Exhaust Emissions Sampling 

DaI-Italia, LLC., Muskogee, OK 

Spray Dryer, Kiln Scrubber, and Trim Kiln Exhausts 

April 11 - 13, 2006 - 

AYmstr^ong En>>ironmental, 17zc. 

Project W-2496-06 

Report Prepared For: 

Bob Hurt ' 

Daltile 

7834 C. F. Hawn Freeway 

Dallas, TX 75217 

Report Prepared April 18, 2006 By: 

Arr7zstrong Envir•onnaental, Inc. 

7715 Sovereign Row 

Dallas, Texas 75247 

(214) 631-0021 
TABLE 4F CaNTENTS 

P age 

T. Introduction 1 

II. Summary 2-7 

III. Procedures 8 - 14 

IV. Appendices 

A. Calculation Summaries 15 - 31 

B. Confiinuous Elnissions Monitor Summaries 32 - 124 

C. GCIFID Chromatogram Summaries 125 - 155 

D. Analytical Summarnies 156 - 238 

E. Field Data Sheets 239 - 259 

F. Equipment CaliUrations 260 - 278 

G. Standard Gas Certifications 279 - 290 

H. S02 Interference 291 - 307 
SUMMARY OF EMISSIONS TEST DATA 

Table : 3 

Plant : Dal•Italia, Muskogee, OK 

Location : Kiln Scrubber Exhaust 

Operator : R. Taylor, G. Salinas, T. Armstrong 

Test Date : 12•Apr•06 

Repetition : 1 1 2 2 3 3 

STACK GAS 

Temperature, F 137.9 137.7 137.5 137.9 138.1 137.9 

Velocity, fps 30.35 29.40 29.95 29.64 27.36 29.01 

Volume Ftow, acfm 35167.5 34063.3 34699.0 34343.9 31702.9 33610.8 

scfm 23444.6 23352.0 24398.0 24452.2 21705.2 22998.2 

scfh 1406674 1401122 1463881 1467129 1302311 1379892 

Moisture, 0/0 23.92%, 21.78% 19.80% 18.74% 21.84% 21.91% 

CO2, % 3.50 3.50 3.00 3.00 3.50 3.50 

02, % 17.50 17.50 18.00 18.00 17.50 17.50 

SAMPLE 

Start Time, hrs:min 10:20 AM 10:20 AM 12:20 PM 12:20 PM 1:55 PM 1:55 PM 

Finish Time, hrs:min 11:23 AM 11:23 AM 1:23 PM 1:23 PM 2:58 PM 2:58 PM 

Sample Volume, scf 37.779 36.649 38.373 37.122 35.414 37.998 

Isokinetic Ratio, % 99.19634 95.19177 96.81835 92.0814 100.4374 100.2116 

PARTICULATE 

c=:..Front Ha~ 

Sample Weight, mg 108.89 94.99 78.21 

Concentration, gr/sct 0.044474 0.038196 0.034076 

Emissions, Ibs/hr 8.940003 7.990267 6.341765 

Back Half 

Sample Weight, mg 11.40 13.20 7.75 

Concentration, gr/scf 0.004656 0.005308 0.003377 

Emissions, Ibs/hr 0.935954 1.110344 0.628419 

Total Particulate, Ibs/hr 9.875957 9.100611 6.970185 

CARBON MONOXIDE 

Concentration, ppm 162.89 155.58 147.09 

Emissions. Ibs/hr 16.65558 16.59182 1475357 

NITROGEN OXIDE AS NO2 

Concentration, ppm 30.76 32.45 33.52 

Emissions, Ibs/hr 5.167154 5.685317 5.523581 

SULFUR DIOXIDE 

Concentration, ppm 1.03 0.0054 0.48 

Emissions, Ibs/hr 0.240727 0.001316 0110047 

VOC AS C3H8 

Concentration as CH4. ppm WET 13.92 12.80 14.61 

Concentration, as CH4, ppm DRY 18.29571 15.75224 18.70928 

Emissions as CH4, Ibs/hr 1.068997 0.959941 1.072349 

Emissions as Carbon, Ibs/hr 0.801748 0.719955 0.804261 

Emissions as C3H8, Ibs/hr 0.979914 0.879946 0.982986 

HYDROGEN FLUORIDE 

Sample Weight, mg 0.00 0.24 0.46 

Concentration, ppm 0 0.274562 0.514124 

Emissions, Ibs/hr 0 0.218559 0.384922 

CHLORINE 

Sample Weight, mg 0.00 0.00 0.00 

Concentration, ppm 0 0 0 

Emissions, Ibs/hr 0 0 0 

HYDROGEN CHLORIDE 

Sample Weight, mg 0.00 0.34 0.37 

Concentration, ppm 0 0.21313 0.226594 

Emissions, Ibs/hr 0 • 0.029629 .0029628 

1-i 
23.4 23.31 

.419906 1.413232 

61.96 61.86 

5.23091 5.217991 

48.86 49.08 

2.90319 52.63397 

.116575 1.10994 

837431 0.832455 

023527 1.017445 

92.01 89.64 

72.51438 72.70912 

1 :887641 1.843671 

0.41 0.52 

0.091688 0.118584 

0.008482 0.010675 

118.21 108.68 

51.0482 48.30297 

2.427719 2.235277 

SUMMARY OF EMISSIONS TEST DATA 

T able . Q 

Plant : Da!•Italia, Muskogee, OK 

Location : Trim Kiln Exhaust 

Operator : R. Taylor, G. Salinas. T. Armstrong 

Test Date : 13•Apr•06 

Repetition 1 1 2 2 

STACK GAS 

Temperature. F 456.3 456.6 461.2 Q61.4 

Velocity. fps 80.08 80.79 82.15 80.56 

Volume Flow, acfm 15730.0 15869.1 16137.2 15824.8 

scfm 8309.7 8422.5 8468.8 8364.9 

scfh 498579 505351 508127 501893 

Moisture, % 7.51% 7.06% 7.64% 6.95% 

CO2, % 3.00 3.00 3.00 3.00 

02, % 18.00 18.00 18.00 18.00 

SAMPLE 

Start Time, hrs:min 9:20 AM 9:20 AM 10:50 AM 10:50 AM 

Finish Time, hrs:min 10:23 AM 10:23 AM 12:02 PM 12:02 PM 

Sample Volume, scf 53.237 53,388 53.924 53.886 

Isokinetic Ratio, % 103.6873 102.92 103.0525 104.595 

PARTICULATE 

Front I~~ 

ae Weight, mg mpl 47.34 33.71 

Concentration, gr/scf 0.013721 0.009646 

Emissions, Ibs/hr 0.977598 0.700419 

6ack Half 

3 3 

462.7 462.6 

81.43 78.41 

15995.4 15402.8 

8461.5 8139.5 

507691 488372 

6.75% 6.8696 

3.00 3.00 

18.00 18.00 

12:15 PM 12:15 PM 

1:17 PM 1:17 PM 

53.173 52.357 

101.7038 104.4415 

24.79 

0.007194 

0.521911 

Sample Weight, mg 20.20 

Concentration, gr/scf 0.005855 0 

Emissions, Ibslhr 0.417142 0 

Total Particulate, lbs/hr 1.39474 1 

CARBON MONOXIDE 

Concentration, ppm 100.66 

Emissions, Ibs/hr 3.697618 3 

18.05 13.70 

.005165 0.003976 

.375039 0.28843 

.075458 0.81034 

99.81 97.54 

.686532 3.5996 

NITROGEN OX1DE AS NO2 

Concentration, ppm 23.84 

Emissions, Ibs/hr 1.438703 1 

SULFUR D10XIDE 

Concentration, ppm 62.07 

Emissions. lbs/hr 5.211573 

VOC AS C31i8 

Concentration as CH4, ppm WET 49.88 

Concentration, as CH4, ppm DRY 53.66641 5 

Emissions as CH4, Ibs/hr 1.126496 1 

Emissions as Carbon, Ibs/hr 0.844872 0 

Emissions as C31-18, Ibs/hr 1.032621 1 

HYDROGEN FLUORIDE 

Sample Weight, mg 86.71 

Concentration, ppm 68.97436 

Emissions, Ibs/hr 1.80977,C 

CHLORINE 

Sample Weight, mg 0.51 

Concentration, ppm 0.114053 

Emissior+.s, Ebs/hr 0.010624 

HYDROGEN CHLORIDE 

Sample Weight, mg 113.72 

Concentration, ppm 49.56698 

Emissions, ibs/hr 2.373518 

7 
III. PROCEDURES 

The procedure for emissions sampling followed USEPA test methods as detailed in Title 

40: Code of Federal Regulations. The following methods were used: 

Method Title 

1 Sample and Velocity Traverses for Stationary Sources 

2 Determination of Stack Gas Velocity and Volumetric Flow Rate (Type S 

Pitot Tube) 

3 Gas Analysis for the Determination of Dry Molecular Weight 

5 Detennination of Particulate Emissions from Stationary Sources 

6C Determination of Sulfur Dioxide Emissions from Stationary Sources 

(Instrumental Analyzer Procedure) 

7E Determination of Nitrogen Oxides Emissions from Stationary Sources 

(Instrumental Analyzer Procedure) 

10 Detennination of Carbon Monoxide Emissions from Stationary Sources 

18 Measurement of Gaseous Organic Compound Emissions by Gas 

Chromatography 

25A Determination of Total Gaseous Organic Concentration using a Flame 

Ionization Analyzer 

26A Determination of Hydrogen Halides and Halogens Emissions from 

Stationary Sources 

202 Determination of Condensible Particulate Emissions from Stationary 

Sources 

02 and CO2 were determined using FyRite Analyzers. 

PM, HF, and HC1 sampling was perfonned on each source as follows: 

Source Number of Traverse Points M nuteslPoint 

Spray Dryer 24 2•5 

Kiln Scrubber 20 3.0 

Trim Kiln 12 5•0 

The PM sampling train was configured as follows: 

: 
Glass or Stainless Steel sample nozzle 

Heated Glass Lined probe 

Heated Glass Fiber Filter (teflon filter for the Trim Kiln) 

Impinger #1 - 100 mis H20 

Impinger #2 - 100 mis H20 

Impinger #3 - 100 mis H20 

Impinger #4 - Empty 

Impinger #5 - 200 grams Silica Gel 

The probe and prefilter glassware was rinsed with acetone. The irnpingers solutions 

were recovered and' rinsed with H20 and MeCI. The impinger solution was extracted 

with the MeCI rinse. All solutions were evaporated in tared glass beakers, with the 

exception of the impinger solution from the Trim Kiln, which was evaporated in Teflon 

beakers. 

The HF/HC1/C12 sampling train was configured as follows: 

Glass Salnpling Nozzle 

Heated Glass Lined Probe 

Heated teflon filter 

Impinger #1 - 100 mis 0.1 N H2SO4 

Inlpinger #2 - 100 mis 0.1 N H2SO4 

Impinger #3 - 100 mis 0.1 N NaOH 

Impinger 94 - 100 mis 0.1 N NaOH 

Impinger #5 - 200 grams silica Gel 

HF and HCl analysis was performed on the solution from the 1 st and 2nd impinger. 

Chlorine analysis was performed the solution from the 3rd and 4th impingers. Analysis 

was performed using a Dionex LC20 IC/HPLC. Calibrations standards were blended frorn 

a 1002 mg/Lt certified Chloride standard and a 1011 mg/Lt certified Fluoride standard. 

Continuous monitoring was performed as follows: 

Source Com onent Monitor Ran e Standards 

Spay Dryer CO Fuji 3300 0- 100 ppm 49.9ppm, 99.1ppm CO 

in N2 EPA Protocol 1 

Trim Kiln, Kiln CO Fuji 3300 0- 500 200ppm, 494ppm, CO 

Scrubber in N2 EPA Protocol 1 

Spray Dryer, Ki1n NOx EcoPhysics 70s 0-60 ppm 25.5ppm, 51 ppm NOx 

Scrubber, 'I'rim Kiltt in N2 EPA Protocol 1 

Spray Dryer, Kiln S02 Western Research 0- 100 49• 8PPm, 100 ppm S02 

Sci-ubber 721-AT in N2 EPA Protocol 1 

Trinl Kiln S02 Western Research 0- 250 140ppm, 250pprn S02 

721-AT in N2 Epa Protocol 1 

Spray Dryer, Kiln vOC TECO 51 0- 70 19.9ppm, 40.8ppm, 

Scrubbcr, l'rim Kiln 61.7ppm CI44 in N2 

EPA Protocol I 

9 
Methane vvas detem-iined. using a Carle 100 GCIFID calibrated witti the abave CH4 

starndards. San-lples were talcen via a peristaltic punlp -and integrated gas bags. 

10 
Figure I - Spray Dryer Baghouse Exhaust 

roor 

I" 

mmi 

—~ 

~ 

'Ra ck Diemter - 71 inches 

Poiryl #1 - 1.5 inclhes 

Point #2 - 4.75 inches 

Poinl 93 - 8.4 inches 

f'oint #4 -12.6 inches 

Point #5 -17.75 iiiclies 

Poird #6 - 25 ? inches 

Point #7 - 45.7 inchQs 

Point #8 - 53.25 incftes 

F'oirtt #9 - Sa.4 inches 

Poinl #10 - 62.6 inches 

Point #11 - 66.25 inches 

Point #12 - 69.5 inches 
I'igure 2 - Kiln Scrubber ~xhaust 

Sfact: Liameter - 59.5 inches 

Paint #1 -1.5 inclies 

Pnint #2 - 4 .9 inches 

Point #3 - 81 incltes 

Pt7iflt #il - 13A irt c}Zes 

Poitit #5 - 203 inches 

Paint #6 - 39.1 inches 

Pain! #7 - 46.1 inches 

Paint #8 - 50.8 inches 

PoiM #9 - 54.6 inclins 

Point #10 - 5g inches 

~-j 

N 
Figure } - Trim Kiln Exhaust 

aoil 

'i 80" 

~ 

w 

Stack Diarneter - 24.5 inches 

Point #i - 1.1 inches 

Poini #2 - 3.6 inches 

Point #3 - 7.25 inclZes 

Poird #4 -1725 inches 

Poird #5 - 20.91nches 

Point #6 - 23.9 inches 
Fi gLlro 4- CEt,.,l Confi gurati on 

lnstaLl: Fifter, Heated Probe 

Co Ane1yLer' 

Hea#eti 

Ssmple Line 

G as 

FID Analyzer @9g ~ hlo:. Anaiyzer 

purnla 1 -4 S02 A raalyrZer 

Heated tt-lanifoki 

`'atnple ~ 

To Interfernce Train Pr'ocessor Gaiib:'ation Point 

Puttnp 

Bias Calibratinn Sp-an Line 

~ 

•P 

5~ tiample larocessor cansists of ttivo sl7ort stem impingers followed by a 0_3 

PurnP niicron filter 

EfVIISSION TEST SUMMARY 

PLAN T : DaI•:ta1,a. Nfoskogee. OP: 

DATE : I?_-Apr 06 

PLACE : Kiln Scrubber iwxhaus! 

RUN# : 1 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 216.8 

NOZZLE DIAMETER (INCH.) : 0.312 PARTICULATE WEIGHT (Front half mg) : C 

METER COEFFICIENT (Y) : 1 PARTICULATE WEIGHT (Back half mg) : 0 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •0.21 

GAS METER VOL.(Cu.Ft.) : 38.2 PERCENT CO2 3.5 

BAROMETRIC PRESSURc 29.7 PERCENT 02 17.5 

PERCENT CO : 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 59.5 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 19.30907 STACK W1DTH(inchs) : 

NOZZLE AREA (feet): 0.000531 STACK AREA (Sq.Ft.) : 0 

ENTER THE S T ACK AREA SHOWN ABOVE: 19.30907 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 36.6495 

VOLUME OF WATER VAPOR (STD. CU .FT.): 10.2048 

FRACTIONAL MOISTURE CONTENT 0.2178 

DRY BASE: 79.0000 

MOLECU LAR WT. OF STACK GAS (DRY i3ASE): 29.2600 

MOLECU LAR WT. OF STACK GAS (WET BASE): 26.8076 

STACK PRESSURE (inch Hg): 29.6846 

STACK GAS VELOCITY (ft/sec.): 29.4018 

ACTUAL STACK GAS FLOW RATE (ACFM): 34063.27 

STANDARD STACK GAS FLOW RATE (SCFH): 1401122.14 

ISOKINETIC RATIO (%): 95.1918 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 138 0.30 0.547723 1.30 78 78 

2 138 0.30 0.547723 1.30 85 80 

3 138 0.26 0.509902 1.20 87 81 

4 138 0.24 0.489898 110 88 81 

5 138 0.23 0.479583 i.00 89 81 

6 138 0.20 0.447214 0.88 90 82 

7 138 0.19 0.43589 0.84 90 83 

8 138 0.20 0.447214 0.88 94 83 

9 138 0.18 0.424264 0.80 91 83 

10 137 0.15 0.387298 0.66 92 84 

11 136 0.22 0.469042 0.97 87 85 

12 136 0.20 0.447214 0.88 92 85 

13 137 0.20 0.447214 0.89 93 85 

14 137 .0.18 0.424264 0.79 96 85 

15 138 0.19 0.43589 0.84 93 86 

16 137 0.24 0.489898 1.10 94 86 

17 139 0.23 0.479583 1.00 95 87 

18 139 0.27 0.519615 1.20 95 87 

19 138 0.28 0.52915. 1.30 95 87 

20 138 0.24 0.489898 1,07 96 88 

137.7 0.4724 1.0000 91.0000 83.8500 87.4250 

20 
1 137 0.22 0.469042 0.99 

2 138 0.23 0.479583 1,00 

3 138 0.20 0.447214 0.80 

4 138 0.19 0.43589 0.85 

5 13S 0.21 0.458258 0.94 

6 138 0.24 0.489898 1.10 

7 138 0.27 0.519615 1.20 

8 138 0.27 0.519615 1,20 

9 138 0.28 0.52915 1.25 

10 137 0.24 0.489898 1.10 

11 i 35 0.31 0.556776 140 

12 138 0.30 0.547723 1.40 

13 138 0.25 0.5 1.10 

14 138 0.24 0.489898 1.10 

15 ! 38 0.23 0.479583 1.05 

16 138 0.20 0.447214 0.92 

17 138 0.20 0.447214 0.92 

18 138 020 0.447214 0.91 

19 0.19 0.43589 0.87 

20 137 0 15 0.387298 069 

137.85 0.4788 1.0395 

89 

92 

95 

96 

97 

97 

98 

99 

99 

99 

94 

100 

100 

101 

101 

101 

101 

101 

102 

102 

98.2000 

89 

89 

90 

90 

91 

91 

91 

92 

92 

92 

93 

94 

94 

94 

94 

95 

95 

U5 

95 

95 

92.5500 95.3750 

EMISSION TEST SUMNlARY 

aLANT : : 

DATE : :2 A r-;)6 

PLACE . Kiln ~,; -•ut.ber Exnaust 

RUN#: 2 

TEST DURATION (MINUTES) : 

-NOZZLE DIAMETER (INCH.) : 

METER COEFFICIENT (Y) : 

PITOT COEFFICIENT (Cp) : 

GAS METER VOL.(Cu.Ft.) : 

BAROMETRIC PRESSURE : 

60 LIQUID COLLECTED (mis) : 

0.312 PARTICULATE WEIGHT (Front half mg) 

1 PARTICULATE WEIGHT (Back half n ~,g) 

0.84 STATIC PRESSURE (in. H20) : 

39.251 PERCENT CO2 : 

293 ' PERCENT 02 

PERCENT CO : 

18; 9 

a 

C 

-a.22 

3 

18 

0 

FOR CIRCULAR STACK FOR RECTANGULAR- STACK 

STACK DIAMETER (inch): 59.5 STACK LENGTH(inches) : 

STACK AREA (Sq.Ft.) : 19.30907 STACK WIDTH(inches) : 

NOZZLE AREA (feet): 0.000531 STACK AREA (Sq.Ft.) : 

ENTER THE S T ACK AREA SHOWN Ai30VE: 19,30907 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 

VOLUME OF WATER VAPOR (STD. CU .FT.): 

FRACTIONAL MOISTURE CONTENT ( o): 

DRY BASE: 

MOLECULAR WT. OF STACK GAS (DRY i3ASE): 

MOLECULAR WT. OF STACK GAS (WET BASE): 

S T ACK PRESSURE (inch Hg): 

STACK GAS VELOCITY (ft/sec.): 

ACTUAL STACK GAS FLOW RATE (ACFM): 

STANDARD STACK GAS FLOW RATE (SCFH): 

ISOKINETIC RATIO (%): 

POINTS STACK T. DELTA P SQUAR D.P DELTA H 

deg F 

37.1224 

8.5620 

0.1874 

79.0000 

29.2000 

27.1009 

29.6838 

29.6440 

34343.8899 

1467129.37 

92.0814 

METER T. 

INLET 

METER T. 

OUTLET 

0 

21 
EMISSION TEST SUMMARY 

PLANT : D::l.itelia. iyt::skoga?. OK. 

DATE : 12•Apr•06 

PLACE : K,Iri Scrub:-)er Exhaust 

RUN#: 3 

TEST DURA T ION (MINUTES) : 60 LIQUID COLLECTED (mis) : 216 r 

NOZZLE DIAMETER (INCH.) : 0.312 PARTICULATE WEtGHT (Front half mg) : G 

METER COEFFICIENT (Y) : 1 PARTICULATE WEIGHT (Back half mg) : 0 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : .0.2 

GAS METER VOL.(Cu.Ft.) : 40.523 PERCENT CO2 3.5 

BAROMETRIC PRESSURE : 29.7 PERCENT 02 17.5 

PERCENT CO 0 

FOR CIRCULAR S T ACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 59.5 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 19.30907 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0.000531 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 19.30907 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 37.9975 

VOLUME OF WATER VAPOR (STD. CU .FT.): 10.6614 

FRACTIONAL MOISTURE CONTENT (%): 0.2191 

DRY BASE: 79.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29,2600 

MOLECULAR WT. OF STACK GAS (WET BASE): 26,7929 

STACK PRESSURE (inch Hg): 29.6853 

STACK GAS VELOCITY (ft/sec.): 29,0113 

ACTUAL STACK GAS FLOW RATE (ACFM): 33610.8369 

STANDARD STACK GAS FLOW RATE (SCFH): 1379892.29 

ISOKINETIC RATIO (%): 100.2116 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 138 0.29 0.538516 1.40 95 95 

2 138 0.30 0.547723 1.40 103 96 

3 139 0.28 0.52915 1.30 102 97 

4 138 0.26 0.509902 1.20 103 97 

5 138 0.23 0.479583 1.10 103 97 

6 138 0.20 0.447214 0.94 103 98 

7 138 0.18 0.424264 0.85 103 98 

8 138 0.19 0.43589 0.90 103 98 

9 138 0,19 0.43589 0.90 103 98 

10 138 0.17 0.412311 0.80 103 98 

11 138 0.23 0.479583 1.10 101 98 

12 137 0.21 0.458258 0.99 102 99 

13 137 0.20 0.447214 0.94 102 99 

14 137 0.20 0.447214 0.95 103 99 

15 137 0.19 0.43589 0.89 103 99 

16 138 0.20 0.447214 0.95 103 99 

17 138 0.20 0.447214 0.94 103 99 

18 138 0.21 0.458258 0.99 103 99 

19 138 0.22 0.469042 1.00 102 99 

20 138 0.22 0.469042 100 101 100 

137.85 0.4660 1.0270 102.2000 98.1000 100.1500 

?2 
EMISSION TEST SUMMARY 

PLANT : bal-ltal;a. Vw:;kogee. bK 

DATE : 12-4rn•06 

PLACE : l;iEn Scrubbcir Fxiiiust 

RUNr: ? 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 252.3 

NOZZLE DIAMETER (lNCH.) : 0.3C97 PARTICULATE WEIGHT (Front half mg) : 108.89 

METER COEFFICiENT (Y) : 0.972 PARTICULATE WEIGHT (Back hakf mg) : 11.4 

PITOT COEFFICIcNT (Cp) : 0.844 STATIC PRESSURE (in. H20) : •D 21 

GAS METER VOL.(Cu.Ft.) : 40.433 PERCENT CO2 33 

BAROMETRIC PRi=SSURE 29.7 PERCENT 02 17.5 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 59.5 STACK LENGTH('snchs) : 

STACK AREA (Sq.Ft.) : 19.30907 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0.000523 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 19.30907 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 37.7792 

VOLUME OF WATER VAPOR (STD. CU .FT.): 11.8758 

FRACTIONAL MOIS T URE CONTEN T( ~Jo): 0.2392 

DRY BASE: 79.0000 

MOLECULAR WT, OF STACK GAS (DRY BASE): 29.2600 

M0LECULAR WT. OF S T ACK GAS (WET BASE): 26.5670 

STACK PRESSURE (inch Hg): 29.6846 

STACK GAS VELOClTY (ft/sec.): 30.3549 

ACTUAL STACK GAS FLOW RATE (ACFM): 35167.5017 

STANDARD S T ACK GAS FLOW RATE (SCFH): 1406674.11 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0445 

PARTlCULAT;. CONCENTRATION (LBS/SCF): 6.36E•06 

PARTICULATE EMISSION (LBS/HR): 8.9400 

BACK HALF 

PARTICULATE CONCENI'RATION (GR./SCF): 0.0047 

PARTICULATE CONCENTRATION (LBS/SCF): 6.65E-07 

PARTICULATE EMISSION (LBS/HR): 0.9360 

iSOKINETIC RA T f0 {qo): 99.1963 

POINTS STACK T. D"cL T A P SQUAR D.P DELi A H METER T. METER T. 

deg F INLET OUTLET 

1 138 0.21 0.458258 1.00 82 80 

2 138 0.27 0.519615 1.30 84 80 

3 l39 0.29 0.538516 1.40 80" $'J 

4 138 0.27 0.519615 1.30 87 80 

5 138 0.26 0.509902 1.20 88 81 

6 138 0.24 0.489898 1.10 89 81 

7 138 023 0.479583 1.10 89 82 

8 138 0.25 0.5 1.20 90 82 

9 i 38 0.27 0.519615 1.30 90 83 

10 138 0.30 0.547723 1.40 91 83 

11 137 0.17 0.412311 0.84 85 84 

12 137 0.18 0.424264 0.89 85 84 

13 137 0.:9 0.43589 0.94 89 84- 

14 139 0.20 0.447214 0.99 99 84 

15 137 0.2 i 0.458258 1.00 92 84 

16 137 017 0.412311 0.84 94 $5 

17 ? 3$ 0.20 0.447214 0.99 94 86 

18 138 0.21 0.458258 i. 30 95 86 

19 138 0.31 0.556776 1.50 95 37 

20 138 0.33 0.574456 1.60 95 38 

137.85 0.4855 1.1595 89.9500 83.2000 86.5750 

?3 
EMISSION TEST SUMMARY 

PLANT : DaI-It;:Ita. MuSkngeH. OK 

DATE : 12-AFsr-06 

PLACE : Ki}n 3rru!:!'iEtr Exh ~ ust 

RUNst : 2 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 201.3 

NOZZLE DIAMETER (INCH.) : 03097 PARTICULATE WEIGHT (Front half mg) : 34.99 

METER COEFFICIENT (Y) : 0.972 PARTICULATE WEIGHT (Back half mg) : : 3.2 

PITOT COEFFICIENT (Cp) : 0.34 STA T IC PRESSURE (in. H20) : 0.2 

GAS METER VOL.(Cu.FI.) : 4; .752 PERCENT CO2 2 

BAROMETRIC PRESSURE 29.7 PERCENT 02 18 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 59.5 STACK LENGTH(inches) : 

STACK AREA (Sq.Ft.) : 19.30907 STACK WIDTH(inches) : 

NOZZLE AREA (feet): 0.000523 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 19.30907 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 38.3735 

VOLUME OF WATER VAPOR (STD. CU .FT.): 9.4752 

FRACTIONAL MOISTURE CONTENT 0.1980 

DRY BASE: 79.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.2000 

MOLECUL AR WT. OF STACK GAS (WET BASE): 26.9821 

STACK PRESSURE (inch Hg): 29.6853 

STACK GAS VELOCITY (ft/sec.): 29.9506 

ACTUAL STACK GAS FLOW RATE (ACFM): 34699.0433 

STANDARD STACK GAS FLOW RATE (SCFH): 1463881.07 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0382 

PARTICULATE CONCENTRATION (LBS/SCF): 5.46E•06 

PARTICULATE EMISSION (LBS/HR): 7-9903 

BACK HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0053 

PARTICULATE CONCENTRATION (LBS/SCF): 7.58E•07 

PARTICULATE EMISSION (LBS/HR): 1.1103 

ISOKINETIC RATIO (%): 96.8184 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 132 0. i 6 0.4 8.00 90 89 

2 137 0.19 0.43589 0.95 94 90 

3 138 0.20 0.447214 1.00 95 91 

4 138 0.19 0.43589 0.95 95 9 i 

5 137 0.21 0.458258 1.00 96 92 

6 137 0.22 0.469042 1.10 96 92 

7 138 0.25 0.5 1.20 97 92 

8 133 0.27 0.519615 1.30 99 93 

9 138 0.30 0.547723 1.50 101 93 

10 138 0,31 0.556776 1.50 102 93 

11 138 0.21 0.458258 1.00 99 94 

12 138 0.28 0.52915 1.50 10? 94 

13 '. 38 027 0.519615 1 40 101 95 

14 ] 33 0.2E 0.52915 1.50 102 95 

15 138 0.25 0.5 1.30 102 95 

16 133 0.2C, 0.447214 1.00 102 95 

17 12118 0.19 0.43589 1.00 103 95 

18 :36 ~:.21 0.458258 1.10 104 95 

19 138 G.25 0.5 1 3;) 102 95 

20 137 026 0.509902 1 40 103 95 

137.5 0.4829 1.5500 99.2000 93.2000 96.2000 

P 4 
EMISSION TEST SUMMARY 

PLANT : Caf•!talia. OK. 

DATE : . z-Aar•06 

PLACE "ocrunLvr Eyt- aus; 

RUN#: < 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 

NOZZLE DIAMETER (INCH.) : 0.3097 PARTICULATE WEIGHT (Front half mg) : 

METER COEFFICIENT (Y) : 2. 9 72 PARTICULATE WEIGHT (Back hatf mg) : 

?ITOT COEF=ICIENT (Cp) 3.8: STA 7 IC PRESSURE (in. H20) : 

GAS METER VOL.(Cu.Ft.) : 38 78 PERCENT CO2 

BAROMETRIC PRESSURE 24.7 ?ERCENT 02 

PERCENiCO 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAME T ER (inch): 59-5 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : I9.30907 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0.000523 STACK AREA (Sq.Ft.) : 

ENTER THE STACK AREA SHOWN ABOVE: 19.30907 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 35.4140 

VOLUME OF WATER VAPOR (STD. CU .FT.): 9.8941 

FRACTIONAL MOISTURE CONTENT {qo): 0.2184 

DRY BASE: 79.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.2600 

MOLECULAR WT. OF STACK GAS (WET BASE): 26.8011 

ST.4CK PRESSURE (inch Hg): 29.6846 

STACK GAS VELOCITY (ft/sec.): 27.3644 

ACTUAL STACK GAS FLOW RATE (ACFM): 31702.8871 

STANDARD STACK GAS FLOW RATE (SCFH): 1302310,56 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCEN T RATION (GR./SCF): 0.0341 

PARTICULATE CONCENTRATION (LBS/SCF): 4.87E•06 

PARTICULATE EMISSION (LBS/HR): 6.3418 

BACK HALF 

PARTICULA T E CONCENTRATION (GR./SCF): 0.0034 

PARTICULATE CONCENTRATION (LBS/SCF): 4.83E•07 

,PARTICULATE EMISSION (LBS/HR): 0.6284 

ISOKINETIC RATIO (%): 100.4374 

POINTS STACK T. DELTA P SQUAR D.P Dc'LTA H METER T. METER T. 

deg F INLET OUTLET 

1 138 0.20 0.447214 i l C 95 94 

2 138 C.24 0.489898 1.30 100 95 

3 139 0.25 0.5 1.30 102 95 

4 139 0.26 0.509902 1,40 102 95 

5 139 0 24 0.489898 30 103 96 

6 139 0.20 0.447214 : 00 103 96 

7 135 0.21 0.458258 : 1 C 103 96 

fi i 39 0.22 0.469042 1.10 103 96 

9 136 0.23 0.479583 1.20 103 9-3 

10 i 38 0.24 0.489898 1.30 102 96 

11 138 0 15 0.387 298 081 10: 97 

12 137 0, i 7 0.412311 0.92 l O 1 97 

13 138 0. I:; 0.424264 D.97 i 03 97 

14 :3S C; 17 0.412311 0,92 103 97 

15 138 0 15 0.387298 081 103 97 

16 138 0.:8 0.424264 0.97 103 196 

17 I 3 ~+ r?. i 6 0.4 0,£35 110396 

18 1 38 0.14 0.374166 0.76 l Os 96 

19 :"sL 0.16 04 C.f:b 102 97 

20 i 33 ;~ . :;~ 0.387298 0 81 103 97 

138.05 0.4395 1.0395 102,0500 96.1000 

210.2 

78.21 

-021 

3.5 

17.5 

0 

0 

99.0750 

~ v 
0.81 0.9 1.50 85 80 

0.92 0.959166 1.70 85 81 

1.30 1.140175 2.40 86 81 

1.40 1.183216 2.60 88 82 

1.30 1.140175 2.40 87 82 

1.20 1.095445 2.30 88 83 

0.93 0.964365 1.70 85 83 

1.10 1.048809 2.10 86 84 

1.30 1.140175 2.40 87 84 

1.40 1.183216 2.60 89 84 

1.30 1.140175 2.40 91 85 

1. ; 0 1.048809 2.10 91 87 

1.0786 2.1833 87.3333 83.0000 85.1667 

1 

2 

3 

4 

5 

6 

7 

8 

9 

10 

11 

1 2 

434 

459 

459 

458 

456 

456 

452 

460 

459 

460 

^61 

465 

456.58333 

EMISSION TEST SUMMARY 

PLANT 11%11usl,o;ee. C;i! 

DATE : 13 Ahr•06 

PLACE : Trim Kiln Exh,aLas't 

RUN# : _ 

TEST DURATION (MINUTES) : 6C~ LIQUID COLLECTED (mis) : oh.] 

NOZZLE DIAMETER (INCH.) : 0.2483 PARTICULATE WEIGHT (r=ront haff mg) : G 

METER COEFFICIENT (Y) : 1 PARTICULATE WEIGHT (Back half mg) : 0 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : .0.55 

GAS METER VOL.(Cu.Ft.) : 55.256 PERCENT CO2 : 3 

BAROMETRIC PRESSURE : 29.7 PERCENT 02 : 18 

PERCENT CO : 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 24.5 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 3.273856 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0.000336 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 3.273856 

FLOVYS 

SAMPLED VOLUME (STD. CU .FT.): 

VOLUME OF WATER VAPOR (STD. CU .FT.): 

FRACTIONAL MOISTURE CONTENT 

DRY BASE: 

MOLECULAR WT. OF STACK GAS (DRY BASE): 

MOLECULAR WT. OF STACK GAS (WET BASE): 

STACK PRESSURE (inch Hg): 

STACK GAS VELOCITY (ft/sec.): 

ACTUAL STACK GAS FLOW RATE (ACFM): 

STANDARD STACK GAS FLOW RATE (SCFH): 

ISOKINETIC RATIO ( Jo ): 

POINTS STACK T. DELTA P SQUAR D.P DELTA H 

deg F 

53.3883 

4.0527 

0.0706 

79.0000 

29.2000 

28.4098 

29.6596 

80.7872 

15869.132 

505351.318 

102.9200 

METER T. METER T. 

INLET OU T LET 

26 
EMISSION TEST SUMMARY 

PLANT : Dal•I;alia. ,Mi.skogee. 0K 

DATE : i 3 Apr-06 

PLACE : T rim Kiln Exhaust 

?UN# : ~? 

TLST DURaTION (MINUTES) : 

IVOZZLE DIAMETER (INCH.) : 

METER COEFFICIENT (Y) : 

PITOT COEFFICIENT (Cp) : 

GAS METER VOL.(Cu.Ft.) : 

BAROMETRIC PRESSURE : 

60 LIQUfD COLLECTED (mis) : 

0.2483 PARTICULATE WEIGHT (Fron; half mg) 

1 PARTICULATE WEIGHT (Back half mg) 

0.84 STATIC PRESSURE (in. H20) : 

56.517 PERCENT CO2 : 

29.7 PERCENT 02 : 

PERCENT CO : 

0 

0 

0.53 

3 

18 

0 

C 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 24.5 STACK LENGTH(inches) : 

STACK AREA (Sq.Ft.) : 3.273856 STACK WIDTH(inches) : 

NOZZLE AREA (feet): 0.000336 STACK AREA (Sq.Ft.) : 

ENTER THE STACK AREA SHOV'JN ABOVE: 3.273856 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 53.8860 

VOLUME OF WATER VAPOR (STD. CU .FT.): 4.0245 

FRACTIONAL MOISTURE CONTENT (%): 0.0695 

DRY BASE: 79.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.2000 

MOLECULAR WT. OF STACK GAS (WET BASE}: 28.4217 

STACK PRESSURE (inch Hg): 29.6610 

STACK GAS VELOCITY (ft/sec.): 80.5616 

ACTUAL STACK GAS FLOW RATE (ACFM): 15824.8273 

STANDARD STACK GAS FLOW RATE (SCFH): 501893.365 

ISOKINETIC RATIO (%): 104.5950 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 456 0.91 0.953939 1.70 90 87 

2 461 1.20 1.095445 2.30 94 88 

3 462 1.40 1.183216 2.60 93 88 

4 462 -.30 1.140175 2.40 95 89 

5 461 1.20 1.095445 2.30 96 89 

6 460 0.96 0.979796 1.80 100 91 

7 461 1.10 1.048809 2.10 91 89 

8 463 1.20 1.095445 2.30 95 91 

9 463 1.30 1.140175 2.40 96 91 

10 463 1.20 1.095445 2.30 96 92 

11 463 1.10 1.048809 2.10 97 92 

12 462 1.00 1 1.90 97 92 

461.41667 1.0731 2.1833 95.0000 89.9167 92.4583 

2 7 
EM1SSlON TEST SUMMARY 

PLANT : Dai-Italia. tVluskogee, rJK 

DATE : '_ 3-Apr-06 

PLACE : Trirn KiIn Exf;aust 

RUN#: 3 

TEST DURATION (MINUTES) : 60 

NOZZLE DIAMETER (INCH.) : 0.2483 

METER COEFFICIENT (Y) : 1 

PITOT COEFFICIENT (Cp) : 0.84 

GAS METER VOL.(Cu.Ft.) : 55.067 

BAROMETRIC PRESSURE : 29.7 

FOR CIRCULAR STACK 

STACK DIAMETER (inch): 24.5 

STACK AREA (Sq.Ft.) : 3.273856 

NOZZLE AREA (feet): 0.000336 

ENTER THE STACK AREA SHOWN ABOVE: 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 

VOLUME OF WATER VAPOR (STD. CU .FT.): 

FRACTIONAL MOISTURE CONTENT (%): 

DRY BASE: 

MOLECULAR WT, OF STACK GAS (DRY BASE): 

MOLECULAR WT. OF STACK GAS (WET BASE): 

STACK PRESSURE (inch Hg): 

STACK GAS VELOCITY (ft/sec.): 

ACTUAL STACK GAS FLOW RATE (ACFM): 

STANDARD STACK GAS FLOW RATE (SCFH): 

1SOKINETIC RATIO (%): 

LIQUID COLLEC T ED (mis) : 

PARTICULATE WEIGHT (Front half mg) ; 0 

PARTICULATE WEIGHT (Back half rng) : 0 

STATIC PRESSURE (in. H20) : 0.53 

PERCENT CO2 : 3 

PERCENT 02 : 18 

PERCENT CO 0 

FOR RECTANGULAR STACK 

STACK LENGTH(inchs) : 

STACK WIDTH(inchs) : 

STACK AREA (Sq.Ft.) : C 

3.273856 

52.3574 

3.8550 

0.0686 

79.0000 

29.2000 

28.4319 

29.6610 

78.4134 

15402.8489 

488372.192 

104.4415 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 465 0.92 0.959166 1.80 91 91 

2 464 1.20 1.095445 2.30 95 90 

3 463 1.30 1.140175 2.40 97 91 

4 465 1.20 1.095445 2.30 97 91 

5 464 1.10 1.048809 2.10 95 91 

6 437 0.91 0.953939 1.70 95 92 

7 466 1.00 1 1.90 94 92 

8 466 1.20 1.095445 2.30 97 92 

9 466 1.20 1.095445 2.40 98 93 

10 466 1.10 1.048809 2.10 97 93 

11 464 1.00 1 1.90 98 93 

12 465 0.99 0.994987 1.90 98 92 

462.58333 1.0440 2.0917 96.0000 91.7500 93.8750 

s 
EMlSSION TEST SUMMARY 

PLANT : Dat•1*311,12. MU-,:eU~~_ ei~ ","'( 

DATE . : 3 ~.pr Q6 

PLACE : 1 rim ±<,Ar. E>;haus; 

RUN# : 1 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 91.9 

NOZZLE DIAMETER (INCH.) : 0.2487 PARTICULATE WEIGHT (Front half mg) : ti.34 

ME T ER COEFFICIENT (Y) : G.972 PARTICUL ATE WrIGHT (Back nalf mg) : 20.2 

r'1TOT COEFFICIENT (Cp) : 0.8M STATIC PRcSSURE (in. H20) : •0 55 

GAS METER VOL.(Cu.Ft.) : :;6.16 PERCENT CO2 3 

BAROMETRIC PRESSURE 29.7 PERCENT 02 14 

PERCENT CO 0 

FOR CIRCULAR STACK FOR REC T ANGULAR STACK 

STACK DIAMETER (inch): 24.5 STACK L"cNGTH(inchs) : 

STACK AREA (Sq.Ft.) : 3.273856 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0.000337 S T ACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 3.273856 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 53.2366 

VOLUME OF WATER VAPOR (STD. CU .FT.): 4.3257 

FRAC T IONAL MOISTURE CONTENT {qo ): 0.0751 

DRY BASE: 79.0000 

MOLECULAR WT..OF STACK GAS (DRY BASE): 29.2000 

MOLECULAR W T. OF S T ACK GAS (WET BASE): 28.3583 

STACK PRESSURE (inch Hg): 29.6596 

STACK GAS VELOCITY (ft/sec.): 80.0786 

ACTUAL STACK GAS FLOW RATE (ACFM): 15729.9538 

STANDARD STACK GAS i=LOW RATE (SCFH): 498579.228 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0137 

PARTICULATE CONCENTRATION (LBS/SCF): 1.96E•06 

PARTICULATE EMISSION (LBS/HR): 0.9776 

BACK uALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0059 

PARTICULATE CONCENTRATION (LBS/SCF): 8.37E•07 

PARTICULATE EM1SSi0N (LBS/HR): 0.4171 

ISOKINETIC RATIO (aj'o): 103.6873 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 450 1.10 1.048809 2.20 76 76 

2 456 1.30 1.140175 2.60 79 76 

3 457 1.30 1.140175 2.60 81 77 

4 457 1.30 1.140175 2.60 82 78 

5 457 1.10 1.048809 2.20 81 78 

6 456 0. 032 0.959166 :.80 82 79 

7 456 i.20 1.095445 2.40 80 79 

8 A- 58 1.30 1.140175 2.60 83 79 

gt:r(:) 1.30 1.140175 2.60 83 80 

10 460 ;.20 1.095445 2.40 84 gl 

11 116: 1.00 1 2.00 84 81 

12 4.49 ;,ti.16 0.87178 i.50 86 32 

456.33333 1.0684 2.2917 81.6667 78.8333 80.2500 

2~ 
EMISSION TEST SUMMARY 

PLANT : r)a; iiylia. h.4,.is ~ oa_e ~ . Oy 

DATE : 13->'.pr-0h 

PLACE : i rim <<,iln i:.xtiaust 

RUN# : 2 

TEST DURATION (MINUTES) : oU LIQUID COLLECTED (mis) 

NOZZLE DIAMETER (lNC'-f.) : ',12=:87 PARTICULATE WEIGHT (Front half mg) : '.3.71 

iv1ETER COErFICIENT (Y) : 0 9. 2 PARTICULATE WEIGHT (Back half mg) : In'.():5 

PI'OT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : r-53 

GAS METER VOL.(Cu.Ft.) : 57.4:; PERCENT CO2 3 

BAROMETRIC PRESSURE 29.7 PERCENT 02 18 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 24.5 STACK LENGTH(inches) : 

STACK AREA (Sq.Ft.) : 3.273856 STACK WIDTH(inches) : 

NOZZLE AREA (feet): 0.000337 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 3.27 385-6 

FLowS 

SAMPLED VOLUME (STD. CU .FT.): 53.9239 

VOLUME OF WATER VAPOR (STD. CU .FT.): 4.4622 

FRACTIONAL MOISTURE CONTENT (%): 0.0764 

DRY BASE: 79.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.2000 

MOLECULAR WT. OF STACK GAS (WET BASE): 28.3440 

STACK PRESSURE (inch Hg): 29.6610 

STACK GAS VELOCITY (ft/sec.): 82.1520 

ACTUAL STACK GAS FLOW RATE (ACFM): 16137.2302 

STANDARD STACK GAS FLOW RATE (SCFH): 50B126.869 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0096 

PARTICULATE CONCENTRATION (LBS/SCF): 1.38E•06 

PARTICULATE EMISSION (LBS/HR): 0.7004 

BACK HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0052 

PARTICULATE CONCENTRATION (LBS/SCF): 7.38E•07 

PARTICULATE EMISSION (LBS/HR): 0.3750 

ISOKINETIC RATIO (%,): 103.0525 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 460 1.20 1.095445 2.40 82 82 

2 461 1.30 1.140175 2.60 85 82 

3 461 1.30 1.140175 2.60 86 82 

4 461 1.30 1.140175 2.60 87 83 

5 dC 3 1.20 1.095445 2.40 87 84 

6 458 0.87 0.932738 :.70 88 84 

7 460 1.20 1.095445 2.40 85 35 

8 461 1.30 1.140175 2.60 88 85 

9 463 1.30 1.140175 2.6C 89 85 

10 464 1.30 1.140175 2.60 90 86 

11 462 1.20 1.095445 2.40 90 8~ 

12 450 0.92 0.959166 1.80 90 37 

461.16667 1.0929 2.3917 87.2500 84.2500 85.7500 

30 
EMISSION TEST SUMMARY 

?LAN T. "`a? I:a? tc . ~,~ • ISf`•'.^ f~ ~) ~ 

DATE : 13-Apr.06 

PLACE : 7n:-n "'.i?r Exhau,t 

RUN# : 3 

TEST DURATION (MiNUTES) : 60 LIQUiD COLLECTED (mis) : 81.3 

NOZZLE DIAMETER (INCH.) : 0.2467 PARTICULATE WEIGHT (Front half mg) : 24.79 

M"c T rR COEFFICIENT (Y) : 0.972 PARTICULATE WE1GHT (Back half mg) : i 3.7 

PITOT COEFFICIENT (Cp) : 0.84 STATlC PRESSURE (in. H20) : •0,53 

GAS fvlE T ER VOL.(Cu.Ft,) : 56.998 PERCENT CO2 3 

BAROMETRIC PRESSURE . 29.7 PERCENT 02 . 1$ 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR S i ACK 

S T ACK DlAMETER (inch): 24.5 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 3.273856 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0.000337 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOVt N ABOVE: 3.273856 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 53.1727 

VOLUME OF WA T ER VAPOR (S'[D. CU.FT.): 3.8503 

FRACTIONAL MOIS T URE CON T ENT {%): 0.0675 

DRY BASE: 79.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.2000 

MOLECULAR WT. OF STACK GAS (WET BASE): 28.4438 

S TACK PRESSURE (inch Hg): 29:6610 

STACK GAS VELOCiTY (ft/sec.): 81.4302 

ACTUAL STACK GAS FLOW RATE (ACFN+): 15995.4449 

STANDARD STACK GAS FLOW RATE (SCFH): 507691.339 

PARTICULATE 

FRONT HALF 

PARTtCULATE CONCENTRATION (GR./SCF): 0.0072 

PAR i ICULATE CONCENTRATION (LBS/SCF): 1.03E•06 

PARTICULATE EMISSION (LBS/HR): 0.5219 

-BACK HALF 

PARTiCUt.ATE CONCENTRATION (GR./SCF): 0.0040 

PARTICULATE CONCENTRATION (LBS/SCF): 5.6$L•07 

PARTICULATE EMISSION (LBS/HR): 0.2884 

iSOKINETIC RATIO (%a }: 101.7038 

POINTS STACK T. DELTA P SQUAR D.P DELTA H. METER T. METER T. 

deg F INLET OUTLET 

1 462 1.20 1.095445 ' 2.40 87 87 

2 463 :.40 1.183216 2.80 88 87 

3 464 1.30 1.140175 2.60 89 87 

4 465 1.30 1.140175 2.60 90 88 

5 465 1.20 1.095445 2.40 C. 88 

6 455 0.78 0.883176 1.60 90 88 

7 462 1.20 1.095445 2.40 89 88 

8 e-65 1.40 1.183216 2.80 91 89 

9 464 1.30 1.140175 2.60 91 89 

10 466 1.20 1.095445 2.40 91 89 

11 466 1. : 0 1.048809 2.20 9°_ 89 

12 0.83 0.911043 1.70 92 90 

462.66667 1.0843 2.3750 89.9167 88.2500 89.0833 

'? I 
AppendiX' B 
Sheetl 

Summary of CO Analyzer CF 14-, ra:for.s arfcu Bias 

Plant: Daltile, Muskogee.. 

Source: Kiln Scrubber 

Date: 411212006 

Anafyzer Calibratrion Data 

Cylinder Analyzer Absolute % Span 

Value Response Difference 

Zero Gas 0 0.33 0.33 0.066 

Mid Range 200 200.3 0.3 0.06 

High Range 494 490.55 -3.45 -0.69 

System Calibration Bias and Drift Data 

Analyzer Initial Values Final Vaiues Drift Average 

Calibration System System System System Calibration 

Response Cafibration Calibration Calibration Calibration Values 

Response Bias Response Bias 

Run #1 Zero Gas 0.33 -0.03 -0.072 -0.45 -0.156 -0.084 -0.24 

Upscale 200.3 192.7 -1.52 193.63 -1.334 0.186 193.165 

Average CO Concentration: 157.28 

Corrected CO Concentration: 162.8913 

(Equation 6C-1) 

Run #2 Zero Gas 0.33 -0.45 -0.156 -3.68 -0.802 -0.646 -2.065 

Upscaie 200.3 193.63 -1.334 189.78 -2.104 -0.77 191.705 

Average CO Concentration: 148.67 

Corrected CO Concentration: 155.5814 

(Equation 6C-1) 

Run #3 Zero Gas 0.33 -3.68 -0.802 -4.95 -1.056 -0.254 -4.315 

Upscale 200.3 189.78 -2.104 187.63 -2.534 -0.43 188.705 

Average CO Concentration: 137.64 

Corrected CO Concentration: 147.0884 

(Equation 6C-1) 

Page 1 ~ 

.~ 
Sheetl 

Summary of NOx Analyzer Caiibrations and Bias 

Piant: Daltile, Muskogee, OK 

Source: Kiln Scrubber 

Date: 4/12/2006 

Analyzer Calibratrion Data 

Cylinder Anafyzer Absolute % Span 

Value Response Difference 

Zero Gas 0 0 0 0 

Mid Range 25.5 24.8 -0.7 -1.16667 

High Range 51 51 0 0 

System Ca{ibration Bias and Drift Data 

Anafyzer lnitial Values Final Vafues Drift 

Calibration System System System System 

Response Cafibration Calibration Calibration Calibration 

Response Bias Response Bias 

Run #1 Zero Gas 0 0 0 0.5 0.833333 0.833333 

Upsca(e 24.8 23.75 -1.75 23.8 -1.66667 0.083333 

Average NOx Concentration: 28.63 

Corrected NOx Concentration: 30.76259 

(Equation 6C-1) 

Run #2 Zero Gas 0 0.5 0.833333 0.6 1 0.166667 

Upscale 24.8 23.8 -1.66667 23.45 -2.25 -0.58333 

Average NOx Concentration: 29.91 

Corrected NOx Concentration: 32.4455 

(Equation 6C-1) 

Run #3 Zero Gas 0 0.6 1 0.85 1.416667 0.416667 

Upscale 24.8 23.45 -2.25 23.53 -2.11667 0.133333 

Average NOx Concentration: 30.5 

Corrected NOx Concentration: 33.35219 

(Equation 6C-1) 

Average 

Calibration 

Values 

0.25 

23.775 

0.55 

23.625 

0.725 

23.49 

Page 1 ~ ~ 
System Ca6ibration Bias and Drift Data 

AnafyZer Initial Va(ues Final Values Drift 

Calibration System System System System 

Response Catibration Calibration Calibration Calibration 

Response Bias Response Bias 

Run #1 Zero Gas 0.15 0.68 0.53 0 -0.15 

Upscale 49.7 46.63 -3.07 45.6 -4.1 

Average S02 Concentration: 1.29 

Corrected S02 Concentration: 1.033534 

(Equation 6C-1) 

Run #2 Zero Gas 0.15 0 -0.15 -0.25 -0.4 

Upscaie 49.7 45.6 -4.1 46 -3.7 

Average S02 Concentration: -0.12 

Corrected S02 Concentration: 0.005422 

(Equation 6C-1) 

Run #3 Zero Gas 0.15 -0.25 -0.4 -0.8 -0.95 

Upscale 49.7 46 -3.7 45.53 -4.17 

Average S02 Concentration: -0.08 

Corrected S02 Concentration: 0.478743 

(Equation 6C-1) 

Average 

Calibration 

Values 

-0.68 0.34 

-1.03 46.115 

-0.25 -0.125 

0.4 45.8 

-0.55 -0.525 

-0.47 45.765 

SlZeet1 

Summary of Sulfur Dioxide Analyzer Cafibrations and Bias 

PI«nt: Daltile, Muskogee, OrC 

Source: Kiln Scrubber 

Date: 4/12/2006 

Analyzer CaEibratrion Data 

Cylinder Analyzer Absolute % Span 

Va(ue Response Difference 

Zero Gas 0 0.15 0.15 0.15 

Mid Range 49.8 49.7 -0.1 -0.1 

High Range 100 99.8 -0.2 -0.2 

Page 1 P ~~ 
4/11/06 NOx Converter Check 

Date/Time NOx 

mm/dd/yy hh:mm:ss 

04/11/06 17:30:27 _ 

04/11 /06 17:31:27 ~ 

04/1 1106 1 7:32:27 

ippm 

0.039 

39.33594 

51 .277 

_ _ _Zero 

! - 

_ 

 _ _ 

NOx _ 

( 

51 ppm NOx 

04111/06 17:34:27 _ - 30.9961 

- 

04/11 /06 17:38:27 30.98389 

04111 /06 17:33:27 21.60938 ` 

04/11 /06 17:35:27 ^' 31.02686 

04/11 /06 17:36:27 30.99414 

04/11 /06 17:37:27 30.97949 

04/11 /06 17:39:27 30.91114 

~ 

- ----- -~------~ 

Start Converte_r C_heck 

..----- - ~----_ - - 

04/11 /06 17:40:27 J 30.92432 

04/11 /06 17:41:27 30.92286 ' 

04/11 /06 17:42:27 30.89356 

04/11 /06 17:43:27 30.90381 

04/11/0617:44:27 30.86866 

04/11 /06 17:45:27 30.87012 ( ~ 04/11 /06 17:46:27 ( 30.86085 

04/11/0617:47:27 ; 30.85401 -~ 

04/11 /06 17:48:27 30.86427 

04/11 /06 17:49:27 30.85157 

04/11 /06 17:50:27 30.85352 

04/11/06 17:51:27 30.833511 ( ' 

04111 /06 17:52:27 

04/11/0617:53:27 

04/11/06 17:54:27 

30.80665 

30.7671 

430.78565 

04/11 /06 17:55:27 30.76808 

04/11 /06 17:56:27 30.7715 

04/11/06 17:57:27 30.75734 

04/11 /06 17:58:27 30.779311 

04111 /06 17:59:27 30.74953 

04/11 /06 18:00:27 30.77931 

04/11 /06 18:01:27 30.7046 , ( 

04/11 /06 18:02:27 30.71339 

04/11/06 18:03:27 30.70119 _ Stop Converter Check 

04/11 /06 18:04:27 30.71094 - -^~ ( ~-~_-T~I 

Page 1 68 
4/12106 Calibraiions 

DaterTime VOC CO NOx S02 

mm/d&yy hh:mm:ss ppm ppm ppm PPm 

04112/06 08:22:16 1.4 0.0 0.0 0.0 

04112106 0822:26 1.3 

13.0 0.0 0.1 

04/12106 08:22:36 1.2 0.0 0.0 0.1 

04112/06 08:22:46 1.3 0.0 0.0 0.1 

04/12/06 08:22:56 1.4 0.0 0.0 0.1 

04112106 08:23:06 1.4 0.0 0.0 0.1 

04/12106 08:23:16 1.4 0.0 0.0 0.1 

04/12/06 08:23:26 1.3 0.2 0.0 0.1 

04112106 08:23:36 1.4 0.1 7.6 0.0 

04/12/06 08:23:46 1.4 0.1 23.8 0.1 

04/12/06 Oa:23:56 1.4 0.1 24.1 0.1 

04112/06 08:24:06 1.4 03 24.2 0.1 

04112/06 08:24:16 1.4 0.3 24.3 0.2 

04112/06 08:24:26 1.4 0.3 24.3 0.1 

04112/06 08:24:36 1.4 0.3 24.3 0.1 

04/12/06 08:24:46 1.4 0.3 24.4 0.1 

04/12/06 08:24:56 1.4 0.2 24.3 0.1 

04112/06 08:25:06 1.5 0.3 24.7 0.1 

04112/06 08:25:16 1.4 0.3 24.8 0.1 

04/12/06 08:25:26 1.4 0.3 24.8 0.1 

04l12/06 08:25:36 1.4 0.3 24.8 0.2 

04112/06 08:25:46 1.4 0.4 24.8 0.2 

04/12/06 08:25:56 1.3 0.3 24.9 0.2 

04/12/06 08:26:06 1.3 0.3 20.5 0.2 

04/12/06 08:26:16 1.3 0.6 0? 0.2 

04/12/06 08:26:26 1.3 0.4 0.1 0.1 

04/12/06 08:26:36 1.4 0.3 0.0 0.2 

04112106 08:26:46 1.4 0.2 0.0 0.1 

04/12/06 08:26:56 1.3 0.2 0.0 0.1 

04112/06 08:27:06 1.4 0.0 34.6 0.1 

04/12/06 08:27:16 1.4 0.1 50.6 0.2 

04/12/06 08:27:26 1.4 0.2 50.9 0.1 

04/12/06 08:27:36 1.5 -0.1 50.9 0.1 

04/12/06 08:27:46 1.5 -0.1 50.9 0.1 

04/12/06 08:27:56 1.6 0.1 51.0 0.1 

04/12/06 08:28:06 1.5 0.1 51.0 0.2 

04/12/06 08:28:16 1.4 0.1 51.0 0.1 

04112106 08:28:26 1.5 0.2 51.0 0.2 

04112/06 08:28:36 1.5 0.2 41.1 0.2 

04/12/06 08:28:46 1.4 0.3 0.2 0.1 

04/12/06 08:28:56 1.2 0.4 0.1 0.1 

04/12106 0829:06 1.2 0.3 0.1 0.2 

04112/06 08:29:16 1.3 0.2 0.0 0.2 

04/12/06 08:29:26 1.3 0.3 0.0 0.2 

04112106 08:29:36 1.3 0.3 0.0 0.3 

04/12106 08:29:46 1.2 17.1 0.0 0.2 

04/12/06 08:29:56 1.2 172.0 0.0 0.2 

04/12/06 08:30:06 1.4 191.6 0.0 0.2 

04112/06 08:30:16 1.3 192.0 0.0 0.3 

04112/06 08:30:26 1.2 192.1 0.0 0.3 

04112/06 08:30:36 1.4 198.6 0.0 0.3 

04/12/06 08:30:46 1.3 196.7 0.0 0.2 

04/12/06 08:30:56 1.3 196.8 0.0 0.3 

04/12/06 08:31:06 1.4 195.6 0.0 0.2 

04112/06 08:31:16 1.4 195.8 0.0 0.3 

04/12106 08:31:26 1.4 196.1 0.0 0.4 

04/12106 08:31:36 1.3 200.2 0.0 0.3 

04/12106 08:31:46 1.3 200.3 0.0 0.3 

04/12/06 08:31:56 1.3 200.7 0.0 0.3 

04/12/06 08:32:06 1.3 206.7 0.0 03 

04/12/06 08:32:16 1.3 206.5 0.0 0.3 

04/12/06 08:32:26 1.3 196.9 0.0 0.4 

04/12/06 08:32:36 1.3 198.6 0.0 0.5 

04112/06 08:32:46 1.3 201.8 0.0 0.4 

04/12/06 08:32:56 1.4 199.9 0.0 0.3 

04112/06 08:33:06 1.3 200.4 0.0 0.4 

04112106 08:33:16 1.4 200.5 0.0 0.4 

04/12/06 08:33:26 1.3 200.4 0.0 0.4 

Zero NOx 

25.5 ppm NOx 

Zero CO, S02 

51 ppm NOx 

200 ppm CO 

Page 1 R ~ 
41 12106 Calibrations 

04112/06 08:33:36 1.3 181.3 0.0 0.4 

04/12/06 08:33:46 1.4 61.1 0.0 0.3 

04/12/06 08:33:56 1.3 0.7 0.0 0.3 

04112/06 08:34:06 1.3 0.4 0.0 0.3 

04112/06 08:34:16 1.4 0.3 0.0 0.3 

04/12/06 08:34:26 1.2 0.3 0.0 0.0 

04112/06 08:34:36 1.2 0.3 0.0 -0.1 

04/12/06 08:34:46 1.2 0.3 0.0 0.0 

04112106 08:34:56 1.3 0.2 0.0 0.0 

04/12/06 08:35:06 1.4 0.2 0.0 -0.1 

04/12/06 08:35:16 1.2 0.1 0.0 -0.1 

04/12/06 08:35:26 1.2 0.2 0.0 -0.1 

04/12/06 08:35:36 1.2 306.8 0.0 0.0 

04/12/06 08:35:46 1.2 486.4 0.0 0.0 

04/12/06 08:35:56 1.2 489.0 0.0 0.0 

04112/06 08:36:06 12 489.8 0.0 0.0 

04/12/06 08:36:16 1.2 490.5 0.0 0.0 

04/12/06 08:36:26 1.3 490.3 0.0 0.0 494 ppm CO 

04/12106 08:36:36 1.2 490.6 0.0 0.0 

04/12/06 08:36:46 1.1 490.8 0.0 0.0 

04/12/06 08:36:56 1.2 490.7 0.0 0.1 

04/12/06 08:37:06 1.2 366.9 0.0 0.1 

04112106 08:37:16 1.2 32.3 0.0 0.1 

04112106 08:37:26 1.3 1.6 0.0 0.0 

04/12106 08:37:36 1.2 0.3 0.0 0.0 

04112106 08:37:46 1.3 0.2 0.0 0.0 

04112/06 08:37:56 1.2 0.2 0.1 0.0 

04112/06 08:38:06 1.2 0.2 0.1 0.0 

04/12/06 08:38:16 1.2 0.2 0.1 0.1 

04/12/06 08:38:26 1.2 0.2 0.0 0.1 

04/12/06 08:38:36 1.2 0.3 0.0 0.1 

04112106 08:38:46 1.1 0.4 0.0 0.6 

04112106 08:38:56 1.1 0.2 0.0 14.4 

04112106 08:39:06 1.2 0.5 0.0 35.0 

04/12/06 08:39:16 1.1 0.6 0.0 44.7 

04/12/06 08:39:26 1.1 0.7 0.0 48.0 

04/12/06 08:39:36 1.2 0.5 0.0 49.0 

04112106 08:39:46 1.2 0.5 0.0 49.4 

04/12106 08:39:56 1.3 0.5 0.0 49.6 

04/12J06 08:40:06 1.2 0.5 0.0 49.9 

04/12106 08:40:16 1.3 0.6 0.0 50.0 

174/12/06 08:40:26 1.3 0.7 0.0 50.1 

04112106 08:40:36 1.4 0.7 0.0 50.1 

04112/06 08:40:46 1.4 0.6 0.0 50.1 

04/12/06 08:40:56 1.2 0.8 0.0 50.0 

04/12/06 08:41:06 1.3 0.6 0.0 49.8 

04/12/06 08:41:16 1.2 0.7 0.0 49.9 

04/12/06 08:41:26 1.2 0.7 0.0 50.0 

04/12/06 08:41:36 1.2 0.5 0.0 50.1 

04112106 08:41:46 1.1 0.5 0.0 50.1 

04/12/06 08:41:56 1.2 0.5 0.0 50.0 

04112/06 08:42:06 1.2 0.4 0.0 49.9 

04112106 08:42:16 1.1 0.3 0.0 50.1 

04/12/06 08:42:26 1.2 0.3 0.0 49.8 

04/12/06 08:42:36 1.2 0.3 0.0 49.7 

04/12/06 08:42:46 1.2 0.4 0.0 49.7 49.8 ppm S02 

04/12/06 08:42:56 1.1 0.4 0.0 49.7 

04112/06 08:43:06 1.2 0.3 0.0 49.7 

04112106 08:43:16 1.1 0.3 0.0 48.0 

04/12/06 08:43:26 1.1 0.3 0.0 31.9 

04112/06 08:43:36 1.0 0.3 0.0 13.4 

04/12/06 08:43:46 1.0 0.3 0.0 5.1 

04112/06 08:43:56 1.1 0.2 0.0 2.5 

04112106 08:44:06 1.1 0.0 0.3 19.4 

04112106 08:44 :16 1.2 0.2 0.4 63.6 

04112106 08:44:26 1.2 0.3 0.3 88.1 

04112/06 08:44:36 1.2 0.4 0.4 96.0 

04/12106 08:44:46 1.2 0.4 0.3 98.2 

04/12/06 08:44:56 1.2 0.4 0.3 98.8 

04/12/06 08:45:06 1.2 0.5 0.4 99.1 

04/12/06 08:45:16 1.1 0.6 0.3 99.3 

04112/06 08:45:26 1.1 0.7 0.3 99.5 

Page 2 6 lj 
4,12106 Caiibrations 

04/12106 08:45:36 1.1 0.6 0.4 99.5 

04112/06 08:45:46 1.1 0.5 0.3 99.6 

0411V06 08:45:56 1.1 0.5 0.2 99.6 

0412/06 08:46:08 1.1 0.4 0.3 99.6 

04/12106 08:46:16 1.1 0.3 0.3 99.7 

04112/06 08:46:26 1.1 0.3 0.3 99.8 

04/12106 08:46:36 1.1 0.3 0.3 99.8 100 ppm S02 

04/12l06 08:46:46 1.0 0.5 0.3 99.8 

04/12/06 08:46:56 1.1 0.4 0.3 99.8 

041 12106 08:47:05 1.0 0.3 0.3 99.8 

04112106 08:47:16 1.0 0.5 0.2 92.4 

04112/06 08:47:26 1.1 0.3 0.0 51.7 

04112/06 08:47:36 1.1 0.3 0.0 19.7 

04112/06 08:47:46 1.1 0.3 0.0 7.3 

04/12106 08:47:56 1.1 0.3 0.0 3.3 

04/12106 08:48:06 1.1 0.3 0.0 2.0 

04/12/06 08:48:16 1.1 0.3 0.0 1.5 

04112/06 08:48:26 1.1 0.3 0.0 1.2 

04/12106 08:48:36. 1.2 0.2 0.0 1.2 

04112/06 08:48:46 1.1 0.2 0.0 1.1 

04112/06 08:48:56 1.1 0.3 0.0 1.0 

04/12/06 08:49:06 0.4 0.3 0.0 0.9 

04!12/06 08:49:16 0.1 0.3 0.4 0.8 

04/12/06 08:49:26 0.1 0.2 6.4 0.8 

04/12/06 08:49:36 0.1 0.2 13.5 0.9 

04112106 08:49:46 0.1 0.1 18.2 0.9 

04112106 08:49:56 0.1 0.0 20.8 0.7 

04112/06 08:50:06 0.2 -0.1 22.1 0.6 

04/12/06 08:50:16 0.2 -0.2 22.7 0.6 

04/12/06 08:50:26 0.2 -0.2 23.1 0.5 

04/12106 08:50:36 0.2 -0.1 23.2 0.5 

04/12/06 08:50:46 0.2 -0.1 23.4 0.5 

04/12/06 08:50:56 0.2 -0.2 23.6 0.5 

04112/06 08:51:06 0.2 0.0 23.7 0.5 

04112106 08:51:16 0.1 -0.1 23.7 0.7 

04/12/06 08:51:26 0.2 0.0 23.7 0.7 

04/12/06 08:51:36 0.2 -0.1 23.7 0.6 25.5 ppm NOx Bias 

04/12/06 08:51:46 2.9 -0.1 23.8 0.6 Zero CO. S02 Bias 

04/12!06 08:51:56 0.1 0.1 23.8 0.6 

04/12106 08:52:06 0.1 0.2 23.7 0.6 

04112/06 08:52:16 0.1 0.2 23.8 0.6 

04112106 08:52:26 0.6 0.2 23.4 0.6 

04/12/06 08:52:36 0.2 11.6 22.1 0.5 

04/12/06 08:52:46 0.1 82.7 14.2 0.6 

04/12/06 08:52:56 0.2 139.4 6.5 0.5 

04/12/06 08:53:06 0.1 166.4 3.1 0.5 

04/12/06 08:53:16 0.1 178.1 1.7 0.4 

04/12/06 08:53:26 0.0 183.4 1.1 0.3 

04/12106 08:53:36 0.1 186.0 0.8 0.5 

04112/06 08:53:46 0.1 187.7 0.6 0.5 

04/12106 08:53:56 0.1 189.0 0.4 0.5 

04/12/06 08:54:06 0.1 189.9 0.3 0.6 

04/12J06 08:54:16 0.1 190.6 0.2 0.6 

04112106 08:54:26 0.1 191.3 0.1 0.5 

04/12/06 08:54:36 0.1 191.6 0.1 0.5 

04112106 08:54:46 0.1 191.9 0.1 0.5 

04112/06 08:54:56 0.1 192.0 0.0 0.5 

04/12/06 08:55:06 0.1 192.2 0.1 0.5 

04/12/06 08:55:16 0.1 192.3 0.1 0.5 

04!12106 08:55:26 0.2 192.5 0.0 0.5 

04/12/06 08:55:36 0.2 192.6 0.0 0.5 200 ppm CO Bias 

04112/06 08:55:46 0.2 192.7 0.0 0.4 Zero NOx Bias 

04/12/06 08:55:56 0.2 193.0 0.0 0.5 

04112/06 08:56:06 0.3 190.3 0.0 0.5 

04/12/06 08:56:16 0.1 170.8 0.0 0.5 

0412/06 08:56:26 0.1 102.1 0.1 0.5 

04/12/06 08:56:36 0.1 48.0 0.1 0.8 

04/12/06 08:56:46 0.1 24.1 0.0 3.6 

04112106 08:56:56 0.1 14.4 0.1 9.9 

04112!06 08:57:06 0.1 9.3 0.0 16.6 

04/12106 08:57:16 0.1 6.8 0.0 21.8 

Page 3 71 
4112106 Calibrations 

04112r06 08:57:26 0.1 5.4 0.0 25.8 

041't 2106 08:57:36 0.1 4.5 0.0 29.0 

04/12/06 08:57:46 0.1 3.6 0.0 31.5 

04/12/06 08:57:56 0.1 2.8 0.0 33.5 

04/12/06 08:58:06 0.1 2.2 0.0 35.1 

04112106 08:58:16 0.0 2.0 0.0 36.4 

04/12/06 08:58:26 0.0 1.6 0.0 37.8 

04112/06 08:58:36 0.0 1.2 0.0 38.7 C~/12106 08:58:46 0.0 1.0 0.0 38.5 

04112106 08:58:56 0.1 0.9 0.0 40.3 

04112/06 08:59:06 0.1 0.7 0.0 41.1 

04/12/06 08:59:16 0.2 0.5 0.0 41.7 

04112/06 08:59:26 0.1 0.4 0.0 42.2 

04l12/06 08:59:36 0.2 0.4 0.0 42.6 

04112/06 08:59:46 0.1 0.5 0.0 43.0 

04112/06 08:59:56 0.1 0.3 0.0 43.5 

04112/06 09:00:06 0.0 0.3 0.0 43.9 

04112/06 09:00:16 0.1 0.2 0.0 44.2 

04l12/06 09:00:26 0.1 0.1 0.0 44.6 

04112/06 09:00:36 0.1 0.1 0.0 45.0 

04112/06 09:00:46 0.1 0.2 0.0 45.2 

04/12/06 09:00:56 0.1 0.1 0.0 45.3 

04/12I06 09:01:06 0.2 0.1 0.0 45.5 

04112/06 09:01:16 0.1 0.1 0.0 45.7 

04/12106 09:01:26 0.1 0.2 0.0 45.8 1.1 4112106 09:01:36 0.1 0.2 0.0 45.8 

04/12/06 09:01:46 0.1 0.2 0.0 45.9 

04/12106 09:01:56 0.0 0.3 0.0 46.0 

04/12/06 09:02:06 0.0 0.3 0.0 46.1 

04112/06 09:02:16 0.1 0.2 0.0 462 

04/12106 09:02:26 0.1 0.2 0.0 46.3 

04/12106 09:02:36 0.1 0.1 0.0 46.4 

04/12106 09:02:46 0.0 0.1 0.0 46.4 

04f12106 09:02:56 0.1 0.0 0.0 46.5 

04/12/06 09:03:06 0.1 -0.3 0.0 46.7 49.8 ppm S02 Bias 

04/12/06 09:03:16 0.1 -0.1 0.0 46.7 

04112/06 09:03:26 0.1 -0.1 0.0 46.6- 

04/12106 09:03:36 0.5 -0.1 0.0 46.1 

04/12/06 09:03:46 119 0.1 0.0 45.3 

04/12/06 09:03:56 2.2 0.1 0.0 44.1 

04/12J06 09:04:06 2.2 0.2 0.0 42.7 

04112106 09:04:16 2.2 0.3 0.0 39.9 

04712106 09:04:26 0.4 0.3 0.0 35.3 

04112/06 09:04:36 0.0 0.4 0.0 30.2 

04112/06 09:04:46 0.0 0.3 0.0 25.2 

04/12/06 09:04:56 0.1 0.2 0.0 20.9 Zero Air 

04/12/06 09:05:06 0.1 0.3 0.0 17.3 

04/12106 09:05:16 0.1 0.3 0.0 14.6 

04112106 09:05:26 0.1 0.2 0.0 12.7 

04112/06 09:05:36 0.3 0.3 0.0 11.1 

04/12/06 09:05:46 0.5 0.3 -0.1 10.0 

04112/06 09:05:56 1.3 0.4 0.0 8.9 

04J12l06 09:06:06 2.2 0.3 0.0 8.0 

04112J06 09:06:16 2.2 0.5 0.0 7.4 

04/12/06 09:06:26 4.0 0.5 0.0 7.0 

04/12/06 09:06:36 37.4 0.5 0.0 6.9 

04/12/06 09:06:46 40.1 0.4 0.0 6.9 

04/12/06 09:06:56 40.1 0.4 0.0 6.6 

04/12106 09:07:06 40.1 0.3 0.0 6.3 

04112106 09:07:16 40.1 0.3 0.0 5.7 

04/12/06 09:07:26 40.8 0.3 0.0 5.3 

04112/06 09:07:36 40.9 0.3 0.0 5.0 

04/12/06 09:07:46 40.9 0.3 0.0 4.6 

04/12106 09:07:56 40.9 0.3 0.1 4.4 40.8 ppm CH4 

04/12106 09:08:06 41.0 0.4 0.0 4.0 

04112/06 09:08:16 41 .0 0.5 0.0 3.7 

04112/06 09:08:26 40.3 0.3 0.0 3.6 

04/12/06 09:08:36 33.1 0.3 0.0 3.5 

04/12l06 09:08:46 31.3 0.3 0.0 3.5 

04/12/06 09:08:56 10.5 0.3 0.0 3.4 

04/12/06 09:09:06 2.6 0.3 0.0 3.2 

72 

Pape 4 
4112106 Caiibratlans 

04112/06 09:09:16 4.3 0.4 0.0 3.0 

04/12/06 09:09:26 18.6 0.3 0.0 3.0 

04112106 09:09:36 19.2 0.2 0.0 2.9 

04112I06 09:09:46 19.2 0.2 0.0 3.0 '19.9 ppin CHy 

04/12/06 09:09:56 19.1 0.1 0.0 3.1 

04/12/06 09:10:06 19.1 0.1 0.0 3.1 

04/12/06 09:10:16 19.1 0.2 0.0 2.9 

04112l06 09:10:26 17.7 0.3 0.0 2.8 

04112/06 09:10:36 15.1 0:3 0.0 2.8 

04112/06 09:10:46 13.1 0.3 0.0 2.7 

04/12/06 09:10:56 2.6 0.3 0.0 2.6 

04/12106 09:1 1:06 2.8 0.4 0.0 2.4 

04/12106 09:1 'i :16 2.5 0.5 0.0 2.3 

04/12106 09:11:26 2.5 0.4 0.0 2.5 

04l12/06 09:11:36 2.6 0.4 0.0 2.4 

04l12/06 09:11:46 23.1 0.4 0.0 2.4 

04/12106 09:11:56 62.2 0.4 0.1 2.5 

04/12106 09:12:06 62.6 0.3 0.1 2.5 

04/12106 09:12:16 62.6 0.3 0.0 2.5 

04/12/06 09:12:26 62.7 0.3 0.0 2.5 

04/12l06 09:12:36 62.9 0.3 0.0 2.4 61.7 ppm CH4 

04112/06 09:12:46 62.9 0.2 0.9 2.3 

04/12/06 09:12:56 62.9 0.2 0.0 2.2 

04112106 09:13:06 57.6 0.3 0.0 2.1 

04/12/06 09:13:1 fi 48.4 0.3 0.0 2.0 

04/12/06 09:13:26 40.3 0.3 0.0 2.1 

04112/06 09:13:36 3.6 0.3 0.0 2.0 

73 

PagQ 5 
4112106 Run #1 

Date/'ffine VOC CO NOx S02 

mm/dd/yy hh:mm:ss ppm ppm ppm Ppm 

04112106 10:19:51 17.3 167.5 29.0 1.9 

Start Run #1 

04/12/0610:20:01 17.2 166.9 29.0 2.0 

04/12/0610:20:11 17.2 166.9 29.1 2.0 

04/12/0610:20:21 17.0 166.6 29.2 1.9 

341 12106 10:20:31 16.5 166.2 29.3 1.9 

04/12/0610:20:41 16.3 165.5 29.3 1.9 

04!12/0610:20:51 15.3 164.7 28.6 1.9 

04/12/0610:21:01 16.1 164.3 28.0 2.0 

04/12/06 10:21:11 16.1 164.0 28.1 1.9 

04/12/0610:21:21 16.5 164.1 28.4 2.0 

04/1210610:21:31 16.3 164.2 28.9 1.9 

04/12/0610:21:41 15.8 164.2 29.0 1.8 

04/12/0610:21:51 15.4 164.0 28.7 1.9 

04/12/0610:22:01 15.0 163.3 28.6 2.0 

04/12/0610:22:11 14.7 162.3 29.0 2.0 

0411210610:22:21 14.6 161.8 28.9 1.9 

04/12/0610:22:31 14.9 161.4 28.8 1.9 

04/12/0610:22:41 14.3 160.9 29.1 1.9 

04112/0610:22:51 13.8 160.3 30.0 1.7 

04112/0610:23:01 13.4 160.0 30.2 1.7 

04/1210610:23:11 13.0 159.7 29.8 1.8 

04 1 12106 10 :23 :21 12.7 159.1 29.3 1.7 

0411210610:23:31 12.6 158.5 29.1 1.7 

04/1210610:23:41 12.3 158.0 29.0 1.7 

04/1210610:23:51 12.1 157.9 29.0 1.7 

04/1210610:24:01 12.3 157.8 29.1 1.7 

04/12/0610:2411 12.9 157.6 29.1 1.7 

04112/0610:24:21 12.8 157.7 29.0 1.7 

04/12/0610:24:31 12.9 157.8 28.9 1.6 

04/1210610:24:41 12.7 158.0 28.8 1.6 

04/12/0610:24:51 12.6 158.2 28.7 1.8 

04/12/0610:25:01 12.7 158.3 28.9 1.8 

0411 2/06 1 0:25:11 12.9 158.5 28.8 1.8 

04112/0610:25:21 12.9 141.2 28.8 1.7 

04/12/0610:25:31 12.9 158.7 28.9 1.6 

04/12/0610:25:41 12.9 158.5 29.1 1.6 

04/12/0610:25:51 12.8 158.6 29.2 1.8 

04/12/0610:26:01 12.5 158.4 29.3 1.8 

0411210610:26:11 12.3 158.2 29.4 1.7 

04/12/0610:26:21 12.3 157.7 29.4 1.7 

04112/0610:26:31 12.3 157.5 29.5 1.6 

04112/0610:26:41 12.4 157.6 29.5 1.6 

04/12/0610:26:51 12.9 157.9 29.6 1.6 

04112/0610:27:01 13.5 158.2 29.6 1.6 

04/1210610:27:11 13.6 158.7 29.5 1.7 

04/1210610:27:21 13.8 160.2 29.5 1.7 

04112/0610:27:31 14.5 161.4 29.3 1.8 

04112/0610:27:41 14.8 162.6 29.2 1.6 

04/12/0610:27:51 15.0 164.3 29.1 1.6 

04112/0610:28:01 15.1 165.7 29.1 1.7 

0411210610:28:11 15.2 166.8 29.1 1.8 

04112/06 10:28:21 15.2 168.1 29.2 1.7 

04/12/0610:28:31 15.5 168.9 29.1 1.7 

04/12/0610:28:41 15.5 169.9 29.2 1.7 

04112/0610:28:51 15.4 170.9 29.1 1.8 

04/12l06 10:29;01 15.0 171.1 29.0 1.8 

04/12/0610:29:11 14.9 170.9 29.0 1.8 

04/12/0610:29:21 14.9 170.7 29.0 1.9 

04/12/0610:29:31 14.6 170.5 29.0 1.9 

04/12/0610:29:41 14.8 170.0 29.1 1.8 

04/12/0610:29:51 15.1 169.5 28.9 1.8 

04/12/06 10:30:01 15.2 169.3 28.9 1.8 

04112/0610:30:11 15.1 169.3 28.9 1.8 

0411210610:30:21 15.3 169.4 29.1 1.8 

04/12/0610:30:31 15.3 169.7 29.1 1.8 

04112/0610:30:41 15.4 169.9 29.1 1.8 

04/12/0610:30:51 15.5 '169.8 29.2 1.7 

04/1210610:31:01 15.4 169.8 29.1 1.7 

04l12/0610:31:11 15.0 169.9 29.1 1.8 

04112/0610:31:21 14.8 169.5 29.1 1.7 

74 

Page 1 
4/12106 Run #1 

04/12/06 10:31:31 14.3 169.7 29.1 1.7 

04/1210610:31:41 14.1 169.4 29.2 1.8 

04112106 10:31:51 13.6 169.0 29.3 1.8 

04/12/06 10:32:01 '1 3.5 168.6 29.3 1,7 

04/1210610:32:11 13.5 168.0 29.2 1.7 

0411210610:32:21 13.5 168.0 29.3 . 1.8 

04112/0610:32:31 13.7 168.2 29.4 1.9 

0411210610:32:41 13.7 168.5 29.4 1.8 

0411210610:32:51 13.5 168.7 29.2 1.8 

0411210610:33:01 13.5 168.8 29.2 1.7 

04/12/0610:33:11 13.3 168.6 29.1 1.7 

04112f0610:33:21 13.3 167.7 29.2 1.8 

04112/0610:33:31 13.5 167.8 29.2 1.8 

04/12/06 10:33:41 13.5 168.1 29.3 1.8 

04/1210610:33:51 13.4 168.2 29.4 1.8 

04112/0610:34:01 13.6 168.3 29.4 1.9 

04112/0610:34:11 13.7 168.5 29.3 1.8 

04/1210610:34:21 13.7 168.6 29.1 1.7 

0411210610:34:31 13.7 168.6 29.0 1.6 

04112/0610:34:41 13.6 168.0 29.1 1.7 

04/1210610:34:51 13.5 168.0 29.2 1.7 

0411210610:35:01 13.2 168.0 29.3 1.6 

04/1210610:35:11 13.0 168.2 29.4 1.7 

04/12/0610:35:21 13.2 168.4 29.3 1.7 

04112/0610:35:31 13.6 168.2 29.3 1.7 

04112/0610:35:41 13.8 168.7 29.2 1.7 

04/1210610:35:51 13.7 169.3 29.3 1.7 

04112/0610:36:01 13.6 169.8 29.4 1.7 

04/1210610:36:11 13.6 170.0 29.5 1.7 

0411210610:36:21 13.8 169.9 29.5 1.8 

04112/0610:36:31 14.1 169.6 29.4 1.8 

04/1210610:36:41 14.2 169.5 29.5 1.8 

0411210610:36:51 14.3 169.7 29.4 1.9 

0411210610:37:01 14.5 169.9 29.4 1.7 

04112l0610:37:11 14.9 170.3 29.4 1.7 

0411210610:37:21 14.7 170.4 29.5 1.7 

04112106 10:37:31 14.4 171.0 29.5 1.7 

04/1210610:37:41 14.3 171.0 29.5 1.6 

0411210610:37:51 14.5 170.8 29.6 1.6 

04/1210610:38:01 14.3 171.2 29.6 1.6 

0411210610:38:11 14.6 171.4 29.6 1.5 

04112/0610:38:21 15.4 171.7 29.6 1.5 

04l12/0610:38:31 15.7 171.3 29.6 1.5 

0411 2106 1 0:38:41 15.9 172.2 29.5 1.6 

0411210610:38:51 15.8 172.5 29.7 1.6 

04112/0610:39:01 15.8 173.0 29.6 1.6 

0411210610:39:11 15.6 173.4 29.6 1.5 

04/1210610:39:21 15.6 173.2 29.6 1.6 

0411210610:39:31 15.4 173.3 29.6 1.7 

04/12/0610:39:41 15.7 173.0 29.6 1.7 

04/1210610:39:51 15.6 172.5 29.6 1.7 

0411210610:40:01 15.5 171.9 29.7 1.8 

04112/0610:40:11 15.5 171.6 29.6 1.7 

04/1210610:40:21 15.2 171.3 29.7 1.6 

04112/0610:40:31 15.0 170.8 29.7 1.6 

04/1210610:40:41 14.8 170.5 29.8 1.7 

04112/0610:40:51 14.7 170.2 29.8 1.6 

04112/0610:41:01 15.1 170.0 29.8 1.7 

0411210610:41:11 15.7 170.1 29.8 1.8 

04112106 10:41:21 15.4 170 .2- 29.7 1.7 

04/12/06 10:41:31 14.8 170.0 29.8 1.6 

04/1210610:41:41 14.4 169.6 29.7 1.7 

0411210610:41:51 14.2 169.1 29.4 1.6 

04112/0610:42:01 14.1 168.6 29.3 1.6 

04112/0610:42:11 14.3 168.6 29.5 1.6 

04112/0610A2:21 14.2 168.3 29.5 1.6 

04/1210610:42:31 13.9 168.2 29.5 1.5 

0411210610:42:41 13.7 168.0 29.5 1.5 

04/12/0610:42:51 13.4 167.8 29.6 1.5 

04112/0610:43:01 13.1 167.6 29.6 1.5 

04/12/0610:43:11 12.8 167.6 29.7 1.6 

0419 210610:43:21 12.8 167.4 29.7 1.6 

04/1210610:43:31 12.8 167.5 29.7 1.6 

04/12/0610:43:41 13.1 167.6 29.7 1.5 

Page 2 ~ ~ 
4r12i06 Rutl :`.5 

0411210610:43:51 13.7 167.6 29.7 1.4 

04112/0610:44:01 15.4 167.0 29.7 1.5 

04/12/0610:44:11 15.7 166.9 29.7 1.5 

04/12J0610:44:21 15.8 168.0 29.7 1.5 

04l12/0610:44:31 15.5 168.6 29.6 1.5 

04112/0610:44:41 15.4 168.5 29.6 1.5 

04/12/0610:44:51 16.0 168.6 29.7 1.5 

04/12/0610:45:01 14.5 168.3 29.6 1.5 

0411210610:45:11 14.2 167.9 29.7 1.5 

04/12/06 10:45:21 14.3 167.5 29.8 1•5 

04/12/06 10:45:31 14.3 i 67.5 29.8 1.4 

04/12/0610:45:41 14.3 167.8 29.8 1.5 

0411210610:4S:51 14.3 168.2 29.8 1.5 

0411210610:46:01 14.1 168.7 29.8 1.4 

04/12/0610:46:11 14.1 168.8 29.7 1.4 

04112/06 10:46:21 14.2 169.1 29.7 1.6 

04112/0610:46:31 14.5 169.4 29.7 1.6 

04/12/06 10:46:41 14.6 170.1 29.6 1.5 

0411210610:46:51 15.0 170.6 29.4 1.4 

04/12/0610:47:01 15.8 171.9 29.4 1.5 

04/12/06 10:47:11 16.5 173.7 29.3 1.4 

04112/0610:47:21 17.2 175.0 29.2 1.3 

04/1210610:47:31 17.1 175.4 29.2 1.4 

04112/0610:47:41 17.1 175.4 29.4 1.5 

0411210610:47:51 17.0 175.3 29.5 1.5 

04112/06 10:48:01 16.7 175.1 29.6 1.5 

04112/0610:48:11 16.4 174.0 29.6 1.4 

04/12/0610:48:21 15.8 172.7 29.4 1.4 

04112/0610:48:31 15.5 170.0 29.5 1.4 

04112/0610:48:41 15.0 166.0 29.4 1.4 

04/1210610:48:51 14.4 160.0 29.5 1.3 

04/1210610:49:01 14.1 153.2 29.6 1.3 

04/12/0610:49:11 13.8 144.5 29.7 1.3 

04l12/0610:49:21 13.6 136.4 29.9 1.3 

04/1210610:49:31 14.0 128.1 30.2 1.3 

04/12l0610:49:41 14.5 121.8 30.4 1.4 

04/12/0610:49:51 14.5 114.7 30.7 1.4 

04/1 2106 10:50:01 14.4 108.6 31.0 1.3 

0 4/ 12/06 10: 50:11 14.0 104.1 31.3 1.3 

04/12/0610:50:21 13.4 99.7 31.6 1.2 

04/12/0610:50:31 12.8 96.4 31.8 1.2 

04/12/0610:50:41 12.3 94.1 32.0 1.1 

0411210610:50:51 12.3 92.1 32.0 'I.1 

04/12/06 10:51:01 12.4 90.1 32.3 1.1 

04/12/06 10:51:11 12.6 88.6 32.4 1.1 

04112/0610:51:21 12.9 88.1 32.6 1.2 

04112/0610:51:31 12.6 87.7 32.5 1.2 

0411210610:51:41 12.1 87.8 32.5 1.2 

04/1210610:51:51 11.9 88.5 32.3 1.2 

04/1210610:52:01 11.7 90.9 31.8 1.1 

04112/0610:52:11 11.5 94.6 31.3 1.1 

04/12/0610:52:21 11.6 98.4 30.9 1.2 

04112l0610:52:31 11.6 101.3 30.8 1.2 

04112J0610:52:41 11.6 103.4 30.8 1.2 

04J1210610:52:51 11.5 103.8 31.0 1.2 

04112106 10:53:01 11.5 101.6 31.0 1.3 

04/12/0610:53:11 11.2 98.1 31.2 1.3 

0411210610:53:21 10.8 95.4 31.2 1.3 

04/12/0610:53:31 10.7 95.0 30.9 1.1 

04/12/0610:53:41 10.8 97.1 30.3 1.0 

04/12I0610:53:51 11.2 100.9 29.9 1.0 

04/12lO6 10:54:01 11.2 105.4 29.4 1.1 

04/12/0610:54:11 11.1 110.7 28.9 1.2 

04112/0610:54:21 10.9 115.9 28.6 1.2 

04112/0610:54:31 10.7 120.6 28.3 1.2 

0411210610:54:41 10.6 125.7 28.1 1.2 

04112/0610:54:51 10.8 131.1 27.9 1.2 

04/12/0610:55:01 10.9 135.4 27.8 1.3 

04/12/06 10:55:11 11.6 139.1 27.6 1.2 

04112/06 10:55:21 12.2 141.4 27.5 1.3 

04/12106 10:55:31 12.2 144.1 27.5 1.3 

04112/0610:55:41 12.6 146.2 27.3 1.3 

04/12/0610:55:51 12.6 148.7 27.2 1.4 

0411210610:56:01 12.9 150.9 27.1 1.3 

Page 3 76 
4112108 Run #1 

04112/0610:56:11 13.1 153.3 27.1 1.2 

04/12/06 10:56:21 13.3 156.1 27.1 1.1 

0411210610:56:31 13.6 157.9 27.1 1.1 

04112f0610:56:41 13.7 158.7 27.1 1.1 

0411210610:56:51 13.8 159.5 27.1 1.1 

0411210610:57:01 14.0 160.2 27.1 1.1 

04/1210610:57:11 13.7 159.4 27.1 1.1 

04/1210610:5721 13.6 158.9 27.1 1.2 

0411210610:5731 13.5 158.8 27.1 1.3 

04/12/0610:57:41 13.7 159.0 27.3 1.2 

04!1210610:57:51 13.9 159.3 27.2 1.2 

04!12f06 10:58:01 15.0 159.3 27.4 1.2 

04;12106 10:58:11 16.4 159.3 27.4 1.2 

04112/0610:58:21 17.0 159.4 27.5 1.2 

04112/0610:58:31 17.2 159.2 27.6 1.1 

04112/0610:58:41 17.2 158.6 27.6 1.1 

04/1210610:58:51 16.8 157.9 27.7 1.2 

04112/0610:59:01 16.3 157.4 27.6 1.2 

04112/0610:59:11 15.6 157.7 27.5 1.1 

04/12/0610:59:21 15.1 1S8.0 27.1 1.2 

04/12/0610:59:31 14.7 158.0 27.2 1.2 

04/1210610:59:41 14.3 158.0 27.4 1.1 

04/1210610:59:51 13.7 158.2 27.6 1.1 

04/12/06 11:00:01 13.1 158.1 27.7 1.2 

04/12/0611:00:11 12.4 158.0 27.9 1.2 

04112/0611:00:21 12.2 157.7 27.9 1.2 

04112/0611:00:31 12.2 157.3 27.8 1.2 

04112/0611:00:41 12.2 157.3 27.7 1.2 

04/1210611:00:51 12.4 157.2 27.7 1.2 

04/12/06 11:01:01 12.3 157.1 27.8 1.1 

04/12l0611:01:11 12.2 155.9 28.1 1.2 

04112/0611:01:21 12.1 154.9 28.5 1.2 

04112/0611:01:31 12.1 154.3 28.7 1.2 

04/12/06 11:01:41 11.9 154.6 28.7 1.1 

04112/0611:01:51 11.5 154.9 28.6 1.1 

04112/06 11:02:01 11.4 155.1 28.5 1.1 

04112/06 11:02:11 11.7 155.1 28.5 1.2 

04/1210611:02:21 11.7 154.9 28.4 1.1 

04/1210611:02:31 11.6 155.4 28.3 1.0 

04/12/0611:02:41 11.5 155.6 28.1 1.1 

0411 2106 1 1:02:51 11.3 155.8 28.2 1.2 

04/12/0611:03:01 11.1 155.7 28.1 1.2 

0411210611:03:11 11.0 155.4 28.1 1.1 

04/1210611:03:21 11.2 155.3 27.9 1.1 

04/12/06 11:03:31 11.4 155.1 28.0 1.1 

04/1210611:03:41 12.4 154.7 28.0 1.1 

04/12/0611:03:51 13.1 155.0 28.0 1.1 

04/1210611:04:01 13.5 155.5 28.0 1.1 

04/12/0611:04:11 13.6 155.8 28.0 1.1 

0411 2/06 1 1:0421 13.6 156.4 28.0 1.1 

04/12/0611:04:31 13.7 156.6 27.8 1.1 

04/1210611:04:41 13.9 157.3 27.8 1.0 

0411210611:04:51 14.0 157.7 27.8 1.0 

04112/0611:05:01 14.1 157.8 27.9 0.9 

0411210611:05:11 14.3 157.7 27.9 0.9 

04112/0611:05:21 14.3 157.7 27.9 1.0 

04/1210611:05:31 14.1 157.6 27.8 1.0 

04/12/0611:05:41 13.9 157.6 27.8 1.0 

04/12/0611:05:51 13.7 157.5 27.8 1.1 

04/1210611:06:01 13.8 157.4 27.8 1.1 

04/1210611:06:11 14.0 157.2 27.8 1.1 

04112/0611:06:21 14.1 157.0 27.9 1.0 

04112/0611:06:31 14.8 157.0 27.8 0.9 

04112/06 11:06:41 15.3 157.1 27.7 1.0 

04/12/0611:06:51 15.2 157.5 27.6 1.0 

04/1210611:07:01 15.5 157.6 27.6 0.9 

04112/0611:07:11 15.6 157.7 27.4 0.8 

0411210611:07:21 15.1 157.7 27.3 0.9 

04/1210611:07:31 14.9 158.0 26.9 1.0 

0411210611:07:41 15.1 158.3 26.5 1.0 

04/1210611:07:51 15.4 159.2 26.2 0.9 

0411210611:08:01 15.3 160.2 26.1 0.9 

04/1210611:08:11 15.0 161.0 26.0 0.9 

04/12106 11:08:21 14.7 161.2 25.9 1.0 

Page 4 77 
4112106 Run #1 

0411210611:0831 14.1 161.3 25.8 1.0 

04/12106 11:08:41 13.7 161.1 25.6 1.0 

04/12/0611:08:51 13.4 160.8 25.6 1.0 

04112/0611:09:01 12.9 160.7 25.6 0.9 

04112/0611:09:11 12.8 160.3 25.5 1.0 

04112106 11:09:21 13.4 161.2 25.6 1.0 

04/1210611:09:31 13.6 162.2 25.4 0.9 

04/12/0611:09:41 13.6 163.5 25.4 0.8 

04/1210611:09:51 13.6 164.3 25.5 0.8 

04112/0611:10:01 13.5 164.7 25.5 0.9 

04112/0611:10:11 13.1 157.3 25.3 0.7 

04/12/0611:10:21 13.4 165.9 25.3 0.6 

04112/0611:10:31 13.4 166.0 25.3 0.7 

04112/0611:10:41 13.4 166.2 25.2 0.7 

04/12/0611:10:51 13.4 166.3 25.2 0.8 

04/12/0611:11:01 13.5 166.5 25.1 0.8 

04/12/0611:11:11 13.2 166.7 25.1 0.8 

04112106 11:11:21 12.9 166.7 25.1 0.9 

04112l0611:11:31 12.4 166.5 25.1 0.9 

04/12f0611:11:41 12.4 166.4 25.0 0.9 

04112/0611:11:51 12.4 166.2 24.9 0.9 

04/12/0611:12:01 12.6 165.9 24.8 0.8 

0411210611:12:11 13.2 165.8 24.7 0.8 

04/12/0611:12:21 13.4 166.3 24.9 0.8 

04/12/0611:12:31 13.5 166.6 25.1 0.8 

0411210611:12:41 13.4 167.2 25.3 0.7 

04/1210611:12:51 13.5 168.3 25.7 0.7 

0411210611:13:01 13.6 168.6 26.1 0.7 

04/12/0611:13:11 14.0 168.1 26.6 0.7 

0411 2106 1 1:13:21 14.2 167.2 27.3 0.8 

04/12/0611:13:31 14.2 166.1 27.8 0.9 

04/12/0611:13:41 14.2 164.8 28.1 0.9 

04/1210611:13:51 14.1 163.2 28.3 0.8 

04112/0611:14:01 13.7 161.4 28.5 0.8 

04112/0611:14:11 13.5 160.0 28.4 0.8 

04/12/0611:14:21 13.5 159.0 28.1 0.8 

04/12/0611:14:31 13.5 158.5 28.1 0.8 

04/1210611:14:41 13.6 158.2 28.2 0.9 

04/12/06 11:14:51 13.6 157.8 28.4 0.9 

04/12/0611:15:01 13.9 157.8 28.5 0.7 

04/1210611:15:11 14.5 158.0 28.4 0.7 

0411210611:15:21 14.5 158.0 28.5 0.6 

04112/0611:15:31 14.2 158.2 28.5 0.7 

04/12/0611:15:41 14.3 .157.8 28.7 0.7 

04/12/0611:15:51 13.9 157.2 28.8 0.7 

0411210611:16:01 13.9 156.2 28.7 0.7 

04112/0611:16:11 14.1 155.4 28.6 0.6 

04/1 2106 1 1:16:21 14.2 155.2 28.6 0.6 

04/12/0611:16:31 14.5 155.2 28.5 0.6 

04/12/0611:16:41 14.7 155.6 28.3 0.7 

04/12/0611:16:51 14.7 155.9 28.0 0.7 

04/12/0611:17:01 14.3 156.1 27.6 0.6 

04/1210611:17:11 13.9 156.1 27.5 0.5 

04112100" 11:17:21 13.9 155.7 27.6 0.5 

04/12/0611:17:31 13.6 155.3 27.7 0.6 

04/1210611:17:41 13.6 155.0 27.7 0.6 

04/1210611:17:51 13.9 154.4 27.8 0.6 

04112/0611:18:01 14.3 154.6 27.8 0.7 

04112/0611:18:11 14.4 155.6 27.9 0.7 

0411210611:18:21 14.8 156.3 28.0 0.8 

04112/06 11:18:31 15.0 156.8 28.1 0.7 

04112/0611:18:41 14.6 157.0 28.2 0.6 

04/12/0611:18:51 14.6 156.6 28.3 0.7 

04/1210611:19:01 14.5 156.4 28.2 0.6 

04/1210611:19:11 14.9 155.8 28.3 0.6 

04/1210611:19:21 14.9 156.3 28.4 0.7 

04/1210611:19:31 14.6 156.9 28.3 0.7 

04/12/0611:19:41 14.1 157.4 28.3 0.5 

04112/0611:19:51 13.6 157.1 28.6 0.6 

04/12/0611:20:01 13.6 156.7 28.7 0.6 

04/12/0611:20:11 13.7 156.3 28.7 0.6 

04112/0611:20:21 13.6 157.0 28.7 0.6 

0411210611:20:31 13.4 157.0 28.3 0.6 

0411210611:20:41 13.7 156.8 28.1 0.6 

'7 g. 

Page 5 
4112105 Rnn #1 

04112/0611:20:51 13.7 157.2 28.3 0.6 

04112!06 11:21 :01 13.5 157.8 28.4 0.6 

04;12/05 11:21:11 13.3 158.5 28.4 0.5 

04.r1210611:21:21 13.4 158.6 28.5 0.5 

0411210611:21:31 13.5 158.5 28.4 0.4 

04/12/0611:21:41 13.7 158.3 28.4 0.5 

04/1210611:21:51 13.9 158.0 28.4 0.5 

04/12/0611:22:01 14.3 158.3 28.5 0.5 134/1210611:22:11 15.0 158.0 28.4 0.5 

04112/0611:22:21 15.8 157.6 28.3 0.4 

0411210611:22:31 16.2 157.1 28.2 0.5 

04/12/06 11:22:41 15.7 156.7 28.2 0.5 

04/12106 1 y:22:51 15.2 155.8 28.2 0.5 

Stop Run #1 13.92 157.28 28.63 1.29 

04l1210611:23:01 15.0 153.9 28.1 0.6 

04/1210611:23:11 14.8 151.1 28.1 0.6 

04/1 2106 1 1:23:21 14.8 147.5 28.1 0.5 

0411210611:23:31 15.5 144.5 28.1 0.5 

04/12/0611:23:41 15.8 142.4 28.2 0.5 

0411210611:23:51 15.8 141.5 28.3 0.5 

04/12/0611:24:01 16.0 141.2 28.3 0.5 

04/1210611:24:11 16.3 141.1 28.2 0.6 

04/1210611:24:21 15.9 141.6 28.1 0.6 

0411210611:24:31 15.9 141.7 28.1 0.6 

04/1210611:24:41 15.5 141.6 28.1 0.5 

04/1210611:24:51 15.2 141.4 28.2 0.5 

04/12/0611:25:01 15.2 121.9 28.3 0.4 

0411210611:25:11 15.4 141.8 28.4 0.4 

04/1210611:25:21 5.1 140.4 28.5 0.4 

04/12/0611:25:31 3.3 110.0 25.4 0.4 

04112/0611:25:41 3.4 62.4 17.0 0.4 

0411 2/06 1 1:25:51 3.9 35.6 12.1 0.2 

04/12/0611:26:01 3.3 20.6 10.2 0.1 

04/12/0611:26:11 3.2 12.6 8.8 0.1 

04/1210611:26:21 3.1 7.6 7.5 0.1 

0411210611:26:31 3.1 5.0 6.6 0.1 

04/12/06 11:26:41 3.1 3.3 7.4 0.1 

04/12/06 11:26:51 2.7 2.9 15.2 0.1 

04112/0611:27:01 2.2 1.7 20.2 0.1 

04112/0611:27:11 1.8 0.7 22.7 0.1 

04/12/0611:27:21 1.6 0.3 24.3 0.1 

04112/0611:27:31 1.2 0.2 25.3 0.1 

04112/0611:27:41 1.2 0.0 26.0 0.1 

04112/0611:27:51 1.2 -0.1 25.8 0.1 

04/12/0611:28:01 1.3 -0.1 23.2 0.0 

04J12/0611:28:11 1.6 -0.2 21.7 0.0 

04/12/0611:28:21 2.1 -0.1 20.7 0.0 

04/12/06 11:28:31 1.1 10.8 15.4 0.1 

04112/0611:28:41 0.9 81.1 8.6 0.1 

04112/0611:28:51 1.0 130.1 5.8 0.1 

04/1210611:29:01 1.0 155.0 4.6 0.0 

04/1210611:29:11 0.7 168.9 3.9 0.0 

04112/06 11:29:21 0.5 177.1 3.5 0.0 

04112/0611:29:31 0.8 182.7 3.2 0.0 

04/1210611:29:41 0.4 186.8 3.0 0.1 

04/12/0611:29:51 0.4 189.3 2.7 0.0 

0411210611:30:01 0.5 190.8 2.6 0.0 

04112/0611:30:11 0.6 191.6 2.4 0.0 

04112/0611:30:21 0.6 192.4 2.3 0.0 

0411210611:30:31 0.6 192.8 2.2 0.0 

04112106 11:30:41 0.6 193.0 2.1 0.0 

04/12/06 11:30:51 0.5 193.3 2.1 0.0 

04/12/0611:31:01 0.5 193.5 2.0 0.0 

04112/06 11:31:11 0.5 193.5 1.9 0.0 200 ppm CO 

04112/06 11:31:21 0.5 193.8 1.9 0.0 Zero S02 

04/12/06 11:31:31 0.4 193.7 1.8 0.0 

04112106 11:31:41 0.5 193.4 1.8 -0.1 

04/12/06 11:31:51 0.5 182.1 1.7 0.0 

04/12106 11:32:01 0.5 117.9 1.8 0.0 

04112/0611:32:11 0.4 64.1 1.7 0.0 

04/1210611:32:21 0.3 38.2 2.2 0.0 

Page 6 t~y 

! 9, 
4,' 12106 Rurt #1 

04/12i0611:32:31 0.3 24.1 3.9 0.5 

04112/0611:32:41 0.4 16.1 4.6 3.2 

04/1210611:32:51 0.3 10.4 4.0 7.5 

04/1210611:33:01 0.3 6.5 3.3 12.3 

04/12/0611:33:11 0.4 3.8 2.8 16.7 

04I1210611:33:21 0.4 2.2 2.4 20.5 

04/12/0611:33:31 0.4 1.0 2.1 23.6 

04112/0611:33:41 0.4 0.4 1.9 26:1 

04I1210611:33:51 0.4 0.2 1.8 28.3 

04112/0611:34:01 • 0.4 0.1 1.6 30.2 

04/1210611:34:11 0.3 -0.2 1.6 31.8 

04/12/0611:34:21 0.4 -0.4 1.6 33.2 

04112/0611:34:31 0.4 -0.5 1.5 34.5 

04/12/0611:34:41 0.4 -0.6 1.5 35.5 

04/1210611:34:51 0.3 -0.6 1.3 36.5 

04/12/0611:35:01 0.5 -0.4 1.3 37.4 

04/12/0611:35:11 0.3 -0.3 1.3 38.0 

04/12/0611:35:21 0.3 -0.4 1.3 38.6 

04/12/0611:35:31 0.5 -0.5 1.2 39.2 

04/12/0611:35:41 0.4 -0.3 1.1 39.9 

04/12/0611:35:51 0.4 -0.4 1.1 40.4 

04112/0611:36:01 0.4 -0.4 1.0 41.0 

04/12/0611:36:11 0.4 -0.6 1.0 41.4 

04/12/0611:36:21 0.3 -0.6 1.0 41.7 

04112/0611:36:31 0.3 -0.5 1.0 42.0 

04/1210611:36:41 0.4 -0.5 0.9 42.2 

04/1210611:36:51 0.4 -0.5 0.8 42.3 

04/12/0611:37:01 0.4 -0.5 0.8 42.5 

04/12/0611:37:11 0.3 -0.3 0.8 42.8 

04/12/0611:37:21 0.3 -0.4 0.8 43.0 

04112/0611:37:31 0.3 -0.5 0.7 43.1 

04/12/0611:37:41 0.3 -0.5 0.7 43.2 

04/12/0611:37:51 0.3 -0.5 0.6 43.3 

04/12/0611:38:01 0.3 -0.5 0.6 43.5 

04112/0611:38:11 0.2 -0.5 0.6 43.5 

04/12/0611:38:21 0.3 -0.3 0.6 43.5 

04112/0611:38:31 0.3 -0.3 0.6 44.4 

0411210611:38:41 0.3 -0.3 0.6 45.1 

04/1210611:38:51 0.3 -0.2 0.6 45.2 

04/1210611:39:01 0.4 -0.2 0.6 45.4 

04/1210611:39:11 0.2 -0.3 0.5 45.6 

04112/0611:39:21 0.3 -0.5 0.5 45.6 

04/1210611:39:31 0.3 -0.5 0.6 45.6 

04/12/06 11:39:41 0.2 -0.5 0.5 45.6 

0411210611:39:51 0.3 -0.5 0.5 45.5 

04112/0611:40:01 0.4 -0.6 0.5 45.4 

0411210611:40:11 0.5 -0.4 0.5 45.0 

04/12/0611:40:21 1.7 -0.3 0.5 44.1 

04/12/0611:40:31 2.6 -0.2 0.5 43.2 

04/12/0611:40:41 2.6 -0.1 0.5 42.9 

04/12/0611:40:51 2.5 -0.2 0.5 42.2 

04112/0611:41:01 1.5 -0.2 0.5 40.3 

04112/0611:41:11 0.4 -0.3 1.9 37.4 

0411210611:41:21 0.5 -0.7 10.6 33.6 

04/12/0611:41:31 0.6 -1.0 16.2 29.8 

04/12/0611:41:41 0.5 -1.1 19.1 26.3 

0411210611:41:51 0.6 -1.0 20.4 23.2 

0411210611:42:01 0.6 -1.0 21.3 20.6 

0411210611:42:11 0.5 -1.0 22.3 18.3 

04/1210611:42:21 0.5 -0.9 22.8 16.5 

04/1210611:42:31 0.6 -1.0 23.1 14.4 

0411210611:42:41 0.6 -1.0 23.5 12.7 

04/1210611:42:51 0.6 -1.0 23.6 11.1 

04/1210611:43:01 0.6 -1.2 23.7 9.9 

04/12/06 11:43:11 0.5 -1.1 23.7 8.9 

04/12/0611:43:21 0.5 -1.1 23.8 7.9 

04/12/0611:43:31 0.6 -1.1 23.8 7.3 

04112/0611:43:41 0.6 -1.2 23.8 6.7 

04/12/0611:43:51 0.6 -1.0 23.8 5.9 

04/12/0611:44:01 0.5 -0.7 23.8 5.3 

04/12/0611:44:11 0.6 -0.9 23.8 4.9 

04/12/0611:44:21 1.0 -0.7 23.6 4.5 

49.8 ppm S02 

Zero CO, NOx 

25.5 ppm NOx 

Page 7 80 
4112/06 Run V1 

0411210611:44:31 1.5 -0.7 21.7 4.1 

0411210611:44:41 2,7 -0.8 19.4 3.7 

04112106 1 1:44:51 2.9 -0.6 13.7 3.5 

04112105 '! 1:45:01 2.9 -d.4 6.8 3.3 

04112/06 'I 1:45:11 2.6 -0.3 3.4 3.1 

04112/06 1 1:45:21 0.6 -0.6 1.9 3.0 

04i 12l06 11:45:31 0.5 -0.6 1,3 3,0 

04/12/06 11:45:41 0.5 -0.7 1.0 2.9 Zero Air 

04112/0611:45:51 0.5 -0.5 0.8 2.7 

0411210611:46:01 0.4 -0.5 0.7 2.7 

0411210611:46:11 0.5 -0.5 0.6 2.5 

04/1210611:46:21 1.0 -0.4 0.6 2.3 

04/1210611:46:31 1.1 -0.3 0.5 2.1 

04/1210611:46:41 2.5 -0.4 0.5 2.0 

04/1210611:46:51 2.8 -0.3 0.4 1.9 

04112/0611:47:01 2.8 -0.4 0.4 1.7 

0411210611:47:11 2.8 -0.3 0.4 1.6 

04/1210611:47:21 14.1 -0.4 0.3 1.5 

04/12106 1 1:47:31 20.1 -0.7 0.3 1.6 

04/1210611:47:41 20.0 -0.7 0.3 1.6 

0411210611:47:51 20.1 -0.9 0.2 1.4 

04112lQ6 'I 1:48:01 19.9 -1.0 0.2 1.3 19.9 ppm CH4 

04l1210611:48:11 19.9 -1.1 0.2 1.1 

0411210611:48:21 20.1 -1.0 0.2 1.1 

04/1210611:48:31 19.0 -1.0 0.2 1.0 

04l1210611:48:41 15.9 -1.1 0.2 9.0 

Page 8 ~ ~ 
4112106 Run #3 

Date/T'tme VOC CO NOx S02 

mmldd/yy hh:mrn:ss ppm ppm ppm ppm 

04/12/0612:19:51 12.5 141.0 26.9 -0.1 

Start Run #2 

04/12/06 12:20:01 1230 141.1 27.3 -0.2 

041121061220:11 12.3 141.2 26.5 -0.3 

04112/0612:20:21 12.3 141.2 25.7 -0.4 

0411210612:20:31 12.4 141.4 25.8 -0.4 

0411210612:20:41 12.4 141.5 26.2 -0.3 

0411210612:20:51 12.3 141.4 26.3 -0.2 

04/12/06 12:21:01 12.3 141.4 25.5 -0.3 

04112/0612:21:11 12.4 141.3 24.8 -0.5 

04/1210612:21:21 12.8 141.3 25.0 -0.1 

04/1210612:21:31 13.1 141.2 25.6 0.0 

04/12/061221:41 13.4 141.3 26.1 0.0 

04/1210612:21:51 13.4 141.3 26.5 -0.1 

04/12/0612:22:01 13.2 141.3 26.6 -0.1 

04112J0612:22:11 12.8 141.2 26.8 0.0 

04/1210612:22:21 12.3 141.3 26.5 0.0 

04/12/0612:22:31 12.3 141.5 25.7 0.0 

04/1210612:22:41 12.7 141.9 25.0 0.0 

04/12/0612:22:51 13.3 141.8 25.3 0.0 

04/12/0612:23:01 13.5 142.2 26.1 0.0 

04112/0612:23:11 13.4 142.7 26.5 0.1 

0411210612:23:21 13.1 143.5 26.6 0.0 

04/1210612:23:31 13.1 143.7 26.7 0.0 

04112/0612:23:41 13.2 143.9 26.9 0.0 

04/12/0612:23:51 13.3 144.2 27.2 0.0 

04/12/0612:24:01 12.6 144.2 27.5 0.0 

0411210612:24:11 12.4 144.7 27.1 0.0 

0411210612:24:21 12.7 145.0 26.5 0.0 

04112/0612:24:31 12.8 144.9 26.7 0.0 

0411210612:24:41 12.5 144.6 27.2 0.0 

04/12/0612:24:51 12.3 144.1 27.6 0.0 

04112/0612:25:01 12.1 143.8 27.8 0.0 

0411210612:25:11 11.7 143.3 28.0 0.0 

04112/0612:25:21 11.7 142.8 27.7 0.0 

04112/0812:25:31 11.8 142.8 27.3 -0.1 

04112/0612:25:41 12.5 142.7 27.5 -0.1 

04/1210612:25:51 12.5 142.6 27.9 -0.1 

04/12/0612:26:01 12.3 142.4 28.2 -0.1 

0411210612:26:11 12.3 142.4 28.6 0.0 

04/1210612:26:21 12.7 142.4 28.9 0.0 

04112/0612:26:31 12.9 142.4 29.1 0.0 

04/12/0612:26:41 12.6 142.4 29.5 -0.1 

0411210612:26:51 12.3 142.3 29.7 -0.1 

04/1 2/00" 12:27:01 12.1 1412 29.7 -0.1 

04/12/0612:27:11 12.1 141.5 29.2 -0.1 

04/12/0612:27:21 11.8 ' 141.5 29.0 0.0 

04/1210612:27:31 11.6 141.4 29.1 -0.1 

04/12/0612:27:41 11.3 141.1 29.4 0.0 

04/1210612:27:51 10.7 140.9 29.6 -0.1 

04112/0612:28:01 10.5 140.8 29.8 -0.1 

04/1210612:28:11 10.5 140.6 29.9 -0.1 

0411210812:28:21 10.2 140.6 29.9 -0.1 

0411210612:28:31 10.7 140.7 30.0 -0.1 

04/12/0612:28:41 10.6 140.4 29.9 -0.1 

04/12/0612:28:51 10.5 140.4 29.7 0.0 

0411210612:29:01 10.6 140.4 29.3 -0.1 

04/1210612:29:11 10.5 140.3 29.3 -0.1 

04/12/0612:29:21 10.5 140.2 29.4 -0.1 

04/12/0612:29:31 10.6 139.8 29.7 -0.1 

04/1210612:29:41 10.6 139.8 29.8 -0.1 

04112/0612:29:51 10.6 139.6 30.0 -0.2 

04/1210612:30:01 10.6 139.4 30.2 -0.1 

04/1210612:30:11 10.6 139.0 30.4 0.0 

04/1210612:30:21 10.7 138.8 30.2 -0.1 

04/12/06 12:30:31 9 0.5 138.8 29.9 -011 

04112/0612:30:41 10.5 138.6 29.8 -0.1 

04/12/0612:30:51 10.6 138.4 29.8 -0.2 

0411210612:31:01 10.8 137.9 29.9 -0.2 

0411210612:31:11 11.2 137.5 30.0 -0.1 

0411210612:31:21 11.7 137.8 30.2 -0.1 

Page 1 82 
4112/06 Run #t3 

0411210612:31:31 12.2 137.9 30.4 -0.1 

04/1210612:31:41 12.2 138.3 30.4 0.0 

04/1210612:31:51 12.2 138.4 30.5 0.0 

34,1 12/06 i2:32:01 12.3 138.6 30.7 -0.1 

04112106 12:32:11 12.3 138.6 30.8 -0.1 

0411210612:32:21 12.3 137.9 30.8 0.0 

04/1210612:32:31 12.1 137.6 30.8 -0.1 

04/12/0612:32:41 11.8 137.3 30.6 -0.2 

04112/0612:32:51 11.7 136.7 30.3 -0.3 

0411210612:33:01 11.5 136.1 30.0 -0.2 

04112,10612:33:11 11.4 135.1 30.1 -0.2 

04112/0612:33:21 11.2 133.5 30.3 -0.1 

04112/0612:33:31 11.1 132.0 30.4 -0.1 

04112/0612:33:41 10.8 130.9 30.4 0.0 

0411210612:33:51 10.8 129.7 30.4 -0.1 

04112/0612:34:01 11.2 128.6 30.5 -0.1 

04/12/0612:34:11 11.5 127.7 30.8 -0.1 

04/12/0612:34:21 11.6 127.7 30.9 -0.2 

04112/0612:34:31 10.8 128.0 30.8 -0.1 

04112/0612:34:41 11.3 128.4 30.6 -0.1 

04112/0612:34:51 11.2 128.4 30.6 -0.2 

04/1210612:35:01 11.2 128.5 30.6 -0.2 

04112/0612:35:11 11.2 128.4 30.6 -0.1 

04/1210612:35:21 11.0 128.4 30.7 -0.1 

04112/0612:35:31 10.7 128.7 30.6 -0.2 

0411210612:35:41 10.3 128.9 30.6 -0.2 

04/1210612:35:51 10.2 128.8 30.5 -0.3 

04/12/0612:36:01 9.9 128.7 30.6 -0.3 

04112/06 12:36:1 i 9.6 128.4 30.7 -0.3 

04112/0612:36:21 9A 128.1 30.5 -0.3 

04112/0612:36:31 9.3 127.9 30.4 -0.3 

04/1210612:36:41 9.3 127.7 30.5 -0.3 

04/1210612:36:51 9.2 127.6 30.7 -0.3 

04/1210612:37:01 9.9 127.0 30.7 -0.3 

04/12/0612:37:11 9.9 127.8 30.7 -0.2 

04/12/0612:37:21 10.0 127.7 30.8 -0.2 

04/12/0612:37:31 10.0 127.9 30.9 -0.2 

04/1210612:37:41 10.1 127.5 31.0 -0.3 

04/1210612:37:51 9.9 127.7 31.1 -0.4 

04/12/0612:38:01 9.8 128.0 30.9 -0.3 

04112/0612:38:11 9.5 128.3 30.6 -0.2 

04112/0612:38:21 9.4 128.4 29.9 -0.3 

04112/0612:38:31 9.3 128.0 29.2 -0.4 

0411210612:38:41 9.4 127.9 28.8 -0.4 

04112/0612:38:51 9.1 127.9 29.0 -0.4 

04/12/0612:39:01 8.9 127.9 29.6 -0.4 

04/1210612:39:11 8.6 127.8 30.0 -0.4 

0411210612:39:21 8.7 127.3 30.4 -0.3 

04112/0612:39:31 8.8 127.1 30.4 -0.3 

04112/0612:39:41 9.1 126.8 30.6 -0.3 

04/12/0612:39:51 9.6 126:7 30.4 -0.2 

04/12/0612:40:01 10.0 127.4 30.2 -0.1 

04/1210612:40:11 10.4 128.3 30.0 -0.2 

0411210612:40:21 10.8 128.4 30.1 -0.1 

04/1210612:40:31 11.1 129.1 30.4 -0.2 

04112/0612:40:41 11.3 129.4 30.6 -0.2 

04/12/0612:40:51 11.6 129.4 30.6 -0.1 

04/12/0612:41:01 11.5 129.9 30.7 -0.1 

04112/0612:41:11 11.2 129.4 30.9 -0.1 

040'12/06 i 2:41:21 10.7 129.0 31.1 0.0 

0411210612:41:31 10.7 128.6 31.1 -0.1 

04112/0612:41:41 11.1 128.0 31.2 -0.1 

04/12/0612:41:51 10.9 128.1 31.2 -0.1 

04112/0612:42:01 11.3 127.5 31.0 -0.2 

04112/0612:42:11 11.5 126.9 30.6 -0.3 

04112/0612:42:21 11.5 127.0 30.4 -0.2 

04112/0612:42:31 11.8 127.2 30.6 -0.2 

04!1210612:42:41 12.3 127.2 30.7 -0.3 

04/1210612:42:51 12.1 127.7 30.8 -0.2 

0411210612:43:01 12.2 127.9 30.9 -0.1 

04/12/06 12:43:1 i 12.3 128.4 30.9 -0.1 

04/12/0612:43:21 12.3 128.6 30.9 -0.1 

0411210612:43:31 12.1 128.5 31.0 -0.2 

04/1210612:43:41 12.1 128.6 31.0 -0.2 

Page 2 C` ~ 
412106 Run #3 

04/1210612:43:51 11.7 129.2 30.9 -0.1 

04/12/0612:44:01 11.2 129.7 30.9 -0.1 

04/12/0612:44:11 11.0 129.6 30.6 -0.1 

04112/0612:44:21 11.1 129.8 30.5 -0.1 

0411210612:44:31 10.9 130.1 30.4 0.0 

0411210612:44:41 10.6 131.0 30.4 -0.1 

04112/0612:44:51 10.5 131.9 30.6 -0.1 

04/12/0612:45:01 10.3 132.3 30.8 0.0 

04112/0612:45:11 10.3 132.6 30.8 0.0 

04112/0612:45:21 10.4 132.6 30.8 -0.1 

04/12/0612:45:31 10.5 132.3 30.8 0.0 

04/1210612:45:41 10.4 132.6 30.7 0.0 

04/12/0612:45:51 10.4 132.8 30.7 0.0 

04/12/0612:46:01 10.2 132.9 30.7 0.0 

0412/0612:46:11 10.2 132.6 30.8 -0.1 

04112/0612:46:21 10.3 132.6 30.8 0.0 

04/12/0612:46:31 10.4 132.5 30.8 0.0 

04/12/0612:46:41 10.3 132.8 30.9 -0.1 

0411210612:46:51 10.3 133.1 31.0 0.0 

04/12/06 12:47:01 10.3 133.2 31.1 0.0 

04112/0612:47:11 10.2 133.6 31.1 0.0 

04/12/0612:47:21 10.0 134.0 31.1 -0.1 

04/1210612:47:31 9.6 134.3 30.5 0.0 

0411210612:47:41 9.4 134.3 30.1 0.0 

0411210612:47:51 9.6 134.6 29.9 -0.1 

04112/0612:48:01 9.5 135.2 29.7 0.0 

04/12/0612:48:11 9.7 135.8 29.9 0.0 

04112/06 12:48:21 10.0 136.7 30.0 -0.1 

04112/0612:48:31 10.1 138.0 30.3 -0.2 

04112/0612:48:41 10.0 138.7 30.5 -0.2 

04/12/0612:48:51 10.1 139.3 30.7 -0.1 

04/1210612:49:01 10.3 139.4 30.8 -0.1 

0411210612:49:11 10.2 138.7 31.1 -0.1 

04112/0612:49:21 10.4 137.6 31.2 0.0 

04112/0612:49:31 10.6 136.9 31.3 0.0 

04/12/0612:49:41 10.6 136.3 31.3 -0.1 

04112/0612:49:51 10.6 136.0 31.1 -0.1 

0411210612:50:01 10.7 135.9 30.9 -0.1 

0411210612:50:11 10.7 135.7 31.0 -0.1 

04/1210612:50:21 10.6 135.5 31.1 -0.1 

04/12/0612:50:31 10.5 135.2 31.0 -0.1 

04112/0612:50:41 10.6 135.1 30.9 -0.1 

04112/0612:50:51 10.7 135.1 30.7 -0.1 

04/1210612:51:01 10.9 135.6 30.8 -0.1 

04/12/0612:51:11 11.4 135.8 30.9 -0.1 

04/1210612:51:21 11.5 136.3 31.1 -0.1 

04112/061251:31 11.6 136.6 31.2 -0.1 

04112/0612:51:41 11.7 136.6 31.2 -0.1 

04112/0612:51:51 11.6 136.7 31.3 -0.2 

04112/0612:52:01 11.1 136.6 31.2 -0.2 

04112/0612:52:11 11.2 136.7 30.9 -0.1 

04112/0612:52:21 11.4 137.1 30.6 -0.2 

0411210612:52:31 11.3 137.4 30.6 -0.2 

04/1210612:52:41 11.3 137.5 30.8 -0.2 

04/12/0612:52:51 11.3 137.7 31.0 -0.1 

04112/0612:53:01 11.3 137.5 31.0 -0.1 

0411210612:53:11 11.2 137.1 31.1 -0.1 

04/12106 12:53:21 10.8 136.7 31.1 0.0 

04/1210612:53:31 10.8 136.3 31.1 0.0 

04/1210612:53:41 10.6 136.3 31.0 0.0 

04112/06 12:53:51 10.9 136.4 31.1 0.0 

04112/0612:54:01 11.3 136.3 31.1 0.0 

04112/06 12:54:11 11.4 136.2 31.1 0.0 

04112106 12:54:21 11.3 136.3 31.1 0.0 

04/1210612:54:31 11.4 136.3 31.3 0.0 

04/1210612:54:41 11.1 136.7 31.4 0.0 

04112/0612:54:51 11.3 137.0 31.5 -0.1 

04112/0612:55:01 11.1 137.0 31.4 -0.1 

04/12/0612:55:11 10.7 136.7 31.3 0.0 

04112/06 12:55:21 10.5 137.2 31.1 0.0 

0411210612:55:31 10.5 137.5 31.0 0.0 

04112/0612:55:41 10.3 138.0 31.0 -0.1 

04/1210612:55:51 10.0 137.6 31.1 -0.1 

04/1210612:56:01 9.9 137.4 31.1 -0.1 

Page 3 

~ 

•~ 
4,'12/06 Run #3 

0411210612:56:11 9.8 137.0 31.1 -0.1 

0411210612:56:21 9.8 136.7 31.1 -0.1 

04/12106 12:56:31 9.8 136.7 31.0 -0.1 

04/1210612:56:41 10.0 136.6 31.1 -0.1 

04/1210612:56:51 10.5 136.1 31.1 -0,1 

04/1210612:57:01 10.6 136.4 31.1 -0.1 

04/1210612:57:11 10.7 136.6 31.1 -0.1 

04/12/0612:57:21 10.6 137.0 31.4 -0.1 

0411210612:57:31 10.1 137.2 31.4 -0.1 

04112106 12:57:41 10.1 136.9 31.0 -0.1 

04112/0612:57:51 10.1 136.4 30.7 -0.2 

0411210612:58:01 10.0 135.8 30.7 -0.1 

0411210612:58:11 10.0 135.1 30.8 -0.2 

0411210612:58:21 10.3 134.5 30.9 -0.2 

0411210612:58:31 10.3 134.1 30.9 -0.1 

04/12/0612:58:41 10.2 134.4 30.7 -0.1 

04/12/0612:58:51 10.2 135.2 30.3 -0.1 

0411210612:59:01 10.4 136.4 30.1 -0.1 

04112I0612:59:11 10.6 138.4 30.2 -0.1 

04112/0612:59:21 11.2 140.4 30.3 0.0 

04/12/0612:59:31 11.8 141.9 30.2 -0.1 

0411210612:59:41 12.6 144.7 30.0 -0.1 

0411210612:59:51 12.7 148.6 29.9 -0.2 

04/1210613:00:01 12.6 152.8 29.8 -0.2 

04/12/0613:00:11 12.8 155.8 29.4 -0.2 

04/1210613:00:21 13.5 158.0 29.2 -0.2 

04/12/0613:00:31 13.8 158.9 29.2 -0 2 

04112J0613:00:41 142 159.1 29.3 -0.2 

04/1210613:00:51 14.8 159.7 29.4 -0.1 

0411210613:01:01 153 160.7 29.5 -0.1 

04/1210613:01:11 15.7 162.4 29.6 -0.1 

04112/0613:01:21 15.6 163.8 29.6 0.0 

04112/0613:01:31 15.6 166.1 29.5 -0.2 

04112/0613:01:41 15.6 167.8 29.6 -0.2 

04112/0613:01:51 15.8 169.0 29.6 -0.2 

04/1210613:02:01 16.4 170.3 29.6 -0.2 

0411210613:02:11 16.5 171.2 29.7 -0.2 

04112/0613:02:21 16.2 171.9 29.6 -0.2 

04112/0613:02:31 16.3 172.7 29.3 -0.2 

04112/0613:02:41 16.5 173.6 29.1 -0.1 

04/12/0613:02:51 16.4 174.0 29.0 -0.1 

04/12/0613:03:01 16.4 174.4 29.2 -0.1 

04/1210613:03:11 16.7 174.8 29.4 -0.1 

04/1210613:03:21 16.5 174.7 29.5 -0.1 

04/1210613:03:31 16.2 174.7 29.5 -0.2 

04/12/0613:03:41 16.3 174.6 29.2 -0.2 

0411210613:03:51 16.3 174.3 28.9 -0.1 

04/1210613:04:01 16.4 174.3 29.1 -0.1 

04112/0613:04:11 16.5 174.2 29.3 -0.1 

04112/06 13:04:21 16.3 173.9 29.3 -0.1 

04/1210613:04:31 16.0 173.7 29.5 -0.1 

04/1210613:04:41 16.0 173.4 29.6 -0.2 

04112/0613:04:51 15.8 173.2 29.6 -0.1 

0411210613:05:01 16.0 172.9 29.6 -0.1 

04/1210613:05:11 16.0 172.6 29.7 -0.1 

04/12/0613:05:21 16.0 172.1 29.8 -0.1 

04112/0613:05:31 16.2 172.4 29.8 -0.1 

04/12/0613:05:41 16.2 172.9 29.7 -0.1 

04/1210613:05:51 16.4 173.6 29.8 -0.3 

0411210613:06:01 16.7 173.6 29.7 -0.2 

04/1210613:06:11 16.7 173.7 29.7 -0.2 

04112/0613:06:21 16.8 173.6 29.7 -0.2 

04112/0613:06:31 17.0 173.3 29.7 -0.2 

04112/0613:06:41 16.9 173.4 29.8 -0.2 

04/1210613:06:51 16.7 173.5 29.9 -0.1 

04112/0613:07:01 16.3 174.0 29.8 -0.3 

04112/0613:07:11 15.5 174.1 29.9 -0.2 

04/12/0613:07:21 15.0 173.7 29.8 -0.1 

04/1210513:07:31 14.8 173.7 29.9 -0.1 

0411210613:07:41 14.3 173.3 29.9 -0.1 

04/1210613:07:51 14.3 173.0 29.7 -0.1 

04112/0613:08:01 14.8 172.9 29.6 -0.1 

0411210613:0$:11 15.3 173.2 29.6 -0.1 

04/12/0613:08:21 15.5 173.7 29.7 -0.2 

Page 4 

a 
4112/06 Rur► #3 

04112/0613:08:31 15.8 174.0 29.8 -0.2 

04112/0613:08:41 15.9 174.4 29.9 -0.2 

0411210613:08:51 15.9 174.5 30.0 -0.2 

04/1210613:09:01 16.1 174.5 30.0 -0.3 

0411210613:09:11 15.9 174.5 30.0 -0.2 

0411210613:09:21 15.8 174.3 30.0 -0.1 

04112106 13:09:31 16.1 174.8 30.0 0.0 

0411210613:09:41 16.2 175.4 30.0 0.0 

04112/0613:09:51 15.6 175.4 29.8 0.0 

04/12/0613:10:01 15.4 175.2 29.6 -0.1 

04/1210613:10:11 15.0 175.1 29.6 -0.1 

04/1210613:10:21 15.3 175.5 29.5 0.0 

0411210613:10:31 15.7 175.7 29.5 -0.1 

04/1210613:10:41 15.9 175.8 29.7 -0.1 

0411210613:10:51 16.4 175.7 29.9 0.0 

04112/0613:11:01 16.7 174.8 30.0 0.0 

04112/0613:11:11 16.9 173.6 30.1 0.0 

04/12/0613:11:21 16.9 172.1 30.2 0.0 

04112/0613:11:31 16.8 171.0 30.2 0.0 

0411210613:11:41 16.7 170.7 29.9 -0.1 

0411210613:11:51 16.5 170.3 29.8 -0.1 

04/12/0613:12:01 16.5 170.1 29.7 -0.1 

04112/0613:12:11 16.6 169.8 29.6 0.0 

04/12/0613:12:21 16.8 169.5 29.7 0.0 

04/12/0613:12:31 17.1 170.0 29.8 -0.1 

04/12/0613:12:41 16.9 170.6 29.9 -0.1 

04/12/0613:12:51 16.6 170.7 30.3 -0.1 

04/12/0613:13:01 16.4 170.8 30.3 -0.1 

0411210613:13:11 16.5 170.3 30.3 -0.1 

0411210613:13:21 16.3 169.9 30.2 0.0 

04/12/0613:13:31 16.4 169.8 30.2 0.0 

04/12/0613:13:41 16.6 169.4 30.2 -0.1 

0411210613:13:51 16.9 169.5 30.2 -0.1 

04112/0613:14:01 17.0 170.1 30.1 -0.2 

04112/0613:14:11 17.1 170.3 30.2 -0.1 

04/12/0613:14:21 16.9 170.1 30.2 0.0 

04/12/06 13:14:31 16.6 170.2 30.1 0.0 

04/1210613:14:41 16.6 170.4 29.8 0.0 

04112J08 13:14:51 16.6 170.5 29.8 -0.1 

04/12/0613:15:01 16.8 170.8 29.7 0.0 

04112106 13:15:11 16.6 171.8 29.7 0.0 

0411210613:15:21 16.5 172.4 30.0 -0.1 

0411210613:15:31 16.2 172.7 30.2 -0.1 

04112/0613:15:41 15.7 172.3 30.2 0.0 

04112/0613:15:51 15.1 172.0 30.3 0.0 

04112/0613:16:01 14.6 172.0 30.2 0.0 

04112/0613:16:11 14.7 171.7 30.0 0.0 

04/12/0613:16:21 14.6 171.5 30.0 0.0 

04/12J0613:16:31 15.3 171.3 29.9 0.0 

04/1210613:16:41 15.3 171.2 30.0 0.0 

04/12/0613:16:51 15.3 171.4 30.1 -0.1 

04112/0613:17:01 15.4 171.4 30.0 -0.1 

04/1210613:17:11 15.4 171.7 29.9 -0.2 

04/12/0613:17:21 15.6 172.1 30.0 -0.2 

04/12/0613:17:31 15.6 172.4 30.1 -0.2 

0411210613:17:41 15.7 172.5 30.3 -0.1 

04112/0613:17:51 15.7 172.8 30.2 -0.1 

0411210613:18:01 15.8 172.5 30.3 -0.1 

04/12/06 13:18:11 16.0 172.5 30.4 0.0 

04/121061318:21 15.6 'l72.6 30.4 0.0 

0411210613:18:31 15.3 171.9 30.4 -0.1 

04112106 13:18:41 14.7 171.9 30.4 0.0 

0411210613:18:51 14.5 171.7 30.1 -0.1 

041121061319:01 14.5 171.8 30.0 -0.1 

0411210613:19:11 14.9 171.7 30.1 -0.1 

04112/0613:19:21 15.4 171.6 30.2 -0.1 

04112/0613:19:31 15.7 171.4 30.2 -0.1' 

04112/0613:19:41 15.6 171.7 30.3 0.0 

04/1210613:19:51 15.4 171.6 30.3 -0.1 

04/1210613:20:01 14.9 171.7 30.1 -0.1 

04112/0613:20:11 15.1 172.1 30.0 -0.2 

04112/0613:20:21 15.6 172.1 30.2 -0.1 

04112/0613:20:31 15.8 171.9 30.3 -0.1 

0411210613:20:41 15.8 171.8 30.1 -0.1 

RC) 

Page 5 
4112/06 Run #3 

0411210613:20:51 15.9 172.4 30.1 -0.2 

0411210613:21:01 15.9 173.0 30.1 -0.2 

04112/06 13:2'I :;1 15.6 173.0 30.2 -0.2 

04/1210613:21:21 15.0 172.7 30.2 -0.1 

0411210613:21:31 14.9 172.4 30.0 -0.1 

04/1210613:21:41 14.9 172.3 29.8 -0.1 

0411210613:21:51 15.2 172.3 29.8 -0.1 

04112/0613:22:01 15.7 171.8 29.9 -0.2 

0411210613:22:11 16.4 171.0 30.0 -0.2 

04/1210613:22:21 16.8 170.5 30.1 -0.2 

0411210613:22:31 16.9 170.3 30.1 -0.1 

0411210613:22:41 16.8 170.5 30.1 -0.1 

0411210613:22:51 16.8 170.9 29.9 -0.2 

Stop Run 02 12.80 148.67 29.91 -0.12 

04112/0613:23:01 16.7 171.3 29.8 -0.2 

0411210613:23:11 16.9 171.7 29.9 -0.1 

04/1210613:23:21 16.9 171.9 30.0 -0.2 

04112/0613:23:31 16.0 171.8 30.0 -0.2 

0411210613:23:41 6.6 167.7 29.8 -0.2 

0411210613:23:51 3.9 120.5 25.2 -0.2 

0411210613:24:01 3.3 66.1 15.7 -0.4 

04/1210613:24:11 2.1 37.7 11.0 -0.4 

04112/0613:24:21 1.5 21.3 8.2 -0.5 

0411210613:24:31 1.2 13.9 7.2 -0.5 

0411210613:24:41 1.2 7.6 7.3 0.0 

0411210613:24:51 1.6 3.0 7.0 1.9 

04112106 13:25:01 1.5 13.6 6.2 5.1 

04/1210613:25:11 1.1 79.9 5.4 8.3 

04/1210613:25:21 0.9 67.2 4.7 10.4 

04/12106 13:25:31 1.0 31.0 4.3 12.0 

04/12/06 13:25:41 0.9 14.2 4.1 14.3 

04l12/0613:25:51 0.9 7.1 3.8 17.2 

04/12/0613:26:01 0.7 3.3 3.6 20.1 

0411210613:26:11 0.7 1.3 3.5 22.7 

04l1210613:26:21 0.9 0.1 3.3 24.9 

04112J0613:26:31 0.8 -0.5 3.2 27.1 

04112{0613:26:41 0.7 -1.2 3.1 28.9 

04112/0613:26:51 0.5 -'1.$ 3.0 30.7 

04l12I0613:27:01 0.5 -2.0 2.9 31.9 

0417210613:27:11 0.5 -2.1 2.8 33.2 

04112/0613:27:21 0.5 -2.3 2.7 34.2 

04/12/0613:27:31 0.5 -2.5 2.6 35.1 

04/12/0613:27:41 0.6 -2.7 2.5 36.0 

04/12l0613:27:51 0.6 -2.7 2.4 36.9 

04112/0613:28:01 0.6 -3.0 2.3 37.6 

04112l0613:28:11 0.6 -3.1 2.3 38.2 

04/1210613:28:21 0.5 -3.2 2.2 38.7 

0411210613:28:31 0.7 -3.4 2.1 39.0 

04l1210613:28:41 0.6 -3.3 2.1 39.5 

04/12/06 13:28:51 0.5 -3.3 2.0 39.9 

04112/0613:29:01 0.8 -3.4 1.9 40.3 

04/1210613:29:11 0.5 -3.3 1.8 40.8 

04/1210613:29:21 0.4 -3.2 1.8 41.3 

04112/0613:29:31 0.4 -3.3 1.7 41.5 

04/1210613:29:41 0.5 -3.3 1.6 41.9 

04/12/0613:29:51 0.5 -3.4 1.5 42.2 

04/1210613:30:01 0.5 -3.4 1.5 42.3 

04/1210613:30:11 0.5 -3.4 1.5 42.5 

04/12/0613:30:21 0.5 -3.5 1.5 42.6 

04112/0613:30:31 0.5 -3.6 1.4 42.8 

0411210613:30:41 0.5 -3.5 1.4 42.9 

04/1210613:30:51 0.5 -3.6 1.3 43.2 

0411210613:31:01 0.5 -3.4 1.3 45.2 

04/12/0613:31:11 0.5 -3.4 1.2 45.4 

04/1210613:31:21 0.6 -3.4 1.2 45.6 

0411210613:31:31 0.6 -3.5 1.2 45.7 

04/1210613:31:41 0.6 -3.6 1.2 45.8 

04112/06 13:31:51 0.6 -3.6 1.1 46.0 

0411210613:32:01 0.6 -3.7 1.0 46.0 

04112106 13:32:11 0.6 -3.7 1.0 46.0 49.8 ppm S02 

04/12i06 13:32:21 0.6 -3.6 1.0 46.0 Zero CO 

87 

Page 6 
4112ro6 Rtl , #3 

04/1210613:32:31 0.6 -3.7 1.0 46.1 

04/12/0613:32:41 0.9 -3.5 1.1 45.7 

04/12/06 13:32:51 0.9 13.2 1.1 45.3 

04112/0613:33:01 0.9 89.3 1.0 45.1 

04112/0613:33:11 0.9 136.9 0.9 43.0 

04/1210613:33:21 0.9 159.3 0.8 39.0 

04/1210613:33:31 0.9 171.8 0.8 34.4 

04112/0613:33:41 0.9 177.9 0.7 30.1 

0411210613:33:51 0.7 161.8 0.7 26.4 

04112/0613:34:01 0.5 184.1 0.7 23.1 

04112/0613:34:11 0.8 186.1 0.7 20.3 

04/1210613:34:21 0.9 187.2 0.8 17.8 

04112106 13:34:31 0.9 188.0 0.7 15.7 

04112106 13:34:41 1.0 188.5 0.7 13.9 

04112J0613:34:51 1.0 189.0 0.6 12.3 

04/12/0613:35:01 0.8 189.3 0.6 10.9 

04112I0613:35:11 0.6 189.6 0.6 9.7 

04112/0613:35:21 0.5 189.8 0.6 8.7 

04112/06 13:35:31 0.5 189.9 0.6 7.7 200 ppm CO 

04/12/0613:35:41 0.7 189.8 0.6 7.0 Zero NOx 

04112/0613:35:51 0.8 189.6 0.6 6.2 

04/12/0613:36:01 0.9 189.8 0.5 5.4 

04/12/0613:36:11 0.9 190.0 0.5 4.8 

04/12/0613:36:21 1.0 183.7 0.5 4.3 

04/1210613:36:31 0.9 152.8 1.3 3.6 

04/1210613:36:41 0.6 83.4 9.5 3.3 

04/1210613:36:51 0.6 42.5 16.5 3.0 

04/12/0613:37:01 0.9 23.0 19.6 2.7 

04112106 13:37:11 0.9 13.7 21.1 2.5 

04/1210613:37:21 0.7 7.5 22.0 2.2 

0411210613:37:31 0.7 3.8 22.5 1.9 

04112/0613:37:41 0.7 1.8 22.7 1.6 

0411210613:37:51 0.6 0.3 23.0 1.5 

04/12/0613:38:01 0.6 -0.3 23.1 1.2 

04/12/0613:38:11 0.9 -1.1 23.3 1.0 

04/12/0613:38:21 0.6 -1.7 23.3 0.8 

04112/0613:38:31 0.5 -2.2 23.3 0.7 

04/12/0613:38:41 0.6 -2.6 23.4 0.6 

04/12/0613:38:51 0.7 -2.9 23.4 0.4 

04/1210613:39:01 0.6 -2.9 23.4 0.3 

04/12/06 13:39:11 0.6 -2.7 23.4 0.3 25.5 ppm NOx 

04112/06 13:39:21 0.8 -3.0 23.5 0.2 Zero VOC 

04112/0613:39:31 0.9 -3.0 23.5 0.1 

04/1210613:39:41 1.1 -3.1 23.3 0.1 

04/12/0613:39:51 1.9 -3.2 21.4 0.1 

04112/0613:40:01 2.9 -3.0 19.0 0.0 

04/1210613:40:11 2.8 -2.7 12.0 0.0 

04/12/0613:40:21 2.8 -2.9 5.8 0.0 

04/1210613:40:31 1.2 -3.2 3.0 0.0 

04/12l0613:40:41 0.7 -3.3 1.7 0.1 

04/12/0613:40:51 0.7 -3.4 1.2 02 

04/12/0613:41:01 1.0 -3.5 1.1 0.2 

04/12/0613:41:11 1.2 -3.5 0.9 0.1 

04112/0613:41:21 2.3 -3.7 0.8 0.1 

04/1210613:41:31 2.8 -3.4 0.8 0.1 

04/1210613:41:41 2.8 -3.2 0.7 0.1 

04/12/0613:41:51 11.8 -2.9 0.7 0.0 

04/12/0613:42:01 20.1 -3.0 0.6 0.0 

0411210613:42:11 20.2 -3.2 0.5 0.0 

04/12106 13:42:21 20.2 -3.4 0.5 0.0 19.9 ppm CH4 

04112/0613:42:31 20.2 -3.4 0.5 0.1 

04/12/0613:42:41 20.2 -3.4 0.5 0.1 

0411210613:42:51 20.2 -3.5 0.4 0.0 

04112/0613:43:01 18.1 -3.4 0.4 0.0 

0411210613:43:11 16.4 -3.3 0.4 -0.1 

04112/0613:43:21 8.7 -3.3 0.3 -0.2 

0411210613:43:31 3.0 -3.1 0.3 -0.3 

04112/06 13:43:41 2.9 -3.3 0.4 -0.3 Zero S02 

04/12/0613:43:51 3.0 -3.2 0.4 -0.2 

04/12/0613:44:01 3.0 -3.1 0.4 -0.2 

~ 

Page 7 
4112/06 Run 93 

DaSe,Tirne VOC CO NOx S02 

mmldd/yy hh:mm:ss ppm ppni pPm ppi-ii 

04/1210613:54:51 15.5 148.4 28.5 -0.5 

Start Run #3 

0411210613:55:01 15.5 147.8 28.7 -0.5 

04/12J0613:55:11 15.4 148.3 28.9 -0.5 

04!1210613:55:21 14.8 149.1 29.1 -0.5 

3411210613:65:31 14.4 149.8 29.0 -0.4 

04112/0613:55:41 14.1 150.3 28.7 0.0 

0411210613:55:51 14.0 150.8 28.4 0.0 

04112/0613:56:01 13.8 151.2 28.3 0.0 

04/12/0613:5611 13.8 151.4 28.6 0.0 

04/1210613:56:21 13.9 151.6 28.7 0.0 

04/1210613:56:31 13.6 152.1 28.5 -0.1 

0411210613:56:41 13.5 152.1 28.0 -0.1 

04112/0613:56:51 13.1 152.0 28.0 -0.1 

04/1210613:57:01 12.8 151.3 28.0 -0.1 

04/1210613:57:11 12.7 150.6 27.9 -0.1 

04/12/0613:57:21 12.4 149.8 27.9 -0.1 

04/1210613:57:31 12.0 148.9 27.9 -0.1 

0411210613:57:41 12.1 148.0 27.7 -0.1 

04/12/0613:57:51 12.4 147.6 27.3 -0.1 

04112/0613:58:01 12.4 147.2 27.5 -0.2 

04/12/0613:58:11 12.2 147.0 27.9 -0.1 

04112/0613:58:21 11.7 147.0 28.2 -0.2 

0411210613:58:31 11.2 147.0 28.3 -0.3 

04112/0613:58:41 11.4 147.3 28.2 -0.2 

04/1210613:58:51 11.6 148.1 28.5 -0.2 

04/1210613:59:01 11.9 148.6 28.8 -0.2 

04l1210613:53:11 12.5 148.8 29.1 -0.2 

04/1210613:59:21 12.4 149.5 29.0 -0.2 

04112/0613:59:31 12.4 150.2 28.3 -0.2 

0411210613:59:41 12.9 150.3 27.8 -0.3 

04/12/0613:59:51 13.3 149.7 28.2 -0.2 

04112/0614:00:01 13.2 149.1 29.0 -0.2 

04112/0614:00:11 13.3 149.0 29.4 -0.2 

04/12/0614:00:21 13.4 149.2 29.7 -0.2 

04/1210614:00:31 13.5 149.3 29.8 -0.2 

04/1210614:00:41 13.2 149.3 29.9 -0.3 

04/12/0614:00:51 13.3 149.0 29.8 -0.1 

0411210614:01:01 13.3 148.6 30.0 -0.1 

0411210614:01:11 13.0 148.3 30.0 -0.1 

04112/0614:01:21 12.9 147.5 30.1 -0.1 

04112/0614:01:31 12.8 147.1 30.3 -0.2 

04112/0614:01:41 12.3 146.6 30.4 -0.2 

0411210614:01:51 12.3 145.9 30.3 -0.1 

04/12/0614:02:01 13.2 145.8 29.8 0.0 

04/12/0614:02:11 13.5 145.8 29.9 0.0 

04112/0614:02:21 13.7 146.1 30.2 0.0 

04/12/0614:02:31 13.7 145.5 30.5 0.0 

04112/0614:02:41 13.5 145.3 30.7 0.0 

0411210614:02:51 13.4 145.1 30.6 0.0 

0411210614:03:01 13.5 144.5 30.5 0.0 

04112/0614:03:11 13.4 144.4 30.5 0.0 

0411210614:03:21 13.0 144.0 30.5 0.1 

04/12/0614:03:31 12.8 143.9 30.6 0.0 

04/1210614:03:41 13.1 143.7 30.4 0.0 

04/12/0614:03:51 13.1 143.5 30.5 -0.1 

0411210614:04:01 12.8 143.3 30.6 0.0 

04112/0614:04:11 12.3 143.0 30.9 0.0 

04112/0614:04:21 11.7 142.6 30.9 0.0 

0411210614:04:31 11.5 142.7 30.6 0.0 

04/1210614:04:41 11.7 142.7 30.2 0.0 

0411210614:04:51 12.1 142.6 30.3 -0.1 

04112/06 14:05:01 12.4 142.6 30.7 -0.1 

0411210614:05:11 12.4 142.7 31.0 0.0 

04/1210614:05:21 12.7 142.9 31.3 -0.1 

04112/0614:05:31 12.4 143.0 31.5 -0.1 

0411210614:05:41 12.3 143.0 31.5 -0.1 

0411210614:05:51 12.2 143.0 31.5 -0.1 

0411210614:06:01 12.1 142.6 31.5 0.0 

04112/0614:06:11 12.1 142.3 31.5 0.0 

0411210614:06:21 11.8 142.6 31.5 0.0 

®A 

Page 1 
4112/0v nun t#3 

04112/0614:06:31 11.6 142.8 31.5 0.0 

0411210614:06:41 11.1 142.8 31.5 -0.1 

04112106 14:06:51 10.8 142.6 31.2 -0.1 

04/12/0614:07:01 10.6 142.3 31.2 0.0 

04/1210614:07:11 10.5 142.2 31.3 0.0 

0411210614:07:21 10.4 142.4 31.4 0.0 

04/1210614:07:31 10.6 142.4 31.4 -0.1 

04/12/0614:07:41 10.9 142.2 31.5 0.0 

04112/0614:07:51 11.3 142.0 31.6 0.0 

04112/0614:08:01 11.4 142.3 31.6 0.0 

0411210614:08:11 11.4 142.2 31.7 0.0 

04112/0614:08:21 11.4 142.5 31.7 -0.1 

04/1210614:08:31 11.4 142.7 31.8 0.0 

04/1210614:08:41 11.4 142.8 31.8 -0.1 

04/12/0614:08:51 11.1 143.1 31.9 -0.1 

04/12/0614:09:01 11.0 143.5 31.8 0.0 

04/1210614:09:11 11.0 143.6 31.5 0.0 

0411210614:09:21 11.2 143.6 31.4 -0.1 

04/12/0614:09:31 11.4 143.7 31.5 -0.1 

04/12/0614:09:41 11.4 143.5 31.5 -0.1 

04/12/0614:09:51 11.3 143.6 31.7 -0.1 

04/12J0614:10:01 11.4 143.6 31.8 -0.1 

04112/0614:10:11 11.4 143.5 31.8 -0.1 

04112106 14:10:21 11.6 143.8 31.8 0.0 

04/12/0614:10:31 12A 144.1 31.8 -0.1 

04112/06 14:10:41 13.1 143.9 32.0 -0.1 

04112106 14:10:51 13.2 144.4 31.8 -0.1 

04/1210614:11:01 13.2 144.6 31.8 -0.1 

04112/0614:11:11 13.1 144.5 31.8 -0.1 

04/12106 14:11:21 13.1 144.1 31.8 -0.1 

04112/0614:11:31 12.8 143.7 31.8 0.0 

04112/0614:11:41 12.6 143.5 31.8 -0.1 

04/12/0614:11:51 12.9 143.4 31.5 -0.1 

0411210614:12:01 13.1 143.7 31.4 -0.2 

04/1210614:12:11 13.1 144.0 31.5 -0.1 

04/12/06 14:12:21 12.7 143.7 31.8 -0.1 

04112/0614:12:31 12.3 143.8 32.0 0.0 

04112/0614:12:41 11.8 143.5 32.0 0.0 

04/1210614:12:51 11.6 143.0 32.0 -0.1 

04112/0614:13:01 11.6 142.8 31.9 -0.1 

04/12/0614:13:11 11.7 142.6 31.9 -0.2 

04/12/0614:13:21 12.2 143.2 32.0 -0.1 

04/1210614:13:31 12.9 144.1 32.0 -0.1 

04/12/0614:13:41 13.3 144.6 32.2 -0.1 

04/12/06 14:13:51 13.4 144.1 31.9 -0.1 

04/12/0614:14:01 13.1 143.7 31.7 -0.2 

04/1210614:14:11 12.9 143.9 31.6 -0.1 

04/1210614:14:21 12.2 144.0 31.7 -0.1 

04/12/0614:14:31 12.0 143.6 31.9 -0.1 

04/12/0614:14:41 11.4 143.8 31.7 -0.2 

04/12/0614:14:51 11.5 143.8 31.3 -0.3 

0411210614:15:01 11.5 144.0 31.1 -0.2 

0411210614:15:11 11.7 144.2 31.3 -0.2 

04112/0614:15:21 11.6 144.5 31.6 -0.1 

04112/0614:15:31 11.9 144.3 31.8 -0.1 

04/1210614:15:41 12.0 144.1 31.9 -0.1 

04/1210614:15:51 12.2 143.7 31.9 -0.1 

04112/0614:16:01 12.5 143.8 31.9 0.0 

04/12/0614:16:11 12.9 143.6 31.9 0.0 

04112/0614:16:21 13.6 143.6 32.0 -0.1 

04/12/0614:16:31 13.7 143.7 31.7 -0.2 

04112/0614:16:41 13.8 143.7 31.8 -0.1 

0411210614:16:51 13.7 144.2 31.9 -0.1 

0411210614:17:01 13.6 144.5 32.0 -0.1 

04112/0614:17:11 13.4 144.7 32.1 0.0 

04/12/0614:17:21 13.3 144.5 32.1 0.0 

04/12/0614:17:31 13.0 144.7 32.0 0.0 

04112/0614:17:41 12.6 144.8 31.7 -0.1 

04/12/06 14:17:51 12.2 145.1 31.7 -0.1 

0411210614:18:01 11.9 145.2 31.9 -0.1 

0411210614:18:11 11.5 144.9 31.9 -0.1 

04112/0614:18:21 11.0 144.5 32.1 -0.1 

0411210614:18:31 10.6 143.8 32.2 -0.1 

04/12/0614:18:41 10.6 143.3 32.1 -0.2 

Page 2 

90 
4112106 Run #3 

0411210514:18:51 11.1 143.6 32.0 -0.2 

04112/0614:19:01 11.9 144.2 32.0 -0.2 

04112/0614:19:11 12.3 144.3 31.7 -0.1 

04112J0614:19:21 12.4 144.2 31.5 -0.1 

04/12/06 14:19:31 12.4 143.8 31.4 -0.1 

04112/0614:19:41 12.1 143.1 31.5 0.0 

04/12106 14:19:51 12.0 141.7 31.5 0.0 

0411210614:20:01 11.8 140.7 31.5 -0.1 

0411210614:20:11 11.8 138.3 31.5 -0.1 

0411210614:20:21 11.3 133.6 31.6 -0.1 

0411210614:20:31 11.2 126.8 31.7 -0.1 

04112/06 14:20:41 11.2 119.5 31.7 0.0 

04112/0614:20:51 11.4 111.4 31.8 -0.1 

04/1210614:21:01 11.6 104.7 31.9 -0.2 

04/1210614:21:11 11.7 100.7 31.9 -0.2 

04/1210614:21:21 11.9 98.3 31.7 -0.1 

0411210614:21:31 12.2 98.0 31.5 0.0 

04/1210614:21:41 12.2 99.8 31.2 -0.1 

04/1210614:21:51 12.4 102.8 30.8 -0.1 

0411210614:22:01 12.8 106.4 30.2 -0.2 

04/1210614:22:11 12.9 111.2 30.0 -0.2 

04/12/0614:22:21 13.1 115.7 29.9 -0.2 

0411210614:22:31 13.2 120.5 29.9 -0.1 

0411210614:22:41 12.6 123.6 30.1 -0.1 

0411210614:22:51 13.0 125.6 30.3 -0.1 

0411210614:23:01 13.4 127.6 30.4 -0.2 

04112/0614:23:11 14.1 129.0 30.7 -0.1 

0411210614:23:21 14.3 131.5 30.8 -0.2 

0411210614:23:31 14.2 133.3 30.9 -0.2 

04/121061423:41 14.6 134.4 31.0 -0.2 

04/12/0614:23:51 14.4 136.0 31.1 -0.1 

04/1210614:24:01 14.5 137.4 31.1 -0.1 

0411210614:24:11 14.5 138.8 31.2 -0.1 

0411210614:24:21 14.4 140.2 31.3 -0.1 

0411210614:24:31 14.3 141.2 31.4 -0.1 

04/1210614:24:41 14.5 142.4 31.4 -0.1 

0411210614:24:51 15.3 143.4 31.3 -0.1 

0411210614:25:01 15.5 144.6 31.3 0.0 

04/12/0614:25:11 15.5 145.8 31.4 -0.1 

04/12/0614:25:21 15.4 146.9 31.2 -0.1 

04/1210614:25:31 14.9 147.8 31.0 -0.1 

0411210614:25:41 15.0 148.4 30.8 -0.1 

04112/0614:25:51 14.2 93.0 30.4 -0.2 

04112/0614:26:01 14.6 149.3 30.6 -0.1 

04112/0614:26:11 14.8 149.7 30.5 -0.1 

0411210614:26:21 14.8 149.0 30.3 -0.1 

04/1210614:26:31 14.2 149.0 30.1 -0.1 

0411210614:26:41 13.9 149.5 29.7 -0.1 

04/12/0614:26:51 13.9 150.0 29.5 0.0 

04112/0614:27:01 14.0 150.4 29.4 0.0 

04/1210814:27:11 10.9 132.8 27.9 -1.3 

04/1210614:27:21 17.7 91.8 31.6 1.5 

04/12106 14:27:31 17.2 111.5 31.5 1.4 

04112f0614:27:41 20.0 161.0 32.7 2.1 

04112/0614:27:61 19.7 161.8 32.8 2.1 

04112/0614:28:01 19.2 160.6 32.8 2.1 

04112/06 1 4:28:11 18.9 158.3 32.8 2.0 

0411210614:28:21 13.3 145.3 30.2 -0.1 

0411210614:28:31 12.8 141.5 30.3 -0.1 

04/1210614:28:41 12.7 138.0 30.3 0.0 

04112/0614:28:51 13.1 133.6 30.0 0.0 

04/1210614:29:01 13.5 129.5 29.9 0.0 

0411210614:29:11 13.7 126.8 30.0 -0.1 

04/12/0614:29:21 14.1 124.8 30.3 -0.1 

0411210614:29:31 14.3 123.8 30.5 0.0 

0411210614:29:41 14.4 123.3 30.5 -0.1 

0411210614:29:51 14.7 123.2 30.6 -0.1 

04112/0614:30:01 14.8 123.6 30.6 -0.1 

04/12/0614:30:11 15.0 124.0 30.5 -0.1 

04/1210614:30:21 15.2 124.7 30.4 -0.1 

0411210614:30:31 16.0 125.6 30.4 -0.2 

04112/0614:30:41 16.4 126.5 30.5 -0.1 

04/12/0614:30:51 16.8 127.3 30.7 0.0 

0411210614:31:01 17.1 127.9 30.8 -0.1 

Page 3 9 1 
4!12/06 Rur, r,3 

04/1210614:31:11 17.1 128.5 30.7 -0.2 

04112l0614:31:21 17.0 128.7 30.6 -0.2 

0411210614:31:31 16.8 129.0 30.6 -0.3 

04112/0614:31:41 16.2 129.6 30.6 -0.2 

04112/0614:31:51 16.1 130.1 30.1 -0.2 

04/12/0614:32:01 16.2 130.6 30.0 -0.1 

04/1210614:32:11 16.5 130.9 30.2 -0.1 

04112/06 14:32 21 16.5 131.1 30.5 -0.1 

0411210614:3231 16.0 131.2 30.8 -0.1 

04112/0614:32:41 15.7 130,9 31.0 -0.1 

04/1210614:32:51 15.7 130.5 30.9 -0.1 

04112/0614:33:01 15.7 130.2 30.6 -0.2 

04/12/0614:33:11 15.8 130.2 30.6 -0.2 

04112/0614:33:21 16.4 130.4 30.4 -0.1 

0411210614:33:31 16.8 130.8 30.2 -0.1 

0411210614:33:41 16.7 131.5 30.3 -0.2 

04112/0614:33:51 16.9 131.6 30.2 -0.3 

04112/0614:34:01 17.2 131.8 30.1 -0.3 

0411210614:34:11 17.2 132.1 29.8 -0.2 

0411210614:34:21 17.1 132.2 29.8 -0.1 

04/12/0614:34:31 17.0 131.7 29.7 -0.1 

04/12/0614:34:41 16.4 131.1 29.6 -0.2 

04/12/0614:34:51 15.8 131.0 29.5 -0.1 

04/12/0614:35:01 15.5 131.0 29.0 -0.1 

04J12/0614:35:11 15.4 131.0 28.7 -0.1 

0411210614:35:21 15.2 130.5 26.8 -0.1 

04/12/0614:35:31 15.1 130.0 29.0 -0.1 

04112/0614:35:41 15.3 129.4 29.2 -0.2 

04/1210614:35:51 15.6 129.3 29.3 -0.3 

04/1210614:36:01 15.6 129.4 29.6 -0.2 

04/1210614:36:11 15.8 129.5 29.6 -0.1 

04/12/0614:36:21 16.3 130.0 29.8 -0.1 

04/1210614:36:31 16.3 131.2 29.8 -0.2 

04112/0614:36:41 16.3 131.9 29.9 -0.2 

04/1210614:36:51 16.2 132.5 30.0 -0.2 

04/12J0614:37:01 16.0 132.8 30.0 -0.2 

04/12/0614:37:11 16.0 133.2 30.0 -0.3 

04J12/0614:37:21 15.4 133.2 30.1 -0.3 

0411210614:37:31 15.6 133.1 29.8 -0.2 

04/12/0614:37:41 15.6 133.4 29.6 -0.3 

04/1210614:37:51 15.7 133.6 29.7 -0.1 

04/12/0614:38:01 15.6 133.3 29.7 -0.1 

04f1210614:38:11 15.5 133.1 29.7 -0.2 

04112/0614:38:21 15.7 132.9 29.8 -0.2 

04/1210614:38:31 16.0 132.1 29.6 -0.3 

04/1210614:38:41 16.3 131.7 29.4 -0.3 

04/1210614:38:51 16.4 131.6 29.0 -0.4 

04/12/0614:39:01 16.6 131.3 28.7 -0.4 

0411210614:39:11 17.1 131.6 28.2 -0.3 

0411210614:39:21 17.2 132.5 28.0 -0.3 

0411210614:39:31 17.3 133.6 28.0 -0.3 

04/1210614:39:41 17.8 134.4 28.0 -0.2 

0411210614:39:51 18.0 135.2 28.1 -0.3 

04/12/0614:40:01 18.7 135.8 28.2 -0.3 

04112/0614:40:11 19.2 136.3 28.3 -0.3 

04/12/0614:40:21 19.2 137.2 28.5 -0.2 

04/1210614:40:31 19.1 138.5 28.7 -0.1 

04/12/0614:40:41 19.1 139.8 28.8 -0.2 

04/12/0614:40:51 18.9 140.3 29.1 -0.3 

04112/0614:41:01 18.6 140.6 29.4 -0.4 

04/1210614:41:11 18.1 140.6 29.6 -0.1 

04112/0614:41:21 17.5 140.4 29.7 -0.1 

04112/0614:41:31 17.1 140.1 29.8 -0.1 

04/1210614:41:41 16.8 139.7 29.6 -0.1 

04/1210614:41:51 17.0 139.0 29.6 -0.1 

04112/0614:42:01 17.3 138.4 29.8 -0.1 

04112/0614:42:11 17.3 138.1 30.2 -0.1 

04/12J0614:42:21 17.5 137.3 30.6 -0.1 

04112/0614:42:31 17.7 136.8 31.0 -0.1 

0411210614:42:41 17.8 136.0 31.2 -0.1 

04112/0614:42:51 17.5 135.4 31.3 -0.1 

04/12/0614:43:01 17.3 134.9 31.1 -0.1 

04/12/0614:43:11 17.1 134.5 30.8 -0.1 

0411210614:43:21 16.7 134.6 30.6 -0.1 

Page 4 
4i12106 Run 93 

04/12/06 14:43:31 16.3 134. 2 30.8 0.0 

04/12/0614:43:41 15.9 133.8 30.9 0.0 

04/1210614:43:51 15.6 133.1 30.8 0.0 

0412/0614:44:01 15.1 132.2 30.8 0.0 

04d12/0614:44:11 15.0 131.3 30.7 0.0 

0411210614:44:21 15.1 130.9 30.5 0.0 

0411210614:44:31 15.4 130.5 30.7 0.0 

04112/0614:44:41 15.6 130.1 31.0 -0.1 

04112/0614:44:51 161 130.1 31.1 -0.1 

0411210614:45:01 15.7 130.3 31.1 -0.1 

04112/0614:45:11 14.8 130.8 30.7 0.0 

04/1210614:45:21 15.4 131.5 30.1 0.0 

04/1210614:45:31 15.5 132.4 29.9 0.0 

04/12/0614:45:41 15.8 133.3 30.1 0.0 

04112/0614:45:51 16.3 133.9 30.4 0.0 

04112/0614:46:01 17.0 134.2 30.8 0.0 

04/1210614:46:11 17.0 134.4 30.9 0.0 

04/12/0614:46:21 17.0 134.2 30.8 0.0 

04112/0614:46:31 17.0 133.8 30.8 0.0 

04112J0614:46:41 16.5 133.2 30.6 0.0 

04/12/0614:46:51 16.2 132.6 30.5 0.0 

04/12/0614:47:01 16.0 131.7 30.4 0.0 

0411210614:47:11 16.4 131.4 30.3 -0.1 

04112/0614:47:21 16.4 130.9 30.3 -0.1 

04112/0614:47:31 16.5 130.7 30.3 -0.1 

04;12/0614:47:41 17.2 130.6 30.2 -0.1 

0411210614:47:51 17.3 131.5 30.3 0.0 

04/12/0614:48:01 17.4 132.6 30.4 0.0 

04/1210614:48:11 17.9 133.8 30.3 -0.1 

04/1210614:48:21 18.0 134.6 30.3 0.0 

04/1210614:48:31 18.0 135.5 30.3 0.0 

04/1210614:48:41 18.2 136.1 30.1 -0.1 

04112/0614:48:51 18.5 136.7 30.1 -0.2 

04/12/0614:49:01 18.4 137.0 30.2 -0.1 

04/12/0614:49:11 17.8 137.3 30.1 -0.1 

04112/0614:49:21 17.5 137.7 29.6 0.0 

04112/0614:49:31 17.4 138.0 29.3 -0.1 

04/12/0614:49:41 17.4 137.9 29.5 0.0 

04/12/0614:49:51 17.4 137.8 29.8 0.0 

04/1210614:50:01 17.6 137.3 29.8 0.0 

04/1210614:50:11 17.7 137.1 30.0 -0.1 

04112/0614:50:21 17.9 137.0 30.2 -0.1 

04/12/0614:50:31 18.5 136.9 30.2 -0.1 

04112/0614:50:41 19.1 137,0 30.3 -0.2 

04112/0614:50:51 18.7 137.3 30.3 -0.1 

04/12/0614:51:01 18.4 137.5 30.2 -0.1 

04/12/0614:51:11 18.3 137.3 30.0 -0.1 

04/12/0614:51:21 182 136.8 30.0 -0.1 

0411210614:51:31 18.4 136.5 30.0 -0.1 

04112J0614:51:41 18.3 136.4 30.1 -0.2 

04112/0614:51:51 18.3 136.5 30.2 -0.2 

04/1210614:52:01 18.3 136.2 30.4 -0.1 

04/12/0614:52:11 18.0 135.9 30.5 -0.1 

04/12/0614:52:21 17.9 135.7 30.3 0.0 

0411210614:52:31 17.7 135.2 30.2 -0.1 

04/12/0614:52:41 17.4 134.4 30.2 -0.1 

04!1210614:52:51 17.1 134.0 30.4 -0.1 

04/1210614:53:01 16.9 133.3 30.5 -0.1 

04/12/0614:53:11 16.8 132.5 30.7 -0.1 

04/12/0614:53:21 16.8 132.0 30.8 -0.1 

04/12/0614:53:31 17.0 131.8 30.6 -0.1 

04/1210614:53:41 16.8 132.4 30.3 -0.1 

04112/0614:53:51 17.1 133.4 30.0 -0.2 

04/1210614:54:01 17.0 133.9 30.3 -0.3 

04112/0614:54:11 16.8 134.2 30.5 -0.2 

04/12/0614:54:21 16.6 134.6 30.4 -0.2 

0411210614:54:31 16.5 134.9 30.4 -0.1 

04/12/0614:54:41 16.5 135.1 30.4 -0.1 

04/12/0614:64:51 16.5 135.4 30.6 -0.2 

04/12/0614:55:01 16.4 135.4 30.7 -0.2 

04112/0614:55:11 16.2 135.1 30.9 -0.1 

04/12/0614:55:21 16.3 134.5 30.9 0.0 

04/1210614:55:31 15.9 133.8 31.0 -0.1 

04112/0614:55:41 15.6 133.3 30.9 -0.1 

Page 5 `-ti ~ 
4!12106 Run V3 

04/12/0614:55:51 15.5 132.8 30.9 -0.2 

04/12/0614:56:01 15.7 132.2 30.8 -0.2 

04112/0614:56:11 15.9 131.6 30.8 -0.2 

04/12/0614:56:21 16.4 131.2 30.9 -0.2 

04112/0614:56:31 16.3 131.3 30.9 -0.2 

04l12/0614:56:41 16.1 131.1 30.8 -0.2 

04/1210614:56:51 16.1 131.1 30.7 -0.1 

04112/0614:57:01 16.4 131.0 30.8 -0.1 

0411210614:57:11 16.4 130.7 31.1 -0.2 

0411210614:57:21 16.6 130.5 31.2 -0.1 

04/1210614:57:31 16.7 130.6 31.3 -0.1 

04/12/0614:57:41 16.8 131.3 31.3 -0.2 

04/12/0614:57:51 16.9 131.8 31.2 -0.1 

Stop Run #3 14.61 137.64 30.50 -0.08 

04/12/0614:58:01 11.5 131.9 31.0 -0.1 

04/12/0614:58:11 5.1 114.6 29.5 -0.2 

04/1210614:58:21 4.9 63.7 19.6 -0.3 

04/12/0614:58:31 4.2 31.6 12.5 -0.5 

04/12/0614:58:41 3.9 16.4 9.4 -0.6 

04/12/0614:58:51 5.6 8.1 7.6 -0.6 

04/12/0614:59:01 5.4 3.8 6.7 -0.7 

04/1210614:59:11 4.3 34.8 6.0 -0.7 

04112/0614:59:21 3.3 105.6 5.6 -0.7 

0411210614:59:31 2.8 141.4 5.1 -0.8 

0411210614:59:41 2.6 162.6 4.5 -0.7 

04/1210614:59:51 2.2 173.3 4.1 -0.5 

04112/0615:00:01 2.1 177.8 3.9 -0.6 

04112/06 15:00:11 2.0 180.7 3.7 -0.6 

04/12/0615:00:21 1.9 183.3 3.6 -0.7 

04/1210615:00:31 1.9 184.8 3.5 -0.8 

04/1210615:00:41 1.9 185.9 3.4 -0.9 

04/1210615:00:51 1.7 186.6 3.3 -019 

04/12/0615:01:01 1.8 187.1 3.2 -0.8 

04112/0615:01:11 1.5 187.4 3.1 -0.8 

04112/0615:01:21 1.4 187.4 3.0 -0.8 

04l12/06 15:01:31 1.4 187.6 3.0 -0.8 200 ppm CO 

04/12106 15:01:41 1.4 187.7 2.8 -0.8 Zero S02 

04/1210615:01:51 1.3 187.8 2.7 -0.8 

04/12/0615:02:01 1.3 180.3 2.7 -0.8 

04f1210fi 15:02:11 1.2 115.9 2.6 -0.9 

04/12/0615:02:21 1.1 56.0 2.8 -0.8 

04/12/0615:02:31 1.1 27.3 3.3 0.3 

0411210615:02:41 1.0 14.6 3.2 3.9 

04112/0615:02:51 1.0 8.7 2.8 8.8 

04112/0615:03:01 0.9 4.5 2.6 13.5 

04/12/0615:03:11 0.9 1.6 2.5 17.5 

04112/0615:03:21 0.9 0.2 2.4 20.8 

04/12/0615:03:31 0.9 -0.6 2.3 23.7 

04112/0615:03:41 1.0 -1.8 2.2 26.0 

04/12106 15:03:51 1.0 -2.6 2.1 27.8 

04/12/0615:04:01 0.9 -3.3 2.0 29.4 

04/12/0615:04:11 1.0 -3.6 1.9 31.1 

04112/0615:04:21 0.8 -3.9 1.9 32.3 

04112/0615:04:31 0.9 -4.2 1.8 33.4 

0411210615:04:41 1.0 -4.4 1.7 34.6 

04/12/0615:04:51 0.9 -4.7 1.7 35.3 

0411210615:05:01 1.0 -4.9 1.7 36.1 

0411210615:05:11 0.9 -4.9 1.6 36.8 

04/1210615:05:21 0.9 -4.9 1.6 37.6 

04112/0615:05:31 0.9 -5.0 1.5 38.3 

04/12/0615:05:41 0.9 -4.9 1.5 38.8 

04/12/0615:05:51 0.9 -5.1 1.5 39.4 

04/12/0615:06:01 1.0 -5.3 1.5 39.9 

04/12/0615:06:11 1.0 -5.2 1.4 40.5 

04/12/0615:06:21 1.0 -5.4 1.4 40.9 

04/12/0615:06:31 1.0 -5.1 1.3 41.3 

04/1210615:06:41 1.0 -4.9 1.3 41.5 

04/1210615:06:51 1.0 -5.1 1.3 41.7 

04/12/0615:07:01 1.0 -5.1 1.2 42.0 

04/1210615:07:11 0.9 -5.0 1.2 42.2 

04112/0615:07:21 0.9 -4.8 1.2 42.3 

Page 6 94 
4/12106 Run #3 

04/12/0615:07:31 0.7 -4.8 1.2 42.6 

04112/0615:07:41 0.9 -5.0 1.2 42.8 

0411210615:07:51 0.9 -4.8 1.2 42.7 

04; 12/06 15:08:01 0.7 -4.8 1.1 42.8 

04/12/0615:08:11 0.8 -4.7 1.1 43.0 

04/1210615:08:21 0.9 -4.9 1.0 43.7 

04/1210615:08:31 0.8 -4.8 1.0 44.4 

04!1210615:08:41 0.9 -4.9 0.9 44.4 

04,12106 15:08:51 1.0 -5.1 0.9 44.5 

04!12l0615:09:01 1.0 -5.0 0.9 44.8 

04!1210615:09:11 1.0 -4.9 0.8 45.1 

0411210615:09:21 1.0 -5.1 0.9 45.3 

04112/0615:09:31 0.8 -5.1 0.9 45.4 

04112/0615:09:41 0.5 -5.1 0.9 45.4 

04112/0615:09:51 0.9 -5.0 0.9 45.4 

04/12/06 15:10:01 0.9 -5.0 0.9 45.5 49.8 ppm S02 

04/12/06 15:10:11 0.9 -5.1 0.8 45.6 Zero CO, NOx 

04/12/06 15:10:21 0.9 -4.7 0.8 45.6 

0411210615:10:31 0.9 -4.7 0.8 45.4 

04/12/0615:10:41 1.3 -4.6 0.9 44.5 

04/1210615:10:51 2.8 -4.7 0.9 43.4 

04/12/0615:11:01 2.9 -4.6 0.9 42.8 

0411210615:11:11 2.8 -4.6 0.9 42.4 

0411210615:11:21 2.0 -4.7 0.9 40.8 

04/12/06 1 5:11:31 1.0 -4.8 2.0 37.6 

0411210615:11:41 1.0 -4.8 10.4 33.7 

04112/0615:11:51 1.0 -5.0 16.5 29.5 

04112/0615:12:01 0.9 -5.1 19.6 25.9 

0411210615:12:11 1.0 -4.9 20.9 22.7 

04/1210615:12:21 1.0 -5.1 21.7 20.0 

04/12/0615:12:31 1.1 -5.2 22.3 17.5 

04/12/0615:12:41 1.0 -5.0 22.7 15.5 

04/1210615:12:51 1.0 -5.1 22.9 13.7 

04/1210615:13:01 0.9 -4.8 23.1 12.0 

04/12/0615:13:11 0.9 -4.9 23.3 10.6 

0411210615:13:21 1.0 -5.1 23.3 9.2 

04112/0615:13:31 1.0 -5.3 23.4 8.1 

04112/0615:13:41 1.0 -5.4 23.5 7.3 

04/12/0615:13:51 1.0 -5.4 23.5 6.5 

04/12l0615:14:01 0.9 -5.3 23.5 5.7 

04/12/06 15:14:11 0.8 -5.5 23.5 5.0 25.5 ppni NOx 

04/12/06 15:14:21 1.0 -5.4 23.6 4.3 Zero VOC 

04112/0615:14:31 0.9 -5.4 23.5 3.8 

04112/0615:14:41 1.0 -5.3 23.5 3.5 

04/1 2/06 15:14:51 16.7 -5.3 22.7 3.1 

04/12/0615:15:01 20.1 -5.2 18.5 2.7 

04112/06 15:15:11 20.1 -5.3 9.1 2.4 19.9 ppm CH4 

04/12/0615:15:21 20.1 -5.6 4.2 2.0 

0411210615:15:31 20.1 -5.5 2.4 1.9 

04112/06 15:15:41 20.2 -5.4 1.6 1.7 

04112/06 15:15:51 19.9 -5.5 1.2 1.6 

Page 7 

(~ J 
Jheet i 

Summary of CO Analyzer Calibrations and Sia! ~ 

Plant: Daitile, Muskogee, OK 

Source: Trim Kiln 

Date: 4/13/2006 

Analyzer Calibratrion Data 

Cylinder Anafyzer Absolute % Span 

Value Response Difference 

Zero Gas 0 1.53 1.53 0.306 

Mid Range 200 200.45 0.45 0.09 

High Range 494 491.85 -2.15 -0.43 

System Calibration Bias and Drift Data 

Analyzer Initial Values Final Values 

Cafibration System System System System 

Response Calibration Calibration Calibration Calibration 

Response Bias Response Bias 

Run #1 Zero Gas 1.53 0.45 -0.216 1.33 -0.04 

Upscale 200.45 195.08 -1.074 195.8 -0.93 

Average CO Concentration: 98.81 

Corrected CO Concentration: 100.6631 

(Equation 6C-1) 

Run #2 Zero Gas 1.53 1.33 -0.04 1.58 0.01 

Upscale 200.45 195.8 -0.93 193.78 -1.334 

Average CO Concentration: 97.94 

Corrected CO Concentration: 99.81121 

(Equation 6C-1) 

Run #3 Zero Gas 1.53 1.58 0.01 -1.13 -0.532 

Upscale 200.45 193.78 -1.334 192.3 -1.63 

Average CO Concentration: 94.26 

Corrected CO Concentration: 97.53909 

(Equation 6C-1) 

Drift Average 

Calibration 

Values 

0.176 0.89 

0.144 195.44 

0.05 1.455 

-0.404 194.79 

-0.542 0.225 

-0.296 193.04 

Page 1 96 
Systenz Calibration Bias and Drift Data 

Analyzer Initial Values Fina! Values 

Cafibration System System System System 

Response Calibration Calibration Calibration Calibration 

Response Bias Response Bias 

Run #1 Zero Gas -0.12 0.2 0.128 1.58 0.68 

Upscale 100.25 93.68 -2.628 94.8 -2.18 

Average S02 Concentration: 58.83 

Corrected S02 Concentration: 62.06749 

(Equation 6C-1) 

Run #2 Zero Gas -0.12 1.58 0.68 -0.13 -0.004 

Upscale 100.25 94.8 -2.18 94.58 -2.268 

Average S02 Concentration: 58.95 

Corrected S02 Concentration: 61.96456 

(Equation 6C-1) 

Run #3 Zero Gas -0.12 -0.13 -0.004 -0.58 -0.184 

Upscafe 100.25 94.58 -2.268 93.15 -2.84 

Average S02 Concentration: 57.93 

Corrected S02 Concentration: 61.86054 

(Equation 6C-1) 

Drift Average 

Calibration 

Values 

0.552 0.89 

0.448 94.24 

-0.684 0.725 

-0.088 94.69 

-0.18 -0.355 

-0.572 93.865 

Sheetl 

Surnmary of Sulfur Dioxicie Analyzer Calibrations and Bias 

Plant: Daltile, Muskogee, OK 

Source: Trim Kiln 

Date: 4/13/2006 

Analyzer Calibratrion Data 

Cylinder Anaiyzer Absolute % Span 

Value Response Difference 

Zero Gas 0 -0.12 -0.12 -0.048 

Mid Range 100 100.25 0.25 0.1 

High Range 250 251.85 1.85 0.74 

Page 1 9 '~ 
Sheet1 

Summary of NOx Analyzer Calibrations and Bias 

Plant: Daltile, Muskogee, OK 

Source: Trim Kiln 

Date: 4/13/2006 

Analyzer Catibratrion Data 

Cylinder Analyzer Absolute % Span 

Vaiue P.esponse Difference 

Zero Gas 0 0 0 0 

Mid Range 25.5 25.1 -0.4 -0.66667 

High Range 51 51.73 0.73 1.216667 

System Calibration Bias and Drift Data 

Analyzer Initial Va(ues Final Values Drift 

Cafibration System System System System 

Response Calibration Calibration Calibration Calibration 

Response Bias Response Bias 

Run #1 Zero Gas 0 -0.05 -0.08333 0.6 1 1.083333 

Upscale 25.2 24.45 -1.25 23.98 -2.03333 -0.78333 

Average NOx Concentration: 22.66 

Corrected NOx Concentration: 23.84367 

(Equation 6C-1) 

Run #2 Zero Gas 0 0.6 1 0.78 1.3 0.3 

Upscate 25.2 23.98 -2.03333 23.7 -2.5 -0.46667 

Average NOx Concentration: 21.93 

Corrected NOx Concentration: 23.39611 

(Equation 6C-1) 

Run #3 Zero Gas 0 0.78 1.3 0.7 1.166667 -0.13333 

Upscale 25.2 23.7 -2.5 23.35 -3.08333 -0.58333 

Average NOx Concentration: 21.57 

Corrected NOx Concentration: 23.31205 

(Equation 6C-1) 

Average 

Calibration 

Values 

0.275 

24.215 

0.69 

23.84 

0.74 

23.525 

Page 1 98 
4.13/06 Caiibrations 

Datefl`ime VOC CO NOx S02 

mnildd/yy hh:mm:ss pprn ppm ppm ppm 

04/13106 08:03:37 2.7 0.4 -0.1 -0.2 

04!13106 08:03:47 2.7 0.5 -0.1 -0.1 

04113106 08:03:57 2.8 0.4 -0.1 -0.1 Zero S02 

04/13106 08:04:07 2.6 0.3 -0.1 -0.1 

04/13/06 08:04:17 2.6 0.3 0.0 -0.2 

04113106 08:04:27 2.7 0.2 0.0 -0.2 

04113/06 08:04:37 2.8 0.4 0.0 0.2 

04113/06 08:04:47 2.8 0.4 0.2 18.0 

04/13!06 08:04:57 2.6 0.5 0.3 65.0 

04/13106 08:05:07 2.5 0.9 0.3 91.7 

04113106 08:05:17 2.5 0.9 0.4 100.6 

04/13106 08:05:27 2.6 1.0 0.4 103.3 

04/13/06 08:05:37 2.6 0.7 0.4 104.1 

04/13/06 08:05:47 2.7 0.7 0.3 104.7 

04113106 08:05:57 2.7 0.7 0.4 105.0 

04/13/06 08:06:07 2.7 0.7 0.3 105.1 

04/13/06 08:06:17 2.7 0.8 0.3 105.3 

04/13106 08:06:27 2.8 0.7 0.2 105.5 

04/13/06 08:06:37 2.7 1.0 0.3 102.9 

04/13f06 08:06:47 2.7 1.3 0.3 100.3 

04113106 08:06:57 2.8 1.1 0.3 100.3 100 ppm S02 

04/13106 08:07:07 2.8 1.1 0.3 100.3 

04113/06 08:07:17 2.8 1.2 0.3 100.1 

04113106 08:07:27 2.7 1.2 0.3 99.9 

04/13106 08:07:37 2.6 1.4 0.3 99.8 

04113106 08:07:47 2.7 1.5 0.2 99.8 

04113/06 08:07:57 2.8 1.6 0.2 99.7 

04/13/06 08:08:07 2.8 1.8 0.2 93.1 

04/13/06 08:08:17 2.8 1.6 0.0 52.7 

04/13/06 08:08:27 2.7 1.5 0.0 19.3 

04113106 08:08:37 2.7 1.5 0.0 6.7 

04113106 08:08:47 2.9 1.3 0.0 2.6 

04/13/06 08:08:57 2.9 0.8 0.2 24.4 

04113/06 08:09:07 2.7 1.0 0.5 132.6 

04113106 08:09:17 2.8 9.0 0.5 212.1 

04/13/06 08:09:27 2.9 12 0.5 240.3 

04/13/06 08:09:37 2.7 1.6 0.4 248.0 

04/13106 08:09:47 2.7 1.8 0.3 250.2 

04113106 08:09:57 2.9 1.8 0.4 251.0 

04/13/06 08:10:07 2.7 1.8 0.4 251.3 

04/13/06 08:10:17 2.7 1.8 0.4 251.7 

04/13/06 08:10:27 2.8 1.4 0.4 251.9 

04/13/06 08:10:37 2.8 1.1 0.4 251.8 250 ppm S02 

04/13/06 08:10:47 2.7 1.1 0.4 251.8 

04113/06 08:10:57 2.8 0.9 0.3 231.9 

04/13106 08:11:07 2.9 1.2 0.3 233.2 

04/13106 08:11:17 2.8 1.1 0.0 127.2 

04/13106 08:11:27 2.7 1.0 0.0 45.2 

04113/06 08:11:37 2.8 1.0 0.0 14.8 

04/13106 08:11:47 2.9 1.2 0.0 5.6 

04/13/06 08:11:57 2.9 1.2 0.0 2.8 

04113/06 08:12:07 2.9 1.1 0.0 1.8 

04/13/06 08:12:17 2.8 1.0 0.0 1.3 

04J13/06 08:12:27 3.1 1.0 0.0, 1.1 

04113106 0B12:37 3.1 1.1 -01 1.0 

04/13/06 08:12:47 3.1 1.0 -0.1 0.9 

04/13/06 08:12:57 3.1 1.0 -0.1 0.7 

04/13/06 08:13:07 2.0 1.0 -0.1 0.7 

04!13106 08:13:17 1.2 0.9 0.6 0.6 

04113/06 08:13:27 1.0 0.9 7.6 0.5 

04/13/06 08:13:37 0.8 0.7 15.0 0.4 

04/13/06 08:13:47 0.6 0.7 19.6 0.4 

04113106 08:13:57 0.6 0.7 21.9 0.4 

04/13/06 08:14:07 0.5 0.8 22.9 0.4 

04/13/06 08:14:17 0.5 0.6 23.4 0.3 

04113106 08:14:27 0.5 0.6 -23.8 0.2 

04113106 08:14:37 0.6 0.7 24.1 0.3 

04/13106 08:14:47 0.6 0.7 24.2 0.3 

04/13/06 08:14:57 0.6 0.6 24.3 0.3 

Page 1 .99 
413106 Calibrations 

04113/06 08:15:07 0.6 0.5 24.4 0.3 

04/13/06 08:15:17 0.6 0.4 24.4 0.2 

04113106 08:15:27 0.6 0.5 24.5 0.2 

04!13/06 08:15:37 0.5 0.4 24.4 0.2 

04113106 08:15:47 0.5 0.4 24.5 0.2 

04/13/06 08:15:57 0.5 0.5 24.4 0.2 

04113/06 08:16:07 0.6 0.4 24.4 0.2 

04113/06 08:16:17 0.9 0.5 24.4 0.2 

04113106 08:16:27 1.1 4.6 24.3 0.2 

04/13106 08:16:37 1.0 64.6 19.3 0.2 

04/13/06 08:16:47 1.0 132.5 9.4 0.2 

04113/06 08:16:57 1.0 164.9 4.4 0.2 

04113106 08:17:07 0.7 178.9 2.3 0.2 

04113106 08:17:17 0.5 184.8 1.4 0.2 

04/13106 08:1727 0.6 188.1 1.0 0.2 

04/13106 08:17:37 0.6 190.2 0.7 0.2 

04113/06 08:17:47 0.4 191.7 0.5 0.2 

04113106 08:17:57 0.5 192.8 0.3 0.2 

04/13106 08:18:07 0.5 193.2 0.3 0.2 

04/13106 08:18:17 0.4 193.7 0.1 0.2 

04/13106 08:18:27 0.4 193.8 0.1 0.2 

04/13J06 08:18:37 0.4 194.2 0.1 0.2 

04/13/06 08:18:47 0.4 194.3 0.0 0.2 

04/13/06 08:18:57 0.4 194.5 0.0 0.2 

04/13106 08:19:07 0.4 194.8 0.0 0.2 

04113106 08:19:17 0.5 194.9 -0.1 0.2 

04/13/06 08:19:27 0.5 195.1 -0.1 0.2 

04113/06 08:19:37 0.6 195.1 0.0 0.0 

04/13/06 08:19:47 O.a 195.2 0.0 0.1 

04/13/06 08:19:57 0.6 186.3 0.0 0.0 

04/13/06 08:20:07 0.5 118.5 0.2 0.1 

04113/06 08:20:17 0.4 57.6 0.3 6.0 

04/13/06 08:20:27 0.4 28.3 0.3 23.6 

04/13/06 08:20:37 0.5 16.7 0.3 42.3 

04/13/06 08:20:47 0.6 11.5 0.3 55.7 

04/13/06 08:20:57 0.5 8.7 0.3 64.2 

04113/06 08:21:07 0.5 6.6 0.3 69.9 

04/13/06 08:21:17 0.4 5.2 0.3 73.8 

04113/06 08:21:27 0.3 4.0 0.4 76.4 

04/13/06 08:21:37 0.3 3.3 0.4 78.7 

04113J06 08:21:47 0.4 2.6 0.4 80.6 

04/13/06 08:21:57 0.5 2.1 0.4 82.3 

04/13/06 08:22:07 0.6 1.5 0.4 83.6 

04/13/06 08:22:17 0.6 1.4 0.4 84.4 

04/13/06 08:22:27 0.6 1.3 0.4 85.0 

04/13J06 08:22:37 0.5 1.0 0.4 85.8 

04/13/06 08:22:47 0.5 0.9 0.4 86.4 

04/13106 08:22:57 0.4 0.9 0.4 87.0 

04/13106 08:23:07 0.3 0.9 0.4 87.6 

04/13/06 08:23:17 0.2 1.0 0.4 88.0 

04113/06 08:23:27 0.3 1.2 0.3 88.4 

04113106 08:23:37 0.3 1.1 0.3 89.0 

04113/06 08:23:47 0.3 1.1 0.3 89.4 

04/13/06 08:23:57 0.4 1.2 0.3 89.7 

04/13106 08:24:07 0.4 1.2 0.2 90.0 

04113106 08:24:17 0.4 1.1 0.3 90.2 

04113106 08:24:27 0.4 1.0 0.4 90.6 

04113/06 08:24:37 0.3 1.1 0.4 90.9 

04/13/06 08:24:47 0.3 1.2 0.3 91.1 

04113/06 08:24:57 0.3 1.3 0.3 91.3 

04/13/06 08:25:07 0.2 1.3 0.3 91.4 

04/13106 08:25:17 0.3 1.3 0.3 91.8 

04113/06 08:25:27 0.3 1.2 0.2 91.9 

04/13/06 08:25:37 0.4 0.9 0.3 92.0 

04113106 08:25:47 0.4 0.9 0.4 92.2 

04/13/06 08:25:57 0.4 0.8 0.2 92.3 

04/13/06 08:26:07 0.6 0.8 0.2 92.5 

04/13/06 08:26:17 0.5 0.7 0.3 92.6 

04/13/06 08:26:27 0.4 0.8 0.3 92.8 

04113/06 08:26:37 0.3 1.1 0.3 92.9 

04/13J06 08:26:47 0.3 1.2 0.3 93.0 

04/13/06 08:26:57 0.4 1.2 0.3 93.2 

25.5 ppm I, IOx 3ias 

Zero CO, $02 

200 ppm CO 

Zero NOx 

Page 2 -t0 0 
4

1 13106 Calibrrations 

04/13106 08:27:07 0.4 1.4 0.3 93.3 

04113/06 08:27:17 0.6 1.4 0.3 93.5 

04113/06 08:27:27 0.6 1.3 0.3 93.5 

04/13106 08:27:37 0.5 1.3 0.3 93.6 

04113/06 08:27:47 0.5 1.3 0.4 93.8 100 ppm S02 

04113/06 08:27:57 0.5 1.1 0.3 93.6 

04/13/06 08:28:07 0.9 1.3 0.3 93.7 

04113;06 08:28:17 0.6 1.2 0.3 93.5 

04113/06 08:28:27 0.5 1.4 0.3 91.1 

04113106 08:28:37 0.5 1.5 0.1 77.1 

04113l06 08:28:47 0.5 1.3 0.0 54.1 

04/13106 08:28:57 0.5 1.5 0.0 34.8 

04113106 08:29:07 0.5 1.5 0.0 22.4 

04113106 08:29:17 0.4 1.6 0.0 15.4 

04/13/06 08:29:27 0.4 1.4 0.0 11.4 

04/13106 08:29:37 0.2 1.7 0.0 9.7 

04/13/06 08:29:4 7 0.0 1.6 -D.1 8.2 

04/13106 08:29:57 0.0 1.6 -0.1 7.0 

04/13/06 08:30:07 0.0 1.6 -0.1 6.2 Zero Air 

04l1 3/06 08:30:17 0.0 1.6 -0.1 5.7 

04/13/06 08:30:27 0.0 1.6 -0.1 5.2 

04/13/06 08:30:37 0.1 1.5 -0.1 4.7 

04113l06 08:30:47 0.2 1.4 -0.1 4.4 

04/13/06 08:30:57 0.2 1.6 -0.1 4.3 

04113106 08:31:07 0.8 1.5 -0.1 3.9 

04/13/06 08:31:17 2.1 1.6 0.0 3.8 

04/13106 08:31:27 2.4 1.7 0.0 4.1 

04l13/06 08:31:37 2.6 1.7 0.0 5.0 

04113J06 08:31:47 28.9 1.6 0.1 6.3 

04/13J06 08:31:57 40.4 1.6 0.0 7.4 

04/13/06 08:32:07 40.2 1.5 0.0 7.5 

04/13106 08:32:17 4.7 1.3 -0.1 6.8 

04/13106 08:32:27 0.0 1.3 0.0 5.6 

04113106 08:32:37 0.0 1.0 0.0 4.6 

04/13/06 08:32:47 0.0 1.2 0.0 3.9 

04/13/06 08:32:57 0.0 1.2 0.0 3.6 

04113106 08:33:07 0.1 1.2 0.0 3.6 

04/13/06 08:33:17 0.1 1.3 0.0 3.7 

04/13/06 08:33:27 0.1 1.3 0.0 4.1 

04113106 08:33:37 0.1 1.2 0.0 4.3 

04113/06 08:33:47 0.1 1.0 0.0 4.9 

04/13/06 08:33:57 0.1 1.0 0.0 5.4 

04/13/06 08:34:07 0.1 0.9 0.0 5.8 

04/13/06 08:34:17 0.2 0.7 0.0 5.8 

04113/06 08:34:27 12.3 ' 0.7 0.0 5.4 

04/13/06 08:34:37 0.1 0.9 0.0 4.7 

04113106 08:34:47 0.1 1.1 0.0 3.9 

04l13/06 08:34:57 0.1 1.0 0.0 3.3 

04113106 08:35:07 0.1 1.0 0.0 2.9 

04/13/06 08:35:17 0.5 1.1 0.0 2.7 

04/13/06 08:35:27 2.1 1.0 0.0 2.5 

04113/06 08:35:37 2.3 1.0 0.0 2.3 

04/13/06 08:35:47 2.7 0.9 0.0 2.5 

04/13/06 08:35:57 27.5 1.0 0.0 2.8 

04/13/06 08:36:07 40.0 0.9 0.0 2.9 

04/13106 08:36:17 39.9 0.9 0.0 3.0 

04/13/06 08:36:27 39.8 0.6 0.0 2.9 

04l13/06 08:36:37 39.7 0.8 0.0 2.6 

04113/06 08:36:47 40.9 0.8 0.1 2.4 

04113/06 08:36:57 41.0 0.9 0.1 2.1 

04113/06 08:37:07 40.7 0.9 0.0 1.8 

04/13/06 08:37:17 40.9 1.0 0.0 1.8 

04/13106 08:37:27 40.7 1.2 0.0 1.6 40.8 ppm CH4 

04/13106 08:37:37 40.9 1.5 -0.1 1.5 

04/13/06 08:37:47 40.7 1.6 0.0 1.4 

04113106 08:37:57 38.3 1.7 0.0 1.4 

04113106 08:38:07 27.0 1.8 0.0 1.4 

04113106 08:38:17 3.1 1.6 0.0 1.3 

04113/06 08:38:27 2.7 1.7 0.0 1.5 

04113/06 08:38:37 16.9 1.8 0.0 1.5 

04113106 08:38:47 19.2 1.9 0.0 1.6 

Page 3 

1.01 
4113106 Calibraifons 

04/13/06 08:38:57 19.1 1.6 -0.1 1.7 

04113/06 08:39:07 19.0 1.4 0.0 1.8 19.9 ppm CH4 

04113106 08:39:17 19.0 1.3 0.1 1.7 

04/13106 08:39:27 19.0 1.0 0.1 1.6 

04113/06 08:39:37 19.1 1.1 0.0 1.4 

04113106 08:39:47 19.1 1.3 0.0 1.3 

04/13/06 08:39:57 18.6 1.5 0.0 1.2 

04/13/06 08:40:07 16.8 1.4 0.0 1.3 

04113/06 08:40:17 4.2 1.3 0.0 1.3 

04113106 08:40:27 3.3 1.5 0.0 1.4 

04113/06 08:40:37 54.9 1.6 0.0 1.5 

04113106 08:40:47 62.4 1.6 0.0 1.6 

04113106 08:40:57 62.4 1.5 0.1 1.8 

04/13106 08:41:07 62.4 1.5 0.1 1.8 

04/13/06 08:41:17 62.3 1.6 0.1 1.7 

04/13/06 08:41:27 62.2 1.7 0.1 1.5 61.7 ppm CH4 

04113106 08:41:37 62.2 1.7 0.1 1.2 

04/13/06 08:41:47 62.1 1.7 0.1 1.2 

04/13106 08:41:57 59.4 1.7 0.1 1.2 

04/13/OS 08:42:07 49.4 1.7 0.1 1.0 

04113/06 08:42:17 5.3 1.7 0.1 1.2 

04/13J06 08:42:27 2.8 1.6 0.0 1.4 

04/13106 08:42:37 2.8 1.9 0.1 1.5 

04113106 08:42:47 2.6 2.0 0.1 1.6 

04/13/06 08:42:57 2.6 2.0 0.0 1.6 

04113/06 08:43:07 2.7 1.9 0.0 1.7 

04113/06 08:43:17 2.6 1.8 0.0 1.9 

04113/06 08:43:27 2.7 1.8 0.0 2.0 

04/13106 08:43:37 2.7 1.9 0.0 2.4 

04/13/06 08:43:47 2.7 1.8 0.0 3.0 

04/13/06 08:43:57 2.6 1.8 0.1 3.5 

04/13/06 08:44:07 2.8 1.5 0.1 3.7 

04113/06 08:44:17 2.9 1.4 0.1 3.8 

04113/06 08:44:27 2.9 1.3 0.1 3.8 

04/13106 08:44:37 2.8 1.2 0.0 3.5 

04/13/06 08:44:47 2.7 1.2 0.0 3.5 Zera NOx Cal 

04/13/06 08:44:57 2.9 1.2 0.0 3.5 

04113/06 08:45:07 2.8 1.1 0.0 3.3 

04113106 08:45:17 2.8 0.8 10.9 3.4 

04113106 08:d5:27 2.8 1.0 24.7 2.9 

04/13/06 08:45:37 2.8 1.1 24.9 1.9 

04/13106 08:45:47 2.9 1.1 25.0 1.3 

04/13/06 08:45:57 3.0 1.2 25.1 1.0 

04113/06 08:46:07 2.9 1.5 25.1 1.0 25.5 ppm NOx Cal 

04/13/06 08:46:17 2.9 1.6 25.1 0.8 Zero CO Cal 

04113106 08:46:27 2.7 1.8 25.1 0.9 

04/13106 08:46:37 2.6 2.0 8.4 0.9 

04/13/06 08:46:47 2.5 1.9 0.0 1.5 

04/13106 08:46:57 2.5 1.6 0.0 2.1 

04113/06 08:47:07 2.7 1.4 0.5 2.2 

04/13/06 08:47:17 2.9 1.4 49.6 1.9 

04/13/06 08:47:27 2.8 1.5 51.3 1.3 

04/13/06 08:47:37 2.8 1.8 51.5 1.1 

04/13/06 08:47:47 2.7 1.8 51.6 0.9 

04/13/06 08:47:57 2.7 1.9 51.7 0.9 

04/13/06 08:48:07 2.7 2.0 51.7 0.9 51.0 ppm NOx Cal 

04/13106 08:48:17 2.6 2.0 51.7 0.9 

04/13/06 08:48:27 2.5 1.9 51.8 0.7 

04/13106 08:48:37 2.5 1.9 26.6 0.7 

04/13/06 08:48:47 2.4 2.0 0.1 1.0 

04113106 08:48:57 2.6 1.2 0.0 1.4 

04/13106 08:49:07 2.7 0.9 0.0 1.5 

04113106 08:49:17 2.6 2.0 -0.1 1.5 

04/13106 08:49:27 2.5 141.4 -0.1 1.5 

04/13/06 08:49:37 2.6 198.8 0.0 1.3 

04/13/06 08:49:47 2.5 199.5 -0.1 1.0 

04/13/06 08:49:57 2.4 199.9 0.0 0.9 

04/13106 08:50:07 2.4 200.2 0.0 0.9 

04/13/06 08:50:17 2.4 200.1 0.0 0.8 

1. 0.2 

Page 4 
4113/0v Calihratians 

04!13106 08:50:27 2.5 200.3 0.0 0.9 200 ppm CO Cat 

04/13/06 08:50:37 2.4 200.6 0.0 0.8 

04/13106 08:50:47 2.4 200.8 0.0 0.9 

04113/06 08:50:57 2.4 101.0 -0.1 1.0 

04113106 08:51:07 2.4 10.0 -0.1 1.1 

04/13106 08:51:17 2.2 2.6 -0.1 1.2 

04113/06 08:51:27 2.3 2.0 0.0 1.3 

04/13/06 08:51:37 2.2 49.9 0.0 1.2 

04113/06 08:51:47 2.3 446.1 0.0 1.2 

04113/06 08:51:57 2.4 430.0 0.0 1.0 

04113/06 08:52:07 2.4 490.9 0.0 1.0 

04113106 08:52:17 2.5 491.3 0.0 0.9 

04/13/06 08:52:27 2.4 491.7 -0.1 1.0 494 ppm CO Cat 

04/13/06 08:52:37 2.3 492.1 0.0 0.8 

04/13/06 08:52:47 2.3 492.3 -0.1 1.0 

04113/06 08:52:57 2.4 209.7 -0.1 1.0 

04113/06 08:53:07 2.6 8.5 0.0 0.9 

04/13/06 08:53:17 2.5 2.6 0.0 1.0 

04113106 08:53:27 2.4 2.1 0.0 1.1 

04!13106 08:53:28 ~ 2.6 1.9 -0.1 1.2 

103 

Page 5 
4113/06 Run S11 

DatelTfine VOc c0 NOx S02 

mmlddlyy hh:mm:ss ppm ppm ppm ppm 

04113106 09:19:51 50.3 110.4 223 55.0 

Start Run u1 

04/13106 09:20:01 50.7 111.6 22.3 55.0 Start Interference Sample 

04113/06 09:20:11 49.4 112.5 22.2 55.0 

04/13106 09:20:21 48.4 112.8 22.3 54.9 

04113f06 09:20:31 49.5 112.9 22.2 54.9 

04/13/06 09:20:41 48.9 113.4 22.2 55.0 

04/13/06 09:20:51 49.0 113.6 22.2 54.9 

04/13l06 09:21:01 49.3 113.9 22.2 54.8 

04/13106 09:21:11 48.9 114.4 22.2 54.6 

04/13106 09:21:21 49.2 114.7 22.3 54.5 

04/13/06 09:21:31 49.6 114.6 22.3 54.4 

04113106 09:21:41 50.1 114.1 22.3 54.4 

04113106 09:21:51 49.1 113.8 22.3 54.5 

04/13/06 09:22:01 49.6 113.4 22.4 54.5 

04/13/06 09:22:11 49.0 113.7 22.3 54.6 

04113/06 09:22:21 49.2 114.2 22.3 54.6 

04113106 09:22:31 48.7 115.0 22.5 54.8 

04/13106 09:22:41 48.2 115.3 22.5 55.1 

04113106 09:22:51 48.0 114.5 22.7 55.2 

04/13/06 09:23:01 48.9 112.7 22.8 55.3 

04113106 09:23:11 48.8 109.7 22.8 55.1 

04/13106 09:23:21 49.1 107.9 23.0 55.1 

04/13106 09:23:31 49.3 105.9 23.1 55.5 

04113/06 09:23:41 49.0 103.9 23.1 55.5 

04l13/06 09:23:51 48.4 100.5 23.1 55.0 

04/13/06 09:24:01 49.0 97.9 23.0 54.4 

04/13106 09:24:11 48.9 96.1 22.8 54.1 

04/13/06 09:24:21 49.2 94.7 22.7 54.1 

04113106 09:24:31 49.3 94.3 22.6 54.3 

04/13/06 09:24:41 49.2 94.0 22.6 54.3 

04113/06 09:24:51 49.8 93.9 22.5 54.2 

04113/06 09:25:01 50.0 94.0 22.5 54.1 

04/13/06 09:25:11 50.5 94.4 22.5 54.1 

04/13106 09:25:21 49.6 94.8 22.6 54.0 

04113106 09:25:31 49.7 95.4 22.6 53.9 

04113106 09:25:41 50.0 95.7 22.7 53.6 

04/13106 09:25:51 49.7 96.7 22.7• 53.6 

04/13/06 09:26:01 49.6 97.6 22.7 53.7 

04/13/06 09:26:11 49.7 97.9 22.7 53.9 

04/13106 09:26:21 49.3 97.7 22.7 53.9 

04/13/06 09:26:31 49.6 97.5 22.8 54.0 

04/13/06 09:26:41 50.1 97.2 22.8 53.9 

04113/06 09:26:51 50.0 97.4 22.8 54.0 

04/13106 09:27:01 49.4 97.7 22.7 54.2 

04/13106 09:27:11 ' 49.5 97.7 22.7 54.3 

04/13106 09:27:21 49.7 98.1 22.8 54.4 

04/13106 09:27:31 49.8 98.2 22.8 54.7 

04113106 09:27:41 49.6 98.3 22.8 55.0 

04/13106 09:27:51 49.9 98.1 22.7 55.2 

04/13/06 09:28:01 49.6 97.4 22.7 55.4 

04/13106 09:28:11 49.8 96.5 22.7 55.5 

04/13106 09:28:21 50.1 95.5 22.7 55.5 

04113106 09:28:31 50.0 95.1 22.7 55.5 

04/13/06 09:28:41 50.1 94.9 22.7 56.4 

04/13/06 09:28:51 49.7 94.9 22.7 55.2 

04/13/06 09:29:01 49.8 95.4 22.7 55.2 

04113106 09:29:11 50.5 95.6 22.7 55.2 

04/13/06 09:29:21 50.4 95.8 22.7 55.3 

04/13/06 09:29:31 50.7 96.2 22.7 55.1 

04/13106 09:29:4 i 50.1 96.7 22.6 55.2 

04/13106 09:29:51 50.3 97.3 22.5 55.0 

04/13106 09:30:01 50.6 97.7 22.6 54.9 

04/13106 09:30:11 51.0 97.8 22.6 54.8 

04/13106 09:30:21 50.1 98.4 22.6 54.7 

04/9 3106 09: 30:31 49.3 98.6 22.6 54.8 

04/13106 09:30:41 50.1 98.3 22.7 54.7 

04113106 09:30:51 49.7 98.2 22.6 54.6 

04/13/06 09:31:01 50.2 98.3 22.6 54.6 

04113/06 09:31:11 49.7 98.4 22.6 54.7 

04/13/06 09:31:21 50.3 98.2 22.7 54.8 

1()d. 

Page 1 
4113106 Run #1 

04/13/06 09:31:31 49.9 97.6 • 22.7 54.7 

04/13/06 09:31:41 49.8 96.6 22.7 54.4 

04113/06 09:31:51 51.0 ' 96.0 22.7 54.2 

04113106 09:32:01 50.2 95.9 22.7 54.1 

04/13106 09:32:11 50.6 96.1 22.7 54.0 

04113/06 09:32:21 50.2 96.2 22,7 53.9 

04113/06 09:32:31 50.5 96.3 22.7 54.0 

04/13/06 09:32:41 51.3 97.0 22.7 54.0 

04/13/06 09:32:51 51.1 97.9 22.9 54.3 

04/13106 09:33:01 51.1 97.8 22.8 54.7 

04/13/06 09:33:11 50.5 98.1 22.7 54.5 

04113!06 09:33:21 50.3 98.2 22.7 54.4 

04/13/06 09:33:31 49.9 98.2 22.7 54.6 

04113l06 09:33:41 50.6 98.0 22.7 54.6 

04/13/06 09:33:51 50.2 98.4 22.7 55.0 

04/13/06 09:34:01 50.9 98.5 22.7 55.4 

04/13106 09:34:11 51.0 98.5 22.6 55.6 

04/13106 09:34:21 51.0 98.4 22.6 55.8 

04/13/06 09:34:31 50.9 98.4 22.7 56.1 

04/13/06 09:34:41 51.2 98.2 22.7 56.6 

04/13/06 09:34:51 50.6 98.3 22.6 56.7 

04113I06 09:35:01 50.7 98.3 22.7 56.7 

04/13/06 09:35:11 50.8 98.4 22.8 56.8 

04113l06 09:35:21 51.2 98.4 22.8 57.0 

04113/06 09:35:31 50.6 98.8 22.7 57.0 

04113/06 09:35:41 50.5 99.2 22.7 57.2 

04113/06 09:35:51 50.3 99.4 22.7 57.3 

04/13106 09:36:01 50.1 99.1 22.7 57.5 

04I13106 09;36:11 51.5 98.6 22.7 57,6 

04/13106 09:36:21 51.3 98.6 22.7 57.7 

04/13106 09:36:31 51.1 98.7 22.7 57.7 

04113106 09:36:41 51.1 98.5 22.8 57.7 

04/13106 09:36:51 51.3 98.4 22.9 58.0 

04/13106 09:37:01 50.4 98.5 22.8 57.9 

04/13106 09:37:11 50.8 98.4 22.8 57.7 

04/13106 09:37:21 51.4 98.1 22.8 57.8 

04/13106 09:37:31 50.9 98.2 22.8 58.0 

04/13106 09:37:41 51.7 98.5 22.8 58.4 

04/13/06 09:37:51 51.2 98.4 22.8 58.5 

04/13106 09:38:01 51.0 98.5 22.9 58.6 

04/13/06 09:38:11 50.9 98.8 22.9 58.9 

04/13/06 09:38:21 51.3 99.0 23.0 59.1 

04/13/06 09:38:31 50.5 99.3 22.9 59.2 

04113/06 09:38:41 51.3 99.3 23.0 59.2 

04113106 09:38:51 50.6 99.6 22.9 59.3 

04113106 09:39:01 50.5 100.1 22.8 59.3 

04/13/06 09:39:11 50.2 100.3 22.9 59.2 

04113l06 09:39:21 50.2 100.3 22.9 59.2 

04/13/06 09:39:31 50.4 100.3 22.8 59.4 

04/13/06 09:39:41 50.5 100.0 22.8 59.5 

04/13/06 09:39:51 50.1 99.8 22.8 59.5 

04113106 09:40:01 50.3 100.0 22.8 59.8 Stop tnterference Sample 

04/13/06 09:40:11 50.7 100.0 22.8 60.0 Average 55.6 

04113/06 09:40:21 49.9 100.6 22.7 60,1 

04113106 09:40:31 49.8 100.7 22.7 59.9 

04/13/06 09:40:41 49.7 100.4 22.8 60.0 

04/13106 09:40:51 49.6 100.0 22.7 60.0 

04/13106 09:41:01 49.5 99.6 22.8 60.0 

04/1 3106 09:41:11 49.8 99.2 22.8 60.1 

04113106 09:41:21 49.6 98.8 22.8 60.2 

04/13106 09:41:31 49.5 98.7 ` 22.8 60.2 

04/13106 09:41:41 49.3 98.7 22,8 60.2 

04/13106 09:41:51 48.7 99.3 22.8 60.1 

04113/06 09:42:01 48.7 99.8 22.8 60.1 

04/13/06 09:42:11 48.9 100.2 22.8 60.1 

04/13/06 09:42:21 48.9 100.4 22.8 60.1 

04/13106 09:42:31 49.4 100.5 22.8 60.0 

04/13/06 09:42:41 48.2 100.4 22.9 59.8 

04113106 09:42:51 48.9 99.9 22.9 59.7 

04113106 09:43:01 48.5 99.6 22.9 59.6 

04/13106 09:43:11 49.2 99.4 22.8 59.7 

04J13106 09:43:21 49.3 99.7 22.8 59.8 

04/13J06 09:43:31 48.7 100.1 22.8 59.8 

04/13/06 09:43:41 49.2 100.8 22.9 59.9 

Page 2 ~ ~ J 
4113106 Run #1 

04113/06 09:43:51 49.1 101.3 22.8 59.7 

04/13/06 09:44:01. 49.1 102.0 22.8 89 V 

04113106 09:44:11 48.9 102.5 22.8 ::9.6 

04113l06 09:44:21 48.5 103.0 22.7 59.7 

04113/06 09:44:31 48.8 103.1 22.7 59.7 

04/13106 09:44:41 49.9 103.0 22.7 59.6 

04113106 09:44:51 47.5 103.1 22.7 59.7 

04113/06 09:45:01 48.0 102.8 22.8 59.6 

04/13/06 09:45:11 47.9 101.8 22.8 59.7 

04113106 09:45:2 i 47.8 101.1 22.8 59.7 

04113/06 09:45:31 49.1 100.4 22.8 59.7 

04/13/06 09:45:41 48.8 99.7 22.8 59.7 

04113/06 09:45:51 49.2 99.4 22.7 59.7 

04/13/06 09:46:01 48.6 99.5 22.8 59.9 Start Inlerference Sample 

04/13/06 09:46:11 48.9 99.2 22.8 59.8 

04/13106 09:46:21 48.6 98.9 22.8 59.8 

04113106 09:46:31 48.7 98.7 22.8 59.9 

04113/06 09:46:41 48.5 98.8 22.7 59.6 

04113106 09:46:51 48.9 98.8 22.7 59.6 

04/13/06 09:47:01 48.6 98.5 22.7 59.7 

04/13106 09:47:11 48.5 98.6 22.7 59.7 

04/13/06 09:47:21 48.9 98.7 22.8 60,0 

04/13/06 09:47:31 48.3 98.8 22.8 60.0 

04/13106 09:47:41 48.2 98.5 22.8 60.2 

04/13/06 09:47:51 48.5 98.4 22.7 60.2 

04/13/06 09:48:01 49.0 98.4 22.7 60.1 

04113/06 09:48:11 49.1 98.5 22.7 60.2 

04/13/06 09:48:21 48.8 98.3 22.7 60.3 

04113106 09:48:31 50.6 98.5 22.7 60.2 

04/13/06 09:48:41 47.7 98.5 22.7 60.1 

04/13/06 09:48:51 49.1 98.4 22.7 60.0 

04/13/06 09:49:01 49.1 98.2 22.7 60.1 

04113/06 09:49:11 49.0 98.0 22.7 60.1 

04113106 09:49:21 49.5 98.1 22.7 60.0 

04/13106 09:49:31 49.3 97.9 22.8 60.0 

04113106 09:49:41 49.6 97.6 22.7 60.2 

04113/06 09:49:51 49.3 97.3 22.7 60.1 

04113106 09:50:01 50.1 97.1 22.7 59.9 

04/13/06 09:50:11 49.9 97.1 22.7 59.7 

04/13106 09:50:21 50.1 97.2 22.8 59.7 

04113106 09:50:31 49.7 97.5 22.8 59.7 

04/13/06 09:50:41 50.2 97.8 22.8 59.7 

04/13106 09:50:51 50.1 98.1 22.8 59.9 

04/13/06 09:51:01 49.5 98.4 22.8 60.0 

04/13/06 09:51:11 48.8 98,7 22,7 60.0 

04/13/06 09:51:21 49.1 98.8 22.6 59.8 

04/13l06 09:51:31 51.3 98.8 22.7 59.6 

04/13706 09:51:41 50.7 99.3 22.7 59.5 

04113l06 09:51:51 50.4 99.9 22.7 59.5 

04113/06 09:52:01 49.4 99.9 22.7 59.4 

04113/06 09:52:11 49.5 99.9 22.7 59.6 

04/13106 09:52:21 50.9 .99.7 22.7 59.7 

04/13/06 09:52:31 51.4 99.6 22.7 59.7 

04/13/06 09:52:41 51.0 99.9 22.7 59.7 

04l13106 09:52:51 50.8 100.0 22.6 59.7 

04113106 09:53:01 51.3 99.7 22.7 59.8 

04/13/06 09:53:11 51.2 99.5 22.7 60.0 

04/13/06 09:53:21 51.0 99.6 22.6 60.0 

04113/06 09:53:31 51.2 99.5 22.7 59.9 

04113/06 09:53:41 51.9 99.8 22.7 59.9 

04113106 09:53:51 51.3 100.4 22.7 59,9 

04113106 09:54:01 51.1 101.7 22.7 59.8 

04113106 09:54:11 50.8 102.6 22.6 59.8 

04113/06 09:54:21 49.9 103.0 22.7 60.0 

04/,13106 09:54:31 49.5 102.8 22.7 60.1 

04/13106 09:54:41 50.3 102.3 22.7 60.2 

04/13I06 09:54:51 50.2 100.6 22.7 60.3 

04/13/06 09:55:01 50.7 98.5 22.6 60.5 

04/13/06 09:55:11 51.1 97.1 22,6 60.3 

04113/06 09:55:21 51.1 96.5 22.7 60.2 

04113106 09:55:31 51.3 96.1 22.6 60.2 

04l13106 09:55:41 51.2 96.1 22.6 60.1 

04/13106 09:55:51 51.1 96.2 22.7 60.0 

04/13/06 09:56:01 51.2 96.6 22.7 60.1 

106 

Page 3 
4/13/06 Run tt1 

04113J06 09:56:11 51.6 971 22.7 60.2 

04113/06 09 , 56:21 51.2 98.1 22.6 60.2 

04/13106 09:56:31 51.6 98.5 22.7 60.1 

04/13106 09:56:41 51.5 98.7 22.6 59.9 

04113/06 09;56:51 50.7 98.7 22.6 59.9 

04113/06 09:57:01 504 98.5 22.6 59.8 

04113/06 09:57:11 50.9 98.0 22 6 60.0 

04113106 09:57:21 50.9 97.7 22.6 60.2 

04113106 09:57:31 50.0 97.5 22.6 60.3 

04113/06 09:57:41 49.8 98.1 22.5 60.4 

04113106 09:57:51 49.6 98.3 22.5 60.4 

04113/06 09:58:01 50.1 98.5 22.5 60.4 

04/13106 09:58:11 50.3 98.4 22.6 60.4 

04/13/06 09:58:21 50.0 98.2 22.6 60.3 

04/13106 09:58:31 49.9 97.9 22.7 60.3 

04113/06 09:58:41 49.7 98.0 22.6 60.1 

04113/06 09:58:51 49.1 98.1 22.7 60.3 

04/13/06 09:59:01 492 98.2 22.7 60.4 

04113/06 09:59:11 49.7 98.3 22.7 60.6 

04113106 09:59:21 48.5 98.2 22.7 60.7 

04113/06 09:59:31 48,4 97.9 22.6 60.7 

04/13/06 09:59:41 48.8 97.2 22.6 60.3 

04113/06 09:59:51 48.9 96.8 22.7 60.2 

0411310610:00:01 49.0 96.8 22.7 60.1 

04/13106 10:00:11 48.7 97.0 22.7 60,1 

04113/0610:00:21 49.1 97.2 22.7 60,3 

0411 3/06 1 0:00:31 49.2 97.1 22.7 60.3 

0411310610:00:41 48.7 96.8 22.7 60.2 

0411310610:00:51 48.7 97.1 22.7 60.2 

0411310610:01:01 48.8 96.9 22.7 60.2 

0411310610:01:11 49.4 96.6 22.7 60.2 

04113/0610:01:21 49.0 96.9 22.7 60.2 

0411310610:01:31 49.6 96.9 22.7 60.1 

04113/0610:01:41 49.1 97.4 22.7 60.4 

04113/0610:01:51 49.0 97.4 22.7 60.4 

0411310610:02:01 49.1 97.0 22.7 60.4 

04113/0610:02:11 48.9 96.8 22.7 60.5 

04/1310610:02:21 48.6 96.9 22.7 60.6 

04/1310610:02:31 48.5 96.9 22.8 60.5 

0411310610:02:41 48.7 96.8 22.8 60.7 

04113/0610:02:51 48.8 96.8 22.7 60.7 

04113/0610:03:01 48.7 96.6 22.7 60.7 

04113/0610:03:11 48.5 96.4 22.7 60.6 

04113106 10 03:21 48.6 96.4 22.7 60.4 

04113106 10:08:31 48.9 96.1 22.7 60.5 

0411 3106 1 0:03:41 48.5 95.8 22.8 60.5 

04/13/0610:03:51 49.0 95.9 22.7 60.5 

04/13/0610:04:01 49.0 96.3 22.7 60.6 

04113/0610:04:11 49.3 96.8 22.6 60.4 

04113/0610:04:21 48.9 96.9 22.6 60.4 

0411310610:04:31 49.4 96.8 22.7 60.4 

0411310610:04:41 49.4 96.7 22.7 60.3 

04I1310610:04:51 49.1 96.6 22.6 60.3 

0411310610:05:01 48.7 96.5 22.7 60.4 

04/1310610:05:11 49.6 96.4 22.6 60.3 

04/1310610:05:21 49.3 96.7 22.6 60.3 

04/13106 10 05:31 49.3 97.0 22.6 60.5 

04/1310610:05:41 49.3 97.3 22.6 60.7 

04/1310610:05:51 49.4 97.3 22.6 60.9 

04113/06 10:06:01 49.5 97.4 22.6 60.8 Stop Interference Sainple 

04113/0610:06:11 49.2 97.6 22.6 60.8 Average 60.1 

0411310610:06:21 49.1 98.0 22.5 60.9 

04113/0610:06:31 49.4 97.9 22.5 61.0 

0411310610:06:41 49.3 97.3 22.6 61.0 

0411310610:06:51 49.6 97.1 22.6 61.1 

04113106 10:07:01 49,1 96.8 22.6 61.1 

0411310610:07:11 49.9 96.1 22.6 61.2 

04/1310610:07:21 50.8 95.9 22.6 61.2 

04/1310610:07:31 50.9 95.8 22.6 61.1 

04113/0610:07:41 50.4 95.7 22.6 61.0 

04113/0610:07:51 51.4 95.6 22.6 61.0 

0411310610:08:01 50.7 95.8 22.6 61.1 

04/1310610:08:11 50.7 95.8 22.7 61.0 

04113/06 10:08:21 506 95.8 22.7 61.2 

10 

Page 4 
4/13106 Run #1 

0411310610:08:31 50.1 96.1 22.6 61.1 

0411310610:08:41 50.3 96.7 22.6 61.1 

04/1310610:08:51 50.3 97.1 22.7 61.0 

04/13/0610:09:01 50.7 97.6 22.7 60.9 

04113/0610:09:11 50.5 97.5 22.7 60.8 

0471310610:09:21 50.7 97.5 22.6 60.6 

04/1310610:09:31 50.7 97.6 22.6 60.5 

04/13/0610:09:41 50.3 97.7 22.6 60.5 

04/1310610:09:51 50.2 97.5 22.6 60.5 

04/13/0610:10:01 51.1 97.4 22.6 60.5 

04/13/06 10:10 - 11 51.1 97.3 22.6 60.5 

04/13/0610:10:21 50.2 97.5 22.5 60.4 

0411310610:10:31 51.4 97.9 22.6 60.3 

0411310610:10:41 51.2 97.8 22.6 60.1 

04/1310610:10:51 50.9 97.6 22.6 60.1 

04/13/0610:11:01 50.5 97.3 22.6 59.9 

04/13/0610:11:11 50.2 97.0 22.6 59.9 

0411310610:11:21 50.5 96.7 22.6 59.9 

04113/0610:11:31 50.9 96.5 22.6 59.9 

04/1310610:11:41 51.0 96.4 22.6 59.9 

04/13/0610:11:51 51.0 96.6 22.6 59.9 

04113/0610:12:01 51.3 96.3 22.6 60.0 

04/13/0610:12:11 50.9 96.1 22.6 60.0 

04/1310610:12:21 51.5 96.2 22.6 60.0 

04/1310610:12:31 51.5 96.6 22.6 60.1 

04113/0610:12:41 51.3 96.7 22.6 60.2 

04113/0610:12:51 51.1 96.3 22.5 60.2 

04/13/0610:13:01 50.9 96.2 22.6 60.2 

04113/0610:13:11 51.4 96.0 22.6 60.3 

04113/0610:13:21 51.2 96.1 22.6 60.4 

04113/0610:13:31 50.9 98.2 22.6 60.5 

04/1310610:13:41 50.8 96.2 22.5 60.3 

04/1310610:13:51 51.0 96.3 22.5 60.3 

04/13/0610:14:01 50.3 96.5 22.5 60.2 

04113/0610:14:11 50.7 96.1 22.6 60.3 

04/13/06 10:14:21 504 95.8 22.6 60.3 

04/1310610:14:31 50.6 95.7 22.6 60.3 

0411310610:14:41 51.2 95.8 22.6 60.7 

04113/061014:51 50.9 95.7 22.6 60.7 

0411310610:15:01 50.9 95.9 22.6 60.7 

04/13/0610:15:11 50.7 96.4 22.5 60.7 

0411310610:15:21 51.0 97.0 22.5 60.7 

04/1310610:15:31 50.3 97.4 22.5 60.8 

0411310610:15:41 51.0 97.5 22.4 60.9 

0411310610:15:51 49.9 98.0 22.4 61.2 

04/13/0610:16:01 50.0 97.9 22.4 61.5 

0411310610:16:11 50.1 97.9 22.4 61.5 

04/1310610:16:21 49.7 98.1 22.5 61.5 

04113/0610:16:31 50.1 97.9 22.6 61.5 

04/13/0610:16:41 50.0 97.7 22.5 61.5 

04113/0610:16:51 50.2 97.9 22.6 61.4 

04/13/0610:17:01 50.6 97.8 22.5 61.3 

04/1310610:17:11 50.5 97.4 22.5 61.2 

04/13/0610:17:21 50.9 96.9 22.6 61.1 

04/13/0610:17:31 50.5 96.7 22.5 61.2 

04113/0610:17:41 50.3 96.7 22.5 61.3 

04/13/0610:17:51 50.3 96.7 22.4 61.3 

04113/0610:18:01 60.0 97.3 22.4 61.2 

04/13/0610:18:11 49.4 98.0 22.4 61.3 

04/13/0610:18:21 49.7 98.2 22.5 61.3 

04/1310610:18:31 49.4 98.0 22.5 61.1 

04/13/061018:41 50.0 97.8 22.4 61.2 

04/13/0610:18:51 49.1 97.7 22.4 61.2 

04113/0610:19:01 49.5 98.1 22.4 61.2 

04/1310610:19:11 48.9 98.8 22.5 61.2 

0411310610:19:21 48.8 99.4 22.5 61.2 

04113/0610:19:31 48.6 99.3 22.5 61.1 

04/13/0610:19:41 49.2 98.6 22.5 60.9 

04/13/0610:19:51 49.5 97.9 22.5 60.8 

04/13/0610:20:01 49.4 97.4 22.5 60.7 

04/13/0610:20:11 50.1 97.3 22.5 60.7 

04J1310610:20:21 49.7 97.2 22.6 60.6 

04113/0610:20:31 49.4 97.5 22.6 60.6 

04/13/0610:20:41 49.5 97.7 22.6 60,6 

108 

Page 5 
4113106 Run #1 

0411310610:20:51 49.3 98.0 22.6 60.6 

0411310610:21:01 49.2 98.1 22.6 60.5 

04/13/06 10:21 11 493 98.2 22.6 60.6 

04/1310610:21:21 491 98.4 22.6 60.7 

0411310610:21:31 49,5 98.7 22.6 60.7 

0411310610:21:41 50.0 99.2 22.6 60.7 

04/1310610:21:51 49.3 99.8 22.6 60.9 

04113/0610:22:01 49.2 100.1 22.6 60.8 

0411310610:22:11 48.9 100.3 22.6 60.8 

0411310610:22:21 49.6 100.5 22.7 60.7 

04!1310610:22:31 49.3 100.3 22.6 60.7 

04113/0610:22:41 48.5 73.3 22.6 60.6 

0411310610:22:51 48.5 100.2 22.6 60,6 

Stop Run #1 49.88 98.81 22.66 58.83 

0411310610:23:01 28.8 100.1 22.5 60.5 

04113/0610:23:11 10.1 91.3 22.0 60.3 

04/13/0610:23:21 11.6 56.4 16.0 57.8 

0411310610:23:31 9.4 29.7 9.5 50.7 

04113106 10:23:41 7.7 18.0 6.5 41.5 

04/13106 10:23:51 68 11.9 4.9 33.0 

0411310610:24:01 6.3 8.1 3.9 26.2 

04/13106 10:24 11 5.1 6.1 3.2 21.1 

04113106 10:24:21 3.2 9.3 2.7 17.2 

04113/0610:24:31 2.3 63.3 2.1 14.0 

04/13106 10:24:41 1.7 114.9 2.0 11.6 

04/ 13106 10: 24: 51 1.3 153.0 1.7 10.4 

04/13106 10:25:01 1.1 175.3 1.4 8.7 

0411310610:25:11 1.0 186.4 1.2 7.1 

04! 13106 10:25- 21 0.9 191.1 1.1 5.9 

0411310610:25:31 0.8 193.0 1.0 5.0 

04113/06 10:25:41 0.8 193.8 1.0 4.3 

04113/0610:25:51 0.9 194.2 0.9 3.8 

04/1310610:26:01 1.0 194.8 0.9 3.5 

0411310610 - 26:11 0.8 195.1 0.8 3.3 

0411310610:26:21 0.5 195.5 0.8 3.1 

0411310610:26:31 0.5 195.6 0.7 2.9 

04113/0610:26 - 41 0.5 195.8 0.7 2.8 

04/1310610:26:51 0.6 195.8 0.6 2.5 

0411310610:27:01 0.6 195.8 0.6 2.4 

04/13/06 10:27:11 0.6 195.8 0.5 2.4 

04113i0610:27:21 0.7 195.7 0.5 2.3 

04113106 10:27:31 0.6 175.3 1.0 2.1 

0411310610:27:41 0.4 104.5 8.1 2.2 

04/13/06 10:27:51 0.5 51.9 16.2 2.1 

04/1310610:28:01 0.5 26.2 20.2 2.1 

0411310610:28:11 0.5 15.7 22.0 2.1 

0411310610:28:21 0.4 10.9 22.7 2.0 

04/ 13106 10:28:31 0.3 8.1 23.2 1.9 

04/13/0610:28:41 0.5 6.3 23.4 2.0 

04/13/06 10:28:51 0.5 5.1 23.5 1.9 

0411310610:29:01 0.3 4.4 23.6 1.9 

04/1310610:29:11 0.4 3.8 23.7 1.7 

04r 13106 10:29: 21 0.5 3.4 23.8 1.8 

04113/0610:29:31 0.4 3.2 23.8 1.7 

0411310610:29:41 0.2 3.0 23.9 1.5 

0411310610:29:51 0.3 2.9 24.0 1.5 

0411310610:30:01 0.4 2.5 23.9 1.6 

04113J0610:30:11 0.6 2.4 23.9 1.6 

04/13/0610:30:21 0.6 2.3 23.9 1.6 

04/13106 10:30:31 1.3 2.1 24.0 1.5 

04/13106.10:30:41 2.7 1.8 23.2 1.5 

04/13106 10:30:51 2.8 2.0 16.6 1.5 

04/13106 1031:01 2.9 1.9 8.3 1.5 

04/13/06 10:31:11 1.4 1.9 4.1 1.7 

04113/06 10:31:21 0.6 1.7 2.3 2.1 

04/13/06 10:31:31 0.4 1.5 1.6 6.0 

04/13/06 10:31:41 0.6 1.3 1.2 16.7 

04/ 13/06 10:31: 51 0.6 1.3 1.1 31.9 

04113/06 10:32:01 0.5 1.5 1.1 46.8 

04/13/06 10:32:11 0.5 1.7 1.1 58.6 

04/13106 10:32:21 05 1.7 1.0 67.3 

200 ppm CO 

Zero NOx 

25.5 ppm NOx 

Zero S02 

Page 6 

109 
4113106 Ruri # i 

0411310610:32:31 4.4 1.6 0.9 73.7 

0411310610:32:41 0.4 1.5 0.8 78.5 

04/1310610:32:51 0.5 1.5 0.7 82.1 

0411310610:33:01 0.4 1.4 0.6 84.4 

0411310610:33:11 0.4 1.3 0.6 85.9 

04l1310610:33:21 0.4 1.5 0.5 87.3 

04113/0610:33:31 0.5 1.4 0.5 88.9 

0411310610:33:41 0.4 1.3 0.5 90.2 

04/13/06 10:33:51 0.5 1.3 0.5 91.2 

0411310610:34:01 0.5 1.2 0.4 91.8 

0411310610:34:11 0.4 1.3 0.4 92.4 

04113/0610:34:21 0.4 1.4 0.3 92.6 

04113/0610:34:31 0.4 1.5 0.4 92.8 

0411310610:34:41 0.3 1.2 0.4 93.2 

0411310610:34:51 0.2 1.3 0.4 93.5 

0411310610:35:01 0.2 1.3 0.4 93.8 

0411310610:36:11 0.2 1.5 0.3 93.9 

0411310610:35:21 0.3 1.4 0.3 94.1 

04/1310610:35:31 0.2 1.3 0.4 94.4 

0411310610:35:41 0.2 1.4 0.4 94.5 

0411310610:35:51 0.0 1.5 0.4 94.5 

04113/0610:36:01 0.2 1.5 0.4 94.5 

0411310610:36:11 0.1 1.3 0.5 94.6 

04113/0610:36:21 0.3 1.3 0.4 94.8 

04l1310610:36:31 0.4 1.3 0,4 94.9 

0411310610:36:41 20.5 1.4 0.4 94.9 

0411310610:36:51 41.8 1.5 0.4 94.7 

0411310610:37:01 41.9 1.5 0.3 90.0 

04113106 10:37:11 41.9 1.5 0.1 77.8 

04113r0610:37:21 41.8 1.5 0.1 62.2 

0411310610:37:31 41 .9 1.6 0.0 47.8 

04113/0610:37:41 41.9 1.4 0.0 36.4 

04/13/0610:37:51 41.9 1.3 0.0 28.1 

Zero VOC 

100 ppm S02 

Zero CO 

40.8 ppm CH4 

~ ~_ a 

Page 7 
4113106 Run #2 

DatefTime VOC c0 NOx S02 

mm/dd/yy hh:mrn:ss ppm ppm ppm ppm 

0411310610:49:51 48.4 95.6 21.2 57.2 

Start Run #2 

04/1310610:50:01 48.8 95.4 21.3 57.4 

04/13/0610:50:11 48.7 95.4 21.2 57.4 

04/1310610:50:21 48.5 95.3 21.3 57.6 

0411310610:50:31 48.2 95,5 21.4 57.8 

0411310610:60'41 48.6 96.1 21,4 58.1 

0411310610:50:51 49.0 96.7 21.3 58.4 

0411310610:51:01 49.3 97.0 21.4 58.4 

04113/0610:51:11 48,9 97.6 21.5 58.3 

0411310610:51:21 48.9 97.6 21.4 58.3 

0411310610:51:31 49.3 97.4 21.5 58.5 

04/13/0610:51:41 48.9 97.4 21.6 58.5 

04/13/0610:51:51 49.3 97.4 21.6 58.5 

0411310610:52:01 49.6 97.7 21.7 58.5 

0411310610:52:11 49.3 98.0 21.7 58.6 

04113/06 10:52:21 49.0 98.0 21.8 586 

04/1310610:52:31 48.9 97.6 21.8 58.6 

04/1310610:52:41 49.2 96.9 21.8 58.6 

04/13/0610:52:51 48.9 96.8 21.8 58.6 

04113/0610:53:01 49.2 96.4 21.7 58.7 

04113106 10:53:11 49.0 96.3 21,7 58.7 

0411310610:53:21 49.4 96.5 21.8 68.8 

04/1310610:53:31 49.4 97.3 21.8 58.8 

04113:0610:53:41 49.2 98.2 21.7 58.8 

04113/0610:53:51 49.1 98.6 21.6 58.9 

0411310610:54:01 49.5 96.6 21.7 59.0 

04/13/0610:54:11 49.3 98.5 217 59.0 

04113/0610:54:21 49.5 98.2 21.7 58.9 

0411310610:54:31 49.4 98.4 21.7 58.7 

0411310610:54:41 49.5 98.8 21.7 58.6 

04/13/06 10:54:51 497 99.5 21.7 58.7 

04/13/06 10:55:01 49.0 99.7 21.6 58.9 

0411310610:55:11 49.3 99.7 21.6 59.0 

0411310610:55:21 49.4 99.5 21.6 59.0 

04113/0610:55:31 49.1 99.5 21.6 59.1 

04113/0610:55:41 48.9 99.2 21.6 59.2 

0411310610:55:51 49.3 98.9 21.5 59.1 

04113/0610:56:01 48.9 98.6 21.6 59.0 

04113/0610:56:11 49.3 98.0 21.6 58.9 

04113/0610:56:21 49.9 97.9 21.6 58.9 

0411310610:56:31 49.7 98.2 21.6 59.0 

04/1310610:56:41 49.2 98.8 21.5 59.0 

04/1310610:56:51 48.7 99.2 21.5 59.0 

0411310610:57:01 49.3 99.3 21.5 59.0 

04113/0610:57:11 49.1 99.1 21.6 59.1 

04113/0610:57:21 49.1 98.7 21.5 59.0 

04/1310610:57:31 491 98.2 21.5 58.9 

04113/0610:57:41 49.5 97.8 21.5 58.9 

04/13106 10:57: 51 49,2 97.5 21.5 59.0 

0411310610:58:01 48.7 97.3 21.6 59.0 

04113/06 10:58: 11 49.3 97.2 21.7 58.9 

0411310610:58.21 49.1 97.5 21.7 58.9 

04113/06 10: 58: 31 49.3 98.0 21.7 58.8 

04113/0610:58:41 49.1 98.8 21.7 58.8 

04113/0610:58:51 48.9 99.5 21.6 58.8 

0411310610:59:01 48.5 99.8 21.6 58.7 

04/1310610:59:11 48.2 100.1 21.6 58.7 

04/1310610:59:21 48.9 99.8 21.7 58.8 

04/13/0610:59:31 48.5 99.6 21.8 58.9 

04/1310610:59:41 49.2 99.4 21.8 59.0 

04/1310610:59:51 49.3 98,9 21.7 58.9 

04113/06 11:00:01 49.2 98.8 21,7 58.9 Stari Interference SampEe 

04/13/0611:00:11 48.5 98.5 21.6 58.8 

04/13/0611:00:21 49.2 98.3 21.6 58.9 

0411310611:00:31 48.6 98.7 21.7 58.8 

04i13106 11 •00:41 49.2 98.9 21.7 58.7 

0411 3106 1 1:00:51 49.2 991 21.7 58.8 

04113k06 11:01:01 48.9 i 00.7 21.7 58.9 

04113/0611:01:11 48.6 101.2 21.7 59.0 

0411310611:01:21 48.8 101.5 21.6 591 

Page 1 1' 1. 1 
4/13/06 Run ii2 

0411310611:01:31 49.6 100.9 21.6 59.0 

04113106 11:01:41 491 100.1 21.7 590 

04713/0611:01:51 46.8 99.3 21.7 56.8 

04/1310611:02:01 48.6 98.6 21.6 58.7 

04113/0611:02:11 49.0 96.2 21.5 58.7 

04/13/0611:02:21 49.1 98.1 21.7 58.7 

0411310611:02:31 49.5 98.1 21.7 58.7 

04/1310611:02:41 49.1 98.1 21.7 58.7 

0411310611:02:51 48.7 97.8 21.8 58.8 

0411310611:03:01 49.1 97.9 21.6 58.9 

04/13/0611:03:11 48.9 98.4 21.7 59.0 

04113/0611:03:2 1 49.1 99.3 21.7 59.0 

04113/0611:03:31 48.5 99.7 21.7 59.1 

04/13/0611:03:41 48.8 100.1 21.8 59.0 

04/13/0611:03:51 48.7 100.0 21.8 59.0 

04113/0611:04:01 48.4 99.6 21.8 59.1 

0411310611:04:11 49.2 98.6 21.8 59.1 

04113/0611:04:21 49.0 98.3 21.8 59.0 

04/13/06 11:04:31 49.3 - 98.1 21.7 59.1 

04/1310611:04:41 49.1 98.1 21.8 59.1 

04/1310611:04:51 49.4 98.2 21.8 59.0 

04/13/0611:05:01 48.2 98.9 21.7 59.0 

04/13/0611:05:11 49.0 98.8 21.6 58.9 

04113/0611:05:21 48.9 98.9 21.6 56.9 

04/13/0611:05:31 48.0 99.2 21.8 58.8 

04/1310611:05:41 48.8 98.7 21.7 58.9 

04/13/0611:05:51 48.7 98.6 21.7 59.0 

04113/0611:06:01 49.0 98.3 21.8 59.1 

04/13/0611:06:11 49.2 98.3 21.9 59.1 

04/13/0611:06:21 49.5 98.2 21.9 59.2 

04/1310611:06:31 49.1 98,1 21.8 59.2 

04/13/0611:06:41 49.3 98.0 21.8 59.2 

04/13/0611:06:51 48.9 98.2 21.8 59.4 

04113/0611:07:01 48.6 98.5 21.8 59.4 

04/13/0611:07:11 48.1 98.9 21.7 59.3 

04/13/0611:07:21 48.3 99.3 21.7 59.2 

04113/0611:07:31 48.5 99.4 21.8 59.1 

0411310611:07:41 48.8 99.4 21.8 59.2 

04/13/0611:07:51 49.2 99.0 21.9 59.2 

04/13/0611:08:01 46.6 98.5 21.6 59.2 

04/13/0611:08:11 48.6 98.1 21.9 59.2 

04/13/0611:08:21 48.4 97.7 21.9 59.1 

04/1310611:08:31 48.1 97.6 21.9 59.1 

0411310611:08:41 48.2 97.6 21.9 59.1 

0411310611:08:51 48.5 97.2 22.1 59.1 

04/13/0611:09:01 48.0 97.2 22.0 59.2 

04/1310611:09:11 48.6 97.1 22.0 59.2 

0411310611:09:21 48.6 96.9 22.1 59.3 

04113/0611:09:31 48.1 96.8 22.0 59.2 

04113/0611:09:41 48.4 96.9 22.0 59.2 

04113/0611:09:51 47.9 97.0 22.0 59.2 

04/13/0611:10:01 48.1 96.9 21.9 59.2 

04/13/0611:10:11 48.4 96.9 21.9 59.3 

04113/0611:10:21 48.3 96.8 22.0 59.2 

04113/0611:10:31 48.6 96.7 22.0 59.1 

04/13/0611:10:41 47.9 96.9 22.0 59.1 

04/1310611:10:51 48.4 97.0 21.9 59.2 

04/13/0611:11:01 48.6 96.7 21.9 59.3 

0411310611:11:11 48.9 97.0 21.9 59.2 

04/1310611:11:21 48.8 97.4 21.9 59.2 

04/13/0611:11:31 48.4 97.9 21.9 59.2 

0411310611:11:41 48.2 97.7 21.9 59.1 

04/13/0611:11:51 48.6 97.9 21.9 58.9 

0411310611:12:01 48.3 98.0 21.8 59.1 

04/13/0611:12:11 48.4 98.0 21.8 59.1 

04/1310611:12:21 48.5 98.0 21.8 59.3 

04/13/0611:12:31 48.1 98.3 21.9 59.3 

04113/0611:12:41 48.6 98.6 21.9 59.3 

0411310611:12:51 48.6 98.7 21.9 59,5 

04113/0611:13:01 48.7 98.1 21.9 59.5 

04/13/0611:13:11 48.1 97.8 21.9 59.4 

04/13/0611:13:21 48.3 97,5 21.9 59.4 

04113/0611:13:31 48.1 97.0 21.9 59.3 

04113/0611:13:41 48.9 96.4 21.9 59.4 

Page 2 1 1 . 2 
4.1 13106 Run n2 

04/1310611:13:51 48.8 96.1 21.9 59.4 

04113106 11: 14: 01 49,0 95.9 21.9 59.5 

04/1310611:14:11 49.0 95.9 21.9 59.5 

0411310611:14:21 49.3 96.1 21.9 59.6 

04113/06 11: 14:31 48.9 96.4 21.9 59.7 

04113!06 11 ~ 14:41 49.0 96.7 21.9 59.8 

04113/0611:14:51 49.5 96.9 22.0 59.8 

04/13106 11:15; 01 48.8 97.3 22.0 59.7 

04/1310611:15:11 49.0 97.4 22.0 59.7 

0411310611:15:21 48.7 97.6 22.0 59.6 

04113i0611:15:31 48.4 97.9 21.9 59.6 

04113/0611:15:41 48.7 97.6 22.1 59.4 

04113/06 11 : 15: 51 48.3 97.6 22.0 59.3 

04113/0611:16:01 48.9 97.3 22.0 59.5 

0411310611:16:11 48.7 97.4 22.0 59.5 

0411310611:16:21 49.4 97.3 22.0 59.4 

04/13106 11:16:31 49,1 97.3 21.9 59.3 

0411310611:16:41 49.1 97.4 22.0 59.3 

04/1310611:16:51 49.4 97.4 22.0 59.3 

04113/0611:17:01 49.0 97.4 21.9 59.2 

04/1310611:17:11 49.4 97.3 22.0 59.1 

0411310611:17:21 49.8 97.3 22.0 59.3 

0411310611:17:31 50.3 97.3 22.0 59.2 

04113/0611:17:41 50.3 97.6 21.8 59.2 

04113/0611:17:51 49.5 97.9 21.8 59.2 

04/1310611:18:01 49.2 98.2 21.9 59.2 

04/1 3106 1 1:18:11 49.3 98.4 21.9 59.2 

04113/0611:18:21 49.3 98.3 21.8 59.2 

04113/0611:18:31 49.6 98.2 21.8 59.1 

0411310611:18:41 49.5 98.3 21.9 591 

04/1 3106 1 1:18:51 49.8 98.3 21.9 59.1 

0411 3/06 1 1:19:01 49.7 98.1 21.9 59.1 

04/13/06 11 - 19:11 496 97.8 21.9 59.2 

04/1310611:19:21 50.0 97.7 21.8 59.3 

04113/0611:19:31 49,8 97.6 21.9 59.1 

04/1 3106 1 1:19:41 49.7 97.6 21.8 58.9 

04/13/0611:19:51 49.5 98.1 21.8 58.9 

04113l06 11:20:01 48.9 98.0 21.9 58.8 Stop Interference Sample 

04113/0611:20:11 49.2 97.6 22.0 58.8 Average 59.2 

04/1310611:20:21 49.4 97.2 21.9 58.7 

04/1310611:20:31 49.6 96.6 21.7 58.6 

04/13/0611:20:41 49.3 96.1 21.8 58.5 

04113/0611:20:51 49.6 95.5 21.9 58.2 

04113/0611:21:01 49.5 95.2 21.9 58.3 

04/13/0611:21:11 49.2 95.1 21.9 58.4 

04/13/06 11:21 : 21 49.4 95.1 21.8 58.6 

04/1310611:21:31 49,7 95.4 21.7 58.5 

04/13/0611:21:41 49.7 95.7 21.7 58.5 

04113/0611:21:51 49.6 96.1 21.6 58.5 

0411310611:22:01 50.1 96.5 21.7 58.4 

04/1310611:22:11 49.8 97.1 21.7 58.3 

04/13/0611:22:21 50.0 97.6 21.7 58.4 

04113/0611:22:31 49.8 98.2 21.7 58.5 

04113/0611:22:41 49.2 98.5 21.8 58.6 

04/13/0611:22:51 48.7 98.8 21.8 58.6 

04/1310611:23:01 48.8 99.3 21.8 58.6 

04113/0611:23:11 48.8 99.6 21.8 58.8 

04113/0611:23:21 48.5 100.0 21.8 59.0 

0411310611:23:31 48.7 100.1 21.8 58.9 

04/1310611:23:41 48.2 99.9 21.8 58.9 

0411310611:23:51 48.5 99.5 21.7 58.9 

04113/0611:24:01 48.1 99.0 21.7 58.7 

0411310611:24:11 48.1 98.5 21.7 58.7 

04/13/0611:24:21 47.9 97.7 21.7 58.7 

0411310611:24:31 48.1 97.4 21.7 58.6 

04/13/0611:24:41 48.3 96.8 21.8 58.5 

003/0611:24:51 48.1 96.8 21.7 58.5 

04/1310611:25:01 48.1 97.3 21.7 58.5 

04/1310611:25:11 48.0 97.8 21.7 58.4 

04/1310611:25:21 48.2 98.1 21.7 58.3 

0411310611:25:31 48.0 98.2 21.6 58.3 

04/1310611:25:41 47.8 98.1 21.7 58.3 

0411310611:25:51 48.1 97.7 21.7 58.4 

04/13/0611:26:01 47.8 97.6 21.7 58.4 

Page 3 1 

1. 3 
4113/06 Run #2 

04/131061126:11 47.8 97.3 21.7 58.3 

04/13/0611:26:21 48.4 97.5 21.7 58.3 

04113/0611:26:31 47.5 97.6 21.7 58.3 

0411310611:26:41 47.2 98.2 21.7 58.4 

04/1310611:26:51 48.0 98.2 21.7 58.3 

04113/0611:27:01 47.7 98.0 21.8 58.3 

04113/0611:27:11 48.0 97.6 21.8 58.3 

04/13/0611:27:21 47.6 97.3 21.8 58.2 

0411310611:27:31 47.8 97.3 21.8 58.1 

0411310611:27:41 47.8 97.5 21.7 57.9 

04/131061127:51 47.9 97.6 21.7 57.9 

04/1310611:28:01 47.6 97.6 21.8 57.8 

04/13/0611:28:11 47.4 97.7 21.9 57.7 

04/13/0611:28:21 47.6 97.9 21.9 57.9 

04113/0611:28:31 47.9 98.0 21.8 57.8 

04/13/0611:28:41 47.8 98.2 21.9 57.7 

04/1310611:28:51 47.4 98.1 21.9 57.8 

04/13/06 11;29:01 47.5 97.7 21.8 57.7 

04/13/0611:29:11 47.0 97.4 21.9 57.6 

04/13/0611:29:21 48.1 97.0 21.9 57.6 

0411310611:29:31 47.8 97.0 21.8 57.7 

04/1310611:29:41 47.4 97.3 21.8 57.6 

04/1310611:29:51 47.6 97.5 21.8 57.6 

04/13/0611:30:01 47.8 97.3 21.9 57.8 

04113/0611:30:11 48.5 97.1 21.9 57.8 

0411310611:30:21 48.2 97.1 22.0 57.8 

04/1310611:30:31 47.9 97.3 22.0 57.9 

0411310611:30:41 47.8 97.2 22.1 57.9 

04/13/0611:30:51 47.6 97.0 22.1 58.1 

04113/06 11: 31:01 48.1 97.1 22.1 58.2 

0411310611:31:11 47.9 97.5 22.1 58.3 

04/1310611:31:21 47.6 98.0 22.1 58.3 

04/1310611:31:31 47.5 98.4 22.1 58.2 

04113/0611:31:41 47.7 99.3 22.1 58.4 

0411310611:31:51 47.8 99.5 22.1 58.5 

04/13/0611:32:01 48.5 99.2 22.1 58.5 

04113/0611:32:11 48.7 98.8 22.1 58.4 

0411310611:32:21 47.6 98.9 22.0 58.5 

0411310611:32:31 48.5 98.5 22.1 58.4 

04/13/0611:32741 48.7 98.2 22.1 58.5 

04/13/061132:51 48.0 98.3 22.1 58.6 

0411310611:33:01 48.1 98.4 22.0 58.6 

04/13/0611:33:11 48.1 98.2 22.1 58.5 

04/13/0611:33:21 48.5 98.2 22.2 58.4 

04113/0611:33:31 49.0 97.9 22.2 58.5 

0411310611:33:41 49.0 98.2 22.2 58.7 

04/1310611:33:51 49.3 98.8 22.1 58.8 

04/13/0611:34:01 49.0 99.1 22.1 59.0 

04/13/0611:34:11 48.6 99.5 22.1 59.1 

04113/06 11:34:21 48.6 100.1 22.1 59.1 

04113/0611:34:31 48.1 100.2 22.2 59.1 

04/1310611:34:41 49.0 99.8 22.1 59.1 

04/1 3106 1 1:34:51 49.1 99.8 22.2 59.1 

04/13106 11:35:01 49,1 99.9 22.1 59.2 

04/13/0611:35:11 48.0 75.6 21.8 58.3 

04/13/0611:35:21 48.0 46.3 21.6 57.1 

04/1310611:35:31 48.8 100.3 22.2 59.4 

04/ 13106 11:35:41 49.3 100,1 22.1 59.6 

04/13106 11:35:51 48.8 100.1 22.1 59.5 

04/1310611:36:01 48.9 100.3 22.2 59.2 

04113/0611:36:11 48,7 100.3 22.1 59.2 

0411310611:36:21 49.1 99.9 22,2 59.3 

0411310611:36:31 49.9 99.2 22.3 59.3 

04/13/0611:36:41 49.6 98.6 22.3 59.1 

04/1310611:36:51 50.1 98.5 22.3 69.1 

04113/0611:37:01 49.7 98,7 22.2 59.1 

04113/0611:37:11 49.5 98.9 22.3 59.0 

04/13/0611:37:21 49.3 99.4 22.3 59.0 

04/1310611:37:31 49.2 99.9 22.4 59.0 

04/1310611:37:41 49.6 99.7 22.3 59.1 

04/13/06 11:37:51 49.4 99.4 - 22.4 59.3 

04/13/0611:38:01 49.8 99.1 22.4 59.3 

0411310611:38:11 49.7 98,7 22.3 59.3 

0411310611:38:21 50.1 98.7 22.3 59.4 

114 

Page 4 
4113106 Run #2 

04/13106 11:38:31 49.7 98.6 22.4 59.2 

04/13/06 11:38:41 502 98.8 22,5 59.2 

04/13!0611:38:51 49.8 98.8 22.5 59.2 

04/1310611:39:01 50.2 98.9 22.4 59.2 

04113/0611:39:11 50.0 99.4 22.3 59.4 

0411 3106 1 1:39:21 49.3 99.4 22.3 59.5 

0411 3/06 1 1:39:31 49.8 99.4 22.3 59.4 

0411 3106 1 1:39:41 49.6 99.2 22.3 59.3 

0411310611:39:51 50.0 98.9 22.3 59.3 

04113/0611:40:01 50.0 98.6 22.4 59.4 

0411310611:40:11 49.8 98.2 22.3 59.4 

0411 3106 1 1:40:21 49.7 97.9 22.3 59.4 

04/13!06 11:40:31 49.7 97.5 22.3 594 

04/13/06 11:40:41 49.9 97.3 22.4 59.4 

04/13/0611:40:51 49.1 97.4 22.4 59.4 

04/13/06 11:41:01 49.2 973 22.4 59.5 

04113/0611:41:11 49.6 97.6 22.3 59.5 

04113/0611:41:21 50.0 97,8 22.3 59,6 

04113/0611:41:31 49.9 98.3 22.3 59.6 

04/1 3106 11 A1:41 49.7 98.8 22.4 59.5 

0411310611:41:51 49.2 98.9 22.4 59.3 

04/1310611:42:01 49.9 99.4 22.3 59.1 

04/1310611:42:11 49.4 99.5 22.3 59.1 

0411310611:42:21 49.4 99.4 22.3 59.1 

04/1310611:42:31 49.1 99.4 22.3 59.2 

04/13/0611:42:41 49.6 99.3 22.3 59.3 

04/1310611:42:51 50.5 99.3 22.3 59.4 

0411310611:43:01 49.8 99.8 22.3 59.4 

04113/0611:43:11 50.2 99.9 22.3 59.6 

0411310611:43:21 49.5 99.9 22.2 59.7 

041131061143:31 49.2 100.0 22.3 59.8 

04/1310611:43:41 49.1 100.1 22.2 59.7 

04/13/0611:43:51 48.6 99.9 22.4 59.6 

04/13J0611:44:01 48.8 99.9 22.4 59.7 

0411 3106 1 1:44:11 48.7 99.8 22.3 59,8 

04/13/06 11:44:21 48.7 99.7 22.3 591 

04/1310611:44:31 48.7 99.7 22.2 59.7 

04/1310611:44:41 48.6 99.2 22.3 59.7 

0411310611:44:51 48.8 98.5 22.4 59.7 

0411 3/06 1 1:45:01 48.9 97.8 22.4 59.8 

04/1310611:45:11 49.0 97.4 22.4 59.8 

0411 3/06 1 1:45:21 49.2 96.9 22.3 59.8 

04113/0611:45:31 49.4 96.6 22.3 59.5 

04/13/0611:45:41 48.9 96.7 22.3 59.7 

04/1310611:45:51 48.9 97.3 22.3 59.7 

04/1310611:46:01 48.2 98.2 22.1 59.6 

0411310611:46:11 48.6 98.8 22.1 59.6 

0411310611:46:21 48.3 99.3 22.2 59.6 

0411310611:46:31 48.5 100.2 22.2 59.6 

0411310611:46:41 48.8 100.7 22.3 59.6 

0411310611:46:51 48.8 101.1 22.2 59.7 

0411310611:47:01 48.4 100.9 22.2 59.6 

0411 3106 1 1:47:11 48.1 100.7 22.2 59.5 

0411 3106 1 1:47:21 48.2 99.8 22.2 59.6 

04113/0611:47:31 48.6 99.2 22.2 59.6 

04113/0611:47:41 49.0 99.1 22.3 59.4 

04/13/06 11'47:51 48.7 99.1 22.2 59.4 

04113J0611:48:01 48.8 99.2 22.2 59.4 

04/13/0611:48:11 48.6 99.3 22.2 59.4 

0411310611:48:21 48.9 99.2 22.3 59.4 

0411310611:48:31 48.4 98.6 22.3 59.4 

04/13/06 11 - 48:41 48.5 97.9 22.3 59.3 

04/1310611:48:51 48.7 97.3 22.3 59.3 

04/13/0611:49:01 48.2 97.1 22.3 59.3 

0411310611:49:11 48.9 97.3 22.3 59.4 

0411310611:49:21 48.7 97.6 22.3 59.4 

04!13J06 11:49:31 48.7 97.6 22.3 593 

04/13/0611:49:41 48.3 97.7 22.3 59.3 

04113/0611:49:51 49.0 97.6 22.1 59.3 

0411310611:50:01 49.0 97.6 22.2 59.4 

04113/0611:50:11 49.7 97.8 22.1 59.3 

04113J0611:50:21 49.4 98.2 22.1 59.2 

0411310611:50:31 49.4 98.7 22.2 59.4 

0411310611:50:41 49.7 98.8 22.2 59.4 

Page 5 1 1. ~ 
4113106 Run #2 

04113/0611:50:51 49.1 99.0 22.1 59.2 

04/1310611:51:01 48.9 99.4 22.1 59.1 

04113/0611:51:11 48.9 99.1 22.1 591 

04113/0611:51:21 49.0 98.6 22.1 59.1 

0411310611:51:31 48.2 98.2 22.0 58.9 

04/1310611:51:41 48.6 97.7 22.1 58.8 

04/1310611:51:51 47.8 68.0 22.0 58.7 

Stop Run #2 48.86 97.94 21.93 58.95 

04/13/06 11:52:01 48.5 96.1 22.2 58.7 

0411310611:52:11 33.4 95.2 22.1 58.7 

04/13/0611:52:21 14.8 89.4 21.8 58.5 

0411310611:52:31 19.3 58.0 16.8 56.3 

04/1 3106 1 1:52:41 20.0 29.8 10.4 50 a 

04/1310611:52:51 20.2 16.4 7.2 42.6 

04/1310611:53:01 20.4 9.9 6.0 35.4 

04113/0611:5311 18.1 6.4 5.7 29.7 

04/1310611:53:21 15.3 4.6 5.4 24.8 

0411310611:53:31 12.8 3.3 4.8 21.2 

04/1310611:53:41 9.4 2.6 4.1 18.4 

04/13/0611:53:51 7.1 7.4 3.4 15.5 

04113/0611:54:01 4.8 64.6 2.6 12.7 

04113/06 11:54:11 3.7 116.5 2.4 10.6 

04113/0611:54:21 3.2 151.6 2.3 9.9 

04/1310611:54:31 2.9 175.2 1.7 8.3 

04/13106 11:54:41 2.6 184.5 1.5 6.6 

04/13/0611:54:51 2.4 188.9 1.3 5.0 

0411310611:55:01 2.3 191.1 1.2 3.9 

0411310611:55:11 2.2 192.3 1.2 ' 3.1 

04113/0 6 11: 5 5: 21 2.2 19 3. 0 1.1 2.5 

04/13/06 11:55:31 2.0 193.4 1.0 2.1 

04 / 13106 11: 55:41 2.0 193.6 1.0 1.7 

04 / 13/06 11: 55:51 1.9 193.7 1.0 1.5 

04113/0611:56:01 1.9 193.7 0.9 1.0 

04/1310611:56:11 1.9 193.7 0.8 0.7 

04113/06 11:56:21 1.9 193.8 0.7 0.6 

04113106 11:56:31 1.9 193.9 0.7 0.5 

04/13/0611:56:41 1.8 194.1 0.7 0.5 

04/13/06 11:56:51 1.9 184.7 0.7 0.4 

04/13/0611:57:01 1.6 118.7 5.2 0.3 

04113/06 11:57:11 1.4 59.4 14.1 0.2 

04/13/06 11:57:21 1.3 29.9 19.1 0.2 

04/13/06 11:57:31 1.2 16.2 21.3 0.2 

04/1310611:57:41 1.3 9.9 22.4 0.2 

04/1310611:57:51 1.1 6.8 22.9 0.1 

04113/0611:58:01 1.0 5.3 23.1 0.1 

04/13/0611:58:11 1.2 4.4 23.3 -0.1 

04/13/0611:58:21 1.2 3.7 23.4 0.0 

04113/0611:58:31 1.2 2.9 23.5 0.0 

04/1310611:58:41 1.3 2.4 23.5 -0.1 

04/1310611:58:51 1,3 2.1 23.6 0.0 

04/13/0611:59:01 1.3 1.8 23.7 0.0 

04/13/0611:59:11 1.1 1.6 23.7 -0.1 

04/13/0611:59:21 1.1 1.5 23.7 -0.2 

04/13/0611:59:31 1.1 1.4 23.7 -0.2 

0411310611:59:41 1.4 1.2 23.7 -0.1 

04113/0611:59:51 1.8 1.1 23.6 -0.1 

04/13/0612:00:01 3.0 1.0 23.5 -0.1 

0411310612:00:11 3.5 1.1 20.8 -0.1 

04/13/06 12:00:21 3.8 1.2 11.6 -0.1 

04/1310612:00:31 3.7 1.2 5.8 -0.1 

04113J0612:00:41 3.3 1.0 3.1 0.0 

04113/0612:00:51 2.0 0.7 1.9 0.0 

04/13/0612:01:01 1.6 0.4 1.5 2.7 

04/13/06 12:01:11 1.3 0.3 1.3 12.0 

04/1 3106 1 2:01:21 1.1 0.3 1.1 24.7 

04113/0612:01:31 1.1 0.2 1.0 37.1 

04/1310612:01:41 1.2 0.3 1.0 48.0 

04/13106 12:01:51 1.3 0.3 1.0 57.0 

04113/0612:02:01 1.1 0.3 1.0 64.2 

04113/0612:02:11 0.9 0.4 0.9 69.9 

04113/0612:02:21 1.1 0.5 0.7 74.2 

200 ppm CO 

Zero NOx 

25.5 ppm NOx 

Zero CO, S02 

11.6 

Page 6 
4113106 Ftun 42 

04113/0612:02:31 1.2 0.4 0.7 77.4 

04l13/06 12:02:41 1.1 0.4 0.7 80.2 

04113/0612:02:51 1.1 0.3 0.6 82.1 

04113106 12:03:01 1.1 0.4 0.6 83.5 

04/1310612:03:11 1.1 0.3 0.7 84.5 

0411310612:03:21 1.1 0.3 0.6 85.3 

0411310612:03:31 1.1 0.3 0.5 86.4 

04/1310612:03:41 1.0 -18.2 0.6 86.8 

0411310612:03:51 1.0 -53.5 0.5 86.6 

0411310612:04:01 1.0 0.3 0.5 89.3 

0411310612:04:11 1:0 0.3 0.6 90.0 

04/1310612:04:21 1.0 0.3 0.5 90.5 

0411310612:04:31 1.1 0.3 0.5 91.2 

04113/06 12:04:41 1.1 0.4 0.5 91.6 

04113/0612:04:51 1.1 0.3 0.4 92.0 

0411310612:05:01 1.0 0.3 0.4 92.4 

0411310612:05:11 1.0 0.3 0.4 92.6 

0411310612:05:21 1.0 0.3 0.4 92.9 

04113/0612:05:31 0.8 0.2 0.4 93.1 

04/1310612:05:41 0.8 0.2 0.5 93.2 

04/1310612:05:51 0.8 0.2 0.4 93.4 

04113/0612:06:01 0.9 0.2 0.5 93.6 

0411310612:06:11 1.0 0.0 0.4 93.8 

04113/0612:06:21 1.1 0.0 0.4 93.9 

04/13/06 12:06:31 1.1 0.1 0.3 93.9 

0411310612:06:41 0.8 0.1 0.4 94.2 

0411310612:06:51 0.8 0.0 0.4 94.2 

0411310612:07:01 1.0 0.0 0.4 94.3 

0411310612:07:11 1.0 0.0 0.4 94.4 

0411310612:07:21 0.9 0.2 0.3 94.4 

0411310612:07:31 0.8 0.2 0.4 94.6 

04113l0612:07:41 0.8 0.3 0.4 94.5 

04113/0612:07:51 0.9 0.3 0.5 94.6 

04/1310612:08:01 1.2 0.2 0.4 94.6 

0411310612:08:11 23.6 0.2 0.5 94.6 

04l13/0612:08:21 42.1 0.3 0.4 94.4 

0411310612:08:31 41.8 0.3 0.3 89.7 

04113/0612:08:41 41.7 0.3 0.1 78.2 

0411310612:08:51 41.8 0.3 0.1 64.5 

04113106 12:09:01 41.8 0.3 0.1 51.3 

0411310512:09:11 41.8 0.3 0.1 40.5 

04/13/06 12:09:21 41.7 0.3 0.1 31.8 

04113/0612:09:31 41.6 0.3 0.1 25.2 

Zero VOC 

100 ppm S02 

40.8 ppm CH4 

11. "' 

Page 7 
4/13106 Rtm 93 

Date/Tfine VOC CO NOx S02 

mm/dd/yy hh:mm:ss ppm ppm ppm ppm 

04/1310612:14:51 49.0 93.5 21.0 58.2 

start Run tt3 

04113/0612:15:01 48.8 94.0 20.9 58.4 

04113/0612:15:11 49.1 94.5 20.9 5B.4 

04113/0612:15:21 48.7 94.7 21.0 58.6 

0411310612:15:31 48.8 94.8 21.1 58.8 

0411310612:15:41 48.6 94.7 21.0 59.0 

0411310612:15:51 48.5 94.2 21.0 59.0 

04113/0612:16:01 48.5 94.2 21.0 59.0 

04/13/0612:16:11 48.4 94.3 21.0 59.0 

04/1310612:16:21 47.9 94.5 21.1 59.3 

04113/0612:16:31 48.0 94.7 21.1 59.4 

04/1310612:16:41 48.2 94.9 21.1 59.6 

04/1310612:16:51 48.3 94.9 21.2 59.5 

04113/0612:17:01 48.2 95.3 21.2 59.7 

04/13/0612:17:11 47.8 95.7 21.1 59.6 

04/1310612:1721 47.9 96.1 21.1 59.6 

0411310612:17:31 47.8 96.6 21.1 59.6 

04/1310612:17:41 47.5 96.8 21.1 59.6 

04/1310612:17:51 47.4 97.3 21.2 59.6 

04113/0612:18:01 47.3 97.4 21.2 59.6 

0411310612:18:11 47.7 97.4 21.3 59.5 

0411310612:18:21 47.4 96.9 21.3 59.5 

04113f0612:18:31 47.5 96.2 21.2 59.4 

04/1310612:18:41 48.0 95.3 21.3 59.4 

04/13/0612:18:51 48.2 95.1 21.2 59.5 

0411310612:19:01 47.4 95.1 21.2 59.6 

04/13/0612:19:11 47.9 95.2 21.3 59.4 

04113/0612:19:21 48.2 94.9 21.3 59.2 

04/1310612:19:31 47.8 94.9 21.3 59.2 

04/13/0612:19:41 47.9 95.3 21.4 59.2 

04113/0612:19:51 47.7 96.0 21.5 59.1 

04/13/0612:20:01 47.2 96.7 21.4 59.2 

04113/0612:20:11 47.6 96.8 21.4 59.2 

04113/0612:20:21 48.0 96.8 21.4 59.2 

0411310612:20:31 48.0 96.5 21.4 59.1 

0411310612:20:41 48.4 96.1 21.5 59.2 

04/13/0612:20:51 48.1 95.6 21.5 59.2 

04113/0612:21:01 48.0 95.5 21.5 59.2 

0411310612:21:11 48.1 95.4 21.4 59.1 

04113/0612:21:21 48.2 95.3 21.5 59.1 

04/1310612:21:31 49.2 95.3 21.6 59.0 

04/1310612:21:41 47.9 95.1 21.6 59.0 

04/1310612:21:51 48.6 94.6 21.6 59.1 

04/1310612:22:01 48.3 94.1 21.7 59.1 

04/13/0612:22:11 48.5 93.8 21.7 59.1 

0411310612:22:21 48.6 93.3 21.6 59.1 

04/13/0612:22:31 48.6 93.6 21.6 59.1 

04/13/0612:22:41 48.3 93.3 21.5 59.1 

04113/0612:22:51 48.3 93.1 21.6 59.0 

04/1310612:23:01 49.3 92.5 21.7 59.1 

0411310612:23:11 49.4 91.9 21.6 59.1 

04113/061223:21 49.3 91.9 21.6 59.1 

04113/0612:23:31 49.5 91.9 21.6 59.0 

04/1310612:23:41 50.4 92.1 21.6 58.9 

04113/0612:23:51 50.6 92.5 21.6 59.0 

04113/0612:24:01 50.0 92.9 21.6 58.9 

04113/0612:24:11 49.7 93.1 21.7 58.9 

04113/0612:24:21 49.7 93.6 21.7 59.0 

0411310612:24:31 50.3 94.0 21.7 59.1 

0411310612:24:41 50.3 94.4 21.7 59.1 

04/1310612:24:51 50.7 94.7 21.7 58.9 

04113/0612:25:01 50.3 94.7 21.7 58.9 

04/1310612:25:11 50.0 94.9 21.6 58.9 

04/1310612:25:21 50.2 94.9 21.6 58.9 

04/1310612:25:31 50.0 95.5 21.6 58.8 

04/13/0612:25:41 50.0 95.8 21.5 58.8 

04/13J0612:25:51 49.2 96.4 21.5 58.7 

04/1310612:26:01 49.5 95.4 21.6 58.8 

04/1310612:26:11 49.4 96.4 21.7 58.8 

04/13/0612:26:21 49.6 96.1 21.6 58.7 

Page 1 118 
4113106 Run #3 

04113/0612:26:31 49.5 95.6 21.6 58.5 

04113/0612:26:41 49.9 95.5 21.7 58.4 

0411310612:26:51 49.7 94.9 21.7 58.3 

04/13/0612:27:01 49.9 94.4 21.7 58.2 

0411310612:27:11 50.4 94.1 21.8 58.2 

04113/06 12:27:21 49.9 94.1 21.8 58.4 

04/1310612:27:31 50.0 94.4 21.8 58.4 

04/1310612:27:41 50.3 94.8 21.6 58.3 

04113106 12:27:51 49.9 95.5 21.6 56.2 

0411310612:28:01 49.5 95.8 21.5 58.1 

04/13106 12:28:1 , 49.4 96.0 21.6 58.0 

04/1310612:28:21 49.6 95.8 21.6 57.9 

0411310612:28:31 49.9 95.6 21.6 58.1 

04113/0612:28:41 50.0 95.2 21.6 58.1 

04113/0612:28:51 50.4 94.7 21.6 58.1 

04113/0612:29:01 50.5 94.5 21.6 58.0 

0411310612:29:11 49.8 94.4 21.6 58.0 

04113/0612:29:21 50.0 94.3 21.6 58.0 

0411310612:29:31 50.1 94.4 21.6 58.0 

04/1310612:29:41 49.9 94.3 21.5 57.9 

04113/0612:29:51 49.9 94.4 21.5 57.9 

0411310812:30:01 50.0 94.5 21.5 57.7 

0411310612:30:11 49.4 94.8 21.6 57.8 

04/13/0612:30:21 49.6 95.0 21.5 57.8 

04113/061230:31 49.3 95.6 21.5 57.8 

04l1310612:30:41 48.7 96.1 , 21.5 57.8 

04/13/0612:30:51 48.2 96.3 21.5 57.8 

04/13/0612:31:01 47.9 96.7 21.5 57.7 

04/13/0612:31:11 48.0 96.3 21.5 57.5 

04113/0612:31:21 47.9 96.3 21.4 57.5 

04/1310612:31:31 48.0 96.3 21.5 57.3 

0411310612:31:41 48.1 96.3 21.5 57.1 

04/1310612:31:51 47.8 96.3 21.5 57.1 

04/1310612:32:01 48.4 96.0 21.6 57.2 

04/13/0612:32:11 48.2 95.7 21.5 57.2 

04/1310612:32:21 47.8 95.3 21.5 57.1 

04113/0612:32:31 48.0 95.4 21.5 57.1 

04113/0612:32:41 47.6 95.5 21.5 57.4 

04113/0612:32:51 47.7 95.7 21.6 57.4 

04/13/0612:33:01 48.0 95.5 21.7 57.5 

04/1310612:33:11 48.2 95.2 21.6 57.6 

04/1310612:33:21 48.7 95.0 21.6 57.6 

0411310612:33:31 47.8 94.8 21.6 57.8 

04/1310612:33:41 48.0 95.3 21.6 57.7 

0411310612:33:51 47.7 95.6 21.6 57.7 

04/1310612:34:01 47.4 95.9 21.6 57.8 

04/1310612:34:11 47.2 96.4 21.6 57.9 

04/1310612:34:21 47.7 96.5 21.6 57.8 

04/13/0612:34:31 47.9 96.5 21.5 57.8 

04/1310612:34:41 47.3 96.0 21.5 57.7 

04/1310612:34:51 48.2 95.3 21.5 57.7 

0411310612:35:01 47.9 94.5 21.6 57.7 

04113/0612:35:11 48.0 94.2 21.7 57.6 

04/1310612:36:21 48.0 94.0 21.6 57.4 

0411310612:35:31 48.2 93.9 21.6 57.4 

04/13/0612:35:41 48.3 94.0 21.6 57.4 

0411310612:35:51 48.2 94.3 21.5 57.3 

04/13/0612:36:01 47.7 94.8 21.6 57.3 

04113/0612:36:11 47.9 95.0 21.5 57.2 

04113/0612:36:21 48.2 95.2 21.5 57.2 

04/13/0612:36:31 47.1 95.4 21.6 57.1 

04/1310612:36:41 47.5 95.3 21.6 57.3 

0411 3106 1 2:36:51 47.6 95.2 21.5 57.2 

04/1310612:37:01 47.3 95.6 21.5 57.2 

04/13/0612:37:11 47.3 95.7 21.4 57.2 

04/1310612:37:21 47.3 95.8 21.4 57.3 

0411310612:37:31 47.3 95.6 21.5 57.2 

04113/0612:37:41 48.0 95.3 21.5 57.1 

04/1310612:37:51 47.7 95.5 21.5 57.1 

0411310612:38:01 47.3 96.0 21.5 57.2 

04113/0612:38:11 47.2 96.4 21.5 57.1 

04/13/0612:38:21 47.4 96.4 21.5 57.2 

04/13/0612:38:31 47.6 96.6 21.4 57.2 

04/1310612:38:41 47.3 96.1 21.5 57.3 

Page 2 j i g, 
4113i06 Rur #3 

04113/0612:38:51 47.4 95.5 21.5 57.3 

0411310612:39:01 48.6 95.2 21.4 57.4 

04/1310612:39:11 48.0 94.9 21.4 57.3 

0411310612:39:21 49.3 94.5 21.5 57.3 

04/13/0612:39:31 49.2 94.2 21.4 57.3 

04/1310612:39:41 49.3 94.0 21.4 57.2 

04/1310612:39:51 49.5 93.9 21.4 57.2 

04/1310612:40:01 49.6 93.8 21.3 57.0 

4411310612:40:11 49.9 94.1 21.4 57.0 

0411310612:40:21 49.4 94.7 21.5 57.3 

04/13/0612:40:31 49.4 94.8 21.6 57.3 

0411310612:40:41 49.3 95.0 21.6 57.4 

04J1310612:40:51 492 95.4 21.5 57.4 

04/13/0612:41:01 49.0 95.0 21.4 57.4 

04/1310612:41:11 49.7 94.4 21.6 57.2 

04/13/0612:41:21 49.9 94.5 21.6 57.0 

04/1310612:41:31 49.5 94.8 21.6 56.9 

0411310612:41:41 49.6 94.8 21.6 56.9 

0411310612:41:51 49.5 95.0 21.7 56.9 

04/13/0612:42:01 49.4 95.1 21.6 56.9 

04/1310612:42:11 49.6 94.8 21.6 56.9 

04/1310612:4221 49.7 95.1 21.7 56.9 

04/13/0612:42:31 49.8 95.2 21.7 57.0 

04113/0612:42:41 49.4 95.9 21.7 57.0 

04/13/0612:42:51 50.4 96.4 21.7 57.0 

3411310612:43:01 49.6 96.8 21.8 57.1 

04113/0612:43:11 49.6 97.0 21.7 57.3 

04113/0612:43:21 49.9 96.7 21.6 57.3 

0411310612:43:31 49.4 96.9 21.6 57.3 

04/13/0612:43:41 49.6 96.7 21.6 57.2 

04/1310612:43:51 49.7 96.8 21.6 57.1 

04/13/0612:44:01 49.0 96.9 21.5 57.0 

04/13/0612:44:11 49.5 97.0 21.5 57.0 

0411310612:44:21 49.5 97.2 21.6 57.0 

04/13/0612:44:31 49.8 96.8 21.6 57.0 

04113/0612:44:41 49.6 95.9 21.7 57.1 

04113/0612:44:51 49.9 94.9 21.7 57.0 

04113/06 12:45:01 50.1 93.9 21.7 57.1 

04113/0612:45:11 50.0 93.8 21.6 57.1 

0411310612:45:21 49.9 94.3 21.7 57.3 

04113/0612:45:31 49.6 95.0 21.6 57.4 

0411310612:45:41 49.8 96.0 21.6 57.3 

0411310612:45:51 49.8 96.3 21.6 57.2 

04/1310612:46:01 49.8 96.3 21.6 57.2 

04/1310612:46:11 49.4 96.1 21.6 57.3 

04/13/0612:46:21 49.6 95.8 21.6 57.4 

0411310612:46:31 49.5 95.7 21.6 57.4 

04/1310612:46:41 49.7 95.5 21.6 57.2 

04/13/0612:46:51 49.9 95.1 21.5 57.4 

04113/0612:47:01 49.6 94.8 21.4 57.3 

0411310612:47:11 49.5 94.6 21.5 57.3 

04/13/0612:47:21 49.6 94.4 21.6 57.3 

04/1310612:47:31 49.5 95.0 21.6 57.4 

04/1310612:47:41 49.4 95.9 21.6 57.6 

04/13/0612:47:51 49.3 96.8 21.5 57.5 

04/1310612:48:01 49.1 97.3 21.5 57.7 

04113/0612:48:11 48.7 97.3 21.5 57.7 

04/13/0612:48:21 48.6 96.8 21.6 57.8 

04/1310612:48:31 49.1 96.4 21.6 57.9 

0411310612:48:41 48.9 95.8 21.5 57.7 

0411310612:48:51 49.0 95.3 21.6 57.8 

0411310612:49:01 48.8 95.3 21.6 57.7 

04113l0612:49:11 48.7 95.3 21.6 57.6 

04f1310612:49:21 48.9 95.6 21.6 57.7 

04113/0612:49:31 48.1 63.9 21.4 55.1 

0411310612:49:41 47.6 21.7 21.4 56.9 

0411310612:49:51 48.2 94.8 21.6 58.0 

04/1310612:50:01 47.9 94.1 21.6 58.0 

0411310612:50:11 48.3 93.9 21.6 57.9 

0411310612:50:21 48.2 93.9 21.5 57.9 

04/13/0612:50:31 48.0 94.4 21.5 57.9 

04113/0612:50:41 47.9 94.4 21.5 57.8 

04/13/0612:50:51 47.9 94.9 21.5 57.8 

04/1310612:51:01 47.7 95.1 21.5 57.8 

Page 3 120 
411310$ Rtjn 93 

04/1310612:51:11 47.8 94.9 21.6 57.9 

04/13106 12:51:21 48.0 94.8 21.5 58.0 

041310612:51:31 48.2 94.6 21.5 57.9 

04113/0612:51:41 48.0 94.9 21.6 57.9 

0411310612:51:51 47.7 95.2 21.6 58.0 

04/13/0612:52:01 48.1 95.1 21.7 57.9 

04113/0612:52:11 47.8 95.0 21.6 57.7 

04!13/06 12:52:21 48.5 95.2 21.6 57.7 

44l13t0612:52:31 47.9 95.3 21.6 57.7 

0411310612:52:41 47.5 95.3 21.6 57.9 

04/1310612:52:61 47.8 95.0 21.6 58.2 

0411310612:53:01 48.5 94.6 21.7 58.4 

04113/0612:53:11 48.9 94.6 21.7 58.2 

0411310612:53:21 48.7 94.4 21.8 58.1 

04/1310612:53:31 48.9 94.4 21.8 58.2 

0411310612:53:41 48.6 94.6 21.8 58.1 

04/13/0612:53:51 48.2 95.2 21.7 58.1 

04113/0612:54:01 48.2 95.6 21.7 58.1 

04/13/0612:54:11 48.0 95.5 21.8 58.1 

0411310612:54:21 48.0 95.6 21.9 58.1 

04/13/0612:54:31 48.8 95.3 21.9 58.1 

04/13/0812:54:41 48.4 94.8 21.9 58.3 

04113/0612:54:51 48.8 94.4 21.9 58.4 

04/13/0612:55:01 49.1 94.4 21.9 58.3 

04/1310612:55:11 49.1 94.5 21.9 58.3 

0411310612:55:21 48.7 95.2 22.0 58.3 

04/13/0612:55:31 49.3 95.4 21.9 58.6 

0411310612:55:41 48.9 95.8 21.9 58.6 

04/1310612:55:51 49.0 96.4 21.9 58.5 

04/1310612:56:01 48.4 97.1 21.9 58.4 

04/13/0612:56:11 48.1 97.2 21.9 58.5 

04113/0612:56:21 48.7 96.9 21.9 58.6 

04/1310612:56:31 48.9 96.7 22.0 58.6 

04/13/0612:56:41 48.9 96.2 22.0 58.4 

04/1310612:56:51 49.1 95.9 22.0 58.2 

04/13/0612:57:01 49.2 95.8 22.0 58.3 

04113!0612:57:11 48.8 95.4 21.9 58.3 

04/1310612:57:21 48.6 94.9 21.8 58.3 

04/13/0612:57:31 49.3 94.1 21.8 58.2 

04113/0612:57:41 50.0 93.7 21.9 58.1 

04113/0612:57:51 50.5 93.8 21.9 58.1 

04113/0612:58:01 50.0 94.2 21.9 58.0 

0411310612:58:11 50.3 94.6 21.9 58.0 

04113/0612:58:21 50.0 94.7 21.9 58.1 

04/13/0612:58:31 50.2 94.5 21.9 58.2 

0411310612:58:41 50.3 94.3 22.0 58.1 

04113/0612:58:51 50.1 94.1 22.0 58.1 

04/13/06 12:59:01 50.5 93.7 21.9 58.3 

04/1310612:59:11 50.4 93.3 21.8 58.2 

04113/0612:59:21 51.3 93.4 21.7 57.9 

04/1310612:59:31 51.3 93.6 21.8 57.9 

04/1310612:59:41 51.2 93.9 21.9 57.9 

04113/0612:59:51 51.6 94.0 21.8 58.1 

04113/0613:00:01 51.4 93.8 21.8 58.1 

0411 3/06 1 3:00:11 51.6 93.6 21.9 58.0 

0411310613:00:21 50.8 93.8 21.8 58.0 

04113/0613:00:31 51.8 93.9 21.8 57.9 

0411310613:00:41 51.6 94.2 21.8 57.9 

04/13/0613:00:51 51.2 94.5 21.7 57.8 

04/13106 13:01:01 51.1 94.7 21.7 57.8 

04/1310613:01:11 50.8 95.0 21.7 57.9 

04113/0613:01:21 50.6 95.0 21.6 57.9 

04/1310613:01:31 51.2 94.9 21.6 57.9 

0411310613:01:41 51.4 95.0 21.7 57.8 

04/13/0613:01:51 51.3 95.1 21.7 57.7 

0411310613:02:01 51.2 95.4 21.7 57.9 

04/13/0613:02:11 50.1 95.7 21.7 57.7 

04/1310613:02:21 50.7 95.8 21.6 57.6 

04/1310613:02:31 50.1 95.8 21.6 57.6 

0411310613:02:41 50.6 96.0 21.6 57.7 

04/13/0613:02:51 50.1 96.2 21.6 57.5 

04/1310613:03:01 50.2 96.2 21.7 57.4 

0411310613:03:11 50.2 95.6 21.6 57.5 

04/1310613:03:21 49.9 95.0 21.6 57.5 

Page 4 1?1 
4/13i05 Run 93 

04/13/0613:03:31 50.4 93.9 21.5 57.4 

04/1310613:03:41 50.0 93.2 21.6 57.5 

04/13/0613:03:51 50.1 92.3 21.6 57.6 

04J1310613:04:01 50.0 91.8 21.7 57.4 

04r13106 13:04:1 Z 50.1 91.8 21.7 57.4 

04113/0613:04:21 49.6 92.5 21.7 57.4 

04/1310613:04:31 49.2 93.3 21.6 57.4 

04/13J0613:04:41 49.5 93.6 21.7 57.3 

0411310613:04:51 49.2 93.8 21.7 57.3 

04/1310613:05:01 49.3 93.4 21.7 57.4 

04/13/0613:05:11 49.2 93.1 21.7 57.3 

0413/0613:05:21 49.4 93.0 21.5 57.3 

0411310613:05:31 48.5 93.3 21.6 57.3 

04l13/0613:05:41 48.4 93.5 21.7 57.2 

0411310613:05:51 48.7 93.8 21.7 57.1 

0411310613:06:01 48.2 94.4 21.5 57.1 

04/1310613:06:11 48.8 94.6 21.5 57.1 

04113/0613:06:21 48.2 94.7 21.5 57.1 

0411310613:06:31 48.7 94.7 21.6 57.1 

04/13/0613:06:41 48.5 94.2 21.6 57.2 

04113/0613:06:51 48.3 93.3 21.6 57.3 

04/1310613:07:01 49.0 92.9 21.6 57.5 

04/13/0613:07:11 49.0 92.9 21.5 57.5 

04/1310613:07:21 48.2 93.2 21.5 57.6 

04/13/0613:07:31 47.8 93.3 21.6 57.6 

04/1310613:07:41 48.4 93.1 21.6 57.7 

04/13/0613:07:51 48.8 93.0 21.6 57.9 

04/13/0613:08:01 49.4 93.3 21.6 57.9 

04/13/0613:08:11 48.7 93.2 21.5 57.9 

04/1310613:08:21 48.7 93.6 21.4 57.8 

04/13/0613:08:31 48.2 93.8 21.6 57.8 

04/1310613:08:41 48.1 93.5 21.5 57.9 

0411310613:08:51 48.1 93.4 21.4 57.9 

04/1310613:09:01 48.7 93.0 21.4 57.9 

04113/0613:09:11 48.5 92.5 21.5 57.8 

04113J0613:09:21 48.8 92.0 21.6 57.9 

04/13/0613:09:31 49.0 91.8 21.5 58.1 

04/13/0613:09:41 49.1 92.0 21.5 58.1 

04113/0613:09:51 49.3 92.0 21.5 58.0 

04113/0613:10:01 48.8 91.7 21.5 58.2 

04/13/0613:10:11 49.1 91.8 21.6 58.1 

04/1310613:10:21 49.0 92.1 21.5 58.1 

04113/061310:31 48.7 93.3 21.4 58.0 

04/1310613:10:41 48.1 94.0 21.5 57.9 

04/13/0613:10:51 48.2 94.5 21.5 57.8 

04/1310613:11:01 48.0 94.5 21.5 58.1 

04/1310613:11:11 48.4 94.4 21.4 58.0 

04/1310613:11:21 48.7 93.9 21.4 58.0 

04/1310613:11:31 49.2 93.1 21.5 57.9 

04113/0613:11:41 49.6 92.4 21.5 57.7 

04113/0613:11:51 49.6 91.8 21.6 57.8 

04/1310613:12:01 49.8 92.0 21.5 57.8 

0411310613:12:11 50.1 92.5 21.4 57.8 

04/1310613:12:21 49.7 92.7 21.4 57.8 

0411310613:12:31 49.4 93.3 21.5 57.8 

04/13/0613:12:41 49.7 93.1 21.5 57.7 

0411310613:12:51 50.5 93.0 21.5 57.6 

0411310613:13:01 49.9 93.2 21.5 57.6 

0411310613:13:11 49.8 93.3 21.4 57.6 

04/13/06 13:13:21 49.1 93.2 21.5 57.8 

04/13/0613:13:31 49.3 93.1 21.5 57.7 

04/1310613:13:41 50.0 92.8 21.5 57.6 

04/13/0613:13:51 50.4 92.4 21.5 57.5 

04/1310613:14:01 50.4 92.0 21.5 57.6 

04/13/0613:14:11 50.4 91.8 21.6 57.7 

04/13/0613:14:21 50.9 91.7 21.6 57.7 

04/13/0613:14:31 51.0 91.4 21.6 57.9 

04/13/0613:14:41 51.7 91.3 21.6 58.0 

04/13/0613:14:51 51.0 91.3 21.5 57.7 

04/13/06 13:15:01 51.2 91.9 21.5 57.6 

04/1310613:15:11 50.5 92.6 21.5 57.7 

0411310613:15:21 50.3 92.7 21.5 57.6 

04/1310613:15:31 50.6 92.5 21.5 57.6 

04/13/0613:15:41 50.4 92.4 21.5 57.6 

Page 5 1?2 
4!13/06 Run tt3 

04113/0613:15:51 51.0 92.3 21.6 57.6 

04113l0613:16:01 50.8 92.6 21.5 57.7 

0411310613:16:11 51.1 92.8 21.5 57.4 

04/1310613:16:21 50.4 93.3 21.4 57.3 

04/1310613:16:31 50.0 93.8 21.5 57.4 

04/1310613:16:41 49.6 52.3 21.3 55.8 

04/13/0613:16:51 49.7 87.1 21.4 57.1 

Stop Run #3 49.08 94.26 21.57 57.93 

04113/0613:17:01 37.7 92.8 21.6 57.0 

04113/0613:17:11 8.5 87.6 21.3 56.9 

04!1310613:17:21 9.9 57.6 16.5 54.5 

04113/0613:17:31 8.8 28.9 9.6 48.1 

04/13/06 13:17:41 6.9 15.2 5.9 40.3 

04/1310613:17:51 4.7 9.0 4.2 33.1 

04113/0613:18:01 3.6 45.7 3.2 26.6 

04/1310613:18:11 3.1 109.8 2.4 20.4 

04/13I06 13:18:21 3.1 143.7 2.6 16.1 

04J1310613:18:31 2.9 167.2 2.2 13.1 

04113106 13:18:41 2.9 178.7 1.7 10.6 

04113106 13:18:51 2.8 183.9 1.5 8.3 

04/13/06 13:19:01 2.7 187.0 1.3 6.3 

04113106 13:19:11 2.5 189.0 1.2 4.5 

04113l0613:19:21 2.5 190.3 1.2 3.2 

04113/06 13:19:31 2.4 190.9 1.2 2.1 

04113106 13:19:41 2.6 '191.4 1.1 1.3 

04/13/06 13:19:51 2.6 191.5 1.0 0.7 

04113/06 13:20:01 2.4 191.9 0.9 0.3 

04/13/06 13:20:11 2.4 191.9 0.9 0.1 

0411310613:20:21 2.3 192.2 0.9 -0.1 

04/1310613:20:31 2.2 192.3 0.8 -0.3 

04l1310613:20:41 2.1 192.3 0.7 -0.5 

04/1310613:20:51 2.3 192.3 0.7 -0.7 

04113/0613:21:01 2.4 192.3 0.6 -0.8 

04/13/0613:21:11 2.4 192.1 0.6 -0.9 

04/13/0613:21:21 2.3 191.9 0.7 -1.0 

04/1310613:21:31 2.1 179.0 0.8 -1.1 

04113l0613:21:41 1.8 108.6 6.7 -1.2 

0411310613:21:51 1.7 52.4 15.1 -1.2 

04l1310613:22:01 1.8 24.1 19.5 -1.2 

0411310613:22:11 2.1 12.3 21.4 -1.4 

04113/0613:22:21 2.0 6.5 22.3 -1.5 

04/13l0613:22:31 2.1 3.9 22.7 -1.5 

0411310613:22:41 1.9 2.5 22.9 -1.6 

0411310613:22:51 1.9 1.5 23.0 -1.7 

04/13l0613:23:01 1.8 1.0 23.1 -1.7 

04/13l0613:23:11 1.8 0.4 23.2 -1.8 

04l1310613:23:21 1.9 0.3 23.3 -2.0 

04113/0613:23:31 1.8 0.2 23.3 -1.9 

0411310613:23:41 1.9 -0.1 23.3 -1.9 

04113/0613:23:51 1.8 -0.2 23.3 -1.9 

0411310613:24:01 1.9 -0.5 23.4 -2.0 

0413/0613:24:11 1.9 -0.7 23.4 -2.1 

04/13l0613:24:21 2.3 -0.8 23.3 -2.0 

0411 3/06 1 3:24:31 2.6 -1.0 23.3 -2.1 

04/1310613:24:41 3.4 -1.0 22.9 -2.1 

04/13!0613:24:51 3.9 -0.7 20.4 -2.1 

04113/0613:25:01 4.5 -0.5 11.7 -1.8 

04/13/0613:25:11 3.7 -0.6 5.8 -1.8 

04/1310613:25:21 2.6 -0.6 3.1 -1.5 

04113/061325:31 2.1 -0.9 1.9 2.6 

04/13/0613:25:41 2.1 -1.0 1.4 13.1 

04113I0613:25:51 1.8 -1.3 1.3 25.1 

04l13/0613:26:01 1.9 -1.3 1.3 36.6 

04113/0613:26:11 2.0 -1.3 1.3 46.7 

04l13J0613:26:21 1.9 -1.2 1.1 55.2 

04/1310613:26:31 1.8 -1.3 1.0 62.5 

04/13/0613:26:41 1.9 -1.3 0.9 68.6 

04/13J0613:26:51 1.8 -1.4 0.8 73.6 

04/1310613:27:01 1.8 -1.5 0.7 77.3 

04113/0613:27:11 1.7 -1.3 0.7 80.6 

200 ppm CO 

Zero NOx, S02 

25.5 ppm NOx 

Page 6 1?3 
4,13106 Run #3 

04113,10613:27:21 1.6 -1.3 0.7 83.1 

04/1310613:27:31 1.6 -1.4 0.7 84.7 

04/13/0613:27:41 1.7 -1.3 0.6 86.2 

04/13/0613:27:51 1.6 -1.4 0.6 87.5 

0411310613:28:01 1.5 -1.5 0.6 88.6 

04/1310613:28:11 1.5 -1.4 0.5 89.4 

04/13/0613:28:21 1.3 -1.5 0.5 90.1 

04/13/0613:28:31 1.5 -1.4 0.5 90.6 

04113/06 13:28:41 1.2 -1.5 0.4 90.8 

0411310613:28:51 1.2 -1.5 0.5 91.2 

04113/06 13:29:01 1.5 -1.5 0.4 91.6 

04113/0613:29:11 1.7 -1.4 0.3 91.9 

04/13/0613:2921 1.7 -1.5 0.3 92.0 

04113/0613:29:31 1.7 -1.5 0.3 92.2 

0411310613:29:41 1.4 -1.5 0.4 92.5 

04/1310613:29:51 1.5 -1.6 0.4 92.7 

04/13/0613:30:01 1.5 -1.7 0.4 92.7 

04/13/0613:30:11 1.5 -1.6 0.4 92.8 

0411310613:30:21 1.5 -1.5 0.4 93.0 

04/13/0613:30:31 1.4 -1.5 0.4 93.0 

04/1310613:30:41 1.7 -1.1 0.4 93.1 

0411310613:30:51 1.3 -0.9 0.4 93.2 

04/1310613:31:01 1.4 -1.1 0.3 93.2 

04/13/06 13:31:11 1.6 -1.0 0.3 93.1 100 ppm S02 

04/1310613:31:21 1.5 -1.2 0.3 93.2 Zero VOC. CO 

0411310613:31:31 1.6 4.2 0.4 93.1 

04/13/0613:31:41 1.7 -1.2 0.4 93.1 

04/1310613:31:51 1.9 -1.2 0.4 93.1 

04/13/0613:32:01 33.0 -1.1 0.4 93.2 

04/1310613:32:11 42.1 -1.1 0.4 92.3 

04/13/0613:32:21 41.9 -1.0 0.1 84.1 

04/13/0613:32:31 41.9 -1.2 0.1 69.3 

04/1310613:32:41 41.8 -1.2 0.0 54.0 

04/1310613:32:51 41.8 -1.3 0.0 41.1 

04113/06 13:33:01 41.8 -1.4 0.0 31.3 

04113/06 13:33:11 41.8 -1.2 0.0 23.9 40.8 ppm Methane 

04113/0613:33:21 41.8 -1.1 0.0 18.8 

04/1310613:33:31 41.8 -1.2 0.1 14.5 

0411310613:33:41 41.9 -1.1 0.1 11.6 

04113/0613:33:51 41.9 -1.2 0.1 9.7 

1?4 

Page 7 
Appendix C 
..._.J_._ _ ~__. _ .. . ............ . .....-.. .. 

Comments: G'l .7 ppm Methane 

•s.00omV 

Retentro 0.050 .-,___ }- 

~ 

0.800 - 

1 

1.133 f . - - - A,lethane 

16,00otnV 

865 

4 

Component Retention Area Extemal 

- 0.050 4.521 0.00 

- 0.800 1.865 0.00 

Methane 1.133 28.054 64.86 

34.440 64.86 

1. 13 8 
. . J .. _«. ~. ~ .. . .. ~...... . ...~ ...... 

Comments: 61. i ppm Methane 

•B.OaUmV 

Retentio 

'! 6.000mV 

ExternallArea 

0.100 - ~~— 0.0=.913 

0.400 ~ . 0.00J2.482 

0.63; 0.00/1.882 

1 133 

I 

- ` ~ Methane 61.S3126.692 

2 

3 

4 

~ 

Component Retentian Area Extemai 

0.100 0.913 0.00 

- 0.400 2.482 0.00 

• 0.633 1.882 0.00 

Nlettsane 1.133 26.692 63.58 

31.969 61.56 
~ornrnents: 61.7 ppm M¢thane 

-8.000mV 76.000mV 

P,etent 

0.333 

0.766 

1 133 

CoRtponeRt FZeteritlon 

- 0.333 

- 0.766 

Methane 1.133 

Area Extemal 

1.982 0.00 

4.133 0.00 

26.567 61.28 

32.682 61.28 

140 
. - - ~ -•--- - .. . .. _ _ . _. ._. . _ 

COmments: Run #2 Bag Sample 

•8.000mV 1 B.00OrnV 

0 083 ! 

O.A86 _ d.d0/9.643 

0.800 . U.0710.700 

~133~~ Meftne I 8.53;4,058 

Camponent Retentian Area External 

- 0.083 1.657 0.00 

0.466 1.613 0.00 

• 0.800 0.700 0.00 

Aiethane 1.133 4.058 8.53 

8.029 8.63 

744 
Comments: Run #2 Bag Sample 

-8.000mV 16.000mV 

QOfOf~ t 

0.09 B 

0.300 

0.600 

0 6s0 

1.133 

Component Fietention Area ExterrEal 

- 0,016 1.078 0.00 

- 0.300 2.813 0.00 

- 0.600 1194 0.00 

- 0.850 0.990 0.00 

Methane 1.133 3.764 7.91 

9.839 7.91 
r'a icabya#.: yaua. .d—To i i e...— + ..,~ 

Cornments: Run 92 Bag Sample 

-5.00+OmV 1fi.000mV 

ExtemalfArea 

i 133 

Component F2etention Area Extemal 

- 0.818 0.962 0.00 

Methane 1.133 3.823 8.04 

4.785 8.04 

L~.816 
, _ . 

---- w--•-- 

Cornments: 6 i .7 pprn II!{ettiane 

v nnn...%r i6.OQOmV 

I3.01 g~

tl 

0 316 

0.583 

0.653 

' 150 

Camponent Retentian Area Ext•emat 

. 0.016 1.565 0.00 

- 0.316 0.574 0.00 

0.583 0.744 0.00 

- 0-833 0.811 0.00 

hAethane 1.150 25:849 59.55 

29.543 59.65 

L+ 
Gomrnents: 61 .7 ppm Methane 

•B.000mV 16.000mV 

0.3t35 .379 

0.883 

1 133 4 Mlethane .94/26.a42 

Component netentian 

• 0.3v"6 

- 0.683 

Methane 1.133 

Area Extemal 

1.379 0.00 

2.093 0.00 

26.842 61.94 

30.314 61.94 

14 ~ ~ 
16.00Omv 

ExtemBElArea 

57 

•8.ODO.mV 

rZetenti - 

0.26$ 

0.800 

9;"E33 

„. 

Comments: 61. i ppm IlEiethane 

Component Reterrfion 

- o.2s6 

d.8QQ 

Methane 1.133 

Area ExtemaE 

2.22D 0.00 

4.393 0.00 

26.957 62.22 

33.870 62.22 

1,16 
. ~.~w~ .Jww\ ~ w\M\.►• ti"I ~ 1 \lL..~~ V \V.V\r.•'TV 

Comrrients: RLtn 43 Gas Bag 

•8.00DrnV 16.000rnV ' 

Retentl 

0 200 

0.833 

1150 

Camponent Retent€an 

- 0.200 

• 0.833 

Methane 1.150 

Area Extemat 

3.853 0.00 

1.474 0.00 

4.726 9.93 

10.053 9.93 

~ 
. , ._ ..---. _ .. . .._.._.. . _....,..... 

Cornments: Run #3 Gas Bag 

-8.000mV 96AlYJmV 

0.258 .523 

0.800 

1.133 1 IJleihene ~ 9.92I4.718 

Camponent Retention Area ExiQmak 

- 0.266 1.523 0.00 

- 0.800 4.527 0.00 

MetRane 1.133 4.718 9.92 

10.767 9.92 

~. . 

~ ~V 
Comments: Run #3 Gas Bag 

16.00OmV -8.000mV 

Retentiti 

0 316 

+3.783 

1133 

1 

2 

3 

4 

Component Retention Area Eactemat 

- 0.316 0.966 0.00 

- 0.783 3.697 0.00 

Methane 1133 4.902 10.30 

9.466 10.30 

149 
J . _ ~ ~ .. . ~r r.r • ..r •. . 

Cornrnents: 61.7 ppm Niethane 

•8.004mV . 16.00OmV 

0o~o~t 

O.QOQ 

O.S66 

1 133 

Cornponent Retention Acea Extemai 

• 0.000 3.780 0.00 

- 0.366 0.891 0.00 

N{ethane 1.133 26.986 62.29 

31.657 62.29 

~ EJL"1 
.r.ullvlw VM~r. V1/ 1 iJt_VVV i Y.~/~J.JV 

Com=nsnts: 61 .7 ppm Nietiane 

-8.000mV 18.000mV 

Retettl 

0.900 

0.400 

0.600 

Componert Retention Area Extemat 

• 0.100 0.987 0.00 

- 0.400 2.210 0.00 

- 0.600 1.169 0.00 

Mcihane 1750 27.023 62.38 

31.389 62.3$ 

151 
. ....~..... ........ ~ .. .......... .-r.v..•ti, 

Comments: 61.7 ppm 4L4efhane 

-s.000mv 

Reterstio 

0.300 

0.846 

1 

1.150 

2 

3 

Componertt Retention Area Extemal 

- 0.300 1.967 0,00 

- 0.816 4.191 0.00 

Methane 1.150 26.026 59.9B 

32.184 59.98 

18 OOOmV 

Extertsa!lArea 

• • 0.0011 .967 

: - 0.0014.191 

Methane 59.98126.026 

~ 52 
Cornrnents: Recovery Stuay Run #3 3aa 

-s.acoMv 

Ketent 

0,050 

0 400 

0.700 

' 133 

~t j,.-' t 1 +1^ r•=y . L ~ 7 f ~a.,~ 1~.,~~cY`. ` i • ~ 

1 

16.00Omv 

Corntaanent Retention Area Extemal 

- 0.050 2.116 0.00 

0.400 1112 0.00 

- 0.700 0.519 0.00 

?Acthane 1133 13.692 30.18 

17,439 3018 

2-5 

~ 

5 ~. 

, e.) +,~ 3 0 -7 

1.53 
., _.. _r. ~ . _ .. . .._ ....... . .........,._ 

Comments: Recovery 5tuay Rur #3 Bag 

-$.000mV 16.00JmV 

Component Retentior: Area Extemal 

0.200 1 .9 i a 0.00 

0.516 0.580 OAO 

0.766 0.515 0,00 

Methane 1.950 13.301 29.23 

16.366 29.23 

1 rn ~. 
Cornments: Recovery Stucly Run 03 Bag 

-8.000mv 18.000mV 

netentio ExtemaGArea 

0.083 j B.00Pt.9S5 

4 450 - 10.0010.982 

1 135 1 ~ I _ - -- - ARethane ~ ~ 27.59/12.627 

~ 

Camponerzt Retention Area Extemat 

• 0.083 1.956 0.00 

- 0.450 0.962 0A0 

Methane 1.133 12.52: 27.59 

15.544 27.59 

I 1rl-. 5 
Appendix I) 
FILTER ANALITICAL DATA 

Company: Dal-Itafia, Muskogee, OK 

Date: 4/12l06 

Location: Kiln Scrubber Exhaust 

Run 1 Run 2 Run 3 

Filter ID Number .50 ~: 

Date of Weighing 41171~qi 4f'~ fi~46: 

Time ::Z:23: ~fy1: 7~22 A~1 :: ~ 2:~:~tM : 

Gross Filter Wt. .7. 

Date of Weighing 

Time :~: 2 ~ :: Pi1t1 

Gross Filter Wt. 

Ave. Gross Filter Wt. 0.3939 0.3788 0.3902 

Date of Weighing 

Time i 14 ~~ ? A~!1; ~~~:38:i!aN(: 

Filter Tare Wt. 

Date of Weighing :2}V06: 100' 

Time :9:2.7:AM: :3:0~IIRM 

Filter Tare Wt. 

Ave. Filter Tare Wt. 0.3611 0.3618 0.3612 

Wt. of PM on Filter (grams) 0.0328 0.0170 0.0290 

Total Weight of Particulate (mg) 32.8 17.0 29.0 

160 
PARTICULATEANALYTXCALDATAFORNY 

Cnmpmny: oautona.Musxnmnu OK 

oote 4/12/06 

LocoUon: Kx|nScruubmExhauot 

Run1 Run2 nun3 

oonsitv(pa) ' 

exonxoonnontramon(:o) 

ninuevo|uma(Vaw) 7. 

neaiuuainRinoo(Wo)=Oo°Vow°pa --__10.0V003. 

Dato o,woi8hing ! | 

Time 

Qro»»VVei8ht 

Dote ufvVwi8hinQ ~ ww 

Timo 

Q,00uvvoiQht ! 

Oate o/VVoi8hinQ 

Time 

BoaxorTaroWei8ht / 

Doto ofYVoiQhin8 i 6. 

Timo 

BeokorTmrwvVo|Qht 

AxaroQoQruxsVveight 

Luuo 8|ank Roxidua(Wa) 0.0003 0.0003 

xv o,a8o B no er x T are VV | uo ~t 1{06.7u483 1{04.7144' _--

113.3236 

Time 

Time 

Time 

161 
PARTICULATE ANALYTICAL DATA FORM 

Company: Dal•Italia, Muskogee, OK 

Date: 4/12/06 

Location: Kiln Scrubber MeCL Rinse 

Run 1 Run 2 Run 3 

Density (Pa) 

Blank Concentration (Ca) io* 

Rinse Volume (Vaw) 

Residue in Rinse (Wa) = Ca*Vaw*Pa 0.0000 0.0000 0.0000 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing i .8 

Time 

Gross Weight 

Date of Weighing 2 

Time '.,7 .1 4 .,'A 

Beaker Tare Weight • 1 i -3: 5 ®r 5 4":: 

Date of Weighing 2 

Time .8* 

Beaker Tare Weight i 1 5< 45 

Average Gross Weight 115.1974 113.5067 108.6863 

Less Blank Residue (Wa) 0.0000 0.0000 0.0000 

Average Beaker Tare Weight 115.1911 113.5054 . 108.6846 

Weight of Particulate in Rinse (mg) 6.30 1.30 1.70 

METHYLENE CHLORIDE BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight I.Q. 5,19 .5 2:: 

Average Gross Weight 105.19935 

Date of Weighing 

Time 

Tare Weight 

Date of Weighing 

Time .2 ;4-* ?~ R. N4.- 

Tare Weight 9~2: 

Average Tare Weight 105.19935 

Weight of Blank (Ma) 0 

Ca= Ma/(Va'Pa) = g/g 0 

Note: In no case should a blank residue greater than 0.01 mg/g or 0.001% of the blank 

lweight be -subtracted from the sample weight. IS2 
oompany' oawmxa.muoxogoo ox 

omo:4/z2/O6 

Lonabmn: KxnSoubbo, Impinger Smmiun 

nun1 nun2 Run3 

o enoi ~ v( P a) / 

o|anx ooncpntration (Ce) ' 

R|nxovo|umo (vow) 

neo.duoin ninuo(vvo)=Ca°vow-*pa -----{0 .0003' --_-_

0. 000:3 -__-/0 .)0{3~ 

Doto ofvveiBhin8 

Timo ' 

G,000Woight 

Datp ofVVei8hin0 ! | 

Timo 

omuuvvniQht 10 139 -N; 

oatev/wwiohing 

Timo ~ aoaxo,Ta,eWeight !!! ! 

Douo of WeighinQ 

Tima ' MA 

BaakenTaroWeight ! ~~~ ~ 

avera8oGnmoWwight 

L000 B|onk Rooidua(Wa) 

Avera8p BookorTanovYe8ht 

-_-

103 .3864~ _-

102,7360 ---108 .7697' 

Vvei8ht n/ Partiuu|atp in R/n»o (m0) 5i

1J0 --_-_ 11 . 90~ '_-_--- 6. 05 

Time 

Time 

Time 

~ 

~ C~ ' ' `/ 
Run2 

! ! 

0.3964 

OFM

-------- 

~~-~~ 

0.0202 

~~~ 

Run3 

0.4009 

0.3833 ----' 

0.0176 

^-~ 

Cornpany: DoAboUa.W4uakogeo.OK 

Date: 4/13100 

Lmcodon: ThrnKi|nExhoumt 

Runl 

Oate Weighing #1.177/M$' 

T|me i 

OobeofVVaigh|ng 

|/nne 

..... 

Oat»ofVVeighing 

||rne 

F|lterToraVVt. 

0.3773 

..... 

18.0 

DohsofVVeigh|ng 

Time 

~ 

~~~

`t

~ r` 
Companx oautaUa.Muoxnuee Ox 

nmte:4/z3/O6 

Lnnmuon: TrimKi|nExhouot 

Run1 Run2 Mun3 

Don,itv0Pm 

Q|mnkCunoentmdion(Ca) | 

Rinoovo|umo (/aw) 

HooiduoinRinoo(wm)=Cm°Vaw°pm 0.0003 _---_

0. 00x02~ -----{0. 0003~ 

Date uYWeigh|ng 

Tima 

GmuoWei8ht 

Dmte ofWei8hing ~ Time 

GmooWeiQh1 

Oatoofwui8hing 

Tima jA 

Boako,Tm,oWai8ht 

Doto ofWoi8h|nQ 

Timo 

BookorTomVve|Qht 

AvmoQaQmsxVVeight 113.6347 104.7395 l 

LesoB|onkResidue(Na) 

AvormQaBomkerTaraVVeiOht 

---

113.6057 1{04.7258 106.5415' 

vVoi0htnx pmrLiou|ato in Rinse(mg) 28.74_ 13.51_ 7.19_ 

Time 

Time 

~ C~=" 
PARTICULATE ANALYTICAL DATA FORM 

Conipany: Dal-Italia, Muskogee, OK 

Date: 4/13/06 

Location: Trim Kiln MieCL Rinse 

Run 1 Run 2 Run 3 

Density (Pa) ~ : 1,36: 

Blank ConcenLration (Ca) 

Rinse Volume (Vaw) 

Residue in Rinse (Wa) = Ca*Vaw*Pa 0.0000 0.0000 0.0000 

Date of Weighing 

Time 4., M: 75. i 7 .7 

Gross Weight i 1- 0 ZZ 

Date of Weighing 

Time 4 .M: 

Gross Weight 

Date of Weighirig 6; 2 

Time 7 ".0 AM 0.*4;4 M - 7t,0 5'A 

Beaker Tare Weight 

Date of Weighing 

Time 

Beaker T are Weigh't 1.10 .54:88: 

Average Gross Weight 107.5859 110.5503 107.8992 

Less Blank Residue (Wa) 0.0000 0.0000 - 0.0000 

Average Beaker Tare Weight 107.5836 110.5488 107.8969 

Weight of Particulate in Rinse (mg) 2.30 1.50 2.25 

METHYLENE CHLORIDE BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing 

Time 

Gross Weight 

Da'te of Weighing 41' 6 

Time 

Gross Weight 

Average Gross Weight 105.19935 

Date of Weighing 

Time 

Tare Weight 

Date of Weighing 

Time 

Tare Weight 

Average Tare Weight 105.19935 

Weight of Blank (Ma) 0 

Ca= Ma/(Va.1.Pa) = g/g 0 

Note: In no case SIIOLIld a blank residue greater than 0.01 mg/g or 0.001% of the blank 

lweiaht be subtracted from the sample weight. i66 
company: OaUtaVo, mu,kooea.On 

oote: 4/13/06 

LncaUnn: Thm0m. Imp i nger Solutiun 

nunz Runo Run3 

Donu|ty(pa) 

exonxConoontra |unOCo 

R|nooVo|umo(Vow) 

nouidupinR|nno(Na)=Co°Vmw°Pm 0.0003 

oate o/WoighinQ ` 

Timo 

omsoWnmht 

DatoofWeigh|ng 

Time 

Gmou vva|ght 

Doto ofWei8hinQ 

Timo 

Boaxe, TomWeiQhd 

Dote o/WeighinQ ' 

Time 

oeaxa,TamWeigm 

vwerageQmooWeight 

LoauB|onkRooidue(wa} 

A verogo 8 oo or k T a,o vv i h ag ~ 127.4529 __-

126.0700~ 130.3480 

vvoigh't-oxporticu|atoinR|nso(mg) 

-_-_-- 17.9V0 _-_-_- 17 . 05 _--__ 11 .45' 

Time 

Time 

Time 

167 
Sheetl 

Summary of Hydrogen Fluoride, Hydrogen Chloride, and Chlorine Analysis 

Plant: Dal-Italia, Muskogee, OK 

Location: Kiln Scrubber L 

Date: 4112106 

Run # 

, 

Imp # Volume Dilution 

-- . _,.. ~ FI-, uglml - HCI, 

-. _ .. mg - CI-, ug/ml 'HCI, mg 

_ _-- - •- - - 

1 1& 2 500 1 0; 

.- - 

0l- 0 0 

1,1 & 2 500 

. . . . . 1 0; 

. . 0, 0 0 

Average-- 

. 

--- - 0 ; 

. 0 

2 1& 2 _._.. _ 500, ------._ - ~ - 

1 0.451 

- 

 0.236925 ~ 0.64 ~ 0.32896 

2 1 &_2 _ , -. . _500, i 046 -• 1 0242 . 19 , . ~ .--- --_ _ 

0.68 - 

- 

_- - - ._- 

034952 

.. .. __ . 

, ~ Average -1 ----- ( 0.239558 ~ 

 - 

0.33924 

3 1 &2 

-- - - 

500 ;_ 

- - - _ 

1j 0.84 

- ` 0.44226 ; - __-- 0.71 r 0.36494 

3;1 & 2 

. 

' 500! 

.. 1' 0.89 ~ 0.468585_,_ 0.73 . _- ' - ----- 

0.37522 — 

- -- ------._.. 

Average ; 0.455423; 0.37008 

I 

iRun # ;Imp # ;Volume -Dilution CI-, ug/ml 

' 

~HCI, mg_ 

1 3& 4 250 1 0 i 0

1

. ; 

1 : 3 & 4 250; 1 0 

 0_ 

0 , 

. ._. 

2 3 & 4 - - 250~

----. _. 

_. __.._. . 

1.;__ .- 

0

----- 

0 

' 2' 3 & 4 250 

. . ~ - - -- - - - 

.- 

1 0~ ~ ._ 

- - .- -- -- 

0 ' ; -- --- J 

- ,_ 

0 ~ ~ 3:3 & 4 

' 

250! 

! 

1 01 01 

. 

3 4 

• 3& 

• 250. 

-r - 

1 0 0' 

. 

0, 

Page 1 
Sheetl 

Summary of Hydrogen Fluoride, Hydrogen Chloride, and Chlorine Analysis 

Plant: Da!-Italia, Muskogee, OK 

Location: Trim Kiln ' 

Date: 4/131061 

._ Run # -Imp # 

_. . -- -- - --- - - -•-- ~ ---- - - - Volume FI-, ug/ml HCI, mg CI-, uglml 

. - -- - --- - ------ - -_ _. _.._ 

_Dilution 

- - HCI, mg 

... . -- 

1,1 & 2 300 10 27.97 ; 

- ,.. 88.35723 ; 36.85 , 

. . - • 

113.6454 

- -- 

1 ~1 & 2 

- 

, 300 ~ . - 1Q 93.07187 _ 26. , _ . . . . _ - .._ 85 ~ .. ... _ 

;l 369 . 113 79 .96 

.. _... _. _ 

; 

. 

; l 

; , 

,Average ~ 86.71455 1 ~ 113.7225 

 _---- 

2-' 

1& 2 

-- ~ -- -- 

° -- -------+-- 

-- 300 j 

.-- - -- ~..__. 

- 1_ 0 j -- -- 290- -. -3 _ - 

----- ----- - 

91.705771 

- --------- a38.011 --- 

~ - - --- ---- 

117.2228 

211 & 2 300 11 - 10 ~ 29.22 

- --- 

92.30598 

-----•- 

~ 38.651 -119.1966 

--------_ 

--- AverageL 

I _ 92.00588 i -- 

. -- - 

118.2097 

. _ .._ __ _.... 

3 i 1 & 2 

: 

' 300 ' 

. 

, . ~ . . 

10 

28.97; 91.51623 

- ~._ _ ._ ._ 34.81 , 107.354 

.-_ 

3;1& 2 300 10 27.78? 

- - . _. 87.75702 - - - 

35.67 110.0063 

- 

Average 89.63663 ' 108.6802 

Run # ;_mp # I iVolume ;Dilution CI-, uglml i HCI, 

--- ~ mg 

--.._... ~.. - . - - --- -- -- - -- 

1; 3& 4 -•--.-._.. . 

~ . . .. _._; 

250 _ ..__ _ _- 1~ - 1.99 0.4975 ~ __ 

 --------_ 

1 ' 3& 4 

. ... _ __.- 

250 

- - - - -- - - ------__ . . _ _ . . 1 L - - - --

2.08 

~ 0.50875 

._ ~ 

2,3 4 „ 250'; 

, . _ , . 1' 1.7 

. ---- ---. - 

0.425 

. 2;3 & 4 i 250! 1'i 

- ~ - 

` 0.4125' 

~ 

. ~ _ _ 

_.53

_ _ _ 

, . ~ _ 

-- . ~ .. . - - l =. - -- ~. 0 

_. 

3: 3& 4 i_ 250 ; 1; 2.15 ~ 75~ __. . 

3!3 & 4 250 ~ - 1 f 2i 0.5 ~ 

. _. . ' ~-- - 

0.518751 

1_6a 

Page 1 
1.024.00OmV 

Area Ey ~ erna 

105.95 ti/A 

457.85 5.2 

256.05 3.9 

Conditions z 5.06 ug/ml Fl- in H2SO4 

: 5.01 ug/ml Cl— in H2SO4 

Date : 04/14/2006 

Time : 10:46:50 

1. 0 4 0 0 rn V 

Component, Retenti 

(unkf..OWR) 0.85 

Fl- I . 

ci - 1.60 

op ..... ....... 

ol 

21 

: 

.............. ................ . .... ............. I .............. I . . .......... ............... ... ................ ....... ........... ............. ...... I ................... ..... I ............. 

Component Number Reteiition 

Fl- 1 1.016 

ci- 2 1.600 

N 

Area External Units 

457.85 5.20 ug/ml 

256.05 3.95 ug/ml 

713.90 9.16 

171 
--1. f32 . 4 0 0 in V :1024 ,.000mV 

Component Retention 

( unknawn ) 0. 

~~

nknown) o. 

Ci- 1. 

Area Eyterni 

166.35 NO 

105.20 N!f 

•442.55 5.{ 

251.80 3.8 

Condit ions :§ :ft H@rfli 

Date : 04/14/2006 

Time : 10=49.14 

Component Number Rete nt i a n Area External Units 

F1-- 1 1.016 442.55 5.02 cag/m1. 

C1-- 2 1.566 251.80 3.89 ug/m1 

2 694.35 8.91 

1.72 
( unknown ) 0.85 

F1- ?. 

C1- 1.60 

122.70 h'lR 

882.85 10.4 

450.50 7.5 

Area External Units 

882.85 10.40 ug/m1 

450.50 7.50 ug/m1 

1333_35 17.89 

Camponent 

F1-- 

C1— 

Number Retention 

1 1.016 

2 1.600 

lr~ 

} f 

C;On.di1..t 1S = ~..~ f L'g. 1m1. F1 -1n h' 2SO4 

ug/rni C1— in 1-12SO4 

Oate = 04114/2006 

Time - 10:57-°51 

— 1 02 . 4 0 C? m V 102 4 , On0mV 

ComDonent Reientian Area ErLerna 

373 
1024.000mv 

61 ......................... ................ 

.............. . ....... .......... .. .... .................. 

6 

2 

-102.400m1/ 

Component Retention 

(UnkDown) 0.01 

(Unknown) 0.83 

Fl- 1. 

ci- 1.56 

Area Exterpa 

229.10 NIA. 

115.50 N/A 

866.70 N 10.2 

497.15 8.0 

C- c-, r(%-. 10 ri S --%=k-1TS ugfM! F H.2S 0 4. 

I - 0, Oj,,/ = Sftlel ug/ml Cl- in H28O4 

Date 04/14/2006 

Time 11:00:10 

4 

Component Number Retention Area- External Units 

Fl- 1 1.016 866.70 M 10.20 ug/ml 

ci- 2 1.566 497.15 8.09 ug/m7. 

2 1363.85 18.29 

174 
-102 . 14tGOmv 1024 .0OOmiJ 

Component Retention 

(unknoun) 0. 

Cl- i. 

Area EXtern: 

112.30 N/i 

17II2.60 20.: 

1059.89 17.; 

Canditiorrs z 20.22 ug/m~ F~~-- ~.n H2504 

=20.04.ug/ ~t C- i n F12804 

Oate = 04/14/2006 

T i me = 11 = 09 = 47 

Component 

F1-- 

C1--- 

2 

Number Retention Area External Units 

1 1.016 1782.60 20.39 ug/ml 

2 1.600 1059.89 17.72 ug/m 1 

2842 _ 49 38.11 

3 '~~ 
Area Externa 

112.50 H/A 

1746.50 19.9 

1064.65 17,7' 

GondItions - ?-3 _22 t !gArd FJ.-- in F.1 2S0n, 

'- 20.04 ug/mX Cl-- in hE22-SO4. 

Date = 04/14/2006 

TimP = 11:12:26 

--102 . 404mV 

Component Retention 

{unknown} 0. 

F1- 1. 

C1- 1. 

;l J24 . OOOmV 

i . . ...... ~'3 » . » . . .»..... » . . ». «» ..»... ...«...» .... ............».... ................_... ........... ...» .....«» .».... «.»...... .. ............. « ........ .«.,..« . 

.~ 

.~ 

833 

1 ...... _........ ........

. :- ..::.::.::..............,..::: ,:n,:.....,.... ~ ,I. ,» ....._. 

'~~ ......_ 600 

2' 

3 ... : 

, . 

4 

. ~ 

: # 

~ . ... : 

ComQonent Number Retention Area External Units 

F .1-- 1 1.016 17446.50 19.98 ug/ml 

Cx- 2 1.600 1064.65 17.79 ug/ml 

N 2811.15 37.76 

176 
o n d _ i o ns 0 4 1. m I r, H 21 S 0 4 

40,08 u.g/ml CI.— in H2504 

Date = 04/14/2006 

Ti'me = 11:21:39 

—102.4OOmV 1024.00OmV - 

-omponent Reteption Area Exte-ina 

(unknown) 0.8 

Fl- 1. 

ci- 1.6 

............................................................................._....._....................-..............................,...........................,..........,...................................,............................. ..i 

. . 

so 

.............. . . 

.......... . . ................... . ..... . ........ ............... . . . ............. 

66 

.............. ............ ....... 

2 ........ 

;,I 

4 

6 

............. .............. .. . ......... .............. .............. ......... ....... .................... 

122.45 NIP. 

31462.30 39. ~ 

2372.70 M 491.4 

Component 

Fl— 

ci — 

~ 

Number Retention Area External Unite 

1 1.050 3462.30 39.51 ug/ml 

2 1.666 2372.70 M 42.44 ug/ml 

5835.00 81-95 

i 7Y 
10 M' 4 0 017t 4r 

Component RetenU: on 

1024 . JOOmV 

Area Cxtprni 

130.00 Pt/f 

3439.00 39.2 

2147.75 N 40.3 

(unknown) 0. 

r" 1  - 

Concii± ions = 40.44 ug/irl Fl-- zn H2SOA- 

= 40 _08 ug/m1 C].- in H2s04 

Date = 04/14/2006 

Time = 11:24-19 

~ 

Component Numb'er Retention Area External Units 

F ]. -- 1 1.033 3439.00 39.25 ug/'ml 

C1-- 2 1.633 2247.75 M 40.30 ug/ml 

2 5686.75 79.55 

178 
AMQUNT I14JECTEt? 

AREA 0.000 

0.000 

3450.650 

40.440 

1, 

2 

3 

4 

5 

Calibrotion file - FI-,caI 

Avg slope of curve = 86.11 

Y-a x i s i nter cept = 0.00 

Coeff of .l. a. n r egr .' 0.97 

No. Area Amount CF 

ca = 0.000 0.000 0.000 

1: 450.200 5. 060 88.972 

2: 874.775 10.110 86.526 

3: 1764.550 20.220 87.268 

4 = 3450 .650 40.440 85.328 

179 
AMOUN`f' IN3ECTED 

AREA 0.000 

O . C?OC 

2310.225 

40.080 

1 

2 

3 

~ 

~ 

5 

Calibratxon i ji le - :C-+. - _ cal 

Avg slop© of curve ~ 53.95 

YMa xi s i ntercept : 0.00 

Coe•Ff of l a. n r egr ~ 0.87 

No MArea Amount CF 

0= 0.000 0.000 0.000 

1 = 253.925 5.010 50.684 

2 » 476 .•075 10.020 47.512 

3: 1062 .?_70 20.040 53.007 

4= 2310.225 40.080 57.640 

.180 
Conditions = Dal-Ital i a, Kiln SGrubber 

= Run #1 Imps 1 & 2 

= Volume 500 mis, Dilution 1J1 

Date : 04f 14/2Q06 

Time = 12=10:21 

- 102 . 40OmV 

CoMponent Reten " 

( unknawn ) 0. 

1024 . 00OmV 

Area Externe 

75.45 N/A 

Component Number Retention Area External Units 

n 0 .0a 0.00 

187 
Condit.ions = Oal-Yta? ia, hiln 5crubber 

= Run #1 Imps I & 2 

= Volume 500 mis , Dilution 1/1 

13ate = 04f14/2006 

Time = 12=12:58 

--.1CJ2 .4t~Om~ 

COnponent Rete€1'ti 

(unknot-in) 0.85 

1024 . OOOmV 

on ...._~ ........ ~~... ._............_.............. . .................,....._ .__.,....... ....MM...._. _.......... ........... ~ .............................................._...._.., 

p '{ ~ 

3 ~ 

2 . ...... ;' . ! 

• I 

3 . .... : 

4 . ...... : 

: ! 

~ . , • ~ 

. ~ 

...... .. ...... _...._.............._.....__._...._.... ..... ............ .... .._....... ..._............... .._...w._........._..._.... ............ ............_._. . ................ _ ..............., i 

Area katerrii 

1i1.55 EllF 

Component hlumber P.etention Area External Units 

d 0.00 • i ♦ 

r r~ i 
—102 .400mV 1 024 . OOOmV 

CoMponenL Heten ' 

~V/ti 

0.4 

0.6 

N/a 

Area Externa 

20.10 

40.10 M 

32.60 

67.05 

(unknown) 0. 

F1- 1. 

CI- 1. 

(unknown) 1. 

Co-ndita.ons = Dal,-Stalia slldln Scrubber 

- Rv n#2 I mps 1& 2 

= Volume 500 mis, Dilution 1f1 

Date : 04714/2005 

Time - 12=22-21 

Gomponent 

F1 — 

Ci— 

EA 

Number Retention 

1 1.050 

2 1.650 

Qrea Exter nal Units 

40.10 M 0.45 ug/ml 

32.60 0.64 ug/ml 

72.70 1.09 

189 
(unknown) 0. 

Cl - 1. 

4unknown ) 1, 

79.20 M NlAl 

40.50 FE 0.4 

34.50 0.5 

72.95 NlA 

C~.~ riditions - Dal—Italia, I.iln 

z Run #2 Imps 1 & 2 

= Volume 500 mis , .Dilutian 1/1 

Date ' = 04f14/2006 

Time - 12=24 =56 

---1. 02 . 4 OOmV 1024 .000mti1 

Component Retention Rrea Externc 

Camponent 

F l — 

cl2 

Number Retention 

J. 1.050 

2 1.6 33 

Area External Units 

40.50 Ni 0.46 «g/ml 

34.50 0.68 1..1 .,~~' / 1n l 

75.00 1.14 

190 
Conponent 

(unknown) 

(unknown) 

F1- 

(unknown) 

C1- 

(unknorin) 

-.1 G2 , 4JOmV 

Retenti-on 

0. 

0. 

~ . 

~ . 

~ . 

Area Extern 

26.00 N/ 

31.50 

74.99 

83.90 

36.20 

65.40 

1 (324 . OOOmV 

o~ 

~ r 

0. 

NI 

Area External Units 

74.99 0_84 ug/ml 

36.20 0.71 (Ag/tn 1. 

111.19 1 .5b 

Component Number Retention 

Fl— 1 1.066 

Ci— 2 1.650 

2 

C-onditi.ons = nzl-Italia, Ki.Ln Serubber 

~ Run #3 Imps 1 & 2 

= Volume 50 ~3 mis, Diluton 1/1 

Date : 04/14/2006 

Time = 12=33=55 

1Q1 
W. 

O.B. 

fa! A 

0.7: 

N/A 

22.35 

79.07 M 

79.53 PI 

37.10 h! 

52.85 fi 

Component 

(unknown) 

(unknown) 

F1- 

(unknown) 

Cl- 

(unknown) 

--3. ~J2 .400rnV 

Retent' 

0.0 

o.s 

1. 

t.~ 

1.6 

1.8 

1 Q24 . OOOmV 

Area Laterna 

28.30 N/A 

Ccnditions = Dal—Ita1. ia , Ki.ln Sorubber 

= Run #3 Imps 1 & 2 

= Volume 500 mis, Dilution 1/3. 

Date = 04/14/2006 

Time = 12 : 37 = 24 

F1— 

C.l 

Component 

2 

Number Retention 

1 1.066 

2 1.650 

Area External Units 

79.07 M 0.89 ug/ml 

37 .1.0 M 0.73 ug/m 1 

116.17 1.62 

~~ ~2 
C0 r•( d i t i a TI W- D a":_ ._. ;: t a a. ia, T ri tri K?_ 1 n 

:.Run #1 Imps 1 & 2 

: Volume 300 mis, Dilution 1/10 

E3ate = 04/14./2006 

T i me = 12 : 4•6 = 20 

— 1 02 . f OOmV 

Component Retent' 

(unknown) 0.0 

(unknown) 0.6 

Fi- 1. 

rl- 1.7 

1024.00OmV 

a -------- , ~

-. ...............»... ...«..............«......................................:::x:m:natr.:tacei:tus::t::r::it:r.iatnet:tiusat::;:t• 

~ .~ . 

.:......... ......... ........... ...........,.............-:,• 

2 ~

....... 

:~ ,. 

3't

......» ; 

e , 

S • 

~ '• . 

4 

 » ...... : 

. 

~ . 

f ~ 

~ . . ~ .... . 

' • 

~ • • ~ 6I....,.. ; 

t 

. I 

ion 

o a ~ 

._.....__.w._...~ 

f~ 

: 

331 j; 

Area Externz 

35.80 t11fi 

51.55 h/P 

2410,40 M 27.9 

2109.00 M 36.8 

Component 

F1- 

c i 

KA 

Number Retention Area External Units1 1.050 24 10 . 40 Ni 27.97 ug/rn? 

2 1.716 2109 .00 11 36.85 ug/mi. 

4519.40 64.81 

.1Q3 
Area Exterri. 

31.10 ti/i 

2324-05 H 26.' 

2112.24 H 301. , 

Conditioris : Dal-Italia, Trim Kiln 

: Run #1 Imps I & 2 

: Volume 300 mls, Dilution*1/10 

Date : 04/14/2006 

Time z 12:48:52 

-102.4OOmV 

Component Reten 

( unknovin 

Flci1.024.00OmV 

.. . ........................................... .......... ............ ......................... .... ................. ........ ... ................................. ........... .. ......... ............ .......... 

~ ; ; 

78 

716 ............... ...... . ...... . ... . 

21 

3 .. ...... 

5[ 

Component Number Retention Area External Units 

Fl— 1 1.050 2324.05 M 26.93 ug/ml 

C l- 2 1.716 2112.24 11 36.90 ug/ml 

2 4436.28 63.83 

1 Q. 4 
Oondi- tions - Dal--zta.lia, Trim Kiln 

= Run #2 Imps 1 & 2 

= Volume 300 mls, Oilution 1/10 

Date = 04/14/2006 

Time = 12-57=50 

--102 .400rnV 

r.omponent Re;.en . 

( unknawn ) 0. 

F 1 - i . 

C1-- 1. 

Area Externi 

28.25 h/ , 

2498.95 N 29.f 

2181.40 H 38.i 

3.024 , OOOmV 

Component Number Retention Area External. Units 

~ 1- 1 1. 06.6 2498 - 95 11 29.03 ug /m 1 

Cl.— 2 1.716 2181.40 M 38.01. ug/ml 

2 4680.35 67.04 
Conditions : Dal -Italia, Trirn Killn 

: Run 42 Imps I & 2 

z Volume 300 mls, Dilution 1/10 

Date : 04/14/2006 

Time ". 13:00'.14 

-102.4OOmV 

Component Retention 

(unknoWD) 0. 

(unknown) 0. 

Fl- 1. 

ci- 1. 

1024.00OmV 

000 

. . ...... . .. ......... . . ............. .......... ..... . ....... .......... I .............. I ... ..... ......................... ......... 

516 

J 

........... . .................. ..... 

....... ........ u t ti I tt; -as t:33 III g; Im III I III III tto ImIll III I III III III in 1" 1- 

J 

70 ............. ..... .......... 

.. ..... ...... ............... 

2 

4 

. ..... .............. .... ...... . ................ .............. ...... ..................... 

tirea Externa.' 

23.30 NIA 

23.535 N/A 

2514.85 M 29.2, 

2221 .30 M 38.6%' 

Component Number R~tention Area External Units 

Fl- 1 1.050 2514.85 M 29.22 Lig/ml 

ci- 2 1.700 2221.30 M 38.65 ug/ml 

2 4736.15 67.87 
Dal—Italia, Ty-im Kiln 

Ruri #3 Imps I & 2 

V41ume , 300 m1s,, Dilution 1/10 

Date : 04/14/2006 

Time : 13:09:02 

—102.400niV 

component Retenti 

1024.00OmV 

u n 1. noii n 0.81 

Cl - 1.08 

( it n k now 11 1.43 

ci- 1.75 

on 

......................... 

6i 

:I ............. .................. . . ..... .. ... . m ::z I an :3 m 1:3 14 1 m m 141 a 1 1!1 w m :;j M• 

31 ........ . ...... ................... . ........ 

311 1. 

:1 ........... 

0 

2 

31 

41 

6 

. .......... .................. ........ ........... ...... . .............. .......................... . . ..... 

Area Externa: 

242.30 t-VA 

2494.20 28.97 

229.75 N/A 

1982.20 

Component Number Retention Area, External Units 

1 1.083 2494.20 28.97 ug/ml 

c 2 1.750 1982.20 34.81 ug/m1. 

2 4.4,76.40 6:3 -78 

19 7 
o -,- -'-1 t ~-- - t s - - a.. 1 - LJ I -'t-;a 'L i a , Tr 1 m K ri 

- Run #3 Imps I & 2 

: Volume 300 mls, Dilution 1/10 

Date : 04/14/2006 

Time : 13:.11".30 

-102.4OOmV 

LomponenL xetent 

I tin knOWD) 0.7 

Fl- I 

cl- 1.7 

1024.00OmV 

------- ---- 

501 1[ 

...................... ... ... .... ............. 

16 . ........ ............. ........................ ....... ..... ............................................ ... 

3 

4 

6 

. ......... 

Area Externa 

50.90 N/A 

2394.90 M 27.7 

2035.55 M 35.6 

Component 

FlclrA 

Number Retention Area External Units 

1 1.050 2394.90 1\1 27.78 ug/ml 

2 1.716 2035.55 11 35 .67 Lig/ml. 

4430.45 63.45 

198 
Condi Liuns - Dalw-Ital.ia , TrI.rr N;Ji ln 

= H23o4 Blank 

Date : 04/14/2006 

Time : 13 = 2C3 = 40 

- 1 U2 . 400;r;V 1 n?4 . OOOmV 

Comaonent ?e4Ant:on 

( unknow, n ) 0.15 

(unknok n) 0.85 

Area Extern; 

28.40 iiIA 

157.20 t/p 

\ 

Compone r3t Number Retention Area External Units 

0 0.00 0.00 

19 ~9 
3[ 

 A 

....... ...... I ... . . .. . ............................. 

on 

ol.... I ................. ..... . ....... .......... ... . ......... 

j. C-24, 000mV 

31 ......... 

J. 2. 

—102.4OOmV 

(Un Umponent Retenti 

known) 0.00 

(unknown) 0.83 

Fl- 1. 

ci- 1.58 

Area Externa 

146.90 Nlt 

157.05 h K 11.4 

1680.20 N 19.9 

1037.10 19.6 

co,ndi•ions Dad—ItaliLa, Trim Kiln 

20.22 ug/ml FI.— in'H2SO4 

20.04 ug/ml Cl— in H2SO4 

Date = 04/14/2006 

Time = 13:22:57 

4t...... 

51 

6 

............ ------ 

Component Number Retention Area External Units 

Fl- 1 .1.033 1680 .20 1,111 19.26 ug/m1. 

cI-- I-583 1037.10 1.9 . 6 1 u V rn.1 

2 2717.30 38.87 

0 0 
Conditi-ons = 5.01 ug/M'L Cl - :Ln NaOH 

Date 04/17/2006 

Time = 08".17:10 

-102.4-00mV 1.024.00OmV 

Compopept Retention 

(uBhown) 0.85 0! 

1 i...».» ,='3 ............ 

61 

21 

3~. »._. ; ; 

41 

61 

......................... .......... ............... ............... ............. ................ . ...... ................ ............ ..................... ................. ........ .... ........... 

ci - 1.81 

Area E X ,%., e T I, a 

1205.20 IWA 

291.45 M 4.4- 

Component Number Retention Ar ea External Units 

c). - 2 1.816 291 .05 M 4.44 ug/ml 

1 291.05 4.44 

2 O'l 
Condi.tiGns -5.0:t u ~,~ rnl C1--_ 3 i: ~`i~~~H 

flate = 04/17/2006 

Time : 08=21=16 

—3.02 . 4,00mRJ 102•4 ., 000mv 

Component ?eLentic;t ~ Rre~ t~t~,rnz. 

----------- ~ ----------------- ~ -----------------------....-- .--------------------.......---- ~ ---.....------------------- .------................................._......................................_.................................................._.......................... 

(unknown) 0.83 

Cl- 1.81 

I ~.. .... ~. 

:r 

2 ~ 

~....~.. : 3

1 

I : 

~ ~........ : 

~ ....~.. : 

1187.10 NIA 

293.60 M 4M 

Component Number Retention Area Externai Units 

C1-- 2 1.816 293.60 M 4 .4.8 ug/ml 

1 293 _ b0 4.48 

202 
( upkilokin ) 4.83 

Cl- 1.81 

1159.20 N/R 

521.40 P1 14.0; 

ro;i d i t'"..ions "- 10.02 l.E9/i7?.i 

Qate = 04f17f2006 

Timc - 08:25.03 

—102 . 4nQE"nV 

rompor,A nt f;etent ion 

10 ' Y . C) 0 :,' M V 

Prea EYt.eE n; 

Component NLimber Retention Area External Units 

~ 1- 2 1.816 521w 4a 11 10.02 uq/rn:L 

~ 521 .40 10.02 

203 
Conditions - 14.02 ug/rnI :in No4H 

Date : 04/17/2006 

Time ; 08=28=34 

~~1.02 ,.4•0OmV 

Componpnt RoteRtion 

(unknown) 0. 

C1- 1. 

1. 024 . ~1C)~.~mV 

Area Externa 

1162.10 N/4 

516.10 M 9.9 

Component Number Retention Area External Units 

C1— 2 1.816 516.10 M 9.90 ug/ml 

1 516.10 9.90 

2 n 4- 
f-o nd i ti c, ns = 15 . 03 c.! g/ ml 0l ..-- i ri Nat31l 

DatQ : 04/17f2006 

Time = 08=32=10 

-102 . 4OOmV 

Componeni. Re{en . 

(unknown) 0. 

ci- I . 

1024 .00OmV 

ATea Ext.T n= 

1128.34 N/f 

854.44 H 15.( 

Component Number Retention Area 

C 1:-- 2 1 . 81. 6 854.40 I1 

1 854.40 

External Units 

15.03 (Ig/m:L 

15.03 

2n5 
1 G2{- . OOOmV 

. 15 , 0:~ u C-1J`rn1 C n N,::~ 0H 

= 44/17/2006 

= 08=35=27 

0~ ., ~ 0 0 m ~,1 

C:onditionw 

Date 

Titne 

Componenf Petentian 

(unknawn) 0. 

el- 1.. 

Area Externa 

1108.40 N/P 

802.80 Pt 14 . 2- 

Component Number Retention Area External Units 

C1 - 2 1.816 802.80 M 14.26 ug/ml 

1 802.80 14.26 

206 
Con di tiors:S 

Date 

Time 

Compo7svi r~~ }ent ~ 4n 

(unknawn) 0. 

CI- 1. 

: 20 .o! ug/mi C1— 1 rj t4a0i-! 

= 04/ 17/2E)O6 

= 08=39=d1 

Id2 _ 400rnV 1024 .00OmV 

Arca Externa 

1098.80 NlA 

1193.60 M 20,9: 

I 

component h[umber Retention Area External Units 

ci- 2 1.833 1193.60 M 20.93 ug/ml 

1 1193.60 20.93 

207 
Conditiarts : 20 _C= ~'T ugf":Y~ ? a_n INIa'OH, 

Date : 04/17/2006 

7ime - 08 = 41-`- 50 

—102 .40OmV 

Component Retention 

(unknown) - o. 

Ct- 1. 

1024 . OUOmV 

Area ~.-zterni 

991.20 lV/P 

i198.50 m 21.0 

Component Number Retention Area External Units 

C1. — 2 1.833 1198.50 Ni 21.01 ug/ml 

1 1198.50 21 .01 

~~ s 
AMOUNT INJECTED 

AREA 0.000 

0 . OOC) 

1'-IL96.050 

20.040 

1 

2 

3 

4 

9 

calibration fila -. cl- Clal 

Avg slope of curve: 59.68 

Y-axis intercept: 0.00 

Coe-ff of lin regr: 0.81 

No. Area Amount CF 

0: 0.000 0.000 0.000 

1: 292.325 5.010 58.348 

- 518.750 10.020 51.771 

3 828.600 15.030 55.3.30 

4 1196-050 20.040 59.683 

209 
Conditio-tis : Dai-ltalicsx, Kilil 'Scrubber 

: Run #1 Imps 3 & 4 

: Volume 250 Dilution 1/1 

Date : 04/17/2006 

Time " 09.".11.-21 

-102.4OOmV 

compopent Retenti 

(u ilk now 11) 0.83 

~

unknown ~ 1 : 90 

unknown 2 

1.024.000mV 

Area ExteTne" 

556.35 N/A 

125.40 NIA 

216.80 N/A 

02 

................ ......... . ....... 

2 ....».. 

6 ........ 

...... ..... 

Component Number Retention Area External Units 

op, 0.00 0.00 

216 
L o n d ]. t ]. o ns 

Date 

Time 

Coraponpni Reten . 

(un-knowr) 0. 

~

unknown ~ 1. , unknown 2. 

- t.) al —rtai za , !\i I n =ti ruh- bei 

~ Run #1 Zmps 3 & 4- 

: Volume 250 Dilution 1/1 

: 04r17f2006 

: 09 : 1.4 : 01 

1.02 . 4OOmV 102"4 .00OmV 

Area Externa 

571.85 h/A 

223.60 1i/ A 

223.70 N/A 

Component Number Retention Area Exter nal Units 

0 0_ 00 0.00 

217 
$

unknot~ n ) 1.93 

,unknown} 2. 

, i : : . 3_ rI .1 C..:1^U. t~1>t~ i 

~ 3 ~; 4 

Di.lution I/1 

:1.;32q• .C? ~`7Dm ~J 

io~ 

...................... _................. .................... . ... ... ..... .................. .... ....... ........ .......................... . ....... ......... ................. . ............ ............. ................................................ .................... ...... 

, 

, 

.~ 3: ~ t 

„ ~ ........ ; ......». y=::r . 

~ ......... t.•~ ' 

,..:.....: t 

.~ 

" »... : i ' ....:.... » • .• • ••. •-•..•••• = ~m=r.m:raennu=aJat:tn[tr.tznttttr ~ 2 ::::~•. ~ ~_ 

3 

. ~ . , 

: I 

4 ..... ; 

~ 

51f

....... ; 

t , ; 

; • 

6' 

~...._..w..._.... ........ ... .............. ... .......................... .. ..... .................... ........ ....... ......... ................................ ............... .... ...................... 

C Gi :_ — .1. Z. ai I i G1 

- 1?un #2 Imp 

= Volurne 250 

Date = 04/17/200e 

T im w= 09 = 22 = 45 

~~ 1 02 . 4OOmV 

uomponept Rete ~ L' 

(un(cnou ~ n) 0.8 

Area Externa 

580.90 IUA 

1641.50 N/R 

326.54 N/A 

Component ivumber Retention Area External Units 

n 0.00 o _oa 

018 
c ti.:r n d i %. t o n s • g ~? 1 - I t a 1 l 4~ ., -- c r u b b e r 

= Run #2 Impe 3 & 4 

= Volume 250 Dilution 1/1 

Date : 04J17r2006 

Time - 09-25=29 

—102 .400mV 

OmPonen't ReTeti' , 

n known) 0. 

unknown 1. 

un;cnawn 2. 

1024.000inV 

Area Externa 

577.15 N/A 

1604.55 iV/A 

320.75 N/A 

Component hlumber Retention Area External Units 

C} 0.00 0.00 

219 
0 -n n d. L IL-. I'L 0 11-1 S : D a -a l i a C 1- L Ob bi& r 

: Run #3 Imps 3 & 4 

: Volume 250 Dilution 1/1 

Date : 04/17/2006 

Time : 09:34:30 

-102.400ffiV 

Componept ReteDti 

(unknown) 0.85 

(unknown) 2. 

1024.000mV 

on 

0 .............. 

2 ...... 

3 

4 ...... 

5~......_ : ~ 

6 

I ..... . .......... . ....... . ....... . .......................... 

Area ExteTna 

630.50 ti/A 

241.80 N/A, 

Component Numbet Retention Area External Units 

Et 0.00 0.00 

9

2 

. 0 

,. 

I 
c-or,di.tions - Dal--Itali.a,. ;:i.ln Sot u ~ber 

: Run #3 Imps 3& 4 

= Vo3ume 250 Dilution 1/1 

Date = 04/17/2006 

Time : 09=37=12 

-- 1 Q 2. 4 c) O mV 

Component Reteniion 

'Un{,nowr.) 0. 

uEtknolrn 1. 

un k nown 2, 

1 024 . 000mV 

Area Externa 

561.30 N14 

103.80 NIA 

248.70 h/A 

Cornponent Number Retention Area External Units 

x COMM, s •• 

221 
Rrea Externe 

781.41 M. NIR 

116.14 

531.74 NIA 

Condii.ions = Dal—It a1 ia. zTr im Ki ln 

: Run #1 Imps 3 & 4 

= VQlume 250 Dilution 1/1 

Date = 04/17/2006 

Time - 09=46-04 

— 1 G2 . 400mV 

Component Reten 

( unknown ) 0. 

C1- 1. 

(unknown) 2. 

1.024 ..00OmV 

i ~ ._....._.»...... ~ .» ............_...._....»...........»w...._..._....._............._...._._.»................_.........».»..........._.» ...............».............._._........».......................». i 

9JJ ~•. ,.:.:nerr ~ 

733; ~ 

~......... ~ r~ .....»,.... 

2 ~~. 

3 ....... : 

4 

5 ~»...... ; 

5 . ».... ; 

Companent Number Retention Area External Units 

C1.-- 2 1.733 116.10 M 1.99 ug /m 1 

1 116.10 1.99 

2 2-2 
Condit'Lons z Dal-Italia, Trim Kiln 

z Run #1 Imps 3 & • 

: Volume 250 Dilution 1/1 

Date : 04/17/2006 

Time : 09:48:55 

--- 102.40n-mV 

coloponepi't Reten 

(unknown) 0. 

(Unhown) 0. 

ci- 1. 

(upknown) 1. 

1024.00OmV 

........... . .......... .......... ......... ......... ............................... . .......... . ................................................................. .................................................... . ................................. . .............................. 

450 

833 

1 ~»«..... 

'.i..il~ , "' 

~ 

2 

3i ».».» : ~ 

41 

6 

k0a ExternS 

206.60 KIIA 

766.30 N / P" 

121.65 H 2.0 

531.70 N/A 

Component Number Retention Area External Units 

cl- 2 1.733 121.65 M 2.08 ug/ml 

1 2.08 

2P3 
1024.00OmV 

Area Externa 

834 .70 N ti/Al 

99 .40 M 1.71 

542.80 N/A 

87.35 ii/A 

Conditi•ns Dal-.Ita.).ia, Tir-im Kilri 

Run #2 Imps 3 & 4 

Volume 250 Dilution 1/1 

Date 04/1712006 

Time 09:58:13 

--'.02 .400rriV 

uomponenL metenti 

kunkpowo) 

ci- 1,66 

unknown 1.95 

unknown ~ 2. 

41 

6-- 

..... . .. . .......... 

Component Number Retention A-rea External Units 

cl- 2 1.666 99.40 M 1.70 ug/ml 

1 99.40 1.70 

OB 

3 

~ !. 

0 

2 

2P4 
Condit ions Dal-Ital-ia,, Trim K i l i-I 

Run #2 Imps 3 & 4 

Volume 250 Dilution 1/1 

Date = 04/17/2006 

Time = 10:09:57 

-102.4OOmV 

uompoDent Retent 

Ik un k now n) 0.8 

C l- 1.6 

unknown 1.9 

unknowni 2. 

102"4 OOOmV 

IH 

33 

16 

50 

2 

41 

6 

........... .................. ....................... ....... .......... . ........................... ............ .. ........ ...................... .... ...... ........... 

Area Externa 

836.30 H N/A 

93.25 H 1.6 

537.86 N/A 

82.30 ii/A 

Component Number Retention Area Ekternal Units 

ci— 2 1.666 93.25 M 1.60 UgIml 

1 93.25 1.60 

2 2 wo 
i. o i i{~ J. t:t v n` s • L.j a .14L_ 

= Run #3 Tmps 3 & 4 

= Volume 250 Dilution 1/1 

aate : 04/17/2066 

rime = 10:19.19 

— 1 U2 . f.QamV 1024 . OofJmV 

Component Retention ~ .. .............,,.... ~ .. ........................................................................................_.......................,,..,.............,..................,......................,,................... .....,.........................,........,,.....,.........' Ar ea E xterrli 

. 4.833i 

~ 

~ ~ , ......... »» 

.... •t ~ 

.t ~ • 

` 8 60.53 P1 ~if~ 

C1- 1.666 

~1 

,Inl 125.65M 21 

1.954 ~.. ~r,k ,kl . : 527.44 N/R ~

unknown 

unknoun ~ 2. 21....»., 74.70 N/A 

Compone»t Number Retention firea External Units 

C1-- 2 1.666 125.65 M 2.15 u.g/rnl 

1 125.65 2.15 

926 
Component 

~ unknown } 

~ unknowp; 

C1- 

unknown 

unknown ~ 

- w02 . 4OCSmV 

Reter 

0. 

0. 

1, 

?, 

:€. 024 . 0OOrriV 

Area Ea -Lerna 

122.30 N/A 

857.00 tr•/A 

116.70 M 2.0 

534.90 N/A 

70.95 NIA 

niticn^ - Da1.--italia, Tr° 7 ff: ':i? n 

: Ru n#3 I mps 3& 4 

= 'dolume 250 Dilution 1!1 

Date : 04! 1 i t2006 

Time = 10-22=15 

Camponent NUniber - Retention Area External Units 

cl- 2 1.650 116 .70 Nf 2.00 ug/m1 

1 116.70 2.00 

227 
o ris 

Da-te 

Time 

compoDent Reten 

D al — I T-1- i rf! K 

5 -01 ug/ml C' i ri lqIOH 

04/17/2006 

10.-31:45 

102.4-00MV 1.024.00OmV 

Area Externa. 

1209.85 H N/A 

306.20 H 5.3, 

(unknown) 0, 

ci- 1. 

Component Number Retention Area External Units 

Cl - 2 1.800 306.20 M 55.32 ug/ml. 

I 306.20 5.32 
Conditions 

Date 

Time 

Component RetentioD 

D a. 1 — I t a 1 i a. Ti- i ri L 11<ii' 1 rn 

NaOH Blank 

04/17 ~'2006 

10: 34: 30 

1, 0 "c"',- A 0 0 m V 1.024.00OmV 

Area Externa 

(uDknown) 0.83 31 1188.00 NIA 

2 

M® 

6 

............. .......... .. ....................... — .. . ....... . ........... . . ................. . ................. ... . ... 

Component Number Retention Area Ex"Cernal Uni"Ce 

'ED 

22,9 
J11n1plo 

'Jun bor 

(]f1tt1 11111A 

Srnm(tioci Sa,ttltlot( 

( — `llf 

-7 ,•~ _. 

—t--- ------ 

Cl~p 

JL- 5 ~" ' 

_

Ilolinc 

* ,~ tat Io) 

fluli cn ~ i ocl b: Siyn ~ lu,a) 

/lnalysos floqu 

/— - 

Q~ 

c~afi 

Da1u ~ Timo 

0 

irod 

c~ 

`0 

 b 

w~ 

~ s i~„~,~ ~ h; 

(locuivod l>y: (Sit~ n 1 a) 

Ilocoivoci by ( Sigrtaltrm) 

'1A.UntiT ~ iONU I-NVIRONtU1ENTAL 7INQ : 

771_ 5 SOVi-'_1: G'.LCJIl T~ Ow 

D A L L/'a S, 'T' X 7 5 2+" 7 CHAI N OF CUSTODY RFCORD 

[Na.ma o( Unil nrtcl Acicfiass: 

D ~ ~ ~,`{-~..~ ~ • 

nl(oNE cio. (2'14) 631 -_ - 002 -i. 

FAX rro_ ( 214) 905-063 4 

tlolirn<pisno(i t,y: ( Sigrtaluro) 

(' C 

Uoscriplion o{ Samplos Z ~j 

te f V. _._._.~ 

g4 5 r~>` i~ ~ ~- r _ ~ 

C- G t '~ 

~ 

 ~ 

+C-(— C. 

~ ~

. 

~ _ 7 

_ 

~=. ~e~ L C.~ t- ~~ 5«'•~~~~T_ ~ 

S~rs Aer ~ 

iLl 

~`~~ ; ~-~~~~ l , 

4csia ri"L 

~_

~-- 

 flelinc~~ isltcci by:

. Dato 7imo 110 ^— y: ('u na rc (Sign,tluru) 

~J r q o 

~p.ttci Titttu f tcaivcd by: ( iJrt1luro) ~ flolintttlishuc{ by: (Sir,)n.-iltiru) 

~ U: to - l intn ~(locoivec) lor Laboratory by: (Sig.) --- l):rio ~ Tin,o flrsrr,arlks ~ 

~ Oislrilttrlion: Orit)intt) /\ccomltarties Sltilmtent 

Q Cnpy to Clioittl('roiect Ccxticlirlittor 
~' b ~P~ ~Prr~ p-t ~~ 

ki fIy 

amov ,,.A 1_,,,Vm01uV1E,irAL, INQ 

sovereigiA 

. Row 

D A L L A S y '1`X 7 5 2 +-7'-.- CHAI N Oic: CUSTODY RECORD 

I - Namo of Uiiii tifi(I Addios - s-_ 

1) 110 N E "Pi 0 . (2-14•) 63 -1-002 -1 

FAX NO- (214) 9o5—•0634 

Samplo Diiiii 'I i$110 

Humbor Sounplod Samplod 

~ ~ L~ ~, ~. 

~~ '~(t~ 

Lo L 

LA.; _4" 

I _.. l. ~— ~ l d C-!L plIVA 

~~ i I ~-F vv ~~-t ~~~ PC, ci10 _Z.'D 

I 10 1111 (t!j 1) y : (SXI V"1 I I I 10) f 

. 1,11 , Dal Tiiiio 110c>01 m ute) 1101inquished by : ("'Sign"Jimo) I loi~Pb y - ~ ~ ~y ~(~ ~:3~ _ ~. _ -- ~- --_. . _ _-._ -- - _ .._ ____ 

floli (pi lo(i y: U nalmo) 011(i Tiiiio coived Eignalts i) 

flolin(pislio(i by: (si gnatulo) Mato Tiiiio llowived lor Labofalmy by: (Sig 

Distilbution: Odginal Accompanies Shipment 

Copy 10 Clio 111/1 , rojeci Cooldinalor 

4~f ..~•.{~ ~ , ~ s j~i1., ~; ~~ ~~.-. 

~_~✓ .~® .w y — 

.~-~~-~ ri ~ . 

Dosctipliati of Samplos 

_Tii-i%_o nomarks 

Analy sos floquiiod 

~--- -- --- ------" ~,~• 

Humalks 

,Ab 

6111 

NO bo--Ic -'s- 

'C_ 

tjo 

IV, 

Ivo 

 -- L``~~~

``" : ~ -= 

CL 

~D L-~ra.`Cr C~ 

Titiio flocAlivoti hy : (sigoatmo) 

'f illio noco VI)d by .. (sij)(1.11mill 

Datu 

Belinquishu'd by : -( Signalo)* m D am 
Samplo 

NUrltbof 

Urttu 1 Snmp1(xJ : 

iZ 

T lrtta 

iar n~~ lUt1 Uoscriplion ol Santplus 

L - - 

Lo— 

l ,ce, 6e, 

- ~g ► ~ ,. ~~ I 

~;lb _ ~ ` ~ ~ ~~ ~t : _ ✓~ 

flulin ~~' 1 by - Sil~n~ mrt) Jatt Tinto Ilocctivt` y: (Sigr ~tf u!) I

1 ay I luntbclrs 

9 zTtl 

---~--~- - 

_ ~3 t;• _ 

's 

~ . gq ~

'~v

- - ~ 

~~ ~ 

I►b ~~~~>s ~~ G'e ~ 6~ r~ V ari 0 N tv1 EN r AL 1 I N C 

., 

771.5 ,~ ove-r c i gn Row 

D A L LA S, -T' X 7 5 2-'+°7 ': . CHA1 N OF i.USTODY RECORD 

Namo ol Urtil nnJ /1cldtu:.s; 

o ~ 

.. 

m 

.r) N 

l- C 

3 U 

Z U 

n _ 

ll>rl r c~ risha I h.(Siyn a ttnu) — Oatri ~— Tilrtrt 11 tived by, rgnaluru ~ -- 

flolinqrisltoc! by: (Siortahn(i) _--- ~ Uato Tirtto IlocoivLxl lor 1_ab01a101y hy: (Sig.) 

N Uisllit)ution: Oric)irtal ncc:orttpanies Shipmenl 

-~ 

Iv cofty lo cliol,llt'rojec:l Coalcfin,,lor 

r l( O N c N o.( 21 4 ), ti :S -1------0 0 x- 1 

r-AX t40_ ( 2 -t 4) 905--0634 

VAnalysos lioquirocl ----~ ----- _ _ -- - -- 

_ c . 

~ ~,f~~ ! 

~ ~ 

Q"0 

~ 

~ 

_ ------____—... ~S_------- 

_ ~'tG-~~~~d -•_- ~ - ---- 

~~- 

--- __ ~__ - ~-~----- 

~%° 

Zl o C . 

-- -- - -- -------'---- ~-~!~`-- -.---__ 

Z ( .~ ~•-~S ~ l~ 

flulitirp,isired by: (Sigrtarulo) ~ Ualu Titno floc,tivud 1 y: (SiSJn:rttno) f 

flulilttluislrtx! by: (Siortaluru) --- ~f)ctlu -- Tittto (lucltivu<) by: (Sinrtalurtt) - — 

- ---~

0:110 -- -- Tirrru i f- irtrt,arks 
Aiii lysos lloquifod AN p _ ,, V 

~~~; ~~r. 

4 .c~, 14rrrr, ~tr cs 

6 

~ ~ --- 

-~ -- 

w 

Ing I lumber; 

v 4N 

1-1 

t702- -J.1% f IC-ly 

Flelimplished by : (Sitjfiltllljfti) -I —"- 

BelinquiMled by : (signalulo) 

= ___ ~ i 

iilu Tiitio 

D►lu 

e Zoo 

~,►o _ L

~~~_ ~ ~ __ - . - 

(f 

_ _~_ ~ ~-~C-lc~. ~; 

llocolivod by : ( sitInalm I 

flucoivod by: (Sl ij iiiittiio) 

LNVIHONMENTAL, INQ P110141H * 140, (2-14.) , 63 -1-00 2-'1 

'7"/1.5 Sc)vc-r-e -ign IRON•] FAX tio- (214) 905-0634- 

D A L L A S y I'X 7 5 2.* 7 CHAI N OF "U" U STODY RECORD 

Namo of Unit nii(I Addtoss: 

,~- l ~~+~. l ~~ ~.- ~ ~ ~- ~~ 

~ ~-~- 

IlUnibor Stim lutJ S mplod 

~~ 

qj ~~ _ 

~~ ~~~ ~ 

Na 61~- b (ct- 4L 

&'7 f - ~~ ~~ - 3 ~~o - lF L o ~ $f~.,~~.. 

~O ~ l 1.~ _ ~ r,G ___ ~~~~ --- 

142,0, 

floiin( o( )y (Si riat~ ) — ) ato Tiiii(i 11ocoiv 

11,31i croist (J y - I 91► alum) 0-.116 Tiiiio 'Ignatut 

Dosc6plion of Samplus 

~; ~ : c~ 6e- I 

; '('- c- e.- &e,l 

~ e4t7 ,s..~ 

1101in(pishod by., (signalum) Dato Tiitto flocoivcd lor Labofatw y by: (Sig .) Dato Tillio Flommiks 

Distilbution: Otiginal Accompanies Shipment 

(0'), 

Copy 10 Clio W/Plojecl Gooldinalof 
. 

: ' 

. ~ ~' ` , ; / 

q-1 6 i~ 

Silica GeI Weights 

Company:; ~ = ~ , ; ~i( ; , 1+~:~.; ~, - Test Dates: 

.,. 

, 

l 

Location(Sotirce ~) RLn r;' 1 Run= ~~- Runn _ ~ 

r 

1 ! 

0~ I Z 

207. 9 

2'.'18 
Appendix E 
FI-E•D DATA 

PLANIT: ~ J 

D,4=r-: 

REPETITION: 7 

LOCATION (Z-, OURCE-.): ,--,,, nwlprN -G1 --;RS 

0H:-:R.A,TOR: rhpa.L 

SAIvIPLE TRAINT 

bETER BOX 9: _-#2 

BAROINIETRIC PRESSURE: 3 l o 6 

-ANOIENIT TEINIPEPLMFUJREP: 4 

ASST_T.N,lF_D,\40IS7IJRE: 2.,~~,o -ru5 

PROBE LENGTH: 600 .3 NOZZLEDIA.METEK, 3 0? 1 

STACK DUMETER: f 

hfETER H: CO2 02 

C FACTOR: 

METER CO-EFFICIENT: 

FILTER TARE: 

PRE-TEST LtA.K.'CHECK ~POST-TEST LEAK CHE 

Meter: 6.,noo cu.ft. in. HG M-ter- cuft in. HG 

Pitots: ~ el-,- (o), in.. H2O. Pitots: (o, in. k20 

am W.111nWqw_ 

" 

 ".-emlEnNo w-Elfil m, 104 W'

, I ME t W~ ,,, u Well. NOW. I m i OM. 

! ~'~ 'r~ , ( f' )t~ l ~O~I /, ~' * A. 

n3 P, .1 g -,: 2- ; ~ -6 Vqqc( -6 q I S~~ 

~. . ~. :~3 ~~ I . a 7 ./. ~, v ' ~ - ~I ~ 3 I, -~ . ................. l ~a~ I ~-~ 71., _5 ~6 1 , ~ a ;po" 

y l . 

. I, 9? z) 

~ : ~~ 3~ .~~ 1 .~ ,~ 1/yo - * .7 , ~ ~~ 

(. : ^ l • ~ / 7 ~ ~ ~ / ;7,r-& %2 

Z, 

2 12-6 

~ - ~r !~ ~ ~, I ~ , ~ C) a3 

r~ I - r• 7 3 1 25~; 6 1? 1 /7 

=~- 

•

~b I ~ I I I ~ 

.

y~-. 3 ~~ 1 ' I I ~ 1 1/ I,/ 7 . I 1 1 ? -2 1 d 

L I ~ ~~ 7 i. ~ ~ ~-~.,~v. ~ (~ I,~ 19 

3 - 1132 1, > ~ , y I ~-~;, ~' ~ ~ I ; 6C ~ ~ 

~ I ." i . S:5 zrri 

S7, 3 Y k S. llrT__ A s~_ l ~ 

~ I •, ~ ~ f [73r ! ~ ~ ~ ~.~-~ f ~ ~ I~ ~ c7 1-~,) i . / f ~ /~ ~ ~ ~ 3--d ~ f ~7 ! z ''L i G ~' ~ / ~ ~ P o PV I r 33' I f ~• ~~~~.~ f'~'~. I r 1. 16 9 1 

ir.o.~ I I 11 1 !16?,? 3 -31 I ' I I I JI 

!I I f { ~ I I I I I' I I ! I_ 

[A " ~ 3 3 I I I I 12 41 6j 

7 / 1 

C; 

~

1 
n! J[PmTGERS 

1`? ttk7~ 

~.~ ~~•~ ~...~ 

2 

-AJ 

17znal 

2-Y ~ 

lG~ 

~•O ~ , ,~ 

CO2 02 

. ~ja • ~ ~ 

PQST-TESE_4,K CHP. 

Meter: o' cu.f( ~ .%D 11)1r in. HG 

l.7. i21. x?O 

G•1ELD :l?ATA 

?L:3.. a . n =- % `l / /~~ 

DATE: U--1.2 'c~` ~ 

REPLTITlOr : -? f 

7.QCATi0?~ r,.S4Ux.CE -): ~ 

0?~~ ~. ± O~: <~ S • 

SA?NP,t"E TRA.~~T 4: ! ~ 

NCH T.1l.:,-R BOx ,~: i ~ 

BAROMETRIC PRESSURE: 

AIMB.1.Nr' 

ASSUI,~D MOISTtI`' tE : 

PROB LENGTH: ~ r 

r~ E 

N 02ZLE D L4METER: 301 1 310 ,A•~i> 

STACK DL4METER: 

I1xETER H: 

C FACTOR: , c~ 

METER CO-EF'F'ICIE?!'T: 

FIL=R T.ARt: 

PRE-TEST LEA.K C}3ECK 

p e~tec. ~~ cu.n 

@ ~ri , u 

 HG 

 n • 

RL:v' ::•s` ~vr. r 

~ ,, O .FiR~~~ 

"N.M. 

 S'~f 

~Y3r ?~ 

t ~{ 

'~~~~, '~. t~ 

RZ•r . Y` 

R2

, 

v t~Xt 

~~ ~? 

s ~Q~ 

if`s - `E ,4 

~ ~ _ 

.C~' . ~ ro 

~~~~~ ~M. ~~Y~ CI • ~ !o~ Se: ,CRID.. ~i~Z'~1111'O . ft~~ 

/ ~~. ~, . 

~ 63 -~ ~ ~~~ ~ , ~ l I . ~s" ~ 9.~ ~ ~a yJ ~ '3. 

::~=:. ,• ~; I , , I 1. ~I - ~2_ S^ f/, ~ 

1 ' 13L , / g I •ss ! 73 , t/ f' 

11 ,3 -2-;~ i I .v ? , I ~ I ~ ? ~s 

:3S ? - .2a I ,/ 196- 

•216 A _;-:11 ~ 1 1 '/, c;? ~!z 76 i0 

l 

r • 

~' C?3 "~;b /c) 

, 

j. .53 

~ ! : s~ I ~ •~~ I - < "3 p-, 

~ I:J I ► r' 7 ' I' ~~ I ~ dl Ic/S . 

I 1 oe 8~ 

1f7•1 5 

C) 

/q I lbo e;2 ~~.~ 

I I X I l 1~ I 

1/2)L 1 , ~~ I ,-3 I ~~S-, I ~ I1,-;,.g ;'7 ~~ I~' ~ ~~ '' : ~~ I I~~ I•~~ I 1 , /, ~ I~ 

, ~ . s I ~~s f~ la~~l~`~ 1~ 1 

lf3

+ 

' r9 

__1_ I I I I I I I l I I I 

_. I I I I I I ~ (, isa I I I 124 i ~ 
FIELD T3ATA 

?LA `T 'JG• ~ • r trc ~ t L 

DATE: C f c6 

REP.ETI TIO2~r: ;? 

I,CGCATION (SOLRCr ::-): 

OPEtZATOR: 

, 

NSTER. Box r: ~t 

BAROMETRIC PRESSURE: 

E\~ t' TIvT-.=,I vAiUP..c,: ~ 

A SS'tTItiTED iv10IST"uRP: ~;6 °'/.- 

PROBE LENGTri: G ~ 

NOZZLE DLg.METER: ,r 3c) ~F~ 

STACKDL4112ETER: 

N'IETER H: 

C FACTOR: s`~ 

METER CO-EFFICIENT:, 7 j L. 

FII,TER TARE: L 

PRE-TEST LE.A.K CHECK 

Meter:G• cu.ft, @ in. HG 

Pitnts• ✓ n in . mo 

iTIPPN GERS 

6 

..,, 

7~ Y _ 

J 

7'

6 

 ~2 

2_L ©1Z 

CO2 . 02 

3.> 

~•-~~- ~ ~ 7~ 

POST-TEST LEAK CHECK 

Meterr, .0 00 cu.ft. @ ! 0in. HG 

Pitrnt•c i (a~ !~''71in- 142n 

` x~ 

~5.~~ 

~~ •~ a ~4v ~ R'W" '~ j' ~11~ 

. •• res + c 

44 `C~~ ~• ~~~ r 1 ~ ~ ~ ~ ~ ~ ~~~ R

aa 

~ ~ / l3• S~~ / '3 k ; - ~~' /, ~ r / , ~ S S~ 1667C~ 

I~.S / I I 1// 9 1do I 

i ew 39~, _ 

6 t 

Z3 ~ I r ~ I 7. .~, .5 C)3 ~6 09 

~ I:•/ I ~ I~ O~l 

. _ I, ~~J ~~ ~~ a~~ ~ i~' 

! ~ I I I .o~•~ . / • ~ r` I '~7` ~ ! / 

, 

- 3F- I I,.9V I. 1 /- 0-s 

I y~~s~ 

1 6/ r ~ . l,~ ~ . ~ ~,3 ~~ 177 ~ l~ 

1/ ~ a 19 7 l g~. 3~ 1 I ~ 

q ,0,2- 1, w a ~V I 

sg 97 ! • f? /J ! ct r ~ 

%3 

6 3 

I76. Il"•71A~s I~'~s~ 1~ 6i/ 

~~. 7 ~ ~ ~~ y~~I I I~ I I I~ ~• ~" ~~ i I 1 I 

. I I 1 I' ~ • ; I I ( I 

I6I 
I.hIMENTGERS 

~ Iil 

 v~I~

al 

:192 

473 f00 

r'~ ' .-~4 l L)O r C70 

_. 

' 6 

CO2 02 

1!` ~ 

PQST-TEST_LF.,,K C Ft 

Meter: d' , G~r/Scu.~ @~~ in. HG 

Di bniv1_11_1~ - /ii1 ~~. 

~}' FI ELD •/ ~'~ .l_ ~. 

t~L=i..~~ T: ~c ~~.~~ ~~~l.U~iGI~ ( '~ri , l ~ 

~ 

DA t//'1,?- . ! 

REbFTITION: 

LOCS. T1ON (SO vRCE 

..r:rvP::.P..~':'OR: •~ 

S?lv/i LE TRATN r: 1' ~' ~_ 

I~E TER BOX r: 10 ~ 

B AROMETRIC PRESSHRE: 2.`~ 

AIvf3 NT TEMP :RAT'uTRE: 9'-" 

ASS'vNCED MOIS T.-R—E: r ~ 

PROPE LENGTH: ~ ~ 

h 0 ZZLE DLAMETER: , 31 Z ~ • ~f ~ • f ~' 

STACh: DL4METER:5. 7~"` 

METER H: 

C FACTOR: , 

NMTER CO-EFFICIENT: 1,b 

FMTER TA.RB: 

PRE-'TEST IfEAK CHECK 

Meter: 6. cu.ft. Qa in. HG 

Pitntc' tnl ~ ! in T47C1 

PEN. 

t ~3

INx

~ 

rY ~I~'~ ;C~i..~T °'Lt • IrC-t '~ ~tt ~t. c?a :C 0 ~ '~.L• ;~rty~ 

Le), ~ ~o -Za "~. ~~~ ~~ 

3. 

2-3 gl•~ <<~ 

4s! I 

,~ 

C e~-5-7 1 J 

1/3~,. Z f 1 7~3, SF-F 3 

~ : \~- . ~::.•; ;. ~ 1 , `~ ~~/ '~••~ ( v • {~ .~J" ::jS-- I• 

31 ,: z _ _ I ~ 5-9~ J j, W- 73 2,~~ I,~:~ ~ 

3 

~.6 -6 . ~ ~ gS— 0,0ol ~ 

k=1 

~ 1 - ~'~- .: I .3 r ! S ' ~ I '• / I ~~~ r I f}.~ ~L~~ .6 ~ 

Eq 03, ~3' 

1 t -7-3 I 0 . )~1 C-6 I F—;—T~ 

2o I I13 , L I I.o~ 3, ~. '$ I 26z 1 Z~q- I~ 

I 
PL ~7T: r :~; ~ ; , I ~ ~~ 

r ~'t.~~,,~ .~~ 

~.~~~,~ r~.~ r:~ 

DATE: y f 2 G` 

REPETITIONT: 

L4CATION (S O Uk2CE :') J~~"' ~'1 IMPZNGERS 

0PERAT0R:-4Lq"-- ~ ~ 

S:~LE TRAI~I z: ~ `' 

±nitiai 

~ i I~ 

xinai 

) C f 

IvETER BOX 

B AROMETRIC

. 

 P' SSURE: 25 

r2 1`~~ ~~ 1'~ 

ASSU~~D MOIaT'u~. ZG' 

.A?~~BTENT TEMPERATU—RE: S2> 

^5-L 

PROBE LENGTH. • 

STACK DIAMETER: 

NOZZLE DIAMETER: 

METER H: ~{~~ 

C FACTOR: . F 

CO2 

3 

02 

J ~ 

METER CO-EF'B'ICIENT: 1,0 ! 

FILTER TARE: - 

PRE-TEST LEA.K CHECK 

Meter: 3. op7cu.ft. @_/ ~. in HG 

POST-TEST LE• _4K C1TEC 

Meter: o- 0)/e) cu.ft. @ n. HG 

Pitots: (a, ~ in: H20 Pitots: ~~-~ in: H2G 

IN :#~ " ~`~ltg 

~. ~ 

~ ~m ; ~ ` y 

~ ~i ~~~C~~~iFC~~~l.. 

~ ~ ~~iiu i ~k~ ~. : 

.~~ ~c+ tle"t~ 

~ m p" 

 ~ "''et'~1~ gn . 

l 1019 Lz If7- ► 20 

47~ D~ ~ 

~ ~--.~ z 3 S ' 1 , ~y ~• ~ ~~: ~~ 1 0 I 

4:7 

. ~,•~ .t~.: ~ ~~:~. 

3 1 

~ 1-` ~:• ~~ I I I ~~ i ~ ~-~. - Ls' ~ 5.7 

~ I = ~~ I s 3 10 ~~ 1 .% ~• / 1 - 1;~T I 4;r ~ 

CI 

 3 

. -. ~ 

I 

,~.~ ~~ 1 o z s—► Al ~ 

36 z.. ~,=:~ :: ~-~. ~~~ 1~ y I 

~~~ 1~ z A`Z- 

~ ;0S- L 

I r I i ~-~ 1 ~ 

~ I-~~t I I 13 y I• L . I., ~ ~~.~~. ,-~l~~~l ~~ I~ I~~` I 3~ , 

38 ~`f ~ ~-~71-- L.~ 

L.3I 

Avc. 
FI-E.ILD :DAT~'~ 

Pi....=u\TT: ~ _:' l ~r~~~ 

,s 

DAT'r'.: 

~REPETITIO'NT: 

~TOCyTiOIN (s U;RCE 

OPERATOR: 7z-f' 

T RAIN r: ~ 

IvETER BOX :4 : I iD 

BAIZONXETRIC PRESSURE: 

~ IhIBIEINi T7W--ED.A_nT ~ : 

.ASSu?NhEJ AfOI: i urZ':: 

?RO3E LENGTH: 6 ' 

NOZZLE DL4METER: 

STACK DLAAMETERJS, S'- 

METER rI: /. y/6 

C FACTOR: _ g-W 

METER CO-EFFICI'ENT:I- ~ 

F i L i—ER T_ARE: 

PI2E-TEST LE 4k; C1,IECK' 

Meter: cu.ft. ~y? in. HG 

Pitots: /. ,- r.ni. .f- ~y iti . H2n 

;1xPINGERS 

Iilitial ~ iiial 

42~°~' 

L D ~ hv . 

.L✓ ~j~ti~A ~ !'~ ~ v , r

..—. 

2 Z~ ~ J 

CO2 02 

3- s'" ~ ~, r— 

PQST-TEST LEAK CHECK. 

Meter : a, oI 6 cu.ft. @ ~n. HG 

PitnYs• 'v n G i n T~,)CI 

•~n..~t'L~ ~.~~`,T, im _'s~r ",C1~ "'~.~~",,~°:t,~~~ ~~''~~~'' 

~~~CM~'.~~'..."r.~".~i~•~r .~~~~~E;.,=~ Ci.c$Si~:~'~ 

.•.. sh ,~ tJl~~'~' 

n .,';~..+,? - ~R:Z~ ~ - ~✓.7 

~inlil 

:.. }~S1..A !<~ 

c~ita, ~`'.. . .,~ 

.~n~".' 'S'N , ,•, .~li~~ ...'-....Ye°t, ~ ~ r.y 

e.x-:x•; ~.w~ 

'~G?ven 

~ ;,OULIC~7~:~ xem. 

•• n iii 

'.~. 

G r 1 : ~"i -- ~ 1 ~ ~ f ~~ I ~. ~- .~r .~ f • ~~- ~ ~°~` ! 2s~ ~ 

L ' i .SV ~ ! ~ ~ L ~ ! ~~ f .~j• 1 . ~v~ ~ i ~1/ n,•~~' 3 

• 

ZT~ 

 J 

~ ! ~' ~`~ 

, ~ 

~ ! ~ ~~ ~~ • ~ , ~3 I :, ~ ~~ ~ - ,. ! ~a~ ~ ( ,z:s-a~ ~-s~~~ ~ 

I Is7- Gi__- 3 

~ I '. ~3 ~13~ 0 1 ~ ! ,. ~. ~:~,~~: 

~,.~,~~~•• 

:~~ 1 L~•. ~~ ! ~ 

jJ9 ~ j~ ` ~: . ~ f ~.. . ~ 

~ a: ~ 03 •.`~ ~ ~ ~ :~ ( ~ 

. ~ •;~-~~ l~3~ .-~~- ~ ,~..~ z~ 1 a~ =~~: ~~~-,.~~~1~ ; 

i ~kp ~ Z ~ 

! . ! I. ~ ~ / !. ! r K ' I ~j`•'.~i ::L / V ~ ! ~'~ •?j} ~ ~\' ... ' . 

jr/ ~ I~ ` ~~r 

• ~/ (. ~ ✓`~ 

. . • 

/~ I 

~i ~~ 

I 

~ 4 I • 

• 

jV%Lg Z3 • o 1 

~ /0.Z i ~'i~ ~ 25Y 

L.. , r~ ~r V I ~ ~ ~2 '~ ~ 3 

/ 3 + oL• • 1 L ~ 1 `~,~ 

~ ~ = ~~ !• 3 ( b 1 S , ~ 1~~3 ~ .~ 1 p 3 ~'j ~ ~~- ~ Y ~ 

I ~ 

~ I - yo I I Ja I.0 c/ I I d I"--, I / -/ j G'% J I Ls1 I/ 

3 7/2~1 

, v-s ~ai. Il~ ie-sT- 

' ~ ~ •i . I f ~ • ~ ; ~ 

IIA•= i I I I I I I I I I 1 1251I 
FL0W DATA 

i

.. ..'... ....... ___......._.' 

, 

PLA.N'T ~ 

DATE: 

RU : 1~T ~ •;~ ~ I~'~ ~ ~~~eC.~~. 

Ce"

LoCA''IO ~ti (SOURCE r): ~~~~ ~ ~~3~ r 

OPERATOR: 

AMBIENT TEMPERATURE: 

BARC)METRIC PRESSTJ-RE: CO2 

ASSUIVIED MOISTURE: 

STACK DLAMETER: 

C FACTOR: 

COMMENTS: 

02 

21;2 
FTELD JDAT.-k 

P 

v . I '//,~ r, 

L.A21 \T: 

DATE-: 

REPF T7 

, A T j D'N' k,S 0 U- _ R C E 

s-kmPLF,TR.A,-,N. -L 

•MTER BOX 

BAROMETRIC PRESSURE: Z 7-4L CO, 

Al\,Ml=—N, T TEIN~'EP_k=RE: In ASSUINED, MOISTIURE''7-7.5 

PROBE LENGTH: 3_5 ~ ~z~~ . ~~ 

NOZLLF, DIAMETER:, V-1 

,.:S.TACK DIAMETER: IV. 

'A'r -,.Pl'.N - GE -RS 

Iiiitial 

2 

i fl 

#6 

r i rn 

~ ~, ~s 

c-7 

hiETER H: CO2 

C FACTOR:, 

METER CO-EFFICrENT: 

FILTER TARE: 

PRE-rEST LE-4-K CHF, 

metero• ~cu.ft. 

in* 

HG 

PiLots: a, I in,:H20, 

/s POST-TEST LE-4K CEIECK. 

Meter: cult. in. HG 
.~1'f ~ ~r~~ %~", c-` 

?L~~T: P¢ 1 l ri~.~ET.~D D:~T.~ 

DATE: 

REPETITZO _N: Z, 

r,~ r I.00ATIOT (SO`RCE ~):~ ~,, ~ I7YIPLt'GERS 

Op'—PR-,k T OR: I11Zt1al F IIIa! 

SATv~LE TR.4I;~F r: ~ ~ ~ 1 /-w /.3`I.• ~

BOX r: 11.3 

BAROMETRIC PRESSURE: #; (do 1 067 

~~IENT' i~~ fPER4i UPtE:

ASSTJ D MOIS T t~-RE: ~ 

r.~ 

r5 Z~~ ' '~ 

~_ 

Z>r ~'~ 

'ROBE LENGTrI: 

IdOZZLE DL4METER:,.?jy ~~ ~ y' 8 

STACK DLOIET~ :~y,~ 

METER H: /. ~ 7 CO2 02 

C FACTOR: . FqMETER CO-EMCIENT: . 77 Z.~ 3 C? FILTER TA.RB: ~ 3 7 2 

PRE-TEST LE4K ~ECK 

Meter:p o°O cu.f`t~(a~/S in. HG 

POST-TEST LE.4K CHECK 

Meter:~~° cu.ft. @/.~in. HG 

Pit.ots: . ~ (r~ ~' f in.. H2O. Pitots: "n. H20 

~ 

••u11 • Y ~1 

e 

/ le?f's-0 ~6 , ~' l~ 1 'FL Z,s~rl c' I a 

I . 3 ! 

47 

lzo 

Y l . os - ~~' ~ , I ,:c . ~, 6 ' ~~ • !~~ ~ 1 i 

.t~- 

~ ! ~ , ~-- ' y~~~ 6• ~ , l~Z, y-. 

~ , ~ ! ~:.- : 

Z3~ • • I 

>> ,.7i ~,3r, ! g.~' 

~ 

:. 70 1 lD 

• ~- ~I ~ ; z~ ~~~ I ~~ . 3 . . , ~ ~ 1z4z r 

~ . : 3 ~ ! ! ~/ . 3 ! • ~ Z • ~ ~ 2~/ 3 ~ `~ z6~ ~ ~l . 

~~ I = ~ ~ ~ • . ! ~-z . . I . I - ~~ ~ I ~~, ~ ~ ~ ~~ ~.~ I C 

z 

zO: 0 1 

! ! I I , I ~ ! • 

I •' ! ~ ! ! I ~ ~ i f ~ 

„_. I I I I I ~, ysl I I I254 
1 PLA.NT: ~ . l~r~ 

FIEL•D DATA 

DA'I'E: `//! 

PE?'BTITiON: 

L0~. :T10IN (`0 U`tr C.ri 1S,U)J.:\ Gx:.RS 

OP~R.~TOR: y~'-i-` Ini:ial : iiial 

SANi.?LE iRAIN r: 1 ~ ri / dd L j~ ~ fu ; 3'

I~~TER BOX 7 : ! ► ~ 

PRESS ~iRE:2~~~ 

r2 ~ J ~~ Z 

BAR4METRIC ~3/ 60 

~~lf B1~NT TF_r-f?E~~T~L,E: 

=:SSV~D MOZSTIUR.: 

44-~ 

~5~ a' ~~r' 

6 

~ t 3 •~ 

PROBE LENGTH: 

N0ZZLEDL4..NSETER:. 

STACk DIAMETER: Zq. 

AZETER H:l, CO2 02 

C FACTOR: 

. ~ A'1ETER CO-EFFxCTEr'T: ~ ~ Z p 

FILT'ER TARE: _ 

PRE-TEST LE_A ~s: CHE ~C ,. POST-TEST LEAK CH.ECK 

.Meter: o- U~cu.ft. ~ , !' in. HG Meter: o.oaa cu.f. @ t ? in. HG 

Pitots: L~` ' a, - z - in: .H2O_ Pitots: v 0 s, 7- in. H20 

c T3m •`.. ii ei" M. 'IN-0 U ~C ' D C1riD G 

( • 

igs~~ ~'~- ~ f & 7s` /0 

. .: 61 6 ~ l 

3

. _Z..r- ~v 11J I I Z, 

14 ~. — 11,3 1 12,6 ~. y i ~~ ~ r~~ ~~ ZZ 

z ZFr., To , 

_ , C V7 a- IL W~-- (6 

1 l~ 12 1 

I I z 

© 

• ~ I J" QZ i ~~ l r L ..~ `b ~ O1Z71-7 IZ-CC l oec 1 // 

1 ~ ~ : 6 . ( . ~ Z•Z 3~3-~' ~/ ~~ ~S~ ~~ 1/ 

14.~r .3 I 1 . I . ~ 72, ~~ ~s—t'~ ~' ~o 

" I I~ zzY35g I 

. ► ► . , , , 
Ft~L.'D D:7.rJ.A 

PL aNT: 

DATr.: 

R. EPETIT O ~ LOCAT:OA7lS hR CE r) :~, , r K, ( " 

O?ER,.A.TOR: ~ S 

S?i'LE Tr2AIN :#: 

NSTER BOX :: / o 

BAROMETRZC PRESSURE: 

Q MBIENT TErAPERa TUR~~ : SsS 

ASSU-l\,fF-D MOIS TURE: 

PROBE LENGT H: ; '~ '' 

I\7 0ZZLE DIAMETF{.R: , 2

q` ' ~~ `l ~ 1•~ ' ~r~•q~3 

STACK DLA.METER:~#.'j` ~

11 ~ETER H: 1, y~ ~ 

C FACTOR: 

METER CO-EFFICIENT: I. ~ 

r'TLTER TARr:-~" 

PRE-TEST LEA.K CHECK 

- n SPIN G.ERS 

=ni.t:al 

C7, 

Tj !'1 W `~~-II `7 .✓ 

CO2 

~ 

_3 

POST-TEST LE_4K CHECK 

7.1 lal l vs 

cf3 

Gb ' ~ 

02 

l ~f 
I7ti7PPNGERS 

l.iitia; 

A 

j cJ J 

~_>" ~,?, r'4.~ 

~ 

/w 

r6 

' BSfv 

CO2 02 

3 l~ 

PQST-TEST LE4S~ CHECK 

Meter: 0.0 1cu.ft. a(~ ~T in. HG 

Pitots: v' n r- -j in. I420 

:FTELD DAT'A 

L c, 

DATE: '4 - r,) -o ~- 

REPE i ITI ON : T, 

:.C)CATiO-N (SOuRCL,-j: 

; ~--- 

OPERATOR: ~' . C - 

S ~,.?~,TLE T R.yINT r: 

r•CPTER BOX y: I v 

BAROMETRIC PRESST3RE: a F, ? 

.'j'..\J7r_:~ 1 iilvT.L~~.a~-t-Pw: g ~ ~ 5 

ASSi,fi,fED MOISi'L-RZ-: 7 

PROBE LEN=: ~p x 

NOZZLE DL4METER: ~ r STACK DL4.I12ETER: ~ j

METER H: f. Lfl(v 

C FACTOR: . ~v 

METER CO-EFFICIEhrT: 

FILTER TARfi:-- 

PRE-TEST LEAK CHEC~ 

Meter: cu.ft. @ !S'Iri. HG 

Pitats- . i (a~ iin_ H20 

Ctti ~ D 

'.a - 

: t~ '.l 

~ 

, 

f- ~ 0J 

C4 104 s 

I -, ~~ ~ ~ ~ ~ ~~ •~~ ~~~ ~ 

I Z.cq 

I. I 

U 371 /2 1.A . , /~ ~, G~ iXol? 

d r L67' 1 6-6-I. 

01, 6 I I I 

1 -I 
FIELD DATA 

PL.ANT: ~ ~t 1C 

DATE: ~ J7 /. ~j ~ 

REPETI OI~4: ' 3 

LOCATION (SOIIRCE 

OPERATOR: --5 l 

SA.MELE TRAiN ~:y ~c( 

METER BOX 

B 

#: ~j 

ARdMETRI~PRESSURE: Zf7 •~ 

AIvMIENT,~TEI0PER4TURE: '70 

ASSUhED MOiSTVRE: 7- 

~ROBE LENG- TH: 50 ` 

NOZZLE DIAMETER: . La,; 

STACK DIAMETEt:Z',q/ 

?VIETER H: 

C FACTOR: , k'q 

METER CO EFFICIENT: l, o 

FII.TER T.ARE ,--- 

PRE-TEST LEAK CHECK . 

Meterk::2.oc., 5`ca.ft. @ /r&. HG 

Pitots: 4-- na, ~ L in. H20 

IMWINGERS 

~ Tiutial 

sI /vo 

i ~ 

#2 I 'fo 

413 r'y° 1 IP~.~ t~ 

Z=4 /Lej 

-rur6 

CO2 

3 

~ 

POST-TEST LEAK CHECK 

Pitots: U ~ vo ~(a ,@s ~ in Fi20 

Final 

~ 17,9 

p 7 

02 

1q 

19 

L u1 7rr 1 PI N ~• 

+~s c~~ 

.(.~~ 

~~,, ~` 

~~~lipC~ 

'`~- ~, 

~:~ ~~ :, ~Tm 

:;.~oiitl 

i WMi'•~ `~'\. 

-.-o Ac:.~ .,~~z 

.. 

r. ~ , g~ ~ ~j_ 7L 

L . ` ~ 

f.. t.. ..-s iK~: ' /i /~ ~ • ~ 3 f • D : ~ (7GY ~ ~ . 3 ` 

I ~~ •: ~ ~ I ~ , y_ , 

6V 

7. 

~ 

~ 

, 

~~ 7 

! r ~(~ ~ • ~ /~ / / (/t~ 2 e~ v 

(7/ 

ll 

• ~['% `, •i 0 =ti / , q 7 I ~` i ~ / ., ;. . _

~ • i ~i 7 ~lo r / ~%,~ 

: ..3 ~ ~ . C +~ - 

I 3 

~ 

. ~ 

I I 1 

I I %~ > . I 

2 .~1 ~ 
FLE1W DATA 

PLANT ~ 

DATE: 

RU ~ , N n. 

~ 

i 

LOCATION (SOURCE n): ~% 

OPERg.TOR: X17"'- AMBIENT TEMPERATURE: 

BAROMETRIC PRESSURE: CO2 02 

ASSUMED MOZSTURE: 

STACK DIAMETER: 

C FACTOR: 

~ COMMENTS: 259 

APE Armstrong Environmental Inc. CONVERSION FACTORS 

EPA Method 5 

522 Series Meter Box Calibration 1 mm Hg - 0.13330 kPa 

Pre-Test Oririce Method 1 cm = 0.39370 inch 

Englisti Meter Box Units, English IC Factor 1 mm - 0.03937 inch 

1 cu ft = 28.32 liters 

eter Box f 10 Date: -------------------------> 03/15l06 

trial #: 30272 Barometric Pressure: ----------> 29.95 (in. Hg) 

Tfreoretica) Critical Vacuum:---> 14.13 (in. Hg) 

illltt 

IPORTAI% For valid lest resulls, Itre Actual Vactrum should be 1 lo 2 in. Hg greater than the Theorelical Critical Vacuuni shown above. 

1PORTAI% 

t!!!l •. 

The Critical Orifice Coefficient, K', rnrrsl be enlered in English units, (ft)"3•(deg R)^0.5/((in.Hg)'(min)). 

------ --------- DRY GAS METER READINGS ------------ -CRITICAL ORIFICE READINGS- 

-- Average Temperalutes -- 

Volunie Voitime Voliirrie Initial Temps. Final Temps. Orifice K' Oririce Actua) -- Ambiont Temperature -- DGM DGM Ambient 

ciH Tin e Initial Final Totat Inlet Outlet Inlel Oullel Serial# Coelficiont Vacuum (rtilial Final Average Outlet Overall Temp 

► H20) (niin) (cu fl) (cu ft) (cu ft) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) (deg F7 (deg F) (deg R) (deg R) (deg R) 

0.24 5.00 652.700 654.270 1.570 66.0 65.0 66.0 65.0 40 0.242 23.0 64.0 64.0 64.0 525.0 525.5 524.0 

0.50 5.00 654.600 656.847 2.247 66.0 66.0 66.0 66.0 48 0.344 21.0 63.0 64.0 63.5 526.0 526.0 523.5 

0.93 5.00 657.500 660.520 3.020 66.0 66.0 67.0 66.0 55 0.464 19.5 64.0 64.0 64.0 526.0 526.3 524.0 

1.60 5.00 661.300 665.172 3.872 67.0 66.0 68.0 66.0 63 0.693 18.0 64.0 64.0 64.0 526.0 526.8 524.0 

2.90 5.00 656.000 671.320 5.320 68.0 66.0 71.0 68.0 73 0.824 16.0 64.0 64.0 64.0 527.0 528.3 524.0 

................................................. 

RESULTS 

 ................................................... 

• DRY GAS METER --- --------- ORIFICE --------- -- DRY GAS METER -- --------- ORIFICE --------- 

XUME VOLUME VOLUME VOLUME VOLUME CALIBRATION FACTOR CALIBRATION FACTOR 

ORRECT CORRECTED CORRECT CORRECT NOMINAL Y dHQ 

Vm(std) Vm(std) Vcr(std) Vcr(sld) Vcr Value Variation Value Variation 

(cu ft) (liters) (cu fl) (lilers) (cu fl) (number) (number) (in H20) (in H20) 

1.579 0.1 1.585 0.1 1.572 1.004 0.003 1.352 -0.0635 

2.260 0.1 2.253 0.1 2.233 0.997 -0.003 1.391 -0.024 

3.039 0.1 3.035 0.1 3.010 0.999 -0.002 1.427 0.011 

3.899 0.2 3.882 0.2 3.850 0.996 -0.005 1.500 0.084 

5.359 0.2 5.389 0.2 5.345 1.006 0.006 1.408 -0.008 

Average Y ------- > 1.000 1.416 <------- Average dH@ 

ote: For Calibration Factor Y, the ratio of the reading of the cafibration meler to the dry gas meler, 

acceptabie tolorance of individtial valttes from the averago is +-0.02. 

For Orifice Calibration Factor dH@, tlte orifice differential pressure in inches of H20 ltial equales to 0.75 efm_of air 

at 68 F and 29.92 inches of I-ig, acceptable jolerance of individual Nalues from lhe average is +-0.2. 

.-.~- _ 

SIGNED:~/ f ~. ~ /~s"'L i ~1. Date:~ ` /-J,~f ~ •~ 

i 

N) 

cn 

Q 
Temperature Meter Calibrations 

Meter Box #: 10 

Date: 03/15/06 

Calibrated By: RT 

Emtech 42312 

Degrees F Calibrator Probe Stack Oven Exit Auxillary 

Point 1 32 33 32 34 32 32 

Point 2 212 213 212 214 212 212 

Point 3 752 754 752 754 752 752 

Emtech 42312 

Degrees R Calibrator Probe Stack Oven Exit Auxillary 

Point 1 492 493 492 494 492 492 

Point 2 672 673 672 674 672 672 

Point 3 1212 1214 1212 1214 1212 1212 

Percent Difference 

Probe Stack Oven Exit Auxiflary 

Point 1 0.20284 0 0.404858 0 0 

Point 2 0.148588 0 0.296736 0 0 

Point 3 0.164745 0 0.164745 0 0 

261 
Armstrong Environmental Inc. CONVERSION FACTORS 

EPA Method .ri 

511 Series Meter Box Calibration - 

1 mm Hg = 0.13330 kPa 

Post-Test Orifice Method 1 cm = 0.39370 inch 

English Meter Box Units, English K' Factor 1 mm - 0.03937 inch 

t cu ft = 28.32 liters 

er Box fi 10 Date: ---------- ---- ----------- > 04/14/06 

al #: 30272 Barometric Pressure: ----------> 29.75 (in. Hg) 

Theoretical Critical Vacuum: --- > 14.03 (in. Hg) 

I!I 

'ORTAt. For valid test results, the Actual Vacuum shouid be 1 to 2 in. Hg greater than the Theoretical Critical Vacuum shown above. 

'ORTAI\ The Critical Orifice Coefficient, K', rnust be entered in English units, (1()^3'(deg R)"0.5/((In.Hg)"(min)). 

1!! 

---------------- DRY GAS METER READINGS ---------------- -CRITICAL ORIFICE READINGSTheoreticai Critical Vacuum: --- > 14.03 (in. Hg) 

Voltrmo Volume Volume Initial Temps. Final Temps. Orifice K' Orifice Actual -- Ambient Temperature -- DGM DGM Ambient 

dH Time Initial Final Total Inlet Outlet Inlet Outlet Seriai# Coeffcient Vacuum Initial Final Average Outlet Overall Teinp 

120) (min) (cu ft) (cu ft) (cu ft) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (cieg R) 

0.92 6.00 99.700 103.374 3.674 77.0 76.0 78.0 77.0 55 0.464 19.5 76.0 76.0 76.0 536.5 537.0 536.0 

0.92 6.00 103.700 107.377 3.677 78.0 77.0 78.0 77.0 55 0.464 19.5 76.0 75.0 75.5 537.0 537.5 535.5 

0.92 7.00 107.800 112.085 4.285 78.0 77.0 78.0 77.0 55 0.464 19.5 76.0 76.0 76.0 537.0 537.5 536.0 

. .............................................. RESULTS .... ... ............................................ 

)RY GAS METER --- --------- ORIFICE --------- -- DRY GAS METER -- 

.UME VOLUME VOLUME VOLUME VOLUME CALIBRATION FACTOR 

tRECTI CORRECTED CORRECTI CORRECTI NOMINAL Y 

'm(std) Vm(std) Vcr(std) Vcr(std) Vcr Value Variation 

(cu ft) (liters) (cu ft) (liters) (cu ft) (number) (number) 

3.599 0.1 3.577 0.1 3.653 0.994 -0.001 

3.598 0.1 3.578 0.1 3.651 0.994 -0.000 

4.193 0.2 4.173 0.2 4.262 0.995 0.001 

Average Y -------> 0.995 

For Calibration Factor Y, the ratio of the reading of the calibralion meter to the dry gas meter, 

acceptable tolerance of individual values frorn the average is +-0.02. 

--------- ORIFICE --------- 

CALIBRATION FACTOR 

dH@ 

Value Variation 

(in H20) (in H20) 

1.425 0.0013 

1.422 -0.001 

1.424 0.000 

1.424 <------- Ave rag e d H@ 

For Orifice Calibration Factor dH@, the orifice differential press ein inches of H20 that equates to 0.75 cfm of air 

at 68 F and 29 `92_inchUTW)lg, accepta Io,tolerance ndi 'dual vaiues from the average is +-0.2. 

~~ ..i' 

SIGNED: % i ~~i •'/,1~~ 

.. ~. Date: 

,. 

T\:) 

Im 

T\D 
Temperature Meter Calibrations 

Meter Box #: 10 

Date: 04/14/06 

Calibrated By: RT 

Emtech 42312 

Degrees F Calibrator Probe Stack Oven Exit Auxillary 

Point 1 32 32 31 32 31 31 

Point 2 212 212 211 212 211 211 

Point 3 752 752 751 751 751 751 

Emtech 42312 

Degrees R Calibrator Probe Stack Oven Exit Auxillary 

Point 1 492 492 491 492 491 491 

Point 2 672 672 671 672 671 671 

Point 3 1212 1212 1211 1'211 1211 1211 

Percent Difference 

Probe Stack Oven Exit Auxillary 

Point 1 0 0.203252 0 0.203252 0.203252 

Point 2 0 0.14881 0 0.14881 0.14881 

Point 3 0 0.082508 0.082508 0.082508 0.082508 

2. ~ 3 
Armstrong Environmental Inc. CONVERSION FAC'TORS 

EPA Melhad 5 

522 Series Meter Box Celibratlon 1 mm H 0.13330 kPa fl 

Pre-Tesl Orifice Malhod 1 cm = 0.39370 inch 

English Meter Box Unils, English K' Factor 1 mm - 0.03937 Inch 

1 cu ft = 28.32 liters 

leter Box x 11 Date: ----------- ------- -----•-> 03/15l06 

eriat #: 40312 Barometric Pressttre: ----------> 29.90 (in. Hg) 

Theoretical Critical Vacrrum:---> 14.10 (In. Hg) 

tlliltt 

APORTAN For valid lesl resulls, ttie Actual Vacuuni should be 1 to 2 in. Hg greater than the Theoretical Crilical Vacuum shovin above. 

Ai'ORTAN The Critical Orifice Coefficienl. IC, niusl be entered in English uniis, (ft)^3'(deg R)"0.5/((in.Hg)'(min)). 

I!!t+!! 

--- ---- ------ --- DRY GAS METER READINGS ---- ------------ -CRITICAL ORIFtCE READINGS- 

-- Average Temperatures -- 

Volunie Voltniie Volunie Initiat Temps. Final Temps. Orifiee K' Orifice Actua! -- Ambienl Tomperature -- DGM DGM Ainbionl 

dH Time htilial Final Total Inlet Oullot Inlet Oullet Serial# Coefficient Vacuum Initia) Final Average Outlet Overall Temp 

n H20) (niiil) (cu Il) (cu fl) (cu ft) (deg F) (deg F) (deg F) (deg F) (ntrmber) (see above) (in Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (dog R) 

0.25 10.00 694.400 697.623 3.223 67.0 65.0 67.0 66.0 40 0.242 23.5 67.0 67.0 67.0 525.5 526.3 527.0 

0.52 6.00 699.700 702.473 2.773 67.0 66.0 67.0 67.0 48 0.344 21.5 67.0 68.0 67.5 526.5 526.8 527.5 

0.96 5.00 703.000 706.105 3.105 67.0 67.0 68.0 67.0 55 0.464 20.0 68.0 68.0 68.0 527.0 527.3 528.0 

1.60 7.00 706.800 712.360 5.560 68.0 67.0 69.0 67.0 63 0.593 18.0 68.0 68.0 68.0 527.0 527.8 528.0 

3.10 7.00 713.100 720.754 7.654 69.0 67.0 72.0 68.0 73 0.824 16.0 68.0 68.0 68.0 527.5 529.0 528.0 

................................................. RESULTS ................................................... 

- DRY GAS METER --- --------- ORtFICE --------- -- DRY GAS METER -- --------- ORIFICE 

JLUME VOLUME 

ORRECT CORRECTED 

Vm(std) Vin(sld) 

(ctr ft) (liters) 

3.232 0.1 

2.780 0.1 

3.113 0.1 

5.579 0.2 

7.690 0.3 

VOLUME VOLUME VOLUME 

CORRECT CORRECT NOMINAL 

Vcr(std) Vcr(sld) Vcr 

(cu fl) (liters) (cu ft) 

3.156 0.1 3.153 

2.689 0.1 2.690 

3.018 0.1 3.021 

5.405 0.2 5.411 

7.504 03 7.512 

CALIBRATION FACTOR 

Y 

Value Varialion 

(number) (number) 

0.976 0.005 

0.967 -0.004 

0.969 -0.002 

0.969 -0.003 

0.976 0.004 

CALIBRATION FACTOR 

dHO 

Value Variation 

(in H20) (in H20) 

1.418 -0.0602 

1.459 -0.019 

1.484 0.006 

1.511 0.033 

1.518 0.040 

Average Y -------> 0.972 1.478 <------- Average dH@ 

Ae: For Calibration Factor Y, the ratio of the reading of the calibration molar to Ihe dry gas moter, 

acceptable toterance of individual values from lhe average is +-0.02. 

For Orifice Calibration Factor dH@, lfie orifice differential pressure in inches of H20 that equates to 0.75 cfm of air 

al 68 F and 29.92 inches of Hg, acceptablelerance ' divid lues (rom the average is +-0.2. 

~'"'- 

SIGNED: `1•~'`

~

^.•rf ..y`'~^ r-~✓ Dale: 

J' 

: V 

r I 

t^~ 
Temperature Meter Ca(ibrations 

Meter Box #: 11 

Date: 03115106 

Calibrated By: RT 

Emtech 42312 

Degrees F Calibrator Probe Stack Oven Exit Auxillary 

Point 1 32 31 31 32 32 32 

Point 2 212 212 213 213 212 212 

Point 3 752 753 753 753 753 753 

Emtech 42312 

Degrees R Calibrator Probe Stack Oven Exit Auxillary 

Point 1 492 491 491 492 492 492 

Point 2 672 672 673 673 672 672 

Point 3 1212 1213 1213 1213 1213 1213 

Percent Difference 

Probe Stack Oven Exit Auxillary 

Point 1 0.203252 0.203252 0 0 0 

Point 2 0 0.148588 0.148588 0 0 

Point 3 0.08244 0.08244 0.08244 0.08244 0.08244 

265 
ORIFICE 

CALIBRATION FACTOR 

dH@ 

Value Variation 

(in H20) (in H20) 

1.495 0.0023 

1.493 -0.000 

1.491 -0.002 

1.493 <------- Average dH@ 

Arinstrong Environmenta) Inc. CONVERSION FACTORS 

EPA Method 5 

APEX INSTRUMENTS 

511 Series Meter Box Calibration 1 mm Hg : 0.13330 kPa 

Post-Test Orifice Method 1 cm = 0.39370 inch 

English Meter Box Units, English IC Factor 1 mm = 0.03937 inch 

1 cu ft = 28.32 liters 

;ter E3ox 1 11 Date: ----------------------- -> 04/14/06 

-rial #: 73 Barometric Pressure: ----------> 29.75 (in. Hg) 

Tlieoretical Critical Vacuum:---> 14.03 (in. Hg) 

1!liil 

PORTAP For vaiid test resuits, the Actual Vacuum should be 1 to 2 in. Hg greater than the Theoretical Critical Vacuum sliown above. 

PORTAP The Critical Orifice Coefficient, iC, must be entered in Englislt units, (ft)"3"(deg R)"0.5/((in.Hg)`(min)). 

!!ii!! 

---------------- DRY GAS METER READINGS ---------------- -CRITICAL ORIFICE READINGSTheoretical Critical Vacuum:---> 14.03 (in. Hg) 

Volurne Volume Volume Initial Temps. Final Temps. Orifice iC Orifice Actual -- Ambient Temperature -- DGM DGM Anibient 

(1H Time Initial Final Total Inlet Outlet Inlet Outlet Serial# Coefficient Vacuum Initial Final Average Ou#let Overall Ternp 

i H20) (min) (cu ft) (cu ft) (cu ft) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (deg R) 

0.96 7.00 325.500 329.853 4.353 73.0 72.0 74.0 73.0 55 0.464 20.0 75.0 75.0 75.0 532.5 533.0 535.0 

0.96 7.00 330.200 334.571 4.371 74.0 73.0 75.0 74.0 55 0.464 20.0 75.0 75.0 75.0 533.5 534.0 535.0 

0.96 7.00 335.200 339.572 4.372 75.0 74.0 75.0 74.0 55 0.464 20.0 75.0 75.0 75.0 534.0 534.5 535.0 

.A4:krrRlififr ~ .ffA.AfA. A.flAfiftfrrrr..Afr1AAAAAA RESULTS ArA..IfIfAA11fAAA AffAfAAA+AfArrfArflf+iirrlfA AAAAAA 

• DRY GAS METER --- --------- ORIFICE --------- -- DRY GAS METER -- 

JLUME VOLUME VOLUME VOLUME VOLUME CALIBRATION FACTOR 

ORRECT CORRECTED CORRECT CORRECT NOMINAL Y 

Vm(std) Vm(std) Vcr(std) Vcr(std) Vcr Value Variatlon 

(cu ft) (liters) (cu ft) (liters) (cu ft) (number) (number) 

4.296 0.2 4.177 0.2 4.258 0.972 0.001 

4.306 0.2 4.177 0.2 4.258 0.970 -0.001 

4.303 0.2 4.177 0.2 4.258 0.971 -0.000 

Average Y -------> 0.971 

ote: For Calibration Factor Y, the ratio of the reading of the calibration meter to the dry gas meter, 

acceptabie tolerance of itidividual values from the average is +-0.02. 

For Orifice Calibration Factor dH@, the orifice differential pressure in inches of H20 that equates to 0.75 cfm of air 

at 68 F and 29.92 inches of, Hg, accepta I tolerance of I Wdual valUes from the average is +-0.2. 

SIGNED ~ . ~- ~---~' A- ~/ Date: aw C

G 

.> 

~ 

~ 

~ 
Temperature Meter Calibrations 

Meter Box #: 11 

Date: 04/14/06 

Calibrated By: RT 

Emtech 42312 

Degrees F Calibrator Probe Stack Oven Exit Auxillary 

Point 1 32 31 31 32 32 32 

Point 2 212 212 213 213 213 212 

Point 3 752 753 753 754 753 753 

Emtech 42312 

Degrees R Calibrator Probe . Stack Oven Exit Auxillary 

Point 1 492 491 491 492 492 492 

Point 2 672 672 673 673 673 672 

Point 3 1212 1213 1213 1214 1213 1213 

Percent Difference 

Probe Stack Oven Exit Auxillary 

Point 1 0.203252 0.203252 0 0 0 

Point 2 0 0.148588 0.148588 0.148588 0 

Point 3 0.08244 0.08244 0.164745 0.08244 0.08244 

267 
I"` i i ~ ~ "41 ~ ~f= C T 

~ . PI i ~ i IU3r 1iti..F~~C~ i+?;, J ~.T ~. ~ _", 

y 

-- -- --- ----- - - %+G ; 

S?mDz;. 

.~^•~~ ~~ ~ ,ll :~I ,. v, 

~ ur P'•::::~p~ : 

`" , C• )J1 . . 

~-~~----, ~ • i 

• ~~ 'd'`

;_K--

._~ 

/' .f lr •!f { II: i.a[ ~i I• • # A 

'st:Slus: 4 Clclrt -KaNr Gr 'Nr

SNtu IE : ~ !• .:: ~ Jt t,^,c[ :r. 1O'::C CNn• tx.rt 

LLJ I , 

~ I

LJ ~, 

Dt:t[( IrOt:sTrrG ttvtt r:3 ~ 710N v~ 

f~i ~ T~~wICtN: T. TntN :iICK C[:t[[ IN01(LTIa: t[v(l ~~ IN: 1• 

pS1T)ON ipt ptT[tnlwlM: p 

Z~ ---- ~ // -- • l, ` ~.~--'1• J—.—.L__.z.... 

I 

`Y 

,~ ~~ 

.2 

lC3 

:[C11tt tIt2ICaTtN: t:f'L( 

Oft'1:~ i(.f ~ y'~ ;rw ~~ rNG 

/ I 

/~~ 

,. . 

D[c•[t .)Nn , tat)NG t(ttt cslrroN 

IGt .lL'( wINING r! 1n ~ Lf 

Commen ts : 

./ 1 e ~, el ? ' 

n.ibS jL C)iis? 

damaged? 

I < w, < I 

1 ~ -100 < r, 2 < -10° ~ 

7

~ j — J ° < 51 C :5 0 

7 I -5 0 < 62 < 

~ Y ~ I 

S A 

~ . ZJ 

Of 

, I 1.05 J t < P a < 1. 5 D -- ~ 

1.051t<Pb<1.5 

~ I 

J~ 

? ~ 

3/1611 .< p ~ .~ 3/8 11 

r ~ 

I 

A tan Y < 0.125" 

r C3 A tan 3< 0. 03125" 

, 

pa - P b — 0•.053 

, 

, 

h' i i.ot tube/probe numaer ~ mee ~ 5 Or AY.C ~ eCS al l S ~ °C1 i iCat +OnS 

cri -Leria and/or appl icabl e design +=eatures* and i- hereby assigne a 

o; tot tube cal i brat.ion f actor o ' 0.84. ' l 

S ~ g nz ;.u, 

/. c ~ :~•' 

0a t? 

'Se'z' 40 ,.:.R 60, ~~ 01. =C, ~ f0. IO ~ t i''teiil° ~' G. VeY1'~f : ~1e LRiflitllJlT~ 

? 1 ~1z:1 ' ~ :b°_Ck 0' :h° aP.d t}1e 'iriflU^ 2I= i1c t 

Separc:i°n bet.:een the pito: ano :he na__:e as Snown at 

:he 

2R8 
~ i F u i TU3= il;;? - C; -,"~;~ :~~ i r~. S~,~ L i 

1 J L t•. f 

~ 

1, 

] ~ . _ 

Pcst SGmml.e 

`~• ~ ~ ~1

~r %~.'~ ~~ 

 :~ 

~.f M•MNpI [ I i 

f'•i ~Ii I ~j[ , . 

r=-'✓~-~ , , 

~ ~ 3/i in. 

r— ~•~ ~•T— ~` ~ } ~' ~ 

'b 1 

:rl•;V rtc[SSU2[ 9P[N{N: r•LN( Of 

SwxLL R :vlN :Ii. pC AIOr[ ihE W.da[ IxtRt Llul(, I 

Y ~ ~ 

t 

' 1 i 

0(. .C: INp/Ct.'tN; i;YC: 01t710r 

/'J ,OCT«r1&;IN: Y. TNEN :=LCLYATIN: DC-RC! IYOICETIN: lfYCl 

OSITION fDl D(T[Rn1rlN4 g 

Z

I _. --. \ . ~,~ . —. •~; . _G—^--~-.!• ~: -'ze. 

~ y 

~ I 

I 

I a* 

:SGR:S iM ~ ICiTIN: L:YCL 

POSISI:r W. 3(T( .rlrC 

•~s' 

•~- 

~ - 

.~ •. 

^_ 

•— 

.—. .—.>` 

OIG~C~ ,IMOICaTlK LI':Il OSITION 

~ pl: •}[Ti ~ wININ(, ~ , •w/ j! 

Commenis: 

1 e v e l? 

r ✓ (1 j !'✓ o ~- S truc t i 1'nS 7 i !i `✓ ! 

1 1 . • 

da;Tlaged? 

3 -10 0 < a, < ~ 10" 7i 

-100 < a 2 < T100 3 

y _,.^ O < d i <+ C o L. 

~ _ 8 0 < a2 < +6 0 ~ 

3 Y 2- 

1 3 f 

a 1 ~ 33 7, 

~ 1'-r- 1.05Dt< ~ a<1.5Dt' ~~~~ 

1.05D1<P <1.5Dt ~ b 

3/16 1~ .< ,< 3/8 ,1 

b,> Z~ ( 

, Z-5f 

3 f~ 

~ 

'7 r

~ 

.~.:.~~ 

Dt 

A tan Y< 0.125" 

f 0 /0 A tan 9< 0-03125" 

P a= P b_ 0. 0 6 3" /,7 

r'i t(? t. tllbe/probe numver !Tleets or eXceeis al 1 speci i ic? tionS 

criteria and/or appl icabl e design f eatures* an,d.-•i -s ;nareby assiqnp,~a 

pitot tube cal ibration factor o -170.84. 

S iS n a t u r~: 

,See 40 C=A 00, Vci. Q,tic. 100, hiA=hod 2. 1'erijv ,hs mini:rur-i 

2:1'1.r.h 5° ~

:r2Ck rJi :fl° :Fixl"0=0Uol° $nCi i1e ITIirlr:Jr" ?/4 inCh 

seaera:ion bezaFen the pitot t',:be and the noz.le ts shown a: 

-

ile :0v G. .'1S ~2~ 0 

D~~a 6~ 

2F9 
"- 1 

_ _ ~---Li. 

~ <<JT iU3} iNS?tC T I ~!t~~ af~.i ~. S~l~~ i 

O— JC~.~i0 1 e ?os Samol e 

. , 

~" ~ (• )rc ,a. ~ 

 •, ~ :.: rc. : '~ ✓'i -- 

~%. : .r,_v •: I i ~ _ . 

~!_.. bL 

i • L ~ , ( 'D y 

~!' :~.a:' st!:S:li: D!!Nlw: :iw! Cn ?: ~?~ •'.:li ~ 

5..+.L: i .~ !♦ ... pR .1DY: Tw; NO:.LC 

~ 

~ 

, 

OCGRiC IMOICI ~ , NG l:L'El ~ :51710N 

103 D(T! ~nl~'~N~ T. 'N( ► CtLCVIjT , M: 2. 0l.R!! INDICRTIwG L!Y(L 

OLITION OR O(T(RnIwINC 8 

-- ~ 

i~ 

_ ~ = i °2 lL'31 

`CGRCC INDIC3T,wGLlvC1 

7St.10 ~ :G~ :L•f• ~ I>t ~ wG 

..`;~/i 

., 

:C.".•CS ~ NOIC ~TING lC ~'(l GS ~ 710• 

f:i .TC'Lr ~ .Mtw. ~~ •nf ~~ 

Commen ts : 

~ I 

ievei? ~~ ._ 1 

J D s i,'" i1 C 

, 

r' L/ damaged? 

~ -1 o ° < w I < 11 0° ~ I 

~ -140 0 < a2 < :100 ~ 

~ 1 

— J °< $1 < - 5) ° ~ 

~ -5 0 < 5 2 < ;5 0 ! l 

Y 

• ~?~ A 

r ~ _ 

.05 DL < P a< 1 . 5 D L 

J 

1.050-<Pb<1.5 Dt ~ 

, 

3/1611 .< 0t `< 3/8 , I 

A tan y < 0.125" . ~/-~ ~ . 

A t. a n 9< 0.03125" ~ 

I pa = pb ± 0. 063" 

,• 

? i to ~ tubC/probe nul-~E~ er Q ~ m?e t:s or exceeds al l speci ; ications 

cr ~iteria and/or appl icab'1 e design ~ eatures* and 's here ~y assigne-e a 

pi ~ot ~ ube cal i bra ;.i on f ac ~ or ot 0.84. f'~~~~ 

S i C ii C (.1~ 

'see 4C, . " : 65, :•01 . =2 , No. . -.0, we _nod 2. 'rer•. fy _ne mini:nvm 

2 : L"l• = ~ L t`L I O -. L !~ ~ ~• ? n ~ s, . ~z i ~ ' , 7_ t,: ~-:o ~ oua cr,c . ~ _ ;, i inu-. 1 + ~ n_h. 

$e78'diiDn bet :Ee.^. L!',e p':o: .tl5e 2nd :h4 ^:,i: l e. t> S"ow.^, b: 

.^p :n ^.i i t};1 ~ aan.G 

2'7-0 
aaamm 

'Y.; sA;SSW( Oo:Mlxt r;sti( Of TMt 1T0: 7JlE 

SwAli {: fY1* pt aIOr( iNf Iq:2LE txtx• ;aHr. 

Y~ ~► 1 

_ t ~I i —► 

! 

D(LRt( IrpKiTlttC G::'EG MITIDr 

9~ 0(T(rr ~ 1r: :sttLls:lw: Z. 

~—•-- ~ ~,•-- '-

~~ 

i! 

t 

« 

1~ 

I 

D(GRtt IYDItITIM: l[wtl 

OSITIOr !Ot D(TEr~ IMIMG 0 

.~-•- -~ 

^` Y 

~--~• ~ 

;~~' 

ao • ~ s 

~-~ %2* ~ 

^s6att IwDlaTtrt ttVtt 

~ OSISIJM TLT. ~ ('(.•IINIM7 

. t •~- /i 

-i ° 1 • 1, •-- 

, 

..___ — - -•~r. ,• 

Dt+ ~ tt.IMO1t ~T1~~ GtTEt •ciltla ~ 

ct a(T:... ~ .1.: 3, .~~ G. 

Comments: 

PT i Ji ;'J8- :NSP6CT1 ON Dr. iA 3HO- -c 

~ r=_iz?.M,tJle PosL -, :. r'? nla 

~ ~ o ~• ~ ~' ~~. ~ r /~ , r . / ~ 

. ~ • .__...~ 

. ~ _ 

.,,(...;-..• ~ . 

D 

`...~ •G • jii i1. j ' r 1 

i ° v° 1? ~ ~ 

! 1 I S ~re• :ri. K.7: i1( \~/~_J~ ~ , ' ! ^ ~ ' ~ ; I 

I ! • .. .. , . , 1 . 

I damaged? 

.~+. -10° < r ~. < - 10° I I 

I 

} -10 0 < w2 < T10 0 ~ 

► 7, -5 0 < 3 2 < =5 0 j 

-~ ° < ~ 2 < .i.50 

~ Y 

8 

A 

1.05Dt<Pa<1.5Dt,t

1 .OS Dt < ?b < 1 .6 D t 

3/ 1611 .< D L'< 3/8 " 

A tan Y< 0.126 1 t 

A tan 8< 0.03125" 

P a = Pb _ 0.063" 

~ ~ ~ 

J0 

~r 

..~~' 

~ 

, . ~ ' 

.--- .. 

•3 S 

~ C~ 

~ a ~~ rneets cr e ~,ceeds al i speci ~ icata~ ns Pi ~ ot tuoe/probe n ~~ma..r 

criteria and/or appl icabi e design f eatures* and i hereby assiqned ' 

pi tot tube cal i b ration fac tor of 0.84. 

. f s • M 1 ~ 

, o n a t u r - '-) 

iJ : 

-See 40 C=% 50, 7o~i. 42, tic. 100, NetncC 2. Veri'y tne ririanu2:nt` se.JGL k 0-' t^e Z`p.*'occ;tpie Znd .h: mirinum 3/4 inch 

SeQ21'BLiGI1 tJELueen :ne j:l:^vt :Ube dnd. tf1°_ ncZZle c5 5!'10wn Er 

:he to: a; Lh,s Dage. 

271 
'I J8L ; .- ~'-'• 

~ ~!?l e 

_ . ~ '.. 1 ^ f ~ j,-_ ___ ^J 1 ~ . -- ~ • t- 

; v; .•~~ ...r r '~ . 

-- - ---~~ •:~i.i 

1eVp1? 

112 

~ ~ C 

~ ~ i '~•} 1% ! 

-:--~— ~ c~ s~ u c o s ~ 1i t ~ 

i" ~ 1 i ~ • J 

~~~' ~i ~ , ~='; ~t t ~ •, -i— ~ ~ i ~ damaoed? ----I ., ~ J •rr l i' i"r ~ ' ~ i •; - ~ ~ D i ~ o 

1!: Irrl.:' 1at• t53 ~a, OrCMIM: r ta+, Or ?>: r • r ~~~: 'JII I I ~ ~ — 1 O O < v 1 < ` ~ f'1 V 

Sr.,clt Sf tetc .:: rJt iSOvt 2nI ~O::LI txTl ~ e I.utt. 

-10 0 < a2 < +100 

, 1 I 

« « 

-5 0 < 6, < .0 ~

. 

~--~ - 6 0 < 62 <. 5 0 ~ 

OE:r,tt ,+OJCCTJNC tt:'£t .CSJTIOr I r ( 

r0i OLif si~~N: 1. ~ NLM :slCt.3'IlG :. O(;RCt g jl 

_ 

y f( I ~'. __ti r,•_ - — .i a ~ I 

A 

~ ~~ 

~ 1.05D ~-<P

a 

 <1.5Dt l~ f ir 

~ 1 rI ., ! f♦ L

~J 

` ,;! ~~ 1. 05 D< P ~ < 1. S D ~. ~ ~ .T y. f` ~, t o ~ 

_ r~ .1 0~ "n~ ~. , /-" 

. . 

.~ ~ -i•\f 3/ 16t1 .< D 4

- ~< 3/8" 

0 ...~~' ~' C•"\ri 1 

afWr.t IIt2 It ~TJn. ttv[l L 

osl 'IOV iCR a?rr ~~ Mltl3 r~•~~ 

p, awi ar r• ~ I A t a n y < 0 125 

~ . 0 

~ an 8 < 0 . 0312 -

~

It 

_ ^ 

Pa = P' _ 0. 063" 

otcr.tc • ~ NO,carJNc u•:It restf ~ o+ {~ ~ 

rCr 7t'.:.w ~ „r: :, .w ~ S, • / 

Comments: 

:'; tot tube/probe number 0 mee `s ol- px.ceecs al l speci -F ica tions 

cri -LLeria and/or appl icab e design reatures* anri is hereby assig A ed a 

p i ~ot tubE cal i braiion rac ~or o'~ 0. 8~ . 

S i gra ~ur~,~? 

` ~~-! ! %~S ``~ !

l 1 ~~•~ ~' 

Jc._ 

'S°2 -J ...'!! 53, vGI. 2, mG. t g.o, Mc:h0d 2. 1J 2t'iT}' :hp ttitliTUm 

_ ir_.. se. ~ ecS ~ ` :h ~ :r°^foc^.up1e at:d the rinimu: ~ 3r= inch 

SE7Z•'B:IOn vECwE°^ :hE p'. L0t ~ U'Jf: Ln ~ =he TOZ: ie LS S ~'IOwn ~J t 

:h ~;:o; o` :i:is pa9°• 

272 
;'~ . t ; ., t . ._ -. ~ . _ ~ ::. Y;....: ~ .r.:~;:r::•.'.'~ r .. ; ~~. t`_ ° _ t . .i , r _ . I 

I .~.~.rt . .. ♦ 17. ~

l.IS ... fl. ..J. » .=f.. ~°. . . r. . ..... .. s~ _. .. _' .UL.. a.Z'~~GL~~'.~~ali~~.rl• ~d'L.IlJJ1J, ~.r~ -' `... _..l': _! _ _ ~ 1 . . . .. :/t. t- . .. t.... ._ -..... . . _. -_- .~~ 

~( ~ ~'` ~- I~ : I;~• ~~'} 17 ;~ 

./• E-5 ~ 

...~ 

~~~: .~ ~~~ ? i ~~ ~ ~ ! ~ ~ ! ~ ~ ~ ~,~ i ~ ~ ~ k' .~,:7 ~--~— ; ,~ ~ ~.~-~rs.~; j v :-.~ 

t ~ ~~ ~ ~ ~~ ~ ► ~ ,._G~ r f ~~ I ~{; ~ ~~ ~ ~ r ~-J . ~ ~- ~ ti ~,J ~, : ~ ~ j~= ► ~=~ ~ ~r ~~~ ; ~_ 

f',• ;~ ,~ i. I ~• ~: ~, 5 I •~'~ I '~ ~ . G I ~ ~' ~' ~~' f ~ I~ ~ ~ i ~.~j~ ,~. 

1. 

r7 t 7s L 2_5 .7 I , 1`— 

-7~V' rt ~ _ 1 7 , eo 

JI L ~ C~ i ~ ~ c ~ ~ ! ~ ~ i I• C7 I `~ :N !~ I i ~ ~ f3 K • ~'j ( — ~ ~ 1 aT/ 1r r;r ~• ~' ~ ff •, 1 •• ~ j• ~ i 

7 _~s" I 9 ~ . 7 ~ I 06 '' ' ,~ ••I .~ ~ ~ 

' • •R- -j _ • f ~l '~ 2 / !~'~ ~ j . 

f r s-f+ ~. ~ )

i ~ ~ , '~ , ! ~ lJ j. n ~ ✓ ~v. ~ ! ~ J ! `i ~t~h I i ~ C # I ./f1. ~ '1 

o z 1- I -~ I .'f' •~ I• ~ 

J'•~ if ~! `1 ! ,I ' 1 V ! i' l= ~~ I r ~ I ~!~ C~ . ~ .~. i S~ ~ ~! `~•~. 

aLt 

f 'S : O Jr ~a `1 i ~ : r~• ! = ! ~ ~ ~ I `~ , ~ G' I ri ~ ~ ^ ' I ► r, ~~, C~1 '

0 7 0 '2 7 1 7 v I „^' F 17 ;Tr'''~s'~ . t ~•.~ 

~ t ~ ~~ i ~ ~ ' I ~ ~ • ~ 1 ~ i `~ ~ i z~ . ~ ~ Z~ ~.s . • % r 

o o o ~ o • l c~ i?~ , 1 I I`, ~~,,c ro/ f"' 

1 r rD o,S i 1' 7D 2•G o '-- • r' ~~~~~:~~;E ;~ 

- • I / 

~

7 

z 

.siu' %ny eq _ bll 

. .( ~ ~ I. ~ z, ! 7 W 1 

i• 

6 '77 e4,hriKs` ~.c 

~~-Ic7 I ~ ~ ~~=~ f ?~ ~`~~~ I 

~ %~:~ f^: ~ ! ! ~ 1 r. I fr l .) i .-: ~ ! _} r. i , j ~ i ! ! ;~. i ~... ~ ~~ t' "~ `- • ~ 

C)~ 

I I 2q I`9, 1 a.. 

Ci i ! J i ' ) O yy~ ~ ; (n : ` J :' 't-) ~

°i 

i 21 7 / I ? ~` ~ 5 I l~ ~' I ~~ ~ ~'s Z - . ..~ i ., 

 it : o~I~~t 2 I~ 

~ .~ ~ {, .,, ~ I ~ ~' ~;~ I ~ 'G ~> 7~ l~ - ! ; ~, ;--- I -- i •; :. ~.~..• , , 4,,-- _ . 

~ 

~ ![ f1 . ~ o . f ~ ~ I • I ~ ' ~ ~ I z' .9: i ,-=--- ! ~ t , ~ ~~ ~ 

'72— ! .Z~7 ~ ~%'~ ~ ~ ~ ~ ! ~ un , 0~ 

r~ r.;T~ > e3 1'' ~~~~_~_~Il~ 

273 
NOZZLE- I NSPECTION AhD hiEASURLEMENT DATA SHLEET 

Da~~J—~~..~~ ~. Oa ~ E Jatilnl?d ~ ~,. ~/10 i~!^ ~ Zie }tiiJTi'~~ Y'0."~.~ 10 ~ 

J " 

Presample Inspection 

I hereby certt;i fy tna'L the above referenced nozzl e appears to be 

round, shara-edged, ► ree of ni cks and d?nts nd i s- judged acc ptabl e 

for us? at this time. ~. 

. ~ 

Last Previ ously Measured 2 ` _ 

~lozzle Area , Ecc SL3 , t 'sigra ~ ure 

Da:.e l-leasured ~ l~- Q • 

Postsampl e Measurernent 

Measure three di ameters as shown; measurement i s 

i n i nches; record be1 ovi; perf orrn cal cul ati ons. # 

l..3a e7 2.. 3ic 3.:3lb 

Average DiamntAr , 30 1 -7• 

Area - ` rr D2r = Ld~ G o S a ..7jfr 2 

l: i r. r 

Thi s area s ~nall-~ u.sed i n dfata red;;ct i on. 

sj%na ~vr~ 

~ a L= 

date 

\ 

3 \ 

'i 

; 

rl 

~ 

1 

r• ~ 

• - . . ~ . I:..Xi.^.; ~uul 81 i~'r:r ~ !° di T7ei'El1c2 QEt`.'Weei'1 1cr . 

~os: d1 ~ iil~ Le;' c'ild Si;~a~~~ : s ~ 

;;!•J'tj incnes 

274 
NOZZLE I NSPECTION -!'~ ND hiEASUREMENT DATA SHEET 

?n? ~'~( i —~~~,~ ri ~' P,aT.2 Saf.l:) I 2d q 1( (~.~ t~nz z i ,. ar 

l ~ 

?resample Inspection 

I hereby certify that the above ref erenced nozzl e appears to be 

round, shara-edged, free of nicks and d-onts and is' judged acce table 

for use at this time. 

, 

Last previously Measured ,, r 

Nozzle area 6,.oC,03q( ft2 sigr,ature 

Date Nfeasured ~ 10 (~.(~ date 

Pos tsampl e Measurement 

Measure tnree di a meters as sho.,rn; measurement i s 

i n i nches; record bel ow; perform cal cul at i ons. ` 

1. .151 2 .s, Z~`Z 3. • 0,)C3 

;.veraoe Di amnter 

p,re3 D2 

4 y 144 _ 

Thi s area snal-L be—used i n dat a raduct i on. 

s nat 1i~~ -- 

d a L-: 

• 2S Z 

d . 000 2 ~ 

~ 

1 

h;ar;^um a; iow hle ciifere ce beL~~reen i ~ rces: ci ~~,e;.er =_ ~n ~~a11?Jt 

di a,,e ter_ i s 0.004 i ncnes 
NOZZLE INSPECTION AND MEASUREMENT DATA SHEET 

, C 

~~mnin ~~ P•'ama ~~~ ~~-~...1 `u. ._Date Samnled~~ 13 G ~ _ . Nozzle Number 

~ J 

Presample Inspection 

I hereby certi fy that the above referenced nozzl e appears to be . 

round, sharp-edg*ed, free of nicks and dents and is- judged acceptable 

for use at this time. 

'. 

Last Previously Measured 

Nozzle Area ~o©a33 ~ ft

2 

signatur 

Date Measured date 

Postsample Measurement 

Meas ure tliree di ameters as shown; measurernent i s 

i n i nchzs; record bei ovr; perforrn cal cul ations. ' 

1. . Z9 9 2. i 2~ { l 3. p 2q 7 

Average D i ameter 

A,rea = n D2 ~ 2 

4y '12~

ft 

fhis ar ~ all use in data reduction. 

sicn ~

_ 

? ~ 

datF 

\ 

3 ~ 

, ~ z 

. . _•- . ~ 

* MaxiMUm allov/aale diffea•ence betweeri largest diameier and smallest 

diareter,is 0.004 inches 
NOZZLc I ~~ SPr CTI ON ~ti,ND liLASUREMEN T DATA SH ~~ T 

rnr'1;'..'?~~ ~'`~ a (~',e 

, j ~ D

"_

(,

i

'~~~ j ~. '~ c;:. ~ S3li1 ~. 1?d `C ~ 2. f~tt~ ~~ 7? ~ a ~;sJj-'!~ n, ► ~ (Z. ~r ~_ 

Presample Inspz-ction 

I hereby certify that the above ref erenced nozzl e appears to be 

round, snarp-edged, fr-oe oz nicks and de' and is- judged a ceptable 

for use at thi's time. v~-- 

, 

Last Previ ously Measured 

Nozzl e krea ~ cco ~ 3 ~ f t 2 s i araturz 

Da te Measured date 

Postsample MeasuremenL 

Maasure three di a meters as shown; rne.asurAment i s 

i n i nches; r?cord bel ovr; perform cal cul ations. 4- 

i. -3t-),- *2. ► 3ll 3. 313 

Ave rage D i amn ~ er 3 j Z 

Area = ,r D2 

4 

~ . 144 r ©0f 

2 

T ni s area s a) Usad%In data redUci ±on. 

\ 

; 

:, 

~,nat v 

da 

~ 

al,or;GcJe d" ~ 'ere:;ce J ~ eLWe e(1 1 a CCe$ :d'1 mc- e° Y c 1d $m? 1 l c5 t 

L i d:Ti: ;.e T i S J. 0::i4 1 7cne5 

277 
NOZ ZL c i NSP = CT I ON AND Mt--ASUPcMrr_- NT DA T A SHcF T 

r On ~~ ~•,~ ~'?:~a~ 

• J 

r pt, -T-~f~ , Ck LJa ~a ~C~?~ ar ~ rl 7 i.. yilJ;~~ D 1^ ~ ~. z 

PresamQle Inspection 

I hereby certify tha ~. the above referenced nozzl e appears to be . 

round, sharp-edged, frea of nicks and deny -and i s judged accep ~ abl e 

for use a-t thi s time. 

Last Previ ously Measurzd 

iNozzl e Area •. 6663 f t 2 s i ona t. 

Date weasured g/ I .~ • ~ date ~/f3 

Postsampl e Measurernent 

Mea.sure three di ame ters as 'shown; me.zsuremen't i s 

i ni nches; record bel ovr; •perf orm cal cul ai i ons. t 

1. y 24 g 2. - 2_q°1 3. , 24 Ct 

Ave rage D i ame ter 

0,000,3 37 -

v2 

1 

\ 

~ 

na t,ur'~ 

, f 

..- 

.Gl.r 

, y 

~ -- 

tweeri t ~ rees: diameter and sma?last 

is 0.004 incnes 

Area D2 

41' ; ~ . 

Tris area sh 

, zq ~ `7 

_ 

sed ✓/i data r?duc.ion. 

278 

! • t;~ •' xz 'ttii .._ . 

C 

~~. ~ ~~` ~~ I: ~+~ ~: ~~ ti: •~ c. . . 

.. R i 

~s•— ask-. .. i ne Ga= PrvfEGsicrca{s'• 

16S0 Enterprise Parkway 

Twinsburg, Ohio 44087 

21 S-648-4000 

`;fE ~

c 

 v~ .-

~.~.~ a: 

s r ~ .

:~.~ 

; ~[• ~ r• ~+' i.Y r. °t .~. .. Sti ^. r,. 1. E: ~ r ~ . /. ~. ~ } : n 

Customer: MATHESON TRI-GAS - DALLAS 

Cylinder Number: SX-32759 

Cvlinder pressure: 2000 

Last Analysis date: 5/3/2005 

Expiration Date: 5/3/08 

Component : Methane 

Certified Conc: 40.8 PPM ± 1% rREL 

Protocol: Reference # t_ot # 

G 1 329498 109-66-43191 

DO:N.OT*USE -.T-H.IS:CYLINDE-R• WHEN THE•,. = 

f'RES

~

SURE FALLS:BEL01N 1.5.0 PSIG 

~ 

REPLICATE RESPONSES 

Date: 5/3/2005 Date: 

40.8 PPM 

40.8 PPM 

40.7 PPM 

BALANCE GAS: Air 

REFERENCE STANDARDS _ 

Component: Methane 

SRM #: SRM-2750 

Cylinder #: SX-20007 , ~ 

. • 

Concentration: 48.80 pprrt 

CERTIFICATION INSTRUMENTS 

- . r 

Component: Methane ; 

Make/Model: Varian 3800 GC 

Serial Number: LR-92489 `- 

Measurement Principle: TC, FID - 

Last Ca(ibration: 4/26/2005 

Nates: 

This certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous 

Calibration Standards September 1997, using procedure G1 and/or G2. 

~ nai ~~ st ~n /,~~,~ ~ . 

..,.~;c ' 

Date 51412005 

279 
~► ~ l~~~~-~~~ !<~ ~ ~ : -;~~ ;• - 

TRi ~ GAS 

ask. . .The Gzs Profess!iona(sT" 

1650 Enterprise Parkway 

Twinsburg, Ohio 44087 

215-648-4000 

~C~S. F"!'~'~' l~'^S ~` !: n. F i•~ •w.~ ~ :~t I.r •~t~4 /~.f^P:€ fsi.

w ~. : .- rs F !~ ~lp-~ ~ 

t' ! °'` •, . f ~. ~ ~ F ~ . . i ~{^~. c v: L. :.+~ .~ 

~ ustomer: MA i HESON TRI-GAS - DALLAS 

;vlinder Nurnber: SX-34951 

;y!inder pressure: 2000 

_ast Analysis date: 5/3/2005 

cxpiration Date: 5/3I08 

Component : Methane 

Certified Cona: 61.7 PPM ± i % REL 

Protocol: Reference # Lot # 

G 1 329498 109-56-43192 

DO.'NOT USE THIS CYLINDE.R WHEN-THE 

PRESSURE ;F~1LLS; BELOW 1.50 PSIG. . 

, • 

REPLICATE RESPONSES 

Date: 5/3/2005 Date: 

61.7 PPM 

61.8 PPM 

61.5 PPM 

3ALANCE GAS: Air = - 

REFERENCE STANDARDS 

Component: Methane 

• ; -. - , SRM #: SRM-2750 - 

Cylinder n: SX-20007 

, 

Concentration: 48.80 ppm 

LERTIFICATION INSTRUMENTS - 

Component: Methane _ 

Make/Model: Varian 3800 -GC - 

Serial Number: LR-92489 

Measurement Principle: TC, FID ` 

Last Calibration: 4/26/2005 : 

Notes: 

This certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous 

Calibration Standards September 1997, using procedure G1 andlor G2. 

:na!yst ; ~ ~ c ~ `~~ ,!' Date 51412005 

WE 
Specialty Ga.~ Products 

3106 Pasadena Frceway 

Pasadena, Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

Date: 3/2212005 

Customer. Trigas Project: 14445 

Description: Methane in Air - EPA Protocol Exp. Date: 3/22/2008 

Cylinder No: SX31814 Cylinder Pressure: 1950psig 

Requested Certified 

Component Concentration Concentration Accuracy 

Methane 20 ppm 19.9 ppm 1% 

Air, Balance 

Reference Standard 

Description Exairation date Cylinder Number Concentration 

SRM 6/1/2008 FF23319 49.22 ppm Methane 

Instrumentation 

Qescription Model # Date Last Clibrated PrinciQie 

Horiba Process Analyzer FIA-510 3121/2005 FIA 

Anaylsis Results: Z= zero gas, S= standard gas, X= sample gas 

First Triad - Methane 

Z1= 1.60 S1= 492.30 X1= 199.70 

S2= 492.70 Z2= -0.10 X2= 198.60 

Z3= -0.70 X3= 199.50 S3= 490.40 

Curve: Y=-0.09706+0.099752*X 

Average = 19.87pm 

~ 

. f i 

Analyst: /. 

THIS STANDARD 1S NIST TRACEABLE. 1T WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 
AP 3106 Pasadena Freeway 

Pasadena, Texas 77503 

(713) 534-82 1 7 Fax(713) 534-8133 

Specialty Gas Praducts 

Date: 6127/2005 

Customer: Matheson - Trigas 

Description: NO in N2 - EPA Protocol 

Cylinder No: EB0001164 

Com Aonent 

Nitric Oxide 

Nitrogen, Balance 

Reference Standard 

Description 

GMIS 

Instrumentation 

Average = 50.3ppm 

Curve: Y = 0.33645 + 0.099857'"X 

Project: 16015 

Exp. Date: 6/27/2007 

Cylinder Pressure: 1900psig 

Certified 

Concentration 

50.4 ppm 

NOx: 51 ppm 

Cylinder. Number 

N D22557 

Accuracy 

1% 

Concentration 

99.8 PPM no 

Principle 

CHEMI 

X1= 502.80 

X2= 502.40 

S3= 994.20 

Average = 50.53ppm 

Requested 

Concentration 

50 ppm 

Expiration date 

11/22/2006 

Description Model # Date Last Clibrated 

Horiba Process Analyzer CLA-510-NO 6/16/2005 

Anaylsis Results: Z= zero gas, S= standard gas, X= sample gas 

First Triad - NO Second Triad - NO 

Z1= -1.20 S1= 994.80 X1= 498.30 Z1= -1.10 S1= 998.50 

S2= 994.10 Z2= -1.30 • X2= 498.40 S2= 998.20 Z2= -0.70 

73= -1.10 X3= 499.80 S3= 997.40 Z3= -0.80 X3= 500.80 

----~_ 

Analyst: ~ ...r 

/ 

THIS STANDARD IS NIST TRACEABL E. IT V1IAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

~ 82 
~ 3106 Pasadena Freeway 

Pasadena, Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

Specralty Gas Products 

Date: 6127I2005 

Castorner: Matheson - Trigas Project: 16014 

Description: NO in N2 - EPA Protocol Exp. Date: 6127l2007 

Cylinder No: EB0001156 Cylinder Pressure: 1900psig 

Requested Certified 

Component Concentration Concentration Accuracy 

Nitric Oxide 25 ppm 25.0 ppm 1% 

Nitrogen, Balance 

NOx: 25.5 ppm 

Reference Standard 

Description Expiration date Cylinder Number Concentration 

GMIS 11/22I2006 ND22557 99.8 PPM no 

Instrumentation 

Description Model # Date Last C(ibrated Principle 

Horiba Process Analyzer CLA-510-NO 6/16/2005 CHEMI 

Anaylsis Results: Z= zero gas, S= standard gas, X= sarnple gas 

First Triad - NO Second Triad - NO 

Z1= -1.20 S1= 994.80 X1= 244.50 Z1= -1.10 S1= 998.50 X1= 247.10 

S2= 994.10 Z2= -1.30 X2= 244.80 S2= 998.20 Z2= -0.70 X2= 247.00 

Z3= -1.10 X3= 246.10 S3= 997.40 Z3= -0.80 X3= 246.40 S3= 994.20 

Average = 24.90ppm Average = 25.00ppm 

Curve: Y = 0.33645 + 0.099857"`X 

; 

Analy s,t/ 

THIS STAN R~ISNIST TRACEABLE. IT WAS CERTiFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PS1G 

283 
Specialty Products

3106 Pasadena Freeway 

Pasadena,Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

Date: 6/27/2005 

Customer: Trigas Project: 16017 

Description: CO in N2 - EPA Protocol Exp. Date: 6/27/2008 

Cytinder No: EB0000701 Cylinder Pressure: 1900psig 

Requested Certified 

Comaonent Concentration Concentration Accuracy 

Carbon Monoxide 50. ppm 49.9 ppm 1% 

Nitrogen, Balance 

Reference Standard 

Description Expiration date Cylinder Number Concentration 

NTRM 5/29/2006 SX19190 994.2 ppm CO 

Instrumentation 

Descriation Model # Date Last Clibrated Principle 

Horiba Process Analyzer VIA-510-CO 6/10/2005 NDIR 

Anaylsis Results: Z= zero gas, S= standard gas, X= sampie gas 

First Triad - CO Second Triad - CO 

Z1= -0.90 S1= 204.90 X1= 198.70 Z1= -0.40 S1= 513.30 X1= 497.10 

S2= 204.80 Z2= -0.80 X2= 198.60 S2= 513.20 Z2= -0.40 X2= 497.10 

Z3= -0.80 X3= 198.60 S3= 204.90 Z3= -0.40 X3= 496.90 S3= 513.20 

Y=0.28607+0.250309*X Y=0.031031 +0.100163'X 

Average = 49.94ppm Average = 49.82ppm 

~~ ~•~ 

;naiyst: 

~ . 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

n0 NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

284 
Specialty Ga.~ Pr®d~.,~ ct.~ 

3106 Pasadsna Freeway 

Pasadena, Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

Date: 6/27/2005 

Customer: Trigas Project: 16018 

Description: CO in N2 - EPA Protocoi Exp. Date: 6l27l2008 

Cyiinder No: EB0000761 Cylinder Pressure: 1900psig 

Requested Certified 

Component Concentration Concentration Accuracv 

Carbon Monoxide 100 ppm 99.1 ppm 1% 

Nitrogen, Balance 

Reference Standard 

Description Expiration date Cylinder Number Concentration 

NTRM 5129l2006 SX19190 994.2 ppm CO 

Instrumentation 

Description Model # Date Last Ciibrated Principle 

Horiba Process Analyzer VIA-510-CO 6/10/2005 NDIR 

Anaylsis Results: Z= zero gas, S= standard gas, X= sample gas 

First Triad - CO Second Triad - CO 

Z1= -0.90 S1= 204.90 X1= 396.60 Z1= -0.40 S1= 513.30 X1= 985.70 

S2= 204.80 Z2= -0.80 X2= 396.60 S2= 513.20 Z2= -0.40 X2= 985.40 

Z3= -0.80 X3= 396.50 S3= 204.90 Z3= -0.40 X3= 985.20 S3= 513.20 

Y=0.28607+0.250309'X Y=0.031031 +0.100163'X 

Average = 99.45ppm Average = 98.74ppm 

Analyst: ---~ ~ 

~ 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES, 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 

285 
Specialty Gas ,~'rod~ct.~ 

3106 Pasadena Freeway 

Pasadena, Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

Date: 8/1612004 

Customer. Matheson - Trigas Project: 10548 

Description: CO, 02 in N2 - EPA Protocol Exp. Date: 8/162007 

Cylinder No: CC187154 Cylinder Pressure: 1900psig 

Requested Certified 

Component Concentration Concentration Accuracy 

Carbon Monoxide 200ppm 200ppm 1% 

Nitrogen, Balance 

Reference Standard 

Description Expiration date Cylinder Number Concentration 

GMIS 4/6/2006 CC177636 994.2 ppm CO 

Instrumentation 

Description Model # Date Last Ciibrated Principle 

Horiba Process Analyzer VIA-510-CO 8/6/2004 NDIR 

Anaylsis Results: Z= zero gas, S= standard gas, X= sample gas 

First Triad - CO Second Triad - CO 

Z1= -0.3 S1= 993.5 X1= 199.9 Z1= -0.4 S1= 995.5 X1= 200.6 

S2= 993.20 Z2= -0.30 X2= 200.00 S2= 995.80 Z2= -0.30 X2= 200.60 

Z3= -0.30 X3= 199.90 S3= 993.00 Z3= -0.30 X3= 200.60 S3= 9995.60 

Curve: Y=-0.0-893=1.001139X 

Average =199.6ppm Average = 199.8ppm 

Analyst: 

Ling Wen 

THIS STANDARD IS NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG 286 
Project: 10549 

Exp. Date: 8/162007 

Cylinder Pressure: 1900psig 

Certified 

Concentration 

494ppm 

Accuracy 

1% 

Cyiinder Number Concentration 

CC177636 994.2 ppm CO 

Spect'alty Gas P 

3106 Pasadena Freeway 

Pasadena,Texas 77503 

(713) 534-8217 Fax(713) 534-8133 

Date: 8/1612004 

Customer: Matheson - Trigas 

Description: CO 302 in N2 - EPA Protocol 

Cylinder No: CC176507 

Requested 

Comaonent Concentration 

Carbon Monoxide 500ppm 

Nitrogen, i3alance 

Reference Standard 

Description Expiration date 

GMIS 416l2006 

instrumentation 

Description Model # 

Horiba Process Analyzer VIA-510-CO 

Anayisis Results: Z= zero gas, S= standard gas, X= sampfe gas 

First_Triad - CO 

Z1= -0.3 S1= 993.5 X1= 494.2 

S2= 993.20 Z2= -0.30 X2= 494.00 

Z3= -0.30 X3= 493.90 S3= 993.00 

Curve: Y=-0.6893+1.001139X 

Average =494.1 ppm 

Date Last Ciibrated Principle 

8/6/2004 NDIR 

Second Triad - CO 

Z1= -0.4 S1= 995.5 X 1= 495.4 

S2= 995.80 Z2= -0.30 X2= 495.60 

Z3= -0.30 X3= 495.50 S3= 995.60 

Average = 494.4ppm 

Analyst :_ 

Ling r 

THIS STANDARD 1S NIST TRACEABLE. IT WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THtS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PS1G 

287 
. ~,: ~ ~ ► r- ~ = 3't46 Pasadena Freeway : ~E,~~':--~ ~ ~ 0 ~°~: 

 71

Pasadena TX 77503 

~~ TRE-GAS`' ~ ""-•' 3-534-8217 

~ slc. e-s ?ro'ess}on: is Certificate of Analysis - EPA Protocol Mixtures 

Customer: MTG-CALI CROSSING Protocol: Reference # Lot# 

Cylinder Number: CC165296 G1 21555 

Cylinder Pressure: 1900 PSIG DO NOT USE THIS CYLINDER WHEN THE PRESSURE 

Last Analysis Date: 3/20/2006 FALLS BELOW 150 PSIG 

Expiration Date: 3120/2008 

REPLICATE RESPONSES 

Component: Sulfur Dioxide Date: 3/10/2006 Date: 3/20/2006 

250.30 250.20 

Mean Conc: 250 ppm +/- 1% rel 250.00 250.00 

250.10 250.00 

BALANCE GAS: Nitrogen 

REFERENCE STANDARDS: 

Component: Sulfur Dioxide 

Reference Standard: GMIS 

Cylinder #: ND22558 

Concentration: 502.1 ppm 

Exp. Date: 4/7/2007 

CERTIFICATION INSTRUMENTS 

Component: Sulfur Dioxide 

Make/Model: Horiba VIA-510 

Serial Number: 42321590023 

Measurement Principle: NDIR 

Last Calibration: 2l22/2006 

Notes: 

This Certification was performed according to EPA Traceability Protocol for Assay & Ceitification of Gaseous 

Calibration Standards September 1997, using procedure G1 and/or G2. 

_ .. 

Analyst: ~ Date: 

Manufactured By Specialty Gas Products, a Matheson Tri-Gas Company, Pasadena, Texas. 

.~ 
~ R o. = r-- r•~ fi 3'~ 06 Pasader,a F reeway 

AVAL : ~r c ~~^~lT f--X ~ Z~ Pasadena, TX 77503 

~ R i ~ G ~"

~ 

~ S t? 713-534-8217 

-ascc ... 1'h-a Gas Certificate of Analysis - EPA Protocol M'sxtures 

Customer: MTG-Cali Crossing Protocol: Reference # Lot# 

Cylinder Number: CC176977 G1 20832 

Cyiinder Przssure: 1900 PSIG DO NOT USE THIS CYLINDER V'JHEN THE PRESSURE 

Last Anaiysis Date: 2113I2005 FALLS. BELOW 1 SO PSIG . 

Expiration Date: 2113l2008 

REPLICATE RESPONSES 

Component: Sulfur Dioxide Date: 2/6I2006 Date: 2/13/2006 

49.44 50.22 

Mean Conc: 49.8 ppm +/- 1% rel 49.65 49.91 

49.78 49.88 

BALANCE GAS: Nitrogen 

REFERENCE STANDARDS: 

Component: Sulfur Dioxide 

Reference Standard: GMIS 

Cylinder #: CC177775 

Concentration: 101.3 pprn 

Exp. Date: 9/412006 

CERTIFICATION INSTRUMENTS 

Component: Sulfur Dioxide 

MakelModel: Horiba VIA-510 

Serial Number: 42321590023 

Measurement Principie: NDIR 

Last Calibration: 2/712006 

Notes: 

This Certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous 

Cafibration Standards September 1997, using procedure G1 andlor G2. 

Anafyst: ~: ----? Date: 

~ 

Manufactured By Specialty Gas Products, a Matheson Tri-Gas Company, Pasadena, Texas. 

2R9 
3106 Pasadena Freeway 

i v E !•-~ ,i 

~. ~ t s~~ ` Pasadena, TX 77503 

~ R F ` G f~-~ ~3 713-534-821 7 

---5i:. ..Ths Cas ^r•;if¢gsictnnEs Cercificate of Analysis - EPA Protoco! Mixtures 

Customer: 

Cylinder Number: 

Cyiinder Pressure: 

Last Anaiysis Date: 

Expiration Date: 

MTG-Cali Crossing 

CC177031 

1900 PSIG 

2/13/2006 

211312008 

Protocol: Reference # Lot# 

G 1 20829 

DO NOT USE THIS CYLINDER WHEN THE PRESSURE 

FALLS BELOW 150 PSIG 

Component: Sulfur Dioxide 

Mean Conc: 100 ppm +!- 1% rel 

BALANCE GAS: Nitrogen 

REFERENCE STANDARDS: 

Component: Sulfur Dioxide 

REPLICATE RESPONSES 

Date: 2/6/2006 Date: 2/13J2006 

100.60 100.30 

100.30 100.10 

100.30 100.10 

Reference Standard: GMIS 

Cyli nder #: N D22558 

Concentration: 502.1 ppm 

Exp. Date: 9/4/2006 

CERTIFICATION INSTRUMENTS 

Component: Sulfur Dioxide 

Make/Model: Horiba VIA-510 

Serial Number: 42321590023 

Measurement Principle: NDIR 

Last Calibration: 1/16/2006 

Notes: 

This Certification was performed according to EPA Traceability Protocol for Assay & Certification of Gaseous 

Calibration Standards September 1997, using procedure G1 andlor G2. 

~ ` 

. Analyst: r ~ ~~ 2~~/. " Date: ~i`fff ~ -~ \i 

~ 

Manufacturzd By Specialty Gas Products, a Matheson Tri-Gas Company, Pasadena, Texas. 

290 
~ .A

~ppendi~ H 
Sheetl 

Summary ofS- ~2 lnterfernc Samiing e p , 

.. . ._.. . . . r.. _.. 

~ Run # _: Method 6 ;Mehtod 6G % Difference 

1; 56.41 ' 55:6 i 1.4359161 

. _ 

, .. . . _.. _ .._ _.... .... _._ . ...._ ~~ . 

~ 2. 59.02 60.1 -1.82989 

3 ; 59.34 ; 59.2; - 0.235929 ! 

Page 1 ~ q ~ 
EMISSiON TEST SUMMARY 

PLANT : Da11ile. Mtjskogee, UK. 

DATE : I3-Apr•06 

PLACE : T rim Kiln Exhaust. S02 lnier-ference Tra1n 

RUN# : i 

TEST DURATION (MINUTES) : 20 LIQUiD COLLECTED (mis) : 0 

NOZZLE DIAMETER (INCH.) : 0 Sulfur Dioxide Weight, mg : 1.97 

METER COEFFICIENT (Y) : 0.9726 0 

PITOT COEFF1CiENT (Cp) : 0 STATIC PRESSURE (in. H20) : 0 

GAS METER VOL.(Cu.Ft.) : 0.4907 PERCENT CO2 : 0 

BAROMETRIC PRESSURE : 29.7 PERCEN T 02 : 0 

PERCENT CO : 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 0 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 0 STACK WIDTH(inchs) : 

NOZZLE AREA (#eet): 0 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 0 

FL01NS 

SAMPLED VOLUME (STD. CU .FT.): 0.4635 

Sulfur Dioxide, ppm : 56.4073 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

J. 0 0.03 79.5 79.5 

2 0 79.5 79.5 

3 0 79.5 79.5 

4 0 79.5 79.5 

5 0 79.5 79.5 

#D(V/O! 0.0000 0.0300 79.5000 79.5000 79.5000 

2Q~ ~ M 
EMtSSfON TEST SUMMARY 

PLANT : Dalti!e. Musl',o ;ee. OK 

DATE : 13-Apr•06 

PLACE : Trim Kiln Exh@ust, S02 IntPrference Train 

RUN# : 2 

TEST DURATION (MINUTES) : 20 LIQUID COLLEC T ED (mis) : 0 

NOZZLE DIAMETER (INCH.) : 0 Sulfur Dioxide Weight, mg : 2.4n 

METER COEFFICIENT (Y) : 0.9726 0 

PITOT CO'EFFICIENT (Cp) : 0 STATIC PRESSURE (in. H20) : 0 

GAS METER VOL.(Cu.Ft.) : 0.5849 PERCENT CO2 : 0 

BAROMETRIC PRESSURE . 29.7 PERCENT 02 : 0 

PERCENT CO : 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 0 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 0 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 0 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 0.5532, 

Sulfur Dioxide, ppm : 59.0166 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 0 0.03 78.8 78.8 

2 0 78.8 78.8 

3 0 78.8 78.8 

4 0 78.8 78.8 

5 0 78.8 78.8 

#D1V/0! 0.0000 0.0300 78..8000 78.8000 78.8000 

2Q3 
EMISSION TEST SUMMARY 

PLANT : DaItilp, Muskogee, !DK 

DATE : 13-Apr-06 

PLACE : Trim Kiln Exheust. S02 fnterference Train 

RUN# : 3 

TEST DURATION (MINUTES) : 20 LIQUID COLLECTED (mis) : 

NOZZLE DIAMETER (INCH.) : 0 Sulfur Dioxide Weight, mg : 

METER COEFFICIENT (Y) : 0.9726 

PITOT COEFFICIENT (Cp) : 0 STATIC PRESSURE (in. H20) : 

GAS METER VOL.(Cu.Ft.) : 0.5828 PERCENT CO2 : 

BAROMETRIC PRESSURE : 29.7 PERCENT 02 : 

PERCENT CO : 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 0 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 0 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0 STACK AREA (Sq.Ft.) : 

ENTER THE STACK AREA SHOWN ABOVE: 0 

FLOWS 

0 

2.46 

0 

0 

0 

0 

0 

C 

SAMPLED VOLUME (STD. CU .FT.): 

Sulfur Dioxide, ppm : 

P01 NTS STACK T. DELTA P SQUAR D. P DELTA H 

deg F 

1 

2 

3 

4 

5 

#DIV/0! 

0.5501 

59.3480 

METER T. 

I N LET 

79.88 

79.88 

79.88 

79.88 

79.88 

~;~:~: ~ ~, 

~ 

N 

• 

• 

,, 

C~lloZlZsZol 

0.03 

0.0300 

METER T. 

OUTLET 

79.88 

79.88 

79.88 

79.88 

79.88 

79.8800 79.8800 

2P4 
Sulfur Dioxide Barium-Thorin Analysis 

Plant: Dal•Italia, Muskogee, OK 

Location: Trim Kiln 

Date: 13•Apr•06 

Standardization Ba (CIO2)4 

Titration (mis) Avg. Titration (mls) 

9.766667 

Blank Titration (mis) Avg. Blank (mis) 

V 0.1 

Volume of Standard Sulfuric Acid (mis) 

Normality of Standard Sulfuric Acid 

Normality: 0.010239 

Aliquot Average 

Run # Location Volume Dilution Volume Titration Titration 

(m I S) (MIS) (MIS) (m I S) (MIS) 

1 Imp 1-2 1.3 

2 Imp 1.2 1.6 

. . . 

3 Im 

. . . . . . . . . 

p 1-2 1.6 

Run # Location Total Grams Total Mg 

1 Imp 1 & 2 S02 0.001966 1.97 

2 Imp I & 2 S02 0.002457 2.46 

3 Imp I & 2 S02 0.002457 2.46 

295 
r} s ~ S 

I f q 70, 

~ ; 5 ~ ~' ~ ~~ t 75' 2, 

~ n ~ • ~; ~ ~ ~ S~,j ~- ~' 

10 07 t ~ 3 

~ ` S ~ L ~.~-._.__. ~ ~.~.~_~~ ---~__.__.. ~ .._..._..___.__.._.__, 

1 ~ ~~ ~ ~'~~~ ~ ~ ~ ~ ~ ~ l ~ 

~ ( ~~ o,~" ~ 6 t z ~ ~ ~. ~ 

~~f~ ~~7~ o ~~ E 8 

~ i lS~ ~'~~zt . ~ z7 

110 2~za ~ ~f ~-~ 

~ ~:~~ ~~ ,r~l 

W ~ 

5~ (o 

C9 c f 

s ~ z~ 

996 
., 

'Summary o€ S02 lnteri ernc¢ Cneck 

........__....._. . _._._. _.__..._.__..._.____.___.__ __._... ._ _._......._ ~ .---•---.... ~ ........._:_._._... ---_..._ _._ 

_.._ _ . _ _ . ___,. 

Pta 

_ 

nz : valiie, Dai; as

..

, i 

Locafi on : ~ : Pi an i4 

--- 

_Scru bber ---- 

: 

`Monitor:'1Nes'tern ~Research 72'! -hi __... -- .._...._-.._...., ..__._....__._.____. _......_.._.._..`.._.__.~_.... ---, , --- 

.....__ 

3 -- • ._...._ 

RunM

' 

i l 2 

_Monii:or_S02 , ppm_ i 0 ~ .. _._..........._.- ~ 0i --.. .__..._.. _...._...._.__.. ~.~._._.... l 0 

Method 6 S02 E 0 _M_oaiiied -- --- -__ ry0 ; 0 

% DiITerence ^i 0P i ~0l ~~ 0 

J0 2 

Paae i ~ 
Sulfur TA)ioxide Bariurril-Thiorin. A' naly-;-is 

Plant: D2!tile. DaJlas, T' 

Location: Piant #4 Scrubbell 

Date: 20-Jul-03 

S;andardizabon 'Da (C-102)4 

Ti'Lra'tion (mls) Ava. Titra ion (mls) 

10.5 

Blank Titration (mis) Avg. Blank (mls) 

0.1 

Volume of Standard Sulfuric Acid (mls) 

Normality of Silandard Sulful-ic Acid 

Normality: 0.00.01524 

Aliquot' Average 

R u n = Location Volume Dilution Volume Titration Titr2tion 

(MIS) (MIS) (MIS) (MIS) (MIS) 

imo -1-2 

2 imp 2.2 M 0.1 

3 1 mp .2 0.1 

Run = Location Tok-al Grams Total Mg 

I Imp 2 & 3 S02 0 0.00 

2 1 mp 2 & 3 S02 0 0.00 

3 1 r-,):) 2 &- 3 S02 0 0.00 

303 
ZJ 

iL ---- L 

i ' 

~ 

~- - 

. . ^ 

. -- 

~~y~ ~ . 

^x\/ .~ 
cM1SS 0N TF.STSUIVfM.-A.RY 

PLr.N i : Ja;:ile Daiscs. : ; 

JA i E: 9-Ju,-03 

RLACE 

R 1Jh\= . 1 

TES i DURA T ION (MINU T tS) : 50 LiQUID COLLEC T ED (mis) : 0 

NOZZLE D1AME T ER (iNC!-I.) : 0 S02 Samp1e Weighl, mg: 0 

tVIE T ER COErEICIEN T(Y) : 0.944 0 

?I T OT COEF r=lCl; N T(Ca) : 0 S T A T IC ?RESSURE (in. ;'20) : 0 

GAS NfE T ER VOL.(Cu.ri.) : 1.818 PE?CErV T CO2 . 0 

3AROiViE T RIC PP,ESSURE : 29.5 PERCEN i 02 : 0 

PERCENT CO : 0 

FLOWS 

Sk(diPLED VOLUME (S T D. CU.F i.): 1.5737 

S02, ppm: 0.0000 

POIN i S STACK T. DcL T A P SQUA ~ D.P DEL T A H METEP. T. M ~TER T. 

oeg r 1NLET OUTL ET 

1 0 o.00 72 72 

2 0 72 72 

3 0 72 72 

" 0 73 73 

5 0 73 73 

5 0 73 73 

7 0 73 73 

8 0 74 74 

9 0 75 75 

?0 0 75 75 

11 0 75 75 

1-2 0 76 76 

~D(VIO! 0.0000 0.0000 73.5833 73.5833 73.5833 

~~ 5 
EMISSION TEST SUMMARY 

,-- ~ LA,1~ ~ : Dai ~ iia, Da,l_,s, T Y. 

DATE : '9•JuI•03 

PLACE : ?lani a Scrubber 

RUh'= : 2 

T ES T DURA T ION (MiINU T ES) : 50 LIQUID COLLEC T ED (mis) : 0 

NOZZL E DIAMETER (INCH.) : 0 S02 Sample Wz-ight, mg: 0 

METER COEF F ICIENT (Y) : 0.944 0 

PITOT COEFFICIENT (Cp) : 0 STATiC PRESSURE (in. H20) : 0 

GAS ME T EP, VOL.(Cu.Ft.) : 1.843 PERCENT CO2 : 0 

3AROME T RIC PR; SSUP.E : 29.5 PERCEN T 02 : 0 

PtRCENT CO : 0 

FLOWS 

SAMPLEU VOL UME (S T D. CU.FT.): 1.6694 

S02, ppm: 0.0000 

POINTS S T ACK T. DEL T A P SQUAR D.r' DEL TA y METE.R T. METER T. 

deg F 1NLET OUTLET 

? 0 0.00 82 82 

2 0 81 az 

3 0 81 a? 

~ 0 82 82 

3 0 82 82 

6 0 82 82 

7 0 82 82 

8 0 83 83 

9 0 83 83 

~ 0 0 83 83 

1? 0 83 83 

12 0 8A 84 

=D1V/0! 0.0000 0.0000 82.3333 82.3333 82.3333 

P6 
EMISSlON TEST 5UMMAP•.Y 

PL AN T: Daltile, Dailas, T); 

DA T L : 9•Ju! •03 

PLACE : ?lari< < S.- rubber 

TES T DUP,ATION (IAlNls T ES) : 

NOZZLE DIAME T tR (INCH.) : 

MET ER COtF F iCl EN T(Y) : 

PI ~ 0 T COEF=lC(EN T(Cp) : 

GAS ME T cR VOL.(Cu.Ft.) : 

BAROME T RIC PRESSUP.E : 

FLOWS 

60 LIQUI D COLLEC T ED (mls) : 

0 S02 Samqle INeight, mg: 

0.94^- 

0 S T ATIC PRESSURE (in. H20) : 

1.857 PLRCEN T CO2 : 

29.5 PERCEN T 02 : 

PERCENT CO : 

0 

0 

0 

J 

0 

0 

0 

SAMPLED VOL UML (ST.D: CU.F T.): 1.68 - 8 1

S02, ppm: 0.0000 

POINTS STACK T. DEL T A P SQUAR D.P DLLTA H ME TECR T. METER T. 

deo F INL ET OU T LE T 

1 0 0.09 86 86 

2 0 83 83 

3 0 82 82 

4 3 82 82 

5 0 82 82 

6 0 82 82 

7 0 82 82 

8 fl 82 82 

9 0 82 82 

10 0 82 82 

11 0 82 82 

i? 0 82 82 

nDlV Ot 0.0000 0.0000 82.41n7 82.4167 82.4167 

P7