# Cenogenics Corporatio n 10 0 Rout e 52 0 •Drawe r30 8 Morganville , Ne wJerse y0775 1 Telephon e (732 ) 536-645 7 •(800 ) 747-945 7 Fa x(732 ) 972-852 7 •e-mail : cenogenics@verizon.ne t I n th e Matte ro f Cenogenic s Corporatio n FAADocke t No . CP10EA000 7 FDMSNo . FAA-2010-078 6 CERTIFICAT E O F SERVIC E I hereb ycertif ytha tth e Answe rfollowin g ha s bee n sen tthi s dat e byFedera l Expres s addresse d a s follows : Origina l an d On e Cop y Th e Honorabl e Ronni e A . Yoder , Chie fAdministrativ e LawJudg e U.S . Departmen t o fTransportatio n Offic e o fHearings , M-20 , Roo m E l 2-32 0 120 0 Ne wJerse yAvenue , S.E . Washington , D C 2059 0 Hearin g Docke tClerk , AGC-43 0 Federa l Aviatio n Administratio n Wilbu rWrigh tBuildin g - Suit e 2 W100 0 80 0 Independenc e Avenue , S.W . Washington , D C 2059 1 Jeanin e C . Gotimer , Complainant' s Counci l Attorney , Offic e o fth e Regiona l Council , EAL- 7 Easter n Regio n Federa l Aviatio n Administratio n 1 Aviatio n Plaz a Jamaica , N Y1143 4 i j j X I C O rn-H m

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Respectfull ysubmitted , Cenogenic s Corporatio n 10 0 Rout e 520,Drawe r308 y/ ^ MorganvilteC^077 ^

Z ' /-^""^ y Bvj^^/^<i%^^<^^- ^ ' A ^ Michae l Kat z ~) Presiden t Date : Augus t26 , 201 0

Certifie d T o IS O 900 1 an d IS O 1348 5

# Cenogenics Corporatio n 10 0 Rout e 52 0 •Drawe r30 8 Morganville , Ne wJerse y0775 1 Telephon e (732 ) 536-645 7 •(800 ) 747-945 7 Fa x(732 ) 972-852 7 •e-mail : cenogenics@verizon.ne t Augus t25 , 201 0 U.S . Departmen to fTransportatio n Offic e ofHearings , M-20 , Roo m E l 2-32 0 12 0 Ne wJerse yAvenue , S.E . Washington , D C 2059 0 To : Th e Honorabl e Ronni e A . Yoder , Chie fAdministrativ e La wJudg e Re : I n th e Matte rofCenogenic s Corporatio n FAADocke tNumber : CP10EA000 7

Answe r Cenogenic s Corporation , th e respondent , hereb yfile s it s Answe rt o th e complain tfile d Augus t 4 , 201 0 a s show n i n th e abov e state d docke t number . Cenogenic s take s th e positio n tha tth e allegation s i n th e abov e complain tar e withou tmeri t an d reques ta re-consideratio n o fth e civi l penalty . W e presen tth e followin g i n supporto fou r positio n (pleas e not e th e complain tnumber s reference d belo war e thos e cite d i n th e lette rdate d Augus t4 , 2010) : Referenc e Complain tNumbe r2 : relate d t o 4 9 C.F.R . 172.704 , Trainin g W e disagre e wit h th e allegation tha t Cenogenic s Corporatio n ha s no ttraine d it s hazma t employee s i n accordanc e wit h C.F.R . 172.70 4 an d woul d lik e t o presen tth e followin g evidenc e i n supporto fou rposition . Cenogenic s ha s i n plac e an d ha s ha d i n plac e trainin g procedure s an d record s t o satisf yth e requirement s o fth e abov e cod e o ffedera l regulation . •Cenogenic s ha s i n place , an d ha s ha d i n place , sinc e th e onse to fou rshippin g th e hazardou s materia l i n questio n a procedur e fo rpackagin g th e productfo rshipment . Se e attache d Standar d Operatin g Procedur e (S.O.P.) , PG-0573-0 5 (Attachmen t 1) . Pleas e not e tha tthi s procedur e ha s bee n revise d 5 time s (evidence d b yth e generatio n number , th e las t tw o digit s o fth e S.O.P . number) , a s require d byregulatorychange s ove rth e years . Onl yon e employe e ha s responsibilit yfo rth e packagin g o fth e product , Bert Valville , th e productio n technician . Prio rt o packagin g an d shippin g th e produc t i n question , th e ne wemployee , Bertran d Valville , wh o manufacture d an d package d th e productreceive d "function-specific " trainin g ( a s require d by172.704(1 ) an d (2) ) an d wa s supervise d bymyself , Nitz a Katz . Ber tValvill e wa s teste d bydemonstratin g hi s abilityt o perfor m th e tas k

correctl yunde rm ysupervision . W e conside rcorrec twor k performanc e i s th e bes t an d mos t"appropriat e means " o ftestin g (172.70 2 (d ) state s "...employe r shal l ensur e tha teac h o fit s hazma temployee s i s teste d byappropriat e means....") . Attache d (Attachmen t 2 ) i s Ber tValvule' s trainin g recor d (S.O.P . OP-00111-04 ) fo ral l o f Certifie d T o IS O 900 1 an d IS O 1348 5th e Organization' s Standar d Operatin g Procedure s (a n FDA/IS O requirement) . Th e employe e an d instructo rsignature s ar e recor d o ftraining . Evidenc e o fprope rwor k performanc e (test ) i s recorde d bym ysignatur e unde r"Trainin g Effectiv e Date" . Pleas e refe rt o th e S.O.P . title d "Packagin g Develope rfo rAustria" , S.O.P . PG-0573-05 . I hav e highlighte d th e relevan t referenc e fo ryou rreview . Safetytrainin g (a s require d unde r172.70 4 (3) ) a s wel l a s PP E (Persona l Protectiv e Equipmen ta s require d by172.70 4 (3 ) (ii) ) i s provide d t o eac h employe e tha t handle s hazardou s materials , a s require d byOSH Aan d als o withi n th e scop e of172.704 , withi n day s afte rth e starto femployment . Pleas e referenc e attache d Chemica l Hygien e Plan , S.O.P . SF-0025-0 2 (Attachmen t 3) , Bloodborn e Pathoge n Exposur e Contro l Plan , S.O.P . SF-0023-0 2 (Attachmen t 4 ) an d Chemica l Hazar d Communicatio n Plan , S.O.P . SF-0098-0 1 (Attachmen t 5) . I hav e als o attached , a s evidenc e o ftraining , th e signe d trainin g record s fo rthes e procedure s fo rou rnewes temployee , Bertran d Valvill e (Attachment s 6-8) . Pleas e not e th e startin g dat e o fhi s employmen twa s 2/17/0 9 an d th e trainin g wa s conducte d fro m 2/18/0 9 throug h 3/16/09 . Emergencyrespons e an d securit yawarenes s trainin g ( 172.70 4 (3)(i) , (4 ) an d (5 ) ar e provide d i n th e Occupan tEmergencyRespons e Plan , S.O.P . SF-00153-03 . Th e procedur e (Attachmen t9) , an d a signe d trainin g recor d (Attachmen t10 ) ar e attache d fo r you rreview . Pleas e not e tha t though th e reference s cite d fo rthi s procedur e ar e CF R 121.1 2 an d CF R 73.1 2 (USD Aan d CDC) , CF R 172.704 , unde r(5 ) (b ) allow s tha t trainin g " require d byothe rFedera l o rinternationa l agencies , ma yb e use d t o satisfy th e trainin g requirement s i n paragrap h (a ) " . I n additio n t o th e abov e safet ydocument s use d fo rhazardou s material s safet ytraining , eac h o fou rmanufacturin g instructio n procedure s i s precede d bya sectio n title d "Caution " i n whic h th e safet yprecaution s fo rth e specifi cchemicals and/o rbiologica l material s use d i n tha tprocedur e ar e detailed . Al l o fou rmanufacturin g procedure s requir e verificatio n bya "checker " fo reac h critica l ste p o fth e process . Thi s i s a n FD A requirement . I n essence , eac h operato ri s bein g teste d eac h tim e he/sh e use s a hazardou s materia l i n th e manufactur e o fa product . Subsequen t t o th e inspectio n bySpecia l Agen tCharie s Odu m an d a thi s suggestion , I registere d fo ra n onlin e Dangerou s Good s trainin g wit h DG I an d complete d certification . Attache d i s a cop yo fm yD G certificat e (Attachmen t 11) . Ou rmetho d fo rtestin g ha s bee n fo rth e employe e t o sho whis/he rabilit yt o perfor m th e wor k correctly . W e conside rthi s th e mos t "appropriat e means" . Th e work s i s inspecte d bya Superviso rin-hous e an d byou rfreigh t fonwarde r(se e respons e t o Number s 3 , 4 an d 5) . However , atth e suggestio n o fth e inspector , followin g m ycertification , I adde d a n additiona l test . I prepare d writte n function-specifi ctest s fo rth e tw o employee s involve d i n aspect s o fth e D G shipping . Attache d ar e copie s o fth e test s (Attachment s 1 2 an d 13) . Referenc e Complain tNumber s 3 an d 4 an d 5 , Shipper' s Declaratio n fo rDangerou s Good s Trainin g fo rEilee n Kerste r

•Eilee n Kerste ri s th e Organization' s exportsecretaryan d custome rservic e representative . Sh e doe s no t handl e hazardou s materials . He rfunctio n wit h respec t t p hazardou s materia l shippin g i s t o complet e al l o fth e documentatio n require d fo rth e Organization' s shipments . Eilee n Kerste rha s bee n mad e awar e o fth e natur e o fou r producttha t i s considere d dangerou s good s an d ha s ha d trainin g i n th e completio n o f th e Shipper' s Declaratio n o fDangerou s Goods . He r"function-specific " trainin g an d

£3 -testing , a s wel l a s min e an d Mr . Katz's , ha s bee n provide d byou rfreigh t fonwarder , Ai r Se a Internationa l Forwarding , Inc . a s permitte d unde r4 9 C.F.R . 172.702(c) , "Trainin g mayb e provide d byth e hazma temploye ro rothe rpubli co rprivat e sources." . Sh e prepare s th e declaratio n unde rth e direc t supervisio n o fRayTobia , presiden to fAi rSea , wh o i s certifie d byDG I Trainin g Cente rt o shi p dangerou s good s an d renew s hi s certificatio n everytw o years . Mr . Tobi a review s th e D G Declaratio n fo reac h shipmen t an d inspect s th e carg o fo rprope rpackagin g an d labeling . Therefore , Eilee n Kerste ris , i n effect , bein g teste d eac h tim e a shipmen t i s prepared . Additionally , th e carg o an d documentatio n i s inspecte d byth e airiine' s hazardou s materia l specialis tprio rt o shipping . W e conside rthi s a n "appropriat e means " o ftestin g sinc e ther e ca n b e n o bette rtes ttha n correc t wor k performance . I hav e attache d fo ryou rrevie wa cop yo fRay Tobia' s D G certificat e (Attachmen t14 ) an d a lette rfro m RayTobi a (Attachmen t 15 ) describin g th e procedur e w e hav e ha d i n plac e fo rth e pas t 1 4 year s fo rth e direction , supervisio n an d revie wo fth e D G shipmen tan d documentation . Furthe rt o th e evidenc e presente d above , I fin d th e allegatio n tha tEilee n Kerste rha d no t receive d function-specifi ctrainin g illogical . A s describe d above , he rfunctio n withi n th e organizatio n wit h respec tt o D G i s t o complet e th e documentation . I fEilee n Kerste rha d no tha d awarenes s training , ho wi s i t tha tsh e kne wtha tth e Declaratio n Fo rDangerou s Good s wa s a regulatoryrequirement ? Ha d sh e no tbee n properi ytrained , ho wi s i t tha t sh e kne who wt o correctl yfil l ou tth e Declaration ? Referenc e Complain tNumbe r6 , Genera l Trainin g

•Onl ytw o employee s hav e responsibilit yfo rD G shipment s tha tar e sen tbyair , th e technicia n tha tmanufacture s an d package s th e produc tan d th e exportsecretarytha t prepare s th e documentation . Bot h o fthes e individual s hav e ha d functio n specifi ctrainin g an d performe d thei rtask s unde rth e direc t supervisio n o fa n immediat e superviso ro ra D G certifie d individual . Pleas e referenc e m yresponse s above . Referenc e Complain tNumbe r7 , Emergenc yTelephon e Numbe r

•Cenogenic s ha s provide d tw o telephon e number s o n th e Shipper' s Declaratio n Fo r Dangerou s Good s wher e eithe rMichae l Kat z o rmysel fca n b e reache d at al l time s whe n shippin g DG . On e numbe ri s th e busines s numbe ran d th e secon d numbe ri s ou rhom e number . Sinc e m yhusban d an d I hav e overiappin g wor k hours , on e o rth e othe rca n b e reache d a tal l time s durin g th e shippin g o fDG . Attache d ar e copie s o fth e D G Declaratio n fo rth e tw o shipment s i n questio n (Attachment s 1 6 an d 17) . Pleas e not e at th e botto m right o feac h for m tha tther e ar e tw o telephon e number s liste d next t o th e lin e "2 4 hr . Emergencycontac tTel . No." . Referenc e Complain t Number s 8 an d 9 , UN117 0 Ethano l Solutio n » W e disagre e wit h th e allegation tha t w e use d th e incorrec tdescriptio n fo rth e D G i n questio n fo rth e followin g reason . Th e shipmen t i n questio n unde ryou rnumbe r8 an d 9 i s th e VDR LAntigen , a diagnosti creagen tfo rth e detectio n o fsyphili s infections . Th e product consist s o fa solutio n o fethanol , cardiolipin , cholestero l an d lecithin . Onl yth e

t,i _ethano l solutio n i s liste d a s dangerou s goods . Therefore , th e prope rshippin g nam e a s show n i n bot h o fth e DG R tables , CFR172.10 1 an d th e lAT Atabl e 4. 2 i s ethano l solutio n an d th e U N numbe rshow n i n bot h table s i s UN1170 . 1 hav e attache d copie s o fth e relevan tpage s o fbot h table s fo ryou rrevie w(Attachment s 1 8 an d 19) . Th e lATA regulatio n 4.1.2.1(c ) state s tha tth e generi cdescriptio n (i n thi s case , a s yo u stated , "Flammabl e Liquids" ) i s t o b e use d onl ywhe n "a n articl e o rsubstance i s no tliste d by nam e i n th e Lis to fDangerou s Goods" . Pleas e referenc e attache d photocop yfro m th e lATADangerou s Good s Regulation s (Attachmen t 20) . I n thi s case , sinc e th e prope r nam e o fth e hazardou s materia l wa s liste d (ethano l solution ) i n bot h th e DG R an d th e lAT Atables , i ti s require d i n th e description . Fo rthi s reaso n w e use d "ethano l solution " wit h it s correspondin g U N numbe ra s th e description . Also , pleas e not e tha t fo rbot h th e generi can d th e prope rname , th e hazardou s clas s an d th e packin g grou p ar e th e same . Referenc e Complain tNumbe r10 , Shipmen t UN198 6

•Fo rthi s produc talso , w e woul d lik e t o offe rreason s fo rou rdescriptio n use . Th e product solutio n i n thi s shipmen tconsist s o fspeciall ydenature d ethy l alcoho l wit h toluene , hydroge n peroxid e an d water . Th e toluen e i s no t a separat e componen ttha t i s adde d t o th e formulation ; i t i s th e denaturin g agen to fth e ra wmateria l ethy l alcohol . Th e toluen e i s als o classifie d a s a flammabl e an d i s th e sam e clas s an d packagin g grou p a s th e alcohol . Th e secon d componen t mos t contributin g t o th e hazar d o fth e mixtur e i s hydroge n peroxide . However , th e fina l concentratio n o fth e hydroge n peroxid e i n th e mixtur e i s muc h les s tha n 8% . Th e 172.10 1 tabl e o fhazardou s substance s onl y describe s hazardou s condition s o fhydroge n peroxid e solution s ata concentratio n ofat leas t8 % (Attachmen t21) . Additionally , th e lAT ALis to fDangerou s Goods , tabl e 4. 2 (Attachmen t22) , describe s hydroge n peroxid e solution s o fles s tha n 8 % a s "no t restricted" . I ti s therefore , no ta requiremen t t o provid e th e nam e o fthi s componen t i n th e descriptio n sinc e th e concentratio n i n th e produc t i s les s tha n 8 % an d therefore , no t considere d a hazardou s material . I hav e attache d oU rmanufacturin g protocol , S.O.P . MP-0531-04 , an d testin g dat a fo rthi s produc ta s recor d o fverificatio n o fth e concentratio n o fth e hydroge n peroxid e i n ou r reagen tsolutio n (Attachmen t23) . I n addition , I woul d lik e t o stat e tha tCenogenic s Corporation , a s a medica l devic e manufacturer , i s regulate d bynumerou s governmen t agencies . W e ar e a smal l compan yo fonl ynin e employees . I n ou rtwenty-eigh tyea rhistory , w e hav e neve rattempte d t o defy , circumven t o r ignor e regulations . W e ar e legall yregistere d an d regulari yinspecte d byth e FDA , USDA , CD C an d OSHA . Additionally , w e ar e registere d t o IS O 900 1 an d IS O 1348 5 ( a voluntary Internationa l Standar d Organization) . They , too , audi t ou rOrganizatio n annuall yfo rcomplianc e t o th e IS O Standar d a s wel l a s complianc e t o internationa l regulatio n tha tappl yt o ou rindustry . I a m prou d t o reporttha tw e hav e a n excellen ttrac k record . A tn o tim e durin g ou rhistoryha s an y agencyfoun d tha tw e wer e i n defianc e o fregulatoryrequirements . W e certainl ymad e n o attemp tt o avoi d D G regulation s a s i s evidence d byou rcompletio n o fth e Declaratio n o f Dangerou s Good s an d th e numerou s procedure s w e hav e i n place . Furthermore , w e wer e forthrigh twit h informatio n requeste d byth e FA Aagents . W e wer e als o happ yan d quic k t o compl ywit h th e suggestion s mad e byth e agen tan d viewe d thes e a s improvement s t o ou r alread yexistin g procedures . I offe rthi s informatio n a s evidenc e tha tCenogenic s i s an d alway s ha s bee n awar e o fan d mad e everyeffort t o compl ywit h an yan d al l applicabl e regulatoryrequirements . We , therefore , fee l tha tth e fact s an d circumstances , a s demonstrated , d o no t

warran tth e propose d civi l penalty . Than k yo u fo ryou rconsideration . Furthe rt o ou rAnswer , w e woul d appreciat e a n opportunit yt o presen t financia l statement s showin g w e hav e suffere d significan tfinancia l lose s makin g i t a sever e hardshi p t o payth e fin e a s proposed . W e woul d als o appreciat e knowin g th e financia l reportin g forma t an d documentatio n require d fo ryou rcourt' s examination . I n addition , w e believ e ou rresponse s showin g tha tw e tak e th e shipmen t o fhazardou s material s seriously , wor k har d t o b e i n complianc e an d immediatel yundertak e suggestion s fo rimprovemen t ca n provid e a basi s fo r settlement . You rkin d consideratio n i n allowin g th e hearin g i n thi s matte rb e hel d i n Newark , Ne wJerse y woul d b e appreciated . Respectfull ysubmitted . Nitz a Kat z Vic e Presiden tan d Qualit yManage r Enclosures : Attachment s Nos. 1 - 2 3 an d Certificat e o fServic e

### ATTACHMEN T1 CENOGENIC S CORPORATIO N PACKAGIN G PROCEDUR E STOO LBLOO D TES TDEVELOPIN G SOLUTIO N FO R DIPR O Procedur e prepare d by : Michae l Lock e Date : 2/1/0 8 S.O.P . PG-0573-0 5 Procedur e approve d by : Nitz a Kat z Date : 2/1/0 8 Supersedes : PG-0573-0 4 CONTAINE R NOTE : Th e S.B . Developin g Solutio n i s filtere d directl yint o th e shippin g container . SPECIFICATIONS : 1 5 gallo n Dele xplasti cdrum , tighthea d ST15 G T H P LDRUM , 0203-whit e U N COD E 

### 1H1/Y1.8/10 0 Maximu m fil l allowe d i n dru m i s 6 0 liters . VENDOR : Nationa l Packagin g 6 5 Railroa d Avenu e ^ ^ %-^ ^ Ridgefield , Ne wJerse y0765 7 

### FAX : (201)941-877 7 ••• J -•%• •'• •

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### FO R PIC KUP : 6 0 Nort h Unio n Hillside , Ne wJerse y (908 ) 688-429 9 LABELS : 1 . CUSTOME R ADDRES S LABE L 2 . DEVELOPE R REAGEN T LO TNUMBE R EXPIRATIO N DAT E VOLUM E CONTAINE R NUMBE R ( 1 o f2 , 2 o f2 , etc. ) # ^ \ ^STOO LBLOO D TES TDEVELOPIN G SOLUTIO N FO R DIPR O S.O.P . PG-0573-0 4 PAG E 2 o f2



### 3 . ALCOHOLS , FLAMMABLE , TOXIC , N.O.S . U N NO . 198 6 CLASS/DIVISIO N 3 PACKIN G INST . 30 7 (ETHY LALCOHOL ) PACKIN G GROU P I I PLEAS E KEE P DRU M UPRIGH T 4 . FLAMMABL E LABE L(se e attache d sample ) 5 . CARG O ONL YLABE L(se e attache d sample ) actua l wordin g i s DANGE R D O NO TLOA D I N PASSENGE R AIRCRAF T 6 . TOXI C 6 LABE L(se e attache d sample ) 7 . ARRO WLABE L(se e attache d sample ) NOTE : D O NO TUS E OXIDIZE R LABEL . OFFIC E AShipper' s Declaratio n an d a n R/ Afor m mus tb e completed . Th e J R includ e "U N 1986 " i n U N o rI.D . No . field . ^ ^ 1>- larsmo n mus t

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### CHEMICA LHYGIEN E PLA N FO R LABORATOR YDIAGNOSTICS/CENOGENIC S Procedur e Prepare d b y^^^^^yy^^^ l Dat e y^^/< ^ ^ SOP : SF-0025-0 2 Procedur e Approve d h\ i y^^-^^t^^u^f-^y^^yy^^ Dat e ///^Ap . Supersedes : SF-0025-0 1 Introduction : Th e purpos e o fthi s Chemica l Hygien e Pla n i s t o provid e employee s wh o hav e occupationa l exposur e t o laborator ychemical s wit h procedure s an d practice s tha t wil l protec tthe m fro m healt h hazard s presente d b ylaborator^^mical s i n th e workplace . Th e procedure s an d practice s herei n wil l mee tthejie^S^m'ent s se tfort h i n 2 9 CF R Part1910.1450 . .^^® ^



# G Exposur e Determination : ^^ ^ A tthi s facilit yonl ysom e o fth e employee s hav e AG)mi|B|tnJ>n£i l exposur e t o laboratory chemicals . Th e followin g jo b classification s an d ta^lgp^r e a s follows : 1 . Productio n Manage ran d LaboratoryTechnicians : Direc thands-on-contac twit h a variet yo flaboratorychemicals . 2 . Shippin g Clerk : Responsibl e fo rreceivin g laborator ychemical s int o th e warehous e an d transportin g the m t o th e laboratory . Implementatio n Schedul e an d Methods : Engineerin g an d wor k practic e control s wil l b e utilize d t o reduc e o reliminat e th e exposur e t o laborator ychemicals . Th e procedure s an d practice s herei n fal l unde rth e followin g headings : 1 . Genera l Principle s fo rWor k wit h LaboratoryChemical s 2 . Label s an d Symbol s 3 . Hazar d Identificatio n 4 . AComplet e Lis to fal l LaboratoryChemical s 5 . Persona l Protectiv e Equipmen t(PPE ) 6 . Additiona l Protectiv e Equipmen t 7 . Usag e o fRespirator s 8 . Designate d Workspac e 9 . Receivin g an d Storag e o fLaboratoryChemical s 10 . Hazardou s Wast e Disposa l 11 . Housekeepin g 12 . Spill s an d Accident s 13 . Firs tAi d Trainin g 14 . Fire Plan/EmergencyContact s 15 . Medica l Pla n 16 . Informatio n an d Trainin gCHEMICA LHYGIEN E PLA N FO R S.O.P . SF-0025-0 2 PAG E 2

LABORATOR YDIAGNOSTICS/CENOGENIC S

1 . Renera l Prinriple s fo rwor k wit h i ahoratnr yChemical s 

### Th e followin g shoul d b e use d fo ral l laboratorywor k wit h laboratorychemicals : a . Rea d al l "Cautions " o n Maste rProductio n Record s (MRP) . b . Becom e knowledgeabl e o fth e Materia l Safet yDat a Shee t (MSDfi£^V4l*chemica l befor e usin g i ti n a procedure . B e awar e o fal l healt h hazar^^^ d precaution s outline d i n th e MSDS . c . B e abl e t o identif yal l Hazard Symbol s an d Nationa l Fire Protectio n Associatio n (NFPA ) Wamin g Diamond s o n al l laboratorychemicals . (Se e Appendi xA) . d . D o no tsmel l o rtast e chemicals . e . Avoi d eating , drinking , smoking , gu m chewin g o rapplyin g cosmetic s i n area s wher e laboratorychemical s ar e present . f . D o no tus e damage d glassware . g . Us e labwar e onl yfo rit s intende d use . h . Was h hand s befor e leavin g th e laboratory . i . Avoi d practica l joke s tha twil l startl e anothe rworker . j . D o no tmout h suctio n fo rpipettin g o rstartin g a siphon . k . Confin e lon g hai ran d loos e clothing . D o no t wea rsandals , perforate d shoe s o r ope n toe d shoes . I . Alway s us e persona l protectiv e equipmen t(PPE) , suc h as , gloves , labcoats , faceshield s o rgoggle s whe n state d i n a n MSD S o rth e "Cautions " section s o fa n S.O.P. . m . Us e appropriat e respirato rprotectio n whe n state d i n a n MSD S o rth e "Cautions " section s o fa n S.O.P. . n . Avoi d us e o fcontac tlense s i n th e laboratory . I fcontac tlense s ar e necessary , infor m a superviso rs o specia l precaution s ca n b e taken , o . Us e th e hoo d i n th e Bacti-la b fo rprocedure s involvin g th e releas e o ftoxi cchemica l vapor s o rdust , p . Alway s wor k

i n a wel l ventilate d are a whe n usin g laboratorychemical s tha t releas e hazardou s vapors . Us e ceilin g ventilatio n fan s wher e available , q . Neve rleav e a procedur e i n proces s unattended . r. Neve rwor k

alon e i n th e buildin g i fth e procedure s bein g conducte d are hazardous , s . Reportal l spill s an d accident s immediatel yt o a Supervisor , t . B e aler tt o unsaf e condition s an d reportthe m t o a Supervisor , u . Neve rdischarg e t o th e sewe racid s an d base s o ran yothe rlaboratorychemica l tha t ca n caus e a fire , explosio n o rstructura l damage . V . Deposi tHazardou s Wast e i n it s appropriatel ymarke d container .CHEMICA LHYGIEN E PLA N FO R S.O.P . SF-0025-0 2 PAG E 3

LABORATOR YDIAGNOSTICS/CENOGENIC S

2 . I ahel s an d Symhok - C Jf ^ 

### Man ylabel s an d symbol s ar e presen tthroughou tth e laborav^^i n warehous e wamin g employee s wit h occupationa l exposur e t o specia l hazard : Al l empM^m^wit h occupationa l exposur e mus tb e knowledgeabl e o fth e following : C^TV ^ a . Hazard Symbols : Thes e ar e symbol s foun d poste d o n al l l^b^pi^grs rchemicals . The ydescrib e laboratorychemical s a s poisonous , corrosiver^im^ng , harmfu l an d irritating , flammable , oxidizin g o rradioactiv e (Se e AppendMiA) . Posters ca n b e foun d i n al l rooms equippe d fo rhandlin g laboratorychemicals . b . Nationa l Fire Protectio n Associatio n (NFPA) : Th e NFPADiamon d i s foun d poste d o n al l laboratorychemicals . I trate s laboratorychemical s base d o n thei rdegre e o f Flammability , Reactivity , Healt h Hazard s an d Specia l Waming s (Se e Appendi xB) . Poster s ca n b e foun d i n al l room s equippe d fo rhandlin g laboratorychemicals . c . Biohazar d Label : Th e Biohazar d labe l i s poste d o n al l refrigerator s an d freezer s wher e foo d an d beverag e storag e i s no tpermitted . 3 . Hayarr i Iriantifination : 

### Wit h respec tt o labels , symbol s an d MSDS's : a . Employe rshal l ensur e al l label s o n incomin g hazardou s chemical s are no tremove d o rdefaced . b . Al l MSDS' s tha tare receive d wit h incomin g hazardou s chemical s are t o b e file d i n a kno wlocatio n an d availabl e t o al l employee s wit h occupationa l exposure. 4 . Complet e Li.<; to fLaborator yChpmirai s 

### A tthi s facilit yal l th e chemical s use d i n an yS.O.P . hav e bee n compile d int o a lis tshowin g thei rchemica l description , hazard s tha tapply , inventoryrange s an d storag e an d locatio n code s tha tappl y(Appendi xC) . Eac h chemica l liste d i s supporte d wit h a n MSD S file d i n th e Bact i Lab . Al l employee s mus trevie wthi s lis twit h thei rsupervisor . Whe n ne w chemical s ar e introduce d int o procedures , the ywil l b e adde d t o thi s list . 5 . Persona l Prntertiv e Fqiiipmen t(PPF ) 

### Employee s havin g occupationa l exposur e t o laboratorychemical s are require d t o wea rPP E whe n handlin g hazardou s chemicals . A tthi s facilit yth e followin g item s ar e available : a . La b Coat s b . Disposabl e Late xGlove s c . Fac e Shields , Face Mask s an d Goggle s Employee s havin g occupationa l exposur e mus tobsenA e th e followin g precaution s fo rusin g PPE : a . Alway s remov e PP E befor e leavin g thi s facility . Neve rbrin g hom e PP E tha tha s bee n wo m i n th e cours e o fth e day . b . Remov e laboratorycost s immediatel yupo n significan tcontaminatio n wit h a hazardou s chemical .CHEMICA LHYGIEN E PLA N FO R S.O.P . SF-0025-0 2 PAG E 4

LABORATOR YDIAGNOSTICS/CENOGENIC S 

### c . Inspec tdisposabl e late xglove s fo rtear s o rwea k spots . d . Inspec tfac e shields , fac e mask s an d goggle s fo rcracks , puncture s o rothe r physica l defects . e . Was h hand s afte rwearin g protectiv e gloves . 6 . Additiona l Protectiv e Equipment : A tthi s facilit yAdditiona l Protectiv e Equipmen ti s define d as : ^ a . LaboratoryHood s b . Ceilin g Ventilatio n Fan s ^ ^ • ^ 

### c . Fire Extinguisher s i^ ^ d . "Survivair " Full-fac e Respirato ran d "Flexi-Star " Hga^JL e Respiratory\ e . Eyewash/Showe ro A^" " f . Overhea d Sprinkle rSyste m vCw) ^ inVpr * Th e laborator yhoo d i n th e Bacti-La b shoul d b e use d fo rariy^procedure utilizin g a volatil e chemica l whic h release s toxi cvapors . I n orde rt o increas e th e performanc e o fth e hood , th e sas h shoul d b e dow n a tal l time s providin g a shiel d betwee n th e employe e an d hazardou s chemicals . Th e ceilin g ventilatio n fa n i n th e Bacti-La b mus tb e operatin g whe n a n MSD S o r "Cautions " sectio n o fa n S.O.P . call s fo radequat e ventilation . Th e window s i n La b 3 mus tb e ope n whe n a n MSD S o ra "Cautions " sectio n i n a n S.O.P . call s fo radequat e ventilation . Fire extinguisher s are locate d i n th e hallwa yborderin g al l laborator yrooms . Employee s wit h occupationa l exposur e shoul d b e knowledgeabl e o fho wt o operat e a fir e extinguisher . Th e "Survivair " Respirato ro r"Flexl-Star " Respirato rmus tb e wor n whe n handlin g hazardou s organi cchemicals . Th e MSD S o fsuc h a chemica l wil l stat e unde rth e Precaution s sectio n t o us e a respirato ro fthi s type . Th e Eyewash/Showe rmus tb e use d whe n a n employe e ha s bee n splashe d wit h a hazardou s chemica l i n th e eye s o rskin . 7 . Usag e o fRespirato r A tthi s facilit yther e ar e tw o type s o frespirators : a . "Survivair " Full-fac e respirato r b . "Flexi-Sta rHalf-fac e respirato r Employee s usin g eithe ro fthes e respirator s fo rth e firs ttime , shoul d hav e a superviso rsho wthe m th e prope rwa yt o fi tth e respirator . Th e manufacturer' sCHEMICA LHYGIEN E PLA N FO R S.O.P . SF-0025-0 2 PAG E 5

LABORATOR YDIAGNOSTICS/CENOGENIC S



### instructio n manual s fo rbot h respirator s ar e kep t i n th e Equipmen t fil e unde r Respirators . Th e instructio n manual s shoul d b e reviewe d wit h th e employe e befor e usin g th e respirators , c . Eac h tim e a n employe e use s eithe ro fth e respirators , he/sh e mus t sig n of fo n th e Respirato rLo g Shee t(Appendi xD 1 an d D2) . Thes e lo g sheet s ar e attache d t o th e sid e o fth e boxe s i n whic h th e respirator s ar e stored . 8 . Designate d Workspace : Employee s wit h occupationa l exposur e ma yonl yhandlin g labqr^|SF^''^emical s i n th e followin g locations : a . Bacti-la b b . La b 2 c . La b 3 Onl yth e Bacti-la b an d La b 3 ca n b e use d whe n handlin g hazardou s chemical s tha t releas e toxi cvapors . Thes e are th e onl ytw o laboratorie s equippe d wit h adequat e ventilation . 9 . Receivin g an d Storag e A tthi s facility , th e Shippin g Cler k mus tkno wth e Hazard Symbol s an d NFP AWarnin g Diamond s printe d o n incomin g laboratorychemicals . Whe n appropriate , PP E mus tb e wor n whe n handlin g hazardou s chemicals . Th e storag e o fa chemica l i s dependen to n it s handlin g an d storag e instruction s state d o n th e MSDS . Th e MSD S wil l outlin e th e appropriat e environment , compatibl e chemical s an d incompatibl e chemical s wit h whic h a laboratorychemica l ma yo rma yno t b e stored . Befor e a laborator ychemica l ca n b e store d i n a n area , th e followin g guideline s shoul d b e observed : a . Hav e ful l knowledg e o fa laboratorychemical' s storag e condition s a s state d i n th e MSDS . b . Inspec tth e potentia l storag e are a fo ran ychemica l an d physica l incompatibilities . (EX. ) Isopropy l alcoho l ca n no tb e store d nea ra n ope n flame . c . Remov e an ychemica l o rphysica l incompatibl e substance s fro m th e potentia l storag e site . 10 . Hazardou s Wast e Disposal : Th e onl ytyp e o fhazardou s wast e generate d a tthi s facilit yi s a chlorofor m raffinate . T o insur e minima l har m t o employee s wit h occupationa l exposur e an d t o th e environment , th e followin g guideline s mus tb e observe d whe n handlin g chlorofor m raffinate : a . Alway s wea radequat e an d appropriat e PP E a s state d i n th e MSD S (e.g . late x gloves , la b coat , respirator )CHEMICA LHYGIEN E PLA N FO R S.O.P . SF-0025-0 2 PAG E 6

LABORATOR YDIAGNOSTICS/CENOGENIC S



### b . Neve rpou rth e chlorofor m raffinat e dow n th e drain . c . Alway s remov e th e chlorofor m raffinat e immediatel yfro m th e workspac e t o a designate d area . A tthi s facility , th e designate d are a i s locate d outsid e th e Machin e Room . Afifty-fiv e gallo n stee l dru m ha s bee n designate d fo r chlorofor m raffinat e disposal . I ti s cleari ymarke d wit h a n orang e an d whit e "Hazardou s Waste " sign . d . Contac ta Superviso rwhe n th e stee l dru m i s hal fful l s o tha tth e hazardou s wast e cartag e compan y(Mariso l Inc. ) ca n b e notifie d o fa pick-up . 

# i Th e leve l o fchlorofor m raffinat e i n th e stee l dru m ca n no texcee d "^S B gallons . A woode n dipstic k

ha s bee n calibrate d t o 2 5 gallon s an d mus tbj^ii||r a whe n determinin g th e amoun to fhazardou s wast e presentl yi n th e stee l d^ffif.^pn e calibrate d woode n dipstic k i s marke d a s "Chlorofor m Raffinat e Dipstick " ai^^fore d behin d th e Machin e Roo m entrance . 11 . Housekeepin g o y Thi s facilit ywil l b e maintaine d i n suc h a wa ya s t o provid e a>Bleii n an d saf e workplace . Th e followin g shal l b e instituted : a . Regula rfloo rcleaning s b . Regula rremova l o ftras h c . Informa l inspection s o fth e facilit y d . Calibration/maintenanc e schedul e - al l safet yequipmen twil l b e calibrate d and/o rinspected . Documentatio n wil l b e kep ti n th e Calibratio n Schedulin g Fil e an d th e Equipmen tFil e fo reac h piec e o fsafet yequipment . i . Eye wash/Showe r- inspection s accordin g t o th e manufacturer s instructions , ii . Respirator s - Inspection s accordin g t o th e manufacturer s instructions , iii . Laboratoryhood s - Annua l inspections/calibration s b yMedica l Repai r Laboratories , iv . Fire Extinguisher s - Annua l inspection s performe d b yth e Maribor o Townshi p Fire Department . V . Ventilatio n Fa n - Periodicall yinspecte d t o chec k efficienc yo fai r draw . e . Clea rpassageway s throug h hallway s shal l b e maintained . Hallway s are no tb e use d as storag e areas . 12 . Spill s an d Accident s I fa spil l o racciden tdoe s occur , th e followin g step s mus t b e taken : a . Contac ta superviso rimmediately . b . Refe rt o th e specifi cMSD S fo rth e prope rclean-up , disposa l an d medica l procedures . Al l MSDS' s wil l hav e a sectio n outlinin g emergenc yprocedures ; however , i n genera l th e followin g shoul d b e exercised :• ^ CHEMICA LHYGIEN E PLA N FO R S.O.P . SF-0025-0 2 PAG E 7

LABORATOR YDIAGNOSTICS/CENOGENIC S



### i . Ey e Contac t- Promptl yflus h eye s wit h wate rfo ra prolonge d perio d o ftim e an d see k

medica l attention , ii . Ingestio n - Encourag e th e victi m t o drin k larg e amount s o fwater , iii . Ski n Contac t - Promptl yflus h th e affecte d are a wit h wate ran d remov e an ycontaminate d clothing , iv . Clean-U p - Promptl yclea n u p spill s usin g appropriat e PP E an d disposa l means . ^^W^^-' " 

### 13 . Fire Plan/EmergencyContac tjem?^^^ ' Throughou tth e laborator yan d warehous e are Fire Evacuatio^^q^^F^l^n s i n eac h o fth e rooms . Th e Fire Evacuatio n Rout e Pla n i s specifi cfo readSr^iln , outlinin g th e safes t rout e fo rtha tlocatio n (Appendi xE 1 an d E2) . " . \ Al l exit s are cleari ymarke d wit h re d an d whit e "Exit " signs . r\V\ Vv^ - Al l doorway s tha td o no tlea d t o a n exi tare cleari ymarke d with'^i^e d an d whit e "N o Exit " signs . A teac h telephone . Emergencynumber s are clearlymarke d wit h orang e an d whit e "Police , Fire , Ambulance " labels . Al l employee s a tthi s facilit ywil l b e traine d i n th e usag e o fth e fir e extinguisher s b y Jerse yCoas tFir e Company . Ne wemployee s wil l b e traine d b ythei rsupervisor . Thei r trainin g wil l b e documente d o n th e In-Hous e Fire Extinguishe rTrainin g Documen t (Appendi xG) . 14 . Medica l Pla n A tthi s facility , wheneve ra n employe e wit h occupationa l exposur e develop s sign s o r symptom s associate d wit h a hazardou s chemical , tha temploye e wil l b e provide d wit h th e opportunit yt o receiv e medica l attention . Ai l medica l examination s an d follow-u p consultation s shal l b e performe d b ya license d physicia n a tn o cos tt o th e employee , withou t loss o fpa yan d a t a reasonabl e tim e an d place . Th e employe rmus trecor d a n employee' s wor k relate d acciden to n th e OSH A20 0 For m an d kee p th e for m file d unti l February1 , whe n i t the n i s poste d i n a publi care a unti l Marc h 1 (Appendi xF) . Th e followin g informatio n mus tb e provide d t o th e physicia n b ya supervisor : a . identit yo fth e hazardou s chemical(s ) t o whic h th e employe e ma yhav e bee n exposed .CHEMICA LHYGIEN E PLA N FO R S.O.P . SF-0025-0 2 PAG E 8 N LABORATOR YDIAGNOSTICS/CENOGENIC S



### b . Adescriptio n o fth e condition s whic h th e exposur e occ u c . Adescriptio n o fan ysign s o rsymptoms . | Th e employe rshal l obtai n a writte n opinio n fro m th e examiningQJ|)y^ia n whic h shal l includ e th e following : a . An yrecommendatio n fo rfurthe rmedica l follow-up . b . Th e resul to fth e medica l examinatio n an d an yassociate d tests . c . An ymedica l conditio n whic h ma yb e reveale d i n th e examinatio n whic h may plac e th e employe e a trisk a s a resul t o fexposur e t o a hazardou s workplace . d . Astatemen ttha tth e employe e ha s bee n informe d b yth e physicia n o fth e result s o fth e consultatio n o rmedica l examinatio n an d an ymedica l conditio n tha tma yrequir e furthe rexaminatio n o rtreatment . e . Th e writte n opinio n shal l no trevea l specifi cfinding s o fdiagnoses unrelate d t o occupationa l exposure . 15 , Informatio n an d Trainin g A tthi s facilit yal l employee s wit h occupationa l exposur e wil l b e adequatel yinforme d abou tth e wor k

i n th e laboratory , it s risks an d wha tt o d o i fa n acciden toccurs . Suc h informatio n shal l b e provide d a tth e tim e o fa n employee' s initia l assignmen tt o a wor k are a wher e hazardou s chemical s are presen tan d prio rt o assignment s involvin g ne wexposur e situations . Th e employee s shal l b e informe d of : a . Th e content s o f2 9 CF P Part1910.1450 . b . Th e content s o fthi s Chemica l Hygien e Plan . c . Al l MSDS' s associate d wit h hazardou s chemicals . Thi s wil l includ e th e followin g information : i . Permissibl e exposur e limit s fo rOSHA . ii . Sign s an d symptom s associate d wit h exposur e t o hazardou s chemicals , iii . Method s an d observation s tha t ar e use d t o detec tth e presenc e o r releas e o fa hazardou s chemical , iv . Th e physica l an d healt h hazard s o fa hazardou s chemical . V . Appropriat e PPE . vi . Appropriat e wor k practices , vii . Emergencyprocedures . d . Measure s tha tare take n fo rmedica l examination s an d consultations . Th e employee s shal l b e traine d in : a . Th e prope rus e o fth e fir e extinguishers , "Survivair " an d "Flexi-Star " respirator s an d Firs tAid . Trainin g record s wil l b e documente d an d kep to n fil e unde rthi s Chemica l Hygien e Plan .CHEMICA LHYGIEN E PLA N FO R S.O.P . SF-0025-0 2 PAG E 9

LABORATOR YDIAGNOSTICS/CENOGENIC S



### b . Readin g an d understandin g a n MSDS . c . Hazard Label s an d NFP Aidentification . d . Recognizin g th e releas e o fhazardou s chemical s i n th e workplace . e . Recognizin g sign s an d symptom s associate d wit h a hazardou s chemica l exposure . f . Hazardou s Wast e disposal . g . Escap e route s durin g a fir e evacuation . ; y> Th e individua l conductin g th e trainin g shal l b e knowled^i^bl e o fiJis^^ytmo tmatter . Employee s mus tsig n a Trainin g Documen tstatin g thS^Tn^i e receive d trainin g i n thi s Chemica l Hygien e Pla n an d understan d ho wi tpertain s t o thei rwor k environmen t (Appendi xH) .CHEMICA LHYGIEN E PLA N FO R S.O.P . SF-0025-0 2 PAG E 1 0

LABORATOR YDIAGNOSTICS/CENOGENIC S 

# ^3'"" % Reference s "Exposur e t o Hazardou s Chemica l i n Laboratories" , U.S . Dept . gf^f ^ &'t)ccupationa l Safet yan d Healt h Administration , OSH A3119 , 1989 , pp . "Hazar d Communicatio n : AComplianc e Kit"" , McLaughlin , An n (U.€r?yp^t.^vrLabor ) an d Pendergrass , Joh n A . (Occupationa l Safet yan d Healtf>0«a(^imstration) , OSH A 3104 , 1988 , pp . A 1 - J5 . V) ^ Standar d title : Occupatio n Exposur e t o Hazardou s Chemica l i n Laboratories . Standar d number : 1910.145 0 Standar d title : Nationa l Researc h Counci l Recommendation s Concernin g Chemica l Hygien e i n Laboratorie s (non-Mandatory) . Standar d number : 1910-145 0 Ap p A .

### ATTACHMEN T4 CENOGENIC S CORPORATIO N GENERA LOPERATION S # ^ ' ^



### BLOODBORN E PATHOGEN S EXPOSUR E CONTRO LPLA N *" - ^^^ ^ Procedur e Prepare d b yy.-1^^AfJ:/7^.,^sA^-'''^^ ^ Date_^jw^^SOP : SF-0023-0 2 Procedur e Approve d b y/%:,<y4j ^ fyi^& " DaXe^JJll^^Z ^ Supersedes : SF-0023-0 1 A . Introductio n Th e OSH ABloodborn e Pathogen s Standard , 2 9 CF R 1910.1030 , detail s th e prope r procedure s tha tmus tb e practice d a tfacilitie s tha thandl e potentiall yinfectiou s materials . A tthi s facility , potentiall yinfectiou s material s ar e define d a s an ywhol e blood , plasma , o r seru m o fhuma n origin . Befor e an ypotentiall yinfectiou s material s ca n b e accepte d a tthi s facility , a n HIV/HBV/HC Vcertificatio n mus t b e received . Al l potentiall yinfectiou s material s are teste d fo rHIV/HBV/HC Vb yFD Aapprove d method s an d guarantee d b ylicense d broker s t o b e negativ e fo rthes e bloodborn e diseases . Nevertheless , th e genera l precaution s outline d i n thi s Exposur e Contro l Pla n mus tb e followe d whe n handlin g potentiall y infectiou s materials . B . Purpos e Th e purpos e o fthi s pla n i s to : 1 . Eliminat e o rminimiz e th e potentia l hazar d fro m exposur e t o potentiall yinfectiou s materials . 2 . Compl ywit h th e OSH ABloodborn e Pathogen s Standard , 2 9 CF R 1910.1030 . C . Exposur e Determinatio n A tthi s facilit yonl ysom e o fth e employee s hav e occupationa l exposure . Th e followin g jo b classification s an d task s are listed : 1 . Productio n Superviso ran d LaboratoryTechnicians : Direc thands-on - contac t wit h a variet yo fhuma n sera , eithe rnorma l o rpositiv e fo rspecifi canalytes . 2 . Packagin g Crew : Dispensin g a variet yo fcontro l ser a int o reagen tbottles .BLOODBORN E PATHOGEN S S.O.P . SF-0023-0 2 PAG E 2 ^ EXPOSUR E CONTRO LPLA N



### 3 . LaboratoryAssistant : Washin g decontaminate d glassware^<N^I||^i^e"labware , an d othe rlabwar e apparatus . ^ ' \'N!' C 

### V^ ^ D . Implementatio n Schedul e an d Methodolog y^ ' ;^-' ^

\? i Engineerin g an d wor k

practic e control s wil l b e utilize d t o eliminateng rminimiz e exposur e o femployee s a tthi s facility . Th e followin g control s wil l b e utilized : 1 . Genera l Principle s fo rWorkin g wit h Potentiall yInfectiou s Material s i n th e Laboratory 2 . Availabl e Persona l Protectiv e Equipmen t (PPE ) 3 . Additiona l Protectio n (ie . Hood , U VLight , Disinfectants ) 4 . Launderin g o fPP E 5 . Housekeepin g 6 . Regulate d Wast e 7 . Bloo d Drawin g Needl e Disposa l 8 . Labelin g 9 . Hepatiti s B Vaccinatio n 10 . Exposur e Inciden t 11 . Informatio n an d Trainin g 1 . Genera l Principle s fo rHandlin g Potentiall yInfectiou s Material s i n th e Laboratory Th e followin g genera l guideline s shoul d b e observe d whe n handlin g potentiall yinfectiou s materials : a . Neve rtouc h you rfac e o rmout h i n th e laboratory . b . Alway s us e persona l protectiv e equipmen twhe n handlin g potentiall yinfectiou s materials . c . Alway s was h hand s thoroughl ywit h a germicida l soa p afte reac h procedure , especiall ybefor e usin g th e restroom s o reating . Germicida l soap s ar e foun d i n bot h ^ restrooms , th e Bacti-La b an d La b 3 .BLOODBORN E PATHOGEN S S.O.P . SF-0023-0 2 PAG E 3

EXPOSUR E CONTRO LPLA N 

### d . Eating , drinking , gu m chewin g o rapplyin g cosmetic s i n th e labora^ol^^^pltthibited . Smokin g i s prohibite d i n al l area s o fth e laboratory , fron toffiq^lXVi^\Jt^irehouse . e . Confin e lon g hai ran d loos e clothing . \ J ^ g f . Contac tlense s canno tb e wor n whe n handlin g potentiall^|^|^^08'm«erials . I f contac tlense s ar e necessary , goggle s mus tb e worn . | | ^ - ' g . D o no twea rsandals , perforate d shoe s o ropen-toe d shoe s i n th e laboratory . Neve r wal k barefoote d i n th e laboratory . h . Neve rmout h pipe tpotentiall yinfectiou s materials . i . An ymisconduc ttha twil l startl e anothe remployee , resultin g i n spillin g a potentiall y infectiou s materia l i s prohibited . j . Neve rus e damage d glassware . k . Alway s repor tspill s an d accident s t o a superviso rimmediately . 2 . Persona l Protectiv e Eguipmen t(PPE ) Employee s havin g occupationa l exposur e are require d t o us e PP E whe n handlin g potentiall yinfectiou s materials . A tthi s facilit yth e followin g item s ar e available : a . Launderabl e la b coats , gowns , an d smocks . b . Disposabl e an d steril e wrappe d gloves . c . Fac e shields , fac e masks , goggles . Employee s havin g occupationa l exposur e mus tobserv e th e followin g precaution s fo r usin g PPE : a . Alway s remov e PP E befor e leavin g thi s facility . Neve rbrin g hom e PP E tha t ha s bee n wor n i n th e cours e o fth e day . b . Plac e PP E i n appropriatel ydesignate d area s afte rusage . i. ) La b Coats , gowns , an d smock s ar e t o b e hun g o n th e coa trac k outsid e th e entranc e t o th e laboratory . Persona l clothin g canno tb e hun g o n th e sam e coa track . Persona l clothin g wil l b e hun g i n th e fron toffic e closet . I f la b coats , gowns , o rsmock s hav e com e i n contac twit h potentiall y infectiou s material s (i.e . spills , splashes) , the ymus tb e treate d a s i n Sectio n D , No . 4 , Laundering .BLOODBORN E PATHOGEN S S.O.P . SF-0023-0 2 \ \ PAG E 4 EXPOSUR E CONTRO LPLA N \ ^ '

"•'""•• .' ' V 'v'^s-^ '

* •••• , : . •-•,-* . ^ • 

### ii. ) Goggles , fac e shields , an d fac e mask s ar e kep tU i 1[be , l^act i Roo m an d Loadin g Room . I fth e goggle s o rfac e sl^ ^ ""i&bme i n contac twit h potentiall yinfectiou s material s (ie . spills , splashes) , the yshoul d b e wipe d clea n wit h a n appropriat e disinfectan t(Sectio n D , No . 5 , Housekeeping ) o r expose d t o U Vligh tovernight . I fth e fac e mask s shoul d com e i n contac t wit h potentiall yinfectiou s materials , the yshoul d b e immediatel yremove d an d place d i n a "Biohazard " bag . iii. ) Neve rwas h o rdecontaminat e disposabl e glove s fo rreuse . Afte rusage , plac e i n "Biohazard " bag s an d autoclav e fo r3 0 minute s a t121 ° C . iv. ) Utilit yglove s an d dishwashin g glove s mayb e decontaminate d fo rreus e i f th e integrit yo fth e glov e ha s no tbee n change d i n an yway . Discar d i f cracking , peeling , tearing , o rpuncturin g i s present . V. ) Alway s was h hand s whe n glove s are remove d an d befor e enterin g th e bathroom s o rlunchroom . 3 . Additiona l Protectio n Employee s havin g occupationa l exposur e mus tlimi t thei rwor k wit h potentiall yinfectiou s material s t o thos e room s equippe d wit h Additiona l Protection . Additiona l protectio n i s define d fo rthi s facilit ya s havin g on e o ral l o fth e following : a . Room s equippe d wit h U Vlights . b . Room s equippe d wit h biologica l hoods . c . Room s equippe d wit h a ful l bottl e o fa n appropriat e disinfectan t(Sectio n D , No . 5 , Housekeeping) . Th e onl yroom s i n thi s facilit ytha tca n b e use d fo rhandlin g potentiall yinfectiou s material s are : a . Bact i Roo m b . La b 2 c . La b 3 d . Loadin g Roo m 4 . Launderin g o fPP EBLOODBORN E PATHOGEN S S.O.P . SF-0023-0 2 PAG E 5

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### Employee s wit h occupationa l exposur e canno t remov e thei rlabcoats,r^dy^i^sX^ rsmock s fro m thi s facilit yt o tak e hom e an d launder . v^^-^A)*^^ Weekl ylaunderin g o fla b coats , gowns , an d smock s wil l tak e plac e a tno^^^cg^. ^ th e employee s wit h occupationa l exposure . Ever yFrida yla b coats , gg^^ ^ liti^^a^ i wil l b e place d i n th e "Biohazard " bi n i n th e Furnac e Roo m an d wil l b e il^d^^iiu^h e employee s b yth e followin g Monday . Newl ylaundere d PP E wil l b e store d o n th e shel fabov e th e coa t rac k outsid e th e laborator yentrance . I fth e la b coat s an d gown s ar e no tread yfo rth e employee s o n th e followin g Monday , the n thes e item s wil l b e provide d b yth e employe ra t n o cos tt o th e employee . I fa n acciden toccur s (ie . spill , splash ) wher e a la b coat , gown , o rsmoc k i s penetrate d b y a potentiall yinfectiou s material , the n th e garmen tmus tb e remove d immediatel yan d place d i n th e "Biohazard " bin . Areplacemen tla b coa to rgow n wil l b e provide d fo rth e employee . 5 . Housekeepin g Availabl e t o th e employee s wit h occupationa l exposur e ar e disinfectant s wit h germicidal , fungicidal , an d virucida l properties . Thes e includ e 2 % Lysol , 70 % Isopropy l alcohol , an d 1 % Sodiu m hypochlorit e solution s ( househol d bleac h dilute d 1:5) . Thes e disinfectant s mus tb e use d t o clea n item s tha thav e ha d contac twit h potentiall yinfectiou s materials . A tthi s facility , PP E mus tb e wor n whil e cleanin g wit h on e o fth e abov e mentione d disinfectant s i n th e followin g situations : a . Al l equipmen tan d wor k surface s tha thav e com e i n contac twit h potentiall y infectiou s material s mus tb e soake d o rwipe d down . Thi s include s al l glassware , pipets , Nalgen e bran d labware , countertops , biologica l hoo d benches , an d floor s (i f spill s occur) . b . Protectiv e covering s suc h a s parafilm , autoclav e paper , o raluminu m foi l shoul d b e place d i n a n autoclavabl e "Biohazard " bag . Th e ba g shoul d b e place d unde rU V ligh tovernigh to rautoclave d fo r3 0 minute s a t121 ° C . Th e counte rto p belo wth e protectiv e covering s shoul d b e wipe d dow n an d replace d wit h a ne wcovering . c . Ai l material s use d i n cleanin g a spil l (i.e . rags , towels , sponges ) mus t b e thoroughl y soaked , expose d t o U Vligh tovernight , o rimmediatel yplace d i n a n autoclavabl e "Biohazard " ba g an d autoclave d fo r3 0 minute s a t121 ° C . d . Al l glassware , Nalgen e bran d labware , an d filte rpres s apparatus , mus t b e filled , sprayed , o rflushe d an d place d i n a n autoclavabl e basi n befor e bringin g t o th e sink . e . Reusabl e receptacles , suc h as , basins , pails , o rcan s tha t hav e com e i n contac twit h potentiall yinfectiou s material s mus t b e wipe d dow n afte reac h use .BLOODBORN E PATHOGEN S S.O.P . SF-0023-0 2 PAG E 6

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# .c\\^\ ^ f . Broke n glas s shoul d b e spraye d an d picke d u p wit h tongs , forcep^i<^%.brus h an d dustpan . Th e broke n glas s wil l b e place d i n a n "Biohazai^SMj^^i^^tddlave d fo r 3 0 minute s a t121 ° C . Th e item s use d t o pic k u p th e bi^^^l^ s wil l b e spraye d o rwashe d dow n an d place d unde rU Vligh tovernight . g . Al l filte rpresses , Cornwal l syringes , loadin g hoses , an d glas s connecto rtube s mus t b e flushe d an d soake d wit h a n approve d disinfectan tbefor e the yca n b e brough t t o th e sink . h . Glas s o rplasti cslide s mus tb e soake d befor e the yca n b e brough tt o th e sink . A slid e bucke twit h a n approve d disinfectan tshoul d b e prepare d ahea d o ftim e whe n anticipatin g th e us e o fglas s slide s wit h potentiall yinfectiou s materials . 6 . Regulate d Wast e Locate d i n th e Bacti-Lab , La b 2 , an d La b 3 ther e i s a n 8 1/2 " x11 " autoclavabl e "Biohazard " ba g basket . Thes e autoclavabl e "Biohazard " ba g basket s ar e t o b e use d fo r th e disposa l o fpipe ttips , dispenstirs , woode n mixin g sticks , an d cultur e tube s tha t hav e ha d contac twit h potentiall yinfectiou s materials . Als o availabl e ar e 12 " x24 " an d 24 " x36 " autoclavabl e "Biohazard " bag s tha tshoul d b e use d fo rlarge rvolume s o fwast e tha thav e com e i n contac twit h potentiall yinfectiou s materials . Item s tha tmus tb e autoclave d wil l follo wthes e guidelines : a . Onl yth e abov e mentione d autoclavabl e "Biohazard " marke d bag s ca n b e used . b . Autoclavabl e "Biohazard " bag s mus tb e securel yclose d wit h autoclavabl e tape ; however , a vente d openin g mus tb e allowed . c . Al l autoclavabl e "Biohazard " bag s mus tb e place d i n a n autoclavabl e basi n t o avoi d leakage . d . Onc e th e autoclavabl e "Biohazard " bag s hav e bee n autoclave d fo r3 0 minute s a t 121 ° C , the n the yma yb e place d i n th e regula rtrash . e . I fwast e materia l ha s bee n expose d t o U Vligh tovernight , i tma yb e place d i n th e regula rtras h i fdisposable , o rbrough tt o th e sin k i fwashable .BLOODBORN E PATHOGEN S S.O.P . SF-0023-0 2

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### 7 . Bloo d Drawin g Needl e Disposa l ri^" ^ W WA' ' • 

### Disposabl e needle s shal l b e discarde d immediatel yo ra s soo n a s possibl e i n a re d "Biohazard " containe rtha tha s a one-wa ylock-tigh tlid , i s puncture-resistan t plastic , an d ha s lea k proo fseams . Thi s containe rwil l b e maintaine d uprigh tan d no t allowe d t o overflow . Ful l container s wil l b e autoclave d fo r3 0 minute s a t121 ° C an d discarde d i n th e regula rtrash . Th e re d "Biohazard " containe rshal l b e easil yaccessibl e t o employee s wit h occupationa l exposur e an d locate d onl yi n La b 3 , wher e bloo d drawin g occurs . 8 . Labelin g Fluorescen torang e o rorange-re d "Biohazard " label s wil l b e affixe d t o al l refrigerator s an d freezer s containin g potentiall yinfectiou s materials . Thes e label s wil l war n al l employee s ( includin g thos e employee s wit h n o occupationa l exposure ) tha tfoo d an d drink s canno t b e store d i n th e "Biohazard " labele d refrigerator s o rfreezers . Th e sam e "Biohazard " label s wil l als o b e affixe d t o th e laundrybi n an d t o disposabl e needl e container . 9 . Hepatiti s B Vaccin e Thi s facilit ywil l mak e availabl e th e Hepatiti s B vaccin e t o th e employee s wit h occupationa l exposure . Th e Hepatiti s B vaccinatio n serie s wil l be : a . Mad e availabl e a tn o cos t t o th e employee . b . Mad e availabl e t o th e employe e a t a reasonabl e tim e an d place . c . Performe d b ya license d physician . d . Provide d accordin g t o th e recommendation s o fth e U.S . Publi cHealt h Service . e . Offere d afte rth e employe e ha s receive d inciden texposur e training . Documentatio n o fth e Hepatiti s B vaccinatio n serie s wil l b e maintaine d fo ral l employee s wit h occupationa l exposure . i fa n employe e wit h occupationa l exposur e decline s th e Hepatiti s B vaccinatio n serie s offered , the n h e o rsh e mus tsig n th e OSH Arequire d waive rindicatin g thei rrefusa l (Se e Appendi xA) . However , i fth e employe e a ta late rdat e decide s t o accep tth e vaccination , th e vaccinatio n shal l the n b e mad e available . Documentatio n o fth e vaccinatio n waiver s wil l b e maintaine d fo ral l employee s wit h occupationa l exposure .BLOODBORN E PATHOGEN S S.O.P . SF-0023-0 2 PAG E 8

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### 10 . Exposur e Incident s - ' 

# l # ^ A n exposur e inciden ti s define d as : •**> • M •^^i ^ 

### A n acciden tresultin g i n a potentiall yinfectiou s materia l enterin g a n employee' s eyes , nose , mouth , o rope n woun d i n th e ski n vi a splashing , spilling , bein g cu tb ybroke n glass , o rbein g stuc k

wit h a needle . I fa n exposur e inciden tdoe s occur , th e employe e wil l b e offere d a confidentia l medica l examinatio n an d a pos texposur e follow-u p a tn o cos tt o th e employee . Thes e are th e step s tha tmus tb e take n i fth e employe e consent s t o medica l care : a . Acop yo fTh e Bloodborn e Pathogen s Standard , 29CF R 1910.1030 , an d a n Exposur e Inciden tReport(Se e Appendi xB ) mus t b e complete d b ya superviso r an d give n t o th e attendin g license d physician . b . Bloo d testin g t o determin e HBV , HC Vo rHI Vinfectivit yonl yi fth e employe e consents . c . Th e superviso rshal l obtai n an d provid e th e employe e wit h a cop yo fth e evaluatin g physician' s writte n opinio n withi n 1 5 day s o fth e completio n o fth e evaluation . Th e writte n opinio n o fth e physicia n ma yonl ycontai n th e followin g information : i. ) Astatemen ttha tth e employe e ha s bee n informe d o fth e results . ii. ) Astatemen ttha tth e employe e ha s bee n tol d abou tan ymedica l condition s whic h requir e furthe revaluatio n o rtreatmen tresultin g fro m th e exposur e t o potentiall yinfectiou s materials . d . Al l documentatio n pertainin g t o a n exposur e inciden t wil l b e maintaine d i n bot h th e OSH Aan d Employe e Files . 11 . Informatio n an d Trainin g Employee s wit h occupationa l exposur e wil l receiv e informatio n an d trainin g o n th e following : a . Acop yo fthi s Exposur e Contro l Pla n an d th e OSH ABloodborn e Pathogen s Standard , 2 9 CF R 1910.1030 . b . A n explanatio n o fth e task s tha tma yinvolv e exposure .BLOODBORN E PATHOGEN S S.O.P . SF-0023-0 2 PAG E 9

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## -\ n

c . A n explanatio n o n ho wt o reduc e exposur e b yusingrPP^ ) " Tt ^ ' ' d . Ademonstratio n o n ho wt o us e PP E correctly . ,. , ;^J;C e . Hand-out s tha tdiscus s epidemiolog yan d mode s o ftr^p;i»mh^\) fbloodborn e pathogen s (Appendi xE) . f . Hand-out s tha tdetai l informatio n o n th e Hepatiti s B vaccinatio n serie s regardin g it s purpose , benefits , sid e effects , numbe ro fvaccination s (Appendi xD) , an d declinatio n statemen t(Appendi xA) . g . Adiscussio n o fth e procedure s t o follo wi fa n exposur e inciden toccurs . Th e individua l conductin g th e trainin g shal l b e knowledgeabl e o fth e subjec tmatter . Employee s mus tsig n a Trainin g Documen tstatin g the yhav e receive d trainin g i n thi s Exposur e Contro l Pla n an d it s Appendices , an d understan d ho wi tpertain s t o thei rwor k environmen t(Appendi xC) .BLOODBORN E PATHOGEN S S.O.P . SF-0023-0 2 PAG E 1 0

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### Reference s ^vS ' 

### 1 . "Draf tSampl e Written : Bloodborn e Pathoge n Exposur e Contro l ^^ro#^6lnplianc e wit h OSH AStandar d 2 9 CF R 1910.1030" , W l Dept . o fHealt h an d Socia l Service s (Sectio n o f Occupationa l Health) , 1992 , pp.1-17 . 2 . "Hepatiti s B Vaccin e (Vaccines , Viral)" , Fact s an d Comparisons , Novembe r1989 , pp . 467a-468 . 3 . "Hepatiti s B , ADiseas e i n Nee d o fPrevention, " Merc k an d Co. , 1991 , pp . 1-12 . 4 . Occupationa l Exposur e t o Bloodborn e Pathogens ; Fina l Rul e (2 9 CF R Part1910.1030) . Federa l Register . Vol . 58 , No . 235 , Dec . 6 , 1991 , pp.64175-64182 . 5 . "Occupationa l Exposur e t o Bloodborn e Pathogens" , U.S . Dept . o fLabo ran d Occupationa l Safet yan d Healt h Administration , OSH A3127 , 1992 , pp . 1-22 .BLOODBORN E PATHOGEN S S.O.P . SF-0023-0 2 PAG E 1 1

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### APPENDI XA

HEPATITI S B VACCINATIO N DECLINATIO N STATEIVtt N ..... . i: J\XV i - l

''•':.'* ' y 0 

### I understan d tha tdu e t o m yoccupationa l exposur e t o bloo d o rothe rpotentiall yinfectiou s material s I ma yb e a trisk o facquirin g hepatiti s B viru s (HBV ) infection . I hav e bee n give n th e opportunit yt o b e vaccinate d wit h th e hepatiti s B vaccine , a tn o charg e t o myself . However , I maydeclin e hepatiti s B vaccinatio n a tthi s time . I understan d tha tb ydeclinin g thi s vaccin e I continu e t o b e a trisk o facquirin g hepatiti s B , a seriou s disease . I fi n th e futur e i continu e t o hav e occupationa l exposur e t o bloo d o rothe rpotentiall yinfectiou s material s an d I wan tt o b e vaccinate d wit h th e hepatiti s B vaccine , I ca n receiv e th e vaccinatio n serie s a tan ytim e an d a tn o charg e t o me .

Employe e signatur e Dat e

Superviso rsignatur e Dat e^ BLOODBORN E PATHOGEN S S.O.P . SF-0023-0 2 PAG E 1 2

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### APPENDI XB

, -•(=:' •• • \ f^. \r 

### EXPOSUR E INCIDEN TREPOR To(^V^ ' \

p \ y , Dat e o fexposur e incident: . Nam e o femployee : Nam e o fsuperviso ri twa s reporte d to : Employee' s dutie s a tth e tim e o fth e exposur e incident :

Rout e o fexposure :

Actio n Taken : Ha s th e employe e receive d th e Hepatiti s vaccinatio n series ? Ye s N o Amedica l examinatio n an d post-exposur e follow-u p examinatio n ha s bee n offere d t o m e a s a resul to fa n exposur e inciden ti n whic h I wa s involved . I hav e accepte d I hav e decline d ai l medica l consultation s offere d t o m e b yLaborator yDiagnostics/Cenogenics . Employe e signatur e Date _ Superviso rApprova l Dat e^ BLOODBORN E PATHOGEN S S.O.P . SF-0023-0 2 PAG E 1 3

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### APPENDI XC TRAININ G DOCUMEN T I hav e receive d th e Informatio n an d Trainin g o n th e Bloodborn e Pathoge n Exposur e Contro l Pla n fo rLaborator yDiagnostics/Cenogenics . I receive d th e followin g informatio n an d trainin g i n th e session : 1 . Acop yo fthi s Exposur e Contro l Pla n an d th e Bloodborn e Pathogen s Standard , 2 9 CF R 1910.1030 . 2 . A n explanatio n o fth e task s tha t mayinvolv e exposur e t o potentiall yinfectiou s materials . 3 . A n explanatio n o n ho wt o reduc e exposur e b ywearin g PPE . 4 . Ademonstratio n o n ho wt o us e PP E correctly . 5 . Adiscussio n take n fro m Appendi xC o n th e epidemiolog yan d mode s o f transmissio n o fbloodborn e pathogens . 6 . Adiscussio n take n fro m Appendi xD o n th e Hepatiti s B vaccinatio n serie s regardin g it s purpose , benefits , sid e effects , numbe ro fvaccination s an d declinatio n statement . 7 . Adiscussio n o n th e procedure s t o follo wi n cas e a n exposur e inciden toccurs . A s a n Employe e wit h occupationa l exposur e I a m awar e o fan d understan d th e safet y measur e I shoul d execut e whe n handlin g potentiall yinfectiou s materials . I hav e rea d an d understan d th e Exposur e Contro l Pla n fo rthi s facility . I hav e ha d a n opportunit yt o as k question s an d hav e the m answered . I als o understand , tha tI ma ya tan ytime , as k question s o fm yimmediat e superviso rpertainin g t o prope rsafet yprocedure s o ran yothe r topi cdiscusse d i n th e training . Employe e signatur e Dat e Superviso rapprova l Dat eBLOODBORN E PATHOGEN S S.O.P . SF-0023-0 2 PAG E 1 4

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### APPENDI XD fO^ k HEPATITI S B VACCINATIO N _^w . %'^ V Introductio n Th e Hepatiti s B vaccinatio n serie s offere d b yLaboratoryDiagnostics/Cenogenic s wil l b e administere d b ya license d physicia n a ta loca l medica l facility . Th e vaccinatio n serie s i s provide d t o employee s wit h occupationa l exposur e a tn o cos tan d a ta convenien ttim e an d place . Th e employe e ha s th e rightt o declin e th e vaccinatio n series , however , th e employe e ma yop ta ta late rdat e t o hav e th e vaccinatio n serie s administere d a tn o cos tan d a ta convenien ttim e a tinsta-Care . Backgroun d Ther e ar e tw o varietie s o fth e Hepatiti s B vaccine . Bot h type s o fthi s vaccin e hav e bee n show n t o induc e protectiv e antibodie s agains tHepatiti s B infectio n i n individual s wh o hav e receive d th e three-sho tvaccination . Bot h type s o fth e Hepatiti s B vaccin e hav e bee n prove n t o las tfo ra tleas tfiv e year s i n individual s receivin g th e three-sho t vaccination . Finally , dat a ha s als o show n tha t th e transmissio n o fAI D b yth e Hepatiti s B vaccinatio n doe s no texis tfo reithe rvaccin e type . Administratio n o fth e Hepatiti s B Vaccin e Th e Hepatiti s B vaccin e consist s o fa serie s o fthre e injections . Thes e injection s ar e give n i n th e deltoi d muscl e o fth e uppe rarm . Th e vaccinatio n schedul e consist s o fa n initia l injection , anothe rinjectio n on e mont h later , an d a fina l injectio n si xmonth s fro m th e initia l injection . Al l thre e injection s mus tb e administere d fo rthi s vaccinatio n t o b e effective . Aschedul e o fth e employee' s injection s wil l b e maintaine d b yth e medica l car e facilit yan d als o i n ou rEmploye e Files . Benefit s o fth e Hepatiti s B Vaccin e Th e Hepatiti s B vaccinatio n serie s provide s activ e immunit yagains tHepatiti s B fo r employee s wit h occupationa l exposur e t o potentiall yinfectiou s materials . Employee s havin g occupationa l exposur e hav e a greate rrisk o fcontractin g Hepatiti s B becaus e o f th e frequen thandlin g o fbloo d an d bloo d product s o fhuma n origin . Althoug h al l potentiall yinfectiou s material s use d a tLaborator yDiagnostics/Cenogenic s ar e certifie d b ylicense d broker s t o b e HBV , HCV/HI Vnegative , ther e doe s exis t th e potentia l risk o fexposure . Th e Hepatiti s B vaccinatio n serie s reduce s tha trisk o fexposur e b y providin g immunizatio n agains t thi s bloodborn e disease .BLOODBORN E PATHOGEN S S.O.P . SF-0023-0 2 PAG E 1 5

EXPOSUR E CONTRO LPLA N 

### Advers e Reaction s A s wit h an yvaccination , ther e exist s th e potentia l fo radvers e reaction s t o occu ri n certai n individuals . I ti s possibl e tha t non e o fth e advers e reactionsyW^ ^ wil l b e experience d b ya n employe e receivin g th e Hepatiti s B vaccipalitf^ruH ^ thes e advers e reaction s hav e bee n reporte d i n studie s an d shoul^l^\maa e apparen t t o th e employee . Th e followin g advers e reaction s ma yoccur : 1 . Injectio n sit e - loca l sorenes s an d swellin g o fth e upper^rm5% ^ I 2 . G l trac t- nausea , vomiting , diminishe d appetite , diarrhea . 3 . Centra l Nervou s Syste m - headache , lightheadedness , dizziness , irritability , disturbe d sleep . 4 . Respiratory- cough , flu-lik e conditions . 5 . Bod ya s a whol e - fatigue , feve r> 100°F , sweating , chills , flushing . Conclusio n Base d o n th e abov e information , employee s wit h occupationa l exposur e ca n personall y decid e i fthe ywan tt o accep tth e Hepatiti s B vaccinatio n series . I fa n employe e choose s th e Hepatiti s B vaccinatio n series , a n appointmen t a ta loca l medica l car e facilit ywil l b e schedule d a ta convenien ttim e fo rth e employe e t o begi n th e vaccinatio n series . Al l subsequen t appointmen twil l als o b e schedule d a t a convenien t tim e fo rth e employee . I fa n employe e choose s t o declin e th e Hepatiti s B vaccination , the ymus tcomplet e a Declinatio n Statemen t(Appendi xAo fthi s S.O.P) . I n eithe r circumstance , documentatio n o fth e employee' s decisio n wil l b e maintaine d i n th e OSH Aan d Employe e Files .BLOODBORN E PATHOGEN S S.O.P . SF-0023-0 2 PAG E 1 6

EXPOSUR E CONTRO LPLA N 

### APPENDI XE 

# ^0\S 0 TRANSMISSIO N O F BLOODBORN E PATHOGEN S Bloodborn e Pathogen s ar e define d a s pathogeni cmicroorganism s tha tar e presen t i n huma n bloo d an d capabl e o fcausin g diseas e i ftransmitte d t o others . Thi s grou p o f microorganism s include s thos e responsibl e fo rth e transmissio n o fHepatiti s B (HBV) , Hepatiti s C (HCV ) an d HI Vinfection . Hepatiti s B viru s ma yb e foun d i n bloo d an d othe rbod yfluids , suc h a s urine , tears , semen , vagina l secretion s an d breas tmilk . Hepatiti s i s usuall ysprea d b ycontac twit h infecte d bloo d o rbloo d products . Transmissio n o fHepatiti s ca n occu rb ybloo d transfusion s involvin g infecte d blood , clos e persona l contac t(ie . sexua l contact , sharin g o frazors , sharin g o ftoothbrushes ) an d usin g infecte d needles . HI Vha s onl ybee n show n t o exis ti n bloo d an d bloo d products . A s o fdate , HI Vha s onl y bee n show n t o b e transmitte d b yillici tinjectabl e dru g use , sexua l contac tan d bloo d transfusion s wit h infecte d blood . Person s a tincrease d risk o fcontractin g thes e bloodborn e disease s ar e thos e wh o frequentl yhandl e infecte d bloo d an d othe rbod yfluid s i n th e cours e o fthei rwork , thos e wh o liv e i n crowde d condition s (HBV) , thos e wit h poo rhygien e (HBV ) an d thos e wh o hav e man ysexua l contacts .ATTACHMEN T5 LABORATOR YDIAGNOSTIC S CO. , INu .

GENERA LOPERATION S <\^ \ CHEMICA LHAZAR D COMMUNICATIO N PLA N Procedur e Prepare d bY..,-^?^'-;.L - ;.c . /:. •L/"' } ^' ^ V'>^..->^ . •

- Date^'v'^ ; ''^^' - SOP : SF-0098-0 1

- - /- " Procedur e Approve d \i>i_.^'--^U^Ti''2'L^^^^^ Dat e ' y^/f P Supersedes : non e INTRODUCTIO N Th e OSH AChemica l Hazar d Communicatio n Standard , 2 9 CF R 1910.1200 , ensure s tha t al l employer s receiv e th e necessar yinformatio n neede d t o properl yInfor m an d trai n thei r employee s an d t o pu t| n plac e employe e protectio n programs . Th e pla n als o provide s necessar yinformatio n t o employee s s o the yca n participat e in , an d support , th e protectiv e measure s i n plac e a tthei rworkplace . NOTE : Acop yo fthi s standar d i s o n fil e i n th e Regulator yFil e cabine tfo rreview . Al l

question s and/o rconcern s ma yb e brough t t o th e attentio n o fth e Productio n Supervisor . PURPOS E Th e purpos e o fthi s pla n i s t o infor m yo u tha t ou rcompan yi s i n complianc e wit h thi s OSH A standar d by : 1 . compilin g a lis to fhazardou s chemicals , 2 . usin g MSDS' s (Materia l Safet yDat a Sheets) , 3 . ensurin g container s ar e properi ylabele d an d Identified , an d 4 . providin g al l affecte d employee s wit h training . LIS TO F HAZARDOU S CHEMICAL S A . DEFINITION S 1 . "Hazardou s chemical " mean s an ychemica l whic h i s a physica l hazar d o ra healt h hazard . 2 . "Hazar d warning " mean s an ywords , pictures , symbols , o rcombinatio n thereo f appearin g o n a labe l o rothe rappropriat e for m o fwarnin g whic h conve yth e specifi c physica l an d healt h hazard(s) , includin g targe torga n effects , o fth e chemical(s ) i n th e container(s) . (Se e th e definition s fo r"physica l hazard " an d "healt h hazard " t o determin e th e hazard s whic h mus tb e covered. ) 3 . "Healt h hazard " mean s a chemica l fo rwhic h ther e i s statisticall ysignifican t evidenc e base d o n a tleas ton e stud yconducte d i n accordanc e wit h establishe d scientifi cCHEMICA LHAZAR D COMMUNICATIO N PLA N S.O.P . SF-0098-0 1 ^v^ \ PAG E 2 principle s tha tacut e o rchroni chealt h effect s maYJwkcu ri n expose d ^ployees . Th e ter m "healt h hazard " include s chemical s whic h ar e carcinoger\j^|^^itif l o rhighl ytoxi c agents , reproductiv e toxins , irritants , corrosive|g^^^i^ers , hepatotoxins , nephrotoxins , neurotoxins , agent s whic h ac to n t ^ JiCTratopoieti csystem , an d agent s whic h damag e th e lungs , skin , eyes , o rmucou s membranes . 4 . "Physica l hazard " mean s a chemica l fo rwhic h ther e i s scientificall yvali d evidenc e tha ti ti s a combustibl e liquid , a compresse d gas , explosive , flammable , a n organi c peroxide , a n oxidizer , pyrophoric , unstabl e (reactive ) o rwater-reactive . 5 . "Identity " mean s an ychemica l o rcommo n nam e whic h i s indicate d o n th e materia l safet ydat a shee t(MSDS ) fo rth e chemical . Th e identit yuse d shal l permi tcross reference s t o b e mad e amon g th e require d lis to fhazardou s chemicals , th e labe l an d th e MSDS . B . LISTIN G Refe rt o Appendi xAan d B fo rcomplet e listin g o fchemicals . II . LABELIN G AN D OTHE R FORM S O F WARNIN G A . DEFINITIO N "Label " mean s an ywritten , printed , o rgraphi cmateria l displaye d o n o raffixe d t o container s o fhazardou s chemicals . B . Eac h containe ro fhazardou s chemical s mus tb e marke d wit h th e followin g information : 1 . Identit yo fth e hazardou s chemical , 2 . Appropriat e hazar d warnings , an d 3 . Nam e an d addres s o fth e chemica l manufacturer , importe ro rothe rresponsibl e party . C . Chemica l manufacturers , importers , distributors , o remployer s wh o becom e newl yawar e o f an ysignifican tinformatio n regardin g th e hazard s o fa chemica l shal l revis e th e label s fo rth e chemica l withi n thre e month s o fbecomin g awar e o fth e ne winformation . Label s o n container s o fhazardou s chemical s shippe d afte rtha ttim e shal l contai n th e ne winformation . I fth e chemica l i s no tcurrentl yproduce d o rImported , th e chemica l manufacturers , importers , distributor , o remploye rshal l ad d th e informatio n t o th e labe l befor e th e chemica l i s shippe d o rintroduce d int o th e workplac e again .CHEMICA LHAZAR D COMMUNICATIO N PLA N S.O.P . SF-0098-0 1 . ; PAG E 3 

## 3 ^ ,..v'V';. - (II . MATERIA LSAFET YDAT ASHEET S (MSDS's ) A . DEFINITIO N <;"*; ' - ' "Materia l safet ydat a shee t(MSDS) " mean s writte n o rprinte d materia l concernin g a hazardou s chemica l whic h i s prepare d i n accordin g wit h paragrap h (g ) o fth e 1910.120 0 OSH Aregulation . Th e Materia l Safet yDat a Shee t(MSDS ) i s a detaile d informatio n bulleti n prepare d b yth e manufacture ro rimporte ro fa chemica l tha tdescribe s th e physica l an d chemica l properties , physica l an d healt h hazards , route s o fexposure , precaution s fo rsaf e handlin g an d use , emergenc yan d first-ai d procedures , an d contro l measures . Informatio n o n a n MSD S aid s i n th e selectio n o fsaf e product s an d help s prepar e employer s an d employee s t o respon d effectivel yt o dail yexposur e situation s a s wel l a s t o emergenc y situations . B . LOCATIO N Copie s o fal l MSDS' s fo ral l chemical s i n us e ar e kep t i n th e Laborator yRa wMaterial s Fil e Cabine tan d ar e readil yavailabl e t o al l employee s durin g eac h wor k shift . Th e Laborator ypersonne l i s responsibl e fo racquirin g MSDS's . Th e vendo rwil l b e contacte d i fa n MSD S i s no tsupplie d wit h a n Initia l shipmen t (S.O.P . RM-0020) . IV . TRAININ G A . Employee s wh o wor k wit h o rwh o ar e potentiall yexpose d t o hazardou s chemical s wil l receiv e Initia l trainin g o n th e Hazar d Communicatio n Standar d an d th e saf e us e o fthos e hazardou s chemicals . Wheneve ra ne whazar d i s introduced , additiona l trainin g wil l b e provided . Supervisor s wil l b e traine d regardin g hazard s an d appropriat e protectiv e measure s s o the ywil l b e availabl e t o answe rquestion s fro m employee s an d provid e monitorin g o fsaf e wor k practices . Th e trainin g pla n wil l emphasiz e thes e items :

•Summar yo fth e OSH Astandar d an d thi s writte n procedure . •Chemica l an d physica l propertie s o fhazardou s material s (e.g. , flas h point , reactivity ) an d method s tha tca n b e use d t o detec tth e presenc e o rreleas e o fchemicals .

•Physica l hazard s o fchemical s (e.g. , potentia l fo rfire , explosion , etc.) .

•Healt h hazards , includin g sign s an d symptom s o fexposure , associate d wit h exposur e t o chemical s an d an ymedica l conditio n know n t o b e aggravate d b yexposur e t o th e chemical .CHEMICA LHAZAR D COMMUNICATIO N PLA N S.O.P . SF-0098-0 1 \ PAG E 4

•Procedure s t o protec tagains thazard s (e.g. , oefe^^ rprotectiv e equipmen t required , prope ruse , an d maintenance ; wor k practl<?e^ ^

metho^^^ssUr e prope rus e an d handlin g o fchemicals ; an d procedure s fo rem^rgerj^|^i^p|^^e) .

•Wor k procedure s t o follo wt o assur e protectio n whe n cleanin g hazardou s chemica l spill s an d leaks .

•Wher e MSDS' s ar e located , ho wt o rea d an d Interpre tth e Informatio n o n bot h label s an d MSDS's , an d ho wemployee s ma yobtai n additiona l hazar d information . Retrainin g i s require d whe n th e hazar d change s o rwhe n a ne whazar d i s introduce d int o th e workplace , bu tI twil l b e compan ypolic yt o provid e trainin g regularly . B . NON-ROUTIN E TASK S Periodically , employee s ar e require d t o perfor m hazardou s non-routin e tasks . Som e example s o fnon-routin e task s are : confine d spac e entry , tan k cleaning , an d paintin g reacto rvessels . Prio rt o startin g wor k o n suc h projects , eac h affecte d employe e wil l b e give n informatio n b yth e Superviso rabou tth e hazardou s chemical s h e o rsh e ma y encounte rdurin g suc h activity . Thi s informatio n wil l includ e specifi cchemica l hazards , protectiv e an d safet ymeasure s th e employe e ca n use , an d step s th e compan yi s usin g t o reduc e th e hazards , includin g ventilation , respirators , presenc e o fanothe remploye e an d emergenc yprocedures . C . Upo n completio n o ftraining , refe rt o Appendi xC . V . CONTRACTO R EMPLOYER S Upo n notificatio n th e superviso rwil l advis e outsid e contractor s i n perso n o fan ychemica l hazard s tha tma yb e encountere d i n th e norma l cours e o fthei rwor k o n th e premises , th e labelin g syste m i n use , th e protectiv e measure s t o b e taken , an d th e saf e handlin g procedure s t o b e used . I n additio n thes e individual s wil l b e informe d o fth e locatio n an d availabilit yo fMSDS's . Eac h contracto rbringin g chemical s on-sit e mus t provid e u s wit h th e appropriat e hazar d informatio n o n thes e substances , includin g th e label s use d an d th e precautionar ymeasure s t o b e tak e i n workin g th e thes e chemicals .CHEMICA LHAZAR D COMMUNICATIO N PLA N S.O.P . SF-0098-0 1 PAG E 5 APPENDI XA NOTE : Thi s listin g contain s al l know n chemical s whic h ma yo rma yno tcurrentl yb e i n us e o ri n

stoc k i n eithe rlocation . Althoug h th e chemical s liste d ar e classifie d a s hazardou s a s state d I n thei rrespectiv e MSDS , th e quantitie s house d i n bot h location s d o no t mee t DE P hazar d threshol d a s define d b yth e Communit yRigh tt o Knoi^vy-purvey . sopropy l alcoho l (fo rcleaning ) \ j .Tsaft*^"^*-! ^ Warehous e Locatio n oCv*?^ ^ :'?;^ . Speciall yDenature d Alcoho l (SDA ) 12A-3 , Anhydrous , 20 0 Proo f;fl0%i;t^Jcp6^ ) Ethy l Alcohol , Anhydrous , 20 0 Proo f(VDR LAntigen ) ^ S # Phenol , 1.0 % solutio n i n suspensio n (Febril e Antigens ) Formaldehyde , 1.0 % solutio n i n suspensio n (Febril e Antigens ) Hydroge n peroxid e (Developer ) Sodiu m azide , a s a preservativ e i n solutio n (0.1% ) Thlmerosal , a s a preservativ e i n solutio n (0.02% ) Gu m Guala cPowde r Methy l Ethy l keton e Sodiu m hypochlorit e (bleach ) Crodasea l (Ammoniu m hydroxide , 0.8% ) Crysta l violet , powdere d dy e Brillian tgreen , powdere d dy e Proflavin e hemisulfate , powdere d dy e Laborator yLocatio n Isopropy l alcoho l Speciall yDenature d Alcoho l (SDA) , 12A-3 , Anhydrous , 20 0 Proo f Ethy l Alcohol , 3A , Anhydrous , 20 0 Proo f Ammoniu m hydroxid e Bariu m chlorid e Bori caci d Brillian tgreen , dy e Carbo n tetrachlorid e Chlorofor m Citri caci d Coverag e Plu s (disinfectant ) Crysta l violet , dy e Formaldehyde , 37 % Glacia l Aceti cAci d Glutaraldehyde , 25 % aqueou s Gu m guala cpowde rCHEMICA LHAZAR D COMMUNICATIO N PLA N S.O.P . SF-0098-0 1 PAG E 6

Hydrochlori cAci d Hydroge n peroxid e Lacti cacid , 85 % Pheno l Propan e fuel , min i tank s Phosphori cacid , 85 % Potassiu m hydroxid e Potassiu m permanganat e Sodiu m azid e ^ Sodiu m borat e (Borax ) decahydrat e cC^^ Sodiu m borohydrid e \ Sodiu m hydroxid e Sodiu m hypochlorit e (Bleach ) , " * Sodiu m oxalat e Sodiu m phosphate , dibasic , heptahydrat e Sodiu m phosphate , monobasic , dihydrat e Sulfuri caci d Thermometer s (mercury ) Thlmerosa l Trito n X-10 0 APPENDI XB NOTE : Thi s listin g contain s chemical s classifie d a s hazardou s a s state d i n thei rrespectiv e

MSDS's . VThes e chemical s ma yo rma yno t b e currentl yi n stoc k o ri n us e an d ar e locate d i n th e laborator yonl yfo rR&D . R& D CHEMICAL S (LABORATOR YLOCATIO N ONLY ) Aceton e Ammoniu m oxalate , monohydrat e Ammoniu m thiocyanat e Arseni cTrioxid e Bariu m oxide , anhydrou s Bariu m dioxid e Brucin e Cadmiu m chloride , 2.5-Hydrat e Calciu m chloride , dihydrat e Calciu m hydroxid e Calciu m oxid e Chloroaceti caci d Chlortetracyclln e hydrochlorid eCHEMICA LHAZAR D COMMUNICATIO N PLA N S.O.P . SF-0098-0 1 PAG E 7

Cobal toxid e Coppe r(II ) oxid e Cupri cacetate , monohydrat e N , N-Dlethy l - 1, 4 - Phenylenedlamine , 97 % N , N-Dlmethylformamid e 3 , 3 ' - Dlmethoxybenzidlne , 97 % Dimethy l Sulfoxid e m-Dinltrobenzen e Ethylenediamlnetetraacetl caci d (EDTA ) Ether , anhydrou s Ferri csulfate , n-Hydrat e Hydrazin e sulfat e Iodin e Laury l Sulfat e (Sodiu m Dodecy l Sulfat e (SDS ) Lea d sub-acetat e Lea d (II ) sulfide , -20 0 mes h Lithiu m nitrat e Magnesiu m Magnesiu m nitrat e Magnesiu m perchlorat e (anhydrone ) Manganes e Dioxid e Mercuri cAcetat e Mercuri cChlorid e Mercuri cIodide , Re d Mercuri cNitrate , Monohydrat e Molybdenu m Trioxid e p-Nltroanilin e Oakit e 3 2 4-PhenylazoanlHn e hydrochloride , 97 % Phenylmethylsulfony l fluorid e Phosphoru s Oxychlorid e Potassiu m chromat e Potassiu m cyanid e Potassiu m dlchromat e Potassiu m nitrat e Silve rcarbonate , 99 % Sodiu m arsenate , dibasic , 7-hydrat e Sodiu m arsenlt e Sodiu m Bisulfit e Sodiu m Cyanid e Sodiu m fluorid e Sodiu m nitrat e Sodiu m nitrit e Sodiu m phosphate , Tribaslc , 12-Hydrat eCHEMICA LHAZAR D COMMUNICATIO N PLA N S.O.P . SF-0098-0 1 PAG E

tert-Buty l alcoho l Toluen e sulfoni caci d o-Toluldln e Trichloroaceti cacid , soli d Tri s (hydroxymethyl ) amlnomethan e hydrochlorid e Vanady l sulfat e Zin cacetate , dihydrat e

'•••> MCHEMICA LHAZAR D COMMUNICATIO N PLA N S.O.P . SF-0098-0 1 PAG E 9

APPENDI XC TRAININ G DOCUMEN T I hav e receive d th e followin g Informatio n an d Trainin g Sernlrlfe^ n "th e Chemica l Hazar d Communicatio n Pla n fo rLaborator yDiagnostics/Cenogenics : a . Acop yo fthi s Chemica l Hazar d Communicatio n Pla n an d a n explanatio n o fth e standar d upo n whic h i ti s based . b . Understandin g th e hazar d warnings , label s an d th e NFP A(Nationa l Fire Protectio n Association ) symbol s o n chemica l containers . c . Understandin g a Materia l Safet yDat a Shee t(MSDS ) an d wher e the yma yb e located . d . Knowin g whe n Persona l Protectiv e Equipmen t(PPE ) i s appropriate . e . Recognizin g th e sign s an d symptom s associate d wit h exposur e t o hazardou s chemicals . A s a n employe e wit h a potentia l fo roccupationa l exposure , I a m awar e o fan d understan d th e safet ymeasure s I shoul d execut e whe n handlin g hazardou s laborator ychemicals . I hav e rea d an d understan d th e Chemica l Hazar d Communicatio n Pla n fo rthi s facility . I hav e ha d a n opportunit yt o as k question s an d hav e the m answered . I als o understan d tha t I ma ya tan ytime , as k question s o fm yimmediat e superviso rpertainin g t o prope rsafet yprocedure s o ran yothe rtopi cdiscusse d i n th e trainin g seminar . Employee' s signature : Date : Trainin g Supervisor : Date :ATTACHMEN T6

CHEMICA LHYGIEN E PLA N FO R LABORATOR YDIAGNOSTICS/CENOGENIC S S.O.P . SF-0025-0 2 PAG E 1 2 Appendi xH TRAININ G DOCUMEN T I hav e receive d th e Informatio n an d Trainin g Semina ro n Laborator yDiagnostics/Cenogenics . I receive d th e follow i session : ica l Tlygien e Pla n fo r formatio n an d trainin g i n thi s a . Acop yo fthi s Chemica l Hygien e Pla n an d a n exj^a^i^^Mfri ^ upon . jKm e standar d i t i s base d b . Understandin g a Materia l Safet yDat a Shee tan d knowin g wher e the yar e filed . c . Understandin g th e Hazar d Label s an d th e NFP Asymbols . d . Knowin g whe n PP E i s appropriate . e . Recognizin g th e sign s an d symptom s associate d wit h exposur e t o hazardou s chemicals . f . Knowin g th e prope rdisposa l o fhazardou s waste . g . Trainin g i n ho wt o us e fir e extinguishers , respirator s an d Firs t Aid . h . Kno wth e fir e evacuatio n pla n fo rth e laborator yan d warehouse . A s a n employe e wit h occupationa l exposure , I a m awar e o fan d understan d th e safet y measure s I shoul d execut e whe n handlin g hazardou s laborator ychemicals . I hav e rea d an d understan d th e Chemica l Hygien e Pla n fo rthi s facility . I hav e ha d a n opportunit yt o as k question s an d hav e the m answered . I als o understan d tha tI ma ya t an ytime , as k question s o fm yimmediat e superviso rpertainin g t o prope rsafet yprocedure s o ran yothe r topi cdiscusse d i n th e trainin g seminar . Employee' s signature : Approve d by : 

# 6..^l/ M Da.e: S/^/ ° 

# 1 Dat e . <P/y^/o ^ATTACHMEN T7

BLOODBORN E PATHOGEN S S.O.P . SF-0023-0 2 PAG E 1 3 EXPOSUR E CONTRO LPLA N

APPENDI XC TRAININ G DOCUMEN T I hav e receive d th e Informatio n an d Trainin g o n th e Bloodborn e Pathoge n Exposur e Contro l Pla n fo rLaborator yDiagnostics/Cenogenics . i receive d th e followin g informatio n an d trainin g i n th e session : 1 . Acop yo fthi s Exposur e Contro l Pla n an d th e Bloodborn e Pathogen s Standard , 2 9 CF R 1910.1030 . 2 . A n explanatio n o fth e task s tha t ma yinvolv e exposur e t o potentiall yinfectiou s materials . 3 . A n explanatio n o n ho wt o reduc e exposur e b ywearin g PPE . 4 . Ademonstratio n o n ho wt o us e PP E correctly . 5 . Adiscussio n take n fro m Appendi xC o n th e epidemiolog yan d mode s o f transmissio n o fbloodborn e pathogens . 6 . Adiscussio n take n fro m Appendi xD o n th e Hepatiti s B vaccinatio n serie s regardin g it s purpose , benefits , sid e effects , numbe ro fvaccination s an d declinatio n statement . 7 . Adiscussio n o n th e procedure s t o follo wi n cas e a n exposur e inciden toccurs . A s a n Employe e wit h occupationa l exposur e I a m awar e o fan d understan d th e safet y measur e I shoul d execut e whe n handlin g potentiall yinfectiou s materials . I hav e rea d an d understan d th e Exposur e Contro l Pla n fo rthi s facility . I hav e ha d a n opportunit yt o as k question s an d hav e the m answered . I als o understand , tha tI ma ya tan ytime , as k question s o fm yimmediat e superviso rpertainin g t o prope rsafet yprocedure s o ran yothe r topi cdiscusse d i n th e training . ^ ^ , ^ r Employe e signatur e /^-^M^ ^ ' ^ / •" ' Dat e '_ _ Superviso rapprova l / '^''^>-%-^<^<^<T [ Dat e ^'^y<yj: -ATTACHMEN T8

CHEMICA LHAZAR D COMMUNICATIO N PLA N S.O.P . SF-0098-0 1 PAG E 9

APPENDI XC TRAININ G DOCUMEN T I hav e receive d th e followin g informatio n an d Trainin g Semina ro n th e Chemica l Hazar d Communicatio n Pla n fo rLaborator yDiagnostics/Cenogenics : a . Acop yo fthi s Chemica l Hazar d Communicatio n Pla n an d a n explanatio n o fth e standar d upo n whic h i ti s based . b . Understandin g th e hazar d warnings , label s an d th e NFP A(Mi^^i fF^lr e Protectio n Association ) symbol s o n chemica l containers . "** ' ^ ^ c . Understandin g a Materia l Safet yDat a Shee t(MSDS ) an d wher e the yma yb e d . Knowin g whe n Persona l Protectiv e Equipmen t(PPE ) i s appropriate. \ xj N V ' " e . Recognizin g th e sign s an d symptom s associate d wit h exposur e t o hazardou s chemicals . A s a n employe e wit h a potentia l fo roccupationa l exposure , I a m awar e o fan d understan d th e safet ymeasure s I shoul d execut e whe n handlin g hazardou s laborator ychemicals . I hav e rea d an d understan d th e Chemica l Hazar d Communicatio n Pla n fo rthi s facility . I hav e ha d a n opportunit yt o as k question s an d hav e the m answered . I als o understan d tha ti ma ya t an ytime , as k question s o fm yimmediat e superviso rpertainin g t o prope rsafet yprocedure s o ran yothe rtopi cdiscusse d i n th e trainin g seminar . Employee' s signature : l\iA^~k^\/iJ^'^ ^ Date:__^2___ _ Trainin g Supervisor : /^^InS^-^A^^O ^ Date : <^/yjyiP pATTACHMEN T9 CENOGENIC S CORPORATIO N GENERA LOPERATION S OCCUPAN TEMERGENC YRESPONS E PLA N Procedur e prepare d by : Nitz a Kat z Date : 7/1/0 5 S.O.P . SF-00153-0 3 Procedur e approve d by : Michae l Kat z Date : 7/1/0 5 Supercedes : SF-00153-0 2 PURPOSE : Th e purpos e o fthi s procedur e i s t o defin e th e actio n pla n require d i n th e cas e o fa n emergency . REFERENCE : 9 CF R 121.1 2 an d 4 2 CF R 73.1 2 CENOGENIC S LOCATION S 1 . Laborator yan d office : 10 0 Rout e 52 0 Morganville , N J 0775 1 732-536-645 7 tel . 732-972-852 7 fa x inguirv(S)cenogenics.co m 2 . Warehous e an d packaging : 71 2 Gines i Driv e Morganville , N J 0775 1 732-972-214 5 3 . Exit s ar e marke d o n th e floo rplan s fo reac h building . Floo rplan s ar e poste d i n eac h building . I ti s require d tha tth e are a aroun d eac h exi tremain s clea ran d fre e o fan y obstacl e tha tcoul d hinde racces s t o th e door . 4 . Al l exit s ar e cleari ymarke d wit h "EXIT " signs . Al l exist s ar e equippe d wit h emergenc y exi tlights . Th e exit s light s ar e teste d monthl yt o assur e tha t the yar e I n workin g orde r a s describe d I n S.O.P . SF-005 4 (Emergenc yLigh tInspectio n Procedure) . COMPAN YCONTACT S Fo rquestion s pertainin g t o th e Occupan t Emergenc yRespons e Plan , contact : Michae l Katz , Presiden t Nitz a Katz , Vic e Presiden t 609-259-001 0 (hom e tel. ) EMERGENC YNUMBER S 1 . Cenogenic s maintain s a lis to fcontac tname s an d number s fo remergenc ysituations . Refe rt o attachmen t"Emergenc yTelephon e Number" . 2 . Th e lis to femergenc ynumber s i s poste d b yeac h telephone .Oocupan tEmergenc yPla n S.O.P . SF-00153-0 3 Pag e 2 of5 EVACUATIO N Fo ran yo fth e emergenc ydescribe d below , whe n yo u ar e instructe d t o leav e th e buildin g an d repor tt o you rsupervisor : 1 . Employee s workin g i n th e laborator ybuildin g locate d a t10 0 Rt . 520 , repor t t o th e superviso ra tth e warehous e buildin g locate d a t71 2 Gines i Drive . 2 . Employee s workin g i n th e warehous e buildin g locate d a t71 2 Gines i Driv e repor t t o th e superviso ra t th e laborator ybuildin g locate d a t10 0 Rt . 520 . I ti s th e responsibilit yo fth e superviso rt o accoun t fo rth e safet yo fal l employee s befor e the yar e dismissed . FIR E EMERGENC Y 1 . Fir e extinguisher s ar e locate d throughou t th e buildin g a teac h location . Th e fir e extinguisher s ar e service d annually . Eac h employe e i s traine d o n th e us e o fth e fir e extinguishe ra t th e tim e o femploymen t(referenc e Chemica l Hygien e Plan , S.O.P . SF 0025) . . . f Th e "Machin e Room " i n th e laborator ybuildin g i s equippe d with^|^iyi<fa d automati c sprinklers . 3 . Bot h location s ar e equippe d wit h smok e detectors . 4 . Th e laborator ybuilding' s securit ysyste m ha s smoke , hea tancTnoo^dfector s an d i s connecte d t o a centra l station . I n cas e o fa fire , th e alar m wil l Mun d an d th e fir e an d polic e departmen twil l automaticall yb e notified . 5 . I n cas e o ffire , g o t o th e neares t phon e awa yfro m th e fir e are a an d dia l 911 . I fi t i s no t possibl e t o safel ycal l fro m insid e o fth e building , leav e th e buildin g IMMEDIATEL Yb y wa yo fth e neares texit . D O NO Tsto p t o collec t persona l items . Onc e safel youtsid e o f th e building , us e a cel l phon e t o cal l 911 . Onc e safel youtsid e o fth e building , repor t t o you rsupervisor . 6 . I n cas e o fa n emergenc ywher e i t i s necessar yt o evacuat e th e building , i t i s th e responsibilit yo fth e superviso rt o accoun tfo rth e eac h membe ro fth e staff . I fa n individua l i s missing , i tmus tb e reporte d t o th e emergenc yrespons e uni t (fir e dept. , police , etc.) . 7 . Th e emergenc yrespons e uni t wil l determin e whe n an d i fi t i s saf e t o re-ente rth e building . You rsuperviso rwil l le t yo u kno wwhethe rt o retur n t o th e buildin g o rg o hom e an d wai tfo rfurthe rinstruction . GA S EMERGENC Y 1 . I n th e cas e o fa natura l ga s leak , phon e N J Natura l Ga s (800 ) 222-122 2 IMMEDIATELY . 2 . Evacuat e th e buildin g t o a saf e locatio n outsid e th e buildin g an d repor t t o you r supervisor . Befor e leavin g th e building . I t i s th e responsibilit yo feac h superviso rt o assur e tha tan ypotentia l hazar d suc h a s ope n flame s ar e turne d off .Occupan tEmergenc yPla n S.O.P . SF-00153-0 3 Pag e 3 o f5 3 . I ti s th e responsibilit yo fth e superviso rt o accoun t fo reac h membe ro fth e staff . I fa n individua l i s missing , i tmus tb e reporte d t o th e emergenc yrespons e uni t(fir e dept , police , etc.) . 4 . N J Natura l Ga s wil l determin e whe n an d i fi t i s saf e t o re-ente rt o th e building . You r superviso rwil l le tyo u kno wwhethe rt o retur n t o th e buildin g o rg o hom e an d wai t fo r furthe rinstruction . WEATHE R EMERGENC Y 1 . I n cas e o fa weathe remergency , i t i s th e discretio n o fth e compan ymanagemen t whethe ri ti s necessar yt o clos e th e company . 2 . I n cas e o finclemen tweathe rprio rt o reportin g t o work , pleas e contac tth e compan y managemen t(referenc e Emergenc yTelephon e Numbers ) fo rcompan yclosing . CHEMICA LHAZAR D INFORMATIO N AN D EMERGENC Y 1 . Referenc e Chemica l Hygien e Plan , S.O.P . SF-002 5 an d Chemica l Hazar d Communicatio n Plan , SF-0098 . 2 . Referenc e th e "CAUTION " sectio n o feac h standin g operatin g procedur e fo rth e prope ruse , handlin g an d emergenc yactio n fo ran ypotentiall yhazardou s chemical . BIOLOGICA LHAZAR D INFORMATIO N AN D EMERGENC Y^^s? W 1 . Referenc e Bloo d Born e Pathoge n Exposur e Contro l Plan , S.O.P . SF « 2 . Referenc e th e "CAUTION " sectio n o feac h standin g operal^ttf^procedur e fo rth e prope ruse , handlin g an d emergenc yactio n fo ran ypotentiall yhazardou s blolo|pica l material . '^ "



# ^^0^ ^ SELEC TAGEN TINFORMATIO N AN D EMERGENC Y^ 1 . Cenogenic s posses s th e followin g selec tagents : a . Brucell a melitensis , strai n Rev . 1 Brucell a melitensi s cultur e i s use d i n th e preparatio n o fBrucell a melitensi s antigen , a diagnosti creagen tuse d t o detec t th e presenc e o fB . melitensi s antibodie s i n serum . b . Brucell a abortus , strai n 1119- 3 Brucell a abortu s i s use d i n th e preparatio n o fBrucell a abortu s antige n an d Ros e Benga l Brucell a abortu s antigen , diagnosti creagent s use d t o detec tth e presenc e o fB . abortu s antibodie s i n serum . 2 . I n th e cas e o fbroke n contaminate d glass , d o no tpic k u p b yhand . Us e a brus h an d dustpa n an d plac e th e broke n glas s i n a sharp s containe rfo rprope rdisposal . Decontaminat e th e la b benc h o rth e floo rwit h a disinfectan t solution . Th e brus h an d th e dustpa n mus tb e autoclave d i n a seale d autoclav e ba g befor e washing . 3 . I n th e cas e o fa n acciden t tha t ma yhav e cause d exposur e t o th e selec t agen t (i.e . punctur e fro m contaminate d needle , etc.) , repor tt o th e R O Immediatel yan d see k medica l attention . Refe rt o th e Emergenc yPhon e Numbe rLis t poste d b yeac h phon e

### Occupan tEmergenc

yPla n S.O.P . SF-00153-0 3 Pag

e 4 o f5 fo rth e nam e an d telephon e numbe ro fth e docto rand/o rhospital . Reportpotentia l exposur e t o th e doctor . 4 . Shoul d a n individua l wit h acces s t o th e selec tagen tsuspec ttha the/sh e ha s bee n expose d t o th e selec tagen tan d i s exhibitin g symptom s o finfectio n (i.e . fever , headache , flu-lik e symptoms) , reportt o th e R O immediatel yan d see k medica l attention . Refe rt o th e EmergencyPhon e Numbe rLis tposte d a teac h phon e fo rth e nam e an d numbe ro fth e docto rand/o rhospital . Reportpotentia l exposur e t o th e doctor . 5 . Los s o fkey s t o an yo fth e followin g i s considere d a compromis e t o th e securit yo fth e selec tagents : a . ke yt o refrigerato rwher e culture s are stored , ^awt . ^ b . ke yt o th e freeze rwher e th e selec tagent s are stored , .^f^ ^ $ c . ke yt o th e bacteriolog ylaboratory , ^ ' " d . ke yt o th e bacteriolog yincubator , e . ke yt o th e manufacturin g filin g cabinets , f . ke yt o th e laboratorybuilding . 

# tOH^WtHl\^\ - I n cas e o floss , repor tt o th e RO immediately . I t i s th e responsibilit yo fth e R O t o investigat e an d assur e tha tal l sensitiv e record s pertainin g t o th e selec t agen tar e i n place . Th e RO mus taccoun tfo rth e selec t agen tinventory . I feverythin g i s i n order , th e loc k mus tb e replaced . Recor d o freplacemen tan d ke yassignmen tmus tb e maintained . 6 . I fi ti s determine d tha tsensitiv e record s ar e missin g o rth e selec tagen tinventory canno tb e reconcile d o rappear s t o have bee n altered , th e prope rauthoritie s mus t b e notifie d immediately . Th e managemen tofficia l mus timmediatel ynotif yAPHI S orally an d the n th e appropriat e Federal , Stat e an d loca l la wenforcemen tagencie s (refe rt o EmergencyPhon e Numbe rLis tposte d byeac h phone) . Th e ora l reportmus tb e followe d withi n seve n day s b ya writte n report , APHI S For m 204 3 (se e attached) . 7 . I ti s th e responsibilit yo fth e managemen tt o notif yth e authoritie s o fa n unauthorize d reques tt o transfer , a n unauthorize d release , los s and/o rthef to fth e selectagents . Th e managemen tofficia l mus timmediatel ynotif yAPHI S orall yan d the n th e appropriat e Federal , Stat e an d loca l la wenforcemen tagencie s (refe rt o Emergency Phon e Numbe rLis tposte d byeac h phone) . Th e ora l repor tmus tb e followe d withi n seve n day s b ya writte n report , APHI S For m 2043 (se e attached) . SUSPICIOU S OBJEC TO R SUSPICIOU S PERSON S 1 . I fa tan ytim e you receiv e a letter , envelop e o rparce l an d fo rwhateve rreaso n you suspec ttha ti tcoul d b e dangerous , brin g i tt o th e attentio n o fyou rsuperviso r IMMEDIATELY . I fth e superviso ri s unabl e t o properl yidentif yth e objec to rth e sourc e o fth e objec tan d als o determine s i tt o b e o fa suspiciou s nature , th e loca l polic e shoul d b e notifie d IMMEDIATEL Yan d give n a ful l descriptio n o fth e objec ti n question . DO NO

Topen . 2 . Unauthorize d entryint o Cenogenic s building s i s PROHIBITED . I fa n unauthorize d individua l wishe s t o ente rth e buildin g an d canno tadequatel yexplai n th e reaso n o r ca n no tsho wadequat e credential , refus e entry . Not e tha tal l regulatoryagent s (FDA , USDA , Police , etc. ) ar e require d b yla wt o sho wprope ridentification . Yo u mus tas k t oOccupan tEmergenc yPla n S.O.P . SF-00153-0 3 Page s o f5 se e identificatio n an d notif yyou rsuperviso rbefor e allowin g admittanc e t o th e building . Th e laborator ybuildin g doe s no t permi t unescorte d visitors . Al l visitor s mus t sig n i n an d ou ti n th e visitor s lo g a tth e fron t offic e (referenc e S.O.P . Bio-Safet yan d Securit y Plan , S.O.P . SF-00125) . 3 . I fa n individua l wh o i s refuse d entry , become s persisten tan d refuse s t o leav e o r enter s th e building , D O NO Tbecom e confrontational . G o t o th e neares t saf e telephon e an d cal l th e polic e (911) . 4 . I fyo u notic e a suspiciou s perso n o rvehicl e lurkin g outsid e o fth e building , D O NO T APPROACH . Notif yth e polic e (911) .

^^^• . ^ BOM B THREA T.^^^ ^ ^ 1 . I n th e cas e o fa bom b threat , phon e th e loca l emergenc ypolice^i^j^^^^ATELY . 2 . Evacuat e th e buildin g t o a saf e locatio n outsid e th e buildin^in d repor tJ o supervisor . 

# m % 3 . I tI s th e responsibilit yo fth e superviso rt o accoun t fo rth e eac h membe ro fth e staff . I f a n individua l i s missing , i tmus t b e reporte d t o th e emergenc yrespons e uni t (fir e dept. , police , etc.) . 4 . Th e emergenc yrespons e uni t wil l determin e whe n an d i fi t i s saf e t o re-ente rt o th e building . You rsuperviso rwil l le tyo u kno wwhethe rt o retur n t o th e buildin g o rg o hom e an d wai tfo rfurthe rinstruction . TRAININ G AN D RECORD S 1 . Al l Cenogenics ' employee s shal l b e traine d b yth e compan ymanagemen t i n th e Occupan t Emergenc yRespons e Plan . 2 . Al l traine d personne l mus t sig n th e "OCCUPAN TEMERGENC YPLA N TRAININ G RECORD " statin g tha tthe yhav e receive d trainin g i n th e Occupan t Emergenc yPlan , understan d al l aspect s o fth e Pla n an d hav e ha d a n opportunit yt o as k question s (se e attached) . RECOR D 1 . "OCCUPAN TEMERGENC YPLA N TRAININ G RECORD " wil l b e maintaine d i n th e regulator yfil e locate d i n th e laborator ybuilding . 2 . Th e organizatio n wil l maintai n a recor d o fa n emergenc yrespons e i n th e regulator y file . Th e recor d shoul d identif yth e incident , th e emergenc yresponder , describ e respons e actio n take n an d evaluat e th e effectivenes s o fth e response . REVIE W Thi s pla n wil l b e reviewe d b yth e R O annuall yan d update d a s deeme d necessar yb y change s i n th e company , governmen t regulation s and/o ra s a correctiv e actio n t o a n ineffectiv e inciden tresponse .

### ATTACHMEN T1 0 CENOGENIC S CORPROATATIO N OCCUPAN TEMERGENC YPLA N TRAININ G RECOR D I hav e receive d trainin g o n th e Occupan tEmergencyPla n describin g th e safet yan d securit ymeasure s I shoul d emplo yi n th e cas e o fan yo fth e emergencysituation s describe d i n th e Plan . Additionally , I hav e receive d informatio n relate d t o th e select agent s possesse d byCenogenics , Brucell a abortu s an d Brucell a mQlite^isis . I receive d th e followin g instructiona l material : =*-^ . v' ^ ^ a . Acop yo fth e Occupan tEmergencyPla n *-vK'^\V\V ' b . Acop yo fth e SelectAgen tRis k Assessmen t oCXX'^ Yy ^ ' ^ c . Acop yo fth e Brucell a Materia l SafetyDat a Shee t A s a n employe e o fCenogenic s Corporation , I a m awar e o fan d understan d th e safetyan d securitymeasure s I shoul d execut e i n cas e o fa n emergencytha tcoul d threate n m ysafety , th e safetyo fm yfello wemployee s an d th e securit yo fth e select agent s possesse d byth e Organization . I hav e rea d an d understan d th e Occupan t EmergencyPlan . I hav e ha d a n opportunit yt o as k question s an d hav e the m answered . I als o understan d tha tI may , a tan ytime , as k question s o fth e R O (Responsibl e Official) , Nitz a Katz , pertainin g t o prope rsafet yan d security procedure s o ran yothe rtopi cdiscusse d durin g th e trainin g session .

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### ATTACHMEN T1 2 CENOGENIC S CORPORATIO N DANGEROU S GOOD S DOCUMENTATIO N FUNCTION-SPECIFI C TES T Tes tprepare d by : Nitz a Kat z Date ; 7/14/0 9 S.O. P SF-00158-0 1 Nam e d ((:<: •y- J AC LO-^T C Positio n ^

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QUESTION S tf^^iW^ ^ Fil l i n appropriat e answer s i n th e spac e provided . 1 . Lis tth e Cenogenics ' product s tha tcontai n dangerou s goods . 2 . Wha tdocumentatio n i s require d fo rshippin g th e dangerou s goods ? 3 . Wher e ar e th e require d form s kept ? 4 . Wher e ca n you purchas e forms , i frequired ?Dangerou s Good s Documentatio n Functio n Specifi cTes t Pag e 2 o f2



### 5 . Fo reac h o fth e product s liste d i n questio n 1 , lis tth e followin g information : Produc t1 Produc t2 Cenogenics ' product ^^-j^'i-i : A;^c/vt - £. ^ 1-. Uf^ - ^ 

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### 6 . Whic h o fth e Cenogenics ' produc tma yb e transporte d a s "Carg o Aircraf t Only" ? 

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### Wha ti s th e Cenogenics ' procedure t o b e followe d afte rcompletio n o fth e Dangerou s Good s Documentation ? 

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### eG-0^7S-< ^ 4 . Ho wofte n shoul d yo u verif ytha t th e procedure fo rpackagin g th e D G i s curren t wit h th e require d regulations ?

5 . Wha t D G label s ar e currentl yrequired ? 3 ) TOT^'C^^ , ^ (jf^GK XI'^W^tvli ,Dangerou s Good s Packagin g Functio n Specifi cTes tS.O.P . SF-00159-0 1 Pag e 2 o f2



### 6 . Wher e ar e th e D G label s kept ?

7 . Wher e you ca n yo u purchas e D G labels , i frequired ?

8 . I n additio n t o th e D G labels , wha tothe rlabelin g i s required ?

9 . Wha tcontaine ri s use d t o packag e th e product ? 10 . I fyo u hav e question s regardin g th e documentatio n o fDG , t o who m shoul d yo u direc tyou rquestions ? 

# C Employee : Passe d tes t'•' ^ /^^<- ^

Faile d tes t %j^^-/^ M Dat e 7/^^'^ / Tes tgrade d b yU-jf^j^^t'^A . Dat e

### ATTACHMEN T1 5 

# Ai r Se aInternationa l Forwarding , Inc . Augus t24 , 201 0 1405 Rout e 18 , Sntt e 20 6 OldBridee , Ne

w Jenc ? 0885 7 Teleibon e 732-607-060 0 

# OP" ' Cenogenic s Corporatio n ^ ^ Route 52 0 \^ J Morganville , N J ^" ^ Attn : Mrs.Nitz a Kat z Subject : (Hazardou s Materia l Shipment s W e a s you rfreigh tforwarder , fo rtha tpas t1 4 years , hav e handle d you rshipments , bot h no n hazardou s an d hazardou s W e provkle d genera l awarenes s trainin g an d functio n specifi ctrainin g t o you rhazma temployee s responsibl e fo rshippin g hazardou s material s i n accordanc e wit h 172.704 . I n addition , I examin e th e company' s document s fo rproperprocedur e an d carg o fo rproperpackagin g an d labelin g a s a mean s o ftesting . Regarxtin g you rhazardou s shipments , w e hav e alway s ha d a procedur e i n plac e wher e a s you r offic e wil l fa xu s a cop yo fth e complete d shipper s declaratio n fo rhazardou s materials , I bein g certifie d t o handl e hazaixlou s material s b yair , personall yrevie wyou rdocuments , an d the n confim n wit h you roffic e i fthe yar e correc to ran ychange s nee d t o b e made . I n addition , al l carg o i s inspected , agai n b ym e per^nally , t o ensur e prope rpackin g i s used . Further , whe n w e tende rth e carg o t o an yairiine , th e entir e shipmen ti s agai n inspecte d b ytha t particula rairtine s hazardou s materia l specialist . I fther e i s somethin g w e ma yhav e misse d o r overtooked , o ra mistak e tha twa s mad e th e airiin e wil l rejec tit . Al l shipment s ar e inspecte d b yu s usin g th e lAT ADangerou s Good s B yAi rregulations . Further , I hav e attache d m ycurren tcertificat e whic h show s tha tw e a m propert ytraine d t o handl e hazardou s material s b yair . Shouk l yo u hav e an yquestions , o rrequir e an yfurthe rinfonnation , pleas e fee l fre e t o contac tm e a t an ytime . Sincer e Ai rSHIPPER' S DECLARATIO N FO R DANGEROU S GOOD S

Shiplpe r CENOGENIC S CORPORATIO N 10 0 ROUT E 52 0 - DRAWE R 30 8 MORGANVILLE , NE WJERSE Y0775 1 U.S.A . Ai rWaybil l No . ATTACHMEN T1 6 Pag e 1 of Page s Shipper' s Referenc e Numbe r (optional ) Consigne e GRUP O MEXLA B SUSAN AGOME Z PALAFO X#548 6 ZAPOPAN , JALISC O MEXICO , Two complete d an d signe d copie s o fthi s Declaratio n mus t b e hande d t o th e operator . 

# S I 0^\\ - WARNIN G TRANSPOR TDETAIL S Thi s shipmen t i s withi n th e limitation s prescribe d for : (delet e non-applicable) ^ PASSENGE R AN D CARG O AIRCRAF T 

### XXX

. xxjo a :J5NLXXXX X AirportofDestination : Airport o fDeparture :

GUADALAJAR AAIRPOR T Failur e t o compl yi n al l res|ftct a wT m th e applicabl e Dangerou s Good s Regulatiorrc^a yb e I n breac h o f th e applicabl e law , subjec tt o lega l penalties . 5|ftct a wT

m orrc^a vb

Shipmen t type : (delet e non-applicable ) NON-RADIOACTIV E fXXaOQQCXiXtO f NATUR E AN D QUANTIT YO F DANGEROU S GOOD S

Dangerou s Good s Identificatio n U N o r I D No . Prope rShippin g Nam e Clas s o rDivisio n (Subsidiar y Risk ) Pack in g Grou p Quantit yan d

typ e ofpackin g Packin g Inst . Authorizatio n

UN117 0 ETHANO LSOLUTIO N 1 FIBERBOAR D BO XX2 LITE R 30 5

Additiona l Handlin g Informatio n

2 4 hr. Emergenc yContac tTel . No . (732 ) 536-6457/(609 ) 259-001 0 I hereb ydeclar e tha tth e content s o fthi s consignmen tar e full yan d accuratel ydescribe d abov e b yth e prope rshippin g name , an d ar e classified , packaged , marke d an d labelled/placarded , an d ar e i n al l respect s i n prope rconditio n fo rtranspor t accordin g t o applicabl e internationa l an d nationa l governmenta l regulations . I declar e tha tal l o fth e applicabl e ai rtranspor trequirement s hav e bee n met . Name/Titl e o fSignatory EILEE N KERSTE R - SECRETAR Y Plac e an d Dat e MORGANVILLE , N J 10/27/0 8 Si c jur e '^arrfry g above ) 

# >dhz u STYLE * F07L C LABELI*IASTE R ® (800 ) 621-580 8 www.labelmaster.co mSHIPPER' S DECLARATIO N FO R DANGEROU S GOOD S

G'^Q^INIC S CORPORATIO N 10 0 ROUT E 52 0 - DRAWE R 30 8 IVIORGANViLLE , NE WJERSE Y0775 1 U.S.A . Ai rWaybil l No . 

### ATTACHMENT S Pag e o

f Page s Shipper' s Referenc e Numbe r (optional ) 

# i

I Consigne e SCHENKE R STINNNE S LOGISTIC S - IMPOR T AIRPOR TVIENN A A-130 0 VIENNA , AUSTRI A FOR : DIPROME D A-248 4 WEIGELSDOR F 

# t # Two complete d an d signe d copie s o fthi s Declaratio n mus t b e hande d t o th e operator . TRANSPOR TDETAIL S Thi s shipmen t i s withi n th e limitation s prescribe d for : AirportofDeparture :

Airporto fDestination : VIENNA , AUSTRI A WARNIN G Failur e t o compl yi n al l respe^jA^Tm rth e applicabl e Dangerou s Good s Regulations^^ yb e i n breac h o f th e applicabl e law , subjec tt o lega l penalties . Shipmen ttype : (delet e non-applicable ) 

### I NON-RADIOACTIV E yKxaoKxarxxao; : NATUR E AN D QUANTIT YO F DANGEROU S GOOD S

Dangerou s Good s Identificatio n U N o r I D No . Prope rShippin g Nam e Class o rDivisio n (Subsidiar

y Risk ) Pack

in g Grou p Quantit yan d typ e o fpackin g Packin g

Inst . Authorizatio n

UN198 6 ALCOHOLS , FLAMMABLE ,

TOXIC , N.O.S . (ETHY LALCOHOL ) 3(6.1 ) 4 PLASTI C DRUM S X 57.7 5 LITER S 1 PLASTI C DRU M X

4 4 LITER S 30 7

30 7

Additiona l Handlin g Informatio n iCAO/IAT A

2 4 hr . Emergenc yContac t Tel . No . (732 ) 536-6457/(609 ) 259-001 0 I hereb ydeclar e tha tth e content s o fthi s consignmen tar e full yan d accuratel ydescribe d abov e b yth e prope rshippin g name , an d ar e classified , packaged , marke d an d labelled/placarded , an d ar e i n al l respect s i n prope rconditio n fo rtranspor taccordin g t o applicabl e internationa l an d nationa l governmenta l regulations . I declar e tha tal l o fth e applicabl e ai rtranspor trequirement s hav e bee n met . Name/Titl e o fSignatory EILEE N KERSTE R - SECRETAR Y Plac e an d Dat e MORGANVILLE , N J 03/20/0 9 SignsHtlre (sBeyt^ M above) „y ^ y STYLE * F07L C LABELt*lASTE R ® (800 ) 621-580 8 www.labelmaster.co m

### lAT

ADangerou s Good s Regulation s ATTACHMEN T1 8 

# • A A

A

D D D A UN / I D no . A 316 6

316 6

308 2 307 7 255 8 202 3

275 2

327 2 103 5 196 1

117 0 249 1

249 1 347 5 347 5 347 5

117 0 Prope rShippin g Name/Descriptio n B Engines , Interna l combustion , flammable ga s powere d Engines , Interna l combustion , flammabl e liqui d powere d Engines , rocltet , se e Roclie tmotor s t(U N 0186) , Roclte t motor s wit h hypergoli cliquid s t (U N 0250) , Roclie t motor s t(U N 0280) , Rocke tmotor s t(U N 0281) , Rocl(e tmotor s wit h hypergoli cliquid s t(U N 0322) , Rocl(e tmotors , liqui d fuelle d t(U N 0395) , Rocice t motors , liqui d fuelle d t(U N 0396 ) Environmentall yhazardou s substance , liquid , n.o.s . - k Environmentall yhazardou s substance , solid , n.o.s , i t EiTibromohydri n Epichlorohydri n 1,2-Epoxybutane , stabilized , se e 1,2-Butylen e oxide , stabilize d (U N 3022 ) Epoxyethane , se e Ethylen e oxid e (U N 1040 ) 1,2-Epoxy-3-ethoxypropan e 2,3-Epoxy-1-propanal , se e Glycidaldehyd e (U N 2622 ) 2,3-Epoxypropy l ethy l ether , se e 1,2-Epoxy-3-ethoxypropan e (U N 2752 ) Esters , n.o.s . * Ethan e Ethane , refrigerate d liqui d Ethanethiol , se e Ethy l mereapta n (U N 2363 ) Ethano l Ethanolamin e Ethano l amin e dinitrat e Ethanolamin e solutio n Ethano l an d gasolin e mbctur e wit h mor e tha n 10 % ethano l Ethano l an d moto rspiri tmixtur e wit h mor e tha n 10 % ethano i Ethano l an d petro l mixtur e wit h mor e tha n 10 % ethano i Ethano i aqueou s solution s containin g 24 % o rles s alcoho l b yvolum e Ethano l solutio n Ether , se e Diethy l ethe r(U N 1155 ) Clas s o r Oiv . (Su b Risk ) C 9

9

9 9 6. 1 (3 ) 6. 1 (3 )

3

3 2. 1 2. 1 3 8 8 3 3 3

3 Hazard

l.abel(5 ) D Miscellaneou s

Miscellaneou s

Miscellaneou s Miscellaneou s

Toxi cS Ramm . liqui d

Ramm . liqui d

Flamm , liqui d Flamm . ga s

Flamm . liqui d Corrosiv e Corrosiv e Flamm . liqui d Flamm . liqui d Flamm . liqui d

Flamm . liqui d P

G E

II I II I

I I

II I

I I II I

I I II I II I II I I I I I I I

I I II I E Q se e 2. 7 F E O

E O

E 1 E l

E4

E 1

E 2 E 1 E O

E 2 E l E 1 E l E 2 E 2 E 2

E 2 E l Passenge ran d

Cara o Aircraf t Lt d Qty Pkg Ins t G

Y91 4 Y91 1

- Y60 9

Y30 9

Y30 5 Y30 9

-

- Y3Q 5 Y30 9 Y81 8

YB1 8 Y30 5 Y30 5 Y30 5

Y30 5 Y30 9 Ma

xNet Qty/Pk g H

30kg G 30l(g G

- 1 L

10 L

1 L 1 0 L ~

- 1 L 1 0 L 1 L 1 L 1 L 1 L 1 L

1 L 1 0 L Pkg

Ins t 1 Ma xNe t CMy/Pk g J Forbidde n 900

91 4 91 1 N o limi t

45 0 L 400 k g 1 Forbidde n 609

30 9

305 309 5 L

6 0 L.

5 L 6 0 L 1 Forbidde n 1 1 Forbidde n 30 5 309 81 8 For i 81 8 305 305 30 5 Not R 30 5 309 5 L 50 L 5 L idde n 5 L 5 L 5 L 5 L sstricted 5 L 60 L Carg o

Aircraf t Onl u Pk g Ins t K 90 0

900

91 4 91 1 Ma

xNet Qty/Pk g _L_ j N o limi t

N o limi t

45 0 L 40 0 k g Forbidde n 61 1

31 0

307 31 0 200 For t 30 7 31 0 82 0 For i 82 0 307 307 30 7 Not R 307 31 0 6 0 L

22 0 L

6 0 L 22 0 L 15 0 k g Idde n 6 0 L 22 0 L 6 0 L idde n 6 0 L 6 0 L 6 0 L 6 0 L jstricte d 6 0 L 22 0 L ~ ^

,- 3 s i 4, i J A B A 7 M A1 3 A7 Q 

### m A1 J -.l i > A 9 ^ A15« ^ m i A156 ; •V * Ali i

A3 : A 1 . ; A3 i Afaa = A 3 A3 : A1S 6 A15 6 A16 6

A 3 A58 

### 19 4 SOt h EDITION , 1 JANUA B FO R EXPIJ^NATIO N O F TH E ABBREVIATION S AN D REFERENC E MARKS , SE E APPE N->\wii'ii rhj i,iirjwirj , i. ( !_ • 

### ATTACHMEN T1 9

r^ttb t 

### fp^ -

G

G

- J

* •

D Dynamite , se e Explosive , blast ing , typ e A . Efectmlyt e (sa d o ralkali ) fo r batteries , se e Batter yfluid , aci d o rBatter yfluid , alkali . Elevate d temperatur e liquid , flamrtiable , n.o.s. , wit h flas h poin taeor e 37. 8 C , a to r abov e it s flas h point . Elevate d temperatur e liquid , n.o.s. , a to rabov e 10 0 C an d belo wit s flas h poin t(includin g molte n metals , molte n salts . etcj . Elevate d temperatur e solid , n.o.s. , a to rabov e 24 0 C , se e §U3.24T(hl(4) . Engines , interna l combustion . ffammabl e ga s povmrad . Engines , interna l combustion . flammabl e liqui d powered . Environmentall yhazardou s sub stances , liquid , n.o.s . Environmentall yhazardou s sub stances , solid , n.o.s . Epictilorotiydri n 1,2-EpoKy-3-ettioxypropan e Esters , n.o. s Etchin g acid , liquid , n.o.s. , se e Hydrofluori cacid , solutio n etc . Ethan e Ettiane-Propan e mixture , refrig erate d linuld . Ettian e refrigerate d liqui d ethanolamin e dinitrat e Etiiono l o rEthy l alcoho l o rEth ano l solution s o rEthy l alcoho l solutions Ethanolamin e o rEthanolamin e solutions . Ether , se e Diethy l ethe r Ethers , n.o. s 3 9

9 9 9 9 9 6. 1 6. 1 3 3

2. 1 2. 1 2 1 Forbidde n

3

8 3 UN325 6 UN325 7

UN326 8 UN3ie 6 UN318 6 UN308 2 UN307 7 UN202 3 UN275 2 UN327 2

UN103 5 1^196 1 UN196 1 UN117 0

UN249 1 UN327 1 il

l il l

il l

II I II I 1 1 1 II I I I II I

I I II I II I 1 1 3

9

9 9 9 9 9 6.1. 3 6.1, 3 3 3 3 2. 1 2. 1 2. 1 3 3 B 3 I81,T3 , TP3 , TP2 9 IB1,T3 , TP3 , TP2 9

13 5 8 , 146 , IB3 , T4 , TP1,TP2 9 8 , 146 , B54 , (B8 ,

N2 0 T14 , TP2 , TP1 3 1B2 , T7 , TP2 , TP1 3 B3 , T2 , TP 1 IB2 , T7 , TP1 , TPB , TP2 8 IB3 , T4 , TP1 , TP2 9 B1 , B 1

T75 , TP 5 T75 , TP 5 24 , IB2 , T4 , TP 1 24 , B1 , IB3 , T2 ,

TP 1 IB3 , T4 , TP 1 IB2 , T7 , TP1 , TPB , TP2 8 Non e ... .

Non e ... . 247(h ) (4) . 22 0 22 0 15 5 15 5 Non e .. . Non e ... . 15 0 15 0 15 0 30 6 Non e ... . Non e ... . 15 0 15 0 15 4 15 0 Non e ... .

Non e ... .

Non e ... . 22 0 22 0 20 3 21 3 20 1 20 2 20 3 20 2 20 3 30 4 31 6 Non e ... . 20 2 20 3 20 3 20 2 24 7

24 7

24 7 22 0 22 0 24 1 24 0 24 3 24 3 24 2 24 2 24 2 30 2 314 , 315 . 31 5 24 2 24 2 24 1 24 2 Forbidde n

Forbidde n N o limi t N o limi t N o limi t Forbidde n 5 L 6 0 L 5 L

Forbidde n FortJidde n Forbidde n 5 L 6 0 L 5 L N o limi t

N o limi t N o limi t N o limi t Forbidde n 6 0 L 22 0 L 6 0 L

15 0 k g Forbidde n Forbidde n 8 0 L 22 0 L 6 0 L 4 0 4 0 TO

( B t/ ) m D ) o 0 1 a i n T ) ( B 0 O CQ 3 > a 3 p 

### o

4 0 4 0

" J

r o

### lAT ADangerou s Good s Regulation s ATTACHMEN T2 0



# I I 4. 1 Refrigeran tgas , n.o.s . U N 107 8

Seleniu m compound , solid , n.o.s . U N 328 3 (d ) Genera l n.o.s . entrie s coverin g a grou p o fsub stance s o rarticle s meetin g th e criteri a o fon e o rmor e classe s o rdivisions , fo rexampl e U N 175 9 U N 281 0 Corrosiv e solid , n.o.s . Toxi cliquid , organic , n.o.s . 4.1.0. 3 Self-reactiv e substance s o fDivisio n 4. 1 mus tb e assigne d t o on e o fth e generi centrie s liste d i n Appendi xC. 1 i n accordanc e wit h th e classificatio n prin ciple s describe d i n 2.4.2.3. 3 o fth e U N Recommen dations . 4.1.0. 4 Organi cperoxide s o fDivisio n 5. 2 mus t b e as signe d t o on e o fth e generi centrie s liste d i n Appendi xC. 2 i n accordanc e wit h th e classificatio n principle s describe d i n 2.5.3. 3 o fth e U N Recommendations . 

### 4.1. 1 Item s Liste d B yNam e 4.1.1. 1 I fth e nam e i s known , g o directl yt o th e Lis t o f Dangerou s Good s (Subsectio n 4.2) . 4.1.1. 2 I fth e U N o rI D numbe ri s known , g o t o th e Numerical/Cross-referenc e Inde x(Subsectio n 4.3 ) t o fin d th e Lis to fDangerou s Goods . 

### 4.1. 2 Item s No tListe d b yNam e 4.1.2. 1 Whe n a n articl e o rsubstanc e i s no t liste d by nam e i n th e Lis t o fDangerous Goods , th e shippe rmust : (a ) determin e tha t th e articl e o rsubstanc e i s no t forbidde n byreferrin g t o th e characteristic s i n Sub sectio n 2. 1 an d th e classificatio n criteri a describe d i n Sectio n 3 ; (b ) i fth e ite m i s no tforbidden , classif yi tb ycomparin g it s propertie s wit h th e classificatio n criteri a describe d i n Sectio n 3 . I fth e ite m ha s mor e tha n on e hazard , th e shippe rmus trefe rt o Subsectio n 3.1 0 t o determin e th e primaryhazard ; (c ) us e th e generi co rn.o.s . prope rshippin g nam e whic h mos taccuratel ydescribe s th e articl e o rsubstance . Prope rshippin g name s mus t b e determine d i n th e orde rshow n i n 4.1.0.2 . Thi s mean s tha t a substanc e i s onl yassigne d t o a n entryo ftyp e 4.1.0. 2 (c ) i fi t canno tb e assigne d t o a n entryo ftyp e 4.1.0. 2 (b ) an d t o a n entryo ftyp e 4.1.0. 2 (d ) i fi t canno t b e assigne d t o a n entryo f 4.1.0.2(b ) o r4.1.0.2(c) . Exampl e 1 : Methyl-n-amy l carbinol , a n alcoho l wit h a flas h poin to f54° C (130°F) , i s no tliste d b ynam e s o i tmus t b e declare d unde rth e mos taccuratel y descriptiv e nam e whic h i s Alcohol , n.o.s . (Methyl-n-amy l carbinol ) rathe rtha n Flammabl e liquid , n.o.s.-k . Exampl e 2 : Ethy l cyclohexane , a hydrocarbo n wit h a flas h poin to f35° C (95°F ) i s no tliste d b ynam e s o i t mus tb e declare d unde rth e mos taccuratel ydescrip tiv e nam e whic h i s Hydrocarbons , liquid , n.o.s . rathe rtha n Flammabl e liquid , n.o.s.-k . (d ) Generi co rn.o.s . prope rshippin g names , i | byth e inclusio n o fth e "* " symbo l i n Colunin | Lis to fDangerou s Good s mus tb e suppletner t th e technica l o rchemica l grou p name s i n bra . immediatel yfollowin g th e prope rshippin g na W requiremen t doe s no t appl yt o controlle d su ^ whe n thei rdisclosur e i s prohibite d bynation j internationa l convention . Fo rexplosive s ofi th e dangerou s good s descriptio n may plemente d b yadditiona l descriptiv e tex t to j commercia l o rmilitarynames . Th e techni c mus t b e a recognize d chemica l o roth 6 currentl yuse d i n scientifi can d technica l hai\ text s an d journals . Trad e name s mus t not Fo ra pesticide , onl yth e IS O commo n nan othe rname(s ) liste d i n th e Worl d Healt h i (WHO ) Recommende d Classificatio n o fPes 6 Hazar d an d Guideline s t o Classification, ^ name(s ) o fth e activ e substance(s ) mus t b e u | Exampl e 3 : Th e prope rshippin g nam e tur e o fFreon ®

1 4 an d Freon ®

2 3 i s R gas , n.o.s . (Tetrafluoromethane , Trifluoro n Freon ® 1 4 an d Freon ®

2 3 ar e no t a

c becaus e the yar e trad e names . Exampl e 4 : Asoli d pesticid e produc t Carbofuran . I t wil l b e declare d a s Carbama i aide , solid , toxi c(Carbofuran) , U N 2757 . Exampl e 5 : Amixtur e consistin g o fxyt i acetone , exhibitin g a flas h poin to f24° C (7^ a n Initia l boilin g poin t abov e 35° C (95°F) , classifie d usin g a prope rshippin g nam e ratel yrepresent s it s hazar d an d it s appllcati i i n a for m tha t i s t o b e use d a s a pain t femo | a generi centry . Pain t relate d material , U K appropriate . O n th e othe rhand , i fi t doe s suc h a function , bu t i s use d (fo rexample , intermediat e i n a manufacturin g process , simpl e n.o.s . prope rshippin g nam e ma y Flammabl e liquid , n.o.s.- k (e ) Wher e ther e i s an ydoub t a s t o whethe ra articl e o rsubstanc e i s permitte d fo rtransppf l o runde rwha t conditions , th e shippe rand/or f mus t consul t a n appropriat e nationa l authorit ) (f ) Hydrate s ma yb e include d unde rth e proper i nam e fo rth e anhydrou s substance . 4.1.2. 2 Tabl e 4.1. Alist s al l th e n.o.s . entrie s j mai n generi centries , groupe d b yhazar d clas s or | Withi n eac h hazar d clas s o rdivisio n th e place d int o thre e groups , wher e appropriate , a s I (a ) specifi centrie s coverin g a grou p o fsubst i article s o fa particula rchemica l o rtechnica l i (b ) pesticid e entries , fo rClas s 3 an d Divisio n 6. 1 (c ) genera l entrie s coverin g a grou p o fsubs U article s havin g on e o rmor e genera l properties . Generi co rn.o.s . prope rshippin g name s follo w "* " symbo l mus tb e supplemente d wit h th e tec chemica l grou p name , se e 4.1.2.1(d) . Th e most | prope rshippin g nam e mus t alway s b e used . 

### 12 2 SOtt i EDITION , 1 JANU I

### ATTACHMEN T2 1

•>\UnJ'U f h j l.)i73*irB , M f W Hydrogen , compresse d

Hydroge n cyanide , solutio n i n al coho l wit h no tmor g tha n 4 5 percen thydroge n cyanide . Hydroge n cyanide , stabilize d wh b les s tha n 3 percen twater . Hydroge n cyanide , stabilized , wit h fes s tha n 3 percen twate r an d absorbe d i n a porou s Iner tmaterial . Hydroge n fluoride , anhydrou s ... . Hydroge n iodide , anhydrou s Hydroge n iodid e solution , se e Hydriodi cacid , solution . Hydroge n peroxid e an d peroxy aceti caci d mixtures , stabilize d wit h acids , wate ran d no t mor e tha n 5 percen tpemxy acati cacid Hydroge n peroxide , aqueou s so lution s wH h mor e tha n 4 0 per cen tbu tno tmor e tha n 6 0 percen thydroge n peroxid e (stabilize d a s necessary) . Hydroge n peroxide , aqueou s so lution s wit h no tles s tha n 2 0 percen tbu tno tmor e tha n 4 0 percen thydroge n peroxid e (stabilize d a s necessary) . Hydroge n peroxide , aqueou s so lutions , wit h no tles s tha n 8 percen tbu t les s tha n 2 0 per cen thydroge n peroxide , (sta bilize d a s necessary) . Hydroge n parcen tstabilize d o r Hydroge n peroxid e aqueou s solutions , stabilize d wit h mo m tha n 6 0 percen thydroge n par oxide . Hydrogen , refrigerate d liqui d (cryogeni cliquid) . Hydroge n selenlde , anhydmu s . . Hydroge n sulfate , se e Sulfuri c acid . UN104 9 UN329 4 UN105 1 UN161 4

UN105 2 UN219 7 UN314 9

UN201 4

UN201 4

UN298 4

UN201 5

UN196 6 UN220 2 1

1 1

1

I I

I I

1 1

II I

1 2. 1 6.1, 3 6.1, 3 6. 1 8,6. 1 2. 3

5.1 , 8

5.1, 8

5.1. 8

5. 1

5.1. 8

2. 1 2.3 , 2.1 . 2 , B9 , B14 , B32 ,

B74 , T20 , TP2 , TP13 , TP38 , TP4 5 1,835,861 , B65 , B77 , B8 2

5

3 , B7 , B45 , B71 , B77 , T10 , TP 2 3,81 4

145 , A2 , A3 , A6 , B53 , IB2 , IPS , T7 , TP2 , TPB ,

TP2 4 12 , A3 , A6 , B53 , BBO , BB1 , BBS , IB2 , IPS , T7 , TP2 , TPS , TP24 ,

TP3 7 A2 , A3 , A6 , 853 , IB2 , IPS , T7 , TP2 , TP6 , TP24 ,

TP3 7 A 1 , IB2 , IPS , T4 , TP1,TP6 , TP24 ,

TP3 7 12 , A3 , A6 , B53 , BBO , 881 , 885 , T10 , TP2 , TPB , TP24 , TP3 7 T75 , TP S

1 30 6 Non e ... . Non e ... . Non e ... . Non e ... . Non e ... . Non e ... .

Non e ... .

Non e ... .

15 2

Non e ... .

Non e ... . Non e ... . 30 2

22 7

19 5 19 5

16 3 30 4

20 2

20 2

20 2

20 3

20 1

31 6 19 2 302 ,

314 . 24 4

24 4 Non e ... . 24 3 314 , 315 . 24 3

24 3

24 3

24 1

24 3

318 , 319 . 24 5 Forbidde n

Forbidde n Forbidde n FortJidde n Forbidde n Forbidde n

FortJidde n Forbidde n 15 0 k g

Forbidde n Forbidde n Forbidde n Forbidde n Forbidde n

Forbid de n

Forbid de n Forbidde n Forbidde n 40,5 7 4 0

4 0 25,4 0

4 0 4 0

25 , 66 , 75 , 10 6

25 , 66 , 7S , 10 6

25 , 66 , 75 , 10 6 25 , 75 , 10 6

25 , 66 , 75 , 10 6

4 0 4 0 7 0

( B t n ( D 0 ) O 3 - 0 1 3 a i n • V m n D > 7 0 (O b > 3 Cr t > a 3 3 * o O

ur > ^ r o

~ A o

### ATTACHMEN T2 2 

## Identificatio n ^r-—"'' ^ £'.•• • 

# i & Prope rShippin g ^ S ' Name/Descriptio n 

# fELge n bromid e solution , se e Hydrobromi caci d ^roge n cliloride , anhydrou s Lj^ge n cliloride , refrigerate d liqui d 

## w ^drogen , compresse d M^jfoae n cyanide , aqueou s solutio n Wbrnimor e tha n 20 % hydroge n cyanid e iuflraoe n cyanide , solutio n i n alcoho l p h notmore tha n 45 % hydroge n cyanid e i^foae n cyanide , stabilize d gi^alnin g les s tha n 3 % wate r ivdrage n cyanide , stabilize d lontainin g les s tha n 3 % wate ran d absorbe d i n a porou s •iSer tmateria l jiydrage n cyanide , unstabilize d ^rogendifiuorides , solid , n.o.s . Hydrogendifluorldes , solution , n.o.s . Hydroge n fluoride, anhydrou s Hydroge n fluorid e solution , se e Hydrofluori caci d (U N 1790 ) Hydroge n I n meta l hydrid e storag e syste m HydrAge n i n a meta l hydrid e storag e syste m containe d I n equipmen t Hydroge n i n a meta l hydrid e storag e syste m packe d wit h equipmen t Hydroge n iodide , anhydrou s Hydroge n iodid e solution , se e Hydriodi caci d (U N 1787 ) iiydrogen , liquid , se e Hydrogen , refrigerate d liqui d Hydroge n peroxid e an d peroxyaceti caci d mixtur e stabilize d wit h acid(s) , wate ran d no l mor e tha n 5 % peroxyaceti caci d "yj">98 n peroxide , aqueou s solutio n Wrt h 20 % o rmor e bu t40 % o rles s hydroge n peroxid e (stabilize d a s necessary ) JStJ^Se n peroxide , aqueou s solutio n • TM B/ . o rmor e bu tles s tha n 20 % hydroge n peroxid e (stabilize d a s necessary ) Hydroge n peroxide , aqueou s solutio n wi n more tha n 40 % bu t60 % o rles s hydroge n peroxid e tstabihze d a s necessary ) Hydroge n peroxide , aqueou s solution , stabilize d « wmor e tha n 60 % hydroge n peroxid e ydroge n peroxide , aqueou s solutio n wit h les s tha n 8 % "yoroge n peroxid e (stabilize d a s necessary ) Hydroge n peroxide , stabilize d Clas s o r Div . (Su b Risk) C 2.3(8 ) 2. 3 (8 ) 2. 1 6. 1 6.1(3 ) 6. 1 (3 ) 6 1

8 8(6.1 ) 8(6.1 )

2. 1 2. 1 2. 1 2. 3 (8 )

5 1(8 ) 5. 1 (8 )

5. 1 5. 1 (8 )

5. 1 (8 )

5 1(8 ) Hazard

Label(s ) D

Flamm . ga s

Corrosiv e Corrosiv e & Toxi c

Flamm . ga s Flamm . ga s Flamm . ga s

Oxidize r& Corrosiv e Oxidize r& Corrosiv e Oxidize r P G

E

I I II I I I II I

I I I I II I E Q se e 2. 7 F

EO

E 2 E l E 2 E l

E O E O E O

E 2 E 2 E 1 Passenge ran d

Carg o Aircraf t Lt d Qtv Pk g Ins t G

-

-

-

-

-

-

-

- Y81 5 Y82 5 Y80 9 Y81 9

-

-

-

-

-

Y50 1 Y50 1 Y51 4

-

-

-

- Ma xNet Qty/Pk g H

-

-

-

-

-

-

-

5 k g 5 k g 0. 5 L 1 L

-

_

0. 5 L 0. 5 L

1 L

-

-

-

- Pkg Ins t 1 Ma xNet Qty/Pk g J

Forbidde n 1 t Forbidde n 1 1 Forbidde n 1 Forbidde n 1 1 Forbidde n 1 1 Forbidde n 1 1 Forbidde n 1 1 Forbidde n 81 5 82 5 80 9 81 9 1 5 k g 2 5 k g 1 L 5 L Forbidde n

Forbidde n 1 Forbidde n 1 1 FortJidde n 1 1 Forbidde n

50 1 50 1 51 4 1 L

1 L 2. 5 L Forbidde n Fort)idde n 1 1 No tRestricte d 1 1 Forbidde n 1 Carg o

Aircraf t Onl y Pk g Ins t K Ma xNet Qty/Pk g L

Forbidde n 1 1 Forbidde n 1 20 0 15 0 k g Forbidde n 1 I Forbidde n 1 1 Forbidde n 1 i Forbidde n 1 1 Forbidde n 81 7 82 6 81 3 82 1 5 0 k g 10 0 k g 3 0 L 6 0 L Forbidde n

21 4 21 4 21 4 For t

50 6 50 6 51 5 10 0 k g

G 10 0 k g G 10 0 k g G jidde n

5 L 5 L 3 0 L 1 Forbidde n 1 1 Forbidde n 1 1 No t Restncte d 1 1 Forbidde n 1 S.P .

se e 4. 4 M

A 2

A 1

A 3

A 2

A 1 A14 3 A 1 A14 3 A 1 A14 3 A 2

A9 6

A 2 A7 5 ER G Cod e N

2C P 2C P 10 L 6 L 6 F 6 H 6 L

e L 8 L S P 8 P 8 P

10 L 10 L 10 L 2C P

5 C

5 C 5i . 5 C

5 C

5 C i|vp'°'^ ' ' JANUAR

Y200 9 LANATIO N O F TH E ABBREVIATION S AN D REFERENC E MARKS , SE E APPENDI XB . 

### 21 1CENOGENIC S CORPORATIO N MASTE R PRODUCTIO N RECOR D ATTACHMEN T2 3 DEVELOPIN G SOLUTIO N FOFLSTOO LBLOO D TES T

- ^ ^ - ' NIT 5 Procedur e prepare d b y Procedur e approve d b y LO TNUMBE R 0531-0 4 MP-0531-0 3 Assig n lo t numbe ra s pe rS.O.P . OP-0024 . 

## BATC H VOLUM E ADJUSTE D BATC H VOLUM E NOTE : Th e usua l batc h volum e fo rroutin e productio n i s 193. 9 liters . However , th e

developin g solutio n ma yb e prepare d i n smalle ro rlarge rbatche s a s require d (ie . specia l reques tb ycustomer) . Th e volum e o frequire d ingredient s mus t b e adjuste d proportionately . Recor d al l calculation s o n th e bac k o fthi s sheet . FORMULA : INGFIEDIENTS Deionize d wate r H2O2 , 30 % Stabilize d Alcohol , denature d anhydrous , SDA-12 A LOT/MFR . QUANTITY REQUIRE D PE R 193. 9 L 19.0 5 L 17.2 5 L 157. 6 L QUANTIT Y

ADDE D OPERATO R CHECKE R DAT E

NOTE : INGREDIENT S REQUIRE D FO R TESTIN G

2 N Sulfuri caci d Standardize d potassiu m permanganat e (KMnOJ , 0. 1 N Deionize d wate r CAUTION S 1 . Follo wal l safet yprecaution s outline d i n Chemica l Hygien e Plan , S.O.P . SF-0025 . 2 . Hydroge n peroxid e wil l irritat e th e ski n o n contact . Wea rrubbe rgloves , an d fac e shiel d o r goggle s t o protec tski n an d eyes . 3 . Solutio n ma yonl yb e prepare d i n a vente d room . Us e exhaus tfa n an d respirato rmask . 4 . Protec tsolutio n fro m hea tan d light . 5 . D o no tus e ope n flame s i n wor k area . 6 . Cove rmixin g tan k afte rmixing . Kee p tan k covere d a tal l time s t o reduc e fume s an d fir e hazard . 7 . Follo wcaution s fo rpotassiu m permanganat e outline d i n S.O.P . SD-0535 .DEVELOPIN G SOLUTIO N FO R STOO LBLOO D TES T

LO TNUMBE R S.O.P . MP-0531-0 4 PAG E 2

.fP^ i 

## J \*

INSTRUCTION S 

# <m "h . % HECK . DAT E Was h mixin g tan k

wit h denature d anhydrou s alcoho l an d allo wt o ai rdry . Ad d deionize d wate rt o tank . Ad d hydroge n peroxid e t o tank . Ad d alcoho l t o tank . Mi xwit h electri cstirre rfo ra minimu m o f2 0 - 3 0 minutes . Obtai n a sampl e o fapproximatel y2 0 m l fro m bot h th e botto m o fth e tan k an d th e top . Perfor m potassiu m permanganat e titratio n procedur e a s describ e unde r"TESTING " t o determin e th e hydroge n peroxid e concentration . Titratio n shoul d b e performe d a t leas ttwic e o n eac h sample . I fresult s ar e no t withi n specifications , mi xagai n an d repea t testin g befor e makin g an yadjustments . I frepeate d testin g confirm s tha tth e produc t i s no twithi n specifications , mak e necessar yadjustment s an d repea tmixing . H,0 : VOL . H,0, : VOL . LOT/MFR . ALCOHOL : VOL . LOT/MFR . Perfor m potassiu m permanganat e titratio n o n adjuste d batch . 10 . Filte rsolutio n throug h 0. 8 micro n membran e an d stor e i n tightl yseale d (DO T approved ) plasti cdrums . Stor e a troo m temperatur e protecte d fro m hea t an d light . 1 1 . Submi ta sampl e (±2 0 ml ) t o Qualit yContro l fo rproduc t releas e testing . Giv e thi s procedur e t o a Superviso rfo rrevie wan d approval . TESTIN G INSTRUCTION S NOTE : Testin g performe d a s pe rUS P XX , N F XV , pag e 381 . 1 . Ad d 2 0 m l o fdeionize d wate rt o a 25 0 m l flask . 2 . Usin g a 2 m l pipet , delive r2 m l o fth e developin g solutio n t o b e teste d t o th e flask . 3 . Ad d 2 0 m l o f2 N sulfuri caci d t o th e flask . 4 . Fil l bure twit h standardize d potassiu m permanganate . Recor d startin g volum e i n char t below . 5 . Plac e a magne t I n th e flas k an d produc e a vorte xwit h a magneti cstirrer . 6 . Titrat e eac h sampl e t o en d point : releas e potassiu m permanganat e int o th e flas k dropwis e unti l a fain t pin k colo rappear s an d persist s fo ra t leas t1 5 seconds . Rea d colo ragains t a whit e background . Recor d endin g volum e o fpotassiu m permanganat e i n char tbelo wDEVELOPIN G SOLUTIO N FO R STOO LBLOO D TES TS.O.P . MP-0531-0 4

LOTNUMBE R 7 . Calculat e th e H2O 2 concentration . Eac h m l o f0.1 N potassiu m pernah g PAG E 3

s equivaienW o 1.70 1 m g o f H2O2 : VxN fX1.70 1 X10 0 o rVxN fx1.70 1

2 mi x100 0 (mg ) 2 0 Tak e th e averag e o fa tleas ttw o trial s fro m bot h th e to p an d th e botto m sample s teste d fo rth e fina l result . Th e differenc e betwee n th e tw o results , however , ma yno tdiffe rmor e tha n 5% . HYDROGE N PEROXID E SPECIFICATION : 3.63 % - 4.02 % SAMPL E (TOP/BOTTOM ) TRIA LNUMBE R KMnO^ BEGINNIN G VOL . ENDIN G VOL . V= m l USE D HYDROGE N PEROXID E % AVERAG E Sulfuri cacid , 2N : LOT/EX P KMnO^ : LOT/EX P Normalit yfacto r(Nf )

Reviewe d an d approve d b y Dat e