 87 3 464 1.30 1.140175 2.60 89 87 4 465 1.30 1.140175 2.60 90 88 5 465 1.20 1.095445 2.40 C. 88 6 455 0.78 0.883176 1.60 90 88 7 462 1.20 1.095445 2.40 89 88 8 e-65 1.40 1.183216 2.80 91 89 9 464 1.30 1.140175 2.60 91 89 10 466 1.20 1.095445 2.40 91 89 11 466 1. : 0 1.048809 2.20 9°_ 89 12 0.83 0.911043 1.70 92 90

462.66667 1.0843 2.3750 89.9167 88.2500 89.0833 

# '? I

# AppendiX ' B

# Sheetl

Summary of CO Analyzer CF 14-, ra:for.s arfcu Bias

Plant: Daltile, Muskogee.. Source: Kiln Scrubber Date: 411212006



# Anafyzer Calibratrion Data



# Cylinder Analyzer Absolute % Span Value Response Difference Zero Gas 0 0.33 0.33 0.066 Mid Range 200 200.3 0.3 0.06 High Range 494 490.55 -3.45 -0.69

System Calibration Bias and Drift Data

Analyzer Initial Values Final Vaiues Drift Average Calibration System System System System Calibration Response Cafibration Calibration Calibration Calibration Values

Response Bias Response Bias

Run #1 Zero Gas 0.33 -0.03 -0.072 -0.45 -0.156 -0.084 -0.24

Upscale 200.3 192.7 -1.52 193.63 -1.334 0.186 193.165 Average CO Concentration: 157.28 Corrected CO Concentration: 162.8913 (Equation 6C-1)

Run #2 Zero Gas 0.33 -0.45 -0.156 -3.68 -0.802 -0.646 -2.065

Upscaie 200.3 193.63 -1.334 189.78 -2.104 -0.77 191.705 Average CO Concentration: 148.67 Corrected CO Concentration: 155.5814 (Equation 6C-1)

Run #3 Zero Gas 0.33 -3.68 -0.802 -4.95 -1.056 -0.254 -4.315

Upscale 200.3 189.78 -2.104 187.63 -2.534 -0.43 188.705 Average CO Concentration: 137.64 Corrected CO Concentration: 147.0884 (Equation 6C-1)

Page 1 ~ 

# .~

# Sheetl

Summary of NOx Analyzer Caiibrations and Bias

Piant: Daltile, Muskogee, OK Source: Kiln Scrubber Date: 4/12/2006



# Analyzer Calibratrion Data Cylinder Anafyzer Absolute % Span Value Response Difference Zero Gas 0 0 0 0 Mid Range 25.5 24.8 -0.7 -1.16667 High Range 51 51 0 0



# System Ca{ibration Bias and Drift Data

Anafyzer lnitial Values Final Vafues Drift Calibration System System System System Response Cafibration Calibration Calibration Calibration

Response Bias Response Bias

Run #1 Zero Gas 0 0 0 0.5 0.833333 0.833333

Upsca(e 24.8 23.75 -1.75 23.8 -1.66667 0.083333 Average NOx Concentration: 28.63 Corrected NOx Concentration: 30.76259 

# (Equation 6C-1)

Run #2 Zero Gas 0 0.5 0.833333 0.6 1 0.166667

Upscale 24.8 23.8 -1.66667 23.45 -2.25 -0.58333 Average NOx Concentration: 29.91 Corrected NOx Concentration: 32.4455 

# (Equation 6C-1)

Run #3 Zero Gas 0 0.6 1 0.85 1.416667 0.416667

Upscale 24.8 23.45 -2.25 23.53 -2.11667 0.133333
Average NOx Concentration: 30.5 Corrected NOx Concentration: 33.35219 (Equation 6C-1) Average Calibration Values

0.25 23.775

0.55 23.625

0.725 23.49

Page 1 

# ~ ~

# System Ca6ibration Bias and Drift Data AnafyZer Initial Va(ues Final Values Drift Calibration System System System System Response Catibration Calibration Calibration Calibration

Response Bias Response Bias

Run #1 Zero Gas 0.15 0.68 0.53 0 -0.15

Upscale 49.7 46.63 -3.07 45.6 -4.1
Average S02 Concentration: 1.29 Corrected S02 Concentration: 1.033534 (Equation 6C-1)

Run #2 Zero Gas 0.15 0 -0.15 -0.25 -0.4

Upscaie 49.7 45.6 -4.1 46 -3.7
Average S02 Concentration: -0.12 Corrected S02 Concentration: 0.005422 (Equation 6C-1)

Run #3 Zero Gas 0.15 -0.25 -0.4 -0.8 -0.95

Upscale 49.7 46 -3.7 45.53 -4.17 Average S02 Concentration: -0.08 Corrected S02 Concentration: 0.478743 

# (Equation 6C-1) Average Calibration Values

-0.68 0.34 -1.03 46.115

-0.25 -0.125 0.4 45.8

-0.55 -0.525 -0.47 45.765 

# SlZeet1

Summary of Sulfur Dioxide Analyzer Cafibrations and Bias

PI«nt: Daltile, Muskogee, OrC Source: Kiln Scrubber Date: 4/12/2006



# Analyzer CaEibratrion Data Cylinder Analyzer Absolute % Span Va(ue Response Difference Zero Gas 0 0.15 0.15 0.15 Mid Range 49.8 49.7 -0.1 -0.1 High Range 100 99.8 -0.2 -0.2

Page 1 P ~~

# 4/11/06 NOx Converter Check



# Date/Time NOx mm/d 

# d/ yy hh:mm:s 

# s 04/11/06 17:30:27 _ 04/11 /06 17:31:27 ~ 

# 04/1 1106 1 7:32:27 

# ippm 0.039 39.33594 51 .277 _ _ _Zero

! -

_ 

# _ _

NOx

_ ( 51 ppm NOx
04111/06 17:34:27 _ - 30.9961

-

04/11 /06 17:38:27 30.98389 04111 /06 17:33:27 21.60938 `
04/11 /06 17:35:27 ^' 31.02686 04/11 /06 17:36:27 30.99414 

# 04/11 /06 17:37:27 30.97949
04/11 /06 17:39:27 30.91114 ~



# - ----- - ~ 

# ------ ~



# Start Converte_r C_heck

..----- - ~ 

# ----_ - -

04/11 /06 17:40:27 J 30.92432 04/11 /06 17:41:27 30.92286 ' 04/11 /06 17:42:27 30.89356 04/11 /06 17:43:27 30.90381 04/11/0617:44:27 30.86866 04/11 /06 17:45:27 30.87012 ( ~ 

# 04/11 /06 17:46:27 ( 30.86085 04/11/0617:47:27 ; 30.85401

- ~ 

# 04/11 /06 17:48:27 30.86427 04/11 /06 17:49:27 30.85157 04/11 /06 17:50:27 30.85352 04/11/06 17:51:27 30.833511 ( ' 04111 /06 17:52:27 04/11/0617:53:27 04/11/06 17:54:27 30.80665 30.7671
4 

# 30.78565 04/11 /06 17:55:27 30.76808 04/11 /06 17:56:27 30.7715 04/11/06 17:57:27 30.75734 04/11 /06 17:58:27 30.779311 04111 /06 17:59:27 30.74953 04/11 /06 18:00:27 30.77931 04/11 /06 18:01:27 30.7046 , ( 04/11 /06 18:02:27 30.71339 04/11/06 18:03:27 30.70119

_ Stop Converter Check 04/11 /06 18:04:27 30.71094 - -^ ~ 

# (

~ - ~ _-T

~ 

# I

Page 1 684/12106 Calibraiions

DaterTime VOC CO NOx S02 mm/d&yy hh:mm:ss ppm ppm ppm PPm 04112/06 08:22:16 1.4 0.0 0.0 0.0 04112106 0822:26 1.3 1 3.0 0.0 0.1 04/12106 08:22:36 1.2 0.0 0.0 0.1 04112/06 08:22:46 1.3 0.0 0.0 0.1 04/12/06 08:22:56 1.4 0.0 0.0 0.1 04112106 08:23:06 1.4 0.0 0.0 0.1 04/12106 08:23:16 1.4 0.0 0.0 0.1 04/12/06 08:23:26 1.3 0.2 0.0 0.1 04112106 08:23:36 1.4 0.1 7.6 0.0 04/12/06 08:23:46 1.4 0.1 23.8 0.1 04/12/06 Oa:23:56 1.4 0.1 24.1 0.1 04112/06 08:24:06 1.4 03 24.2 0.1 04112/06 08:24:16 1.4 0.3 24.3 0.2 04112/06 08:24:26 1.4 0.3 24.3 0.1 04112/06 08:24:36 1.4 0.3 24.3 0.1 04/12/06 08:24:46 1.4 0.3 24.4 0.1 04/12/06 08:24:56 1.4 0.2 24.3 0.1 04112/06 08:25:06 1.5 0.3 24.7 0.1 04112/06 08:25:16 

### 1.4 0.3 24.8 0.1 04/12/06 08:25:26 1.4 0.3 24.8 0.1 04l12/06 08:25:36 1.4 0.3 24.8 0.2 04112/06 08:25:46 1.4 0.4 24.8 0.2 04/12/06 08:25:56 1.3 0.3 24.9 0.2 04/12/06 08:26:06 1.3 0.3 20.5 0.2 04/12/06 08:26:16 1.3 0.6 0? 0.2 04/12/06 08:26:26 1.3 0.4 0.1 0.1 04/12/06 08:26:36 1.4 0.3 0.0 0.2 04112106 08:26:46 1.4 0.2 0.0 0.1 04/12/06 08:26:56 1.3 0.2 0.0 0.1 04112/06 08:27:06 1.4 0.0 34.6 0.1 04/12/06 08:27:16 1.4 0.1 50.6 0.2 04/12/06 08:27:26 1.4 0.2 50.9 0.1 04/12/06 08:27:36 1.5 -0.1 50.9 0.1 04/12/06 08:27:46 1.5 -0.1 50.9 0.1 04/12/06 08:27:56 1.6 0.1 51.0 0.1 04/12/06 08:28:06 1.5 0.1 51.0 0.2 04/12/06 08:28:16 1.4 0.1 51.0 0.1 04112106 08:28:26 1.5 0.2 51.0 0.2 04112/06 08:28:36 1.5 0.2 41.1 0.2 04/12/06 08:28:46 1.4 0.3 0.2 0.1 04/12/06 08:28:56 1.2 0.4 0.1 0.1 04/12106 0829:06 1.2 0.3 0.1 0.2 04112/06 08:29:16 1.3 0.2 0.0 0.2 04/12/06 08:29:26 1.3 0.3 0.0 0.2 04112106 08:29:36 1.3 0.3 0.0 0.3 04/12106 08:29:46 1.2 17.1 0.0 0.2 04/12/06 08:29:56 1.2 172.0 0.0 0.2 04/12/06 08:30:06 1.4 191.6 0.0 0.2 04112/06 08:30:16 1.3 192.0 0.0 0.3 04112/06 08:30:26 1.2 192.1 0.0 0.3 04112/06 08:30:36 1.4 198.6 0.0 0.3 04/12/06 08:30:46 1.3 196.7 0.0 0.2 04/12/06 08:30:56 1.3 196.8 0.0 0.3 04/12/06 08:31:06 1.4 195.6 0.0 0.2 04112/06 08:31:16 1.4 195.8 0.0 0.3 04/12106 08:31:26 1.4 196.1 0.0 0.4 04/12106 08:31:36 1.3 200.2 0.0 0.3 04/12106 08:31:46 1.3 200.3 0.0 0.3 04/12/06 08:31:56 1.3 200.7 0.0 0.3 04/12/06 08:32:06 1.3 206.7 0.0 03 04/12/06 08:32:16 1.3 206.5 0.0 0.3 04/12/06 08:32:26 1.3 196.9 0.0 0.4 04/12/06 08:32:36 1.3 198.6 0.0 0.5 04112/06 08:32:46 1.3 201.8 0.0 0.4 04/12/06 08:32:56 1.4 199.9 0.0 0.3 04112/06 08:33:06 1.3 200.4 0.0 0.4 04112106 08:33:16 1.4 200.5 0.0 0.4 04/12/06 08:33:26 1.3 200.4 0.0 0.4 Zero NOx

25.5 ppm NOx Zero CO, S02

51 ppm NOx

200 ppm CO

Page 1 

### R ~41 12106 Calibrations

04112/06 08:33:36 1.3 181.3 0.0 0.4 04/12/06 08:33:46 1.4 61.1 0.0 0.3 04/12/06 08:33:56 1.3 0.7 0.0 0.3 04112/06 08:34:06 1.3 0.4 0.0 0.3 04112/06 08:34:16 1.4 0.3 0.0 0.3 04/12/06 08:34:26 1.2 0.3 0.0 0.0 04112/06 08:34:36 1.2 0.3 0.0 -0.1 04/12/06 08:34:46 1.2 0.3 0.0 0.0 04112106 08:34:56 1.3 0.2 0.0 0.0 04/12/06 08:35:06 1.4 0.2 0.0 -0.1 04/12/06 08:35:16 1.2 0.1 0.0 -0.1 04/12/06 08:35:26 1.2 0.2 0.0 -0.1 04/12/06 08:35:36 1.2 306.8 0.0 0.0 04/12/06 08:35:46 1.2 486.4 0.0 0.0 04/12/06 08:35:56 1.2 489.0 0.0 0.0 04112/06 08:36:06 12 489.8 0.0 0.0 04/12/06 08:36:16 1.2 490.5 0.0 0.0 04/12/06 08:36:26 1.3 

### 490.3 0.0 0.0 494 ppm CO 04/12106 08:36:36 1.2 

### 490.6 0.0 0.0 04/12/06 08:36:46 1.1 

### 490.8 0.0 0.0 04/12/06 08:36:56 1.2 490.7 0.0 0.1 04/12/06 08:37:06 1.2 366.9 0.0 0.1 04112106 08:37:16 1.2 32.3 0.0 0.1 04112106 08:37:26 1.3 1.6 0.0 0.0 04/12106 08:37:36 1.2 0.3 0.0 0.0 04112106 08:37:46 1.3 0.2 0.0 0.0 04112/06 08:37:56 1.2 0.2 0.1 0.0 04112/06 08:38:06 1.2 0.2 0.1 0.0 04/12/06 08:38:16 1.2 0.2 0.1 0.1 04/12/06 08:38:26 1.2 0.2 0.0 0.1 04/12/06 08:38:36 1.2 0.3 0.0 0.1 04112106 08:38:46 1.1 0.4 0.0 0.6 04112106 08:38:56 1.1 0.2 0.0 14.4 04112106 08:39:06 1.2 0.5 0.0 35.0 04/12/06 08:39:16 1.1 0.6 0.0 44.7 04/12/06 08:39:26 1.1 0.7 0.0 48.0 04/12/06 08:39:36 1.2 0.5 0.0 49.0 04112106 08:39:46 1.2 0.5 0.0 49.4 04/12106 08:39:56 1.3 0.5 0.0 49.6 04/12J06 08:40:06 1.2 0.5 0.0 49.9 04/12106 08:40:16 1.3 0.6 0.0 50.0 174/12/06 08:40:26 1.3 0.7 0.0 50.1 04112106 08:40:36 1.4 0.7 0.0 50.1 04112/06 08:40:46 1.4 0.6 0.0 50.1 04/12/06 08:40:56 1.2 0.8 0.0 50.0 04/12/06 08:41:06 1.3 0.6 0.0 49.8 04/12/06 08:41:16 1.2 0.7 0.0 49.9 04/12/06 08:41:26 1.2 0.7 0.0 50.0 04/12/06 08:41:36 1.2 0.5 0.0 50.1 04112106 08:41:46 1.1 0.5 0.0 50.1 04/12/06 08:41:56 1.2 0.5 0.0 50.0 04112/06 08:42:06 1.2 0.4 0.0 49.9 04112106 08:42:16 1.1 0.3 0.0 50.1 04/12/06 08:42:26 1.2 0.3 0.0 49.8 04/12/06 08:42:36 1.2 0.3 0.0 

### 49.7 04/12/06 08:42:46 1.2 0.4 0.0 

### 49.7 49.8 ppm S02 04/12/06 08:42:56 1.1 0.4 0.0 

### 49.7 04112/06 08:43:06 1.2 0.3 0.0 

### 49.7 04112106 08:43:16 1.1 0.3 0.0 48.0 04/12/06 08:43:26 1.1 0.3 0.0 31.9 04112/06 08:43:36 1.0 0.3 0.0 13.4 04/12/06 08:43:46 1.0 0.3 0.0 5.1 04112/06 08:43:56 1.1 0.2 0.0 2.5 04112106 08:44:06 1.1 0.0 0.3 19.4 04112106 08:44 :16 1.2 0.2 0.4 63.6 04112106 08:44:26 1.2 0.3 0.3 88.1 04112/06 08:44:36 1.2 0.4 0.4 96.0 04/12106 08:44:46 1.2 0.4 0.3 98.2 04/12/06 08:44:56 1.2 0.4 0.3 98.8 04/12/06 08:45:06 1.2 0.5 0.4 99.1 04/12/06 08:45:16 1.1 0.6 0.3 99.3 04112/06 08:45:26 1.1 0.7 0.3 99.5



### Page 2 6 lj4,12106 Caiibrations

04/12106 08:45:36 1.1 0.6 0.4 99.5 04112/06 08:45:46 1.1 0.5 0.3 99.6 0411V06 08:45:56 1.1 0.5 0.2 99.6 0412/06 08:46:08 1.1 0.4 0.3 99.6 04/12106 08:46:16 1.1 0.3 0.3 99.7 04112/06 08:46:26 1.1 0.3 0.3 

### 99.8 04/12106 08:46:36 1.1 0.3 0.3 

### 99.8 100 ppm 

### S02 04/12l06 08:46:46 1.0 0.5 0.3 

### 99.8 04/12/06 08:46:56 1.1 0.4 0.3 99.8 041 12106 08:47:05 1.0 0.3 0.3 99.8 04112106 08:47:16 1.0 0.5 0.2 92.4 04112/06 08:47:26 1.1 0.3 0.0 51.7 04112/06 08:47:36 1.1 0.3 0.0 19.7 04112/06 08:47:46 1.1 0.3 0.0 7.3 04/12106 08:47:56 1.1 0.3 0.0 3.3 04/12106 08:48:06 1.1 0.3 0.0 2.0 04/12/06 08:48:16 1.1 0.3 0.0 1.5 04112/06 08:48:26 1.1 0.3 0.0 1.2 04/12106 08:48:36. 1.2 0.2 0.0 1.2 04112/06 08:48:46 1.1 0.2 0.0 1.1 04112/06 08:48:56 1.1 0.3 0.0 1.0 04/12/06 08:49:06 0.4 0.3 0.0 0.9 04!12/06 08:49:16 0.1 0.3 

### 0.4 0.8 04/12/06 08:49:26 0.1 0.2 

### 6.4 0.8 04/12/06 08:49:36 0.1 0.2 13.5 0.9 04112106 08:49:46 0.1 0.1 18.2 0.9 04112106 08:49:56 0.1 0.0 20.8 0.7 04112/06 08:50:06 0.2 -0.1 22.1 0.6 04/12/06 08:50:16 0.2 -0.2 22.7 0.6 04/12/06 08:50:26 0.2 -0.2 23.1 0.5 04/12106 08:50:36 0.2 -0.1 23.2 0.5 04/12/06 08:50:46 0.2 -0.1 23.4 0.5 04/12/06 08:50:56 0.2 -0.2 23.6 0.5 04112/06 08:51:06 0.2 0.0 23.7 0.5 04112106 08:51:16 0.1 -0.1 23.7 0.7 04/12/06 08:51:26 0.2 

### 0.0 23.7 0.7 04/12/06 08:51:36 0.2 

### -0.1 23.7 0.6 25.5 ppm NOx Bias 04/12/06 08:51:46 2.9 

### -0.1 23.8 0.6 Zero CO. S02 Bias 04/12!06 08:51:56 0.1 

### 0.1 

### 23.8 0.6 04/12106 08:52:06 0.1 0.2 23.7 0.6 04112/06 08:52:16 0.1 0.2 23.8 0.6 04112106 08:52:26 0.6 0.2 23.4 0.6 04/12/06 08:52:36 0.2 11.6 22.1 0.5 04/12/06 08:52:46 0.1 82.7 14.2 0.6 04/12/06 08:52:56 0.2 139.4 6.5 0.5 04/12/06 08:53:06 0.1 166.4 3.1 0.5 04/12/06 08:53:16 0.1 178.1 1.7 0.4 04/12/06 08:53:26 0.0 183.4 1.1 0.3 04/12106 08:53:36 0.1 186.0 0.8 0.5 04112/06 08:53:46 0.1 187.7 0.6 0.5 04/12106 08:53:56 0.1 189.0 0.4 0.5 04/12/06 08:54:06 0.1 189.9 0.3 0.6 04/12J06 08:54:16 0.1 190.6 0.2 0.6 04112106 08:54:26 0.1 191.3 0.1 0.5 04/12/06 08:54:36 0.1 191.6 0.1 0.5 04112106 08:54:46 0.1 191.9 0.1 0.5 04112/06 08:54:56 0.1 192.0 0.0 0.5 04/12/06 08:55:06 0.1 192.2 0.1 0.5 04/12/06 08:55:16 0.1 192.3 0.1 0.5 04!12106 08:55:26 0.2 

### 192.5 0.0 0.5 04/12/06 08:55:36 0.2 

### 192.6 0.0 0.5 200 ppm CO Bias 04112/06 08:55:46 0.2 192.7 

### 0.0 0.4 Zero NOx Bias 04/12/06 08:55:56 0.2 

### 193.0 0.0 0.5 04112/06 08:56:06 0.3 190.3 0.0 0.5 04/12/06 08:56:16 0.1 170.8 0.0 0.5 0412/06 08:56:26 0.1 102.1 0.1 0.5 04/12/06 08:56:36 0.1 48.0 0.1 0.8 04/12/06 08:56:46 0.1 24.1 0.0 3.6 04112106 08:56:56 0.1 14.4 0.1 9.9 04112!06 08:57:06 0.1 9.3 0.0 16.6 04/12106 08:57:16 0.1 6.8 0.0 21.8



### Page 3 

# 714112106 Calibrations

04112r06 08:57:26 0.1 5.4 0.0 25.8 041't 2106 08:57:36 0.1 4.5 0.0 29.0 04/12/06 08:57:46 0.1 3.6 0.0 31.5 04/12/06 08:57:56 0.1 2.8 0.0 33.5 04/12/06 08:58:06 0.1 2.2 0.0 35.1 04112106 08:58:16 0.0 2.0 0.0 36.4 04/12/06 08:58:26 0.0 1.6 0.0 37.8 04112/06 08:58:36 0.0 1.2 0.0 38.7 C

~ /12106 08:58:46 0.0 1.0 0.0 38.5 04112106 08:58:56 0.1 0.9 0.0 40.3 04112/06 08:59:06 0.1 0.7 0.0 41.1 04/12/06 08:59:16 0.2 0.5 0.0 41.7 04112/06 08:59:26 0.1 0.4 0.0 42.2 04l12/06 08:59:36 0.2 0.4 0.0 42.6 04112/06 08:59:46 0.1 0.5 0.0 43.0 04112/06 08:59:56 0.1 0.3 0.0 43.5 04112/06 09:00:06 0.0 0.3 0.0 43.9 04112/06 09:00:16 0.1 0.2 0.0 44.2 04l12/06 09:00:26 0.1 0.1 0.0 44.6 04112/06 09:00:36 0.1 0.1 0.0 45.0 04112/06 09:00:46 0.1 0.2 0.0 45.2 04/12/06 09:00:56 0.1 0.1 0.0 45.3 04/12I06 09:01:06 0.2 0.1 0.0 45.5 04112/06 09:01:16 0.1 0.1 0.0 45.7 04/12106 09:01:26 0.1 0.2 0.0 45.8

1
. 1 4112106 09:01:36 0.1 0.2 0.0 45.8 04/12/06 09:01:46 0.1 0.2 0.0 45.9 04/12106 09:01:56 0.0 0.3 0.0 46.0 04/12/06 09:02:06 0.0 0.3 0.0 46.1 04112/06 09:02:16 0.1 0.2 0.0 462 04/12106 09:02:26 0.1 0.2 0.0 46.3 04/12106 09:02:36 0.1 0.1 0.0 46.4 04/12106 09:02:46 0.0 0.1 0.0 46.4 04f12106 09:02:56 0.1 0.0 0.0 46.5 04/12/06 09:03:06 0.1 -0.3 0.0 46.7 49.8 ppm S02 Bias 04/12/06 09:03:16 0.1 -0.1 0.0 46.7 04112/06 09:03:26 0.1 -0.1 0.0 46.6 - 04/12106 09:03:36 0.5 -0.1 0.0 46.1 04/12/06 09:03:46 119 0.1 0.0 45.3 04/12/06 09:03:56 2.2 0.1 0.0 44.1 04/12J06 09:04:06 2.2 0.2 0.0 42.7 04112106 09:04:16 2.2 0.3 0.0 39.9 04712106 09:04:26 0.4 0.3 0.0 35.3 04112/06 09:04:36 0.0 0.4 0.0 30.2 04112/06 09:04:46 0.0 0.3 0.0 25.2 04/12/06 09:04:56 0.1 0.2 0.0 20.9 Zero Air 04/12/06 09:05:06 0.1 0.3 0.0 17.3 04/12106 09:05:16 0.1 0.3 0.0 14.6 04112106 09:05:26 0.1 0.2 0.0 12.7 04112/06 09:05:36 0.3 0.3 0.0 11.1 04/12/06 09:05:46 0.5 0.3 -0.1 10.0 04112/06 09:05:56 1.3 0.4 0.0 8.9 04J12l06 09:06:06 2.2 0.3 0.0 8.0 04112J06 09:06:16 2.2 0.5 0.0 7.4 04/12/06 09:06:26 4.0 0.5 0.0 7.0 04/12/06 09:06:36 37.4 0.5 0.0 6.9 04/12/06 09:06:46 40.1 0.4 0.0 6.9 04/12/06 09:06:56 40.1 0.4 0.0 6.6 04/12106 09:07:06 40.1 0.3 0.0 6.3 04112106 09:07:16 40.1 0.3 0.0 5.7 04/12/06 09:07:26 40.8 0.3 0.0 5.3 04112/06 09:07:36 40.9 0.3 0.0 5.0 04/12/06 09:07:46 40.9 0.3 0.0 4.6 04/12106 09:07:56 40.9 0.3 0.1 4.4 40.8 ppm CH4 04/12106 09:08:06 41.0 0.4 0.0 4.0 04112/06 09:08:16 

## 41 .0 0.5 0.0 3.7 04112/06 09:08:26 40.3 0.3 0.0 3.6 04/12/06 09:08:36 33.1 0.3 0.0 3.5 04/12l06 09:08:46 31.3 0.3 0.0 3.5 04/12/06 09:08:56 10.5 0.3 0.0 3.4 04/12/06 09:09:06 2.6 0.3 0.0 3.2 

# 72 Pape 44112106 Caiibratlans

04112/06 09:09:16 4.3 0.4 0.0 3.0 04/12/06 09:09:26 18.6 0.3 0.0 3.0 04112106 09:09:36 19.2 0.2 0.0 2.9 04112I06 09:09:46 

### 19.2 0.2 0.0 3.0 '19.9 ppin CHy 04/12/06 09:09:56 

### 19.1 0.1 0.0 3.1 04/12/06 09:10:06 

### 19.1 0.1 0.0 3.1 04/12/06 09:10:16 19.1 0.2 0.0 2.9 04112l06 09:10:26 17.7 0.3 0.0 2.8 04112/06 09:10:36 15.1 0:3 0.0 2.8 04112/06 09:10:46 13.1 0.3 0.0 2.7 04/12/06 09:10:56 2.6 0.3 0.0 2.6 04/12106 09:1 1:06 2.8 0.4 0.0 2.4 04/12106 09:1 'i :16 2.5 0.5 0.0 2.3 04/12106 09:11:26 2.5 0.4 0.0 2.5 04l12/06 09:11:36 2.6 

### 0.4 0.0 2.4 04l12/06 09:11:46 23.1 

### 0.4 0.0 2.4 04/12106 09:11:56 62.2 0.4 0.1 2.5 04/12106 09:12:06 62.6 0.3 0.1 2.5 04/12106 09:12:16 62.6 0.3 0.0 2.5 04/12/06 09:12:26 

### 62.7 0.3 0.0 2.5 04/12l06 09:12:36 

### 62.9 0.3 0.0 2.4 61.7 ppm CH4 04112/06 09:12:46 

### 62.9 0.2 0.9 2.3 04/12/06 09:12:56 

### 62.9 0.2 0.0 2.2 04112106 09:13:06 57.6 0.3 0.0 2.1 04/12/06 09:13:1 fi 48.4 0.3 0.0 2.0 04/12/06 09:13:26 40.3 0.3 0.0 2.1 04112/06 09:13:36 3.6 0.3 0.0 2.0



# 73 PagQ 5

### 4112106 Run #1

Date/'ffine VOC CO NOx S02 mm/dd/yy hh:mm:ss ppm ppm ppm Ppm 04112106 10:19:51 17.3 167.5 29.0 1.9

Start Run #1 04/12/0610:20:01 17.2 166.9 29.0 2.0 04/12/0610:20:11 17.2 166.9 29.1 2.0 04/12/0610:20:21 17.0 166.6 29.2 1.9 341 12106 10:20:31 16.5 166.2 29.3 1.9 04/12/0610:20:41 16.3 165.5 29.3 1.9 04!12/0610:20:51 15.3 164.7 28.6 1.9 04/12/0610:21:01 16.1 164.3 28.0 2.0 04/12/06 10:21:11 16.1 164.0 28.1 1.9 04/12/0610:21:21 16.5 164.1 28.4 2.0 04/1210610:21:31 16.3 164.2 28.9 1.9 04/12/0610:21:41 15.8 164.2 29.0 1.8 04/12/0610:21:51 15.4 164.0 28.7 1.9 04/12/0610:22:01 15.0 163.3 28.6 2.0 04/12/0610:22:11 14.7 162.3 29.0 2.0 0411210610:22:21 14.6 161.8 28.9 1.9 04/12/0610:22:31 14.9 161.4 28.8 1.9 04/12/0610:22:41 14.3 160.9 29.1 1.9 04112/0610:22:51 13.8 160.3 30.0 1.7 04112/0610:23:01 13.4 160.0 30.2 1.7 04/1210610:23:11 13.0 159.7 29.8 1.8 04 1 12106 10 :23 :21 12.7 159.1 29.3 1.7 0411210610:23:31 12.6 158.5 29.1 1.7 04/1210610:23:41 12.3 158.0 29.0 1.7 04/1210610:23:51 12.1 157.9 29.0 1.7 04/1210610:24:01 12.3 157.8 29.1 1.7 04/12/0610:2411 12.9 157.6 29.1 1.7 04112/0610:24:21 12.8 157.7 29.0 1.7 04/12/0610:24:31 12.9 157.8 28.9 1.6 04/1210610:24:41 12.7 158.0 28.8 1.6 04/12/0610:24:51 12.6 158.2 28.7 1.8 04/12/0610:25:01 12.7 158.3 28.9 1.8 0411 2/06 1 0:25:11 12.9 158.5 28.8 1.8 04112/0610:25:21 12.9 141.2 28.8 1.7 04/12/0610:25:31 12.9 158.7 28.9 1.6 04/12/0610:25:41 12.9 158.5 29.1 1.6 04/12/0610:25:51 12.8 158.6 29.2 1.8 04/12/0610:26:01 12.5 158.4 29.3 1.8 0411210610:26:11 12.3 158.2 29.4 1.7 04/12/0610:26:21 12.3 157.7 29.4 1.7 04112/0610:26:31 12.3 157.5 29.5 1.6 04112/0610:26:41 12.4 157.6 29.5 1.6 04/12/0610:26:51 12.9 157.9 29.6 1.6 04112/0610:27:01 13.5 158.2 29.6 1.6 04/1210610:27:11 13.6 158.7 29.5 1.7 04/1210610:27:21 13.8 160.2 29.5 1.7 04112/0610:27:31 14.5 161.4 29.3 1.8 04112/0610:27:41 14.8 162.6 29.2 1.6 04/12/0610:27:51 15.0 164.3 29.1 1.6 04112/0610:28:01 15.1 165.7 29.1 1.7 0411210610:28:11 15.2 166.8 29.1 1.8 04112/06 10:28:21 15.2 168.1 29.2 1.7 04/12/0610:28:31 15.5 168.9 29.1 1.7 04/12/0610:28:41 15.5 169.9 29.2 1.7 04112/0610:28:51 15.4 170.9 29.1 1.8 04/12l06 10:29;01 15.0 171.1 29.0 1.8 04/12/0610:29:11 14.9 170.9 29.0 1.8 04/12/0610:29:21 14.9 170.7 29.0 1.9 04/12/0610:29:31 14.6 170.5 29.0 1.9 04/12/0610:29:41 14.8 170.0 29.1 1.8 04/12/0610:29:51 15.1 169.5 28.9 1.8 04/12/06 10:30:01 15.2 169.3 28.9 1.8 04112/0610:30:11 15.1 169.3 28.9 1.8 0411210610:30:21 15.3 169.4 29.1 1.8 04/12/0610:30:31 15.3 169.7 29.1 1.8 04112/0610:30:41 15.4 169.9 29.1 1.8 04/12/0610:30:51 15.5 '169.8 29.2 1.7 04/1210610:31:01 15.4 169.8 29.1 1.7 04l12/0610:31:11 15.0 169.9 29.1 1.8 04112/0610:31:21 14.8 169.5 29.1 1.7 

# 74 Page 1

### 4/12106 Run #1

04/12/06 10:31:31 14.3 169.7 29.1 1.7 04/1210610:31:41 14.1 169.4 29.2 1.8 04112106 10:31:51 13.6 169.0 29.3 1.8 04/12/06 10:32:01 '1 3.5 168.6 29.3 1,7 04/1210610:32:11 13.5 168.0 29.2 1.7 0411210610:32:21 13.5 168.0 29.3 . 1.8 04112/0610:32:31 13.7 168.2 29.4 1.9 0411210610:32:41 13.7 168.5 29.4 1.8 0411210610:32:51 13.5 168.7 29.2 1.8 0411210610:33:01 13.5 168.8 29.2 1.7 04/12/0610:33:11 13.3 168.6 29.1 1.7 04112f0610:33:21 13.3 167.7 29.2 1.8 04112/0610:33:31 13.5 167.8 29.2 1.8 04/12/06 10:33:41 13.5 168.1 29.3 1.8 04/1210610:33:51 13.4 168.2 29.4 1.8 04112/0610:34:01 13.6 168.3 29.4 1.9 04112/0610:34:11 13.7 168.5 29.3 1.8 04/1210610:34:21 13.7 168.6 29.1 1.7 0411210610:34:31 13.7 168.6 29.0 1.6 04112/0610:34:41 13.6 168.0 29.1 1.7 04/1210610:34:51 13.5 168.0 29.2 1.7 0411210610:35:01 13.2 168.0 29.3 1.6 04/1210610:35:11 13.0 168.2 29.4 1.7 04/12/0610:35:21 13.2 168.4 29.3 1.7 04112/0610:35:31 13.6 168.2 29.3 1.7 04112/0610:35:41 13.8 168.7 29.2 1.7 04/1210610:35:51 13.7 169.3 29.3 1.7 04112/0610:36:01 13.6 169.8 29.4 1.7 04/1210610:36:11 13.6 170.0 29.5 1.7 0411210610:36:21 13.8 169.9 29.5 1.8 04112/0610:36:31 14.1 169.6 29.4 1.8 04/1210610:36:41 14.2 169.5 29.5 1.8 

### 0411210610:36:51 14.3 169.7 29.4 1.9 0411210610:37:01 14.5 169.9 29.4 1.7 04112l0610:37:11 14.9 170.3 29.4 1.7 0411210610:37:21 14.7 170.4 29.5 1.7 04112106 10:37:31 14.4 171.0 29.5 1.7 04/1210610:37:41 14.3 171.0 29.5 1.6 0411210610:37:51 14.5 170.8 29.6 1.6 04/1210610:38:01 14.3 171.2 29.6 1.6 0411210610:38:11 14.6 171.4 29.6 1.5 04112/0610:38:21 15.4 171.7 29.6 1.5 04l12/0610:38:31 15.7 171.3 29.6 1.5 0411 2106 1 0:38:41 15.9 172.2 29.5 1.6 0411210610:38:51 15.8 172.5 29.7 1.6 04112/0610:39:01 15.8 173.0 29.6 1.6 0411210610:39:11 15.6 173.4 29.6 1.5 04/1210610:39:21 15.6 173.2 29.6 1.6 0411210610:39:31 15.4 173.3 29.6 1.7 04/12/0610:39:41 15.7 173.0 29.6 1.7 04/1210610:39:51 15.6 172.5 29.6 1.7 0411210610:40:01 15.5 171.9 29.7 1.8 04112/0610:40:11 15.5 171.6 29.6 1.7 04/1210610:40:21 15.2 171.3 29.7 1.6 04112/0610:40:31 15.0 170.8 29.7 1.6 04/1210610:40:41 14.8 170.5 29.8 1.7 04112/0610:40:51 14.7 170.2 29.8 1.6 04112/0610:41:01 15.1 170.0 29.8 1.7 0411210610:41:11 15.7 170.1 29.8 1.8 04112106 10:41:21 15.4 170 .2- 29.7 1.7 04/12/06 10:41:31 14.8 170.0 29.8 1.6 04/1210610:41:41 14.4 169.6 29.7 1.7 0411210610:41:51 14.2 169.1 29.4 1.6 04112/0610:42:01 14.1 168.6 29.3 1.6 04112/0610:42:11 14.3 168.6 29.5 1.6 04112/0610A2:21 14.2 168.3 29.5 1.6 04/1210610:42:31 13.9 168.2 29.5 1.5 0411210610:42:41 13.7 168.0 29.5 1.5 04/12/0610:42:51 13.4 167.8 29.6 1.5 04112/0610:43:01 13.1 167.6 29.6 1.5 04/12/0610:43:11 12.8 167.6 29.7 1.6 

### 0419 210610:43:21 12.8 167.4 29.7 1.6 04/1210610:43:31 12.8 167.5 29.7 1.6 04/12/0610:43:41 13.1 167.6 29.7 1.5

Page 2 

# ~ ~4r12i06 Rutl :` .5

0411210610:43:51 13.7 167.6 29.7 1.4 04112/0610:44:01 15.4 167.0 29.7 1.5 04/12/0610:44:11 15.7 166.9 29.7 1.5 04/12J0610:44:21 15.8 168.0 29.7 1.5 04l12/0610:44:31 15.5 168.6 29.6 1.5 04112/0610:44:41 15.4 168.5 29.6 1.5 04/12/0610:44:51 16.0 168.6 29.7 1.5 04/12/0610:45:01 14.5 168.3 29.6 1.5 0411210610:45:11 14.2 167.9 29.7 1.5 04/12/06 10:45:21 14.3 167.5 29.8 1•5 04/12/06 10:45:31 14.3 i 67.5 29.8 1.4 04/12/0610:45:41 14.3 167.8 29.8 1.5 0411210610:4S:51 14.3 168.2 29.8 1.5 0411210610:46:01 14.1 168.7 29.8 1.4 04/12/0610:46:11 14.1 168.8 29.7 1.4 04112/06 10:46:21 14.2 169.1 29.7 1.6 04112/0610:46:31 14.5 169.4 29.7 1.6 04/12/06 10:46:41 14.6 170.1 29.6 1.5 0411210610:46:51 15.0 170.6 29.4 1.4 04/12/0610:47:01 15.8 171.9 29.4 1.5 04/12/06 10:47:11 16.5 173.7 29.3 1.4 04112/0610:47:21 17.2 175.0 29.2 1.3 04/1210610:47:31 17.1 175.4 29.2 1.4 04112/0610:47:41 17.1 175.4 29.4 1.5 0411210610:47:51 17.0 175.3 29.5 1.5 04112/06 10:48:01 16.7 175.1 29.6 1.5 04112/0610:48:11 16.4 174.0 29.6 1.4 04/12/0610:48:21 15.8 172.7 29.4 1.4 04112/0610:48:31 15.5 170.0 29.5 1.4 04112/0610:48:41 15.0 166.0 29.4 1.4 04/1210610:48:51 14.4 160.0 29.5 1.3 04/1210610:49:01 14.1 153.2 29.6 1.3 04/12/0610:49:11 13.8 144.5 29.7 1.3 04l12/0610:49:21 13.6 136.4 29.9 1.3 04/1210610:49:31 14.0 128.1 30.2 1.3 04/12l0610:49:41 14.5 121.8 30.4 1.4 04/12/0610:49:51 14.5 114.7 30.7 1.4 04/1 2106 10:50:01 14.4 108.6 31.0 1.3 0 4/ 12/06 10: 50:11 14.0 104.1 31.3 1.3 04/12/0610:50:21 13.4 99.7 31.6 1.2 04/12/0610:50:31 12.8 96.4 31.8 1.2 04/12/0610:50:41 12.3 94.1 32.0 1.1 0411210610:50:51 12.3 92.1 32.0 'I.1 04/12/06 10:51:01 12.4 90.1 32.3 1.1 04/12/06 10:51:11 12.6 88.6 32.4 1.1 04112/0610:51:21 12.9 88.1 32.6 1.2 04112/0610:51:31 12.6 87.7 32.5 1.2 0411210610:51:41 12.1 87.8 32.5 1.2 04/1210610:51:51 11.9 88.5 32.3 1.2 04/1210610:52:01 11.7 90.9 31.8 1.1 04112/0610:52:11 11.5 94.6 31.3 1.1 04/12/0610:52:21 11.6 98.4 30.9 1.2 04112l0610:52:31 11.6 101.3 30.8 1.2 04112J0610:52:41 11.6 103.4 30.8 1.2 04J1210610:52:51 11.5 103.8 31.0 1.2 04112106 10:53:01 11.5 101.6 31.0 1.3 04/12/0610:53:11 11.2 98.1 31.2 1.3 0411210610:53:21 10.8 95.4 31.2 1.3 04/12/0610:53:31 10.7 95.0 30.9 1.1 04/12/0610:53:41 10.8 97.1 30.3 1.0 04/12I0610:53:51 11.2 100.9 29.9 1.0 04/12lO6 10:54:01 11.2 105.4 29.4 1.1 04/12/0610:54:11 11.1 110.7 28.9 1.2 04112/0610:54:21 10.9 115.9 28.6 1.2 04112/0610:54:31 10.7 120.6 28.3 1.2 0411210610:54:41 10.6 125.7 28.1 1.2 04112/0610:54:51 10.8 131.1 27.9 1.2 04/12/0610:55:01 10.9 135.4 27.8 1.3 04/12/06 10:55:11 11.6 139.1 27.6 1.2 04112/06 10:55:21 12.2 141.4 27.5 1.3 04/12106 10:55:31 12.2 144.1 27.5 1.3 04112/0610:55:41 12.6 146.2 27.3 1.3 04/12/0610:55:51 12.6 148.7 27.2 1.4 0411210610:56:01 12.9 150.9 27.1 1.3



### Page 3 

# 764112108 Run #1

04112/0610:56:11 13.1 153.3 27.1 1.2 04/12/06 10:56:21 13.3 156.1 27.1 1.1 0411210610:56:31 13.6 157.9 27.1 1.1 04112f0610:56:41 13.7 158.7 27.1 1.1 0411210610:56:51 13.8 159.5 27.1 1.1 0411210610:57:01 14.0 160.2 27.1 1.1 04/1210610:57:11 13.7 159.4 27.1 1.1 04/1210610:5721 13.6 158.9 27.1 1.2 0411210610:5731 13.5 158.8 27.1 1.3 04/12/0610:57:41 13.7 159.0 27.3 1.2 04!1210610:57:51 13.9 159.3 27.2 1.2 04!12f06 10:58:01 15.0 159.3 27.4 1.2 04;12106 10:58:11 16.4 159.3 27.4 1.2 04112/0610:58:21 17.0 159.4 27.5 1.2 04112/0610:58:31 17.2 159.2 27.6 1.1 04112/0610:58:41 17.2 158.6 27.6 1.1 04/1210610:58:51 16.8 157.9 27.7 1.2 04112/0610:59:01 16.3 157.4 27.6 1.2 04112/0610:59:11 15.6 157.7 27.5 1.1 04/12/0610:59:21 15.1 1S8.0 27.1 1.2 04/12/0610:59:31 14.7 158.0 27.2 1.2 04/1210610:59:41 14.3 158.0 27.4 1.1 04/1210610:59:51 13.7 158.2 27.6 1.1 04/12/06 11:00:01 13.1 158.1 27.7 1.2 04/12/0611:00:11 12.4 158.0 27.9 1.2 04112/0611:00:21 12.2 157.7 27.9 1.2 04112/0611:00:31 12.2 157.3 27.8 1.2 04112/0611:00:41 12.2 157.3 27.7 1.2 04/1210611:00:51 12.4 157.2 27.7 1.2 04/12/06 11:01:01 12.3 157.1 27.8 1.1 04/12l0611:01:11 12.2 155.9 28.1 1.2 04112/0611:01:21 12.1 154.9 28.5 1.2 04112/0611:01:31 12.1 154.3 28.7 1.2 04/12/06 11:01:41 11.9 154.6 28.7 1.1 04112/0611:01:51 11.5 154.9 28.6 1.1 04112/06 11:02:01 11.4 155.1 28.5 1.1 04112/06 11:02:11 11.7 155.1 28.5 1.2 04/1210611:02:21 11.7 154.9 28.4 1.1 04/1210611:02:31 11.6 155.4 28.3 1.0 04/12/0611:02:41 11.5 155.6 28.1 1.1 0411 2106 1 1:02:51 11.3 155.8 28.2 1.2 04/12/0611:03:01 11.1 155.7 28.1 1.2 0411210611:03:11 11.0 155.4 28.1 1.1 04/1210611:03:21 11.2 155.3 27.9 1.1 04/12/06 11:03:31 11.4 155.1 28.0 1.1 04/1210611:03:41 12.4 154.7 28.0 1.1 04/12/0611:03:51 13.1 155.0 28.0 1.1 04/1210611:04:01 13.5 155.5 28.0 1.1 04/12/0611:04:11 13.6 155.8 28.0 1.1 0411 2/06 1 1:0421 13.6 156.4 28.0 1.1 04/12/0611:04:31 13.7 156.6 27.8 1.1 04/1210611:04:41 13.9 157.3 27.8 1.0 0411210611:04:51 14.0 157.7 27.8 1.0 04112/0611:05:01 14.1 157.8 27.9 0.9 0411210611:05:11 14.3 157.7 27.9 0.9 04112/0611:05:21 14.3 157.7 27.9 1.0 04/1210611:05:31 14.1 157.6 27.8 1.0 04/12/0611:05:41 13.9 157.6 27.8 1.0 04/12/0611:05:51 13.7 157.5 27.8 1.1 04/1210611:06:01 13.8 157.4 27.8 1.1 04/1210611:06:11 14.0 157.2 27.8 1.1 04112/0611:06:21 14.1 157.0 27.9 1.0 04112/0611:06:31 14.8 157.0 27.8 0.9 04112/06 11:06:41 15.3 157.1 27.7 1.0 04/12/0611:06:51 15.2 157.5 27.6 1.0 04/1210611:07:01 15.5 157.6 27.6 0.9 04112/0611:07:11 15.6 157.7 27.4 0.8 0411210611:07:21 15.1 157.7 27.3 0.9 04/1210611:07:31 14.9 158.0 26.9 1.0 0411210611:07:41 15.1 158.3 26.5 1.0 04/1210611:07:51 15.4 159.2 26.2 0.9 0411210611:08:01 15.3 160.2 26.1 0.9 04/1210611:08:11 15.0 161.0 26.0 0.9 04/12106 11:08:21 14.7 161.2 25.9 1.0



### Page 4 

# 77

### 4112106 Run #1

0411210611:0831 14.1 161.3 25.8 1.0 04/12106 11:08:41 13.7 161.1 25.6 1.0 04/12/0611:08:51 13.4 160.8 25.6 1.0 04112/0611:09:01 12.9 160.7 25.6 0.9 04112/0611:09:11 12.8 160.3 25.5 1.0 04112106 11:09:21 13.4 161.2 25.6 1.0 04/1210611:09:31 13.6 162.2 25.4 0.9 04/12/0611:09:41 13.6 163.5 25.4 0.8 04/1210611:09:51 13.6 164.3 25.5 0.8 04112/0611:10:01 13.5 164.7 25.5 0.9 04112/0611:10:11 13.1 157.3 25.3 0.7 04/12/0611:10:21 13.4 165.9 25.3 0.6 04112/0611:10:31 13.4 166.0 25.3 0.7 04112/0611:10:41 13.4 166.2 25.2 0.7 04/12/0611:10:51 13.4 166.3 25.2 0.8 04/12/0611:11:01 13.5 166.5 25.1 0.8 04/12/0611:11:11 13.2 166.7 25.1 0.8 04112106 11:11:21 12.9 166.7 25.1 0.9 04112l0611:11:31 12.4 166.5 25.1 0.9 04/12f0611:11:41 12.4 166.4 25.0 0.9 04112/0611:11:51 12.4 166.2 24.9 0.9 04/12/0611:12:01 12.6 165.9 24.8 0.8 0411210611:12:11 13.2 165.8 24.7 0.8 04/12/0611:12:21 13.4 166.3 24.9 0.8 04/12/0611:12:31 13.5 166.6 25.1 0.8 0411210611:12:41 13.4 167.2 25.3 0.7 04/1210611:12:51 13.5 168.3 25.7 0.7 0411210611:13:01 13.6 168.6 26.1 0.7 04/12/0611:13:11 14.0 168.1 26.6 0.7 0411 2106 1 1:13:21 14.2 167.2 27.3 0.8 04/12/0611:13:31 14.2 166.1 27.8 0.9 04/12/0611:13:41 14.2 164.8 28.1 0.9 04/1210611:13:51 14.1 163.2 28.3 0.8 04112/0611:14:01 13.7 161.4 28.5 0.8 04112/0611:14:11 13.5 160.0 28.4 0.8 04/12/0611:14:21 13.5 159.0 28.1 0.8 04/12/0611:14:31 13.5 158.5 28.1 0.8 04/1210611:14:41 13.6 158.2 28.2 0.9 04/12/06 11:14:51 13.6 157.8 28.4 0.9 04/12/0611:15:01 13.9 157.8 28.5 0.7 04/1210611:15:11 14.5 158.0 28.4 0.7 0411210611:15:21 14.5 158.0 28.5 0.6 04112/0611:15:31 14.2 158.2 28.5 0.7 04/12/0611:15:41 14.3 .157.8 28.7 0.7 04/12/0611:15:51 13.9 157.2 28.8 0.7 0411210611:16:01 13.9 156.2 28.7 0.7 04112/0611:16:11 14.1 155.4 28.6 0.6 04/1 2106 1 1:16:21 14.2 155.2 28.6 0.6 04/12/0611:16:31 14.5 155.2 28.5 0.6 04/12/0611:16:41 14.7 155.6 28.3 0.7 04/12/0611:16:51 14.7 155.9 28.0 0.7 04/12/0611:17:01 14.3 156.1 27.6 0.6 04/1210611:17:11 13.9 156.1 27.5 0.5 04112100" 11:17:21 13.9 155.7 27.6 0.5 04/12/0611:17:31 13.6 155.3 27.7 0.6 04/1210611:17:41 13.6 155.0 27.7 0.6 04/1210611:17:51 13.9 154.4 27.8 0.6 04112/0611:18:01 14.3 154.6 27.8 0.7 04112/0611:18:11 14.4 155.6 27.9 0.7 0411210611:18:21 14.8 156.3 28.0 0.8 04112/06 11:18:31 15.0 156.8 28.1 0.7 04112/0611:18:41 14.6 157.0 28.2 0.6 04/12/0611:18:51 14.6 156.6 28.3 0.7 04/1210611:19:01 14.5 156.4 28.2 0.6 04/1210611:19:11 14.9 155.8 28.3 0.6 04/1210611:19:21 14.9 156.3 28.4 0.7 04/1210611:19:31 14.6 156.9 28.3 0.7 04/12/0611:19:41 14.1 157.4 28.3 0.5 04112/0611:19:51 13.6 157.1 28.6 0.6 04/12/0611:20:01 13.6 156.7 28.7 0.6 04/12/0611:20:11 13.7 156.3 28.7 0.6 04112/0611:20:21 13.6 157.0 28.7 0.6 0411210611:20:31 13.4 157.0 28.3 0.6 0411210611:20:41 13.7 156.8 28.1 0.6 

# '7 g.
Page 5

### 4112105 Rnn #1

04112/0611:20:51 13.7 157.2 28.3 0.6 04112!06 11:21 :01 13.5 157.8 28.4 0.6 04;12/05 11:21:11 13.3 158.5 28.4 0.5 04.r1210611:21:21 13.4 158.6 28.5 0.5 0411210611:21:31 13.5 158.5 28.4 0.4 04/12/0611:21:41 13.7 158.3 28.4 0.5 04/1210611:21:51 13.9 158.0 28.4 0.5 04/12/0611:22:01 14.3 158.3 28.5 0.5

1 34/1210611:22:11 15.0 158.0 28.4 0.5 04112/0611:22:21 15.8 157.6 28.3 0.4 0411210611:22:31 16.2 157.1 28.2 0.5 04/12/06 11:22:41 15.7 156.7 28.2 0.5 04/12106 1 y:22:51 15.2 155.8 28.2 0.5
Stop Run #1 13.92 157.28 28.63 1.29

04l1210611:23:01 15.0 153.9 28.1 0.6 04/1210611:23:11 14.8 151.1 28.1 0.6 04/1 2106 1 1:23:21 14.8 147.5 28.1 0.5 0411210611:23:31 15.5 144.5 28.1 0.5 04/12/0611:23:41 15.8 142.4 28.2 0.5 0411210611:23:51 15.8 141.5 28.3 0.5 04/12/0611:24:01 16.0 141.2 28.3 0.5 04/1210611:24:11 16.3 141.1 28.2 0.6 04/1210611:24:21 15.9 141.6 28.1 0.6 0411210611:24:31 15.9 141.7 28.1 0.6 04/1210611:24:41 15.5 141.6 28.1 0.5 04/1210611:24:51 15.2 141.4 28.2 0.5 04/12/0611:25:01 15.2 121.9 28.3 0.4 0411210611:25:11 15.4 141.8 28.4 0.4 04/1210611:25:21 5.1 140.4 28.5 0.4 04/12/0611:25:31 3.3 110.0 25.4 0.4 04112/0611:25:41 3.4 62.4 17.0 0.4 0411 2/06 1 1:25:51 3.9 35.6 12.1 0.2 04/12/0611:26:01 3.3 20.6 10.2 0.1 04/12/0611:26:11 3.2 12.6 8.8 0.1 04/1210611:26:21 3.1 7.6 7.5 0.1 0411210611:26:31 3.1 5.0 6.6 0.1 04/12/06 11:26:41 3.1 3.3 7.4 0.1 04/12/06 11:26:51 2.7 2.9 15.2 0.1 04112/0611:27:01 2.2 1.7 20.2 0.1 04112/0611:27:11 1.8 0.7 22.7 0.1 04/12/0611:27:21 1.6 0.3 24.3 0.1 04112/0611:27:31 1.2 0.2 25.3 0.1 04112/0611:27:41 1.2 0.0 26.0 0.1 04112/0611:27:51 1.2 -0.1 25.8 0.1 04/12/0611:28:01 1.3 -0.1 23.2 0.0 04J12/0611:28:11 1.6 -0.2 21.7 0.0 04/12/0611:28:21 2.1 -0.1 20.7 0.0 04/12/06 11:28:31 1.1 10.8 15.4 0.1 04112/0611:28:41 0.9 81.1 8.6 0.1 04112/0611:28:51 1.0 130.1 5.8 0.1 04/1210611:29:01 1.0 155.0 4.6 0.0 04/1210611:29:11 0.7 168.9 3.9 0.0 04112/06 11:29:21 0.5 177.1 3.5 0.0 04112/0611:29:31 0.8 182.7 3.2 0.0 04/1210611:29:41 0.4 186.8 3.0 0.1 04/12/0611:29:51 0.4 189.3 2.7 0.0 0411210611:30:01 0.5 190.8 2.6 0.0 04112/0611:30:11 0.6 191.6 2.4 0.0 04112/0611:30:21 0.6 192.4 2.3 0.0 0411210611:30:31 0.6 192.8 2.2 0.0 04112106 11:30:41 0.6 193.0 2.1 0.0 04/12/06 11:30:51 0.5 193.3 2.1 0.0 04/12/0611:31:01 0.5 

### 193.5 2.0 0.0 04112/06 11:31:11 0.5 193.5 1.9 0.0 200 ppm CO 04112/06 11:31:21 0.5 193.8 1.9 0.0 Zero S02 04/12/06 11:31:31 0.4 193.7 1.8 0.0 04112106 11:31:41 0.5 193.4 1.8 -0.1 04/12/06 11:31:51 0.5 182.1 1.7 0.0 04/12106 11:32:01 0.5 117.9 1.8 0.0 04112/0611:32:11 0.4 64.1 1.7 0.0 04/1210611:32:21 0.3 38.2 2.2 0.0

Page 6 t

~ y

! 9

,

### 4,' 12106 Rurt #1

04/12i0611:32:31 0.3 24.1 3.9 0.5 04112/0611:32:41 0.4 16.1 4.6 3.2 04/1210611:32:51 0.3 10.4 4.0 7.5 04/1210611:33:01 0.3 6.5 3.3 12.3 04/12/0611:33:11 0.4 3.8 2.8 16.7 04I1210611:33:21 0.4 2.2 2.4 20.5 04/12/0611:33:31 0.4 1.0 2.1 23.6 04112/0611:33:41 0.4 0.4 1.9 26:1 04I1210611:33:51 0.4 0.2 1.8 28.3 04112/0611:34:01 

## • 0.4 0.1 1.6 30.2 04/1210611:34:11 0.3 -0.2 1.6 31.8 04/12/0611:34:21 0.4 -0.4 1.6 33.2 04112/0611:34:31 0.4 -0.5 1.5 34.5 04/12/0611:34:41 0.4 -0.6 1.5 35.5 04/1210611:34:51 0.3 -0.6 1.3 36.5 04/12/0611:35:01 0.5 -0.4 1.3 37.4 04/12/0611:35:11 0.3 -0.3 1.3 38.0 04/12/0611:35:21 0.3 -0.4 1.3 38.6 04/12/0611:35:31 0.5 -0.5 1.2 39.2 04/12/0611:35:41 0.4 -0.3 1.1 39.9 04/12/0611:35:51 0.4 -0.4 1.1 40.4 04112/0611:36:01 0.4 -0.4 1.0 41.0 04/12/0611:36:11 0.4 -0.6 1.0 41.4 04/12/0611:36:21 0.3 -0.6 1.0 41.7 04112/0611:36:31 0.3 -0.5 1.0 42.0 04/1210611:36:41 0.4 -0.5 0.9 42.2 04/1210611:36:51 0.4 -0.5 0.8 42.3 04/12/0611:37:01 0.4 -0.5 0.8 42.5 04/12/0611:37:11 0.3 -0.3 0.8 42.8 04/12/0611:37:21 0.3 -0.4 0.8 43.0 04112/0611:37:31 0.3 -0.5 0.7 43.1 04/12/0611:37:41 0.3 -0.5 0.7 43.2 04/12/0611:37:51 0.3 -0.5 0.6 43.3 04/12/0611:38:01 0.3 -0.5 0.6 43.5 04112/0611:38:11 0.2 -0.5 0.6 43.5 04/12/0611:38:21 0.3 -0.3 0.6 43.5 04112/0611:38:31 0.3 -0.3 0.6 44.4 0411210611:38:41 0.3 -0.3 0.6 45.1 04/1210611:38:51 0.3 -0.2 0.6 45.2 04/1210611:39:01 0.4 -0.2 0.6 45.4 04/1210611:39:11 0.2 -0.3 

### 0.5 45.6 04112/0611:39:21 0.3 

### -0.5 0.5 45.6 04/1210611:39:31 0.3 

### -0.5 0.6 45.6 04/12/06 11:39:41 0.2 

### -0.5 0.5 45.6 0411210611:39:51 0.3 -0.5 0.5 45.5 04112/0611:40:01 0.4 -0.6 0.5 45.4 0411210611:40:11 0.5 -0.4 0.5 45.0 04/12/0611:40:21 1.7 -0.3 0.5 44.1 04/12/0611:40:31 2.6 -0.2 0.5 43.2 04/12/0611:40:41 2.6 -0.1 0.5 42.9 04/12/0611:40:51 2.5 -0.2 0.5 42.2 04112/0611:41:01 1.5 -0.2 0.5 40.3 04112/0611:41:11 0.4 -0.3 1.9 37.4 0411210611:41:21 0.5 -0.7 10.6 33.6 04/12/0611:41:31 0.6 -1.0 16.2 29.8 04/12/0611:41:41 0.5 -1.1 19.1 26.3 0411210611:41:51 0.6 -1.0 20.4 23.2 0411210611:42:01 0.6 -1.0 21.3 20.6 0411210611:42:11 0.5 -1.0 22.3 18.3 04/1210611:42:21 0.5 -0.9 22.8 16.5 04/1210611:42:31 0.6 -1.0 23.1 14.4 0411210611:42:41 0.6 -1.0 23.5 12.7 04/1210611:42:51 0.6 -1.0 23.6 11.1 04/1210611:43:01 0.6 -1.2 23.7 9.9 04/12/06 11:43:11 0.5 -1.1 23.7 8.9 04/12/0611:43:21 0.5 -1.1 23.8 7.9 04/12/0611:43:31 0.6 -1.1 

### 23.8 7.3 04112/0611:43:41 0.6 -1.2 

### 23.8 6.7 04/12/0611:43:51 0.6 -1.0 23.8 5.9 04/12/0611:44:01 0.5 -0.7 

### 23.8 5.3 04/12/0611:44:11 0.6 -0.9 23.8 4.9 04/12/0611:44:21 1.0 -0.7 23.6 4.5 49.8 ppm S02 Zero CO, NOx

25.5 ppm NOx

Page 7 

# 80

### 4112/06 Run V1

0411210611:44:31 1.5 -0.7 21.7 4.1 0411210611:44:41 2,7 -0.8 19.4 3.7 04112106 1 1:44:51 2.9 -0.6 13.7 3.5 04112105 '! 1:45:01 2.9 -d.4 6.8 3.3 04112/06 'I 1:45:11 2.6 -0.3 3.4 3.1 04112/06 1 1:45:21 0.6 -0.6 1.9 3.0 04i 12l06 11:45:31 0.5 -0.6 1,3 3,0 04/12/06 11:45:41 0.5 -0.7 1.0 2.9 Zero Air 04112/0611:45:51 0.5 -0.5 0.8 2.7 0411210611:46:01 0.4 -0.5 0.7 2.7 0411210611:46:11 0.5 -0.5 0.6 2.5 04/1210611:46:21 1.0 -0.4 0.6 2.3 04/1210611:46:31 1.1 -0.3 0.5 2.1 04/1210611:46:41 2.5 -0.4 0.5 2.0 04/1210611:46:51 2.8 -0.3 0.4 1.9 04112/0611:47:01 2.8 -0.4 0.4 1.7 0411210611:47:11 2.8 -0.3 0.4 1.6 04/1210611:47:21 14.1 -0.4 0.3 1.5 04/12106 1 1:47:31 20.1 -0.7 0.3 1.6 04/1210611:47:41 20.0 -0.7 0.3 1.6 0411210611:47:51 20.1 -0.9 0.2 1.4 04112lQ6 'I 1:48:01 19.9 -1.0 0.2 1.3 19.9 ppm CH4 04l1210611:48:11 19.9 -1.1 0.2 1.1 0411210611:48:21 20.1 -1.0 0.2 1.1 04/1210611:48:31 19.0 -1.0 0.2 1.0 04l1210611:48:41 15.9 -1.1 0.2 9.0



### Page 8 

# ~ ~4112106 Run #3

Date/T'tme VOC CO NOx S02 

### mmldd/yy hh:mrn:ss ppm ppm ppm ppm 04/12/0612:19:51 12.5 141.0 26.9 -0.1


### Start Run #2 04/12/06 12:20:01 1230 141.1 27.3 -0.2 041121061220:11 12.3 141.2 26.5 -0.3 04112/0612:20:21 12.3 141.2 25.7 -0.4 0411210612:20:31 12.4 141.4 25.8 -0.4 0411210612:20:41 12.4 141.5 26.2 -0.3 0411210612:20:51 12.3 141.4 26.3 -0.2 04/12/06 12:21:01 12.3 141.4 25.5 -0.3 04112/0612:21:11 12.4 141.3 24.8 -0.5 04/1210612:21:21 12.8 141.3 25.0 -0.1 04/1210612:21:31 13.1 141.2 25.6 0.0 04/12/061221:41 13.4 141.3 26.1 0.0 04/1210612:21:51 13.4 141.3 26.5 -0.1 04/12/0612:22:01 13.2 141.3 26.6 -0.1 04112J0612:22:11 12.8 141.2 26.8 0.0 04/1210612:22:21 12.3 141.3 26.5 0.0 04/12/0612:22:31 12.3 141.5 25.7 0.0 04/1210612:22:41 12.7 141.9 25.0 0.0 04/12/0612:22:51 13.3 141.8 25.3 0.0 04/12/0612:23:01 13.5 142.2 26.1 0.0 04112/0612:23:11 13.4 142.7 26.5 0.1 0411210612:23:21 13.1 143.5 26.6 0.0 04/1210612:23:31 13.1 143.7 26.7 0.0 04112/0612:23:41 13.2 143.9 26.9 0.0 04/12/0612:23:51 13.3 144.2 27.2 0.0 04/12/0612:24:01 12.6 144.2 27.5 0.0 0411210612:24:11 12.4 144.7 27.1 0.0 0411210612:24:21 12.7 145.0 26.5 0.0 04112/0612:24:31 12.8 144.9 26.7 0.0 0411210612:24:41 12.5 144.6 27.2 0.0 04/12/0612:24:51 12.3 144.1 27.6 0.0 04112/0612:25:01 12.1 143.8 27.8 0.0 0411210612:25:11 11.7 143.3 28.0 0.0 04112/0612:25:21 11.7 142.8 27.7 0.0 04112/0812:25:31 11.8 142.8 27.3 -0.1 04112/0612:25:41 12.5 142.7 27.5 -0.1 04/1210612:25:51 12.5 142.6 27.9 -0.1 04/12/0612:26:01 12.3 142.4 28.2 -0.1 0411210612:26:11 12.3 142.4 28.6 0.0 04/1210612:26:21 12.7 142.4 28.9 0.0 04112/0612:26:31 12.9 142.4 29.1 0.0 04/12/0612:26:41 12.6 142.4 29.5 -0.1 0411210612:26:51 12.3 142.3 29.7 -0.1 04/1 2/00" 12:27:01 12.1 1412 29.7 -0.1 04/12/0612:27:11 12.1 141.5 29.2 -0.1 04/12/0612:27:21 11.8 ' 141.5 29.0 0.0 04/1210612:27:31 11.6 141.4 29.1 -0.1 04/12/0612:27:41 11.3 141.1 29.4 0.0 04/1210612:27:51 10.7 140.9 29.6 -0.1 04112/0612:28:01 10.5 140.8 29.8 -0.1 04/1210612:28:11 10.5 140.6 29.9 -0.1 0411210812:28:21 10.2 140.6 29.9 -0.1 0411210612:28:31 10.7 140.7 30.0 -0.1 04/12/0612:28:41 10.6 140.4 29.9 -0.1 04/12/0612:28:51 10.5 140.4 29.7 0.0 0411210612:29:01 10.6 140.4 29.3 -0.1 04/1210612:29:11 10.5 140.3 29.3 -0.1 04/12/0612:29:21 10.5 140.2 29.4 -0.1 04/12/0612:29:31 10.6 139.8 29.7 -0.1 04/1210612:29:41 10.6 139.8 29.8 -0.1 04112/0612:29:51 10.6 139.6 30.0 -0.2 04/1210612:30:01 10.6 139.4 30.2 -0.1 04/1210612:30:11 10.6 139.0 30.4 0.0 04/1210612:30:21 10.7 138.8 30.2 -0.1 04/12/06 12:30:31 

## 9 0.5 138.8 29.9 -011 04112/0612:30:41 10.5 138.6 29.8 -0.1 04/12/0612:30:51 10.6 138.4 29.8 -0.2 0411210612:31:01 10.8 137.9 29.9 -0.2 0411210612:31:11 11.2 137.5 30.0 -0.1 0411210612:31:21 11.7 137.8 30.2 -0.1



### Page 1 

# 824112/06 Run #t3

0411210612:31:31 12.2 137.9 30.4 -0.1 04/1210612:31:41 12.2 138.3 30.4 0.0 04/1210612:31:51 12.2 138.4 30.5 0.0 34, 1 12/06 i2:32:01 12.3 138.6 30.7 -0.1 04112106 12:32:11 12.3 138.6 30.8 -0.1 0411210612:32:21 12.3 137.9 30.8 0.0 04/1210612:32:31 12.1 137.6 30.8 -0.1 04/12/0612:32:41 11.8 137.3 30.6 -0.2 04112/0612:32:51 11.7 136.7 30.3 -0.3 0411210612:33:01 11.5 136.1 30.0 -0.2 04112, 1 0612:33:11 11.4 135.1 30.1 -0.2 04112/0612:33:21 11.2 133.5 30.3 -0.1 04112/0612:33:31 11.1 132.0 30.4 -0.1 04112/0612:33:41 10.8 130.9 30.4 0.0 0411210612:33:51 10.8 129.7 30.4 -0.1 04112/0612:34:01 11.2 128.6 30.5 -0.1 04/12/0612:34:11 11.5 127.7 30.8 -0.1 04/12/0612:34:21 11.6 127.7 30.9 -0.2 04112/0612:34:31 10.8 128.0 30.8 -0.1 04112/0612:34:41 11.3 128.4 30.6 -0.1 04112/0612:34:51 11.2 128.4 30.6 -0.2 04/1210612:35:01 11.2 128.5 30.6 -0.2 04112/0612:35:11 11.2 128.4 30.6 -0.1 04/1210612:35:21 11.0 128.4 30.7 -0.1 04112/0612:35:31 10.7 128.7 30.6 -0.2 0411210612:35:41 10.3 128.9 30.6 -0.2 04/1210612:35:51 10.2 128.8 30.5 -0.3 04/12/0612:36:01 9.9 128.7 30.6 -0.3 04112/06 12:36:1 i 9.6 128.4 30.7 -0.3 04112/0612:36:21 9A 128.1 30.5 -0.3 04112/0612:36:31 9.3 127.9 30.4 -0.3 04/1210612:36:41 9.3 127.7 30.5 -0.3 04/1210612:36:51 9.2 127.6 30.7 -0.3 04/1210612:37:01 9.9 127.0 30.7 -0.3 04/12/0612:37:11 9.9 127.8 30.7 -0.2 04/12/0612:37:21 10.0 127.7 30.8 -0.2 04/12/0612:37:31 10.0 127.9 30.9 -0.2 04/1210612:37:41 10.1 127.5 31.0 -0.3 04/1210612:37:51 9.9 127.7 31.1 -0.4 04/12/0612:38:01 9.8 128.0 30.9 -0.3 04112/0612:38:11 9.5 128.3 30.6 -0.2 04112/0612:38:21 9.4 128.4 29.9 -0.3 04112/0612:38:31 9.3 128.0 29.2 -0.4 0411210612:38:41 9.4 127.9 28.8 -0.4 04112/0612:38:51 9.1 127.9 29.0 -0.4 04/12/0612:39:01 8.9 127.9 29.6 -0.4 04/1210612:39:11 8.6 127.8 30.0 -0.4 0411210612:39:21 8.7 127.3 30.4 -0.3 04112/0612:39:31 8.8 127.1 30.4 -0.3 04112/0612:39:41 9.1 126.8 30.6 -0.3 04/12/0612:39:51 9.6 126:7 30.4 -0.2 04/12/0612:40:01 10.0 127.4 30.2 -0.1 04/1210612:40:11 10.4 128.3 30.0 -0.2 0411210612:40:21 10.8 128.4 30.1 -0.1 04/1210612:40:31 11.1 129.1 30.4 -0.2 04112/0612:40:41 11.3 129.4 30.6 -0.2 04/12/0612:40:51 11.6 129.4 30.6 -0.1 04/12/0612:41:01 11.5 129.9 30.7 -0.1 04112/0612:41:11 11.2 129.4 30.9 -0.1 040'12/06 i 2:41:21 10.7 129.0 31.1 0.0 0411210612:41:31 10.7 128.6 31.1 -0.1 04112/0612:41:41 11.1 128.0 31.2 -0.1 04/12/0612:41:51 10.9 128.1 31.2 -0.1 04112/0612:42:01 11.3 127.5 31.0 -0.2 04112/0612:42:11 11.5 126.9 30.6 -0.3 04112/0612:42:21 11.5 127.0 30.4 -0.2 04112/0612:42:31 11.8 127.2 30.6 -0.2 04!1210612:42:41 12.3 127.2 30.7 -0.3 04/1210612:42:51 12.1 127.7 30.8 -0.2 0411210612:43:01 12.2 127.9 30.9 -0.1 04/12/06 12:43:1 i 12.3 128.4 30.9 -0.1 04/12/0612:43:21 12.3 128.6 30.9 -0.1 0411210612:43:31 12.1 128.5 31.0 -0.2 04/1210612:43:41 12.1 128.6 31.0 -0.2

Page 2 C` 

# ~412106 Run #3

04/1210612:43:51 11.7 129.2 30.9 -0.1 04/12/0612:44:01 11.2 129.7 30.9 -0.1 04/12/0612:44:11 11.0 129.6 30.6 -0.1 04112/0612:44:21 11.1 129.8 30.5 -0.1 0411210612:44:31 10.9 130.1 30.4 0.0 0411210612:44:41 10.6 131.0 30.4 -0.1 04112/0612:44:51 10.5 131.9 30.6 -0.1 04/12/0612:45:01 10.3 132.3 30.8 0.0 04112/0612:45:11 10.3 132.6 30.8 0.0 04112/0612:45:21 10.4 132.6 30.8 -0.1 04/12/0612:45:31 10.5 132.3 30.8 0.0 04/1210612:45:41 10.4 132.6 30.7 0.0 04/12/0612:45:51 10.4 132.8 30.7 0.0 04/12/0612:46:01 10.2 132.9 30.7 0.0 0412/0612:46:11 10.2 132.6 30.8 -0.1 04112/0612:46:21 10.3 132.6 30.8 0.0 04/12/0612:46:31 10.4 132.5 30.8 0.0 04/12/0612:46:41 10.3 132.8 30.9 -0.1 0411210612:46:51 10.3 133.1 31.0 0.0 04/12/06 12:47:01 10.3 133.2 31.1 0.0 04112/0612:47:11 10.2 133.6 31.1 0.0 04/12/0612:47:21 10.0 134.0 31.1 -0.1 04/1210612:47:31 9.6 134.3 30.5 0.0 0411210612:47:41 9.4 134.3 30.1 0.0 0411210612:47:51 9.6 134.6 29.9 -0.1 04112/0612:48:01 9.5 135.2 29.7 0.0 04/12/0612:48:11 9.7 135.8 29.9 0.0 04112/06 12:48:21 10.0 136.7 30.0 -0.1 04112/0612:48:31 10.1 138.0 30.3 -0.2 04112/0612:48:41 10.0 138.7 30.5 -0.2 04/12/0612:48:51 10.1 139.3 30.7 -0.1 04/1210612:49:01 10.3 139.4 30.8 -0.1 0411210612:49:11 10.2 138.7 31.1 -0.1 04112/0612:49:21 10.4 137.6 31.2 0.0 04112/0612:49:31 10.6 136.9 31.3 0.0 04/12/0612:49:41 10.6 136.3 31.3 -0.1 04112/0612:49:51 10.6 136.0 31.1 -0.1 0411210612:50:01 10.7 135.9 30.9 -0.1 0411210612:50:11 10.7 135.7 31.0 -0.1 04/1210612:50:21 10.6 135.5 31.1 -0.1 04/12/0612:50:31 10.5 135.2 31.0 -0.1 04112/0612:50:41 10.6 135.1 30.9 -0.1 04112/0612:50:51 10.7 135.1 30.7 -0.1 04/1210612:51:01 10.9 135.6 30.8 -0.1 04/12/0612:51:11 11.4 135.8 30.9 -0.1 04/1210612:51:21 11.5 136.3 31.1 -0.1 04112/061251:31 11.6 136.6 31.2 -0.1 04112/0612:51:41 11.7 136.6 31.2 -0.1 04112/0612:51:51 11.6 136.7 31.3 -0.2 04112/0612:52:01 11.1 136.6 31.2 -0.2 04112/0612:52:11 11.2 136.7 30.9 -0.1 04112/0612:52:21 11.4 137.1 30.6 -0.2 0411210612:52:31 11.3 137.4 30.6 -0.2 04/1210612:52:41 11.3 137.5 30.8 -0.2 04/12/0612:52:51 11.3 137.7 31.0 -0.1 04112/0612:53:01 11.3 137.5 31.0 -0.1 0411210612:53:11 11.2 137.1 31.1 -0.1 04/12106 12:53:21 10.8 136.7 31.1 0.0 04/1210612:53:31 10.8 136.3 31.1 0.0 04/1210612:53:41 10.6 136.3 31.0 0.0 04112/06 12:53:51 10.9 136.4 31.1 0.0 04112/0612:54:01 11.3 136.3 31.1 0.0 04112/06 12:54:11 11.4 136.2 31.1 0.0 04112106 12:54:21 11.3 136.3 31.1 0.0 04/1210612:54:31 11.4 136.3 31.3 0.0 04/1210612:54:41 11.1 136.7 31.4 0.0 04112/0612:54:51 11.3 137.0 31.5 -0.1 04112/0612:55:01 11.1 137.0 31.4 -0.1 04/12/0612:55:11 10.7 136.7 31.3 0.0 04112/06 12:55:21 10.5 137.2 31.1 0.0 0411210612:55:31 10.5 137.5 31.0 0.0 04112/0612:55:41 10.3 138.0 31.0 -0.1 04/1210612:55:51 10.0 137.6 31.1 -0.1 04/1210612:56:01 9.9 137.4 31.1 -0.1

Page 3 ~ 

### •~4,'12/06 Run #3

0411210612:56:11 9.8 137.0 31.1 -0.1 0411210612:56:21 9.8 136.7 31.1 -0.1 04/12106 12:56:31 9.8 136.7 31.0 -0.1 04/1210612:56:41 10.0 136.6 31.1 -0.1 04/1210612:56:51 10.5 136.1 31.1 -0,1 04/1210612:57:01 10.6 136.4 31.1 -0.1 04/1210612:57:11 10.7 136.6 31.1 -0.1 04/12/0612:57:21 10.6 137.0 31.4 -0.1 0411210612:57:31 10.1 137.2 31.4 -0.1 04112106 12:57:41 10.1 136.9 31.0 -0.1 04112/0612:57:51 10.1 136.4 30.7 -0.2 0411210612:58:01 10.0 135.8 30.7 -0.1 0411210612:58:11 10.0 135.1 30.8 -0.2 0411210612:58:21 10.3 134.5 30.9 -0.2 0411210612:58:31 10.3 134.1 30.9 -0.1 04/12/0612:58:41 10.2 134.4 30.7 -0.1 04/12/0612:58:51 10.2 135.2 30.3 -0.1 0411210612:59:01 10.4 136.4 30.1 -0.1 04112I0612:59:11 10.6 138.4 30.2 -0.1 04112/0612:59:21 11.2 140.4 30.3 0.0 04/12/0612:59:31 11.8 141.9 30.2 -0.1 0411210612:59:41 12.6 144.7 30.0 -0.1 0411210612:59:51 12.7 148.6 29.9 -0.2 04/1210613:00:01 12.6 152.8 29.8 -0.2 04/12/0613:00:11 12.8 155.8 29.4 -0.2 04/1210613:00:21 13.5 158.0 29.2 -0.2 04/12/0613:00:31 13.8 158.9 29.2 -0 2 04112J0613:00:41 142 159.1 29.3 -0.2 04/1210613:00:51 14.8 159.7 29.4 -0.1 0411210613:01:01 153 160.7 29.5 -0.1 04/1210613:01:11 15.7 162.4 29.6 -0.1 04112/0613:01:21 15.6 163.8 29.6 0.0 04112/0613:01:31 15.6 166.1 29.5 -0.2 04112/0613:01:41 15.6 167.8 29.6 -0.2 04112/0613:01:51 15.8 169.0 29.6 -0.2 04/1210613:02:01 16.4 170.3 29.6 -0.2 0411210613:02:11 16.5 171.2 29.7 -0.2 04112/0613:02:21 16.2 171.9 29.6 -0.2 04112/0613:02:31 16.3 172.7 29.3 -0.2 04112/0613:02:41 16.5 173.6 29.1 -0.1 04/12/0613:02:51 16.4 174.0 29.0 -0.1 04/12/0613:03:01 16.4 174.4 29.2 -0.1 04/1210613:03:11 16.7 174.8 29.4 -0.1 04/1210613:03:21 16.5 174.7 29.5 -0.1 04/1210613:03:31 16.2 174.7 29.5 -0.2 04/12/0613:03:41 16.3 174.6 29.2 -0.2 0411210613:03:51 16.3 174.3 28.9 -0.1 04/1210613:04:01 16.4 174.3 29.1 -0.1 04112/0613:04:11 16.5 174.2 29.3 -0.1 04112/06 13:04:21 16.3 173.9 29.3 -0.1 04/1210613:04:31 16.0 173.7 29.5 -0.1 04/1210613:04:41 16.0 173.4 29.6 -0.2 04112/0613:04:51 15.8 173.2 29.6 -0.1 0411210613:05:01 16.0 172.9 29.6 -0.1 04/1210613:05:11 16.0 172.6 29.7 -0.1 04/12/0613:05:21 16.0 172.1 29.8 -0.1 04112/0613:05:31 16.2 172.4 29.8 -0.1 04/12/0613:05:41 16.2 172.9 29.7 -0.1 04/1210613:05:51 16.4 173.6 29.8 -0.3 0411210613:06:01 16.7 173.6 29.7 -0.2 04/1210613:06:11 16.7 173.7 29.7 -0.2 04112/0613:06:21 16.8 173.6 29.7 -0.2 04112/0613:06:31 17.0 173.3 29.7 -0.2 04112/0613:06:41 16.9 173.4 29.8 -0.2 04/1210613:06:51 16.7 173.5 29.9 -0.1 04112/0613:07:01 16.3 174.0 29.8 -0.3 04112/0613:07:11 15.5 174.1 29.9 -0.2 04/12/0613:07:21 15.0 173.7 29.8 -0.1 04/1210513:07:31 14.8 173.7 29.9 -0.1 0411210613:07:41 14.3 173.3 29.9 -0.1 04/1210613:07:51 14.3 173.0 29.7 -0.1 04112/0613:08:01 14.8 172.9 29.6 -0.1 0411210613:0$:11 15.3 173.2 29.6 -0.1 04/12/0613:08:21 15.5 173.7 29.7 -0.2

Page 4 

# a4112/06 Rur► #3

04112/0613:08:31 15.8 174.0 29.8 -0.2 04112/0613:08:41 15.9 174.4 29.9 -0.2 0411210613:08:51 15.9 174.5 30.0 -0.2 04/1210613:09:01 16.1 174.5 30.0 -0.3 0411210613:09:11 15.9 174.5 30.0 -0.2 0411210613:09:21 15.8 174.3 30.0 -0.1 04112106 13:09:31 16.1 174.8 30.0 0.0 0411210613:09:41 16.2 175.4 30.0 0.0 04112/0613:09:51 15.6 175.4 29.8 0.0 04/12/0613:10:01 15.4 175.2 29.6 -0.1 04/1210613:10:11 15.0 175.1 29.6 -0.1 04/1210613:10:21 15.3 175.5 29.5 0.0 0411210613:10:31 15.7 175.7 29.5 -0.1 04/1210613:10:41 15.9 175.8 29.7 -0.1 0411210613:10:51 16.4 175.7 29.9 0.0 04112/0613:11:01 16.7 174.8 30.0 0.0 04112/0613:11:11 16.9 173.6 30.1 0.0 04/12/0613:11:21 16.9 172.1 30.2 0.0 04112/0613:11:31 16.8 171.0 30.2 0.0 0411210613:11:41 16.7 170.7 29.9 -0.1 0411210613:11:51 16.5 170.3 29.8 -0.1 04/12/0613:12:01 16.5 170.1 29.7 -0.1 04112/0613:12:11 16.6 169.8 29.6 0.0 04/12/0613:12:21 16.8 169.5 29.7 0.0 04/12/0613:12:31 17.1 170.0 29.8 -0.1 04/12/0613:12:41 16.9 170.6 29.9 -0.1 04/12/0613:12:51 16.6 170.7 30.3 -0.1 04/12/0613:13:01 16.4 170.8 30.3 -0.1 0411210613:13:11 16.5 170.3 30.3 -0.1 0411210613:13:21 16.3 169.9 30.2 0.0 04/12/0613:13:31 16.4 169.8 30.2 0.0 04/12/0613:13:41 16.6 169.4 30.2 -0.1 0411210613:13:51 16.9 169.5 30.2 -0.1 04112/0613:14:01 17.0 170.1 30.1 -0.2 04112/0613:14:11 17.1 170.3 30.2 -0.1 04/12/0613:14:21 16.9 170.1 30.2 0.0 04/12/06 13:14:31 16.6 170.2 30.1 0.0 04/1210613:14:41 16.6 170.4 29.8 0.0 04112J08 13:14:51 16.6 170.5 29.8 -0.1 04/12/0613:15:01 16.8 170.8 29.7 0.0 04112106 13:15:11 16.6 171.8 29.7 0.0 0411210613:15:21 16.5 172.4 30.0 -0.1 0411210613:15:31 16.2 172.7 30.2 -0.1 04112/0613:15:41 15.7 172.3 30.2 0.0 04112/0613:15:51 15.1 172.0 30.3 0.0 04112/0613:16:01 14.6 172.0 30.2 0.0 04112/0613:16:11 14.7 171.7 30.0 0.0 04/12/0613:16:21 14.6 171.5 30.0 0.0 04/12J0613:16:31 15.3 171.3 29.9 0.0 04/1210613:16:41 15.3 171.2 30.0 0.0 04/12/0613:16:51 15.3 171.4 30.1 -0.1 04112/0613:17:01 15.4 171.4 30.0 -0.1 04/1210613:17:11 15.4 171.7 29.9 -0.2 04/12/0613:17:21 15.6 172.1 30.0 -0.2 04/12/0613:17:31 15.6 172.4 30.1 -0.2 0411210613:17:41 15.7 172.5 30.3 -0.1 04112/0613:17:51 15.7 172.8 30.2 -0.1 0411210613:18:01 15.8 172.5 30.3 -0.1 04/12/06 13:18:11 16.0 172.5 30.4 0.0 04/121061318:21 15.6 'l72.6 30.4 0.0 0411210613:18:31 15.3 171.9 30.4 -0.1 04112106 13:18:41 14.7 171.9 30.4 0.0 0411210613:18:51 14.5 171.7 30.1 -0.1 041121061319:01 14.5 171.8 30.0 -0.1 0411210613:19:11 14.9 171.7 30.1 -0.1 04112/0613:19:21 15.4 171.6 30.2 -0.1 04112/0613:19:31 15.7 171.4 30.2 -0.1' 04112/0613:19:41 15.6 171.7 30.3 0.0 04/1210613:19:51 15.4 171.6 30.3 -0.1 04/1210613:20:01 14.9 171.7 30.1 -0.1 04112/0613:20:11 15.1 172.1 30.0 -0.2 04112/0613:20:21 15.6 172.1 30.2 -0.1 04112/0613:20:31 15.8 171.9 30.3 -0.1 0411210613:20:41 15.8 171.8 30.1 -0.1 

# RC) Page 54112/06 Run #3

0411210613:20:51 15.9 172.4 30.1 -0.2 0411210613:21:01 15.9 173.0 30.1 -0.2 04112/06 13:2'I :;1 15.6 173.0 30.2 -0.2 04/1210613:21:21 15.0 172.7 30.2 -0.1 0411210613:21:31 14.9 172.4 30.0 -0.1 04/1210613:21:41 14.9 172.3 29.8 -0.1 0411210613:21:51 15.2 172.3 29.8 -0.1 04112/0613:22:01 15.7 171.8 29.9 -0.2 0411210613:22:11 16.4 171.0 30.0 -0.2 04/1210613:22:21 16.8 170.5 30.1 -0.2 0411210613:22:31 16.9 170.3 30.1 -0.1 0411210613:22:41 16.8 170.5 30.1 -0.1 0411210613:22:51 16.8 170.9 29.9 -0.2
Stop Run 02 12.80 148.67 29.91 -0.12

04112/0613:23:01 16.7 171.3 29.8 -0.2 0411210613:23:11 16.9 171.7 29.9 -0.1 04/1210613:23:21 16.9 171.9 30.0 -0.2 04112/0613:23:31 16.0 171.8 30.0 -0.2 0411210613:23:41 6.6 167.7 29.8 -0.2 0411210613:23:51 3.9 120.5 25.2 -0.2 0411210613:24:01 3.3 66.1 15.7 -0.4 04/1210613:24:11 2.1 37.7 11.0 

### -0.4 04112/0613:24:21 1.5 21.3 8.2 -0.5 0411210613:24:31 1.2 13.9 7.2 -0.5 0411210613:24:41 1.2 7.6 7.3 0.0 0411210613:24:51 1.6 3.0 7.0 1.9 04112106 13:25:01 1.5 13.6 6.2 5.1 04/1210613:25:11 1.1 79.9 5.4 8.3 04/1210613:25:21 0.9 67.2 4.7 10.4 04/12106 13:25:31 1.0 31.0 4.3 12.0 04/12/06 13:25:41 0.9 14.2 4.1 14.3 04l12/0613:25:51 0.9 7.1 3.8 17.2 04/12/0613:26:01 0.7 3.3 3.6 20.1 0411210613:26:11 0.7 1.3 3.5 22.7 04l1210613:26:21 0.9 0.1 3.3 24.9 04112J0613:26:31 0.8 -0.5 3.2 27.1 04112{0613:26:41 0.7 -1.2 3.1 28.9 04112/0613:26:51 0.5 -'1.$ 3.0 30.7 04l12I0613:27:01 0.5 -2.0 2.9 31.9 0417210613:27:11 0.5 -2.1 2.8 33.2 04112/0613:27:21 0.5 -2.3 2.7 34.2 04/12/0613:27:31 0.5 -2.5 2.6 35.1 04/12/0613:27:41 0.6 -2.7 2.5 36.0 04/12l0613:27:51 0.6 -2.7 2.4 36.9 04112/0613:28:01 0.6 -3.0 2.3 37.6 04112l0613:28:11 0.6 -3.1 2.3 38.2 04/1210613:28:21 0.5 -3.2 2.2 38.7 0411210613:28:31 0.7 -3.4 2.1 39.0 04l1210613:28:41 0.6 -3.3 2.1 39.5 04/12/06 13:28:51 0.5 -3.3 2.0 39.9 04112/0613:29:01 0.8 -3.4 1.9 40.3 04/1210613:29:11 0.5 -3.3 1.8 40.8 04/1210613:29:21 0.4 -3.2 1.8 41.3 04112/0613:29:31 0.4 -3.3 1.7 41.5 04/1210613:29:41 0.5 -3.3 1.6 41.9 04/12/0613:29:51 0.5 -3.4 1.5 

### 42.2 04/1210613:30:01 0.5 -3.4 1.5 42.3 04/1210613:30:11 0.5 -3.4 1.5 42.5 04/12/0613:30:21 0.5 -3.5 1.5 42.6 04112/0613:30:31 0.5 -3.6 1.4 42.8 0411210613:30:41 0.5 -3.5 1.4 42.9 04/1210613:30:51 0.5 -3.6 1.3 43.2 0411210613:31:01 0.5 -3.4 1.3 45.2 04/12/0613:31:11 0.5 -3.4 1.2 45.4 04/1210613:31:21 0.6 -3.4 1.2 45.6 0411210613:31:31 0.6 -3.5 1.2 45.7 04/1210613:31:41 0.6 -3.6 1.2 45.8 04112/06 13:31:51 0.6 -3.6 1.1 46.0 0411210613:32:01 0.6 -3.7 1.0 

### 46.0 04112106 13:32:11 0.6 

## -3.7 1.0 

### 46.0 49.8 ppm S02 04/12i06 13:32:21 0.6 

### -3.6 1.0 46.0 Zero CO 

# 87

Page 64112ro6 Rtl , #3

04/1210613:32:31 0.6 -3.7 1.0 46.1 04/12/0613:32:41 0.9 -3.5 1.1 45.7 04/12/06 13:32:51 0.9 13.2 1.1 45.3 04112/0613:33:01 0.9 89.3 1.0 45.1 04112/0613:33:11 0.9 136.9 0.9 43.0 04/1210613:33:21 0.9 159.3 0.8 39.0 04/1210613:33:31 0.9 171.8 0.8 34.4 04112/0613:33:41 0.9 177.9 0.7 30.1 0411210613:33:51 0.7 161.8 0.7 26.4 04112/0613:34:01 0.5 184.1 0.7 23.1 04112/0613:34:11 0.8 186.1 0.7 20.3 04/1210613:34:21 0.9 187.2 0.8 17.8 04112106 13:34:31 0.9 188.0 0.7 15.7 04112106 13:34:41 1.0 188.5 0.7 13.9 04112J0613:34:51 1.0 189.0 0.6 12.3 04/12/0613:35:01 0.8 189.3 0.6 10.9 04112I0613:35:11 0.6 189.6 0.6 9.7 04112/0613:35:21 0. 

### 5 189.8 0.6 8.7 04112/06 13:35:31 0.5 189.9 0.6 7.7 200 ppm CO 04/12/0613:35:41 0.7 189.8 0.6 7.0 Zero NOx 04112/0613:35:51 0.8 189.6 0.6 6.2 04/12/0613:36:01 0.9 189.8 0.5 5.4 04/12/0613:36:11 0.9 190.0 0.5 4.8 04/12/0613:36:21 1.0 183.7 0.5 4.3 04/1210613:36:31 0.9 152.8 1.3 3.6 04/1210613:36:41 0.6 83.4 9.5 3.3 04/1210613:36:51 0.6 42.5 16.5 3.0 04/12/0613:37:01 0.9 23.0 19.6 2.7 04112106 13:37:11 0.9 13.7 21.1 2.5 04/1210613:37:21 0.7 7.5 22.0 2.2 0411210613:37:31 0.7 3.8 22.5 1.9 04112/0613:37:41 0.7 1.8 22.7 1.6 0411210613:37:51 0.6 0.3 23.0 1.5 04/12/0613:38:01 0.6 -0.3 23.1 1.2 04/12/0613:38:11 0.9 -1.1 23.3 1.0 04/12/0613:38:21 0.6 -1.7 23.3 0.8 04112/0613:38:31 0.5 -2.2 23.3 0.7 04/12/0613:38:41 0.6 -2.6 23.4 0.6 04/12/0613:38:51 0.7 -2.9 23.4 0.4 04/1210613:39:01 0.6 -2.9 23.4 0.3 04/12/06 13:39:11 0.6 -2.7 23.4 0.3 25.5 ppm NOx 04112/06 13:39:21 0.8 -3.0 23.5 0.2 Zero VOC 04112/0613:39:31 0.9 -3.0 23.5 0.1 04/1210613:39:41 1.1 -3.1 23.3 0.1 04/12/0613:39:51 1.9 -3.2 21.4 0.1 04112/0613:40:01 2.9 -3.0 19.0 0.0 04/1210613:40:11 2.8 -2.7 12.0 0.0 04/12/0613:40:21 2.8 -2.9 5.8 0.0 04/1210613:40:31 1.2 -3.2 3.0 0.0 04/12l0613:40:41 0.7 -3.3 1.7 0.1 04/12/0613:40:51 0.7 -3.4 1.2 02 04/12/0613:41:01 1.0 -3.5 1.1 0.2 04/12/0613:41:11 1.2 -3.5 0.9 0.1 04112/0613:41:21 2.3 -3.7 0.8 0.1 04/1210613:41:31 2.8 -3.4 0.8 0.1 04/1210613:41:41 2.8 -3.2 0.7 0.1 04/12/0613:41:51 11.8 -2.9 0.7 0.0 04/12/0613:42:01 20.1 -3.0 0.6 0.0 0411210613:42:11 20.2 -3.2 0.5 0.0 04/12106 13:42:21 20.2 -3.4 0.5 0.0 19.9 ppm CH4 04112/0613:42:31 20.2 -3.4 0.5 0.1 04/12/0613:42:41 20.2 -3.4 0.5 0.1 0411210613:42:51 20.2 -3.5 0.4 0.0 04112/0613:43:01 18.1 -3.4 0.4 0.0 0411210613:43:11 16.4 -3.3 0.4 -0.1 04112/0613:43:21 8.7 -3.3 0.3 -0.2 0411210613:43:31 3.0 -3.1 0.3 -0.3 04112/06 13:43:41 2.9 -3.3 0.4 -0.3 Zero S02 04/12/0613:43:51 3.0 -3.2 0.4 -0.2 04/12/0613:44:01 3.0 -3.1 0.4 -0.2



# ~ Page 74112/06 Run 93



### DaSe,Tirne VOC CO NOx S02 mmldd/yy hh:mm:ss ppm ppni pPm ppi

- ii 04/1210613:54:51 15.5 148.4 28.5 -0.5

Start 

### Run #3 0411210613:55:01 15.5 147.8 28.7 -0.5 04/12J0613:55:11 15.4 148.3 28.9 -0.5 04!1210613:55:21 14.8 149.1 29.1 -0.5 3411210613:65:31 14.4 149.8 29.0 -0.4 04112/0613:55:41 14.1 150.3 28.7 0.0 0411210613:55:51 14.0 150.8 28.4 0.0 04112/0613:56:01 13.8 151.2 28.3 0.0 04/12/0613:5611 13.8 151.4 28.6 0.0 04/1210613:56:21 13.9 151.6 28.7 0.0 04/1210613:56:31 13.6 152.1 28.5 -0.1 0411210613:56:41 13.5 152.1 28.0 -0.1 04112/0613:56:51 13.1 152.0 28.0 -0.1 04/1210613:57:01 12.8 151.3 28.0 -0.1 04/1210613:57:11 12.7 150.6 27.9 -0.1 04/12/0613:57:21 12.4 149.8 27.9 -0.1 04/1210613:57:31 12.0 148.9 27.9 -0.1 0411210613:57:41 12.1 148.0 27.7 -0.1 04/12/0613:57:51 12.4 147.6 27.3 -0.1 04112/0613:58:01 12.4 147.2 27.5 -0.2 04/12/0613:58:11 12.2 147.0 27.9 -0.1 04112/0613:58:21 11.7 147.0 28.2 -0.2 0411210613:58:31 11.2 147.0 28.3 -0.3 04112/0613:58:41 11.4 147.3 28.2 -0.2 04/1210613:58:51 11.6 148.1 28.5 -0.2 04/1210613:59:01 11.9 148.6 28.8 -0.2 04l1210613:53:11 12.5 148.8 29.1 -0.2 04/1210613:59:21 12.4 149.5 29.0 -0.2 04112/0613:59:31 12.4 150.2 28.3 -0.2 0411210613:59:41 12.9 150.3 27.8 -0.3 04/12/0613:59:51 13.3 149.7 28.2 -0.2 04112/0614:00:01 13.2 149.1 29.0 -0.2 04112/0614:00:11 13.3 149.0 29.4 -0.2 04/12/0614:00:21 13.4 149.2 29.7 -0.2 04/1210614:00:31 13.5 149.3 29.8 -0.2 04/1210614:00:41 13.2 149.3 29.9 -0.3 04/12/0614:00:51 13.3 149.0 29.8 -0.1 0411210614:01:01 13.3 148.6 30.0 -0.1 0411210614:01:11 13.0 148.3 30.0 -0.1 04112/0614:01:21 12.9 147.5 30.1 -0.1 04112/0614:01:31 12.8 147.1 30.3 -0.2 04112/0614:01:41 12.3 146.6 30.4 -0.2 0411210614:01:51 12.3 145.9 30.3 -0.1 04/12/0614:02:01 13.2 145.8 29.8 0.0 04/12/0614:02:11 13.5 145.8 29.9 0.0 04112/0614:02:21 13.7 146.1 30.2 0.0 04/12/0614:02:31 13.7 145.5 30.5 0.0 04112/0614:02:41 13.5 145.3 30.7 0.0 0411210614:02:51 13.4 145.1 30.6 0.0 0411210614:03:01 13.5 144.5 30.5 0.0 04112/0614:03:11 13.4 144.4 30.5 0.0 0411210614:03:21 13.0 144.0 30.5 0.1 04/12/0614:03:31 12.8 143.9 30.6 0.0 04/1210614:03:41 13.1 143.7 30.4 0.0 04/12/0614:03:51 13.1 143.5 30.5 -0.1 0411210614:04:01 12.8 143.3 30.6 0.0 04112/0614:04:11 12.3 143.0 30.9 0.0 04112/0614:04:21 11.7 142.6 30.9 0.0 0411210614:04:31 11.5 142.7 30.6 0.0 04/1210614:04:41 11.7 142.7 30.2 0.0 0411210614:04:51 12.1 142.6 30.3 -0.1 04112/06 14:05:01 12.4 142.6 30.7 -0.1 0411210614:05:11 12.4 142.7 31.0 0.0 04/1210614:05:21 12.7 142.9 31.3 -0.1 04112/0614:05:31 12.4 143.0 31.5 -0.1 0411210614:05:41 12.3 143.0 31.5 -0.1 0411210614:05:51 12.2 143.0 31.5 -0.1 0411210614:06:01 12.1 142.6 31.5 0.0 04112/0614:06:11 12.1 142.3 31.5 0.0 0411210614:06:21 11.8 142.6 31.5 0.0 

# ®

A Page 14112/0v nun t#3

04112/0614:06:31 11.6 142.8 31.5 0.0 0411210614:06:41 11.1 142.8 31.5 -0.1 04112106 14:06:51 10.8 142.6 31.2 -0.1 04/12/0614:07:01 10.6 142.3 31.2 0.0 04/1210614:07:11 10.5 142.2 31.3 0.0 0411210614:07:21 10.4 142.4 31.4 0.0 04/1210614:07:31 10.6 142.4 31.4 -0.1 04/12/0614:07:41 10.9 142.2 31.5 0.0 04112/0614:07:51 11.3 142.0 31.6 0.0 04112/0614:08:01 11.4 142.3 31.6 0.0 0411210614:08:11 11.4 142.2 31.7 0.0 04112/0614:08:21 11.4 142.5 31.7 -0.1 04/1210614:08:31 11.4 142.7 31.8 0.0 04/1210614:08:41 11.4 142.8 31.8 -0.1 04/12/0614:08:51 11.1 143.1 31.9 -0.1 04/12/0614:09:01 11.0 143.5 31.8 0.0 04/1210614:09:11 11.0 143.6 31.5 0.0 0411210614:09:21 11.2 143.6 31.4 -0.1 04/12/0614:09:31 11.4 143.7 31.5 -0.1 04/12/0614:09:41 11.4 143.5 31.5 -0.1 04/12/0614:09:51 11.3 143.6 31.7 -0.1 04/12J0614:10:01 11.4 143.6 31.8 -0.1 04112/0614:10:11 11.4 143.5 31.8 -0.1 04112106 14:10:21 11.6 143.8 31.8 0.0 04/12/0614:10:31 12A 144.1 31.8 -0.1 04112/06 14:10:41 13.1 143.9 32.0 -0.1 04112106 14:10:51 13.2 144.4 31.8 -0.1 04/1210614:11:01 13.2 144.6 31.8 -0.1 04112/0614:11:11 13.1 144.5 31.8 -0.1 04/12106 14:11:21 13.1 144.1 31.8 -0.1 04112/0614:11:31 12.8 143.7 31.8 0.0 04112/0614:11:41 12.6 143.5 31.8 -0.1 04/12/0614:11:51 12.9 143.4 31.5 -0.1 0411210614:12:01 13.1 143.7 31.4 -0.2 04/1210614:12:11 13.1 144.0 31.5 -0.1 04/12/06 14:12:21 12.7 143.7 31.8 -0.1 04112/0614:12:31 12.3 143.8 32.0 0.0 04112/0614:12:41 11.8 143.5 32.0 0.0 04/1210614:12:51 11.6 143.0 32.0 -0.1 04112/0614:13:01 11.6 142.8 31.9 -0.1 04/12/0614:13:11 11.7 142.6 31.9 -0.2 04/12/0614:13:21 12.2 143.2 32.0 -0.1 04/1210614:13:31 12.9 144.1 32.0 -0.1 04/12/0614:13:41 13.3 144.6 32.2 -0.1 04/12/06 14:13:51 13.4 144.1 31.9 -0.1 04/12/0614:14:01 13.1 143.7 31.7 -0.2 04/1210614:14:11 12.9 143.9 31.6 -0.1 04/1210614:14:21 12.2 144.0 31.7 -0.1 04/12/0614:14:31 12.0 143.6 31.9 -0.1 04/12/0614:14:41 11.4 143.8 31.7 -0.2 04/12/0614:14:51 11.5 143.8 31.3 -0.3 0411210614:15:01 11.5 144.0 31.1 -0.2 0411210614:15:11 11.7 144.2 31.3 -0.2 04112/0614:15:21 11.6 144.5 31.6 -0.1 04112/0614:15:31 11.9 144.3 31.8 -0.1 04/1210614:15:41 12.0 144.1 31.9 -0.1 04/1210614:15:51 12.2 143.7 31.9 -0.1 04112/0614:16:01 12.5 143.8 31.9 0.0 04/12/0614:16:11 12.9 143.6 31.9 0.0 04112/0614:16:21 13.6 143.6 32.0 -0.1 04/12/0614:16:31 13.7 143.7 31.7 -0.2 04112/0614:16:41 13.8 143.7 31.8 -0.1 0411210614:16:51 13.7 144.2 31.9 -0.1 0411210614:17:01 13.6 144.5 32.0 -0.1 04112/0614:17:11 13.4 144.7 32.1 0.0 04/12/0614:17:21 13.3 144.5 32.1 0.0 04/12/0614:17:31 13.0 144.7 32.0 0.0 04112/0614:17:41 12.6 144.8 31.7 -0.1 04/12/06 14:17:51 12.2 145.1 31.7 -0.1 0411210614:18:01 11.9 145.2 31.9 -0.1 0411210614:18:11 11.5 144.9 31.9 -0.1 04112/0614:18:21 11.0 144.5 32.1 -0.1 0411210614:18:31 10.6 143.8 32.2 -0.1 04/12/0614:18:41 10.6 143.3 32.1 -0.2



### Page 2 

# 904112106 Run #3

0411210514:18:51 11.1 143.6 32.0 -0.2 04112/0614:19:01 11.9 144.2 32.0 -0.2 04112/0614:19:11 12.3 144.3 31.7 -0.1 04112J0614:19:21 12.4 144.2 31.5 -0.1 04/12/06 14:19:31 12.4 143.8 31.4 -0.1 04112/0614:19:41 12.1 143.1 31.5 0.0 04/12106 14:19:51 12.0 141.7 31.5 0.0 0411210614:20:01 11.8 140.7 31.5 -0.1 0411210614:20:11 11.8 138.3 31.5 -0.1 0411210614:20:21 11.3 133.6 31.6 -0.1 0411210614:20:31 11.2 126.8 31.7 -0.1 04112/06 14:20:41 11.2 119.5 31.7 0.0 04112/0614:20:51 11.4 111.4 31.8 -0.1 04/1210614:21:01 11.6 104.7 31.9 -0.2 04/1210614:21:11 11.7 100.7 31.9 -0.2 04/1210614:21:21 11.9 98.3 31.7 -0.1 0411210614:21:31 12.2 98.0 31.5 0.0 04/1210614:21:41 12.2 99.8 31.2 -0.1 04/1210614:21:51 12.4 102.8 30.8 -0.1 0411210614:22:01 12.8 106.4 30.2 -0.2 04/1210614:22:11 12.9 111.2 30.0 -0.2 04/12/0614:22:21 13.1 115.7 29.9 -0.2 0411210614:22:31 13.2 120.5 29.9 -0.1 0411210614:22:41 12.6 123.6 30.1 -0.1 0411210614:22:51 13.0 125.6 30.3 -0.1 0411210614:23:01 13.4 127.6 30.4 -0.2 04112/0614:23:11 14.1 129.0 30.7 -0.1 0411210614:23:21 14.3 131.5 30.8 -0.2 0411210614:23:31 14.2 133.3 30.9 -0.2 04/121061423:41 14.6 134.4 31.0 -0.2 04/12/0614:23:51 14.4 136.0 31.1 -0.1 04/1210614:24:01 14.5 137.4 31.1 -0.1 0411210614:24:11 14.5 138.8 31.2 -0.1 0411210614:24:21 14.4 

### 140.2 31.3 -0.1 0411210614:24:31 14.3 141.2 31.4 -0.1 04/1210614:24:41 14.5 142.4 31.4 -0.1 0411210614:24:51 15.3 143.4 31.3 -0.1 0411210614:25:01 15.5 144.6 31.3 0.0 04/12/0614:25:11 15.5 145.8 31.4 -0.1 04/12/0614:25:21 15.4 146.9 31.2 -0.1 04/1210614:25:31 14.9 147.8 31.0 -0.1 0411210614:25:41 15.0 148.4 30.8 -0.1 04112/0614:25:51 14.2 93.0 30.4 -0.2 04112/0614:26:01 14.6 149.3 30.6 -0.1 04112/0614:26:11 14.8 149.7 30.5 -0.1 0411210614:26:21 14.8 149.0 30.3 -0.1 04/1210614:26:31 14.2 149.0 30.1 -0.1 0411210614:26:41 13.9 149.5 29.7 -0.1 04/12/0614:26:51 13.9 150.0 29.5 0.0 04112/0614:27:01 14.0 150.4 29.4 0.0 04/1210814:27:11 10.9 132.8 27.9 -1.3 04/1210614:27:21 17.7 91.8 31.6 1.5 04/12106 14:27:31 17.2 111.5 31.5 1.4 04112f0614:27:41 20.0 161.0 32.7 2.1 04112/0614:27:61 19.7 161.8 32.8 2.1 04112/0614:28:01 19.2 160.6 32.8 2.1 04112/06 1 4:28:11 18.9 158.3 32.8 2.0 0411210614:28:21 13.3 

### 145.3 30.2 -0.1 0411210614:28:31 12.8 141.5 30.3 -0.1 04/1210614:28:41 12.7 138.0 30.3 0.0 04112/0614:28:51 13.1 133.6 30.0 0.0 04/1210614:29:01 13.5 129.5 29.9 0.0 0411210614:29:11 13.7 126.8 30.0 -0.1 04/12/0614:29:21 14.1 124.8 30.3 -0.1 0411210614:29:31 14.3 123.8 30.5 0.0 0411210614:29:41 14.4 123.3 30.5 -0.1 0411210614:29:51 14.7 123.2 30.6 -0.1 04112/0614:30:01 14.8 123.6 30.6 -0.1 04/12/0614:30:11 15.0 124.0 30.5 -0.1 04/1210614:30:21 15.2 124.7 30.4 -0.1 0411210614:30:31 16.0 125.6 30.4 -0.2 04112/0614:30:41 16.4 126.5 30.5 -0.1 04/12/0614:30:51 16.8 127.3 30.7 0.0 0411210614:31:01 17.1 127.9 30.8 -0.1



### Page 3 

# 9 14!12/06 Rur, r,3

04/1210614:31:11 17.1 128.5 30.7 -0.2 04112l0614:31:21 17.0 128.7 30.6 -0.2 0411210614:31:31 16.8 129.0 30.6 -0.3 04112/0614:31:41 16.2 129.6 30.6 -0.2 04112/0614:31:51 16.1 130.1 30.1 -0.2 04/12/0614:32:01 16.2 130.6 30.0 -0.1 04/1210614:32:11 16.5 130.9 30.2 -0.1 04112/06 14:32 21 16.5 131.1 30.5 -0.1 0411210614:3231 16.0 131.2 30.8 -0.1 04112/0614:32:41 15.7 130,9 31.0 -0.1 04/1210614:32:51 15.7 130.5 30.9 -0.1 04112/0614:33:01 15.7 130.2 30.6 -0.2 04/12/0614:33:11 15.8 130.2 30.6 -0.2 04112/0614:33:21 16.4 130.4 30.4 -0.1 0411210614:33:31 16.8 130.8 30.2 -0.1 0411210614:33:41 16.7 131.5 30.3 -0.2 04112/0614:33:51 16.9 131.6 30.2 -0.3 04112/0614:34:01 17.2 131.8 30.1 -0.3 0411210614:34:11 17.2 132.1 29.8 -0.2 0411210614:34:21 17.1 132.2 29.8 -0.1 04/12/0614:34:31 17.0 131.7 29.7 -0.1 04/12/0614:34:41 16.4 131.1 29.6 -0.2 04/12/0614:34:51 15.8 131.0 29.5 -0.1 04/12/0614:35:01 15.5 131.0 29.0 -0.1 04J12/0614:35:11 15.4 131.0 28.7 -0.1 0411210614:35:21 15.2 130.5 26.8 -0.1 04/12/0614:35:31 15.1 130.0 29.0 -0.1 04112/0614:35:41 15.3 129.4 29.2 -0.2 04/1210614:35:51 15.6 129.3 29.3 -0.3 04/1210614:36:01 15.6 129.4 29.6 -0.2 04/1210614:36:11 15.8 129.5 29.6 -0.1 04/12/0614:36:21 16.3 130.0 29.8 -0.1 04/1210614:36:31 16.3 131.2 29.8 -0.2 04112/0614:36:41 16.3 131.9 29.9 -0.2 04/1210614:36:51 16.2 132.5 30.0 -0.2 04/12J0614:37:01 16.0 132.8 30.0 -0.2 04/12/0614:37:11 16.0 133.2 30.0 -0.3 04J12/0614:37:21 15.4 133.2 30.1 -0.3 0411210614:37:31 15.6 133.1 29.8 -0.2 04/12/0614:37:41 15.6 133.4 29.6 -0.3 04/1210614:37:51 15.7 133.6 29.7 -0.1 04/12/0614:38:01 15.6 133.3 29.7 -0.1 04f1210614:38:11 15.5 133.1 29.7 -0.2 04112/0614:38:21 15.7 132.9 29.8 -0.2 04/1210614:38:31 16.0 132.1 29.6 -0.3 04/1210614:38:41 16.3 131.7 29.4 -0.3 04/1210614:38:51 16.4 131.6 29.0 -0.4 04/12/0614:39:01 16.6 131.3 28.7 -0.4 0411210614:39:11 17.1 131.6 28.2 -0.3 0411210614:39:21 17.2 132.5 28.0 -0.3 0411210614:39:31 17.3 133.6 28.0 -0.3 04/1210614:39:41 17.8 134.4 28.0 -0.2 0411210614:39:51 18.0 135.2 28.1 -0.3 04/12/0614:40:01 18.7 135.8 28.2 -0.3 04112/0614:40:11 19.2 136.3 28.3 -0.3 04/12/0614:40:21 19.2 137.2 28.5 -0.2 04/1210614:40:31 19.1 138.5 28.7 -0.1 04/12/0614:40:41 19.1 139.8 28.8 -0.2 04/12/0614:40:51 18.9 140.3 29.1 -0.3 04112/0614:41:01 18.6 140.6 29.4 -0.4 04/1210614:41:11 18.1 140.6 29.6 -0.1 04112/0614:41:21 17.5 140.4 29.7 -0.1 04112/0614:41:31 17.1 140.1 29.8 -0.1 04/1210614:41:41 16.8 139.7 29.6 -0.1 04/1210614:41:51 17.0 139.0 29.6 -0.1 04112/0614:42:01 17.3 138.4 29.8 -0.1 04112/0614:42:11 17.3 138.1 30.2 -0.1 04/12J0614:42:21 17.5 137.3 30.6 -0.1 04112/0614:42:31 17.7 136.8 31.0 -0.1 0411210614:42:41 17.8 136.0 31.2 -0.1 04112/0614:42:51 17.5 135.4 31.3 -0.1 04/12/0614:43:01 17.3 134.9 31.1 -0.1 04/12/0614:43:11 17.1 134.5 30.8 -0.1 0411210614:43:21 16.7 134.6 30.6 -0.1

Page 44i12106 Run 93

04/12/06 14:43:31 16.3 134. 2 30.8 0.0 04/12/0614:43:41 15.9 133.8 30.9 0.0 04/1210614:43:51 15.6 133.1 30.8 0.0 0412/0614:44:01 15.1 132.2 30.8 0.0 04d12/0614:44:11 15.0 131.3 30.7 0.0 0411210614:44:21 15.1 130.9 30.5 0.0 0411210614:44:31 15.4 130.5 30.7 0.0 04112/0614:44:41 15.6 130.1 31.0 -0.1 04112/0614:44:51 161 130.1 31.1 -0.1 0411210614:45:01 15.7 130.3 31.1 -0.1 04112/0614:45:11 14.8 130.8 30.7 0.0 04/1210614:45:21 15.4 131.5 30.1 0.0 04/1210614:45:31 15.5 132.4 29.9 0.0 04/12/0614:45:41 15.8 133.3 30.1 0.0 04112/0614:45:51 16.3 133.9 30.4 0.0 04112/0614:46:01 17.0 134.2 30.8 0.0 04/1210614:46:11 17.0 134.4 30.9 0.0 04/12/0614:46:21 17.0 134.2 30.8 0.0 04112/0614:46:31 17.0 133.8 30.8 0.0 04112J0614:46:41 16.5 133.2 30.6 0.0 04/12/0614:46:51 16.2 132.6 30.5 0.0 04/12/0614:47:01 16.0 131.7 30.4 0.0 0411210614:47:11 16.4 131.4 30.3 -0.1 04112/0614:47:21 16.4 130.9 30.3 -0.1 04112/0614:47:31 16.5 130.7 30.3 -0.1 04;12/0614:47:41 17.2 130.6 30.2 -0.1 0411210614:47:51 17.3 131.5 30.3 0.0 04/12/0614:48:01 17.4 132.6 30.4 0.0 04/1210614:48:11 17.9 133.8 30.3 -0.1 04/1210614:48:21 18.0 134.6 30.3 0.0 04/1210614:48:31 18.0 135.5 30.3 0.0 04/1210614:48:41 18.2 136.1 30.1 -0.1 04112/0614:48:51 18.5 136.7 30.1 -0.2 04/12/0614:49:01 18.4 137.0 30.2 -0.1 04/12/0614:49:11 17.8 137.3 30.1 -0.1 04112/0614:49:21 17.5 137.7 29.6 0.0 04112/0614:49:31 17.4 138.0 29.3 -0.1 04/12/0614:49:41 17.4 137.9 29.5 0.0 04/12/0614:49:51 17.4 137.8 29.8 0.0 04/1210614:50:01 17.6 137.3 29.8 0.0 04/1210614:50:11 17.7 137.1 30.0 -0.1 04112/0614:50:21 17.9 137.0 30.2 -0.1 04/12/0614:50:31 18.5 136.9 30.2 -0.1 04112/0614:50:41 19.1 137,0 30.3 -0.2 04112/0614:50:51 18.7 137.3 30.3 -0.1 04/12/0614:51:01 18.4 137.5 30.2 -0.1 04/12/0614:51:11 18.3 137.3 30.0 -0.1 04/12/0614:51:21 182 136.8 30.0 -0.1 0411210614:51:31 18.4 136.5 30.0 -0.1 04112J0614:51:41 18.3 136.4 30.1 -0.2 04112/0614:51:51 18.3 136.5 30.2 -0.2 04/1210614:52:01 18.3 136.2 30.4 -0.1 04/12/0614:52:11 18.0 135.9 30.5 -0.1 04/12/0614:52:21 17.9 135.7 30.3 0.0 0411210614:52:31 17.7 135.2 30.2 -0.1 04/12/0614:52:41 17.4 134.4 30.2 -0.1 04!1210614:52:51 17.1 134.0 30.4 -0.1 04/1210614:53:01 16.9 133.3 30.5 -0.1 04/12/0614:53:11 16.8 132.5 30.7 -0.1 04/12/0614:53:21 16.8 132.0 30.8 -0.1 04/12/0614:53:31 17.0 131.8 30.6 -0.1 04/1210614:53:41 16.8 132.4 30.3 -0.1 04112/0614:53:51 17.1 133.4 30.0 -0.2 04/1210614:54:01 17.0 133.9 30.3 -0.3 04112/0614:54:11 16.8 134.2 30.5 -0.2 04/12/0614:54:21 16.6 134.6 30.4 -0.2 0411210614:54:31 16.5 134.9 30.4 -0.1 04/12/0614:54:41 16.5 135.1 30.4 -0.1 04/12/0614:64:51 16.5 135.4 30.6 -0.2 04/12/0614:55:01 16.4 135.4 30.7 -0.2 04112/0614:55:11 16.2 135.1 30.9 -0.1 04/12/0614:55:21 16.3 134.5 30.9 0.0 04/1210614:55:31 15.9 133.8 31.0 -0.1 04112/0614:55:41 15.6 133.3 30.9 -0.1

Page 5 `-ti 

# ~4!12106 Run V3

04/12/0614:55:51 15.5 132.8 30.9 -0.2 04/12/0614:56:01 15.7 132.2 30.8 -0.2 04112/0614:56:11 15.9 131.6 30.8 -0.2 04/12/0614:56:21 16.4 131.2 30.9 -0.2 04112/0614:56:31 16.3 131.3 30.9 -0.2 04l12/0614:56:41 16.1 131.1 30.8 -0.2 04/1210614:56:51 16.1 131.1 30.7 -0.1 04112/0614:57:01 16.4 131.0 30.8 -0.1 0411210614:57:11 16.4 130.7 31.1 -0.2 0411210614:57:21 16.6 130.5 31.2 -0.1 04/1210614:57:31 16.7 130.6 31.3 -0.1 04/12/0614:57:41 16.8 131.3 31.3 -0.2 04/12/0614:57:51 16.9 131.8 31.2 -0.1 Stop Run #3 14.61 137.64 30.50 -0.08

04/12/0614:58:01 11.5 131.9 31.0 -0.1 04/12/0614:58:11 5.1 114.6 29.5 -0.2 04/1210614:58:21 4.9 63.7 19.6 -0.3 04/12/0614:58:31 4.2 31.6 12.5 -0.5 04/12/0614:58:41 3.9 16.4 9.4 -0.6 04/12/0614:58:51 5.6 8.1 7.6 -0.6 04/12/0614:59:01 5.4 3.8 6.7 -0.7 04/1210614:59:11 4.3 34.8 6.0 -0.7 04112/0614:59:21 3.3 105.6 5.6 -0.7 0411210614:59:31 2.8 141.4 5.1 -0.8 0411210614:59:41 2.6 162.6 4.5 -0.7 04/1210614:59:51 2.2 173.3 4.1 -0.5 04112/0615:00:01 2.1 177.8 3.9 -0.6 04112/06 15:00:11 2.0 180.7 3.7 -0.6 04/12/0615:00:21 1.9 183.3 3.6 -0.7 04/1210615:00:31 1.9 184.8 3.5 -0.8 04/1210615:00:41 1.9 185.9 3.4 -0.9 04/1210615:00:51 1.7 186.6 3.3 -019 04/12/0615:01:01 1.8 187.1 3.2 -0.8 04112/0615:01:11 1.5 187.4 3.1 -0.8 04112/0615:01:21 1.4 

### 187.4 3.0 -0.8 04l12/06 15:01:31 1.4 

### 187.6 3.0 -0.8 200 ppm CO 04/12106 15:01:41 1.4 

### 187.7 2.8 

### -0.8 Zero S02 04/1210615:01:51 1.3 

### 187.8 2.7 

### -0.8 04/12/0615:02:01 1.3 180.3 2.7 -0.8 04f1210fi 15:02:11 1.2 115.9 2.6 -0.9 04/12/0615:02:21 1.1 56.0 2.8 -0.8 04/12/0615:02:31 1.1 27.3 3.3 0.3 0411210615:02:41 1.0 14.6 3.2 3.9 04112/0615:02:51 1.0 8.7 2.8 8.8 04112/0615:03:01 0.9 4.5 2.6 13.5 04/12/0615:03:11 0.9 1.6 2.5 17.5 04112/0615:03:21 0.9 0.2 2.4 20.8 04/12/0615:03:31 0.9 -0.6 2.3 23.7 04112/0615:03:41 1.0 -1.8 2.2 26.0 04/12106 15:03:51 1.0 -2.6 2.1 27.8 04/12/0615:04:01 0.9 -3.3 2.0 29.4 04/12/0615:04:11 1.0 -3.6 1.9 31.1 04112/0615:04:21 0.8 -3.9 1.9 32.3 04112/0615:04:31 0.9 -4.2 1.8 33.4 0411210615:04:41 1.0 -4.4 1.7 34.6 04/12/0615:04:51 0.9 -4.7 1.7 35.3 0411210615:05:01 1.0 -4.9 1.7 36.1 0411210615:05:11 0.9 -4.9 1.6 36.8 04/1210615:05:21 0.9 -4.9 1.6 37.6 04112/0615:05:31 0.9 -5.0 1.5 38.3 04/12/0615:05:41 0.9 -4.9 1.5 38.8 04/12/0615:05:51 0.9 -5.1 1.5 39.4 04/12/0615:06:01 1.0 -5.3 1.5 39.9 04/12/0615:06:11 1.0 -5.2 1.4 40.5 04/12/0615:06:21 1.0 -5.4 1.4 40.9 04/12/0615:06:31 1.0 -5.1 1.3 41.3 04/1210615:06:41 1.0 -4.9 1.3 41.5 04/1210615:06:51 1.0 -5.1 1.3 41.7 04/12/0615:07:01 1.0 -5.1 1.2 42.0 04/1210615:07:11 0.9 -5.0 1.2 42.2 04112/0615:07:21 0.9 -4.8 1.2 42.3

Page 6 

# 94

### 4/12106 Run #3

04/12/0615:07:31 0.7 -4.8 1.2 42.6 04112/0615:07:41 0.9 -5.0 1.2 42.8 0411210615:07:51 0.9 -4.8 1.2 42.7 04; 12/06 15:08:01 0.7 -4.8 1.1 42.8 04/12/0615:08:11 0.8 -4.7 1.1 43.0 04/1210615:08:21 0.9 -4.9 1.0 43.7 04/1210615:08:31 0.8 -4.8 1.0 44.4 04!1210615:08:41 0.9 -4.9 0.9 44.4 04,12106 15:08:51 1.0 -5.1 0.9 44.5 04!12l0615:09:01 1.0 -5.0 0.9 44.8 04!1210615:09:11 1.0 -4.9 0.8 45.1 0411210615:09:21 1.0 -5.1 0.9 45.3 04112/0615:09:31 0.8 -5.1 0.9 45.4 04112/0615:09:41 0.5 -5.1 0.9 45.4 04112/0615:09:51 0.9 -5.0 0.9 45.4 04/12/06 15:10:01 0.9 -5.0 0.9 45.5 49.8 ppm S02 04/12/06 15:10:11 0.9 -5.1 0.8 45.6 Zero CO, NOx 04/12/06 15:10:21 0.9 -4.7 0.8 45.6 0411210615:10:31 0.9 -4.7 0.8 45.4 04/12/0615:10:41 1.3 -4.6 0.9 44.5 04/1210615:10:51 2.8 -4.7 0.9 43.4 04/12/0615:11:01 2.9 -4.6 0.9 42.8 0411210615:11:11 2.8 -4.6 0.9 42.4 0411210615:11:21 2.0 -4.7 0.9 40.8 04/12/06 1 5:11:31 1.0 -4.8 2.0 37.6 0411210615:11:41 1.0 -4.8 10.4 33.7 04112/0615:11:51 1.0 -5.0 16.5 29.5 04112/0615:12:01 0.9 -5.1 19.6 25.9 0411210615:12:11 1.0 -4.9 20.9 22.7 04/1210615:12:21 1.0 -5.1 21.7 20.0 04/12/0615:12:31 1.1 -5.2 22.3 17.5 04/12/0615:12:41 1.0 -5.0 22.7 15.5 04/1210615:12:51 1.0 -5.1 22.9 13.7 04/1210615:13:01 0.9 -4.8 23.1 12.0 04/12/0615:13:11 0.9 -4.9 23.3 10.6 0411210615:13:21 1.0 -5.1 23.3 9.2 04112/0615:13:31 1.0 -5.3 23.4 8.1 04112/0615:13:41 1.0 -5.4 23.5 7.3 04/12/0615:13:51 1.0 -5.4 23.5 6.5 04/12l0615:14:01 0.9 -5.3 

### 23 .5 5.7 04/12/06 15:14:11 0.8 -5.5 23.5 5.0 25.5 ppni NOx 04/12/06 15:14:21 1.0 -5.4 23.6 4.3 Zero VOC 04112/0615:14:31 0.9 -5.4 23.5 3.8 04112/0615:14:41 1.0 -5.3 23.5 3.5 04/1 2/06 15:14:51 16.7 -5.3 22.7 3.1 04/12/0615:15:01 20.1 -5.2 18.5 2.7 04112/06 15:15:11 20.1 -5.3 9.1 2.4 19.9 ppm CH4 04/12/0615:15:21 20.1 -5.6 4.2 2.0 0411210615:15:31 20.1 -5.5 2.4 1.9 04112/06 15:15:41 20.2 -5.4 1.6 1.7 04112/06 15:15:51 19.9 -5.5 1.2 1.6



## Page 7 ( ~ 

## J

# Jheet i

Summary of CO Analyzer Calibrations and Sia!

~ 

# Plant: Daitile, Muskogee, OK 

# Source: Trim Kiln Date: 4/13/2006



# Analyzer Calibratrion Data Cylinder Anafyzer Absolute % Span Value Response Difference Zero Gas 0 1.53 1.53 0.306 Mid Range 200 200.45 0.45 0.09 High Range 494 491.85 -2.15 -0.43

System Calibration Bias and Drift Data



# Analyzer Initial Values Final Values Cafibration System System System System Response Calibration Calibration Calibration Calibration

Response Bias Response Bias
Run #1 Zero Gas 1.53 0.45 -0.216 1.33 -0.04

Upscale 200.45 195.08 -1.074 195.8 -0.93 Average CO Concentration: 98.81 Corrected CO Concentration: 100.6631 (Equation 6C-1)
Run #2 Zero Gas 1.53 1.33 -0.04 1.58 0.01

Upscale 200.45 195.8 -0.93 193.78 -1.334 Average CO Concentration: 97.94 Corrected CO Concentration: 99.81121 

# (Equation 6C-1)

Run #3 Zero Gas 1.53 1.58 0.01 -1.13 -0.532

Upscale 200.45 193.78 -1.334 192.3 -1.63 

# Average CO Concentration: 94.26 Corrected CO Concentration: 97.53909 (Equation 6C-1) Drift Average Calibration Values

0.176 0.89 0.144 195.44

0.05 1.455 -0.404 194.79

-0.542 0.225 -0.296 193.04



# Page 1 96

# Systenz Calibration Bias and Drift Data Analyzer Initial Values Fina! Values Cafibration System System System System 

# Response Calibration Calibration Calibration Calibration

Response Bias Response Bias

Run #1 Zero Gas -0.12 0.2 0.128 1.58 0.68

Upscale 100.25 93.68 -2.628 94.8 -2.18 Average S02 Concentration: 58.83 Corrected S02 Concentration: 62.06749 (Equation 6C-1)

Run #2 Zero Gas -0.12 1.58 0.68 -0.13 -0.004

Upscale 100.25 94.8 -2.18 94.58 -2.268 Average S02 Concentration: 58.95 Corrected S02 Concentration: 61.96456 (Equation 6C-1)

Run #3 Zero Gas -0.12 -0.13 -0.004 -0.58 -0.184

Upscafe 100.25 94.58 -2.268 93.15 -2.84 Average S02 Concentration: 57.93 Corrected S02 Concentration: 61.86054 (Equation 6C-1) Drift Average Calibration Values

0.552 0.89 0.448 94.24

-0.684 0.725 -0.088 94.69

-0.18 -0.355 -0.572 93.865 Sheetl



# Surnmary of Sulfur Dioxicie Analyzer Calibrations and Bias

Plant: Daltile, Muskogee, OK Source: Trim Kiln Date: 4/13/2006



# Analyzer Calibratrion Data Cylinder Anaiyzer Absolute % Span Value Response Difference Zero Gas 0 -0.12 -0.12 -0.048 Mid Range 100 100.25 0.25 0.1 High Range 250 251.85 1.85 0.74



# Page 1 9 ' 

# ~

# Sheet1

Summary of NOx Analyzer Calibrations and Bias

Plant: Daltile, 

# Muskogee, OK Source: 

# Trim Kiln Date: 

# 4/13/2006



# Analyzer Catibratrion Data Cylinder Analyzer Absolute % Span Vaiue P.esponse Difference Zero Gas 0 0 0 0 Mid Range 25.5 25.1 -0.4 -0.66667 High Range 51 51.73 0.73 1.216667

System Calibration Bias and Drift Data



# Analyzer Initial Va(ues Final Values Drift Cafibration System System System System Response Calibration Calibration Calibration Calibration

Response Bias Response Bias
Run #1 Zero Gas 0 -0.05 -0.08333 0.6 1 1.083333

Upscale 25.2 24.45 

# -1.25 23.98 -2.03333 -0.78333 Average NOx 

# Concentration: 22.66 Corrected NOx Concentration: 23.84367 (Equation 6C-1)

Run #2 Zero Gas 0 0.6 1 0.78 1.3 0.3

Upscate 25.2 23.98 -2.03333 23.7 -2.5 -0.46667 Average NOx Concentration: 21.93 Corrected NOx 

# Concentration: 23.39611 (Equation 6C-1)

Run #3 Zero Gas 0 0.78 1.3 0.7 1.166667 -0.13333

Upscale 25.2 23.7 -2.5 23.35 -3.08333 -0.58333 Average NOx Concentration: 21.57 Corrected NOx Concentration: 23.31205 (Equation 6C-1) Average Calibration Values

0.275 24.215

0.69 23.84

0.74 23.525

Page 1 

# 984.13/06 Caiibrations

Datefl`ime VOC CO NOx S02 mnildd/yy 

### hh:mm:ss pprn ppm ppm ppm 04/13106 08:03:37 2.7 0.4 -0.1 -0.2 04!13106 08:03:47 2.7 0.5 -0.1 

### -0.1 04113106 08:03:57 2.8 0.4 -0.1 

### -0.1 Zero S02 04/13106 08:04:07 2.6 0.3 -0.1 

## -0.1 04/13/06 08:04:17 2.6 0.3 0.0 

### -0.2 04113106 08:04:27 2.7 0.2 0.0 -0.2 04113/06 08:04:37 2.8 0.4 0.0 0.2 04113/06 08:04:47 2.8 0.4 0.2 18.0 04/13!06 08:04:57 2.6 0.5 0.3 65.0 04/13106 08:05:07 2.5 0.9 0.3 91.7 04113106 08:05:17 2.5 0.9 0.4 100.6 04/13106 08:05:27 2.6 1.0 0.4 103.3 04/13/06 08:05:37 2.6 0.7 

### 0.4 104.1 04/13/06 08:05:47 2.7 0.7 0.3 104.7 04113106 08:05:57 2.7 0.7 0.4 105.0 04/13/06 08:06:07 2.7 0.7 0.3 105.1 04/13/06 08:06:17 2.7 0.8 0.3 105.3 04/13106 08:06:27 2.8 0.7 0.2 105.5 04/13/06 08:06:37 2.7 1.0 0.3 102.9 04/13f06 08:06:47 2.7 1.3 0.3 

## 100.3 04113106 08:06:57 2.8 1.1 0.3 

## 100.3 100 ppm S02 04/13106 08:07:07 2.8 1.1 0.3 

### 100.3 04113/06 08:07:17 2.8 1.2 0.3 

## 100.1 04113106 08:07:27 2.7 1.2 0.3 99.9 04/13106 08:07:37 2.6 1.4 0.3 99.8 04113106 08:07:47 2.7 1.5 0.2 99.8 04113/06 08:07:57 2.8 1.6 0.2 99.7 04/13/06 08:08:07 2.8 1.8 0.2 93.1 04/13/06 08:08:17 2.8 1.6 0.0 52.7 04/13/06 08:08:27 2.7 1.5 0.0 19.3 04113106 08:08:37 2.7 1.5 0.0 6.7 04113106 08:08:47 2.9 1.3 0.0 2.6 04/13/06 08:08:57 2.9 0.8 0.2 24.4 04113/06 08:09:07 2.7 1.0 0.5 132.6 04113106 08:09:17 2.8 9.0 0.5 212.1 04/13/06 08:09:27 2.9 12 0.5 240.3 04/13/06 08:09:37 2.7 1.6 0.4 248.0 04/13106 08:09:47 2.7 1.8 0.3 250.2 04113106 08:09:57 2.9 1.8 

### 0.4 251.0 04/13/06 08:10:07 2.7 1.8 

### 0.4 251.3 04/13/06 08:10:17 2.7 1.8 0.4 251.7 04/13/06 08:10:27 2.8 1.4 0.4 

### 251.9 04/13/06 08:10:37 2.8 1.1 0.4 

### 251.8 250 

### ppm S02 04/13/06 08:10:47 2.7 1.1 

### 0.4 251.8 04113/06 08:10:57 2.8 0.9 0.3 

## 231.9 04/13106 08:11:07 2.9 1.2 0.3 233.2 04/13106 08:11:17 2.8 1.1 0.0 127.2 04/13106 08:11:27 2.7 1.0 0.0 45.2 04113/06 08:11:37 2.8 1.0 0.0 14.8 04/13106 08:11:47 2.9 1.2 0.0 5.6 04/13/06 08:11:57 2.9 1.2 0.0 2.8 04113/06 08:12:07 2.9 1.1 0.0 1.8 04/13/06 08:12:17 2.8 1.0 0.0 1.3 04J13/06 08:12:27 3.1 1.0 0.0, 1.1 04113106 0B12:37 3.1 1.1 -01 1.0 04/13/06 08:12:47 3.1 1.0 -0.1 0.9 04/13/06 08:12:57 3.1 1.0 -0.1 0.7 04/13/06 08:13:07 2.0 1.0 -0.1 0.7 04!13106 08:13:17 1.2 0.9 0.6 0.6 04113/06 08:13:27 1.0 0.9 7.6 0.5 04/13/06 08:13:37 0.8 0.7 15.0 0.4 04/13/06 08:13:47 0.6 0.7 19.6 0.4 04113106 08:13:57 0.6 0.7 21.9 0.4 04/13/06 08:14:07 0.5 0.8 22.9 0.4 04/13/06 08:14:17 0.5 0.6 23.4 0.3 04113106 08:14:27 0.5 0.6 -23.8 0.2 04113106 08:14:37 0.6 0.7 24.1 0.3 04/13106 08:14:47 0.6 0.7 24.2 0.3 04/13/06 08:14:57 0.6 0.6 24.3 0.3

Page 1 

# .99413106 Calibrations

04113/06 08:15:07 0.6 0.5 24.4 0.3 04/13/06 08:15:17 0.6 0.4 24.4 0.2 04113106 08:15:27 0.6 0.5 24.5 0.2 04!13/06 08:15:37 0.5 

### 0.4 

### 24.4 0.2 04113106 08:15:47 0.5 

### 0.4 24.5 0.2 04/13/06 08:15:57 0.5 

### 0.5 

## 24.4 0.2 04113/06 08:16:07 0.6 0.4 24.4 0.2 04113/06 08:16:17 0.9 0.5 24.4 0.2 04113106 08:16:27 1.1 4.6 24.3 

### 0.2 04/13106 08:16:37 1.0 64.6 19.3 

### 0.2 04/13/06 08:16:47 1.0 132.5 9.4 0.2 04113/06 08:16:57 1.0 164.9 4.4 0.2 04113106 08:17:07 0.7 178.9 2.3 

### 0.2 04113106 08:17:17 0.5 184.8 1.4 0.2 04/13106 08:1727 0.6 188.1 1.0 0.2 04/13106 08:17:37 0.6 190.2 0.7 0.2 04113/06 08:17:47 0.4 191.7 0.5 0.2 04113106 08:17:57 0.5 192.8 0.3 0.2 04/13106 08:18:07 0.5 193.2 0.3 0.2 04/13106 08:18:17 0.4 193.7 0.1 0.2 04/13106 08:18:27 0.4 193.8 0.1 0.2 04/13J06 08:18:37 0.4 194.2 0.1 0.2 04/13/06 08:18:47 0.4 194.3 0.0 0.2 04/13/06 08:18:57 0.4 194.5 0.0 0.2 04/13106 08:19:07 0.4 194.8 0.0 0.2 04113106 08:19:17 0.5 194.9 

### -0.1 0.2 04/13/06 08:19:27 0.5 195.1 

### -0.1 0.2 04113/06 08:19:37 0.6 

### 195.1 0.0 0.0 04/13/06 08:19:47 O.a 

### 195.2 0.0 0.1 04/13/06 08:19:57 0.6 186.3 0.0 0.0 04/13/06 08:20:07 0.5 118.5 0.2 0.1 04113/06 08:20:17 0.4 57.6 0.3 6.0 04/13/06 08:20:27 0.4 28.3 0.3 23.6 04/13/06 08:20:37 0.5 16.7 0.3 42.3 04/13/06 08:20:47 0.6 11.5 0.3 55.7 04/13/06 08:20:57 0.5 8.7 0.3 64.2 04113/06 08:21:07 0.5 6.6 0.3 69.9 04/13/06 08:21:17 0.4 5.2 0.3 73.8 04113/06 08:21:27 0.3 4.0 0.4 76.4 04/13/06 08:21:37 0.3 3.3 0.4 78.7 04113J06 08:21:47 0.4 2.6 0.4 80.6 04/13/06 08:21:57 0.5 2.1 0.4 82.3 04/13/06 08:22:07 0.6 1.5 0.4 83.6 04/13/06 08:22:17 0.6 1.4 0.4 84.4 04/13/06 08:22:27 0.6 1.3 0.4 85.0 04/13J06 08:22:37 0.5 1.0 0.4 85.8 04/13/06 08:22:47 0.5 0.9 0.4 86.4 04/13106 08:22:57 0.4 0.9 0.4 87.0 04/13106 08:23:07 0.3 0.9 0.4 87.6 04/13/06 08:23:17 0.2 1.0 0.4 88.0 04113/06 08:23:27 0.3 1.2 0.3 88.4 04113106 08:23:37 0.3 1.1 0.3 89.0 04113/06 08:23:47 0.3 1.1 0.3 89.4 04/13/06 08:23:57 0.4 1.2 0.3 89.7 04/13106 08:24:07 0.4 1.2 0.2 90.0 04113106 08:24:17 0.4 1.1 0.3 90.2 04113106 08:24:27 0.4 1.0 0.4 90.6 04113/06 08:24:37 0.3 1.1 0.4 90.9 04/13/06 08:24:47 0.3 1.2 0.3 91.1 04113/06 08:24:57 0.3 1.3 0.3 91.3 04/13/06 08:25:07 0.2 1.3 0.3 91.4 04/13106 08:25:17 0.3 1.3 0.3 91.8 04113/06 08:25:27 0.3 1.2 0.2 91.9 04/13/06 08:25:37 0.4 0.9 0.3 92.0 04113106 08:25:47 0.4 0.9 0.4 92.2 04/13/06 08:25:57 0.4 0.8 0.2 92.3 04/13/06 08:26:07 0.6 0.8 0.2 92.5 04/13/06 08:26:17 0.5 0.7 0.3 92.6 04/13/06 08:26:27 0.4 0.8 0.3 92.8 04113/06 08:26:37 0.3 1.1 0.3 92.9 04/13J06 08:26:47 0.3 1.2 0.3 93.0 04/13/06 08:26:57 0.4 1.2 0.3 93.2 25.5 ppm I , IOx 3ias Zero CO, $02

200 ppm CO Zero 

### NOx

Page 2 

# -t0 04 1 13106 Calibrrations

04/13106 08:27:07 0.4 1.4 0.3 93.3 04113/06 08:27:17 0.6 1.4 0.3 93.5 04113/06 08:27:27 0.6 1.3 0.3 93.5 04/13106 08:27:37 0.5 1.3 0.3 

### 93.6 04113/06 08:27:47 0.5 1.3 0.4 

### 93.8 100 ppm S02 04113/06 08:27:57 0.5 1.1 0.3 

### 93.6 04/13/06 08:28:07 0.9 1.3 0.3 

### 93.7 04113;06 08:28:17 0.6 1.2 0.3 93.5 04113/06 08:28:27 0.5 1.4 0.3 91.1 04113106 08:28:37 0.5 1.5 0.1 77.1 04113l06 08:28:47 0.5 1.3 0.0 54.1 04/13106 08:28:57 0.5 1.5 0.0 34.8 04113106 08:29:07 0.5 1.5 0.0 22.4 04113106 08:29:17 0.4 1.6 0.0 15.4 04/13/06 08:29:27 0.4 1.4 0.0 11.4 04/13106 08:29:37 0.2 1.7 0.0 9.7 04/13/06 08:29:4 7 0.0 1.6 -D.1 8.2 04/13106 08:29:57 

### 0.0 1.6 -0.1 7.0 04/13/06 08:30:07 

### 0.0 1.6 -0.1 6.2 Zero Air 04l1 3/06 08:30:17 

### 0.0 1.6 -0.1 5.7 04/13/06 08:30:27 

### 0.0 1.6 -0.1 5.2 04/13/06 08:30:37 0.1 1.5 -0.1 4.7 04113l06 08:30:47 0.2 1.4 -0.1 

### 4.4 04/13/06 08:30:57 0.2 1.6 -0.1 4.3 04113106 08:31:07 0.8 1.5 -0.1 3.9 04/13/06 08:31:17 2.1 1.6 0.0 3.8 04/13106 08:31:27 2.4 1.7 0.0 4.1 04l13/06 08:31:37 2.6 1.7 0.0 5.0 04113J06 08:31:47 28.9 1.6 0.1 6.3 04/13J06 08:31:57 

### 40.4 1.6 0.0 7.4 04/13/06 08:32:07 40.2 1.5 0.0 7.5 04/13106 08:32:17 4.7 1.3 -0.1 6.8 04/13106 08:32:27 0.0 1.3 0.0 5.6 04113106 08:32:37 0.0 1.0 0.0 4.6 04/13/06 08:32:47 0.0 1.2 0.0 3.9 04/13/06 08:32:57 0.0 1.2 0.0 3.6 04113106 08:33:07 0.1 1.2 0.0 3.6 04/13/06 08:33:17 0.1 1.3 0.0 3.7 04/13/06 08:33:27 0.1 1.3 0.0 4.1 04113106 08:33:37 0.1 1.2 0.0 4.3 04113/06 08:33:47 0.1 1.0 0.0 4.9 04/13/06 08:33:57 0.1 1.0 0.0 5.4 04/13/06 08:34:07 0.1 0.9 0.0 5.8 04/13/06 08:34:17 0.2 0.7 0.0 5.8 04113/06 08:34:27 12.3 ' 0.7 0.0 5.4 04/13/06 08:34:37 0.1 0.9 0.0 4.7 04113106 08:34:47 0.1 1.1 0.0 3.9 04l13/06 08:34:57 0.1 1.0 0.0 3.3 04113106 08:35:07 0.1 1.0 0.0 2.9 04/13/06 08:35:17 0.5 1.1 0.0 2.7 04/13/06 08:35:27 2.1 1.0 0.0 2.5 04113/06 08:35:37 2.3 1.0 0.0 2.3 04/13/06 08:35:47 2.7 0.9 0.0 2.5 04/13/06 08:35:57 27.5 1.0 0.0 2.8 04/13/06 08:36:07 40.0 0.9 0.0 2.9 04/13106 08:36:17 39.9 0.9 0.0 3.0 04/13/06 08:36:27 39.8 0.6 0.0 2.9 04l13/06 08:36:37 39.7 0.8 0.0 2.6 04113/06 08:36:47 40.9 0.8 0.1 

### 2.4 04113/06 08:36:57 41.0 0.9 0.1 2.1 04113/06 08:37:07 40.7 0.9 0.0 1.8 04/13/06 08:37:17 

### 40.9 1.0 0.0 1.8 04/13106 08:37:27 

### 40.7 1.2 0.0 1.6 40.8 ppm CH4 04/13106 08:37:37 

### 40.9 1.5 -0.1 1.5 04/13/06 08:37:47 

### 40.7 1.6 0.0 1.4 04113106 08:37:57 38.3 1.7 0.0 1.4 04113106 08:38:07 27.0 1.8 0.0 1.4 04113106 08:38:17 3.1 1.6 0.0 1.3 04113/06 08:38:27 2.7 1.7 0.0 1.5 04113/06 08:38:37 16.9 1.8 0.0 1.5 04113106 08:38:47 19.2 1.9 0.0 1.6



### Page 3 

# 1.014113106 Calibraifons

04/13/06 08:38:57 19.1 1.6 -0.1 1.7 04113/06 08:39:07 19.0 1.4 0.0 1.8 19.9 ppm CH4 04113106 08:39:17 19.0 1.3 0.1 1.7 04/13106 08:39:27 19.0 1.0 0.1 1.6 04113/06 08:39:37 19.1 1.1 0.0 1.4 04113106 08:39:47 19.1 1.3 0.0 1.3 04/13/06 08:39:57 18.6 1.5 0.0 1.2 04/13/06 08:40:07 16.8 1.4 0.0 1.3 04113/06 08:40:17 4.2 1.3 0.0 1.3 04113106 08:40:27 3.3 1.5 0.0 1.4 04113/06 08:40:37 54.9 1.6 0.0 1.5 04113106 08:40:47 62.4 1.6 0.0 1.6 04113106 08:40:57 62.4 1.5 0.1 1.8 04/13106 08:41:07 62.4 1.5 0.1 1.8 04/13/06 08:41:17 

### 62.3 1.6 0.1 1.7 04/13/06 08:41:27 

### 62.2 1.7 0.1 1.5 61.7 ppm CH4 04113106 08:41:37 

### 62.2 1.7 0.1 1.2 04/13/06 08:41:47 

### 62.1 1.7 0.1 1.2 04/13106 08:41:57 59.4 1.7 0.1 1.2 04/13/OS 08:42:07 49.4 1.7 0.1 1.0 04113/06 08:42:17 5.3 1.7 0.1 1.2 04/13J06 08:42:27 2.8 1.6 0.0 1.4 04/13106 08:42:37 2.8 1.9 0.1 1.5 04113106 08:42:47 2.6 2.0 0.1 1.6 04/13/06 08:42:57 2.6 2.0 0.0 1.6 04113/06 08:43:07 2.7 1.9 0.0 1.7 04113/06 08:43:17 2.6 1.8 0.0 1.9 04113/06 08:43:27 2.7 1.8 0.0 2.0 04/13106 08:43:37 2.7 1.9 0.0 2.4 04/13/06 08:43:47 2.7 1.8 0.0 3.0 04/13/06 08:43:57 2.6 1.8 0.1 3.5 04/13/06 08:44:07 2.8 1.5 0.1 3.7 04113/06 08:44:17 2.9 1.4 0.1 3.8 04113/06 08:44:27 2.9 1.3 0.1 3.8 04/13106 08:44:37 2.8 1.2 

### 0.0 3.5 04/13/06 08:44:47 2.7 1.2 

### 0.0 3.5 Zera NOx Cal 04/13/06 08:44:57 2.9 1.2 

### 0.0 3.5 04113/06 08:45:07 2.8 1.1 

### 0.0 3.3 04113106 08:45:17 2.8 0.8 10.9 3.4 04113106 08:d5:27 2.8 1.0 24.7 2.9 04/13/06 08:45:37 2.8 1.1 24.9 1.9 04/13106 08:45:47 2.9 1.1 25.0 1.3 04/13/06 08:45:57 3.0 

### 1.2 25.1 1.0 04113/06 08:46:07 2.9 

### 1.5 25.1 1.0 25.5 ppm NOx Cal 04/13/06 08:46:17 2.9 1.6 

### 25.1 0.8 Zero CO Cal 04113106 08:46:27 2.7 

### 1.8 25.1 0.9 04/13106 08:46:37 2.6 2.0 8.4 0.9 04/13/06 08:46:47 2.5 1.9 0.0 1.5 04/13106 08:46:57 2.5 1.6 0.0 2.1 04113/06 08:47:07 2.7 1.4 0.5 2.2 04/13/06 08:47:17 2.9 1.4 49.6 1.9 04/13/06 08:47:27 2.8 1.5 51.3 1.3 04/13/06 08:47:37 2.8 1.8 51.5 1.1 04/13/06 08:47:47 2.7 1.8 51.6 0.9 04/13/06 08:47:57 2.7 1.9 

### 51.7 0.9 04/13/06 08:48:07 2.7 2.0 51.7 0.9 51.0 ppm NOx Cal 04/13106 08:48:17 2.6 2.0 

### 51.7 0.9 04/13/06 08:48:27 2.5 1.9 51.8 0.7 04/13106 08:48:37 2.5 1.9 26.6 0.7 04/13/06 08:48:47 2.4 2.0 0.1 1.0 04113106 08:48:57 2.6 1.2 0.0 1.4 04/13106 08:49:07 2.7 0.9 0.0 1.5 04113106 08:49:17 2.6 2.0 -0.1 1.5 04/13106 08:49:27 2.5 141.4 -0.1 1.5 04/13/06 08:49:37 2.6 198.8 0.0 1.3 04/13/06 08:49:47 2.5 199.5 -0.1 1.0 04/13/06 08:49:57 2.4 199.9 0.0 0.9 04/13106 08:50:07 2.4 200.2 0.0 0.9 04/13/06 08:50:17 2.4 

### 200.1 0.0 0.8 

# 1. 0.2
Page 4

### 4113/0v Calihratians

04!13106 08:50:27 2.5 200.3 0.0 0.9 200 ppm CO Cat 04/13/06 08:50:37 2.4 200.6 0.0 0.8 04/13106 08:50:47 2.4 200.8 0.0 0.9 04113/06 08:50:57 2.4 101.0 -0.1 1.0 04113106 08:51:07 2.4 10.0 -0.1 1.1 04/13106 08:51:17 2.2 2.6 -0.1 1.2 04113/06 08:51:27 2.3 2.0 0.0 1.3 04/13/06 08:51:37 2.2 49.9 0.0 1.2 04113/06 08:51:47 2.3 446.1 0.0 1.2 04113/06 08:51:57 2.4 430.0 0.0 1.0 04113/06 08:52:07 2.4 490.9 0.0 1.0 04113106 08:52:17 2.5 491.3 0.0 0.9 04/13/06 08:52:27 2.4 491.7 -0.1 1.0 494 ppm CO Cat 04/13/06 08:52:37 2.3 492.1 0.0 0.8 04/13/06 08:52:47 2.3 492.3 -0.1 1.0 04113/06 08:52:57 2.4 209.7 -0.1 1.0 04113/06 08:53:07 2.6 8.5 0.0 0.9 04/13/06 08:53:17 2.5 2.6 0.0 1.0 04113106 08:53:27 2.4 2.1 0.0 1.1 04!13106 08:53:28

~ 2.6 1.9 -0.1 1.2



# 103
Page 54113/06 Run S11

DatelTfine VOc c0 NOx S02 mmlddlyy hh:mm:ss ppm ppm ppm ppm 04113106 09:19:51 50.3 110.4 223 55.0

Start Run u1 04/13106 09:20:01 50.7 111.6 22.3 55.0 Start Interference Sample 04113/06 09:20:11 49.4 112.5 22.2 55.0 04/13106 09:20:21 48.4 112.8 22.3 54.9 04113f06 09:20:31 49.5 112.9 22.2 54.9 04/13/06 09:20:41 48.9 113.4 22.2 55.0 04/13/06 09:20:51 49.0 113.6 22.2 54.9 04/13l06 09:21:01 49.3 113.9 22.2 54.8 04/13106 09:21:11 48.9 114.4 22.2 54.6 04/13106 09:21:21 49.2 114.7 22.3 54.5 04/13/06 09:21:31 49.6 114.6 22.3 54.4 04113106 09:21:41 50.1 114.1 22.3 54.4 04113106 09:21:51 49.1 113.8 22.3 54.5 04/13/06 09:22:01 49.6 113.4 22.4 54.5 04/13/06 09:22:11 49.0 113.7 22.3 54.6 04113/06 09:22:21 49.2 114.2 22.3 54.6 04113106 09:22:31 48.7 115.0 22.5 54.8 04/13106 09:22:41 48.2 115.3 22.5 55.1 04113106 09:22:51 48.0 114.5 22.7 55.2 04/13/06 09:23:01 48.9 112.7 22.8 55.3 04113106 09:23:11 48.8 109.7 22.8 55.1 04/13106 09:23:21 49.1 107.9 23.0 55.1 04/13106 09:23:31 49.3 105.9 23.1 55.5 04113/06 09:23:41 49.0 103.9 23.1 55.5 04l13/06 09:23:51 48.4 100.5 23.1 55.0 04/13/06 09:24:01 49.0 97.9 23.0 54.4 04/13106 09:24:11 48.9 96.1 22.8 54.1 04/13/06 09:24:21 49.2 94.7 22.7 54.1 04113106 09:24:31 49.3 94.3 22.6 54.3 04/13/06 09:24:41 49.2 94.0 22.6 54.3 04113/06 09:24:51 49.8 93.9 22.5 54.2 04113/06 09:25:01 50.0 94.0 22.5 54.1 04/13/06 09:25:11 50.5 94.4 22.5 54.1 04/13106 09:25:21 49.6 94.8 22.6 54.0 04113106 09:25:31 49.7 95.4 22.6 53.9 04113106 09:25:41 50.0 95.7 22.7 53.6 04/13106 09:25:51 49.7 96.7 22.7• 53.6 04/13/06 09:26:01 49.6 97.6 22.7 53.7 04/13/06 09:26:11 49.7 97.9 22.7 53.9 04/13106 09:26:21 49.3 97.7 22.7 53.9 04/13/06 09:26:31 49.6 97.5 22.8 54.0 04/13/06 09:26:41 50.1 97.2 22.8 53.9 04113/06 09:26:51 50.0 97.4 22.8 54.0 04/13106 09:27:01 49.4 97.7 22.7 54.2 04/13106 09:27:11 ' 49.5 97.7 22.7 54.3 04/13106 09:27:21 49.7 98.1 22.8 54.4 04/13106 09:27:31 49.8 98.2 22.8 54.7 04113106 09:27:41 49.6 98.3 22.8 55.0 04/13106 09:27:51 49.9 98.1 22.7 55.2 04/13/06 09:28:01 49.6 97.4 22.7 55.4 04/13106 09:28:11 49.8 96.5 22.7 55.5 04/13106 09:28:21 50.1 95.5 22.7 55.5 04113106 09:28:31 50.0 95.1 22.7 55.5 04/13/06 09:28:41 50.1 94.9 22.7 56.4 04/13/06 09:28:51 49.7 94.9 22.7 55.2 04/13/06 09:29:01 49.8 95.4 22.7 55.2 04113106 09:29:11 50.5 95.6 22.7 55.2 04/13/06 09:29:21 50.4 95.8 22.7 55.3 04/13/06 09:29:31 50.7 96.2 22.7 55.1 04/13106 09:29:4 i 50.1 96.7 22.6 55.2 04/13106 09:29:51 50.3 97.3 22.5 55.0 04/13106 09:30:01 50.6 97.7 22.6 54.9 04/13106 09:30:11 51.0 97.8 22.6 54.8 04/13106 09:30:21 50.1 98.4 22.6 54.7 04/9 3106 09: 30:31 49.3 98.6 22.6 54.8 04/13106 09:30:41 50.1 98.3 22.7 54.7 04113106 09:30:51 49.7 98.2 22.6 54.6 04/13/06 09:31:01 50.2 98.3 22.6 54.6 04113/06 09:31:11 49.7 98.4 22.6 54.7 04/13/06 09:31:21 50.3 98.2 22.7 54.8 

# 1()d. Page 14113106 Run #1

04/13/06 09:31:31 49.9 97.6 • 22.7 54.7 04/13/06 09:31:41 49.8 96.6 22.7 54.4 04113/06 09:31:51 51.0 ' 96.0 22.7 54.2 04113106 09:32:01 50.2 95.9 22.7 54.1 04/13106 09:32:11 50.6 96.1 22.7 54.0 04113/06 09:32:21 50.2 96.2 22,7 53.9 04113/06 09:32:31 50.5 96.3 22.7 54.0 04/13/06 09:32:41 51.3 97.0 22.7 54.0 04/13/06 09:32:51 51.1 97.9 22.9 54.3 04/13106 09:33:01 51.1 97.8 22.8 54.7 04/13/06 09:33:11 50.5 98.1 22.7 54.5 04113!06 09:33:21 50.3 98.2 22.7 54.4 04/13/06 09:33:31 49.9 98.2 22.7 54.6 04113l06 09:33:41 50.6 98.0 22.7 54.6 04/13/06 09:33:51 50.2 98.4 22.7 55.0 04/13/06 09:34:01 50.9 98.5 22.7 55.4 04/13106 09:34:11 51.0 98.5 22.6 55.6 04/13106 09:34:21 51.0 98.4 22.6 55.8 04/13/06 09:34:31 50.9 98.4 22.7 56.1 04/13/06 09:34:41 51.2 98.2 22.7 56.6 04/13/06 09:34:51 50.6 98.3 22.6 56.7 04113I06 09:35:01 50.7 98.3 22.7 56.7 04/13/06 09:35:11 50.8 98.4 22.8 56.8 04113l06 09:35:21 51.2 98.4 22.8 57.0 04113/06 09:35:31 50.6 98.8 22.7 57.0 04113/06 09:35:41 50.5 99.2 22.7 57.2 04113/06 09:35:51 50.3 99.4 22.7 57.3 04/13106 09:36:01 50.1 99.1 22.7 57.5 04I13106 09;36:11 51.5 98.6 22.7 57,6 04/13106 09:36:21 51.3 98.6 22.7 57.7 04/13106 09:36:31 51.1 98.7 22.7 57.7 04113106 09:36:41 51.1 98.5 22.8 57.7 04/13106 09:36:51 51.3 98.4 22.9 58.0 04/13106 09:37:01 50.4 98.5 22.8 57.9 04/13106 09:37:11 50.8 98.4 22.8 57.7 04/13106 09:37:21 51.4 98.1 22.8 57.8 04/13106 09:37:31 50.9 98.2 22.8 58.0 04/13106 09:37:41 51.7 98.5 22.8 58.4 04/13/06 09:37:51 51.2 98.4 22.8 58.5 04/13106 09:38:01 51.0 98.5 22.9 58.6 04/13/06 09:38:11 50.9 98.8 22.9 58.9 04/13/06 09:38:21 51.3 99.0 23.0 59.1 04/13/06 09:38:31 50.5 99.3 22.9 59.2 04113/06 09:38:41 51.3 99.3 23.0 59.2 04113106 09:38:51 50.6 99.6 22.9 59.3 04113106 09:39:01 50.5 100.1 22.8 59.3 04/13/06 09:39:11 50.2 100.3 22.9 59.2 04113l06 09:39:21 50.2 100.3 22.9 59.2 04/13/06 09:39:31 50.4 100.3 22.8 59.4 04/13/06 09:39:41 50.5 100.0 22.8 59.5 04/13/06 09:39:51 50.1 99.8 22.8 59.5 

### 04113106 09:40:01 50.3 100.0 22.8 59.8 Stop tnterference Sample 04/13/06 09:40:11 50.7 100.0 22.8 60.0 Average 55.6 04113/06 09:40:21 49.9 100.6 22.7 60,1 04113106 09:40:31 49.8 100.7 22.7 59.9 04/13/06 09:40:41 49.7 100.4 22.8 60.0 04/13106 09:40:51 49.6 100.0 22.7 60.0 04/13106 09:41:01 49.5 99.6 22.8 60.0 04/1 3106 09:41:11 49.8 99.2 22.8 60.1 04113106 09:41:21 49.6 98.8 22.8 60.2 04/13106 09:41:31 49.5 98.7 ` 22.8 60.2 04/13106 09:41:41 49.3 98.7 22,8 60.2 04/13106 09:41:51 48.7 99.3 22.8 60.1 04113/06 09:42:01 48.7 99.8 22.8 60.1 04/13/06 09:42:11 48.9 100.2 22.8 60.1 04/13/06 09:42:21 48.9 100.4 22.8 60.1 04/13106 09:42:31 49.4 100.5 22.8 60.0 04/13/06 09:42:41 48.2 100.4 22.9 59.8 04113106 09:42:51 48.9 99.9 22.9 59.7 04113106 09:43:01 48.5 99.6 22.9 59.6 04/13106 09:43:11 49.2 99.4 22.8 59.7 04J13106 09:43:21 49.3 99.7 22.8 59.8 04/13J06 09:43:31 48.7 100.1 22.8 59.8 04/13/06 09:43:41 49.2 100.8 22.9 59.9



### Page 2 

# ~ ~ J4113106 Run #1

04113/06 09:43:51 49.1 101.3 22.8 59.7 04/13/06 09:44:01. 49.1 102.0 22.8 89 V 04113106 09:44:11 48.9 102.5 22.8 ::9.6 04113l06 09:44:21 48.5 103.0 22.7 59.7 04113/06 09:44:31 48.8 103.1 22.7 59.7 04/13106 09:44:41 49.9 103.0 22.7 59.6 04113106 09:44:51 47.5 103.1 22.7 59.7 04113/06 09:45:01 48.0 102.8 22.8 59.6 04/13/06 09:45:11 47.9 101.8 22.8 59.7 04113106 09:45:2 i 47.8 101.1 22.8 59.7 04113/06 09:45:31 49.1 100.4 22.8 59.7 04/13/06 09:45:41 48.8 99.7 22.8 59.7 04113/06 09:45:51 49.2 99.4 22.7 59.7 

### 04/13/06 09:46:01 48.6 99.5 22.8 59.9 Start Inlerference Sample 04/13/06 09:46:11 48.9 99.2 22.8 59.8 04/13106 09:46:21 48.6 98.9 22.8 59.8 04113106 09:46:31 48.7 98.7 22.8 59.9 04113/06 09:46:41 48.5 98.8 22.7 59.6 04113106 09:46:51 48.9 98.8 22.7 59.6 04/13/06 09:47:01 48.6 98.5 22.7 59.7 04/13106 09:47:11 48.5 98.6 22.7 59.7 04/13/06 09:47:21 48.9 98.7 22.8 60,0 04/13/06 09:47:31 48.3 98.8 22.8 60.0 04/13106 09:47:41 48.2 98.5 22.8 60.2 04/13/06 09:47:51 48.5 98.4 22.7 60.2 04/13/06 09:48:01 49.0 98.4 22.7 60.1 04113/06 09:48:11 49.1 98.5 22.7 60.2 04/13/06 09:48:21 48.8 98.3 22.7 60.3 04113106 09:48:31 50.6 98.5 22.7 60.2 04/13/06 09:48:41 47.7 98.5 22.7 60.1 04/13/06 09:48:51 49.1 98.4 22.7 60.0 04/13/06 09:49:01 49.1 98.2 22.7 60.1 04113/06 09:49:11 49.0 98.0 22.7 60.1 04113106 09:49:21 49.5 98.1 22.7 60.0 04/13106 09:49:31 49.3 97.9 22.8 60.0 04113106 09:49:41 49.6 97.6 22.7 60.2 04113/06 09:49:51 49.3 97.3 22.7 60.1 04113106 09:50:01 50.1 97.1 22.7 59.9 04/13/06 09:50:11 49.9 97.1 22.7 59.7 04/13106 09:50:21 50.1 97.2 22.8 59.7 04113106 09:50:31 49.7 97.5 22.8 59.7 04/13/06 09:50:41 50.2 97.8 22.8 59.7 04/13106 09:50:51 50.1 98.1 22.8 59.9 04/13/06 09:51:01 49.5 98.4 22.8 60.0 04/13/06 09:51:11 48.8 98,7 22,7 60.0 04/13/06 09:51:21 49.1 98.8 22.6 59.8 04/13l06 09:51:31 51.3 98.8 22.7 59.6 04/13706 09:51:41 50.7 99.3 22.7 59.5 04113l06 09:51:51 50.4 99.9 22.7 59.5 04113/06 09:52:01 49.4 99.9 22.7 59.4 04113/06 09:52:11 49.5 99.9 22.7 59.6 04/13106 09:52:21 50.9 .99.7 22.7 59.7 04/13/06 09:52:31 51.4 99.6 22.7 59.7 04/13/06 09:52:41 51.0 99.9 22.7 59.7 04l13106 09:52:51 50.8 100.0 22.6 59.7 04113106 09:53:01 51.3 99.7 

### 22.7 59.8 04/13/06 09:53:11 51.2 99.5 22.7 60.0 04/13/06 09:53:21 51.0 99.6 22.6 60.0 04113/06 09:53:31 51.2 99.5 22.7 59.9 04113/06 09:53:41 51.9 99.8 22.7 59.9 04113106 09:53:51 51.3 100.4 22.7 59,9 04113106 09:54:01 51.1 101.7 22.7 59.8 04113106 09:54:11 50.8 102.6 22.6 59.8 04113/06 09:54:21 49.9 103.0 22.7 60.0 04/,13106 09:54:31 49.5 102.8 22.7 60.1 04/13106 09:54:41 50.3 102.3 22.7 60.2 04/13I06 09:54:51 50.2 100.6 22.7 60.3 04/13/06 09:55:01 50.7 98.5 22.6 60.5 04/13/06 09:55:11 51.1 97.1 22,6 60.3 04113/06 09:55:21 51.1 96.5 22.7 60.2 04113106 09:55:31 51.3 96.1 22.6 60.2 04l13106 09:55:41 51.2 96.1 22.6 60.1 04/13106 09:55:51 51.1 96.2 22.7 60.0 04/13/06 09:56:01 51.2 96.6 22.7 60.1 

# 106

Page 34/13/06 Run tt1

04113J06 09:56:11 51.6 971 22.7 60.2 04113/06 09 , 56:21 51.2 98.1 22.6 60.2 04/13106 09:56:31 51.6 98.5 22.7 60.1 04/13106 09:56:41 51.5 98.7 22.6 59.9 04113/06 09;56:51 50.7 98.7 22.6 59.9 04113/06 09:57:01 504 98.5 22.6 59.8 04113/06 09:57:11 50.9 98.0 22 6 60.0 04113106 09:57:21 50.9 97.7 22.6 60.2 04113106 09:57:31 50.0 97.5 22.6 60.3 04113/06 09:57:41 49.8 98.1 22.5 60.4 04113106 09:57:51 49.6 98.3 22.5 60.4 04113/06 09:58:01 50.1 98.5 22.5 60.4 04/13106 09:58:11 50.3 98.4 22.6 60.4 04/13/06 09:58:21 50.0 98.2 22.6 60.3 04/13106 09:58:31 49.9 97.9 22.7 60.3 04113/06 09:58:41 49.7 98.0 22.6 60.1 04113/06 09:58:51 49.1 98.1 22.7 60.3 04/13/06 09:59:01 492 98.2 22.7 60.4 04113/06 09:59:11 49.7 98.3 22.7 60.6 04113106 09:59:21 48.5 98.2 22.7 60.7 04113/06 09:59:31 48,4 97.9 22.6 60.7 04/13/06 09:59:41 48.8 97.2 22.6 60.3 04113/06 09:59:51 48.9 96.8 22.7 60.2 0411310610:00:01 49.0 96.8 22.7 60.1 04/13106 10:00:11 48.7 97.0 22.7 60,1 04113/0610:00:21 49.1 97.2 22.7 60,3 0411 3/06 1 0:00:31 49.2 97.1 22.7 60.3 0411310610:00:41 48.7 96.8 22.7 60.2 0411310610:00:51 48.7 97.1 22.7 60.2 0411310610:01:01 48.8 96.9 22.7 60.2 0411310610:01:11 49.4 96.6 22.7 60.2 04113/0610:01:21 49.0 96.9 22.7 60.2 0411310610:01:31 49.6 96.9 22.7 60.1 04113/0610:01:41 49.1 97.4 22.7 60.4 04113/0610:01:51 49.0 97.4 22.7 60.4 0411310610:02:01 49.1 97.0 22.7 60.4 04113/0610:02:11 48.9 96.8 22.7 60.5 04/1310610:02:21 48.6 96.9 22.7 60.6 04/1310610:02:31 48.5 96.9 22.8 60.5 0411310610:02:41 48.7 96.8 22.8 60.7 04113/0610:02:51 48.8 96.8 22.7 60.7 04113/0610:03:01 48.7 96.6 22.7 60.7 04113/0610:03:11 48.5 96.4 22.7 60.6 04113106 10 03:21 48.6 96.4 22.7 60.4 04113106 10:08:31 48.9 96.1 22.7 60.5 0411 3106 1 0:03:41 48.5 95.8 22.8 60.5 04/13/0610:03:51 49.0 95.9 22.7 60.5 04/13/0610:04:01 49.0 96.3 22.7 60.6 04113/0610:04:11 49.3 96.8 22.6 60.4 04113/0610:04:21 48.9 96.9 22.6 60.4 0411310610:04:31 49.4 96.8 22.7 60.4 0411310610:04:41 49.4 96.7 22.7 60.3 04I1310610:04:51 49.1 96.6 22.6 60.3 0411310610:05:01 48.7 96.5 22.7 60.4 04/1310610:05:11 49.6 96.4 22.6 60.3 04/1310610:05:21 49.3 96.7 22.6 60.3 04/13106 10 05:31 49.3 97.0 22.6 60.5 04/1310610:05:41 49.3 97.3 22.6 60.7 04/1310610:05:51 49.4 97.3 22.6 60.9 04113/06 10:06:01 49.5 97.4 22.6 60.8 Stop Interference Sainple 04113/0610:06:11 49.2 97.6 22.6 60.8 Average 60.1 0411310610:06:21 49.1 98.0 22.5 60.9 04113/0610:06:31 49.4 97.9 22.5 61.0 0411310610:06:41 49.3 97.3 22.6 61.0 0411310610:06:51 49.6 97.1 22.6 61.1 04113106 10:07:01 49,1 96.8 22.6 61.1 0411310610:07:11 49.9 96.1 22.6 61.2 04/1310610:07:21 50.8 95.9 22.6 61.2 04/1310610:07:31 50.9 95.8 22.6 61.1 04113/0610:07:41 50.4 95.7 22.6 61.0 04113/0610:07:51 51.4 95.6 22.6 61.0 0411310610:08:01 50.7 95.8 22.6 61.1 04/1310610:08:11 50.7 95.8 22.7 61.0 04113/06 10:08:21 506 95.8 22.7 61.2 

# 10

Page 44/13106 Run #1

0411310610:08:31 50.1 96.1 22.6 61.1 0411310610:08:41 50.3 96.7 22.6 61.1 04/1310610:08:51 50.3 97.1 22.7 61.0 04/13/0610:09:01 50.7 97.6 22.7 60.9 04113/0610:09:11 50.5 97.5 22.7 60.8 0471310610:09:21 50.7 97.5 22.6 60.6 04/1310610:09:31 50.7 97.6 22.6 60.5 04/13/0610:09:41 50.3 97.7 22.6 60.5 04/1310610:09:51 50.2 97.5 22.6 60.5 04/13/0610:10:01 51.1 97.4 22.6 60.5 04/13/06 10:10 - 11 51.1 97.3 22.6 60.5 04/13/0610:10:21 50.2 97.5 22.5 60.4 0411310610:10:31 51.4 97.9 22.6 60.3 0411310610:10:41 51.2 97.8 22.6 60.1 04/1310610:10:51 50.9 97.6 22.6 60.1 04/13/0610:11:01 50.5 97.3 22.6 59.9 04/13/0610:11:11 50.2 97.0 22.6 59.9 0411310610:11:21 50.5 96.7 22.6 59.9 04113/0610:11:31 50.9 96.5 22.6 59.9 04/1310610:11:41 51.0 96.4 22.6 59.9 04/13/0610:11:51 51.0 96.6 22.6 59.9 04113/0610:12:01 51.3 96.3 22.6 60.0 04/13/0610:12:11 50.9 96.1 22.6 60.0 04/1310610:12:21 51.5 96.2 22.6 60.0 04/1310610:12:31 51.5 96.6 22.6 60.1 04113/0610:12:41 51.3 96.7 22.6 60.2 04113/0610:12:51 51.1 96.3 22.5 60.2 04/13/0610:13:01 50.9 96.2 22.6 60.2 04113/0610:13:11 51.4 96.0 22.6 60.3 04113/0610:13:21 51.2 96.1 22.6 60.4 04113/0610:13:31 50.9 98.2 22.6 60.5 04/1310610:13:41 50.8 96.2 22.5 60.3 04/1310610:13:51 51.0 96.3 22.5 60.3 04/13/0610:14:01 50.3 96.5 22.5 60.2 04113/0610:14:11 50.7 96.1 22.6 60.3 04/13/06 10:14:21 504 95.8 22.6 60.3 04/1310610:14:31 50.6 95.7 22.6 60.3 0411310610:14:41 51.2 95.8 22.6 60.7 04113/061014:51 50.9 95.7 22.6 60.7 0411310610:15:01 50.9 95.9 22.6 60.7 04/13/0610:15:11 50.7 96.4 22.5 60.7 0411310610:15:21 51.0 97.0 22.5 60.7 04/1310610:15:31 50.3 97.4 22.5 60.8 0411310610:15:41 51.0 97.5 22.4 60.9 0411310610:15:51 49.9 98.0 22.4 61.2 04/13/0610:16:01 50.0 97.9 22.4 61.5 0411310610:16:11 50.1 97.9 22.4 61.5 04/1310610:16:21 49.7 98.1 22.5 61.5 04113/0610:16:31 50.1 97.9 22.6 61.5 04/13/0610:16:41 50.0 97.7 22.5 61.5 04113/0610:16:51 50.2 97.9 22.6 61.4 04/13/0610:17:01 50.6 97.8 22.5 61.3 04/1310610:17:11 50.5 97.4 22.5 61.2 04/13/0610:17:21 50.9 96.9 22.6 61.1 04/13/0610:17:31 50.5 96.7 22.5 61.2 04113/0610:17:41 50.3 96.7 22.5 61.3 04/13/0610:17:51 50.3 96.7 22.4 61.3 04113/0610:18:01 60.0 97.3 22.4 61.2 04/13/0610:18:11 49.4 98.0 22.4 61.3 04/13/0610:18:21 49.7 98.2 22.5 61.3 04/1310610:18:31 49.4 98.0 22.5 61.1 04/13/061018:41 50.0 97.8 22.4 61.2 04/13/0610:18:51 49.1 97.7 22.4 61.2 04113/0610:19:01 49.5 98.1 22.4 61.2 04/1310610:19:11 48.9 98.8 22.5 61.2 0411310610:19:21 48.8 99.4 22.5 61.2 04113/0610:19:31 48.6 99.3 22.5 61.1 04/13/0610:19:41 49.2 98.6 22.5 60.9 04/13/0610:19:51 49.5 97.9 22.5 60.8 04/13/0610:20:01 49.4 97.4 22.5 60.7 04/13/0610:20:11 50.1 97.3 22.5 60.7 04J1310610:20:21 49.7 97.2 22.6 60.6 04113/0610:20:31 49.4 97.5 22.6 60.6 04/13/0610:20:41 49.5 97.7 22.6 60,6 

# 108

Page 54113106 Run #1

0411310610:20:51 49.3 98.0 22.6 60.6 0411310610:21:01 49.2 98.1 22.6 60.5 04/13/06 10:21 11 493 98.2 22.6 60.6 04/1310610:21:21 491 98.4 22.6 60.7 0411310610:21:31 49,5 98.7 22.6 60.7 0411310610:21:41 50.0 99.2 22.6 60.7 04/1310610:21:51 49.3 99.8 22.6 60.9 04113/0610:22:01 49.2 100.1 22.6 60.8 0411310610:22:11 48.9 100.3 22.6 60.8 0411310610:22:21 49.6 100.5 22.7 60.7 04!1310610:22:31 49.3 100.3 22.6 60.7 04113/0610:22:41 48.5 73.3 22.6 60.6 0411310610:22:51 48.5 100.2 22.6 60,6
Stop Run #1 49.88 98.81 22.66 58.83

0411310610:23:01 28.8 100.1 22.5 60.5 04113/0610:23:11 10.1 91.3 22.0 60.3 04/13/0610:23:21 11.6 56.4 16.0 57.8 0411310610:23:31 9.4 29.7 9.5 50.7 04113106 10:23:41 7.7 18.0 6.5 41.5 04/13106 10:23:51 68 11.9 4.9 33.0 0411310610:24:01 6.3 8.1 3.9 26.2 04/13106 10:24 11 5.1 6.1 3.2 21.1 04113106 10:24:21 3.2 9.3 2.7 17.2 04113/0610:24:31 2.3 63.3 2.1 14.0 04/13106 10:24:41 1.7 114.9 2.0 11.6 04/ 13106 10: 24: 51 1.3 153.0 1.7 10.4 04/13106 10:25:01 1.1 175.3 1.4 8.7 0411310610:25:11 1.0 186.4 1.2 7.1 04! 13106 10:25 - 21 0.9 191.1 1.1 5.9 0411310610:25:31 0.8 193.0 1.0 5.0 04113/06 10:25:41 0.8 193.8 1.0 4.3 04113/0610:25:51 0.9 194.2 0.9 3.8 04/1310610:26:01 1.0 194.8 0.9 3.5 0411310610

- 26:11 0.8 195.1 0.8 3.3 0411310610:26:21 0.5 195.5 0.8 3.1 0411310610:26:31 0.5 195.6 0.7 2.9 04113/0610:26

- 41 0.5 

### 195.8 0.7 2.8 04/1310610:26:51 0.6 

### 195.8 0.6 2.5 0411310610:27:01 0.6 

### 195.8 0.6 2.4 04/13/06 10:27:11 0.6 

### 195.8 0.5 2.4 04113i0610:27:21 0.7 195.7 0.5 2.3 04113106 10:27:31 0.6 175.3 1.0 2.1 0411310610:27:41 0.4 104.5 8.1 2.2 04/13/06 10:27:51 0.5 51.9 16.2 2.1 04/1310610:28:01 0.5 26.2 20.2 2.1 0411310610:28:11 0.5 15.7 22.0 2.1 0411310610:28:21 0.4 10.9 22.7 2.0 04/ 13106 10:28:31 0.3 8.1 23.2 1.9 04/13/0610:28:41 0.5 6.3 23.4 2.0 04/13/06 10:28:51 0.5 5.1 23.5 1.9 0411310610:29:01 0.3 4.4 23.6 1.9 04/1310610:29:11 0.4 3.8 23.7 1.7 04r 13106 10:29: 21 0.5 3.4 23.8 1.8 04113/0610:29:31 0.4 3.2 23.8 1.7 0411310610:29:41 0.2 3.0 23.9 1.5 0411310610:29:51 0.3 2.9 

### 24.0 1.5 0411310610:30:01 0.4 2.5 

### 23.9 1.6 04113J0610:30:11 0.6 2.4 

### 23.9 1.6 04/13/0610:30:21 0.6 2.3 

### 23.9 1.6 04/13106 10:30:31 1.3 2.1 24.0 1.5 04/13106.10:30:41 2.7 1.8 23.2 1.5 04/13106 10:30:51 2.8 2.0 16.6 1.5 04/13106 1031:01 2.9 1.9 8.3 1.5 04/13/06 10:31:11 1.4 1.9 4.1 1.7 04113/06 10:31:21 0.6 1.7 2.3 2.1 04/13/06 10:31:31 0.4 1.5 1.6 6.0 04/13/06 10:31:41 0.6 1.3 1.2 16.7 04/ 13/06 10:31: 51 0.6 1.3 1.1 31.9 04113/06 10:32:01 0.5 1.5 1.1 46.8 04/13/06 10:32:11 0.5 1.7 1.1 58.6 04/13106 10:32:21 05 1.7 1.0 67.3 200 ppm CO Zero NOx

25.5 ppm NOx Zero S02

Page 6 

# 1094113106 Ruri # i

0411310610:32:31 4.4 1.6 0.9 73.7 0411310610:32:41 0.4 1.5 0.8 78.5 04/1310610:32:51 0.5 1.5 0.7 82.1 0411310610:33:01 0.4 1.4 0.6 84.4 0411310610:33:11 0.4 1.3 0.6 85.9 04l1310610:33:21 0.4 1.5 0.5 87.3 04113/0610:33:31 0.5 1.4 0.5 88.9 0411310610:33:41 0.4 1.3 0.5 90.2 04/13/06 10:33:51 0.5 1.3 0.5 91.2 0411310610:34:01 0.5 1.2 0.4 91.8 0411310610:34:11 0.4 1.3 0.4 92.4 04113/0610:34:21 0.4 1.4 0.3 92.6 04113/0610:34:31 0.4 1.5 0.4 92.8 0411310610:34:41 0.3 1.2 0.4 93.2 0411310610:34:51 0.2 1.3 0.4 93.5 0411310610:35:01 0.2 1.3 0.4 93.8 0411310610:36:11 0.2 1.5 0.3 93.9 0411310610:35:21 0.3 1.4 0.3 94.1 04/1310610:35:31 0.2 1.3 0.4 94.4 0411310610:35:41 0.2 1.4 0.4 94.5 0411310610:35:51 0.0 1.5 0.4 94.5 04113/0610:36:01 0.2 1.5 0.4 94.5 0411310610:36:11 0.1 1.3 0.5 94.6 04113/0610:36:21 

### 0.3 1.3 0.4 94.8 04l1310610:36:31 0.4 1.3 0,4 94.9 0411310610:36:41 

### 20.5 1.4 0.4 94.9 0411310610:36:51 41.8 1.5 0.4 94.7 0411310610:37:01 41.9 1.5 0.3 90.0 04113106 10:37:11 41.9 1.5 0.1 77.8 04113r0610:37:21 41.8 1.5 0.1 62.2 0411310610:37:31 

### 41 .9 1.6 0.0 47.8 04113/0610:37:41 41.9 1.4 0.0 36.4 04/13/0610:37:51 41.9 1.3 0.0 28.1 

### Zero VOC

100 ppm S02 

### Zero CO

40.8 ppm CH4



# ~ ~ 

# _ a Page 74113106 Run #2

DatefTime VOC c0 NOx S02 mm/dd/yy hh:mrn:ss ppm ppm ppm ppm 0411310610:49:51 48.4 95.6 21.2 57.2

Start Run #2 04/1310610:50:01 48.8 95.4 21.3 57.4 04/13/0610:50:11 48.7 95.4 21.2 57.4 04/1310610:50:21 48.5 95.3 21.3 57.6 0411310610:50:31 48.2 95,5 21.4 57.8 0411310610:60'41 48.6 96.1 21,4 58.1 0411310610:50:51 49.0 96.7 21.3 58.4 0411310610:51:01 49.3 97.0 21.4 58.4 04113/0610:51:11 48,9 97.6 21.5 58.3 0411310610:51:21 48.9 97.6 21.4 58.3 0411310610:51:31 49.3 97.4 21.5 58.5 04/13/0610:51:41 48.9 97.4 21.6 58.5 04/13/0610:51:51 49.3 97.4 21.6 58.5 0411310610:52:01 49.6 97.7 21.7 58.5 0411310610:52:11 49.3 98.0 21.7 58.6 04113/06 10:52:21 49.0 98.0 21.8 586 04/1310610:52:31 48.9 97.6 21.8 58.6 04/1310610:52:41 49.2 96.9 21.8 58.6 04/13/0610:52:51 48.9 96.8 21.8 58.6 04113/0610:53:01 49.2 96.4 21.7 58.7 04113106 10:53:11 49.0 96.3 21,7 58.7 0411310610:53:21 49.4 96.5 21.8 68.8 04/1310610:53:31 49.4 97.3 21.8 58.8 04113:0610:53:41 49.2 98.2 21.7 58.8 04113/0610:53:51 49.1 98.6 21.6 58.9 0411310610:54:01 49.5 96.6 21.7 59.0 04/13/0610:54:11 49.3 98.5 217 59.0 04113/0610:54:21 49.5 98.2 21.7 58.9 0411310610:54:31 49.4 98.4 21.7 58.7 0411310610:54:41 49.5 98.8 21.7 58.6 04/13/06 10:54:51 497 99.5 21.7 58.7 04/13/06 10:55:01 49.0 99.7 21.6 58.9 0411310610:55:11 49.3 99.7 21.6 59.0 0411310610:55:21 49.4 99.5 21.6 59.0 04113/0610:55:31 49.1 99.5 21.6 59.1 04113/0610:55:41 48.9 99.2 21.6 59.2 0411310610:55:51 49.3 98.9 21.5 59.1 04113/0610:56:01 48.9 98.6 21.6 59.0 04113/0610:56:11 49.3 98.0 21.6 58.9 04113/0610:56:21 49.9 97.9 21.6 58.9 0411310610:56:31 49.7 98.2 21.6 59.0 04/1310610:56:41 49.2 98.8 21.5 59.0 04/1310610:56:51 48.7 99.2 21.5 59.0 0411310610:57:01 49.3 99.3 21.5 59.0 04113/0610:57:11 49.1 99.1 21.6 59.1 04113/0610:57:21 49.1 98.7 21.5 59.0 04/1310610:57:31 491 98.2 21.5 58.9 04113/0610:57:41 49.5 97.8 21.5 58.9 04/13106 10:57: 51 49,2 97.5 21.5 59.0 0411310610:58:01 48.7 97.3 21.6 59.0 04113/06 10:58: 11 49.3 97.2 21.7 58.9 0411310610:58.21 49.1 97.5 21.7 58.9 04113/06 10: 58: 31 49.3 98.0 21.7 58.8 04113/0610:58:41 49.1 98.8 21.7 58.8 04113/0610:58:51 48.9 99.5 21.6 58.8 0411310610:59:01 48.5 99.8 21.6 58.7 04/1310610:59:11 48.2 100.1 21.6 58.7 04/1310610:59:21 48.9 99.8 21.7 58.8 04/13/0610:59:31 48.5 99.6 21.8 58.9 04/1310610:59:41 49.2 99.4 21.8 59.0 04/1310610:59:51 49.3 98,9 21.7 58.9 04113/06 11:00:01 49.2 98.8 21,7 58.9 Stari Interference SampEe 04/13/0611:00:11 48.5 98.5 21.6 58.8 04/13/0611:00:21 49.2 98.3 21.6 58.9 0411310611:00:31 48.6 98.7 21.7 58.8 04i13106 11 •00:41 49.2 98.9 21.7 58.7 0411 3106 1 1:00:51 49.2 991 21.7 58.8 04113k06 11:01:01 48.9 i 00.7 21.7 58.9 04113/0611:01:11 48.6 101.2 21.7 59.0 0411310611:01:21 48.8 101.5 21.6 591

Page 1 

# 1' 1. 14/13/06 Run ii2

0411310611:01:31 49.6 100.9 21.6 59.0 04113106 11:01:41 491 100.1 21.7 590 04713/0611:01:51 46.8 99.3 21.7 56.8 04/1310611:02:01 48.6 98.6 21.6 58.7 04113/0611:02:11 49.0 96.2 21.5 58.7 04/13/0611:02:21 49.1 98.1 21.7 58.7 0411310611:02:31 49.5 98.1 21.7 58.7 04/1310611:02:41 49.1 98.1 21.7 58.7 0411310611:02:51 48.7 97.8 21.8 58.8 0411310611:03:01 49.1 97.9 21.6 58.9 04/13/0611:03:11 48.9 98.4 21.7 59.0 04113/0611:03:2 1 49.1 99.3 21.7 59.0 04113/0611:03:31 48.5 99.7 21.7 59.1 04/13/0611:03:41 48.8 100.1 21.8 59.0 04/13/0611:03:51 48.7 100.0 21.8 59.0 04113/0611:04:01 48.4 99.6 21.8 59.1 0411310611:04:11 49.2 98.6 21.8 59.1 04113/0611:04:21 49.0 98.3 21.8 59.0 04/13/06 11:04:31 49.3

- 98.1 21.7 59.1 04/1310611:04:41 49.1 98.1 21.8 59.1 04/1310611:04:51 49.4 98.2 21.8 59.0 04/13/0611:05:01 48.2 98.9 21.7 59.0 04/13/0611:05:11 49.0 98.8 21.6 58.9 04113/0611:05:21 48.9 98.9 21.6 56.9 04/13/0611:05:31 48.0 99.2 21.8 58.8 04/1310611:05:41 48.8 98.7 21.7 58.9 04/13/0611:05:51 48.7 98.6 21.7 59.0 04113/0611:06:01 49.0 98.3 21.8 59.1 04/13/0611:06:11 49.2 98.3 21.9 59.1 04/13/0611:06:21 49.5 98.2 21.9 59.2 04/1310611:06:31 49.1 98,1 21.8 59.2 04/13/0611:06:41 49.3 98.0 21.8 59.2 04/13/0611:06:51 48.9 98.2 21.8 59.4 04113/0611:07:01 48.6 98.5 21.8 59.4 04/13/0611:07:11 48.1 98.9 21.7 59.3 04/13/0611:07:21 48.3 99.3 21.7 59.2 04113/0611:07:31 48.5 99.4 21.8 59.1 0411310611:07:41 48.8 99.4 21.8 59.2 04/13/0611:07:51 49.2 99.0 21.9 59.2 04/13/0611:08:01 46.6 98.5 21.6 59.2 04/13/0611:08:11 48.6 98.1 21.9 59.2 04/13/0611:08:21 48.4 97.7 21.9 59.1 04/1310611:08:31 48.1 97.6 21.9 59.1 0411310611:08:41 48.2 97.6 21.9 59.1 0411310611:08:51 48.5 97.2 22.1 59.1 04/13/0611:09:01 48.0 97.2 22.0 59.2 04/1310611:09:11 48.6 97.1 22.0 59.2 0411310611:09:21 48.6 96.9 22.1 59.3 04113/0611:09:31 48.1 96.8 22.0 59.2 04113/0611:09:41 48.4 96.9 22.0 59.2 04113/0611:09:51 47.9 97.0 22.0 59.2 04/13/0611:10:01 48.1 96.9 21.9 59.2 04/13/0611:10:11 48.4 96.9 21.9 59.3 04113/0611:10:21 48.3 96.8 22.0 59.2 04113/0611:10:31 48.6 96.7 22.0 59.1 04/13/0611:10:41 47.9 96.9 22.0 59.1 04/1310611:10:51 48.4 97.0 21.9 59.2 04/13/0611:11:01 48.6 96.7 21.9 59.3 0411310611:11:11 48.9 97.0 21.9 59.2 04/1310611:11:21 48.8 97.4 21.9 59.2 04/13/0611:11:31 48.4 97.9 21.9 59.2 0411310611:11:41 48.2 97.7 21.9 59.1 04/13/0611:11:51 48.6 97.9 21.9 58.9 0411310611:12:01 48.3 98.0 21.8 59.1 04/13/0611:12:11 48.4 98.0 21.8 59.1 04/1310611:12:21 48.5 98.0 21.8 59.3 04/13/0611:12:31 48.1 98.3 21.9 59.3 04113/0611:12:41 48.6 98.6 21.9 59.3 0411310611:12:51 48.6 98.7 21.9 59,5 04113/0611:13:01 48.7 98.1 21.9 59.5 04/13/0611:13:11 48.1 97.8 21.9 59.4 04/13/0611:13:21 48.3 97,5 21.9 59.4 04113/0611:13:31 48.1 97.0 21.9 59.3 04113/0611:13:41 48.9 96.4 21.9 59.4



### Page 2 

# 1 1 . 2

### 4. 1 13106 Run n2

04/1310611:13:51 48.8 96.1 21.9 59.4 04113106 11: 14: 01 49,0 95.9 21.9 59.5 04/1310611:14:11 49.0 95.9 21.9 59.5 0411310611:14:21 49.3 96.1 21.9 59.6 04113/06 11: 14:31 48.9 96.4 21.9 59.7 04113!06 11
~ 14:41 49.0 96.7 21.9 59.8 04113/0611:14:51 49.5 96.9 22.0 59.8 04/13106 11:15; 01 48.8 97.3 22.0 59.7 04/1310611:15:11 49.0 97.4 22.0 59.7 0411310611:15:21 48.7 97.6 22.0 59.6 04113i0611:15:31 48.4 97.9 21.9 59.6 04113/0611:15:41 48.7 97.6 22.1 59.4 04113/06 11 : 15: 51 48.3 97.6 22.0 59.3 04113/0611:16:01 48.9 97.3 22.0 59.5 0411310611:16:11 48.7 97.4 22.0 59.5 0411310611:16:21 49.4 97.3 22.0 59.4 04/13106 11:16:31 49,1 97.3 21.9 59.3 0411310611:16:41 49.1 97.4 22.0 59.3 04/1310611:16:51 49.4 97.4 22.0 59.3 04113/0611:17:01 49.0 97.4 21.9 59.2 04/1310611:17:11 49.4 97.3 22.0 59.1 0411310611:17:21 49.8 97.3 22.0 59.3 0411310611:17:31 50.3 97.3 22.0 59.2 04113/0611:17:41 50.3 97.6 21.8 59.2 04113/0611:17:51 49.5 97.9 21.8 59.2 04/1310611:18:01 49.2 98.2 21.9 59.2 04/1 3106 1 1:18:11 49.3 98.4 21.9 59.2 04113/0611:18:21 49.3 98.3 21.8 59.2 04113/0611:18:31 49.6 98.2 21.8 59.1 0411310611:18:41 49.5 98.3 21.9 591 04/1 3106 1 1:18:51 49.8 98.3 21.9 59.1 0411 3/06 1 1:19:01 49.7 98.1 21.9 59.1 04/13/06 11 - 19:11 496 97.8 21.9 59.2 04/1310611:19:21 50.0 97.7 21.8 59.3 04113/0611:19:31 49,8 97.6 21.9 59.1 04/1 3106 1 1:19:41 49.7 97.6 21.8 58.9 04/13/0611:19:51 49.5 98.1 21.8 58.9 04113l06 11:20:01 48.9 98.0 21.9 58.8 Stop Interference Sample 04113/0611:20:11 49.2 97.6 22.0 58.8 Average 59.2 04/1310611:20:21 49.4 97.2 21.9 58.7 04/1310611:20:31 49.6 96.6 21.7 58.6 04/13/0611:20:41 49.3 96.1 21.8 58.5 04113/0611:20:51 49.6 95.5 21.9 58.2 04113/0611:21:01 49.5 95.2 21.9 58.3 04/13/0611:21:11 49.2 95.1 21.9 58.4 04/13/06 11:21 : 21 49.4 95.1 21.8 58.6 04/1310611:21:31 49,7 95.4 21.7 58.5 04/13/0611:21:41 49.7 95.7 21.7 58.5 04113/0611:21:51 49.6 96.1 21.6 58.5 0411310611:22:01 50.1 96.5 21.7 58.4 04/1310611:22:11 49.8 97.1 21.7 58.3 04/13/0611:22:21 50.0 97.6 21.7 58.4 04113/0611:22:31 49.8 98.2 21.7 58.5 04113/0611:22:41 49.2 98.5 21.8 58.6 04/13/0611:22:51 48.7 98.8 21.8 58.6 04/1310611:23:01 48.8 99.3 21.8 58.6 04113/0611:23:11 48.8 99.6 21.8 58.8 04113/0611:23:21 48.5 100.0 21.8 59.0 0411310611:23:31 48.7 100.1 21.8 58.9 04/1310611:23:41 48.2 99.9 21.8 58.9 0411310611:23:51 48.5 99.5 21.7 58.9 04113/0611:24:01 48.1 99.0 21.7 58.7 0411310611:24:11 48.1 98.5 21.7 58.7 04/13/0611:24:21 47.9 97.7 21.7 58.7 0411310611:24:31 48.1 97.4 21.7 58.6 04/13/0611:24:41 48.3 96.8 21.8 58.5 003/0611:24:51 48.1 96.8 21.7 58.5 04/1310611:25:01 48.1 97.3 21.7 58.5 04/1310611:25:11 48.0 97.8 21.7 58.4 04/1310611:25:21 48.2 98.1 21.7 58.3 0411310611:25:31 48.0 98.2 21.6 58.3 04/1310611:25:41 47.8 98.1 21.7 58.3 0411310611:25:51 48.1 97.7 21.7 58.4 04/13/0611:26:01 47.8 97.6 21.7 58.4

Page 3 1 1 . 34113/06 Run #2

04/131061126:11 47.8 97.3 21.7 58.3 04/13/0611:26:21 48.4 97.5 21.7 58.3 04113/0611:26:31 47.5 97.6 21.7 58.3 0411310611:26:41 47.2 98.2 21.7 58.4 04/1310611:26:51 48.0 98.2 21.7 58.3 04113/0611:27:01 47.7 98.0 21.8 58.3 04113/0611:27:11 48.0 97.6 21.8 58.3 04/13/0611:27:21 47.6 97.3 21.8 58.2 0411310611:27:31 47.8 97.3 21.8 58.1 0411310611:27:41 47.8 97.5 21.7 57.9 04/131061127:51 47.9 97.6 21.7 57.9 04/1310611:28:01 47.6 97.6 21.8 57.8 04/13/0611:28:11 47.4 97.7 21.9 57.7 04/13/0611:28:21 47.6 97.9 21.9 57.9 04113/0611:28:31 47.9 98.0 21.8 57.8 04/13/0611:28:41 47.8 98.2 21.9 57.7 04/1310611:28:51 47.4 98.1 21.9 57.8 04/13/06 11;29:01 47.5 97.7 21.8 57.7 04/13/0611:29:11 47.0 97.4 21.9 57.6 04/13/0611:29:21 48.1 97.0 21.9 57.6 0411310611:29:31 47.8 97.0 21.8 57.7 04/1310611:29:41 47.4 97.3 21.8 57.6 04/1310611:29:51 47.6 97.5 21.8 57.6 04/13/0611:30:01 47.8 97.3 21.9 57.8 04113/0611:30:11 48.5 97.1 21.9 57.8 0411310611:30:21 48.2 97.1 22.0 57.8 04/1310611:30:31 47.9 97.3 22.0 57.9 0411310611:30:41 47.8 97.2 22.1 57.9 04/13/0611:30:51 47.6 97.0 22.1 58.1 04113/06 11: 31:01 48.1 97.1 22.1 58.2 0411310611:31:11 47.9 97.5 22.1 58.3 04/1310611:31:21 47.6 98.0 22.1 58.3 04/1310611:31:31 47.5 98.4 22.1 58.2 04113/0611:31:41 47.7 99.3 22.1 58.4 0411310611:31:51 47.8 99.5 22.1 58.5 04/13/0611:32:01 48.5 99.2 22.1 58.5 04113/0611:32:11 48.7 98.8 22.1 58.4 0411310611:32:21 47.6 98.9 22.0 58.5 0411310611:32:31 48.5 98.5 22.1 58.4 04/13/0611:32741 48.7 98.2 22.1 58.5 04/13/061132:51 48.0 98.3 22.1 58.6 0411310611:33:01 48.1 98.4 22.0 58.6 04/13/0611:33:11 48.1 98.2 22.1 58.5 04/13/0611:33:21 48.5 98.2 22.2 58.4 04113/0611:33:31 49.0 97.9 22.2 58.5 0411310611:33:41 49.0 98.2 22.2 58.7 04/1310611:33:51 49.3 98.8 22.1 58.8 04/13/0611:34:01 49.0 99.1 22.1 59.0 04/13/0611:34:11 48.6 99.5 22.1 59.1 04113/06 11:34:21 48.6 100.1 22.1 59.1 04113/0611:34:31 48.1 100.2 22.2 59.1 04/1310611:34:41 49.0 99.8 22.1 59.1 04/1 3106 1 1:34:51 49.1 99.8 22.2 59.1 04/13106 11:35:01 49,1 99.9 22.1 59.2 04/13/0611:35:11 48.0 75.6 21.8 58.3 04/13/0611:35:21 48.0 46.3 21.6 57.1 04/1310611:35:31 48.8 100.3 22.2 59.4 04/ 13106 11:35:41 49.3 100,1 22.1 59.6 04/13106 11:35:51 48.8 100.1 22.1 59.5 04/1310611:36:01 48.9 100.3 22.2 59.2 04113/0611:36:11 48,7 100.3 22.1 59.2 0411310611:36:21 49.1 99.9 22,2 59.3 0411310611:36:31 49.9 99.2 22.3 59.3 04/13/0611:36:41 49.6 98.6 22.3 59.1 04/1310611:36:51 50.1 98.5 22.3 69.1 04113/0611:37:01 49.7 98,7 22.2 59.1 04113/0611:37:11 49.5 98.9 22.3 59.0 04/13/0611:37:21 49.3 99.4 22.3 59.0 04/1310611:37:31 49.2 99.9 22.4 59.0 04/1310611:37:41 49.6 99.7 22.3 59.1 04/13/06 11:37:51 49.4 99.4

- 22.4 59.3 04/13/0611:38:01 49.8 99.1 22.4 59.3 0411310611:38:11 49.7 98,7 22.3 59.3 0411310611:38:21 50.1 98.7 22.3 59.4 

# 114
Page 44113106 Run #2

04/13106 11:38:31 49.7 98.6 22.4 59.2 04/13/06 11:38:41 502 98.8 22,5 59.2 04/13!0611:38:51 49.8 98.8 22.5 59.2 04/1310611:39:01 50.2 98.9 22.4 59.2 04113/0611:39:11 50.0 99.4 22.3 59.4 0411 3106 1 1:39:21 49.3 99.4 22.3 59.5 0411 3/06 1 1:39:31 49.8 99.4 22.3 59.4 0411 3106 1 1:39:41 49.6 99.2 22.3 59.3 0411310611:39:51 50.0 98.9 22.3 59.3 04113/0611:40:01 50.0 98.6 22.4 59.4 0411310611:40:11 49.8 98.2 22.3 59.4 0411 3106 1 1:40:21 49.7 97.9 22.3 59.4 04/13!06 11:40:31 49.7 97.5 22.3 594 04/13/06 11:40:41 49.9 97.3 22.4 59.4 04/13/0611:40:51 49.1 97.4 22.4 59.4 04/13/06 11:41:01 49.2 973 22.4 59.5 04113/0611:41:11 49.6 97.6 22.3 59.5 04113/0611:41:21 50.0 97,8 22.3 59,6 04113/0611:41:31 49.9 98.3 22.3 59.6 04/1 3106 11 A1:41 49.7 98.8 22.4 59.5 0411310611:41:51 49.2 98.9 22.4 59.3 04/1310611:42:01 49.9 99.4 22.3 59.1 04/1310611:42:11 49.4 99.5 22.3 59.1 0411310611:42:21 49.4 99.4 22.3 59.1 04/1310611:42:31 49.1 99.4 22.3 59.2 04/13/0611:42:41 49.6 99.3 22.3 59.3 04/1310611:42:51 50.5 99.3 22.3 59.4 0411310611:43:01 49.8 99.8 22.3 59.4 04113/0611:43:11 50.2 99.9 22.3 59.6 0411310611:43:21 49.5 99.9 22.2 59.7 041131061143:31 49.2 100.0 22.3 59.8 04/1310611:43:41 49.1 100.1 22.2 59.7 04/13/0611:43:51 48.6 99.9 22.4 59.6 04/13J0611:44:01 48.8 99.9 22.4 59.7 0411 3106 1 1:44:11 48.7 99.8 22.3 59,8 04/13/06 11:44:21 48.7 99.7 22.3 591 04/1310611:44:31 48.7 99.7 22.2 59.7 04/1310611:44:41 48.6 99.2 22.3 59.7 0411310611:44:51 48.8 98.5 22.4 59.7 0411 3/06 1 1:45:01 48.9 97.8 22.4 59.8 04/1310611:45:11 49.0 97.4 22.4 59.8 0411 3/06 1 1:45:21 49.2 96.9 22.3 59.8 04113/0611:45:31 49.4 96.6 22.3 59.5 04/13/0611:45:41 48.9 96.7 22.3 59.7 04/1310611:45:51 48.9 97.3 22.3 59.7 04/1310611:46:01 48.2 98.2 22.1 59.6 0411310611:46:11 48.6 98.8 22.1 59.6 0411310611:46:21 48.3 99.3 22.2 59.6 0411310611:46:31 48.5 100.2 22.2 59.6 0411310611:46:41 48.8 100.7 22.3 59.6 0411310611:46:51 48.8 101.1 22.2 59.7 0411310611:47:01 48.4 100.9 22.2 59.6 0411 3106 1 1:47:11 48.1 100.7 22.2 59.5 0411 3106 1 1:47:21 48.2 99.8 22.2 59.6 04113/0611:47:31 48.6 99.2 22.2 59.6 04113/0611:47:41 49.0 99.1 22.3 59.4 04/13/06 11'47:51 48.7 99.1 22.2 59.4 04113J0611:48:01 48.8 99.2 22.2 59.4 04/13/0611:48:11 48.6 99.3 22.2 59.4 0411310611:48:21 48.9 99.2 22.3 59.4 0411310611:48:31 48.4 98.6 22.3 59.4 04/13/06 11

- 48:41 48.5 97.9 22.3 59.3 04/1310611:48:51 48.7 97.3 22.3 59.3 04/13/0611:49:01 48.2 97.1 22.3 59.3 0411310611:49:11 48.9 97.3 22.3 59.4 0411310611:49:21 48.7 97.6 22.3 59.4 04!13J06 11:49:31 48.7 97.6 22.3 593 04/13/0611:49:41 48.3 97.7 22.3 59.3 04113/0611:49:51 49.0 97.6 22.1 59.3 0411310611:50:01 49.0 97.6 22.2 59.4 04113/0611:50:11 49.7 97.8 22.1 59.3 04113J0611:50:21 49.4 98.2 22.1 59.2 0411310611:50:31 49.4 98.7 22.2 59.4 0411310611:50:41 49.7 98.8 22.2 59.4

Page 5 

# 1 1.
~4113106 Run #2

04113/0611:50:51 49.1 99.0 22.1 59.2 04/1310611:51:01 48.9 99.4 22.1 59.1 04113/0611:51:11 48.9 99.1 22.1 591 04113/0611:51:21 49.0 98.6 22.1 59.1 0411310611:51:31 48.2 98.2 22.0 58.9 04/1310611:51:41 48.6 97.7 22.1 58.8 04/1310611:51:51 47.8 68.0 22.0 58.7
Stop Run #2 48.86 97.94 21.93 58.95

04/13/06 11:52:01 48.5 96.1 22.2 58.7 0411310611:52:11 33.4 95.2 22.1 58.7 04/13/0611:52:21 14.8 89.4 21.8 58.5 0411310611:52:31 19.3 58.0 16.8 56.3 04/1 3106 1 1:52:41 20.0 29.8 10.4 50 

## a 04/1310611:52:51 20.2 16.4 7.2 42.6 04/1310611:53:01 20.4 9.9 6.0 35.4 04113/0611:5311 18.1 6.4 5.7 29.7 04/1310611:53:21 15.3 4.6 5.4 24.8 0411310611:53:31 12.8 3.3 4.8 21.2 04/1310611:53:41 9.4 2.6 4.1 18.4 04/13/0611:53:51 7.1 7.4 3.4 15.5 04113/0611:54:01 4.8 64.6 2.6 12.7 04113/06 11:54:11 3.7 116.5 2.4 10.6 04113/0611:54:21 3.2 151.6 2.3 9.9 04/1310611:54:31 2.9 175.2 1.7 8.3 04/13106 11:54:41 2.6 184.5 1.5 6.6 04/13/0611:54:51 2.4 188.9 1.3 5.0 0411310611:55:01 2.3 191.1 1.2 3.9 0411310611:55:11 2.2 192.3 1.2 ' 3.1 04113/0 6 11: 5 5: 21 2.2 19 3. 0 1.1 2.5 04/13/06 11:55:31 2.0 193.4 1.0 2.1 04 / 13106 11: 55:41 2.0 193.6 1.0 1.7 04 / 13/06 11: 55:51 1.9 193.7 1.0 1.5 04113/0611:56:01 1.9 

### 193.7 0.9 1.0 04/1310611:56:11 1.9 

### 193.7 0.8 0.7 04113/06 11:56:21 1.9 193.8 

### 0.7 0.6 04113106 11:56:31 1.9 193.9 

### 0.7 0.5 04/13/0611:56:41 1.8 194.1 0.7 0.5 04/13/06 11:56:51 1.9 184.7 0.7 0.4 04/13/0611:57:01 1.6 118.7 5.2 0.3 04113/06 11:57:11 1.4 59.4 14.1 0.2 04/13/06 11:57:21 1.3 29.9 19.1 0.2 04/13/06 11:57:31 1.2 16.2 21.3 0.2 04/1310611:57:41 1.3 9.9 22.4 0.2 04/1310611:57:51 1.1 6.8 22.9 0.1 04113/0611:58:01 1.0 5.3 23.1 0.1 04/13/0611:58:11 1.2 4.4 23.3 -0.1 04/13/0611:58:21 1.2 3.7 23.4 0.0 04113/0611:58:31 1.2 2.9 23.5 0.0 04/1310611:58:41 1.3 2.4 23.5 -0.1 04/1310611:58:51 1,3 2.1 23.6 0.0 04/13/0611:59:01 1.3 

### 1.8 23.7 0.0 04/13/0611:59:11 1.1 

### 1.6 23.7 -0.1 04/13/0611:59:21 1.1 

### 1.5 23.7 -0.2 04/13/0611:59:31 1.1 

### 1.4 23.7 -0.2 0411310611:59:41 1.4 1.2 23.7 -0.1 04113/0611:59:51 1.8 1.1 23.6 -0.1 04/13/0612:00:01 3.0 1.0 23.5 -0.1 0411310612:00:11 3.5 1.1 20.8 -0.1 04/13/06 12:00:21 3.8 1.2 11.6 -0.1 04/1310612:00:31 3.7 1.2 5.8 -0.1 04113J0612:00:41 3.3 1.0 3.1 0.0 04113/0612:00:51 2.0 0.7 1.9 0.0 04/13/0612:01:01 1.6 0.4 1.5 2.7 04/13/06 12:01:11 1.3 0.3 1.3 12.0 04/1 3106 1 2:01:21 1.1 0.3 1.1 24.7 04113/0612:01:31 1.1 0.2 1.0 37.1 04/1310612:01:41 1.2 0.3 1.0 48.0 04/13106 12:01:51 1.3 0.3 1.0 57.0 04113/0612:02:01 1.1 0.3 1.0 64.2 04113/0612:02:11 0.9 0.4 0.9 69.9 04113/0612:02:21 1.1 0.5 0.7 74.2 200 ppm CO Zero NOx

25.5 ppm NOx Zero CO, S02



# 11.6 Page 6

### 4113106 Ftun 42

04113/0612:02:31 1.2 0.4 0.7 77.4 04l13/06 12:02:41 1.1 0.4 0.7 80.2 04113/0612:02:51 1.1 0.3 0.6 82.1 04113106 12:03:01 1.1 0.4 0.6 83.5 04/1310612:03:11 1.1 0.3 0.7 84.5 0411310612:03:21 1.1 0.3 0.6 85.3 0411310612:03:31 1.1 0.3 0.5 86.4 04/1310612:03:41 1.0 -18.2 0.6 86.8 0411310612:03:51 1.0 -53.5 0.5 86.6 0411310612:04:01 1.0 0.3 0.5 89.3 0411310612:04:11 1:0 0.3 0.6 90.0 04/1310612:04:21 1.0 0.3 0.5 90.5 0411310612:04:31 1.1 0.3 0.5 91.2 04113/06 12:04:41 1.1 0.4 0.5 91.6 04113/0612:04:51 1.1 0.3 0.4 92.0 0411310612:05:01 1.0 0.3 0.4 92.4 0411310612:05:11 1.0 0.3 0.4 92.6 0411310612:05:21 1.0 0.3 0.4 92.9 04113/0612:05:31 0.8 0.2 0.4 93.1 04/1310612:05:41 0.8 0.2 0.5 93.2 04/1310612:05:51 0.8 0.2 0.4 93.4 04113/0612:06:01 0.9 0.2 0.5 93.6 0411310612:06:11 1.0 0.0 0.4 93.8 04113/0612:06:21 1.1 0.0 0.4 93.9 04/13/06 12:06:31 1.1 0.1 0.3 93.9 0411310612:06:41 0.8 0.1 0.4 94.2 0411310612:06:51 0.8 0.0 0.4 94.2 0411310612:07:01 1.0 0.0 0.4 94.3 0411310612:07:11 1.0 0.0 0.4 94.4 0411310612:07:21 0.9 0.2 0.3 94.4 0411310612:07:31 

### 0.8 0.2 0.4 94.6 04113l0612:07:41 

### 0.8 0.3 0.4 94.5 04113/0612:07:51 

### 0.9 0.3 0.5 94.6 04/1310612:08:01 1.2 0.2 0.4 

### 94.6 0411310612:08:11 23.6 0.2 0.5 

### 94.6 04l13/0612:08:21 42.1 0.3 0.4 94.4 0411310612:08:31 41.8 0.3 0.3 89.7 04113/0612:08:41 41.7 0.3 0.1 78.2 0411310612:08:51 

### 41.8 0.3 0.1 64.5 04113106 12:09:01 

### 41.8 0.3 0.1 51.3 0411310512:09:11 41.8 0.3 0.1 40.5 04/13/06 12:09:21 

### 41.7 0.3 0.1 31.8 04113/0612:09:31 41.6 0.3 0.1 25.2 Zero VOC

100 ppm S02

40.8 ppm CH4



# 11. "' 

### Page 74/13106 Rtm 93

Date/Tfine VOC CO NOx S02 mm/dd/yy hh:mm:ss ppm ppm ppm ppm 04/1310612:14:51 49.0 93.5 21.0 58.2

start Run tt3 04113/0612:15:01 48.8 94.0 20.9 58.4 04113/0612:15:11 49.1 94.5 20.9 5B.4 04113/0612:15:21 48.7 94.7 21.0 58.6 0411310612:15:31 48.8 94.8 21.1 58.8 0411310612:15:41 48.6 94.7 21.0 59.0 0411310612:15:51 48.5 94.2 21.0 59.0 04113/0612:16:01 48.5 94.2 21.0 59.0 04/13/0612:16:11 48.4 94.3 21.0 59.0 04/1310612:16:21 47.9 94.5 21.1 59.3 04113/0612:16:31 48.0 94.7 21.1 59.4 04/1310612:16:41 48.2 94.9 21.1 59.6 04/1310612:16:51 48.3 94.9 21.2 59.5 04113/0612:17:01 48.2 95.3 21.2 59.7 04/13/0612:17:11 47.8 95.7 21.1 59.6 04/1310612:1721 47.9 96.1 21.1 59.6 0411310612:17:31 47.8 96.6 21.1 59.6 04/1310612:17:41 47.5 96.8 21.1 59.6 04/1310612:17:51 47.4 97.3 21.2 59.6 04113/0612:18:01 47.3 97.4 21.2 59.6 0411310612:18:11 47.7 97.4 21.3 59.5 0411310612:18:21 47.4 96.9 21.3 59.5 04113f0612:18:31 47.5 96.2 21.2 59.4 04/1310612:18:41 48.0 95.3 21.3 59.4 04/13/0612:18:51 48.2 95.1 21.2 59.5 0411310612:19:01 47.4 95.1 21.2 59.6 04/13/0612:19:11 47.9 95.2 21.3 59.4 04113/0612:19:21 48.2 94.9 21.3 59.2 04/1310612:19:31 47.8 94.9 21.3 59.2 04/13/0612:19:41 47.9 95.3 21.4 59.2 04113/0612:19:51 47.7 96.0 21.5 59.1 04/13/0612:20:01 47.2 96.7 21.4 59.2 04113/0612:20:11 47.6 96.8 21.4 59.2 04113/0612:20:21 48.0 96.8 21.4 59.2 0411310612:20:31 48.0 96.5 21.4 59.1 0411310612:20:41 48.4 96.1 21.5 59.2 04/13/0612:20:51 48.1 95.6 21.5 59.2 04113/0612:21:01 48.0 95.5 21.5 59.2 0411310612:21:11 48.1 95.4 21.4 59.1 04113/0612:21:21 48.2 95.3 21.5 59.1 04/1310612:21:31 49.2 95.3 21.6 59.0 04/1310612:21:41 47.9 95.1 21.6 59.0 04/1310612:21:51 48.6 94.6 21.6 59.1 04/1310612:22:01 48.3 94.1 21.7 59.1 04/13/0612:22:11 48.5 93.8 21.7 59.1 0411310612:22:21 48.6 93.3 21.6 59.1 04/13/0612:22:31 48.6 93.6 21.6 59.1 04/13/0612:22:41 48.3 93.3 21.5 59.1 04113/0612:22:51 48.3 93.1 21.6 59.0 04/1310612:23:01 49.3 92.5 21.7 59.1 0411310612:23:11 49.4 91.9 21.6 59.1 04113/061223:21 49.3 91.9 21.6 59.1 04113/0612:23:31 49.5 91.9 21.6 59.0 04/1310612:23:41 50.4 92.1 21.6 58.9 04113/0612:23:51 50.6 92.5 21.6 59.0 04113/0612:24:01 50.0 92.9 21.6 58.9 04113/0612:24:11 49.7 93.1 21.7 58.9 04113/0612:24:21 49.7 93.6 21.7 59.0 0411310612:24:31 50.3 94.0 21.7 59.1 0411310612:24:41 50.3 94.4 21.7 59.1 04/1310612:24:51 50.7 94.7 21.7 58.9 04113/0612:25:01 50.3 94.7 21.7 58.9 04/1310612:25:11 50.0 94.9 21.6 58.9 04/1310612:25:21 50.2 94.9 21.6 58.9 04/1310612:25:31 50.0 95.5 21.6 58.8 04/13/0612:25:41 50.0 95.8 21.5 58.8 04/13J0612:25:51 49.2 96.4 21.5 58.7 04/1310612:26:01 49.5 95.4 21.6 58.8 04/1310612:26:11 49.4 96.4 21.7 58.8 04/13/0612:26:21 49.6 96.1 21.6 58.7

Page 1 

# 1184113106 Run #3

04113/0612:26:31 49.5 95.6 21.6 58.5 04113/0612:26:41 49.9 95.5 21.7 58.4 0411310612:26:51 49.7 94.9 21.7 58.3 04/13/0612:27:01 49.9 94.4 21.7 58.2 0411310612:27:11 50.4 94.1 21.8 58.2 04113/06 12:27:21 49.9 94.1 21.8 58.4 04/1310612:27:31 50.0 94.4 21.8 58.4 04/1310612:27:41 50.3 94.8 21.6 58.3 04113106 12:27:51 49.9 95.5 21.6 56.2 0411310612:28:01 49.5 95.8 21.5 58.1 04/13106 12:28:1

, 49.4 96.0 21.6 58.0 04/1310612:28:21 49.6 95.8 21.6 57.9 0411310612:28:31 49.9 95.6 21.6 58.1 04113/0612:28:41 50.0 95.2 21.6 58.1 04113/0612:28:51 50.4 94.7 21.6 58.1 04113/0612:29:01 50.5 94.5 21.6 58.0 0411310612:29:11 49.8 94.4 21.6 58.0 04113/0612:29:21 50.0 94.3 21.6 58.0 0411310612:29:31 50.1 94.4 21.6 58.0 04/1310612:29:41 49.9 94.3 21.5 57.9 04113/0612:29:51 49.9 94.4 21.5 57.9 0411310812:30:01 50.0 94.5 21.5 57.7 0411310612:30:11 49.4 94.8 21.6 57.8 04/13/0612:30:21 49.6 95.0 21.5 57.8 04113/061230:31 49.3 95.6 21.5 57.8 04l1310612:30:41 48.7 96.1

, 21.5 57.8 04/13/0612:30:51 48.2 96.3 21.5 57.8 04/13/0612:31:01 47.9 96.7 21.5 57.7 04/13/0612:31:11 48.0 96.3 21.5 57.5 04113/0612:31:21 47.9 96.3 21.4 57.5 04/1310612:31:31 48.0 96.3 21.5 57.3 0411310612:31:41 48.1 96.3 21.5 57.1 04/1310612:31:51 47.8 96.3 21.5 57.1 04/1310612:32:01 48.4 96.0 21.6 57.2 04/13/0612:32:11 48.2 95.7 21.5 57.2 04/1310612:32:21 47.8 95.3 21.5 57.1 04113/0612:32:31 48.0 95.4 21.5 57.1 04113/0612:32:41 47.6 95.5 21.5 57.4 04113/0612:32:51 47.7 95.7 21.6 57.4 04/13/0612:33:01 48.0 95.5 21.7 57.5 04/1310612:33:11 48.2 95.2 21.6 57.6 04/1310612:33:21 48.7 95.0 21.6 57.6 0411310612:33:31 47.8 94.8 21.6 57.8 04/1310612:33:41 48.0 95.3 21.6 57.7 0411310612:33:51 47.7 95.6 21.6 57.7 04/1310612:34:01 47.4 95.9 21.6 57.8 04/1310612:34:11 47.2 96.4 21.6 57.9 04/1310612:34:21 47.7 96.5 21.6 57.8 04/13/0612:34:31 47.9 96.5 21.5 57.8 04/1310612:34:41 47.3 96.0 21.5 57.7 04/1310612:34:51 48.2 95.3 21.5 57.7 0411310612:35:01 47.9 94.5 21.6 57.7 04113/0612:35:11 48.0 94.2 21.7 57.6 04/1310612:36:21 48.0 94.0 21.6 57.4 0411310612:35:31 48.2 93.9 21.6 57.4 04/13/0612:35:41 48.3 94.0 21.6 57.4 0411310612:35:51 48.2 94.3 21.5 57.3 04/13/0612:36:01 47.7 94.8 21.6 57.3 04113/0612:36:11 47.9 95.0 21.5 57.2 04113/0612:36:21 48.2 95.2 21.5 57.2 04/13/0612:36:31 47.1 95.4 21.6 57.1 04/1310612:36:41 47.5 95.3 21.6 57.3 0411 3106 1 2:36:51 47.6 95.2 21.5 57.2 04/1310612:37:01 47.3 95.6 21.5 57.2 04/13/0612:37:11 47.3 95.7 21.4 57.2 04/1310612:37:21 47.3 95.8 21.4 57.3 0411310612:37:31 47.3 95.6 21.5 57.2 04113/0612:37:41 48.0 95.3 21.5 57.1 04/1310612:37:51 47.7 95.5 21.5 57.1 0411310612:38:01 47.3 96.0 21.5 57.2 04113/0612:38:11 47.2 96.4 21.5 57.1 04/13/0612:38:21 47.4 96.4 21.5 57.2 04/13/0612:38:31 47.6 96.6 21.4 57.2 04/1310612:38:41 47.3 96.1 21.5 57.3



# Page 2 

# j i 

# g,4113i06 Rur #3

04113/0612:38:51 47.4 95.5 21.5 57.3 0411310612:39:01 48.6 95.2 21.4 57.4 04/1310612:39:11 48.0 94.9 21.4 57.3 0411310612:39:21 49.3 94.5 21.5 57.3 04/13/0612:39:31 49.2 94.2 21.4 57.3 04/1310612:39:41 49.3 94.0 21.4 57.2 04/1310612:39:51 49.5 93.9 21.4 57.2 04/1310612:40:01 49.6 93.8 21.3 57.0 4411310612:40:11 49.9 94.1 21.4 57.0 0411310612:40:21 49.4 94.7 21.5 57.3 04/13/0612:40:31 49.4 94.8 21.6 57.3 0411310612:40:41 49.3 95.0 21.6 57.4 04J1310612:40:51 492 95.4 21.5 57.4 04/13/0612:41:01 49.0 95.0 21.4 57.4 04/1310612:41:11 49.7 94.4 21.6 57.2 04/13/0612:41:21 49.9 94.5 21.6 57.0 04/1310612:41:31 49.5 94.8 21.6 56.9 0411310612:41:41 49.6 94.8 21.6 56.9 0411310612:41:51 49.5 95.0 21.7 56.9 04/13/0612:42:01 49.4 95.1 21.6 56.9 04/1310612:42:11 49.6 94.8 21.6 56.9 04/1310612:4221 49.7 95.1 21.7 56.9 04/13/0612:42:31 49.8 95.2 21.7 57.0 04113/0612:42:41 49.4 95.9 21.7 57.0 04/13/0612:42:51 50.4 96.4 21.7 57.0 3411310612:43:01 49.6 96.8 21.8 57.1 04113/0612:43:11 49.6 97.0 21.7 57.3 04113/0612:43:21 49.9 96.7 21.6 57.3 0411310612:43:31 49.4 96.9 21.6 57.3 04/13/0612:43:41 49.6 96.7 21.6 57.2 04/1310612:43:51 49.7 96.8 21.6 57.1 04/13/0612:44:01 49.0 96.9 21.5 57.0 04/13/0612:44:11 49.5 97.0 21.5 57.0 0411310612:44:21 49.5 97.2 21.6 57.0 04/13/0612:44:31 49.8 96.8 21.6 57.0 04113/0612:44:41 49.6 95.9 21.7 57.1 04113/0612:44:51 49.9 94.9 21.7 57.0 04113/06 12:45:01 50.1 93.9 21.7 57.1 04113/0612:45:11 50.0 93.8 21.6 57.1 0411310612:45:21 49.9 94.3 21.7 57.3 04113/0612:45:31 49.6 95.0 21.6 57.4 0411310612:45:41 49.8 96.0 21.6 57.3 0411310612:45:51 49.8 96.3 21.6 57.2 04/1310612:46:01 49.8 96.3 21.6 57.2 04/1310612:46:11 49.4 96.1 21.6 57.3 04/13/0612:46:21 49.6 95.8 21.6 57.4 0411310612:46:31 49.5 95.7 21.6 57.4 04/1310612:46:41 49.7 95.5 21.6 57.2 04/13/0612:46:51 49.9 95.1 21.5 57.4 04113/0612:47:01 49.6 94.8 21.4 57.3 0411310612:47:11 49.5 94.6 21.5 57.3 04/13/0612:47:21 49.6 94.4 21.6 57.3 04/1310612:47:31 49.5 95.0 21.6 57.4 04/1310612:47:41 49.4 95.9 21.6 57.6 04/13/0612:47:51 49.3 96.8 21.5 57.5 04/1310612:48:01 49.1 97.3 21.5 57.7 04113/0612:48:11 48.7 97.3 21.5 57.7 04/13/0612:48:21 48.6 96.8 21.6 57.8 04/1310612:48:31 49.1 96.4 21.6 57.9 0411310612:48:41 48.9 95.8 21.5 57.7 0411310612:48:51 49.0 95.3 21.6 57.8 0411310612:49:01 48.8 95.3 21.6 57.7 04113l0612:49:11 48.7 95.3 21.6 57.6 04f1310612:49:21 48.9 95.6 21.6 57.7 04113/0612:49:31 48.1 63.9 21.4 55.1 0411310612:49:41 47.6 21.7 21.4 56.9 0411310612:49:51 48.2 94.8 21.6 58.0 04/1310612:50:01 47.9 94.1 21.6 58.0 0411310612:50:11 48.3 93.9 21.6 57.9 0411310612:50:21 48.2 93.9 21.5 57.9 04/13/0612:50:31 48.0 94.4 21.5 57.9 04113/0612:50:41 47.9 94.4 21.5 57.8 04/13/0612:50:51 47.9 94.9 21.5 57.8 04/1310612:51:01 47.7 95.1 21.5 57.8

Page 3 

# 120411310$ Rtjn 93

04/1310612:51:11 47.8 94.9 21.6 57.9 04/13106 12:51:21 48.0 94.8 21.5 58.0 041310612:51:31 48.2 94.6 21.5 57.9 04113/0612:51:41 48.0 94.9 21.6 57.9 0411310612:51:51 47.7 95.2 21.6 58.0 04/13/0612:52:01 48.1 95.1 21.7 57.9 04113/0612:52:11 47.8 95.0 21.6 57.7 04!13/06 12:52:21 48.5 95.2 21.6 57.7 44l13t0612:52:31 47.9 95.3 21.6 57.7 0411310612:52:41 47.5 95.3 21.6 57.9 04/1310612:52:61 47.8 95.0 21.6 58.2 0411310612:53:01 48.5 94.6 21.7 58.4 04113/0612:53:11 48.9 94.6 21.7 58.2 0411310612:53:21 48.7 94.4 21.8 58.1 04/1310612:53:31 48.9 94.4 21.8 58.2 0411310612:53:41 48.6 94.6 21.8 58.1 04/13/0612:53:51 48.2 95.2 21.7 58.1 04113/0612:54:01 48.2 95.6 21.7 58.1 04/13/0612:54:11 48.0 95.5 21.8 58.1 0411310612:54:21 48.0 95.6 21.9 58.1 04/13/0612:54:31 48.8 95.3 21.9 58.1 04/13/0812:54:41 48.4 94.8 21.9 58.3 04113/0612:54:51 48.8 

### 94.4 21.9 58.4 04/13/0612:55:01 49.1 

### 94.4 21.9 58.3 04/1310612:55:11 49.1 94.5 21.9 58.3 0411310612:55:21 48.7 95.2 22.0 58.3 04/13/0612:55:31 49.3 95.4 21.9 58.6 0411310612:55:41 48.9 95.8 21.9 58.6 04/1310612:55:51 49.0 96.4 21.9 58.5 04/1310612:56:01 48.4 97.1 21.9 58.4 04/13/0612:56:11 48.1 97.2 21.9 58.5 04113/0612:56:21 

### 48.7 96.9 21.9 58.6 04/1310612:56:31 48.9 96.7 22.0 58.6 04/13/0612:56:41 48.9 96.2 22.0 58.4 04/1310612:56:51 49.1 95.9 22.0 58.2 04/13/0612:57:01 49.2 95.8 22.0 58.3 04113!0612:57:11 48.8 95.4 21.9 58.3 04/1310612:57:21 48.6 94.9 21.8 58.3 04/13/0612:57:31 49.3 94.1 21.8 58.2 04113/0612:57:41 50.0 93.7 21.9 58.1 04113/0612:57:51 50.5 93.8 21.9 58.1 04113/0612:58:01 50.0 94.2 21.9 58.0 0411310612:58:11 50.3 94.6 21.9 58.0 04113/0612:58:21 50.0 94.7 21.9 58.1 04/13/0612:58:31 50.2 94.5 21.9 58.2 0411310612:58:41 50.3 94.3 22.0 58.1 04113/0612:58:51 50.1 94.1 22.0 58.1 04/13/06 12:59:01 50.5 93.7 21.9 58.3 04/1310612:59:11 50.4 93.3 21.8 58.2 04113/0612:59:21 51.3 93.4 21.7 57.9 04/1310612:59:31 51.3 93.6 21.8 57.9 04/1310612:59:41 51.2 93.9 21.9 57.9 04113/0612:59:51 51.6 94.0 21.8 58.1 04113/0613:00:01 51.4 93.8 21.8 58.1 0411 3/06 1 3:00:11 51.6 93.6 21.9 58.0 0411310613:00:21 50.8 93.8 21.8 58.0 04113/0613:00:31 51.8 93.9 21.8 57.9 0411310613:00:41 51.6 94.2 21.8 57.9 04/13/0613:00:51 51.2 94.5 21.7 57.8 04/13106 13:01:01 51.1 

### 94.7 21.7 57.8 04/1310613:01:11 50.8 95.0 21.7 57.9 04113/0613:01:21 50.6 95.0 21.6 57.9 04/1310613:01:31 51.2 94.9 21.6 57.9 0411310613:01:41 51.4 95.0 21.7 57.8 04/13/0613:01:51 51.3 95.1 21.7 57.7 0411310613:02:01 51.2 95.4 21.7 57.9 04/13/0613:02:11 50.1 95.7 21.7 57.7 04/1310613:02:21 50.7 95.8 21.6 57.6 04/1310613:02:31 50.1 95.8 21.6 57.6 0411310613:02:41 50.6 96.0 21.6 57.7 04/13/0613:02:51 50.1 96.2 21.6 57.5 04/1310613:03:01 50.2 96.2 21.7 57.4 0411310613:03:11 50.2 95.6 21.6 57.5 04/1310613:03:21 49.9 95.0 21.6 57.5

Page 4 

# 1?14/13i05 Run 93

04/13/0613:03:31 50.4 93.9 21.5 57.4 04/1310613:03:41 50.0 93.2 21.6 57.5 04/13/0613:03:51 50.1 92.3 21.6 57.6 04J1310613:04:01 50.0 91.8 21.7 57.4 04r13106 13:04:1 Z 50.1 91.8 21.7 57.4 04113/0613:04:21 49.6 92.5 21.7 57.4 04/1310613:04:31 49.2 93.3 21.6 57.4 04/13J0613:04:41 49.5 93.6 21.7 57.3 0411310613:04:51 49.2 93.8 21.7 57.3 04/1310613:05:01 49.3 93.4 21.7 57.4 04/13/0613:05:11 49.2 93.1 21.7 57.3 0413/0613:05:21 49.4 93.0 21.5 57.3 0411310613:05:31 48.5 93.3 21.6 57.3 04l13/0613:05:41 48.4 93.5 21.7 57.2 0411310613:05:51 48.7 93.8 21.7 57.1 0411310613:06:01 48.2 94.4 21.5 57.1 04/1310613:06:11 48.8 94.6 21.5 57.1 04113/0613:06:21 48.2 94.7 21.5 57.1 0411310613:06:31 48.7 94.7 21.6 57.1 04/13/0613:06:41 48.5 94.2 21.6 57.2 04113/0613:06:51 48.3 93.3 21.6 57.3 04/1310613:07:01 49.0 92.9 21.6 57.5 04/13/0613:07:11 49.0 92.9 21.5 57.5 04/1310613:07:21 48.2 93.2 21.5 57.6 04/13/0613:07:31 47.8 93.3 21.6 57.6 04/1310613:07:41 48.4 93.1 21.6 57.7 04/13/0613:07:51 48.8 93.0 21.6 57.9 04/13/0613:08:01 49.4 93.3 21.6 57.9 04/13/0613:08:11 48.7 93.2 21.5 57.9 04/1310613:08:21 48.7 93.6 21.4 57.8 04/13/0613:08:31 48.2 93.8 21.6 57.8 04/1310613:08:41 48.1 93.5 21.5 57.9 0411310613:08:51 48.1 93.4 21.4 57.9 04/1310613:09:01 48.7 93.0 21.4 57.9 04113/0613:09:11 48.5 92.5 21.5 57.8 04113J0613:09:21 48.8 92.0 21.6 57.9 04/13/0613:09:31 49.0 91.8 21.5 58.1 04/13/0613:09:41 49.1 92.0 21.5 58.1 04113/0613:09:51 49.3 92.0 21.5 58.0 04113/0613:10:01 48.8 91.7 21.5 58.2 04/13/0613:10:11 49.1 91.8 21.6 58.1 04/1310613:10:21 49.0 92.1 21.5 58.1 04113/061310:31 48.7 93.3 21.4 58.0 04/1310613:10:41 48.1 94.0 21.5 57.9 04/13/0613:10:51 48.2 94.5 21.5 57.8 04/1310613:11:01 48.0 94.5 21.5 58.1 04/1310613:11:11 48.4 94.4 21.4 58.0 04/1310613:11:21 48.7 93.9 21.4 58.0 04/1310613:11:31 49.2 93.1 21.5 57.9 04113/0613:11:41 49.6 92.4 21.5 57.7 04113/0613:11:51 49.6 91.8 21.6 57.8 04/1310613:12:01 49.8 92.0 21.5 57.8 0411310613:12:11 50.1 92.5 21.4 57.8 04/1310613:12:21 49.7 92.7 21.4 57.8 0411310613:12:31 49.4 93.3 21.5 57.8 04/13/0613:12:41 49.7 93.1 21.5 57.7 0411310613:12:51 50.5 93.0 21.5 57.6 0411310613:13:01 49.9 93.2 21.5 57.6 0411310613:13:11 49.8 93.3 21.4 57.6 04/13/06 13:13:21 49.1 93.2 21.5 57.8 04/13/0613:13:31 49.3 93.1 21.5 57.7 04/1310613:13:41 50.0 92.8 21.5 57.6 04/13/0613:13:51 50.4 92.4 21.5 57.5 04/1310613:14:01 50.4 92.0 21.5 57.6 04/13/0613:14:11 50.4 91.8 21.6 57.7 04/13/0613:14:21 50.9 91.7 21.6 57.7 04/13/0613:14:31 51.0 91.4 21.6 57.9 04/13/0613:14:41 51.7 91.3 21.6 58.0 04/13/0613:14:51 51.0 91.3 21.5 57.7 04/13/06 13:15:01 51.2 91.9 21.5 57.6 04/1310613:15:11 50.5 92.6 21.5 57.7 0411310613:15:21 50.3 92.7 21.5 57.6 04/1310613:15:31 50.6 92.5 21.5 57.6 04/13/0613:15:41 50.4 92.4 21.5 57.6

Page 5 

# 1?24!13/06 Run tt3

04113/0613:15:51 51.0 92.3 21.6 57.6 04113l0613:16:01 50.8 92.6 21.5 57.7 0411310613:16:11 51.1 92.8 21.5 57.4 04/1310613:16:21 50.4 93.3 21.4 57.3 04/1310613:16:31 50.0 93.8 21.5 57.4 04/1310613:16:41 49.6 52.3 21.3 55.8 04/13/0613:16:51 49.7 87.1 21.4 57.1
Stop Run #3 49.08 94.26 21.57 57.93

04113/0613:17:01 37.7 92.8 21.6 57.0 04113/0613:17:11 8.5 87.6 21.3 56.9 04!1310613:17:21 9.9 57.6 16.5 54.5 04113/0613:17:31 8.8 28.9 9.6 48.1 04/13/06 13:17:41 6.9 15.2 5.9 40.3 04/1310613:17:51 4.7 9.0 4.2 33.1 04113/0613:18:01 3.6 45.7 3.2 26.6 04/1310613:18:11 3.1 109.8 2.4 20.4 04/13I06 13:18:21 3.1 143.7 2.6 16.1 04J1310613:18:31 2.9 167.2 2.2 13.1 04113106 13:18:41 2.9 178.7 1.7 10.6 04113106 13:18:51 2.8 183.9 1.5 8.3 04/13/06 13:19:01 2.7 187.0 1.3 6.3 04113106 13:19:11 2.5 189.0 1.2 4.5 04113l0613:19:21 2.5 190.3 1.2 3.2 04113/06 13:19:31 2.4 190.9 1.2 2.1 04113106 13:19:41 2.6 '191.4 1.1 1.3 04/13/06 13:19:51 2.6 191.5 1.0 0.7 04113/06 13:20:01 2.4 191.9 0.9 0.3 04/13/06 13:20:11 2.4 191.9 0.9 0.1 0411310613:20:21 2.3 192.2 0.9 -0.1 04/1310613:20:31 2.2 

### 192.3 0.8 -0.3 04l1310613:20:41 2.1 

### 192.3 0.7 -0.5 04/1310613:20:51 2.3 

### 192.3 0.7 -0.7 04113/0613:21:01 2.4 

### 192.3 0.6 -0.8 04/13/0613:21:11 2.4 192.1 0.6 -0.9 04/13/0613:21:21 2.3 191.9 0.7 -1.0 04/1310613:21:31 2.1 179.0 0.8 -1.1 04113l0613:21:41 1.8 108.6 6.7 -1.2 0411310613:21:51 1.7 52.4 15.1 -1.2 04l1310613:22:01 1.8 24.1 19.5 -1.2 0411310613:22:11 2.1 12.3 21.4 -1.4 04113/0613:22:21 2.0 6.5 22.3 -1.5 04/13l0613:22:31 2.1 3.9 22.7 -1.5 0411310613:22:41 1.9 2.5 22.9 -1.6 0411310613:22:51 1.9 1.5 23.0 -1.7 04/13l0613:23:01 1.8 1.0 23.1 -1.7 04/13l0613:23:11 1.8 

### 0.4 23.2 -1.8 04l1310613:23:21 1.9 0.3 23.3 -2.0 04113/0613:23:31 1.8 0.2 23.3 -1.9 0411310613:23:41 1.9 -0.1 

### 23.3 -1.9 04113/0613:23:51 1.8 -0.2 

### 23.3 -1.9 0411310613:24:01 1.9 -0.5 

### 23.4 -2.0 0413/0613:24:11 1.9 -0.7 

### 23.4 -2.1 04/13l0613:24:21 2.3 -0.8 23.3 -2.0 0411 3/06 1 3:24:31 2.6 -1.0 23.3 -2.1 04/1310613:24:41 

### 3.4 -1.0 22.9 -2.1 04/13!0613:24:51 3.9 -0.7 20.4 -2.1 04113/0613:25:01 4.5 -0.5 11.7 -1.8 04/13/0613:25:11 3.7 -0.6 5.8 -1.8 04/1310613:25:21 2.6 -0.6 3.1 -1.5 04113/061325:31 2.1 -0.9 1.9 2.6 04/13/0613:25:41 2.1 -1.0 

### 1.4 13.1 04113I0613:25:51 1.8 -1.3 1.3 25.1 04l13/0613:26:01 1.9 -1.3 1.3 36.6 04113/0613:26:11 2.0 -1.3 1.3 46.7 04l13J0613:26:21 1.9 -1.2 1.1 55.2 04/1310613:26:31 1.8 -1.3 1.0 62.5 04/13/0613:26:41 1.9 -1.3 0.9 68.6 04/13J0613:26:51 1.8 -1.4 0.8 73.6 04/1310613:27:01 1.8 -1.5 0.7 77.3 04113/0613:27:11 1.7 -1.3 0.7 80.6 200 ppm CO Zero NOx, S02

25.5 ppm NOx

Page 6 

# 1?34,13106 Run #3

04113,10613:27:21 1.6 -1.3 0.7 83.1 04/1310613:27:31 1.6 -1.4 0.7 84.7 04/13/0613:27:41 1.7 -1.3 0.6 86.2 04/13/0613:27:51 1.6 -1.4 0.6 87.5 0411310613:28:01 1.5 -1.5 0.6 88.6 04/1310613:28:11 1.5 -1.4 0.5 89.4 04/13/0613:28:21 1.3 -1.5 0.5 90.1 04/13/0613:28:31 1.5 -1.4 0.5 90.6 04113/06 13:28:41 1.2 -1.5 0.4 90.8 0411310613:28:51 1.2 -1.5 0.5 91.2 04113/06 13:29:01 1.5 -1.5 0.4 91.6 04113/0613:29:11 1.7 -1.4 0.3 91.9 04/13/0613:2921 1.7 -1.5 0.3 92.0 04113/0613:29:31 1.7 -1.5 0.3 92.2 0411310613:29:41 1.4 -1.5 0.4 92.5 04/1310613:29:51 1.5 -1.6 0.4 92.7 04/13/0613:30:01 1.5 -1.7 0.4 92.7 04/13/0613:30:11 1.5 -1.6 0.4 92.8 0411310613:30:21 1.5 -1.5 0.4 93.0 04/13/0613:30:31 1.4 -1.5 0.4 93.0 04/1310613:30:41 1.7 -1.1 0.4 93.1 0411310613:30:51 1.3 -0.9 0.4 93.2 04/1310613:31:01 

### 1.4 -1.1 0.3 93.2 04/13/06 13:31:11 1.6 

### -1.0 0.3 93.1 100 ppm S02 04/1310613:31:21 1.5 

### -1.2 0.3 93.2 Zero VOC. CO 0411310613:31:31 1.6 

### 4.2 0.4 93.1 04/13/0613:31:41 1.7 -1.2 0.4 93.1 04/1310613:31:51 1.9 -1.2 0.4 93.1 04/13/0613:32:01 33.0 -1.1 0.4 93.2 04/1310613:32:11 42.1 -1.1 0.4 92.3 04/13/0613:32:21 41.9 -1.0 0.1 84.1 04/13/0613:32:31 41.9 -1.2 0.1 69.3 04/1310613:32:41 41.8 -1.2 0.0 54.0 04/1310613:32:51 41.8 -1.3 0.0 41.1 04113/06 13:33:01 

### 41.8 -1.4 0.0 31.3 04113/06 13:33:11 

### 41.8 -1.2 0.0 23.9 40.8 ppm Methane 04113/0613:33:21 41.8 -1.1 0.0 18.8 04/1310613:33:31 

### 41.8 -1.2 0.1 14.5 0411310613:33:41 41.9 -1.1 0.1 11.6 04113/0613:33:51 41.9 -1.2 0.1 9.7



# 1?4
Page 7

# Appendix C

# ..._. J _._ _ ~ 

# __. _ .. . ............ . .....-.. .. Comments: G'l .7 ppm Methane

•s.00omV 

### Retentro 

### 0.050 .-,___ } 

### -

~

0.800 - 1 1.133 f 

### . - - - A,lethane 16,00otnV



### 865

4



## Component Retention Area Extemal

- 0.050 4.521 0.00

- 0.800 1.865 0.00 Methane 1.133 28.054 64.86
34.440 64.86



# 1. 13 8. . J .. _«. ~. ~ .. . .. ~ ...... . ... ~ ...... 

## Comments: 61. i ppm Methane

•B.OaUmV 

### Retentio '! 6.000mV 

### ExternallArea 0.100 - 

### ~~ — 0.0=.913
0.400 

### ~ . 0.00J2.482 0.63; 0.00/1.882

1 133 I - ` 

### ~ Methane 61.S3126.692

2

3

4

~ 

### Component Retentian Area Extemai

0.100 0.913 0.00

- 0.400 2.482 0.00

• 0.633 1.882 0.00 Nlettsane 1.133 26.692 63.58

31.969 61.56~ 

## ornrnents: 61.7 ppm M¢thane

-8.000mV 76.000mV 

### P,etent

0.333

0.766
1 133

CoRtponeRt FZeteritlon

- 0.333

- 0.766 

### Methane 1.133 Area Extemal

1.982 0.00 4.133 0.00 26.567 61.28

32.682 61.28



# 140

# . - -

~ 

# -•--- - .. . .. _ _ . _. ._. . _ COmments: Run #2 Bag Sample

•8.000mV 

### 1 B.00OrnV

0 083 ! 

### O.A86

_ d.d0/9.643
0.800 . U.0710.700

~133~~ Meftne I 8.53;4,058



### Camponent Retentian Area External

- 0.083 1.657 0.00 0.466 1.613 0.00

• 0.800 0.700 0.00 Aiethane 1.133 4.058 8.53

8.029 8.63



# 744

## Comments: Run #2 Bag Sample

-8.000mV 16.000mV QOfOf

~ t 0.09 B 0.300 0.600 0 6s0 1.133



### Component Fietention Area ExterrEal

- 0,016 1.078 0.00

- 0.300 2.813 0.00

- 0.600 1194 0.00

- 0.850 0.990 0.00 Methane 1.133 3.764 7.91

9.839 7.91r'a icabya#.: yaua. .d—To i i e...— + .., ~ 

## Cornments: Run 92 Bag Sample

-5.00+OmV 

### 1fi.000mV ExtemalfArea

133 i



### Component F2etention Area Extemal

- 0.818 0.962 0.00 

### Methane 1.133 3.823 8.04
4.785 8.04 L~ 

### .816, _ . ---- w--•-- 

## Cornments: 6 i .7 pprn II!{ettiane

v nnn...%r i6.OQOmV I3.01 g

~ tl
0 316 0.583 0.653
' 150



### Camponent Retentian Area Ext•emat

. 0.016 1.565 0.00

- 0.316 0.574 0.00 0.583 0.744 0.00

- 0-833 0.811 0.00 hAethane 1.150 25:849 59.55

29.543 59.65

L+

## Gomrnents: 61 .7 ppm Methane

•B.000mV 16.000mV

0.3t35 .379

0.883

1 133 4 

### Mlethane .94/26.a42



### Component netentian

• 0.3v"6

- 0.683 

### Methane 1.133 Area Extemal

1.379 0.00 2.093 0.00 

### 26.842 61.94

30.314 61.94



# 14 ~ ~

### 16.00Omv ExtemBElArea

57 •8.ODO .mV rZetenti - 0.26$

0.800 9;"E33 „. 

### Comments: 61. i ppm IlEiethane

Component Reterrfion

- o.2s6

d.8QQ Methane 1.133 Area ExtemaE
2.22D 0.00 4.393 0.00 26.957 62.22
33.870 62.22



# 1,16. ~.~w~ .Jww\ ~ w\M\.►• ti"I ~ 1 \lL..

~~ V \V.V\r.•'TV 

## Comrrients: RLtn 43 Gas Bag

•8.00DrnV 16.000rnV ' Retentl 0 200

0.833 1150

Camponent Retent€an

- 0.200
• 0.833 

### Methane 1.150 Area Extemat

3.853 0.00 1.474 0.00 4.726 9.93

10.053 9.93

~

# . , ._ ..---. _ .. . .._.._.. . _....,..... Cornments: Run #3 Gas Bag

-8.000mV 96AlYJmV

0.258 

### .523

0.800
1.133 1 IJleihene 

# ~ 9.92I4.718



### Camponent Retention Area ExiQmak

- 0.266 1.523 0.00

- 0.800 4.527 0.00 MetRane 1.133 4.718 9.92
10.767 9.92

~ . . 

# ~ ~V

## Comments: Run #3 Gas Bag

16.00OmV

-8.000mV Retentiti

0 316

+3.783
1133 1

2

3

4



### Component Retention Area Eactemat

- 

### 0.316 0.966 0.00

- 

### 0.783 3.697 0.00 Methane 1133 

### 4.902 10.30
9.466 

### 10.30



# 149J . _ ~ ~ .. . ~ r r.r • ..r •. . 

## Cornrnents: 61.7 ppm Niethane

•8.004mV

. 

### 16.00OmV

0o~o~t O.QOQ

O.S66

1 133



### Cornponent Retention Acea Extemai

• 0.000 3.780 0.00

- 0.366 0.891 0.00 N{ethane 1.133 26.986 62.29

31.657 62.29



# ~ EJL"1.r.ullvlw VM~r. V1/ 1 iJt_VVV i Y.~/~J.JV 

## Com=nsnts: 61 .7 ppm Nietiane

-8.000mV 18.000mV Retettl 0.900 0.400 0.600



### Componert Retention Area Extemat

• 0.100 0.987 0.00

- 0.400 2.210 0.00

- 0.600 1.169 0.00 Mcihane 1750 27.023 62.38

31.389 62.3$



# 151. ....~..... ........ ~ .. .......... .-r.v..•ti, 

## Comments: 61.7 ppm 4L4efhane

-s.000mv Reterstio

0.300

0.846 1 1.150

2

3



### Componertt Retention Area Extemal

- 0.300 1.967 0,00

- 0.816 4.191 0.00 Methane 1.150 26.026 59.9B
32.184 59.98 18 OOOmV Extertsa!lArea

• • 0.0011 .967

: - 0.0014.191 Methane 59.98126.026



# ~ 

# 52

## Cornrnents: Recovery Stuay Run #3 3aa



# -s.acoMv Ketent 0,050
0 400 0.700

' 133 

### ~ t j ,. - ' t 1 +1 ^ r •=y

. L 

### ~ 7 f 

### ~a.,~ 1~. , ~~ c Y`. ` i • 

### ~

1

16.00Omv

Corntaanent Retention Area Extemal

- 0.050 2.116 0.00 0.400 1112 0.00

- 0.700 0.519 0.00 ?Acthane 1133 13.692 30.18
17,439 3018



# 2-5

~



# 5

~ 

# .

, e

. ) + , ~ 

# 3 0

- 7



# 1.53

# ., _.. _r.

~ 

# . _ .. . .._ ....... . .........,._ Comments: Recovery 5tuay Rur #3 Bag

-$.000mV 16.00JmV



### Component Retentior: Area Extemal

0.200 1 .9 i a 0.00 0.516 0.580 OAO 

### 0.766 0.515 0,00 Methane 1.950 13.301 29.23

16.366 29.23



# 1 r n ~ 

# .

## Cornments: Recovery Stucly Run 03 Bag

-8.000mv 18.000mV netentio ExtemaGArea 0.083 

# j B.00Pt.9S5

4 450 - 10.0010.982

1 135 1 

# ~ I _ - -- - ARethane 

# ~ ~ 27.59/12.627



### ~



### Camponerzt Retention Area Extemat

• 0.083 1.956 0.00



### - 0.450 0.962 0A0 Methane 1.133 12.52: 27.59

15.544 27.59



# I 1rl

- . 5

# Appendix I)

## FILTER ANALITICAL DATA

Company: Dal-Itafia, Muskogee, OK Date: 4/12l06 Location: Kiln Scrubber Exhaust Run 1 Run 2 Run 3

Filter ID Number .50


# ~ : Date of Weighing 

# 41171

~ 

# qi 4f'

~ 

# fi

~ 

# 46:

Time 

# ::Z:23:

~ 

# fy1: 7~ 

# 22 A

~ 

# 1 :: ~ 2:~:~tM : Gross Filter Wt. .7

. Date of Weighing

Time : ~ 

# : 2

~ 

# :: Pi1t1 Gross Filter Wt.

Ave. Gross Filter Wt. 0.3939 0.3788 0.3902
Date of Weighing

Time i 

# 14

~~ 

# ? A

~ 

# !1;

~~~ 

# :38:i!aN(: Filter Tare Wt. Date of Weighing :2}V06: 100'

Time :9:2.7:AM: :3:0

~ 

# IIRM Filter Tare Wt.

Ave. Filter Tare Wt. 0.3611 0.3618 0.3612 Wt. of PM on Filter (grams) 0.0328 0.0170 0.0290 Total Weight of Particulate (mg) 32.8 17.0 29.0



# 160

## PARTICULATEANALYTXCALDATAFORNY Cnmpmny: oautona.Musxnmnu OK oote 4/12/06 LocoUon: Kx|nScruubmExhauot Run1 Run2 nun3 oonsitv(pa) '
exonxoonnontramon(:o) ninuevo|uma(Vaw) 

# 7. neaiuuainRinoo(Wo)=Oo°Vow°pa --__10.0V003.

Dato o,woi8hing ! |

Time Qro»»VVei8ht Dote ufvVwi8hinQ ~ 

# ww

Timo Q,00uvvoiQht !

Oate o/VVoi8hinQ

Time BoaxorTaroWei8ht / Doto ofYVoiQhin8 i 

# 6.

Timo BeokorTmrwvVo|Qht AxaroQoQruxsVveight Luuo 8|ank Roxidua(Wa) 0.0003 0.0003 xv B x T VV |

~ 

## t o,a8o no er are uo 1{06.7u483 1{04.7144 '

_ -- 113.3236



# Time

Time

Time

161

# PARTICULATE ANALYTICAL DATA FORM
Company: Dal•Italia, Muskogee, OK Date: 4/12/06 Location: Kiln Scrubber MeCL Rinse Run 

# 1 Run 2 Run 

# 3 Density (Pa) Blank Concentration (Ca) 

## io* Rinse Volume (Vaw) Residue in Rinse (Wa) 

# = Ca*Vaw*Pa 

## 0.0000 0.0000 0.0000

Date of Weighing

Time Gross Weight
Date of Weighing i 

# .8

Time Gross Weight

Date of Weighing 2

Time 

## '. ,7 .1 4 .,'A Beaker Tare •

Weight 

## 1 i -3: 5 ®r 5 4"::
Date of Weighing 

## 2

Time 

## .8* Beaker Tare Weight i 1 

## 5< 45
Average Gross Weight 

## 115.1974 113.5067 108.6863 Less Blank Residue (Wa) 

## 0.0000 0.0000 0.0000 Average Beaker Tare Weight 

## 115.1911 113.5054

. 108.6846 Weight of Particulate in Rinse (mg) 

## 6.30 1.30 1.70



# METHYLENE CHLORIDE BLANK ANALYTICAL DATA FORM
Blank Volume (Va) Date of Weighing

Time Gross Weight Date of Weighing

Time Gross Weight 

# I.Q. 5,19 .5 2::
Average Gross Weight 

## 105.19935 Date of Weighing

Time Tare Weight
Date of Weighing

Time 

## .2 ;4-* ? ~ 

## R. N4.- Tare Weight 

## 9~ 

## 2: Average Tare Weight 

## 105.19935 Weight of Blank (Ma) 

## 0 Ca= Ma/(Va'Pa) 

# = g/g 0 Note: In no case should a blank residue greater than 

# 0.01 mg/g or 

# 0.001% of the blank 

## lweight be - subtracted from the sample weight. 

# IS2

# oompany' oawmxa.muoxogoo ox omo:4/z2/O6 Lonabmn: KxnSoubbo, Impinger Smmiun

nun1 nun2 Run3

o P enoi

~ 

# v( a) / o|anx ooncpntration (Ce) ' R|nxovo|umo (vow) neo.duoin ninuo(vvo)=Ca°vow-*pa -----{ 0

. 0003 ' --_-_ 0

. 000 : 3 -__-/ 0 .) 0 { 3 ~ 

# Doto ofvveiBhin8

Timo ' G,000Woight Datp ofVVei8hin0 ! |

Timo omuuvvniQht 10 139 -N;

oatev/wwiohing

Timo ~ 

# aoaxo,Ta,eWeight !!! ! Douo of WeighinQ

Tima ' 

# MA BaakenTaroWeight ! ~~~ ~ 

# avera8oGnmoWwight L000 B|onk Rooidua(Wa) Avera8p BookorTanovYe8ht -_- 103

. 3864 ~

_ - 

# 102,7360

--- 108 .7 697 ' Vvei8ht n/ Partiuu|atp in R/n»o (m0) 5 

# i 1 J 0 --_-_ 11

. 90 ~ 

# '_-_--- 6

. 05



# Time

Time

Time

~ ~ C~ 

# ' ' `/

# Run2
! !

0.3964



# OFM --------

~~-~~

0.0202

~~~ Run3

0.4009

0.3833 ----'
0.0176
^-~ Cornpany: DoAboUa.W4uakogeo.OK Date: 4/13100 Lmcodon: ThrnKi|nExhoumt Runl

Oate W eighing 

# #1.177/M$'

T|me i

OobeofVVaigh|ng

|/nne

..... Oat»ofVVeighing

||rne F|lterToraVVt.

0.3773

.....
18.0 DohsofVVeigh|ng

Time

~ ~~~ `t ~ 

# r`

## Companx oautaUa.Muoxnuee Ox nmte:4/z3/O6 Lnnmuon: TrimKi|nExhouot Run1 Run2 Mun3 Don,itv0Pm Q|mnkCunoentmdion(Ca) | Rinoovo|umo (/aw) HooiduoinRinoo(wm)=Cm°Vaw°pm 0.0003 _---_ 0

. 00 x 02 ~ 

## -----{ 0

. 0003 ~ 

## Date uYWeigh|ng

Tima GmuoWei8ht Dmte ofWei8hing ~



## Time GmooWeiQh1

Oatoofwui8hing

Tima 

# jA Boako,Tm,oWai8ht Doto ofWoi8h|nQ

Timo BookorTomVve|Qht AvmoQaQmsxVVeight 113.6347 104.7395 l LesoB|onkResidue(Na) AvormQaBomkerTaraVVeiOht

--- 

## 113.6057 1{04.7258 106.5415 ' vVoi0htnx pmrLiou|ato in Rinse(mg) 28.74_ 13.51_ 7.19_

Time

Time

~ C~="

# PARTICULATE ANALYTICAL DATA FORM
Conipany: Dal-Italia, Muskogee, OK Date: 4/13/06 Location: Trim Kiln MieCL Rinse Run 

## 1 Run 2 Run 

## 3 Density (Pa)

~ : 

## 1,36:
Blank ConcenLration (Ca) Rinse Volume (Vaw) Residue in Rinse (Wa) 

## = Ca*Vaw*Pa 

# 0.0000 0.0000 0.0000

Date of Weighing

Time 

## 4 ., 

# M: 7

5 . i 

# 7 .7 Gross Weight 

# i 1- 0 ZZ Date of Weighing

Time 

## 4 .M: Gross Weight

Date of Weighirig 

## 6

; 

## 2

Time 

# 7 ".0 AM 0.*4;4 M 

# - 7t , 0 5'A Beaker Tare Weight Date of Weighing

Time Beaker 

## T are Weigh't 

# 1.10 .54:88: Average Gross Weight 

# 107.5859 110.5503 107.8992 Less Blank Residue (Wa) 

# 0.0000 0.0000 - 0.0000 Average Beaker Tare Weight 

# 107.5836 110.5488 

# 107.8969 Weight of Particulate in Rinse (mg) 

# 2.30 1.50 2.25



# METHYLENE 

# CHLORIDE BLANK ANALYTICAL DATA 

# FORM
Blank Volume (Va) Date of Weighing

Time Gross Weight Da'te of Weighing 

## 41' 

# 6

Time Gross Weight Average Gross Weight 

# 105.19935 Date of Weighing

Time Tare Weight Date of Weighing

Time Tare Weight Average Tare Weight 

# 105.19935 Weight of Blank (Ma) 

# 0 Ca= Ma/(Va.1.Pa) 

## = g/g 

# 0
Note: In no case 

## SIIOLIld a blank residue greater than 

## 0.01 mg/g or 

## 0.001% of the blank 

## lweiaht be subtracted from the sample weight. 

# i66

# company: OaUtaVo, mu,kooea.On oote: 4/13/06 LncaUnn: Thm0m. Imp i 

# nger Solutiun nunz Runo Run3 Donu|ty(pa) exonxConoontra |unOCo R|nooVo|umo(Vow) nouidupinR|nno(Na)=Co°Vmw°Pm 0.0003

oate o/WoighinQ `

Timo omsoWnmht DatoofWeigh|ng

Time Gmou vva|ght

Doto ofWei8hinQ

Timo Boaxe, TomWeiQhd Dote o/WeighinQ '

Time oeaxa,TamWeigm vwerageQmooWeight LoauB|onkRooidue(wa} A 8 k T vv i h ~ 

# verogo oo or a,o ag 127.4529 __- 126

. 0 7 00 ~ 

# 130.3480 vvoigh't-oxporticu|atoinR|nso(mg) -_-_-- 1 7. 9 V 0 _-_-_- 17

. 05 _--__ 11

. 45 '

Time

Time

Time



# 167

# Sheetl

Summary of Hydrogen Fluoride, Hydrogen Chloride, and Chlorine Analysis

Plant: Dal-Italia, Muskogee, OK Location: Kiln Scrubber L Date: 4112106
Run #

, Imp # Volume Dilution
-- . _,.. ~ 

# FI-, uglml

- HCI,

-. _ .. mg

- 

# CI-, ug/ml 'HCI, mg

_ _-- - •- - - 1 1& 2 500 1 0; .- - 0l - 0 0 1,1 & 2 500

. . . . . 1 0;

. . 0, 0 0 Average--

. --- - 0



# ;

. 0
2 1& 2

_._.. _ 

# 500,

------._ - ~ 

# -

1 0. 

# 451

- 0.236925 ~ 

# 0.64 ~ 

# 0.32896 2 1 &_2

_ , -. .

_500, i 046 -• 1

. 

# .

0242 

# 19 ,

~ 

# .--- --_ _ 0.68 - - _- - - ._- 034952

.. .. __ .

, ~ 

# Average

- 1
----- ( 0.239558 ~ 

# 0.33924 - 3 1 &2
-- - - 500 ;_

- - - _ 1j 0 .84 

# - ` 

# 0.4 422 

# 6 

# ; - __-- 0.71 r 0.36494 3;1 & 2

. ' 500!

.. 1' 0.89 ~ 

## 0.46 

# 8585_,_ 0.73 . ' _- - ----- —

0.37522 - -- ------._.. Average ; 0.455423; 0.37008 I iRun # ;Imp # ;Volume -Dilution CI-, ug/ml ' mg_

~ 

# HCI, 1 3& 4 250 1 0 i 0 1

. ; 1 : 3 & 4 250; 1 0 0_ 0 ,

. ._. 2 3 & 4 - - 250

~ 

# ----. _.

_. __.._. . 1.;__ 

# .- 0 ----- 0 

# ' 2



# ' 3 & 4 250

. . ~ 

# - - -- - - - .-

1 0 ~ ~ ._



# - - .- -- --

0 ' ; -- --- J 

# - ,_ 0 ~
~ 

# 3:3 & 4 '

250! !

1 01 01 . 3 4

• 

# 3& • 

# 250. -r - 

# 1 0 0' . 

## 0,



# Page 1

# Sheetl

Summary of Hydrogen Fluoride, Hydrogen Chloride, and Chlorine Analysis

Plant: Da!-Italia, Muskogee, OK Location: Trim Kiln ' Date: 4/131061

._ Run # -Imp # _. . -- -- - --- - - -•--

~ 

# ---- - - - Volume FI-, ug/ml HCI, mg CI-, uglml

. - -- - --- - ------ - -_ _. _.._ _Dilution - - HCI, mg

... . -- 1,1 & 2 300 10 27.97 ;
- ,.. 88.35723 ; 36.85 ,

. . - • 113.6454

- -- 1

~ 

# 1 & 2
- , 300
~



# . 1Q - 93.07187

_ 26. ,
_ . . . . _ - .._ 85

~ 

# .. ... _ ; 369

. l 113 79

.96

.. _... _. _ ;

. ; l ; , ,Average
~ 

# 86.71455 1
~ 

# 113.7225 _---- 

# 2 -' 1& 2

-- ~ 

# -- -- ° 

# -- -------+--

-- j

300


# .-- - -- ~ 

# ..__. - 1_ 290-



# 0 j -- --

- . -

3



# _ - ----- ----- -



# 91.705771 - --------- a

# 38.011

--- ~ 

# - - --- ---- 117.2228 211 & 2 300 1 1 - 10
~ 

# 29.22
- --- 92.3 

# 0598 -----•-

~ 

# 38.651



# - 119.1966

--------_ --- AverageL 

# I _

92.00588 i --

. -- - 118.2097

. _ .._ __ _.... 3 i 1 & 2

: 

# ' 300 ' .

, . ~ 

# . .



# 10 28.97; 91.51623

- ~ 

# ._ _ ._ ._ 34.81 , 107.354

.-_ 3;1& 2 300 10 27.78?
- - . _. 87.75702

- - - 35.67 110.0063

- Average 89.63663 ' 108.6802

I Run # ;_mp # iVolume ; Dil 

# ution CI-, uglml i HCI,

~ 

# --- mg --.._... ~ 

# .. - . - - --- -- -- - -- 1; 3& 4 -•--.-._.. . ~ 

# . . .. _._;

250

_ ..__ _ _ - 1~ 

# - 1.99 0.4975

~ 

# __ --------_ 1 ' 3& 4

. ... _ __.- 250
- - - - -- - - ------__ . . _ 1 L

_ . . - - - -- 2.08

~ 

# 0.50875

._ ~ 

# 2,3 4

„ 250';

, . _ , . 1' 1.7

. ---- ---. - 0.425

. 2;3 & 4 i 250! 1' i

- ~ -



# ` 0.4125'

~

. ~ 

# _ _ _.53 _ _ _ , . ~ 

# _ 

# -- .

~ 

# .. . - - l =. - --

~ 

# . 0
_. 3: 3& 4 i_ 250 ; 1; 2.15

~ 75~ 

# __. . 3!3 & 4 250
~ 

# - 1 f 2i 0.5
~ 

# . _. . '

~ 

# -- - 0.518751



# 1_6a Page 1

## 1.024.00OmV 

# Area Ey

~ 

# erna



# 105.95 

# ti/A 457.85 5.2

256.05 3.9 

# Conditions z 5.06 

# ug/ml Fl- in H2SO4

: 5.01 ug/ml 

# Cl— in H2SO4 Date 

# : 04/14/2006 Time 

# : 10:46:50



# 1. 

# 0 4 

# 0 0 rn V Component, Retenti



# (unkf..OWR) 

# 0.85 Fl- 

# I .

ci 

# - 1.60 op

..... .......



# ol 

# 21

:

.............. ................ . .... ............. I
.............. I
. . .......... ............... ... ................ ....... ........... ............. ...... I
................... ..... I
............. 

# Component Number Reteiition
Fl- 1 1.016 ci- 

# 2 1.600



# N 

# Area External Units
457.85 5.20 

# ug/ml 256.05 3.95 ug/ml

713.90 9.16



# 171

## :1024 ,.000mV --1. f32 . 4 0 0 in V 

# Component Retention 

# ( unknawn ) 0.



# ~~ nknown) o.



# Ci- 1. Area Eyterni 166.35 NO

105.20 N!f •442.55 5.{

251.80 3.8 

# Condit ions :§ :ft H@rfli

Date : 04/14/2006 

# Time : 10=49.14

Component 

# Number Rete nt i a n Area 

# External Units
F1-- 1 1.016 442.55 5.02 cag/m1. 

# C1-- 2 1.566 

# 251.80 3.89 ug/m1

2 694.35 8.91



# 1.72

# ( unknown ) 0.85



# F1- ?.

C1- 1.60 

# 122.70 h'lR 

# 882.85 10.4

450.50 7.5



# Area External Units

882.85 10.40 ug/m1 450.50 7.50 ug/m1



# 1333_35 17.89 Camponent
F1-- 

# C1— 

# Number Retention
1 1.016 2 1.600

lr~ } 

## f 

# C;On.di1..t 1S = f ~..~ 

# L'g. 1 m1. F1 - 1n h' 2SO4

ug/rni C1— in 1-12SO4 Oate = 04114/2006 

# Time - 10:57-°51

— 1 02 . 4 0 C? m V 

# 102 4 , On0mV 

# ComDonent Reientian Area ErLerna



# 373

## 1024.000mv 

# 61

......................... ................ .............. . ....... .......... .. .... ..................

6 

# 2 -102.400m1/ Component Retention (UnkDown) 0.01
(Unknown) 0.83 Fl- 1.


# ci- 1.56 Area Exterpa 229.10 

# NIA.

115.50 N/A 866.70 N 10.2

497.15 8.0 C

- c- , r(%-. 10 

## ri S 

# --%=k

- 1TS ugfM! F 

## H.2S 0 4. I - 0, Oj,,/ = Sftlel 

# ug/ml Cl- in H28O4 Date 04/14/2006 Time 11:00:10



# 4

Component Number Retention Area- External Units

Fl- 1 1.016 866.70 M 10.20 ug/ml 

# ci- 2 1.566 497.15 8.09 ug/m7.

2 1363.85 18.29



# 174

# 1024 .0OOmiJ -102 . 1 4

tGOmv Component Retention



# (unknoun) 0.



# Cl- i. 

# Area EXtern:

112.30 N/i 17II2.60 20.:

1059.89 17.; Canditiorrs z 20.22 ug/m 

# ~ F~~-- ~ .n H2504



# = 20.04. 

# ug/

~ 

# t C- i n F12804 Oate = 04/14/2006 T i me = 11 = 09 = 47



# Component
F1-- C1---

2 

# Number Retention Area External Units

1 1.016 1782.60 20.39 ug/ml 2 1.600 1059.89 17.72 ug/m 1

2842 _ 49 38.11



# 3 '~~

# Area Externa

112.50 H/A 1746.50 19.9

1064.65 

# 17,7' GondItions - ?-3 _22 t !gArd FJ.-- in F. 1 2S0n,



# '- 20.04 ug/mX Cl-- in hE22

- SO4. Date = 04/14/2006 

# TimP = 11:12:26

--102 . 404mV 

# Component Retention

{unknown} 0. 

# F1- 1.

C1- 1. ;l J24 . OOOmV i

. . ...... ~ '3 » . » .

. .»..... » . . ». «» ..»... ...«...» .... ............».... ................_... ........... ...» .....«» .».... «.»...... .. ............. « ........ .«.,..« .

. ~

.~ 

# 833 1 

# ...... _........ .. 

# . . 

# ... . 

# . :- ..::.::.::..............,..::: , :n , :.....,.... 

# ~
, I. ,» ....._.

'

~~ 

# ......_ 600 

# 2'

3

... :



# , . 4

. ~ 

## : #

~ 

## . ... :



# ComQonent 

# Number Retention Area External Units
F .1-- 1 1.016 17446.50 19.98 ug/ml 

# Cx- 2 1.600 1064.65 17.79 ug/ml

N 

## 2811.15 37.76



# 176

# o n d _ 

# i o ns 0 

# 4 1. m I r, H 2 1 S 0 

# 4 40,08 u.g/ml 

# CI.— in H2504 

# Date = 04/14/2006 Ti'me = 11:21:39

—102.4OOmV 1024.00OmV - 

# -omponent 

# Reteption Area Exte- ina



# (unknown) 

# 0.8 Fl- 

# 1.

ci- 1.6 ............................................................................._....._....................-..............................,...........................,..........,...................................,.............................

.. i 

# . .



# so

.............. . .

. . ................... . ..... . ........ .......... ............... . . . .............


# 66

.............. ............ ....... 

# 2

........ 

# ;,I

4

6

............. .............. .. . ......... .............. .............. ......... ....... .................... 122.45 

# NIP. 31462.30 

# 39. ~


# 2372.70 M 

# 491.4

Component
Fl— ci —

~ 

# Number Retention Area External Unite



# 1 1.050 

# 3462.30 39.51 ug/ml 

# 2 1.666 2372.70 

# M 42.44 ug/ml

5835.00 81-95



# i 

# 7Y

## 10 M' 4 0 017t 4r



## Component RetenU

: on 

# 1024 . JOOmV 

# Area Cxtprni

130.00 Pt/f 3439.00 39.2



# 2147.75 N 40.3 

# (unknown) 0. r" 1
- 

## Concii± ions = 40.44 ug/irl Fl-- zn H2SOA- = 40 _08 ug/m1 C].- in H2s04 

# Date = 04/14/2006 

# Time = 11:24-19

~



# Component 

# Numb'er Retention Area External Units
F ]. -- 1 1.033 3439.00 39.25 ug/'ml 

# C1-- 2 1.633 2247.75 M 40.30 ug/ml

2 5686.75 79.55



# 178

# AMQUNT I14JECTEt?

AREA 0.000 0.000

3450.650 40.440
1,

2 3

4

5 

# Calibrotion file - FI-,caI

Avg slope of curve = 86.11 Y-a x i s i nter cept = 0.00 Coeff of .l. 

# a. n r egr .' 0.97
No. Area Amount CF


# ca 

# = 0.000 0.000 0.000 1: 450.200 5. 060 88.972 2: 874.775 10.110 86.526 3: 1764.550 20.220 87.268 4 

# = 3450 .650 40.440 85.328



# 179

# AMOUN`f' IN3ECTED

AREA 0.000 O . C?OC



# 2310.225 40.080
1 

# 2 3

~

~

5 

# Calibratxon i ji le - :C - +. - _ cal



# Avg slop© of curve

~ 

# 53.95 YMa xi s i ntercept : 0.00 

# Coe•Ff of l a. n r egr

~ 

# 0.87
No M Area Amount CF
0= 0.000 0.000 0.000 1 = 253.925 5.010 50.684 2 » 476 .•075 10.020 47.512 3: 1062 .?_70 20.040 53.007 4= 2310.225 40.080 57.640



# .180

# Conditions = Dal-Ital i a, Kiln SGrubber = Run #1 Imps 1 & 2 = Volume 500 mis, Dilution 1J1 Date : 04f 14/2Q06 Time = 12=10:21

- 102 . 40OmV CoMponent Reten "

( unknawn ) 0. 1024 . 00OmV Area Externe

75.45 N/A

Component Number Retention Area External Units



# n 0 .0a 0.00



# 187

# Condit.ions = Oal-Yta? ia, hiln 5crubber = Run #1 Imps I & 2 = Volume 500 mis , Dilution 1/1 13ate = 04f14/2006 Time = 12=12:58

--.1CJ2 .4t ~Om~ 

# COnponent Rete€1'ti

(unknot-in) 0.85 1024 . OOOmV
on 

# ...._ ~ 

# ........ ~~ 

# ... ._............_.............. . .................,....._ .__.,....... ....MM...._. _.......... ...........
~ 

# .............................................._...._..,

'{ 

# ~ p

3 ~


# 2 . ...... ;'

. ! • I


# 3 . .... :

4 . ...... :

: !

~ 

# . , •

~

. ~



# ...... .. ...... _...._.............._.....__._...._.... ..... ............ .... .._....... ..._............... .._...w._........._..._.... ............ ............_._. . ................ _ ..............., i Area katerrii

1i1.55 EllF



# Component hlumber P.etention Area 

# External Units

d 0.00 

# • i♦



# r r ~ 

# i

## 1 024 . OOOmV —102 .400mV 

# CoMponenL Heten '

~ 

# V/ti 0.4



# 0.6 

# N/a 

# Area Externa

20.10 40.10 M



# 32.60 67.05 (unknown) 0. 

# F1- 1.

CI- 1. (unknown) 1. 

# Co-ndita.ons = Dal,-Stalia s lldln Scrubber

- Rv n#2 I mps 1& 2 = Volume 500 mis, Dilution 1f1 Date : 04714/2005 

# Time - 12=22-21



# Gomponent 

# F1

— 

## Ci—

EA 

# Number Retention

1 1.050 2 1.650 

# Qrea Exter nal Units


# 40.10 M 0.45 ug/ml 32.60 0.64 ug/ml

72.70 1.09



# 189

# (unknown) 0.

Cl

- 

# 1. 4unknown ) 1, 79.20 M NlAl 

# 40.50 FE 0.4

34.50 0.5 

# 72.95 NlA C~.~ 

# riditions - Dal—Italia, I.iln

z Run #2 Imps 1 & 2 = Volume 500 mis , .Dilutian 1/1 Date ' = 04f14/2006 Time - 12=24 =56

---1. 02 . 4 OOmV 1024 .000mti1 

# Component Retention Rrea Externc

Camponent
F l —

# cl2 

# Number Retention

J. 1.050 2 1.6 33 

# Area External Units

40.50 Ni 0.46 «g/ml 34.50 0.68 1..1 .,

~~ 

## ' / 1n l

75.00 1.14



# 190

# Conponent



# (unknown)
(unknown) F1- 

# (unknown) C1- 

# (unknorin) -.1 G2 , 4JOmV



# Retenti-on 0.

0.

~

.



### ~ 

# .

~

. 

# Area Extern 26.00 N/



# 31.50 74.99 

# 83.90
36.20 65.40 1 (324 . OOOmV



# o~

~ 

# r 

# 0. 

# NI

Area External Units
74.99 0_84 ug/ml 36.20 0.71 (Ag/tn 1.

111.19 1 .5b Component 

# Number Retention
Fl— 1 1.066 

# Ci— 2 1.650

2 

# C-onditi.ons = nzl-Italia, Ki.Ln Serubber

~ 

# Run #3 Imps 1 & 2 

# = Volume 50

~ 

# 3 mis, Dilut on 1/1 Date : 04/14/2006 

# Time = 12=33=55



# 1Q1

## W. O.B

. 

# fa! A 

# 0.7: 

# N/A 22.35 

# 79.07 M 79.53 PI 37.10 h! 52.85 fi 

# Component 

# (unknown)
(unknown) F1- 

# (unknown) Cl- (unknown) --3.

~ 

# J2 .400rnV 

# Retent' 0.0



# o.s 1. t.~ 

# 1.6 1.8 1 Q24 . OOOmV 

# Area Laterna 28.30 N/A Ccnditions = Dal—Ita1. ia , Ki.ln Sorubber

= Run #3 Imps 1 & 2 = Volume 500 mis, Dilution 1/3. Date = 04/14/2006 

# Time = 12 : 37 = 24



# F1— C.l Component

2 

# Number Retention

1 1.066 2 1.650 

# Area External Units

79.07 M 0.89 ug/ml 37 .1.0 M 0.73 ug/m 1



# 116.17 1.62



# ~2 ~~

# C0 r•( d i t i a TI W- D a":_ ._. ;: t a a. ia, T ri tri K?_ 1 n 

# :.Run #1 Imps 1 & 2 : Volume 300 mis, Dilution 1/10 E3ate = 04/14./2006 T i me = 12 : 4•6 = 20

— 1 02 . f OOmV 

# Component Retent' (unknown) 0.0 (unknown) 0.6 Fi- 1.



# rl- 1.7 1024.00OmV

a -------- , 

### ~ -. ...............»... ...«..............«......................................:::x:m:natr.:tacei:tus::t::r::it:r.iatnet:tiusat::;:t•



### ~ 

# .~ .

.:......... ......... ........... ...........,.............-:,• 2 

# ~ ....... : 

# ~ ,.

3' t ......» ;

e , S •

~ '•

. 

## 4 » ...... :

.

~
.
f ~

~ . . ~ .... .

' •

~ • • ~ 

# 6I

....,.. ; t

. I 

# ion o a 

# ~ ._.....__.w._... 

# ~

f~ : 

# 331 j; 

# Area Externz 35.80 

## t11fi
51.55 h/P 

# 2410,40 M 27.9

2109.00 M 36.8



# Component
F1- c i

KA 

# Number 

# Retention Area External Units 1 1.050 24 10 . 40 Ni 27.97 

# ug/rn? 2 1.716 2109 .00 11 36.85 ug/mi.

4519.40 64.81



# .1Q3

# Area Exterri.

31.10 

# ti/i 2324-05 H 26.'

2112.24 H 

# 30

1. , Conditioris : 

# Dal-Italia, Trim Kiln

: 

# Run #1 

# Imps I & 

# 2
: 

# Volume 300 

# mls, Dilution*1/10 Date : 

# 04/14/2006 Time z 

# 12:48:52

-102.4OOmV Component Reten

( 

## unknovin

# Flci1.024.00OmV

.. . ........................................... .......... ............ ......................... .... ................. ........ ... ................................. ........... .. ......... ............ ..........



## ~ ; ; 

# 78

............... 

# 716 ...... . ...... . ... . 

# 21

3 

## .. ......



# 5[

Component 

# Number Retention Area External Units 

# Fl— 1 1.050 

# 2324.05 M 26.93 

# ug/ml C 

# l- 2 1.716 

# 2112.24 11 36.90 

# ug/ml



# 2 4436.28 63.83



# 1 

# Q . 

# 4

# Oondi- tions - Dal--zta.lia, Trim Kiln 

# = Run #2 Imps 1 & 2 = Volume 300 mls, Oilution 1/10 Date = 04/14/2006 

# Time = 12-57=50

--102 .400rnV 

# r.omponent 

# Re;.en .

( unknawn ) 0. F 1

- 

## i .

C1-- 1. 

# Area Externi

28.25 h/ , 

## 2498.95 N 29.f

2181.40 H 38.i 3.024 , OOOmV



# Component 

# Number Retention Area External. Units

~ 

# 1- 1 1. 06.6 2498 - 95 11 29.03 ug /m 1 

# Cl.— 2 1.716 2181.40 M 38.01. ug/ml

2 4680.35 67.04

# Conditions : 

# Dal -Italia, Trirn Killn : Run 42 Imps I & 2 z Volume 300 mls, Dilution 1/10 Date : 04/14/2006 Time ". 13:00'.14

-102.4OOmV Component Retention 

# (unknoWD) 0. (unknown) 0. 

# Fl- 1.



## ci- 1. 

# 1024.00OmV

000 

# . . ...... . .. ......... . . ............. .......... ..... . ....... .......... I .............. I 

# ... ..... ......................... .........

516 J



# ........... . .................. .....

....... ........ u t ti I tt; -as t:33 III g; Im III I III III tto ImIll III I III III III in 1" 1-

J 

# 70 ............. ..... ..........

.. ..... ...... ............... 

# 2

4

. ..... .............. .... ...... . ................ .............. ...... ..................... 

# tirea Externa.' 23.30 

# NIA

23.53 5 N/A 

# 2514.85 M 29.2,



# 2221 .30 

# M 38.6%'



# Component Number R

~ 

# tention Area External Units
Fl- 1 1.050 

# 2514.85 M 29.22 

# Lig/ml ci- 2 1.700 2221.30 

# M 38.65 ug/ml



# 2 4736.15 67.87

## Dal—Italia, Ty-im Kiln Ruri #3 Imps I & 2 V41ume , 300 m1s,, Dilution 1/10 Date : 04/14/2006 Time : 13:09:02

—102.400niV component Retenti 1024.00OmV

u n 1. noii n 0.81 

# Cl - 1.08 

# ( it n k now 11 

## 1.43 

# ci- 1.75 on

.........................
6i :I



## ............. ..................

. . ..... .. ... . m ::z I an :3 m 1:3 14 1 m m 141 a 1 1!1 w m :;j M• 

## 31

........ . ...... ................... . ........ 31 1 1.

:1


## ........... 0 2 

# 31

41

6

. 

## .......... .................. ........ ........... ...... . .............. .......................... . . ..... Area Externa:

242.30 t-VA
2494.20 28.97 229.75 N/A
1982.20

Component Number Retention Area, External Units

1 1.083 2494.20 28.97 ug/ml 

# c 2 1.750 1982.20 34.81 ug/m1.

2 4.4,76.40 6:3 -78



# 19 7

# o -,- -' 

# - 1 

# t

~ 

# -- - 

# s - - a.. 1 - 

# I -

't-;a 'L i a , 

# Tr 1 

# m K ri t LJ

- 

# Run #3 

# Imps I & 

# 2
: 

# Volume 300 

# mls, Dilution 1/10 

# Date : 

# 04/14/2006 Time : 13:.11".30



# -102.4OOmV 

# LomponenL xetent

I tin knOWD) 

# 0.7 

# Fl- I

cl- 1.7 1024.00OmV

------- ----



# 501 

# 1[

... ... ....

...................... .............


# 16
. ........ ............. ........................

....... ..... ............................................ ...



# 3



# 4

6

. ......... 

# Area Externa

50.90 N/A 

# 2394.90 M 27.7

2035.55 

# M 35.6

Component
FlclrA 

# Number Retention Area External Units
1 1.050 2394.90 1\1 27.78 ug/ml 

# 2 1.716 

# 2035.55 11 35 .67 

# Lig/ml.

4430.45 63.45



# 198

# Condi Liuns - Dalw-Ital.ia , TrI.rr N;Ji ln = H23o4 Blank Date : 04/14/2006 Time : 13 = 2C3 = 40



# 1 n?4 . OOOmV - 1 U2 . 400;r;V Comaonent ?e4Ant:on 

# ( unknow , n ) 0.15
(unknok n) 0.85 Area 

# Extern; 28.40 iiIA

157.20 

# t/p

\ 

# Compone r3t 

# Number Retention Area External Units

0 0.00 0.00



# 19

~ 

# 9

## 3[ A

....... ...... I

... . . .. . ............................. 

## on 

# ol .... I 

## ................. ..... . ....... .......... ... . ......... j. C-24, 000mV



# 31 ......... J. 2. —102.4OOmV Umponent Retenti (Un 

# known) 0.00
(unknown) 0.83 Fl- 1.


# ci- 1.58 Area Externa 146.90 Nlt

157.05 h K 11.4 

## 1680.20 N 19.9



## 1037.10 19.6 co,ndi•ions Dad—Ital iLa, Trim Kiln 20.22 ug/ml FI.— in'H2SO4 20.04 ug/ml Cl— in H2SO4 Date = 04/14/2006 Time = 13:22:57



# 4t ......

51

6

............ ------

Component Number Retention Area External Units

Fl- 1 .1.033 1680 .20 1 , 111 

## 19.26 ug/m1. cI-- I-583 1037.10 1.9 . 6 1 u V rn.1

2 2717.30 38.87



# 0 0

# Conditi-ons = 5.01 

# ug/M'L Cl - 

# :Ln NaOH Date 04/17/2006 Time = 

# 08".17:10

-102.4-00mV 1.024.00OmV Compopept Retention



# (uBhown) 0.85 0! 1 i...».» ,='3

............



# 61 

# 21


# 3~ . »._. ; ;



# 4 1

6 1

......................... .......... ............... ............... ............. ................ . ...... ................ ............ ..................... ................. ........ .... ........... 

# ci - 1.81 Area E X , %., e T I , a

1205.20 IWA

291.45 M 4.4-

Component Number Retention 

# Ar ea External Units c). - 2 

# 1.816 

# 291 .05 

# M 4.44 ug/ml

1 291.05 

# 4.44



# 2 

# O'l

# Condi.tiGns -5.0:t u ~,~ 

# rnl C1--_ 3 i: ~`i~~~H 

## flate = 04/17/2006 Time : 08=21=16



# —3.02 . 4,00mRJ 102•4 ., 000mv 

# Component ?eLentic;t ~ Rre~ t~t~ 

# ,rnz.

-----------

~ 

# -----------------

~ 

# -----------------------....-- . 

# --------------------.......----

~ 

# ---.....------------------- . 

# ------................................._......................................_.................................................._..........................

(unknown) 0.83



# Cl- 1.81 I

~ 

## .. .... ~ 

## . 

# :r

2

~



### ~ 

## .... ~ 

## .. : 3 1 

# I :

~ ~ 

## ........ :

~ 

## .... ~ 

## .. : 

# 1187.10 NIA

293.60 M 4M

Component 

# Number Retention Area Externai Units

C1-- 2 1.816 293.60 M 4 .4.8 ug/ml

1 293 _ b0 4.48



# 202

## ( upkilokin ) 4.83



# Cl- 1.81 1159.20 N/R



# 521.40 P1 14.0; ro;i d i t '"..ions "- 10.02 l.E9/i7?.i Qate = 04f17f2006 Timc - 08:25.03



# —102 . 4nQE"nV rompor,A nt f;etent ion 10 ' Y . C) 0 :,' M V 

# Prea EYt.eE n;

Component NLimber Retention Area External Units

~ 

# 1- 2 1.816 521w 4a 11 10.02 uq/rn:L

~ 

# 521 .40 10.02



# 203

# Conditions - 14.02 ug/rnI :in No4H Date : 04/17/2006 Time ; 08=28=34

~~1.02 ,.4•0OmV 

# Componpnt RoteRtion

(unknown) 0.



# C1- 1. 1. 024 . ~1C)~.~mV 

# Area Externa

1162.10 N/4

516.10 M 9.9



# Component Number Retention Area External Units
C1— 2 1.816 516.10 M 9.90 ug/ml

1 516.10 9.90



# 2 n 4-

### f-o 

## nd i ti c, 

## ns = 15 . 03 c.! g/ ml 0l

. .-- i ri Nat31l DatQ : 04/17f2006 Time = 08=32=10

-102 . 4OOmV Componeni. Re{en

.

(unknown) 0.



# ci- I . 1024 .00OmV ATea Ext.T n=

1128.34 N/f

854.44 H 15.(

Component Number Retention Area
C 1:-- 2 1 . 81. 6 854.40 I1

1 854.40 External Units 15.03 (Ig/m:L

15.03



# 2n5

## 1 G2{- . OOOmV 

# . 15 , 0: ~ u 

# C-1J`rn1 C n N, ::

~ 

# 0H = 44/17/2006 

# = 08=35=27

0~ 

## ., ~ 

## 0 0 m

~ 

## , 1 

# C:onditionw 

# Date Titne

Componenf Petentian



# (unknawn) 0.

el- 1.. 

# Area Externa

1108.40 N/P

802.80 Pt 14 . 2-



# Component 

# Number Retention Area External Units
C1

- 

## 2 1.816 802.80 M 14.26 ug/ml

1 802.80 14.26



# 206

# Con di tiors:S Date Time

Compo7svi r

~~ 

# }ent

~ 

# 4n

(unknawn) 0.



# CI- 1. : 20 .o! ug/mi C1— 1 rj t4a0i-! 

# = 04/ 17/2E)O6 = 08=39=d1

Id2 _ 400rnV 

# 1024 .00OmV 

# Arca Externa

1098.80 NlA

1193.60 M 20,9:

I 

# component h[umber Retention Area 

# External Units ci- 2 1.833 1193.60 M 

# 20.93 ug/ml

1 1193.60 

# 20.93



# 207

# Conditiarts : 20 _C=

~ 

# 'T ugf":Y

~ 

# ? a_n INIa'OH, Date : 04/17/2006 7ime - 08 = 41-`- 50

—102 .40OmV 

# Component Retention



# (unknown) - o.

Ct- 1. 

# 1024 . OUOmV Area

~ 

## .-zterni

991.20 lV/P



# i198.50 m 21.0

Component 

# Number Retention Area External Units
C1. — 2 1.833 1198.50 Ni 21.01 ug/ml

1 1198.50 21 .01



# ~~ 

# s

# AMOUNT INJECTED

AREA 0.000 0 . OOC)

1'-IL96.050 

# 20.040
1

2

3

4

9 calibration fila -. 

# cl- Clal



# Avg slope of curve: 59.68 Y-axis intercept: 0.00 Coe-ff of lin regr: 0.81
No. Area Amount CF 0: 0.000 0.000 0.000 1: 292.325 5.010 58.348



# - 518.750 10.020 51.771 3 828.600 15.030 55.3.30 4 1196-050 20.040 59.683



# 209

# Conditio- tis : 

# Dai-ltalicsx, Kilil 'Scrubber
: Run #1 Imps 3 & 4
: Volume 250 Dilution 1/1 Date : 04/17/2006 Time " 09.".11.-21

-102.4OOmV compopent Retenti



# (u ilk now 1 1) 0.83



# ~ unknown 

# ~ 1 : 90 

# unknown 2 1.024.000mV Area ExteTne"

556.35 N/A



# 125.40 

# NIA 216.80 

# N/A 02

................ ......... . .......



# 2

....»..



# 6

........

...... .....

Component Number Retention Area External Units

op, 0.00 0.00



# 216

## L o n d ]. t ]. o ns



# Date Time

Coraponpni Reten .

(un-knowr) 0.



# ~ unknown 

# ~ 1. , unknown 2. 

# - t.) al —rtai za , !\i I n =ti ruh- bei

~ 

# Run #1 Zmps 3 & 4- : Volume 250 Dilution 1/1
: 04r17f2006 : 09 : 1.4 : 01

1.02 . 4OOmV 102"4 .00OmV 

# Area Externa

571.85 h/A

223.60 1i/ A 

# 223.70 

# N/A

Component Number Retention Area 

# Exter nal Units

0 0_ 00 0.00



# 217

# $ unknot

~ 

# n ) 1.93

,unknown} 2. , i : : . 3_ rI .1 C..:1 ^ U. t~ 1> t~ i

~ 

# 3

~ 

# ; 4 

# Di.lution I/1

:1.;32q• .C?

~ 

# `7Dm ~J 

## io~


# ...................... _................. .................... . ... ... ..... .................. .... ....... ........ .......................... . ....... ......... ................. . ............ ............. ................................................ .................... ...... , ,

.~ 3 : ~ t

„ ~
........ ; ......». y=::r

.

~

......... t.• ~ ' ,..:.....: t

.~

" »... : i ' ....:.... » • .• • ••. •-•..•••• = 

### ~ m=r.m:raennu=aJat:tn[tr.tznttttr 

### ~ 

# 2 

# :::: ~•. ~ ~_

3

. ~



# . , : I 4



# ..... ;

~

51 f 

# ....... ;

t 

### , ; ; •

6'

~ 

# ...._..w..._.... ........ ... .............. ... .......................... .. ..... .................... ........ ....... ......... ................................ ............... .... ...................... C Gi :_ — .1. Z. ai I i G1



# - 1?un #2 Imp = Volurne 250 Date = 04/17/200e T im w= 09 = 22 = 45

~~ 1 02 . 4OOmV 

# uomponept Rete

~ 

# L'

(un(cnou

~ 

# n) 0.8 Area Externa

580.90 IUA



# 1641.50 N/R 326.54 

# N/A



# Component ivumber Retention 

# Area External Units



# n 0.00 o _oa



# 018

# c ti.:r n d i %. t o n s • g

~ 

# ? 1 - I t a 1 l 4

~ 

# ., -- c r u b b e r 

# = Run #2 Impe 3 & 4 = Volume 250 Dilution 1/1 Date : 04J17r2006 Time - 09-25=29

—102 .400mV OmPonen't ReTeti' ,



# n known) 0.



# unknown 1. un;cnawn 2. 1024.000inV 

# Area Externa

577.15 N/A

1604.55 iV/A 320.75 N/A



# Component hlumber Retention Area 

# External Units

C} 0.00 0.00



# 219

# 0 -n n 

## d. L IL-. I'L 

## 0 11-1 

## S : D a -a l i a 

## C 1- L Ob bi& 

## r : 

# Run #3 

# Imps 3 & 

# 4
: 

# Volume 250 

# Dilution 1/1 

# Date : 

# 04/17/2006 Time : 

# 09:34:30

-102.400ffiV Componept 

# ReteDti

(unknown) 

## 0.85

(unknown) 2. 

## 1024.000mV



# on



# 0

..............



# 2

......



# 3



# 4

......



# 5~ 

# ......_ :

~

6

I

..... . .......... . ....... . ....... . .......................... 

# Area ExteTna

630.50 

# ti/A



# 241.80 N/A,

Component Numbet Retention 

# Area External Units

Et 0.00 0.00



# 9 2 . 0

,.

I

# c-or,di.tions - Dal--Itali.a,. ;:i.ln Sot u

~ 

# ber : Run #3 Imps 3& 4 = Vo3ume 250 

# Dilution 1/1 Date = 04/17/2006 Time : 09=37=12

-- 1 Q 2. 4 c) O mV 

# Component Reteniion



# 'Un{,nowr.) 0.



# uEtknolrn 1. 

# un k 

# nown 2, 1 024 . 000mV 

# Area Externa



# 561.30 N14

103.80 NIA 248.70 h/A



# Cornponent Number Retention Area External Units

x COMM, 

# s ••

221

# Rrea Externe

781.41 M. NIR

116.14 

# 531.74 NIA 

# Condii.ions = Dal—It a1 ia. z Tr im Ki ln



# : Run #1 Imps 3 & 4 = VQlume 250 Dilution 1/1 Date = 04/17/2006 

# Time - 09=46-04

— 1 G2 . 400mV 

# Component Reten

( unknown ) 0.



# C1- 1. 

# (unknown) 2. 1.024 ..00OmV

i



# ~ 

# ._....._.»...... ~ 

# .» ............_...._....»...........»w...._..._....._............._...._._.»................_.........».»..........._.» ...............».............._._........».......................». i

9JJ 

# ~ •. ,.:.:nerr 

# ~

733; ~

~ 

## ......... ~ r~ 

## .....»,.... 

# 2

~~ 

## .

3 ....... :

4

5

~ 

## »...... ;



# 5 . ».... ;



# Companent 

# Number Retention Area External Units
C1.-- 2 1.733 116.10 M 1.99 

# ug /m 1

1 116.10 1.99



# 2 2-2

# Condit'Lons z 

# Dal-Italia, Trim Kiln
z 

# Run #1 

# Imps 3 & 

# • : 

# Volume 250 Dilution 1/1 

# Date : 

# 04/17/2006 Time : 09:48:55



# --- 102.40n-mV 

# coloponepi't Reten
(unknown) 

# 0. 

# (Unhown) 0.

ci- 1. 

# (upknown) 1. 1024.00OmV

........... . .......... .......... ......... ......... ............................... . .......... . ................................................................. .................................................... . ................................. . .............................. 

# 450 

# 833

1 

# ~ »«..... '.i
.. il 

# ~ , "'



# ~

2

3i ».».» : 

## ~



# 41



# 6 k0a 

# ExternS

206.60 

# KIIA 766.30 

# N / 

# P"

121.65 H 

# 2.0


# 531.70 N/A

Component 

# Number Retention Area External Units 

# cl- 2 1.733 121.65 

# M 2.08 ug/ml

1 

# 2.08



# 2P3

## 1024.00OmV Area 

## Externa

834 

# .70 N ti/Al



# 99 

# .40 M 1.71 

# 542.80 N/A 87.35 ii/A 

# Conditi•ns Dal-.Ita.).ia, Tir-im Kilri Run #2 Imps 

# 3 & 4 Volume 

# 250 Dilution 

# 1/1 Date 04/1712006 Time 

# 09:58:13



# --'.02 .400rriV uomponenL metenti



# kunkpowo)



# ci- 1,66 unknown 

# 1.95 unknown 

# ~ 2.



# 41

6--



# ..... . .. . ..........
Component Number Retention A-rea External Units


# cl- 2 

# 1.666 99.40 M 

# 1.70 ug/ml



# 1 99.40 

# 1.70

OB

3



# ~ !. 

# 0 

# 2



# 2P4

## Condit ions Dal-Ital -ia,, Trim K i l i-I 

## Run #2 Imps 3 & 4 Volume 250 Dilution 1/1 Date = 04/17/2006 Time = 10:09:57

-102.4OOmV uompoDent Retent

I k 

## un k now n) 0.8

C l- 1.6 unknown 1.9 unknowni 2. 102"4 OOOmV IH



## 33

16 50 2



# 41

6

........... .................. ....................... ....... .......... 

# . ........................... ............ .. ........ ...................... .... ...... ........... 

# Area Externa

836.30 H N/A

93.25 H 1.6 537.86 

# N/A 82.30 ii/A

Component Number Retention 

# Area Ekternal Units 

# ci— 2 1.666 

# 93.25 M 1.60 UgIml

1 93.25 1.60



# 2 2 wo

# i. o i i{ ~ 

# J. t:t v n` s • L.j a . 14 L_ 

# = Run #3 Tmps 3 & 4 = Volume 250 Dilution 1/1 aate : 04/17/2066 rime = 10:19.19

— 1 U2 . f.QamV 1024 . OofJmV 

# Component Retention



# ~ .. .............,,.... 

# ~ .. ........................................................................................_.......................,,..,.............,..................,......................,,................... .....,.........................,........,,.....,.........' Ar 

# ea E 

# xterr li

. 

# 4.833i

~ ~ 

# , . 

# ........ ~ »»

.... • t ~

.t ~ • 

# ` 8 60.53 P1 ~if~



## C1- 1.666 

# ~ 1

, 

## Inl 125.65M 21



# 1.954


# ~ .. 

# ~ r , k , kl

. : 527.44 N/R



# ~ unknown unknoun 

# ~ 2. 21 ....»., 74.70 N/A

Compone»t 

# Number Retention 

# firea External Units
C1-- 

# 2 1.666 125.65 M 2.15 u.g/rnl

1 

# 125.65 2.15



# 926

# Component

~ 

# unknown }

~ 

# unknowp;

C1- 

# unknown 

# unknown 

# ~ - w02 . 4OCSmV



# Reter
0.
0.

1, ?, 

# :€. 024 . 0OOrriV Area Ea

- Lerna 122.30 N/A
857.00 tr•/A



# 116.70 M 2.0 534.90 N/A 

# 70.95 NIA niticn^ - Da1.--italia, Tr° 7 ff: ':i? n



# : Ru n#3 I mps 3& 4 = 'dolume 250 Dilution 1!1 Date : 04! 1 i t2006 

# Time = 10-22=15

Camponent 

# NUniber - Retention Area External Units 

# cl- 2 1.650 116 .70 Nf 2.00 ug/m1



# 1 116.70 2.00



# 227

# o ris
Da-te Time



# compoDent Reten D al — I T-1 - i rf! 

# K 

# 5 -01 ug/ml C' i ri lqIOH 

# 04/17/2006 10.-31:45

102.4-00MV 1.024.00OmV Area Externa.

1209.85 H N/A

306.20 H 5.3, (unknown) 0,



# ci- 1.

Component Number Retention Area External Units
Cl - 2 1.800 306.20 M 55.32 ug/ml.

I 306.20 5.32

## Conditions


# Date Time

Component RetentioD D a. 

# 1 — I t a 

# 1 i a. Ti- i ri L 11<i i' 

# 1 rn NaOH Blank 04/17

~ 

## '2006 

# 10: 34: 

# 30

1, 0 "c"' , - A 0 0 m V 

# 1.024.00OmV Area Externa

(uDknown) 0.83 

# 31 1188.00 NIA



# 2



# M®

6

............. .......... .. ....................... 

# — .. . ....... . ........... . . ................. . ................. ... . ... 

# Component Number Retention Area 

# Ex"Cernal Uni"Ce

'ED



# 22,9J11n1plo

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# 259APE Armstrong Environmental Inc. CONVERSION FACTORS EPA Method 5 522 Series Meter Box Calibration 1 mm Hg - 0.13330 kPa Pre-Test Oririce Method 1 cm = 0.39370 inch Englisti Meter Box Units, English IC Factor 1 mm - 0.03937 inch 1 cu ft = 28.32 liters eter Box f 10 Date: -------------------------> 03/15l06 trial #: 30272 Barometric Pressure: ----------> 29.95 (in. Hg) Tfreoretica) Critical Vacuum:---> 14.13 (in. Hg)

illltt 

### IPORTAI% For valid lest resulls, Itre Actual Vactrum should be 1 lo 2 in. Hg greater than the Theorelical Critical Vacuuni shown above. 1PORTAI% t!!!l •. 

### The Critical Orifice Coefficient, K', rnrrsl be enlered in English units, (ft)"3•(deg R)^0.5/((in.Hg)'(min)).

------ --------- DRY GAS METER READINGS ------------ -CRITICAL ORIFICE READINGS-
-- Average Temperalutes -- 

### Volunie Voitime Voliirrie Initial Temps. Final Temps. Orifice K' Oririce Actua) -- Ambiont Temperature -- DGM DGM Ambient ciH Tin e Initial Final Totat Inlet Outlet Inlel Oullel Serial# Coelficiont Vacuum (rtilial Final Average Outlet Overall Temp► 

### H20) (niin) (cu fl) (cu ft) (cu ft) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) (deg F7 (deg F) (deg R) (deg R) (deg R) 0.24 5.00 652.700 654.270 1.570 66.0 65.0 66.0 65.0 40 0.242 23.0 64.0 64.0 64.0 525.0 525.5 524.0 0.50 5.00 654.600 656.847 2.247 66.0 66.0 66.0 66.0 48 0.344 21.0 63.0 64.0 63.5 526.0 526.0 523.5 0.93 5.00 657.500 660.520 3.020 66.0 66.0 67.0 66.0 55 0.464 19.5 64.0 64.0 64.0 526.0 526.3 524.0 1.60 5.00 661.300 665.172 3.872 67.0 66.0 68.0 66.0 63 0.693 18.0 64.0 64.0 64.0 526.0 526.8 524.0 2.90 5.00 656.000 671.320 5.320 68.0 66.0 71.0 68.0 73 0.824 16.0 64.0 64.0 64.0 527.0 528.3 524.0

................................................. RESULTS ...................................................
• DRY GAS METER --- --------- ORIFICE --------- -- DRY GAS METER -- --------- ORIFICE ---------



### XUME VOLUME VOLUME VOLUME VOLUME CALIBRATION FACTOR CALIBRATION FACTOR ORRECT CORRECTED CORRECT CORRECT NOMINAL Y dHQ Vm(std) Vm(std) Vcr(std) Vcr(sld) Vcr Value Variation Value Variation (cu ft) (liters) (cu fl) (lilers) (cu fl) (number) (number) (in H20) (in H20) 1.579 0.1 1.585 0.1 1.572 1.004 0.003 1.352 -0.0635 2.260 0.1 2.253 0.1 2.233 0.997 -0.003 1.391 -0.024 3.039 0.1 3.035 0.1 3.010 0.999 -0.002 1.427 0.011 3.899 0.2 3.882 0.2 3.850 0.996 -0.005 1.500 0.084 5.359 0.2 5.389 0.2 5.345 1.006 0.006 1.408 -0.008 

# Average Y ------- > 1.000 1.416 <------- Average dH@

ote: For Calibration Factor Y, the ratio of the reading of the cafibration meler to the dry gas meler, acceptabie tolorance of individtial valttes from the averago is +-0.02. 

### For Orifice Calibration Factor dH@, tlte orifice differential pressure in inches of H20 ltial equales to 0.75 efm_of air at 68 F and 29.92 inches of I-ig, acceptable jolerance of individual Nalues from lhe average is +-0.2.

.-. ~ - _ SIGNED:

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. Date: 

### ~ 

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# Temperature Meter Calibrations

Meter Box #: 10 

# Date: 03/15/06 

# Calibrated By: RT

Emtech 42312 Degrees F Calibrator Probe Stack Oven Exit Auxillary

Point 1 32 33 32 34 32 32

Point 2 212 213 212 214 212 212
Point 3 752 754 752 754 752 752

Emtech 42312 Degrees R Calibrator Probe Stack Oven Exit Auxillary

Point 1 492 493 492 494 492 492

Point 2 672 673 672 674 672 672

Point 3 1212 1214 1212 1214 1212 1212

Percent Difference Probe Stack Oven Exit Auxiflary

Point 1 0.20284 0 0.404858 0 0

Point 2 0.148588 0 0.296736 0 0

Point 3 0.164745 0 0.164745 0 0



# 261

### Armstrong Environmental Inc. CONVERSION FACTORS EPA Method .ri 511 Series Meter Box Calibration - 1 mm Hg = 0.13330 kPa Post-Test Orifice Method 1 cm = 0.39370 inch English Meter Box Units, English K' Factor 1 mm - 0.03937 inch t cu ft = 28.32 liters er Box fi 10 Date: ---------- ---- ----------- > 04/14/06 

### al #: 30272 Barometric Pressure: ----------> 29.75 (in. Hg) Theoretical Critical Vacuum: --- > 14.03 (in. Hg)



### I!I 'ORTAt. For valid test results, the Actual Vacuum shouid be 1 to 2 in. Hg greater than the Theoretical Critical Vacuum shown above. 'ORTAI\ The Critical Orifice Coefficient, K', rnust be entered in English units, (1()^3'(deg R)"0.5/((In.Hg)"(min)). 1!!

---------------- DRY GAS METER READINGS ---------------- -CRITICAL ORIFICE READINGSTheoreticai Critical Vacuum: --- > 14.03 (in. Hg) Voltrmo Volume Volume Initial Temps. Final Temps. Orifice K' Orifice Actual -- Ambient Temperature -- DGM DGM Ambient 

### dH Time Initial Final Total Inlet Outlet Inlet Outlet Seriai# Coeffcient Vacuum Initial Final Average Outlet Overall Teinp 120) (min) (cu ft) (cu ft) (cu ft) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (cieg R) 0.92 6.00 99.700 103.374 3.674 77.0 76.0 78.0 77.0 55 0.464 19.5 76.0 76.0 76.0 536.5 537.0 536.0 0.92 6.00 103.700 107.377 3.677 78.0 77.0 78.0 77.0 55 0.464 19.5 76.0 75.0 75.5 537.0 537.5 535.5 0.92 7.00 107.800 112.085 4.285 78.0 77.0 78.0 77.0 55 0.464 19.5 76.0 76.0 76.0 537.0 537.5 536.0

. .............................................. RESULTS

.... ... ............................................ )RY GAS METER --- --------- ORIFICE --------- -- DRY GAS METER --

.UME VOLUME VOLUME VOLUME VOLUME CALIBRATION FACTOR tRECTI CORRECTED CORRECTI CORRECTI NOMINAL Y 'm(std) Vm(std) Vcr(std) Vcr(std) Vcr Value Variation (cu ft) (liters) (cu ft) (liters) (cu ft) (number) (number) 3.599 0.1 3.577 0.1 3.653 0.994 -0.001 3.598 0.1 3.578 0.1 3.651 0.994 -0.000 4.193 0.2 4.173 0.2 4.262 0.995 0.001 

# Average Y -------> 0.995

For Calibration Factor Y, the ratio of the reading of the calibralion meter to the dry gas meter, acceptable tolerance of individual values frorn the average is +-0.02. --------- ORIFICE ---------

CALIBRATION FACTOR dH@ Value Variation (in H20) (in H20) 1.425 0.0013 1.422 -0.001 1.424 0.000 

# 1.424 <------- Ave rag e d H@

For Orifice Calibration Factor dH@, the orifice differential press ein inches of H20 that equates to 0.75 cfm of air 

## at 68 F and 29 `

92_inchUTW)lg, accepta Io , tolerance ndi 'dual vaiues from the average is +-0.2.

~~ ..i' 

## % i

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# i •'/,1 

# ~~ SIGNED:

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## . Date:

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## m T\D

# Temperature Meter Calibrations

Meter Box #: 10 

# Date: 04/14/06 

# Calibrated By: RT

Emtech 42312 Degrees F Calibrator Probe Stack Oven Exit Auxillary

Point 1 32 32 31 32 31 31

Point 2 212 212 211 212 211 211

Point 3 752 752 751 751 751 751

Emtech 42312 Degrees R Calibrator Probe Stack Oven Exit Auxillary

Point 1 492 492 491 492 491 491

Point 2 672 672 671 672 671 671

Point 3 1212 1212 1211 1'211 1211 1211

Percent Difference Probe Stack Oven Exit Auxillary

Point 1 0 0.203252 0 0.203252 0.203252

Point 2 0 0.14881 0 0.14881 0.14881

Point 3 0 0.082508 0.082508 0.082508 0.082508



# 2.

~ 

# 3Armstrong Environmental Inc. CONVERSION FAC'TORS EPA Melhad 5 522 Series Meter Box Celibratlon 1 mm H 0.13330 kPa fl Pre-Tesl Orifice Malhod 1 cm = 0.39370 inch English Meter Box Unils, English K' Factor 1 mm - 0.03937 Inch 1 cu ft = 28.32 liters leter Box x 11 Date: ----------- ------- -----•-> 03/15l06 eriat #: 40312 Barometric Pressttre: ----------> 29.90 (in. Hg) Theoretical Critical Vacrrum:---> 14.10 (In. Hg)

tlliltt APORTAN For valid lesl resulls, ttie Actual Vacuuni should be 1 to 2 in. Hg greater than the Theoretical Crilical Vacuum shovin above. Ai'ORTAN The Critical Orifice Coefficienl. IC, niusl be entered in English uniis, (ft)^3'(deg R)"0.5/((in.Hg)'(min)). I!!t+!!

--- ---- ------ --- DRY GAS METER READINGS ---- ------------ -CRITICAL ORIFtCE READINGS- 

### -- Average Temperatures -- Volunie Voltniie Volunie Initiat Temps. Final Temps. Orifiee K' Orifice Actua! -- Ambienl Tomperature -- DGM DGM Ainbionl dH Time htilial Final Total Inlet Oullot Inlet Oullet Serial# Coefficient Vacuum Initia) Final Average Outlet Overall Temp 

### n H20) (niiil) (cu Il) (cu fl) (cu ft) (deg F) (deg F) (deg F) (deg F) (ntrmber) (see above) (in Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (dog R) 0.25 10.00 694.400 697.623 3.223 67.0 65.0 67.0 66.0 40 0.242 23.5 67.0 67.0 67.0 525.5 526.3 527.0 0.52 6.00 699.700 702.473 2.773 67.0 66.0 67.0 67.0 48 0.344 21.5 67.0 68.0 67.5 526.5 526.8 527.5 0.96 5.00 703.000 706.105 3.105 67.0 67.0 68.0 67.0 55 0.464 20.0 68.0 68.0 68.0 527.0 527.3 528.0 1.60 7.00 706.800 712.360 5.560 68.0 67.0 69.0 67.0 63 0.593 18.0 68.0 68.0 68.0 527.0 527.8 528.0 3.10 7.00 713.100 720.754 7.654 69.0 67.0 72.0 68.0 73 0.824 16.0 68.0 68.0 68.0 527.5 529.0 528.0

................................................. RESULTS ...................................................

- DRY GAS METER --- --------- ORtFICE --------- -- DRY GAS METER -- 

### --------- ORIFICE


## JLUME VOLUME ORRECT CORRECTED Vm(std) Vin(sld) (ctr ft) (liters) 3.232 0.1 2.780 0.1 3.113 0.1 5.579 0.2 7.690 0.3 

## VOLUME VOLUME VOLUME CORRECT CORRECT NOMINAL Vcr(std) Vcr(sld) Vcr (cu fl) (liters) (cu ft) 3.156 0.1 3.153 2.689 0.1 2.690 3.018 0.1 3.021 5.405 0.2 5.411 7.504 03 7.512 CALIBRATION FACTOR Y Value Varialion 

### (number) (number) 0.976 0.005 0.967 -0.004 0.969 -0.002 0.969 -0.003 0.976 0.004 

### CALIBRATION FACTOR dHO Value Variation (in H20) (in H20) 1.418 -0.0602 1.459 -0.019 1.484 0.006 1.511 0.033 1.518 0.040 

# Average Y -------> 0.972 1.478 <------- Average dH@

Ae: For Calibration Factor Y, the ratio of the reading of the calibration molar to Ihe dry gas moter, acceptable toterance of individual values from lhe average is +-0.02. 

### For Orifice Calibration Factor dH@, lfie orifice differential pressure in inches of H20 that equates to 0.75 cfm of air al 68 F and 29.92 inches of Hg, acceptablelerance ' divid lues (rom the average is +-0.2.

~ 

### '"'- SIGNED: `1•

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### Dale:

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: V

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# Temperature Meter Ca(ibrations

Meter Box #: 11 

# Date: 03115106 

# Calibrated By: RT

Emtech 42312 Degrees F Calibrator Probe Stack Oven Exit Auxillary

Point 

# 1 32 31 31 32 32 32

Point 2 212 212 213 213 212 212

Point 3 752 753 753 753 753 753

Emtech 42312 Degrees R Calibrator Probe Stack Oven Exit Auxillary

Point 1 492 491 491 492 492 492

Point 2 672 672 673 673 672 672

Point 3 1212 1213 1213 1213 1213 1213

Percent Difference Probe Stack Oven Exit Auxillary

Point 1 0.203252 0.203252 0 0 0

Point 2 0 0.148588 0.148588 0 0

Point 3 0.08244 0.08244 0.08244 0.08244 0.08244



# 265

### ORIFICE

CALIBRATION FACTOR dH@ Value Variation (in H20) (in H20) 1.495 0.0023 1.493 -0.000 1.491 -0.002 

# 1.493 <------- Average dH@ Arinstrong Environmenta) Inc. CONVERSION FACTORS EPA Method 5 

## APEX INSTRUMENTS 511 Series Meter Box Calibration 1 mm Hg : 0.13330 kPa Post-Test Orifice Method 1 cm = 0.39370 inch English Meter Box Units, English IC Factor 1 mm = 0.03937 inch 1 cu ft = 28.32 liters ;ter E3ox 1 11 Date: ----------------------- -> 04/14/06 -rial #: 73 Barometric Pressure: ----------> 29.75 (in. Hg) Tlieoretical Critical Vacuum:---> 14.03 (in. Hg)

1!liil 

## PORTAP For vaiid test resuits, the Actual Vacuum should be 1 to 2 in. Hg greater than the Theoretical Critical Vacuum sliown above. PORTAP The Critical Orifice Coefficient, iC, must be entered in Englislt units, (ft)"3"(deg R)"0.5/((in.Hg)`(min)). !!ii!!

---------------- DRY GAS METER READINGS ---------------- -CRITICAL ORIFICE READINGSTheoretical Critical Vacuum:---> 14.03 (in. Hg) 

## Volurne Volume Volume Initial Temps. Final Temps. Orifice iC Orifice Actual -- Ambient Temperature -- DGM DGM Anibient (1H Time Initial Final Total Inlet Outlet Inlet Outlet Serial# Coefficient Vacuum Initial Final Average Ou#let Overall Ternp i H20) (min) (cu ft) (cu ft) (cu ft) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (deg R) 0.96 7.00 325.500 329.853 4.353 73.0 72.0 74.0 73.0 55 0.464 20.0 75.0 75.0 75.0 532.5 533.0 535.0 0.96 7.00 330.200 334.571 4.371 74.0 73.0 75.0 74.0 55 0.464 20.0 75.0 75.0 75.0 533.5 534.0 535.0 0.96 7.00 335.200 339.572 4.372 75.0 74.0 75.0 74.0 55 0.464 20.0 75.0 75.0 75.0 534.0 534.5 535.0

.A4:krrRlififr

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## RESULTS ArA..IfIfAA11fAAA AffAfAAA+AfArrfArflf+iirrlfA AAAAAA



### • DRY GAS METER --- --------- ORIFICE --------- -- DRY GAS METER --
JLUME VOLUME VOLUME VOLUME VOLUME CALIBRATION FACTOR ORRECT CORRECTED CORRECT CORRECT NOMINAL Y Vm(std) Vm(std) Vcr(std) Vcr(std) Vcr Value Variatlon 

### (cu ft) (liters) (cu ft) (liters) (cu ft) (number) (number) 4.296 0.2 4.177 0.2 4.258 0.972 0.001 4.306 0.2 4.177 0.2 4.258 0.970 -0.001 4.303 0.2 4.177 0.2 4.258 0.971 -0.000 

# Average Y -------> 0.971

ote: For Calibration Factor Y, the ratio of the reading of the calibration meter to the dry gas meter, acceptabie tolerance of itidividual values from the average is +-0.02. 

## For Orifice Calibration Factor dH@, the orifice differential pressure in inches of H20 that equates to 0.75 cfm of air at 68 F and 29.92 inches of, Hg, accepta I tolerance of I 

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# Temperature Meter Calibrations

Meter Box #: 11 

# Date: 04/14/06 

# Calibrated By: RT

Emtech 42312 Degrees 

# F Calibrator Probe Stack Oven Exit Auxillary
Point 1 32 31 31 32 32 32
Point 2 212 212 213 213 213 212
Point 3 752 753 753 754 753 753

Emtech 42312 Degrees 

# R Calibrator Probe

. 

# Stack Oven Exit Auxillary
Point 1 492 491 491 492 492 492
Point 2 672 672 673 673 673 672
Point 3 1212 1213 1213 1214 1213 1213

Percent Difference Probe Stack Oven Exit Auxillary
Point 1 0.203252 0.203252 0 0 0
Point 2 0 0.148588 0.148588 0.148588 0
Point 3 0.08244 0.08244 0.164745 0.08244 0.08244



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# 273

# NOZZLE- I NSPECTION AhD hiEASURLEMENT DATA SHLEET

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, 

# Last previously Measured ,, r Nozzle area 6,.oC,03q( ft 2 sigr,ature

Date Nfeasured ~ 

# 10 ( ~.(~ 

# date



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# Presample Inspection 

# I hereby certi fy that the above referenced nozzl e appears to be . round, sharp-edg*ed, free of nicks and dents and is- judged acceptable for use at this time. 

# '. Last Previously Measured Nozzle Area
~ o©a33 ~ ft 2 signatur
Date Measured date

Postsample Measurement 

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# 1. 

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# Presample Inspz-ction 

# I hereby certify that the above ref erenced nozzl e appears to be round, snarp-edged, fr-oe oz nicks and de' and is- judged a ceptable for use at thi's time. v
~ 

# --

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# Last Previ ously Measured Nozzl e krea ~



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# . the above referenced nozzl e appears to be . round, sharp-edged, frea of nicks and deny - and i s judged accep

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# abl e for use a

- t thi s time. Last Previ ously Measurzd iNozzl e Area •. 6663 f t 2 s i ona t.
Date weasured 

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1. y 24 g 

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# ~ s•— ask-. .. i ne Ga= PrvfEGsicrca{s'• 16S0 Enterprise Parkway Twinsburg, Ohio 44087

21 S-648-4000


# `;fE

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# Customer: MATHESON TRI-GAS - DALLAS Cylinder Number: SX



## - 32759 

# Cvlinder pressure: 2000 Last Analysis date: 5/3/2005 Expiration Date: 5/3/08

Component : Methane
Certified Conc: 40.8 PPM ± 1% rREL 

# Protocol: Reference # t_ot # G 1 329498 109-66-43191


# DO:N.OT*USE

- .T-H.IS:CYLINDE-R• WHEN THE•,. = f'RES

~ 

# SURE FALLS:BEL01N 1.5.0 PSIG

~ 

## REPLICATE RESPONSES
Date: 5/3/2005 Date:

40.8 PPM 40.8 PPM 40.7 PPM

BALANCE GAS: Air

REFERENCE STANDARDS

_

Component: Methane SRM #: SRM-2750 Cylinder #: SX-20007 , ~



## . • Concentration: 48.80 pprrt

CERTIFICATION INSTRUMENTS 

# - . r

Component: Methane ; Make/Model: Varian 3800 GC Serial Number: LR-92489 `- Measurement Principle: TC, FID - Last Ca(ibration: 4/26/2005

Nates:



# This certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous Calibration Standards September 1997, using procedure G1 and/or G2.

~ 

# nai

~~ 

# st 

# ~ 

# n /, ~~,~ ~

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# ;c ' 

## Date 

# 51412005



# 279

# ~► 

# ~ l~~~~-~~~ !<~ ~ ~ : -; 

# ~~ ;• -



# TRi

~ 

# GAS ask. . .The Gzs Profess!iona(sT" 

## 1650 Enterprise Parkway Twinsburg, Ohio 44087

215-648-4000

~C~ S. F"!' ~'~' l

~ '^S
~

` !: n. F i•~ •w.~ ~ :~ t I.r • ~t~4 /~.f^P:€ fsi. ~l p- ~ ~ w ~ . : .- rs F ! ~ t' ! °'` •, . f ~. ~ ~ F ~ . . i ~ {^

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### ~ 

## ustomer: MA i HESON TRI-GAS - DALLAS ;vlinder Nurnber: SX-34951 ;y!inder pressure: 2000 _ast Analysis date: 5/3/2005 cxpiration Date: 5/3I08

Component : Methane

Certified Cona: 61.7 PPM ± i % REL Protocol: Reference # Lot # G 1 329498 109-56-43192
DO.'NOT USE THIS CYLINDE.R WHEN-THE 

# PRESSURE ; 

# F~ 1LLS; BELOW 1.50 PSIG. .

, •
REPLICATE RESPONSES
Date: 5/3/2005 Date:

61.7 PPM 61.8 PPM 61.5 PPM



# 3ALANCE GAS: Air = -

REFERENCE STANDARDS

Component: Methane • ; -. - , SRM #: SRM-2750 - Cylinder n: SX-20007

, Concentration: 48.80 ppm



# LERTIFICATION INSTRUMENTS -

Component: Methane _ Make/Model: Varian 3800 -GC - Serial Number: LR-92489 Measurement Principle: TC, FID ` Last Calibration: 4/26/2005 :

Notes:



# This certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous Calibration Standards September 1997, using procedure G1 andlor G2.



# :na!yst 

# ; ~ ~ c ~ `~~ 

# ,!' Date 

# 51412005


# WE

# Specialty 

# Ga
.~ 

# Products

3106 Pasadena Frceway Pasadena, Texas 77503 (713) 534-8217 Fax(713) 534-8133
Date: 3/2212005 Customer. Trigas Project: 14445 Description: Methane in Air - EPA Protocol Exp. Date: 3/22/2008 Cylinder No: SX31814 Cylinder Pressure: 1950psig Requested Certified Component Concentration Concentration Accuracy 

## Methane 20 ppm 19.9 ppm 1% Air, Balance

Reference Standard Description Exairation date Cylinder Number Concentration 

## SRM 6/1/2008 FF23319 49.22 ppm Methane 

# Instrumentation Qescription Model # Date Last Clibrated PrinciQie 

## Horiba Process Analyzer FIA-510 3121/2005 FIA 

# Anaylsis Results: Z= zero gas, S= standard gas, X= sample gas

First Triad - Methane Z1= 1.60 S1= 492.30 X1= 199.70 S2= 492.70 Z2= -0.10 X2= 198.60 Z3= -0.70 X3= 199.50 S3= 490.40 Curve: Y=-0.09706+0.099752*X Average = 19.87pm



# ~
. f i 

## Analyst: /.


# THIS STANDARD 1S NIST TRACEABLE. 1T WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG

# AP 3106 Pasadena Freeway 

# Pasadena, Texas 77503 (713) 534-82 1 7 Fax(713) 534-8133 

# Specialty Gas Praducts

Date: 6127/2005 Customer: Matheson - Trigas Description: NO in N2 - EPA Protocol 

# Cylinder No: EB0001164

Com Aonent 

# Nitric Oxide Nitrogen, Balance

Reference Standard Description 

# GMIS Instrumentation

Average = 50.3ppm Curve: Y = 0.33645 + 0.099857'"X Project: 16015 Exp. Date: 6/27/2007 

# Cylinder Pressure: 1900psig Certified Concentration 

# 50.4 ppm
NOx: 51 ppm

Cylinder. Number 

# N D22557 

# Accuracy 1%

Concentration 

## 99.8 PPM no

Principle 

## CHEMI

X1= 502.80 X2= 502.40 S3= 994.20 

# Average = 50.53ppm Requested Concentration 

## 50 ppm



# Expiration date 11/22/2006

Description Model # Date Last Clibrated 

# Horiba Process Analyzer CLA-510-NO 6/16/2005 

# Anaylsis Results: Z= zero gas, S= standard gas, X= sample gas

First Triad - NO Second Triad - NO 

## Z1= -1.20 S1= 994.80 X1= 498.30 Z1= -1.10 S1= 998.50 

# S2= 994.10 Z2= -1.30 • X2= 498.40 S2= 998.20 Z2= -0.70 7 

# 3= -1.10 X3= 499.80 S3= 997.40 Z3= -0.80 X3= 500.80

----
~ 

## _ Analyst:

~ 

## ...r

/ THIS STANDARD IS NIST TRACEABL E. IT V1IAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

# DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG



# ~ 

# 82

# ~ 3106 Pasadena Freeway Pasadena, Texas 77503 (713) 534-8217 Fax(713) 534-8133 

# Specralty Gas Products

Date: 6127I2005 

# Castorner: Matheson - Trigas Project: 16014 Description: NO in N2 - EPA Protocol Exp. Date: 6127l2007 Cylinder No: EB0001156 Cylinder Pressure: 1900psig Requested Certified Component Concentration Concentration Accuracy 

# Nitric Oxide 25 ppm 25.0 ppm 1% Nitrogen, Balance NOx: 25.5 ppm Reference Standard Description Expiration date Cylinder Number Concentration 

# GMIS 11/22I2006 ND22557 99.8 PPM no Instrumentation Description Model # Date Last C(ibrated Principle 

# Horiba Process Analyzer CLA-510-NO 6/16/2005 CHEMI Anaylsis Results: Z= zero gas, S= standard gas, X= sarnple gas

First Triad - NO Second Triad - NO 

# Z1= -1.20 S1= 994.80 X1= 244.50 Z1= -1.10 S1= 998.50 X1= 247.10 S2= 994.10 Z2= -1.30 X2= 244.80 S2= 998.20 Z2= -0.70 X2= 247.00 Z3= -1.10 X3= 246.10 S3= 997.40 Z3= -0.80 X3= 246.40 S3= 994.20 Average = 24.90ppm Average = 25.00ppm Curve: Y = 0.33645 + 0.099857"`X

; s,t/ Analy



# THIS STAN R 

# ~

ISNIST TRACEABLE. IT WAS CERTiFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PS1G



# 283

# Products

Specialty
3106 Pasadena Freeway 

# Pasadena,Texas 77503 (713) 534-8217 Fax(713) 534-8133
Date: 6/27/2005 Customer: Trigas Project: 16017 Description: CO in N2 - EPA Protocol Exp. Date: 6/27/2008 Cytinder No: EB0000701 Cylinder Pressure: 1900psig Requested Certified 

# Comaonent Concentration Concentration Accuracy Carbon Monoxide 50. ppm 49.9 ppm 1% Nitrogen, Balance

Reference Standard 

# Description Expiration date Cylinder Number Concentration NTRM 5/29/2006 SX19190 994.2 ppm CO 

# Instrumentation
Descriation Model # Date Last Clibrated Principle 

## Horiba Process Analyzer VIA-510-CO 6/10/2005 NDIR 

# Anaylsis Results: Z= zero gas, S= standard gas, X= sampie gas
First Triad - CO Second Triad - CO 

## Z1= -0.90 S1= 204.90 X1= 198.70 Z1= -0.40 S1= 513.30 X1= 497.10 S2= 204.80 Z2= -0.80 X2= 198.60 S2= 513.20 Z2= -0.40 X2= 497.10 Z3= -0.80 X3= 198.60 S3= 204.90 Z3= -0.40 X3= 496.90 S3= 513.20
Y=0.28607+0.250309*X Y=0.031031 +0.100163'X 

# Average = 49.94ppm Average = 49.82ppm



# ~
~ ~•~ 

## ;naiyst:

~ . 

## THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. n0 NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

# 284

# Specialty 

# Ga
.~ 

# Pr ® 

# d

~ 

# ., ~ 

# ct
.~ 3106 Pasadsna Freeway Pasadena, Texas 77503 (713) 534-8217 Fax(713) 534-8133
Date: 6/27/2005 Customer: Trigas Project: 16018 Description: CO in N2 - EPA Protocoi Exp. Date: 6l27l2008 Cyiinder No: EB0000761 Cylinder Pressure: 1900psig Requested Certified Component Concentration Concentration Accuracv 

## Carbon Monoxide 100 ppm 99.1 ppm 1% Nitrogen, Balance



# Reference Standard Description Expiration date Cylinder Number Concentration 

## NTRM 5129l2006 SX19190 994.2 ppm CO Instrumentation Description Model # Date Last Ciibrated Principle 

## Horiba Process Analyzer VIA-510-CO 6/10/2005 NDIR 

# Anaylsis Results: Z= zero gas, S= standard gas, X= sample gas
First Triad - CO Second Triad - CO 

## Z1= -0.90 S1= 204.90 X1= 396.60 Z1= -0.40 S1= 513.30 X1= 985.70 S2= 204.80 Z2= -0.80 X2= 396.60 S2= 513.20 Z2= -0.40 X2= 985.40 Z3= -0.80 X3= 396.50 S3= 204.90 Z3= -0.40 X3= 985.20 S3= 513.20
Y=0.28607+0.250309'X Y=0.031031 +0.100163'X Average = 99.45ppm Average = 98.74ppm

Analyst:

--- ~ ~

~ 

# THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES, DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

# 285

# Specialty 

# Ga s , ~' 

# ro d~c 

# t .~ 3106 Pasadena Freeway Pasadena, Texas 77503 (713) 534-8217 Fax(713) 534-8133

Date: 8/1612004 Customer. Matheson - Trigas Project: 10548 Description: CO, 02 in N2 - EPA Protocol Exp. Date: 8/162007 Cylinder No: CC187154 Cylinder Pressure: 1900psig Requested Certified Component Concentration Concentration Accuracy
Carbon Monoxide 200ppm 200ppm 1% 

# Nitrogen, Balance
Reference Standard Description Expiration date Cylinder Number Concentration
GMIS 4/6/2006 CC177636 994.2 ppm CO
Instrumentation Description Model # Date Last Ciibrated Principle Horiba Process Analyzer VIA-510-CO 8/6/2004 NDIR Anaylsis Results: Z= zero gas, S= standard gas, X= sample gas
First Triad - CO Second Triad - CO Z1= -0.3 S1= 993.5 X1= 199.9 Z1= -0.4 S1= 995.5 X1= 200.6 S2= 993.20 Z2= -0.30 X2= 200.00 S2= 995.80 Z2= -0.30 X2= 200.60 Z3= -0.30 X3= 199.90 S3= 993.00 Z3= -0.30 X3= 200.60 S3= 9995.60
Curve: Y=-0.0

- 893=1.001139X Average =199.6ppm Average = 199.8ppm

Analyst: Ling Wen

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

# 286

## Project: 10549 Exp. Date: 8/162007 Cylinder Pressure: 1900psig
Certified Concentration 

## 494ppm Accuracy


## 1%

Cyiinder Number Concentration CC177636 994.2 ppm CO 

# Spect'alty Gas P
3106 Pasadena Freeway Pasadena,Texas 77503 (713) 534-8217 Fax(713) 534-8133

Date: 8/1612004 Customer: Matheson - Trigas Description: CO 3 02 in N2 - EPA Protocol Cylinder No: CC176507 Requested Comaonent Concentration 

## Carbon Monoxide 500ppm Nitrogen, i3alance Reference Standard Description Expiration date GMIS 416l2006
instrumentation Description Model 

## # Horiba Process Analyzer VIA-510-CO Anayisis Results: Z= zero gas, S= standard gas, X= sampfe gas First_Triad - CO 

## Z1= -0.3 S1= 993.5 X1= 494.2 S2= 993.20 Z2= -0.30 X2= 494.00 Z3= -0.30 X3= 493.90 S3= 993.00 Curve: Y=-0.6893+1.001139X Average =494.1 ppm Date Last Ciibrated Principle
8/6/2004 NDIR

Second Triad - CO 

## Z1= -0.4 S1= 995.5 X 1= 495.4 S2= 995.80 Z2= -0.30 X2= 495.60 Z3= -0.30 X3= 495.50 S3= 995.60
Average = 494.4ppm

Analyst :_ 

## Ling r
THIS STANDARD 1S NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THtS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PS1G 

# 287. ~,: ~ ~ ► r - ~ 

### = 3't46 Pasadena 

## F reeway 

# : ~E,~~ ':-- 

# ~ ~ ~ 

# 0 ~°~:

71 

## Pasadena TX 77503 

# TRE-GAS`'

~ ~~ 

### ""-•' 3-534-8217

~ 

# slc. e-s ?ro'ess}on: is Certificate of Analysis - EPA Protocol Mixtures

Customer: MTG-CALI CROSSING Protocol: Reference # Lot# Cylinder Number: CC165296 G1 21555 Cylinder Pressure: 1900 PSIG DO NOT USE THIS CYLINDER WHEN THE PRESSURE Last Analysis Date: 3/20/2006 FALLS BELOW 150 PSIG 

# Expiration Date: 3120/2008 REPLICATE RESPONSES
Component: Sulfur Dioxide Date: 3/10/2006 Date: 3/20/2006 250.30 250.20 Mean Conc: 250 ppm +/- 1% rel 250.00 250.00 250.10 250.00 BALANCE GAS: Nitrogen

REFERENCE STANDARDS: Component: Sulfur Dioxide Reference Standard: GMIS

Cylinder #: ND22558 Concentration: 502.1 ppm Exp. Date: 4/7/2007 

# CERTIFICATION INSTRUMENTS Component: Sulfur Dioxide Make/Model: Horiba VIA-510 Serial Number: 42321590023 Measurement Principle: NDIR Last Calibration: 2l22/2006

Notes: This Certification was performed according to EPA Traceability Protocol for Assay & Ceitification of Gaseous Calibration Standards September 1997, using procedure G1 and/or G2.

_ .. Analyst: 

# ~ Date:

Manufactured By Specialty Gas Products, a Matheson Tri-Gas Company, Pasadena, Texas.



# .~~ R o. = r-- r• ~ fi 

## 3'

~ 

## 06 Pasader,a F 

## r eeway

AVAL 

### : ~ r c ~~^~ 

### lT f

-- X ~ Z~ 

### Pasadena, TX 77503

~ 

# R i

~ 

# G

~" ~



### ~ 

### S t? 713-534-8217 

# -ascc ... 1'h-a Gas Certificate of Analysis - EPA Protocol M'sxtures

Customer: MTG-Cali Crossing Protocol: Reference # Lot# Cylinder Number: CC176977 G1 20832 Cyiinder Przssure: 1900 PSIG DO NOT USE THIS CYLINDER V'JHEN THE PRESSURE Last Anaiysis Date: 2113I2005 FALLS. BELOW 1 SO PSIG . 

# Expiration Date: 2113l2008 REPLICATE RESPONSES
Component: Sulfur Dioxide Date: 2/6I2006 Date: 2/13/2006 49.44 50.22 Mean Conc: 49.8 ppm +/- 1% rel 49.65 49.91 49.78 49.88 BALANCE GAS: Nitrogen

REFERENCE STANDARDS: Component: Sulfur Dioxide Reference Standard: GMIS

Cylinder #: CC177775 Concentration: 101.3 pprn Exp. Date: 9/412006 

# CERTIFICATION INSTRUMENTS Component: Sulfur Dioxide MakelModel: Horiba VIA-510 Serial Number: 42321590023 Measurement Principie: NDIR Last Calibration: 2/712006

Notes: This Certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous 

# Cafibration Standards September 1997, using procedure G1 andlor G2. Anafyst:

~ 

# : ----? Date:

~ 

# Manufactured By Specialty Gas Products, a Matheson Tri-Gas Company, Pasadena, Texas.



# 2R9

## 3106 Pasadena Freeway i v E !•- ~ , i

~. ~ t s ~~ 

### ` Pasadena, TX 77503

~ 

# R F ` 

# G f~-~ ~



### 3 713-534-821 7 

# ---5i:. ..Ths Cas ^r•;if¢gsictnnEs Cercificate of Analysis - EPA Protoco! Mixtures

Customer: Cylinder Number: Cyiinder Pressure: Last Anaiysis Date: Expiration Date: MTG-Cali Crossing CC177031 1900 PSIG 2/13/2006 211312008 Protocol: Reference # Lot# G 1 20829

DO NOT USE THIS CYLINDER WHEN THE PRESSURE

FALLS BELOW 150 PSIG



# Component: Sulfur Dioxide
Mean Conc: 100 ppm +!- 1% rel
BALANCE GAS: Nitrogen

REFERENCE STANDARDS: Component: Sulfur Dioxide REPLICATE RESPONSES

Date: 2/6/2006 Date: 2/13J2006

100.60 100.30 100.30 100.10 100.30 100.10

Reference Standard: GMIS

Cyli nder #: N D22558 Concentration: 502.1 ppm Exp. Date: 9/4/2006 CERTIFICATION INSTRUMENTS Component: Sulfur Dioxide Make/Model: Horiba VIA-510 Serial Number: 42321590023 Measurement Principle: NDIR Last Calibration: 1/16/2006

Notes: This Certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous Calibration Standards September 1997, using procedure G1 andlor G2. 

# ~ ` . r ~ ~~ 2~~/. Analyst: " Date:

~ 

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## ~ -~ \i



# ~ Manufacturzd By Specialty Gas Products, a Matheson Tri-Gas Company, Pasadena, Texas.



# 290~ 

# .A

~ 

# ppendi

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# H

# Sheetl



# p e - Summary ofS

~ 

# 2 lnterfernc Samiing ,
.. . ._.. . . . r .. _..

~ 

# Run # _: Method 6 ; Mehtod 6G % Difference

1; 56.41 ' 55 : 6 i 1.4359161



# . _

, 

# .. . . _.. _ .._ _.... .... _._ . ...._ ~~ .



## ~ 2. 59.02 60.1 -1.82989

3 ; 59.34 ; 59.2; - 0.235929 !

Page 1 ~ q ~

# EMISSiON TEST SUMMARY

PLANT : Da11ile. Mtjskogee, UK. 

# DATE : I3-Apr•06 PLACE : T rim Kiln Exhaust. S02 lnier

- ference Tra1n RUN# : i TEST DURATION (MINUTES) : 20 LIQUiD COLLECTED (mis) : 0 

# NOZZLE DIAMETER (INCH.) : 0 Sulfur Dioxide Weight, mg : 1.97 METER COEFFICIENT (Y) : 0.9726 0 PITOT COEFF1CiENT (Cp) : 0 STATIC PRESSURE (in. H20) : 0 GAS METER VOL.(Cu.Ft.) : 0.4907 PERCENT CO2 : 0 BAROMETRIC PRESSURE : 29.7 PERCEN T 02 : 0 PERCENT CO : 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

# STACK DIAMETER (inch): 0 STACK LENGTH(inchs) : STACK AREA (Sq.Ft.) : 0 STACK WIDTH(inchs) : NOZZLE AREA (#eet): 0 STACK AREA (Sq.Ft.) : 0



# ENTER THE STACK AREA SHOWN ABOVE: 0


# FL01NS SAMPLED VOLUME (STD. CU .FT.): 0.4635

Sulfur Dioxide, ppm : 56.4073


# POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

J. 0 0.03 79.5 79.5 2 0 79.5 79.5 3 0 79.5 79.5 4 0 79.5 79.5 5 0 79.5 79.5 #D(V/O! 0.0000 0.0300 79.5000 79.5000 79.5000



# 2Q~

~ M

# EMtSSfON TEST SUMMARY

PLANT : Dalti!e. Musl',o ;ee. OK DATE : 13-Apr•06 PLACE : Trim Kiln Exh@ust, S02 IntPrference Train RUN# : 2 TEST DURATION (MINUTES)

: 

# 20 LIQUID COLLEC T ED (mis)

: 

# 0 NOZZLE DIAMETER (INCH.)

: 

# 0 Sulfur Dioxide Weight, mg

: 

# 2.4n METER COEFFICIENT (Y)

: 

# 0.9726 0 PITOT CO'EFFICIENT (Cp)

: 

# 0 STATIC PRESSURE (in. H20)

: 

# 0 GAS METER VOL.(Cu.Ft.)

: 

# 0.5849 PERCENT CO2

: 

# 0 BAROMETRIC PRESSURE

. 

# 29.7 PERCENT 02

: 

# 0 PERCENT CO

: 

# 0

FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 0 STACK LENGTH(inchs)

: 

# STACK AREA (Sq.Ft.)

: 

# 0 STACK WIDTH(inchs)

: 

# NOZZLE AREA (feet): 0 STACK AREA (Sq.Ft.)

: 

# 0
ENTER THE STACK AREA SHOWN ABOVE: 0


# FLOWS SAMPLED VOLUME (STD. CU .FT.): 0.5532,

Sulfur Dioxide, ppm

: 

# 59.0166
POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T.

deg F INLET OUTLET

1 0 0.03 78.8 78.8 2 0 78.8 78.8 3 0 78.8 78.8 4 0 78.8 78.8 5 0 78.8 78.8
#D1V/0! 0.0000 0.0300 78..8000 78.8000 78.8000



# 2Q3

# EMISSION TEST SUMMARY

PLANT : DaItilp, Muskogee, !DK DATE : 13-Apr-06 PLACE : Trim Kiln Exheust. S02 fnterference Train RUN# : 3 TEST DURATION (MINUTES) : 20 LIQUID COLLECTED (mis) : 

# NOZZLE DIAMETER (INCH.) : 0 Sulfur Dioxide Weight, mg : METER COEFFICIENT (Y) : 0.9726 PITOT COEFFICIENT (Cp) : 0 STATIC PRESSURE (in. H20) : GAS METER VOL.(Cu.Ft.) : 0.5828 PERCENT CO2 : BAROMETRIC PRESSURE : 29.7 PERCENT 02 : 

# PERCENT CO :
FOR CIRCULAR STACK FOR RECTANGULAR STACK 

# STACK DIAMETER (inch): 0 STACK LENGTH(inchs) : STACK AREA (Sq.Ft.) : 0 STACK WIDTH(inchs) : 

# NOZZLE AREA (feet): 0 STACK AREA (Sq.Ft.) :

ENTER THE STACK AREA SHOWN ABOVE: 0


# FLOWS 0 

## 2.46 0 0 

# 0 0 

# 0

C

SAMPLED VOLUME (STD. CU .FT.): Sulfur Dioxide, ppm :
P01 NTS STACK T. DELTA P SQUAR D. P DELTA H

deg F
1 2 3 4 5

#DIV/0! 0.5501 59.3480

METER T. I N LET

79.88 79.88 79.88 79.88 79.88

~;~:~: ~ ~, ~ 

# N
• •

,,



### C~ 

## lloZlZsZol 0.03

0.0300 

# METER T. OUTLET

79.88 79.88 79.88 79.88 79.88
79.8800 79.8800



# 2P4

# Sulfur Dioxide Barium-Thorin Analysis

Plant: Dal•Italia, Muskogee, OK Location: Trim Kiln Date: 13•Apr•06 Standardization Ba (CIO2)4 Titration (mis) Avg. Titration (mls) 9.766667 Blank Titration (mis) Avg. Blank (mis) 

# V 0.1

Volume of Standard Sulfuric Acid (mis) Normality of Standard Sulfuric Acid Normality: 0.010239 Aliquot Average Run # Location Volume Dilution Volume Titration Titration 

## (m I S) (MIS) (MIS) 

## (m I S) (MIS)



## 1 Imp 1-2 1.3

2 Imp 1.2 1.6

. . . 

## 3 Im . . . . . . . . . 1.6

p 1-2

Run # Location Total Grams Total Mg

1 Imp 1 & 2 S02 0.001966 1.97

2 Imp I & 2 S02 0.002457 2.46

3 

## Imp I & 2 S02 0.002457 2.46



# 295

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# 'Summary o€ S02 lnter i 

# ernc¢ Cneck


# ........__....._. . _._._. _.__..._.__..._.____.___.__ __._... ._ _._......._ ~ 

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# __... -- .._...._-.._...., ..__._....__._.____. _......_.._.._..`.._.__.

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# _.... ---, -- -

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# .....__ - 

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# ._...._ Run M ' i l 

# 2

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# pm_ i 0 ~ 

# _Monii:or_S02

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# .. _._..........._.- ~ 

## 0 

# i --.. .__..._.. _...._...._.__.. ~.~ 

# ._._....

l 0 

## Metho 

# d 6 S02 E 0 _M_ oaiiie 

# d -- --- -__ ry 0 

## ; 0 

## % DiITerence ^i 0P i ~0l ~~ 0



# J0 2 Paae i

~

# Sulfur T A)ioxide 

# Bariurril-Thiorin. A' 

# naly-;-is

Plant: D2!tile. DaJlas, T' Location: Piant #4 Scrubbell Date: 20-Jul-03 S;andardizabon 'Da (C-102)4 Ti'Lra'tion (mls) Ava. Titra ion (mls) 10.5 Blank Titration (mis) Avg. Blank (mls) 0.1

Volume of Standard Sulfuric Acid (mls) Normality of Silandard Sulful-ic Acid 

## Normality: 0.00.01524 Aliquot' Average R u n = Location Volume Dilution Volume Titration Titr2tion (MIS) (MIS) (MIS) (MIS) (MIS)


## imo - 1-2

2 imp 2.2 M 

## 0.1

3 1 mp .2 0.1

Run = Location Tok-al 

## Grams Total Mg

I Imp 2 & 3 S02 0 0.00

2 1 mp 2 & 3 S02 0 0.00

3 1 r- ,):) 2 &- 3 S02 0 0.00



# 303

# ZJ

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# L iL

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# . ^

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# ^x\/ . ~

# cM1SS 0N TF.ST SUIVfM.-A.RY

PLr.N i : Ja;:ile Daiscs. : ; JA i E: 9-Ju,-03 RLACE R 1 Jh\= . 1 

# TES i DURA T ION (MINU T tS) : 50 LiQUID COLLEC T ED (mis) : 0 NOZZLE D1AME T ER (iNC!-I.) : 0 S02 Samp1e Weighl, mg: 0 tVIE T ER COErEICIEN T(Y) : 0.944 0 ?I T OT COEF r=lCl; N T(Ca) : 0 S T A T IC ?RESSURE (in. ;'20) : 0 GAS NfE T ER VOL.(Cu.ri.) : 1.818 PE?CErV T CO2

. 0 3AROiViE T RIC PP,ESSURE : 29.5 PERCEN i 02 : 0 

# PERCENT CO : 0


# FLOWS Sk(diPLED VOLUME (S T D. CU.F i.): 1.5737 S02, ppm: 0.0000



# POIN i S ST ACK T. DcL T A P SQUA ~ 

# D.P DEL T A H METEP. T. M

~ 

# TER T.

oeg r 1NLET OUTL ET

1 0 o.00 72 72 

# 2 0 72 72 3 0 72 72 " 0 73 73 5 0 73 73 5 0 73 73 7 0 73 73 8 0 74 74 9 0 75 75 ?0 0 75 75 11 0 75 75 1 

# -2 0 76 76

~ 

## D(VIO! 

# 0.0000 0.0000 73.5833 73.5833 73.5833



# ~~ 5

# EMISSION TEST SUMMARY

,-- ~ 

# LA,1 ~ ~ 

# : Dai

~ 

# iia, Da,l_,s, T Y. DATE : '9•JuI•03 PLACE : ?lani a Scrubber RUh'= : 2 

# T ES T DURA T ION (MiINU T ES) : 50 LIQUID COLLEC T ED (mis) : 0 NOZZL E DIAMETER (INCH.) : 0 S02 Sample Wz-ight, mg: 0 METER COEF F ICIENT (Y) : 0.944 0 

# PITOT COEFFICIENT (Cp) : 0 STATiC PRESSURE (in. H20) : 0 GAS ME T EP, VOL.(Cu.Ft.) : 1.843 PERCENT CO2 : 0 3AROME T RIC PR; SSUP.E : 29.5 PERCEN T 02 : 0 PtRCENT CO : 0


# FLOWS SAMPLEU VOL UME (S T D. CU.FT.): 1.6694 S02, ppm: 0.0000


# POINTS S T ACK T. DEL T A P SQUAR D.r' DEL TA y METE.R T. METER T.

deg F 1NLET OUTLET

? 0 0.00 82 82 

# 2 0 81 az 

# 3 0 81 a?

~ 

# 0 82 82 3 0 82 82 6 0 82 82 7 0 82 82 8 0 83 83 

# 9 0 83 83

~ 

# 0 0 83 83 1? 0 83 83 12 0 8A 84

=D1V/0! 0.0000 0.0000 82.3333 82.3333 82.3333



# P6

# EMISSlON TEST 5UMMAP•.Y

PL AN T: Daltile, Dailas, T); DA T L : 9•Ju! •03 PLACE : ?lari< < S.- rubber



# TES T DUP,ATION (IAlNls T ES) : NOZZLE DIAME T tR (INCH.) : MET ER COtF F iCl EN T(Y) : PI ~ 

# 0 T COEF=lC(EN T(Cp) : GAS ME T cR VOL.(Cu.Ft.) : 

# BAROME T RIC PRESSUP.E :



# FLOWS 60 LIQUI D COLLEC T ED (mls) : 0 S02 Samqle INeight, mg: 0.94^- 0 S T ATIC PRESSURE (in. H20) : 1.857 PLRCEN T CO2 : 29.5 PERCEN T 02 : 

# PERCENT CO : 0 0 0 

# J 0 0 0



# SAMPLED VOL UML (ST.D: CU.F T.): 1.68 1 - 8 S02, ppm: 0.0000

POINTS STACK T. DEL T A P SQUAR D.P DLLTA H ME TECR T. METER T.

deo F INL ET OU T LE T

1 0 0.09 86 86 2 0 83 83 3 0 82 82 4 3 82 82 5 0 82 82 6 0 82 82 7 0 82 82 8 fl 82 82 9 0 82 82 10 0 82 82 11 0 82 82 i? 0 82 82



# nDlV Ot 0.0000 0.0000 82.41n7 82.4167 82.4167



# P7