# Liquid Waste Feed Samp le Composite Data Sheet
Projec t N ame Veolia

- Sauge t, I L Date 

### 10 

## ta-311) Project N umbe r 

### 40942525.20.{)2 C onditi on N o. 1 Facility Un i t4 Run No 

## l! Stream Name Uqu l d Waste Feed (LWF) Start T ime 

## 1a.U Composite Sample 10 V$4

- lWF

- 1 18 -COM P )& Stop Tim e 

# li&& Operator

Sampl e Number Ti m e Volume/Mass Sample Numb er Time Volume/Mass 1 

# ta..&s 

# a.**eo"'~..,** 21 2 

### •a.!i} 22 3 tl() 

# 8 23 

### 4 

## tla) 2 4 

## s I 'Ut) 25 6 

# ibH 26 7 

## I 'tO& 27 8 

### I 

## 'leU 28 9

### l'tl~ 2 9 1 0**J~t•n** 

### 30 11 

### I 

# "o t, 3 1 12

### l.U**~)** 32 1 3 

## l$'1&**~** 

## 1- 33 14 

### ···'IJ-:1 34 15 35 16 36 1 7 37 1 8 38 19 3 9 20 F inal Volume**~,(,OO...,L,** Comments: C o ll ect appropr i ate l y -sized and equa l all q uots and transfer Imme diat e l y Into a 4 -l ite r composite ja r
. Collect a sepa rate 

### 500 m l bottle of sam ple at ea c h S<Jmpllng ti me t o be r e t ai ned i n arc hives.



# ePA**~Ht V~olil:\**  

# s 't •**~** 

## f-**-~(,<..** 

## SQto'\11'\(ld

## ~IOI'fl**~~ ~l~ll"'** 

.5/)$

.. ()5 $ub.Somp/e C4Nif!X'SI Ie ReWskm**I)IJr~ :**  June 2012 Rsvf«•'UI ' Juno2013 E-377 

## VESO I3800

# URS

''"' " ' I 

# I Vld • " 

# ' ' """ " w'udt 

# s ·tr,
.... )•"'1'/, )' DAILY .RECORD OF EVENTS



## o?co 

# 411

# ~~r··'**~.~t(** 

# f.• s:k. 

## W"'-lf.tr. c.IJ 1 

## r ·"" >, 

# h,l ]u'f. 

# nr s**'"''** Ofl'[.'f, j 

## clrcf, .,..; Por((i -to 

# M•.:I, ,M ..c(

# c:f,ly. j¥.)';. 

# J'C'··," fu Jn./ 

# 7**""'f''·J."'~~v.-/ <r** **·** /f./:1 

# Tr.•trf· rf •1

# /o.f,<f**~J"** 

# <A" 

# I J ""w'f '? of 

## ;,fpl•or. IIHS**~!j'~ ~vrt**  

### i..A. I 

## ''to

## f/-"'f~ (b;, )Jt. 

## [.(f , .c/ 

# r-4**,.,..pie~** 

## aT /OJ) 

## fp

.. (/ le-tA\ 

### f;. 

## sfr-,-$

. l:l.':>'J**ll~91\** 

### ll.u.l\ 

## a.A,**'-ollec~ ~ptlte** **~Q"'piP~** (...l

### ~H%J 

## Pb.L-1 1 

# :n**H~.0.'1a.O** 

### 11>'> 1.1!-\ 

### J<...IJ. hrull 

## tl\'h, Lo\\P.d &a"'plf' 

## (v ,.,p3.A**ll~** 

## lu15'**l'~b** tal\icJ ..,f"IL

### ;:>01·'~/qs**~4t'IN) m~\4\~**  hQ,I\

### f"'~ <Ji·rhol' 

## C-1 

## \H'J OI Vb.**l--lb~ H~-~Wb**  

## l'ri'f 1-\\'_jqls lroli\ Qhd; 1

### t.oll~-d-**::.o,,.,,l~ (.c~** **p). j**  

## (n.J.. UApaP.-Il.Jp) Q 

## I J$"0') 

### l'i1b**i..<:lllet~** 

# c..p 1 \ f•

### r.'l-**n~~.,** 

## t..l '.**~** 

## ·**'fCl~** fl 

## b L · 

### :,?>() HI)

. O.d.{,(, 

### tS'1.1

## [)~ q
.. 

# d**I'~ trt~Jn**  

# tfld 5 ,

## ~o**ii Q<..\-** **~;qn~plr** C..t''"l'3C.

## q~**IIJ3f R.I.lt>~!l** **C..utl\pl~lt'.** I 'J'f7 

## Lol\td**~I"** 

### b..t 

### ;,Qh •JIIr ; 'or 

## Cl rth•vt U 

## ' .1-\ -\ UFi 

## fib ,l-toa

. \-\().**~d.~'\** 

# U\ !H -l•lL

# t:~~l"!' ,fhtk

. r\(l (f t(•l

# ~U~td**~rJ .~.ll'r\<1**  (11-C\J "'

# -·~l"i**~~~., .**  

# 1/l I



# I 

# t.**~GJ~Q** I
E · 378 

## VES01380l

## Fi e l d B a lan ce C alibrati o n {; heck Project Name

__**...;V:.;C,;O:;:Iia;.: S:::;a~u~ge~t~,**  

### I:,;:L

__ Project Number

__**.: 4:::094::.::.;2:;5;25~.2;::0.0=2::...-**  F;cllltv

___**_; U:::n~lt:.:** **:_** _ _ _ Ba l nnta 1 0

___ _ 

## S .;.

'i .:.;

¥.=....

_

Calibration In i tials 

# c.t:il**C~clcedby** 

### Date 

### IOR'tfl)

## -~ 

# --- -- j 

# - We!cbt" 

# ---- "' 

# --· "'**~~~~** 

# w . 20**~Q** . ... 

### . 50**~.a** c.-CIMd<of 

### 100 

# -.:n . ; tolonc.o uslnc stud t nt WelJ l!ts 

### 200**~0() ::,**  SWdent Wol gk t S

e t 10: 500 

## 4"

. 1**\41,,~** 

### 1000 

## 1000

- 7



# u....a,_oo_.,...,.
__ lOJ.

,.,.
_ _ _ towdlj>-lftiU<-l=t.-

...**IOOOudSO<lg>n~- fw** **•- --**  

# ' ""

-- ... -·-·s0.$11.

....... _'"_

....**~** Percent OUfetenee • 

### balanoe 

### rudlng- actual 

### mass x 100 

### actual 

### mass

ct>S · 08B I f'/o/d l•faltCf (•l•brollon

,., f.M !!01'·010**R~llisio" !Jot~**  MGI"Cit 10/1 Rllol,.wd: Uy 1011

E-379 

## VE S013802

# < m (I) 0 w 00 0 

### w 

## Waste Samp le Logbo o k 

# Veo lia -Sauget , IL

- Unit 4 CPT Project Numb e r 40942510.20 P 11 g e 11 o f29



### Samp l e 10 Code Strea m F ract i on Cond Run Dat e 

# run. TW GW C om ments

### ~~~~~B~~~~~~~1~~----**~~~~ --** **--~ --** **--~~ ~~~** **~~ 4-** **~03~,~~~~-7~5~ 1.** **~' -+----** **~-- --** **~**



## ivs'-as-tv.-GraO e u Solids 

### .wM 1

### ~

..,., .,. 12A.Q1b 7 BoAk Solds 

### Alcltie 1**~**

### ivs'-BS·1~-GI1lb 8 

### B1tk**~** 

### AttNv e 1 2A h

...

### ,,...1~2A USolds

### ~ 1 2B

### , 

### IU(



## VS4- 8 S- 1 2B-Gtsb 4 Bull< Solds A reN vo 

## 1 26 11l )

tvs4-BS·12B-Gr8b a BIAk**~** 

### Archive 

### 1 2B 

## 'at 1 128-Gtab 7 Bu1< Solids ArriWe 

### 1 2B**'iO~**


### lvS4-8S- 128-<l<tlb 

### 9 Bulk Solids 

### Arc!M 

### 1 28 

## I'\ 1(. 

# i**lv~B~12B-Gllll11** 8\Ak Solds 

### AttiWe 1 2B 

# I 1 SOf.**~-** • o<- 

### 128-GraO 1 2 U Sold:s 

### Attti<e I 2B 

### I**'f~ \**  128-G<ID 13 &A Sold:s 

### ArrHre 1 2B

- 

## I 

# ot

# < m Vl 0



# ..... 00

### ~ 

## Samp l e 10 

## Code**I'JS4-CS.1~1** jvS4-CS-12A-Gnb 1 12A-Gnb2 jvS4-<:S-12A-Gnb 3 jvS4-CS-12A.Qab**~** 

### jvS4-CS-12A-Qab 5**~** 

### ... '**~** 

### 12A-Grab 6 lvS4-CS-12M>r.lb 7 jvs.I -CS · 12A.Qab 8**""· ~·1~**  

### VS4-CS. 1 2B-Comp28

### lv54-CS·1~2C VS4.CS.12S.Grab 1 VS4 · CS·12B-Gtab 2 V$4-CS-128-Gr«l 3 VS4·CS·128.(l<ab 4 jYS4-CS.128-Gnlb 5 VS4 · CS·128-Glab 6**~CS-128-Gnlb** 

### 7 jvS4-CS-12S-Grlb 8

### ~S-1**28-Gnlb** 9 jvS4-CS-1211-Gqb 10 jvS4-CS.128-Grab 11 i'Y:.«:S-1211-Gqb 12 IVS4-CS-128-Gnlb t3**~- r><'1~1** **4** 

## Stream Conlaincrlzed 

### SCllds Cont;inertzed 

### Solids 

### Coo illiuerlzed Sob 

### Contalnec12ed Scids Cooail-fled 5alds CooUinellz.ed 5alds 

### Co 

### ICaiobd 

### Solds**~Solidi Contail~ed**  Solids 

### Ccnllhlrized Solids 

### Coolaileriled Solkls Ccntafnerizcd Solcls 

### Conlalneolzed Sol ds 

### Conlaln«im sonds**Cool~~Wirltcd** 

### Solids Conl8 1 nerlzed So l ids 

### Coolailto1led 

### Solds Conlaileltled Solids Cootafnedzcd Sold$ 

### Conllllnlrized Solids Containerized 

### Solids 

### Coo o:ailoerized Scllds**~Solids** 

### Coollaloerbd Solds CcniiNized Solds 

### Continlrtzed Solds 

## W a st e Sample Logb o ok 

# V e olla-Sauget , ll

- Unit 4 CPT Pr oj ect Numb e r 4 09 4 25 1 0

. 20 Fraction C ond 

## R un Dat e Time 

## TW**~** 

### 1 

### 1A

## II)**1~"6'ito** 

### Alltive 1 2A 

## I:>'Hof Alltive 1 2A 

# ()'oro Aod1IYe 1 2A 

### IO()fi Aod1IYe 1 2A**~~** 

### ArciWe 1 2A 

### I · '-**10~6"** 

### AJd<lve 1 2A 

### ArciWe I 2A Aldl!Ye 

### 1 

### 2A**~** 

### 1 

### 28 

# I'" _, Ill 

## 1!.35 Phys/Comp , 

# Meta " 1 

### 28 

## tS'o<J**Ph~** 

### 1 

### 28 

# ....s:**IS'~$"'** AodWe 1 28

## ~~ Aldllve 

### 1 

### 2B**~~ o**  

### AoltiYe f 

### 2B**1~$** 

### Ardl lvo 1 

### 2B 

## llf-6 AoltiYe 1 2B 

## ll ' f Ar<t!Ne 1 

### 2B 

### I U O Ardi.e 1 

### 28 

### l 'tOif ArdVve 1 

### 2B

# ·~ Atthlve f 

### 2B**114~** 

### MJ:We 1 28 

## l'tfo An:td.e 1 2B 

### lfO ,- A:tiM 1 

### 2B**~O** 

### Aldllve 

### 1 

### 28 

# .... I U S' Aldllve 

### 1 2B Page 1 9of29



### GW 

## C om ments**~** • • " '**5" 12.** **~** 

### '$ () '"'**·** 

# , , ,tl

...**~1 0**  

## (, 

## '"( a. · , • •

# ~ "' ""**~~~~ -.** **1,1~ "1**  

## '-1'\ 'iq**~()** 

## ·,**1, 58** **0~** 

## SO't "' 

## .. , ·,17 -tJ<\**.s,** 

# .. ... 3zi!o o...**~<;** 

## 3 \**1~0 "1** **·.** 

## 1 , 8'\b c.**~~%~** 

# qa, · , 

# a.**·~i q** **~~"ic, '50** **~** 

# a.ou."'**'.i~k\** 

## f/l 

# i**Q, lt5'(\** 

### sn~

### 118**~,~ ~0~** 

### ~<**r, '·~~qo.** **~<tiC~** 

# RS ·, 1 ,/o?l"\ S'l?,e,

### ~**~** 

### ' I, (\Oa_t. 

## SCI{a \0\ 

### ! 

## ),C\'1'\"**'j\ ~**  

### «>. I 

# I P>

### ~ 

# 1 , 7'\a, "\**0~** 

# !a'

. •

I, ")!).(\ 

# t\**'"** 

# ... ; '34; 

# • . nr q 1f11{ q 

# ta ·. \,')3 0

_ '\

# < tTl 

## en 0 w 00 0 V> 

### Sample JD Code Stream**lvS4-U!W·12A~1** Low BIJ IJqi.WI Waste 

### lv<:Lt I>W.12A-Gr.lb 1 Low BIJ**~l.id** 

### Wua 

### lv<:Lt IN< 1 2A-G"ab 2 Low BIJ 

### l4ld Wtt#! 

### lv<:Lt IIW.12A-Gfab 3 Low Blu 

### l4ld Waste

### ~l8W-12A-Gr.lb 4 Low 

### BlJ 

### l4ld Waste**,..,. ~**  ""'·12A-Gr.lb 5 Low BIJ 

## l4id 

# w-**~** A11/- 12Mllab 6 Low Blu Liquid Wale lvS4-LSW- 1 2A-Gr.lb 7 Low 

### Blu Liquid Wasle**~o.tc:LJ** AW.12A-Gr.lb 

# a Low 

### Bar !.quid WISIO lvS4-U!W- 1 28-Conll2A Low81U**~uid** wasre f..IS4-U!W·129-C<rnp28 Low 

### B1u liquid Wasle

### ~BW·1~ Low &I Liquid Waste ivS4-L9W · 1 2B-G<all 1 Low Bill**~l.id** Wasut ivS4-LBW· 1 28-G<ab 2 Low B1U l iquid Waste f./sw.aw -128-Qab 3 Low 

### Bru Liquid Waste jltS4-L9 1'1-1 2B-Giab 4 Low Bill**~uld** Waste fvS4-LBW · 128-G<ab 5 LowBiuliquidWaskl !'Js4·lBW-128-Gr.lb 6 Low BIJ Liquid Waslt VS4-LSW-128-Gnlb 7 Low Btu liquid Wasle !vS4-LBW · 128-Grnb 8 Low BIJ liquid Waslle

### ~BW**1~9** Low 

### Bal Liquid WatS/e !VS+l.BW · 128-Grab 10 Low Btu Liquid Waslle jv$4·1.8\\'
· 128-Gnlb 11 Low Btu 

### liQUid Wasle

....,._, -- 1 28-(lrlb 1 2 Low 

### Bcu Uqud 

## w .... lvS4-U!W-128-Gnb 13 Low 

### Blu Liquid Wasle

### ~W-128-Gnb 1 4 Low 

### lllu 

### l.i!IMII'Iasle 

## Wa ste Sam ple Logbook Psge11 of16 

# Veolia-Sauget , IL

- Uni t 4 CPT Project Number 40942525

. 20 Fraction Cond 

### Run 

### Date 

# rnne lW 

### G W 

### Comments**~** 1 

### 2A

## Ill**~s** a.')OIIl

......

.AictiMe 1 2A**0<\ l~**  

## SOQ,.L**~** 1 2A 

### 11,50 NclliYe 1 2A**00~** 

# .wwe 1 

### 2A I <l ie)**~** 1 2A 

### 1-o..**3~** 

### ·'- ArdliYe 1 2A Archive 1 2A 

### ArdWe 1 

### 2A**~** 1 

### 28 

# .. ll t M**~~~**

## I~**') QO**  ool Pllys/Coo'lp, 1/.elals 1 2 8

## ~II' l)OQ 

### ooL**~** 1 

### 28**~**

## ~~" Arcl\iva 1 

### 28 

## 1.:»'5"**O'I l..**  Arcl\lve 1 28**~'S O**  ArdWe 

### 1 29 

## l'fO'f Ar

ch i'lll 

### 1 

### 28**·~()** Arcl'jve 1 

### 28**I~M ·**  

### ArdWe I 

### 28 

### l)f O Arthlw 1 

### 28 

## ,. 115 Arcl'ive 1 

### 28 

## l'liO Ntll>e 1 28 

## 11115 Archive 1 28 

### l'lfO ArdiNe 1 29 

### I S1)f Ntll>e 

### 1 

### 28 

# . ..**~** 

### ArdWe 1 

### 28 

# .. t 'B S" 

# ..... AlrJwe 1 

### 28 

# -

# < (Tl 

## en 0



# ..... 00

## ~ Sample 

### 10 Codo 11M:cq>1 ·12A.Qab 1**~.** 

### - ·12J..Gr31>2**~BW·12A.Qab** 

### 3 j>'S4-IIBW-12J..Gr31> 4 12A-Ollb5 

### IJS4.HBW · I1A-Gnlb 6**. '~**  

### - 12J..Gr31> 7 VS4-HBW-12J..Gr31> 8**VS4-H BW** **2~2A W-1~28**  

### VS4-HBW · I28-Cornp 2C VS4-HBW·I2B.Qab I \IS4-HBW-128-Gtab 2 VS4-HBW· 1 2 1 Hifab 3 Vs4-liBW-128-Gtab4 VS4-HBW-128-Grab 5 VS4-HBW-12B.Qab 6 VS4-HBW.128-Grab 7 VS4-HBW-128.(ifab 8 V$4-HBW · 128-Grab 9 \154-HBW

- 128-Grab 10 VS4-HOW.128-Grab 11 V$4-HBW

- 128-Grab 12**~.** •rn 

### - 128-Gtab 13 

### V$4-HB\'H!li.Qab 14 

### Stream**~** 

## a.I.JQ<.Id 

# w-**~** 

### Btu liQIM Wasle 

## Hi!tllllu liqiM 

## w-e**~B** 

### .. i.4*1Waste**~** 

### lllu 

### I.JQ<.Id Wil51e 

### Hi;h lllu 

### I.JQ<.Id Want High 

### lllu Uquld 

### Wesle**~** lllu Ucpj Waste 

### High 

### lllu UqiAd 

### Waste H

igh Btu UqoM Waste**~** 

### lllu UqiAd 

### Waste High Blu 

### Llqi.id Waste**H~** 

### BIU LIQUid Wasl& Higtl 

### Bill U qi.id W11$1e High B t u Uquld WilSie HfGh Btu UqoAd Waste High Btu liquid Waste High Btu Liquid 

### WISie**H~** Btu 

### Uquld Waste High 

### BIU Uqi.id Waste Higlllllu UqiAd 

### Wasil!**H~** 

### Bill liquid wasm 

### Hi;tllllu Uquid 

### Wasle H9\lllu l.iquC Wast! 

### Higlllllu Uqo.id Wa,i!**~** 

## a. Uquid 

### WIISt: 

## Waste Sample Logbook**P~tge3of16** 

# V eoli a-S a ug et, IL

- Uni t 4 C PT Project Number 40942525 .20 Fraction 

### Cond 

## Run Data 

## nme TW 

### G W Comments**~** 

### 1 

### 2A

# ~'" 1111C. a,')C)o,.\..

AtciiYe 1 

### 2A**'t }€.**  

# -so o ., L Ndive 

### 1 2A

### il1'~ 

# \ AII:Me I 

### 2A 

# roar. AII:Me I 

### 2A

# ·~**'** lvti:We 

### 1 2A**~** 

# ..**10~ ~**  

### oVc:hiYe 1 

### 2A AII:Me 

### I 

### 2A ArchNe 1 

### 2A Phys/C<lmp I 

### 2B 

# jta,h\ lUi'**i,"/fJ~to L** **Metals** 

### 1 28 

## 11114 

## l5Q()IIIL Phys/Colre> 

### 1 

### 2B I'IJI>**a. c.oo,..~.,** 

AtdM I 

### 28**~~~** 

### 'JOO .,.L 

### Atcltive 1 

### 28**~'S\** Arch i ve I 

### 28 

### llO(a AtdM 

### 1 

### 2B 

# na \ A/chive 1 

### 2B 

## l'n6' An:me 

### 1 28 

## IW I An;f1ive 

### 1 

### 2B 

## I"'OC. Atetive I 28**lit~** 

## I AtdiYe 

### I 

### 2B 

### I 

## 'Of. AtrJVve 

### 1 

### 2B**l'l~l** 

### AII:Me 1 2a 

### ICjOC. AtrJWe I 

### 28 

# 15'. , AII:Me 1 2a 

# -

...

### ~ 

# -· AtdiYe 

### I 2B

### Waste Sample Logbook Pa ge 3 of29 

# Veolia-Sauget , IL

- Unit 4 CPT Project Number 40942510.2 0 Sample 

### 10 Code Stream Fraction Cond Ru n Date 

# nmo TW GW 

### Comments**~Wf·12A-Ccmp 1**  Ucpd Wasle 

### Feed PhysJC<mp 

### 1 2A

## ~lA 

## t o:.r l.,;oo..-l lv54-t \\

'F 

### ·12A-Gnb 1 Liquid 

### W_,. Feed Alf:tive 

### 1 2A

## '\**)? ~**  

## ... l lvS4-tWF·12A.Qab 2 UcpdW asleFeed 

### MJWe 1 2A 

# Q"a**~V.'F·** 12A.Qab 3 lJqoJd Wasle 

### Feed IJ!1:We 

### 1 2A 

### 1007 iVSLLWF·12A-Gnb t 

### l4'!WISliiFeed MtWe 

### 1 2A**~**

### ~WF-12A-Gnb s UcpdWuFeed 

### Ndive 1 2A 

### -&. 

### 10&7 

# ,_ jvs4.t. WF · 12A -Grnb 6 Liquid 

### Waste Feed An;hive 

### 1 2A**~Wf.12A.Qab** 

### 7 

### Uquid Waste 

### Feed AtdM 1 2A

### ~4-LWF·**12A-Gtab8 ~**  Wasls 

### Feed Arcllive 1 

### 2A !'Js4-LY1f·128-Car92A Uquid Was te Feed Pnys/Cornp 1 2S

### ~ •• It

\**1'3'>~-**

### zs-~--\ jvS4-l W

F

· 12

. B.(;anp28 Uquid Wae10 Feed P hys/Canp, Mctlls 

### 1 28 

### l')o"?-

# ~3o~-**' jvs4-** **LWF ·1~2C**  Uquld Was le feed 

### Pl1ys/Con'cl i 

### 2S

### IS"~1- 

# z '-00 .......1 VS4-t WF · 12S..Grab 1 liQuid Waste Feed AleMe 

### 1 28**,~,.,** 

## 600111 L I'JS 4-LWF ·12S-Gta b 2**Llqu~** 

### Wae lt Feed Atthl'le 1 

### 2B**13- S~**  

### VS 4 -I.WF· 1 28-Grab 3 liQuid WMie Feed AleMe 1 

### 28 

### 110'7 IVS 4-LWF· 1 28-Gtab 4 Liquid Wasle Feed 

### M:l1 1ve 1 

### 2 8

### li**~** 

## jv54-t Wf 

### · 1 28-Gtab 5 

### llQu1d Was • Feed Nti:M 

### 1 2S 

# II 'U S jvS4-LW F

· 12B · Gtab 6 Liq uid W ale F eed 

### M:l1ive 1 

### 28 

### Ill 

# $d. jvs4-LWF · 129-Gtab 7 llQu1d 

### Waste Feed Alf:tive 1 2B

### 07 VS4 -LW F · 1 28-Gtab 8 Uquld Waste 

### Feed Ardlive 1 

### 28**lot~·** 

# 1\'54-t Wf. 1 28-Gt&O 9 Liquid 

### Wasle 

### Feed NUtie 1 2S**1'1~7** 

### VSLt WF

- 128-G rab 10 Uquld Wast a 

### Feed 1\rdiYe 1 28 

### l't5,}



# .. (., 

# .. < • ['I") 

## en 0**~WF 128-Gtab**  

### 11 Uquid 

### W_,. Feed NUtie \ 

### 2S 

## tfOJ**~WF-129-Gtab** 12 Uqu1d Waste 

### feed Alf:tive I 

### 28

# ·~**~WF·** 

### 1 29-Gtab 13 Uqu1d Waele 

### Feed 

### Mme 1 

### 2B**~** 

### l fl7 

# -**~** 

# ..., VS4-l.WF·128-Gt3b 14 Uquid 

### w.sle F eed A:dM I 

### 2B 00 0



# .....

# Bulk Solids Sample Compo s ite Data Sheet

P

r oject Name Veolla

- Sauge t ,ll D1te

### IC!f~l\11'3 Project Number 4094252S.20.02 Condition 

### No

. 1 

### Facili ty Unit 4 Run No

# -~ Stream Name Bulk Solids (BS) 

### Stannme 

# ()<\at Composite Simpl e 10 VS4 -BS-liA_ 

### <OMP_ I

_ Stop Time

### ~0% Oper a tor
Sample Number Tim e Vol u m e/ Mass Sample Number n me Volume/Mass 1**()q_~E., ~0~(\**  

### 21 2 

# o 1 

## U"I 

## '5'1**a. ~**  

### 22 3 

### 1 0 0{,**'jla.~** 23 4**10~** 

# "t<\a' 24 5

### t<n~**4,~~** 

### 25 6 26 

### 7 27 8 28 9 29 10 30 11 31 12 

### 32 13 

### 33 1 4 

### 34 15 35 

### 16 36 

### 17 37 18 38 

### 19 39 20 

### Flnal Vo lu m e/M as s

### "il~<~. Commen t s: Collett solids In 1000 

### m l) ar l abe l ed f or Archive

. Take**approp< te** **y~lzed** 

### a nd equo l a li quots r rom ea ch j ar to p rep are t he composite sample in a 4 llter j ar . Reco r d the volume/mass of each 

### aliquot used to prepare the composite sample on the d•ta 

## snw . Retain the remain i ng sample in the 1000 

### ml ja rs and archive

.

SO:J •O!! Sd>-.S.IfiPk CDff!POSile

- O.tc: ,.,..l(J/2**R<~** ,_20/J E-385 

## VES013808

# Bulk Solids Sample Composite Data Sheet Projec t Name Veo li a- Sa uget , ll Date 

### \ 01&11/1} Proj ect Numbe r 4094 2525

. 20.02 Co ndi tion N o
. 1**F~<lll\Y** Un lt4 Run No

### ~6

Stre am Nam e Bu lk Solids ( B S) S tat lT i me**~~~()** Composite S a mple 10 VS4-8S-l i.l :CO MP !A S top Time

## j~?.~ Oper a tor

Sampl e Number Time Volume/M ass Sample Numb e r Time Volume/Mass 1 

## tal(. 

## 'i06q 21 2

### ~~~I 

# If\(,, 22 3

### I~**t;O~~** 23 4

## ~~~**' G"l~c:..**  24 5 

## \ ?,"lt

## 4.1\'\~ 25 6 26 7 

### 27 8 28 9 29 

### 10 30 11 31 12 32 13 33 14 34 15 35 

### 16 36 17 37 18 38 19 39 20 Final Volume/Mas s

### ~.slq~ Comments : C oU ect s olids In 1000 ml ja r l ab e l ed for Archi ve
. Tak e a pp r opr l ately-s l le d and eq ua l allquots from each jar to prepa r e th e co mpo si te sample In a • Uter jar. Record the volume/mass of eadl aliquot used to prepare the composite soomple on tb e data meet

. Retain the r emaining samp l e In the 1000 m f jars and archive

.**~~~ I~** **U ~IOrl\**  1\' "lt (.

. . IOii.'ll\3**~-05** S<I/>-S<»op/< C""V»'il< RcofsiM (>m; J- !lOll Re>f•

- J .,.. ZOIJ

E

· 386 

## VES013809

# Bulk 

# Solids Sample Composite D ata Sheet

Pro j ect N ame Veolia

- Sauget, ll**O•t~** 

## IO(a.'tfl3 Proje ct N u mber 409 4 2525

. 20.0 2 Con d i t ion No

. 1 Fac!Rty Unlt4 Run No

### a.~ Stre a m Name 8u l k Solids (B S ) S tart Time

### ~~~(, Composite samp l eiD**VS4·B S.1~** **;C OM** **~** S t op Time 

## I '60EI Ope r a t or

5amplo Number T im e Volume/Moss Sample Number Time Volum o / Mass 1 

### I 

# a_%**~** 

## 10 tc 21 2**13.~1**

### Q.CI~ 22 3**t~Ot;.**

### a.q~ 

# '\ 23 4**tl~ \** 

### ~()?!**'\** 24 

## s

## ~\~**~'l~** 2 5 6 

### I'" 

# slit\ 26 7 

### I '40 

## El**?,0"7~** 27 8 

### IIU\ 

## &1\1 Clj 28 

### 9 

## I "tl'-**d.<\{,~** 29 1 0

### I~ 

# lil**--1\~~** 30 11 

### \ '\"0{,

### '30~~ 31 12 

### 3 2 13 33 

### 14 

### 3 4 1S 

### 35 16 36 17 3 7 

### 18 38 19 3 9 

### 20 Final V o lume / M ass 

# .,**~~~~** Comm en ts : Co iled soli ds in 1000 ml j ar labele d fo r Ar ch ive. T ak e ap p r o p r ia te ly

- size d a nd equal all quots fro m**~a ch**  j ar t o prep ar e t he compos i te sample in a 4 Liter )ilr. Record t he volum e/m ass of each aliquot used to prepare the composite sample on the dat a sheet

. Reta in t h e r emai nin g sa mpl e I n the 1000 ml j ars an d a r c h iv e .

.st>S · o5 Sub-SM¥>/< C""'f"S/r<**~Dille:** JUM Mit R

e vkntl: June 201.1 E·38 7 

## VES013810

# Bulk Solids Sample Composite Data Sheet
Project Nam e Veoh

- Savget, ll Oote

### l()l~**'tl 13**  Project Numbe r 4094 2525. 2()-() 2 Cond itio n No

. 1 Facility Un l t4 Run N o**$.~** Stre am Name Bulk SOlid s (BS) Start lime**~%** Composite Samp l e 10**VS4-85-I. ~OMP** **~** St op Ti me

### ~~~**~** Ope rator

Sample Number Tim e Volum e /Ma ss Sam ple Number llmc Volume/Ma ss 1

### ·~3E,**~06 "1**  2 1 2

### 1~1$1 

# Sl'i 'I 22 

### 3 

## nO E. 

# 0.1\1{**~** 23 4**1\~** 

## I

# i.4\~' 24 5 

# ,u , Q.,{,.., 25 

### 6 

## I 

# '3's 

# l**~a-a~** 26 

### 7 I 

## '\04**~Cl9l~:j** 27 8 

## I I\& \**~~ .**  28 

### 9**\It~~** 

# a.'\IJ\'.o,_ 29 

### 10 

## 1 \.I'SI**30\~** 3 0 11 

## I**~Ot.**

### ~~, 31 12 

## I**IS~** 

# I**'J-4\7~** 32 13**'S~** 

# Q.l\&, 33 

### 1 4 

### 34 15 

### 35 16 36 17 3 7 

### 18 38 

### 19 39 

### 20 Final Volume/Mass

### ·a,q\7~ Comments: Coh ect s ol ids In 1000 ml jar labeled f or A r ch i lf<!

. Take ap pro priat ely-s ite d and equal allquots from ea ch j ar to prep are the composite s a mple I n a 4 liter jar

. RKO r d the volume/mass o f each aliquot used to prepare the c:omposlte sample on the data 

### sheet Re t ain the remalnl"ff sample i n th e 10 00 m l Ja rs a nd ar chi ve .

SDS ·O!J 5<4>-Sompk Ctxop os/to**k.-.isio•t>tt~<;** J

- 21) /2 -d:J-21)13 E-388 

## VESO I38 ll

# Containerized Solids Sample Composite Data Sheet Proj ect Name Vco li a - Sau get, l l Da t e**1()~~113** Pro j e ct N u m b er 4 094 2S25. 2 CHJ2 Cond i tion N o. 1 fidii iV Lin i t 4 Ru n No 

## dl'\ S t r e a m N ome Contai n erized So l i d s ( CS ) S tar t Ti m e

### c~~sCom po si t e Sam ple 10 VS4 < H iA, <O MP

_ I

_ Stop 

### r.m e

### 5" Op erato r

Sam p le C o ntain er 10 Ti m e Volume/ S omple C onta iner 10 Time Volume/ N umber M a ss Nu m be r M ass 1

### ~ 

# <:l<\l1**~0.~** 21 2 

## 'ill.**Q~lO**

### 'SIS**~** 2 2 3 

# ,-o**~00'$**

## 'SO~~ 2 3 4 

## bO \Oa.Q 

## "1%(\ 24 5**~,** 

# \Ol' 'tl\ 

# 'c.. 2S 6 

### 26 7 27 

### 8 28 

### 9 29 

### 10 

### 30 11 31 

### 12 32 13 

### 33 

### 1 4 34 

### 15 35 16 36 

### 1 7 37 18 3 8 

### 19 3 9 

### 20 A n a l Vol u me/M ass

### a,5t&~ Comm e n t s: T ake a pp ropr i at ely-s i ted an d equala l lqu o ts f r om ea ch con ta ln e rto p r e pare th e comp osi te samp l e i n o 4 · U t ar jar

. Reco rd the vo l u m e/mass o f each ali q u o t used to prepar e the compo s ite s a mpl e on the d a ta s h e et

. Collea a repres enta tive a liquo t of the rem a inin g materia l In • 500 m l j a r t o be arch ived

.**SDS-05~ /cc-pnllc**  l& 'ffiMft**:** June. lOll Rcl'l<.&aa!V..,. 10 / J 

## V

E S01 3 81 2

# Containerized Solids Sample Composite Da t a Sheet

P r oject Nam e**Ve oli<~**  Sa u . get , l l Date 

## l al<i\4/1'3 Project Number 

### 40942525.20.02 Cond it ion No. 1 Facility Unlt4 R un No 

# 0.9 Strum Na me Contai n erlted So lkh (CS) Start Tlme 

# 1a.w Compcsl te Samp le tD V S4 .CS

- 1 U ..COM JIU S top T i m e

### ~~~6' OporatOf

Samp le ConllllneriD nme Volum e/ Sample Conta i ner 1 0 

### Time Volume/ Number Mass Number 

### Mass 

### 1 

### 'lit).**I• U~** **-i'()/ ~**  

### 21 

### 2

### ~a 

# 1 a '5d!> 

# "'en e. 22 3 

# so**\~OS** 

### ')() '-\!!! 2 3 4 

## 60 1UO**()~~** 2 4 

## s 4'6**~** 

# '5"'00 ell 25 6 

## -_, 26 7 

### 27 8 28 9 29 10 

### 30 11 

### 31 12 

### 32 13 33 14 

### 34 15 

### 35 16 36 

### 17 37 

### 18 38 

### 19 39 

### 20 Fina l vot

....... 

## /Mass**~.~1\~** ComrMnts: Tak e appropr iat e ly-sized and equal a llquots from ea ch cont ain er t o prepare the compo$lte samp l e In a 4 -Uter jar. Record th e volume/m ass of each a liq uo t used to prepare t h e compoSite sam ple o n t h e data sheet. Co llect a represent a t ive aliquot of the ,_alnlng material In • 500 ml Jar t o be archived

.**SDS·OIJ5l.<b-s...plc~te** /&- {)of<.· JIN 2()/i! 

# Re.wr.m

.... 2(//] 

## VESOI3813

# Containerized Solids Samp l e Composi t e Data Sheet

Pr oje ct Na r ne V e olla -S a ug e t, II

. Date 

### l <l I 

## <l.'\ 

## 1 13 Project N um ber 40942S2S

. 20.02 Co nd ition N o. 1 Facility Unlt 4 Run No 

# o.B
Stream N a me Contai n e r i z ed S ol i d s {CS) S t ar! T i me**1~)1!)** Composite Samp l e 10 VSH :S

-l

t.1 · COMP J.l Stop Time 

### 1 665" Ope ra 

### tO<

Sa mple Co n t ain e r ID 

## rrme Volume/ Sa mp le Con t ainer I D Tl m e Volum e / N umbe r M ass Number 

### M ass 1**~~** 

## IUS'**a~q_~** 2 1 

### 2 

# 40.**~~ 0** 

### ~~**~** 22 3 

## S'b I 

# '305' 

# i:l''" 23 4

### ~C>**~~ 0** 

## .1~~ 24 5

### b~ 

## 1 335**~~7~~~** 2 5 

### 6 

# BO l')'iiO

# ~'~ 26 7

### ~~ 

## 1\iOS**&.'\'\~** 27 8

### 'I~ 

# 1ttao**3~\1:1,** 28 

### 9 

### 10% 

# 1435**Mi ~**  2

. 9 1 0 

## I I 

# f> 1 1 

## HO**~q!iiq** 30 11

### a~ I**~0** 

# 5"**~cu** 

# .... 3 1 12 32 13 

### 33 

### 14 34 15 35 

### 16 36 

### 17 37 18 >8 19 39 20 fl nol V o l u me/M ass

### ~%()'\ Comments: Take ap proprt at ely-5l zod and equal aliquots frO<n each oon ta iner to pr epa r e t h e co m pos i te sa m p le I n a 4

- U ter far. Reco rd t he vo l ume/ m ass o f each ali q u ot u sed to p repl! r e t h e composit e s amp l e on tho data s heet. Coile<1 a r epr eJent a tlve afiq uot of the remaining materia l in a 500 ml)ar t o be arch ive d

.

SDS-D!i.SU. · Sanp/c**~rc** Rtvf- Oafc ' J.,.. 20/l**R-.~v** .... 20tJ 

## VESOJ381 4

# Containerized Solids Sample Composite Data S he et Proj ect N ame Ve o 1ia- Sau get , IL 

### Da te 

## \()I 

# 0.'\ (I 

# 3 ProjeCt Number 40942525.21).()2 

### CO ndition No

. 1 

### F

acility 

### Unit 4 Ru n No 

# o.t Stream Name Con ta i ne riztd S olids (CS) Start nme 

# \ •l! Composite Samp. le 10**VS4-CS.l COM** **~** 

### S to pnme 

### I 

### '535' Op erator

sample 

### V olume/ S•m p le Container to 

### Time Volume/ Conta lnecr 10 Time 

### Number M W Number 

### Mass l

### ~ 

## 1&.31)**10()~** 21 2 

# q. 13.,0**~~~** .. 

### 22 3

### ~0 

## 1\0S'**~!:){)~** 

### 23 4

### ~0 

## J'?>a. O**,'\\** 24 5

### b~**~~5'**

## a~~<\ 25 6 

## &(') 

# 1oso**3e~~** 26 7

## \~ 

## I 'l OS'**a<l~** 27 8 

# <u I 'I 

## ilO**~00~** 28 

### 9

### \~t, 

# , ..**~, 3Q'jj~**  

### 29 10 

# \\l tt.t 'iO**oCIO~** 

### 30 11

### l~b 

## I**'S O~** 

### '30,}**_~** 31 12 

## l'a b**1r~o ,n~**  

### 32 13 

### 11( 

# 3**\'S~5 \0~**  33 14 34 

### IS 35 16 36 

### 17 37 

### 18 38 

### 19 39 20 

### Fina l Volume/Mass

## ~'**~~** Comments: Tak e ap p ropria tely-sited and equ a laliquots from ea ch container to prepare t he**compos~•** 

### sample In 

### a 4·Uier jar. Record t he volume/mass of each a liquot use d to pr•par e the compo si te sample o n the data she et

. Coll ett a representa t i ve aliq uot of the re main ing ma terial lrl a 500 ml jar to be a r chived.

SD$ -«1 SIA>-s-p/e 

### c-,- · ..**·ISIM Of!~9{"""**  EOJZ fh<o -d; J""" <OIJ 

## VESOI3815

# Liquid Waste Feed Sample Composite Data Sheet**Proj~** N ame Veolla- Sauget, ll Dat e

### ti~~Jt> P

ro

ject N umbe r 40942S2.5

. 20-02 Co nd itio n No

. 1 Fa ciUcy Unit Z R un N o

### ~/>.. Stream N ame Lo w BTU liqui d Was t e (LBW) Stan T ime

# <:~'a**c** Composite Sample 10**VS3-lB IY** **.(OMP** 

## .L Sl

. opTlme

### {)a~ Operat o r

Sample Number Tlme Volume/Mass S amp le N umber Time Vo lum e/Mass l

### 0~~0 'S()O 

## toL 21 

### 2**oq~o** 2Z 3 

### \()()') 23 4 

### I 

## Cla,o 24 5 

## 1035' 2S 6 26 

### 7 27 8 

### 28 9 29 1 0 

### 30 

## u 31 

### 1 2 3 2 13 

### 3 3 14 34 15 

### 35 16 

### 3 6 1 7 37 

### 18 38 

### 19 39 20 F ina l Vo lume

### ~-~0() Ill 

### L.
Comments: Co llect approl)(late l y -s i z ed a n d eq u•l all q u ots a nd t ransfe r Im me diatel y I nto a 4- ll t er compo site Ja r
. Colle<t a separate 500 ml bo!Ue o f sample at each samplins time t o be reta ined in archiv es
.

### ~"'\)\~!, 

## (,.0\ltc..\od**~rotrl ~-II**  

### ..**~.~~ SI)S** **~** S<lb-$Dmpk Compont• flv m;., O.lt' J- 20/1 Rni<o ..J:J

.... Z0/1 E ·3 93 

## VESOI3816

# Liquid Wast e Feed Sample Composit e Data Sheet ProjeCt N ame veo na - Sauget , t l D ate 

### \01**~'Ill)** ProjeCt N u mbe r 4094 2525. 2()-02 Con d i ti on No. 1 Fadllty Unlt2 Rim No

### a.~ Su ea mName Low B T U Uquld W aste (LBW ) S tart 11me 

# I 

# a.:!!,- Composlte Sample tO VS34.8\V·1 -" : 00MP .Mi St op Tlmo 

# \ s ls Oper a t o r

Sample N umber Tlmo Vo l ume/Mass Sample Numbt!r Timet Volume/Man 1

### 1~**'!. ~** 

## ~00 "" '- 21 2 

# 1a.'iO 22 3 

# t l o 'S 23 4 

### 1 

### 'l 

# a.o 2 4 5 

## I l lS" 

# . .. 25 6 

### 26 

### 7 

### 27 8 28 

### 9 29 

### 1 0 3 0 11 31 

### 12 32 13 

### 33 14 34 

### 15 35 1 6 36 

### 17 37 18 38 

### 1 9 39 

### 20 Final Vo l ume 

# a. , 'i'00111\...

Commen t s : Coll ect appro p r iatel y - sized an d equ a l a llq uo ts and transfe r I mme d iate l y I nt o a 4 ·Uter com po site Ja r
. Co lt ea a s eparat e SOO ml bottle of sa mple at each sampling time to 

### be retained in ar chives.

### ~a 

# ..... o t

td hiJI'\ 

# x - 1 \**~\ tlllf'>** 

$ll5 • 06 S..C · SM>pk C""'i'i'Ir•**~~o-.om.:** J-**201~** 1/o

- Jilt¥ 20/3 E·3 9 4 

## VE S013817

# Liquid Wast e F eed Sample Composite Data Sheet

Pr oj ect Name VeoHa -Sauge t , ll Date**1ora.~113** Project N u mbe r 

### 4094 2525

. 20. 02 Co ndi t ion No

. 1 Faclfitv 

### Untt 2 Run No 

# &.B
Stream Name lOW BTU liquid Was t e (l 8 W) Start Tl mc

### ~~**~S'** Composite SampltiD**VSH8W ·J.o!l** **<OMP ~**  Stop Tlme 

## \S'O, Operato r

sample N umber T1me Volume/Mass Sample Numbe< Time Volume/Mass 

### 1

### ~~~lj**~00** 

### ...**~** ll 2 

## IUO 22 3 

## \606' 23 4 

### l 

# \d-o 24 

## s 11'36' 25 6 

### I**~'SO** 26 

### 7 

## \'iOS 27 8 

## I"\**~0** 

### 28 9**II%~~** 29 

### 10**I~** 

## !5() 30 11 

### l'fOf -I- 31 12 32 13 33 

### 1 4 34 15 35 

### 16 36 

### 1 7 

### 37 18 

### 36 

### 1 9 3 9 20 F i nal Volumo 

### ; , \OOM._

Comm e nts: Collect appropriately-sized a n d eq ual allquots and transfer Imme dia te ly Into a**<~-titer** composlte)ar. Colle<! a separate 500 ml bottle of samp l e at each sampling lime to be retained In archives.



## 'i>q_""\)1 

# Q(\**~UII'I\ \\** 

### ~~..tQII"' 

## <.-#/1._.-f A,.o, 

# i 

# c... r £. 

### VS3-J_gW-l:Z..I3- 

## eo ... f'2P. -1::111 

## P

SOS.(IfSSub ·SM!plo C011Y"'SII• l«riskm 

## t:Jtn-.· JU/re 1011 ll"""""'*J

- Z0/3



## VESOI3818

# Liquid Waste Feed Sam pl e Compos it e Data S h eet Project Naill<! Veo fl a -Sauget , l l Dote**,~,** 

# ..**~113** Pro j ect N umber 4 0942525

. 20.02 Condition No

. 1 Facility Uni t l R un No 

# a.& Stream Name Low B TIJ ll quld waste (l 8W) Start Tlme 

## l iJ-'3) Co mp osite Sample ID**VSH8W f.t-** **COM ~**  Stop l i mo 

# 1HS" Ope<ator

Sample N umber 

### TTme Vol umt/ Mus sample Numb er Time Volume/Ma ss 1

### \;}.**~~ ~()()**  f'l '- 21 

### 2

### l~iO 2 2 

### 3 

# -noS l3 

### 4 I

### ~0.0 24 

## s**~~~'J** 

### 25 6 

### l l'lO 26 

### 7 

## ,**cto~** 

### 27 8 

### I 

### "16.() 28 9 

# ,q·u· 29 

### 10**14~0** 

### 30 II 

### \ fOG" 31 12 

# 11 no 32 13 

### l'i!i" 1- 3 3 

### 14 

### 34 15 

### 35 16 36 

### 17 37 

### 18 38 19 

### 39 

### 20 Fmol Volume 

## i,(:.OO "'L
Comments : CoUect ap p r oprlately · slted a n d equal al l quots an d transfer Immediately Int o a 4 · Uter com posite jar

. Coll ect a separa te 500 ml bottle of sample at each sampf111g tlme to be reta i Md I n archives

.



# f.Q""9**1~** 

# holt\ "t. " l\ 5**~(QQI'I\**

$()$..()!! Sub..sa.pl<**~;,.** lll

>fliM Drzr

..

• J- Mft 111""-d: ' """ 20/J E

·396 

## VESOJ3819

# Liquid Waste Feed Sample Compo s ite Data S h eet
P

roj ect N ame v eol la

- Saug e t , ll D a te I()

### 1~1\1\3 Project N umbe r 40942 5 25.20-02 Cooditlon 

### N o . 1 

### F adllty U n i

t4 R u n 

### N o

### a~ St

r eam N a m e H i&h B T

U liquid W<Ut e (HBW) Start Time 

## C(\S{, Composi te Sample 10**VS3- HBW-l** **<OMP** 

### .1:_ StOP Time Opera to r
Sample Number Tlmo Volume/Mass Sample Numbet 

### nme Volume/ Mass 1

### 01:\~E.**~00** 

## h\1. 21 2

### O~'S**I** 22 3 

### \00& 23 4 

### \()**~\** 2 4 5

### \()-a~ 

# .. 25 6 26 7 

### 27 8 28 9 29 

### 1 0 30 11 

### 31 12 3 2 13 

### 33 1 4 34 lS 

### 35 16 36 17 

### 37 1 8 38 19 3 9 2 0 Final Volume 

# •• 150()

.... \...**Comm~** Co lle<! apprOPriately-sized 

### and equal 

### aliqu ots end transfe r 

### immedi at ely in to 

### a 4- Uter composi te jar

. Co llect a sepa r ate SOO ml b ottle o r samp l e at eac h sam p ling ti me to be re ta in e d In archiv es
.

### !.~c-.o**~~~ ~IOI't\** 

### ~-~**~\~ft\**

5().5-05 Sub.s.n,pie**~··**

- O.te: J- 21>/l Rew..-I:J<JM//!()1) E-397 

## VES013820

# Liquid Waste Feed Sample Composite Data Sheet

P roject Na me Vcolla -Sauget, IL Dote

## ~~ 

# ta. 't l 

# n Projecl N umber 4 09 4 2S2S

. 2D-02 Condition No. 1 Fa cilit y U n it 4 Run No

### 0.~ St rtam Na me High BTU Uquld Wast e (HBW) Start 

### llm e

### ~~{, Co mposite S omp le 1 0

### VS**l!.! :C** **OM ~**  Stop Time

### ral~ ()per.! tor

Sample Number Tim e Vclume/ M •u Sample Nu m be r llmo Volume/ M ass 1 

## 1 

# a**~€.** 

## 'l 0() ttl 

# L. 21 2 

# 'n 1 22 3**1~0{,** 23 4

### I~(} 

## I 24 

## s ll**~5' -~**  2S 6 

### 26 7 27 

### 8 

### 28 9 29 10 30 11 

### 31 

## ' 1 2 32 13 33 

### 1 4 34 1S 3S 

### 16 36 17 37 

### 18 38 19 

### 39 20 F i na l Volume

### .-oo 

# "'\.

Comments : Collect**ap.,ro priate** **ly~lzed** and equala Oqu ots and transfer Immediately Into a 4- U ter composite jar

. Collect a separate 500 m l bottle of sam pl e at each sampl ing tim e 

### to be retaine d in arc hives

.



# sa"'o\ ed**~"' -Ia..** **~+r(Qrn**

SDS -O!J SlJb.Sompk C/Jmpos l f• -·(}Qte: JUM/0/C l/o-JUN20JJ
E · 398 

## VES013821

# Liquid Waste Feed Sample Composite Data Sheet
Pro je ct No me V I!OI I a - 

### S au g e t , l l D ote 

## \()flit 

# /13 Project 

### Numb« 40942525

. 20-02 Condition N o
. 1 Fad Illy 

### Unit 4 

### R un No 

# a. s Slteam Na me High OTU liquid Wa ste (HBW) 

### Sta rt llme**1~){,** 

### Comp osit e Sa mple 1 0**VS3 HBW** **.C OM** **A\_** 

### S t op llme 

## I 'SOE. Oper a tOt

Sample Number llme V olu me / M ass Sample Numbe r 

## rune Volume/Mess l

### 1~**14** 

# -aoo**~>~L** 

### 2 1 2**Ia,_~ )**  

### 22 3**\~6b** 

### 23 4**ll~l** 

### 2 4 5 

# rns- 2 5 6 

### ll'f 

## I 2 6 7 

## l'lO' 27 8

### l'l~\ 28 9 

### I**'t~'** 29 1 0 

## l't'rl 30 11 

# \.;or.



# - 1- 31 1 2 32 

### 13 33 

### 14 3 4 15 35 

### 1 6 3 6 

### 17 3 7 18 

### 38 19 

### 39 20 Final Vol u m e 

## 'i , 100 .,.I.
Comments : 

### Coll e ct**appro riately~lzed**  and equ a l allquots a nd trons! er Immediately in t o a 4
- LHer composite jar

. 

### Co ll ect a s epa r ate 50 0 ml b ottle of s amp l e 

### at ea c h sam p ling 

### ti me to be ret ai ned In arch ives.

### qlflp**I~ ~1'1\**  

# "1.**~**

## st~111.**c.t ~w** **t** 

## , .J. 

## ...t ..,. .. .. . .**~ ~**  

## - ., , ew- roz. B- Gt>"'4f 

# z (}

-**~p**

$0$· 05 SUb -samp/o C O/IIfN>S II

< ltz -"lon l>ote : J-l0/2 -J-lOJJ



## VESO I 3822

# Liquid Waste Feed Sample Composite Data Sheet Project Name Veolia -Sauget, t l Date**~1, \113**  Project N um ber 4094 2525.2 0-<12 Co nd i tio n No

. 1 

### FadiKy Unlt4 Run No

### ~! Stream Name 

### 1-i l gh BTU Li q ui d Was t e 

### ( fl OW) Start Time

### ~~~6 Composite Samp le I D VS3-HBW

- 1 !l_

- COMP 

### j&. Stop Time 

## l 'ilEl Op era to r


### Sample N umber Time 

### Vo lu mo/Mau Semple Number Time 

### Volum e/ Mass 1**~l{.** 

# a o <:> ,. \... 21 

### 2**\a.,~)** 

### 22 3 I 

## lOE. 23 4 

### ll <1.. \ 24 5 

## IllS' 2 5 

### 6 t \'tl 26 7 

## Ill OE. 2 1 8 

### I 

## 'il-l 28 9**1~\,** 29 10

### Itt~ 

# I 30 11 I**~0(,** 31 

### 12

# •"~ I 32 13 

## I**fl~ -~**  33 

### 14 34 1S 3 5 

### 16 36 17 37 18 38 

### 19 39 

### 20 F inal Volumo 

# a , \.oo

...**~** 

### Comments : Co llect ap p r opriate ly

- sized a n d e qu al a ll qu ots and tran sfe r Im medi a te l y I

n

to a 4-U t e r co mp os i t e j ar . Collect a 

### sep arat e 500 

### m l bottle of sam ple at ea ch 

### sam pli ng tlme 

### to be 

### r etaine d in archives.

### ~llfo\Qild**f\1** 1'1\**~-** 

## " \<1..**b\- ~~** **SO$ ~**  Sub-Somplo Ccmpqs ll • 1/cvfPH 0.10' J""" 20U 1/c -d: Jllf¥ 2(/JJ E · 400 

## V£8013823

# Liquid Wast e Feed Sa mpl e Composite Data Sheet Projact Name Veoll •- Sauget , ll D at e

### l()j~~"' Pro j ect Number 

### 4 0942525

. 2().02 Condition No

. 1
Faci li ty Un it 4 Run N o

### ~A Stream Name liq uid Waste Feed (L\VF) Stott Time 

# <:><\37 Composite Sam ple ID VSHWF · l !t. · COM P 

### .1_ Sto p Ti me 

## 103J Clpe<ator

Sampl e Number Time Volume/Mass Somp le Number 

### Time Volum9/Mass 1**C)'\~7 ~()()**  

## .... L. 2l 

### 2

## 0"~~ 22 3 

## \007 23 4 

## I OU. 24 

## s 10&'7 

# • 25 6 26 7 2? 

### 8 

### 28 9 

### 29 10 3 0 11 

### 31 12 

### 32 13 33 

### 14 34 

### 15 35 16 36 17 3 1 

### 18 38 

### 19 39 

### 20 Flnal Volume 

# a ,'ioo "'t.

Comments : Collect appr o prlatelv-<fud and equ a l allq uots a nd transfer Imm ediately i nto 1 4-Ute r compo site ja r . Coll ect a separat e 500 m l bo ttle of sample at each sampllns time to be retained in a rchiVI!s.

## ~lt\t;)l9d**~~"'** 

# '1.**-0.~**

## ~h~q"'

SDS-M Sub-s-pie**~tit•** Rcrtslt:HJ l»Je: JtJM 2012 l&>i<w<dl J-lOIJ E-401 

## VES0138 2 4

# Liquid Waste Feed Sa mple Compos i te Data Sheet

Pr o je ct Na m e Veoll a - Sau get, ! L Oite 

### 1 01**a.~** 

## IB P

ro

j e ct Nu m b er 4094 2525. 2 0.02 Condition No. 1 Fa dilly Unlt 4 Run N o

### a.~**tr~am** Na me Liquid w as t e Feed ( L W F I S tar t lim e 

# la-37 Compos i te Samp le 10 VS4-lWf.1 i!-c O M!>M Stop Time 

## I US' Op era tor

Sample N umb or Time Volum e /Mass S a mple Number Time Volum e /Mass 1

### ~3"7 

# ;;oo hll.... 2 1 2

### \aos~ 22 3 

# \\OJ 23 4 

### tlU, 2 4 5

### 1~H**·** 

# .. 25 6 26 7 27 

### 8 2 8 9 29 

### 1 0 30 1l 3 1 12 3 2 13 

### 33 14 34 1S 35 1 6 

### 3 6 17 37 lll 38 

### 19 39 20**l~lvc ume** 

### ~.~oo 

# "''-

Comments: Co llect approp ria t e l y-sized a nd equa l & liquets and transfer Imm ed ia tely Int o a 4-Ut e r c ompo si t e j a r . Collect a separate SOO 

### mt bottle of sample a t eo ch sampl in& llme to be reta i n ed in ardllves.

## SI\10\0I~d**~(1)11\ )(~old.** 

### s\~**~t~ SI>S·o551.b-~C-Ito**  /&tii'NM l>ot.: JUM l'OJl 

# Ra

- !Uf'ClOIJ E· 4 02 

## VES013825

# Liquid Waste Feed Sample Composite Data Sheet
Project Name Veolf a - Sau se t I L Dat e 

## \ ()fa-4113 Project Number 40942525

. 2().<)2 Condition N o. 1 Facili ty U n it4 Run No 

# 0.\\ Stream Na me Liquid Wa ste Feed (LWFJ Start Time

### ~~n Composite Sample 1 0**VS4·LW F-l** **.COM ~**  Stop n me 

## \'iO? Operator

Sample Number Time Volume/Man Sample Num ber 

### Tome**Volume/~** 1

### ~S7 

## l ()() "'L. 21 2**I~U** 22 3 

## \l01 23 4**\'H.~** 

### 24 

## s l'U!i 25 6 

# 1na 26 7**\~07** 27 8**PI~** 

### 28 9 

### I 

## '43'7 29 

### 1 0 

### 1 

# 'in 30 11 

## l'r07 

## + 3 1 

### 12 32 

### 13 33 14 34 15 35 

### 16 36 17 3 7 

### 18 38 

### 19 39 

### 20 Final Volume 

## ?1 1 

## 100 ,..L,

Comm ents: Colloo approp rlitely-slze d and equa l allquots and trans f er Immed i ately Into a 4-Uter composite jar. Collect a separate soo ml bottle of ••mpl e at each samprons time to be retained in archives

.

## ~IC\gll'd tl'l)tr\

### y.~~**s~t(Q"'**

### ~U...,f-u.4.

## d·Pi·~f- 

## .. - 

# ,. ... A 

# v<>-4-

- 

# r..w F'

- -l'2. P.

- / ""**::t-~** 

### - 

## t>JP**SD$-0$51.0-~** CMipMI« bWsfwt Ottte :**J~~Z** 20./1 fl<y(<w<i/; J.-2013 E-403 

## VES013826

# Liquid Wa s te Feed Sample Composite Data She e t Proje ct N•m e V eo ila- SaUGet , tL Dat e 

### 10(0.'1 

## fl3 Pr oject Number 409415 25.2 <Hl2 CD oo rtion No

. 1 Fac ility Unit4 Run N o 

# a..s Stream N ame Uqu l d Was t e Fee d (LWF) Start Tim e

### ~l/ composit e S ample 1 0 IIS4-l WH &l .CO M P 

### _!S, Stop Tlme 

# \ 'i?.J Ope ro t o r

Sample Number Time Volume/Mass s.tnp!e Number Tl me Volume/Mass 1**10}.~** 

### 7 

# a.oo ... L 21 2 

## ll'W 22 3 

## l'\0 7 23 4**l)i).~** 

### 2 4 

## s nH · 25 6 

# nu 26 7 

## 1'\01 27 

### 8 

# 11tn 28 

### 9 

# I'll? 29 10**\'\\'"~** 30 11 

## 1,-ol 31 1 2 

## tU4 32 13 

## 1n1 

## _ ... 33 

### 14 34 15 3 5 16 36 17 37 18 38 

### 19 39 20 final Vo lume 

# a , c.oo ...**~.,** Comments : Co ll ett app ro p tfa t ely ·shed and e qua l aliq uots and tra ns f er Immediat ely Int o a 4 · Uie< composite jar

. Co ll ett a separa te SOO m l bottl e of sample a t e a c h sampl i ng time to be ret ai ned I n arch i v es
.

## ~""~\9d

# ~"'**1- i.~** **~~r@QI'\**

5()$-05 Sui>- S<IiyM Car .pD$1/o fb!g(siotf**/)of~** J lllt Z()Jt 

# R.- J- 20 1 3 E-4 04 

## V

E SOl382 7

# URS DAILY RECORD OF EVENTS

I """\ • I l l. ) I



### n

## ~ 

# Otf•tt**l, J**  

# (., ;! •. 

# a

r

l•**~~~** 

# •• , 1, )""" tl'-lfl

..... IUJ. 

# r. Lt.i, I,.HJ..A. 

# J·Ur "''d"J'

# ~"~'" '·•r•-!•Y**~of J'••"Y** **~~L-.,,..,** 

# SiF·**r{ .tt~**  'q

## foft'pl~• j ((. 

### h 

# "'J'• 

# r ff•""J•<•f/,-u!"·{·**~J~** 

# s-,. p.,,. 

# :r.**·~** 

# •• A t

.,,. h

... ,. ,.,. 3**~** 

### c .. 

## <1•14 lliO • .,.. 

# 11.,..**~A** 

### - 

# v,. 

# H**tiS~** 

# ft, ''" f.••**~A** 

## -**1/~** 

## I , 

# A>•**~.** 

## 6 ,. 1Lll\**~~.u,.lt(** 

### 11'?1(, 

# C.d lH.I- 

### S l'"l

### ~**~"I\~** 

## <-1**~** 

## 't% PV

. L**~~--~** 

## II!.J**~~\'\ 4~'1** **t\L\Ill~** 

## hq,,n**<.o,.pl~~~·,** ( tl l''\ <, n l\\vlr 

## Cr., r opl.A q \ 

## IIJ3'; 1'1'\ t 

### [..c)llr.c,l**~~>1\,.~** .<llo**jl•~** 

## c..1 " I"'"St P L> 

### L

### ~~~~ 

## IJJ 

# a**11.~**

## I~ II

## kt\11,1~ 

# hq,., I..Oo o\ltk ' 

## 1 

## LCJ\1tC.I ':xlmjllt

## Ct.**.pl.~** 

## q\ lbCr) 

### t\Ttl IT, 

## a,;d 

# fs**~** l'toh'"'UII'Iplf\l 1.\.1

### ll>fi~)J) 

### I 

## \'.i LO\lPQ 

## lit •U

### ~M**~\q_** 

## L\ 

## \l-nq7 

# Ph '-**~)** 

## 1 I d 

# I\"'**\~'i** I [h 

## qrd 

# rs**~{Q** If\ 

### I.Ot 'I 

### I 

# l I 

# Cot." \**~1'11t** t 

### Len 

## t ' Q 

## I II.?.') 1114 rt) 

# s .,(f llk3o 

## lo**~** 

## ' 

# !.t•- 'Q 

## \1)**~to** 

## 0•'1 c.l**1-1-~11** 

## tl:.'t• I l .,.,,,

# !t,~o Ttttl

# <•"'rl•1<~**j,.;~ts ~d"'~** **S"""' :**  tr 

# r./..15**~/~** 

# b: , • "**~** dw·

# /'{jf~;tr 

# f<i!"fks C"'"'('l•i<**'[oC~ .**  

# 1

# ~ 16

# ~~'"" • II 

# f"pcr

# tl•**·~** / Cu(.,

.

# ~-"" Cuc.f lo 

# l(iv.,; 

# He-6 ; ,., .**~~5~ 1**  {f,rtd 01\

## · 

# w••l

.... II ,f**lo~'"j** 

# dovL 

# c. ...., ,,**~h /l**  

# . .. 

# .t I ul 

## (04 ·

E-405 

## VES013828

## Field Balan c e Calib ration Check P

ro

j ect Nome

___**v;;e;;o;.:;li~a i:S;;au~g~e~t,;:'** **;;. l**  

### _ _ Project N umbe r
__**_.::.409= :.;2,52;5::;** **~40::..() 2**  

### _ _ Facility ----, ,-;.U;,;n:;it;:.3 :,.- - - 

### B

alance 1 0

_ _

# ..;.**'i .:....:.** **_:..; ;..;** **--**
Callb<otlon lniUals (Itt'> Chec)(ed by Dat e

### ~2.'5'**1~**



# ..........**~** 

# ... ......,,_ l$nce kad1nc 

# ..,..,_. w..;po" (!.-- Perc:tnt**o~·** ld lei**~MioO!ld** ld 20 

## tp.o 50 

# s:o.o**co ~rotloft**  Cbocl< of 

### e•nc. UNna Stvder.t 

### 100 

### 100. 0**welch~>** 

### 200 

### z_po . 0

St

udtnt W ei c h t S•t ID : 500 

## 5"00 • 

# l 

# Hl l r 'g 1000 I O DO

. 

### "2-.



### """""- ...;p...., .. ..,-**~** 

### .. ' • tho bolloc! -used toweiP ....-. .,...., ., .. 10001.- tho IIXlD ond 

# soo..-- lor , 

# ,_.,..co«<

• Tb kCJ; t tNI! aiWil for PftUI'!I: cflft!lnntl: It 

### .o.s • nw. .. c.ollnMc<l U5i!l&. this**~** 

### Percent 

# DUfee a • ba!anoe 

# =:'ma ss x 

### 100

&/JS·08D < Fkld 8•'-• C•Hbf'<IIIM hr EM SoP · OIO ll<wsiolt O.lc .' M....-IJil0/1 R

• "-- JIJ!y 1011

E-40 6 

## VES013829

# < t'l'1 Vl 0



# ..... 00 

### w 0 m 

# .. !:l 

## Sample 1 0 

## Code Stream

### ~S4-S$.13A.Qrno1 USc*ls

### ~54-BS. t3A.(;rab I USalcl$

### ~S4-8S-13M>rab 2 N:Salcl$ IVS4-es-t3M>rab 3 

### lUI Solds lvS4-Bs.t3A.(;rab

. fUI:SCllds

-**~~** 13Mlrab 5 

### lUI Said$

### ~S4-BS.**t3A.(;rab** 6 N:Scllds

- · · ""13A.(ltab 7 

### lUI Salcl$ 

### lvS4-IlS-13Mlr sb 8 

### Ill* Sob

### r.-s4-ll$-13~2A MSolds

### >~**'** 00 

### -13!l.Comp28**B~Sold s** 

### -B**S-13~2C** BUlk 

### Solid$ r-s4- I!S · 138-Gtab 1 Bt* Solds

### ~-8S.I3S.G**rab** 2 Bu lk 

### Solids V$4 -ll$
· 138-Grab 3 Bult Solids 

### V$4-Bs- 1 38-G rab 4 Bulk Sdids 

### VS4-BS·138-Gtab5 Bill Solidi 

### lvS4-Bs. 13B-Gr.!D 6**B~** 

### ScAlds V$4-SS-138-Gtab 7 

### illlllt Solids 

### lvS4-8S.138- Gr.ID 8 MSolids V$4-85-138-Gtab**~** 

### illllk Solids lvS4-IIs.138-Gr.!D 10 

### Ill* Solids lvS4-BS.138.(ltab 11 

### 9ult Solids 138-Gr.!D 1 2 lli*Solds

, ,..., "" 138-Gr.!D 13 

### 9tA1< Solids

### ~S.13B-Gr.!D ,. USCllds 

### Waste Sample 

## Logbook 

# Veolia-Sauget, IL

- Unit 4 CPT Project Number 40942510

. 20 Fract ion Cond 

## Run Date 

# nme**~** 1 

### 3A

### 0**~)~**



### An:iWe 

### 1 3A

### ~'\**?. E.**  NdWe 1 

### 3A 

### 0'\<tl Nrtitve 1 

### 3A 

## aOO(; Attt.iw> 1 

### 3A 

### I ()d.) 

### AlrtWe 1 3A

### 10**~** NrtM 1 

### 3A Atd:ive 1 

### 3A AII:Me 1 

### 3A l'llysiComp 

### 1 

### 38**~Yar,JS _** **~** Pllys/Corrc> ,**~** 

### 1 

### 38 

# lCM' Phys/Canp 

### 1 

### 3 8**I(,~E,** 

### Alehl\18 1 38**ll~** 

### An:hive 

### 1 

### 38

### ll~ Atchlve 1 

### 38

### ~~ Atchiw 

### 1 

### 3 8 

## I'll I Atchlve 

### 1 38 

## \'llf An:tllve 1 38

### 1~1 Atchlve 

### 1 38

# ·~ Arthlve I 38

### 1'5~1 Atd1lve 

### 1 38

### 16~6 Ardi

.. 

### 1 38 

## l'iJ Atd1lve 

### 1 38 

## K66 M:IM 1 

### 38

# ·~· Alr1We 

### 1 

### 38 

# .**~** M:IM 1 

### 38 Page 13 of 29



## TW GW 

## Comments

## -:l~~**~** 

## ql.\i**f,~~**

## t.**'t7~ ~~** **1~**

### 5'\**~ h_~O~** 



## 10 6 ,**1,£> ~**  

### __,**;1 9-~<1** **.** 

## l ,

l

..**~ ~~** **q** 

# 'Slli**a.Q~**

### ~'S8ct**111,~1'&** 

# -r:\_!1**~,~~ '6Cl** **\~~t a;~** **~~** 

# 1:.\h**a, s'\~** 

## 1~**\, \0,** **~**

### Eo~

## ~**~'ill, ,(.(\** **8~**

## 514**~ .!1** **8~ 5'3~** 

## ~~~**~~0 ~**  

# \**~:** 

# ..**a4~** 

## I_,!**&a ~** 

# '~**~ ~,** **,~**

# tii en 0 

# ...., 00 

### w 

# - Samp le 10 Code

"' ·**~~** 13A-Comp1 VS4·CS. 1 3A·Grnb 1

" "'**"~** 13A-Grab 2 VS+CS- 1 3A-G<ab 3 VS4·CS·13A-G r a

b 4 VS+CS-13A-Grlb 5 VS4-CS. 1 3A · Grab 6 VS4-CS · 13A-G<ab 7

\J<!A I'< 1 3A•GraiJ 8

### ~S4-CS**138~2A** ' "'**~~** 13S.Comp28**~S4-CS.138~ 2C**  VS+CS-138-Gtab 1 i'fS4-CS.136-Grab 2 VS4-CS.13B-G<eb3

### ~54-CS-138-G<ab 4 VS4 · CS. 1 38 -G rnb 5 VS4-CS-13fi.Giab 6**~S4-CS.13B-Grab** 7**~S4-CS.13B-Grnb** 8

### ~54-CS-138-Gtab 

### 9 V

S

4·CS· 138-Grab 10 VS4-CS-1JB.Gaob 11**~CS.13B-Grab** 12 VS4-CS ·13 B-G<eb 13 'JS4.CS- 1 38-Grab 14 

### Stream**~Sclids** Coolalnerized Solids C<Jllalnerized 

### Solds Coolllinerized Sclids Con lalnerlz ed S<lllds 

### Contamtzed 

### Solds Coo lalneriz ed Solids 

### Conlalnerized So41ds C<Jllaineriz ed 

### &lQds Ccnlainelized ScCJds Continerized 

### Solds C

ontai neri zed Sef i ds Coolalnerized Solids Coollllneriled Soids 

### Containerized Solids Cootainerized Sold! Conta l nelized So li ds Coolailerized Solids Contllnerlzed S<lllds Ccnlalneri zed Solids Conlainefized 

### Solids Conta i nelized Solids Cootanemed Solids Contalnelized 

### Solids Cootainerized So l ids C<Jllalneri2ed 

### Solids 

## Waste Sam pl e Logbook 

# V eo li a-Sa u ge t , IL

- Un it 4 C PT Project N umber 40942510.20 Fr action 

### Cond Run 

### Date 

### T i me**~** 1 3A 

### "'Q,t., 10,.. Arc:hiYe 1 

### 3A

### <J\~ AroNve 1 3A

## ~'50 Archive 1 3A**~()~** Archive 1 3A**~** 

### Arr:Hve 1 3A 

### l0\0 Archive 1 3A 

### Ardllve 1 3A 

### Arctil-e 1 3A 

### PhysiColrll 1 38 

# '·· I'B'i'**~.Melals** 

### 1 

### 39**I~** 

### Phys/C omp 1 3B 

## IUS' Arc:l1i'le 1 39 

## I'U! ArchMI 1 

### 3B 

## tl'JO Arc:h ive 1 3 B 

### I 

# 'to'S ArrJiole 1 3B 

### tctao Archive 1 

### 38

### l't~ ArohM! 1 3B

### !It~ ArthiYe 1 3B 

## 1'5W ArChive 1 38

### l'f~ ArohiYe 1 38 

# lflS" Arell lvo 1 38 

# •m Archive 

### 1 3B 

# 1&06 Arthive 1 38 

## IWO ArChive 1 

### 9 8**~** 

# \taf Arthive 1 38 

### TW GW 

### Comments

### TJ**C\ ~tn-:"** 

### ~'-**~** 

## .l,Cl'iO <\

# ~'"' '13. 

# i I 

## , 1.\Ba(\**'\~~~**

## ~.~~ 'i;)3tA 

# c,c ·**lpcJ.~**

### 5~ ?Oj

### I.a.~~~



# as**I\~ 3.~~** **,~** 

# ;a**~-** 

# '3a.**~** 

# a.<:m' 'S()fA IQ.. \I 

# no Cll

### ll~a<i 

## l<> :,**1,~ 3.~~** 

## ~ 

# • .**,1\~ m~:,** 

# 10~**'·~~~ 'iOC~** 

## ·**~~**



## 'SifG**8~;** 

## l,'iO'\c:; 

# Sl§**<t''t~ ,87·~** 

## ~ l Qq j

# ·~~~**~~ 1!4\** **~ 1,30S~** 

### ~~<1**~.., »l~** 

## ~El!C\**~'lj 1,1~,** **s~**

### lq**~~** 

## 't'l'l C\

# < m (J} 0 

### '-' 00 

### '-' N 

### Sample 10 Code

### ~S4-l8\'**~1**



### ... .. "".t- llMlnb 1**~** 

### RW

. Il,t,-Gr*> 2 

### lv<:...o

- -1 3A-Gtab 3**~v.,..,...,,JMlnb<** 

### iv<:...o "W·13A-Gr*> 5

### ~W·I3A-Grab6 lv<:...o ""'-**~~** 7

### ~S4-LBW-13A**·Grab8** 

### iv<:...o "W· 138-Ccrrp21\



# - 13&-Comp28

### lvS4-**LBW 13B~2C** **~** 

### RW.1J8.Gtab 1

### ~W·13B**Grab** 2 lvS4-lBW · 130.{;rab 3 

### iv<:...o RW

. 

### I JB.Grab 4 VS44..B W

- 1 38-Grab 5 jvs+ulw

- 1 38-Grab s """" ' ""' · I JB.Qab 7 VS4-I.BW · 13B-Grab8

### 1'1**-138-Giab** 9**~** 

### RW.IJB.Qab 10 VS4-l.BW

- 

### 1 38-Grab 11

""'

. • .... 1JB.Gr.lb 12 

### b.. RW.1J8.Gtab 13

### ~$4-lBW-139-Grab ,. 

### Stream Low 

### Bw Uquid 

### W asil lDw lll.o 

### Up!**Was~&** lDw 

### BIU Uquid 

### W

### Low Btl Uquid 

# wLow lll.o 

### Up! Wasllt low BIU Uquid 

### W asllt Low BIU Lip! 

### Wasm**LowBIU~~** 

### low BIU ll"'id**Wa ~**  

### Low BIU Uquid 

### Wasll! Low BIU UquidWasle low 

### Bill Uquid Wasil! low 

### Bill Uquid 

# wlow Btu**~ld** 

### w aste l ow Btu l i quid W as t

o low 

### Btu Liquid 

### W asla low Btu**~id** 

### Wasle low 

### BIU**ll ~**  

### Waste low lll.o 

### Uquid 

### Waste 

### Low BW Liquid WilSie low 

### Bill Liquid 

### WLow BIU Uquid 

### Waste Low 

### BW**~id** 

### W3SI8 Low BIU Uqud Wasil 

### Low 

### lll.l Uquid 

# wLow 

### Bill Uqw l Waste 

## Waste Sample Logbook Pege 13of16 

# V eo lla-S au g et, ll

- Un i t 4 C PT Proj ec t N umber 40942525

. 20 Fraction Cond Run 

### Date 

### Time TW G W Comments

# ""~ 1 

### 3A 

# "M. l OlS'**.L 'S110** **~**

AldWe 1 3A

### ~~ 

## '5 foe)

_ "ll. MJWe 

### I 3A**oq~** 

### MJWe 1 

### 3A 

## I I 

## OO'f MtfNe 

### I 3A**I~** AtrJiNe 

### 1 

### 3A**~** 

### 10\$'


## ... Aictive I 

### 3A kttive 

### I 

### 3A All:hive 1 

### 3A PhysK:omp 

### 1 38

## ~Ia 

## t'4W**il;'500~ Mel;als**  

### 1 38 

### IE.Qf 

## 1,lOO

.. t.

# ""~ 1 38**6~**

### ~.~ 

# ...**~.** An:tt;e 

### 1 38 

## J'Uf' 61)0 ""' Archive 

### 1 

### 38 

## 1 »0 Arcl\lve 

### 1 

### 38 

# J'tof Atthive 

### 1 38 

## t CfiO Arclive 

### I 

### 38 

## lCI» Archive 

### 1 38 N'S() MtfNe 

### I 38 

# ISOS A rchive 

### 1 

### 38

### I~ Archive 

### I 38 

# •mMir-e 1 

### 38 

## )Sf() Archive 

### 1 38 

# L40r .t.'dM 

### I 

### 38**I~** .t.'ltliYe 

### I 

### 38 

# ... ''***~** 

# .. Arclive 

### 1 

### 33

## Was te Sampl e Logbook Page 5of16 

# Veolia-Sauget , IL

- Unit 4 C PT Project Number 4 09-42525.20 Sample 10 Code Stream 

### Fraction 

## Cond Run 

### Date 

### Time TW GW Comme nts**•~** un 

### llA-Ccnlll**~** 

### Ba11.41<1 

## w.a**~** 1 3A

## ~.**~ lrl~** **'5oO** 

## .. l IJA .(lQb I**~** Ball.lqiAcl Wasut 

### AAme I 3A 

# j() q,(, 1$00 "'-**~QW.I3Minlb2 ttg~**  

### Bill IJqiAcl 

# w- lvrJWe 1 3A 

# jo<\ fl f.ls.uiBW·IJA.(lQbJ**~** 

### Bill UqUd Waste 

### lvrJWe 1 3A 

## oof.**~8W-13A.(lQb4 ~**  

### 8a.t UqrJd Wasle 

### lvrJWe 1 3A 

## tOi-l lvs.uiBW-13A.(lQb 5 High 

### Blu IJqiAcl Wos1e 

### lvrJWe 1 3A 

# ....**I~** 

### ....L.**iv~BW 13A.(lQb**  S High 8tr Uquid Wasle 

### AltiM 1 3A 

# ....**~SW I3A-Grall7**  H;j>Blu 

### liquid Waste Ald1M! 1 3A VS4-HBW · 1JA-Gtlb 

## a Hlglllllu Liquid 

### WoJSle AltiM 1 3A 

## 1- 

# - - 

# - --- -...

## ·~· ""W.138-<:omp2A High BIU liquid Wos1e 

### PllJSICarll 1 JB

### I'~J 

# .. l '\3f**.~** 

# ...**~...** VS4-HBW·138-Comp28 Higtl 

### Bill Llqllld Wasle**Physl~.** Mela!s 1 

### J8 

## 140b 

# , , 300

.... 1**~BW·1JB.C4mp2C** High BIU**llq~** 

### Waste**~** I 

### J8 

## l&,E.**&.,la co** **~** VS4-M8W·13B-Grlll1 High 

### Bill**Llq~ld** Wasto An:ll!lle I 

### J8**,~** 

# ..**~OO** 

### ... L. jvsol.HBW·138.Qab 2 

### Higtl BIU**llq~** Waste An:ll!lle 1 

### 3B 

### ll'S 

### I V$4-HBW-13 8 -Grab 3 H igh BIU Liquid Waste An:ll lve 1 

### 3B 

## \1\0' lvS4-HBV1 · 138·Gtab 4 

### Hlg1 BIU Liql.id Waste 

### AldlM! 1 38 

# ,,.., VS4-H8W·13S.Gtob 5 High B:u Liquid Wasle 

### Ard1!11e 1 

### 3B 

## 1'4lf**~BW·I38-Gfab6 tf9\81UL~Was1B**  

### An:lwYe 1 38**l't~** 

## I f.IS4-HBW-13&<1rlob 7 Hlgilfllu Llql.id Wa51e An:lllve 1 38**~~** lvSoi-HBW-138-Grall& High BIU 

### lkJJ!d Was NciM 1 3B

### l~\ f./$4-HBW-138-Gtat> 9 HlgiiBOJ Llql.id Waste M:lllve 

### 1 3B 

# """' jvs4-HBW- 138-Grall10 

### Hll;tl 

### Bil1.41<1 wage 

### An:lwYe 1 38

### \~'1 

# Z' lv54-H8W-138-Gtatl 11 High Bill 

### llql.id Wa51e Aldllve 1 

### 3B

### ~ 

# < 0 ITl (/) 0 

# -

....**~81V 138-Gtatl12**  Higll Bill 

### UqrJd Was>e 

### A.'tt.lw 1 38

### 1~\**~BW·138-Gtatl** 13 Hlgll BOJ**~Waste** AlftiNe 1 

### 3B 

# - IQl. 

## .J:

· 1



### J8.Gtab 14 ltgl BIU 

## 1.4111 Wil$111 

### lvrJWe 1 

### 38 

# - -· 

# - - 00 w w

# < m 

## en 0 

### w 00

### ~ S ample 1 0 C od o**~Wf·1~1** jvsA.I.WF · 1l-'.Qnb 1

### ~WF·134-Grab 2 jvsA.I.WF·1JA.Grlb 3 VS4-tWF·134-Grab 4

### ~Wf·13A-Grab5 VS4-tWF·13A-Grab 6

### ~WF·13A-Grab 7 jvsA.I.WF·13A-Grab 8 VS4-LWF·138.ccntp2A 

## jvs4.l. WF·138-Colr!>2ll VS4·LWF-138.Cctrll2C jvs4-LWF-138-Grab 1 !v*WF·13s.Gtab 2 jvS4-LW F

·138-Grab 3

### ~WF·138-GI1b. VS4-LWF-138·Grab 5 

# jVS4-l. Wf· 138-Grab 6

### ~54-tWF-13&-Gr.lb 7 !'JS4-l.Wf·138-Grab 8

### ~WF·1J8.G-1b9 VS4-tWF·138-Grab 10

### ~S4tWF·138-Grab 11 jvs4-l.WF·138.(3rab 12

### ~Wf·138-Grab 13**~WF· 3a-Gnl>**  

### 14 

### S tr eam 

### l.ll!uld 

## wz:a Feed UqUd Was!e F* UqUd Wale 

### Feed UqUdW-Feed UqUdWaslefeed UqUd Wasil Feed UqiAd 

### Was18 Feed UqUd Vlw.e 

### Feed UqUdWamF* Uquld Wasle Feed UqUd W.W 

### Feed Uquld Waste Feed Uquld 

### Was:a Feed LiqUid 

### Waste F* LIQuid IVOSUl Feed 

### UqUd Wasle Feed Uquld W a ste Feed Uquld 

### Wasta Feed Uquld Wasle Feed Uquld Wasle Feed Uquld 

### Wasle Fted Uquld WaS1e Feed Liquid 

### Was18 Feed Liquid 

### WaslB Feed UqUd Wasle Feed UqUdWas18Feed 

## Was t e Sample Logbook 

# V eolia -S auge t , IL

- Un it 4 C PT Project Number Ml942510.20 Fra c ti o n Cond 

### Ru n D ate 

### Ti me**~** 

### 1 :1-' 

# !""

.. ,, ,**o~J** An:hM! 

### 1 :1-' 

## I<R!7 MtM 1 :1-'**~,~** 

### AlrHte 1 3A 

### 100? Nttive 

### 1 3A**~oM'.** Nfjtve 

### 1 3A**~** 

### 1017 AldWe 

### 1 

### 3A AldM I 

### 3A 

# - -

- A:ciWe 1 

### 3A Ph)'S/Conl> I 

### 38 

# r- , ,, I'QS"**Ph~ ~**  

### 1 

### 38 

## 1(,01 PhY'fCo<r!> 

### 1 38**,.,~,**



### Archlva 

### 1 38

### 1~7 Atehive 

### 1 

### 38 

# 11¥ Arch i ve 

### 1 

### 38 

## 11.\0., Atr:Nve 1 38

# ·~ Arehlve 

### 1 

### 38**\~** 

### Arehlve 1 38 

## r'lU AteiWe 

### 1 3B**,~,** 

### Archive 

### 1 

### 38

### \~ MtM 1 3B 

## 1$}7 Archlva 

### 1 38 

## 1m Atdive 

### 1 3B 

## l{t)7 Mme 1 

### 38

# ·~ Mme 1 38 .t-

### 1~17 Aldwe 1 3S 

# -**P~e5of29**



### TW GW Co m ments

# ~ ' '500 "' I..**~00** 

### .. ...



### .I-



# -

• •**10()~ ~,!00**  

## .. 1..

## -.~..L

iO() " '- 

### I 

### f

I

I

I 

# .l.

## Waste Sample Logbo o k Po g e 15 of29 

# V eo lia-Sauget , IL • Un it 4 CPT Pr oject Numb e r 40942510

. 20 Sample 10 Code St ream Fraction 

### Cond R un Date 

### Time 

### TW GW Comment s**·~·** 

### ... 14A-Ccn:c>1 &*Solds**~** 

### 1 4A

.... lrl 

# llfl 1.?31"' k"' ' "" 14A-Gfab I &*Sdids Atdiw 

### 1 4A 

### l()'f 

# S?a," I I

### ?,~7"'**~~ '**  eo 

### 14A-Grlll 2 S.Solds Atdiw 

### 1 4A 

### II**!~(a ,**  

# .. 1 ,\3\o. 14A-Grlll3 8ult Scllds An:IM 

### I 4A 

### 11

.. \**1N~o.** 

# 1, EM>q 14A.Gni>4 S.Sclds 

### Nrme 1 

### 4A 

## \\lG**E,"J~~** 

# l ,Etl'i (11



## , .,**14A~5** &*Scllds 

### lvtme 

### 1 4A 

# ..L ll fl**~l o.**  

# . . .,a , a 14A.Gnb 6 

### IliA Scllds AldM 

### 1 4A 

# 1\ /**~BS.14A-Glab** 7**~lk** Sdids 

### .Ait:tM 1 4A 

# ."' 7**""'"'' 1~8**  Ill* 

### Solids NdWe 

### 1 

### 4A 

# "' J ivs+SS.146-Ccmp2A 

### 81Ak Sdids**~** 

### 1 

### 48 

# """ 7**jvs.t.as-1~28** BUlk Solids**Ph~.Me~als** 

### 1 

### 48 

# "' /**lv~-Bs.** 

### HB-Cornp2C BlAk Sclds**Phys.~** 

### 1 

### 48 

# "' 7**IIS4-8S.1~** 

### 1**Bui~S~** 

### Atehive 1 48 

# "' / IIS4-6S-148-Giill> 2 

### 8'* Soids Archive 

### 1 48 

# 1 "".. / VSL8S.148-(lra!> 3 Bu lk Solid$ ArthNe 

### 1 

### 48 

# """"**~Bs-148-Giab** 4 Bulk Solds Arthi'le 

### I 48 

# 7' VSL8S.148-(lrab 5 Bulk 

### Solids Arctm 

### 1 48 

# / 

# """ ivs+Bs-148-Giab 8 

### 8'* Solids Ald!ive 

### 1 

### 48 

# v 

# " VS4-Bs-14B-Grab 

### 1 Bulk Solids 

### Archive 1 48 

# / 

# "' lvs+es-148-Giab 

## a BIAI<Sclds 

### Arcl'iVe 1 

### 48 

# / 

# '\**VS4-Bs-1~** 

### 9 

### l!ullt Solids 

### A«me 1 

### 48 

# / "'\ i'J$o4-Bs.148-Giab 10 

### BlAkSolds Atti1MI 

### 1 48 

### / 

# '\..**~So4-Bs-1~** 11 &*Solds Atti1MI 

### 1 

### 48 

# / 

# .""

. ... 1 48-Giab 12 

### MSolds An:IM 

### 1 48 

# v 

# "'**lvS4-Bs-1~** 

### 13 

### l!ullt Solds Ndllve 

### 1 48 

# / 

# \.

.... 148-Giab 14 IIUic Solds 

### AtdWa 1 48 

# 1 /

## W ast e Sample Lo gboo k Page 23 o f 29 

# Veolia-Sa u get, I L

- Unit 4 CPT P r o jec t N u m b er 4 094 25 10

. 20 Sam p le 1 0 

## Co d e Stream Fr acti on Cond 

## R un Date Tlme 

### lW 

### G W 

## Com me n t s**lv~1~1** 

### Codao•W>d Sal4s**~** 

### 1 4A 

# " ' 0**~** 

# iVs4·CS- 14A-Gial> 1 

### COl iCJIII(!ftzed Sal4s 

### AtttM 

### 1 4A

# ·**~ 5'** **~** 

# 7t, ·.**10~<\** VSI-CS-14A-G!al> 2**~Sdldl** NrJ:M 

### 1 4A 

## 0 05**S"l ~** **~~** 

# l , an co 1 4

A-G!al>3 COialn•lzel Sal4s NritYe 

### 1 4A 1 10()

## 7'\**~ ~**  

# ·,**~~~ (."** **1~ 4**  Ccr1lainellzed 

### S:lllls 

### Mme 1 4A 

# "''"**~ ·.** **\~1\** .. 14A-Gral> s COiitaoeized Sclds**Atdl.~** 1 4A 

# """**II~** 

## l);l5 "1 

# n ct j**rJO ~** **WI~·** 

### 14A-G!al>6 Conlainlrlzed 

### Sdldl AldWe 

### 1 

# "" I'-. 

# -,
14A-Gral> 7 C<lnlalnerized Solids 

### Arrffle 1 <lA 

# ..... 

# 7 lvS+CS-14A-Grab 8 CallillnetlzAid**~** 

### Archive 

### 1 

# "" 

# "' / VS4-CS-1 4B-Comp2A**~Solids** 

### P liys/Comp 1 

### 48 

# / jvs4-CS-148.¢oal>2B Contalnellzed Solids**~,p,Melals** 1 48 

# " / lvS4-cS-1 4 S.Comp2C Conllonertzed Sclds**Phy~** 

### 1 48 

# '\. 

# 7 jvS4-CS- 148-G! ab 1 Containerized Solids Archive 

### 1 4B 

# / lvS4-CS. 148-Grab 2 Con1anertzed 

### Sclds Arci1Ne 

### 1 48 

# '\. 

# 7 lvs 4-cs- 1 48-Grnb 3 Co"talnerized 

### Solids Archive 

### 1 4B 

# "" / lvS4-cS. 1 4B-Grab 4 Coolalncrized 

### Solds Archive 

### 1 48 

# ' [7 V$4- C S- 1 4 8-Grnb 5 Conlalnof1zed 

### Solidi Arclllve 

### 1 48 

# I 

# "' lvS4-cS-1 48-Grab 6 Cot1cDinert!ed 

### Sclcls Artlllw 1 

### 48 

# 7 

# "' lvS4-CS-1 48-Grab 7 Containeriz ed Sclllds An::ili ve 1 

### 4B 

### / 

# "'**~S-1 48-Gtab**  8 

### Con!M\ertzed 

### Sdlcls Archive I 

### 48 

# \..**jvSl-CS-1~b** 

### 9 Contafncrized 

### Solkb Archive 

### 1 48 

# / 

# '**lu.~ r~**  

### 1 48-Qal> 

### 10 COIIIIinerized 

### Sc:lcls Archive I 

### 48 

## ' 

# ""
rn 

# : < w jvS<-CS-148-G!ab 

### 1 1 Conllilleriad Sclds Archive 

### 1 48 /

## ~**1~12** 

### COI,._tud 

### Sdlcls Archive I 48 

# / 

# "' ('1'1 tl.l ""'

### "'**1~13** CotltJIMrtzed Sclcls Atc1M I 

### 48 / 

# '\ 0 

# - ..., •w**~'<'1~1 4**  

### Contanartzed 

### Sclds Archive 

### 1 48 

# 1 / 

# ' 00 

# ..., 0>

# < m en 0 

### Sampl e 10 Code**VS4-LBW·14A~1** VS4-I.BW-14A-Grab 1**~** - · 1<1A-Grab 2 lll:L.I R\'1-14A-Grab 3 VS4-LBW·14A-Grab4 VS4-LBW-14A-Grab 5 VS4-LBW·14A-Grab 6 VS4-LBW-14A·G r at> 7 VS4UW·14A-Grab 8**VS4UW·1~ VS4-l.SW.1~29** **~AW.1~** VS4-LBW· 1 48-Grab 1**V~LBW-148-Gr.lb** 2 VS4-LBW

- 14 8-Grab 3 VS4-LBW-1 4B ·G rab 4 VS4-LBW · 14B-Grab 5 VS4UW

- 146-Grab 6
vc:.u --148-Grab 7 iVS4 -t BW•148-Gtab 8

### ~BW**148-Gra b**  9 VS4-tBW·14B·Gr.lb 10 VS4-LBW · 148-Gtab 1 1 VS4-LBW·148-Grab 12 VS4UW · 146-Grab 13

### ~W-146-Grab 14 

### Stream Low Bll Uquld Waste lowBli UquldWasle 

### Low B!U UqlidWasto 

### Low Bll Uquid Wasle Low 

### Bill Uqlid waste Low 

### Bill Liquid Waste low 

### Btu Uquia W as te 

### Low Bill Uquid Waste low 

### Btl Uquid Waste Low B!U Uquid Waste low 

### Btl Uqlid Wasle low Btu Llquld Wasle Low B!U UQ\Jllj 

### W.. Low ew Uq!MI Waste 

### Low B ill Liqu id W aste Low B !U Uquld Waste 

### low Btullquld Waste low 

### Btu Uquitl Waste 

### Low 8!U Liquid Wasla 

### Low 8!U Uquld Wasle Low Btu 

### Uquld Waslil Low 

### Btu Liquid Waste 

### LowBtullquldWaste 

### low Btu Liquid Wasle Low BW Liquid Waste low 

### 8lu l.iquid Wasle 

## Waste Sample LogJtook 

# V eo l ia -S a u ge t , IL - U nit 4 CPT Project Numbe r 40942525

. 20 Fra c tion Cond Run 

### Date 

### T i me lW Phys/Comp 1 4A 

# ''IG \\6'0

AlrJWe 1 4A 

### 10,0 An:l1lve 1 4A**\1()~** 

### AlrJWe 1 4A

### ~~~~ AlrJWe 1 4A 

## IIJS Artlllve 1 4A 

# ..... 11'50 Artll i ve 1 4A 

# " Ardlive 1 4 A 

# " Artllfve 1 4 A 

# "' Pltys/C<lmp 

# , 4B 

# " F'hys/Comp , Metals 1 4B 

# "' PIJ)'SIComp 1 4B 

# ""'-

Arclive 1 4B 

# " Archive 1 4B A

rth i ve I 4B Arclllve 1 4B Atthlve 1 48 Atthlvo 1 4B AldM I 4B 

# / An:hive 1 

### 48 

# / An:hlve 1 4B 

# I AtchiY(l 1 

### 48 

# / Arl:h!ve 1 4B 

# / Atchlve 1 48 

## / Atchlve 1 

### 4B 

# / Ard1iYe 1 4B 

# / { Page 15of16



### GW Comments 

# z.5oo ....-\ <;()() 

### "L



# ... / / 

# I I / 

# / 

# ' / ' 

# /

' · 

# ',, 

# v L , 

# / 

# " v 

# "' ""'- 

# " '\ \.,_ 

# '\ \ \

## Waste Sample Logbook PBge 7 of16 

# Veolia-Sauget , IL

- 

# Unit 4 CPT Project Number 40942525.20 Sample 10 Code Strea m Fraction 

### Cond R un Date 

### Time TW 

### GW Comments VS4-Ii6W- 1

. 4A

.Qln1 p1**~Uqu idW** **as le**  Pl1y!IC<Im p 1 4A

### J,, liS) 

## 3. , 91Q.,.L VS4-Ii BW-1 4A-Gmb 1 High 

# ew Uqui! 

### Was1e**~** 1 4A 

### I O'i**~OO"' L**  V$4-li BW· 

### W.-Grab 2 Hig h 

### Btu U1 1id 

### Was1e Althive 1 4A**ll ~**  V

S4-HB W · 14A -Gn!b 3 H igh Btu Liquid Wasle A rch ive 1 4 A 

### II 

# a.+ VS4-IiBW-14A.Gnlb 4 Hlgh Bill LqlidW 3518**~** 1 4A**,,~,** \ls4.H B W

- 14A-Gnlb 5 High 

### B1u Liquid Wasle Nctr.e 1 4A 

# ... 1151



# _ ..., V

S4-H BW-14A -Grab 6 Hig h Btu Liquid Wasle 

### Althlve 1 

### 4A 

# """ /

• ' VS4- HBW-14A .Qab 7 H igh Btu Liqui d Waste A rch ive 1 4A 

# r-.. 

# /

"" ·**u~** · 14A.Gnlb8 

### High 

### Btu l.iqoid Wasle 

### AtdWe 1 

### 4A 

# "

. / VS4-If B W

- 148-Comp2A High B tu U quid**Wa~** 

### Phys/Comp 1 4B 

# / V

S4-H BW

- 14 8-Cort1' 2B High Btu Uq\Ad Wasle 

### Phys iCOII '9, Metals 1 

### 48 

# ""' / VS4-H BW

- 14 B.Qln1p2C H igh 

### Btu Liquid Was te 

### Phys/Comp 1 4B 

# / V

S4-IfBW-148-Gr.lb 1 H igh 

### Blu l.iqoid Wasle M:J:Cve 1 4B 

# L VS4-If B W·1 4B ·Gr.l b 2 H i gh B1u Liqlid W asle An:live 

# ' 48 ' 

# / ' V$4-H BW

- 1 48 -Gmb 3 High 

### Btu U1 1i d Wast e 

### Archive 1 4B 

# ' , / VS4-IfBW · 1 4 8-Gtab 4 H igh Btu**~id** W aste 

### An:hive 1 4B 

# /


# . VS4-HS W- t48-Gnlb 5 High B:U 

### liquid Waste 

### ArdiNe 1 48 

# / ' VS4-If 8W

- 148- G r ab 6 H igh Btu L iq lid**wa ~**  An:hi\ '8 1 4B 

## / ' VS4-If BW. I A 8-G r ab 

### 1 Hig h 

### 8lu U1uid WastD 

### Archi ve 1 48 

# / V$4-liBW-1 4 8-Gtab 8 High 

### Blu l.iqoid Waste MJ:r;e 1 4B 

# / ' VS4-H S W

- 14B.Qab 9 High Btu Llqui.d W aste Arel1ive 1 

### 48 

### / 

# ' ' , V

S4-HBW-14B · Gr.lb 1 0 High Btu Uqlid Wa ste A tehive 1 

### 4 8 

# /_ 

# '\

m



### .... VS4-If8 W- 14B-Gmb 1 1 High 

### Btu Uquld W as lll 

### ArtN ve 1 

### 48 

# v '\. < ;;; VS4-Ii8 W. 1 48-Grab 12 High 

### Blu l.iqoid W 3Sie 

### ArdiNe 1 

### 48 

# / 

# \. m f/} 0 

# - v.> VS4-HBW · 14 EI-G t ab 13 High B tu Liq uid 

### Wasle Archive 1 4B 

# I 

# ' VS4-H B W· 1 4B · Grab 1 4 High B tu 

### li quid Wa s l a Ate hlve 

### 1 

### 48 

# L 00 w 00

# < m en 0 <.> 00 

### w 

# "' Sample 10 Code

### jvutWF-~1**~WF-141.Grab** 1

### ~WF·1"'.GGII> 2 jvS4-LWF·14A.()Qb 3 tvutWF· 1 4A-Gn!b 4

### ~WF-14MlhbS**~WF-14A-<bb** 

### 6

### ~Wf-14Minb 7**~WF-1 4A-Grab**  

### 8 lv mw F- 1411-Con1l2A

### lvS4-t.WF-1~**V. 'F-1~2C**  ivsH WF ·1 48-Gnlll 1 VS4-lWF· 14B- Gn!b 2 lvSHWF· 14B ·G rab 3 lv S4-lWF ·1 48-Grab 4 lvS4-t.WF·I48-Grab 5

### ~-lWF**-1 48.Q'ab**  6 VS4-lWF-148-Gnlb 7 VS4-lWF·1 4 B-Grab 8 i"S4-t.Wf·14B-Grab 9**~WF-14Grlb** 

### 10

### ~Wf-148-Grabll**~WF-14&-Grlll** 

### 12

### ~WF-148-Grab 13

### ~WF-148-Gnlll1**4** S t ream 

## Lt!l*l 

# w- Feed 

### UqoJd 'II- 

### Feed Liquid W asle 

### Feed Uquld 

### WIISIII Feed**UqoJd~F eed**  

### UqoJd 

# was-. Feed 

### Liquid 

# was-. Feed Uqu'4 Weste Feed Liquid WM!e F eed Liquid Waste F eed Liquid 

### waste Feed 

### UqUd W3s1e Feed i.lqiAcS 

### Waste Feed Uqukl W os te Feed Uqu l d Wa ste Feed Liquid W aste Feed 

### l.lquid Wasle Feed Liquid Wasle Feed 

### l.lquid Wasle Feed Uquld Wasle Feed Uqllld Wasle Feed 

### Uqukl Wasle 

### Feed Uqukl 

### waste Feed Liquid W3Sie feed 

### UquldWastafeed 

### Uquld Waste Feed 

## Waste Sample Logbook 

# Veolia-Sauget , IL

- Unit 4 CPT Pr o je c t Nu m ber 4094 2 51 0.20 F r action Cond 

## Run Date 

## Time TW**~** 

### 1 4A 

# "'*'• 110

Att:hNe 

### 1 4A

### \}O**"J~** Ndive 

### 1 4A 

## \107 Ardive 

### 1 4A 

# lla.o. Att:hNe 

### 1 4A 

## \1 37 Arri:lft 

### 1 4A

### '.**~** 

# "'* l><dM 

### 1 4A 

# " AA:hf.le 1 

### 4A AlrtWe 

### 1 4A**Ph~** 

### 1 48 

### Phys/Cornp , Me!ab 

### 1 

### 48**~** 

### 1 

### 48 AtdWe 

### 1 48 Atctive 

### 1 48 Atchive 

### 1 48 Archive 

### 1 

### 49 AtciWe 

### 1 48 Att:hNe 

# , 48 

### Altl1iVe 1 48 

### Atctwve 

### 1 48 Atcli';e 

# , 48 

# / Atclive I 

### 48 

# v hrtiiO I 

### 48 

# / Atclive 

### I 

### 48 

# v Atclive 

### I 

### 48 

# / Atclive 1 48 

# 1 / Page Tof'Z!J



### GW Comments 

## 'l5CO..L 'SO O "' L



## .L. 

## / 

# / 

# 7 / 

# / 

# / 

# 7 / / 

# i/ 

# 7 / 

# 7
/ 

# '

, 

## .

... 

# "-.: '\. \

# < m 

## en 0 

### w 00 

# ... 0 

### Sample 10 Code 

### M:Lr.t**·11~** 

### I**118-GIIb** 

### 2 I\IS4-Cl · IIB-Gtab 3 !Vl:O.t'1.11 8-Gllb 4 

### "-roo ·12B.Qab 1**~· 2&G'Ib2**  

### tvs..a..I28-GIIb 3 VS4-Cl · I28-GIIb 4 jvs4-CL· l 

### J8.Grab I 

### VS4-CI. ·138-Grab 2 VS4.Q.· 1 38-Gnlb 3 lvS4-Cl·138-Gnl> 4 jvS4-CL·I 48-GIIb 1 jvS4-Cl · 148-Grab 2 VS4 · C l · 14 B-G r ab 3 VS4-Cl· 14 9 -Gr ab 4 

### S tream**CNcme~M:I CNcme~MI** **atme~M:I** 

### Ctloc1ne SpiiOOg 

### Mtl Cl*xfno**~** 

### ll.ll**atme~MI** 

### Cl1larl:le**~** 

### M:f**atme~Mtl** 

### Chtome Sp'l$ng 

### Mil 

### Clllotlne Splldng M d**C!Qine~MI** 

### atme Spldng 

### tAll Olloftne 

### Splldng Mil 

### Chlorine Splldng Mil 

### C

h lorine Spll< l ng Mil Chlorine Spiking 

### MS 

## Waste Sa

. mp l e Logbook Poge 25 of 29 

# V e oli a- S a u ge t , IL • U nit 4 C PT Project Numbe

. r 

## 40942 5 10 .20 Frac ti on 

### Cond 

## Run Date 

## TIII19 TW G W Comments AldiYe 1 

### 18 

# I',B**~** hrJiye 

### 1 IS**·~o** Alrtjye 1 

### 1 8 

### l 'SI 

## 'J AlrJWe 1 18 •"- 

# ' " ") AI1::IM 1 

### 28 

## r v'

• '1tt**~,,** 

### MJiNe 1 28 

### I 

# 1 m AI1::IM 1 28 l 'il7 tvcme 1 

### 28

### ~ 

## 1'5 '1 7 Archillll 

### 1 38 

# rc-A l 3)' Archive 

### 1 

### 38 

## 1 '43<. Nrfue 

### 1 38 

# ii Wi NrJWe 

### I 38 I

. 

## 1 4>'\3 Ardll"..e 

### 1 48 

### Ardlillll 

### 1 49 Archive 1 4 8 

### AJchi>.., 1 

### 4B

# < m en 0



# .....**~** Sa m p le 1 0 Co d e**~B-118-Giab** 1 lvS4-PB-119-Q&b2**~** 

### ..

, "" 118-Giab 3 118-Giab 4**V~128-Grab** 

### 1 lvS4-1'8-12B-G"ab 2**~** 

### ... . .... 128-Q-ab 3 12&Giab 4 \IS4.4'S·IJI!..Gr ab 1**~B-13e.Gtab2** 

### VS4.P8-138-Grab 3**VS4-f>8.1~4** 

### lv54-PB-149-Qlll> 1 VS4-P8-14B-Giab 2 VS4.PB · 14B·G rab 3 j\'S4-PB-148-Gr ab 4 

### Str e am**Wd~MI** le ad Sph"og Ml 

### Lead 

## spu.g Ml Laad Sph"og loa 

### Lead Sjtilg .., 

### Lead Sjtilg ..., 

### Lead 

## Stlldna Mil 

### Lead Sjtilg 

### 11.1 Lead Sjlldng**~** 

### Lead Spiklng 

### Ma Lead 

### Splkilg MG**LaadSpi~MII** L

ead**Sll«~** Ml1 Lead Spiking MU lead Sp ik ing Mil Laad Spllilng Mil 

## Waste Sample Logbo o k Pag e 2 6 o f29 

# V eo l ia

- Saug e t , IL

- Un it 4 C PT P roj ect Num be r 4 09 4 2510

. 20 Fraction 

### Cond R u n 

### Da le 

## Time 1W GW C o m m ent s An:live 1 1 8**~~~, .,,**  

## laa{, Mtiw 1 1 8 

### l"l\(0 Mtr.e 

### 1 1 8 

## 1 S t 5**/~~awe** 

### I 1 6**~'-** 

### 1 , 1 MJWe 

# ' 2B 

## ;o, ol'\' , 

# . •**,~** 

### AtdWe 

### 1 2a**~** 

### Aldivs 1 

### 2B 

# , ,., 7

Anme 1 

### 28 L.-

### 7 NrJiYe 

### I 

### 38

## ~ltll**~%** Archive 

### 1 

### 38 

### l 'H f> Archive 

### 1 3 8 

# ' " t; AtdlM! 

### I 

### 38 L

# '"**~** AtdlM! 1**~** Archive 

### 1 

### 48 Alchive 1 

### 48 M:llve 1 

### 49

## Waste Samp l e Logbook Pag e 2 7 of 29

### eo**ia ~S** **au et,**  

# ll**~** 

# Un i t 4 CPT Pr oj e ct Nu m be r 4 09 42 5 1 0. 20 Sample 10 Cod e S tream F r a ction Cond 

## Run Da t e 

# n me TW 

### G W Comments**~$4-HG-1 1**  e.G r ab 1 Mer cury Spilling Sol n 

### MeUis 1 1 6 

# .. ,.,, ,**~** ! f l\**So\; ~t** **~~~ -1\~** **~** 

# na · <:mro VS4-HG-1 1 B-Gtab 2 Merary Spi ki ng Soln Meta l s 

### 1 1 8 

### 1 3

'4 0 VS4-HG- 1 1 8-Gral>3 t.\era)ry $pkilg Soln 

### Me1als 1 18 

### I f IS"**~HG-11 8-Gial4**  Menuy Spiking Sdn Mo:ais 1 18**~** 

# ... 

# , ,, l**~54-HG-128-Giab l**  M erary Spllng 

### Soln Melals 

### 1 

### 28

### "'**t;~c ~** 

### l.~sVS4·HG- 1 2 B -Giab2 Me rcu ry S pik i n g S o l n 

### Metals 1 2 8

### ~~~~ VS4·HG-12B-Go-.b3 Mercury Spii<Wlg 

### Soln MeUis I 28 

### ) 'S\7**~$4-HG-** 12B-Grab4 Mela.ly 

### SplOOg Soln 

### Mel3s 1 

### 2B 

# . ..**,~,**

### ~HG- I J8.Grab1 Mercuy Spjl(ing Soln 

### Metas 1 3 8

### Of**,~**

# ~ VS4- HG· I 36- Gtab2 Me rru ry Sp i k ing So l n M eta l s 1 

### 38 

# , 

# ..**~** VS4-HG- 1 3B-G rab3 Mercu ry Sp lldn g Soln M e

tals 

### 1 38 

## 'biS' VS4-HG-1 38-Giab4 Men:lly Spidng Soln Melals 1 

### 38 

# . 

# '"eel VS4-HG- 148-Grab1 Mercury Spll<frlg 

### Soln Mas 1 

### 4B VS4-HG- 14 8-Giab 2 Memo ry Spi k ing Soln Metals 1 

### 4B VS4

- HG -1 4B- Grab3 Merc\wy 

### Spik ing Soln Metals 1 48 VS4-HG- 14S-G;ab4 Merclly Spiking Sol n Meesls 

### 1 

### 46



# l

## Wa ste Sample Logbook Page 28 of 29 

# V eo lia-S auget , IL- Unit 4 CPT Project Number 40942 5 1 0.20 Sample ID Code Stream Fraction Cond Run Da te Time 

### TW GW Com m ents VS+CR-1 18 -Grab 1 Chromium Sp ik ing So l n Metals 1 18 

### r"Ju,.J**IQ~**

### ~S+CR· Hs.GaD2 

# ammnn Spbg Sc*l Mell!is I 19

### ~0 VS4·CR·1 1 8
- Grnb3 Chromium Spiking Soln Mell!is 1 1 8 

### 15"15" VS4-CR-118-Grab4 Chromilm Spikilg Soln 

### Metals 

### 1 1 8 

### •**\~!JJ**

### ~S4-CR-128-Grabl OvaTUn 

### Spiking 

### Sdn Mel3s 1 28 

# r ur ., l

. 

# t an VS4-CR

- 12B-Grab2 Chromium Spi ki ng Soln Metals 1 

### 28 ,.j 

### l'r 

## 11 ' VS4-CR· 128-Giab3 Chronilrn Spikilg Soln 

### Me1a/.s I 28

## ~ 1'5 1\?.**~S+CR- 128-Grab4**  

### Clvcmiml Spiking Soln Metals 1 28 

# . .**m~..-** VS4-CR·13B-Grab 1 Cl\romi\Jm Spi k in g Sol n Me1a l s 1 

### 38

## ~19**--.~** 

# ...**I'S~ ~S+CR** **13B-Grab2** Chrooil.rn Spiting Soln 

### Metals I 38**1'1 ~,** **~S4-CR·1 38-Gra** **b3** Chroml!m Spo'l<ing Solo Metals 1 

### 38

# '"'~ VS4·C R-1 38-Grab4 ChromiJm Sp lkilg Soln Meta l s 1 

### 38 

# , _ 

# ... I 

## f.ct} I'S4-CR·1-48-Grab1 Cl1romiiMn Spicing Sc*l Metals 

### I 

### 48 

# "" / VS+CR·148·Grab2 Chromhlm Spi king Soln 

### Metals 1 

### 48 

# " / VS4 ·C R·14B-Grnb3 Ch r omium SpiiOOg Soln 

### Me lal s 1 

### 48 

# ""' /**~S4-CR 148-Grlb4**  Clvomlum Spti1g Soln 

### Metals 

### I 48 

# " / VS4· 

# - ,_ ' 

# / VS4- 

## . , 

# v 

# . L

### ~54- 

# ' / VS4

-

## J~ VS4· 

# /**~**

### ~S+ 

# /

...**~** VS+ 

# / 

# ' "-**~S+** 

# /**~**

### ~54- ./ 

# ...**~** VS+

# --**-~**

# Bulk So lid s Sam ple Co mposit e Data S h ee t

P roject Name V eo ll a- Sa uge t, IL O at e**\l)l~'t** 

### /1} Project N umbe r 409425 25 .2(H)2 Condition N o.. 1 F<>e Wit y U n lt 4 R:un No 

# 3 1\
Stream Nam e Bu lk So lid s (B S ) S tart Ti me 

## () q&(, Composit e sa mple 10**\IS4 BS-** **.COMP** ..I:_ Stop Time 

## \IHf. Ope r.> tor

Smlp l e Numbtr Tlmt Vo lu me/ M oss Sample Numb er 

### lime Volume/Mau 1 

## cq!.l. 'S**\E.~** 2 1 2 

### Oq'J\**'SO()~** 22 3 

### \ OOf.

### 5"'**1,~** 23 4 

# a o-.\**(Clt~** 

### 24 

## s \ o'!ll:a**~aGe,** 2 S 6 26 7 

### 27 8 2 8 9 29 

### 10 3 0 11 

### 31 12 32 

### 13 3 3 14 34 1S 3 5 

### 16 36 17 

### 37 18 

### 3 8 1 9 3 9 20 Final Vo l umo/Mass

### ~%~ts Comments: C ollect sofi ds in 1000 ml jar lab elod for Ald\lve. Ta ke a p propr1a t el y -sizod and o.qual a Uquots from ea d\ Jar to p r epa re the compos ite sa mple I n a 4 liter ja r . Record the v olu me/ma s.s o f e a ch a li q uo t u s e d t o p re p a r e the comp os it e s am p l e o n t he data sh e'l l R

etai n t h e re mal n l11 g sam p l e In th e l OOO ml ja rs and ar chive

.

SbS-M SUb-Slnlpk 

## c.,.m. -Oatc J.,.Z0/1**/&t'~c/:** JUM 20/J E-421 

## VE SOI3844

# Bu l k Solids Samp l e Composite Data Sheet Projecl**Nam~** Veolla

-**S.uge~** l l Date 

## ) () 10.,113 Project Number 40941525

. 20·02 Condition No

. 1 Facility Un lt4 Run No

### ~~ Stream Name Bulk Solids (BS) Start Time

### l<l~ 

# I Composire Sample ID VS4·BS-1M -CO MP j_ Stop Time 

### II 

## S") Operator

Sample Nu mber Tlmo V olume/Mass Sample Num ber Time Volume/Mass 1

### a~ 

# I**~0~(\** 

### 21 2 

## \ \OE.

## ~~ 22 3

### \\~\ 

# Sl'lao. 23 4 

# \I''-**'i\~** 24 5 

## \ 1'5 

# I**'50~c;** lS 6 

### 26 7 27 8 28 9 29 

### 10 30 11 31 12 

### 32 13 

### 33 1 4 34 

### 15 35 

### 16 36 17 3 7 

### 18 38 

### 19 39 20 Fina l Volume/Mass

### ~~':!,\~ Comme nts: CoUe<:t so lids In 1000 m l) a r laoo l o:d f o r Archive. Take approprlately · siled and equal aliquots fr om each jar to prepare the composite sample in a 4 Uter jar

. Record the volume/mass of eadlaHquot used to p r epar e the compOSite sample on lhe data sheet. Retain tile '""'a ining sample in the 1000 ml j ars and a r chive.**SDS~** Sflb.S ¥k C"""'"'""



### - o.te: J- Z0/2 -J-2011 E -42 2 

## VESOJ3845

# Bulk Solids Sam p le Composite Data Sh eet ProjeaName Veollo

-**~Uge1.** Jl Date 

### 10 

## li.f/13 Proje<:t Nu mber 4 094252.5.20.02 Condltlon No. 1 Faclllly Un i t 4 Run No 

# ofl Stream Name Bu lk Soli d$ (BS) Start Tlme 

# rnE. Composite**~mple** 10 VS4..f!S. 1Jl.**.COM ~**  Stop Time 

# \'l\5" Operator

Samp le N umber Tlmo Volum e/Mass**~mple** N umber Time Volume/Mau 1

### \1~**~I '\**  21 2 

## l '?t'5 \ 

# 510 

# co 22 

### 3**1~0() ~0~**  

### C\ 23 4 

## \If 

## G.\ 5()\t**~** 

### 24 

## s**l'i\~ ~()\"\**  2S 

### 6 26 7 27 

### 8 

### 28 9 29 

### 10 30 11 3 1 

### 12 32 13 33 1 4 34 15 35 

### 16 

### 36 17 

### 37 

### 18 38 

### 19 39 

### 20 final Volume/Mass 

## Q,'S-·Cil



## - Comments: Collect so lid s I n 1000 ml jar l abelitd f or Nchlve. Take approprlate l y.<ized and equa l all quots from ead1jar to prepare th e compo<lte s a mple In a 4 Uter jar

. Record the wlume/mass of ea d1allquot used 

### to prepare the composite sample on the data shoel. Retain the rema i ning sample In t he 1000 ml ja rs a nd a rchive.

$()$...()$ Sd> SeiifCI!! C«ffi''U /I

c Rovtsioh C.tC' J- MIZ R.!M • -.d: Jfll?te Z0/1 E

· 423 

## VES013846

# Bulk Solids Samp l e Composite Data Sheet

P

roject Name Veolia- S:. uget , l l Da t e 1()

### 1~5**13** Project Nu m b er**40942525.2~2** Con diti on No

. 1 Fad lily Unit 4 Run N o 

# 36 Stream Name Bulk SoHds (BS) St art Time 

## 1 3'SE. Com posite S amp l e 10 VSHIS. 11t -eO MPit Stop Time**j{,O~** Opera !Or

Samp l e Numb.,- Time Volume/Mass Sample Number Time Volume/M ass 1

### n~**3C:l7~** 21 

### 2 

## ll'fl

## ~"G 22 3 

# I**~tO<:.**

### ~ll~ 23 4 

## I "\ 

# fl. \**~~~** 24 5 

# ll\15'" 30(.9 25 6 

### \I{JI**~t)O~** 26 7 

### I**~(I()** 

### l()()

. «<J 27 8 

# ,,. , l06" 28 9**\~ fa**  

# 907f 29 10 

## l'S".f\**~~,** 30 11

## \'(,~ 

## 3:1"7g 3 1 

### 12 32 13 33 14 34 

### 1 5 35 

### 16 36 

### 17 37 

### 18 38 19 

### 39 

### 20 F inal Volume / Mass

### i,3'ti~ Comm ent£ Col i«t solids In 1000 ml jar labeled for Arcnfve. Tak e approp riately-si zed a nd eq ual allquots from eacn ja r to pre pare the composi t e sample in a 4llter jar. Record the volume/mass of

.. th a fiquot used to prepare the composite .ample on the da ta shect Reta in the r e main i ng samp l e In the 1000 ml j ars and arc hive

.

SDS-O!J**~te** 

# c.,.,-;,.**-O.~J-Ml i!** 


## VES013847

# Bu l k Solid s Sample Composite Data Sheet
Proje« Nam e Ve<>!ia

-**Sauge~** I L Date 

## \()**/~'S (I~**  P roject Number 40942525 .20.()2 Co ndition No

. Fa cility Unit4 Ru n No 

# 3&
Strtam Name eul k Solids (es) S tart 

### lime 

# ll" Compo s ite S.mp l e 10 VS4·85-1 Jl.**-C OMP** **~(.** Stop Tlme

## lb~" Opera to r

Sample Number Time Volume/Moss Somple Numb er 

### lime Volume/Mass 1

### 13~{.**~()Cq_** 21 2 

## ll ,. l**~()'\cit** 22 3 

## I 

## 'l ()(,**300~** 23 4 

## I 'till**l.OO~** 24 

## s 

# ,, ..**~**

### ~~'\~ 25 6 

# 1'\H**~()\9** 26 

### 7 

# 'r;o'**'aOI~** 

### 2 7 

### 8 

## \'Si.\ j:X>3 28 9 

### I 

## 'Slt**~'\** 29 10**,,~,** 

# ..**,~** 30 11 

## 1606**~l:kJ** 3 1 12**,~,**

### ~~s 32 13

### ~~**~~** 33 14 34 15 

### 35 16 

### 36



### . 17 3 7 18 38 19 

### 39 

### 20 Fi nal Volume/Moss

### 3.'\~**CI!**

commen t s: Collect solid s I n 1000 mlj a r l a b e llld fo r Archive. T ake app r opriately-sized and equa l aliquou from each j ar to prepare the composi te samp l •ln a 4 U t er ja r. Record t he vo l ume /mau of each a l iquot use d to prepare the composite samp le on t he dat a shee t

. Re tain the remirinin& somple in the 1 000 ml jars a nd archive.

SDS-D!J 5«>-Sc<ttp!. &_.;to

- 06fa ; J- 2012 R- J-20 13 E· 4 2S 

## VES013848

# Conta i nerized Solids Sa mple Com p osite Data Sheet

ProJect N ome Veolla

- sau get, I L Date**1:1/~ 511~**  

### P

roj ec t Number 40942S25.2Q-0 2 Co nd ition N o. 1 Fatllll'/ 

### Unl t4 Run No

### 3~ sueamName 

### Containerize<! Sol i d s ( CS) Start Time 

## O qi!,- Composite S.mple 10 VS4-CS-1 3**MP** 

### .1_ Stop Time 

### 1

## ~'s Operator

Sample Cont ainer 1 0 Time 

### Volume/ Sample 

### Contain er 10 Time Volume/ Nu mber 

### Mass Numoor Mass 1**~~**

# I'"'&~ '500

_ '\ 21 2

### ~d. Qq'{O

### ~~~ 22 

### 3 

## 50 I ClO$"**~~ ~**  23 4

### Cl 

## IO<aO**9)~** 24 

## s 

## 70 IOt.s-

### '6~~ 2S 

### 6 2 6 

### 7 

### 27 8 28 

### 9 29 

### 10 30 11 

### 31 12 32 13 33 

### 14 3 4 15 3 S 

### 16 36 

### 17 37 18 38 

### 19 39 

### 20 Fklol Volume/Mass

### ol~11c:. Co mment$! Take appr op r late l y · $l!e<l and equal all q uots f ro m eac h con t illner to pre p are t h e composite samp le I n a 4-llter J ar . Reca<d the volume/mass of each a li quot used to prepare t he composite sample o n th e dat a sheet

. Collect a representa!M aliquot of the "'maln i ng material in • 

### 500 m lj ar to oo archived

.



## VESO I 3849

# Containeri ze d Solids Sample Compo s ite Data Sheet
Project Name 

### Veolia

- Sauget, ll Date 

### \ 0**~** 

## s; /13 Pr oject**um~ r**  4 09 42S2S.:Z0.02 Conditi o n No
. 1 

### Facil i ty u"lt 4 Run N o 

# <tA
Strea m Name 

### co n ulnerized Soli ds (CSJ S l<l rt Time

## lC~c) Composit e sample 10**V54.a- .COMP_** **I** 

### Stop Time 

# 1\50
O pe rator



### Samp le V o lume/ Sample CO nta i ner lD 

### Tlm e Vo l ume / Con t ainer 10 

### nme N

um ber Mass 

### N u mb'e r M ass 1 

# ?'0 IO'!Q**'5'00~** 21 2

### ~~ 

## 110?**5G~~** 22 3

## ~~**~** 

## 'Stl()

_ '\ 23 4

### \tl~ 

## \ 1 '36"'**1)\'l~** 

### 24 

## s \\14**11~0 ~tl**  25



# - 6 2 6 

### 7 27 8 

### 2 8 9 29 

### 10 30 11 31 1 2 32 13 33 

### 1 4 3 4 

### 1 S 35 

### 16 36 

### 1J 37 

### 18 38 

### 1 9 

### 39 

### 20 Fina l Vo l ume/Mo ss 

## Cl,{d,)G

Com m e n

t s: Ta ke a pproptlately ·si ted and equa l allquoiS from e ach conlalner to prepare the 

### composit e sample In a 4-Uter jar. Re<:Ord t he volume/m a ss of oadt ali q uot used lo prepa r e th e comp osite samp l e on the da t a sheet. Colloct a r ep re se ntativ e a liquo t ol

. t t> e re m aining ma t er ial I n a S OO m l jar 1 0 

### be ar chi ved.

SD$ .Q!15lh-s.mpk C...,.s/fo R<.;,ion Q!4'nf """lO J Z 1/oW. W<d: ;...., ZO J J 

## V ES0 1 385 0

# Containerized So li ds Sample Composite Data Sheet

Pro ject Nam e Veo l ia

- Saug et, IL Date

### to/a.~**/I~** P

roject Nu mber 409425 2$.20·02 Co n d i tion No. 1 

### Facility Unlt4 Run No 

# 38 Stre!m Name Containerized Solids (CS) Start lime**~~~,.** 

### Composite Sample 1 0 VS4-(S..1 lt -COM f'iA 

### Stop lime 

# '"asOpmto r

Sample Volume/ Samp le Contaln cr 10 T ime 

### Volume/ Container 10 

# nme Number Mass 

### Number Mass 1

### ~d.

# ·~~~ 'l('.l)t; 21 

### 2

### '\~ 

# \ 3'j 0**so~c;** 

### 22 3 

## \0 I '1()6 ' 

### I$0C.c:. 23 4

### ~<D 

## 14c).<l**'Sill~** 24 5 

# 70**l'i~6" ~(1::)~**  25 

### 6 

### 26 

### 7 

### 27 8 28 9 

### 29 10 30 

### 11 31 12 

### 32 13 33 14 34 IS 

### 35 16 36 

### 17 37 18 38 19 39 20 

### Final Volume/Mass

### a.~119 Comments: Take appropriatelv · sltod and equal a li quots f r om**e~c h**  

### conta i ner to prepare the composite sample I n a 4-llter j ar . Recond the 

### vo lu me /mass of each a li quot used to prepare the composi te samp le on the data sheet. Collect a representative a[(quot of tM remain in g materi al In a SOO ml j a r to be arch iv ed

.



## VES013851

# Containerized So lid s Sam ple Composite Data Sheet Proji!CI Nam e Veo lla- saoaet , ll Date 

## 10 1&.6'/13 Pro]e<t Number**40942525 .2** **~2** Conditi on No, 1 

### Foclllty Unit 4 Run No 

# -a& Stream N ame 

### Conta l nerlud Solids (CS) Start 

### Tune

## 13'3~ Composite Samp leiD VS4-CS -1 }!

### <O**~** Stop Time

### I~S' Operat

. or

samp to Container tD Time Volume/ Sample Con to lntr ID Time 

### Vol.ume/ Number 

### Mass Number 

### Man 1

### ~~ 

## l llf li:Rq 21 

### 2 

# '\a. \ \tO**~'{~** 22 3 

## '50 I 

# 'tOt**1100~** 23 

### c**~~** 

## '1{)..0**~1t)** 24 5 

# 70 l'tl6**~0-'** 25 6 

## 10 

## 1'450**3()(,~** 26 7 

# a&**'~'" ~qc.**  27 

### 8 

# <\\ IIJt()

## '()~ 28 9 

# \o q_**~!i**

### 3\~ 29 10 

# 1\1\ I 'S"f O**a.q o~**  30 

## u 

# I ll \ E.06'**~** 31 12 32 13 

### 33 

### 14 34 15 35 

### 16 36 17 

### 37 18 38 19 

### 39 20 

### f inal Volume/Mass 

# '3,3W-c,

Comments : Tak e a pjl(Opl'iatojy-<lzed and equal all quot s from eacll con ta in er to prepare tile composi te s a mp l e In a ._Uter**~r .**  

### Record tile volome/miS1 of 

### uc:tt aliquot used to prepa re tht composite somple on the dot a sheet Col'.aa representotm af<1uot ol 

### the remolnlnc moter1olln • SOO 

### milo< to be atdlM!dst>S-OS Sd>-samplo C-11• ll•vW •n 

### t>t!,.i1f""" 2012 R.w.

...

d: /UM 10/J 

## VESOI 3852

# Containeriz e d Solids Samp l e Composit e Data Sheet

P r o j ect N ame Veo li a -Sau ge t. I L Dat e

### OIU/1~ P r

oje ct N um '* 4094 252 5

. 20-02 C onditi o n N o
. l Fac ilit y U n l

t4 RuoN o

### ~e. Str eam Name C on ta l n e rlz:ed So li ds [ CSI S t art nm e

### 1~35" Composit e Sampl e ID**VS4.CH f!** **.CO MP** **~** Stop r om e

### 1£.3**~** Operato r

Sam p le Contal oer 1 0 

## r '""' Volume/ Samp l e Con t o l ner 1 0 11 mc Volume / Nu m ber Mass Numbe r M us l 

# -oa... I US 

## 1ole, 2 1 2

### ~.ta..**1~6 "$~(4**  22 3 

### '5() 

# 1'405'**~** 23 4

## '&fJt~ 

# I 'U-6**?!O\~** 24 5 

### 7 () 

# l'i15 l O \q 2S 6 

# ?,C) \It 'SCI**lO\~** 2 6 

### 7

## &~**,~,.**

### ~<teo 27 8 

# <\'\**,,.~()**

### 3~ 2& 9 

# ltR l**'5~5"** 

## 3\**~** 29 

### 10 

# H\ I SSO**~~** 30 

### 11 

## 1:\.'7 \{,06"**~lq** 3 1 1 2 

### l l7

### ~~0

## 30d~ 32 

## u 

# tq)**~~** 

### "l)l 

## '"I 33 14 34 

### 15 3 5 

### 16 36 17 

### 3 7 

### 18 38 

### 1 9 39 

### 20 Final Volumo/Mas s

### ~!{ll>q Comme ots: Ta k

e**app<oprlat el~** **ed** and equalaliqu o t s from e ach con tai ner t o p r e pare the composite samp l e In • 

### 4-Uter ) a . r . R

ec ord the volume / mau o f each a li quot u s ed t o prej)are th e com p osit e sa m p

le on t

. he data sh eet. Coll ec t a rep r esenta tive ali quo t o f t he remain ing ma te ri al in a 500 ml j a r t o be arc h iv ed

.

5tJS

.. M SI.O$ '**JtPk 

### eo,.,pos tt

• PniHM**/Jd r~** **:** J I/IM 2011**ReW~ IJT** **it!** ZOJ' 

## VESOI3853

# Liquid Waste Feed Sample Composite Data Sheet Project Name Veolia- sauget, I L D ate 

## 10 /.l'i/13 Project Number 

### 40942525.20-()2 Con d iti on No

. 1 Factrrtv Unit 2 Run No 

# 3 A Stre.-am Name Low BTU Uquld Waste (UIW) Start Time 

# o q,l r Composite Samp l e 10**VSHSW·l ~A** **COMP** 

# L St o p Time**1~'!1~** O

p e r ata<

Sa

m ple N umbti' Ti me Volumt/M

... Sample Pl umber Time Volume/Miss 1**0,~~** 

## '5 00 

## " 1.- 21 2 

## 0,'\0 2 2 

### 3 

### I OOG" 23 4**10 ~**  

### 24 5**() ~~**  

# . 25 6 

### 26 7 2 7 8 2 8 9 

### 29 1 0 30 11 

### 31 12 32 13 

### 33 1 4 

### 34 15 35 16 36 

### 17 37 1 8 38 19 39 20 F inal V olll m e 

### & , 'l(lO 

## "' I..

Comments: Collect**appropria~ed** and equal afiquots and tr.lnsfer Imm ediately Into a 4 -U ter composite jar

. Coll ect a separate 500 m l bottle of sample at each samplingtlme to be reta ined in arch ives.



## Sq

# "'~ 

# \ed**"'** 

# ')( -l \ s i teQ""

$05-115 SdJ..S.,.,S.**·** P•-• t>m : J.,.. ZQ/2 llc-.J: Juno ZQIJ E-43 1 

## VES013854

# L i qu i d Waste Feed Samp l e Compo s ite Data Sheet
Pr o jeaName Veol l a - Sa1J8et , I L Dat e 

## I () 

# r**~~** 

# 113 P

roject N u mber 4 09425 25.20.02 cond i tion 

### No

. I**Fac ~tv**  U ni t 2 Run N o 

# 'iA. S

tr e am N am e low BTU Li q ui d W as t e ( L BW) Sta r t T ime 

# I OSO Composi te Sam ple 10 V S3 · L B

W · @ <O MP 

### j_ Stop Ti me 

# 1150 Ope<a t or

Sample N u mber Time Vol u me/M ass Samp l e Humber 

### T1me Vo l umo/lmss 1

### 10**~0** 'iO () " \... 2 1 

### 2 

### \**\0~** 

### 22 3 

# \ ta,.O 23 

### 4 

# 1\35' 24 5 

## \150 1- 

### 2S 6 26 7 27 8 28 

### 9 29 

### 10 

### 30 11 

### 3 1 12 

### 32 1 3 

### 33 

### 14 34 15 3 5 

### 16 35 

### 17 37 1 8 

### 38 19 

### 39 20 F ina l Volume

### a..~oo 

## "'L
Comme n ts: Col l ect a pp rop riatel v · si l e d an d e qu al a ll q uots a n d t r a ns f er Im mediately I n t o a 4 -Ut er c o mpo si t e jar

. COllect a se parate soo ml bot tl e of s a mp l e at ea ch s a m pl i ng lime t o be r e t a i ned in arch ives • 

## .lQ 

# r-.p\t>d**tolo'l** 

# i-- \) 'b 

# \r l'lllr\

5DS

- 06**Sub~** Canpcsi te R. W I IOII O. t< : J ""' 201 2

, .., .,.. , J

- 2013



## V

ES 0 13 855

# Liquid Waste Feed Sample Composite Data Sheet
Project Name veolla- Sauget, I L Date 

### 10la..'O 113 PrOject Numbe r**4094 2S2** **20~2** Condition No. 1 Facinty Unit2 Run No

## ~P> S

tr eam Name L ow BTU U qu i d Waste (LBW) Start Time 

## 13"&5'
Co m posite Sample 10 VSHBW · l 'U

### COM~ Stop Tim e

## l't~6' Operato r

s-pleNumlw Tlme Volume/Ma5$ sample Number Tlme Vo l ume/Mass 1 

# 113f '500 

## 1'\\.. 21 

### 2

### \~'lO 

### 22 3**l't() ~**  

### 23 4 

## 1'\lO 24 5

# '"'3~ 

# ..... 25 6 26 7 27 8 28 9 29 10 30 11 31 12 

### 3 2 13 

### 33 14 34 15 35 16 

### 36 17 

### 37 18 38 19 

### 39 20 Final Volume

### a,~oo 

# ...**~...** Comments: Collect appropriately-sized and eq uala liquot.s and transfer Im med i ately I n t o a 4 · liter com posite jar

. Collect a sepa rat e 5 00 ml bottle of sample at each samp li ng time to be reta i ned in arch i ves
.



# <..o\lecW**~otn** 

# ;.-1\**~"'**

Sf>S.()$ Sub-Somplo Composite**R~vlsicm** t>Dta : JUM 201.1 Reviewe t/: June 2013 E -4 33 

## VES013856

# Liquid Waste Feed Sample Composite Data Sheet
Projec.t Na me Veo li a - sauget ,ll Date 

### 10/ tl!i/13 Project N umber 40942525.2G-02**on d~** **oo** No. 1 Fa dllty Unlt2 Run No 

## 39 Stream Name low B TU Uquld Waste (LBW) Start Time 

# IllS' Compos it e Samplo iO VSH.BW·1 ia -coM I'i.l Stop 11me

### I~CI-s' Operator

Sample Num ber Time Volume/Ma ss sample Number T1me Vo l u me/M•ss 1

### 13~S"' 

### <;**()~** 

## "'l. 21 2

### ll~ 22 3 

# l it Of 23 4 

## \ltlO 24 

### 5

## 1'4~~ 25 6 

## I**'4~** 26 7

### ~~ 27 8 

# , no 28 9 

# \'U6 29 10 

# 1 no 30 1J 

## 1 {.0f 

# .._ 31 12 32 13 33 

### 14 34 

### 15 35 1 6 36 

### 17 

### 37 18 38 19 39 20 Fl naiVolurM 

## 3 300 1"\L
Com,.,.,nts : Collect appropriate l y-sited and equala li q uots and**tr~nsfe r**  Immediate l y i nto a 4·Uter comp os it e ja r
. Collect a se pa r ate 500 ml bott l e of sample at ea ch samp li n g time to be retaine d in archives.



# &n"" D 

# \ed.**~"' ¥~** **\\ ~\r-eq,....** **5DS.(/6~1<C-IO** l&t'isionl>ate: JUM 2011 lhodew<tr. , ... 20JJ E-434 

## VES013857

# Liquid Waste Feed Sample Com pos ite Data Sheet Project Name veolia

- sauget, IL Date 

### !o 

## l &'S/13 Proje<:t Number 4 094252S .2 o-() 2 Conditio n No

. 1 facility Unit 2 Run N o 

## 36 St r eam Name Low BTU Uqu i d Waste (LBW) Star t Tim e

### r~~5' COmpoSite Sampl e 1 0**VSHBW COMP** **•<.** S to p Time

### ~lS" Operator

Sample Number Time Volume/Mass Sample Number Time Volume/Mass 1 

## 111')**'!)()~** "'\... 21 2

### \~'l6 

### \ 22 3 

## 1 1( 0'; 2J 4 

# \"'oo 24 5 

# I**'tl~** 2 5 6 

## 1'\C)O 26 7 

## t'$' 0,. 27 8 

# \ "60 28 9 

# IUS" 29 10 

# "w 30 11 

## I**tiC)~** 31 12 

# 1£.6.0 32 13 

# l f>U 

# - 33 14 34 15 35 16 36 17 37 18 

### 38 19 39 20 Final Volume 

# a. "oo ,..,L,
Co""'""'ts: Collect ap p rop riately-si zed a n d e q ual allquots and tr an sfer i mmedia tely into a 4 · L i te r comp os ite jar. Collect a separate 500 m l botUe of sample at ea ch sampling ti me to be r etained I n a r ch i ves.

## ~ 

## ... t:.\ed.**~~l'f\ ~~t\** **~\tt<tl'\**

5D5·0il Svb·Sompl< C«npMite R

e vi

sion !Xtfc: June 2012 R.-,f, JUfiB20/J E-435 

## VES013858

# Liquid W as t e F ee d S a mple Composite D a ta S h ee t Project N a me Veollil

-**sauae~** ll Date 

## 1 01&.15 / 13 Project N umber 40942525.20.02 co.Mition No
. 1 f ac Hity un l t4 Run 111 0

### ~~ Stre am Nam e H i gh BTU Liqui d Waste ( H BW) S t art Tim e 

# 01\**~'** COmpos i te samp le 1 0 VS3

- HBW

- 1!t, <O M P_ \

_ St o p Tim e 

### I**0~ ~**  Oper ato r

S

e m p le N um ber Time V olume /M oss S ample N umber 

## nme V o lu me/ Mass 1 

## O f U'- <; () C) "' 

### L. 21 l**0,~,** 22 

### 3**I~** 23 4**to~\** 24 5 

## \ 0?. 4 25 6 2 6 

### 7 2 7 

### 8 28 9 2 9 

### 10 30 11 31 

### 12 32 

### 13 33 

## u 34 15 35 16 36 

### 1 7 

### 37 1 8 3 8 19 

### 39 20 Fin al Vo l u me 

# a. , TO() 

### eo.\..-

tomnMn ts: COllect appro p riately-sized 

### anll equal allquots 

### and transfe r immed iat ely into a 4-Uter composite )ar

. Collect a separate soo ml bottle of sample at each samplin g time to be reta ined i n archives.



# Sqh\owd**~()"" "'1** **--l ~**  

# s**~~ S()$.4165~~~~·**  f«,y(tfon """' ' JWI< <012 

## ltevl•'""" J,_.,. 2013 E-436 

## V ES 0 1 3 859

# Liquid Waste Feed Sample Composite Data Sheet

Pro j ect Name v e ol la

-**•ue ~**  l l Date 

## lCIIU/13 Pr oje(t Numbe r 4 09 4 25 2 5.20-42 Cond i tion No . I Facility U nlt4 Run No

# "'~ Stream Name High BTU liqui d Wo s to (H B W ) Stort Time

### 10~ 

# I Co mpos ite Samp l e ID VS3-HOW · l .!iA .COMP ...\_ St o p Time

### 1\~) Operator

sample Number 

## nme Volume/Mass Sample Number 

### Tim• volume/Mass 1 

### \0'! 

# I**~QC)** 

### ML 21 2**\\()~** 

### 22 3 

## l 

# t•' 23 4

### \\~ 2 4 5 

## \ I 

## 'i I 

# .. 25 6 26 

### 7 27 8 

### 28 9 29 10 30 11 31 

### 1 2 32 13 33 

### 14 34 

### 1 5 3 5 1 6 

### 36 

### 1 7 37 18 

### 38 19 

### 39 20 F i n a l Volume

## ~~001'1\... Comments : Co l le c t apprepriately • sized and eq u a l allqu o t s and t r an s fer i mm ediate ly i n to a**L~e r**  co mpoSit e )ar. Coll ect • s ep ara t e soo m l bottle of samp l e 

### at eadl sam p Un a U me t o b e r eta i ned in arch i ves . 

## SQ

# "'**~** \fld 

# fi'Qw-,**M~ <r.h~WI** **Sl>S ~**  Svi>-Sompt. t:.mpcsile Rc vis>oo o.t. : Jllfl< i!0/ 2 1/evi<wt:d: J..,. i!0/3 E- 437 

## VES013860

# Liquid Waste Feed Sample Composite Data Sheet Project Name Veolla -Sauget, l l Date 

## ll:l la.StlJ Proj ect N u mber 4094 2525

. 20 · 02 Cond itio n No. 1 Facility Unit4 Run No

### ~s Stream N ame High STU liquid Waste ( HBW) Start rrne 

## 11 )t Compos i te sample ID VS3+18W -lA. <OMP i! Stop Tome

### 1~3S" Operator

SampiR Number T ime Volume/Mass Sample Number Tlme Volume/Ma ss 1 

# 11'3' 1500 fill 21 2**l'~'il** 22 3 

### ll{()(. 23 4

### 14~\ 24 5 

# \'tl5**-~** 25 6 

### 2 6 7 27 8 

### 28 9 

### Z9 10 30 lJ 

### 31 

### 12 

### 32 13 

### 33 

### 14 34 

### 15 3 5 

### 16 36 17 

### 37 18 

### 38 19 

### 39 20 F lnoiVolu me 

## Q.,'$'00 ,..L
comments; 

### Co ll ect a p propr1ate lv ·s l zed an d eq ual al i quo ts and transfer Immediately Int o a 4
- llter composite ja r. 

### Collect a separ at e 5 00 m l bot tl e of sample a t each samp li ng time to be reta in ed In arch i ves.

## ~ 

# ...**~\~ ~**  

# 'J.-Ia.**~\f{lt)W\**

51>5-05 SobScntp/<**~1'tc** 1/eYisitx; Cot .: J,_ to/2**R~viewed:** 

### June 10/.J E- 43 8 

## VES013861

# Liquid Waste Feed Sample Composite Data Sheet
Project Name Veoll a - Sauge t, ll Da te 

## I() ll!i/13 Project Number 40942525.21).(12 Condition No

. 1 Facility Unh 4 Run No 

# oB St.ream Name Hi8h BTU Liquid Waste (HBW) Start Time 

# tnt Composite Samp ieiD VS3 · HBW· l ll : COMP ai Stop Time 

### 1 

# ta & Ope r ator



### Sample Numbt< Time 

### Volume/ Mass Sample Number nme 

### Volume/ Mass 

### 1

### Ill**~ "i~**  

### ,..\... 21 2

### \~S 

# I 22 

### 3

# '"~ 23 4

## ~~~ 24 5 

# \'ilS 2S 6 

# \'t\1 26 7

### I,G~ 27 

### 8 

## \UI 28 9 

### I 

## 6")4 29 

### 10 

## I'S**~I** 30 11

### ~~~**~** 

# ... 31 12 32 

### 13 

### 33 14 

### 34 15 

### 35 16 36 17 37 

### 18 38 

### 19 3 9 20 Fin al Volume 

## 3 • 

# '300 """
Comments : 

### Collect appropriately-sized and equal a li quot> and transfer Immediately i n to a 4-ll\er composi te jar

. Collect 

### a separate SOD ml bottle of sample at each 

### sampling time to be**ret<~ ln** **ed** 

### in an:hives

.

### Socllf\p\~d**~~Of'\ ~-t** **~**

## ~htql"\

SlJ.$4 St.b-$1% ¥ ClJtytrdte**.rs rwoC.rw** **:** 

### J.,.zorz 11<-J.,..zo/J**E~39** 

## VES013862

# Liquid Waste Feed Sample Composite Data Sheet

Pro je ct Name Veotia- sauget, I L oate 

### 1 () 

## 1 

## tl..S 113
Pr oject N u mber 4094252 5

. 20-{)2 Condkion N o
. 1 Faci lity Unl 1 4 Run No 

# 36 Stream Nom e High BTU liquid Wute (HBW) Start T ime 

# l Sl' CornpoM!e Samp l e I D VS3-HBW · l }). -coM pff, Stop Time 

## \**f:,~(.** OP*rator

Sample Numb er Tim e Volume/Ma ss Sample Number Tlmo Vo l um e/ Ma ss 1

### l~lf. 

### 'i () 

## 0 "' 

## L 2 1 2 

# ll.,l 22 3

# ·~~ 23 4

### 14~1 2 4 5

### 11.\l~ 

## I l 2S 6 

## I I{ 

# 'Sf 26 

### 7 

# \,0, 27 8 

# , ...**~,** 

### 28 9 

## )**'$~"** 29 1D 

## l'fS\ 30 

## u**~~~** 3 1 12 

## \.HI 32 13

### 1{,3~ 

# ... 33 

### 1 4 34 

### 15 35 16 36 

### 17 37 18 38 19 39 

### 20 Final Volume 

# i ,(,00 .1>1\.

Comments : Collect op p r oP<Iale ly-si zed and equal al i q uots an d tran sf er Immedia t e l y into • 4.Uter com po s i te jar

. Co ll ect a se pa rate 500 mt bo ttle or sample at e a c h samp ling t i me t o be re t a i ne d i n a r d1ivcs

.

# Slcl~\ed**~"' 'f-·1~** **$~~1(\**

.505 · 05 .5/Jb.Scfopt.**~If•** Re'lishn D4te. · Jur.c 20 1 2**Rn'ie~Wd: J~**  ZOJJ E-4 4 0 

## VES OL3863

# Liquid Wast e Feed S a mpl e Co mpo s ite Data Sheet
Project Name Veoll>

-**Sauge~** ll Date

### I()**J~Ij /\3**  Project Number 40942525.20.02 Condi tion No

. 1 Facil i ty Un lt4 R un No 

# 31\
Stream Name Liquid Wast e Feed (LWFI Start 11me 

# Mn Composite Sample 10**VS4-LWF-J .COMP**  

### _L Stop lime 

## IO'll) Operator

Sample Number nme V olume/Mass Sample Number Time VokJme/Mass 1 

## Olt37 'I()() 

### Ml.. 21 2**oq~t~** 

# I 22 3 

### 1()(>., 

### 23 4 

### \0

.. 24 

### 5**0~7** 25 6 

### 26 7 

### 27 8 28 9 29 JO 30 11 

### 31 12 32 13 

### 33 lA 34 

### 15 35 

### 16 36 

### 17 37 18 38 

### 19 39 20 Flna l Volume 

# &,too 

# ..**~..** Com m enu: CoYect appropriately-sized and equal allquots and transfer Immediately Into a 4 -l.l ler compos i te jar

. Collec:la separate 500 ml bottle of sample at each umpf111g lime to be retained in archives

.

### ~..,p\fd

## ~IV\**~.q.~** .1.**SDS·~** SU....S...,Ie 

### c_.;rc lie- (Jotrl: JUM ZO/l**~d:JUM20fJ** E· 44 1 

## VESOI 3864

# Liquid Wa ste Feed Sample Composit e Data Sheet

Pro ject Nam e Veol l a - Saugel, l l Da t e

### I~ 

## I**~~/13** P

r oj ect Nvmber 40942525.20-<12 Cond ition N o. 1 Fac il ity Un it4 Run No 

# "'"' Srrnm Nam e Uqutd Waste Feed (lWI') Start nme**16~** Compos i t e Sa mple I D VS4·lWf ·1

j! ·COMP 

### j_ Stop Tlme

### 11'5~ ()pe<ator

Sampl e Number Time Volume/Mass Samp le**Num~r** Time Volume/Ma n 1

### \()~ 

### 'i ()() "' \.. 21 2 

### \\(I) 22 

### 3 

# Ha.d- 23**~ \\~J**  24 5 

## \I**~d..** 25 6 26 

### 7 27 

### 8 28 9 29 

### 10 30 ll 

### 31 12 32 

### 13 

### 33 1 4 

### 34 15 35 

### 16 36 17 

### 37 

### 18 38 

### 1 9 39 20 Anal Volume

### Q,~OOI'\L.
Commen t

. s: Collect appropriately-<lzed and equ al aliquots and transfer Immed ia tel y Into a 4-litl!f co mposite jar. Co llect a sep arate 500 ml bottle of "m p ! e at eadl sam pfin& lime to be retained i n arch i ves .

## ~ 

# .... plt\'1 trOll\**1. ~** **lii ~(JI\\** **. stJS** **·OIJ ~**  

# c"""""; '•

- o. .. : J- .1'012 --.q,J..,.ZOJJ E-44 2 

## VES013865

# Liquid Waste Feed Sampl e C ompo s ite Data Sheet
Projeet N ame Veolia

- Sauget,ll Date 

## 101

...**~11 3**  P

r o

j cet N um be r 4 0942 525.2 0

- 0 2 Coh d i tlon No

. 1 faci l i t y Unit 4 Ru n N o

### ~& Stream Name li q ui d W a ste F..ed ( L W F ) scar t 11me 

# \'3'31
COm p o si t e Sa mp l e 10 

### VS 4·LW F- lll < oM I'lll S top 11 m e

### \~l~ Ope rat or

Sample Num be r Time Vol u rM/Mass S ample N umlar Time Vo lume/Mass 1

### ~?137 

# , o a "'\... 21 2

### a~ 22 3 

### \1\0) 23 4

# '"~ 24 5

# 'l~ ..... 25 

### 6 26 

### 7 27 8 28 9 29 

### 1 0 3 0 11 

### 31 

### 12 32 13 33 

### 14 34 15 

### 35 16 36 

### 17 3 7 18 38 19 

### 39 2D f" ...a l Vol u m o 

# a. t 00 "''--

C

o mm e n ts: C oli e< t appro p riately

- siz ed an d equal allquo ts a n d tr an sfer Im medi a t ely Int o a 4 ·ll ter c ompo s i t e jar

. C

ollect a se p ara te SOD m i bottle of samp l e at e ach samp lins time to be re ta in ed i n ar ch ives.

## 'i>~~**\~ ~** **1--~ ftQW\** **$()$.()5~~silo** ReWsiDI! Dol• : JUtW 2012 R

..,._ J .,..zo/1 E·« · J 

### VES013866

# Liquid Waste Feed Sample Composite Data Sheet
Project Na me Veolla**sauge ~**  IL Date 

## 1**ol~~/l~** Proj<ct Number 40942525.20-C2 Conditlon No. 1 Fac ility Uni t4 Run N o 

# ?»& SirnmName Uquld Waste Feed (lWF) Start nme 

# l3l1 Composite Sample 10 VS4 · LWF · 13._**..CO M~**  S top Time

### 1~7 Op•rator

Sample N umber 

### nm e Volume/Mass Somple Number nme Volume/Mass 1**1\~7** 

## SSQ() "'\.. 21 2

### ~~osa. 22 3 

## 1'\0J 23 4

# '"~ 24 5

### \l~ 2 5 6

## ~'t~~ 26 

### 7 

# \li<n 27 8 

## 1$» 23 9 

## I'H) 29 1 0

## ·~56 30 11 

## \f:.O) 

## _ 

# .. 31 12 

### 32 13 

### 33 14 

### 34 1S 

### 35 16 

### 36 17 37 18 38 

### 19 39 

### 2 0

. Final V olume 

## 1)00 "'L

Comments : Co llect appro pria tely-si zed and equal**r~quots** and transfer Immedi ate ly I nto a 4-Uier composite jar. Collec t a separate 500 ml bott l e of sam pl e at each sampling tim e to be re tained in archive s.

### s,qlt\~**~** 

# E-tt

...**"t-~**

## 5h~fC'I

SDS-0 5 Sub-.$<Nlopk CINI!P"slte Rt1isitM (Jote: June 20 12 -J-:t013 E· 444 

## VES013867

# Liquid Waste Feed Sampl e Composite Data Sheet Project Name V eo lla- Sauget, l l Date 

### l()fa.'i" 

## 113 Project Number 40942525

. 20-02 Condition No

. 1 Facility Unlt4 Run No

### ~8 Stream Nam e Uqu i d Waste Feed (LWFI Stan Time 

## l\a7
Com posite S ample ID**VS4·lWF-t :Sl** **-co MP~**  Stop Time

### 1~7 Operator

Sample Number Ttma Volume/MIS$ Sample Nu mber 

### Timt Volume/MIS$ 

### 1 

# \'lJ ')<X) "'\.. 

### 21 2

### 11~~ 22 3 

## \ItO) 23 4

## 1'\~~ 24 

## s**I'll~** 2S 

### 6

## ·~a. 26 7 

## \tO) 27 8

### 1'1~ 28 9

## \~~7 29 10

### lit~ 30 11 

# ,,0, 31 1

. 2

### l~n 32 13 

# l(,l'


# - 33 14 

### 34 15 35 16 

### 36 17 

### 37 

### 18 38 19 39 

### 20 Final Volume

### ~ 

## ,\.00 

## 11\\.

Comments: Collect appropriately -s ited and equalallquots an d tr.msfer Immed i ately Int o a 4·Uter composite j ar . Colle<;! a separote 500 ml bottle of sample at eacfl sampling time to be reta ined in archives.

## ~""1)\~u**tto~** 

# j.-?.6.**$~1et1ft\**

SD5 ·05**Sui>~ID** C"""""'re flnilitM tJott. • JUM 20tz**R•vf~d:** JUM ZOlJ 1>-4<15 

## VESOI3868m**~** 

# ..**Pro]~** Na me ycol!a- sa us s; t
. !l/ Un i t 4 cpr Project Numb Of 4 0 94252 5 .2().()2 

## Solution Prepa ratio n Log

SOllltlon Oltt,.,-**~** .... Ill -.I No.

# rl-!~aa. t ofu.lt3 

## .\" t.c**~0** 

## 1**lbl~** 

# z•

# "~ z.. 

# , ..**,. ~** **>OI,ul ~** **\\IIU~O** 

### I

# ~- 

# " 

# ..

l o 

# 12UIJ \ O"f 0 

## It, <!Po( •ell<.

..**<\\.~0,**

## ~ I 'L._

### •61nl~**IO'o~<":,o ~**  

# tb\ 1L**1\Cfo~otO'l** VJ.l,/1. 

## 12.* 

# ljr,_**~i'** 

## 0-c**lof,.\ t~** 

## •'>·U-z.~**to~ ~__ol**  

## ft.

..**IO'o~~ I0~\1!>** 

## "'tL~**~**

### ~"ll 

## ...**~..** 

# ....

• E><llhtlon Date 11 30 d"YYIfter "'-""" -"" addle poi3<Wm**~---** 

# _**_..,~-..Oiircln** ldJtr ,



## ._ .._ a.-A 2. CZ....'f"'\-'--'l 

## ••**~** 

## IM• \-**~** 

## R ,.7 ..t'-Oj Mass O<**o. w•**  YolutM

### "l 

### 50 II 

## \n\•1,**?.3~** '\00 

### 1\\12-1" loo


## Sbo**~** 

# ....**to t!ll~** 



## -soo "lo'\ 

## tOft'\\t'..



## Soo 

# z..o, lo( rs/ro,

ctoo l oo 

## 11\l>\\1..., 

# I 

# -**td-l~**

# ~"'

\011'<

...

### ~**~ ~**  oa t • I o / 

### J.J.(, !> Pose _1

_ of 

## .i!!(_

Redpu t o Mak e 1 Ut er**Sulfuric~** Pe rmanpn.1 t• IOOmiWam 100 m1 Corcentnttd H)
. so

.. Ollua !D 1 L 

## ...aume oiOcKMnO, Ni tti< Add/Hydros en l't

rooddt SOOmiWeter 50 ml conetntratod KNO, '33lmllO!IH,o, onut.t to ll vo lu me

0.1 N Nlulc Add



### 900mlwate r G.! m l Conuntratod KNO, 01tu1e to ll VO:ume 8N Hydrod11 0<ic Ac i d 

### 250mlwa

.. r 690 ml Conce ntrat ed HO

DUuu to ll volume**~-oh:-_,_,_'-"9** R.vMo!IDtzl

...

• J..-yl0/3

### Pro j ect Name yeq t la

- 

### Sauget. IL I 

### Unit 4 CPT Project Numb er 4Q942S25.2!H12

hf Rtaaent No. \ 

## Htt.<:**~o** l-**~0,_** 

## 3 II.

. \ 

### -{ 

### tfV(.c_ 

### 11,_0

_**~**

### A-.:..\..o~ 

# " l.vl't 

## Reage n t Use Log

Manufacturer 1 l ot Numbe r 

## ?**'-'~~** 

### -wt4L<- 

## '3T 6 Y t 11S 

## t--\6£. 

# ., ...**~.,t,** 

## ?**Cl~~lo>IHLC. ~(.**  

### S"tc..t8 Mtv 

## ?.I**"~':f** Date Optned bplm;on Date 1 

### to\U.h!> 

### tolz;t.l 

### N 

## rolu.lr3**/O(U/1~**

...**(2~\** 

### r!o**Jofz:~l** 

### •I(,

ro 

## 1 'ZJ((**~** 

## ro 

# r vtt • 't to I**t.oslt~** 

### t•l 1..s It'( (o**/1.~** 

## II'!>**t<>f~{ I~**  Date**toll~( r~**  

### Pilge ...L_ oi 

# a:_

lnitialt 

### j:Vfu**(~"' ~**  ";::.MJ611.

### ~ 

## \C.cW\

'ms GOdt**m~** be used: ITB •J.T. B.alcer, M al • Ma£1W!d:toct1:; A**c.Ad'~Jn to** **r;** P • Phannc.a, v = VW'R. f = Alhtr, Mat= Mwon 2**E~ rat** **n** Oate I s 11 prOVIded by m anvfactu r er or 12 m onlh s aft 6 r openin&. F0$

.. 029 RtMgu/f lise L119 R«-llisiM Dots: jt.fiiJIY'Y 20/J