VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Facility Sample Date Resin Type Sample 

No.

Analyte 

Category Analysis Method CAS No. HAP

Concentration 

(ppmw)

Non-Detect?

Note(s)

Yellow highlight indicates the start of a 

new sample number

Shintech Addis, LA 01/03/13 Suspension 1 Alcohol SW-846-8015C 107211 Ethylene glycol 4 Non-detect

Shintech Addis, LA 01/03/13 Suspension 1 Alcohol SW-846-8015C 67561 Methanol 28

Shintech Addis, LA 01/03/13 Suspension 1 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.19 J

Shintech Addis, LA 01/03/13 Suspension 1 Aldehyde SW-846-8315A 50000 Formaldehyde 0.525 J

Shintech Addis, LA 01/03/13 Suspension 1 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect R

Shintech Addis, LA 01/03/13 Suspension 1 SVOC SW-846-8270D 98862 Acetophenone 1.55 J

Shintech Addis, LA 01/03/13 Suspension 1 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/03/13 Suspension 1 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect R

Shintech Addis, LA 01/03/13 Suspension 1 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect R

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect R

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.012

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.049

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.019

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect UJ

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/03/13 Suspension 1 VC EPA Method 107 75014 Vinyl chloride 0.08

No data generated, day 31 data inserted.

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/03/13 Suspension 1 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.789

Shintech Addis, LA 01/04/13 Suspension 2 Alcohol SW-846-8015C 107211 Ethylene glycol 4 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 Alcohol SW-846-8015C 67561 Methanol 36

Shintech Addis, LA 01/04/13 Suspension 2 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.26

Shintech Addis, LA 01/04/13 Suspension 2 Aldehyde SW-846-8315A 50000 Formaldehyde 0.564

Shintech Addis, LA 01/04/13 Suspension 2 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect UJ

Shintech Addis, LA 01/04/13 Suspension 2 SVOC SW-846-8270D 98862 Acetophenone 1.35

Shintech Addis, LA 01/04/13 Suspension 2 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.013

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.046

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.02

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 VC EPA Method 107 75014 Vinyl chloride 0.097

No data generated, day 32 data inserted.

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Addis, LA 01/04/13 Suspension 2 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.79

Shintech Addis, LA 01/05/13 Suspension 3 Alcohol SW-846-8015C 107211 Ethylene glycol 4 Non-detect UJ

Shintech Addis, LA 01/05/13 Suspension 3 Alcohol SW-846-8015C 67561 Methanol 40

Shintech Addis, LA 01/05/13 Suspension 3 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.21

Shintech Addis, LA 01/05/13 Suspension 3 Aldehyde SW-846-8315A 50000 Formaldehyde 0.56

Shintech Addis, LA 01/05/13 Suspension 3 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 SVOC SW-846-8270D 98862 Acetophenone 1.11

Shintech Addis, LA 01/05/13 Suspension 3 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.013

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.050

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.020

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 VC EPA Method 107 75014 Vinyl chloride 0.069 J

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/05/13 Suspension 3 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.929

12/12/2013 VI Confidential 1 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Addis, LA 01/06/13 Suspension4 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Addis, LA 01/06/13 Suspension4 Alcohol SW-846-8015C 67561 Methanol 42

Shintech Addis, LA 01/06/13 Suspension4 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.29

Shintech Addis, LA 01/06/13 Suspension4 Aldehyde SW-846-8315A 50000 Formaldehyde 0.57

Shintech Addis, LA 01/06/13 Suspension4 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 SVOC SW-846-8270D 98862 Acetophenone 0.78

Shintech Addis, LA 01/06/13 Suspension4 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.029

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.052

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.064

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 VC EPA Method 107 75014 Vinyl chloride 0.085

J

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/06/13 Suspension4 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.782

Shintech Addis, LA 01/07/13 Suspension5 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Addis, LA 01/07/13 Suspension5 Alcohol SW-846-8015C 67561 Methanol 39

Shintech Addis, LA 01/07/13 Suspension5 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.5

Shintech Addis, LA 01/07/13 Suspension5 Aldehyde SW-846-8315A 50000 Formaldehyde 0.553

Shintech Addis, LA 01/07/13 Suspension5 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 SVOC SW-846-8270D 98862 Acetophenone 0.996

Shintech Addis, LA 01/07/13 Suspension5 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.034

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.058

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.088

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 VC EPA Method 107 75014 Vinyl chloride 0.175

J

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/07/13 Suspension5 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.937

Shintech Addis, LA 01/08/13 Suspension6 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Addis, LA 01/08/13 Suspension6 Alcohol SW-846-8015C 67561 Methanol 55

Shintech Addis, LA 01/08/13 Suspension6 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.42

Shintech Addis, LA 01/08/13 Suspension6 Aldehyde SW-846-8315A 50000 Formaldehyde 0.558

Shintech Addis, LA 01/08/13 Suspension6 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 SVOC SW-846-8270D 98862 Acetophenone 0.89

Shintech Addis, LA 01/08/13 Suspension6 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

R

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.017

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.048

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.022

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 VC EPA Method 107 75014 Vinyl chloride 0.1

J

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/08/13 Suspension6 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.572

Shintech Addis, LA 01/09/13 Suspension7 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Addis, LA 01/09/13 Suspension7 Alcohol SW-846-8015C 67561 Methanol 53

Shintech Addis, LA 01/09/13 Suspension7 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.87

Shintech Addis, LA 01/09/13 Suspension7 Aldehyde SW-846-8315A 50000 Formaldehyde 0.305

12/12/2013 VI Confidential 2 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Addis, LA 01/09/13 Suspension7 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 SVOC SW-846-8270D 98862 Acetophenone 1.1

Shintech Addis, LA 01/09/13 Suspension7 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.022

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.06

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.043

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 VC EPA Method 107 75014 Vinyl chloride 0.083

J

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/09/13 Suspension7 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.719

Shintech Addis, LA 01/10/13 Suspension8 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 01/10/13 Suspension8 Alcohol SW-846-8015C 67561 Methanol 44

Shintech Addis, LA 01/10/13 Suspension8 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.77

Shintech Addis, LA 01/10/13 Suspension8 Aldehyde SW-846-8315A 50000 Formaldehyde 0.419

Shintech Addis, LA 01/10/13 Suspension8 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect UJ

Shintech Addis, LA 01/10/13 Suspension8 SVOC SW-846-8270D 98862 Acetophenone 1.15

Shintech Addis, LA 01/10/13 Suspension8 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/10/13 Suspension8 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/10/13 Suspension8 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect UJ

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

R

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.007

J

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.031

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.015

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect UJ

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/10/13 Suspension8 VC EPA Method 107 75014 Vinyl chloride 0.062

J

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/10/13 Suspension8 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.654

J

Shintech Addis, LA 01/11/13 Suspension9 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 Alcohol SW-846-8015C 67561 Methanol 26

J

Shintech Addis, LA 01/11/13 Suspension9 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.37

Shintech Addis, LA 01/11/13 Suspension9 Aldehyde SW-846-8315A 50000 Formaldehyde 0.522

Shintech Addis, LA 01/11/13 Suspension9 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect UJ

Shintech Addis, LA 01/11/13 Suspension9 SVOC SW-846-8270D 98862 Acetophenone 0.99

Shintech Addis, LA 01/11/13 Suspension9 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.017

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.1

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.031

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect UJ

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 VC EPA Method 107 75014 Vinyl chloride 0.091

J

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/11/13 Suspension9 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.708

Shintech Addis, LA 01/12/13 Suspension 10 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 01/12/13 Suspension 10 Alcohol SW-846-8015C 67561 Methanol 57

Shintech Addis, LA 01/12/13 Suspension 10 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.48

Shintech Addis, LA 01/12/13 Suspension 10 Aldehyde SW-846-8315A 50000 Formaldehyde 0.391

Shintech Addis, LA 01/12/13 Suspension 10 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect UJ

Shintech Addis, LA 01/12/13 Suspension 10 SVOC SW-846-8270D 98862 Acetophenone 1.15

Shintech Addis, LA 01/12/13 Suspension 10 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/12/13 Suspension 10 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

12/12/2013 VI Confidential 3 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Addis, LA 01/12/13 Suspension 10 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.02

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.114

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.036

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect UJ

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/12/13 Suspension 10 VC EPA Method 107 75014 Vinyl chloride 0.1

J

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/12/13 Suspension 10 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.816

Shintech Addis, LA 01/13/13 Suspension 11 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 Alcohol SW-846-8015C 67561 Methanol 48

Shintech Addis, LA 01/13/13 Suspension 11 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.28

Shintech Addis, LA 01/13/13 Suspension 11 Aldehyde SW-846-8315A 50000 Formaldehyde 0.428

Shintech Addis, LA 01/13/13 Suspension 11 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect UJ

Shintech Addis, LA 01/13/13 Suspension 11 SVOC SW-846-8270D 98862 Acetophenone 1.13

Shintech Addis, LA 01/13/13 Suspension 11 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.023

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.094

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.035

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect UJ

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 VC EPA Method 107 75014 Vinyl chloride 0.033

J

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/13/13 Suspension 11 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.619

Shintech Addis, LA 01/14/13 Suspension 12 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 Alcohol SW-846-8015C 67561 Methanol 47

Shintech Addis, LA 01/14/13 Suspension 12 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.33

Shintech Addis, LA 01/14/13 Suspension 12 Aldehyde SW-846-8315A 50000 Formaldehyde 0.25

Shintech Addis, LA 01/14/13 Suspension 12 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect UJ

Shintech Addis, LA 01/14/13 Suspension 12 SVOC SW-846-8270D 98862 Acetophenone 1.02

Shintech Addis, LA 01/14/13 Suspension 12 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.02

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.079

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.046

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect UJ

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 VC EPA Method 107 75014 Vinyl chloride 0.132

J

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/14/13 Suspension 12 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.612

Shintech Addis, LA 01/15/13 Suspension 13 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 Alcohol SW-846-8015C 67561 Methanol 35

Shintech Addis, LA 01/15/13 Suspension 13 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.16

Shintech Addis, LA 01/15/13 Suspension 13 Aldehyde SW-846-8315A 50000 Formaldehyde 0.397

Shintech Addis, LA 01/15/13 Suspension 13 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 SVOC SW-846-8270D 98862 Acetophenone 0.93

Shintech Addis, LA 01/15/13 Suspension 13 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 SVOC SW-846-8270D 108952 Phenol 0.011

J

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

12/12/2013 VI Confidential 4 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.024

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.098

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.072

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 VC EPA Method 107 75014 Vinyl chloride 0.055

J

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/15/13 Suspension 13 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.708

Shintech Addis, LA 01/16/13 Suspension 14 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 Alcohol SW-846-8015C 67561 Methanol 40

Shintech Addis, LA 01/16/13 Suspension 14 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.34

Shintech Addis, LA 01/16/13 Suspension 14 Aldehyde SW-846-8315A 50000 Formaldehyde 0.5

Shintech Addis, LA 01/16/13 Suspension 14 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 SVOC SW-846-8270D 98862 Acetophenone 0.83

Shintech Addis, LA 01/16/13 Suspension 14 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.017

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.102

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.03

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect UJ

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 VC EPA Method 107 75014 Vinyl chloride 0.082

J

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/16/13 Suspension 14 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.78

Shintech Addis, LA 01/17/13 Suspension 15 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 01/17/13 Suspension 15 Alcohol SW-846-8015C 67561 Methanol 67

J

Shintech Addis, LA 01/17/13 Suspension 15 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.37

Shintech Addis, LA 01/17/13 Suspension 15 Aldehyde SW-846-8315A 50000 Formaldehyde 0.508

Shintech Addis, LA 01/17/13 Suspension 15 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

R

Shintech Addis, LA 01/17/13 Suspension 15 SVOC SW-846-8270D 98862 Acetophenone 1.46

Shintech Addis, LA 01/17/13 Suspension 15 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/17/13 Suspension 15 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

R

Shintech Addis, LA 01/17/13 Suspension 15 SVOC SW-846-8270D 108952 Phenol 0.015

J

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

R

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.014

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.109

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.03

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

R

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/17/13 Suspension 15 VC EPA Method 107 75014 Vinyl chloride 0.085

J

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/17/13 Suspension 15 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.846

Shintech Addis, LA 01/18/13 Suspension 16 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 Alcohol SW-846-8015C 67561 Methanol 42

Shintech Addis, LA 01/18/13 Suspension 16 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.8

Shintech Addis, LA 01/18/13 Suspension 16 Aldehyde SW-846-8315A 50000 Formaldehyde 0.513

Shintech Addis, LA 01/18/13 Suspension 16 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 SVOC SW-846-8270D 98862 Acetophenone 1.52

Shintech Addis, LA 01/18/13 Suspension 16 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

12/12/2013 VI Confidential 5 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.023

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.126

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.056

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 VC EPA Method 107 75014 Vinyl chloride 0.077

J

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/18/13 Suspension 16 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.981

Shintech Addis, LA 01/19/13 Suspension 17 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 Alcohol SW-846-8015C 67561 Methanol 36

Shintech Addis, LA 01/19/13 Suspension 17 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.92

Shintech Addis, LA 01/19/13 Suspension 17 Aldehyde SW-846-8315A 50000 Formaldehyde 0.552

Shintech Addis, LA 01/19/13 Suspension 17 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 SVOC SW-846-8270D 98862 Acetophenone 1.79

Shintech Addis, LA 01/19/13 Suspension 17 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.015

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.129

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.042

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 VC EPA Method 107 75014 Vinyl chloride 0.061

J

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/19/13 Suspension 17 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 1.09

Shintech Addis, LA 01/20/13 Suspension 18 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 Alcohol SW-846-8015C 67561 Methanol 38

Shintech Addis, LA 01/20/13 Suspension 18 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.91

Shintech Addis, LA 01/20/13 Suspension 18 Aldehyde SW-846-8315A 50000 Formaldehyde 0.578

Shintech Addis, LA 01/20/13 Suspension 18 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 SVOC SW-846-8270D 98862 Acetophenone 1.65

Shintech Addis, LA 01/20/13 Suspension 18 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.013

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.112

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.039

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 VC EPA Method 107 75014 Vinyl chloride 0.055

J

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/20/13 Suspension 18 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 1.22

Shintech Addis, LA 01/21/13 Suspension 19 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 Alcohol SW-846-8015C 67561 Methanol 36

Shintech Addis, LA 01/21/13 Suspension 19 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.84

Shintech Addis, LA 01/21/13 Suspension 19 Aldehyde SW-846-8315A 50000 Formaldehyde 0.5

Shintech Addis, LA 01/21/13 Suspension 19 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 SVOC SW-846-8270D 98862 Acetophenone 1.59

Shintech Addis, LA 01/21/13 Suspension 19 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.015

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.121

12/12/2013 VI Confidential 6 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.030

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 VC EPA Method 107 75014 Vinyl chloride 0.062

J

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/21/13 Suspension 19 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 1.09

Shintech Addis, LA 01/22/13 Suspension 20 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 Alcohol SW-846-8015C 67561 Methanol 34

Shintech Addis, LA 01/22/13 Suspension 20 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.99

Shintech Addis, LA 01/22/13 Suspension 20 Aldehyde SW-846-8315A 50000 Formaldehyde 0.554

Shintech Addis, LA 01/22/13 Suspension 20 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 SVOC SW-846-8270D 98862 Acetophenone 1.59

Shintech Addis, LA 01/22/13 Suspension 20 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.017

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.141

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.035

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect UJ

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 VC EPA Method 107 75014 Vinyl chloride 0.1

J

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/22/13 Suspension 20 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 1.25

Shintech Addis, LA 01/23/13 Suspension 21 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 Alcohol SW-846-8015C 67561 Methanol 37

Shintech Addis, LA 01/23/13 Suspension 21 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.55

Shintech Addis, LA 01/23/13 Suspension 21 Aldehyde SW-846-8315A 50000 Formaldehyde 0.45

Shintech Addis, LA 01/23/13 Suspension 21 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 SVOC SW-846-8270D 98862 Acetophenone 1.31

Shintech Addis, LA 01/23/13 Suspension 21 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.018

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.132

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.039

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect UJ

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 VC EPA Method 107 75014 Vinyl chloride 0.085

J

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/23/13 Suspension 21 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 1.07

Shintech Addis, LA 01/24/13 Suspension 22 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 Alcohol SW-846-8015C 67561 Methanol 40

Shintech Addis, LA 01/24/13 Suspension 22 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.79

Shintech Addis, LA 01/24/13 Suspension 22 Aldehyde SW-846-8315A 50000 Formaldehyde 0.451

Shintech Addis, LA 01/24/13 Suspension 22 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 SVOC SW-846-8270D 98862 Acetophenone 1.5

Shintech Addis, LA 01/24/13 Suspension 22 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.019

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.083

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.037

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

12/12/2013 VI Confidential 7 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect UJ

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 VC EPA Method 107 75014 Vinyl chloride 0.071

J

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/24/13 Suspension 22 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 1.15

Shintech Addis, LA 01/25/13 Suspension 23 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 Alcohol SW-846-8015C 67561 Methanol 38

Shintech Addis, LA 01/25/13 Suspension 23 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.57

Shintech Addis, LA 01/25/13 Suspension 23 Aldehyde SW-846-8315A 50000 Formaldehyde 0.322

Shintech Addis, LA 01/25/13 Suspension 23 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 SVOC SW-846-8270D 98862 Acetophenone 1.55

Shintech Addis, LA 01/25/13 Suspension 23 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

R

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.016

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.129

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.024

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

R

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 VC EPA Method 107 75014 Vinyl chloride 0.095

J

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/25/13 Suspension 23 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 1.28

Shintech Addis, LA 01/26/13 Suspension 24 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 Alcohol SW-846-8015C 67561 Methanol 44

Shintech Addis, LA 01/26/13 Suspension 24 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.67

Shintech Addis, LA 01/26/13 Suspension 24 Aldehyde SW-846-8315A 50000 Formaldehyde 0.311

Shintech Addis, LA 01/26/13 Suspension 24 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 SVOC SW-846-8270D 98862 Acetophenone 1.31

Shintech Addis, LA 01/26/13 Suspension 24 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.014

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.095

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.019

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 VC EPA Method 107 75014 Vinyl chloride 0.073

J

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/26/13 Suspension 24 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 1.3

Shintech Addis, LA 01/27/13 Suspension 25 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 Alcohol SW-846-8015C 67561 Methanol 46

Shintech Addis, LA 01/27/13 Suspension 25 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.69

Shintech Addis, LA 01/27/13 Suspension 25 Aldehyde SW-846-8315A 50000 Formaldehyde 0.247

Shintech Addis, LA 01/27/13 Suspension 25 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 SVOC SW-846-8270D 98862 Acetophenone 1.25

Shintech Addis, LA 01/27/13 Suspension 25 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.015

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.125

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.020

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

12/12/2013 VI Confidential 8 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 VC EPA Method 107 75014 Vinyl chloride 0.075

J

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/27/13 Suspension 25 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 1.46

Shintech Addis, LA 01/28/13 Suspension 26 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 Alcohol SW-846-8015C 67561 Methanol 46

Shintech Addis, LA 01/28/13 Suspension 26 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.54

Shintech Addis, LA 01/28/13 Suspension 26 Aldehyde SW-846-8315A 50000 Formaldehyde 0.252

Shintech Addis, LA 01/28/13 Suspension 26 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.035 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 SVOC SW-846-8270D 98862 Acetophenone 0.51

Shintech Addis, LA 01/28/13 Suspension 26 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.025 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 SVOC SW-846-8270D 123319 Hydroquinone 0.05 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 SVOC SW-846-8270D 108952 Phenol 0.005 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.021

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.125

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.031

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 VC EPA Method 107 75014 Vinyl chloride 0.133

J

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/28/13 Suspension 26 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 1.22

Shintech Addis, LA 01/29/13 Suspension 27 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 Alcohol SW-846-8015C 67561 Methanol 36

Shintech Addis, LA 01/29/13 Suspension 27 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.57

Shintech Addis, LA 01/29/13 Suspension 27 Aldehyde SW-846-8315A 50000 Formaldehyde 0.314

Shintech Addis, LA 01/29/13 Suspension 27 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.035 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 SVOC SW-846-8270D 98862 Acetophenone 0.53

Shintech Addis, LA 01/29/13 Suspension 27 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.025 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 SVOC SW-846-8270D 123319 Hydroquinone 0.05 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 SVOC SW-846-8270D 108952 Phenol 0.005 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.012

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.091

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.017

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 VC EPA Method 107 75014 Vinyl chloride 0.083

J

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/29/13 Suspension 27 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.759

Shintech Addis, LA 01/30/13 Suspension 28 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 Alcohol SW-846-8015C 67561 Methanol 48

Shintech Addis, LA 01/30/13 Suspension 28 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.65

Shintech Addis, LA 01/30/13 Suspension 28 Aldehyde SW-846-8315A 50000 Formaldehyde 0.244

Shintech Addis, LA 01/30/13 Suspension 28 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 SVOC SW-846-8270D 98862 Acetophenone 0.99

Shintech Addis, LA 01/30/13 Suspension 28 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.015

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.095

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.021

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 VC EPA Method 107 75014 Vinyl chloride 0.092

J

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

12/12/2013 VI Confidential 9 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Addis, LA 01/30/13 Suspension 28 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.809

Shintech Addis, LA 01/31/13 Suspension 29 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Addis, LA 01/31/13 Suspension 29 Alcohol SW-846-8015C 67561 Methanol 48

Shintech Addis, LA 01/31/13 Suspension 29 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.8

Shintech Addis, LA 01/31/13 Suspension 29 Aldehyde SW-846-8315A 50000 Formaldehyde 0.198

Shintech Addis, LA 01/31/13 Suspension 29 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Addis, LA 01/31/13 Suspension 29 SVOC SW-846-8270D 98862 Acetophenone 1.1

Shintech Addis, LA 01/31/13 Suspension 29 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 01/31/13 Suspension 29 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 01/31/13 Suspension 29 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect R

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.015

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.104

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.026

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect UJ

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 01/31/13 Suspension 29 VC EPA Method 107 75014 Vinyl chloride 0.073 J

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 01/31/13 Suspension 29 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 1.2

Shintech Addis, LA 02/01/13 Suspension 30 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 Alcohol SW-846-8015C 67561 Methanol 56

Shintech Addis, LA 02/01/13 Suspension 30 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.641

Shintech Addis, LA 02/01/13 Suspension 30 Aldehyde SW-846-8315A 50000 Formaldehyde 0.13

Shintech Addis, LA 02/01/13 Suspension 30 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 SVOC SW-846-8270D 98862 Acetophenone 1.44

Shintech Addis, LA 02/01/13 Suspension 30 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect R

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.020

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.117

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.03

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect R

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 VC EPA Method 107 75014 Vinyl chloride 0.069 J

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Addis, LA 02/01/13 Suspension 30 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 1.13

Shintech Plaquemine, LA 01/03/13 Suspension 1 Alcohol SW-846-8015C 107211 Ethylene glycol 4 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 Alcohol SW-846-8015C 67561 Methanol 57 J

Shintech Plaquemine, LA 01/03/13 Suspension 1 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.98 J

Shintech Plaquemine, LA 01/03/13 Suspension 1 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect UJ

Shintech Plaquemine, LA 01/03/13 Suspension 1 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect UJ

Shintech Plaquemine, LA 01/03/13 Suspension 1 SVOC SW-846-8270D 98862 Acetophenone 4.16

Shintech Plaquemine, LA 01/03/13 Suspension 1 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.01 J

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.031

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.01

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect R

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 VC EPA Method 107 75014 Vinyl chloride 0.015 J

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Plaquemine, LA 01/03/13 Suspension 1 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.57

Shintech Plaquemine, LA 01/04/13 Suspension 2 Alcohol SW-846-8015C 107211 Ethylene glycol 4 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 Alcohol SW-846-8015C 67561 Methanol 58 J

Shintech Plaquemine, LA 01/04/13 Suspension 2 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.4

12/12/2013 VI Confidential 10 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Plaquemine, LA 01/04/13 Suspension 2 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect UJ

Shintech Plaquemine, LA 01/04/13 Suspension 2 SVOC SW-846-8270D 98862 Acetophenone 4.27

Shintech Plaquemine, LA 01/04/13 Suspension 2 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.01

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.037

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.01

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 VC EPA Method 107 75014 Vinyl chloride 0.02

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Plaquemine, LA 01/04/13 Suspension 2 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.638

Shintech Plaquemine, LA 01/05/13 Suspension 3 Alcohol SW-846-8015C 107211 Ethylene glycol 4 Non-detect UJ

Shintech Plaquemine, LA 01/05/13 Suspension 3 Alcohol SW-846-8015C 67561 Methanol 58 J

Shintech Plaquemine, LA 01/05/13 Suspension 3 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.37

Shintech Plaquemine, LA 01/05/13 Suspension 3 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 SVOC SW-846-8270D 98862 Acetophenone 3.54

Shintech Plaquemine, LA 01/05/13 Suspension 3 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.011

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.036

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.008

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 VC EPA Method 107 75014 Vinyl chloride 0.03

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Plaquemine, LA 01/05/13 Suspension 3 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.582

Shintech Plaquemine, LA 01/06/13 Suspension 4 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Plaquemine, LA 01/06/13 Suspension 4 Alcohol SW-846-8015C 67561 Methanol 62 J

Shintech Plaquemine, LA 01/06/13 Suspension 4 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.29

Shintech Plaquemine, LA 01/06/13 Suspension 4 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 SVOC SW-846-8270D 98862 Acetophenone 3.88

Shintech Plaquemine, LA 01/06/13 Suspension 4 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.01

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.041

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.013

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 VC EPA Method 107 75014 Vinyl chloride 0.023

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Plaquemine, LA 01/06/13 Suspension 4 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.673

Shintech Plaquemine, LA 01/07/13 Suspension 5 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Plaquemine, LA 01/07/13 Suspension 5 Alcohol SW-846-8015C 67561 Methanol 63 J

Shintech Plaquemine, LA 01/07/13 Suspension 5 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.25

Shintech Plaquemine, LA 01/07/13 Suspension 5 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 SVOC SW-846-8270D 98862 Acetophenone 1.75

Shintech Plaquemine, LA 01/07/13 Suspension 5 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

12/12/2013 VI Confidential 11 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Plaquemine, LA 01/07/13 Suspension 5 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.01

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.024

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.007

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 VC EPA Method 107 75014 Vinyl chloride 0.02

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Plaquemine, LA 01/07/13 Suspension 5 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.266

Shintech Plaquemine, LA 01/08/13 Suspension 6 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Plaquemine, LA 01/08/13 Suspension 6 Alcohol SW-846-8015C 67561 Methanol 69 J

Shintech Plaquemine, LA 01/08/13 Suspension 6 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.62

Shintech Plaquemine, LA 01/08/13 Suspension 6 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 SVOC SW-846-8270D 98862 Acetophenone 4.6

Shintech Plaquemine, LA 01/08/13 Suspension 6 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.014

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.032

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 J

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.008

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 VC EPA Method 107 75014 Vinyl chloride 0.043

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Plaquemine, LA 01/08/13 Suspension 6 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.487

Shintech Plaquemine, LA 01/09/13 Suspension 7 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Plaquemine, LA 01/09/13 Suspension 7 Alcohol SW-846-8015C 67561 Methanol 63 J

Shintech Plaquemine, LA 01/09/13 Suspension 7 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.08

Shintech Plaquemine, LA 01/09/13 Suspension 7 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 SVOC SW-846-8270D 98862 Acetophenone 4.71

Shintech Plaquemine, LA 01/09/13 Suspension 7 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.03

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.003 J

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 VC EPA Method 107 75014 Vinyl chloride 0.008 J

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Plaquemine, LA 01/09/13 Suspension 7 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.723

Shintech Plaquemine, LA 01/10/13 Suspension 8 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Plaquemine, LA 01/10/13 Suspension 8 Alcohol SW-846-8015C 67561 Methanol 57 J

Shintech Plaquemine, LA 01/10/13 Suspension 8 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.92

Shintech Plaquemine, LA 01/10/13 Suspension 8 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect UJ

Shintech Plaquemine, LA 01/10/13 Suspension 8 SVOC SW-846-8270D 98862 Acetophenone 2.97

Shintech Plaquemine, LA 01/10/13 Suspension 8 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

12/12/2013 VI Confidential 12 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.024

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.004 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 VC EPA Method 107 75014 Vinyl chloride 0.05

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Plaquemine, LA 01/10/13 Suspension 8 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.641

Shintech Plaquemine, LA 01/11/13 Suspension 9 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 Alcohol SW-846-8015C 67561 Methanol 41 J

Shintech Plaquemine, LA 01/11/13 Suspension 9 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.38

Shintech Plaquemine, LA 01/11/13 Suspension 9 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect UJ

Shintech Plaquemine, LA 01/11/13 Suspension 9 SVOC SW-846-8270D 98862 Acetophenone 3.37

Shintech Plaquemine, LA 01/11/13 Suspension 9 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.014

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.065

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.016

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect UJ

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 VC EPA Method 107 75014 Vinyl chloride 0.048

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Plaquemine, LA 01/11/13 Suspension 9 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.895

Shintech Plaquemine, LA 01/12/13 Suspension 10 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 Alcohol SW-846-8015C 67561 Methanol 50 J

Shintech Plaquemine, LA 01/12/13 Suspension 10 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.61

Shintech Plaquemine, LA 01/12/13 Suspension 10 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect UJ

Shintech Plaquemine, LA 01/12/13 Suspension 10 SVOC SW-846-8270D 98862 Acetophenone 3.44

Shintech Plaquemine, LA 01/12/13 Suspension 10 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.013

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.035

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.013

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect UJ

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 VC EPA Method 107 75014 Vinyl chloride 0.057 J

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Plaquemine, LA 01/12/13 Suspension 10 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.583

Shintech Plaquemine, LA 01/13/13 Suspension 11 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Plaquemine, LA 01/13/13 Suspension 11 Alcohol SW-846-8015C 67561 Methanol 61 J

Shintech Plaquemine, LA 01/13/13 Suspension 11 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.64

Shintech Plaquemine, LA 01/13/13 Suspension 11 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/13/13 Suspension 11 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect UJ

Shintech Plaquemine, LA 01/13/13 Suspension 11 SVOC SW-846-8270D 98862 Acetophenone 4.24

Shintech Plaquemine, LA 01/13/13 Suspension 11 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/13/13 Suspension 11 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/13/13 Suspension 11 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.019

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.032

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 J

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.01

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Plaquemine, LA 01/13/13 Suspension 11 VC EPA Method 107 75014 Vinyl chloride 0.104 J

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Plaquemine, LA 01/13/13 Suspension 11 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.519

Shintech Plaquemine, LA 01/14/13 Suspension 12 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 Alcohol SW-846-8015C 67561 Methanol 63 J

Shintech Plaquemine, LA 01/14/13 Suspension 12 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.68

Shintech Plaquemine, LA 01/14/13 Suspension 12 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect UJ

Shintech Plaquemine, LA 01/14/13 Suspension 12 SVOC SW-846-8270D 98862 Acetophenone 3.19

Shintech Plaquemine, LA 01/14/13 Suspension 12 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.009 J

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.028

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.007 J

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect UJ

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 VC EPA Method 107 75014 Vinyl chloride 0.021

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Plaquemine, LA 01/14/13 Suspension 12 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.658

Shintech Plaquemine, LA 01/15/13 Suspension 13 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 Alcohol SW-846-8015C 67561 Methanol 65 J

Shintech Plaquemine, LA 01/15/13 Suspension 13 Aldehyde SW-846-8315A 75070 Acetaldehyde 5

Shintech Plaquemine, LA 01/15/13 Suspension 13 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 SVOC SW-846-8270D 98862 Acetophenone 3.51

Shintech Plaquemine, LA 01/15/13 Suspension 13 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.015

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.034

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.008 J

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 VC EPA Method 107 75014 Vinyl chloride 0.025

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Plaquemine, LA 01/15/13 Suspension 13 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.692

Shintech Plaquemine, LA 01/16/13 Suspension 14 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 Alcohol SW-846-8015C 67561 Methanol 56 J

Shintech Plaquemine, LA 01/16/13 Suspension 14 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.2

Shintech Plaquemine, LA 01/16/13 Suspension 14 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 SVOC SW-846-8270D 98862 Acetophenone 3.43

Shintech Plaquemine, LA 01/16/13 Suspension 14 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.016

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

12/12/2013 VI Confidential 14 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.032

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.01 J

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect UJ

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 VC EPA Method 107 75014 Vinyl chloride 0.045

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Plaquemine, LA 01/16/13 Suspension 14 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.452

Shintech Plaquemine, LA 01/17/13 Suspension 15 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 Alcohol SW-846-8015C 67561 Methanol 86 J

Shintech Plaquemine, LA 01/17/13 Suspension 15 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.98

Shintech Plaquemine, LA 01/17/13 Suspension 15 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 SVOC SW-846-8270D 98862 Acetophenone 4.3

Shintech Plaquemine, LA 01/17/13 Suspension 15 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect R

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.011

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.038

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.009 J

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect R

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 VC EPA Method 107 75014 Vinyl chloride 0.035

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Plaquemine, LA 01/17/13 Suspension 15 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.604

Shintech Plaquemine, LA 01/18/13 Suspension 16 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 Alcohol SW-846-8015C 67561 Methanol 49 J

Shintech Plaquemine, LA 01/18/13 Suspension 16 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.18

Shintech Plaquemine, LA 01/18/13 Suspension 16 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 SVOC SW-846-8270D 98862 Acetophenone 4.34

Shintech Plaquemine, LA 01/18/13 Suspension 16 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.008 J

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.038

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.009 J

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 VC EPA Method 107 75014 Vinyl chloride 0.027

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Plaquemine, LA 01/18/13 Suspension 16 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.856

Shintech Plaquemine, LA 01/19/13 Suspension 17 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 Alcohol SW-846-8015C 67561 Methanol 55 J

Shintech Plaquemine, LA 01/19/13 Suspension 17 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.09

Shintech Plaquemine, LA 01/19/13 Suspension 17 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 SVOC SW-846-8270D 98862 Acetophenone 3.43

Shintech Plaquemine, LA 01/19/13 Suspension 17 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.021

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.028

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 J

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.01

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

12/12/2013 VI Confidential 15 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 VC EPA Method 107 75014 Vinyl chloride 0.099 J

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Plaquemine, LA 01/19/13 Suspension 17 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.365

Shintech Plaquemine, LA 01/20/13 Suspension 18 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 Alcohol SW-846-8015C 67561 Methanol 60 J

Shintech Plaquemine, LA 01/20/13 Suspension 18 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.33

Shintech Plaquemine, LA 01/20/13 Suspension 18 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 SVOC SW-846-8270D 98862 Acetophenone 3.75

Shintech Plaquemine, LA 01/20/13 Suspension 18 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.018

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.028

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 J

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.01

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 VC EPA Method 107 75014 Vinyl chloride 0.082 J

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Plaquemine, LA 01/20/13 Suspension 18 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.363

Shintech Plaquemine, LA 01/21/13 Suspension 19 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 Alcohol SW-846-8015C 67561 Methanol 61 J

Shintech Plaquemine, LA 01/21/13 Suspension 19 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.9

Shintech Plaquemine, LA 01/21/13 Suspension 19 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 SVOC SW-846-8270D 98862 Acetophenone 3.96

Shintech Plaquemine, LA 01/21/13 Suspension 19 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.014

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.027

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.009

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 VC EPA Method 107 75014 Vinyl chloride 0.042

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Plaquemine, LA 01/21/13 Suspension 19 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.36

Shintech Plaquemine, LA 01/22/13 Suspension 20 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 Alcohol SW-846-8015C 67561 Methanol 52 J

Shintech Plaquemine, LA 01/22/13 Suspension 20 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.81

Shintech Plaquemine, LA 01/22/13 Suspension 20 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 SVOC SW-846-8270D 98862 Acetophenone 4.08

Shintech Plaquemine, LA 01/22/13 Suspension 20 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.006

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

12/12/2013 VI Confidential 16 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 VC EPA Method 107 75014 Vinyl chloride 0.047

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Plaquemine, LA 01/22/13 Suspension 20 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.085

Shintech Plaquemine, LA 01/23/13 Suspension 21 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 Alcohol SW-846-8015C 67561 Methanol 56 J

Shintech Plaquemine, LA 01/23/13 Suspension 21 Aldehyde SW-846-8315A 75070 Acetaldehyde 8.31

Shintech Plaquemine, LA 01/23/13 Suspension 21 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 SVOC SW-846-8270D 98862 Acetophenone 4.47

Shintech Plaquemine, LA 01/23/13 Suspension 21 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.011

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.038

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.009 J

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect UJ

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 VC EPA Method 107 75014 Vinyl chloride 0.03

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Plaquemine, LA 01/23/13 Suspension 21 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.58

Shintech Plaquemine, LA 01/24/13 Suspension 22 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 Alcohol SW-846-8015C 67561 Methanol 53 J

Shintech Plaquemine, LA 01/24/13 Suspension 22 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.55

Shintech Plaquemine, LA 01/24/13 Suspension 22 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 SVOC SW-846-8270D 98862 Acetophenone 3.99

Shintech Plaquemine, LA 01/24/13 Suspension 22 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.01

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.044

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.01 J

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect UJ

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 VC EPA Method 107 75014 Vinyl chloride 0.041

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Plaquemine, LA 01/24/13 Suspension 22 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.574

Shintech Plaquemine, LA 01/25/13 Suspension 23 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 Alcohol SW-846-8015C 67561 Methanol 56 J

Shintech Plaquemine, LA 01/25/13 Suspension 23 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.06

Shintech Plaquemine, LA 01/25/13 Suspension 23 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 SVOC SW-846-8270D 98862 Acetophenone 4.1

Shintech Plaquemine, LA 01/25/13 Suspension 23 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 98828 Cumene 0.003 J

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.008 J

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.025

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.004 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 VC EPA Method 107 75014 Vinyl chloride 0.073 J

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

12/12/2013 VI Confidential 17 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Plaquemine, LA 01/25/13 Suspension 23 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.538

Shintech Plaquemine, LA 01/26/13 Suspension 24 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 Alcohol SW-846-8015C 67561 Methanol 57 J

Shintech Plaquemine, LA 01/26/13 Suspension 24 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.96

Shintech Plaquemine, LA 01/26/13 Suspension 24 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 SVOC SW-846-8270D 98862 Acetophenone 4.61

Shintech Plaquemine, LA 01/26/13 Suspension 24 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.01

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.039

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.007 J

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 VC EPA Method 107 75014 Vinyl chloride 0.02

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Plaquemine, LA 01/26/13 Suspension 24 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.6

Shintech Plaquemine, LA 01/27/13 Suspension 25 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 Alcohol SW-846-8015C 67561 Methanol 60 J

Shintech Plaquemine, LA 01/27/13 Suspension 25 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.07

Shintech Plaquemine, LA 01/27/13 Suspension 25 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 SVOC SW-846-8270D 98862 Acetophenone 3.83

Shintech Plaquemine, LA 01/27/13 Suspension 25 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.007

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.021

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.004 J

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 VC EPA Method 107 75014 Vinyl chloride 0.037

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Plaquemine, LA 01/27/13 Suspension 25 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.356

Shintech Plaquemine, LA 01/28/13 Suspension 26 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 Alcohol SW-846-8015C 67561 Methanol 60 J

Shintech Plaquemine, LA 01/28/13 Suspension 26 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.08

Shintech Plaquemine, LA 01/28/13 Suspension 26 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 SVOC SW-846-8270D 98862 Acetophenone 5.02

Shintech Plaquemine, LA 01/28/13 Suspension 26 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.011

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.036

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.006 J

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 VC EPA Method 107 75014 Vinyl chloride 0.03

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Plaquemine, LA 01/28/13 Suspension 26 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.59

Shintech Plaquemine, LA 01/29/13 Suspension 27 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 Alcohol SW-846-8015C 67561 Methanol 56 J

12/12/2013 VI Confidential 18 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Plaquemine, LA 01/29/13 Suspension 27 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.01

Shintech Plaquemine, LA 01/29/13 Suspension 27 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 SVOC SW-846-8270D 98862 Acetophenone 4.22

Shintech Plaquemine, LA 01/29/13 Suspension 27 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.018

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.035

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 J

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.008

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 VC EPA Method 107 75014 Vinyl chloride 0.091 J

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Plaquemine, LA 01/29/13 Suspension 27 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.454

Shintech Plaquemine, LA 01/30/13 Suspension 28 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 Alcohol SW-846-8015C 67561 Methanol 65 J

Shintech Plaquemine, LA 01/30/13 Suspension 28 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.86

Shintech Plaquemine, LA 01/30/13 Suspension 28 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 SVOC SW-846-8270D 98862 Acetophenone 4.78

Shintech Plaquemine, LA 01/30/13 Suspension 28 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.012

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.06

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.008 J

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 VC EPA Method 107 75014 Vinyl chloride 0.058 J

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Plaquemine, LA 01/30/13 Suspension 28 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 1.13

Shintech Plaquemine, LA 01/31/13 Suspension 29 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Plaquemine, LA 01/31/13 Suspension 29 Alcohol SW-846-8015C 67561 Methanol 53 J

Shintech Plaquemine, LA 01/31/13 Suspension 29 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.05

Shintech Plaquemine, LA 01/31/13 Suspension 29 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 SVOC SW-846-8270D 98862 Acetophenone 4.79

Shintech Plaquemine, LA 01/31/13 Suspension 29 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 106990 1,3-butadiene 0.004 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.002 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 71432 Benzene 0.002 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 108907 Chlorobenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 126998 Chloroprene 0.004 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 98828 Cumene 0.002 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.01

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.024

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.004 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 108883 Toluene 0.002 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.002 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.002 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 108054 Vinyl acetate 0.002 Non-detect UJ

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 VC EPA Method 107 75014 Vinyl chloride 0.046 J

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.002 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.004 Non-detect

Shintech Plaquemine, LA 01/31/13 Suspension 29 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.315

Shintech Plaquemine, LA 02/01/13 Suspension 30 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 Alcohol SW-846-8015C 67561 Methanol 53 J

Shintech Plaquemine, LA 02/01/13 Suspension 30 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.17

Shintech Plaquemine, LA 02/01/13 Suspension 30 Aldehyde SW-846-8315A 50000 Formaldehyde 0.568

Shintech Plaquemine, LA 02/01/13 Suspension 30 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 SVOC SW-846-8270D 98862 Acetophenone 3.49

12/12/2013 VI Confidential 19 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Plaquemine, LA 02/01/13 Suspension 30 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.036

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.044

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.002 J

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.014

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 VC EPA Method 107 75014 Vinyl chloride 0.182 J

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Plaquemine, LA 02/01/13 Suspension 30 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.368

Shintech Freeport1, TX 01/03/13 Suspension 1 Alcohol SW-846-8015C 107211 Ethylene glycol 4 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 Alcohol SW-846-8015C 67561 Methanol 47

Shintech Freeport1, TX 01/03/13 Suspension 1 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.59 J

Shintech Freeport1, TX 01/03/13 Suspension 1 Aldehyde SW-846-8315A 50000 Formaldehyde 0.075 Non-detect R

Shintech Freeport1, TX 01/03/13 Suspension 1 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect UJ

Shintech Freeport1, TX 01/03/13 Suspension 1 SVOC SW-846-8270D 98862 Acetophenone 2.52 J

Shintech Freeport1, TX 01/03/13 Suspension 1 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 J

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.054

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.011 J

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect UJ

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/03/13 Suspension 1 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.098

Shintech Freeport1, TX 01/04/13 Suspension 2 Alcohol SW-846-8015C 107211 Ethylene glycol 4 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 Alcohol SW-846-8015C 67561 Methanol 51

Shintech Freeport1, TX 01/04/13 Suspension 2 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.62

Shintech Freeport1, TX 01/04/13 Suspension 2 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect UJ

Shintech Freeport1, TX 01/04/13 Suspension 2 SVOC SW-846-8270D 98862 Acetophenone 4.11

Shintech Freeport1, TX 01/04/13 Suspension 2 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.056

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.012

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/04/13 Suspension 2 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.093

Shintech Freeport1, TX 01/05/13 Suspension 3 Alcohol SW-846-8015C 107211 Ethylene glycol 4 Non-detect UJ

Shintech Freeport1, TX 01/05/13 Suspension 3 Alcohol SW-846-8015C 67561 Methanol 48

Shintech Freeport1, TX 01/05/13 Suspension 3 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.03

Shintech Freeport1, TX 01/05/13 Suspension 3 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 SVOC SW-846-8270D 98862 Acetophenone 3.79

Shintech Freeport1, TX 01/05/13 Suspension 3 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

12/12/2013 VI Confidential 20 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.046

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.01

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/05/13 Suspension 3 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.095

Shintech Freeport1, TX 01/06/13 Suspension 4 Alcohol SW-846-8015C 107211 Ethylene glycol 4 Non-detect UJ

Shintech Freeport1, TX 01/06/13 Suspension 4 Alcohol SW-846-8015C 67561 Methanol 44

Shintech Freeport1, TX 01/06/13 Suspension 4 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.67

Shintech Freeport1, TX 01/06/13 Suspension 4 Aldehyde SW-846-8315A 50000 Formaldehyde 0.152 J

Shintech Freeport1, TX 01/06/13 Suspension 4 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 SVOC SW-846-8270D 98862 Acetophenone 3.07

Shintech Freeport1, TX 01/06/13 Suspension 4 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.058

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.012

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/06/13 Suspension 4 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.086

Shintech Freeport1, TX 01/07/13 Suspension 5 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Freeport1, TX 01/07/13 Suspension 5 Alcohol SW-846-8015C 67561 Methanol 22

Shintech Freeport1, TX 01/07/13 Suspension 5 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.36

Shintech Freeport1, TX 01/07/13 Suspension 5 Aldehyde SW-846-8315A 50000 Formaldehyde 0.186 J

Shintech Freeport1, TX 01/07/13 Suspension 5 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 SVOC SW-846-8270D 98862 Acetophenone 3.67

Shintech Freeport1, TX 01/07/13 Suspension 5 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.044

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.009

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/07/13 Suspension 5 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.063

Shintech Freeport1, TX 01/08/13 Suspension 6 Alcohol SW-846-8015C 107211 Ethylene glycol 4 Non-detect UJ

Shintech Freeport1, TX 01/08/13 Suspension 6 Alcohol SW-846-8015C 67561 Methanol 41

Shintech Freeport1, TX 01/08/13 Suspension 6 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.79

Shintech Freeport1, TX 01/08/13 Suspension 6 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 SVOC SW-846-8270D 98862 Acetophenone 4.43

Shintech Freeport1, TX 01/08/13 Suspension 6 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

12/12/2013 VI Confidential 21 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.06

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.015

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/08/13 Suspension 6 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.097

Shintech Freeport1, TX 01/09/13 Suspension 7 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 Alcohol SW-846-8015C 67561 Methanol 56

Shintech Freeport1, TX 01/09/13 Suspension 7 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.68

Shintech Freeport1, TX 01/09/13 Suspension 7 Aldehyde SW-846-8315A 50000 Formaldehyde 0.075 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect UJ

Shintech Freeport1, TX 01/09/13 Suspension 7 SVOC SW-846-8270D 98862 Acetophenone 3.28

Shintech Freeport1, TX 01/09/13 Suspension 7 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.036

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.014

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/09/13 Suspension 7 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.041

Shintech Freeport1, TX 01/10/13 Suspension 8 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Freeport1, TX 01/10/13 Suspension 8 Alcohol SW-846-8015C 67561 Methanol 56

Shintech Freeport1, TX 01/10/13 Suspension 8 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.77

Shintech Freeport1, TX 01/10/13 Suspension 8 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect UJ

Shintech Freeport1, TX 01/10/13 Suspension 8 SVOC SW-846-8270D 98862 Acetophenone 4.07

Shintech Freeport1, TX 01/10/13 Suspension 8 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.05

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.01

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/10/13 Suspension 8 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.059

Shintech Freeport1, TX 01/11/13 Suspension 9 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Freeport1, TX 01/11/13 Suspension 9 Alcohol SW-846-8015C 67561 Methanol 57

Shintech Freeport1, TX 01/11/13 Suspension 9 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.92

Shintech Freeport1, TX 01/11/13 Suspension 9 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect UJ

Shintech Freeport1, TX 01/11/13 Suspension 9 SVOC SW-846-8270D 98862 Acetophenone 5.08

Shintech Freeport1, TX 01/11/13 Suspension 9 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 SVOC SW-846-8270D 123319 Hydroquinone 0.5 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.034

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.005 J

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/11/13 Suspension 9 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.052

Shintech Freeport1, TX 01/12/13 Suspension 10 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Freeport1, TX 01/12/13 Suspension 10 Alcohol SW-846-8015C 67561 Methanol 59

Shintech Freeport1, TX 01/12/13 Suspension 10 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.43

Shintech Freeport1, TX 01/12/13 Suspension 10 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect UJ

Shintech Freeport1, TX 01/12/13 Suspension 10 SVOC SW-846-8270D 98862 Acetophenone 2.63

Shintech Freeport1, TX 01/12/13 Suspension 10 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.048

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.012

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/12/13 Suspension 10 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.051

Shintech Freeport1, TX 01/13/13 Suspension 11 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 Alcohol SW-846-8015C 67561 Methanol 41

Shintech Freeport1, TX 01/13/13 Suspension 11 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.85

Shintech Freeport1, TX 01/13/13 Suspension 11 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect UJ

Shintech Freeport1, TX 01/13/13 Suspension 11 SVOC SW-846-8270D 98862 Acetophenone 2.8

Shintech Freeport1, TX 01/13/13 Suspension 11 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.041

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.013

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/13/13 Suspension 11 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.06

Shintech Freeport1, TX 01/14/13 Suspension 12 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 Alcohol SW-846-8015C 67561 Methanol 44

Shintech Freeport1, TX 01/14/13 Suspension 12 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.53

Shintech Freeport1, TX 01/14/13 Suspension 12 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect UJ

Shintech Freeport1, TX 01/14/13 Suspension 12 SVOC SW-846-8270D 98862 Acetophenone 3.47

Shintech Freeport1, TX 01/14/13 Suspension 12 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.005 J

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.048

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.013

12/12/2013 VI Confidential 23 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 VC EPA Method 107 75014 Vinyl chloride 0.021

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/14/13 Suspension 12 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.07

Shintech Freeport1, TX 01/15/13 Suspension 13 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 Alcohol SW-846-8015C 67561 Methanol 50

Shintech Freeport1, TX 01/15/13 Suspension 13 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.71

Shintech Freeport1, TX 01/15/13 Suspension 13 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 SVOC SW-846-8270D 98862 Acetophenone 2.47

Shintech Freeport1, TX 01/15/13 Suspension 13 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.045

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.014

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/15/13 Suspension 13 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.068

Shintech Freeport1, TX 01/16/13 Suspension 14 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 Alcohol SW-846-8015C 67561 Methanol 30

Shintech Freeport1, TX 01/16/13 Suspension 14 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.98

Shintech Freeport1, TX 01/16/13 Suspension 14 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 SVOC SW-846-8270D 98862 Acetophenone 2.17

Shintech Freeport1, TX 01/16/13 Suspension 14 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.004 J

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.066

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.018

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 VC EPA Method 107 75014 Vinyl chloride 0.006

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/16/13 Suspension 14 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.109

Shintech Freeport1, TX 01/17/13 Suspension 15 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 Alcohol SW-846-8015C 67561 Methanol 56

Shintech Freeport1, TX 01/17/13 Suspension 15 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.51

Shintech Freeport1, TX 01/17/13 Suspension 15 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 SVOC SW-846-8270D 98862 Acetophenone 3.06

Shintech Freeport1, TX 01/17/13 Suspension 15 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.048

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.012

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/17/13 Suspension 15 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.076

Shintech Freeport1, TX 01/18/13 Suspension 16 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 Alcohol SW-846-8015C 67561 Methanol 39

Shintech Freeport1, TX 01/18/13 Suspension 16 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.36

Shintech Freeport1, TX 01/18/13 Suspension 16 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 SVOC SW-846-8270D 98862 Acetophenone 2.49

Shintech Freeport1, TX 01/18/13 Suspension 16 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.044

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.01

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/18/13 Suspension 16 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.063

Shintech Freeport1, TX 01/19/13 Suspension 17 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 Alcohol SW-846-8015C 67561 Methanol 42

Shintech Freeport1, TX 01/19/13 Suspension 17 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.1

Shintech Freeport1, TX 01/19/13 Suspension 17 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 SVOC SW-846-8270D 98862 Acetophenone 2.35

Shintech Freeport1, TX 01/19/13 Suspension 17 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.004 J

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.043

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.014

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 VC EPA Method 107 75014 Vinyl chloride 0.007

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/19/13 Suspension 17 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.064

Shintech Freeport1, TX 01/20/13 Suspension 18 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 Alcohol SW-846-8015C 67561 Methanol 42

Shintech Freeport1, TX 01/20/13 Suspension 18 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.04

Shintech Freeport1, TX 01/20/13 Suspension 18 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 SVOC SW-846-8270D 98862 Acetophenone 3.87

Shintech Freeport1, TX 01/20/13 Suspension 18 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.039

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.012

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 VC EPA Method 107 75014 Vinyl chloride 0.006

12/12/2013 VI Confidential 25 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/20/13 Suspension 18 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.053

Shintech Freeport1, TX 01/21/13 Suspension 19 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 Alcohol SW-846-8015C 67561 Methanol 44

Shintech Freeport1, TX 01/21/13 Suspension 19 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.49

Shintech Freeport1, TX 01/21/13 Suspension 19 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 SVOC SW-846-8270D 98862 Acetophenone 3.95

Shintech Freeport1, TX 01/21/13 Suspension 19 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 98828 Cumene 0.002 J

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.004 J

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.039 J

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.013

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/21/13 Suspension 19 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.055

Shintech Freeport1, TX 01/22/13 Suspension 20 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 Alcohol SW-846-8015C 67561 Methanol 60

Shintech Freeport1, TX 01/22/13 Suspension 20 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.12

Shintech Freeport1, TX 01/22/13 Suspension 20 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 SVOC SW-846-8270D 98862 Acetophenone 3.8

Shintech Freeport1, TX 01/22/13 Suspension 20 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.061

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.012

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/22/13 Suspension 20 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.082

Shintech Freeport1, TX 01/23/13 Suspension 21 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 Alcohol SW-846-8015C 67561 Methanol 51

Shintech Freeport1, TX 01/23/13 Suspension 21 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.02

Shintech Freeport1, TX 01/23/13 Suspension 21 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 SVOC SW-846-8270D 98862 Acetophenone 3.97

Shintech Freeport1, TX 01/23/13 Suspension 21 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 SVOC SW-846-8270D 123319 Hydroquinone 0.5 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.055

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.013

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/23/13 Suspension 21 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.056

Shintech Freeport1, TX 01/24/13 Suspension 22 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport1, TX 01/24/13 Suspension 22 Alcohol SW-846-8015C 67561 Methanol 55

Shintech Freeport1, TX 01/24/13 Suspension 22 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.24

Shintech Freeport1, TX 01/24/13 Suspension 22 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 SVOC SW-846-8270D 98862 Acetophenone 4.28

Shintech Freeport1, TX 01/24/13 Suspension 22 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.05

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.012

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/24/13 Suspension 22 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.053

Shintech Freeport1, TX 01/25/13 Suspension 23 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 Alcohol SW-846-8015C 67561 Methanol 39

Shintech Freeport1, TX 01/25/13 Suspension 23 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.11

Shintech Freeport1, TX 01/25/13 Suspension 23 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 SVOC SW-846-8270D 98862 Acetophenone 4.66

Shintech Freeport1, TX 01/25/13 Suspension 23 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.048

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.009

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/25/13 Suspension 23 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.063

Shintech Freeport1, TX 01/26/13 Suspension 24 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 Alcohol SW-846-8015C 67561 Methanol 34

Shintech Freeport1, TX 01/26/13 Suspension 24 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.13

Shintech Freeport1, TX 01/26/13 Suspension 24 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 SVOC SW-846-8270D 98862 Acetophenone 2.88

Shintech Freeport1, TX 01/26/13 Suspension 24 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.045

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.009

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/26/13 Suspension 24 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.056

Shintech Freeport1, TX 01/27/13 Suspension 25 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 Alcohol SW-846-8015C 67561 Methanol 40

Shintech Freeport1, TX 01/27/13 Suspension 25 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.78

Shintech Freeport1, TX 01/27/13 Suspension 25 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport1, TX 01/27/13 Suspension 25 SVOC SW-846-8270D 98862 Acetophenone 2.3

Shintech Freeport1, TX 01/27/13 Suspension 25 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.045

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.006

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/27/13 Suspension 25 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.053

Shintech Freeport1, TX 01/28/13 Suspension 26 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 Alcohol SW-846-8015C 67561 Methanol 38

Shintech Freeport1, TX 01/28/13 Suspension 26 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.5

Shintech Freeport1, TX 01/28/13 Suspension 26 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 SVOC SW-846-8270D 98862 Acetophenone 3.29

Shintech Freeport1, TX 01/28/13 Suspension 26 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.041

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.008

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/28/13 Suspension 26 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.048

Shintech Freeport1, TX 01/29/13 Suspension 27 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 Alcohol SW-846-8015C 67561 Methanol 44

Shintech Freeport1, TX 01/29/13 Suspension 27 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.69

Shintech Freeport1, TX 01/29/13 Suspension 27 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 SVOC SW-846-8270D 98862 Acetophenone 4.79

Shintech Freeport1, TX 01/29/13 Suspension 27 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.045

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.007

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 VC EPA Method 107 75014 Vinyl chloride 0.009

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/29/13 Suspension 27 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.052

Shintech Freeport1, TX 01/30/13 Suspension 28 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 Alcohol SW-846-8015C 67561 Methanol 40

Shintech Freeport1, TX 01/30/13 Suspension 28 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.54

Shintech Freeport1, TX 01/30/13 Suspension 28 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 SVOC SW-846-8270D 98862 Acetophenone 2.43

Shintech Freeport1, TX 01/30/13 Suspension 28 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

12/12/2013 VI Confidential 28 of 183
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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.043

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.007

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/30/13 Suspension 28 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.056

Shintech Freeport1, TX 01/31/13 Suspension 29 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 Alcohol SW-846-8015C 67561 Methanol 40

Shintech Freeport1, TX 01/31/13 Suspension 29 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.76

Shintech Freeport1, TX 01/31/13 Suspension 29 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 SVOC SW-846-8270D 98862 Acetophenone 3.14

Shintech Freeport1, TX 01/31/13 Suspension 29 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 J

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.044

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.006

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect J

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 01/31/13 Suspension 29 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.064

Shintech Freeport1, TX 02/01/13 Suspension 30 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 Alcohol SW-846-8015C 67561 Methanol 37

Shintech Freeport1, TX 02/01/13 Suspension 30 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.76

Shintech Freeport1, TX 02/01/13 Suspension 30 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.175 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 SVOC SW-846-8270D 98862 Acetophenone 3.49

Shintech Freeport1, TX 02/01/13 Suspension 30 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.125 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 SVOC SW-846-8270D 123319 Hydroquinone 0.25 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.051

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.01

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 VC EPA Method 107 75014 Vinyl chloride 0.006 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport1, TX 02/01/13 Suspension 30 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.06

Shintech Freeport2, TX 01/03/13 Suspension 1 Alcohol SW-846-8015C 107211 Ethylene glycol 4 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 Alcohol SW-846-8015C 67561 Methanol 29 J

Shintech Freeport2, TX 01/03/13 Suspension 1 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.86 J

Shintech Freeport2, TX 01/03/13 Suspension 1 Aldehyde SW-846-8315A 50000 Formaldehyde 0.331 J

Shintech Freeport2, TX 01/03/13 Suspension 1 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect UJ

Shintech Freeport2, TX 01/03/13 Suspension 1 SVOC SW-846-8270D 98862 Acetophenone 0.254

Shintech Freeport2, TX 01/03/13 Suspension 1 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

12/12/2013 VI Confidential 29 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.008

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 J

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 VC EPA Method 107 75014 Vinyl chloride 0.01 J

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/03/13 Suspension 1 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.013

Shintech Freeport2, TX 01/04/13 Suspension 2 Alcohol SW-846-8015C 107211 Ethylene glycol 4 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 Alcohol SW-846-8015C 67561 Methanol 32 J

Shintech Freeport2, TX 01/04/13 Suspension 2 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.67

Shintech Freeport2, TX 01/04/13 Suspension 2 Aldehyde SW-846-8315A 50000 Formaldehyde 0.574

Shintech Freeport2, TX 01/04/13 Suspension 2 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect UJ

Shintech Freeport2, TX 01/04/13 Suspension 2 SVOC SW-846-8270D 98862 Acetophenone 0.346

Shintech Freeport2, TX 01/04/13 Suspension 2 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.01

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 VC EPA Method 107 75014 Vinyl chloride 0.017

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/04/13 Suspension 2 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.014

Shintech Freeport2, TX 01/05/13 Suspension 3 Alcohol SW-846-8015C 107211 Ethylene glycol 4 Non-detect UJ

Shintech Freeport2, TX 01/05/13 Suspension 3 Alcohol SW-846-8015C 67561 Methanol 31 J

Shintech Freeport2, TX 01/05/13 Suspension 3 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.12

Shintech Freeport2, TX 01/05/13 Suspension 3 Aldehyde SW-846-8315A 50000 Formaldehyde 0.504

Shintech Freeport2, TX 01/05/13 Suspension 3 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.035 Non-detect UJ

Shintech Freeport2, TX 01/05/13 Suspension 3 SVOC SW-846-8270D 98862 Acetophenone 0.595

Shintech Freeport2, TX 01/05/13 Suspension 3 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.025 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 SVOC SW-846-8270D 123319 Hydroquinone 0.05 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 SVOC SW-846-8270D 108952 Phenol 0.005 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.01

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 VC EPA Method 107 75014 Vinyl chloride 0.01

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/05/13 Suspension 3 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.015

Shintech Freeport2, TX 01/06/13 Suspension 4 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Freeport2, TX 01/06/13 Suspension 4 Alcohol SW-846-8015C 67561 Methanol 32 J

Shintech Freeport2, TX 01/06/13 Suspension 4 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.35

Shintech Freeport2, TX 01/06/13 Suspension 4 Aldehyde SW-846-8315A 50000 Formaldehyde 0.641

Shintech Freeport2, TX 01/06/13 Suspension 4 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension 4 SVOC SW-846-8270D 98862 Acetophenone 1.56

Shintech Freeport2, TX 01/06/13 Suspension 4 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension 4 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension 4 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension 4 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension 4 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension 4 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension 4 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension 4 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension 4 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension 4 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension 4 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

12/12/2013 VI Confidential 30 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport2, TX 01/06/13 Suspension4 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003

J

Shintech Freeport2, TX 01/06/13 Suspension4 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension4 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.012

Shintech Freeport2, TX 01/06/13 Suspension4 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension4 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension4 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension4 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension4 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension4 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension4 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension4 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport2, TX 01/06/13 Suspension4 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension4 VC EPA Method 107 75014 Vinyl chloride 0.012

Shintech Freeport2, TX 01/06/13 Suspension4 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension4 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/06/13 Suspension4 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.018

Shintech Freeport2, TX 01/07/13 Suspension5 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Freeport2, TX 01/07/13 Suspension5 Alcohol SW-846-8015C 67561 Methanol 30

J

Shintech Freeport2, TX 01/07/13 Suspension5 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.66

J

Shintech Freeport2, TX 01/07/13 Suspension5 Aldehyde SW-846-8315A 50000 Formaldehyde 0.444

J

Shintech Freeport2, TX 01/07/13 Suspension5 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Freeport2, TX 01/07/13 Suspension5 SVOC SW-846-8270D 98862 Acetophenone 1.54

Shintech Freeport2, TX 01/07/13 Suspension5 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Freeport2, TX 01/07/13 Suspension5 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

R

Shintech Freeport2, TX 01/07/13 Suspension5 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect UJ

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003

J

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.012

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.004

J

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

R

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/07/13 Suspension5 VC EPA Method 107 75014 Vinyl chloride 0.026

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/07/13 Suspension5 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.015

Shintech Freeport2, TX 01/08/13 Suspension6 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Freeport2, TX 01/08/13 Suspension6 Alcohol SW-846-8015C 67561 Methanol 30

J

Shintech Freeport2, TX 01/08/13 Suspension6 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.37

Shintech Freeport2, TX 01/08/13 Suspension6 Aldehyde SW-846-8315A 50000 Formaldehyde 0.709

Shintech Freeport2, TX 01/08/13 Suspension6 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect UJ

Shintech Freeport2, TX 01/08/13 Suspension6 SVOC SW-846-8270D 98862 Acetophenone 0.275

J

Shintech Freeport2, TX 01/08/13 Suspension6 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

Shintech Freeport2, TX 01/08/13 Suspension6 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport2, TX 01/08/13 Suspension6 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002

J

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.012

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002

J

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/08/13 Suspension6 VC EPA Method 107 75014 Vinyl chloride 0.008

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/08/13 Suspension6 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.015

Shintech Freeport2, TX 01/09/13 Suspension7 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Freeport2, TX 01/09/13 Suspension7 Alcohol SW-846-8015C 67561 Methanol 32

J

Shintech Freeport2, TX 01/09/13 Suspension7 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.75

Shintech Freeport2, TX 01/09/13 Suspension7 Aldehyde SW-846-8315A 50000 Formaldehyde 0.349

Shintech Freeport2, TX 01/09/13 Suspension7 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

R

Shintech Freeport2, TX 01/09/13 Suspension7 SVOC SW-846-8270D 98862 Acetophenone 0.075

Shintech Freeport2, TX 01/09/13 Suspension7 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Shintech Freeport2, TX 01/09/13 Suspension7 SVOC SW-846-8270D 123319 Hydroquinone 0.01 Non-detect

Shintech Freeport2, TX 01/09/13 Suspension7 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

R

Shintech Freeport2, TX 01/09/13 Suspension7 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/09/13 Suspension7 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/09/13 Suspension7 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/09/13 Suspension7 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/09/13 Suspension7 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/09/13 Suspension7 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/09/13 Suspension7 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/09/13 Suspension7 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/09/13 Suspension7 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003

J

Shintech Freeport2, TX 01/09/13 Suspension7 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/09/13 Suspension7 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.016

Shintech Freeport2, TX 01/09/13 Suspension7 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport2, TX 01/09/13 Suspension 7 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.004 J

Shintech Freeport2, TX 01/09/13 Suspension 7 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/09/13 Suspension 7 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/09/13 Suspension 7 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/09/13 Suspension 7 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/09/13 Suspension 7 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/09/13 Suspension 7 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport2, TX 01/09/13 Suspension 7 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/09/13 Suspension 7 VC EPA Method 107 75014 Vinyl chloride 0.012

Shintech Freeport2, TX 01/09/13 Suspension 7 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/09/13 Suspension 7 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/09/13 Suspension 7 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.021

Shintech Freeport2, TX 01/10/13 Suspension 8 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Freeport2, TX 01/10/13 Suspension 8 Alcohol SW-846-8015C 67561 Methanol 33 J

Shintech Freeport2, TX 01/10/13 Suspension 8 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.45

Shintech Freeport2, TX 01/10/13 Suspension 8 Aldehyde SW-846-8315A 50000 Formaldehyde 0.416

Shintech Freeport2, TX 01/10/13 Suspension 8 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect UJ

Shintech Freeport2, TX 01/10/13 Suspension 8 SVOC SW-846-8270D 98862 Acetophenone 0.052

Shintech Freeport2, TX 01/10/13 Suspension 8 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Shintech Freeport2, TX 01/10/13 Suspension 8 SVOC SW-846-8270D 123319 Hydroquinone 0.01 Non-detect

Shintech Freeport2, TX 01/10/13 Suspension 8 SVOC SW-846-8270D 108952 Phenol 0.003 J

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.011

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.004 J

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/10/13 Suspension 8 VC EPA Method 107 75014 Vinyl chloride 0.014

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/10/13 Suspension 8 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.017

Shintech Freeport2, TX 01/11/13 Suspension 9 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Freeport2, TX 01/11/13 Suspension 9 Alcohol SW-846-8015C 67561 Methanol 26 J

Shintech Freeport2, TX 01/11/13 Suspension 9 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.96

Shintech Freeport2, TX 01/11/13 Suspension 9 Aldehyde SW-846-8315A 50000 Formaldehyde 0.586

Shintech Freeport2, TX 01/11/13 Suspension 9 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.035 Non-detect UJ

Shintech Freeport2, TX 01/11/13 Suspension 9 SVOC SW-846-8270D 98862 Acetophenone 0.943

Shintech Freeport2, TX 01/11/13 Suspension 9 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.025 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 SVOC SW-846-8270D 123319 Hydroquinone 0.05 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 SVOC SW-846-8270D 108952 Phenol 0.005 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.004 J

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.008

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.004 J

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 VC EPA Method 107 75014 Vinyl chloride 0.044

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/11/13 Suspension 9 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.015

Shintech Freeport2, TX 01/12/13 Suspension 10 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport2, TX 01/12/13 Suspension 10 Alcohol SW-846-8015C 67561 Methanol 31 J

Shintech Freeport2, TX 01/12/13 Suspension 10 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.99

Shintech Freeport2, TX 01/12/13 Suspension 10 Aldehyde SW-846-8315A 50000 Formaldehyde 0.521

Shintech Freeport2, TX 01/12/13 Suspension 10 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect UJ

Shintech Freeport2, TX 01/12/13 Suspension 10 SVOC SW-846-8270D 98862 Acetophenone 1.15

Shintech Freeport2, TX 01/12/13 Suspension 10 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Freeport2, TX 01/12/13 Suspension 10 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Freeport2, TX 01/12/13 Suspension 10 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.004 J

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.011

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.006

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

12/12/2013 VI Confidential 32 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/12/13 Suspension 10 VC EPA Method 107 75014 Vinyl chloride 0.031

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/12/13 Suspension 10 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.017

Shintech Freeport2, TX 01/13/13 Suspension 11 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 Alcohol SW-846-8015C 67561 Methanol 33 J

Shintech Freeport2, TX 01/13/13 Suspension 11 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.63

Shintech Freeport2, TX 01/13/13 Suspension 11 Aldehyde SW-846-8315A 50000 Formaldehyde 0.385

Shintech Freeport2, TX 01/13/13 Suspension 11 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 SVOC SW-846-8270D 98862 Acetophenone 0.923

Shintech Freeport2, TX 01/13/13 Suspension 11 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.01

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.011

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.007

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 VC EPA Method 107 75014 Vinyl chloride 0.072 J

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/13/13 Suspension 11 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.015

Shintech Freeport2, TX 01/14/13 Suspension 12 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 Alcohol SW-846-8015C 67561 Methanol 33 J

Shintech Freeport2, TX 01/14/13 Suspension 12 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.71

Shintech Freeport2, TX 01/14/13 Suspension 12 Aldehyde SW-846-8315A 50000 Formaldehyde 0.475

Shintech Freeport2, TX 01/14/13 Suspension 12 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 SVOC SW-846-8270D 98862 Acetophenone 1.08

Shintech Freeport2, TX 01/14/13 Suspension 12 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.014

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.015

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.008

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 VC EPA Method 107 75014 Vinyl chloride 0.108 J

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/14/13 Suspension 12 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.018

Shintech Freeport2, TX 01/15/13 Suspension 13 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 Alcohol SW-846-8015C 67561 Methanol 30 J

Shintech Freeport2, TX 01/15/13 Suspension 13 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.75

Shintech Freeport2, TX 01/15/13 Suspension 13 Aldehyde SW-846-8315A 50000 Formaldehyde 0.511

Shintech Freeport2, TX 01/15/13 Suspension 13 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 SVOC SW-846-8270D 98862 Acetophenone 0.743

Shintech Freeport2, TX 01/15/13 Suspension 13 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.008

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.004 J

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport2, TX 01/15/13 Suspension 13 VC EPA Method 107 75014 Vinyl chloride 0.021

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/15/13 Suspension 13 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.016

Shintech Freeport2, TX 01/16/13 Suspension 14 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 Alcohol SW-846-8015C 67561 Methanol 28 J

Shintech Freeport2, TX 01/16/13 Suspension 14 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.22

Shintech Freeport2, TX 01/16/13 Suspension 14 Aldehyde SW-846-8315A 50000 Formaldehyde 0.468

Shintech Freeport2, TX 01/16/13 Suspension 14 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 SVOC SW-846-8270D 98862 Acetophenone 1.34

Shintech Freeport2, TX 01/16/13 Suspension 14 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.004 J

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.007

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.003 J

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 VC EPA Method 107 75014 Vinyl chloride 0.022

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/16/13 Suspension 14 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.013

Shintech Freeport2, TX 01/17/13 Suspension 15 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 Alcohol SW-846-8015C 67561 Methanol 45 J

Shintech Freeport2, TX 01/17/13 Suspension 15 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.67

Shintech Freeport2, TX 01/17/13 Suspension 15 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 SVOC SW-846-8270D 98862 Acetophenone 1.28

Shintech Freeport2, TX 01/17/13 Suspension 15 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.018

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.007

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 VC EPA Method 107 75014 Vinyl chloride 0.012

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/17/13 Suspension 15 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.031

Shintech Freeport2, TX 01/18/13 Suspension 16 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 Alcohol SW-846-8015C 67561 Methanol 25 J

Shintech Freeport2, TX 01/18/13 Suspension 16 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.5

Shintech Freeport2, TX 01/18/13 Suspension 16 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 SVOC SW-846-8270D 98862 Acetophenone 1.22

Shintech Freeport2, TX 01/18/13 Suspension 16 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.006

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.022

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.011

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 VC EPA Method 107 75014 Vinyl chloride 0.025

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/18/13 Suspension 16 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.03

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport2, TX 01/19/13 Suspension 17 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 Alcohol SW-846-8015C 67561 Methanol 24 J

Shintech Freeport2, TX 01/19/13 Suspension 17 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.31

Shintech Freeport2, TX 01/19/13 Suspension 17 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 SVOC SW-846-8270D 98862 Acetophenone 0.773

Shintech Freeport2, TX 01/19/13 Suspension 17 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.007

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.019

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.009

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 VC EPA Method 107 75014 Vinyl chloride 0.055

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/19/13 Suspension 17 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.027

Shintech Freeport2, TX 01/20/13 Suspension 18 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 Alcohol SW-846-8015C 67561 Methanol 27 J

Shintech Freeport2, TX 01/20/13 Suspension 18 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.42

Shintech Freeport2, TX 01/20/13 Suspension 18 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 SVOC SW-846-8270D 98862 Acetophenone 1.27

Shintech Freeport2, TX 01/20/13 Suspension 18 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.004 J

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.021

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.009

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 VC EPA Method 107 75014 Vinyl chloride 0.015

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/20/13 Suspension 18 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.026

Shintech Freeport2, TX 01/21/13 Suspension 19 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 Alcohol SW-846-8015C 67561 Methanol 23 J

Shintech Freeport2, TX 01/21/13 Suspension 19 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.63

Shintech Freeport2, TX 01/21/13 Suspension 19 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 SVOC SW-846-8270D 98862 Acetophenone 0.215 J

Shintech Freeport2, TX 01/21/13 Suspension 19 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.018

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.008

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 VC EPA Method 107 75014 Vinyl chloride 0.011

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/21/13 Suspension 19 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.02

Shintech Freeport2, TX 01/22/13 Suspension 20 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 Alcohol SW-846-8015C 67561 Methanol 24 J

Shintech Freeport2, TX 01/22/13 Suspension 20 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.03

Shintech Freeport2, TX 01/22/13 Suspension 20 Aldehyde SW-846-8315A 50000 Formaldehyde 0.749

12/12/2013 VI Confidential 35 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport2, TX 01/22/13 Suspension 20 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect UJ

Shintech Freeport2, TX 01/22/13 Suspension 20 SVOC SW-846-8270D 98862 Acetophenone 0.064 J

Shintech Freeport2, TX 01/22/13 Suspension 20 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 SVOC SW-846-8270D 123319 Hydroquinone 0.01 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect UJ

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.004 J

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 J

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 VC EPA Method 107 75014 Vinyl chloride 0.012

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/22/13 Suspension 20 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.007 J

Shintech Freeport2, TX 01/23/13 Suspension 21 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport2, TX 01/23/13 Suspension 21 Alcohol SW-846-8015C 67561 Methanol 23 J

Shintech Freeport2, TX 01/23/13 Suspension 21 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.19

Shintech Freeport2, TX 01/23/13 Suspension 21 Aldehyde SW-846-8315A 50000 Formaldehyde 0.322

Shintech Freeport2, TX 01/23/13 Suspension 21 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect R

Shintech Freeport2, TX 01/23/13 Suspension 21 SVOC SW-846-8270D 98862 Acetophenone 0.052

Shintech Freeport2, TX 01/23/13 Suspension 21 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Shintech Freeport2, TX 01/23/13 Suspension 21 SVOC SW-846-8270D 123319 Hydroquinone 0.01 Non-detect

Shintech Freeport2, TX 01/23/13 Suspension 21 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect R

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.006

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 J

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/23/13 Suspension 21 VC EPA Method 107 75014 Vinyl chloride 0.01

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/23/13 Suspension 21 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.009 J

Shintech Freeport2, TX 01/24/13 Suspension 22 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 Alcohol SW-846-8015C 67561 Methanol 24 J, VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.65 VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 Aldehyde SW-846-8315A 50000 Formaldehyde 0.347 VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect UJ, VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 SVOC SW-846-8270D 98862 Acetophenone 0.016 VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 SVOC SW-846-8270D 123319 Hydroquinone 0.01 Non-detect VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect UJ, VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J, VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.006 VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.003 J, VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ, VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VC EPA Method 107 75014 Vinyl chloride 0.007 VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect VI Note (10)

Shintech Freeport2, TX 01/24/13 Suspension 22 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.009 J, VI Note (10)

Shintech Freeport2, TX 01/25/13 Suspension 23 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 Alcohol SW-846-8015C 67561 Methanol 23 J

Shintech Freeport2, TX 01/25/13 Suspension 23 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.02 J

Shintech Freeport2, TX 01/25/13 Suspension 23 Aldehyde SW-846-8315A 50000 Formaldehyde 0.075 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect R

Shintech Freeport2, TX 01/25/13 Suspension 23 SVOC SW-846-8270D 98862 Acetophenone 0.027 J

Shintech Freeport2, TX 01/25/13 Suspension 23 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 SVOC SW-846-8270D 123319 Hydroquinone 0.01 Non-detect

12/12/2013 VI Confidential 36 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport2, TX 01/25/13 Suspension 23 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect R

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.022

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.005 J

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 VC EPA Method 107 75014 Vinyl chloride 0.01

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/25/13 Suspension 23 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.027

Shintech Freeport2, TX 01/26/13 Suspension 24 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 Alcohol SW-846-8015C 67561 Methanol 22 J

Shintech Freeport2, TX 01/26/13 Suspension 24 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.84

Shintech Freeport2, TX 01/26/13 Suspension 24 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect R

Shintech Freeport2, TX 01/26/13 Suspension 24 SVOC SW-846-8270D 98862 Acetophenone 0.018 J

Shintech Freeport2, TX 01/26/13 Suspension 24 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 SVOC SW-846-8270D 123319 Hydroquinone 0.01 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect R

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.02

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.006

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 VC EPA Method 107 75014 Vinyl chloride 0.01

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/26/13 Suspension 24 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.024

Shintech Freeport2, TX 01/27/13 Suspension 25 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 Alcohol SW-846-8015C 67561 Methanol 22 J

Shintech Freeport2, TX 01/27/13 Suspension 25 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.59

Shintech Freeport2, TX 01/27/13 Suspension 25 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect R

Shintech Freeport2, TX 01/27/13 Suspension 25 SVOC SW-846-8270D 98862 Acetophenone 0.015

Shintech Freeport2, TX 01/27/13 Suspension 25 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.025

Shintech Freeport2, TX 01/27/13 Suspension 25 SVOC SW-846-8270D 123319 Hydroquinone 0.01 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect R

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 J

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.018

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.004 J

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 VC EPA Method 107 75014 Vinyl chloride 0.008

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/27/13 Suspension 25 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.022

Shintech Freeport2, TX 01/28/13 Suspension 26 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport2, TX 01/28/13 Suspension 26 Alcohol SW-846-8015C 67561 Methanol 21 J

Shintech Freeport2, TX 01/28/13 Suspension 26 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.9

Shintech Freeport2, TX 01/28/13 Suspension 26 Aldehyde SW-846-8315A 50000 Formaldehyde 0.122 J

Shintech Freeport2, TX 01/28/13 Suspension 26 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Shintech Freeport2, TX 01/28/13 Suspension 26 SVOC SW-846-8270D 98862 Acetophenone 0.029

Shintech Freeport2, TX 01/28/13 Suspension 26 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Shintech Freeport2, TX 01/28/13 Suspension 26 SVOC SW-846-8270D 123319 Hydroquinone 0.01 Non-detect R

Shintech Freeport2, TX 01/28/13 Suspension 26 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

12/12/2013 VI Confidential 37 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.022

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.006

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect R

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/28/13 Suspension 26 VC EPA Method 107 75014 Vinyl chloride 0.006

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/28/13 Suspension 26 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.025

Shintech Freeport2, TX 01/29/13 Suspension 27 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 Alcohol SW-846-8015C 67561 Methanol 23 J

Shintech Freeport2, TX 01/29/13 Suspension 27 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.85

Shintech Freeport2, TX 01/29/13 Suspension 27 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect R

Shintech Freeport2, TX 01/29/13 Suspension 27 SVOC SW-846-8270D 98862 Acetophenone 0.014 J

Shintech Freeport2, TX 01/29/13 Suspension 27 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 SVOC SW-846-8270D 123319 Hydroquinone 0.01 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect R

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.023

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.007

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 VC EPA Method 107 75014 Vinyl chloride 0.013

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/29/13 Suspension 27 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.022

Shintech Freeport2, TX 01/30/13 Suspension 28 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 Alcohol SW-846-8015C 67561 Methanol 27 J

Shintech Freeport2, TX 01/30/13 Suspension 28 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.48

Shintech Freeport2, TX 01/30/13 Suspension 28 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect R

Shintech Freeport2, TX 01/30/13 Suspension 28 SVOC SW-846-8270D 98862 Acetophenone 0.025 J

Shintech Freeport2, TX 01/30/13 Suspension 28 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 SVOC SW-846-8270D 123319 Hydroquinone 0.01 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect R

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.026

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.009

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 VC EPA Method 107 75014 Vinyl chloride 0.013

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/30/13 Suspension 28 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.025

Shintech Freeport2, TX 01/31/13 Suspension 29 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport2, TX 01/31/13 Suspension 29 Alcohol SW-846-8015C 67561 Methanol 18 J

Shintech Freeport2, TX 01/31/13 Suspension 29 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.31

Shintech Freeport2, TX 01/31/13 Suspension 29 Aldehyde SW-846-8315A 50000 Formaldehyde 0.093 J

Shintech Freeport2, TX 01/31/13 Suspension 29 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect R

Shintech Freeport2, TX 01/31/13 Suspension 29 SVOC SW-846-8270D 98862 Acetophenone 0.01 Non-detect U

Shintech Freeport2, TX 01/31/13 Suspension 29 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Shintech Freeport2, TX 01/31/13 Suspension 29 SVOC SW-846-8270D 123319 Hydroquinone 0.01 Non-detect

Shintech Freeport2, TX 01/31/13 Suspension 29 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect R

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.029

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.034

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 J

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.011

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 01/31/13 Suspension 29 VC EPA Method 107 75014 Vinyl chloride 0.226 J

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 01/31/13 Suspension 29 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.018

Shintech Freeport2, TX 02/01/13 Suspension 30 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 Alcohol SW-846-8015C 67561 Methanol 18 J

Shintech Freeport2, TX 02/01/13 Suspension 30 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.39

Shintech Freeport2, TX 02/01/13 Suspension 30 Aldehyde SW-846-8315A 50000 Formaldehyde 0.286

Shintech Freeport2, TX 02/01/13 Suspension 30 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.07 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 SVOC SW-846-8270D 98862 Acetophenone 0.973

Shintech Freeport2, TX 02/01/13 Suspension 30 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.05 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 SVOC SW-846-8270D 108952 Phenol 0.01 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.018

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.004 J

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 VC EPA Method 107 75014 Vinyl chloride 0.044

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport2, TX 02/01/13 Suspension 30 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.018

Shintech Freeport3, TX 01/03/13 Suspension 1 Alcohol SW-846-8015C 107211 Ethylene glycol 4 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 Alcohol SW-846-8015C 67561 Methanol 41 J

Shintech Freeport3, TX 01/03/13 Suspension 1 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.95 J

Shintech Freeport3, TX 01/03/13 Suspension 1 Aldehyde SW-846-8315A 50000 Formaldehyde 0.9 J

Shintech Freeport3, TX 01/03/13 Suspension 1 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.035 Non-detect UJ

Shintech Freeport3, TX 01/03/13 Suspension 1 SVOC SW-846-8270D 98862 Acetophenone 0.867

Shintech Freeport3, TX 01/03/13 Suspension 1 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.025 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 SVOC SW-846-8270D 123319 Hydroquinone 0.05 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 SVOC SW-846-8270D 108952 Phenol 0.005 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.007

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VC EPA Method 107 75014 Vinyl chloride 0.038 J

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/03/13 Suspension 1 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.022

Shintech Freeport3, TX 01/04/13 Suspension 2 Alcohol SW-846-8015C 107211 Ethylene glycol 4 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 Alcohol SW-846-8015C 67561 Methanol 38 J

Shintech Freeport3, TX 01/04/13 Suspension 2 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.16

Shintech Freeport3, TX 01/04/13 Suspension 2 Aldehyde SW-846-8315A 50000 Formaldehyde 1.27

Shintech Freeport3, TX 01/04/13 Suspension 2 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect UJ

Shintech Freeport3, TX 01/04/13 Suspension 2 SVOC SW-846-8270D 98862 Acetophenone 0.27

Shintech Freeport3, TX 01/04/13 Suspension 2 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

12/12/2013 VI Confidential 39 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 J

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 VC EPA Method 107 75014 Vinyl chloride 0.019

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/04/13 Suspension 2 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.047

Shintech Freeport3, TX 01/05/13 Suspension 3 Alcohol SW-846-8015C 107211 Ethylene glycol 4 Non-detect UJ

Shintech Freeport3, TX 01/05/13 Suspension 3 Alcohol SW-846-8015C 67561 Methanol 38 J

Shintech Freeport3, TX 01/05/13 Suspension 3 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.19

Shintech Freeport3, TX 01/05/13 Suspension 3 Aldehyde SW-846-8315A 50000 Formaldehyde 0.702

Shintech Freeport3, TX 01/05/13 Suspension 3 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect UJ

Shintech Freeport3, TX 01/05/13 Suspension 3 SVOC SW-846-8270D 98862 Acetophenone 0.28

Shintech Freeport3, TX 01/05/13 Suspension 3 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 J

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 VC EPA Method 107 75014 Vinyl chloride 0.012

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/05/13 Suspension 3 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.048

Shintech Freeport3, TX 01/06/13 Suspension 4 Alcohol SW-846-8015C 107211 Ethylene glycol 4 Non-detect UJ

Shintech Freeport3, TX 01/06/13 Suspension 4 Alcohol SW-846-8015C 67561 Methanol 41 J

Shintech Freeport3, TX 01/06/13 Suspension 4 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.971

Shintech Freeport3, TX 01/06/13 Suspension 4 Aldehyde SW-846-8315A 50000 Formaldehyde 1.06

Shintech Freeport3, TX 01/06/13 Suspension 4 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 SVOC SW-846-8270D 98862 Acetophenone 0.235

Shintech Freeport3, TX 01/06/13 Suspension 4 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 VC EPA Method 107 75014 Vinyl chloride 0.008

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/06/13 Suspension 4 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.041

Shintech Freeport3, TX 01/07/13 Suspension 5 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Freeport3, TX 01/07/13 Suspension 5 Alcohol SW-846-8015C 67561 Methanol 42 J

Shintech Freeport3, TX 01/07/13 Suspension 5 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.906

Shintech Freeport3, TX 01/07/13 Suspension 5 Aldehyde SW-846-8315A 50000 Formaldehyde 1.02

Shintech Freeport3, TX 01/07/13 Suspension 5 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect UJ

Shintech Freeport3, TX 01/07/13 Suspension 5 SVOC SW-846-8270D 98862 Acetophenone 0.15

Shintech Freeport3, TX 01/07/13 Suspension 5 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

Shintech Freeport3, TX 01/07/13 Suspension 5 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport3, TX 01/07/13 Suspension 5 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 J

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/07/13 Suspension 5 VC EPA Method 107 75014 Vinyl chloride 0.008

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/07/13 Suspension 5 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.037

Shintech Freeport3, TX 01/08/13 Suspension 6 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Freeport3, TX 01/08/13 Suspension 6 Alcohol SW-846-8015C 67561 Methanol 40 J

Shintech Freeport3, TX 01/08/13 Suspension 6 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.1

Shintech Freeport3, TX 01/08/13 Suspension 6 Aldehyde SW-846-8315A 50000 Formaldehyde 1.04 J

Shintech Freeport3, TX 01/08/13 Suspension 6 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect UJ

Shintech Freeport3, TX 01/08/13 Suspension 6 SVOC SW-846-8270D 98862 Acetophenone 0.122

Shintech Freeport3, TX 01/08/13 Suspension 6 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 VC EPA Method 107 75014 Vinyl chloride 0.009

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/08/13 Suspension 6 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.038

Shintech Freeport3, TX 01/09/13 Suspension 7 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Freeport3, TX 01/09/13 Suspension 7 Alcohol SW-846-8015C 67561 Methanol 51 J

Shintech Freeport3, TX 01/09/13 Suspension 7 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.89

Shintech Freeport3, TX 01/09/13 Suspension 7 Aldehyde SW-846-8315A 50000 Formaldehyde 0.698

Shintech Freeport3, TX 01/09/13 Suspension 7 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect UJ

Shintech Freeport3, TX 01/09/13 Suspension 7 SVOC SW-846-8270D 98862 Acetophenone 0.317

Shintech Freeport3, TX 01/09/13 Suspension 7 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 VC EPA Method 107 75014 Vinyl chloride 0.01

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/09/13 Suspension 7 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.042

Shintech Freeport3, TX 01/10/13 Suspension 8 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 Alcohol SW-846-8015C 67561 Methanol 59 J

Shintech Freeport3, TX 01/10/13 Suspension 8 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.25

Shintech Freeport3, TX 01/10/13 Suspension 8 Aldehyde SW-846-8315A 50000 Formaldehyde 0.812

Shintech Freeport3, TX 01/10/13 Suspension 8 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.035 Non-detect UJ

Shintech Freeport3, TX 01/10/13 Suspension 8 SVOC SW-846-8270D 98862 Acetophenone 0.408 J

Shintech Freeport3, TX 01/10/13 Suspension 8 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.025 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 SVOC SW-846-8270D 123319 Hydroquinone 0.05 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 SVOC SW-846-8270D 108952 Phenol 0.005 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.003 J

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

12/12/2013 VI Confidential 41 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 VC EPA Method 107 75014 Vinyl chloride 0.013

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/10/13 Suspension 8 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.03

Shintech Freeport3, TX 01/11/13 Suspension 9 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Freeport3, TX 01/11/13 Suspension 9 Alcohol SW-846-8015C 67561 Methanol 48 J

Shintech Freeport3, TX 01/11/13 Suspension 9 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.1

Shintech Freeport3, TX 01/11/13 Suspension 9 Aldehyde SW-846-8315A 50000 Formaldehyde 0.73

Shintech Freeport3, TX 01/11/13 Suspension 9 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect UJ

Shintech Freeport3, TX 01/11/13 Suspension 9 SVOC SW-846-8270D 98862 Acetophenone 0.392

Shintech Freeport3, TX 01/11/13 Suspension 9 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.006

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VC EPA Method 107 75014 Vinyl chloride 0.044

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/11/13 Suspension 9 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.027

Shintech Freeport3, TX 01/12/13 Suspension 10 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 Alcohol SW-846-8015C 67561 Methanol 63 J

Shintech Freeport3, TX 01/12/13 Suspension 10 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.25

Shintech Freeport3, TX 01/12/13 Suspension 10 Aldehyde SW-846-8315A 50000 Formaldehyde 0.894

Shintech Freeport3, TX 01/12/13 Suspension 10 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.035 Non-detect UJ

Shintech Freeport3, TX 01/12/13 Suspension 10 SVOC SW-846-8270D 98862 Acetophenone 0.471

Shintech Freeport3, TX 01/12/13 Suspension 10 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.025 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 SVOC SW-846-8270D 123319 Hydroquinone 0.05 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 SVOC SW-846-8270D 108952 Phenol 0.005 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.01

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.039

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.003 J

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 VC EPA Method 107 75014 Vinyl chloride 0.046

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/12/13 Suspension 10 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.044

Shintech Freeport3, TX 01/13/13 Suspension 11 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 Alcohol SW-846-8015C 67561 Methanol 63 J

Shintech Freeport3, TX 01/13/13 Suspension 11 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.36

Shintech Freeport3, TX 01/13/13 Suspension 11 Aldehyde SW-846-8315A 50000 Formaldehyde 0.77

Shintech Freeport3, TX 01/13/13 Suspension 11 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.035 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 SVOC SW-846-8270D 98862 Acetophenone 0.451

Shintech Freeport3, TX 01/13/13 Suspension 11 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.025 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 SVOC SW-846-8270D 123319 Hydroquinone 0.05 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 SVOC SW-846-8270D 108952 Phenol 0.005 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.029

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.003 J

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 VC EPA Method 107 75014 Vinyl chloride 0.014

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport3, TX 01/13/13 Suspension 11 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.033

Shintech Freeport3, TX 01/14/13 Suspension 12 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport3, TX 01/14/13 Suspension 12 Alcohol SW-846-8015C 67561 Methanol 59 J

Shintech Freeport3, TX 01/14/13 Suspension 12 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.894

Shintech Freeport3, TX 01/14/13 Suspension 12 Aldehyde SW-846-8315A 50000 Formaldehyde 0.7

Shintech Freeport3, TX 01/14/13 Suspension 12 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.035 Non-detect R

Shintech Freeport3, TX 01/14/13 Suspension 12 SVOC SW-846-8270D 98862 Acetophenone 0.405 J

Shintech Freeport3, TX 01/14/13 Suspension 12 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.025 Non-detect

Shintech Freeport3, TX 01/14/13 Suspension 12 SVOC SW-846-8270D 123319 Hydroquinone 0.05 Non-detect R

Shintech Freeport3, TX 01/14/13 Suspension 12 SVOC SW-846-8270D 108952 Phenol 0.005 Non-detect

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect R

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.028 J

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 J

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect UJ

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/14/13 Suspension 12 VC EPA Method 107 75014 Vinyl chloride 0.017 J

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/14/13 Suspension 12 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.018

Shintech Freeport3, TX 01/15/13 Suspension 13 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 Alcohol SW-846-8015C 67561 Methanol 37 J

Shintech Freeport3, TX 01/15/13 Suspension 13 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.16

Shintech Freeport3, TX 01/15/13 Suspension 13 Aldehyde SW-846-8315A 50000 Formaldehyde 0.809

Shintech Freeport3, TX 01/15/13 Suspension 13 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.035 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 SVOC SW-846-8270D 98862 Acetophenone 0.667 J

Shintech Freeport3, TX 01/15/13 Suspension 13 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.025 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 SVOC SW-846-8270D 123319 Hydroquinone 0.05 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 SVOC SW-846-8270D 108952 Phenol 0.005 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VC EPA Method 107 75014 Vinyl chloride 0.017

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/15/13 Suspension 13 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.042

Shintech Freeport3, TX 01/16/13 Suspension 14 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 Alcohol SW-846-8015C 67561 Methanol 47 J

Shintech Freeport3, TX 01/16/13 Suspension 14 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.25

Shintech Freeport3, TX 01/16/13 Suspension 14 Aldehyde SW-846-8315A 50000 Formaldehyde 0.768

Shintech Freeport3, TX 01/16/13 Suspension 14 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.035 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 SVOC SW-846-8270D 98862 Acetophenone 0.479

Shintech Freeport3, TX 01/16/13 Suspension 14 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.025 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 SVOC SW-846-8270D 123319 Hydroquinone 0.05 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 SVOC SW-846-8270D 108952 Phenol 0.005 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.037

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 J

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 VC EPA Method 107 75014 Vinyl chloride 0.007

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/16/13 Suspension 14 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.04

Shintech Freeport3, TX 01/17/13 Suspension 15 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport3, TX 01/17/13 Suspension 15 Alcohol SW-846-8015C 67561 Methanol 32 J

Shintech Freeport3, TX 01/17/13 Suspension 15 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.02

12/12/2013 VI Confidential 43 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport3, TX 01/17/13 Suspension 15 Aldehyde SW-846-8315A 50000 Formaldehyde 0.645

Shintech Freeport3, TX 01/17/13 Suspension 15 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect UJ

Shintech Freeport3, TX 01/17/13 Suspension 15 SVOC SW-846-8270D 98862 Acetophenone 0.326

Shintech Freeport3, TX 01/17/13 Suspension 15 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

Shintech Freeport3, TX 01/17/13 Suspension 15 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport3, TX 01/17/13 Suspension 15 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect UJ

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.027

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.003 J

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/17/13 Suspension 15 VC EPA Method 107 75014 Vinyl chloride 0.019

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/17/13 Suspension 15 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.036

Shintech Freeport3, TX 01/18/13 Suspension 16 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport3, TX 01/18/13 Suspension 16 Alcohol SW-846-8015C 67561 Methanol 37 J

Shintech Freeport3, TX 01/18/13 Suspension 16 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.11

Shintech Freeport3, TX 01/18/13 Suspension 16 Aldehyde SW-846-8315A 50000 Formaldehyde 0.582

Shintech Freeport3, TX 01/18/13 Suspension 16 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect UJ

Shintech Freeport3, TX 01/18/13 Suspension 16 SVOC SW-846-8270D 98862 Acetophenone 0.31

Shintech Freeport3, TX 01/18/13 Suspension 16 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

Shintech Freeport3, TX 01/18/13 Suspension 16 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport3, TX 01/18/13 Suspension 16 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect UJ

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.038

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 J

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/18/13 Suspension 16 VC EPA Method 107 75014 Vinyl chloride 0.023

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/18/13 Suspension 16 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.046

Shintech Freeport3, TX 01/19/13 Suspension 17 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 Alcohol SW-846-8015C 67561 Methanol 39 J

Shintech Freeport3, TX 01/19/13 Suspension 17 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.42

Shintech Freeport3, TX 01/19/13 Suspension 17 Aldehyde SW-846-8315A 50000 Formaldehyde 0.775

Shintech Freeport3, TX 01/19/13 Suspension 17 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect UJ

Shintech Freeport3, TX 01/19/13 Suspension 17 SVOC SW-846-8270D 98862 Acetophenone 0.37

Shintech Freeport3, TX 01/19/13 Suspension 17 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect UJ

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.034

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.003 J

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 VC EPA Method 107 75014 Vinyl chloride 0.028

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/19/13 Suspension 17 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.041

Shintech Freeport3, TX 01/20/13 Suspension 18 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 Alcohol SW-846-8015C 67561 Methanol 39 J

Shintech Freeport3, TX 01/20/13 Suspension 18 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.22

Shintech Freeport3, TX 01/20/13 Suspension 18 Aldehyde SW-846-8315A 50000 Formaldehyde 0.584

Shintech Freeport3, TX 01/20/13 Suspension 18 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 SVOC SW-846-8270D 98862 Acetophenone 0.271

Shintech Freeport3, TX 01/20/13 Suspension 18 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport3, TX 01/20/13 Suspension 18 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.004 J

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.035

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.003 J

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 VC EPA Method 107 75014 Vinyl chloride 0.024

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/20/13 Suspension 18 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.046

Shintech Freeport3, TX 01/21/13 Suspension 19 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 Alcohol SW-846-8015C 67561 Methanol 40 J

Shintech Freeport3, TX 01/21/13 Suspension 19 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.23

Shintech Freeport3, TX 01/21/13 Suspension 19 Aldehyde SW-846-8315A 50000 Formaldehyde 0.509

Shintech Freeport3, TX 01/21/13 Suspension 19 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 SVOC SW-846-8270D 98862 Acetophenone 0.28

Shintech Freeport3, TX 01/21/13 Suspension 19 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.004 J

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.041

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.004 J

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 VC EPA Method 107 75014 Vinyl chloride 0.028

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/21/13 Suspension 19 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.048

Shintech Freeport3, TX 01/22/13 Suspension 20 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 Alcohol SW-846-8015C 67561 Methanol 33 J

Shintech Freeport3, TX 01/22/13 Suspension 20 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.47

Shintech Freeport3, TX 01/22/13 Suspension 20 Aldehyde SW-846-8315A 50000 Formaldehyde 0.838

Shintech Freeport3, TX 01/22/13 Suspension 20 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect R

Shintech Freeport3, TX 01/22/13 Suspension 20 SVOC SW-846-8270D 98862 Acetophenone 0.274

Shintech Freeport3, TX 01/22/13 Suspension 20 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect R

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.037

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.003 J

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 VC EPA Method 107 75014 Vinyl chloride 0.014

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/22/13 Suspension 20 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.042

Shintech Freeport3, TX 01/23/13 Suspension 21 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport3, TX 01/23/13 Suspension 21 Alcohol SW-846-8015C 67561 Methanol 38 J

Shintech Freeport3, TX 01/23/13 Suspension 21 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.37

Shintech Freeport3, TX 01/23/13 Suspension 21 Aldehyde SW-846-8315A 50000 Formaldehyde 1.07

Shintech Freeport3, TX 01/23/13 Suspension 21 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect R

Shintech Freeport3, TX 01/23/13 Suspension 21 SVOC SW-846-8270D 98862 Acetophenone 0.32

Shintech Freeport3, TX 01/23/13 Suspension 21 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

Shintech Freeport3, TX 01/23/13 Suspension 21 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport3, TX 01/23/13 Suspension 21 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect R

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

12/12/2013 VI Confidential 45 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.006

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.024

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.003 J

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/23/13 Suspension 21 VC EPA Method 107 75014 Vinyl chloride 0.021

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/23/13 Suspension 21 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.042

Shintech Freeport3, TX 01/24/13 Suspension 22 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport3, TX 01/24/13 Suspension 22 Alcohol SW-846-8015C 67561 Methanol 41 J

Shintech Freeport3, TX 01/24/13 Suspension 22 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.62

Shintech Freeport3, TX 01/24/13 Suspension 22 Aldehyde SW-846-8315A 50000 Formaldehyde 0.887

Shintech Freeport3, TX 01/24/13 Suspension 22 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect R

Shintech Freeport3, TX 01/24/13 Suspension 22 SVOC SW-846-8270D 98862 Acetophenone 0.335

Shintech Freeport3, TX 01/24/13 Suspension 22 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

Shintech Freeport3, TX 01/24/13 Suspension 22 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport3, TX 01/24/13 Suspension 22 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect R

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.006

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.022

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.004 J

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/24/13 Suspension 22 VC EPA Method 107 75014 Vinyl chloride 0.018

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/24/13 Suspension 22 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.045

Shintech Freeport3, TX 01/25/13 Suspension 23 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 Alcohol SW-846-8015C 67561 Methanol 41 J

Shintech Freeport3, TX 01/25/13 Suspension 23 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.61

Shintech Freeport3, TX 01/25/13 Suspension 23 Aldehyde SW-846-8315A 50000 Formaldehyde 1.03

Shintech Freeport3, TX 01/25/13 Suspension 23 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect R

Shintech Freeport3, TX 01/25/13 Suspension 23 SVOC SW-846-8270D 98862 Acetophenone 0.399 J

Shintech Freeport3, TX 01/25/13 Suspension 23 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect R

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.005 J

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.033

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 J

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 VC EPA Method 107 75014 Vinyl chloride 0.025

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/25/13 Suspension 23 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.044

Shintech Freeport3, TX 01/26/13 Suspension 24 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport3, TX 01/26/13 Suspension 24 Alcohol SW-846-8015C 67561 Methanol 48 J

Shintech Freeport3, TX 01/26/13 Suspension 24 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.1

Shintech Freeport3, TX 01/26/13 Suspension 24 Aldehyde SW-846-8315A 50000 Formaldehyde 0.779

Shintech Freeport3, TX 01/26/13 Suspension 24 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect R

Shintech Freeport3, TX 01/26/13 Suspension 24 SVOC SW-846-8270D 98862 Acetophenone 0.368

Shintech Freeport3, TX 01/26/13 Suspension 24 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

Shintech Freeport3, TX 01/26/13 Suspension 24 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport3, TX 01/26/13 Suspension 24 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect R

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

12/12/2013 VI Confidential 46 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.005 J

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.025

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.003 J

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/26/13 Suspension 24 VC EPA Method 107 75014 Vinyl chloride 0.021

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/26/13 Suspension 24 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.021

Shintech Freeport3, TX 01/27/13 Suspension 25 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport3, TX 01/27/13 Suspension 25 Alcohol SW-846-8015C 67561 Methanol 49 J

Shintech Freeport3, TX 01/27/13 Suspension 25 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.66

Shintech Freeport3, TX 01/27/13 Suspension 25 Aldehyde SW-846-8315A 50000 Formaldehyde 0.767

Shintech Freeport3, TX 01/27/13 Suspension 25 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect R

Shintech Freeport3, TX 01/27/13 Suspension 25 SVOC SW-846-8270D 98862 Acetophenone 0.392 J

Shintech Freeport3, TX 01/27/13 Suspension 25 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.034 J

Shintech Freeport3, TX 01/27/13 Suspension 25 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect

Shintech Freeport3, TX 01/27/13 Suspension 25 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect R

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.005 J

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.033

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.004 J

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/27/13 Suspension 25 VC EPA Method 107 75014 Vinyl chloride 0.026

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/27/13 Suspension 25 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.04

Shintech Freeport3, TX 01/28/13 Suspension 26 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Freeport3, TX 01/28/13 Suspension 26 Alcohol SW-846-8015C 67561 Methanol 45 J

Shintech Freeport3, TX 01/28/13 Suspension 26 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.4

Shintech Freeport3, TX 01/28/13 Suspension 26 Aldehyde SW-846-8315A 50000 Formaldehyde 0.677

Shintech Freeport3, TX 01/28/13 Suspension 26 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.035 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 SVOC SW-846-8270D 98862 Acetophenone 0.58

Shintech Freeport3, TX 01/28/13 Suspension 26 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.025 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 SVOC SW-846-8270D 123319 Hydroquinone 0.05 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 SVOC SW-846-8270D 108952 Phenol 0.005 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.004 J

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.026

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 J

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 VC EPA Method 107 75014 Vinyl chloride 0.018

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/28/13 Suspension 26 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.034

Shintech Freeport3, TX 01/29/13 Suspension 27 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Freeport3, TX 01/29/13 Suspension 27 Alcohol SW-846-8015C 67561 Methanol 48 J

Shintech Freeport3, TX 01/29/13 Suspension 27 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.3

Shintech Freeport3, TX 01/29/13 Suspension 27 Aldehyde SW-846-8315A 50000 Formaldehyde 0.569

Shintech Freeport3, TX 01/29/13 Suspension 27 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.035 Non-detect

Shintech Freeport3, TX 01/29/13 Suspension 27 SVOC SW-846-8270D 98862 Acetophenone 0.699

Shintech Freeport3, TX 01/29/13 Suspension 27 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.025 Non-detect

Shintech Freeport3, TX 01/29/13 Suspension 27 SVOC SW-846-8270D 123319 Hydroquinone 0.05 Non-detect

Shintech Freeport3, TX 01/29/13 Suspension 27 SVOC SW-846-8270D 108952 Phenol 0.005 Non-detect

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.026

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 J

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/29/13 Suspension 27 VC EPA Method 107 75014 Vinyl chloride 0.015

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/29/13 Suspension 27 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.041

Shintech Freeport3, TX 01/30/13 Suspension 28 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect UJ

Shintech Freeport3, TX 01/30/13 Suspension 28 Alcohol SW-846-8015C 67561 Methanol 45 J

Shintech Freeport3, TX 01/30/13 Suspension 28 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.46

Shintech Freeport3, TX 01/30/13 Suspension 28 Aldehyde SW-846-8315A 50000 Formaldehyde 0.572

Shintech Freeport3, TX 01/30/13 Suspension 28 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.035 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 SVOC SW-846-8270D 98862 Acetophenone 0.656

Shintech Freeport3, TX 01/30/13 Suspension 28 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.025 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 SVOC SW-846-8270D 123319 Hydroquinone 0.05 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 SVOC SW-846-8270D 108952 Phenol 0.005 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.029

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 J

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect UJ

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 VC EPA Method 107 75014 Vinyl chloride 0.018

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/30/13 Suspension 28 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.046

Shintech Freeport3, TX 01/31/13 Suspension 29 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 Alcohol SW-846-8015C 67561 Methanol 45 J

Shintech Freeport3, TX 01/31/13 Suspension 29 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.24

Shintech Freeport3, TX 01/31/13 Suspension 29 Aldehyde SW-846-8315A 50000 Formaldehyde 0.58

Shintech Freeport3, TX 01/31/13 Suspension 29 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.035 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 SVOC SW-846-8270D 98862 Acetophenone 0.553

Shintech Freeport3, TX 01/31/13 Suspension 29 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.025 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 SVOC SW-846-8270D 123319 Hydroquinone 0.05 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 SVOC SW-846-8270D 108952 Phenol 0.005 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.025

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 J

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 VC EPA Method 107 75014 Vinyl chloride 0.022

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 01/31/13 Suspension 29 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.036

Shintech Freeport3, TX 02/01/13 Suspension 30 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Shintech Freeport3, TX 02/01/13 Suspension 30 Alcohol SW-846-8015C 67561 Methanol 40 J

Shintech Freeport3, TX 02/01/13 Suspension 30 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.33

Shintech Freeport3, TX 02/01/13 Suspension 30 Aldehyde SW-846-8315A 50000 Formaldehyde 0.602

Shintech Freeport3, TX 02/01/13 Suspension 30 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.014 Non-detect R

Shintech Freeport3, TX 02/01/13 Suspension 30 SVOC SW-846-8270D 98862 Acetophenone 0.354

Shintech Freeport3, TX 02/01/13 Suspension 30 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.01 Non-detect

Shintech Freeport3, TX 02/01/13 Suspension 30 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Non-detect R

Shintech Freeport3, TX 02/01/13 Suspension 30 SVOC SW-846-8270D 108952 Phenol 0.002 Non-detect

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect R

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.024 J

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 J

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

12/12/2013 VI Confidential 48 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect R

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Shintech Freeport3, TX 02/01/13 Suspension 30 VC EPA Method 107 75014 Vinyl chloride 0.02

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Shintech Freeport3, TX 02/01/13 Suspension 30 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.039

Oxy Deer Park, TX 01/07/13 Suspension 1 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 Alcohol SW-846-8015C 67561 Methanol 1 J-estimated sample result

Oxy Deer Park, TX 01/07/13 Suspension 1 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.97

Oxy Deer Park, TX 01/07/13 Suspension 1 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.14 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 SVOC SW-846-8270D 98862 Acetophenone 2.34

Oxy Deer Park, TX 01/07/13 Suspension 1 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.1 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/07/13 Suspension 1 SVOC SW-846-8270D 108952 Phenol 0.02 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.006

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.01

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.005 J-estimated sample result

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 VC EPA Method 107 75014 Vinyl chloride 0.085

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/07/13 Suspension 1 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.004 J-estimated sample result

Oxy Deer Park, TX 01/08/13 Suspension 2 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 Alcohol SW-846-8015C 67561 Methanol 3 J-estimated sample result

Oxy Deer Park, TX 01/08/13 Suspension 2 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.23

Oxy Deer Park, TX 01/08/13 Suspension 2 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.14 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 SVOC SW-846-8270D 98862 Acetophenone 2.27

Oxy Deer Park, TX 01/08/13 Suspension 2 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.1 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/08/13 Suspension 2 SVOC SW-846-8270D 108952 Phenol 0.02 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.026

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.018

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 VC EPA Method 107 75014 Vinyl chloride 0.033

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/08/13 Suspension 2 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.004 J-estimated sample result

Oxy Deer Park, TX 01/09/13 Suspension 3 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 Alcohol SW-846-8015C 67561 Methanol 6 J-estimated sample result

Oxy Deer Park, TX 01/09/13 Suspension 3 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.3

Oxy Deer Park, TX 01/09/13 Suspension 3 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 SVOC SW-846-8270D 51285 2,4-dinitrophenol R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/09/13 Suspension 3 SVOC SW-846-8270D 98862 Acetophenone 1.8

Oxy Deer Park, TX 01/09/13 Suspension 3 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.1 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/09/13 Suspension 3 SVOC SW-846-8270D 108952 Phenol 0.02 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.019

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.024

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.018

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 VC EPA Method 107 75014 Vinyl chloride 0.054

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/09/13 Suspension 3 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.005 J-estimated sample result

Oxy Deer Park, TX 01/10/13 Suspension 4 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 Alcohol SW-846-8015C 67561 Methanol 8 J-estimated sample result

Oxy Deer Park, TX 01/10/13 Suspension 4 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.17

Oxy Deer Park, TX 01/10/13 Suspension 4 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.14 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 SVOC SW-846-8270D 98862 Acetophenone 3.14

Oxy Deer Park, TX 01/10/13 Suspension 4 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.1 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/10/13 Suspension 4 SVOC SW-846-8270D 108952 Phenol 0.02 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.014

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.021

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.009

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 VC EPA Method 107 75014 Vinyl chloride 0.132

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/10/13 Suspension 4 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.004 J-estimated sample result

Oxy Deer Park, TX 01/11/13 Suspension 5 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 Alcohol SW-846-8015C 67561 Methanol 7 J-estimated sample result

Oxy Deer Park, TX 01/11/13 Suspension 5 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.03

Oxy Deer Park, TX 01/11/13 Suspension 5 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.14 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 SVOC SW-846-8270D 98862 Acetophenone 3.02

Oxy Deer Park, TX 01/11/13 Suspension 5 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.1 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/11/13 Suspension 5 SVOC SW-846-8270D 108952 Phenol 0.02 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.004 J-estimated sample result

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.017

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.007

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 VC EPA Method 107 75014 Vinyl chloride 0.041

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/11/13 Suspension 5 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001

Oxy Deer Park, TX 01/12/13 Suspension 6 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 Alcohol SW-846-8015C 67561 Methanol 6 J-estimated sample result

Oxy Deer Park, TX 01/12/13 Suspension 6 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.41

Oxy Deer Park, TX 01/12/13 Suspension 6 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.14 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 SVOC SW-846-8270D 98862 Acetophenone 3.01

Oxy Deer Park, TX 01/12/13 Suspension 6 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.1 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/12/13 Suspension 6 SVOC SW-846-8270D 108952 Phenol 0.02 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.007

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.012

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.013

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 VC EPA Method 107 75014 Vinyl chloride 0.095

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

12/12/2013 VI Confidential 50 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/12/13 Suspension 6 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.002 J-estimated sample result

Oxy Deer Park, TX 01/13/13 Suspension 7 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 Alcohol SW-846-8015C 67561 Methanol 7

Oxy Deer Park, TX 01/13/13 Suspension 7 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.21

Oxy Deer Park, TX 01/13/13 Suspension 7 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.14 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 SVOC SW-846-8270D 98862 Acetophenone 2.81

Oxy Deer Park, TX 01/13/13 Suspension 7 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.1 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/13/13 Suspension 7 SVOC SW-846-8270D 108952 Phenol 0.02 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.013

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.017

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.015

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 VC EPA Method 107 75014 Vinyl chloride 0.047

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/13/13 Suspension 7 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.003 J-estimated sample result

Oxy Deer Park, TX 01/14/13 Suspension 8 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 Alcohol SW-846-8015C 67561 Methanol 8

Oxy Deer Park, TX 01/14/13 Suspension 8 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.03

Oxy Deer Park, TX 01/14/13 Suspension 8 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.14 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 SVOC SW-846-8270D 98862 Acetophenone 3.8

Oxy Deer Park, TX 01/14/13 Suspension 8 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.1 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/14/13 Suspension 8 SVOC SW-846-8270D 108952 Phenol 0.02 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 67663 Chloroform 0.002 J-estimated sample result

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.024

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.046

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.05

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 VC EPA Method 107 75014 Vinyl chloride 0.026

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/14/13 Suspension 8 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.008 J-estimated sample result

Oxy Deer Park, TX 01/15/13 Suspension 9 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 Alcohol SW-846-8015C 67561 Methanol 9

Oxy Deer Park, TX 01/15/13 Suspension 9 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.6

Oxy Deer Park, TX 01/15/13 Suspension 9 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.14 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 SVOC SW-846-8270D 98862 Acetophenone 1.87

Oxy Deer Park, TX 01/15/13 Suspension 9 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.1 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 SVOC SW-846-8270D 123319 Hydroquinone 0.2 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 SVOC SW-846-8270D 108952 Phenol 0.02 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 67663 Chloroform 0.002 J-estimated sample result

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.028

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.032

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.038

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 VC EPA Method 107 75014 Vinyl chloride 0.010 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/15/13 Suspension 9 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.005 J-estimated sample result

Oxy Deer Park, TX 01/16/13 Suspension 10 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 Alcohol SW-846-8015C 67561 Methanol 8

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Oxy Deer Park, TX 01/16/13 Suspension 10 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.33

Oxy Deer Park, TX 01/16/13 Suspension 10 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 SVOC SW-846-8270D 98862 Acetophenone 0.121

Oxy Deer Park, TX 01/16/13 Suspension 10 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 SVOC SW-846-8270D 123319 Hydroquinone 0.01 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 67663 Chloroform 0.001 J-estimated sample result

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J-estimated sample result

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.002 J-estimated sample result

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.003 J-estimated sample result

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 VC EPA Method 107 75014 Vinyl chloride 0.013

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/16/13 Suspension 10 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001

Oxy Deer Park, TX 01/17/13 Suspension 11 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 Alcohol SW-846-8015C 67561 Methanol 10

Oxy Deer Park, TX 01/17/13 Suspension 11 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.94

Oxy Deer Park, TX 01/17/13 Suspension 11 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 SVOC SW-846-8270D 98862 Acetophenone 0.108

Oxy Deer Park, TX 01/17/13 Suspension 11 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/17/13 Suspension 11 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 67663 Chloroform 0.002 J-estimated sample result

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.088

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.018

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.012

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 VC EPA Method 107 75014 Vinyl chloride 0.951

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/17/13 Suspension 11 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.002 J-estimated sample result

Oxy Deer Park, TX 01/18/13 Suspension 12 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 Alcohol SW-846-8015C 67561 Methanol 12

Oxy Deer Park, TX 01/18/13 Suspension 12 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.28

Oxy Deer Park, TX 01/18/13 Suspension 12 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 SVOC SW-846-8270D 98862 Acetophenone 0.056

Oxy Deer Park, TX 01/18/13 Suspension 12 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/18/13 Suspension 12 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.054

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.013

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.007

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 VC EPA Method 107 75014 Vinyl chloride 0.010 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/18/13 Suspension 12 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.003 J-estimated sample result

Oxy Deer Park, TX 01/19/13 Suspension 13 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 Alcohol SW-846-8015C 67561 Methanol 10

Oxy Deer Park, TX 01/19/13 Suspension 13 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.26

Oxy Deer Park, TX 01/19/13 Suspension 13 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 SVOC SW-846-8270D 98862 Acetophenone 0.04

12/12/2013 VI Confidential 52 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Oxy Deer Park, TX 01/19/13 Suspension 13 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/19/13 Suspension 13 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.017

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.011

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.008

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 VC EPA Method 107 75014 Vinyl chloride 0.010 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/19/13 Suspension 13 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.005 J-estimated sample result

Oxy Deer Park, TX 01/20/13 Suspension 14 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 Alcohol SW-846-8015C 67561 Methanol 9

Oxy Deer Park, TX 01/20/13 Suspension 14 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.98

Oxy Deer Park, TX 01/20/13 Suspension 14 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 SVOC SW-846-8270D 98862 Acetophenone 0.034

Oxy Deer Park, TX 01/20/13 Suspension 14 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/20/13 Suspension 14 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.034

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.008

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.006

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 VC EPA Method 107 75014 Vinyl chloride 0.010 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/20/13 Suspension 14 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.003 J-estimated sample result

Oxy Deer Park, TX 01/21/13 Suspension 15 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 Alcohol SW-846-8015C 67561 Methanol 13

Oxy Deer Park, TX 01/21/13 Suspension 15 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.19

Oxy Deer Park, TX 01/21/13 Suspension 15 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 SVOC SW-846-8270D 98862 Acetophenone 0.035

Oxy Deer Park, TX 01/21/13 Suspension 15 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/21/13 Suspension 15 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.028

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.018

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.014

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 VC EPA Method 107 75014 Vinyl chloride 0.207

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/21/13 Suspension 15 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.005 J-estimated sample result

Oxy Deer Park, TX 01/22/13 Suspension 16 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 Alcohol SW-846-8015C 67561 Methanol 7

Oxy Deer Park, TX 01/22/13 Suspension 16 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.19

Oxy Deer Park, TX 01/22/13 Suspension 16 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 SVOC SW-846-8270D 98862 Acetophenone 0.029

Oxy Deer Park, TX 01/22/13 Suspension 16 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/22/13 Suspension 16 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

12/12/2013 VI Confidential 53 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.007

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.015

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.016

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 VC EPA Method 107 75014 Vinyl chloride 0.045

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/22/13 Suspension 16 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.005 J-estimated sample result

Oxy Deer Park, TX 01/23/13 Suspension 17 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 Alcohol SW-846-8015C 67561 Methanol 5

Oxy Deer Park, TX 01/23/13 Suspension 17 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.99

Oxy Deer Park, TX 01/23/13 Suspension 17 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 SVOC SW-846-8270D 98862 Acetophenone 0.042

Oxy Deer Park, TX 01/23/13 Suspension 17 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/23/13 Suspension 17 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.01

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.008

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.008

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 VC EPA Method 107 75014 Vinyl chloride 0.043

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/23/13 Suspension 17 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.004 J-estimated sample result

Oxy Deer Park, TX 01/24/13 Suspension 18 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 Alcohol SW-846-8015C 67561 Methanol 7

Oxy Deer Park, TX 01/24/13 Suspension 18 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.95

Oxy Deer Park, TX 01/24/13 Suspension 18 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 SVOC SW-846-8270D 98862 Acetophenone 0.002 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/24/13 Suspension 18 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.004 J-estimated sample result

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.007

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.005 J-estimated sample result

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 VC EPA Method 107 75014 Vinyl chloride 0.020

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/24/13 Suspension 18 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.006 J-estimated sample result

Oxy Deer Park, TX 01/25/13 Suspension 19 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 Alcohol SW-846-8015C 67561 Methanol 8

Oxy Deer Park, TX 01/25/13 Suspension 19 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.88

Oxy Deer Park, TX 01/25/13 Suspension 19 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 SVOC SW-846-8270D 98862 Acetophenone 0.13

Oxy Deer Park, TX 01/25/13 Suspension 19 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/25/13 Suspension 19 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

12/12/2013 VI Confidential 54 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J-estimated sample result

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.004 J-estimated sample result

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 J-estimated sample result

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 VC EPA Method 107 75014 Vinyl chloride 0.090

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/25/13 Suspension 19 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.003 J-estimated sample result

Oxy Deer Park, TX 01/26/13 Suspension 20 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 Alcohol SW-846-8015C 67561 Methanol 8

Oxy Deer Park, TX 01/26/13 Suspension 20 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.65

Oxy Deer Park, TX 01/26/13 Suspension 20 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 SVOC SW-846-8270D 98862 Acetophenone 0.014

Oxy Deer Park, TX 01/26/13 Suspension 20 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/26/13 Suspension 20 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.002 J-estimated sample result

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VC EPA Method 107 75014 Vinyl chloride 0.040

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/26/13 Suspension 20 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.002 J-estimated sample result

Oxy Deer Park, TX 01/27/13 Suspension 21 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 Alcohol SW-846-8015C 67561 Methanol 9

Oxy Deer Park, TX 01/27/13 Suspension 21 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.21

Oxy Deer Park, TX 01/27/13 Suspension 21 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 SVOC SW-846-8270D 98862 Acetophenone 0.007 J-estimated sample result

Oxy Deer Park, TX 01/27/13 Suspension 21 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.014

Oxy Deer Park, TX 01/27/13 Suspension 21 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/27/13 Suspension 21 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VC EPA Method 107 75014 Vinyl chloride 0.010 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/27/13 Suspension 21 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.002 J-estimated sample result

Oxy Deer Park, TX 01/28/13 Suspension 22 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 Alcohol SW-846-8015C 67561 Methanol 9

Oxy Deer Park, TX 01/28/13 Suspension 22 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.58

Oxy Deer Park, TX 01/28/13 Suspension 22 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 SVOC SW-846-8270D 98862 Acetophenone 0.002 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/28/13 Suspension 22 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

12/12/2013 VI Confidential 55 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VC EPA Method 107 75014 Vinyl chloride 0.019

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/28/13 Suspension 22 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.002 J-estimated sample result

Oxy Deer Park, TX 01/29/13 Suspension 23 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 Alcohol SW-846-8015C 67561 Methanol 10

Oxy Deer Park, TX 01/29/13 Suspension 23 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.77

Oxy Deer Park, TX 01/29/13 Suspension 23 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 SVOC SW-846-8270D 98862 Acetophenone 0.008 J-estimated sample result

Oxy Deer Park, TX 01/29/13 Suspension 23 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/29/13 Suspension 23 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VC EPA Method 107 75014 Vinyl chloride 0.015

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/29/13 Suspension 23 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.002 J-estimated sample result

Oxy Deer Park, TX 01/31/13 Suspension 24 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 Alcohol SW-846-8015C 67561 Methanol 6

Oxy Deer Park, TX 01/31/13 Suspension 24 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.38

Oxy Deer Park, TX 01/31/13 Suspension 24 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 SVOC SW-846-8270D 98862 Acetophenone 0.002 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 01/31/13 Suspension 24 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VC EPA Method 107 75014 Vinyl chloride 0.010 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 01/31/13 Suspension 24 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.002 J-estimated sample result

Oxy Deer Park, TX 02/01/13 Suspension 25 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 Alcohol SW-846-8015C 67561 Methanol 7

Oxy Deer Park, TX 02/01/13 Suspension 25 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.41

Oxy Deer Park, TX 02/01/13 Suspension 25 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 SVOC SW-846-8270D 98862 Acetophenone 0.002 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 02/01/13 Suspension 25 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.036

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.028

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.015

12/12/2013 VI Confidential 56 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 VC EPA Method 107 75014 Vinyl chloride 0.210

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 02/01/13 Suspension 25 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.008 J-estimated sample result

Oxy Deer Park, TX 02/03/13 Suspension 26 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 Alcohol SW-846-8015C 67561 Methanol 6

Oxy Deer Park, TX 02/03/13 Suspension 26 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.96

Oxy Deer Park, TX 02/03/13 Suspension 26 Aldehyde SW-846-8315A 50000 Formaldehyde 0.607

Oxy Deer Park, TX 02/03/13 Suspension 26 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 SVOC SW-846-8270D 98862 Acetophenone 0.006 J-estimated sample result

Oxy Deer Park, TX 02/03/13 Suspension 26 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 02/03/13 Suspension 26 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.004 J-estimated sample result

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.019

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.009

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 VC EPA Method 107 75014 Vinyl chloride 0.031

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 02/03/13 Suspension 26 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.007 J-estimated sample result

Oxy Deer Park, TX 02/04/13 Suspension 27 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 Alcohol SW-846-8015C 67561 Methanol 6

Oxy Deer Park, TX 02/04/13 Suspension 27 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.56

Oxy Deer Park, TX 02/04/13 Suspension 27 Aldehyde SW-846-8315A 50000 Formaldehyde 0.497 J-estimated sample result

Oxy Deer Park, TX 02/04/13 Suspension 27 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 SVOC SW-846-8270D 98862 Acetophenone 0.002 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 02/04/13 Suspension 27 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.008

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.036

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.017

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 VC EPA Method 107 75014 Vinyl chloride 0.045

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 02/04/13 Suspension 27 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.011

Oxy Deer Park, TX 02/05/13 Suspension 28 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 02/05/13 Suspension 28 Alcohol SW-846-8015C 67561 Methanol 8

Oxy Deer Park, TX 02/05/13 Suspension 28 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.12

Oxy Deer Park, TX 02/05/13 Suspension 28 Aldehyde SW-846-8315A 50000 Formaldehyde 0.591

Oxy Deer Park, TX 02/05/13 Suspension 28 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 02/05/13 Suspension 28 SVOC SW-846-8270D 98862 Acetophenone 0.006 J-estimated sample result

Oxy Deer Park, TX 02/05/13 Suspension 28 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Oxy Deer Park, TX 02/05/13 Suspension 28 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 02/05/13 Suspension 28 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.022

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.076

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.047

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

12/12/2013 VI Confidential 57 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 J-estimated sample result

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 02/05/13 Suspension 28 VC EPA Method 107 75014 Vinyl chloride 0.157

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 02/05/13 Suspension 28 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.017

Oxy Deer Park, TX 02/06/13 Suspension 29 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 Alcohol SW-846-8015C 67561 Methanol 9

Oxy Deer Park, TX 02/06/13 Suspension 29 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.91

Oxy Deer Park, TX 02/06/13 Suspension 29 Aldehyde SW-846-8315A 50000 Formaldehyde 0.722

Oxy Deer Park, TX 02/06/13 Suspension 29 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 SVOC SW-846-8270D 98862 Acetophenone 0.019

Oxy Deer Park, TX 02/06/13 Suspension 29 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 02/06/13 Suspension 29 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 106990 1,3-butadiene 0.008 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.004 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 71432 Benzene 0.004 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 108907 Chlorobenzene 0.004 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 67663 Chloroform 0.004 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 126998 Chloroprene 0.008 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.077

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 100414 Ethylbenzene 0.004 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.069

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.004 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.064

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 75092 Methylene chloride 0.004 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 110543 n-Hexane 0.004 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 108883 Toluene 0.004 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.004 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.004 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 108054 Vinyl acetate 0.004 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 593602 Vinyl bromide 0.004 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 VC EPA Method 107 75014 Vinyl chloride 0.694

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.004 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.008 Non-detect

Oxy Deer Park, TX 02/06/13 Suspension 29 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.014 J-estimated sample result

Oxy Deer Park, TX 02/07/13 Suspension 30 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 Alcohol SW-846-8015C 67561 Methanol 8

Oxy Deer Park, TX 02/07/13 Suspension 30 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.36

Oxy Deer Park, TX 02/07/13 Suspension 30 Aldehyde SW-846-8315A 50000 Formaldehyde 0.7

Oxy Deer Park, TX 02/07/13 Suspension 30 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 SVOC SW-846-8270D 98862 Acetophenone 0.005 J-estimated sample result

Oxy Deer Park, TX 02/07/13 Suspension 30 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 02/07/13 Suspension 30 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.037

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.089

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.057

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 VC EPA Method 107 75014 Vinyl chloride 0.187

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 02/07/13 Suspension 30 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.018

Oxy Deer Park, TX 02/08/13 Suspension 31 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 Alcohol SW-846-8015C 67561 Methanol 7

Oxy Deer Park, TX 02/08/13 Suspension 31 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.78

Oxy Deer Park, TX 02/08/13 Suspension 31 Aldehyde SW-846-8315A 50000 Formaldehyde 0.621

Oxy Deer Park, TX 02/08/13 Suspension 31 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.007 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 SVOC SW-846-8270D 98862 Acetophenone 0.007 J-estimated sample result

Oxy Deer Park, TX 02/08/13 Suspension 31 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.005 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Deer Park, TX 02/08/13 Suspension 31 SVOC SW-846-8270D 108952 Phenol 0.001 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.062

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.144

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.096

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 VC EPA Method 107 75014 Vinyl chloride 0.205

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Deer Park, TX 02/08/13 Suspension 31 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.03

Oxy Pasadena, TX 01/13/13 Suspension 1 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 Alcohol SW-846-8015C 67561 Methanol 674

Oxy Pasadena, TX 01/13/13 Suspension 1 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.11

Oxy Pasadena, TX 01/13/13 Suspension 1 Aldehyde SW-846-8315A 50000 Formaldehyde 0.075 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.7 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 SVOC SW-846-8270D 98862 Acetophenone 7.54

Oxy Pasadena, TX 01/13/13 Suspension 1 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.5 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 01/13/13 Suspension 1 SVOC SW-846-8270D 108952 Phenol 0.1 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VC EPA Method 107 75014 Vinyl chloride 0.097

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 01/13/13 Suspension 1 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 Alcohol SW-846-8015C 67561 Methanol 783

Oxy Pasadena, TX 01/14/13 Suspension 2 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.26

Oxy Pasadena, TX 01/14/13 Suspension 2 Aldehyde SW-846-8315A 50000 Formaldehyde 0.075 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.7 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 SVOC SW-846-8270D 98862 Acetophenone 7.8

Oxy Pasadena, TX 01/14/13 Suspension 2 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.5 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 01/14/13 Suspension 2 SVOC SW-846-8270D 108952 Phenol 0.1 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 98828 Cumene 0.002 J-estimated sample result

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VC EPA Method 107 75014 Vinyl chloride 0.011

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 01/14/13 Suspension 2 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 Alcohol SW-846-8015C 67561 Methanol 623

Oxy Pasadena, TX 01/15/13 Suspension 3 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.63

Oxy Pasadena, TX 01/15/13 Suspension 3 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 SVOC SW-846-8270D 98862 Acetophenone 6.53

Oxy Pasadena, TX 01/15/13 Suspension 3 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 SVOC SW-846-8270D 123319 Hydroquinone 0.5 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 98828 Cumene 0.011 J-estimated sample result

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.068 J-estimated sample result

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.01 J-estimated sample result

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 VC EPA Method 107 75014 Vinyl chloride 0.018

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 01/15/13 Suspension 3 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.006 J-estimated sample result

Oxy Pasadena, TX 01/16/13 Suspension 4 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

12/12/2013 VI Confidential 59 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Oxy Pasadena, TX 01/16/13 Suspension 4 Alcohol SW-846-8015C 67561 Methanol 530

Oxy Pasadena, TX 01/16/13 Suspension 4 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.79

Oxy Pasadena, TX 01/16/13 Suspension 4 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 SVOC SW-846-8270D 98862 Acetophenone 7.38

Oxy Pasadena, TX 01/16/13 Suspension 4 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 SVOC SW-846-8270D 123319 Hydroquinone 0.5 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 98828 Cumene 0.002 J-estimated sample result

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.004 J-estimated sample result

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 VC EPA Method 107 75014 Vinyl chloride 0.047

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 01/16/13 Suspension 4 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 Alcohol SW-846-8015C 67561 Methanol 519

Oxy Pasadena, TX 01/17/13 Suspension 5 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.78

Oxy Pasadena, TX 01/17/13 Suspension 5 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 SVOC SW-846-8270D 98862 Acetophenone 7.13

Oxy Pasadena, TX 01/17/13 Suspension 5 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 SVOC SW-846-8270D 123319 Hydroquinone 0.5 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 98828 Cumene 0.005 J-estimated sample result

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.004 J-estimated sample result

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.019

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 108883 Toluene 0.003 J-estimated sample result

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 VC EPA Method 107 75014 Vinyl chloride 0.010 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.003 J-estimated sample result

Oxy Pasadena, TX 01/17/13 Suspension 5 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 Alcohol SW-846-8015C 67561 Methanol 649

Oxy Pasadena, TX 01/18/13 Suspension 6 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.62

Oxy Pasadena, TX 01/18/13 Suspension 6 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 SVOC SW-846-8270D 98862 Acetophenone 3.99

Oxy Pasadena, TX 01/18/13 Suspension 6 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 SVOC SW-846-8270D 123319 Hydroquinone 0.5 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VC EPA Method 107 75014 Vinyl chloride 0.010 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 01/18/13 Suspension 6 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 Alcohol SW-846-8015C 67561 Methanol 557

Oxy Pasadena, TX 01/19/13 Suspension 7 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.94

Oxy Pasadena, TX 01/19/13 Suspension 7 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Oxy Pasadena, TX 01/19/13 Suspension 7 SVOC SW-846-8270D 98862 Acetophenone 5.08

Oxy Pasadena, TX 01/19/13 Suspension 7 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 01/19/13 Suspension 7 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VC EPA Method 107 75014 Vinyl chloride 0.010 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 01/19/13 Suspension 7 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001 J-estimated sample result

Oxy Pasadena, TX 01/20/13 Suspension 8 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 Alcohol SW-846-8015C 67561 Methanol 745

Oxy Pasadena, TX 01/20/13 Suspension 8 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.22

Oxy Pasadena, TX 01/20/13 Suspension 8 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 SVOC SW-846-8270D 98862 Acetophenone 5.47

Oxy Pasadena, TX 01/20/13 Suspension 8 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 01/20/13 Suspension 8 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VC EPA Method 107 75014 Vinyl chloride 0.328

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 01/20/13 Suspension 8 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 Alcohol SW-846-8015C 67561 Methanol 916

Oxy Pasadena, TX 01/21/13 Suspension 9 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.41

Oxy Pasadena, TX 01/21/13 Suspension 9 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 SVOC SW-846-8270D 98862 Acetophenone 5.28

Oxy Pasadena, TX 01/21/13 Suspension 9 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 01/21/13 Suspension 9 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VC EPA Method 107 75014 Vinyl chloride 0.082

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 01/21/13 Suspension 9 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 Alcohol SW-846-8015C 67561 Methanol 673

Oxy Pasadena, TX 01/22/13 Suspension 10 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.93

Oxy Pasadena, TX 01/22/13 Suspension 10 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 SVOC SW-846-8270D 98862 Acetophenone 5.42

Oxy Pasadena, TX 01/22/13 Suspension 10 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 01/22/13 Suspension 10 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

12/12/2013 VI Confidential 61 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VC EPA Method 107 75014 Vinyl chloride 0.010 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 01/22/13 Suspension 10 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 Alcohol SW-846-8015C 67561 Methanol 663

Oxy Pasadena, TX 01/23/13 Suspension 11 Aldehyde SW-846-8315A 75070 Acetaldehyde 8.15

Oxy Pasadena, TX 01/23/13 Suspension 11 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 SVOC SW-846-8270D 98862 Acetophenone 4.72

Oxy Pasadena, TX 01/23/13 Suspension 11 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 01/23/13 Suspension 11 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 98828 Cumene 0.005 J-estimated sample result

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.068 J-estimated sample result

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.009 J-estimated sample result

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.003 J-estimated sample result

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 VC EPA Method 107 75014 Vinyl chloride 0.224

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 01/23/13 Suspension 11 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 Alcohol SW-846-8015C 67561 Methanol 548

Oxy Pasadena, TX 01/24/13 Suspension 12 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.43

Oxy Pasadena, TX 01/24/13 Suspension 12 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 SVOC SW-846-8270D 98862 Acetophenone 6.22

Oxy Pasadena, TX 01/24/13 Suspension 12 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 01/24/13 Suspension 12 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 98828 Cumene 0.002 J-estimated sample result

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VC EPA Method 107 75014 Vinyl chloride 0.010 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 01/24/13 Suspension 12 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 Alcohol SW-846-8015C 67561 Methanol 722

Oxy Pasadena, TX 01/25/13 Suspension 13 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.78

Oxy Pasadena, TX 01/25/13 Suspension 13 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 SVOC SW-846-8270D 98862 Acetophenone 5.76

Oxy Pasadena, TX 01/25/13 Suspension 13 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 01/25/13 Suspension 13 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 98828 Cumene 0.002 J-estimated sample result

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 VC EPA Method 107 75014 Vinyl chloride 0.150

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 01/25/13 Suspension 13 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 Alcohol SW-846-8015C 67561 Methanol 697

Oxy Pasadena, TX 01/26/13 Suspension 14 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.88

Oxy Pasadena, TX 01/26/13 Suspension 14 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 SVOC SW-846-8270D 98862 Acetophenone 7.21

Oxy Pasadena, TX 01/26/13 Suspension 14 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 01/26/13 Suspension 14 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VC EPA Method 107 75014 Vinyl chloride 0.090

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 01/26/13 Suspension 14 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 Alcohol SW-846-8015C 67561 Methanol 722

Oxy Pasadena, TX 01/27/13 Suspension 15 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.7

Oxy Pasadena, TX 01/27/13 Suspension 15 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 SVOC SW-846-8270D 98862 Acetophenone 7.22

Oxy Pasadena, TX 01/27/13 Suspension 15 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 01/27/13 Suspension 15 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 98828 Cumene 0.004 J-estimated sample result

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J-estimated sample result

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 VC EPA Method 107 75014 Vinyl chloride 0.024

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 01/27/13 Suspension 15 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 Alcohol SW-846-8015C 67561 Methanol 832

Oxy Pasadena, TX 01/28/13 Suspension 16 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.65

Oxy Pasadena, TX 01/28/13 Suspension 16 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 SVOC SW-846-8270D 98862 Acetophenone 3.94

Oxy Pasadena, TX 01/28/13 Suspension 16 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 01/28/13 Suspension 16 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 98828 Cumene 0.001 J-estimated sample result

12/12/2013 VI Confidential 63 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VC EPA Method 107 75014 Vinyl chloride 0.015

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 01/28/13 Suspension 16 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 Alcohol SW-846-8015C 67561 Methanol 621

Oxy Pasadena, TX 01/29/13 Suspension 17 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.41

Oxy Pasadena, TX 01/29/13 Suspension 17 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 SVOC SW-846-8270D 98862 Acetophenone 7.66

Oxy Pasadena, TX 01/29/13 Suspension 17 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 01/29/13 Suspension 17 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VC EPA Method 107 75014 Vinyl chloride 0.010 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 01/29/13 Suspension 17 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 Alcohol SW-846-8015C 67561 Methanol 787

Oxy Pasadena, TX 01/30/13 Suspension 18 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.18

Oxy Pasadena, TX 01/30/13 Suspension 18 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 SVOC SW-846-8270D 98862 Acetophenone 4.52

Oxy Pasadena, TX 01/30/13 Suspension 18 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 01/30/13 Suspension 18 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 98828 Cumene 0.002 J-estimated sample result

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VC EPA Method 107 75014 Vinyl chloride 0.010 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 01/30/13 Suspension 18 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 Alcohol SW-846-8015C 67561 Methanol 587

Oxy Pasadena, TX 01/31/13 Suspension 19 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.14

Oxy Pasadena, TX 01/31/13 Suspension 19 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 SVOC SW-846-8270D 98862 Acetophenone 7.71

Oxy Pasadena, TX 01/31/13 Suspension 19 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 01/31/13 Suspension 19 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.002 J-estimated sample result

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.005 J-estimated sample result

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 98828 Cumene 0.002 J-estimated sample result

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 75092 Methylene chloride 0.004 J-estimated sample result

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 VC EPA Method 107 75014 Vinyl chloride 0.010 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 01/31/13 Suspension 19 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 Alcohol SW-846-8015C 67561 Methanol 791

Oxy Pasadena, TX 02/01/13 Suspension 20 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.38

Oxy Pasadena, TX 02/01/13 Suspension 20 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 SVOC SW-846-8270D 98862 Acetophenone 5.43

Oxy Pasadena, TX 02/01/13 Suspension 20 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 02/01/13 Suspension 20 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VC EPA Method 107 75014 Vinyl chloride 0.010 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 02/01/13 Suspension 20 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.003 J-estimated sample result

Oxy Pasadena, TX 02/02/13 Suspension 21 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 Alcohol SW-846-8015C 67561 Methanol 780

Oxy Pasadena, TX 02/02/13 Suspension 21 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.41

Oxy Pasadena, TX 02/02/13 Suspension 21 Aldehyde SW-846-8315A 50000 Formaldehyde 0.247 J-estimated sample result

Oxy Pasadena, TX 02/02/13 Suspension 21 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.7 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 SVOC SW-846-8270D 98862 Acetophenone 11

Oxy Pasadena, TX 02/02/13 Suspension 21 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.5 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 02/02/13 Suspension 21 SVOC SW-846-8270D 108952 Phenol 0.1 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 126998 Chloroprene 0.006 J-estimated sample result

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 98828 Cumene 0.03 J-estimated sample result

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.033 J-estimated sample result

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.016 J-estimated sample result

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 VC EPA Method 107 75014 Vinyl chloride 0.906

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 02/02/13 Suspension 21 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.009 J-estimated sample result

Oxy Pasadena, TX 02/03/13 Suspension 22 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 Alcohol SW-846-8015C 67561 Methanol 736

Oxy Pasadena, TX 02/03/13 Suspension 22 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.09

Oxy Pasadena, TX 02/03/13 Suspension 22 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 SVOC SW-846-8270D 98862 Acetophenone 9.54

Oxy Pasadena, TX 02/03/13 Suspension 22 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 02/03/13 Suspension 22 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 98828 Cumene 0.002 J-estimated sample result

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002 J-estimated sample result

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

12/12/2013 VI Confidential 65 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 VC EPA Method 107 75014 Vinyl chloride 0.036

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 02/03/13 Suspension 22 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 Alcohol SW-846-8015C 67561 Methanol 689

Oxy Pasadena, TX 02/04/13 Suspension 23 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.02

Oxy Pasadena, TX 02/04/13 Suspension 23 Aldehyde SW-846-8315A 50000 Formaldehyde 0.216 J-estimated sample result

Oxy Pasadena, TX 02/04/13 Suspension 23 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 SVOC SW-846-8270D 98862 Acetophenone 5.84

Oxy Pasadena, TX 02/04/13 Suspension 23 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 02/04/13 Suspension 23 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 98828 Cumene 0.003 J-estimated sample result

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VC EPA Method 107 75014 Vinyl chloride 0.010 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 02/04/13 Suspension 23 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 Alcohol SW-846-8015C 67561 Methanol 787

Oxy Pasadena, TX 02/05/13 Suspension 24 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.44

Oxy Pasadena, TX 02/05/13 Suspension 24 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 SVOC SW-846-8270D 98862 Acetophenone 5.9

Oxy Pasadena, TX 02/05/13 Suspension 24 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 02/05/13 Suspension 24 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 98828 Cumene 0.001 J-estimated sample result

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VC EPA Method 107 75014 Vinyl chloride 0.010 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 02/05/13 Suspension 24 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.001 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 Alcohol SW-846-8015C 67561 Methanol 932

Oxy Pasadena, TX 02/06/13 Suspension 25 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.23

Oxy Pasadena, TX 02/06/13 Suspension 25 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 SVOC SW-846-8270D 98862 Acetophenone 8.42

Oxy Pasadena, TX 02/06/13 Suspension 25 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 02/06/13 Suspension 25 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 98828 Cumene 0.002 J-estimated sample result

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J-estimated sample result

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.002 J-estimated sample result

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Oxy Pasadena, TX 02/06/13 Suspension 25 VC EPA Method 107 75014 Vinyl chloride 0.017

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 02/06/13 Suspension 25 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.007 J-estimated sample result

Oxy Pasadena, TX 02/07/13 Suspension 26 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 Alcohol SW-846-8015C 67561 Methanol 932

Oxy Pasadena, TX 02/07/13 Suspension 26 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.95

Oxy Pasadena, TX 02/07/13 Suspension 26 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 SVOC SW-846-8270D 98862 Acetophenone 7.01

Oxy Pasadena, TX 02/07/13 Suspension 26 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 02/07/13 Suspension 26 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 98828 Cumene 0.001 J-estimated sample result

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.003 J-estimated sample result

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.002 J-estimated sample result

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 VC EPA Method 107 75014 Vinyl chloride 0.017

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 02/07/13 Suspension 26 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.005 J-estimated sample result

Oxy Pasadena, TX 02/08/13 Suspension 27 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 Alcohol SW-846-8015C 67561 Methanol 856

Oxy Pasadena, TX 02/08/13 Suspension 27 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.2

Oxy Pasadena, TX 02/08/13 Suspension 27 Aldehyde SW-846-8315A 50000 Formaldehyde 0.203 J-estimated sample result

Oxy Pasadena, TX 02/08/13 Suspension 27 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 SVOC SW-846-8270D 98862 Acetophenone 7.64

Oxy Pasadena, TX 02/08/13 Suspension 27 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 02/08/13 Suspension 27 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 98828 Cumene 0.001 J-estimated sample result

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 J-estimated sample result

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 VC EPA Method 107 75014 Vinyl chloride 0.029

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 02/08/13 Suspension 27 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.003 J-estimated sample result

Oxy Pasadena, TX 02/09/13 Suspension 28 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 Alcohol SW-846-8015C 67561 Methanol 1020

Oxy Pasadena, TX 02/09/13 Suspension 28 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.05

Oxy Pasadena, TX 02/09/13 Suspension 28 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 SVOC SW-846-8270D 98862 Acetophenone 6.91

Oxy Pasadena, TX 02/09/13 Suspension 28 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 02/09/13 Suspension 28 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 98828 Cumene 0.002 J-estimated sample result

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 75092 Methylene chloride 0.001 J-estimated sample result

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 VC EPA Method 107 75014 Vinyl chloride 0.013

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 02/09/13 Suspension 28 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.003 J-estimated sample result

12/12/2013 VI Confidential 67 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Oxy Pasadena, TX 02/10/13 Suspension 29 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 Alcohol SW-846-8015C 67561 Methanol 1000

Oxy Pasadena, TX 02/10/13 Suspension 29 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.3

Oxy Pasadena, TX 02/10/13 Suspension 29 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 SVOC SW-846-8270D 98862 Acetophenone 5.05

Oxy Pasadena, TX 02/10/13 Suspension 29 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 SVOC SW-846-8270D 123319 Hydroquinone R result rejected due to poor analyte efficiency

Oxy Pasadena, TX 02/10/13 Suspension 29 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 98828 Cumene 0.002 J-estimated sample result

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 J-estimated sample result

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 VC EPA Method 107 75014 Vinyl chloride 0.021

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 02/10/13 Suspension 29 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.004 J-estimated sample result

Oxy Pasadena, TX 02/11/13 Suspension 30 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 Alcohol SW-846-8015C 67561 Methanol 1060

Oxy Pasadena, TX 02/11/13 Suspension 30 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.82

Oxy Pasadena, TX 02/11/13 Suspension 30 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.35 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 SVOC SW-846-8270D 98862 Acetophenone 6.98

Oxy Pasadena, TX 02/11/13 Suspension 30 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 SVOC SW-846-8270D 123319 Hydroquinone 0.5 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 SVOC SW-846-8270D 108952 Phenol 0.05 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 106990 1,3-butadiene 0.002 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 126998 Chloroprene 0.002 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 98828 Cumene 0.001 J-estimated sample result

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.002 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 110543 n-Hexane 0.001 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 593602 Vinyl bromide 0.001 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VC EPA Method 107 75014 Vinyl chloride 0.010 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Oxy Pasadena, TX 02/11/13 Suspension 30 VOC SW-846-8260B 108101 4-Methyl 2-pentanone (MIBK) 0.004 J-estimated sample result

Formosa TX 01/07/13 Suspension 1 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/07/13 Suspension 1 Alcohol SW-846-8015C 67561 Methanol 135

Formosa TX 01/07/13 Suspension 1 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.9

Formosa TX 01/07/13 Suspension 1 Aldehyde SW-846-8315A 50000 Formaldehyde 0.056 Non-detect

Formosa TX 01/07/13 Suspension 1 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa TX 01/07/13 Suspension 1 SVOC SW-846-8270D 98862 Acetophenone 5.99

Formosa TX 01/07/13 Suspension 1 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0838 J-estimated value

Formosa TX 01/07/13 Suspension 1 SVOC SW-846-8270D 123319 Hydroquinone 0.102 J-estimated value

Formosa TX 01/07/13 Suspension 1 SVOC SW-846-8270D 108952 Phenol 0.029 Non-detect

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 67663 Chloroform 0.00035 Non-detect

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 98828 Cumene 0.0033

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0175

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.133

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0036

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/07/13 Suspension 1 VC EPA Method 107 75014 Vinyl chloride 0.1

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/07/13 Suspension 1 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/08/13 Suspension 2 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/08/13 Suspension 2 Alcohol SW-846-8015C 67561 Methanol 128

Formosa TX 01/08/13 Suspension 2 Aldehyde SW-846-8315A 75070 Acetaldehyde 1

Formosa TX 01/08/13 Suspension 2 Aldehyde SW-846-8315A 50000 Formaldehyde 0.35

Formosa TX 01/08/13 Suspension 2 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa TX 01/08/13 Suspension 2 SVOC SW-846-8270D 98862 Acetophenone 1.92

Formosa TX 01/08/13 Suspension 2 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.3

Formosa TX 01/08/13 Suspension 2 SVOC SW-846-8270D 123319 Hydroquinone 0.053 J-estimated value

Formosa TX 01/08/13 Suspension 2 SVOC SW-846-8270D 108952 Phenol 0.015 Non-detect

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 67663 Chloroform 0.00062 J-estimated value

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 98828 Cumene 0.0017

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.005

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00084 J-estimated value

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00063 Non-detect

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/08/13 Suspension 2 VC EPA Method 107 75014 Vinyl chloride 0.1

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/08/13 Suspension 2 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/09/13 Suspension 3 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/09/13 Suspension 3 Alcohol SW-846-8015C 67561 Methanol 148

Formosa TX 01/09/13 Suspension 3 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.5

Formosa TX 01/09/13 Suspension 3 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0056 Non-detect

Formosa TX 01/09/13 Suspension 3 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.21 Non-detect

Formosa TX 01/09/13 Suspension 3 SVOC SW-846-8270D 98862 Acetophenone 2.99

Formosa TX 01/09/13 Suspension 3 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.151

Formosa TX 01/09/13 Suspension 3 SVOC SW-846-8270D 123319 Hydroquinone 0.952 J-estimated value

Formosa TX 01/09/13 Suspension 3 SVOC SW-846-8270D 108952 Phenol 0.03 Non-detect

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 67663 Chloroform 0.00094 J-estimated value

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0021

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00063 Non-detect

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/09/13 Suspension 3 VC EPA Method 107 75014 Vinyl chloride Detection Limit Not Reported

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/09/13 Suspension 3 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/10/13 Suspension 4 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/10/13 Suspension 4 Alcohol SW-846-8015C 67561 Methanol 119

Formosa TX 01/10/13 Suspension 4 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.79

Formosa TX 01/10/13 Suspension 4 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0056 Non-detect

Formosa TX 01/10/13 Suspension 4 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa TX 01/10/13 Suspension 4 SVOC SW-846-8270D 98862 Acetophenone 5.17

Formosa TX 01/10/13 Suspension 4 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.018 Non-detect

Formosa TX 01/10/13 Suspension 4 SVOC SW-846-8270D 123319 Hydroquinone 0.0931 J-estimated value

Formosa TX 01/10/13 Suspension 4 SVOC SW-846-8270D 108952 Phenol 0.0348 J-estimated value

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 67663 Chloroform 0.00056 J-estimated value

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0028

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00063 Non-detect

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/10/13 Suspension 4 VC EPA Method 107 75014 Vinyl chloride 0.1

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/10/13 Suspension 4 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/11/13 Suspension 5 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/11/13 Suspension 5 Alcohol SW-846-8015C 67561 Methanol 117

Formosa TX 01/11/13 Suspension 5 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.3

Formosa TX 01/11/13 Suspension 5 Aldehyde SW-846-8315A 50000 Formaldehyde 0.11

Formosa TX 01/11/13 Suspension 5 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.18 Non-detect

Formosa TX 01/11/13 Suspension 5 SVOC SW-846-8270D 98862 Acetophenone 3.35

Formosa TX 01/11/13 Suspension 5 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.032 Non-detect

Formosa TX 01/11/13 Suspension 5 SVOC SW-846-8270D 123319 Hydroquinone 0.105 J-estimated value

Formosa TX 01/11/13 Suspension 5 SVOC SW-846-8270D 108952 Phenol 0.027 Non-detect

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 67663 Chloroform 0.00064 J-estimated value

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0023

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00063 Non-detect

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/11/13 Suspension 5 VC EPA Method 107 75014 Vinyl chloride 0.1

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/11/13 Suspension 5 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/12/13 Suspension 6 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/12/13 Suspension 6 Alcohol SW-846-8015C 67561 Methanol 105

Formosa TX 01/12/13 Suspension 6 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.2

Formosa TX 01/12/13 Suspension 6 Aldehyde SW-846-8315A 50000 Formaldehyde 0.11

Formosa TX 01/12/13 Suspension 6 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa TX 01/12/13 Suspension 6 SVOC SW-846-8270D 98862 Acetophenone 1.91

Formosa TX 01/12/13 Suspension 6 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.195

Formosa TX 01/12/13 Suspension 6 SVOC SW-846-8270D 123319 Hydroquinone 0.33

Formosa TX 01/12/13 Suspension 6 SVOC SW-846-8270D 108952 Phenol 0.03 Non-detect

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 67663 Chloroform 0.00065 J-estimated value

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0352

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00063 Non-detect

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/12/13 Suspension 6 VC EPA Method 107 75014 Vinyl chloride 0.1

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/12/13 Suspension 6 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/13/13 Suspension 7 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/13/13 Suspension 7 Alcohol SW-846-8015C 67561 Methanol 145

Formosa TX 01/13/13 Suspension 7 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.9

Formosa TX 01/13/13 Suspension 7 Aldehyde SW-846-8315A 50000 Formaldehyde 0.089

Formosa TX 01/13/13 Suspension 7 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa TX 01/13/13 Suspension 7 SVOC SW-846-8270D 98862 Acetophenone 10.5

Formosa TX 01/13/13 Suspension 7 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.144

Formosa TX 01/13/13 Suspension 7 SVOC SW-846-8270D 123319 Hydroquinone 0.458

Formosa TX 01/13/13 Suspension 7 SVOC SW-846-8270D 108952 Phenol 0.029 Non-detect

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 67663 Chloroform 0.00069 J-estimated value

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0032

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00063 Non-detect

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/13/13 Suspension 7 VC EPA Method 107 75014 Vinyl chloride 0.1

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/13/13 Suspension 7 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/14/13 Suspension 8 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/14/13 Suspension 8 Alcohol SW-846-8015C 67561 Methanol 112

Formosa TX 01/14/13 Suspension 8 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.2

Formosa TX 01/14/13 Suspension 8 Aldehyde SW-846-8315A 50000 Formaldehyde 0.044

Formosa TX 01/14/13 Suspension 8 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa TX 01/14/13 Suspension 8 SVOC SW-846-8270D 98862 Acetophenone 11.2

Formosa TX 01/14/13 Suspension 8 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.036 Non-detect

Formosa TX 01/14/13 Suspension 8 SVOC SW-846-8270D 123319 Hydroquinone 0.198

Formosa TX 01/14/13 Suspension 8 SVOC SW-846-8270D 108952 Phenol 0.03 Non-detect

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 67663 Chloroform 0.00035 Non-detect

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 98828 Cumene 0.00044 J-estimated value

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0148

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00063 Non-detect

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/14/13 Suspension 8 VC EPA Method 107 75014 Vinyl chloride 0.1

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/14/13 Suspension 8 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/15/13 Suspension 9 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/15/13 Suspension 9 Alcohol SW-846-8015C 67561 Methanol 144

Formosa TX 01/15/13 Suspension 9 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.8

Formosa TX 01/15/13 Suspension 9 Aldehyde SW-846-8315A 50000 Formaldehyde 0.13 J-estimated value

Formosa TX 01/15/13 Suspension 9 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa TX 01/15/13 Suspension 9 SVOC SW-846-8270D 98862 Acetophenone 4.64

Formosa TX 01/15/13 Suspension 9 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.036 Non-detect

Formosa TX 01/15/13 Suspension 9 SVOC SW-846-8270D 123319 Hydroquinone 0.0299 J-estimated value

Formosa TX 01/15/13 Suspension 9 SVOC SW-846-8270D 108952 Phenol 0.029 Non-detect

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 67663 Chloroform 0.0051 J-estimated value

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 98828 Cumene 0.0063 J-estimated value

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00072 Non-detect

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0632 J-estimated value

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0015

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0458

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/15/13 Suspension 9 VC EPA Method 107 75014 Vinyl chloride 0.4

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/15/13 Suspension 9 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/16/13 Suspension 10 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/16/13 Suspension 10 Alcohol SW-846-8015C 67561 Methanol 204

Formosa TX 01/16/13 Suspension 10 Aldehyde SW-846-8315A 75070 Acetaldehyde 12

Formosa TX 01/16/13 Suspension 10 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa TX 01/16/13 Suspension 10 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa TX 01/16/13 Suspension 10 SVOC SW-846-8270D 98862 Acetophenone 8.31

Formosa TX 01/16/13 Suspension 10 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.036 Non-detect

Formosa TX 01/16/13 Suspension 10 SVOC SW-846-8270D 123319 Hydroquinone R R-rejected 

Formosa TX 01/16/13 Suspension 10 SVOC SW-846-8270D 108952 Phenol 0.029 Non-detect

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 67663 Chloroform 0.00035 Non-detect

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0446

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0031

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0018

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/16/13 Suspension 10 VC EPA Method 107 75014 Vinyl chloride Detection Limit Not Reported

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/16/13 Suspension 10 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/17/13 Suspension 11 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/17/13 Suspension 11 Alcohol SW-846-8015C 67561 Methanol 138

Formosa TX 01/17/13 Suspension 11 Aldehyde SW-846-8315A 75070 Acetaldehyde 9.7

Formosa TX 01/17/13 Suspension 11 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa TX 01/17/13 Suspension 11 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa TX 01/17/13 Suspension 11 SVOC SW-846-8270D 98862 Acetophenone 6.2

Formosa TX 01/17/13 Suspension 11 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.204

Formosa TX 01/17/13 Suspension 11 SVOC SW-846-8270D 123319 Hydroquinone R R-rejected 

Formosa TX 01/17/13 Suspension 11 SVOC SW-846-8270D 108952 Phenol 0.029 Non-detect

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 67663 Chloroform 0.00035 Non-detect

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00072 Non-detect

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.696

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 1.68

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0036

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 108054 Vinyl acetate 0.00094 J-estimated value

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/17/13 Suspension 11 VC EPA Method 107 75014 Vinyl chloride 0.4

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/17/13 Suspension 11 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/18/13 Suspension 12 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/18/13 Suspension 12 Alcohol SW-846-8015C 67561 Methanol 165

Formosa TX 01/18/13 Suspension 12 Aldehyde SW-846-8315A 75070 Acetaldehyde 12

Formosa TX 01/18/13 Suspension 12 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa TX 01/18/13 Suspension 12 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.4 Non-detect

Formosa TX 01/18/13 Suspension 12 SVOC SW-846-8270D 98862 Acetophenone 10.5

Formosa TX 01/18/13 Suspension 12 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0979 J-estimated value

Formosa TX 01/18/13 Suspension 12 SVOC SW-846-8270D 123319 Hydroquinone 0.0937 J-estimated value

Formosa TX 01/18/13 Suspension 12 SVOC SW-846-8270D 108952 Phenol 0.059 Non-detect

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 67663 Chloroform 0.00035 Non-detect

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 98828 Cumene 0.00041 J-estimated value

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0473

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.318

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.228

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0018

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/18/13 Suspension 12 VC EPA Method 107 75014 Vinyl chloride 0.3

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/18/13 Suspension 12 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/19/13 Suspension 13 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/19/13 Suspension 13 Alcohol SW-846-8015C 67561 Methanol 177

Formosa TX 01/19/13 Suspension 13 Aldehyde SW-846-8315A 75070 Acetaldehyde 16

Formosa TX 01/19/13 Suspension 13 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa TX 01/19/13 Suspension 13 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa TX 01/19/13 Suspension 13 SVOC SW-846-8270D 98862 Acetophenone 8.77

Formosa TX 01/19/13 Suspension 13 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.036 Non-detect

Formosa TX 01/19/13 Suspension 13 SVOC SW-846-8270D 123319 Hydroquinone 0.174 J-estimated value

Formosa TX 01/19/13 Suspension 13 SVOC SW-846-8270D 108952 Phenol 0.029 Non-detect

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 67663 Chloroform 0.00035 Non-detect

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.09

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.068

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.176

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/19/13 Suspension 13 VC EPA Method 107 75014 Vinyl chloride 0.6

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/19/13 Suspension 13 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/20/13 Suspension 14 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/20/13 Suspension 14 Alcohol SW-846-8015C 67561 Methanol 170

Formosa TX 01/20/13 Suspension 14 Aldehyde SW-846-8315A 75070 Acetaldehyde 10

Formosa TX 01/20/13 Suspension 14 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa TX 01/20/13 Suspension 14 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa TX 01/20/13 Suspension 14 SVOC SW-846-8270D 98862 Acetophenone 11.2

Formosa TX 01/20/13 Suspension 14 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0969 J-estimated value

Formosa TX 01/20/13 Suspension 14 SVOC SW-846-8270D 123319 Hydroquinone 0.0757 J-estimated value

Formosa TX 01/20/13 Suspension 14 SVOC SW-846-8270D 108952 Phenol 0.029 Non-detect

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 67663 Chloroform 0.00035 Non-detect

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0069

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0013

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/20/13 Suspension 14 VC EPA Method 107 75014 Vinyl chloride 0.5

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/20/13 Suspension 14 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/21/13 Suspension 15 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa TX 01/21/13 Suspension 15 Alcohol SW-846-8015C 67561 Methanol 165

Formosa TX 01/21/13 Suspension 15 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.3

Formosa TX 01/21/13 Suspension 15 Aldehyde SW-846-8315A 50000 Formaldehyde 0.036

Formosa TX 01/21/13 Suspension 15 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.01 Non-detect

Formosa TX 01/21/13 Suspension 15 SVOC SW-846-8270D 98862 Acetophenone 0.0015 Non-detect

Formosa TX 01/21/13 Suspension 15 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0018 Non-detect

Formosa TX 01/21/13 Suspension 15 SVOC SW-846-8270D 123319 Hydroquinone R R-rejected 

Formosa TX 01/21/13 Suspension 15 SVOC SW-846-8270D 108952 Phenol 1.2

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 67663 Chloroform 0.00035 Non-detect

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0064

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00063 Non-detect

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/21/13 Suspension 15 VC EPA Method 107 75014 Vinyl chloride 0.2

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/21/13 Suspension 15 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/22/13 Suspension 16 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/22/13 Suspension 16 Alcohol SW-846-8015C 67561 Methanol 170

Formosa TX 01/22/13 Suspension 16 Aldehyde SW-846-8315A 75070 Acetaldehyde 10

Formosa TX 01/22/13 Suspension 16 Aldehyde SW-846-8315A 50000 Formaldehyde 0.28 J-estimated value

Formosa TX 01/22/13 Suspension 16 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa TX 01/22/13 Suspension 16 SVOC SW-846-8270D 98862 Acetophenone 4.93

Formosa TX 01/22/13 Suspension 16 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0657 J-estimated value

Formosa TX 01/22/13 Suspension 16 SVOC SW-846-8270D 123319 Hydroquinone 0.471 J-estimated value

Formosa TX 01/22/13 Suspension 16 SVOC SW-846-8270D 108952 Phenol 0.029 Non-detect

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 67663 Chloroform 0.00035 Non-detect

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00072 Non-detect

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.007

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/22/13 Suspension 16 VC EPA Method 107 75014 Vinyl chloride 0.3

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/22/13 Suspension 16 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/23/13 Suspension 17 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/23/13 Suspension 17 Alcohol SW-846-8015C 67561 Methanol 133

Formosa TX 01/23/13 Suspension 17 Aldehyde SW-846-8315A 75070 Acetaldehyde 13

Formosa TX 01/23/13 Suspension 17 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa TX 01/23/13 Suspension 17 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa TX 01/23/13 Suspension 17 SVOC SW-846-8270D 98862 Acetophenone 8.42

Formosa TX 01/23/13 Suspension 17 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.814

Formosa TX 01/23/13 Suspension 17 SVOC SW-846-8270D 123319 Hydroquinone 0.0431 J-estimated value

Formosa TX 01/23/13 Suspension 17 SVOC SW-846-8270D 108952 Phenol 0.03 Non-detect

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 67663 Chloroform 0.00035 Non-detect

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 98828 Cumene 0.0016

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00072 Non-detect

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0141

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00035 J-estimated value

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0199

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/23/13 Suspension 17 VC EPA Method 107 75014 Vinyl chloride 0.3

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/23/13 Suspension 17 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/24/13 Suspension 18 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/24/13 Suspension 18 Alcohol SW-846-8015C 67561 Methanol 148

Formosa TX 01/24/13 Suspension 18 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.8

Formosa TX 01/24/13 Suspension 18 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa TX 01/24/13 Suspension 18 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa TX 01/24/13 Suspension 18 SVOC SW-846-8270D 98862 Acetophenone 7.2

Formosa TX 01/24/13 Suspension 18 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.036 Non-detect

Formosa TX 01/24/13 Suspension 18 SVOC SW-846-8270D 123319 Hydroquinone R

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa TX 01/24/13 Suspension 18 SVOC SW-846-8270D 108952 Phenol 0.029 Non-detect

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 67663 Chloroform 0.00035 Non-detect

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0163

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0011

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/24/13 Suspension 18 VC EPA Method 107 75014 Vinyl chloride 0.2

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/24/13 Suspension 18 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/25/13 Suspension 19 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/25/13 Suspension 19 Alcohol SW-846-8015C 67561 Methanol 132

Formosa TX 01/25/13 Suspension 19 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.88

Formosa TX 01/25/13 Suspension 19 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0056 Non-detect

Formosa TX 01/25/13 Suspension 19 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa TX 01/25/13 Suspension 19 SVOC SW-846-8270D 98862 Acetophenone 6.84

Formosa TX 01/25/13 Suspension 19 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.124

Formosa TX 01/25/13 Suspension 19 SVOC SW-846-8270D 123319 Hydroquinone 0.102 J-estimated value, VI Note (9.1)

Formosa TX 01/25/13 Suspension 19 SVOC SW-846-8270D 108952 Phenol 0.029 Non-detect

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 67663 Chloroform 0.00072 J-estimated value, VI Note (9.1)

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0289

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0045

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/25/13 Suspension 19 VC EPA Method 107 75014 Vinyl chloride 0.2

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/25/13 Suspension 19 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/26/13 Suspension 20 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/26/13 Suspension 20 Alcohol SW-846-8015C 67561 Methanol 126

Formosa TX 01/26/13 Suspension 20 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.48 J-estimated value, VI Note (9.1)

Formosa TX 01/26/13 Suspension 20 Aldehyde SW-846-8315A 50000 Formaldehyde 0.45 J-estimated value, VI Note (9.1)

Formosa TX 01/26/13 Suspension 20 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa TX 01/26/13 Suspension 20 SVOC SW-846-8270D 98862 Acetophenone 5.5

Formosa TX 01/26/13 Suspension 20 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0389 J-estimated value

Formosa TX 01/26/13 Suspension 20 SVOC SW-846-8270D 123319 Hydroquinone 0.301 J-estimated value

Formosa TX 01/26/13 Suspension 20 SVOC SW-846-8270D 108952 Phenol 0.0377 J-estimated value

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 67663 Chloroform 0.00071 J-estimated value

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0052

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00063 Non-detect

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/26/13 Suspension 20 VC EPA Method 107 75014 Vinyl chloride 0.1

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/26/13 Suspension 20 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/27/13 Suspension 21 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/27/13 Suspension 21 Alcohol SW-846-8015C 67561 Methanol 151

Formosa TX 01/27/13 Suspension 21 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.2

Formosa TX 01/27/13 Suspension 21 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0056 Non-detect

Formosa TX 01/27/13 Suspension 21 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa TX 01/27/13 Suspension 21 SVOC SW-846-8270D 98862 Acetophenone 8.87

Formosa TX 01/27/13 Suspension 21 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.036 Non-detect

Formosa TX 01/27/13 Suspension 21 SVOC SW-846-8270D 123319 Hydroquinone 0.209 J-estimated value

Formosa TX 01/27/13 Suspension 21 SVOC SW-846-8270D 108952 Phenol 0.029 Non-detect

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 67663 Chloroform 0.00087 J-estimated value

12/12/2013 VI Confidential 74 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 98828 Cumene 0.0012

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.525

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0075

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00055 J-estimated value

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0299

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/27/13 Suspension 21 VC EPA Method 107 75014 Vinyl chloride 0.1

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/27/13 Suspension 21 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/28/13 Suspension 22 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/28/13 Suspension 22 Alcohol SW-846-8015C 67561 Methanol 142

Formosa TX 01/28/13 Suspension 22 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.57

Formosa TX 01/28/13 Suspension 22 Aldehyde SW-846-8315A 50000 Formaldehyde 0.094

Formosa TX 01/28/13 Suspension 22 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa TX 01/28/13 Suspension 22 SVOC SW-846-8270D 98862 Acetophenone 5.3

Formosa TX 01/28/13 Suspension 22 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0966 J-estimated value

Formosa TX 01/28/13 Suspension 22 SVOC SW-846-8270D 123319 Hydroquinone 0.657 J-estimated value

Formosa TX 01/28/13 Suspension 22 SVOC SW-846-8270D 108952 Phenol 0.0291 J-estimated value

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 67663 Chloroform 0.00073 J-estimated value

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0113

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00063 Non-detect

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/28/13 Suspension 22 VC EPA Method 107 75014 Vinyl chloride Detection Limit Not Reported

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/28/13 Suspension 22 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/29/13 Suspension 23 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/29/13 Suspension 23 Alcohol SW-846-8015C 67561 Methanol 113

Formosa TX 01/29/13 Suspension 23 Aldehyde SW-846-8315A 75070 Acetaldehyde 1

Formosa TX 01/29/13 Suspension 23 Aldehyde SW-846-8315A 50000 Formaldehyde 0.19

Formosa TX 01/29/13 Suspension 23 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa TX 01/29/13 Suspension 23 SVOC SW-846-8270D 98862 Acetophenone 2.99

Formosa TX 01/29/13 Suspension 23 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.239

Formosa TX 01/29/13 Suspension 23 SVOC SW-846-8270D 123319 Hydroquinone 0.779 J-estimated value

Formosa TX 01/29/13 Suspension 23 SVOC SW-846-8270D 108952 Phenol 0.029 Non-detect

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 67663 Chloroform 0.0004 J-estimated value

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0065

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00063 Non-detect

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/29/13 Suspension 23 VC EPA Method 107 75014 Vinyl chloride 0.2

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/29/13 Suspension 23 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/30/13 Suspension 24 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/30/13 Suspension 24 Alcohol SW-846-8015C 67561 Methanol 119

Formosa TX 01/30/13 Suspension 24 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.79

Formosa TX 01/30/13 Suspension 24 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0056 Non-detect

Formosa TX 01/30/13 Suspension 24 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa TX 01/30/13 Suspension 24 SVOC SW-846-8270D 98862 Acetophenone 5.17

Formosa TX 01/30/13 Suspension 24 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.018 Non-detect

Formosa TX 01/30/13 Suspension 24 SVOC SW-846-8270D 123319 Hydroquinone 0.0931 J-estimated value

Formosa TX 01/30/13 Suspension 24 SVOC SW-846-8270D 108952 Phenol 0.0348 J-estimated value

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 67663 Chloroform 0.00056 J-estimated value

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0028

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00063 Non-detect

12/12/2013 VI Confidential 75 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/30/13 Suspension 24 VC EPA Method 107 75014 Vinyl chloride 0.1

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/30/13 Suspension 24 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 01/31/13 Suspension 25 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 01/31/13 Suspension 25 Alcohol SW-846-8015C 67561 Methanol 169

Formosa TX 01/31/13 Suspension 25 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.6 J-estimated value

Formosa TX 01/31/13 Suspension 25 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa TX 01/31/13 Suspension 25 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa TX 01/31/13 Suspension 25 SVOC SW-846-8270D 98862 Acetophenone 9.89

Formosa TX 01/31/13 Suspension 25 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.036 Non-detect

Formosa TX 01/31/13 Suspension 25 SVOC SW-846-8270D 123319 Hydroquinone 1.56 J-estimated value

Formosa TX 01/31/13 Suspension 25 SVOC SW-846-8270D 108952 Phenol 0.029 Non-detect

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 67663 Chloroform 0.0011

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0077

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00063 Non-detect

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 01/31/13 Suspension 25 VC EPA Method 107 75014 Vinyl chloride 0.2

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 01/31/13 Suspension 25 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 02/01/13 Suspension 26 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 02/01/13 Suspension 26 Alcohol SW-846-8015C 67561 Methanol 156

Formosa TX 02/01/13 Suspension 26 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.1

Formosa TX 02/01/13 Suspension 26 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa TX 02/01/13 Suspension 26 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.22 Non-detect

Formosa TX 02/01/13 Suspension 26 SVOC SW-846-8270D 98862 Acetophenone 5.79

Formosa TX 02/01/13 Suspension 26 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.038 Non-detect

Formosa TX 02/01/13 Suspension 26 SVOC SW-846-8270D 123319 Hydroquinone R R-rejected

Formosa TX 02/01/13 Suspension 26 SVOC SW-846-8270D 108952 Phenol 0.031 Non-detect

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 67663 Chloroform 0.0011

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0076

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00063 Non-detect

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 02/01/13 Suspension 26 VC EPA Method 107 75014 Vinyl chloride 0.1

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 02/01/13 Suspension 26 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 02/02/13 Suspension 27 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 02/02/13 Suspension 27 Alcohol SW-846-8015C 67561 Methanol 118

Formosa TX 02/02/13 Suspension 27 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.9

Formosa TX 02/02/13 Suspension 27 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa TX 02/02/13 Suspension 27 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.21 Non-detect

Formosa TX 02/02/13 Suspension 27 SVOC SW-846-8270D 98862 Acetophenone 5.14

Formosa TX 02/02/13 Suspension 27 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.037 Non-detect

Formosa TX 02/02/13 Suspension 27 SVOC SW-846-8270D 123319 Hydroquinone R

Formosa TX 02/02/13 Suspension 27 SVOC SW-846-8270D 108952 Phenol 0.03 Non-detect

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 67663 Chloroform 0.00099 J-estimated value

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0067

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00063 Non-detect

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa TX 02/02/13 Suspension 27 VC EPA Method 107 75014 Vinyl chloride 0.2

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 02/02/13 Suspension 27 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 02/03/13 Suspension 28 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 02/03/13 Suspension 28 Alcohol SW-846-8015C 67561 Methanol 141

Formosa TX 02/03/13 Suspension 28 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.4

Formosa TX 02/03/13 Suspension 28 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa TX 02/03/13 Suspension 28 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.12 Non-detect

Formosa TX 02/03/13 Suspension 28 SVOC SW-846-8270D 98862 Acetophenone 0.0317 J-estimated value

Formosa TX 02/03/13 Suspension 28 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0227 J-estimated value

Formosa TX 02/03/13 Suspension 28 SVOC SW-846-8270D 123319 Hydroquinone 0.0598 J-estimated value

Formosa TX 02/03/13 Suspension 28 SVOC SW-846-8270D 108952 Phenol 0.018 Non-detect

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00081 Non-detect

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 106990 1,3-butadiene 0.0011 Non-detect

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00097 Non-detect

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 71432 Benzene 0.00068 Non-detect

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 108907 Chlorobenzene 0.00053 Non-detect

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 67663 Chloroform 0.001 J-estimated value

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 126998 Chloroprene 0.00084 Non-detect

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 98828 Cumene 0.0008 Non-detect

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0051

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 100414 Ethylbenzene 0.00065 Non-detect

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0007 Non-detect

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00068 Non-detect

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0019 J-estimated value

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 75092 Methylene chloride 0.002 Non-detect

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 110543 n-Hexane 0.0014 Non-detect

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 108883 Toluene 0.00065 Non-detect

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00086 Non-detect

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00069 Non-detect

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 108054 Vinyl acetate 0.0015 Non-detect

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 593602 Vinyl bromide 0.0005 Non-detect

Formosa TX 02/03/13 Suspension 28 VC EPA Method 107 75014 Vinyl chloride 0.1

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0009 Non-detect

Formosa TX 02/03/13 Suspension 28 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0017 Non-detect

Formosa TX 02/04/13 Suspension 29 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 02/04/13 Suspension 29 Alcohol SW-846-8015C 67561 Methanol 130

Formosa TX 02/04/13 Suspension 29 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.3

Formosa TX 02/04/13 Suspension 29 Aldehyde SW-846-8315A 50000 Formaldehyde 0.033

Formosa TX 02/04/13 Suspension 29 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.01 Non-detect

Formosa TX 02/04/13 Suspension 29 SVOC SW-846-8270D 98862 Acetophenone 0.0015 Non-detect

Formosa TX 02/04/13 Suspension 29 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0018 Non-detect

Formosa TX 02/04/13 Suspension 29 SVOC SW-846-8270D 123319 Hydroquinone R R-rejected

Formosa TX 02/04/13 Suspension 29 SVOC SW-846-8270D 108952 Phenol 0.0015 Non-detect

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 67663 Chloroform 0.00044 J-estimated value

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0014

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00063 Non-detect

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 02/04/13 Suspension 29 VC EPA Method 107 75014 Vinyl chloride 0.1

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 02/04/13 Suspension 29 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa TX 02/05/13 Suspension 30 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa TX 02/05/13 Suspension 30 Alcohol SW-846-8015C 67561 Methanol 117

Formosa TX 02/05/13 Suspension 30 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.26

Formosa TX 02/05/13 Suspension 30 Aldehyde SW-846-8315A 50000 Formaldehyde 0.037

Formosa TX 02/05/13 Suspension 30 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.15 Non-detect

Formosa TX 02/05/13 Suspension 30 SVOC SW-846-8270D 98862 Acetophenone 2.56

Formosa TX 02/05/13 Suspension 30 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.176

Formosa TX 02/05/13 Suspension 30 SVOC SW-846-8270D 123319 Hydroquinone 0.0786 J-estimated value

Formosa TX 02/05/13 Suspension 30 SVOC SW-846-8270D 108952 Phenol 0.022 Non-detect

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 67663 Chloroform 0.00035 Non-detect

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0303

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00055 J-estimated value

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0057

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 75092 Methylene chloride 0.0162 J-estimated value

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 108054 Vinyl acetate 0.00074 Non-detect

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa TX 02/05/13 Suspension 30 VC EPA Method 107 75014 Vinyl chloride 0.1

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa TX 02/05/13 Suspension 30 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa LA 01/02/13 Suspension 1 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa LA 01/02/13 Suspension 1 Alcohol SW-846-8015C 67561 Methanol 23

Formosa LA 01/02/13 Suspension 1 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.1

Formosa LA 01/02/13 Suspension 1 Aldehyde SW-846-8315A 50000 Formaldehyde 0.25

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa LA 01/02/13 Suspension 1 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.02 Non-detect

Formosa LA 01/02/13 Suspension 1 SVOC SW-846-8270D 98862 Acetophenone 3.1

Formosa LA 01/02/13 Suspension 1 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 15

Formosa LA 01/02/13 Suspension 1 SVOC SW-846-8270D 123319 Hydroquinone 0.023 Analyte also detected in method blank.

Formosa LA 01/02/13 Suspension 1 SVOC SW-846-8270D 108952 Phenol 0.005 Non-detect

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0005 Non-detect

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 106990 1,3-butadiene 0.001 Non-detect

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.001 Non-detect

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 126998 Chloroprene 0.025 Non-detect

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0047

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Formosa LA 01/02/13 Suspension 1 VC EPA Method 107 75014 Vinyl chloride 0.047

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Formosa LA 01/02/13 Suspension 1 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001 Non-detect

Formosa LA 01/03/13 Suspension 2 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa LA 01/03/13 Suspension 2 Alcohol SW-846-8015C 67561 Methanol 18.4

Formosa LA 01/03/13 Suspension 2 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.18

Formosa LA 01/03/13 Suspension 2 Aldehyde SW-846-8315A 50000 Formaldehyde 0.02 Non-detect

Formosa LA 01/03/13 Suspension 2 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.02 Non-detect

Formosa LA 01/03/13 Suspension 2 SVOC SW-846-8270D 98862 Acetophenone 4.3

Formosa LA 01/03/13 Suspension 2 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 52

Formosa LA 01/03/13 Suspension 2 SVOC SW-846-8270D 123319 Hydroquinone 0.015 Analyte also detected in method blank.

Formosa LA 01/03/13 Suspension 2 SVOC SW-846-8270D 108952 Phenol 0.005 Non-detect

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0005 Non-detect

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 106990 1,3-butadiene 0.001 Non-detect

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.005 Non-detect

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 126998 Chloroprene 0.025 Non-detect

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Formosa LA 01/03/13 Suspension 2 VC EPA Method 107 75014 Vinyl chloride 0.028

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Formosa LA 01/03/13 Suspension 2 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001 Non-detect

Formosa LA 01/04/13 Suspension 3 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa LA 01/04/13 Suspension 3 Alcohol SW-846-8015C 67561 Methanol 22.5

Formosa LA 01/04/13 Suspension 3 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.18

Formosa LA 01/04/13 Suspension 3 Aldehyde SW-846-8315A 50000 Formaldehyde 0.023

Formosa LA 01/04/13 Suspension 3 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.02 Non-detect

Formosa LA 01/04/13 Suspension 3 SVOC SW-846-8270D 98862 Acetophenone 4

Formosa LA 01/04/13 Suspension 3 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 62

Formosa LA 01/04/13 Suspension 3 SVOC SW-846-8270D 123319 Hydroquinone 0.02 Analyte also detected in method blank.

Formosa LA 01/04/13 Suspension 3 SVOC SW-846-8270D 108952 Phenol 0.005 Non-detect

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0005 Non-detect

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 106990 1,3-butadiene 0.001 Non-detect

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.005 Non-detect

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 126998 Chloroprene 0.025 Non-detect

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Formosa LA 01/04/13 Suspension 3 VC EPA Method 107 75014 Vinyl chloride 0.026

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Formosa LA 01/04/13 Suspension 3 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001 Non-detect

Formosa LA 01/05/13 Suspension 4 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa LA 01/05/13 Suspension 4 Alcohol SW-846-8015C 67561 Methanol 14.8

Formosa LA 01/05/13 Suspension 4 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.77

Formosa LA 01/05/13 Suspension 4 Aldehyde SW-846-8315A 50000 Formaldehyde 0.18

Formosa LA 01/05/13 Suspension 4 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa LA 01/05/13 Suspension 4 SVOC SW-846-8270D 98862 Acetophenone 3.3

Formosa LA 01/05/13 Suspension 4 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 44

Formosa LA 01/05/13 Suspension 4 SVOC SW-846-8270D 123319 Hydroquinone 0.019

Formosa LA 01/05/13 Suspension 4 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Formosa LA 01/05/13 Suspension 4 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0005 Non-detect

Formosa LA 01/05/13 Suspension 4 VOC SW-846-8260B 106990 1,3-butadiene 0.001 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa LA 01/05/13 Suspension4 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.005 Non-detect

Formosa LA 01/05/13 Suspension4 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Formosa LA 01/05/13 Suspension4 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Formosa LA 01/05/13 Suspension4 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa LA 01/05/13 Suspension4 VOC SW-846-8260B 126998 Chloroprene 0.025 Non-detect

Formosa LA 01/05/13 Suspension4 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Formosa LA 01/05/13 Suspension4 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Formosa LA 01/05/13 Suspension4 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Formosa LA 01/05/13 Suspension4 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Formosa LA 01/05/13 Suspension4 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Formosa LA 01/05/13 Suspension4 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa LA 01/05/13 Suspension4 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa LA 01/05/13 Suspension4 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Formosa LA 01/05/13 Suspension4 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Formosa LA 01/05/13 Suspension4 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Formosa LA 01/05/13 Suspension4 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Formosa LA 01/05/13 Suspension4 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Formosa LA 01/05/13 Suspension4 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Formosa LA 01/05/13 Suspension4 VC EPA Method 107 75014 Vinyl chloride 0.018

Formosa LA 01/05/13 Suspension4 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Formosa LA 01/05/13 Suspension4 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001 Non-detect

Formosa LA 01/06/13 Suspension5 Alcohol SW-846-8015C 107211 Ethylene glycol2 Non-detect

Formosa LA 01/06/13 Suspension5 Alcohol SW-846-8015C 67561 Methanol 17.6

Formosa LA 01/06/13 Suspension5 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.5

Formosa LA 01/06/13 Suspension5 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15

Formosa LA 01/06/13 Suspension5 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa LA 01/06/13 Suspension5 SVOC SW-846-8270D 98862 Acetophenone 4.7

Formosa LA 01/06/13 Suspension5 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 19

Formosa LA 01/06/13 Suspension5 SVOC SW-846-8270D 123319 Hydroquinone 0.039

Formosa LA 01/06/13 Suspension5 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0005 Non-detect

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 106990 1,3-butadiene 0.001 Non-detect

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.005 Non-detect

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 126998 Chloroprene 0.025 Non-detect

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Formosa LA 01/06/13 Suspension5 VC EPA Method 107 75014 Vinyl chloride 0.028

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Formosa LA 01/06/13 Suspension5 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001 Non-detect

Formosa LA 01/07/13 Suspension6 Alcohol SW-846-8015C 107211 Ethylene glycol2 Non-detect

Formosa LA 01/07/13 Suspension6 Alcohol SW-846-8015C 67561 Methanol 14

Formosa LA 01/07/13 Suspension6 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.46

Formosa LA 01/07/13 Suspension6 Aldehyde SW-846-8315A 50000 Formaldehyde 0.11

Formosa LA 01/07/13 Suspension6 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa LA 01/07/13 Suspension6 SVOC SW-846-8270D 98862 Acetophenone 3.6

Formosa LA 01/07/13 Suspension6 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 12

Formosa LA 01/07/13 Suspension6 SVOC SW-846-8270D 123319 Hydroquinone 0.02

Formosa LA 01/07/13 Suspension6 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0005 Non-detect

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 106990 1,3-butadiene 0.001 Non-detect

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.005 Non-detect

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 126998 Chloroprene 0.025 Non-detect

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Formosa LA 01/07/13 Suspension6 VC EPA Method 107 75014 Vinyl chloride 0.020

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Formosa LA 01/07/13 Suspension6 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001 Non-detect

Formosa LA 01/08/13 Suspension7 Alcohol SW-846-8015C 107211 Ethylene glycol2 Non-detect

Formosa LA 01/08/13 Suspension7 Alcohol SW-846-8015C 67561 Methanol 18.1

Formosa LA 01/08/13 Suspension7 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.79

Formosa LA 01/08/13 Suspension7 Aldehyde SW-846-8315A 50000 Formaldehyde 0.29

Formosa LA 01/08/13 Suspension7 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa LA 01/08/13 Suspension7 SVOC SW-846-8270D 98862 Acetophenone 0.98

Formosa LA 01/08/13 Suspension7 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 27

Formosa LA 01/08/13 Suspension7 SVOC SW-846-8270D 123319 Hydroquinone 0.033

Formosa LA 01/08/13 Suspension7 SVOC SW-846-8270D 108952 Phenol 0.025 Non-detect

Formosa LA 01/08/13 Suspension7 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0005 Non-detect

Formosa LA 01/08/13 Suspension7 VOC SW-846-8260B 106990 1,3-butadiene 0.001 Non-detect

Formosa LA 01/08/13 Suspension7 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.005 Non-detect

Formosa LA 01/08/13 Suspension7 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Formosa LA 01/08/13 Suspension7 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Formosa LA 01/08/13 Suspension7 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa LA 01/08/13 Suspension7 VOC SW-846-8260B 126998 Chloroprene 0.025 Non-detect

Formosa LA 01/08/13 Suspension7 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Formosa LA 01/08/13 Suspension7 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

12/12/2013 VI Confidential 79 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa LA 01/08/13 Suspension 7 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Formosa LA 01/08/13 Suspension 7 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Formosa LA 01/08/13 Suspension 7 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Formosa LA 01/08/13 Suspension 7 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa LA 01/08/13 Suspension 7 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa LA 01/08/13 Suspension 7 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Formosa LA 01/08/13 Suspension 7 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Formosa LA 01/08/13 Suspension 7 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Formosa LA 01/08/13 Suspension 7 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Formosa LA 01/08/13 Suspension 7 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Formosa LA 01/08/13 Suspension 7 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Formosa LA 01/08/13 Suspension 7 VC EPA Method 107 75014 Vinyl chloride 0.026

Formosa LA 01/08/13 Suspension 7 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Formosa LA 01/08/13 Suspension 7 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001 Non-detect

Formosa LA 01/09/13 Suspension 8 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa LA 01/09/13 Suspension 8 Alcohol SW-846-8015C 67561 Methanol 17.4

Formosa LA 01/09/13 Suspension 8 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.8

Formosa LA 01/09/13 Suspension 8 Aldehyde SW-846-8315A 50000 Formaldehyde 0.028

Formosa LA 01/09/13 Suspension 8 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1 Non-detect

Formosa LA 01/09/13 Suspension 8 SVOC SW-846-8270D 98862 Acetophenone 0.85

Formosa LA 01/09/13 Suspension 8 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 17

Formosa LA 01/09/13 Suspension 8 SVOC SW-846-8270D 123319 Hydroquinone 0.034 Analyte also detected in method blank.

Formosa LA 01/09/13 Suspension 8 SVOC SW-846-8270D 108952 Phenol 0.25 Non-detect

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0005 Non-detect

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 106990 1,3-butadiene 0.001 Non-detect

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.005 Non-detect

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 126998 Chloroprene 0.025 Non-detect

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0033

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Formosa LA 01/09/13 Suspension 8 VC EPA Method 107 75014 Vinyl chloride 0.035

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Formosa LA 01/09/13 Suspension 8 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001 Non-detect

Formosa LA 01/10/13 Suspension 9 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa LA 01/10/13 Suspension 9 Alcohol SW-846-8015C 67561 Methanol 17.4

Formosa LA 01/10/13 Suspension 9 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.6

Formosa LA 01/10/13 Suspension 9 Aldehyde SW-846-8315A 50000 Formaldehyde 0.064

Formosa LA 01/10/13 Suspension 9 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1 Non-detect

Formosa LA 01/10/13 Suspension 9 SVOC SW-846-8270D 98862 Acetophenone 12

Formosa LA 01/10/13 Suspension 9 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 4.6

Formosa LA 01/10/13 Suspension 9 SVOC SW-846-8270D 123319 Hydroquinone 0.5 Non-detect

Formosa LA 01/10/13 Suspension 9 SVOC SW-846-8270D 108952 Phenol 0.25 Non-detect

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0005 Non-detect

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 106990 1,3-butadiene 0.001 Non-detect

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.005 Non-detect

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 126998 Chloroprene 0.025 Non-detect

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.022

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Formosa LA 01/10/13 Suspension 9 VC EPA Method 107 75014 Vinyl chloride 0.046

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Formosa LA 01/10/13 Suspension 9 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001 Non-detect

Formosa LA 01/11/13 Suspension 10 Alcohol SW-846-8015C 107211 Ethylene glycol 2

Formosa LA 01/11/13 Suspension 10 Alcohol SW-846-8015C 67561 Methanol 20.9

Formosa LA 01/11/13 Suspension 10 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.96

Formosa LA 01/11/13 Suspension 10 Aldehyde SW-846-8315A 50000 Formaldehyde 0.02 Non-detect

Formosa LA 01/11/13 Suspension 10 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1 Non-detect

Formosa LA 01/11/13 Suspension 10 SVOC SW-846-8270D 98862 Acetophenone 70

Formosa LA 01/11/13 Suspension 10 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 9

Formosa LA 01/11/13 Suspension 10 SVOC SW-846-8270D 123319 Hydroquinone 0.5 Non-detect

Formosa LA 01/11/13 Suspension 10 SVOC SW-846-8270D 108952 Phenol 0.25 Non-detect

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.025 Non-detect

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 106990 1,3-butadiene 0.05 Non-detect

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.25 Non-detect

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 71432 Benzene 0.07

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 108907 Chlorobenzene 0.05 Non-detect

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 67663 Chloroform 0.079

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 126998 Chloroprene 1.2 Non-detect

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 98828 Cumene 0.05 Non-detect

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.05 Non-detect

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 100414 Ethylbenzene 0.05 Non-detect

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.05 Non-detect

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.05 Non-detect

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.05 Non-detect

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 75092 Methylene chloride 0.5 Non-detect

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 110543 n-Hexane 0.1 Non-detect

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 108883 Toluene 0.05 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.05 Non-detect

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.05 Non-detect

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 108054 Vinyl acetate 0.05 Non-detect

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 593602 Vinyl bromide 0.1 Non-detect

Formosa LA 01/11/13 Suspension 10 VC EPA Method 107 75014 Vinyl chloride 0.038

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.05 Non-detect

Formosa LA 01/11/13 Suspension 10 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.05 Non-detect

Formosa LA 01/12/13 Suspension 11 Alcohol SW-846-8015C 107211 Ethylene glycol2 Non-detect

Formosa LA 01/12/13 Suspension 11 Alcohol SW-846-8015C 67561 Methanol 24.2

Formosa LA 01/12/13 Suspension 11 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.9

Formosa LA 01/12/13 Suspension 11 Aldehyde SW-846-8315A 50000 Formaldehyde 0.2 Non-detect

Formosa LA 01/12/13 Suspension 11 SVOC SW-846-8270D 51285 2,4-dinitrophenol1 Non-detect

Formosa LA 01/12/13 Suspension 11 SVOC SW-846-8270D 98862 Acetophenone5

Formosa LA 01/12/13 Suspension 11 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 3.5

Formosa LA 01/12/13 Suspension 11 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Formosa LA 01/12/13 Suspension 11 SVOC SW-846-8270D 108952 Phenol 0.25 Non-detect

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0005 Non-detect

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 106990 1,3-butadiene 0.001 Non-detect

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.005 Non-detect

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 126998 Chloroprene 0.025 Non-detect

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Formosa LA 01/12/13 Suspension 11 VC EPA Method 107 75014 Vinyl chloride 0.017

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Formosa LA 01/12/13 Suspension 11 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001 Non-detect

Formosa LA 01/13/13 Suspension 12 Alcohol SW-846-8015C 107211 Ethylene glycol2 Non-detect

Formosa LA 01/13/13 Suspension 12 Alcohol SW-846-8015C 67561 Methanol 21.7

Formosa LA 01/13/13 Suspension 12 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.2

Formosa LA 01/13/13 Suspension 12 Aldehyde SW-846-8315A 50000 Formaldehyde 0.2 Non-detect

Formosa LA 01/13/13 Suspension 12 SVOC SW-846-8270D 51285 2,4-dinitrophenol1 Non-detect

Formosa LA 01/13/13 Suspension 12 SVOC SW-846-8270D 98862 Acetophenone 6.8

Formosa LA 01/13/13 Suspension 12 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 1.4

Formosa LA 01/13/13 Suspension 12 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Formosa LA 01/13/13 Suspension 12 SVOC SW-846-8270D 108952 Phenol 0.25 Non-detect

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0005 Non-detect

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 106990 1,3-butadiene 0.001 Non-detect

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.005 Non-detect

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 126998 Chloroprene 0.025 Non-detect

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Formosa LA 01/13/13 Suspension 12 VC EPA Method 107 75014 Vinyl chloride 0.101

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Formosa LA 01/13/13 Suspension 12 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001 Non-detect

Formosa LA 01/14/13 Suspension 13 Alcohol SW-846-8015C 107211 Ethylene glycol2 Non-detect

Formosa LA 01/14/13 Suspension 13 Alcohol SW-846-8015C 67561 Methanol 21.2

Formosa LA 01/14/13 Suspension 13 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.1

Formosa LA 01/14/13 Suspension 13 Aldehyde SW-846-8315A 50000 Formaldehyde 0.025

Formosa LA 01/14/13 Suspension 13 SVOC SW-846-8270D 51285 2,4-dinitrophenol1 Non-detect

Formosa LA 01/14/13 Suspension 13 SVOC SW-846-8270D 98862 Acetophenone 3.8

Formosa LA 01/14/13 Suspension 13 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 2.3

Formosa LA 01/14/13 Suspension 13 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Formosa LA 01/14/13 Suspension 13 SVOC SW-846-8270D 108952 Phenol 0.25 Non-detect

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0005 Non-detect

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 106990 1,3-butadiene 0.001 Non-detect

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.005 Non-detect

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 126998 Chloroprene 0.025 Non-detect

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 98828 Cumene 0.003

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.033

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0031

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Formosa LA 01/14/13 Suspension 13 VC EPA Method 107 75014 Vinyl chloride 0.036

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Formosa LA 01/14/13 Suspension 13 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa LA 01/15/13 Suspension 14 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa LA 01/15/13 Suspension 14 Alcohol SW-846-8015C 67561 Methanol 23.9

Formosa LA 01/15/13 Suspension 14 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.52

Formosa LA 01/15/13 Suspension 14 Aldehyde SW-846-8315A 50000 Formaldehyde 0.05

Formosa LA 01/15/13 Suspension 14 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa LA 01/15/13 Suspension 14 SVOC SW-846-8270D 98862 Acetophenone 5.8

Formosa LA 01/15/13 Suspension 14 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 3.7

Formosa LA 01/15/13 Suspension 14 SVOC SW-846-8270D 123319 Hydroquinone 0.99

Formosa LA 01/15/13 Suspension 14 SVOC SW-846-8270D 108952 Phenol 0.25 Non-detect

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00038 Non-detect

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 106990 1,3-butadiene 0.00012 Non-detect

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00017 Non-detect

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 71432 Benzene 0.00021 Non-detect

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 108907 Chlorobenzene 0.00036 Non-detect

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 67663 Chloroform 0.00036 Non-detect

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 126998 Chloroprene 0.00068 Non-detect

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 98828 Cumene 0.0003 Estimated value between MDL and PQL

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0029

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 100414 Ethylbenzene 0.0002 Non-detect

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00034 Non-detect

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00029 Non-detect

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00036 Non-detect

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 75092 Methylene chloride 0.00081 Non-detect

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 110543 n-Hexane 0.00081 Non-detect

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 108883 Toluene 0.0003 Estimated value between MDL and PQL

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00025 Non-detect

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 108054 Vinyl acetate 0.00033 Non-detect

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 593602 Vinyl bromide 0.00029 Non-detect

Formosa LA 01/15/13 Suspension 14 VC EPA Method 107 75014 Vinyl chloride 0.020

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00041 Non-detect

Formosa LA 01/15/13 Suspension 14 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0002 Non-detect

Formosa LA 01/16/13 Suspension 15 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa LA 01/16/13 Suspension 15 Alcohol SW-846-8015C 67561 Methanol 20.1

Formosa LA 01/16/13 Suspension 15 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.4

Formosa LA 01/16/13 Suspension 15 Aldehyde SW-846-8315A 50000 Formaldehyde 0.057

Formosa LA 01/16/13 Suspension 15 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1 Non-detect

Formosa LA 01/16/13 Suspension 15 SVOC SW-846-8270D 98862 Acetophenone 2.5

Formosa LA 01/16/13 Suspension 15 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 1.6

Formosa LA 01/16/13 Suspension 15 SVOC SW-846-8270D 123319 Hydroquinone 0.21

Formosa LA 01/16/13 Suspension 15 SVOC SW-846-8270D 108952 Phenol 0.25 Non-detect

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0005 Non-detect

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 106990 1,3-butadiene 0.001 Non-detect

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.005 Non-detect

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 126998 Chloroprene 0.025 Non-detect

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Formosa LA 01/16/13 Suspension 15 VC EPA Method 107 75014 Vinyl chloride 0.020

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Formosa LA 01/16/13 Suspension 15 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001 Non-detect

Formosa LA 01/17/13 Suspension 16 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa LA 01/17/13 Suspension 16 Alcohol SW-846-8015C 67561 Methanol 23.5

Formosa LA 01/17/13 Suspension 16 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.19

Formosa LA 01/17/13 Suspension 16 Aldehyde SW-846-8315A 50000 Formaldehyde 0.23

Formosa LA 01/17/13 Suspension 16 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1 Non-detect

Formosa LA 01/17/13 Suspension 16 SVOC SW-846-8270D 98862 Acetophenone 2.7

Formosa LA 01/17/13 Suspension 16 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 5.4

Formosa LA 01/17/13 Suspension 16 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Formosa LA 01/17/13 Suspension 16 SVOC SW-846-8270D 108952 Phenol 0.25 Non-detect

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0025 Non-detect

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 106990 1,3-butadiene 0.005 Non-detect

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.025 Non-detect

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 71432 Benzene 0.005 Non-detect

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 108907 Chlorobenzene 0.005 Non-detect

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 67663 Chloroform 0.005 Non-detect

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 126998 Chloroprene 0.12 Non-detect

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 98828 Cumene 0.005 Non-detect

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.005 Non-detect

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 100414 Ethylbenzene 0.005 Non-detect

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.005 Non-detect

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.005 Non-detect

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.005 Non-detect

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 75092 Methylene chloride 0.05 Non-detect

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 110543 n-Hexane 0.01 Non-detect

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 108883 Toluene 0.005 Non-detect

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.005 Non-detect

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.005 Non-detect

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 108054 Vinyl acetate 0.005 Non-detect

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 593602 Vinyl bromide 0.01 Non-detect

Formosa LA 01/17/13 Suspension 16 VC EPA Method 107 75014 Vinyl chloride 0.013

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.005 Non-detect

Formosa LA 01/17/13 Suspension 16 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0075 Estimated value between MDL and PQL

Formosa LA 01/18/13 Suspension 17 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa LA 01/18/13 Suspension 17 Alcohol SW-846-8015C 67561 Methanol 21.7

Formosa LA 01/18/13 Suspension 17 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.4

Formosa LA 01/18/13 Suspension 17 Aldehyde SW-846-8315A 50000 Formaldehyde 0.18

Formosa LA 01/18/13 Suspension 17 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1 Non-detect

Formosa LA 01/18/13 Suspension 17 SVOC SW-846-8270D 98862 Acetophenone 1.9

Formosa LA 01/18/13 Suspension 17 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 9.2

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa LA 01/18/13 Suspension 17 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Formosa LA 01/18/13 Suspension 17 SVOC SW-846-8270D 108952 Phenol 0.25 Non-detect

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0005 Non-detect

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 106990 1,3-butadiene 0.001 Non-detect

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.005 Non-detect

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 126998 Chloroprene 0.025 Non-detect

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0019

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Formosa LA 01/18/13 Suspension 17 VC EPA Method 107 75014 Vinyl chloride 0.021

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Formosa LA 01/18/13 Suspension 17 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001 Non-detect

Formosa LA 01/19/13 Suspension 18 Alcohol SW-846-8015C 107211 Ethylene glycol 4.9

Formosa LA 01/19/13 Suspension 18 Alcohol SW-846-8015C 67561 Methanol 37.1

Formosa LA 01/19/13 Suspension 18 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.4

Formosa LA 01/19/13 Suspension 18 Aldehyde SW-846-8315A 50000 Formaldehyde 0.065

Formosa LA 01/19/13 Suspension 18 SVOC SW-846-8270D 51285 2,4-dinitrophenol1 Non-detect

Formosa LA 01/19/13 Suspension 18 SVOC SW-846-8270D 98862 Acetophenone 18

Formosa LA 01/19/13 Suspension 18 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 1.9

Formosa LA 01/19/13 Suspension 18 SVOC SW-846-8270D 123319 Hydroquinone 0.7

Formosa LA 01/19/13 Suspension 18 SVOC SW-846-8270D 108952 Phenol 0.25 Non-detect

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.025 Non-detect

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 106990 1,3-butadiene 0.05 Non-detect

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.25 Non-detect

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 71432 Benzene 0.05 Non-detect

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 108907 Chlorobenzene 0.05 Non-detect

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 67663 Chloroform 0.5 Non-detect

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 126998 Chloroprene 1.2 Non-detect

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 98828 Cumene 0.05 Non-detect

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.05 Non-detect

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 100414 Ethylbenzene 0.05 Non-detect

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.05 Non-detect

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.05 Non-detect

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.05 Non-detect

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 75092 Methylene chloride 0.5 Non-detect

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 110543 n-Hexane 0.1 Non-detect

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 108883 Toluene 0.05 Non-detect

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.05 Non-detect

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.05 Non-detect

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 108054 Vinyl acetate 0.05 Non-detect

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 593602 Vinyl bromide 0.1 Non-detect

Formosa LA 01/19/13 Suspension 18 VC EPA Method 107 75014 Vinyl chloride 0.077

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.05 Non-detect

Formosa LA 01/19/13 Suspension 18 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.05 Non-detect

Formosa LA 01/20/13 Suspension 19 Alcohol SW-846-8015C 107211 Ethylene glycol 5.6

Formosa LA 01/20/13 Suspension 19 Alcohol SW-846-8015C 67561 Methanol 24.2

Formosa LA 01/20/13 Suspension 19 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.76

Formosa LA 01/20/13 Suspension 19 Aldehyde SW-846-8315A 50000 Formaldehyde 0.023

Formosa LA 01/20/13 Suspension 19 SVOC SW-846-8270D 51285 2,4-dinitrophenol1 Non-detect

Formosa LA 01/20/13 Suspension 19 SVOC SW-846-8270D 98862 Acetophenone 14

Formosa LA 01/20/13 Suspension 19 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 3.1

Formosa LA 01/20/13 Suspension 19 SVOC SW-846-8270D 123319 Hydroquinone 1.9

Formosa LA 01/20/13 Suspension 19 SVOC SW-846-8270D 108952 Phenol 0.25 Non-detect

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.025 Non-detect

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 106990 1,3-butadiene 0.05 Non-detect

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.25 Non-detect

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 71432 Benzene 0.05 Non-detect

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 108907 Chlorobenzene 0.05 Non-detect

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 67663 Chloroform 0.05 Non-detect

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 126998 Chloroprene 1.2 Non-detect

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 98828 Cumene 0.05 Non-detect

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.05 Non-detect

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 100414 Ethylbenzene 0.05 Non-detect

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.05 Non-detect

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.05 Non-detect

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.05 Non-detect

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 75092 Methylene chloride 0.5 Non-detect

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 110543 n-Hexane 0.1 Non-detect

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 108883 Toluene 0.05 Non-detect

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.05 Non-detect

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.05 Non-detect

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 108054 Vinyl acetate 0.05 Non-detect

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 593602 Vinyl bromide 0.1 Non-detect

Formosa LA 01/20/13 Suspension 19 VC EPA Method 107 75014 Vinyl chloride 0.025

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.05 Non-detect

Formosa LA 01/20/13 Suspension 19 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.05 Non-detect

Formosa LA 01/21/13 Suspension 20 Alcohol SW-846-8015C 107211 Ethylene glycol2 Non-detect

Formosa LA 01/21/13 Suspension 20 Alcohol SW-846-8015C 67561 Methanol 19.8

Formosa LA 01/21/13 Suspension 20 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.1

Formosa LA 01/21/13 Suspension 20 Aldehyde SW-846-8315A 50000 Formaldehyde 0.064

Formosa LA 01/21/13 Suspension 20 SVOC SW-846-8270D 51285 2,4-dinitrophenol1 Non-detect

Formosa LA 01/21/13 Suspension 20 SVOC SW-846-8270D 98862 Acetophenone3

Formosa LA 01/21/13 Suspension 20 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 4.2

Formosa LA 01/21/13 Suspension 20 SVOC SW-846-8270D 123319 Hydroquinone 0.17

Formosa LA 01/21/13 Suspension 20 SVOC SW-846-8270D 108952 Phenol 0.25 Non-detect

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0025 Non-detect

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 106990 1,3-butadiene 0.005 Non-detect

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.025 Non-detect

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 71432 Benzene 0.005 Non-detect

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 108907 Chlorobenzene 0.005 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 67663 Chloroform 0.005 Non-detect

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 126998 Chloroprene 0.12 Non-detect

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 98828 Cumene 0.005 Non-detect

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.005 Non-detect

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 100414 Ethylbenzene 0.005 Non-detect

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.005 Non-detect

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.005 Non-detect

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.005 Non-detect

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 75092 Methylene chloride 0.05 Non-detect

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 110543 n-Hexane 0.01 Non-detect

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 108883 Toluene 0.005 Non-detect

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.005 Non-detect

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.005 Non-detect

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 108054 Vinyl acetate 0.005 Non-detect

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 593602 Vinyl bromide 0.01 Non-detect

Formosa LA 01/21/13 Suspension 20 VC EPA Method 107 75014 Vinyl chloride 0.039

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.005 Non-detect

Formosa LA 01/21/13 Suspension 20 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.005 Non-detect

Formosa LA 01/22/13 Suspension 21 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa LA 01/22/13 Suspension 21 Alcohol SW-846-8015C 67561 Methanol 18.9

Formosa LA 01/22/13 Suspension 21 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.7

Formosa LA 01/22/13 Suspension 21 Aldehyde SW-846-8315A 50000 Formaldehyde 0.16 Analyte also detected in method blank.

Formosa LA 01/22/13 Suspension 21 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa LA 01/22/13 Suspension 21 SVOC SW-846-8270D 98862 Acetophenone 7.7

Formosa LA 01/22/13 Suspension 21 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 1.1

Formosa LA 01/22/13 Suspension 21 SVOC SW-846-8270D 123319 Hydroquinone 1.6

Formosa LA 01/22/13 Suspension 21 SVOC SW-846-8270D 108952 Phenol 0.003 Non-detect

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0038 Non-detect

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 106990 1,3-butadiene 0.0012 Non-detect

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0017 Non-detect

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 71432 Benzene 0.0021 Non-detect

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 108907 Chlorobenzene 0.0036 Non-detect

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 67663 Chloroform 0.0036 Non-detect

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 126998 Chloroprene 0.0068 Non-detect

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 98828 Cumene 0.0023 Non-detect

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0066

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0034 Non-detect

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0029 Non-detect

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0036 Non-detect

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 75092 Methylene chloride 0.0081 Non-detect

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 110543 n-Hexane 0.0081 Non-detect

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 108883 Toluene 0.0027 Non-detect

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0025 Non-detect

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 108054 Vinyl acetate 0.0033 Non-detect

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 593602 Vinyl bromide 0.0029 Non-detect

Formosa LA 01/22/13 Suspension 21 VC EPA Method 107 75014 Vinyl chloride 0.070

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0041 Non-detect

Formosa LA 01/22/13 Suspension 21 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Formosa LA 01/23/13 Suspension 22 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa LA 01/23/13 Suspension 22 Alcohol SW-846-8015C 67561 Methanol 23

Formosa LA 01/23/13 Suspension 22 Aldehyde SW-846-8315A 75070 Acetaldehyde 10

Formosa LA 01/23/13 Suspension 22 Aldehyde SW-846-8315A 50000 Formaldehyde 0.5 Non-detect

Formosa LA 01/23/13 Suspension 22 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1 Non-detect

Formosa LA 01/23/13 Suspension 22 SVOC SW-846-8270D 98862 Acetophenone 11

Formosa LA 01/23/13 Suspension 22 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.84

Formosa LA 01/23/13 Suspension 22 SVOC SW-846-8270D 123319 Hydroquinone 0.19

Formosa LA 01/23/13 Suspension 22 SVOC SW-846-8270D 108952 Phenol 0.25 Non-detect

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0005 Non-detect

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 106990 1,3-butadiene 0.001 Non-detect

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.005 Non-detect

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 126998 Chloroprene 0.025 Non-detect

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0038

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0011

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Formosa LA 01/23/13 Suspension 22 VC EPA Method 107 75014 Vinyl chloride 0.065

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Formosa LA 01/23/13 Suspension 22 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001 Non-detect

Formosa LA 01/24/13 Suspension 23 Alcohol SW-846-8015C 107211 Ethylene glycol 2.7

Formosa LA 01/24/13 Suspension 23 Alcohol SW-846-8015C 67561 Methanol 16.7

Formosa LA 01/24/13 Suspension 23 Aldehyde SW-846-8315A 75070 Acetaldehyde 1

Formosa LA 01/24/13 Suspension 23 Aldehyde SW-846-8315A 50000 Formaldehyde 0.02 Non-detect

Formosa LA 01/24/13 Suspension 23 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1 Non-detect

Formosa LA 01/24/13 Suspension 23 SVOC SW-846-8270D 98862 Acetophenone 3

Formosa LA 01/24/13 Suspension 23 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.96

Formosa LA 01/24/13 Suspension 23 SVOC SW-846-8270D 123319 Hydroquinone 1.6

Formosa LA 01/24/13 Suspension 23 SVOC SW-846-8270D 108952 Phenol 0.25 Non-detect

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0005 Non-detect

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 106990 1,3-butadiene 0.001 Non-detect

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.005 Non-detect

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 126998 Chloroprene 0.025 Non-detect

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Formosa LA 01/24/13 Suspension 23 VC EPA Method 107 75014 Vinyl chloride 0.023

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Formosa LA 01/24/13 Suspension 23 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001 Non-detect

Formosa LA 01/25/13 Suspension 24 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa LA 01/25/13 Suspension 24 Alcohol SW-846-8015C 67561 Methanol 13.5

Formosa LA 01/25/13 Suspension 24 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.94

Formosa LA 01/25/13 Suspension 24 Aldehyde SW-846-8315A 50000 Formaldehyde 0.062

Formosa LA 01/25/13 Suspension 24 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1 Non-detect

Formosa LA 01/25/13 Suspension 24 SVOC SW-846-8270D 98862 Acetophenone 1.9

Formosa LA 01/25/13 Suspension 24 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.41

Formosa LA 01/25/13 Suspension 24 SVOC SW-846-8270D 123319 Hydroquinone 2.9

Formosa LA 01/25/13 Suspension 24 SVOC SW-846-8270D 108952 Phenol 0.25 Non-detect

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0005 Non-detect

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 106990 1,3-butadiene 0.001 Non-detect

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.005 Non-detect

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 126998 Chloroprene 0.025 Non-detect

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.001 Non-detect

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Formosa LA 01/25/13 Suspension 24 VC EPA Method 107 75014 Vinyl chloride 0.011

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Formosa LA 01/25/13 Suspension 24 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001 Non-detect

Formosa LA 01/26/13 Suspension 25 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa LA 01/26/13 Suspension 25 Alcohol SW-846-8015C 67561 Methanol 10.7

Formosa LA 01/26/13 Suspension 25 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.2 Analyte also detected in method blank.

Formosa LA 01/26/13 Suspension 25 Aldehyde SW-846-8315A 50000 Formaldehyde 0.096

Formosa LA 01/26/13 Suspension 25 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1 Non-detect

Formosa LA 01/26/13 Suspension 25 SVOC SW-846-8270D 98862 Acetophenone 1.4

Formosa LA 01/26/13 Suspension 25 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.51

Formosa LA 01/26/13 Suspension 25 SVOC SW-846-8270D 123319 Hydroquinone 1.1

Formosa LA 01/26/13 Suspension 25 SVOC SW-846-8270D 108952 Phenol 0.25 Non-detect

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0005 Non-detect

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 106990 1,3-butadiene 0.001 Non-detect

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.005 Non-detect

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 126998 Chloroprene 0.025 Non-detect

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0011

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Formosa LA 01/26/13 Suspension 25 VC EPA Method 107 75014 Vinyl chloride 0.032

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Formosa LA 01/26/13 Suspension 25 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001 Non-detect

Formosa LA 01/27/13 Suspension 26 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa LA 01/27/13 Suspension 26 Alcohol SW-846-8015C 67561 Methanol 19

Formosa LA 01/27/13 Suspension 26 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.2 Analyte also detected in method blank.

Formosa LA 01/27/13 Suspension 26 Aldehyde SW-846-8315A 50000 Formaldehyde 0.5 Non-detect

Formosa LA 01/27/13 Suspension 26 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1 Non-detect

Formosa LA 01/27/13 Suspension 26 SVOC SW-846-8270D 98862 Acetophenone 4.8

Formosa LA 01/27/13 Suspension 26 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Formosa LA 01/27/13 Suspension 26 SVOC SW-846-8270D 123319 Hydroquinone 2

Formosa LA 01/27/13 Suspension 26 SVOC SW-846-8270D 108952 Phenol 0.25 Non-detect

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.025 Non-detect

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 106990 1,3-butadiene 0.05 Non-detect

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.25 Non-detect

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 71432 Benzene 0.05 Non-detect

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 108907 Chlorobenzene 0.05 Non-detect

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 67663 Chloroform 0.05 Non-detect

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 126998 Chloroprene 1.2 Non-detect

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 98828 Cumene 0.05 Non-detect

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.05 Non-detect

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 100414 Ethylbenzene 0.05 Non-detect

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.05 Non-detect

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.05 Non-detect

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.05 Non-detect

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 75092 Methylene chloride 0.5 Non-detect

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 110543 n-Hexane 0.1 Non-detect

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 108883 Toluene 0.05 Non-detect

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.05 Non-detect

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.05 Non-detect

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 108054 Vinyl acetate 0.05 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 593602 Vinyl bromide 0.1 Non-detect

Formosa LA 01/27/13 Suspension 26 VC EPA Method 107 75014 Vinyl chloride 0.021

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.05 Non-detect

Formosa LA 01/27/13 Suspension 26 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.05 Non-detect

Formosa LA 01/28/13 Suspension 27 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa LA 01/28/13 Suspension 27 Alcohol SW-846-8015C 67561 Methanol 12.2

Formosa LA 01/28/13 Suspension 27 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.1 Analyte also detected in method blank.

Formosa LA 01/28/13 Suspension 27 Aldehyde SW-846-8315A 50000 Formaldehyde 0.1 Non-detect

Formosa LA 01/28/13 Suspension 27 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1 Non-detect

Formosa LA 01/28/13 Suspension 27 SVOC SW-846-8270D 98862 Acetophenone 1.2

Formosa LA 01/28/13 Suspension 27 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.42

Formosa LA 01/28/13 Suspension 27 SVOC SW-846-8270D 123319 Hydroquinone 0.1 Non-detect

Formosa LA 01/28/13 Suspension 27 SVOC SW-846-8270D 108952 Phenol 0.25 Non-detect

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0005 Non-detect

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 106990 1,3-butadiene 0.001 Non-detect

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.005 Non-detect

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 126998 Chloroprene 0.025 Non-detect

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0014

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Formosa LA 01/28/13 Suspension 27 VC EPA Method 107 75014 Vinyl chloride 0.019

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Formosa LA 01/28/13 Suspension 27 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001 Non-detect

Formosa LA 01/29/13 Suspension 28 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa LA 01/29/13 Suspension 28 Alcohol SW-846-8015C 67561 Methanol 19.3

Formosa LA 01/29/13 Suspension 28 Aldehyde SW-846-8315A 75070 Acetaldehyde 8.3

Formosa LA 01/29/13 Suspension 28 Aldehyde SW-846-8315A 50000 Formaldehyde 0.15 Estimated value between MDL and PQL

Formosa LA 01/29/13 Suspension 28 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa LA 01/29/13 Suspension 28 SVOC SW-846-8270D 98862 Acetophenone 4.2

Formosa LA 01/29/13 Suspension 28 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.19 Estimated value between MDL and PQL

Formosa LA 01/29/13 Suspension 28 SVOC SW-846-8270D 123319 Hydroquinone 1.3

Formosa LA 01/29/13 Suspension 28 SVOC SW-846-8270D 108952 Phenol 0.003 Non-detect

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0038 Non-detect

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 106990 1,3-butadiene 0.0012 Non-detect

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0017 Non-detect

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 71432 Benzene 0.0021 Non-detect

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 108907 Chlorobenzene 0.0036 Non-detect

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 67663 Chloroform 0.0036 Non-detect

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 126998 Chloroprene 0.0068 Non-detect

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 98828 Cumene 0.0023 Non-detect

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.14

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 100414 Ethylbenzene 0.002 Non-detect

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0034 Non-detect

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0029 Non-detect

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.01

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 75092 Methylene chloride 0.0081 Non-detect

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 110543 n-Hexane 0.0081 Non-detect

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 108883 Toluene 0.0027 Non-detect

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0025 Non-detect

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 108054 Vinyl acetate 0.0033 Non-detect

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 593602 Vinyl bromide 0.0029 Non-detect

Formosa LA 01/29/13 Suspension 28 VC EPA Method 107 75014 Vinyl chloride 0.204

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0041 Non-detect

Formosa LA 01/29/13 Suspension 28 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.002 Non-detect

Formosa LA 01/30/13 Suspension 29 Alcohol SW-846-8015C 107211 Ethylene glycol 2.1

Formosa LA 01/30/13 Suspension 29 Alcohol SW-846-8015C 67561 Methanol 20.1

Formosa LA 01/30/13 Suspension 29 Aldehyde SW-846-8315A 75070 Acetaldehyde 35

Formosa LA 01/30/13 Suspension 29 Aldehyde SW-846-8315A 50000 Formaldehyde 0.5 Non-detect

Formosa LA 01/30/13 Suspension 29 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1 Non-detect

Formosa LA 01/30/13 Suspension 29 SVOC SW-846-8270D 98862 Acetophenone 4.6

Formosa LA 01/30/13 Suspension 29 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Formosa LA 01/30/13 Suspension 29 SVOC SW-846-8270D 123319 Hydroquinone 2

Formosa LA 01/30/13 Suspension 29 SVOC SW-846-8270D 108952 Phenol 0.25 Non-detect

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.025 Non-detect

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 106990 1,3-butadiene 0.05 Non-detect

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.25

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 71432 Benzene 0.05 Non-detect

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 108907 Chlorobenzene 0.05 Non-detect

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 67663 Chloroform 0.05 Non-detect

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 126998 Chloroprene 1.2 Non-detect

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 98828 Cumene 0.05 Non-detect

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.05 Non-detect

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 100414 Ethylbenzene 0.05 Non-detect

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.05 Non-detect

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.05 Non-detect

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.05 Non-detect

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 75092 Methylene chloride 0.5 Non-detect

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 110543 n-Hexane 0.1 Non-detect

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 108883 Toluene 0.05 Non-detect

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.05 Non-detect

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.05 Non-detect

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 108054 Vinyl acetate 0.05 Non-detect

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 593602 Vinyl bromide 0.1 Non-detect

Formosa LA 01/30/13 Suspension 29 VC EPA Method 107 75014 Vinyl chloride 0.107

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.05 Non-detect

Formosa LA 01/30/13 Suspension 29 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.05 Non-detect

Formosa LA 01/31/13 Suspension 30 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa LA 01/31/13 Suspension 30 Alcohol SW-846-8015C 67561 Methanol 15.2

Formosa LA 01/31/13 Suspension 30 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.88

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa LA 01/31/13 Suspension 30 Aldehyde SW-846-8315A 50000 Formaldehyde 0.064

Formosa LA 01/31/13 Suspension 30 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1 Non-detect

Formosa LA 01/31/13 Suspension 30 SVOC SW-846-8270D 98862 Acetophenone 4.9

Formosa LA 01/31/13 Suspension 30 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.25 Non-detect

Formosa LA 01/31/13 Suspension 30 SVOC SW-846-8270D 123319 Hydroquinone 0.25

Formosa LA 01/31/13 Suspension 30 SVOC SW-846-8270D 108952 Phenol 0.25 Non-detect

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0005 Non-detect

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 106990 1,3-butadiene 0.001 Non-detect

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.005 Non-detect

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 71432 Benzene 0.001 Non-detect

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 108907 Chlorobenzene 0.001 Non-detect

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 126998 Chloroprene 0.025 Non-detect

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 98828 Cumene 0.001 Non-detect

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0072

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 100414 Ethylbenzene 0.001 Non-detect

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001 Non-detect

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 110543 n-Hexane 0.002 Non-detect

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 108883 Toluene 0.001 Non-detect

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.001 Non-detect

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.001 Non-detect

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 108054 Vinyl acetate 0.001 Non-detect

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 593602 Vinyl bromide 0.002 Non-detect

Formosa LA 01/31/13 Suspension 30 VC EPA Method 107 75014 Vinyl chloride 0.015

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001 Non-detect

Formosa LA 01/31/13 Suspension 30 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001 Non-detect

Westlake KY 01/07/13 Suspension 1 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Y

Westlake KY 01/07/13 Suspension 1 Alcohol SW-846-8015C 67561 Methanol 13.2 N

Westlake KY 01/07/13 Suspension 1 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.275 N U

Westlake KY 01/07/13 Suspension 1 Aldehyde SW-846-8315A 50000 Formaldehyde 0.314 N UJ

Westlake KY 01/07/13 Suspension 1 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Y

Westlake KY 01/07/13 Suspension 1 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Y

Westlake KY 01/07/13 Suspension 1 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Y

Westlake KY 01/07/13 Suspension 1 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Y UJ

Westlake KY 01/07/13 Suspension 1 SVOC SW-846-8270D 108952 Phenol 0.00349 Y

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00046 N

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 71432 Benzene 0.00032 N

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y UJ

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y UJ

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y UJ

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/07/13 Suspension 1 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 01/07/13 Suspension 1 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y UJ, Note (3)

Westlake KY 01/08/13 Suspension 2 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Y

Westlake KY 01/08/13 Suspension 2 Alcohol SW-846-8015C 67561 Methanol 32.6 N

Westlake KY 01/08/13 Suspension 2 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.336 N UJ

Westlake KY 01/08/13 Suspension 2 Aldehyde SW-846-8315A 50000 Formaldehyde 0.39 N J

Westlake KY 01/08/13 Suspension 2 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Y

Westlake KY 01/08/13 Suspension 2 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Y

Westlake KY 01/08/13 Suspension 2 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Y

Westlake KY 01/08/13 Suspension 2 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Y UJ

Westlake KY 01/08/13 Suspension 2 SVOC SW-846-8270D 108952 Phenol 0.0349 Y

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 71432 Benzene 0.00023 N J

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/08/13 Suspension 2 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 01/08/13 Suspension 2 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 01/09/13 Suspension 3 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Y

Westlake KY 01/09/13 Suspension 3 Alcohol SW-846-8015C 67561 Methanol 42.6 N

Westlake KY 01/09/13 Suspension 3 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.236 N UJ

Westlake KY 01/09/13 Suspension 3 Aldehyde SW-846-8315A 50000 Formaldehyde 0.275 N UJ

Westlake KY 01/09/13 Suspension 3 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Y

Westlake KY 01/09/13 Suspension 3 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Y

Westlake KY 01/09/13 Suspension 3 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Y

Westlake KY 01/09/13 Suspension 3 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Y UJ

Westlake KY 01/09/13 Suspension 3 SVOC SW-846-8270D 108952 Phenol 0.0349 Y

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y UJ

12/12/2013 VI Confidential 87 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y UJ

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y UJ

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 71432 Benzene 0.00026 N J

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y UJ

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 67663 Chloroform 0.0001 Y UJ

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y UJ

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 98828 Cumene 0.00005 Y UJ

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y J

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y UJ

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y UJ

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y UJ

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y UJ

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 108883 Toluene 0.00004 Y UJ

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y UJ

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y UJ

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y UJ

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/09/13 Suspension 3 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00012 N

Westlake KY 01/09/13 Suspension 3 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y UJ, Note (3)

Westlake KY 01/10/13 Suspension 4 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Y

Westlake KY 01/10/13 Suspension 4 Alcohol SW-846-8015C 67561 Methanol 48.6 N

Westlake KY 01/10/13 Suspension 4 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.248 N UJ

Westlake KY 01/10/13 Suspension 4 Aldehyde SW-846-8315A 50000 Formaldehyde 0.345 N J

Westlake KY 01/10/13 Suspension 4 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Y

Westlake KY 01/10/13 Suspension 4 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Y

Westlake KY 01/10/13 Suspension 4 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Y

Westlake KY 01/10/13 Suspension 4 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Y UJ

Westlake KY 01/10/13 Suspension 4 SVOC SW-846-8270D 108952 Phenol 0.0349 Y

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00055 N J

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 71432 Benzene 0.00043 N J

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/10/13 Suspension 4 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 01/10/13 Suspension 4 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 01/11/13 Suspension 5 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Y

Westlake KY 01/11/13 Suspension 5 Alcohol SW-846-8015C 67561 Methanol 31.3 N

Westlake KY 01/11/13 Suspension 5 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.62 N UJ

Westlake KY 01/11/13 Suspension 5 Aldehyde SW-846-8315A 50000 Formaldehyde 0.244 N UJ

Westlake KY 01/11/13 Suspension 5 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Y

Westlake KY 01/11/13 Suspension 5 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Y

Westlake KY 01/11/13 Suspension 5 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Y

Westlake KY 01/11/13 Suspension 5 SVOC SW-846-8270D 123319 Hydroquinone 1.08 N JN

Westlake KY 01/11/13 Suspension 5 SVOC SW-846-8270D 108952 Phenol 0.0349 Y

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y UJ

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y UJ

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y UJ

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 71432 Benzene 0.00036 N J

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y UJ

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 67663 Chloroform 0.00025 N UJ

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y UJ

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 98828 Cumene 0.00005 Y UJ

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y J

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y UJ

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y UJ

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y UJ

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y UJ

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 108883 Toluene 0.00004 Y UJ

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y UJ

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y UJ

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y UJ

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/11/13 Suspension 5 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 01/11/13 Suspension 5 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y UJ, Note (3)

Westlake KY 01/12/13 Suspension 6 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Y

Westlake KY 01/12/13 Suspension 6 Alcohol SW-846-8015C 67561 Methanol 74.8 N

Westlake KY 01/12/13 Suspension 6 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.389 N J

Westlake KY 01/12/13 Suspension 6 Aldehyde SW-846-8315A 50000 Formaldehyde 0.299 N J

Westlake KY 01/12/13 Suspension 6 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0595 Y

Westlake KY 01/12/13 Suspension 6 SVOC SW-846-8270D 98862 Acetophenone 0.0706 N J

Westlake KY 01/12/13 Suspension 6 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0973 Y

Westlake KY 01/12/13 Suspension 6 SVOC SW-846-8270D 123319 Hydroquinone 0.03 Y UJ

Westlake KY 01/12/13 Suspension 6 SVOC SW-846-8270D 108952 Phenol 0.0329 Y

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 71432 Benzene 0.00024 N J

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 98828 Cumene 0.00005 Y

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/12/13 Suspension 6 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 01/12/13 Suspension 6 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 01/13/13 Suspension 7 Alcohol SW-846-8015C 107211 Ethylene glycol 7.4 N

Westlake KY 01/13/13 Suspension 7 Alcohol SW-846-8015C 67561 Methanol 15.8 N

Westlake KY 01/13/13 Suspension 7 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.53 N J

Westlake KY 01/13/13 Suspension 7 Aldehyde SW-846-8315A 50000 Formaldehyde 0.181 N UJ

Westlake KY 01/13/13 Suspension 7 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Y

Westlake KY 01/13/13 Suspension 7 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Y

Westlake KY 01/13/13 Suspension 7 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Y

Westlake KY 01/13/13 Suspension 7 SVOC SW-846-8270D 123319 Hydroquinone 0.113 N JN

Westlake KY 01/13/13 Suspension 7 SVOC SW-846-8270D 108952 Phenol 0.00349 Y

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 71432 Benzene 0.0003 N J

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/13/13 Suspension 7 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 01/13/13 Suspension 7 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 01/14/13 Suspension 8 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Y

Westlake KY 01/14/13 Suspension 8 Alcohol SW-846-8015C 67561 Methanol 33.9 N

Westlake KY 01/14/13 Suspension 8 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.617 N J

Westlake KY 01/14/13 Suspension 8 Aldehyde SW-846-8315A 50000 Formaldehyde 0.376 N J

Westlake KY 01/14/13 Suspension 8 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Y

Westlake KY 01/14/13 Suspension 8 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Y

Westlake KY 01/14/13 Suspension 8 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Y

Westlake KY 01/14/13 Suspension 8 SVOC SW-846-8270D 123319 Hydroquinone 0.03 Y UJ

Westlake KY 01/14/13 Suspension 8 SVOC SW-846-8270D 108952 Phenol 0.00349 Y

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 71432 Benzene 0.00039 N J

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/14/13 Suspension 8 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 01/14/13 Suspension 8 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 01/15/13 Suspension 9 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Y

Westlake KY 01/15/13 Suspension 9 Alcohol SW-846-8015C 67561 Methanol 36.9 N

Westlake KY 01/15/13 Suspension 9 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.322 N J

Westlake KY 01/15/13 Suspension 9 Aldehyde SW-846-8315A 50000 Formaldehyde 0.407 N J

Westlake KY 01/15/13 Suspension 9 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00316 Y

Westlake KY 01/15/13 Suspension 9 SVOC SW-846-8270D 98862 Acetophenone 0.00365 Y

Westlake KY 01/15/13 Suspension 9 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00516 Y

Westlake KY 01/15/13 Suspension 9 SVOC SW-846-8270D 123319 Hydroquinone 0.015 Y UJ

Westlake KY 01/15/13 Suspension 9 SVOC SW-846-8270D 108952 Phenol 0.00175 Y

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 71432 Benzene 0.00004 Y

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/15/13 Suspension 9 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 01/15/13 Suspension 9 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 01/16/13 Suspension 10 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Y

Westlake KY 01/16/13 Suspension 10 Alcohol SW-846-8015C 67561 Methanol 29.7 N

Westlake KY 01/16/13 Suspension 10 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.34 N J

Westlake KY 01/16/13 Suspension 10 Aldehyde SW-846-8315A 50000 Formaldehyde 0.467 N J

Westlake KY 01/16/13 Suspension 10 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00316 Y

Westlake KY 01/16/13 Suspension 10 SVOC SW-846-8270D 98862 Acetophenone 0.00751 N J

Westlake KY 01/16/13 Suspension 10 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00516 Y

Westlake KY 01/16/13 Suspension 10 SVOC SW-846-8270D 123319 Hydroquinone 0.015 Y UJ

Westlake KY 01/16/13 Suspension 10 SVOC SW-846-8270D 108952 Phenol 0.00175 Y

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 71432 Benzene 0.001 N U

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y UJ

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/16/13 Suspension 10 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 01/16/13 Suspension 10 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 01/17/13 Suspension 11 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Y

Westlake KY 01/17/13 Suspension 11 Alcohol SW-846-8015C 67561 Methanol 44.5 N

Westlake KY 01/17/13 Suspension 11 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.364 N

Westlake KY 01/17/13 Suspension 11 Aldehyde SW-846-8315A 50000 Formaldehyde 0.383 N

Westlake KY 01/17/13 Suspension 11 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00316 Y

Westlake KY 01/17/13 Suspension 11 SVOC SW-846-8270D 98862 Acetophenone 0.00365 Y J

Westlake KY 01/17/13 Suspension 11 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00516 Y

Westlake KY 01/17/13 Suspension 11 SVOC SW-846-8270D 123319 Hydroquinone 0.015 Y UJ

Westlake KY 01/17/13 Suspension 11 SVOC SW-846-8270D 108952 Phenol 0.00175 Y

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 71432 Benzene 0.0002 N J

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/17/13 Suspension 11 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 01/17/13 Suspension 11 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 01/18/13 Suspension 12 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Y

Westlake KY 01/18/13 Suspension 12 Alcohol SW-846-8015C 67561 Methanol 39.2 N

Westlake KY 01/18/13 Suspension 12 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.277 N

Westlake KY 01/18/13 Suspension 12 Aldehyde SW-846-8315A 50000 Formaldehyde 0.469 N

Westlake KY 01/18/13 Suspension 12 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Y

Westlake KY 01/18/13 Suspension 12 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Y

Westlake KY 01/18/13 Suspension 12 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Y

Westlake KY 01/18/13 Suspension 12 SVOC SW-846-8270D 123319 Hydroquinone 0.03 Y UJ

Westlake KY 01/18/13 Suspension 12 SVOC SW-846-8270D 108952 Phenol 0.00349 Y

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 71432 Benzene 0.00016 N J

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/18/13 Suspension 12 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Westlake KY 01/18/13 Suspension 12 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 01/19/13 Suspension 13 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Y

Westlake KY 01/19/13 Suspension 13 Alcohol SW-846-8015C 67561 Methanol 30.7 N

Westlake KY 01/19/13 Suspension 13 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.256 N

Westlake KY 01/19/13 Suspension 13 Aldehyde SW-846-8315A 50000 Formaldehyde 0.413 N

Westlake KY 01/19/13 Suspension 13 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Y

Westlake KY 01/19/13 Suspension 13 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Y

Westlake KY 01/19/13 Suspension 13 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Y

Westlake KY 01/19/13 Suspension 13 SVOC SW-846-8270D 123319 Hydroquinone 0.03 Y UJ

Westlake KY 01/19/13 Suspension 13 SVOC SW-846-8270D 108952 Phenol 0.00349 Y

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 71432 Benzene 0.00004 Y

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/19/13 Suspension 13 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 01/19/13 Suspension 13 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 01/20/13 Suspension 14 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Y

Westlake KY 01/20/13 Suspension 14 Alcohol SW-846-8015C 67561 Methanol 35.3 N

Westlake KY 01/20/13 Suspension 14 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.529 N

Westlake KY 01/20/13 Suspension 14 Aldehyde SW-846-8315A 50000 Formaldehyde 0.461 N

Westlake KY 01/20/13 Suspension 14 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Y

Westlake KY 01/20/13 Suspension 14 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Y

Westlake KY 01/20/13 Suspension 14 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Y

Westlake KY 01/20/13 Suspension 14 SVOC SW-846-8270D 123319 Hydroquinone 0.03 Y UJ

Westlake KY 01/20/13 Suspension 14 SVOC SW-846-8270D 108952 Phenol 0.00349 Y

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 71432 Benzene 0.00046 N J

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 67663 Chloroform 0.00019 N J

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/20/13 Suspension 14 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 01/20/13 Suspension 14 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 01/21/13 Suspension 15 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Y

Westlake KY 01/21/13 Suspension 15 Alcohol SW-846-8015C 67561 Methanol 32.2 N

Westlake KY 01/21/13 Suspension 15 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.97 N

Westlake KY 01/21/13 Suspension 15 Aldehyde SW-846-8315A 50000 Formaldehyde 0.991 N

Westlake KY 01/21/13 Suspension 15 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Y

Westlake KY 01/21/13 Suspension 15 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Y

Westlake KY 01/21/13 Suspension 15 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Y

Westlake KY 01/21/13 Suspension 15 SVOC SW-846-8270D 123319 Hydroquinone 0.03 Y UJ

Westlake KY 01/21/13 Suspension 15 SVOC SW-846-8270D 108952 Phenol 0.00349 Y

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y UJ

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y UJ

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y UJ

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 71432 Benzene 0.00012 N J

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y UJ

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 67663 Chloroform 0.0001 Y UJ

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y UJ

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 98828 Cumene 0.00005 Y UJ

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y UJ

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y UJ

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y UJ

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y UJ

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y UJ

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 108883 Toluene 0.00004 Y UJ

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y UJ

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y UJ

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y UJ

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/21/13 Suspension 15 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 01/21/13 Suspension 15 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y UJ, Note (3)

Westlake KY 01/22/13 Suspension 16 Alcohol SW-846-8015C 107211 Ethylene glycol 5.5 N U

Westlake KY 01/22/13 Suspension 16 Alcohol SW-846-8015C 67561 Methanol 48.7 N

Westlake KY 01/22/13 Suspension 16 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.255 N

Westlake KY 01/22/13 Suspension 16 Aldehyde SW-846-8315A 50000 Formaldehyde 0.308 N

Westlake KY 01/22/13 Suspension 16 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Y

Westlake KY 01/22/13 Suspension 16 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Y

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Westlake KY 01/22/13 Suspension 16 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Y

Westlake KY 01/22/13 Suspension 16 SVOC SW-846-8270D 123319 Hydroquinone 0.03 Y UJ

Westlake KY 01/22/13 Suspension 16 SVOC SW-846-8270D 108952 Phenol 0.00349 Y

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 71432 Benzene 0.00024 N J

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y UJ

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 108883 Toluene 0.00004 Y UJ

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/22/13 Suspension 16 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 01/22/13 Suspension 16 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y UJ, Note (3)

Westlake KY 01/23/13 Suspension 17 Alcohol SW-846-8015C 107211 Ethylene glycol 1.9 N U

Westlake KY 01/23/13 Suspension 17 Alcohol SW-846-8015C 67561 Methanol 25.5 N

Westlake KY 01/23/13 Suspension 17 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.63 N

Westlake KY 01/23/13 Suspension 17 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 N

Westlake KY 01/23/13 Suspension 17 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Y UJ

Westlake KY 01/23/13 Suspension 17 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Y

Westlake KY 01/23/13 Suspension 17 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Y

Westlake KY 01/23/13 Suspension 17 SVOC SW-846-8270D 123319 Hydroquinone 0.156 N JN

Westlake KY 01/23/13 Suspension 17 SVOC SW-846-8270D 108952 Phenol 0.00349 Y UJ

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 71432 Benzene 0.001 N U

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/23/13 Suspension 17 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 01/23/13 Suspension 17 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 01/24/13 Suspension 18 Alcohol SW-846-8015C 107211 Ethylene glycol 4.9 N U

Westlake KY 01/24/13 Suspension 18 Alcohol SW-846-8015C 67561 Methanol 26.9 N

Westlake KY 01/24/13 Suspension 18 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.01 N

Westlake KY 01/24/13 Suspension 18 Aldehyde SW-846-8315A 50000 Formaldehyde 0.277 N

Westlake KY 01/24/13 Suspension 18 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Y

Westlake KY 01/24/13 Suspension 18 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Y

Westlake KY 01/24/13 Suspension 18 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Y

Westlake KY 01/24/13 Suspension 18 SVOC SW-846-8270D 123319 Hydroquinone 0.03 Y UJ

Westlake KY 01/24/13 Suspension 18 SVOC SW-846-8270D 108952 Phenol 0.00349 Y

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 71432 Benzene 0.001 N U

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/24/13 Suspension 18 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 01/24/13 Suspension 18 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 01/25/13 Suspension 19 Alcohol SW-846-8015C 107211 Ethylene glycol 4.1 N U

Westlake KY 01/25/13 Suspension 19 Alcohol SW-846-8015C 67561 Methanol 34.3 N

Westlake KY 01/25/13 Suspension 19 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.135 N J

Westlake KY 01/25/13 Suspension 19 Aldehyde SW-846-8315A 50000 Formaldehyde 0.218 N J

Westlake KY 01/25/13 Suspension 19 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Y

Westlake KY 01/25/13 Suspension 19 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Y

Westlake KY 01/25/13 Suspension 19 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Y

Westlake KY 01/25/13 Suspension 19 SVOC SW-846-8270D 123319 Hydroquinone 0.0349 Y UJ

Westlake KY 01/25/13 Suspension 19 SVOC SW-846-8270D 108952 Phenol 0.00349 Y

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 71432 Benzene 0.00004 Y

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/25/13 Suspension 19 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 01/25/13 Suspension 19 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 01/26/13 Suspension 20 Alcohol SW-846-8015C 107211 Ethylene glycol 3.8 N U

Westlake KY 01/26/13 Suspension 20 Alcohol SW-846-8015C 67561 Methanol 31.8 N

Westlake KY 01/26/13 Suspension 20 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.278 N

Westlake KY 01/26/13 Suspension 20 Aldehyde SW-846-8315A 50000 Formaldehyde 0.476 N

Westlake KY 01/26/13 Suspension 20 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Y

Westlake KY 01/26/13 Suspension 20 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Y

Westlake KY 01/26/13 Suspension 20 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Y

Westlake KY 01/26/13 Suspension 20 SVOC SW-846-8270D 123319 Hydroquinone 0.03 Y R

Westlake KY 01/26/13 Suspension 20 SVOC SW-846-8270D 108952 Phenol 0.00349 Y

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 71432 Benzene 0.00004 Y

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 67663 Chloroform 0.001 Y

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/26/13 Suspension 20 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 01/26/13 Suspension 20 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 01/27/13 Suspension 21 Alcohol SW-846-8015C 107211 Ethylene glycol 1.7 N U

Westlake KY 01/27/13 Suspension 21 Alcohol SW-846-8015C 67561 Methanol 30.8 N

Westlake KY 01/27/13 Suspension 21 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.327 N

Westlake KY 01/27/13 Suspension 21 Aldehyde SW-846-8315A 50000 Formaldehyde 0.51 N

Westlake KY 01/27/13 Suspension 21 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Y

Westlake KY 01/27/13 Suspension 21 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Y

Westlake KY 01/27/13 Suspension 21 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Y

Westlake KY 01/27/13 Suspension 21 SVOC SW-846-8270D 123319 Hydroquinone 0.03 Y R

Westlake KY 01/27/13 Suspension 21 SVOC SW-846-8270D 108952 Phenol 0.00349 Y

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y R

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y R

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 71432 Benzene 0.00004 Y

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 67663 Chloroform 0.0007 N J

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y J

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/27/13 Suspension 21 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00011 N

Westlake KY 01/27/13 Suspension 21 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 N J, Note (3.1)

Westlake KY 01/28/13 Suspension 22 Alcohol SW-846-8015C 107211 Ethylene glycol 3.7 N U

Westlake KY 01/28/13 Suspension 22 Alcohol SW-846-8015C 67561 Methanol 33.8 N

Westlake KY 01/28/13 Suspension 22 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.475 N

Westlake KY 01/28/13 Suspension 22 Aldehyde SW-846-8315A 50000 Formaldehyde 0.534 N

Westlake KY 01/28/13 Suspension 22 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Y

Westlake KY 01/28/13 Suspension 22 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Y

Westlake KY 01/28/13 Suspension 22 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Y

Westlake KY 01/28/13 Suspension 22 SVOC SW-846-8270D 123319 Hydroquinone 0.03 Y R

Westlake KY 01/28/13 Suspension 22 SVOC SW-846-8270D 108952 Phenol 0.00349 Y

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 71432 Benzene 0.00004 Y

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 75092 Methylene chloride 0.00282 N J

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/28/13 Suspension 22 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y J

Westlake KY 01/28/13 Suspension 22 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 01/29/13 Suspension 23 Alcohol SW-846-8015C 107211 Ethylene glycol 3.9 N U

Westlake KY 01/29/13 Suspension 23 Alcohol SW-846-8015C 67561 Methanol 29.6 N

Westlake KY 01/29/13 Suspension 23 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.973 N

Westlake KY 01/29/13 Suspension 23 Aldehyde SW-846-8315A 50000 Formaldehyde 0.393 N

Westlake KY 01/29/13 Suspension 23 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Y

Westlake KY 01/29/13 Suspension 23 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Y

Westlake KY 01/29/13 Suspension 23 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Y

Westlake KY 01/29/13 Suspension 23 SVOC SW-846-8270D 123319 Hydroquinone 0.03 Y UJ

Westlake KY 01/29/13 Suspension 23 SVOC SW-846-8270D 108952 Phenol 0.00349 Y

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 71432 Benzene 0.00012 N J

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 75092 Methylene chloride 0.00234 N J

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/29/13 Suspension 23 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 01/29/13 Suspension 23 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 01/30/13 Suspension 24 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Y UJ

Westlake KY 01/30/13 Suspension 24 Alcohol SW-846-8015C 67561 Methanol 24.2 N J

Westlake KY 01/30/13 Suspension 24 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.462 N

Westlake KY 01/30/13 Suspension 24 Aldehyde SW-846-8315A 50000 Formaldehyde 0.375 N

Westlake KY 01/30/13 Suspension 24 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Y

Westlake KY 01/30/13 Suspension 24 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Y

Westlake KY 01/30/13 Suspension 24 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Y

Westlake KY 01/30/13 Suspension 24 SVOC SW-846-8270D 123319 Hydroquinone 0.03 Y UJ

Westlake KY 01/30/13 Suspension 24 SVOC SW-846-8270D 108952 Phenol 0.00349 Y

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 71432 Benzene 0.00004 Y

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y UJ

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y UJ

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 75092 Methylene chloride 0.00167 N

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/30/13 Suspension 24 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 01/30/13 Suspension 24 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 01/31/13 Suspension 25 Alcohol SW-846-8015C 107211 Ethylene glycol 1 N UJ

Westlake KY 01/31/13 Suspension 25 Alcohol SW-846-8015C 67561 Methanol 27.1 N J

Westlake KY 01/31/13 Suspension 25 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.255 N

Westlake KY 01/31/13 Suspension 25 Aldehyde SW-846-8315A 50000 Formaldehyde 0.35 N

Westlake KY 01/31/13 Suspension 25 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Y

Westlake KY 01/31/13 Suspension 25 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Y

Westlake KY 01/31/13 Suspension 25 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Y

Westlake KY 01/31/13 Suspension 25 SVOC SW-846-8270D 123319 Hydroquinone 0.03 Y UJ

Westlake KY 01/31/13 Suspension 25 SVOC SW-846-8270D 108952 Phenol 0.00349 Y

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 71432 Benzene 0.00014 N J

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 01/31/13 Suspension 25 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 01/31/13 Suspension 25 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 02/01/13 Suspension 26 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Y UJ

Westlake KY 02/01/13 Suspension 26 Alcohol SW-846-8015C 67561 Methanol 33 N J

Westlake KY 02/01/13 Suspension 26 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.375 N

Westlake KY 02/01/13 Suspension 26 Aldehyde SW-846-8315A 50000 Formaldehyde 0.552 N

Westlake KY 02/01/13 Suspension 26 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Y

Westlake KY 02/01/13 Suspension 26 SVOC SW-846-8270D 98862 Acetophenone 0.0173 N J

Westlake KY 02/01/13 Suspension 26 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Y

Westlake KY 02/01/13 Suspension 26 SVOC SW-846-8270D 123319 Hydroquinone 0.03 Y UJ

Westlake KY 02/01/13 Suspension 26 SVOC SW-846-8270D 108952 Phenol 0.00349 Y

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 106990 1,3-butadiene 0.00069 N J

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 71432 Benzene 0.00019 N J

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 02/01/13 Suspension 26 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 02/01/13 Suspension 26 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 02/02/13 Suspension 27 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Y

Westlake KY 02/02/13 Suspension 27 Alcohol SW-846-8015C 67561 Methanol 21.8 N J

Westlake KY 02/02/13 Suspension 27 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.307 N

Westlake KY 02/02/13 Suspension 27 Aldehyde SW-846-8315A 50000 Formaldehyde 0.339 N

Westlake KY 02/02/13 Suspension 27 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Y

Westlake KY 02/02/13 Suspension 27 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Y

Westlake KY 02/02/13 Suspension 27 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Y

Westlake KY 02/02/13 Suspension 27 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Y UJ

Westlake KY 02/02/13 Suspension 27 SVOC SW-846-8270D 108952 Phenol 0.00349 Y

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 71432 Benzene 0.00004 Y

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 67663 Chloroform 0.00022 N J

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 02/02/13 Suspension 27 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 02/02/13 Suspension 27 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 02/03/13 Suspension 28 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Y

Westlake KY 02/03/13 Suspension 28 Alcohol SW-846-8015C 67561 Methanol 44 N J

Westlake KY 02/03/13 Suspension 28 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.296 N

Westlake KY 02/03/13 Suspension 28 Aldehyde SW-846-8315A 50000 Formaldehyde 0.414 N

Westlake KY 02/03/13 Suspension 28 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Y

Westlake KY 02/03/13 Suspension 28 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Y

Westlake KY 02/03/13 Suspension 28 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Y

Westlake KY 02/03/13 Suspension 28 SVOC SW-846-8270D 123319 Hydroquinone 0.03 Y UJ

Westlake KY 02/03/13 Suspension 28 SVOC SW-846-8270D 108952 Phenol 0.00349 Y

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 106990 1,3-butadiene 0.012 Y

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0225 Y

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 71432 Benzene 0.00004 Y

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 02/03/13 Suspension 28 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 02/03/13 Suspension 28 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 02/04/13 Suspension 29 Alcohol SW-846-8015C 107211 Ethylene glycol 2 N

Westlake KY 02/04/13 Suspension 29 Alcohol SW-846-8015C 67561 Methanol 21.4 N J

12/12/2013 VI Confidential 95 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Westlake KY 02/04/13 Suspension 29 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.36 N

Westlake KY 02/04/13 Suspension 29 Aldehyde SW-846-8315A 50000 Formaldehyde 0.451 N

Westlake KY 02/04/13 Suspension 29 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Y

Westlake KY 02/04/13 Suspension 29 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Y

Westlake KY 02/04/13 Suspension 29 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Y

Westlake KY 02/04/13 Suspension 29 SVOC SW-846-8270D 123319 Hydroquinone 0.03 Y UJ

Westlake KY 02/04/13 Suspension 29 SVOC SW-846-8270D 108952 Phenol 0.00349 Y

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 71432 Benzene 0.00004 Y

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 02/04/13 Suspension 29 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 02/04/13 Suspension 29 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake KY 02/05/13 Suspension 30 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Y

Westlake KY 02/05/13 Suspension 30 Alcohol SW-846-8015C 67561 Methanol 34.3 N J

Westlake KY 02/05/13 Suspension 30 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.37 N

Westlake KY 02/05/13 Suspension 30 Aldehyde SW-846-8315A 50000 Formaldehyde 0.474 N

Westlake KY 02/05/13 Suspension 30 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Y

Westlake KY 02/05/13 Suspension 30 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Y

Westlake KY 02/05/13 Suspension 30 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Y

Westlake KY 02/05/13 Suspension 30 SVOC SW-846-8270D 123319 Hydroquinone 3 Y UJ

Westlake KY 02/05/13 Suspension 30 SVOC SW-846-8270D 108952 Phenol 0.0349 Y

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Y

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Y

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Y

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 71432 Benzene 0.00019 N J

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Y

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 67663 Chloroform 0.0001 Y

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 126998 Chloroprene 0.00033 Y

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 98828 Cumene 0.00005 Y

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00012 Y

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Y

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00028 Y

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Y

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00023 Y

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Y

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 110543 n-Hexane 0.00167 Y

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 108883 Toluene 0.00004 Y

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Y

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Y

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Y

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake KY 02/05/13 Suspension 30 VC EPA Method 107 75014 Vinyl chloride 0.01 Y U, Note (2)

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Y

Westlake KY 02/05/13 Suspension 30 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Y Note (3)

Westlake LA 01/07/13 Suspension 1 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Westlake LA 01/07/13 Suspension 1 Alcohol SW-846-8015C 67561 Methanol 14.2 N

Westlake LA 01/07/13 Suspension 1 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.86 N

Westlake LA 01/07/13 Suspension 1 Aldehyde SW-846-8315A 50000 Formaldehyde 0.721 N J

Westlake LA 01/07/13 Suspension 1 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Non-detect

Westlake LA 01/07/13 Suspension 1 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Non-detect

Westlake LA 01/07/13 Suspension 1 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Non-detect

Westlake LA 01/07/13 Suspension 1 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 01/07/13 Suspension 1 SVOC SW-846-8270D 108952 Phenol 0.00349 Non-detect

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 106990 1,3-butadiene 0.00651 N J

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.174 N J

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.37 N

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.106 N J

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect UJ

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 01/07/13 Suspension 1 VC EPA Method 107 75014 Vinyl chloride 2.4 N Note (2)

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00116 N J

Westlake LA 01/07/13 Suspension 1 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00124 Non-detect Note (3)

Westlake LA 01/08/13 Suspension 2 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Westlake LA 01/08/13 Suspension 2 Alcohol SW-846-8015C 67561 Methanol 13.9 N

Westlake LA 01/08/13 Suspension 2 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.28 N

Westlake LA 01/08/13 Suspension 2 Aldehyde SW-846-8315A 50000 Formaldehyde 0.732 N J

Westlake LA 01/08/13 Suspension 2 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 01/08/13 Suspension 2 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 01/08/13 Suspension 2 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 01/08/13 Suspension 2 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 01/08/13 Suspension 2 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00083N

J

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 106990 1,3-butadiene 0.0048 Non-detect

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Non-detect UJ

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 71432 Benzene 0.00004 Non-detect UJ

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Non-detect UJ

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 67663 Chloroform 0.0001 Non-detect UJ

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 126998 Chloroprene 0.00033 Non-detect UJ

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 98828 Cumene 0.00005 Non-detect UJ

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0661N

J

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Non-detect UJ

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.15N

J

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect UJ

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0625N

J

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Non-detect UJ

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 110543 n-Hexane 0.00167 Non-detect UJ

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 108883 Toluene 0.00004 Non-detect UJ

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Non-detect UJ

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00071N

J

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Non-detect UJ

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 01/08/13 Suspension2 VC EPA Method 107 75014 Vinyl chloride 1.1 Note (2)

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00104N

J

Westlake LA 01/08/13 Suspension2 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Non-detect UJ Note (3)

Westlake LA 01/09/13 Suspension3 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Westlake LA 01/09/13 Suspension3 Alcohol SW-846-8015C 67561 Methanol 0.2 Non-detect

Westlake LA 01/09/13 Suspension3 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.48N

U

Westlake LA 01/09/13 Suspension3 Aldehyde SW-846-8315A 50000 Formaldehyde 3.13N UJ

Westlake LA 01/09/13 Suspension3 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 01/09/13 Suspension3 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 01/09/13 Suspension3 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 01/09/13 Suspension3 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 01/09/13 Suspension3 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00062N

J

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 106990 1,3-butadiene 0.00138N

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Non-detect

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 71432 Benzene 0.00014N

J

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Non-detect

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 67663 Chloroform 0.0001 Non-detect

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 126998 Chloroprene 0.00033 Non-detect

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 98828 Cumene 0.00005 Non-detect

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0745N

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Non-detect

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.102N

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0552N

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Non-detect

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 110543 n-Hexane 0.00167 Non-detect

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 108883 Toluene 0.00052N

J

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Non-detect

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00097N

J

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Non-detect

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 01/09/13 Suspension3 VC EPA Method 107 75014 Vinyl chloride 1.3 Note (2)

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00054N

J

Westlake LA 01/09/13 Suspension3 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Non-detect Note (3)

Westlake LA 01/10/13 Suspension4 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Westlake LA 01/10/13 Suspension4 Alcohol SW-846-8015C 67561 Methanol 100.4N

Westlake LA 01/10/13 Suspension4 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.79N

Westlake LA 01/10/13 Suspension4 Aldehyde SW-846-8315A 50000 Formaldehyde 0.86N

J

Westlake LA 01/10/13 Suspension4 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 01/10/13 Suspension4 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 01/10/13 Suspension4 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 01/10/13 Suspension4 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 01/10/13 Suspension4 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.104N

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0927N

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0696N

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 01/10/13 Suspension4 VC EPA Method 107 75014 Vinyl chloride 1.4 

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00098N

J

Westlake LA 01/10/13 Suspension4 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00124 Non-detect Note (3)

Westlake LA 01/11/13 Suspension5 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Westlake LA 01/11/13 Suspension5 Alcohol SW-846-8015C 67561 Methanol 79.6N

Westlake LA 01/11/13 Suspension5 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.77N

U

Westlake LA 01/11/13 Suspension5 Aldehyde SW-846-8315A 50000 Formaldehyde 1.02N

J

Westlake LA 01/11/13 Suspension5 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 01/11/13 Suspension5 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 01/11/13 Suspension5 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 01/11/13 Suspension5 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 01/11/13 Suspension5 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0932N

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0766N

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.062N

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 01/11/13 Suspension5 VC EPA Method 107 75014 Vinyl chloride 1.5 Note (2)

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Westlake LA 01/11/13 Suspension5 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00124 Non-detect Note (3)

Westlake LA 01/23/13 Suspension6 Alcohol SW-846-8015C 107211 Ethylene glycol1N

U

Westlake LA 01/23/13 Suspension6 Alcohol SW-846-8015C 67561 Methanol 130N

Westlake LA 01/23/13 Suspension6 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.996N

Westlake LA 01/23/13 Suspension6 Aldehyde SW-846-8315A 50000 Formaldehyde 0.527N

Westlake LA 01/23/13 Suspension6 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 01/23/13 Suspension6 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 01/23/13 Suspension6 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 01/23/13 Suspension6 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 01/23/13 Suspension6 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Non-detect

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Non-detect

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Non-detect

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 71432 Benzene 0.00004 Non-detect

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Non-detect

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 67663 Chloroform 0.0001 Non-detect

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 126998 Chloroprene 0.00033 Non-detect

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 98828 Cumene 0.00005 Non-detect

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.07N

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Non-detect

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.465N

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0623N

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Non-detect

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 110543 n-Hexane 0.00167 Non-detect

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 108883 Toluene 0.00004 Non-detect

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Non-detect

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00111N

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Non-detect

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 01/23/13 Suspension6 VC EPA Method 107 75014 Vinyl chloride 1.6 Note (2)

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.001N

U

Westlake LA 01/23/13 Suspension6 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.000120 Note (3)

Westlake LA 01/24/13 Suspension7 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Westlake LA 01/24/13 Suspension7 Alcohol SW-846-8015C 67561 Methanol 189N

Westlake LA 01/24/13 Suspension7 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.31N

Westlake LA 01/24/13 Suspension7 Aldehyde SW-846-8315A 50000 Formaldehyde 0.255N

Westlake LA 01/24/13 Suspension7 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0316 Non-detect

Westlake LA 01/24/13 Suspension7 SVOC SW-846-8270D 98862 Acetophenone 0.0365 Non-detect

Westlake LA 01/24/13 Suspension7 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0516 Non-detect

Westlake LA 01/24/13 Suspension7 SVOC SW-846-8270D 123319 Hydroquinone 0.15 Non-detect UJ

Westlake LA 01/24/13 Suspension7 SVOC SW-846-8270D 108952 Phenol 0.0175 Non-detect

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Non-detect

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 106990 1,3-butadiene 0.00225N

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Non-detect

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 71432 Benzene 0.001N

U

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Non-detect

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 67663 Chloroform 0.0001 Non-detect

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 126998 Chloroprene 0.00033 Non-detect

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 98828 Cumene 0.00005 Non-detect

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0509N

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Non-detect

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.42N

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.037N

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Non-detect

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 110543 n-Hexane 0.00167 Non-detect

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 108883 Toluene 0.00004 Non-detect

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Non-detect

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00152N

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Non-detect

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 01/24/13 Suspension7 VC EPA Method 107 75014 Vinyl chloride 1.5 Note (2)

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Non-detect

Westlake LA 01/24/13 Suspension7 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.000120 Note (3)

Westlake LA 01/25/13 Suspension8 Alcohol SW-846-8015C 107211 Ethylene glycol3N

U

Westlake LA 01/25/13 Suspension8 Alcohol SW-846-8015C 67561 Methanol 143N

Westlake LA 01/25/13 Suspension8 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.998N

Westlake LA 01/25/13 Suspension8 Aldehyde SW-846-8315A 50000 Formaldehyde 0.227N

Westlake LA 01/25/13 Suspension8 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 01/25/13 Suspension8 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 01/25/13 Suspension8 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 01/25/13 Suspension8 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 01/25/13 Suspension8 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 01/25/13 Suspension8 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 01/25/13 Suspension8 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Westlake LA 01/25/13 Suspension8 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Westlake LA 01/25/13 Suspension8 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 01/25/13 Suspension8 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 01/25/13 Suspension8 VOC SW-846-8260B 67663 Chloroform 0.01N

U

Westlake LA 01/25/13 Suspension8 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 01/25/13 Suspension8 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 01/25/13 Suspension8 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0968N

Westlake LA 01/25/13 Suspension8 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 01/25/13 Suspension8 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.385N

Westlake LA 01/25/13 Suspension8 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 01/25/13 Suspension8 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0507N

Westlake LA 01/25/13 Suspension8 VOC SW-846-8260B 75092 Methylene chloride 0.013N

J

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Westlake LA 01/25/13 Suspension 8 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 01/25/13 Suspension 8 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 01/25/13 Suspension 8 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 01/25/13 Suspension 8 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 01/25/13 Suspension 8 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 01/25/13 Suspension 8 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 01/25/13 Suspension 8 VC EPA Method 107 75014 Vinyl chloride 1.6 Note (2)

Westlake LA 01/25/13 Suspension 8 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Westlake LA 01/25/13 Suspension 8 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00124 0 Note (3)

Westlake LA 01/26/13 Suspension 9 Alcohol SW-846-8015C 107211 Ethylene glycol 2.3 N U

Westlake LA 01/26/13 Suspension 9 Alcohol SW-846-8015C 67561 Methanol 247 N

Westlake LA 01/26/13 Suspension 9 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.05 N

Westlake LA 01/26/13 Suspension 9 Aldehyde SW-846-8315A 50000 Formaldehyde 0.822 N

Westlake LA 01/26/13 Suspension 9 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 01/26/13 Suspension 9 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 01/26/13 Suspension 9 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 01/26/13 Suspension 9 SVOC SW-846-8270D 123319 Hydroquinone NO RESULT R Note (4)

Westlake LA 01/26/13 Suspension 9 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0616 N

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.324 N

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.039 N

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 75092 Methylene chloride 0.0286 N J

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 01/26/13 Suspension 9 VC EPA Method 107 75014 Vinyl chloride 1.4 Note (2)

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Westlake LA 01/26/13 Suspension 9 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00124 0 Note (3)

Westlake LA 01/27/13 Suspension 10 Alcohol SW-846-8015C 107211 Ethylene glycol 3.5 N U

Westlake LA 01/27/13 Suspension 10 Alcohol SW-846-8015C 67561 Methanol 211 N

Westlake LA 01/27/13 Suspension 10 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.73 N

Westlake LA 01/27/13 Suspension 10 Aldehyde SW-846-8315A 50000 Formaldehyde 0.783 N

Westlake LA 01/27/13 Suspension 10 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 01/27/13 Suspension 10 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 01/27/13 Suspension 10 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 01/27/13 Suspension 10 SVOC SW-846-8270D 123319 Hydroquinone NO RESULT R Note (4)

Westlake LA 01/27/13 Suspension 10 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0404 N J

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.147 N J

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0339 N J

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 75092 Methylene chloride 0.033 N J

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 01/27/13 Suspension 10 VC EPA Method 107 75014 Vinyl chloride 0.8 Note (2)

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Westlake LA 01/27/13 Suspension 10 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00124 0 Note (3)

Westlake LA 01/28/13 Suspension 11 Alcohol SW-846-8015C 107211 Ethylene glycol 3 N U

Westlake LA 01/28/13 Suspension 11 Alcohol SW-846-8015C 67561 Methanol 131 N

Westlake LA 01/28/13 Suspension 11 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.75 N

Westlake LA 01/28/13 Suspension 11 Aldehyde SW-846-8315A 50000 Formaldehyde 0.709 N

Westlake LA 01/28/13 Suspension 11 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 01/28/13 Suspension 11 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 01/28/13 Suspension 11 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 01/28/13 Suspension 11 SVOC SW-846-8270D 123319 Hydroquinone NO RESULT R Note (4)

Westlake LA 01/28/13 Suspension 11 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0861 N J

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.132 N J

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0355 N J

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 75092 Methylene chloride 0.0321 N J

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 01/28/13 Suspension 11 VC EPA Method 107 75014 Vinyl chloride 1.6 Note (2)

12/12/2013 VI Confidential 99 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0321 Non-detect

Westlake LA 01/28/13 Suspension 11 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00124 Non-detect Note (3)

Westlake LA 01/29/13 Suspension 12 Alcohol SW-846-8015C 107211 Ethylene glycol 4.6N

U

Westlake LA 01/29/13 Suspension 12 Alcohol SW-846-8015C 67561 Methanol 126N

Westlake LA 01/29/13 Suspension 12 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.06N

Westlake LA 01/29/13 Suspension 12 Aldehyde SW-846-8315A 50000 Formaldehyde 0.713N

Westlake LA 01/29/13 Suspension 12 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 01/29/13 Suspension 12 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 01/29/13 Suspension 12 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 01/29/13 Suspension 12 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 01/29/13 Suspension 12 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 106990 1,3-butadiene 0.0143N

J

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.129N

J

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.178N

J

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0542N

J

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00241N

J

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 01/29/13 Suspension 12 VC EPA Method 107 75014 Vinyl chloride 1.7 Note (2)

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Westlake LA 01/29/13 Suspension 12 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00124 Non-detect Note (3)

Westlake LA 01/30/13 Suspension 13 Alcohol SW-846-8015C 107211 Ethylene glycol 5.2N

U

Westlake LA 01/30/13 Suspension 13 Alcohol SW-846-8015C 67561 Methanol 184N

Westlake LA 01/30/13 Suspension 13 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.07N

Westlake LA 01/30/13 Suspension 13 Aldehyde SW-846-8315A 50000 Formaldehyde 0.68N

Westlake LA 01/30/13 Suspension 13 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 01/30/13 Suspension 13 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 01/30/13 Suspension 13 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 01/30/13 Suspension 13 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 01/30/13 Suspension 13 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0841N

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.105N

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.027N

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 75092 Methylene chloride 0.0167N

J

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 01/30/13 Suspension 13 VC EPA Method 107 75014 Vinyl chloride 2.5 Note (2)

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Westlake LA 01/30/13 Suspension 13 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001240 Note (3)

Westlake LA 01/31/13 Suspension 14 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect UJ

Westlake LA 01/31/13 Suspension 14 Alcohol SW-846-8015C 67561 Methanol 27N

J

Westlake LA 01/31/13 Suspension 14 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.83N

Westlake LA 01/31/13 Suspension 14 Aldehyde SW-846-8315A 50000 Formaldehyde 0.815N

Westlake LA 01/31/13 Suspension 14 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 01/31/13 Suspension 14 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 01/31/13 Suspension 14 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 01/31/13 Suspension 14 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 01/31/13 Suspension 14 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0549N

J

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.121N

J

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0301N

J

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 01/31/13 Suspension 14 VC EPA Method 107 75014 Vinyl chloride1 Note (2)

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Westlake LA 01/31/13 Suspension 14 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001240 Note (3)

Westlake LA 02/01/13 Suspension 15 Alcohol SW-846-8015C 107211 Ethylene glycol1N

U

Westlake LA 02/01/13 Suspension 15 Alcohol SW-846-8015C 67561 Methanol 29.4N

J

Westlake LA 02/01/13 Suspension 15 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.13N

Westlake LA 02/01/13 Suspension 15 Aldehyde SW-846-8315A 50000 Formaldehyde 0.813N

Westlake LA 02/01/13 Suspension 15 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Westlake LA 02/01/13 Suspension 15 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 02/01/13 Suspension 15 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 02/01/13 Suspension 15 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 02/01/13 Suspension 15 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 106990 1,3-butadiene 0.0105N

J

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0465N

J

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.119N

J

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0348N

J

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 02/01/13 Suspension 15 VC EPA Method 107 75014 Vinyl chloride 0.67 Note (2)

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Westlake LA 02/01/13 Suspension 15 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001240 Note (3)

Westlake LA 02/02/13 Suspension 16 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6N

J

Westlake LA 02/02/13 Suspension 16 Alcohol SW-846-8015C 67561 Methanol 31N

J

Westlake LA 02/02/13 Suspension 16 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.59N

Westlake LA 02/02/13 Suspension 16 Aldehyde SW-846-8315A 50000 Formaldehyde 0.922N

Westlake LA 02/02/13 Suspension 16 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 02/02/13 Suspension 16 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 02/02/13 Suspension 16 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 02/02/13 Suspension 16 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 02/02/13 Suspension 16 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0371N

J

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0938N

J

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0296N

J

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 02/02/13 Suspension 16 VC EPA Method 107 75014 Vinyl chloride 0.71 Note (2)

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Westlake LA 02/02/13 Suspension 16 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.001240 Note (3)

Westlake LA 02/03/13 Suspension 17 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Westlake LA 02/03/13 Suspension 17 Alcohol SW-846-8015C 67561 Methanol 32.3N

J

Westlake LA 02/03/13 Suspension 17 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.4N

Westlake LA 02/03/13 Suspension 17 Aldehyde SW-846-8315A 50000 Formaldehyde 0.92N

Westlake LA 02/03/13 Suspension 17 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 02/03/13 Suspension 17 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 02/03/13 Suspension 17 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 02/03/13 Suspension 17 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 02/03/13 Suspension 17 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.053N

J

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.102N

J

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0273N

J

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 02/03/13 Suspension 17 VC EPA Method 107 75014 Vinyl chloride 0.9 Note (2)

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Westlake LA 02/03/13 Suspension 17 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00124 Non-detect Note (3)

Westlake LA 02/04/13 Suspension 18 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Westlake LA 02/04/13 Suspension 18 Alcohol SW-846-8015C 67561 Methanol 76N

Westlake LA 02/04/13 Suspension 18 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.76N

Westlake LA 02/04/13 Suspension 18 Aldehyde SW-846-8315A 50000 Formaldehyde 0.89N

Westlake LA 02/04/13 Suspension 18 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 02/04/13 Suspension 18 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 02/04/13 Suspension 18 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 02/04/13 Suspension 18 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 02/04/13 Suspension 18 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.099 N J

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.153 N J

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0759 N J

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 02/04/13 Suspension 18 VC EPA Method 107 75014 Vinyl chloride 1.8 Note (2)

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Westlake LA 02/04/13 Suspension 18 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00124 Non-detect Note (3)

Westlake LA 02/05/13 Suspension 19 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Westlake LA 02/05/13 Suspension 19 Alcohol SW-846-8015C 67561 Methanol 26.5 N J

Westlake LA 02/05/13 Suspension 19 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.91 N

Westlake LA 02/05/13 Suspension 19 Aldehyde SW-846-8315A 50000 Formaldehyde 0.765 N

Westlake LA 02/05/13 Suspension 19 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 02/05/13 Suspension 19 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 02/05/13 Suspension 19 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 02/05/13 Suspension 19 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 02/05/13 Suspension 19 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.17 N

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.139 N

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0594 N

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 02/05/13 Suspension 19 VC EPA Method 107 75014 Vinyl chloride 3.6

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Westlake LA 02/05/13 Suspension 19 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00124 Non-detect Note (3)

Westlake LA 02/06/13 Suspension 20 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Westlake LA 02/06/13 Suspension 20 Alcohol SW-846-8015C 67561 Methanol 24.1 N

Westlake LA 02/06/13 Suspension 20 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.24 N U

Westlake LA 02/06/13 Suspension 20 Aldehyde SW-846-8315A 50000 Formaldehyde 0.721 N

Westlake LA 02/06/13 Suspension 20 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 02/06/13 Suspension 20 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 02/06/13 Suspension 20 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 02/06/13 Suspension 20 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 02/06/13 Suspension 20 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0501 N

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0765 N

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0426 N

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 02/06/13 Suspension 20 VC EPA Method 107 75014 Vinyl chloride 0.5 Note (2)

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Westlake LA 02/06/13 Suspension 20 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00124 Non-detect Note (3)

Westlake LA 02/07/13 Suspension 21 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Westlake LA 02/07/13 Suspension 21 Alcohol SW-846-8015C 67561 Methanol 50.7 N

Westlake LA 02/07/13 Suspension 21 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.696 N

Westlake LA 02/07/13 Suspension 21 Aldehyde SW-846-8315A 50000 Formaldehyde 0.586 N

Westlake LA 02/07/13 Suspension 21 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 02/07/13 Suspension 21 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 02/07/13 Suspension 21 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 02/07/13 Suspension 21 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 02/07/13 Suspension 21 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0521 N

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 100414 Ethylbenzene 0.01 N U

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0772 N

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0365 N

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 02/07/13 Suspension 21 VC EPA Method 107 75014 Vinyl chloride 0.7 Note (2)

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Westlake LA 02/07/13 Suspension 21 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00124 Non-detect Note (3)

Westlake LA 02/08/13 Suspension 22 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Westlake LA 02/08/13 Suspension 22 Alcohol SW-846-8015C 67561 Methanol 38.1 N

Westlake LA 02/08/13 Suspension 22 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.51 N

Westlake LA 02/08/13 Suspension 22 Aldehyde SW-846-8315A 50000 Formaldehyde 0.599 N

Westlake LA 02/08/13 Suspension 22 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 02/08/13 Suspension 22 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 02/08/13 Suspension 22 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 02/08/13 Suspension 22 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 02/08/13 Suspension 22 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0528 N

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0729 N

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0458 N

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 02/08/13 Suspension 22 VC EPA Method 107 75014 Vinyl chloride 1.1 Note (2)

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Westlake LA 02/08/13 Suspension 22 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00124 Non-detect Note (3)

Westlake LA 02/09/13 Suspension 23 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Westlake LA 02/09/13 Suspension 23 Alcohol SW-846-8015C 67561 Methanol 30.7 N

Westlake LA 02/09/13 Suspension 23 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.4 N

Westlake LA 02/09/13 Suspension 23 Aldehyde SW-846-8315A 50000 Formaldehyde 0.703 N

Westlake LA 02/09/13 Suspension 23 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 02/09/13 Suspension 23 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 02/09/13 Suspension 23 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 02/09/13 Suspension 23 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 02/09/13 Suspension 23 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.049 N

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.063 N

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.036 N

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 75092 Methylene chloride 0.05 N U

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 02/09/13 Suspension 23 VC EPA Method 107 75014 Vinyl chloride 0.76 Note (2)

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Westlake LA 02/09/13 Suspension 23 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00124 Non-detect Note (3)

Westlake LA 02/10/13 Suspension 24 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Westlake LA 02/10/13 Suspension 24 Alcohol SW-846-8015C 67561 Methanol 27.5 N

Westlake LA 02/10/13 Suspension 24 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.024 N U

Westlake LA 02/10/13 Suspension 24 Aldehyde SW-846-8315A 50000 Formaldehyde 0.03 Non-detect

Westlake LA 02/10/13 Suspension 24 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 02/10/13 Suspension 24 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 02/10/13 Suspension 24 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 02/10/13 Suspension 24 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 02/10/13 Suspension 24 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0456 N

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.058 N

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0327 N

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 75092 Methylene chloride 0.05 N U

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 02/10/13 Suspension 24 VC EPA Method 107 75014 Vinyl chloride 0.73 Note (2)

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Westlake LA 02/10/13 Suspension 24 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00124 Non-detect Note (3)

Westlake LA 02/11/13 Suspension 25 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Westlake LA 02/11/13 Suspension 25 Alcohol SW-846-8015C 67561 Methanol 20.3 N

Westlake LA 02/11/13 Suspension 25 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.642 N

Westlake LA 02/11/13 Suspension 25 Aldehyde SW-846-8315A 50000 Formaldehyde 0.737 N

Westlake LA 02/11/13 Suspension 25 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 02/11/13 Suspension 25 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 02/11/13 Suspension 25 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 02/11/13 Suspension 25 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 02/11/13 Suspension 25 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Non-detect

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 106990 1,3-butadiene 0.00179 N

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Non-detect

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 71432 Benzene 0.00044 N J

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Non-detect

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 67663 Chloroform 0.0001 Non-detect

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 126998 Chloroprene 0.00033 Non-detect

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 98828 Cumene 0.00005 Non-detect

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0223 N

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Non-detect

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0284 N

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0132 N

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Non-detect

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 110543 n-Hexane 0.00167 Non-detect

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 108883 Toluene 0.00004 Non-detect

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Non-detect

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Non-detect

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Non-detect

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 02/11/13 Suspension 25 VC EPA Method 107 75014 Vinyl chloride 0.41 Note (2)

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Non-detect

Westlake LA 02/11/13 Suspension 25 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Non-detect Note (3)

Westlake LA 02/12/13 Suspension 26 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Westlake LA 02/12/13 Suspension 26 Alcohol SW-846-8015C 67561 Methanol 12.6 N

Westlake LA 02/12/13 Suspension 26 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.291 N B

Westlake LA 02/12/13 Suspension 26 Aldehyde SW-846-8315A 50000 Formaldehyde 0.625 N

Westlake LA 02/12/13 Suspension 26 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.00631 Non-detect

Westlake LA 02/12/13 Suspension 26 SVOC SW-846-8270D 98862 Acetophenone 0.00729 Non-detect

Westlake LA 02/12/13 Suspension 26 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0103 Non-detect

Westlake LA 02/12/13 Suspension 26 SVOC SW-846-8270D 123319 Hydroquinone 0.03 Non-detect UJ

Westlake LA 02/12/13 Suspension 26 SVOC SW-846-8270D 108952 Phenol 0.00349 Non-detect

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Non-detect UJ

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 106990 1,3-butadiene 0.00197 N J

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Non-detect UJ

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 71432 Benzene 0.00057 N J

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Non-detect UJ

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 67663 Chloroform 0.0001 Non-detect UJ

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 126998 Chloroprene 0.00033 Non-detect UJ

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 98828 Cumene 0.00005 Non-detect UJ

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.014 N J

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Non-detect UJ

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0123 N J

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect UJ

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00852 N J

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Non-detect UJ

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 110543 n-Hexane 0.00167 Non-detect UJ

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 108883 Toluene 0.00004 Non-detect UJ

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Non-detect UJ

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Non-detect UJ

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Non-detect UJ

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 02/12/13 Suspension 26 VC EPA Method 107 75014 Vinyl chloride 2.7 U

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Non-detect UJ

Westlake LA 02/12/13 Suspension 26 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Non-detect UJ Note (3)

Westlake LA 02/13/13 Suspension 27 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Westlake LA 02/13/13 Suspension 27 Alcohol SW-846-8015C 67561 Methanol 12.1 N

Westlake LA 02/13/13 Suspension 27 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.349 N B

Westlake LA 02/13/13 Suspension 27 Aldehyde SW-846-8315A 50000 Formaldehyde 0.702 N

Westlake LA 02/13/13 Suspension 27 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 02/13/13 Suspension 27 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 02/13/13 Suspension 27 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 02/13/13 Suspension 27 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 02/13/13 Suspension 27 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Non-detect

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 106990 1,3-butadiene 0.00192 N

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Non-detect

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 71432 Benzene 0.00068 N J

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Non-detect

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 67663 Chloroform 0.0001 Non-detect

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 126998 Chloroprene 0.00033 Non-detect

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 98828 Cumene 0.00005 Non-detect

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0247 N

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Non-detect

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0237 N

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00017 N J

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0161 N

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Non-detect

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 110543 n-Hexane 0.00167 Non-detect

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 108883 Toluene 0.00004 Non-detect

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Non-detect

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0006 N J

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Non-detect

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 02/13/13 Suspension 27 VC EPA Method 107 75014 Vinyl chloride 0.31 Note (2)

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Non-detect

Westlake LA 02/13/13 Suspension 27 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00012 Non-detect Note (3)

Westlake LA 02/14/13 Suspension 28 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Westlake LA 02/14/13 Suspension 28 Alcohol SW-846-8015C 67561 Methanol 16.3 N

Westlake LA 02/14/13 Suspension 28 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.928 N

Westlake LA 02/14/13 Suspension 28 Aldehyde SW-846-8315A 50000 Formaldehyde 0.796 N

Westlake LA 02/14/13 Suspension 28 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 02/14/13 Suspension 28 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 02/14/13 Suspension 28 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 02/14/13 Suspension 28 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 02/14/13 Suspension 28 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0635 N

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0586 N

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0383 N

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 02/14/13 Suspension 28 VC EPA Method 107 75014 Vinyl chloride 1.1 Note (2)

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Westlake LA 02/14/13 Suspension 28 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00124 Non-detect Note (3)

Westlake LA 02/15/13 Suspension 29 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Westlake LA 02/15/13 Suspension 29 Alcohol SW-846-8015C 67561 Methanol 16.6 N

Westlake LA 02/15/13 Suspension 29 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.27 N

Westlake LA 02/15/13 Suspension 29 Aldehyde SW-846-8315A 50000 Formaldehyde 0.645 N

Westlake LA 02/15/13 Suspension 29 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 02/15/13 Suspension 29 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 02/15/13 Suspension 29 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 02/15/13 Suspension 29 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 02/15/13 Suspension 29 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.076 N

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.205 N

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0526 N

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 02/15/13 Suspension 29 VC EPA Method 107 75014 Vinyl chloride 0.97 Note (2)

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Westlake LA 02/15/13 Suspension 29 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00124 Non-detect Note (3)

Westlake LA 02/16/13 Suspension 30 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Westlake LA 02/16/13 Suspension 30 Alcohol SW-846-8015C 67561 Methanol 21.5 N

Westlake LA 02/16/13 Suspension 30 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.53 N

Westlake LA 02/16/13 Suspension 30 Aldehyde SW-846-8315A 50000 Formaldehyde 0.824 N

Westlake LA 02/16/13 Suspension 30 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Westlake LA 02/16/13 Suspension 30 SVOC SW-846-8270D 98862 Acetophenone 0.0729 Non-detect

Westlake LA 02/16/13 Suspension 30 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Westlake LA 02/16/13 Suspension 30 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect UJ

Westlake LA 02/16/13 Suspension 30 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Non-detect

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Non-detect

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0886 N

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.239 N

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0447 N

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 75092 Methylene chloride 0.0128 N J

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 593602 Vinyl bromide 0.001 TIC Note (1)

Westlake LA 02/16/13 Suspension 30 VC EPA Method 107 75014 Vinyl chloride 0.91 Note (2)

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Westlake LA 02/16/13 Suspension 30 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00528 Non-detect Note (3), J

Axiall ABD MS 01/14/13 Suspension 1 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 Alcohol SW-846-8015C 67561 Methanol 0.2 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.53

Axiall ABD MS 01/14/13 Suspension 1 Aldehyde SW-846-8315A 50000 Formaldehyde 0.975 Detected in blank

Axiall ABD MS 01/14/13 Suspension 1 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0876 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 SVOC SW-846-8270D 98862 Acetophenone 15.8

Axiall ABD MS 01/14/13 Suspension 1 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.143 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 SVOC SW-846-8270D 123319 Hydroquinone 0.370 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Axiall ABD MS 01/14/13 Suspension 1 SVOC SW-846-8270D 108952 Phenol 0.485 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00465 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 106990 1,3-butadiene 0.012 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0225 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 71432 Benzene 0.00239 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 108907 Chlorobenzene 0.00232 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 67663 Chloroform 0.00545 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 126998 Chloroprene 0.0165 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 98828 Cumene 0.00287 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0271 Estimated Value

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 100414 Ethylbenzene 0.00291 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0140 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00580 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.049 Estimated Value

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 75092 Methylene chloride 0.0209 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 110543 n-Hexane 0.0835 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 108883 Toluene 0.00250 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00690 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00223 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 108054 Vinyl acetate 0.00337 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 01/14/13 Suspension 1 VC EPA Method 107 75014 Vinyl chloride 0.869

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00287 Non-detect

Axiall ABD MS 01/14/13 Suspension 1 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0036 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 Alcohol SW-846-8015C 67561 Methanol 0.2 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 Aldehyde SW-846-8315A 75070 Acetaldehyde 11.600

Axiall ABD MS 01/15/13 Suspension 2 Aldehyde SW-846-8315A 50000 Formaldehyde 1.21

Axiall ABD MS 01/15/13 Suspension 2 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0928 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 SVOC SW-846-8270D 98862 Acetophenone 14.800

Axiall ABD MS 01/15/13 Suspension 2 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.152 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 SVOC SW-846-8270D 123319 Hydroquinone 0.400 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 SVOC SW-846-8270D 108952 Phenol 0.513 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00465 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 106990 1,3-butadiene 0.012 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0225 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 71432 Benzene 0.00239 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 108907 Chlorobenzene 0.00232 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 67663 Chloroform 0.00545 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 126998 Chloroprene 0.0165 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 98828 Cumene 0.00287 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0533

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 100414 Ethylbenzene 0.00291 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0140 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00580 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.128

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 75092 Methylene chloride 0.0209 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 110543 n-Hexane 0.0835 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 108883 Toluene 0.00250 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00690 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00223 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 108054 Vinyl acetate 0.00337 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 01/15/13 Suspension 2 VC EPA Method 107 75014 Vinyl chloride 1.780

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00358 Non-detect

Axiall ABD MS 01/15/13 Suspension 2 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0036 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 Alcohol SW-846-8015C 67561 Methanol 0.2 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.32

Axiall ABD MS 01/16/13 Suspension 3 Aldehyde SW-846-8315A 50000 Formaldehyde 1.32

Axiall ABD MS 01/16/13 Suspension 3 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0770 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 SVOC SW-846-8270D 98862 Acetophenone 18.5

Axiall ABD MS 01/16/13 Suspension 3 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.126 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 SVOC SW-846-8270D 123319 Hydroquinone 0.435 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 SVOC SW-846-8270D 108952 Phenol 0.426 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00465 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 106990 1,3-butadiene 0.0120 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0225 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 71432 Benzene 0.00239 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 108907 Chlorobenzene 0.00232 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 67663 Chloroform 0.00545 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 126998 Chloroprene 0.0165 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 98828 Cumene 0.00287 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00625 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 100414 Ethylbenzene 0.00291 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0140 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00580 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0651

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 75092 Methylene chloride 0.0209 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 110543 n-Hexane 0.0835 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 108883 Toluene 0.00250 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00690 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00223 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 108054 Vinyl acetate 0.00337 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 01/16/13 Suspension 3 VC EPA Method 107 75014 Vinyl chloride 1.17

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00358 Non-detect

Axiall ABD MS 01/16/13 Suspension 3 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0036 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 Alcohol SW-846-8015C 67561 Methanol 0.2 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.97

Axiall ABD MS 01/17/13 Suspension 4 Aldehyde SW-846-8315A 50000 Formaldehyde 1.66

Axiall ABD MS 01/17/13 Suspension 4 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0686 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 SVOC SW-846-8270D 98862 Acetophenone 17.9

Axiall ABD MS 01/17/13 Suspension 4 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.112 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 SVOC SW-846-8270D 123319 Hydroquinone 0.429 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 SVOC SW-846-8270D 108952 Phenol 0.0379 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00186 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 106990 1,3-butadiene 0.00480 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00900 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 71432 Benzene 0.00095 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 108907 Chlorobenzene 0.00092 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 67663 Chloroform 0.00218 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 126998 Chloroprene 0.0066 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 98828 Cumene 0.00115 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0242

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 100414 Ethylbenzene 0.00116 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00560 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00232 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0826

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 75092 Methylene chloride 0.00836 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 110543 n-Hexane 0.0334 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 108883 Toluene 0.00099 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00276 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00089 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 108054 Vinyl acetate 0.00135 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 01/17/13 Suspension 4 VC EPA Method 107 75014 Vinyl chloride 1.86

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00143 Non-detect

Axiall ABD MS 01/17/13 Suspension 4 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0014 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 Alcohol SW-846-8015C 67561 Methanol 0.2 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.55

Axiall ABD MS 01/18/13 Suspension 5 Aldehyde SW-846-8315A 50000 Formaldehyde 1.40

Axiall ABD MS 01/18/13 Suspension 5 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0853 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 SVOC SW-846-8270D 98862 Acetophenone 16.8

Axiall ABD MS 01/18/13 Suspension 5 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.139 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 SVOC SW-846-8270D 123319 Hydroquinone 0.316 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 SVOC SW-846-8270D 108952 Phenol 0.0472 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00186 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 106990 1,3-butadiene 0.00480 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00900 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 71432 Benzene 0.00095 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 108907 Chlorobenzene 0.00092 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 67663 Chloroform 0.00218 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 126998 Chloroprene 0.00660 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 98828 Cumene 0.00115 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0740

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 100414 Ethylbenzene 0.00116 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00560 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00232 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.211

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 75092 Methylene chloride 0.00836 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 110543 n-Hexane 0.0334 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 108883 Toluene 0.00099 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00276 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00089 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 108054 Vinyl acetate 0.00135 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 01/18/13 Suspension 5 VC EPA Method 107 75014 Vinyl chloride 2.700

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00143 Non-detect

Axiall ABD MS 01/18/13 Suspension 5 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0014 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 Alcohol SW-846-8015C 107211 Ethylene glycol 65.9 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 Alcohol SW-846-8015C 67561 Methanol 1650

Axiall ABD MS 01/19/13 Suspension 6 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.77

Axiall ABD MS 01/19/13 Suspension 6 Aldehyde SW-846-8315A 50000 Formaldehyde 1.61

Axiall ABD MS 01/19/13 Suspension 6 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0789 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 SVOC SW-846-8270D 98862 Acetophenone 15.400

Axiall ABD MS 01/19/13 Suspension 6 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.129 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 SVOC SW-846-8270D 123319 Hydroquinone 0.380 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 SVOC SW-846-8270D 108952 Phenol 0.0436 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00465 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 106990 1,3-butadiene 0.0120 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0225 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 71432 Benzene 0.00239 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 108907 Chlorobenzene 0.00232 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 67663 Chloroform 0.00545 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 126998 Chloroprene 0.0165 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 98828 Cumene 0.00287 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.127

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 100414 Ethylbenzene 0.00291 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0682

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00580 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.197

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 75092 Methylene chloride 0.0209 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 110543 n-Hexane 0.0835 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 108883 Toluene 0.00250 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00690 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00223 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 108054 Vinyl acetate 0.00337 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 01/19/13 Suspension 6 VC EPA Method 107 75014 Vinyl chloride 5.350

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00358 Non-detect

Axiall ABD MS 01/19/13 Suspension 6 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0036 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 Alcohol SW-846-8015C 107211 Ethylene glycol 6.5 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 Alcohol SW-846-8015C 67561 Methanol 790

Axiall ABD MS 01/20/13 Suspension 7 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.99

Axiall ABD MS 01/20/13 Suspension 7 Aldehyde SW-846-8315A 50000 Formaldehyde 1.2

Axiall ABD MS 01/20/13 Suspension 7 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 SVOC SW-846-8270D 98862 Acetophenone 14.7

Axiall ABD MS 01/20/13 Suspension 7 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 SVOC SW-846-8270D 123319 Hydroquinone 0.0316 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00465 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 106990 1,3-butadiene 0.0120 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0225 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 71432 Benzene 0.00239 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 108907 Chlorobenzene 0.00232 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 67663 Chloroform 0.00545 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 126998 Chloroprene 0.0165 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 98828 Cumene 0.00287 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00625 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 100414 Ethylbenzene 0.00291 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.386 Estimated value

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00580 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0362 Estimated value

12/12/2013 VI Confidential 107 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 75092 Methylene chloride 0.0209 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 110543 n-Hexane 0.0835 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 108883 Toluene 0.00250 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00690 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00223 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 108054 Vinyl acetate 0.00337 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 01/20/13 Suspension 7 VC EPA Method 107 75014 Vinyl chloride 0.766

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00358 Non-detect

Axiall ABD MS 01/20/13 Suspension 7 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0036 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 Alcohol SW-846-8015C 107211 Ethylene glycol 6.5 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 Alcohol SW-846-8015C 67561 Methanol 673

Axiall ABD MS 01/21/13 Suspension 8 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.70

Axiall ABD MS 01/21/13 Suspension 8 Aldehyde SW-846-8315A 50000 Formaldehyde 1.08

Axiall ABD MS 01/21/13 Suspension 8 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0657 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 SVOC SW-846-8270D 98862 Acetophenone 24.0

Axiall ABD MS 01/21/13 Suspension 8 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.107 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 SVOC SW-846-8270D 123319 Hydroquinone 0.0316 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 SVOC SW-846-8270D 108952 Phenol 0.0364 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00186 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 106990 1,3-butadiene 0.00480 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00900 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 71432 Benzene 0.00095 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 108907 Chlorobenzene 0.00092 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 67663 Chloroform 0.00218 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 126998 Chloroprene 0.00660 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 98828 Cumene 0.00115 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0322

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 100414 Ethylbenzene 0.00116 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0380

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00232 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.107

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 75092 Methylene chloride 0.00836 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 110543 n-Hexane 0.0334 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 108883 Toluene 0.00099 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00276 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00089 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 108054 Vinyl acetate 0.00135 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 01/21/13 Suspension 8 VC EPA Method 107 75014 Vinyl chloride 1.250

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00143 Non-detect

Axiall ABD MS 01/21/13 Suspension 8 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0014 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 Alcohol SW-846-8015C 107211 Ethylene glycol 0.8 Estimated value/detected in blank

Axiall ABD MS 01/22/13 Suspension 9 Alcohol SW-846-8015C 67561 Methanol 1250

Axiall ABD MS 01/22/13 Suspension 9 Aldehyde SW-846-8315A 75070 Acetaldehyde 32.4

Axiall ABD MS 01/22/13 Suspension 9 Aldehyde SW-846-8315A 50000 Formaldehyde 4.37

Axiall ABD MS 01/22/13 Suspension 9 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0678 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 SVOC SW-846-8270D 98862 Acetophenone 21.5

Axiall ABD MS 01/22/13 Suspension 9 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.111 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 SVOC SW-846-8270D 123319 Hydroquinone 0.319 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 SVOC SW-846-8270D 108952 Phenol 0.0375 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00186 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 106990 1,3-butadiene 0.00480 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00900 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 71432 Benzene 0.00095 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 108907 Chlorobenzene 0.00092 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 67663 Chloroform 0.00218 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 126998 Chloroprene 0.00660 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 98828 Cumene 0.00115 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0643

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 100414 Ethylbenzene 0.00116 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00560 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00232 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.144

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 75092 Methylene chloride 0.00836 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 110543 n-Hexane 0.0334 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 108883 Toluene 0.00099 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00276 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00089 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 108054 Vinyl acetate 0.00135 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 01/22/13 Suspension 9 VC EPA Method 107 75014 Vinyl chloride 1.82

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00143 Non-detect

Axiall ABD MS 01/22/13 Suspension 9 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00115 Non-detect

Axiall ABD MS 01/23/13 Suspension 10 Alcohol SW-846-8015C 107211 Ethylene glycol 1.0 Detected in blank

Axiall ABD MS 01/23/13 Suspension 10 Alcohol SW-846-8015C 67561 Methanol 910

Axiall ABD MS 01/23/13 Suspension 10 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.42

Axiall ABD MS 01/23/13 Suspension 10 Aldehyde SW-846-8315A 50000 Formaldehyde 0.381 Estimated Value

Axiall ABD MS 01/23/13 Suspension 10 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0678 Non-detect

Axiall ABD MS 01/23/13 Suspension 10 SVOC SW-846-8270D 98862 Acetophenone 19.7

Axiall ABD MS 01/23/13 Suspension 10 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.111 Non-detect

Axiall ABD MS 01/23/13 Suspension 10 SVOC SW-846-8270D 123319 Hydroquinone 0.306 Non-detect

Axiall ABD MS 01/23/13 Suspension 10 SVOC SW-846-8270D 108952 Phenol 0.0375 Non-detect

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 106990 1,3-butadiene 0.00240 Non-detect

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00450 Non-detect

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 126998 Chloroprene 0.00330 Non-detect

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 98828 Cumene 0.00335 Estimated Value

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.112

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.406

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.259

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00044 Non-detect

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00138 Non-detect

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Axiall ABD MS 01/23/13 Suspension 10 VC EPA Method 107 75014 Vinyl chloride 3.37

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall ABD MS 01/23/13 Suspension 10 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect

Axiall ABD MS 01/24/13 Suspension 11 Alcohol SW-846-8015C 107211 Ethylene glycol 10.4 Detected in blank

Axiall ABD MS 01/24/13 Suspension 11 Alcohol SW-846-8015C 67561 Methanol 901

Axiall ABD MS 01/24/13 Suspension 11 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.16

Axiall ABD MS 01/24/13 Suspension 11 Aldehyde SW-846-8315A 50000 Formaldehyde 0.223

Axiall ABD MS 01/24/13 Suspension 11 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0760 Non-detect

Axiall ABD MS 01/24/13 Suspension 11 SVOC SW-846-8270D 98862 Acetophenone 30.8

Axiall ABD MS 01/24/13 Suspension 11 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.124 Non-detect

Axiall ABD MS 01/24/13 Suspension 11 SVOC SW-846-8270D 123319 Hydroquinone 0.300 Non-detect

Axiall ABD MS 01/24/13 Suspension 11 SVOC SW-846-8270D 108952 Phenol 0.0420 Non-detect

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00186 Non-detect

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 106990 1,3-butadiene 0.00240 Non-detect

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00450 Non-detect

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 71432 Benzene 0.00095 Non-detect

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 108907 Chlorobenzene 0.00092 Non-detect

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 67663 Chloroform 0.00218 Non-detect

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 126998 Chloroprene 0.00660 Non-detect

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 98828 Cumene 0.00115 Non-detect

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0358

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 100414 Ethylbenzene 0.00116 Non-detect

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0382

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00232 Non-detect

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0859

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 75092 Methylene chloride 0.0265 Estimated value

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 110543 n-Hexane 0.0334 Non-detect

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 108883 Toluene 0.00099 Non-detect

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00276 Non-detect

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00089 Non-detect

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 108054 Vinyl acetate 0.00135 Non-detect

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 01/24/13 Suspension 11 VC EPA Method 107 75014 Vinyl chloride 0.934

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00143 Non-detect

Axiall ABD MS 01/24/13 Suspension 11 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0014 Non-detect

Axiall ABD MS 01/25/13 Suspension 12 Alcohol SW-846-8015C 107211 Ethylene glycol 19.7 Detected in blank

Axiall ABD MS 01/25/13 Suspension 12 Alcohol SW-846-8015C 67561 Methanol 2210

Axiall ABD MS 01/25/13 Suspension 12 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.63

Axiall ABD MS 01/25/13 Suspension 12 Aldehyde SW-846-8315A 50000 Formaldehyde 0.419

Axiall ABD MS 01/25/13 Suspension 12 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0686 Non-detect

Axiall ABD MS 01/25/13 Suspension 12 SVOC SW-846-8270D 98862 Acetophenone 38.1

Axiall ABD MS 01/25/13 Suspension 12 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.112 Non-detect

Axiall ABD MS 01/25/13 Suspension 12 SVOC SW-846-8270D 123319 Hydroquinone 0.357 Non-detect

Axiall ABD MS 01/25/13 Suspension 12 SVOC SW-846-8270D 108952 Phenol 0.0379 Non-detect

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00186 Non-detect

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 106990 1,3-butadiene 0.00480 Non-detect

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00900 Non-detect

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 71432 Benzene 0.00095 Non-detect

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 108907 Chlorobenzene 0.00092 Non-detect

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 67663 Chloroform 0.00412 Estimated value

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 126998 Chloroprene 0.00660 Non-detect

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 98828 Cumene 0.00115 Non-detect

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0694

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 100414 Ethylbenzene 0.00116 Non-detect

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.107

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00232 Non-detect

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.218

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 75092 Methylene chloride 0.0303 Estimated value

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 110543 n-Hexane 0.0334 Non-detect

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 108883 Toluene 0.00099 Non-detect

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00276 Non-detect

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00089 Non-detect

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 108054 Vinyl acetate 0.00135 Non-detect

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 01/25/13 Suspension 12 VC EPA Method 107 75014 Vinyl chloride 1.59

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00143 Non-detect

Axiall ABD MS 01/25/13 Suspension 12 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0014 Non-detect

Axiall ABD MS 01/26/13 Suspension 13 Alcohol SW-846-8015C 107211 Ethylene glycol 3.9 Detected in blank

Axiall ABD MS 01/26/13 Suspension 13 Alcohol SW-846-8015C 67561 Methanol 2300

Axiall ABD MS 01/26/13 Suspension 13 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.79

Axiall ABD MS 01/26/13 Suspension 13 Aldehyde SW-846-8315A 50000 Formaldehyde 0.987

Axiall ABD MS 01/26/13 Suspension 13 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0751 Non-detect

Axiall ABD MS 01/26/13 Suspension 13 SVOC SW-846-8270D 98862 Acetophenone 38.2

Axiall ABD MS 01/26/13 Suspension 13 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.123 Non-detect

Axiall ABD MS 01/26/13 Suspension 13 SVOC SW-846-8270D 123319 Hydroquinone 0.361 Non-detect

Axiall ABD MS 01/26/13 Suspension 13 SVOC SW-846-8270D 108952 Phenol 0.0415 Non-detect

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Non-detect

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Non-detect

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Non-detect

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 71432 Benzene 0.00004 Non-detect

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Non-detect

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 67663 Chloroform 0.00010 Non-detect

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 126998 Chloroprene 0.00033 Non-detect

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 98828 Cumene 0.00081 Estimated value

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0359

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Non-detect

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0369

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.123

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Non-detect

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 110543 n-Hexane 0.00167 Non-detect

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 108883 Toluene 0.00004 Non-detect

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Non-detect

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00075 Estimated value

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 108054 Vinyl acetate 0.0006 Non-detect

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 01/26/13 Suspension 13 VC EPA Method 107 75014 Vinyl chloride 1.01

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Non-detect

Axiall ABD MS 01/26/13 Suspension 13 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00007 Non-detect

Axiall ABD MS 01/27/13 Suspension 14 Alcohol SW-846-8015C 107211 Ethylene glycol 3.6 Detected in blank

Axiall ABD MS 01/27/13 Suspension 14 Alcohol SW-846-8015C 67561 Methanol 1710

Axiall ABD MS 01/27/13 Suspension 14 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.59

Axiall ABD MS 01/27/13 Suspension 14 Aldehyde SW-846-8315A 50000 Formaldehyde 0.918

12/12/2013 VI Confidential 109 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Axiall ABD MS 01/27/13 Suspension 14 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Axiall ABD MS 01/27/13 Suspension 14 SVOC SW-846-8270D 98862 Acetophenone 39.9

Axiall ABD MS 01/27/13 Suspension 14 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Axiall ABD MS 01/27/13 Suspension 14 SVOC SW-846-8270D 123319 Hydroquinone 0.345 Non-detect

Axiall ABD MS 01/27/13 Suspension 14 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Non-detect

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Non-detect

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Non-detect

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 71432 Benzene 0.00004 Non-detect

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Non-detect

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 67663 Chloroform 0.00010 Non-detect

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 126998 Chloroprene 0.00033 Non-detect

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 98828 Cumene 0.00129

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0755

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Non-detect

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0521

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.245

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Non-detect

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 110543 n-Hexane 0.00167 Non-detect

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 108883 Toluene 0.00004 Non-detect

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Non-detect

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00128

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Non-detect

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 01/27/13 Suspension 14 VC EPA Method 107 75014 Vinyl chloride 1.54

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Non-detect

Axiall ABD MS 01/27/13 Suspension 14 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00007 Non-detect

Axiall ABD MS 01/28/13 Suspension 15 Alcohol SW-846-8015C 107211 Ethylene glycol 3.2 Detected in blank

Axiall ABD MS 01/28/13 Suspension 15 Alcohol SW-846-8015C 67561 Methanol 1580

Axiall ABD MS 01/28/13 Suspension 15 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.25

Axiall ABD MS 01/28/13 Suspension 15 Aldehyde SW-846-8315A 50000 Formaldehyde 0.978

Axiall ABD MS 01/28/13 Suspension 15 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0742 Non-detect

Axiall ABD MS 01/28/13 Suspension 15 SVOC SW-846-8270D 98862 Acetophenone 16.8

Axiall ABD MS 01/28/13 Suspension 15 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.121 Non-detect

Axiall ABD MS 01/28/13 Suspension 15 SVOC SW-846-8270D 123319 Hydroquinone 0.385 Non-detect

Axiall ABD MS 01/28/13 Suspension 15 SVOC SW-846-8270D 108952 Phenol 0.0411 Non-detect

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Non-detect

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Non-detect

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Non-detect

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 71432 Benzene 0.00004 Non-detect

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Non-detect

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 67663 Chloroform 0.00010 Non-detect

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 126998 Chloroprene 0.00033 Non-detect

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 98828 Cumene 0.00157

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0609

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Non-detect

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0448

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.170

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Non-detect

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 110543 n-Hexane 0.00167 Non-detect

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 108883 Toluene 0.00004 Non-detect

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Non-detect

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00106

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Non-detect

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 01/28/13 Suspension 15 VC EPA Method 107 75014 Vinyl chloride 1.32

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Non-detect

Axiall ABD MS 01/28/13 Suspension 15 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00007 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 Alcohol SW-846-8015C 67561 Methanol 201

Axiall ABD MS 01/29/13 Suspension 16 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.26

Axiall ABD MS 01/29/13 Suspension 16 Aldehyde SW-846-8315A 50000 Formaldehyde 0.496

Axiall ABD MS 01/29/13 Suspension 16 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 SVOC SW-846-8270D 98862 Acetophenone 10.7

Axiall ABD MS 01/29/13 Suspension 16 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 SVOC SW-846-8270D 123319 Hydroquinone 0.300 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00929 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 106990 1,3-butadiene 0.0240 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0450 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 71432 Benzene 0.00478 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 108907 Chlorobenzene 0.00463 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 67663 Chloroform 0.0109 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 126998 Chloroprene 0.0330 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 98828 Cumene 0.00573 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0125 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 100414 Ethylbenzene 0.00581 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0280 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0116 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0538 Estimated value

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 75092 Methylene chloride 0.179 Estimated value

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 110543 n-Hexane 0.167 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 108883 Toluene 0.00499 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0138 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00445 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 108054 Vinyl acetate 0.00674 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 01/29/13 Suspension 16 VC EPA Method 107 75014 Vinyl chloride 0.718

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00716 Non-detect

Axiall ABD MS 01/29/13 Suspension 16 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0072 Non-detect

Axiall ABD MS 01/30/13 Suspension 17 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall ABD MS 01/30/13 Suspension 17 Alcohol SW-846-8015C 67561 Methanol 71.5

Axiall ABD MS 01/30/13 Suspension 17 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.39

Axiall ABD MS 01/30/13 Suspension 17 Aldehyde SW-846-8315A 50000 Formaldehyde 0.653

Axiall ABD MS 01/30/13 Suspension 17 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0701 Non-detect

Axiall ABD MS 01/30/13 Suspension 17 SVOC SW-846-8270D 98862 Acetophenone 14.4

Axiall ABD MS 01/30/13 Suspension 17 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.115 Non-detect

Axiall ABD MS 01/30/13 Suspension 17 SVOC SW-846-8270D 123319 Hydroquinone 0.333 Non-detect

Axiall ABD MS 01/30/13 Suspension 17 SVOC SW-846-8270D 108952 Phenol 0.0388 Non-detect

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00186 Non-detect

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 106990 1,3-butadiene 0.00480 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00900 Non-detect

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 71432 Benzene 0.00095 Non-detect

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 108907 Chlorobenzene 0.00092 Non-detect

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 67663 Chloroform 0.00218 Non-detect

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 126998 Chloroprene 0.00660 Non-detect

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 98828 Cumene 0.00115 Non-detect

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.101

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 100414 Ethylbenzene 0.00116 Non-detect

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0786

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00232 Non-detect

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.250

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 75092 Methylene chloride 0.0329 Estimated value

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 110543 n-Hexane 0.0334 Non-detect

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 108883 Toluene 0.00099 Non-detect

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00276 Non-detect

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00089 Non-detect

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 108054 Vinyl acetate 0.00135 Non-detect

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 01/30/13 Suspension 17 VC EPA Method 107 75014 Vinyl chloride 2.92

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00143 Non-detect

Axiall ABD MS 01/30/13 Suspension 17 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0014 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 Alcohol SW-846-8015C 67561 Methanol 97.0

Axiall ABD MS 01/31/13 Suspension 18 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.28

Axiall ABD MS 01/31/13 Suspension 18 Aldehyde SW-846-8315A 50000 Formaldehyde 1.29

Axiall ABD MS 01/31/13 Suspension 18 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0709 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 SVOC SW-846-8270D 98862 Acetophenone 22.4

Axiall ABD MS 01/31/13 Suspension 18 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.116 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 SVOC SW-846-8270D 123319 Hydroquinone 0.361 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 SVOC SW-846-8270D 108952 Phenol 0.0392 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00465 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 106990 1,3-butadiene 0.0120 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0225 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 71432 Benzene 0.00239 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 108907 Chlorobenzene 0.00232 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 67663 Chloroform 0.00545 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 126998 Chloroprene 0.0165 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 98828 Cumene 0.00287 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0466 Estimated value

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 100414 Ethylbenzene 0.00291 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0798

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00580 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.141

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 75092 Methylene chloride 0.0209 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 110543 n-Hexane 0.0835 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 108883 Toluene 0.00250 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00690 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00223 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 108054 Vinyl acetate 0.00337 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 01/31/13 Suspension 18 VC EPA Method 107 75014 Vinyl chloride 1.26

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00358 Non-detect

Axiall ABD MS 01/31/13 Suspension 18 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0036 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 Alcohol SW-846-8015C 67561 Methanol 175

Axiall ABD MS 02/01/13 Suspension 19 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.59

Axiall ABD MS 02/01/13 Suspension 19 Aldehyde SW-846-8315A 50000 Formaldehyde 1.15

Axiall ABD MS 02/01/13 Suspension 19 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0678 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 SVOC SW-846-8270D 98862 Acetophenone 28.0

Axiall ABD MS 02/01/13 Suspension 19 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.111 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 SVOC SW-846-8270D 123319 Hydroquinone 0.357 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 SVOC SW-846-8270D 108952 Phenol 0.0375 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00465 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 106990 1,3-butadiene 0.0120 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0225 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 71432 Benzene 0.00239 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 108907 Chlorobenzene 0.00232 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 67663 Chloroform 0.00545 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 126998 Chloroprene 0.0165 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 98828 Cumene 0.00287 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.224

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 100414 Ethylbenzene 0.00291 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.235

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00580 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.396

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 75092 Methylene chloride 0.0209 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 110543 n-Hexane 0.0835 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 108883 Toluene 0.00250 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00690 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00223 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 108054 Vinyl acetate 0.00337 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 02/01/13 Suspension 19 VC EPA Method 107 75014 Vinyl chloride 3.00

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00358 Non-detect

Axiall ABD MS 02/01/13 Suspension 19 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0036 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 Alcohol SW-846-8015C 67561 Methanol 116

Axiall ABD MS 02/02/13 Suspension 20 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.50

Axiall ABD MS 02/02/13 Suspension 20 Aldehyde SW-846-8315A 50000 Formaldehyde 0.912

Axiall ABD MS 02/02/13 Suspension 20 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0760 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 SVOC SW-846-8270D 98862 Acetophenone 20.8

Axiall ABD MS 02/02/13 Suspension 20 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0124 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 SVOC SW-846-8270D 123319 Hydroquinone 0.349 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 SVOC SW-846-8270D 108952 Phenol 0.0420 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00465 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 106990 1,3-butadiene 0.0518

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0225 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 71432 Benzene 0.00239 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 108907 Chlorobenzene 0.00232 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 67663 Chloroform 0.00545 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 126998 Chloroprene 0.0165 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 98828 Cumene 0.00287 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.117

12/12/2013 VI Confidential 111 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 100414 Ethylbenzene 0.00291 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0140 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00580 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.305

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 75092 Methylene chloride 0.0209 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 110543 n-Hexane 0.0835 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 108883 Toluene 0.00250 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00690 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00223 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 108054 Vinyl acetate 0.00337 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 02/02/13 Suspension 20 VC EPA Method 107 75014 Vinyl chloride 2.79

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00358 Non-detect

Axiall ABD MS 02/02/13 Suspension 20 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00358 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 Alcohol SW-846-8015C 67561 Methanol 216

Axiall ABD MS 02/03/13 Suspension 21 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.63

Axiall ABD MS 02/03/13 Suspension 21 Aldehyde SW-846-8315A 50000 Formaldehyde 1.16

Axiall ABD MS 02/03/13 Suspension 21 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0734 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 SVOC SW-846-8270D 98862 Acetophenone 20.4

Axiall ABD MS 02/03/13 Suspension 21 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.120 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 SVOC SW-846-8270D 123319 Hydroquinone 0.357 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 SVOC SW-846-8270D 108952 Phenol 0.0406 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00465 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 106990 1,3-butadiene 0.0470 Estimated Value

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0225 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 71432 Benzene 0.00239 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 108907 Chlorobenzene 0.00232 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 67663 Chloroform 0.00545 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 126998 Chloroprene 0.0165 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 98828 Cumene 0.00287 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0957

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 100414 Ethylbenzene 0.00291 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.109

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00580 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.211

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 75092 Methylene chloride 0.0209 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 110543 n-Hexane 0.0835 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 108883 Toluene 0.00250 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00690 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00223 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 108054 Vinyl acetate 0.00337 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 02/03/13 Suspension 21 VC EPA Method 107 75014 Vinyl chloride 1.54

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00358 Non-detect

Axiall ABD MS 02/03/13 Suspension 21 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0036 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 Alcohol SW-846-8015C 67561 Methanol 120

Axiall ABD MS 02/04/13 Suspension 22 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.02

Axiall ABD MS 02/04/13 Suspension 22 Aldehyde SW-846-8315A 50000 Formaldehyde 1.22

Axiall ABD MS 02/04/13 Suspension 22 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0779 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 SVOC SW-846-8270D 98862 Acetophenone 26.6

Axiall ABD MS 02/04/13 Suspension 22 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.127 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 SVOC SW-846-8270D 123319 Hydroquinone 0.437 Estimated value

Axiall ABD MS 02/04/13 Suspension 22 SVOC SW-846-8270D 108952 Phenol 0.0431 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00465 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 106990 1,3-butadiene 0.0120 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0225 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 71432 Benzene 0.00239 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 108907 Chlorobenzene 0.00232 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 67663 Chloroform 0.00545 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 126998 Chloroprene 0.0165 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 98828 Cumene 0.00287 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0447 Estimated value

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 100414 Ethylbenzene 0.00291 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0705

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00580 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.111

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 75092 Methylene chloride 0.0209 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 110543 n-Hexane 0.0835 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 108883 Toluene 0.00250 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00690 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00223 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 108054 Vinyl acetate 0.00337 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 02/04/13 Suspension 22 VC EPA Method 107 75014 Vinyl chloride 1.15

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00358 Non-detect

Axiall ABD MS 02/04/13 Suspension 22 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0036 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 Alcohol SW-846-8015C 67561 Methanol 111

Axiall ABD MS 02/05/13 Suspension 23 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.66

Axiall ABD MS 02/05/13 Suspension 23 Aldehyde SW-846-8315A 50000 Formaldehyde 1.97

Axiall ABD MS 02/05/13 Suspension 23 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0657 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 SVOC SW-846-8270D 98862 Acetophenone 18.3

Axiall ABD MS 02/05/13 Suspension 23 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.107 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 SVOC SW-846-8270D 123319 Hydroquinone 0.333 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 SVOC SW-846-8270D 108952 Phenol 0.0364 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 106990 1,3-butadiene 0.00240 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00450 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 67663 Chloroform 0.0141

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 126998 Chloroprene 0.00330 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.101

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00280 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.385

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 02/05/13 Suspension 23 VC EPA Method 107 75014 Vinyl chloride 1.68

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall ABD MS 02/05/13 Suspension 23 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 Alcohol SW-846-8015C 107211 Ethylene glycol 2.0

Axiall ABD MS 02/06/13 Suspension 24 Alcohol SW-846-8015C 67561 Methanol 242

Axiall ABD MS 02/06/13 Suspension 24 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.65

Axiall ABD MS 02/06/13 Suspension 24 Aldehyde SW-846-8315A 50000 Formaldehyde 1.11

Axiall ABD MS 02/06/13 Suspension 24 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0725 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 SVOC SW-846-8270D 98862 Acetophenone 17.8

Axiall ABD MS 02/06/13 Suspension 24 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.119 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 SVOC SW-846-8270D 123319 Hydroquinone 0.341 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 SVOC SW-846-8270D 108952 Phenol 0.0401 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00465 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 106990 1,3-butadiene 0.0120 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0225 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 71432 Benzene 0.00239 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 108907 Chlorobenzene 0.00232 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 67663 Chloroform 0.00545 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 126998 Chloroprene 0.0165 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 98828 Cumene 0.00287 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.191

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 100414 Ethylbenzene 0.00291 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.132

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00580 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.449

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 75092 Methylene chloride 0.0209 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 110543 n-Hexane 0.0835 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 108883 Toluene 0.00250 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00690 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0223 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 108054 Vinyl acetate 0.00337 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 02/06/13 Suspension 24 VC EPA Method 107 75014 Vinyl chloride 3.11

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00358 Non-detect

Axiall ABD MS 02/06/13 Suspension 24 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0036 Non-detect

Axiall ABD MS 02/07/13 Suspension 25 Alcohol SW-846-8015C 107211 Ethylene glycol 3.3 Detected in blank

Axiall ABD MS 02/07/13 Suspension 25 Alcohol SW-846-8015C 67561 Methanol 273

Axiall ABD MS 02/07/13 Suspension 25 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.92

Axiall ABD MS 02/07/13 Suspension 25 Aldehyde SW-846-8315A 50000 Formaldehyde 0.960

Axiall ABD MS 02/07/13 Suspension 25 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0742 Non-detect

Axiall ABD MS 02/07/13 Suspension 25 SVOC SW-846-8270D 98862 Acetophenone 21.8

Axiall ABD MS 02/07/13 Suspension 25 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.121 Non-detect

Axiall ABD MS 02/07/13 Suspension 25 SVOC SW-846-8270D 123319 Hydroquinone 0.323 Non-detect

Axiall ABD MS 02/07/13 Suspension 25 SVOC SW-846-8270D 108952 Phenol 0.0411 Non-detect

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 106990 1,3-butadiene 0.00240 Non-detect

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00450 Non-detect

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 126998 Chloroprene 0.00330 Non-detect

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0453

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 100414 Ethylbenzene 0.00394 Estimated value; detected in blank

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0467

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.124

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 02/07/13 Suspension 25 VC EPA Method 107 75014 Vinyl chloride 0.976

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall ABD MS 02/07/13 Suspension 25 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 Alcohol SW-846-8015C 67561 Methanol 149

Axiall ABD MS 02/08/13 Suspension 26 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.47

Axiall ABD MS 02/08/13 Suspension 26 Aldehyde SW-846-8315A 50000 Formaldehyde 1.25

Axiall ABD MS 02/08/13 Suspension 26 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.077 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 SVOC SW-846-8270D 98862 Acetophenone 23.4

Axiall ABD MS 02/08/13 Suspension 26 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.126 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 SVOC SW-846-8270D 123319 Hydroquinone 0.390 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 SVOC SW-846-8270D 108952 Phenol 0.0426 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 106990 1,3-butadiene 0.00240 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00450 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 126998 Chloroprene 0.00330 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.11

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 100414 Ethylbenzene 0.00269 Estimated value; detected in blank

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0684

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.230

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 02/08/13 Suspension 26 VC EPA Method 107 75014 Vinyl chloride 2.95

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall ABD MS 02/08/13 Suspension 26 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect

12/12/2013 VI Confidential 113 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Axiall ABD MS 02/09/13 Suspension 27 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 Alcohol SW-846-8015C 67561 Methanol 153

Axiall ABD MS 02/09/13 Suspension 27 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.34

Axiall ABD MS 02/09/13 Suspension 27 Aldehyde SW-846-8315A 50000 Formaldehyde 0.775

Axiall ABD MS 02/09/13 Suspension 27 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0760 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 SVOC SW-846-8270D 98862 Acetophenone 21.8

Axiall ABD MS 02/09/13 Suspension 27 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.124 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 SVOC SW-846-8270D 123319 Hydroquinone 0.323 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 SVOC SW-846-8270D 108952 Phenol 0.0420 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 106990 1,3-butadiene 0.00240 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00450 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 126998 Chloroprene 0.00330 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0182

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0155

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0299

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 02/09/13 Suspension 27 VC EPA Method 107 75014 Vinyl chloride 0.406

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall ABD MS 02/09/13 Suspension 27 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect

Axiall ABD MS 02/10/13 Suspension 28 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall ABD MS 02/10/13 Suspension 28 Alcohol SW-846-8015C 67561 Methanol 162

Axiall ABD MS 02/10/13 Suspension 28 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.82

Axiall ABD MS 02/10/13 Suspension 28 Aldehyde SW-846-8315A 50000 Formaldehyde 0.798

Axiall ABD MS 02/10/13 Suspension 28 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Axiall ABD MS 02/10/13 Suspension 28 SVOC SW-846-8270D 98862 Acetophenone 37

Axiall ABD MS 02/10/13 Suspension 28 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Axiall ABD MS 02/10/13 Suspension 28 SVOC SW-846-8270D 123319 Hydroquinone 0.323 Non-detect

Axiall ABD MS 02/10/13 Suspension 28 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00465 Non-detect

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 106990 1,3-butadiene 0.0120 Non-detect

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.02250 Non-detect

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 71432 Benzene 0.00239 Non-detect

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 108907 Chlorobenzene 0.00232 Non-detect

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 67663 Chloroform 0.00545 Non-detect

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 126998 Chloroprene 0.01650 Non-detect

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 98828 Cumene 0.00287 Non-detect

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0516

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 100414 Ethylbenzene 0.00291 Non-detect

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.124

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00580 Estimated value

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.112

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 75092 Methylene chloride 0.0938 Estimated value

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 110543 n-Hexane 0.0835 Non-detect

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 108883 Toluene 0.00250 Non-detect

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00690 Non-detect

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00223 Non-detect

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 108054 Vinyl acetate 0.00337 Non-detect

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 02/10/13 Suspension 28 VC EPA Method 107 75014 Vinyl chloride 1.12

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00906 Estimated value

Axiall ABD MS 02/10/13 Suspension 28 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 Alcohol SW-846-8015C 67561 Methanol 169

Axiall ABD MS 02/11/13 Suspension 29 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.11

Axiall ABD MS 02/11/13 Suspension 29 Aldehyde SW-846-8315A 50000 Formaldehyde 1.69

Axiall ABD MS 02/11/13 Suspension 29 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0686 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 SVOC SW-846-8270D 98862 Acetophenone 29.5

Axiall ABD MS 02/11/13 Suspension 29 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.112 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 SVOC SW-846-8270D 123319 Hydroquinone 0.333 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 SVOC SW-846-8270D 108952 Phenol 0.0379 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00465 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 106990 1,3-butadiene 0.0120 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0225 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 71432 Benzene 0.00239 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 108907 Chlorobenzene 0.00232 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 67663 Chloroform 0.00545 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 126998 Chloroprene 0.0165 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 98828 Cumene 0.00287 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0654

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 100414 Ethylbenzene 0.00291 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0900

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00580 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.139

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 75092 Methylene chloride 0.0822 Estimated value

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 110543 n-Hexane 0.0835 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 108883 Toluene 0.00250 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00690 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00223 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 108054 Vinyl acetate 0.00337 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 02/11/13 Suspension 29 VC EPA Method 107 75014 Vinyl chloride 1.08

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00358 Non-detect

Axiall ABD MS 02/11/13 Suspension 29 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0036 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 Alcohol SW-846-8015C 67561 Methanol 117

Axiall ABD MS 02/12/13 Suspension 30 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.75

Axiall ABD MS 02/12/13 Suspension 30 Aldehyde SW-846-8315A 50000 Formaldehyde 0.973

Axiall ABD MS 02/12/13 Suspension 30 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0686 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 SVOC SW-846-8270D 98862 Acetophenone 27.3

Axiall ABD MS 02/12/13 Suspension 30 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.112 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Axiall ABD MS 02/12/13 Suspension 30 SVOC SW-846-8270D 123319 Hydroquinone 0.337 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 SVOC SW-846-8270D 108952 Phenol 0.0379 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00465 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 106990 1,3-butadiene 0.0120 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0225 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 71432 Benzene 0.00239 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 108907 Chlorobenzene 0.00232 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 67663 Chloroform 0.00545 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 126998 Chloroprene 0.0165 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 98828 Cumene 0.00287 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00625 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 100414 Ethylbenzene 0.00291 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0535

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00580 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0604

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 75092 Methylene chloride 0.0209 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 110543 n-Hexane 0.0835 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 108883 Toluene 0.00250 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00690 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00223 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 108054 Vinyl acetate 0.00337 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall ABD MS 02/12/13 Suspension 30 VC EPA Method 107 75014 Vinyl chloride 0.391

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00358 Non-detect

Axiall ABD MS 02/12/13 Suspension 30 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0036 Non-detect

Axiall PLQ LA 01/14/13 Suspension 1 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall PLQ LA 01/14/13 Suspension 1 Alcohol SW-846-8015C 67561 Methanol 156

Axiall PLQ LA 01/14/13 Suspension 1 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.15

Axiall PLQ LA 01/14/13 Suspension 1 Aldehyde SW-846-8315A 50000 Formaldehyde 17.7

Axiall PLQ LA 01/14/13 Suspension 1 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Axiall PLQ LA 01/14/13 Suspension 1 SVOC SW-846-8270D 98862 Acetophenone 3.96

Axiall PLQ LA 01/14/13 Suspension 1 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Axiall PLQ LA 01/14/13 Suspension 1 SVOC SW-846-8270D 123319 Hydroquinone 1.68

Axiall PLQ LA 01/14/13 Suspension 1 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 98828 Cumene 0.00205

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0732

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00318

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00751

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 01/14/13 Suspension 1 VC EPA Method 107 75014 Vinyl chloride 1.47

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 01/14/13 Suspension 1 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 01/15/13 Suspension 2 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall PLQ LA 01/15/13 Suspension 2 Alcohol SW-846-8015C 67561 Methanol 0.2 Non-detect

Axiall PLQ LA 01/15/13 Suspension 2 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.28

Axiall PLQ LA 01/15/13 Suspension 2 Aldehyde SW-846-8315A 50000 Formaldehyde 14.8

Axiall PLQ LA 01/15/13 Suspension 2 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0664 Non-detect

Axiall PLQ LA 01/15/13 Suspension 2 SVOC SW-846-8270D 98862 Acetophenone 3.94

Axiall PLQ LA 01/15/13 Suspension 2 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.109 Non-detect

Axiall PLQ LA 01/15/13 Suspension 2 SVOC SW-846-8270D 123319 Hydroquinone 2.52

Axiall PLQ LA 01/15/13 Suspension 2 SVOC SW-846-8270D 108952 Phenol 0.0367 Non-detect

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Non-detect

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Non-detect

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Non-detect

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 71432 Benzene 0.00004 Non-detect

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Non-detect

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 67663 Chloroform 0.0001 Non-detect

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 126998 Chloroprene 0.00033 Non-detect

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 98828 Cumene 0.00068

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0171

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Non-detect

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00111

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00336

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Non-detect

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 110543 n-Hexane 0.00167 Non-detect

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 108883 Toluene 0.00004 Non-detect

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Non-detect

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Non-detect

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Non-detect

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 01/15/13 Suspension 2 VC EPA Method 107 75014 Vinyl chloride 0.478

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Non-detect

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) Detection Limit Not ReportedNon-detect VI Note (7) and (8)

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 179601231 m,p-xylene 0.00012 Non-detect VI Note (7)

Axiall PLQ LA 01/15/13 Suspension 2 VOC SW-846-8260B 95476 o-xylene 0.00007 Non-detect VI Note (7)

Axiall PLQ LA 01/16/13 Suspension 3 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall PLQ LA 01/16/13 Suspension 3 Alcohol SW-846-8015C 67561 Methanol 0.2 Non-detect

Axiall PLQ LA 01/16/13 Suspension 3 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.2

Axiall PLQ LA 01/16/13 Suspension 3 Aldehyde SW-846-8315A 50000 Formaldehyde 16.5

Axiall PLQ LA 01/16/13 Suspension 3 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0678 Non-detect

Axiall PLQ LA 01/16/13 Suspension 3 SVOC SW-846-8270D 98862 Acetophenone 5.73

Axiall PLQ LA 01/16/13 Suspension 3 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.111 Non-detect

Axiall PLQ LA 01/16/13 Suspension 3 SVOC SW-846-8270D 123319 Hydroquinone 3.56

Axiall PLQ LA 01/16/13 Suspension 3 SVOC SW-846-8270D 108952 Phenol 0.0375 Non-detect

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Non-detect

12/12/2013 VI Confidential 115 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Non-detect

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Non-detect

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 71432 Benzene 0.00004 Non-detect

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Non-detect

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 67663 Chloroform 0.0001 Non-detect

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 126998 Chloroprene 0.00033 Non-detect

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 98828 Cumene 0.00054

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0192

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Non-detect

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00154

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00516

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 75092 Methylene chloride 0.00041

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 110543 n-Hexane 0.00167 Non-detect

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 108883 Toluene 0.00004 Non-detect

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Non-detect

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Non-detect

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Non-detect

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 01/16/13 Suspension 3 VC EPA Method 107 75014 Vinyl chloride 0.486

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Non-detect

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) Detection Limit Not ReportedNon-detect VI Note (7) and (8)

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 179601231 m,p-xylene 0.00012 Non-detect VI Note (7)

Axiall PLQ LA 01/16/13 Suspension 3 VOC SW-846-8260B 95476 o-xylene 0.00007 Non-detect VI Note (7)

Axiall PLQ LA 01/17/13 Suspension 4 Alcohol SW-846-8015C 107211 Ethylene glycol 1.3 Non-detect

Axiall PLQ LA 01/17/13 Suspension 4 Alcohol SW-846-8015C 67561 Methanol 135

Axiall PLQ LA 01/17/13 Suspension 4 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.885

Axiall PLQ LA 01/17/13 Suspension 4 Aldehyde SW-846-8315A 50000 Formaldehyde 0.923

Axiall PLQ LA 01/17/13 Suspension 4 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0709 Non-detect

Axiall PLQ LA 01/17/13 Suspension 4 SVOC SW-846-8270D 98862 Acetophenone 6.7

Axiall PLQ LA 01/17/13 Suspension 4 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.116 Non-detect

Axiall PLQ LA 01/17/13 Suspension 4 SVOC SW-846-8270D 123319 Hydroquinone 2.43

Axiall PLQ LA 01/17/13 Suspension 4 SVOC SW-846-8270D 108952 Phenol 0.0392 Non-detect

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Non-detect

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Non-detect

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Non-detect

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 71432 Benzene 0.00004 Non-detect

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Non-detect

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 67663 Chloroform 0.0001 Non-detect

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 126998 Chloroprene 0.00033 Non-detect

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 98828 Cumene 0.00206

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.047

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Non-detect

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00215

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00226

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Non-detect

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 110543 n-Hexane 0.00167 Non-detect

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 108883 Toluene 0.00004 Non-detect

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Non-detect

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Non-detect

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Non-detect

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 01/17/13 Suspension 4 VC EPA Method 107 75014 Vinyl chloride 0.638

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Non-detect

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) Detection Limit Not ReportedNon-detect VI Note (7) and (8)

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 179601231 m,p-xylene 0.00012 Non-detect VI Note (7)

Axiall PLQ LA 01/17/13 Suspension 4 VOC SW-846-8260B 95476 o-xylene 0.00007 Non-detect VI Note (7)

Axiall PLQ LA 01/18/13 Suspension 5 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall PLQ LA 01/18/13 Suspension 5 Alcohol SW-846-8015C 67561 Methanol 0.2 Non-detect

Axiall PLQ LA 01/18/13 Suspension 5 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.24

Axiall PLQ LA 01/18/13 Suspension 5 Aldehyde SW-846-8315A 50000 Formaldehyde 17.2

Axiall PLQ LA 01/18/13 Suspension 5 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0709 Non-detect

Axiall PLQ LA 01/18/13 Suspension 5 SVOC SW-846-8270D 98862 Acetophenone 5.77

Axiall PLQ LA 01/18/13 Suspension 5 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.116 Non-detect

Axiall PLQ LA 01/18/13 Suspension 5 SVOC SW-846-8270D 123319 Hydroquinone 3.8

Axiall PLQ LA 01/18/13 Suspension 5 SVOC SW-846-8270D 108952 Phenol 0.0392 Non-detect

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Non-detect

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Non-detect

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Non-detect

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 71432 Benzene 0.00004 Non-detect

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Non-detect

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 67663 Chloroform 0.0001 Non-detect

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 126998 Chloroprene 0.00033 Non-detect

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 98828 Cumene 0.00346

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.1

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Non-detect

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00498

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00618

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Non-detect

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 110543 n-Hexane 0.00167 Non-detect

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 108883 Toluene 0.00004 Non-detect

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Non-detect

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Non-detect

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Non-detect

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 01/18/13 Suspension 5 VC EPA Method 107 75014 Vinyl chloride 1.99

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Non-detect

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) Detection Limit Not ReportedNon-detect VI Note (7) and (8)

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 179601231 m,p-xylene 0.00012 Non-detect VI Note (7)

Axiall PLQ LA 01/18/13 Suspension 5 VOC SW-846-8260B 95476 o-xylene 0.00007 Non-detect VI Note (7)

Axiall PLQ LA 01/19/13 Suspension 6 Alcohol SW-846-8015C 107211 Ethylene glycol 3.2 Non-detect

Axiall PLQ LA 01/19/13 Suspension 6 Alcohol SW-846-8015C 67561 Methanol 357

Axiall PLQ LA 01/19/13 Suspension 6 Aldehyde SW-846-8315A 75070 Acetaldehyde 12.7

Axiall PLQ LA 01/19/13 Suspension 6 Aldehyde SW-846-8315A 50000 Formaldehyde 8.18

Axiall PLQ LA 01/19/13 Suspension 6 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0671 Non-detect

Axiall PLQ LA 01/19/13 Suspension 6 SVOC SW-846-8270D 98862 Acetophenone 4.9

Axiall PLQ LA 01/19/13 Suspension 6 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.11 Non-detect

Axiall PLQ LA 01/19/13 Suspension 6 SVOC SW-846-8270D 123319 Hydroquinone 7.55

Axiall PLQ LA 01/19/13 Suspension 6 SVOC SW-846-8270D 108952 Phenol 0.0371 Non-detect

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 98828 Cumene 0.00402

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.249

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0118

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0295

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 75092 Methylene chloride 0.0122

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 01/19/13 Suspension 6 VC EPA Method 107 75014 Vinyl chloride 6.22

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 01/19/13 Suspension 6 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 01/20/13 Suspension 7 Alcohol SW-846-8015C 107211 Ethylene glycol 3.2 Non-detect

Axiall PLQ LA 01/20/13 Suspension 7 Alcohol SW-846-8015C 67561 Methanol 414

Axiall PLQ LA 01/20/13 Suspension 7 Aldehyde SW-846-8315A 75070 Acetaldehyde 15.4

Axiall PLQ LA 01/20/13 Suspension 7 Aldehyde SW-846-8315A 50000 Formaldehyde 4.6

Axiall PLQ LA 01/20/13 Suspension 7 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0644 Non-detect

Axiall PLQ LA 01/20/13 Suspension 7 SVOC SW-846-8270D 98862 Acetophenone 6.16

Axiall PLQ LA 01/20/13 Suspension 7 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.105 Non-detect

Axiall PLQ LA 01/20/13 Suspension 7 SVOC SW-846-8270D 123319 Hydroquinone 2.39

Axiall PLQ LA 01/20/13 Suspension 7 SVOC SW-846-8270D 108952 Phenol 0.0356 Non-detect

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0791

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0078

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0103

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 75092 Methylene chloride 0.0126

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 01/20/13 Suspension 7 VC EPA Method 107 75014 Vinyl chloride 1.54

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 01/20/13 Suspension 7 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 01/21/13 Suspension 8 Alcohol SW-846-8015C 107211 Ethylene glycol 3.2 Non-detect

Axiall PLQ LA 01/21/13 Suspension 8 Alcohol SW-846-8015C 67561 Methanol 382

Axiall PLQ LA 01/21/13 Suspension 8 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.472

Axiall PLQ LA 01/21/13 Suspension 8 Aldehyde SW-846-8315A 50000 Formaldehyde 0.499

Axiall PLQ LA 01/21/13 Suspension 8 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Axiall PLQ LA 01/21/13 Suspension 8 SVOC SW-846-8270D 98862 Acetophenone 2.14

Axiall PLQ LA 01/21/13 Suspension 8 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Axiall PLQ LA 01/21/13 Suspension 8 SVOC SW-846-8270D 123319 Hydroquinone 10.6

Axiall PLQ LA 01/21/13 Suspension 8 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0237

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0028

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.013

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 75092 Methylene chloride 0.0153

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 01/21/13 Suspension 8 VC EPA Method 107 75014 Vinyl chloride 0.635

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 01/21/13 Suspension 8 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 01/22/13 Suspension 9 Alcohol SW-846-8015C 107211 Ethylene glycol 1.3 Non-detect

Axiall PLQ LA 01/22/13 Suspension 9 Alcohol SW-846-8015C 67561 Methanol 173

Axiall PLQ LA 01/22/13 Suspension 9 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.03

Axiall PLQ LA 01/22/13 Suspension 9 Aldehyde SW-846-8315A 50000 Formaldehyde 0.758

Axiall PLQ LA 01/22/13 Suspension 9 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0644 Non-detect

Axiall PLQ LA 01/22/13 Suspension 9 SVOC SW-846-8270D 98862 Acetophenone 4.63

Axiall PLQ LA 01/22/13 Suspension 9 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.105 Non-detect

Axiall PLQ LA 01/22/13 Suspension 9 SVOC SW-846-8270D 123319 Hydroquinone 2.52

Axiall PLQ LA 01/22/13 Suspension 9 SVOC SW-846-8270D 108952 Phenol 0.0356 Non-detect

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

12/12/2013 VI Confidential 117 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 98828 Cumene 0.00199

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0642

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00715

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00359

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 01/22/13 Suspension 9 VC EPA Method 107 75014 Vinyl chloride 1.23

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 01/22/13 Suspension 9 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 01/22/13 Suspension 10 Alcohol SW-846-8015C 107211 Ethylene glycol 1.3 Non-detect duplicate

Axiall PLQ LA 01/22/13 Suspension 10 Alcohol SW-846-8015C 67561 Methanol 184

Axiall PLQ LA 01/22/13 Suspension 10 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.941

Axiall PLQ LA 01/22/13 Suspension 10 Aldehyde SW-846-8315A 50000 Formaldehyde 0.638

Axiall PLQ LA 01/22/13 Suspension 10 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0678 Non-detect

Axiall PLQ LA 01/22/13 Suspension 10 SVOC SW-846-8270D 98862 Acetophenone 5.13

Axiall PLQ LA 01/22/13 Suspension 10 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.111 Non-detect

Axiall PLQ LA 01/22/13 Suspension 10 SVOC SW-846-8270D 123319 Hydroquinone 1.9

Axiall PLQ LA 01/22/13 Suspension 10 SVOC SW-846-8270D 108952 Phenol 0.0375 Non-detect

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 98828 Cumene 0.0019

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0672

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00732

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00482

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 01/22/13 Suspension 10 VC EPA Method 107 75014 Vinyl chloride 1.44

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 01/22/13 Suspension 10 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 01/23/13 Suspension 11 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6

Axiall PLQ LA 01/23/13 Suspension 11 Alcohol SW-846-8015C 67561 Methanol 332

Axiall PLQ LA 01/23/13 Suspension 11 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.04

Axiall PLQ LA 01/23/13 Suspension 11 Aldehyde SW-846-8315A 50000 Formaldehyde 2.58

Axiall PLQ LA 01/23/13 Suspension 11 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0644 Non-detect

Axiall PLQ LA 01/23/13 Suspension 11 SVOC SW-846-8270D 98862 Acetophenone 4.2

Axiall PLQ LA 01/23/13 Suspension 11 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.105 Non-detect

Axiall PLQ LA 01/23/13 Suspension 11 SVOC SW-846-8270D 123319 Hydroquinone 4.33

Axiall PLQ LA 01/23/13 Suspension 11 SVOC SW-846-8270D 108952 Phenol 0.0356 Non-detect

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0429

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0028

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00236 Non-detect

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 01/23/13 Suspension 11 VC EPA Method 107 75014 Vinyl chloride 1.2

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 01/23/13 Suspension 11 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 01/24/13 Suspension 12 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall PLQ LA 01/24/13 Suspension 12 Alcohol SW-846-8015C 67561 Methanol 780

Axiall PLQ LA 01/24/13 Suspension 12 Aldehyde SW-846-8315A 75070 Acetaldehyde 12.4

Axiall PLQ LA 01/24/13 Suspension 12 Aldehyde SW-846-8315A 50000 Formaldehyde 1.18

Axiall PLQ LA 01/24/13 Suspension 12 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0709 Non-detect

Axiall PLQ LA 01/24/13 Suspension 12 SVOC SW-846-8270D 98862 Acetophenone 4.63

Axiall PLQ LA 01/24/13 Suspension 12 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.116 Non-detect

Axiall PLQ LA 01/24/13 Suspension 12 SVOC SW-846-8270D 123319 Hydroquinone 4.35

Axiall PLQ LA 01/24/13 Suspension 12 SVOC SW-846-8270D 108952 Phenol 0.0392 Non-detect

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.109

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00589

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0288

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 01/24/13 Suspension 12 VC EPA Method 107 75014 Vinyl chloride 2.6

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 01/24/13 Suspension 12 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 01/25/13 Suspension 13 Alcohol SW-846-8015C 107211 Ethylene glycol 4.8

Axiall PLQ LA 01/25/13 Suspension 13 Alcohol SW-846-8015C 67561 Methanol 359

Axiall PLQ LA 01/25/13 Suspension 13 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.81

Axiall PLQ LA 01/25/13 Suspension 13 Aldehyde SW-846-8315A 50000 Formaldehyde 0.718

Axiall PLQ LA 01/25/13 Suspension 13 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0651 Non-detect

Axiall PLQ LA 01/25/13 Suspension 13 SVOC SW-846-8270D 98862 Acetophenone 3.78

Axiall PLQ LA 01/25/13 Suspension 13 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.106 Non-detect

Axiall PLQ LA 01/25/13 Suspension 13 SVOC SW-846-8270D 123319 Hydroquinone 1.48

Axiall PLQ LA 01/25/13 Suspension 13 SVOC SW-846-8270D 108952 Phenol 0.036 Non-detect

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.107

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00409

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0122

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 75092 Methylene chloride 0.0121

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 01/25/13 Suspension 13 VC EPA Method 107 75014 Vinyl chloride 2.31

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 01/25/13 Suspension 13 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 01/26/13 Suspension 14 Alcohol SW-846-8015C 107211 Ethylene glycol 4.4

Axiall PLQ LA 01/26/13 Suspension 14 Alcohol SW-846-8015C 67561 Methanol 460

Axiall PLQ LA 01/26/13 Suspension 14 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.89

Axiall PLQ LA 01/26/13 Suspension 14 Aldehyde SW-846-8315A 50000 Formaldehyde 2.1

Axiall PLQ LA 01/26/13 Suspension 14 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0678 Non-detect

Axiall PLQ LA 01/26/13 Suspension 14 SVOC SW-846-8270D 98862 Acetophenone 3.75

Axiall PLQ LA 01/26/13 Suspension 14 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.111 Non-detect

Axiall PLQ LA 01/26/13 Suspension 14 SVOC SW-846-8270D 123319 Hydroquinone 0.486

Axiall PLQ LA 01/26/13 Suspension 14 SVOC SW-846-8270D 108952 Phenol 0.0375 Non-detect

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Non-detect

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Non-detect

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Non-detect

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 71432 Benzene 0.00004 Non-detect

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Non-detect

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 67663 Chloroform 0.0001 Non-detect

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 126998 Chloroprene 0.00033 Non-detect

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 98828 Cumene 0.00083

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0802

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Non-detect

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00389

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0114

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Non-detect

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 110543 n-Hexane 0.00167 Non-detect

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 108883 Toluene 0.00004 Non-detect

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Non-detect

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Non-detect

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Non-detect

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 01/26/13 Suspension 14 VC EPA Method 107 75014 Vinyl chloride 3.04

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Non-detect

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) Detection Limit Not ReportedNon-detect VI Note (7) and (8)

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 179601231 m,p-xylene 0.00012 Non-detect VI Note (7)

Axiall PLQ LA 01/26/13 Suspension 14 VOC SW-846-8260B 95476 o-xylene 0.00007 Non-detect VI Note (7)

Axiall PLQ LA 01/27/13 Suspension 15 Alcohol SW-846-8015C 107211 Ethylene glycol 2.1

Axiall PLQ LA 01/27/13 Suspension 15 Alcohol SW-846-8015C 67561 Methanol 477

Axiall PLQ LA 01/27/13 Suspension 15 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.14

Axiall PLQ LA 01/27/13 Suspension 15 Aldehyde SW-846-8315A 50000 Formaldehyde 2.02

Axiall PLQ LA 01/27/13 Suspension 15 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0651 Non-detect

Axiall PLQ LA 01/27/13 Suspension 15 SVOC SW-846-8270D 98862 Acetophenone 4.05

Axiall PLQ LA 01/27/13 Suspension 15 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.106 Non-detect

Axiall PLQ LA 01/27/13 Suspension 15 SVOC SW-846-8270D 123319 Hydroquinone 2.04

Axiall PLQ LA 01/27/13 Suspension 15 SVOC SW-846-8270D 108952 Phenol 0.036 Non-detect

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Non-detect

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Non-detect

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Non-detect

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 71432 Benzene 0.00004 Non-detect

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Non-detect

12/12/2013 VI Confidential 119 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 67663 Chloroform 0.0001 Non-detect

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 126998 Chloroprene 0.00033 Non-detect

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 98828 Cumene 0.00103

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.155

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 100414 Ethylbenzene 0.00005 Non-detect

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0751

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00048 Non-detect

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.11

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 75092 Methylene chloride 0.00133

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 110543 n-Hexane 0.00167 Non-detect

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 108883 Toluene 0.00004 Non-detect

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Non-detect

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00074 Non-detect

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Non-detect

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 01/27/13 Suspension 15 VC EPA Method 107 75014 Vinyl chloride 8.78

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Non-detect

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) Detection Limit Not ReportedNon-detect VI Note (7) and (8)

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 179601231 m,p-xylene 0.00012 Non-detect VI Note (7)

Axiall PLQ LA 01/27/13 Suspension 15 VOC SW-846-8260B 95476 o-xylene 0.00007 Non-detect VI Note (7)

Axiall PLQ LA 01/28/13 Suspension 16 Alcohol SW-846-8015C 107211 Ethylene glycol 3.5

Axiall PLQ LA 01/28/13 Suspension 16 Alcohol SW-846-8015C 67561 Methanol 436

Axiall PLQ LA 01/28/13 Suspension 16 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.17

Axiall PLQ LA 01/28/13 Suspension 16 Aldehyde SW-846-8315A 50000 Formaldehyde 2.96

Axiall PLQ LA 01/28/13 Suspension 16 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0686 Non-detect

Axiall PLQ LA 01/28/13 Suspension 16 SVOC SW-846-8270D 98862 Acetophenone 4.28

Axiall PLQ LA 01/28/13 Suspension 16 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.112 Non-detect

Axiall PLQ LA 01/28/13 Suspension 16 SVOC SW-846-8270D 123319 Hydroquinone 0.31

Axiall PLQ LA 01/28/13 Suspension 16 SVOC SW-846-8270D 108952 Phenol 0.0379 Non-detect

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0427

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0028 Non-detect

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00502

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 75092 Methylene chloride 0.022

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 01/28/13 Suspension 16 VC EPA Method 107 75014 Vinyl chloride 0.916

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 01/28/13 Suspension 16 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 01/29/13 Suspension 17 Alcohol SW-846-8015C 107211 Ethylene glycol 4.9

Axiall PLQ LA 01/29/13 Suspension 17 Alcohol SW-846-8015C 67561 Methanol 319

Axiall PLQ LA 01/29/13 Suspension 17 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.4

Axiall PLQ LA 01/29/13 Suspension 17 Aldehyde SW-846-8315A 50000 Formaldehyde 1.53

Axiall PLQ LA 01/29/13 Suspension 17 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0671 Non-detect

Axiall PLQ LA 01/29/13 Suspension 17 SVOC SW-846-8270D 98862 Acetophenone 4.73

Axiall PLQ LA 01/29/13 Suspension 17 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.11 Non-detect

Axiall PLQ LA 01/29/13 Suspension 17 SVOC SW-846-8270D 123319 Hydroquinone 0.627

Axiall PLQ LA 01/29/13 Suspension 17 SVOC SW-846-8270D 108952 Phenol 0.0371 Non-detect

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.103

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0035

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0175

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 75092 Methylene chloride 0.0257

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 01/29/13 Suspension 17 VC EPA Method 107 75014 Vinyl chloride 2.41

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 01/29/13 Suspension 17 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 01/30/13 Suspension 18 Alcohol SW-846-8015C 107211 Ethylene glycol 4.7

Axiall PLQ LA 01/30/13 Suspension 18 Alcohol SW-846-8015C 67561 Methanol 498

Axiall PLQ LA 01/30/13 Suspension 18 Aldehyde SW-846-8315A 75070 Acetaldehyde 10.7

Axiall PLQ LA 01/30/13 Suspension 18 Aldehyde SW-846-8315A 50000 Formaldehyde 2.07

Axiall PLQ LA 01/30/13 Suspension 18 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0657 Non-detect

Axiall PLQ LA 01/30/13 Suspension 18 SVOC SW-846-8270D 98862 Acetophenone 3.7

Axiall PLQ LA 01/30/13 Suspension 18 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.107 Non-detect

Axiall PLQ LA 01/30/13 Suspension 18 SVOC SW-846-8270D 123319 Hydroquinone 0.202

Axiall PLQ LA 01/30/13 Suspension 18 SVOC SW-846-8270D 108952 Phenol 0.0364 Non-detect

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

12/12/2013 VI Confidential 120 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.13

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0119

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.022

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 75092 Methylene chloride 0.0261

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 01/30/13 Suspension 18 VC EPA Method 107 75014 Vinyl chloride 2.9

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 01/30/13 Suspension 18 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 01/31/13 Suspension 19 Alcohol SW-846-8015C 107211 Ethylene glycol 0.9

Axiall PLQ LA 01/31/13 Suspension 19 Alcohol SW-846-8015C 67561 Methanol 47.2

Axiall PLQ LA 01/31/13 Suspension 19 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.41

Axiall PLQ LA 01/31/13 Suspension 19 Aldehyde SW-846-8315A 50000 Formaldehyde 7.24

Axiall PLQ LA 01/31/13 Suspension 19 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0841 Non-detect

Axiall PLQ LA 01/31/13 Suspension 19 SVOC SW-846-8270D 98862 Acetophenone 4.72

Axiall PLQ LA 01/31/13 Suspension 19 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.137 Non-detect

Axiall PLQ LA 01/31/13 Suspension 19 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect

Axiall PLQ LA 01/31/13 Suspension 19 SVOC SW-846-8270D 108952 Phenol 0.0465 Non-detect

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 67663 Chloroform 0.00782

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.354

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0112

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0454

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 75092 Methylene chloride 0.0361

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 01/31/13 Suspension 19 VC EPA Method 107 75014 Vinyl chloride 5.71

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 01/31/13 Suspension 19 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 02/01/13 Suspension 20 Alcohol SW-846-8015C 107211 Ethylene glycol 0.8

Axiall PLQ LA 02/01/13 Suspension 20 Alcohol SW-846-8015C 67561 Methanol 61.5

Axiall PLQ LA 02/01/13 Suspension 20 Aldehyde SW-846-8315A 75070 Acetaldehyde 15.4

Axiall PLQ LA 02/01/13 Suspension 20 Aldehyde SW-846-8315A 50000 Formaldehyde 2.95

Axiall PLQ LA 02/01/13 Suspension 20 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0809 Non-detect

Axiall PLQ LA 02/01/13 Suspension 20 SVOC SW-846-8270D 98862 Acetophenone 4.17

Axiall PLQ LA 02/01/13 Suspension 20 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.132 Non-detect

Axiall PLQ LA 02/01/13 Suspension 20 SVOC SW-846-8270D 123319 Hydroquinone 0.361

Axiall PLQ LA 02/01/13 Suspension 20 SVOC SW-846-8270D 108952 Phenol 0.0447 Non-detect

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00186 Non-detect

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 106990 1,3-butadiene 0.0048 Non-detect

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.009 Non-detect

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 71432 Benzene 0.00095 Non-detect

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 108907 Chlorobenzene 0.00092 Non-detect

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 67663 Chloroform 0.00218 Non-detect

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 126998 Chloroprene 0.0066 Non-detect

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 98828 Cumene 0.00489

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.218

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 100414 Ethylbenzene 0.00116 Non-detect

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0218

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00232 Non-detect

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0188

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 75092 Methylene chloride 0.00836 Non-detect

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 110543 n-Hexane 0.0334 Non-detect

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 108883 Toluene 0.00099 Non-detect

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00276 Non-detect

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00089 Non-detect

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 108054 Vinyl acetate 0.00135 Non-detect

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 02/01/13 Suspension 20 VC EPA Method 107 75014 Vinyl chloride 3.98

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00143 Non-detect

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0014 Non-detect VI Note (7)

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 179601231 m,p-xylene 0.00248 Non-detect VI Note (7)

Axiall PLQ LA 02/01/13 Suspension 20 VOC SW-846-8260B 95476 o-xylene 0.00145 Non-detect VI Note (7)

Axiall PLQ LA 02/01/13 Suspension 21 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect duplicate

Axiall PLQ LA 02/01/13 Suspension 21 Alcohol SW-846-8015C 67561 Methanol 54.6

Axiall PLQ LA 02/01/13 Suspension 21 Aldehyde SW-846-8315A 75070 Acetaldehyde 11.2

Axiall PLQ LA 02/01/13 Suspension 21 Aldehyde SW-846-8315A 50000 Formaldehyde 3.3

Axiall PLQ LA 02/01/13 Suspension 21 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0671 Non-detect

Axiall PLQ LA 02/01/13 Suspension 21 SVOC SW-846-8270D 98862 Acetophenone 3.2

Axiall PLQ LA 02/01/13 Suspension 21 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.11 Non-detect

Axiall PLQ LA 02/01/13 Suspension 21 SVOC SW-846-8270D 123319 Hydroquinone 0.452

Axiall PLQ LA 02/01/13 Suspension 21 SVOC SW-846-8270D 108952 Phenol 0.0371 Non-detect

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00186 Non-detect

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 106990 1,3-butadiene 0.0048 Non-detect

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.009 Non-detect

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 71432 Benzene 0.00095 Non-detect

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 108907 Chlorobenzene 0.00092 Non-detect

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 67663 Chloroform 0.00218 Non-detect

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 98828 Cumene 0.00426

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.279

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 100414 Ethylbenzene 0.00116 Non-detect

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0288

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00232 Non-detect

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.022

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 75092 Methylene chloride 0.00836 Non-detect

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 110543 n-Hexane 0.0334 Non-detect

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 108883 Toluene 0.00099 Non-detect

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00276 Non-detect

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00089 Non-detect

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 108054 Vinyl acetate 0.00135 Non-detect

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 02/01/13 Suspension 21 VC EPA Method 107 75014 Vinyl chloride 5.99

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00143 Non-detect

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0014 Non-detect VI Note (7)

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 179601231 m,p-xylene 0.00248 Non-detect VI Note (7)

Axiall PLQ LA 02/01/13 Suspension 21 VOC SW-846-8260B 95476 o-xylene 0.00145 Non-detect VI Note (7)

Axiall PLQ LA 02/02/13 Suspension 22 Alcohol SW-846-8015C 107211 Ethylene glycol 0.9

Axiall PLQ LA 02/02/13 Suspension 22 Alcohol SW-846-8015C 67561 Methanol 39.5

Axiall PLQ LA 02/02/13 Suspension 22 Aldehyde SW-846-8315A 75070 Acetaldehyde 8.76

Axiall PLQ LA 02/02/13 Suspension 22 Aldehyde SW-846-8315A 50000 Formaldehyde 2.39

Axiall PLQ LA 02/02/13 Suspension 22 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0678 Non-detect

Axiall PLQ LA 02/02/13 Suspension 22 SVOC SW-846-8270D 98862 Acetophenone 2.21

Axiall PLQ LA 02/02/13 Suspension 22 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.111 Non-detect

Axiall PLQ LA 02/02/13 Suspension 22 SVOC SW-846-8270D 123319 Hydroquinone 0.323 Non-detect

Axiall PLQ LA 02/02/13 Suspension 22 SVOC SW-846-8270D 108952 Phenol 0.0375 Non-detect

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00186 Non-detect

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 106990 1,3-butadiene 0.0143

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.009 Non-detect

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 71432 Benzene 0.00095 Non-detect

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 108907 Chlorobenzene 0.00092 Non-detect

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 67663 Chloroform 0.00218 Non-detect

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 126998 Chloroprene 0.0066 Non-detect

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 98828 Cumene 0.0042

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.461

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 100414 Ethylbenzene 0.00116 Non-detect

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0369

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00232 Non-detect

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0408

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 75092 Methylene chloride 0.00836 Non-detect

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 110543 n-Hexane 0.0334 Non-detect

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 108883 Toluene 0.00099 Non-detect

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00276 Non-detect

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00089 Non-detect

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 108054 Vinyl acetate 0.00135 Non-detect

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 02/02/13 Suspension 22 VC EPA Method 107 75014 Vinyl chloride 8.74

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00143 Non-detect

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0014 Non-detect VI Note (7)

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 179601231 m,p-xylene 0.00248 Non-detect VI Note (7)

Axiall PLQ LA 02/02/13 Suspension 22 VOC SW-846-8260B 95476 o-xylene 0.00145 Non-detect VI Note (7)

Axiall PLQ LA 02/03/13 Suspension 23 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall PLQ LA 02/03/13 Suspension 23 Alcohol SW-846-8015C 67561 Methanol 35.2

Axiall PLQ LA 02/03/13 Suspension 23 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.75

Axiall PLQ LA 02/03/13 Suspension 23 Aldehyde SW-846-8315A 50000 Formaldehyde 1.97

Axiall PLQ LA 02/03/13 Suspension 23 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0686 Non-detect

Axiall PLQ LA 02/03/13 Suspension 23 SVOC SW-846-8270D 98862 Acetophenone 5.18

Axiall PLQ LA 02/03/13 Suspension 23 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.112 Non-detect

Axiall PLQ LA 02/03/13 Suspension 23 SVOC SW-846-8270D 123319 Hydroquinone 0.833

Axiall PLQ LA 02/03/13 Suspension 23 SVOC SW-846-8270D 108952 Phenol 0.0379 Non-detect

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 98828 Cumene 0.0021

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.115

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00647

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00662

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 02/03/13 Suspension 23 VC EPA Method 107 75014 Vinyl chloride 1.73

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 02/03/13 Suspension 23 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 02/04/13 Suspension 24 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall PLQ LA 02/04/13 Suspension 24 Alcohol SW-846-8015C 67561 Methanol 26.1

Axiall PLQ LA 02/04/13 Suspension 24 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.47

Axiall PLQ LA 02/04/13 Suspension 24 Aldehyde SW-846-8315A 50000 Formaldehyde 1.91

Axiall PLQ LA 02/04/13 Suspension 24 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0725 Non-detect

Axiall PLQ LA 02/04/13 Suspension 24 SVOC SW-846-8270D 98862 Acetophenone 4.19

Axiall PLQ LA 02/04/13 Suspension 24 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.119 Non-detect

Axiall PLQ LA 02/04/13 Suspension 24 SVOC SW-846-8270D 123319 Hydroquinone 0.3 Non-detect

Axiall PLQ LA 02/04/13 Suspension 24 SVOC SW-846-8270D 108952 Phenol 0.0401 Non-detect

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0496

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00589

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0055

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 02/04/13 Suspension 24 VC EPA Method 107 75014 Vinyl chloride 0.835

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 02/04/13 Suspension 24 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 02/05/13 Suspension 25 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall PLQ LA 02/05/13 Suspension 25 Alcohol SW-846-8015C 67561 Methanol 32.7

Axiall PLQ LA 02/05/13 Suspension 25 Aldehyde SW-846-8315A 75070 Acetaldehyde 10.3

Axiall PLQ LA 02/05/13 Suspension 25 Aldehyde SW-846-8315A 50000 Formaldehyde 2.98

Axiall PLQ LA 02/05/13 Suspension 25 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0651 Non-detect

Axiall PLQ LA 02/05/13 Suspension 25 SVOC SW-846-8270D 98862 Acetophenone 4.67

Axiall PLQ LA 02/05/13 Suspension 25 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.106 Non-detect

Axiall PLQ LA 02/05/13 Suspension 25 SVOC SW-846-8270D 123319 Hydroquinone 1.12

Axiall PLQ LA 02/05/13 Suspension 25 SVOC SW-846-8270D 108952 Phenol 0.036 Non-detect

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 98828 Cumene 0.00352

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.1

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0182

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0156

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 02/05/13 Suspension 25 VC EPA Method 107 75014 Vinyl chloride 2.52

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 02/05/13 Suspension 25 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 02/06/13 Suspension 26 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall PLQ LA 02/06/13 Suspension 26 Alcohol SW-846-8015C 67561 Methanol 42.7

Axiall PLQ LA 02/06/13 Suspension 26 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.89

Axiall PLQ LA 02/06/13 Suspension 26 Aldehyde SW-846-8315A 50000 Formaldehyde 3.82

Axiall PLQ LA 02/06/13 Suspension 26 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0631 Non-detect

Axiall PLQ LA 02/06/13 Suspension 26 SVOC SW-846-8270D 98862 Acetophenone 4.29

Axiall PLQ LA 02/06/13 Suspension 26 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.103 Non-detect

Axiall PLQ LA 02/06/13 Suspension 26 SVOC SW-846-8270D 123319 Hydroquinone 1.42

Axiall PLQ LA 02/06/13 Suspension 26 SVOC SW-846-8270D 108952 Phenol 0.0349 Non-detect

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 98828 Cumene 0.00296

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.129

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00741

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0175

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 02/06/13 Suspension 26 VC EPA Method 107 75014 Vinyl chloride 2.68

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 02/06/13 Suspension 26 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 02/07/13 Suspension 27 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall PLQ LA 02/07/13 Suspension 27 Alcohol SW-846-8015C 67561 Methanol 10.8

Axiall PLQ LA 02/07/13 Suspension 27 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.666

Axiall PLQ LA 02/07/13 Suspension 27 Aldehyde SW-846-8315A 50000 Formaldehyde 3.5

Axiall PLQ LA 02/07/13 Suspension 27 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0678 Non-detect

Axiall PLQ LA 02/07/13 Suspension 27 SVOC SW-846-8270D 98862 Acetophenone 2.33

Axiall PLQ LA 02/07/13 Suspension 27 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.111 Non-detect

Axiall PLQ LA 02/07/13 Suspension 27 SVOC SW-846-8270D 123319 Hydroquinone 0.223

Axiall PLQ LA 02/07/13 Suspension 27 SVOC SW-846-8270D 108952 Phenol 0.0375 Non-detect

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00009 Non-detect

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Non-detect

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Non-detect

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 71432 Benzene 0.00004 Non-detect

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 108907 Chlorobenzene 0.00004 Non-detect

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 67663 Chloroform 0.0001 Non-detect

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 126998 Chloroprene 0.00033 Non-detect

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 98828 Cumene 0.00083

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0488

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 100414 Ethylbenzene 0.0004

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00242

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00321

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 75092 Methylene chloride 0.00041 Non-detect

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 110543 n-Hexane 0.00167 Non-detect

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 108883 Toluene 0.00004 Non-detect

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00013 Non-detect

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00004 Non-detect

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 108054 Vinyl acetate 0.00006 Non-detect

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 02/07/13 Suspension 27 VC EPA Method 107 75014 Vinyl chloride 0.728

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00007 Non-detect

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) Detection Limit Not ReportedNon-detect VI Note (7) and (8)

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 179601231 m,p-xylene 0.00012 Non-detect VI Note (7)

Axiall PLQ LA 02/07/13 Suspension 27 VOC SW-846-8260B 95476 o-xylene 0.00007 Non-detect VI Note (7)

Axiall PLQ LA 02/08/13 Suspension 28 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall PLQ LA 02/08/13 Suspension 28 Alcohol SW-846-8015C 67561 Methanol 29.3

Axiall PLQ LA 02/08/13 Suspension 28 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.29

Axiall PLQ LA 02/08/13 Suspension 28 Aldehyde SW-846-8315A 50000 Formaldehyde 3.99

Axiall PLQ LA 02/08/13 Suspension 28 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0701 Non-detect

Axiall PLQ LA 02/08/13 Suspension 28 SVOC SW-846-8270D 98862 Acetophenone 4.75

Axiall PLQ LA 02/08/13 Suspension 28 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.115 Non-detect

Axiall PLQ LA 02/08/13 Suspension 28 SVOC SW-846-8270D 123319 Hydroquinone 0.333 Non-detect

Axiall PLQ LA 02/08/13 Suspension 28 SVOC SW-846-8270D 108952 Phenol 0.0388 Non-detect

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 106990 1,3-butadiene 0.00024 Non-detect

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00045 Non-detect

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 98828 Cumene 0.00409

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.148

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 100414 Ethylbenzene 0.00267

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00796

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00671

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 75092 Methylene chloride 0.00418 Non-detect

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 02/08/13 Suspension 28 VC EPA Method 107 75014 Vinyl chloride 2.24

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 02/08/13 Suspension 28 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 02/09/13 Suspension 29 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall PLQ LA 02/09/13 Suspension 29 Alcohol SW-846-8015C 67561 Methanol 38

Axiall PLQ LA 02/09/13 Suspension 29 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.24

Axiall PLQ LA 02/09/13 Suspension 29 Aldehyde SW-846-8315A 50000 Formaldehyde 7.81

Axiall PLQ LA 02/09/13 Suspension 29 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0671 Non-detect

Axiall PLQ LA 02/09/13 Suspension 29 SVOC SW-846-8270D 98862 Acetophenone 3.76

Axiall PLQ LA 02/09/13 Suspension 29 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.11 Non-detect

Axiall PLQ LA 02/09/13 Suspension 29 SVOC SW-846-8270D 123319 Hydroquinone 0.373

Axiall PLQ LA 02/09/13 Suspension 29 SVOC SW-846-8270D 108952 Phenol 0.0371 Non-detect

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 98828 Cumene 0.00496

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.208

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0348

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0148

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 75092 Methylene chloride 0.0149

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 02/09/13 Suspension 29 VC EPA Method 107 75014 Vinyl chloride 3.69

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 02/09/13 Suspension 29 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 02/10/13 Suspension 30 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall PLQ LA 02/10/13 Suspension 30 Alcohol SW-846-8015C 67561 Methanol 47.1

Axiall PLQ LA 02/10/13 Suspension 30 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.31

Axiall PLQ LA 02/10/13 Suspension 30 Aldehyde SW-846-8315A 50000 Formaldehyde 1.98

Axiall PLQ LA 02/10/13 Suspension 30 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0671 Non-detect

Axiall PLQ LA 02/10/13 Suspension 30 SVOC SW-846-8270D 98862 Acetophenone 5.66

Axiall PLQ LA 02/10/13 Suspension 30 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.11 Non-detect

Axiall PLQ LA 02/10/13 Suspension 30 SVOC SW-846-8270D 123319 Hydroquinone 0.28

Axiall PLQ LA 02/10/13 Suspension 30 SVOC SW-846-8270D 108952 Phenol 0.0371 Non-detect

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 98828 Cumene 0.00416

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.113

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00788

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00754

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 75092 Methylene chloride 0.0175

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 02/10/13 Suspension 30 VC EPA Method 107 75014 Vinyl chloride 3.47

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 02/10/13 Suspension 30 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 02/11/13 Suspension 31 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall PLQ LA 02/11/13 Suspension 31 Alcohol SW-846-8015C 67561 Methanol 42.7

Axiall PLQ LA 02/11/13 Suspension 31 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.54

Axiall PLQ LA 02/11/13 Suspension 31 Aldehyde SW-846-8315A 50000 Formaldehyde 2.2

Axiall PLQ LA 02/11/13 Suspension 31 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0657 Non-detect

Axiall PLQ LA 02/11/13 Suspension 31 SVOC SW-846-8270D 98862 Acetophenone 3.79

Axiall PLQ LA 02/11/13 Suspension 31 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.107 Non-detect

Axiall PLQ LA 02/11/13 Suspension 31 SVOC SW-846-8270D 123319 Hydroquinone 0.133

Axiall PLQ LA 02/11/13 Suspension 31 SVOC SW-846-8270D 108952 Phenol 0.0364 Non-detect

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 98828 Cumene 0.00374

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.122

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00694

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00828

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 75092 Methylene chloride 0.0185

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect VI Note (5)

Axiall PLQ LA 02/11/13 Suspension 31 VC EPA Method 107 75014 Vinyl chloride 2.56

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 02/11/13 Suspension 31 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 02/11/13 Suspension 32 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect duplicate

Axiall PLQ LA 02/11/13 Suspension 32 Alcohol SW-846-8015C 67561 Methanol 49

Axiall PLQ LA 02/11/13 Suspension 32 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.85

Axiall PLQ LA 02/11/13 Suspension 32 Aldehyde SW-846-8315A 50000 Formaldehyde 2.08

Axiall PLQ LA 02/11/13 Suspension 32 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0678 Non-detect

Axiall PLQ LA 02/11/13 Suspension 32 SVOC SW-846-8270D 98862 Acetophenone 4.52

Axiall PLQ LA 02/11/13 Suspension 32 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.111 Non-detect

Axiall PLQ LA 02/11/13 Suspension 32 SVOC SW-846-8270D 123319 Hydroquinone 0.134

Axiall PLQ LA 02/11/13 Suspension 32 SVOC SW-846-8270D 108952 Phenol 0.0375 Non-detect

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 98828 Cumene 0.00321

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.112

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00722

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00602

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 75092 Methylene chloride 0.0219

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall PLQ LA 02/11/13 Suspension 32 VC EPA Method 107 75014 Vinyl chloride 2.38

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 02/11/13 Suspension 32 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Axiall PLQ LA 02/12/13 Suspension 33 Alcohol SW-846-8015C 107211 Ethylene glycol 0.6 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 Alcohol SW-846-8015C 67561 Methanol 23.5

Axiall PLQ LA 02/12/13 Suspension 33 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.5

Axiall PLQ LA 02/12/13 Suspension 33 Aldehyde SW-846-8315A 50000 Formaldehyde 2.05

Axiall PLQ LA 02/12/13 Suspension 33 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.0637 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 SVOC SW-846-8270D 98862 Acetophenone 1.52

Axiall PLQ LA 02/12/13 Suspension 33 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.104 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 SVOC SW-846-8270D 123319 Hydroquinone 0.175

Axiall PLQ LA 02/12/13 Suspension 33 SVOC SW-846-8270D 108952 Phenol 0.0353 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00092 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 106990 1,3-butadiene 0.0024 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 71432 Benzene 0.00047 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 108907 Chlorobenzene 0.00046 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 67663 Chloroform 0.00109 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 126998 Chloroprene 0.0033 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 98828 Cumene 0.00057 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00125 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 100414 Ethylbenzene 0.00058 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0028 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00116 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00236 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 75092 Methylene chloride 0.0162

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 110543 n-Hexane 0.0167 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 108883 Toluene 0.00049 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00138 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00044 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 108054 Vinyl acetate 0.00067 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 593602 Vinyl bromide NOT FOUND Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 VC EPA Method 107 75014 Vinyl chloride 0.141

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00071 Non-detect

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0007 Non-detect VI Note (7)

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 179601231 m,p-xylene 0.00124 Non-detect VI Note (7)

Axiall PLQ LA 02/12/13 Suspension 33 VOC SW-846-8260B 95476 o-xylene 0.00072 Non-detect VI Note (7)

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 Aldehyde SW-846-8315A 75070 Acetaldehyde 9.3

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 Aldehyde SW-846-8315A 50000 Formaldehyde 0.26

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 SVOC SW-846-8270D 98862 Acetophenone 0.015 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.018 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 SVOC SW-846-8270D 123319 Hydroquinone 0.0684 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 SVOC SW-846-8270D 108952 Phenol 0.015 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 67663 Chloroform 0.001

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0312

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0113

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 108054 Vinyl acetate 85.8

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VC EPA Method 107 75014 Vinyl chloride 2.9

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa SPVC TX 01/02/13 Suspension Blending, Dispersion, Copolymer 1 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 Aldehyde SW-846-8315A 75070 Acetaldehyde 9.7

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0056 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 SVOC SW-846-8270D 98862 Acetophenone 0.015 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0544

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 SVOC SW-846-8270D 123319 Hydroquinone 0.139 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 SVOC SW-846-8270D 108952 Phenol 0.015 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 67663 Chloroform 0.00035 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00072 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.09

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 108054 Vinyl acetate 239

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VC EPA Method 107 75014 Vinyl chloride 2.8

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa SPVC TX 01/03/13 Suspension Blending, Dispersion, Copolymer 2 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.9

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0056 Non-detect

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 SVOC SW-846-8270D 98862 Acetophenone 0.116

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0379 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 SVOC SW-846-8270D 123319 Hydroquinone 0.0456 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 SVOC SW-846-8270D 108952 Phenol 0.015 Non-detect

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0489

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0405

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0317

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 75092 Methylene chloride 0.0131 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

12/12/2013 VI Confidential 126 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 108054 Vinyl acetate 1360

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VC EPA Method 107 75014 Vinyl chloride 9.89

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/04/13 Suspension Blending, Dispersion, Copolymer 3 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.6

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0056 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 SVOC SW-846-8270D 98862 Acetophenone 0.0685

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.018 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 SVOC SW-846-8270D 123319 Hydroquinone 0.193 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 SVOC SW-846-8270D 108952 Phenol 0.015 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0648

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0118

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0063 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 75092 Methylene chloride 0.0171 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 108054 Vinyl acetate 90.9

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VC EPA Method 107 75014 Vinyl chloride 3.89

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/05/13 Suspension Blending, Dispersion, Copolymer 4 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 Aldehyde SW-846-8315A 75070 Acetaldehyde 28

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 Aldehyde SW-846-8315A 50000 Formaldehyde 0.056 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 SVOC SW-846-8270D 98862 Acetophenone 0.0575

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.018 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 SVOC SW-846-8270D 123319 Hydroquinone R

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 SVOC SW-846-8270D 108952 Phenol 0.015 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 67663 Chloroform 0.00035 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 98828 Cumene 0.00058 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00072 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0105

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.104

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 108054 Vinyl acetate 265

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VC EPA Method 107 75014 Vinyl chloride 5.7

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa SPVC TX 01/06/13 Suspension Blending, Dispersion, Copolymer 5 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 Aldehyde SW-846-8315A 75070 Acetaldehyde 30

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 Aldehyde SW-846-8315A 50000 Formaldehyde 0.056 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.12 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 SVOC SW-846-8270D 98862 Acetophenone 0.34

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.117

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 SVOC SW-846-8270D 123319 Hydroquinone R

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 SVOC SW-846-8270D 108952 Phenol 0.018 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 67663 Chloroform 0.00035 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00072 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00063 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 108054 Vinyl acetate 11.6

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VC EPA Method 107 75014 Vinyl chloride Detection Limit Not ReportedNon-detect VI Note (9)

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa SPVC TX 01/07/13 Suspension Blending, Dispersion, Copolymer 6 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

12/12/2013 VI Confidential 127 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 Alcohol SW-846-8015C 107211 Ethylene glycol 11.7

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 Alcohol SW-846-8015C 67561 Methanol 83.4 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 Aldehyde SW-846-8315A 75070 Acetaldehyde 35

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 SVOC SW-846-8270D 98862 Acetophenone 0.583

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.285

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 SVOC SW-846-8270D 123319 Hydroquinone 0.0263 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 SVOC SW-846-8270D 108952 Phenol 0.015 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 67663 Chloroform 0.00035 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00072 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00035 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00063 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 108054 Vinyl acetate 21.6

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VC EPA Method 107 75014 Vinyl chloride Detection Limit Not ReportedNon-detect VI Note (9)

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa SPVC TX 01/08/13 Suspension Blending, Dispersion, Copolymer 7 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 Aldehyde SW-846-8315A 75070 Acetaldehyde 13

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0056 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.51 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 SVOC SW-846-8270D 98862 Acetophenone 0.492

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.266

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 SVOC SW-846-8270D 123319 Hydroquinone R

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 SVOC SW-846-8270D 108952 Phenol 0.074 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0072 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0035 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0063 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 108054 Vinyl acetate 5.22

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VC EPA Method 107 75014 Vinyl chloride 1.93

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/09/13 Suspension Blending, Dispersion, Copolymer 8 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 Aldehyde SW-846-8315A 75070 Acetaldehyde 23

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 Aldehyde SW-846-8315A 50000 Formaldehyde 0.056 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 SVOC SW-846-8270D 98862 Acetophenone 0.124 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0852 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 SVOC SW-846-8270D 123319 Hydroquinone 0.0438 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 SVOC SW-846-8270D 108952 Phenol 0.015 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.157

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0126

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0497

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 75092 Methylene chloride 0.023 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 108054 Vinyl acetate 239

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VC EPA Method 107 75014 Vinyl chloride 1.77

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/10/13 Suspension Blending, Dispersion, Copolymer 9 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 Aldehyde SW-846-8315A 75070 Acetaldehyde 33

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 Aldehyde SW-846-8315A 50000 Formaldehyde 0.056 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1.6 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 SVOC SW-846-8270D 98862 Acetophenone 0.24 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.29 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 SVOC SW-846-8270D 123319 Hydroquinone R

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 SVOC SW-846-8270D 108952 Phenol 0.24 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0558

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0119

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0187

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 75092 Methylene chloride 0.0197 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 108054 Vinyl acetate 330

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VC EPA Method 107 75014 Vinyl chloride 1.5

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/11/13 Suspension Blending, Dispersion, Copolymer 10 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 Aldehyde SW-846-8315A 75070 Acetaldehyde 12

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0056 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.01 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 SVOC SW-846-8270D 98862 Acetophenone 0.0903

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0037 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 SVOC SW-846-8270D 123319 Hydroquinone 0.0051 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 SVOC SW-846-8270D 108952 Phenol 0.0015 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0256

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0035 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0069 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 75092 Methylene chloride 0.0123 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 108054 Vinyl acetate 202

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VC EPA Method 107 75014 Vinyl chloride 1.4

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/12/13 Suspension Blending, Dispersion, Copolymer 11 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 Aldehyde SW-846-8315A 75070 Acetaldehyde 16

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0056 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.011 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 SVOC SW-846-8270D 98862 Acetophenone 0.0225

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0065

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 SVOC SW-846-8270D 123319 Hydroquinone 0.0057 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 SVOC SW-846-8270D 108952 Phenol 0.0017 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 67663 Chloroform 0.0207

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0266

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0035 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0063 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 75092 Methylene chloride 0.013 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 108054 Vinyl acetate 78.2

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VC EPA Method 107 75014 Vinyl chloride 1.5

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/13/13 Suspension Blending, Dispersion, Copolymer 12 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 Aldehyde SW-846-8315A 75070 Acetaldehyde 32

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 SVOC SW-846-8270D 98862 Acetophenone 0.015 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.018 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 SVOC SW-846-8270D 123319 Hydroquinone 0.316

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 SVOC SW-846-8270D 108952 Phenol 0.015 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

12/12/2013 VI Confidential 129 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 67663 Chloroform 0.0084 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.338

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0321

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.142

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 75092 Methylene chloride 0.0163 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 108054 Vinyl acetate 981

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VC EPA Method 107 75014 Vinyl chloride 5.29

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/14/13 Suspension Blending, Dispersion, Copolymer 13 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 Aldehyde SW-846-8315A 75070 Acetaldehyde 40

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 Aldehyde SW-846-8315A 50000 Formaldehyde 0.28 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 SVOC SW-846-8270D 98862 Acetophenone 0.031 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.036 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 SVOC SW-846-8270D 123319 Hydroquinone 0.666

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 SVOC SW-846-8270D 108952 Phenol 0.03 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0072 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0035 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0063 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 108054 Vinyl acetate 178

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VC EPA Method 107 75014 Vinyl chloride Detection Limit Not ReportedNon-detect VI Note (9)

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/15/13 Suspension Blending, Dispersion, Copolymer 14 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 Alcohol SW-846-8015C 67561 Methanol 46.4

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 Aldehyde SW-846-8315A 75070 Acetaldehyde 33

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.11 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 SVOC SW-846-8270D 98862 Acetophenone 0.0695

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.019 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 SVOC SW-846-8270D 123319 Hydroquinone 0.0964 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 SVOC SW-846-8270D 108952 Phenol 0.015 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0285

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0035 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0074 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 75092 Methylene chloride 0.0118 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 108054 Vinyl acetate 220

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VC EPA Method 107 75014 Vinyl chloride 2.5

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/16/13 Suspension Blending, Dispersion, Copolymer 15 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 Aldehyde SW-846-8315A 75070 Acetaldehyde 33

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 SVOC SW-846-8270D 98862 Acetophenone 0.166

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.036 Non-detect

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 SVOC SW-846-8270D 123319 Hydroquinone 0.051 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 SVOC SW-846-8270D 108952 Phenol 0.029 Non-detect

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 67663 Chloroform 0.008 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.256

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0353

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

12/12/2013 VI Confidential 130 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0409

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 75092 Methylene chloride 0.0303 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 108054 Vinyl acetate 1400

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VC EPA Method 107 75014 Vinyl chloride Detection Limit Not ReportedNon-detect VI Note (9)

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/17/13 Suspension Blending, Dispersion, Copolymer 16 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 Aldehyde SW-846-8315A 75070 Acetaldehyde 38

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.61 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 SVOC SW-846-8270D 98862 Acetophenone 0.229 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.11 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 SVOC SW-846-8270D 123319 Hydroquinone R

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 SVOC SW-846-8270D 108952 Phenol 0.088 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 67663 Chloroform 0.0098 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.195

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0435

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0307

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 75092 Methylene chloride 0.0119 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 108054 Vinyl acetate 795

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VC EPA Method 107 75014 Vinyl chloride 1.43

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/18/13 Suspension Blending, Dispersion, Copolymer 17 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.29 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 Aldehyde SW-846-8315A 50000 Formaldehyde 0.28 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 SVOC SW-846-8270D 98862 Acetophenone 0.03 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.036 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 SVOC SW-846-8270D 123319 Hydroquinone R

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 SVOC SW-846-8270D 108952 Phenol 0.029 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0072 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0035 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0063 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 75092 Methylene chloride 0.014 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 108054 Vinyl acetate 190

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VC EPA Method 107 75014 Vinyl chloride Detection Limit Not ReportedNon-detect VI Note (9)

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/19/13 Suspension Blending, Dispersion, Copolymer 18 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 Aldehyde SW-846-8315A 75070 Acetaldehyde 38

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 SVOC SW-846-8270D 98862 Acetophenone 0.11

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0402 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 SVOC SW-846-8270D 123319 Hydroquinone R

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 SVOC SW-846-8270D 108952 Phenol 0.029 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.104

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.114

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0318

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 75092 Methylene chloride 0.013 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 108054 Vinyl acetate 4500

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VC EPA Method 107 75014 Vinyl chloride 2.7

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/20/13 Suspension Blending, Dispersion, Copolymer 19 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 Aldehyde SW-846-8315A 75070 Acetaldehyde 37

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 SVOC SW-846-8270D 98862 Acetophenone 0.0745 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.036 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 SVOC SW-846-8270D 123319 Hydroquinone 0.75 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 SVOC SW-846-8270D 108952 Phenol 0.029 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0072 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0122

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0063 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 75092 Methylene chloride 0.0139 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 108054 Vinyl acetate 336

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VC EPA Method 107 75014 Vinyl chloride Detection Limit Not ReportedNon-detect VI Note (9)

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/21/13 Suspension Blending, Dispersion, Copolymer 20 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 Aldehyde SW-846-8315A 75070 Acetaldehyde 36

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.01 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 SVOC SW-846-8270D 98862 Acetophenone 0.0015 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0018 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 SVOC SW-846-8270D 123319 Hydroquinone R

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 SVOC SW-846-8270D 108952 Phenol 0.0015 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0072 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0035 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0108

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 75092 Methylene chloride 0.017 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 108054 Vinyl acetate 46.1

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VC EPA Method 107 75014 Vinyl chloride Detection Limit Not ReportedNon-detect VI Note (9)

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/22/13 Suspension Blending, Dispersion, Copolymer 21 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 Alcohol SW-846-8015C 107211 Ethylene glycol 2.1 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 Aldehyde SW-846-8315A 75070 Acetaldehyde 45

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 Aldehyde SW-846-8315A 50000 Formaldehyde 0.28 Non-detect

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 SVOC SW-846-8270D 98862 Acetophenone 0.672

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0815 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 SVOC SW-846-8270D 123319 Hydroquinone 0.151 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 SVOC SW-846-8270D 108952 Phenol 0.029 Non-detect

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 67663 Chloroform 0.0361

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.224

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0939

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0183

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 75092 Methylene chloride 0.0164 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 108054 Vinyl acetate 819

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VC EPA Method 107 75014 Vinyl chloride 2.7

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/23/13 Suspension Blending, Dispersion, Copolymer 22 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 Aldehyde SW-846-8315A 75070 Acetaldehyde 60

12/12/2013 VI Confidential 132 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 Aldehyde SW-846-8315A 50000 Formaldehyde 0.28 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 SVOC SW-846-8270D 98862 Acetophenone 0.1

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0909

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 SVOC SW-846-8270D 123319 Hydroquinone 0.0631 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 SVOC SW-846-8270D 108952 Phenol 0.015 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.114

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0035 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0154

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 75092 Methylene chloride 0.0147 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 108054 Vinyl acetate 47.3

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VC EPA Method 107 75014 Vinyl chloride 2.5

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/24/13 Suspension Blending, Dispersion, Copolymer 23 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 Aldehyde SW-846-8315A 75070 Acetaldehyde 46

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 Aldehyde SW-846-8315A 50000 Formaldehyde 0.28 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 SVOC SW-846-8270D 98862 Acetophenone 0.131

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0442 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 SVOC SW-846-8270D 123319 Hydroquinone 0.151 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 SVOC SW-846-8270D 108952 Phenol 0.015 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0072 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0035 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0063 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 75092 Methylene chloride 0.01 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 108054 Vinyl acetate 8.05

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VC EPA Method 107 75014 Vinyl chloride Detection Limit Not ReportedNon-detect VI Note (9)

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/25/13 Suspension Blending, Dispersion, Copolymer 24 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 Aldehyde SW-846-8315A 75070 Acetaldehyde 24

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 SVOC SW-846-8270D 98862 Acetophenone 0.141

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0363 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 SVOC SW-846-8270D 123319 Hydroquinone 0.267 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 SVOC SW-846-8270D 108952 Phenol 0.015 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0004 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 106990 1,3-butadiene 0.00054 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00049 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 71432 Benzene 0.00034 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 108907 Chlorobenzene 0.00027 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 67663 Chloroform 0.00035 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 126998 Chloroprene 0.00042 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 98828 Cumene 0.0004 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0015

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 100414 Ethylbenzene 0.00032 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.001

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00034 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0011

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 75092 Methylene chloride 0.001 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 110543 n-Hexane 0.0007 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 108883 Toluene 0.00033 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00043 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00035 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 108054 Vinyl acetate 11.4

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 593602 Vinyl bromide 0.00025 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VC EPA Method 107 75014 Vinyl chloride Detection Limit Not ReportedNon-detect VI Note (9)

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00045 Non-detect

Formosa SPVC TX 01/26/13 Suspension Blending, Dispersion, Copolymer 25 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00087 Non-detect

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 Aldehyde SW-846-8315A 75070 Acetaldehyde 57

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 Aldehyde SW-846-8315A 50000 Formaldehyde 0.28 Non-detect

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.2 Non-detect

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 SVOC SW-846-8270D 98862 Acetophenone 0.22

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 1.47

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 SVOC SW-846-8270D 123319 Hydroquinone 0.634 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 SVOC SW-846-8270D 108952 Phenol 0.029 Non-detect

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

12/12/2013 VI Confidential 133 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0625

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0203

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0297

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 75092 Methylene chloride 0.0313 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 108054 Vinyl acetate 476

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VC EPA Method 107 75014 Vinyl chloride 1.3

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/27/13 Suspension Blending, Dispersion, Copolymer 26 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 Aldehyde SW-846-8315A 75070 Acetaldehyde 38

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 SVOC SW-846-8270D 98862 Acetophenone 0.122

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.144

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 SVOC SW-846-8270D 123319 Hydroquinone 0.0826

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 SVOC SW-846-8270D 108952 Phenol 0.015 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0072 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0035 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0063 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 75092 Methylene chloride 0.0274 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 108054 Vinyl acetate 98.7

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VC EPA Method 107 75014 Vinyl chloride Detection Limit Not ReportedNon-detect VI Note (9)

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/28/13 Suspension Blending, Dispersion, Copolymer 27 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 Aldehyde SW-846-8315A 75070 Acetaldehyde 31

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 Aldehyde SW-846-8315A 50000 Formaldehyde 0.53

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 SVOC SW-846-8270D 98862 Acetophenone 0.071

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.018 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 SVOC SW-846-8270D 123319 Hydroquinone R

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 SVOC SW-846-8270D 108952 Phenol 0.015 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0517

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0035 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0494

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 75092 Methylene chloride 0.0537

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 108054 Vinyl acetate 1.74

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VC EPA Method 107 75014 Vinyl chloride Detection Limit Not ReportedNon-detect VI Note (9)

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/29/13 Suspension Blending, Dispersion, Copolymer 28 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 Aldehyde SW-846-8315A 75070 Acetaldehyde 36

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.04 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 SVOC SW-846-8270D 98862 Acetophenone 0.0327

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0072 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 SVOC SW-846-8270D 123319 Hydroquinone R

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 SVOC SW-846-8270D 108952 Phenol 0.0059 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

12/12/2013 VI Confidential 134 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0491

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0161

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0167

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 75092 Methylene chloride 0.0258 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 108054 Vinyl acetate 189

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VC EPA Method 107 75014 Vinyl chloride Detection Limit Not ReportedNon-detect VI Note (9)

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/30/13 Suspension Blending, Dispersion, Copolymer 29 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 Aldehyde SW-846-8315A 75070 Acetaldehyde 39

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 SVOC SW-846-8270D 98862 Acetophenone 0.104

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.018 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 SVOC SW-846-8270D 123319 Hydroquinone 0.0517 J-estimated value, VI Note (9.1)

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 SVOC SW-846-8270D 108952 Phenol 0.015 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0072 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0035 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0063 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 75092 Methylene chloride 0.0521

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 108054 Vinyl acetate 165

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VC EPA Method 107 75014 Vinyl chloride Detection Limit Not ReportedNon-detect VI Note (9)

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 01/31/13 Suspension Blending, Dispersion, Copolymer 30 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 Aldehyde SW-846-8315A 75070 Acetaldehyde 37

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.11 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 SVOC SW-846-8270D 98862 Acetophenone 0.0909

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0196 J-estimated value, VI Note (9.1)

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 SVOC SW-846-8270D 123319 Hydroquinone 0.137 J-estimated value, VI Note (9.1)

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 SVOC SW-846-8270D 108952 Phenol 0.015 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0072 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0065 J-estimated value, VI Note (9.1)

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0063 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 75092 Methylene chloride 0.0509

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 108054 Vinyl acetate 113

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VC EPA Method 107 75014 Vinyl chloride Detection Limit Not ReportedNon-detect VI Note (9)

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 02/01/13 Suspension Blending, Dispersion, Copolymer 31 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.21

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 Aldehyde SW-846-8315A 50000 Formaldehyde 0.047

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.11 Non-detect

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 SVOC SW-846-8270D 98862 Acetophenone 0.026 J-estimated value, VI Note (9.1)

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.019 Non-detect

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 SVOC SW-846-8270D 123319 Hydroquinone R

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 SVOC SW-846-8270D 108952 Phenol 0.016 Non-detect

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 67663 Chloroform 0.0052 J-estimated value, VI Note (9.1)

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.241

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0393

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0917

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 75092 Methylene chloride 0.0472 J-estimated value, VI Note (9.1)

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

12/12/2013 VI Confidential 135 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 108054 Vinyl acetate 749

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VC EPA Method 107 75014 Vinyl chloride Detection Limit Not ReportedNon-detect VI Note (9)

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 02/02/13 Suspension Blending, Dispersion, Copolymer 32 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.44

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 Aldehyde SW-846-8315A 50000 Formaldehyde 0.028

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 SVOC SW-846-8270D 98862 Acetophenone 0.0187 J-estimated value, VI Note (9.1)

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.018 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 SVOC SW-846-8270D 123319 Hydroquinone 0.275 J-estimated value, VI Note (9.1)

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 SVOC SW-846-8270D 108952 Phenol 0.015 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0072 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0108

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0063 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 75092 Methylene chloride 0.0144 J-estimated value, VI Note (9.1)

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 108054 Vinyl acetate 158

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VC EPA Method 107 75014 Vinyl chloride Detection Limit Not ReportedNon-detect VI Note (9)

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 02/03/13 Suspension Blending, Dispersion, Copolymer 33 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 Aldehyde SW-846-8315A 75070 Acetaldehyde 60

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 Aldehyde SW-846-8315A 50000 Formaldehyde 0.28 Non-detect

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.28 Non-detect

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 SVOC SW-846-8270D 98862 Acetophenone 3.44

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.355

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 SVOC SW-846-8270D 123319 Hydroquinone 0.0582 J-estimated value, VI Note (9.1)

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 SVOC SW-846-8270D 108952 Phenol 0.041 Non-detect

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.004 Non-detect

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 67663 Chloroform 0.0035 J-estimated value, VI Note (9.1)

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 98828 Cumene 0.004 Non-detect

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.366

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0132

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0665

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 75092 Methylene chloride 0.0154 J-estimated value, VI Note (9.1)

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 110543 n-Hexane 0.007 Non-detect

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 108054 Vinyl acetate 200

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VC EPA Method 107 75014 Vinyl chloride Detection Limit Not ReportedNon-detect VI Note (9)

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

Formosa SPVC TX 02/04/13 Suspension Blending, Dispersion, Copolymer 34 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 Alcohol SW-846-8015C 107211 Ethylene glycol 2 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 Alcohol SW-846-8015C 67561 Methanol 0.25 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 Aldehyde SW-846-8315A 75070 Acetaldehyde 35

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.1 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 SVOC SW-846-8270D 98862 Acetophenone 0.0181

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.018 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 SVOC SW-846-8270D 123319 Hydroquinone 0.121

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 SVOC SW-846-8270D 108952 Phenol 0.015 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0040 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 106990 1,3-butadiene 0.0054 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0049 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 71432 Benzene 0.0034 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 108907 Chlorobenzene 0.0027 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 67663 Chloroform 0.0035 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 98828 Cumene 0.0040 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0451

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 100414 Ethylbenzene 0.0032 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0091

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0034 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0123

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 75092 Methylene chloride 0.0145

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 110543 n-Hexane 0.0070 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 108883 Toluene 0.0033 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0043 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0035 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 108054 Vinyl acetate 172

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 593602 Vinyl bromide 0.0025 Non-detect

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VC EPA Method 107 75014 Vinyl chloride Detection Limit Not ReportedNon-detect VI Note (9)

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0045 Non-detect

12/12/2013 VI Confidential 136 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa SPVC TX 02/05/13 Suspension Blending, Dispersion, Copolymer 35 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0087 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 Alcohol SW-846-8015C 67561 Methanol 13.2

Formosa DE E2 01/07/13 Emulsion 1 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.38

Formosa DE E2 01/07/13 Emulsion 1 Aldehyde SW-846-8315A 50000 Formaldehyde 4.11

Formosa DE E2 01/07/13 Emulsion 1 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 SVOC SW-846-8270D 98862 Acetophenone 0.00029 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0006 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 01/07/13 Emulsion 1 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0147

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0026 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0147

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 VC EPA Method 107 75014 Vinyl chloride 0.4639

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect

Formosa DE E2 01/07/13 Emulsion 1 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 Alcohol SW-846-8015C 67561 Methanol 21.5

Formosa DE E2 01/07/13 Emulsion 2 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.02

Formosa DE E2 01/07/13 Emulsion 2 Aldehyde SW-846-8315A 50000 Formaldehyde 2.94

Formosa DE E2 01/07/13 Emulsion 2 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 SVOC SW-846-8270D 98862 Acetophenone 0.00029 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0015

Formosa DE E2 01/07/13 Emulsion 2 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 01/07/13 Emulsion 2 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0265

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0026 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.008

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 108054 Vinyl acetate 3.99

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 VC EPA Method 107 75014 Vinyl chloride 1.276

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect

Formosa DE E2 01/07/13 Emulsion 2 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 Alcohol SW-846-8015C 67561 Methanol 66 J-Estimated Value

Formosa DE E2 01/10/13 Emulsion 3 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.04

Formosa DE E2 01/10/13 Emulsion 3 Aldehyde SW-846-8315A 50000 Formaldehyde 0.19 J-Estimated Value

Formosa DE E2 01/10/13 Emulsion 3 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.66 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 SVOC SW-846-8270D 98862 Acetophenone 0.011 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.023 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 01/10/13 Emulsion 3 SVOC SW-846-8270D 108952 Phenol 0.051 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0227

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0026 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.015

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 108054 Vinyl acetate 4.2

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 VC EPA Method 107 75014 Vinyl chloride 1.5788

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect

Formosa DE E2 01/10/13 Emulsion 3 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 Alcohol SW-846-8015C 67561 Methanol 65.2

Formosa DE E2 01/10/13 Emulsion 4 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.74

Formosa DE E2 01/10/13 Emulsion 4 Aldehyde SW-846-8315A 50000 Formaldehyde 0.272 J-Estimated Value

Formosa DE E2 01/10/13 Emulsion 4 SVOC SW-846-8270D 51285 2,4-dinitrophenol R

Formosa DE E2 01/10/13 Emulsion 4 SVOC SW-846-8270D 98862 Acetophenone 0.0014 Non-detect

12/12/2013 VI Confidential 137 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa DE E2 01/10/13 Emulsion 4 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0029 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 01/10/13 Emulsion 4 SVOC SW-846-8270D 108952 Phenol 0.0064 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0054 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 106990 1,3-butadiene 0.048 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0056 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 71432 Benzene 0.0059 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 108907 Chlorobenzene 0.0057 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 67663 Chloroform 0.0051 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 126998 Chloroprene 0.0052 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 98828 Cumene 0.011 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.018

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 100414 Ethylbenzene 0.0057 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0065 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0027 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0132

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 75092 Methylene chloride 0.018 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 110543 n-Hexane 0.012 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 108883 Toluene 0.0057 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0059 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0072 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 108054 Vinyl acetate 6.28

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 593602 Vinyl bromide 0.0067 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 VC EPA Method 107 75014 Vinyl chloride 1.2314

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0048 Non-detect

Formosa DE E2 01/10/13 Emulsion 4 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.006 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 Alcohol SW-846-8015C 67561 Methanol 0.045 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 Aldehyde SW-846-8315A 75070 Acetaldehyde 9.14

Formosa DE E2 01/14/13 Emulsion 5 Aldehyde SW-846-8315A 50000 Formaldehyde 0.013 J-Estimated Value

Formosa DE E2 01/14/13 Emulsion 5 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 SVOC SW-846-8270D 98862 Acetophenone 0.00029 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 01/14/13 Emulsion 5 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0054 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 106990 1,3-butadiene 0.048 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0056 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 71432 Benzene 0.0059 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 108907 Chlorobenzene 0.0057 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 67663 Chloroform 0.0051 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 126998 Chloroprene 0.0052 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 98828 Cumene 0.011 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0066 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 100414 Ethylbenzene 0.0057 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0065 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0027 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0285

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 75092 Methylene chloride 0.018 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 110543 n-Hexane 0.012 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 108883 Toluene 0.0057 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0059 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0072 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 108054 Vinyl acetate 0.0408

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 593602 Vinyl bromide 0.0067 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 VC EPA Method 107 75014 Vinyl chloride Non-detect

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0048 Non-detect

Formosa DE E2 01/14/13 Emulsion 5 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.006 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 Alcohol SW-846-8015C 67561 Methanol 0.045 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 Aldehyde SW-846-8315A 75070 Acetaldehyde 9.08

Formosa DE E2 01/14/13 Emulsion 6 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0246 J-Estimated Value

Formosa DE E2 01/14/13 Emulsion 6 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 SVOC SW-846-8270D 98862 Acetophenone 0.00029 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 01/14/13 Emulsion 6 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0054 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 106990 1,3-butadiene 0.048 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0056 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 71432 Benzene 0.0059 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 108907 Chlorobenzene 0.0057 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 67663 Chloroform 0.0051 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 126998 Chloroprene 0.0052 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 98828 Cumene 0.011 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0066 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 100414 Ethylbenzene 0.0057 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0065 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0027 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0099

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 75092 Methylene chloride 0.018 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 110543 n-Hexane 0.012 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 108883 Toluene 0.0057 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0059 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0072 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 108054 Vinyl acetate 0.86

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 593602 Vinyl bromide 0.0067 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 VC EPA Method 107 75014 Vinyl chloride Non-detect

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0048 Non-detect

Formosa DE E2 01/14/13 Emulsion 6 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.006 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 Alcohol SW-846-8015C 67561 Methanol 93

Formosa DE E2 01/23/13 Emulsion 7 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.04 J-Estimated Value

Formosa DE E2 01/23/13 Emulsion 7 Aldehyde SW-846-8315A 50000 Formaldehyde 0.228

Formosa DE E2 01/23/13 Emulsion 7 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.17 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 SVOC SW-846-8270D 98862 Acetophenone 0.0029 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0059 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 01/23/13 Emulsion 7 SVOC SW-846-8270D 108952 Phenol 0.013 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0026 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0026 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0118

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 VC EPA Method 107 75014 Vinyl chloride 0.1344

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect

Formosa DE E2 01/23/13 Emulsion 7 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 Alcohol SW-846-8015C 67561 Methanol 96.9

Formosa DE E2 01/23/13 Emulsion 8 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.87 J-Estimated Value

Formosa DE E2 01/23/13 Emulsion 8 Aldehyde SW-846-8315A 50000 Formaldehyde 0.241

Formosa DE E2 01/23/13 Emulsion 8 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.17 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 SVOC SW-846-8270D 98862 Acetophenone 0.0029 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0059 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 01/23/13 Emulsion 8 SVOC SW-846-8270D 108952 Phenol 0.013 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 106990 1,3-butadiene R Rejected

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0119

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0026 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0021 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 VC EPA Method 107 75014 Vinyl chloride 0.4777

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect

Formosa DE E2 01/23/13 Emulsion 8 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 Alcohol SW-846-8015C 67561 Methanol 47.9

Formosa DE E2 01/31/13 Emulsion 9 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.82 J-Estimated Value

Formosa DE E2 01/31/13 Emulsion 9 Aldehyde SW-846-8315A 50000 Formaldehyde 0.219 J-Estimated Value

Formosa DE E2 01/31/13 Emulsion 9 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 SVOC SW-846-8270D 98862 Acetophenone 0.00029 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 01/31/13 Emulsion 9 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0026 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0026 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0021 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VC EPA Method 107 75014 Vinyl chloride 1.6468

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect

Formosa DE E2 01/31/13 Emulsion 9 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 Alcohol SW-846-8015C 107211 Ethylene glycol 0.01 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 Alcohol SW-846-8015C 67561 Methanol 56

Formosa DE E2 01/31/13 Emulsion 10 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.42 J-Estimated Value

Formosa DE E2 01/31/13 Emulsion 10 Aldehyde SW-846-8315A 50000 Formaldehyde 0.268 J-Estimated Value

Formosa DE E2 01/31/13 Emulsion 10 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 SVOC SW-846-8270D 98862 Acetophenone 0.00029 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 01/31/13 Emulsion 10 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0097

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0026 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0021 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 VC EPA Method 107 75014 Vinyl chloride 0.4591

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect

Formosa DE E2 01/31/13 Emulsion 10 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 Alcohol SW-846-8015C 67561 Methanol 0.045 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 Aldehyde SW-846-8315A 75070 Acetaldehyde 8.47 J-Estimated Value

Formosa DE E2 02/07/13 Copolymer 11 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0756 J-Estimated Value

Formosa DE E2 02/07/13 Copolymer 11 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 SVOC SW-846-8270D 98862 Acetophenone 0.00029 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0052

Formosa DE E2 02/07/13 Copolymer 11 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 02/07/13 Copolymer 11 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00021 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 106990 1,3-butadiene 0.0019 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00023 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 71432 Benzene 0.00024 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 108907 Chlorobenzene 0.00023 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 67663 Chloroform 0.0002 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 126998 Chloroprene 0.00021 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 98828 Cumene 0.00045 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.00026 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 100414 Ethylbenzene 0.00023 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00026 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0094

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 75092 Methylene chloride 0.0007 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 110543 n-Hexane 0.00046 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 108883 Toluene 0.00023 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00024 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00029 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 108054 Vinyl acetate 0.251

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 593602 Vinyl bromide 0.00027 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 VC EPA Method 107 75014 Vinyl chloride 0.3055

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00019 Non-detect

Formosa DE E2 02/07/13 Copolymer 11 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00024 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 Alcohol SW-846-8015C 67561 Methanol 0.045 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 Aldehyde SW-846-8315A 75070 Acetaldehyde 9.69 J-Estimated Value

Formosa DE E2 02/07/13 Copolymer 12 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0881 J-Estimated Value

Formosa DE E2 02/07/13 Copolymer 12 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 SVOC SW-846-8270D 98862 Acetophenone 0.00029 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 02/07/13 Copolymer 12 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00021 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 106990 1,3-butadiene 0.0019 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00023 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 71432 Benzene 0.00024 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 108907 Chlorobenzene 0.00023 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 67663 Chloroform 0.0002 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 126998 Chloroprene 0.00021 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 98828 Cumene 0.00045 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0297

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 100414 Ethylbenzene 0.00023 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0041

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0154

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 75092 Methylene chloride 0.0007 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 110543 n-Hexane 0.00046 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 108883 Toluene 0.00023 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00024 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00029 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 108054 Vinyl acetate 3.76

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 593602 Vinyl bromide 0.00027 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 VC EPA Method 107 75014 Vinyl chloride 1.0615

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00019 Non-detect

Formosa DE E2 02/07/13 Copolymer 12 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00024 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 Alcohol SW-846-8015C 67561 Methanol 0.045 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.46 J-Estimated Value

Formosa DE E2 02/12/13 Copolymer 13 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0209

Formosa DE E2 02/12/13 Copolymer 13 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 SVOC SW-846-8270D 98862 Acetophenone 0.00029 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 02/12/13 Copolymer 13 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.011 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 106990 1,3-butadiene 0.095 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.011 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 71432 Benzene 0.012 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 108907 Chlorobenzene 0.011 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 67663 Chloroform 0.01 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 126998 Chloroprene 0.01 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 98828 Cumene 0.022 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0637

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 100414 Ethylbenzene 0.011 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.013 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0053 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0491

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 75092 Methylene chloride 0.035 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 110543 n-Hexane 0.023 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 108883 Toluene 0.011 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.012 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.014 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 108054 Vinyl acetate 39.9

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 593602 Vinyl bromide 0.013 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 VC EPA Method 107 75014 Vinyl chloride 2.1305

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0096 Non-detect

Formosa DE E2 02/12/13 Copolymer 13 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.012 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 Alcohol SW-846-8015C 67561 Methanol 0.045 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.11 J-Estimated Value

Formosa DE E2 02/12/13 Copolymer 14 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0175

Formosa DE E2 02/12/13 Copolymer 14 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 SVOC SW-846-8270D 98862 Acetophenone 0.00029 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 02/12/13 Copolymer 14 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.011 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 106990 1,3-butadiene 0.095 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.011 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 71432 Benzene 0.012 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 108907 Chlorobenzene 0.011 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 67663 Chloroform 0.01 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 126998 Chloroprene 0.01 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 98828 Cumene 0.022 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0487

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 100414 Ethylbenzene 0.011 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.013 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0053 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0484

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 75092 Methylene chloride 0.035 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 110543 n-Hexane 0.023 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 108883 Toluene 0.011 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.012 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.014 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 108054 Vinyl acetate 38.5

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 593602 Vinyl bromide 0.013 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 VC EPA Method 107 75014 Vinyl chloride 1.9344

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0096 Non-detect

Formosa DE E2 02/12/13 Copolymer 14 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.012 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 Alcohol SW-846-8015C 67561 Methanol 0.045 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 Aldehyde SW-846-8315A 75070 Acetaldehyde 58.4

Formosa DE E2 02/14/13 Copolymer 15 Aldehyde SW-846-8315A 50000 Formaldehyde 0.6 J-Estimated Value

Formosa DE E2 02/14/13 Copolymer 15 SVOC SW-846-8270D 51285 2,4-dinitrophenol R

Formosa DE E2 02/14/13 Copolymer 15 SVOC SW-846-8270D 98862 Acetophenone 3.08

Formosa DE E2 02/14/13 Copolymer 15 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0059 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 02/14/13 Copolymer 15 SVOC SW-846-8270D 108952 Phenol 0.013 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 2.1 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 106990 1,3-butadiene 19 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 2.3 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 71432 Benzene 2.4 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 108907 Chlorobenzene 2.3 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 67663 Chloroform 2 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 126998 Chloroprene 2.1 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 98828 Cumene 4.5 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 2.6 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 100414 Ethylbenzene 2.3 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 2.6 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 1.1 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 2.1 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 75092 Methylene chloride 7 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 110543 n-Hexane 4.6 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 108883 Toluene 2.3 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 2.4 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 2.9 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 108054 Vinyl acetate 10700

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 593602 Vinyl bromide 2.7 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VC EPA Method 107 75014 Vinyl chloride Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 1.9 Non-detect

Formosa DE E2 02/14/13 Copolymer 15 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 2.4 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 Alcohol SW-846-8015C 67561 Methanol 0.045 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 Aldehyde SW-846-8315A 75070 Acetaldehyde 60.3

Formosa DE E2 02/14/13 Copolymer 16 Aldehyde SW-846-8315A 50000 Formaldehyde 0.61 J-Estimated Value

Formosa DE E2 02/14/13 Copolymer 16 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.17 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 SVOC SW-846-8270D 98862 Acetophenone 2.56

Formosa DE E2 02/14/13 Copolymer 16 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0059 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 02/14/13 Copolymer 16 SVOC SW-846-8270D 108952 Phenol 0.013 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 2.1 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 106990 1,3-butadiene 19 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 2.3 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 71432 Benzene 2.4 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 108907 Chlorobenzene 2.3 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 67663 Chloroform 2 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 126998 Chloroprene 2.1 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 98828 Cumene 4.5 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 2.6 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 100414 Ethylbenzene 2.3 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 2.6 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 1.1 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 2.1 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 75092 Methylene chloride 7 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 110543 n-Hexane 4.6 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 108883 Toluene 2.3 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 2.4 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 2.9 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 108054 Vinyl acetate 10900

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 593602 Vinyl bromide 2.7 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VC EPA Method 107 75014 Vinyl chloride Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 1.9 Non-detect

Formosa DE E2 02/14/13 Copolymer 16 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 2.4 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 Alcohol SW-846-8015C 67561 Methanol 3050

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa DE E2 02/25/13 Emulsion 17 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.7 J-Estimated Value

Formosa DE E2 02/25/13 Emulsion 17 Aldehyde SW-846-8315A 50000 Formaldehyde R Rejected

Formosa DE E2 02/25/13 Emulsion 17 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.083 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 SVOC SW-846-8270D 98862 Acetophenone 0.0014 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0029 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 SVOC SW-846-8270D 123319 Hydroquinone 0.025 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 SVOC SW-846-8270D 108952 Phenol 0.0064 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.21 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 106990 1,3-butadiene 1.9 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.23 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 71432 Benzene 0.24 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 108907 Chlorobenzene 0.23 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 67663 Chloroform 0.2 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 126998 Chloroprene 0.21 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 98828 Cumene 0.45 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 1.28

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 100414 Ethylbenzene 0.23 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.26 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.11 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.798

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 75092 Methylene chloride 0.7 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 110543 n-Hexane 0.46 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 108883 Toluene 0.23 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.24 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.29 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 108054 Vinyl acetate 176

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 593602 Vinyl bromide 0.27 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 VC EPA Method 107 75014 Vinyl chloride 18.1496

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.19 Non-detect

Formosa DE E2 02/25/13 Emulsion 17 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.24 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 Alcohol SW-846-8015C 67561 Methanol 2700

Formosa DE E2 02/25/13 Emulsion 18 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.19 J-Estimated Value

Formosa DE E2 02/25/13 Emulsion 18 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0074 J-Estimated Value

Formosa DE E2 02/25/13 Emulsion 18 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 SVOC SW-846-8270D 98862 Acetophenone 0.00029 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.21 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 106990 1,3-butadiene 1.9 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.23 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 71432 Benzene 0.24 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 108907 Chlorobenzene 0.23 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 67663 Chloroform 0.2 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 126998 Chloroprene 0.21 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 98828 Cumene 0.45 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 1.37

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 100414 Ethylbenzene 0.23 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.26 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.11 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.765

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 75092 Methylene chloride 0.7 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 110543 n-Hexane 0.46 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 108883 Toluene 0.23 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.24 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.29 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 108054 Vinyl acetate 197

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 593602 Vinyl bromide 0.27 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 VC EPA Method 107 75014 Vinyl chloride 15.4083

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.19 Non-detect

Formosa DE E2 02/25/13 Emulsion 18 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.24 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 Alcohol SW-846-8015C 67561 Methanol 82.8

Formosa DE E2 03/07/13 Copolymer 19 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.19

Formosa DE E2 03/07/13 Copolymer 19 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14 J-Estimated Value

Formosa DE E2 03/07/13 Copolymer 19 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 SVOC SW-846-8270D 98862 Acetophenone 0.00029 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0013

Formosa DE E2 03/07/13 Copolymer 19 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 03/07/13 Copolymer 19 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0026 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.006

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0101

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 108054 Vinyl acetate 2.28

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 VC EPA Method 107 75014 Vinyl chloride Non-detect

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect

Formosa DE E2 03/07/13 Copolymer 19 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect

Formosa DE E2 03/07/13 Copolymer 20 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 03/07/13 Copolymer 20 Alcohol SW-846-8015C 67561 Methanol 76.3 J-Estimated Value

Formosa DE E2 03/07/13 Copolymer 20 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.95

Formosa DE E2 03/07/13 Copolymer 20 Aldehyde SW-846-8315A 50000 Formaldehyde 0.126 J-Estimated Value

Formosa DE E2 03/07/13 Copolymer 20 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect

Formosa DE E2 03/07/13 Copolymer 20 SVOC SW-846-8270D 98862 Acetophenone 0.00029 Non-detect

Formosa DE E2 03/07/13 Copolymer 20 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0093

Formosa DE E2 03/07/13 Copolymer 20 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 03/07/13 Copolymer 20 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0101

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0089

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0231

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 108054 Vinyl acetate 6.38

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect

Formosa DE E2 03/07/13 Copolymer 20 VC EPA Method 107 75014 Vinyl chloride 0.5051

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect

Formosa DE E2 03/07/13 Copolymer 20 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 Alcohol SW-846-8015C 67561 Methanol 102

Formosa DE E2 03/12/13 Copolymer 21 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.35

Formosa DE E2 03/12/13 Copolymer 21 Aldehyde SW-846-8315A 50000 Formaldehyde 0.295

Formosa DE E2 03/12/13 Copolymer 21 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.17 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 SVOC SW-846-8270D 98862 Acetophenone 0.0029 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0059 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 03/12/13 Copolymer 21 SVOC SW-846-8270D 108952 Phenol 0.013 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 126998 Chloroprene R Rejected

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0252

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0078

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0171

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 108054 Vinyl acetate 2.2

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 VC EPA Method 107 75014 Vinyl chloride Non-detect

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect

Formosa DE E2 03/12/13 Copolymer 21 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 Alcohol SW-846-8015C 67561 Methanol 76.9 J-Estimated Value

Formosa DE E2 03/12/13 Copolymer 22 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.26

Formosa DE E2 03/12/13 Copolymer 22 Aldehyde SW-846-8315A 50000 Formaldehyde 0.259

Formosa DE E2 03/12/13 Copolymer 22 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.17 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 SVOC SW-846-8270D 98862 Acetophenone 0.0029 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0059 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 03/12/13 Copolymer 22 SVOC SW-846-8270D 108952 Phenol 0.013 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 126998 Chloroprene R Rejected

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0266

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0085

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0181

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 108054 Vinyl acetate 2.79

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 VC EPA Method 107 75014 Vinyl chloride 0.304

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect

Formosa DE E2 03/12/13 Copolymer 22 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 Alcohol SW-846-8015C 67561 Methanol 0.045 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.14 J-Estimated Value

Formosa DE E2 03/18/13 Copolymer 23 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0406 J-Estimated Value

Formosa DE E2 03/18/13 Copolymer 23 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.033 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 SVOC SW-846-8270D 98862 Acetophenone 1.47

Formosa DE E2 03/18/13 Copolymer 23 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0012 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 03/18/13 Copolymer 23 SVOC SW-846-8270D 108952 Phenol 0.0026 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0043 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 106990 1,3-butadiene 0.038 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 71432 Benzene 0.0047 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 108907 Chlorobenzene 0.0046 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 67663 Chloroform 0.0041 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 98828 Cumene 0.0089 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0475

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 100414 Ethylbenzene 0.0046 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0102

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0021 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0274

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 75092 Methylene chloride 0.014 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 110543 n-Hexane 0.0093 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 108883 Toluene 0.0045 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0047 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0057 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 108054 Vinyl acetate 112

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 593602 Vinyl bromide 0.0054 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 VC EPA Method 107 75014 Vinyl chloride 0.8333

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0038 Non-detect

Formosa DE E2 03/18/13 Copolymer 23 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0048 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 Alcohol SW-846-8015C 67561 Methanol 0.045 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.41 J-Estimated Value

Formosa DE E2 03/18/13 Copolymer 24 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0434 J-Estimated Value

Formosa DE E2 03/18/13 Copolymer 24 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.033 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 SVOC SW-846-8270D 98862 Acetophenone 1.29

Formosa DE E2 03/18/13 Copolymer 24 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0012 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 03/18/13 Copolymer 24 SVOC SW-846-8270D 108952 Phenol 0.0026 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0043 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 106990 1,3-butadiene 0.038 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 71432 Benzene 0.0047 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 108907 Chlorobenzene 0.0046 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 67663 Chloroform 0.0041 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 98828 Cumene 0.0089 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0476

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 100414 Ethylbenzene 0.0046 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.009

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0021 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0281

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 75092 Methylene chloride 0.014 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 110543 n-Hexane 0.0093 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 108883 Toluene 0.0045 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0047 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0057 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 108054 Vinyl acetate 114

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 593602 Vinyl bromide 0.0054 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 VC EPA Method 107 75014 Vinyl chloride 0.6553

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0038 Non-detect

Formosa DE E2 03/18/13 Copolymer 24 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0048 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 Alcohol SW-846-8015C 67561 Methanol 22.4

Formosa DE E2 03/27/13 Emulsion 25 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.1

Formosa DE E2 03/27/13 Emulsion 25 Aldehyde SW-846-8315A 50000 Formaldehyde 0.161 J-Estimated Value

Formosa DE E2 03/27/13 Emulsion 25 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 SVOC SW-846-8270D 98862 Acetophenone 0.00029 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 03/27/13 Emulsion 25 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0043 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 106990 1,3-butadiene 0.038 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 71432 Benzene 0.0047 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 108907 Chlorobenzene 0.0046 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 67663 Chloroform 0.0041 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 98828 Cumene 0.0089 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0479

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 100414 Ethylbenzene 0.0046 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0109

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0021 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0329

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 75092 Methylene chloride 0.014 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 110543 n-Hexane 0.0093 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 108883 Toluene 0.0045 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0047 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0057 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 108054 Vinyl acetate 0.022 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 593602 Vinyl bromide 0.0054 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 VC EPA Method 107 75014 Vinyl chloride 0.5743

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0038 Non-detect

Formosa DE E2 03/27/13 Emulsion 25 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0048 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 Alcohol SW-846-8015C 67561 Methanol 47

Formosa DE E2 03/27/13 Emulsion 26 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.19

Formosa DE E2 03/27/13 Emulsion 26 Aldehyde SW-846-8315A 50000 Formaldehyde 0.252

Formosa DE E2 03/27/13 Emulsion 26 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 SVOC SW-846-8270D 98862 Acetophenone 0.00029 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa DE E2 03/27/13 Emulsion 26 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0043 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 106990 1,3-butadiene 0.038 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 71432 Benzene 0.0047 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 108907 Chlorobenzene 0.0046 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 67663 Chloroform 0.0041 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 98828 Cumene 0.0089 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0467

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 100414 Ethylbenzene 0.0046 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0105

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0021 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0295

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 75092 Methylene chloride 0.014 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 110543 n-Hexane 0.0093 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 108883 Toluene 0.0045 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0047 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0057 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 108054 Vinyl acetate 0.022 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 593602 Vinyl bromide 0.0054 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 VC EPA Method 107 75014 Vinyl chloride 0.5793

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0038 Non-detect

Formosa DE E2 03/27/13 Emulsion 26 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0048 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 Alcohol SW-846-8015C 67561 Methanol 36.5

Formosa DE E2 04/01/13 Emulsion 27 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.01

Formosa DE E2 04/01/13 Emulsion 27 Aldehyde SW-846-8315A 50000 Formaldehyde 0.342

Formosa DE E2 04/01/13 Emulsion 27 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 SVOC SW-846-8270D 98862 Acetophenone 0.00029 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0013 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0013 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VC EPA Method 107 75014 Vinyl chloride 0.4078

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect

Formosa DE E2 04/01/13 Emulsion 27 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 Alcohol SW-846-8015C 67561 Methanol 37.2

Formosa DE E2 04/01/13 Emulsion 28 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.88

Formosa DE E2 04/01/13 Emulsion 28 Aldehyde SW-846-8315A 50000 Formaldehyde 0.444

Formosa DE E2 04/01/13 Emulsion 28 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 SVOC SW-846-8270D 98862 Acetophenone 0.00029 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0108

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0013 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0031

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 VC EPA Method 107 75014 Vinyl chloride 0.5673

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect

Formosa DE E2 04/01/13 Emulsion 28 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 Alcohol SW-846-8015C 67561 Methanol 53.1

Formosa DE E2 04/08/13 Emulsion 29 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.67

Formosa DE E2 04/08/13 Emulsion 29 Aldehyde SW-846-8315A 50000 Formaldehyde 0.137

Formosa DE E2 04/08/13 Emulsion 29 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 SVOC SW-846-8270D 98862 Acetophenone 0.00029 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0018 J-estimated value, VI Note (9.1)

Formosa DE E2 04/08/13 Emulsion 29 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 SVOC SW-846-8270D 108952 Phenol 0.0098

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0026 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 4.6 J-estimated value, VI Note (9.1)

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0021 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 VC EPA Method 107 75014 Vinyl chloride 0.1639

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect

Formosa DE E2 04/08/13 Emulsion 29 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 Alcohol SW-846-8015C 67561 Methanol 30.7

Formosa DE E2 04/08/13 Emulsion 30 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.63

Formosa DE E2 04/08/13 Emulsion 30 Aldehyde SW-846-8315A 50000 Formaldehyde 0.156

Formosa DE E2 04/08/13 Emulsion 30 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 SVOC SW-846-8270D 98862 Acetophenone 0.00029 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0026 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 4.5 J-estimated value, VI Note (9.1)

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0021 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 VC EPA Method 107 75014 Vinyl chloride 0.1591

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect

Formosa DE E2 04/08/13 Emulsion 30 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 Alcohol SW-846-8015C 67561 Methanol 2.61

Formosa S2 DE 01/17/13 Emulsion 1 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.0985

Formosa S2 DE 01/17/13 Emulsion 1 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0661

Formosa S2 DE 01/17/13 Emulsion 1 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.17 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 SVOC SW-846-8270D 98862 Acetophenone 0.0029 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0059 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 01/17/13 Emulsion 1 SVOC SW-846-8270D 108952 Phenol 0.013 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0054 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 106990 1,3-butadiene 0.048 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0056 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 71432 Benzene 0.0059 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 108907 Chlorobenzene 0.0057 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 67663 Chloroform 0.0051 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 126998 Chloroprene 0.0052 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 98828 Cumene 0.011 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0066 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 100414 Ethylbenzene 0.0057 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0065 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0027 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0052 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 75092 Methylene chloride 0.018 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 110543 n-Hexane 0.012 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 108883 Toluene 0.0057 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0059 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0072 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 108054 Vinyl acetate 0.028 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 593602 Vinyl bromide 0.0067 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VC EPA Method 107 75014 Vinyl chloride Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0048 Non-detect

Formosa S2 DE 01/17/13 Emulsion 1 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.006 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 Alcohol SW-846-8015C 67561 Methanol 2.82

Formosa S2 DE 01/17/13 Emulsion 2 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.161

Formosa S2 DE 01/17/13 Emulsion 2 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0971

Formosa S2 DE 01/17/13 Emulsion 2 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.17 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 SVOC SW-846-8270D 98862 Acetophenone 0.0029 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0059 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 01/17/13 Emulsion 2 SVOC SW-846-8270D 108952 Phenol 0.013 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0013 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0013 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VC EPA Method 107 75014 Vinyl chloride Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect

Formosa S2 DE 01/17/13 Emulsion 2 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 Alcohol SW-846-8015C 67561 Methanol 5.85

Formosa S2 DE 01/17/13 Emulsion 3 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.983

Formosa S2 DE 01/17/13 Emulsion 3 Aldehyde SW-846-8315A 50000 Formaldehyde 0.361

Formosa S2 DE 01/17/13 Emulsion 3 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa S2 DE 01/17/13 Emulsion 3 SVOC SW-846-8270D 98862 Acetophenone 0.00029 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 01/17/13 Emulsion 3 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00021 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 106990 1,3-butadiene 0.0019 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00023 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 71432 Benzene 0.00026

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 108907 Chlorobenzene 0.00023 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 67663 Chloroform 0.0002 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 126998 Chloroprene 0.00021 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 98828 Cumene 0.00045 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.002

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 100414 Ethylbenzene 0.00023 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00026 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00046

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 75092 Methylene chloride 0.0007 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 110543 n-Hexane 0.00046 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 108883 Toluene 0.00023 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00024 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00029 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 108054 Vinyl acetate 0.0011 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 593602 Vinyl bromide 0.00027 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 VC EPA Method 107 75014 Vinyl chloride 0.1313

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00019 Non-detect

Formosa S2 DE 01/17/13 Emulsion 3 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00024 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 Alcohol SW-846-8015C 67561 Methanol 6.96

Formosa S2 DE 01/17/13 Emulsion 4 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.06

Formosa S2 DE 01/17/13 Emulsion 4 Aldehyde SW-846-8315A 50000 Formaldehyde 0.366 J-Estimated Value

Formosa S2 DE 01/17/13 Emulsion 4 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 SVOC SW-846-8270D 98862 Acetophenone 0.00029 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 01/17/13 Emulsion 4 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00021 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 106990 1,3-butadiene 0.0019 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00023 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 71432 Benzene 0.00029

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 108907 Chlorobenzene 0.00023 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 67663 Chloroform 0.0002 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 126998 Chloroprene 0.00021 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 98828 Cumene 0.00045 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0022

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 100414 Ethylbenzene 0.00023 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.00026 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.00021 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 75092 Methylene chloride 0.0007 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 110543 n-Hexane 0.00046 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 108883 Toluene 0.00023 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00024 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00029 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 108054 Vinyl acetate 0.0011 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 593602 Vinyl bromide 0.00027 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 VC EPA Method 107 75014 Vinyl chloride 0.1124

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00019 Non-detect

Formosa S2 DE 01/17/13 Emulsion 4 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00024 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 Alcohol SW-846-8015C 67561 Methanol 3.19

Formosa S2 DE 01/21/13 Emulsion 5 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.1 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 Aldehyde SW-846-8315A 50000 Formaldehyde 2 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1.7 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 SVOC SW-846-8270D 98862 Acetophenone 0.029 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.059 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 01/21/13 Emulsion 5 SVOC SW-846-8270D 108952 Phenol 0.13 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0054 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 106990 1,3-butadiene 0.048 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0056 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 71432 Benzene 0.0059 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 108907 Chlorobenzene 0.0057 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 67663 Chloroform 0.0051 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 126998 Chloroprene 0.0052 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 98828 Cumene 0.011 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0066 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 100414 Ethylbenzene 0.0057 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0065 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0027 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0052 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 75092 Methylene chloride 0.018 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 110543 n-Hexane 0.012 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 108883 Toluene 0.0057 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0059 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0072 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 108054 Vinyl acetate 0.028 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 593602 Vinyl bromide 0.0067 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VC EPA Method 107 75014 Vinyl chloride 0.1111

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0048 Non-detect

Formosa S2 DE 01/21/13 Emulsion 5 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.006 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 Alcohol SW-846-8015C 67561 Methanol 2.66

Formosa S2 DE 01/21/13 Emulsion 6 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.18 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 Aldehyde SW-846-8315A 50000 Formaldehyde 0.34 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1.7 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 SVOC SW-846-8270D 98862 Acetophenone 0.029 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.059 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 01/21/13 Emulsion 6 SVOC SW-846-8270D 108952 Phenol 0.13 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0054 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 106990 1,3-butadiene 0.048 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0056 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 71432 Benzene 0.0059 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 108907 Chlorobenzene 0.0057 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 67663 Chloroform 0.0051 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 126998 Chloroprene 0.0052 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 98828 Cumene 0.011 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0066 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 100414 Ethylbenzene 0.0057 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0065 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0027 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0052 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 75092 Methylene chloride 0.018 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 110543 n-Hexane 0.012 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 108883 Toluene 0.0057 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0059 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0072 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 108054 Vinyl acetate 0.028 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 593602 Vinyl bromide 0.0067 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 VC EPA Method 107 75014 Vinyl chloride 0.1004

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0048 Non-detect

Formosa S2 DE 01/21/13 Emulsion 6 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.006 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 Alcohol SW-846-8015C 67561 Methanol 13.4

Formosa S2 DE 01/21/13 Emulsion 7 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.42

Formosa S2 DE 01/21/13 Emulsion 7 Aldehyde SW-846-8315A 50000 Formaldehyde 0.111

Formosa S2 DE 01/21/13 Emulsion 7 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1.7 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 SVOC SW-846-8270D 98862 Acetophenone 0.029 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.059 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 01/21/13 Emulsion 7 SVOC SW-846-8270D 108952 Phenol 0.13 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0013 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0013 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VC EPA Method 107 75014 Vinyl chloride 0.1018

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect

Formosa S2 DE 01/21/13 Emulsion 7 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 Alcohol SW-846-8015C 67561 Methanol 12.1

Formosa S2 DE 01/21/13 Emulsion 8 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.74

Formosa S2 DE 01/21/13 Emulsion 8 Aldehyde SW-846-8315A 50000 Formaldehyde 0.1

Formosa S2 DE 01/21/13 Emulsion 8 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1.7 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 SVOC SW-846-8270D 98862 Acetophenone 0.029 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.178

Formosa S2 DE 01/21/13 Emulsion 8 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 01/21/13 Emulsion 8 SVOC SW-846-8270D 108952 Phenol 0.13 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0013 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0013 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VC EPA Method 107 75014 Vinyl chloride 0.0969

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect

Formosa S2 DE 01/21/13 Emulsion 8 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 Alcohol SW-846-8015C 67561 Methanol 26.1

Formosa S2 DE 01/29/13 Emulsion 9 Aldehyde SW-846-8315A 75070 Acetaldehyde 23.3

Formosa S2 DE 01/29/13 Emulsion 9 Aldehyde SW-846-8315A 50000 Formaldehyde 0.179

Formosa S2 DE 01/29/13 Emulsion 9 SVOC SW-846-8270D 51285 2,4-dinitrophenol 17 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 SVOC SW-846-8270D 98862 Acetophenone 0.29 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.59 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 SVOC SW-846-8270D 123319 Hydroquinone 5 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 SVOC SW-846-8270D 108952 Phenol 1.3 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0054 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 106990 1,3-butadiene 0.048 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0056 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 71432 Benzene 0.0059 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 108907 Chlorobenzene 0.0057 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 67663 Chloroform 0.0051 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 126998 Chloroprene 0.0052 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 98828 Cumene 0.011 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0066 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 100414 Ethylbenzene 0.0057 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0065 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0027 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0052 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 75092 Methylene chloride 0.018 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 110543 n-Hexane 0.012 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 108883 Toluene 0.0057 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0059 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0072 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 108054 Vinyl acetate 0.028 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 593602 Vinyl bromide 0.0067 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 VC EPA Method 107 75014 Vinyl chloride 2.1224

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0048 Non-detect

Formosa S2 DE 01/29/13 Emulsion 9 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.006 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 Alcohol SW-846-8015C 67561 Methanol 21

Formosa S2 DE 01/29/13 Emulsion 10 Aldehyde SW-846-8315A 75070 Acetaldehyde 26.5

Formosa S2 DE 01/29/13 Emulsion 10 Aldehyde SW-846-8315A 50000 Formaldehyde 0.212

Formosa S2 DE 01/29/13 Emulsion 10 SVOC SW-846-8270D 51285 2,4-dinitrophenol 17 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 SVOC SW-846-8270D 98862 Acetophenone 0.29 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.59 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 SVOC SW-846-8270D 123319 Hydroquinone 5 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 SVOC SW-846-8270D 108952 Phenol 1.3 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0054 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 106990 1,3-butadiene 0.048 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0056 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 71432 Benzene 0.0059 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 108907 Chlorobenzene 0.0057 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 67663 Chloroform 0.0051 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 126998 Chloroprene 0.0052 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 98828 Cumene 0.011 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0066 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 100414 Ethylbenzene 0.0057 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0065 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0027 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0052 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 75092 Methylene chloride 0.018 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 110543 n-Hexane 0.012 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 108883 Toluene 0.0057 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0059 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0072 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 108054 Vinyl acetate 0.028 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 593602 Vinyl bromide 0.0067 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VC EPA Method 107 75014 Vinyl chloride 1.7713

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0048 Non-detect

Formosa S2 DE 01/29/13 Emulsion 10 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.006 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 Alcohol SW-846-8015C 67561 Methanol 5.54

Formosa S2 DE 02/01/13 Emulsion 11 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.01

Formosa S2 DE 02/01/13 Emulsion 11 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0728

Formosa S2 DE 02/01/13 Emulsion 11 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1.7 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 SVOC SW-846-8270D 98862 Acetophenone 0.029 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.059 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 02/01/13 Emulsion 11 SVOC SW-846-8270D 108952 Phenol 0.13 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0043 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 106990 1,3-butadiene 0.038 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 71432 Benzene 0.0047 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 108907 Chlorobenzene 0.0046 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 67663 Chloroform 0.0041 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 98828 Cumene 0.0089 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0052 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 100414 Ethylbenzene 0.0046 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0052 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0021 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0041 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 75092 Methylene chloride 0.014 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 110543 n-Hexane 0.0093 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 108883 Toluene 0.0045 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0047 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0057 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 108054 Vinyl acetate 0.022 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 593602 Vinyl bromide 0.0054 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VC EPA Method 107 75014 Vinyl chloride 0.3329

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0038 Non-detect

Formosa S2 DE 02/01/13 Emulsion 11 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0048 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 Alcohol SW-846-8015C 67561 Methanol 5.16

Formosa S2 DE 02/01/13 Emulsion 12 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.55 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 Aldehyde SW-846-8315A 50000 Formaldehyde 1 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1.7 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 SVOC SW-846-8270D 98862 Acetophenone 0.029 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.059 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 02/01/13 Emulsion 12 SVOC SW-846-8270D 108952 Phenol 0.13 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0043 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 106990 1,3-butadiene 0.038 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 71432 Benzene 0.0047 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 108907 Chlorobenzene 0.0046 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 67663 Chloroform 0.0041 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 98828 Cumene 0.0089 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0052 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 100414 Ethylbenzene 0.0046 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0052 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0021 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0041 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 75092 Methylene chloride 0.014 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 110543 n-Hexane 0.0093 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 108883 Toluene 0.0045 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0047 Non-detect

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0057 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 108054 Vinyl acetate 0.022 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 593602 Vinyl bromide 0.0054 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 VC EPA Method 107 75014 Vinyl chloride 0.3831

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0038 Non-detect

Formosa S2 DE 02/01/13 Emulsion 12 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0048 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 Alcohol SW-846-8015C 67561 Methanol 1.22

Formosa S2 DE 02/06/13 Emulsion 13 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.87 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 Aldehyde SW-846-8315A 50000 Formaldehyde 1.6 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 SVOC SW-846-8270D 51285 2,4-dinitrophenol 17 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 SVOC SW-846-8270D 98862 Acetophenone 0.29 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.59 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 02/06/13 Emulsion 13 SVOC SW-846-8270D 108952 Phenol 1.3 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0026 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0026 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0021 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VC EPA Method 107 75014 Vinyl chloride 0.3223

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect

Formosa S2 DE 02/06/13 Emulsion 13 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 Alcohol SW-846-8015C 67561 Methanol 1.13

Formosa S2 DE 02/06/13 Emulsion 14 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.3 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 Aldehyde SW-846-8315A 50000 Formaldehyde 2.4 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 SVOC SW-846-8270D 51285 2,4-dinitrophenol 17 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 SVOC SW-846-8270D 98862 Acetophenone 0.29 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.59 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 02/06/13 Emulsion 14 SVOC SW-846-8270D 108952 Phenol 1.3 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0013 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0013 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VC EPA Method 107 75014 Vinyl chloride 0.2677

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect

Formosa S2 DE 02/06/13 Emulsion 14 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 Alcohol SW-846-8015C 67561 Methanol 7.11

Formosa S2 DE 02/11/13 Emulsion 15 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.15 J-Estimated Value

Formosa S2 DE 02/11/13 Emulsion 15 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0565

Formosa S2 DE 02/11/13 Emulsion 15 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.17 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 SVOC SW-846-8270D 98862 Acetophenone 0.0029 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0059 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 02/11/13 Emulsion 15 SVOC SW-846-8270D 108952 Phenol 0.013 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0043 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 106990 1,3-butadiene 0.038 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 71432 Benzene 0.0047 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 108907 Chlorobenzene 0.0046 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 67663 Chloroform 0.0041 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 98828 Cumene 0.0089 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0052 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 100414 Ethylbenzene 0.0046 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0052 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0021 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0041 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 75092 Methylene chloride 0.014 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 110543 n-Hexane 0.0093 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 108883 Toluene 0.0045 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0047 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0057 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 108054 Vinyl acetate 0.022 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 593602 Vinyl bromide 0.0054 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VC EPA Method 107 75014 Vinyl chloride 0.137

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0038 Non-detect

Formosa S2 DE 02/11/13 Emulsion 15 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0048 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa S2 DE 02/11/13 Emulsion 16 Alcohol SW-846-8015C 67561 Methanol 9.21

Formosa S2 DE 02/11/13 Emulsion 16 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.12 J-Estimated Value

Formosa S2 DE 02/11/13 Emulsion 16 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0515

Formosa S2 DE 02/11/13 Emulsion 16 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.17 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 SVOC SW-846-8270D 98862 Acetophenone 0.0029 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0059 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 02/11/13 Emulsion 16 SVOC SW-846-8270D 108952 Phenol 0.013 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0043 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 106990 1,3-butadiene 0.038 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 71432 Benzene 0.0047 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 108907 Chlorobenzene 0.0046 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 67663 Chloroform 0.0041 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 98828 Cumene 0.0089 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0052 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 100414 Ethylbenzene 0.0046 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0052 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0021 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0041 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 75092 Methylene chloride 0.014 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 110543 n-Hexane 0.0093 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 108883 Toluene 0.0045 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0047 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0057 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 108054 Vinyl acetate 0.022 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 593602 Vinyl bromide 0.0054 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VC EPA Method 107 75014 Vinyl chloride 0.1321

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0038 Non-detect

Formosa S2 DE 02/11/13 Emulsion 16 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0048 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 Alcohol SW-846-8015C 67561 Methanol 19

Formosa S2 DE 02/19/13 Emulsion 17 Aldehyde SW-846-8315A 75070 Acetaldehyde 9.16

Formosa S2 DE 02/19/13 Emulsion 17 Aldehyde SW-846-8315A 50000 Formaldehyde 0.144 J-Estimated Value

Formosa S2 DE 02/19/13 Emulsion 17 SVOC SW-846-8270D 51285 2,4-dinitrophenol 3.3 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 SVOC SW-846-8270D 98862 Acetophenone 0.057 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.12 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 SVOC SW-846-8270D 123319 Hydroquinone 1 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 SVOC SW-846-8270D 108952 Phenol 0.26 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0043 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 106990 1,3-butadiene 0.038 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 71432 Benzene 0.0047 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 108907 Chlorobenzene 0.0046 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 67663 Chloroform 0.0041 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 98828 Cumene 0.0089 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0279

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 100414 Ethylbenzene 0.0046 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0052 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0021 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0041 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 75092 Methylene chloride 0.014 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 110543 n-Hexane 0.0093 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 108883 Toluene 0.0045 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0047 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0057 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 108054 Vinyl acetate 0.022 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 593602 Vinyl bromide 0.0054 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 VC EPA Method 107 75014 Vinyl chloride 0.6792

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0038 Non-detect

Formosa S2 DE 02/19/13 Emulsion 17 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0048 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 Alcohol SW-846-8015C 67561 Methanol 14.4

Formosa S2 DE 02/19/13 Emulsion 18 Aldehyde SW-846-8315A 75070 Acetaldehyde 9.68

Formosa S2 DE 02/19/13 Emulsion 18 Aldehyde SW-846-8315A 50000 Formaldehyde 0.159 J-Estimated Value

Formosa S2 DE 02/19/13 Emulsion 18 SVOC SW-846-8270D 51285 2,4-dinitrophenol 3.3 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 SVOC SW-846-8270D 98862 Acetophenone 0.057 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.12 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 SVOC SW-846-8270D 123319 Hydroquinone 1 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 SVOC SW-846-8270D 108952 Phenol 0.26 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0043 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 106990 1,3-butadiene 0.038 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 71432 Benzene 0.0047 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 108907 Chlorobenzene 0.0046 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 67663 Chloroform 0.0041 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 98828 Cumene 0.0089 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0052 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 100414 Ethylbenzene 0.0046 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0052 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0021 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0041 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 75092 Methylene chloride 0.014 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 110543 n-Hexane 0.0093 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 108883 Toluene 0.0045 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0047 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0057 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 108054 Vinyl acetate 0.022 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 593602 Vinyl bromide 0.0054 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VC EPA Method 107 75014 Vinyl chloride 0.2911

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0038 Non-detect

Formosa S2 DE 02/19/13 Emulsion 18 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0048 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 Alcohol SW-846-8015C 67561 Methanol 4.85

Formosa S2 DE 02/27/13 Emulsion 19 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.597 J-Estimated Value

Formosa S2 DE 02/27/13 Emulsion 19 Aldehyde SW-846-8315A 50000 Formaldehyde R Rejected

Formosa S2 DE 02/27/13 Emulsion 19 SVOC SW-846-8270D 51285 2,4-dinitrophenol R Rejected

Formosa S2 DE 02/27/13 Emulsion 19 SVOC SW-846-8270D 98862 Acetophenone 0.00033 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00067 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa S2 DE 02/27/13 Emulsion 19 SVOC SW-846-8270D 108952 Phenol R Rejected

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0013 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0013 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 VC EPA Method 107 75014 Vinyl chloride 0.244

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect

Formosa S2 DE 02/27/13 Emulsion 19 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 Alcohol SW-846-8015C 67561 Methanol 5.02

Formosa S2 DE 02/27/13 Emulsion 20 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.59 J-Estimated Value

Formosa S2 DE 02/27/13 Emulsion 20 Aldehyde SW-846-8315A 50000 Formaldehyde R Rejected

Formosa S2 DE 02/27/13 Emulsion 20 SVOC SW-846-8270D 51285 2,4-dinitrophenol R Rejected

Formosa S2 DE 02/27/13 Emulsion 20 SVOC SW-846-8270D 98862 Acetophenone R Rejected

Formosa S2 DE 02/27/13 Emulsion 20 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) R Rejected

Formosa S2 DE 02/27/13 Emulsion 20 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 02/27/13 Emulsion 20 SVOC SW-846-8270D 108952 Phenol R Rejected

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0013 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0013 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.001 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 VC EPA Method 107 75014 Vinyl chloride 0.1863

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect

Formosa S2 DE 02/27/13 Emulsion 20 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 Alcohol SW-846-8015C 67561 Methanol 6.14

Formosa S2 DE 02/28/13 Emulsion 21 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.95 J-Estimated Value

Formosa S2 DE 02/28/13 Emulsion 21 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0421 J-Estimated Value

Formosa S2 DE 02/28/13 Emulsion 21 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.17 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 SVOC SW-846-8270D 98862 Acetophenone 0.0029 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0109

Formosa S2 DE 02/28/13 Emulsion 21 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 02/28/13 Emulsion 21 SVOC SW-846-8270D 108952 Phenol 0.013 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0043 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 106990 1,3-butadiene 0.038 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 71432 Benzene 0.0047 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 108907 Chlorobenzene 0.0046 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 67663 Chloroform 0.0041 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 98828 Cumene 0.0089 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0052 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 100414 Ethylbenzene 0.0046 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0052 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0021 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0041 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 75092 Methylene chloride 0.014 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 110543 n-Hexane 0.0093 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 108883 Toluene 0.0045 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0047 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0057 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 108054 Vinyl acetate 0.022 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 593602 Vinyl bromide 0.0054 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VC EPA Method 107 75014 Vinyl chloride 0.3659

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0038 Non-detect

Formosa S2 DE 02/28/13 Emulsion 21 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0048 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 Alcohol SW-846-8015C 67561 Methanol 5.17

Formosa S2 DE 02/28/13 Emulsion 22 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.24 J-Estimated Value

Formosa S2 DE 02/28/13 Emulsion 22 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0507 J-Estimated Value

Formosa S2 DE 02/28/13 Emulsion 22 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.17 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 SVOC SW-846-8270D 98862 Acetophenone 0.0029 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0059 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 02/28/13 Emulsion 22 SVOC SW-846-8270D 108952 Phenol 0.013 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0043 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 106990 1,3-butadiene 0.038 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 71432 Benzene 0.0047 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 108907 Chlorobenzene 0.0046 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 67663 Chloroform 0.0041 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 98828 Cumene 0.0089 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0052 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 100414 Ethylbenzene 0.0046 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0052 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0021 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0041 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 75092 Methylene chloride 0.014 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 110543 n-Hexane 0.0093 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 108883 Toluene 0.0045 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0047 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0057 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 108054 Vinyl acetate 0.022 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 593602 Vinyl bromide 0.0054 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 VC EPA Method 107 75014 Vinyl chloride 0.4436

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0038 Non-detect

Formosa S2 DE 02/28/13 Emulsion 22 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0048 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 Alcohol SW-846-8015C 67561 Methanol 6.09

Formosa S2 DE 03/14/13 Emulsion 23 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.56 Resample value

Formosa S2 DE 03/14/13 Emulsion 23 Aldehyde SW-846-8315A 50000 Formaldehyde 1.11 Resample value

Formosa S2 DE 03/14/13 Emulsion 23 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.17 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 SVOC SW-846-8270D 98862 Acetophenone 0.0029 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0059 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 03/14/13 Emulsion 23 SVOC SW-846-8270D 108952 Phenol 0.013 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0026 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0026 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0021 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VC EPA Method 107 75014 Vinyl chloride 0.2036

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect

Formosa S2 DE 03/14/13 Emulsion 23 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 Alcohol SW-846-8015C 67561 Methanol 6.04

Formosa S2 DE 03/14/13 Emulsion 24 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.63 Resample value

Formosa S2 DE 03/14/13 Emulsion 24 Aldehyde SW-846-8315A 50000 Formaldehyde 1.12 Resample value

Formosa S2 DE 03/14/13 Emulsion 24 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.17 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 SVOC SW-846-8270D 98862 Acetophenone 0.0029 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0059 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 03/14/13 Emulsion 24 SVOC SW-846-8270D 108952 Phenol 0.013 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0026 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0026 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0021 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VC EPA Method 107 75014 Vinyl chloride 0.1892

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect

Formosa S2 DE 03/14/13 Emulsion 24 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 Alcohol SW-846-8015C 67561 Methanol 5.72

Formosa S2 DE 03/19/13 Emulsion 25 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.73 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 Aldehyde SW-846-8315A 50000 Formaldehyde 1.4 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.83 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 SVOC SW-846-8270D 98862 Acetophenone 0.014 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.029 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 03/19/13 Emulsion 25 SVOC SW-846-8270D 108952 Phenol 0.064 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0054 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 106990 1,3-butadiene 0.048 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0056 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 71432 Benzene 0.0059 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 108907 Chlorobenzene 0.0057 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 67663 Chloroform 0.0051 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 126998 Chloroprene 0.0052 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 98828 Cumene 0.011 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0066 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 100414 Ethylbenzene 0.0057 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0065 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0027 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0052 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 75092 Methylene chloride 0.018 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 110543 n-Hexane 0.012 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 108883 Toluene 0.0057 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0059 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0072 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 108054 Vinyl acetate 0.028 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 593602 Vinyl bromide 0.0067 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 VC EPA Method 107 75014 Vinyl chloride 0.2229

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0048 Non-detect

Formosa S2 DE 03/19/13 Emulsion 25 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.006 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 Alcohol SW-846-8015C 67561 Methanol 5.29

Formosa S2 DE 03/19/13 Emulsion 26 Aldehyde SW-846-8315A 75070 Acetaldehyde 1.07

Formosa S2 DE 03/19/13 Emulsion 26 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0373

Formosa S2 DE 03/19/13 Emulsion 26 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.83 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 SVOC SW-846-8270D 98862 Acetophenone 0.014 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.029 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 03/19/13 Emulsion 26 SVOC SW-846-8270D 108952 Phenol 0.064 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0054 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 106990 1,3-butadiene 0.048 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0056 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 71432 Benzene 0.0059 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 108907 Chlorobenzene 0.0057 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 67663 Chloroform 0.0051 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 126998 Chloroprene 0.0052 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 98828 Cumene 0.011 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0066 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 100414 Ethylbenzene 0.0057 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0065 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0027 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0052 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 75092 Methylene chloride 0.018 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 110543 n-Hexane 0.012 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 108883 Toluene 0.0057 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0059 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0072 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 108054 Vinyl acetate 0.028 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 593602 Vinyl bromide 0.0067 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VC EPA Method 107 75014 Vinyl chloride 0.1304

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0048 Non-detect

Formosa S2 DE 03/19/13 Emulsion 26 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.006 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 Alcohol SW-846-8015C 67561 Methanol 11.1

Formosa S2 DE 03/27/13 Emulsion 27 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.13

Formosa S2 DE 03/27/13 Emulsion 27 Aldehyde SW-846-8315A 50000 Formaldehyde 0.068 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 SVOC SW-846-8270D 51285 2,4-dinitrophenol R Rejected

Formosa S2 DE 03/27/13 Emulsion 27 SVOC SW-846-8270D 98862 Acetophenone 0.0029 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0059 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 03/27/13 Emulsion 27 SVOC SW-846-8270D 108952 Phenol R Rejected

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0054 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 106990 1,3-butadiene 0.048 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0056 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 71432 Benzene 0.0059 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 108907 Chlorobenzene 0.0057 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 67663 Chloroform 0.0051 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 126998 Chloroprene 0.0052 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 98828 Cumene 0.011 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0066 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 100414 Ethylbenzene 0.0057 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0065 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0027 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0052 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 75092 Methylene chloride 0.018 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 110543 n-Hexane 0.012 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 108883 Toluene 0.0057 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0059 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0072 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 108054 Vinyl acetate 0.028 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 593602 Vinyl bromide 0.0067 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 VC EPA Method 107 75014 Vinyl chloride 0.0865

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0048 Non-detect

Formosa S2 DE 03/27/13 Emulsion 27 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.006 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 Alcohol SW-846-8015C 67561 Methanol 9.11

Formosa S2 DE 03/27/13 Emulsion 28 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.95

Formosa S2 DE 03/27/13 Emulsion 28 Aldehyde SW-846-8315A 50000 Formaldehyde 0.068 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 SVOC SW-846-8270D 51285 2,4-dinitrophenol R Rejected

Formosa S2 DE 03/27/13 Emulsion 28 SVOC SW-846-8270D 98862 Acetophenone 0.0029 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0059 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 SVOC SW-846-8270D 123319 Hydroquinone R Rejected

Formosa S2 DE 03/27/13 Emulsion 28 SVOC SW-846-8270D 108952 Phenol R Rejected

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0054 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 106990 1,3-butadiene 0.048 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0056 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 71432 Benzene 0.0059 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 108907 Chlorobenzene 0.0057 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 67663 Chloroform 0.0051 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 126998 Chloroprene 0.0052 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 98828 Cumene 0.011 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0066 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 100414 Ethylbenzene 0.0057 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0065 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0027 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0052 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 75092 Methylene chloride 0.018 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 110543 n-Hexane 0.012 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 108883 Toluene 0.0057 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0059 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0072 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 108054 Vinyl acetate 0.028 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 593602 Vinyl bromide 0.0067 Non-detect

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Formosa S2 DE 03/27/13 Emulsion 28 VC EPA Method 107 75014 Vinyl chloride 0.0899

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0048 Non-detect

Formosa S2 DE 03/27/13 Emulsion 28 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.006 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 Alcohol SW-846-8015C 67561 Methanol 5.73

Formosa S2 DE 04/01/13 Emulsion 29 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.501

Formosa S2 DE 04/01/13 Emulsion 29 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0868

Formosa S2 DE 04/01/13 Emulsion 29 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1.7 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 SVOC SW-846-8270D 98862 Acetophenone 0.029 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.059 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 SVOC SW-846-8270D 123319 Hydroquinone 0.5 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 SVOC SW-846-8270D 108952 Phenol 0.13 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0026 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0026 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0021 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VC EPA Method 107 75014 Vinyl chloride Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect

Formosa S2 DE 04/01/13 Emulsion 29 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 Alcohol SW-846-8015C 67561 Methanol 6.71

Formosa S2 DE 04/01/13 Emulsion 30 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.54

Formosa S2 DE 04/01/13 Emulsion 30 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0887

Formosa S2 DE 04/01/13 Emulsion 30 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1.7 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 SVOC SW-846-8270D 98862 Acetophenone 0.029 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.059 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 SVOC SW-846-8270D 123319 Hydroquinone 0.5 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 SVOC SW-846-8270D 108952 Phenol 0.13 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0026 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0026 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.0021 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VC EPA Method 107 75014 Vinyl chloride Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect

Formosa S2 DE 04/01/13 Emulsion 30 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 Alcohol SW-846-8015C 67561 Methanol 0.045 Non-detect U

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.149

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 Aldehyde SW-846-8315A 50000 Formaldehyde 0.238

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 SVOC SW-846-8270D 98862 Acetophenone 0.0642

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.001 J

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00021 Non-detect U

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 106990 1,3-butadiene 0.0019 Non-detect U

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00023 Non-detect U

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 71432 Benzene 0.00036 J

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 108907 Chlorobenzene 0.00023 Non-detect U

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 67663 Chloroform 0.0002 Non-detect U

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 126998 Chloroprene 0.00021 Non-detect U

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 98828 Cumene 0.00045 Non-detect U

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.407

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 100414 Ethylbenzene 0.00023 Non-detect U

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.114

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00049 J

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.908

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 75092 Methylene chloride 0.004

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 110543 n-Hexane 0.00046 Non-detect U

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 108883 Toluene 0.00023 Non-detect U

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00024 Non-detect U

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0011

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 108054 Vinyl acetate 0.0011 Non-detect U

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 593602 Vinyl bromide 0.00027 Non-detect U

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VC EPA Method 107 75014 Vinyl chloride 0.084

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00019 Non-detect U

PolyOne Henry IL 01/07/13 Suspension/Blending/Dispersion 1 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00024 Non-detect U

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 Alcohol SW-846-8015C 67561 Methanol 5.18

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.179

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 Aldehyde SW-846-8315A 50000 Formaldehyde 0.321

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 SVOC SW-846-8270D 98862 Acetophenone 0.21

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 U

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00021 Non-detect U

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 106990 1,3-butadiene 0.0019 Non-detect U

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00023 Non-detect U

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 71432 Benzene 0.00048 J

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 108907 Chlorobenzene 0.00023 Non-detect U

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 67663 Chloroform 0.0002 Non-detect U

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 126998 Chloroprene 0.00021 Non-detect U

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 98828 Cumene 0.00053 J

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 1.28

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 100414 Ethylbenzene 0.00023 Non-detect U

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.304

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0019

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 1.52

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 75092 Methylene chloride 0.0007 Non-detect U

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 110543 n-Hexane 0.00046 Non-detect U

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 108883 Toluene 0.00023 Non-detect U

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00024 U

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0015

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 108054 Vinyl acetate 0.0011 Non-detect U

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 593602 Vinyl bromide 0.00027 Non-detect U

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VC EPA Method 107 75014 Vinyl chloride 0.896

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00019 Non-detect U

PolyOne Henry IL 01/08/13 Suspension/Blending/Dispersion 2 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00024 Non-detect U

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 Alcohol SW-846-8015C 67561 Methanol 2

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.117

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 Aldehyde SW-846-8315A 50000 Formaldehyde 0.075

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 SVOC SW-846-8270D 98862 Acetophenone 0.0984

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00021 Non-detect U

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 106990 1,3-butadiene 0.0019 Non-detect U

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00023 Non-detect U

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 71432 Benzene 0.00037 J

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 108907 Chlorobenzene 0.00023 Non-detect U

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 67663 Chloroform 0.0002 Non-detect U

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 126998 Chloroprene 0.00021 Non-detect U

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 98828 Cumene 0.00045 Non-detect U

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.526

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 100414 Ethylbenzene 0.00023 Non-detect U

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.112

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0006 J

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 1.16

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 75092 Methylene chloride 0.0032

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 110543 n-Hexane 0.00049 J

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 108883 Toluene 0.00029 J

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00024 Non-detect U

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0013

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 108054 Vinyl acetate 0.0011 Non-detect U

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 593602 Vinyl bromide 0.00027 Non-detect U

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VC EPA Method 107 75014 Vinyl chloride 13.185

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00019 Non-detect U

PolyOne Henry IL 01/09/13 Suspension/Blending/Dispersion 3 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00024 Non-detect U

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 Alcohol SW-846-8015C 67561 Methanol 15.9

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.547

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 Aldehyde SW-846-8315A 50000 Formaldehyde 1.37

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 SVOC SW-846-8270D 98862 Acetophenone 0.802

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00021 Non-detect U

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 106990 1,3-butadiene 0.0019 Non-detect U

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00023 Non-detect U

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 71432 Benzene 0.0004 J

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 108907 Chlorobenzene 0.00023 Non-detect U

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 67663 Chloroform 0.0002 Non-detect U

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 126998 Chloroprene 0.00021 Non-detect U

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 98828 Cumene 0.00061 J

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.521

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 100414 Ethylbenzene 0.00023 Non-detect U

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.177

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00091 J

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.867

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 75092 Methylene chloride 0.0007 Non-detect U

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 110543 n-Hexane 0.00046 Non-detect U

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 108883 Toluene 0.00023 Non-detect U

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00024 Non-detect U

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0011

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 108054 Vinyl acetate 0.0011 Non-detect U

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 593602 Vinyl bromide 0.00027 Non-detect U

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VC EPA Method 107 75014 Vinyl chloride 7.601 0

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00019 Non-detect U

PolyOne Henry IL 01/10/13 Suspension/Blending/Dispersion 4 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00024 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 Alcohol SW-846-8015C 67561 Methanol 0.847

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.123

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0334

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 SVOC SW-846-8270D 98862 Acetophenone 0.0374

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 SVOC SW-846-8270D 108952 Phenol 0.0024 Non-detect

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0054 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 106990 1,3-butadiene 0.048 Non-detect U

12/12/2013 VI Confidential 156 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0056 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 71432 Benzene 0.0059 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 108907 Chlorobenzene 0.0057 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 67663 Chloroform 0.0051 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 126998 Chloroprene 0.0052 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 98828 Cumene 0.011 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.222

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 100414 Ethylbenzene 0.0057 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0679

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0027 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.425

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 75092 Methylene chloride 0.018 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 110543 n-Hexane 0.012 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 108883 Toluene 0.0057 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0059 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0072 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 108054 Vinyl acetate 0.028 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 593602 Vinyl bromide 0.0067 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VC EPA Method 107 75014 Vinyl chloride 6.841 0

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0048 Non-detect U

PolyOne Henry IL 01/11/13 Suspension/Blending/Dispersion 5 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.006 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 Alcohol SW-846-8015C 67561 Methanol 9.67

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.301

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0243

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 SVOC SW-846-8270D 98862 Acetophenone 0.985

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0011 J

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0054 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 106990 1,3-butadiene 0.048 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0056 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 71432 Benzene 0.0059 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 108907 Chlorobenzene 0.0057 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 67663 Chloroform 0.0051 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 126998 Chloroprene 0.0052 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 98828 Cumene 0.011 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0527

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 100414 Ethylbenzene 0.0057 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0723

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0027 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.226

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 75092 Methylene chloride 0.018 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 110543 n-Hexane 0.012 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 108883 Toluene 0.0057 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0059 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0072 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 108054 Vinyl acetate 0.028 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 593602 Vinyl bromide 0.0067 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VC EPA Method 107 75014 Vinyl chloride 6.793 0

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0048 Non-detect U

PolyOne Henry IL 01/15/13 Suspension/Blending/Dispersion 6 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.006 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 Alcohol SW-846-8015C 67561 Methanol 17.6

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.651

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 Aldehyde SW-846-8315A 50000 Formaldehyde 0.793

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 SVOC SW-846-8270D 98862 Acetophenone 1.01

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0054 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 106990 1,3-butadiene 0.048 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0056 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 71432 Benzene 0.0059 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 108907 Chlorobenzene 0.0057 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 67663 Chloroform 0.0051 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 126998 Chloroprene 0.0052 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 98828 Cumene 0.011 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 1.24

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 100414 Ethylbenzene 0.0057 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.549

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0027 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 1.34

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 75092 Methylene chloride 0.018 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 110543 n-Hexane 0.012 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 108883 Toluene 0.0057 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0059 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0072 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 108054 Vinyl acetate 0.028 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 593602 Vinyl bromide 0.0067 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VC EPA Method 107 75014 Vinyl chloride 7.205

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0048 Non-detect U

PolyOne Henry IL 01/16/13 Suspension/Blending/Dispersion 7 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.006 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 Alcohol SW-846-8015C 67561 Methanol 0.045 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.112

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0371

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 SVOC SW-846-8270D 98862 Acetophenone 0.0389

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0054 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 106990 1,3-butadiene 0.048 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0056 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 71432 Benzene 0.0059 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 108907 Chlorobenzene 0.0057 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 67663 Chloroform 0.0051 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 126998 Chloroprene 0.0052 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 98828 Cumene 0.011 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.33

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VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 100414 Ethylbenzene 0.0057 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.121

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0027 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.549

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 75092 Methylene chloride 0.018 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 110543 n-Hexane 0.012 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 108883 Toluene 0.0059 J

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0059 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0072 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 108054 Vinyl acetate 0.028 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 593602 Vinyl bromide 0.0067 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VC EPA Method 107 75014 Vinyl chloride 6.565

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0048 Non-detect U

PolyOne Henry IL 01/17/13 Suspension/Blending/Dispersion 8 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.006 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 Alcohol SW-846-8015C 67561 Methanol 6.11

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.193

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 Aldehyde SW-846-8315A 50000 Formaldehyde 0.021

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 SVOC SW-846-8270D 98862 Acetophenone 0.591

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0015 J

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0054 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 106990 1,3-butadiene 0.048 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0056 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 71432 Benzene 0.0059 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 108907 Chlorobenzene 0.0057 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 67663 Chloroform 0.0051 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 126998 Chloroprene 0.0052 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 98828 Cumene 0.011 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.268

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 100414 Ethylbenzene 0.0057 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.073

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0027 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.651

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 75092 Methylene chloride 0.018 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 110543 n-Hexane 0.012 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 108883 Toluene 0.0057 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0059 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0072 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 108054 Vinyl acetate 0.028 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 593602 Vinyl bromide 0.0067 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VC EPA Method 107 75014 Vinyl chloride 6.479

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0048 Non-detect U

PolyOne Henry IL 01/18/13 Suspension/Blending/Dispersion 9 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.006 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 Alcohol SW-846-8015C 67561 Methanol 1.85

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.33

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 Aldehyde SW-846-8315A 50000 Formaldehyde 0.155

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 SVOC SW-846-8270D 98862 Acetophenone 0.0252

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0054 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 106990 1,3-butadiene 0.048 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0056 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 71432 Benzene 0.0059 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 108907 Chlorobenzene 0.0057 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 67663 Chloroform 0.0051 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 126998 Chloroprene 0.0052 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 98828 Cumene 0.011 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.811

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 100414 Ethylbenzene 0.0057 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.415

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0027 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 1.13

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 75092 Methylene chloride 0.018 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 110543 n-Hexane 0.012 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 108883 Toluene 0.0057 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0059 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0072 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 108054 Vinyl acetate 0.028 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 593602 Vinyl bromide 0.0067 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VC EPA Method 107 75014 Vinyl chloride 4.861

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0048 Non-detect U

PolyOne Henry IL 01/21/13 Suspension/Blending/Dispersion 10 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.006 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 Alcohol SW-846-8015C 107211 Ethylene glycol 0.01 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 Alcohol SW-846-8015C 67561 Methanol 1.95

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.125

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0477

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 SVOC SW-846-8270D 98862 Acetophenone 0.0581

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0054 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 106990 1,3-butadiene 0.048 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0056 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 71432 Benzene 0.0059 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 108907 Chlorobenzene 0.0057 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 67663 Chloroform 0.0051 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 126998 Chloroprene 0.0052 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 98828 Cumene 0.011 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.478

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 100414 Ethylbenzene 0.0057 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.122

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0027 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.967

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 75092 Methylene chloride 0.018 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 110543 n-Hexane 0.012 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 108883 Toluene 0.0057 Non-detect U

12/12/2013 VI Confidential 158 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0059 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0072 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 108054 Vinyl acetate 0.028 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 593602 Vinyl bromide 0.0067 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VC EPA Method 107 75014 Vinyl chloride 7.447

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0048 Non-detect U

PolyOne Henry IL 01/22/13 Suspension/Blending/Dispersion 11 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.006 Non-detect U

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 Alcohol SW-846-8015C 67561 Methanol 4.36

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.116

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 Aldehyde SW-846-8315A 50000 Formaldehyde 0.059

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 SVOC SW-846-8270D 98862 Acetophenone 0.595

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 U

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00021 Non-detect U

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 106990 1,3-butadiene 0.0019 Non-detect U

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00023 Non-detect U

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 71432 Benzene 0.00086 J

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 108907 Chlorobenzene 0.00023 Non-detect U

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 67663 Chloroform 0.0002 Non-detect U

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 126998 Chloroprene 0.00021 Non-detect U

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 98828 Cumene 0.00095 J

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.242

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 100414 Ethylbenzene 0.00023 Non-detect U

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0969

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect U

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.565

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 75092 Methylene chloride 0.0007 Non-detect U

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 110543 n-Hexane 0.00046 Non-detect U

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 108883 Toluene 0.00023 Non-detect U

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00024 Non-detect U

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00082 J

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 108054 Vinyl acetate 0.0011 Non-detect U

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 593602 Vinyl bromide 0.00027 Non-detect U

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VC EPA Method 107 75014 Vinyl chloride 6.092

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00019 Non-detect U

PolyOne Henry IL 01/28/13 Suspension/Blending/Dispersion 12 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00024 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 Alcohol SW-846-8015C 67561 Methanol 5.03

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.856

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 Aldehyde SW-846-8315A 50000 Formaldehyde 0.583

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 SVOC SW-846-8270D 98862 Acetophenone 0.0142

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0042

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 1.69

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.423

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 1.77

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VC EPA Method 107 75014 Vinyl chloride 6.691

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect U

PolyOne Henry IL 02/04/13 Suspension/Blending/Dispersion 13 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 Alcohol SW-846-8015C 67561 Methanol 9.35

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.604

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 Aldehyde SW-846-8315A 50000 Formaldehyde 0.578

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 SVOC SW-846-8270D 98862 Acetophenone 0.38

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0015 J

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.675

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.184

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 1.01

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VC EPA Method 107 75014 Vinyl chloride 7.217

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect U

PolyOne Henry IL 02/05/13 Suspension/Blending/Dispersion 14 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect U

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 Alcohol SW-846-8015C 67561 Methanol 0.045 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.121

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 Aldehyde SW-846-8315A 50000 Formaldehyde 0.017 J

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 SVOC SW-846-8270D 98862 Acetophenone 0.0247

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.001 J

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.011 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 106990 1,3-butadiene 0.095 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.011 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 71432 Benzene 0.012 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 108907 Chlorobenzene 0.011 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 67663 Chloroform 0.01 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 126998 Chloroprene 0.01 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 98828 Cumene 0.022 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.322

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 100414 Ethylbenzene 0.011 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.121

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0053 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.633

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 75092 Methylene chloride 0.035 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 110543 n-Hexane 0.023 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 108883 Toluene 0.011 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.012 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.014 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 108054 Vinyl acetate 0.056 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 593602 Vinyl bromide 0.013 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VC EPA Method 107 75014 Vinyl chloride 7.831

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0096 Non-detect U

PolyOne Henry IL 02/06/13 Suspension/Blending/Dispersion 15 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.012 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 Alcohol SW-846-8015C 67561 Methanol 0.635

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.112

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0558

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 SVOC SW-846-8270D 98862 Acetophenone 0.04

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0043 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 106990 1,3-butadiene 0.038 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 71432 Benzene 0.0047 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 108907 Chlorobenzene 0.0046 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 67663 Chloroform 0.0041 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 98828 Cumene 0.0089 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.272

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 100414 Ethylbenzene 0.0046 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0962

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0021 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.547

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 75092 Methylene chloride 0.014 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 110543 n-Hexane 0.0093 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 108883 Toluene 0.0045 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0047 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0057 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 108054 Vinyl acetate 0.022 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 593602 Vinyl bromide 0.0054 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VC EPA Method 107 75014 Vinyl chloride 9.898

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0038 Non-detect U

PolyOne Henry IL 02/07/13 Suspension/Blending/Dispersion 16 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0048 Non-detect U

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 Alcohol SW-846-8015C 67561 Methanol 3.28

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.0422

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0068 J

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 SVOC SW-846-8270D 98862 Acetophenone 0.0418

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00021 Non-detect U

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 106990 1,3-butadiene 0.0019 Non-detect U

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00023 Non-detect U

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 71432 Benzene 0.00073 J

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 108907 Chlorobenzene 0.00023 Non-detect U

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 67663 Chloroform 0.0002 Non-detect U

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 126998 Chloroprene 0.00021 Non-detect U

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 98828 Cumene 0.00045 Non-detect U

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.619

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 100414 Ethylbenzene 0.00023 Non-detect U

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.184

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.001 Non-detect

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.946

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 75092 Methylene chloride 0.0007 Non-detect U

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 110543 n-Hexane 0.00046 Non-detect U

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 108883 Toluene 0.00023 Non-detect U

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00024 Non-detect U

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0009 Non-detect J

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 108054 Vinyl acetate 0.0011 Non-detect U

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 593602 Vinyl bromide 0.00027 Non-detect U

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VC EPA Method 107 75014 Vinyl chloride 8.662

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00019 Non-detect U

PolyOne Henry IL 02/08/13 Suspension/Blending/Dispersion 17 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00024 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 Alcohol SW-846-8015C 67561 Methanol 4.4

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.952

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 Aldehyde SW-846-8315A 50000 Formaldehyde 0.492

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 SVOC SW-846-8270D 98862 Acetophenone 0.0222

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

12/12/2013 VI Confidential 160 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 1.84

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.375

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 1.78

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VC EPA Method 107 75014 Vinyl chloride 8.586

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect U

PolyOne Henry IL 02/11/13 Suspension/Blending/Dispersion 18 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 Alcohol SW-846-8015C 67561 Methanol 7.14

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.217

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0216

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 SVOC SW-846-8270D 98862 Acetophenone 0.478

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.769

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0961

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 1.5

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VC EPA Method 107 75014 Vinyl chloride 6.533

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect U

PolyOne Henry IL 02/12/13 Suspension/Blending/Dispersion 19 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 Alcohol SW-846-8015C 67561 Methanol 3.79

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.314

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 Aldehyde SW-846-8315A 50000 Formaldehyde 0.294

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 SVOC SW-846-8270D 98862 Acetophenone 0.0703

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.797

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.225

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 1.24

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VC EPA Method 107 75014 Vinyl chloride 9.583

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect U

PolyOne Henry IL 02/13/13 Suspension/Blending/Dispersion 20 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 Alcohol SW-846-8015C 67561 Methanol 4.08

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.308

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 Aldehyde SW-846-8315A 50000 Formaldehyde 0.274

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 SVOC SW-846-8270D 98862 Acetophenone 0.021

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect U

12/12/2013 VI Confidential 161 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 1.06

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.302

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 1.3

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VC EPA Method 107 75014 Vinyl chloride 7.89

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect U

PolyOne Henry IL 02/14/13 Suspension/Blending/Dispersion 21 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 Alcohol SW-846-8015C 67561 Methanol 0.045 U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.0972

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0129 J

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 SVOC SW-846-8270D 98862 Acetophenone 0.0526

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.307

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.187

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.713

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VC EPA Method 107 75014 Vinyl chloride 8.818

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect U

PolyOne Henry IL 02/15/13 Suspension/Blending/Dispersion 22 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 Alcohol SW-846-8015C 67561 Methanol 9.07

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.163

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0221

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 SVOC SW-846-8270D 98862 Acetophenone 0.0644

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00021 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 106990 1,3-butadiene 0.0019 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00023 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 71432 Benzene 0.00059 J

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 108907 Chlorobenzene 0.00023 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 67663 Chloroform 0.0002 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 126998 Chloroprene 0.00021 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 98828 Cumene 0.00045 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.196

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 100414 Ethylbenzene 0.00023 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0753

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.575

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 75092 Methylene chloride 0.0007 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 110543 n-Hexane 0.00046 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 108883 Toluene 0.00023 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00024 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00068 J

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 108054 Vinyl acetate 0.0011 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 593602 Vinyl bromide 0.00027 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VC EPA Method 107 75014 Vinyl chloride 7.024

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00019 Non-detect U

PolyOne Henry IL 02/19/13 Suspension/Blending/Dispersion 23 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00024 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 Alcohol SW-846-8015C 67561 Methanol 25.2

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.607

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 Aldehyde SW-846-8315A 50000 Formaldehyde 0.912

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 SVOC SW-846-8270D 98862 Acetophenone 0.188

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.726

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.218

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect U

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PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.67

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VC EPA Method 107 75014 Vinyl chloride 5.658

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect U

PolyOne Henry IL 02/20/13 Suspension/Blending/Dispersion 24 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 Alcohol SW-846-8015C 67561 Methanol 12.2

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.138

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0904

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 SVOC SW-846-8270D 98862 Acetophenone 0.569

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0054 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 106990 1,3-butadiene 0.048 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0056 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 71432 Benzene 0.0059 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 108907 Chlorobenzene 0.0057 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 67663 Chloroform 0.0051 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 126998 Chloroprene 0.0052 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 98828 Cumene 0.011 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.67

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 100414 Ethylbenzene 0.0057 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.214

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0027 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.86

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 75092 Methylene chloride 0.018 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 110543 n-Hexane 0.012 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 108883 Toluene 0.0057 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0059 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0072 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 108054 Vinyl acetate 0.028 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 593602 Vinyl bromide 0.0067 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VC EPA Method 107 75014 Vinyl chloride 17.841

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0048 Non-detect U

PolyOne Henry IL 02/25/13 Suspension/Blending/Dispersion 25 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.006 Non-detect U

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 Alcohol SW-846-8015C 107211 Ethylene glycol 0.01 Non-detect U

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 Alcohol SW-846-8015C 67561 Methanol 3.2

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.208

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 Aldehyde SW-846-8315A 50000 Formaldehyde 0.211

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 SVOC SW-846-8270D 98862 Acetophenone 0.0609

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0012 J

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00021 Non-detect U

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 106990 1,3-butadiene 0.0019 Non-detect U

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00023 Non-detect U

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 71432 Benzene 0.00093 J

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 108907 Chlorobenzene 0.00023 Non-detect U

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 67663 Chloroform 0.0002 Non-detect U

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 126998 Chloroprene 0.00021 Non-detect U

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 98828 Cumene 0.00045 Non-detect U

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.638

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 100414 Ethylbenzene 0.00023 Non-detect U

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.377

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0012 Non-detect

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.766

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 75092 Methylene chloride 0.0007 Non-detect U

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 110543 n-Hexane 0.00046 Non-detect U

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 108883 Toluene 0.00023 Non-detect U

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00024 Non-detect U

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0015

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 108054 Vinyl acetate 0.0011 Non-detect U

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 593602 Vinyl bromide 0.00027 Non-detect U

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VC EPA Method 107 75014 Vinyl chloride 7.874

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00019 Non-detect U

PolyOne Henry IL 03/01/13 Suspension/Blending/Dispersion 26 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00024 Non-detect U

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 Alcohol SW-846-8015C 67561 Methanol 3.22

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.89

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 Aldehyde SW-846-8315A 50000 Formaldehyde 0.108

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 SVOC SW-846-8270D 98862 Acetophenone 0.0513

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0051

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect U

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect U

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect U

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect U

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect U

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect U

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect U

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 98828 Cumene 0.0076 J

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.488

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect U

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.245

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect U

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.648

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect U

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect U

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect U

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect U

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect U

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect U

12/12/2013 VI Confidential 163 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect U

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VC EPA Method 107 75014 Vinyl chloride 7.404

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect U

PolyOne Henry IL 03/04/13 Suspension/Blending/Dispersion 27 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect U

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 Alcohol SW-846-8015C 67561 Methanol 4.37

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.204

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 Aldehyde SW-846-8315A 50000 Formaldehyde 0.288

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 SVOC SW-846-8270D 98862 Acetophenone 0.0832

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0011 J

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00021 Non-detect U

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 106990 1,3-butadiene 0.0019 Non-detect U

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00023 Non-detect U

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 71432 Benzene 0.00098 J

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 108907 Chlorobenzene 0.00023 Non-detect U

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 67663 Chloroform 0.0002 Non-detect U

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 126998 Chloroprene 0.00021 Non-detect U

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 98828 Cumene 0.00045 U

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.666

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 100414 Ethylbenzene 0.00023 Non-detect U

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.338

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0012 Non-detect

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.714

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 75092 Methylene chloride 0.0007 Non-detect U

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 110543 n-Hexane 0.00046 Non-detect U

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 108883 Toluene 0.00023 Non-detect U

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00024 Non-detect U

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0015

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 108054 Vinyl acetate 0.0011 Non-detect U

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 593602 Vinyl bromide 0.00027 Non-detect U

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VC EPA Method 107 75014 Vinyl chloride 5.658

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00019 Non-detect U

PolyOne Henry IL 03/05/13 Suspension/Blending/Dispersion 28 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00024 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 Alcohol SW-846-8015C 67561 Methanol 2.38

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.163

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0878

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 SVOC SW-846-8270D 98862 Acetophenone 0.0349

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.457

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.179

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.606

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VC EPA Method 107 75014 Vinyl chloride 6.653

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect U

PolyOne Henry IL 03/06/13 Suspension/Blending/Dispersion 29 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 Alcohol SW-846-8015C 67561 Methanol 1.97

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 Aldehyde SW-846-8315A 75070 Acetaldehyde 0.209

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0108 J

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 SVOC SW-846-8270D 98862 Acetophenone 0.0865

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0014 J

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00021 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 106990 1,3-butadiene 0.0019 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00023 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 71432 Benzene 0.00055 J

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 108907 Chlorobenzene 0.00023 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 67663 Chloroform 0.0002 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 126998 Chloroprene 0.00021 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 98828 Cumene 0.00045 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.232

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 100414 Ethylbenzene 0.00023 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0857

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.646

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 75092 Methylene chloride 0.0007 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 110543 n-Hexane 0.00046 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 108883 Toluene 0.00023 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00024 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00029 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 108054 Vinyl acetate 0.0011 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 593602 Vinyl bromide 0.00027 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VC EPA Method 107 75014 Vinyl chloride 7.069

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00019 Non-detect U

PolyOne Henry IL 03/07/13 Suspension/Blending/Dispersion 30 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00024 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 Alcohol SW-846-8015C 67561 Methanol 75.2

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.53

12/12/2013 VI Confidential 164 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0755

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.17 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 SVOC SW-846-8270D 98862 Acetophenone 2.69

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0059 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 SVOC SW-846-8270D 123319 Hydroquinone 0.05 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 SVOC SW-846-8270D 108952 Phenol 0.013 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.4

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0158

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.869

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VC EPA Method 107 75014 Vinyl chloride 3.818

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect U

PolyOne Pedricktown NJ 01/07/13 Suspension/Dispersion1 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 Alcohol SW-846-8015C 67561 Methanol 55

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 Aldehyde SW-846-8315A 75070 Acetaldehyde 8.77

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 Aldehyde SW-846-8315A 50000 Formaldehyde 0.241

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 SVOC SW-846-8270D 51285 2,4-dinitrophenol 17 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 SVOC SW-846-8270D 98862 Acetophenone 3.52

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.59 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 SVOC SW-846-8270D 123319 Hydroquinone 5 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 SVOC SW-846-8270D 108952 Phenol 1.3 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.252

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0139

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.777

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VC EPA Method 107 75014 Vinyl chloride 4.082

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect U

PolyOne Pedricktown NJ 01/08/13 Suspension/Dispersion2 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 Alcohol SW-846-8015C 67561 Methanol 37.4

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.1

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0619

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.17 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 SVOC SW-846-8270D 98862 Acetophenone 0.966

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0059 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 SVOC SW-846-8270D 123319 Hydroquinone 0.05 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 SVOC SW-846-8270D 108952 Phenol 0.013 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.011 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 106990 1,3-butadiene 0.095 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.011 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 71432 Benzene 0.012 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 108907 Chlorobenzene 0.011 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 67663 Chloroform 0.01 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 126998 Chloroprene 0.01 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 98828 Cumene 0.022 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 1.39

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 100414 Ethylbenzene 0.011 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0499 J

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0053 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 4.92

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 75092 Methylene chloride 0.035 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 110543 n-Hexane 0.023 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 108883 Toluene 0.011 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.012 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.014 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 108054 Vinyl acetate 0.056 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 593602 Vinyl bromide 0.013 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VC EPA Method 107 75014 Vinyl chloride 9.281

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0096 Non-detect U

PolyOne Pedricktown NJ 01/09/13 Suspension/Dispersion3 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.012 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 Alcohol SW-846-8015C 67561 Methanol 46.4

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.04

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 Aldehyde SW-846-8315A 50000 Formaldehyde 0.361

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.17 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 SVOC SW-846-8270D 98862 Acetophenone 1.39

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0059 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 SVOC SW-846-8270D 123319 Hydroquinone 0.05 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 SVOC SW-846-8270D 108952 Phenol 0.013 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect U

12/12/2013 VI Confidential 165 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.208

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0087 J

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.694

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VC EPA Method 107 75014 Vinyl chloride 4.477

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect U

PolyOne Pedricktown NJ 01/10/13 Suspension/Dispersion4 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 Alcohol SW-846-8015C 67561 Methanol 39.5

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.3

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0669

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1.7 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 SVOC SW-846-8270D 98862 Acetophenone 1.57

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.059 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 SVOC SW-846-8270D 123319 Hydroquinone 0.5 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 SVOC SW-846-8270D 108952 Phenol 0.13 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.148

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0102

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.433

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VC EPA Method 107 75014 Vinyl chloride 0.019

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect U

PolyOne Pedricktown NJ 01/11/13 Suspension/Dispersion5 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 Alcohol SW-846-8015C 67561 Methanol 20.4

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.23

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 Aldehyde SW-846-8315A 50000 Formaldehyde 0.158

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1.7 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 SVOC SW-846-8270D 98862 Acetophenone 1.24

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.059 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 SVOC SW-846-8270D 123319 Hydroquinone 0.5 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 SVOC SW-846-8270D 108952 Phenol 0.13 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0043 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 106990 1,3-butadiene 0.038 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 71432 Benzene 0.0047 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 108907 Chlorobenzene 0.0046 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 67663 Chloroform 0.0041 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 98828 Cumene 0.0089 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.361

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 100414 Ethylbenzene 0.0046 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0302

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0021 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 1.11

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 75092 Methylene chloride 0.014 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 110543 n-Hexane 0.0093 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 108883 Toluene 0.0045 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0047 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0057 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 108054 Vinyl acetate 0.022 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 593602 Vinyl bromide 0.0054 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VC EPA Method 107 75014 Vinyl chloride 5.766

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0038 Non-detect U

PolyOne Pedricktown NJ 01/14/13 Suspension/Dispersion6 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0048 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 Alcohol SW-846-8015C 67561 Methanol 29.1

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 Aldehyde SW-846-8315A 75070 Acetaldehyde 8.64

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 Aldehyde SW-846-8315A 50000 Formaldehyde 0.217

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1.7 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 SVOC SW-846-8270D 98862 Acetophenone 0.683

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.059 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 SVOC SW-846-8270D 123319 Hydroquinone 0.5 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 SVOC SW-846-8270D 108952 Phenol 0.13 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect U

12/12/2013 VI Confidential 166 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.159

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0086

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.579

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VC EPA Method 107 75014 Vinyl chloride 2.405

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect U

PolyOne Pedricktown NJ 01/15/13 Suspension/Dispersion7 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 Alcohol SW-846-8015C 67561 Methanol 24.9

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 Aldehyde SW-846-8315A 75070 Acetaldehyde 8.29

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 Aldehyde SW-846-8315A 50000 Formaldehyde 0.556

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1.7 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 SVOC SW-846-8270D 98862 Acetophenone 0.291

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.059 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 SVOC SW-846-8270D 123319 Hydroquinone 0.5 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 SVOC SW-846-8270D 108952 Phenol 0.13 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.186

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0107

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.605

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VC EPA Method 107 75014 Vinyl chloride 3.758

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect U

PolyOne Pedricktown NJ 01/16/13 Suspension/Dispersion8 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 Alcohol SW-846-8015C 67561 Methanol 22.8

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 Aldehyde SW-846-8315A 75070 Acetaldehyde 8.5

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 Aldehyde SW-846-8315A 50000 Formaldehyde 0.31

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 SVOC SW-846-8270D 51285 2,4-dinitrophenol 1.7 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 SVOC SW-846-8270D 98862 Acetophenone 0.18 J

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.059 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 SVOC SW-846-8270D 123319 Hydroquinone 0.5 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 SVOC SW-846-8270D 108952 Phenol 0.13 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.235

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0129

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.727

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VC EPA Method 107 75014 Vinyl chloride 3.009

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect U

PolyOne Pedricktown NJ 01/17/13 Suspension/Dispersion9 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 Alcohol SW-846-8015C 67561 Methanol 27.5

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.03

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 Aldehyde SW-846-8315A 50000 Formaldehyde 0.254

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 SVOC SW-846-8270D 98862 Acetophenone 0.0652

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0769

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0058

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.268

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect U

12/12/2013 VI Confidential 167 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VC EPA Method 107 75014 Vinyl chloride 2.224

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect U

PolyOne Pedricktown NJ 1/XX/2013 Suspension/Dispersion10 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 Alcohol SW-846-8015C 67561 Methanol 56.6

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.14

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 Aldehyde SW-846-8315A 50000 Formaldehyde 0.214

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 SVOC SW-846-8270D 98862 Acetophenone 0.54

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.23

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0119

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.712

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VC EPA Method 107 75014 Vinyl chloride 1.837

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect U

PolyOne Pedricktown NJ 01/20/13 Suspension/Dispersion12 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 Alcohol SW-846-8015C 67561 Methanol 3.49

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.93

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 Aldehyde SW-846-8315A 50000 Formaldehyde 0.455

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 SVOC SW-846-8270D 98862 Acetophenone 0.687

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 SVOC SW-846-8270D 108952 Phenol 0.0022

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.288

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0139

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.928

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VC EPA Method 107 75014 Vinyl chloride 6.352

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect U

PolyOne Pedricktown NJ 01/22/13 Suspension/Dispersion13 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 Alcohol SW-846-8015C 67561 Methanol 18.2

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.45

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 Aldehyde SW-846-8315A 50000 Formaldehyde 0.228

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 SVOC SW-846-8270D 98862 Acetophenone 0.899

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0054 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 106990 1,3-butadiene 0.048 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0056 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 71432 Benzene 0.0059 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 108907 Chlorobenzene 0.0057 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 67663 Chloroform 0.0051 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 126998 Chloroprene 0.0052 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 98828 Cumene 0.011 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.477

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 100414 Ethylbenzene 0.0057 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0268

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0027 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 1.62

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 75092 Methylene chloride 0.018 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 110543 n-Hexane 0.012 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 108883 Toluene 0.0057 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0059 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0072 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 108054 Vinyl acetate 0.028 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 593602 Vinyl bromide 0.0067 Non-detect U

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VC EPA Method 107 75014 Vinyl chloride 3.206

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0048 Non-detect U

12/12/2013 VI Confidential 168 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

PolyOne Pedricktown NJ 01/23/13 Suspension/Dispersion14 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.006 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 Alcohol SW-846-8015C 67561 Methanol 25

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.22

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 Aldehyde SW-846-8315A 50000 Formaldehyde 0.321

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.17 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 SVOC SW-846-8270D 98862 Acetophenone 2.38

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0059 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 SVOC SW-846-8270D 123319 Hydroquinone 0.05 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 SVOC SW-846-8270D 108952 Phenol 0.013 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.168

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0088 J

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.652

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VC EPA Method 107 75014 Vinyl chloride 3.436

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect U

PolyOne Pedricktown NJ 02/04/13 Suspension/Dispersion15 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 Alcohol SW-846-8015C 67561 Methanol 17.5

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.77

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 Aldehyde SW-846-8315A 50000 Formaldehyde 0.432

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 SVOC SW-846-8270D 98862 Acetophenone 0.731

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.215

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.012

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.712

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VC EPA Method 107 75014 Vinyl chloride 5.026

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect U

PolyOne Pedricktown NJ 02/05/13 Suspension/Dispersion16 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 Alcohol SW-846-8015C 67561 Methanol 22.8

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.98

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 Aldehyde SW-846-8315A 50000 Formaldehyde 0.106

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 SVOC SW-846-8270D 98862 Acetophenone 0.479

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.234

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0136

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.863

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VC EPA Method 107 75014 Vinyl chloride 1.917

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect U

PolyOne Pedricktown NJ 02/06/13 Suspension/Dispersion17 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 Alcohol SW-846-8015C 67561 Methanol 30.5

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.93

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 Aldehyde SW-846-8315A 50000 Formaldehyde 0.171

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.083 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 SVOC SW-846-8270D 98862 Acetophenone 0.305 0

12/12/2013 VI Confidential 169 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0029 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 SVOC SW-846-8270D 123319 Hydroquinone 0.0025 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 SVOC SW-846-8270D 108952 Phenol 0.0064 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.011 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 106990 1,3-butadiene 0.095 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.011 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 71432 Benzene 0.012 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 108907 Chlorobenzene 0.011 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 67663 Chloroform 0.01 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 126998 Chloroprene 0.01 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 98828 Cumene 0.022 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.426

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 100414 Ethylbenzene 0.011 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0167 J

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0053 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 1.4

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 75092 Methylene chloride 0.035 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 110543 n-Hexane 0.023 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 108883 Toluene 0.011 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.012 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.014 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 108054 Vinyl acetate 0.056 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 593602 Vinyl bromide 0.013 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VC EPA Method 107 75014 Vinyl chloride 9.631

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0096 Non-detect U

PolyOne Pedricktown NJ 02/07/13 Suspension/Dispersion18 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.012 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 Alcohol SW-846-8015C 67561 Methanol 46.9

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.33

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 Aldehyde SW-846-8315A 50000 Formaldehyde 0.212

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 SVOC SW-846-8270D 98862 Acetophenone 0.395

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00021 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 106990 1,3-butadiene 0.0019 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00023 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 71432 Benzene 0.00024 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 108907 Chlorobenzene 0.00023 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 67663 Chloroform 0.0002 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 126998 Chloroprene 0.00021 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 98828 Cumene 0.00045 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.103

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 100414 Ethylbenzene 0.00023 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0151

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00011 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.296

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 75092 Methylene chloride 0.0007 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 110543 n-Hexane 0.00046 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 108883 Toluene 0.00023 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00024 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.00029 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 108054 Vinyl acetate 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 593602 Vinyl bromide 0.00027 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VC EPA Method 107 75014 Vinyl chloride 3.943

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00019 Non-detect U

PolyOne Pedricktown NJ 02/08/13 Suspension/Dispersion19 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00024 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 Alcohol SW-846-8015C 67561 Methanol 26.4

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 Aldehyde SW-846-8315A 75070 Acetaldehyde 6.22

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 Aldehyde SW-846-8315A 50000 Formaldehyde 0.217

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.17 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 SVOC SW-846-8270D 98862 Acetophenone 0.795

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0059 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 SVOC SW-846-8270D 123319 Hydroquinone 0.05 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 SVOC SW-846-8270D 108952 Phenol 0.013 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.235

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0149

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.922

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VC EPA Method 107 75014 Vinyl chloride 4.58

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect U

PolyOne Pedricktown NJ 02/11/13 Suspension/Dispersion20 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 Alcohol SW-846-8015C 67561 Methanol 16.1

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.22

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 Aldehyde SW-846-8315A 50000 Formaldehyde 0.193

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.17 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 SVOC SW-846-8270D 98862 Acetophenone 0.808

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0059 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 SVOC SW-846-8270D 123319 Hydroquinone 0.05 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 SVOC SW-846-8270D 108952 Phenol 0.013 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect U

12/12/2013 VI Confidential 170 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.21

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0148

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.825

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VC EPA Method 107 75014 Vinyl chloride 4.23

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect U

PolyOne Pedricktown NJ 02/12/13 Suspension/Dispersion22 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 Alcohol SW-846-8015C 67561 Methanol 19.6

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.49

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 Aldehyde SW-846-8315A 50000 Formaldehyde 0.14

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.083 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 SVOC SW-846-8270D 98862 Acetophenone 0.376

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0029 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 SVOC SW-846-8270D 123319 Hydroquinone 0.025 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 SVOC SW-846-8270D 108952 Phenol 0.0064 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.163

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0075

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.535

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VC EPA Method 107 75014 Vinyl chloride 2.86

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect U

PolyOne Pedricktown NJ 02/13/13 Suspension/Dispersion23 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 Alcohol SW-846-8015C 67561 Methanol 14.4

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.19

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 Aldehyde SW-846-8315A 50000 Formaldehyde 0.122

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 SVOC SW-846-8270D 98862 Acetophenone 0.584

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.126

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0129

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.425

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VC EPA Method 107 75014 Vinyl chloride 2.78

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect U

PolyOne Pedricktown NJ 02/14/13 Suspension/Dispersion24 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 Alcohol SW-846-8015C 67561 Methanol 17

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 Aldehyde SW-846-8315A 75070 Acetaldehyde 5.13

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0386

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 SVOC SW-846-8270D 98862 Acetophenone 2.45

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.13

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0174

12/12/2013 VI Confidential 171 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.344

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VC EPA Method 107 75014 Vinyl chloride 2.73

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect U

PolyOne Pedricktown NJ 02/28/13 Suspension/Dispersion25 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 Alcohol SW-846-8015C 67561 Methanol 31.8

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.28

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 Aldehyde SW-846-8315A 50000 Formaldehyde 0.102 J

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 SVOC SW-846-8270D 98862 Acetophenone 1.11

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0011 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 106990 1,3-butadiene 0.0095 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0011 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 71432 Benzene 0.0012 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 108907 Chlorobenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 67663 Chloroform 0.001 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 126998 Chloroprene 0.001 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 98828 Cumene 0.0022 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.693

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 100414 Ethylbenzene 0.0011 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0393

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.00053 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 3.41

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 75092 Methylene chloride 0.0035 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 110543 n-Hexane 0.0023 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 108883 Toluene 0.0011 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0012 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0014 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 108054 Vinyl acetate 0.0056 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 593602 Vinyl bromide 0.0013 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VC EPA Method 107 75014 Vinyl chloride 8.56

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00096 Non-detect U

PolyOne Pedricktown NJ 03/04/13 Suspension/Dispersion27 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0012 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 Alcohol SW-846-8015C 67561 Methanol 13.4

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.6

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 Aldehyde SW-846-8315A 50000 Formaldehyde 0.0875

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 SVOC SW-846-8270D 98862 Acetophenone 1.02

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 SVOC SW-846-8270D 108952 Phenol 0.0013 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0043 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 106990 1,3-butadiene 0.038 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0045 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 71432 Benzene 0.0047 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 108907 Chlorobenzene 0.0046 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 67663 Chloroform 0.0041 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 126998 Chloroprene 0.0042 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 98828 Cumene 0.0089 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.868

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 100414 Ethylbenzene 0.0046 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0508

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0021 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 3.29

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 75092 Methylene chloride 0.014 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 110543 n-Hexane 0.0093 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 108883 Toluene 0.0045 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0047 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0057 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 108054 Vinyl acetate 0.022 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 593602 Vinyl bromide 0.0054 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VC EPA Method 107 75014 Vinyl chloride 8.41

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0038 Non-detect U

PolyOne Pedricktown NJ 03/05/13 Suspension/Dispersion28 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0048 Non-detect U

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 Alcohol SW-846-8015C 67561 Methanol 7.78

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 Aldehyde SW-846-8315A 75070 Acetaldehyde 7.72

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 Aldehyde SW-846-8315A 50000 Formaldehyde 0.447

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 SVOC SW-846-8270D 98862 Acetophenone 3.2

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 SVOC SW-846-8270D 108952 Phenol 0.0027 Non-detect

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.00021 Non-detect U

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 106990 1,3-butadiene 0.0019 Non-detect U

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.00023 Non-detect U

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 71432 Benzene 0.00024 Non-detect U

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 108907 Chlorobenzene 0.00023 Non-detect U

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 67663 Chloroform 0.0002 Non-detect U

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 126998 Chloroprene 0.00021 Non-detect U

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 98828 Cumene 0.0013 Non-detect J

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.151

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 100414 Ethylbenzene 0.00023 Non-detect U

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0606

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0013 Non-detect

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.32

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 75092 Methylene chloride 0.0007 Non-detect U

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 110543 n-Hexane 0.00046 Non-detect U

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 108883 Toluene 0.00023 Non-detect U

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.00024 Non-detect U

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0018 Non-detect

12/12/2013 VI Confidential 172 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 108054 Vinyl acetate 0.0011 Non-detect U

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 593602 Vinyl bromide 0.00027 Non-detect U

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VC EPA Method 107 75014 Vinyl chloride 5.27

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.00019 Non-detect U

PolyOne Pedricktown NJ 03/06/13 Suspension/Dispersion29 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.00024 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 Alcohol SW-846-8015C 67561 Methanol 7.33

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 Aldehyde SW-846-8315A 75070 Acetaldehyde 4.56

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 Aldehyde SW-846-8315A 50000 Formaldehyde 0.128

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.083 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 SVOC SW-846-8270D 98862 Acetophenone 1.19

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.0029 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 SVOC SW-846-8270D 123319 Hydroquinone 0.025 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 SVOC SW-846-8270D 108952 Phenol 0.0064 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0635

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.005 J

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.186

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VC EPA Method 107 75014 Vinyl chloride 1.74

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect U

PolyOne Pedricktown NJ 03/08/13 Suspension/Dispersion30 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 Alcohol SW-846-8015C 67561 Methanol 44

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 Aldehyde SW-846-8315A 75070 Acetaldehyde 3.9

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 Aldehyde SW-846-8315A 50000 Formaldehyde 0.112

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 SVOC SW-846-8270D 98862 Acetophenone 0.497

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 SVOC SW-846-8270D 108952 Phenol 0.0022

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.0821

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.0088 J

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.182

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VC EPA Method 107 75014 Vinyl chloride 1.15

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect U

PolyOne Pedricktown NJ 03/12/13 Suspension/Dispersion31 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 Alcohol SW-846-8015C 67561 Methanol 50.9

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.88

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 Aldehyde SW-846-8315A 50000 Formaldehyde 0.2

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 SVOC SW-846-8270D 98862 Acetophenone 1.18

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 SVOC SW-846-8270D 108952 Phenol 0.0032

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.178

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.01 J

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.394

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VC EPA Method 107 75014 Vinyl chloride 2.09

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect U

PolyOne Pedricktown NJ 03/18/13 Suspension/Dispersion32 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 Alcohol SW-846-8015C 107211 Ethylene glycol 10 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 Alcohol SW-846-8015C 67561 Methanol 50.9

12/12/2013 VI Confidential 173 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 Aldehyde SW-846-8315A 75070 Acetaldehyde 2.88

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 Aldehyde SW-846-8315A 50000 Formaldehyde 0.2

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 SVOC SW-846-8270D 51285 2,4-dinitrophenol 0.017 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 SVOC SW-846-8270D 98862 Acetophenone 1.18

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP) 0.00059 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 SVOC SW-846-8270D 123319 Hydroquinone 0.005 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 SVOC SW-846-8270D 108952 Phenol 0.0032 Non-detect

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane 0.0021 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 106990 1,3-butadiene 0.019 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 540841 2,2,4-trimethylpentane 0.0023 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 71432 Benzene 0.0024 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 108907 Chlorobenzene 0.0023 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 67663 Chloroform 0.002 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 126998 Chloroprene 0.0021 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 98828 Cumene 0.0045 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.178

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 100414 Ethylbenzene 0.0023 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane) 0.01 J

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane) 0.0011 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.394

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 75092 Methylene chloride 0.007 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 110543 n-Hexane 0.0046 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 108883 Toluene 0.0023 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.0024 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.0029 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 108054 Vinyl acetate 0.011 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 593602 Vinyl bromide 0.0027 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VC EPA Method 107 75014 Vinyl chloride 2.09

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.0019 Non-detect U

PolyOne Pedricktown NJ 03/19/13 Suspension/Dispersion33 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures) 0.0024 Non-detect U

Dow Midland MI 02/05/13 Suspension Copolymer 1 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 02/05/13 Suspension Copolymer 1 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 02/05/13 Suspension Copolymer 1 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 02/05/13 Suspension Copolymer 1 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 02/05/13 Suspension Copolymer 1 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 02/05/13 Suspension Copolymer 1 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 02/05/13 Suspension Copolymer 1 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 02/05/13 Suspension Copolymer 1 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 02/05/13 Suspension Copolymer 1 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 02/05/13 Suspension Copolymer 1 VC Dow Method 107 75014 Vinyl chloride Detection Limit Not Reported Non-Detect VI Note (11)

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) Detection Limit Not Reported Non-Detect VI Note (11)

Dow Midland MI 02/05/13 Suspension Copolymer 1 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 02/06/13 Suspension Copolymer 2 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 02/06/13 Suspension Copolymer 2 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 02/06/13 Suspension Copolymer 2 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 02/06/13 Suspension Copolymer 2 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 02/06/13 Suspension Copolymer 2 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 02/06/13 Suspension Copolymer 2 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 02/06/13 Suspension Copolymer 2 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 02/06/13 Suspension Copolymer 2 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 02/06/13 Suspension Copolymer 2 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 02/06/13 Suspension Copolymer 2 VC Dow Method 107 75014 Vinyl chloride Detection Limit Not Reported Non-Detect VI Note (11)

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) Detection Limit Not Reported Non-Detect VI Note (11)

Dow Midland MI 02/06/13 Suspension Copolymer 2 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 02/08/13 Suspension Copolymer 3 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 02/08/13 Suspension Copolymer 3 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 02/08/13 Suspension Copolymer 3 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 02/08/13 Suspension Copolymer 3 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 02/08/13 Suspension Copolymer 3 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 02/08/13 Suspension Copolymer 3 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 02/08/13 Suspension Copolymer 3 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 02/08/13 Suspension Copolymer 3 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 02/08/13 Suspension Copolymer 3 SVOC SW-846-8270D 108952 Phenol

12/12/2013 VI Confidential 174 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 02/08/13 Suspension Copolymer 3 VC Dow Method 107 75014 Vinyl chloride 0.89

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 3.67 VI Note (12)

Dow Midland MI 02/08/13 Suspension Copolymer 3 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 02/11/13 Suspension Copolymer 4 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 02/11/13 Suspension Copolymer 4 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 02/11/13 Suspension Copolymer 4 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 02/11/13 Suspension Copolymer 4 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 02/11/13 Suspension Copolymer 4 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 02/11/13 Suspension Copolymer 4 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 02/11/13 Suspension Copolymer 4 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 02/11/13 Suspension Copolymer 4 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 02/11/13 Suspension Copolymer 4 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 02/11/13 Suspension Copolymer 4 VC Dow Method 107 75014 Vinyl chloride 1.17

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 1.53 VI Note (12)

Dow Midland MI 02/11/13 Suspension Copolymer 4 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 02/12/13 Suspension Copolymer 5 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 02/12/13 Suspension Copolymer 5 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 02/12/13 Suspension Copolymer 5 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 02/12/13 Suspension Copolymer 5 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 02/12/13 Suspension Copolymer 5 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 02/12/13 Suspension Copolymer 5 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 02/12/13 Suspension Copolymer 5 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 02/12/13 Suspension Copolymer 5 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 02/12/13 Suspension Copolymer 5 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 02/12/13 Suspension Copolymer 5 VC Dow Method 107 75014 Vinyl chloride 0.785

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 2.615 VI Note (12)

Dow Midland MI 02/12/13 Suspension Copolymer 5 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 02/13/13 Suspension Copolymer 6 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 02/13/13 Suspension Copolymer 6 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 02/13/13 Suspension Copolymer 6 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 02/13/13 Suspension Copolymer 6 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 02/13/13 Suspension Copolymer 6 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 02/13/13 Suspension Copolymer 6 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 02/13/13 Suspension Copolymer 6 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 02/13/13 Suspension Copolymer 6 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 02/13/13 Suspension Copolymer 6 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC SW-846-8260B 126998 Chloroprene

12/12/2013 VI Confidential 175 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 02/13/13 Suspension Copolymer 6 VC Dow Method 107 75014 Vinyl chloride 1.75

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 2.32 VI Note (12)

Dow Midland MI 02/13/13 Suspension Copolymer 6 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 02/15/13 Suspension Copolymer 7 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 02/15/13 Suspension Copolymer 7 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 02/15/13 Suspension Copolymer 7 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 02/15/13 Suspension Copolymer 7 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 02/15/13 Suspension Copolymer 7 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 02/15/13 Suspension Copolymer 7 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 02/15/13 Suspension Copolymer 7 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 02/15/13 Suspension Copolymer 7 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 02/15/13 Suspension Copolymer 7 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 02/15/13 Suspension Copolymer 7 VC Dow Method 107 75014 Vinyl chloride 0.44

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.865 VI Note (12)

Dow Midland MI 02/15/13 Suspension Copolymer 7 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 02/16/13 Suspension Copolymer 8 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 02/16/13 Suspension Copolymer 8 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 02/16/13 Suspension Copolymer 8 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 02/16/13 Suspension Copolymer 8 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 02/16/13 Suspension Copolymer 8 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 02/16/13 Suspension Copolymer 8 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 02/16/13 Suspension Copolymer 8 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 02/16/13 Suspension Copolymer 8 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 02/16/13 Suspension Copolymer 8 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 02/16/13 Suspension Copolymer 8 VC Dow Method 107 75014 Vinyl chloride Detection Limit Not Reported Non-Detect VI Note (11)

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) Detection Limit Not Reported Non-Detect VI Note (11)

Dow Midland MI 02/16/13 Suspension Copolymer 8 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 02/18/13 Suspension Copolymer 9 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 02/18/13 Suspension Copolymer 9 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 02/18/13 Suspension Copolymer 9 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 02/18/13 Suspension Copolymer 9 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 02/18/13 Suspension Copolymer 9 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 02/18/13 Suspension Copolymer 9 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 02/18/13 Suspension Copolymer 9 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 02/18/13 Suspension Copolymer 9 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 02/18/13 Suspension Copolymer 9 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC SW-846-8260B 75092 Methylene chloride

12/12/2013 VI Confidential 176 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 02/18/13 Suspension Copolymer 9 VC Dow Method 107 75014 Vinyl chloride Detection Limit Not Reported Non-Detect VI Note (11)

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.785 VI Note (12)

Dow Midland MI 02/18/13 Suspension Copolymer 9 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 02/19/13 Suspension Copolymer 10 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 02/19/13 Suspension Copolymer 10 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 02/19/13 Suspension Copolymer 10 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 02/19/13 Suspension Copolymer 10 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 02/19/13 Suspension Copolymer 10 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 02/19/13 Suspension Copolymer 10 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 02/19/13 Suspension Copolymer 10 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 02/19/13 Suspension Copolymer 10 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 02/19/13 Suspension Copolymer 10 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 02/19/13 Suspension Copolymer 10 VC Dow Method 107 75014 Vinyl chloride 1.095

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 1.155 VI Note (12)

Dow Midland MI 02/19/13 Suspension Copolymer 10 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 02/21/13 Suspension Copolymer 11 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 02/21/13 Suspension Copolymer 11 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 02/21/13 Suspension Copolymer 11 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 02/21/13 Suspension Copolymer 11 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 02/21/13 Suspension Copolymer 11 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 02/21/13 Suspension Copolymer 11 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 02/21/13 Suspension Copolymer 11 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 02/21/13 Suspension Copolymer 11 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 02/21/13 Suspension Copolymer 11 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 02/21/13 Suspension Copolymer 11 VC Dow Method 107 75014 Vinyl chloride 0.27

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 1.545 VI Note (12)

Dow Midland MI 02/21/13 Suspension Copolymer 11 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 02/22/13 Suspension Copolymer 12 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 02/22/13 Suspension Copolymer 12 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 02/22/13 Suspension Copolymer 12 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 02/22/13 Suspension Copolymer 12 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 02/22/13 Suspension Copolymer 12 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 02/22/13 Suspension Copolymer 12 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 02/22/13 Suspension Copolymer 12 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 02/22/13 Suspension Copolymer 12 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 02/22/13 Suspension Copolymer 12 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 02/22/13 Suspension Copolymer 12 VC Dow Method 107 75014 Vinyl chloride 0.34

12/12/2013 VI Confidential 177 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 2.01 VI Note (12)

Dow Midland MI 02/22/13 Suspension Copolymer 12 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 02/23/13 Suspension Copolymer 13 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 02/23/13 Suspension Copolymer 13 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 02/23/13 Suspension Copolymer 13 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 02/23/13 Suspension Copolymer 13 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 02/23/13 Suspension Copolymer 13 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 02/23/13 Suspension Copolymer 13 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 02/23/13 Suspension Copolymer 13 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 02/23/13 Suspension Copolymer 13 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 02/23/13 Suspension Copolymer 13 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 02/23/13 Suspension Copolymer 13 VC Dow Method 107 75014 Vinyl chloride 0.885

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 2.16 VI Note (12)

Dow Midland MI 02/23/13 Suspension Copolymer 13 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 02/26/13 Suspension Copolymer 14 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 02/26/13 Suspension Copolymer 14 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 02/26/13 Suspension Copolymer 14 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 02/26/13 Suspension Copolymer 14 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 02/26/13 Suspension Copolymer 14 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 02/26/13 Suspension Copolymer 14 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 02/26/13 Suspension Copolymer 14 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 02/26/13 Suspension Copolymer 14 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 02/26/13 Suspension Copolymer 14 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 02/26/13 Suspension Copolymer 14 VC Dow Method 107 75014 Vinyl chloride 0.995

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 2 VI Note (12)

Dow Midland MI 02/26/13 Suspension Copolymer 14 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 02/27/13 Suspension Copolymer 15 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 02/27/13 Suspension Copolymer 15 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 02/27/13 Suspension Copolymer 15 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 02/27/13 Suspension Copolymer 15 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 02/27/13 Suspension Copolymer 15 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 02/27/13 Suspension Copolymer 15 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 02/27/13 Suspension Copolymer 15 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 02/27/13 Suspension Copolymer 15 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 02/27/13 Suspension Copolymer 15 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 02/27/13 Suspension Copolymer 15 VC Dow Method 107 75014 Vinyl chloride 0.415

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 2.555 VI Note (12)

Dow Midland MI 02/27/13 Suspension Copolymer 15 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 03/01/13 Suspension Copolymer 16 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 03/01/13 Suspension Copolymer 16 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 03/01/13 Suspension Copolymer 16 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 03/01/13 Suspension Copolymer 16 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 03/01/13 Suspension Copolymer 16 SVOC SW-846-8270D 51285 2,4-dinitrophenol

12/12/2013 VI Confidential 178 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Dow Midland MI 03/01/13 Suspension Copolymer 16 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 03/01/13 Suspension Copolymer 16 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 03/01/13 Suspension Copolymer 16 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 03/01/13 Suspension Copolymer 16 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 03/01/13 Suspension Copolymer 16 VC Dow Method 107 75014 Vinyl chloride 0.22

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 2.07 VI Note (12)

Dow Midland MI 03/01/13 Suspension Copolymer 16 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 03/02/13 Suspension Copolymer 17 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 03/02/13 Suspension Copolymer 17 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 03/02/13 Suspension Copolymer 17 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 03/02/13 Suspension Copolymer 17 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 03/02/13 Suspension Copolymer 17 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 03/02/13 Suspension Copolymer 17 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 03/02/13 Suspension Copolymer 17 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 03/02/13 Suspension Copolymer 17 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 03/02/13 Suspension Copolymer 17 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 03/02/13 Suspension Copolymer 17 VC Dow Method 107 75014 Vinyl chloride 0.4

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 3.645 VI Note (12)

Dow Midland MI 03/02/13 Suspension Copolymer 17 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 03/04/13 Suspension Copolymer 18 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 03/04/13 Suspension Copolymer 18 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 03/04/13 Suspension Copolymer 18 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 03/04/13 Suspension Copolymer 18 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 03/04/13 Suspension Copolymer 18 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 03/04/13 Suspension Copolymer 18 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 03/04/13 Suspension Copolymer 18 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 03/04/13 Suspension Copolymer 18 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 03/04/13 Suspension Copolymer 18 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 03/04/13 Suspension Copolymer 18 VC Dow Method 107 75014 Vinyl chloride 0.955

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 2.53 VI Note (12)

Dow Midland MI 03/04/13 Suspension Copolymer 18 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 03/06/13 Suspension Copolymer 19 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 03/06/13 Suspension Copolymer 19 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 03/06/13 Suspension Copolymer 19 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 03/06/13 Suspension Copolymer 19 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 03/06/13 Suspension Copolymer 19 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 03/06/13 Suspension Copolymer 19 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 03/06/13 Suspension Copolymer 19 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 03/06/13 Suspension Copolymer 19 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 03/06/13 Suspension Copolymer 19 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

12/12/2013 VI Confidential 179 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 03/06/13 Suspension Copolymer 19 VC Dow Method 107 75014 Vinyl chloride 0.765

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 3.74 VI Note (12)

Dow Midland MI 03/06/13 Suspension Copolymer 19 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 03/07/13 Suspension Copolymer 20 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 03/07/13 Suspension Copolymer 20 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 03/07/13 Suspension Copolymer 20 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 03/07/13 Suspension Copolymer 20 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 03/07/13 Suspension Copolymer 20 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 03/07/13 Suspension Copolymer 20 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 03/07/13 Suspension Copolymer 20 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 03/07/13 Suspension Copolymer 20 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 03/07/13 Suspension Copolymer 20 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 03/07/13 Suspension Copolymer 20 VC Dow Method 107 75014 Vinyl chloride 0.31

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 1.55 VI Note (12)

Dow Midland MI 03/07/13 Suspension Copolymer 20 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 03/08/13 Suspension Copolymer 21 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 03/08/13 Suspension Copolymer 21 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 03/08/13 Suspension Copolymer 21 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 03/08/13 Suspension Copolymer 21 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 03/08/13 Suspension Copolymer 21 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 03/08/13 Suspension Copolymer 21 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 03/08/13 Suspension Copolymer 21 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 03/08/13 Suspension Copolymer 21 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 03/08/13 Suspension Copolymer 21 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 03/08/13 Suspension Copolymer 21 VC Dow Method 107 75014 Vinyl chloride 1.2

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 2.34 VI Note (12)

Dow Midland MI 03/08/13 Suspension Copolymer 21 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 03/09/13 Suspension Copolymer 22 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 03/09/13 Suspension Copolymer 22 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 03/09/13 Suspension Copolymer 22 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 03/09/13 Suspension Copolymer 22 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 03/09/13 Suspension Copolymer 22 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 03/09/13 Suspension Copolymer 22 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 03/09/13 Suspension Copolymer 22 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 03/09/13 Suspension Copolymer 22 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 03/09/13 Suspension Copolymer 22 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC SW-846-8260B 100414 Ethylbenzene

12/12/2013 VI Confidential 180 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 03/09/13 Suspension Copolymer 22 VC Dow Method 107 75014 Vinyl chloride Detection Limit Not Reported Non-Detect VI Note (11)

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 1.11 VI Note (12)

Dow Midland MI 03/09/13 Suspension Copolymer 22 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 03/10/13 Suspension Copolymer 23 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 03/10/13 Suspension Copolymer 23 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 03/10/13 Suspension Copolymer 23 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 03/10/13 Suspension Copolymer 23 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 03/10/13 Suspension Copolymer 23 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 03/10/13 Suspension Copolymer 23 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 03/10/13 Suspension Copolymer 23 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 03/10/13 Suspension Copolymer 23 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 03/10/13 Suspension Copolymer 23 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 03/10/13 Suspension Copolymer 23 VC Dow Method 107 75014 Vinyl chloride 0.585

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 3.345 VI Note (12)

Dow Midland MI 03/10/13 Suspension Copolymer 23 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 03/11/13 Suspension Copolymer 24 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 03/11/13 Suspension Copolymer 24 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 03/11/13 Suspension Copolymer 24 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 03/11/13 Suspension Copolymer 24 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 03/11/13 Suspension Copolymer 24 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 03/11/13 Suspension Copolymer 24 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 03/11/13 Suspension Copolymer 24 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 03/11/13 Suspension Copolymer 24 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 03/11/13 Suspension Copolymer 24 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 03/11/13 Suspension Copolymer 24 VC Dow Method 107 75014 Vinyl chloride 0.46

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 1.37 VI Note (12)

Dow Midland MI 03/11/13 Suspension Copolymer 24 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 03/12/13 Suspension Copolymer 25 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 03/12/13 Suspension Copolymer 25 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 03/12/13 Suspension Copolymer 25 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 03/12/13 Suspension Copolymer 25 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 03/12/13 Suspension Copolymer 25 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 03/12/13 Suspension Copolymer 25 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 03/12/13 Suspension Copolymer 25 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 03/12/13 Suspension Copolymer 25 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 03/12/13 Suspension Copolymer 25 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

12/12/2013 VI Confidential 181 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 03/12/13 Suspension Copolymer 25 VC Dow Method 107 75014 Vinyl chloride 0.81

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 1.16 VI Note (12)

Dow Midland MI 03/12/13 Suspension Copolymer 25 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 03/16/13 Suspension Copolymer 26 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 03/16/13 Suspension Copolymer 26 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 03/16/13 Suspension Copolymer 26 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 03/16/13 Suspension Copolymer 26 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 03/16/13 Suspension Copolymer 26 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 03/16/13 Suspension Copolymer 26 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 03/16/13 Suspension Copolymer 26 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 03/16/13 Suspension Copolymer 26 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 03/16/13 Suspension Copolymer 26 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 03/16/13 Suspension Copolymer 26 VC Dow Method 107 75014 Vinyl chloride Detection Limit Not Reported Non-Detect VI Note (11)

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.94 VI Note (12)

Dow Midland MI 03/16/13 Suspension Copolymer 26 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 03/17/13 Suspension Copolymer 27 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 03/17/13 Suspension Copolymer 27 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 03/17/13 Suspension Copolymer 27 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 03/17/13 Suspension Copolymer 27 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 03/17/13 Suspension Copolymer 27 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 03/17/13 Suspension Copolymer 27 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 03/17/13 Suspension Copolymer 27 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 03/17/13 Suspension Copolymer 27 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 03/17/13 Suspension Copolymer 27 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 03/17/13 Suspension Copolymer 27 VC Dow Method 107 75014 Vinyl chloride 1.515

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 1.425 VI Note (12)

Dow Midland MI 03/17/13 Suspension Copolymer 27 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 03/18/13 Suspension Copolymer 28 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 03/18/13 Suspension Copolymer 28 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 03/18/13 Suspension Copolymer 28 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 03/18/13 Suspension Copolymer 28 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 03/18/13 Suspension Copolymer 28 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 03/18/13 Suspension Copolymer 28 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 03/18/13 Suspension Copolymer 28 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 03/18/13 Suspension Copolymer 28 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 03/18/13 Suspension Copolymer 28 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 03/18/13 Suspension Copolymer 28 VC Dow Method 107 75014 Vinyl chloride 1.34

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 1.13 VI Note (12)

Dow Midland MI 03/18/13 Suspension Copolymer 28 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 03/19/13 Suspension Copolymer 29 Alcohol SW-846-8015C 107211 Ethylene glycol

12/12/2013 VI Confidential 182 of 183
VI Confidential

PVC MACT S114 Treated WW Sample Results

Submitted to EPA on May 1, 2013

Dow Midland MI 03/19/13 Suspension Copolymer 29 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 03/19/13 Suspension Copolymer 29 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 03/19/13 Suspension Copolymer 29 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 03/19/13 Suspension Copolymer 29 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 03/19/13 Suspension Copolymer 29 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 03/19/13 Suspension Copolymer 29 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 03/19/13 Suspension Copolymer 29 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 03/19/13 Suspension Copolymer 29 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 03/19/13 Suspension Copolymer 29 VC Dow Method 107 75014 Vinyl chloride Detection Limit Not Reported Non-Detect VI Note (11)

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) Detection Limit Not Reported Non-Detect VI Note (11)

Dow Midland MI 03/19/13 Suspension Copolymer 29 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

Dow Midland MI 03/20/13 Suspension Copolymer 30 Alcohol SW-846-8015C 107211 Ethylene glycol

Dow Midland MI 03/20/13 Suspension Copolymer 30 Alcohol SW-846-8015C 67561 Methanol

Dow Midland MI 03/20/13 Suspension Copolymer 30 Aldehyde SW-846-8315A 75070 Acetaldehyde

Dow Midland MI 03/20/13 Suspension Copolymer 30 Aldehyde SW-846-8315A 50000 Formaldehyde

Dow Midland MI 03/20/13 Suspension Copolymer 30 SVOC SW-846-8270D 51285 2,4-dinitrophenol

Dow Midland MI 03/20/13 Suspension Copolymer 30 SVOC SW-846-8270D 98862 Acetophenone

Dow Midland MI 03/20/13 Suspension Copolymer 30 SVOC SW-846-8270D 117817 Bis(2-ethylhexyl) phthalate (DEHP)

Dow Midland MI 03/20/13 Suspension Copolymer 30 SVOC SW-846-8270D 123319 Hydroquinone

Dow Midland MI 03/20/13 Suspension Copolymer 30 SVOC SW-846-8270D 108952 Phenol

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC SW-846-8260B 79345 1,1,2,2-tetrachloroethane

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC SW-846-8260B 106990 1,3-butadiene 5 Non-detect

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC SW-846-8260B 540841 2,2,4-trimethylpentane

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC SW-846-8260B 71432 Benzene

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC SW-846-8260B 108907 Chlorobenzene

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC SW-846-8260B 67663 Chloroform

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC SW-846-8260B 126998 Chloroprene

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC SW-846-8260B 98828 Cumene

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC SW-846-8260B 75003 Ethyl chloride (Chloroethane) 0.5 Non-detect

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC SW-846-8260B 100414 Ethylbenzene

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC SW-846-8260B 107062 Ethylene dichloride (1,2-Dichloroethane)

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC SW-846-8260B 75343 Ethylidene dichloride (1,1-Dichloroethane)

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC SW-846-8260B 74873 Methyl chloride (Chloromethane) 0.5 Non-detect

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC SW-846-8260B 75092 Methylene chloride

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC SW-846-8260B 110543 n-Hexane

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC SW-846-8260B 108883 Toluene

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC SW-846-8260B 71556 Methyl chloroform (1,1,1-Trichloroethane) 0.5 Non-detect

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC SW-846-8260B 79005 1,1,2-Trichloroethane 0.5 Non-detect

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC SW-846-8260B 108054 Vinyl acetate

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC SW-846-8260B 593602 Vinyl bromide 0.5 Non-detect

Dow Midland MI 03/20/13 Suspension Copolymer 30 VC Dow Method 107 75014 Vinyl chloride 0.765

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC Dow Method 75354 Vinylidene chloride (1,1-Dichloroethylene) 0.095 VI Note (12)

Dow Midland MI 03/20/13 Suspension Copolymer 30 VOC SW-846-8260B 1330207 Xylenes (isomers and mixtures)

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VI Confidential

Notes on Aggregated Database

PVC MACT S114 Treated WW Analysis

Submitted to EPA May 1, 2013

Facility Note: The data in tab "VI S114 Treated WW May 1 2013" was aggregated by the VI on May 5-8, 2013 from the database submissions to EPA by PVC MACT WG participants. 

Westlake

Westlake Note (2): The M107 VCM data result was an extrapolated value that was lower than the lowest calibration standard value as per the Method.

Westlake Note (3): The reported value for "Xylenes (isomers and mixtures)" CAS 1330207 is the higher value of the mp-Xylene and o-Xylene results.

Westlake Note (3.1): The reported value for "Xylenes (isomers and mixtures)" CAS 1330207 is the sum of the value of the mp-Xylene and o-Xylene results for Westlake Calvert City KY on January 27, 2013.

Westlake Note (4): Hydroquinone sample result rejected due to lack of recovery in the associated LCS.

Axiall PLQ LA VI Note (5): Reported by Axiall as 0 and restated by VI to be Not Found, consistent with Axiall ABD MS. When detection limits are not reported, it should be stated as such because zeros will be used in limit calculations for that HAP.

Axiall PLQ LA VI Note (6): This is a duplicate sample. Only need to use one of these samples for calculation. Suggest this duplicate not be included in limit calculations for consistency with m30 factor.

Axiall PLQ LA VI Note (7): For xylenes, use highest of three reported values in calculation to be consistent with what others have done.

Axiall PLQ LA VI Note (8): Reported by Axiall as 0 and restated by VI to be Not Reported. When detection limits are not reported, it should be stated as such because zeros will be used in limit calculations for that HAP.

Formosa TX VI Note (9): Reported by Formosa as 0 and restated by VI to be Not Reported. When detection limits are not reported, it should be stated as such because zeros will be used in limit calculations for that HAP.

Formosa TX VI Note (9.1): VI relocated the J indicator out of the value column and into the Notes column to be consistent with other data reported and to allow calculations to be performed on the estimated value.

Shintech Freeport2 TX VI Note (10): Date reported as 1/27/13 by Shintech restated by VI to be 1/24/13 in sequence with surrounding dates.

PolyOne Pedrictown NJ: No sample date was entered for sample header No. 10 cell AG22, Sample header nos. 11,21, & 26 numbers skipped in row22

Dow Midland, MI VI Note (11): Reported by Dow for Dow Method as 0 and restated by VI to be Not Reported. When detection limits are not reported, it should be stated as such because zeros will be used in limit calculations for that HAP.

Dow Midland, MI VI Note (12): Measured value reported for vinylidene chloride based on Dow method of analysis, not M8260B method. Dow's submission has measurements using both methods on different worksheets. Multiple data points for the same day were averaged together.

Note (1): Based on historical data for gases analyzed by SW-846 Method 8260B (SW-5030B Purge and Trap), the method quantitation limit (MQL) for Vinyl Bromide is estimated to be 1 ug/L. Due to the fact that 

calibration standards and verification standards were not readily available, estimated concentrations would be reported for Vinyl Bromide. Estimated concentrations are calculated based on the closest Internal 

Standard.

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