• cargIll '" ." 

Sioux City, IA 


Emission Test R~port 

December 2005 


• 

-

Thompson Environmental Consulting, Inc. " 

a member of THE COMPUI\NCE GROUP 

• 


Environmental Engineering. Permi.tting and Compliance Services 
-.• 


EMISSION TEST REPORT 


for 


Cargill Incorporated 
 . located in 

Sioux City, Iowa 


on 


December 12-15,2005 


Conducted by 

Comprehensive Emission Services~ me. 


P.O. Box 910 


Waukee, Iowa 50263 


(515) 987-0200 


Project No. 11805 

• 

• . TABLE OF CONTENTS 

CONTENTS 

Preface....................................................................... : ................................................. 2 


Introduction................................................................................................................3 


Swnmary ofResults ............................................................................................... : .... 4 


Sampling and Analytical Procedures .........................................................................6 


Ml7 Sampling Apparatus ..........................................................................................7 


Test Results .................................................................................................................8 


Appendix A - Example Calculations 


Appendix B ~ Laboratory Data Forms 


AppendixC -Field Data Forms 


Appendix D - Pretest Calibrations 


Appendix E - Postiest Calibrations 


Appendix F - Process Data . 


Appendix G - Opacity Certification 


TABLES 

Table 1, Swnmruy ofTest Results for the Bean Dust Bagfilter (EP 2) .....................4 


Table 2, Summary ofTest Results for the West Grain Filter (EP 1) .........................5 


Table 3, Test Results for the Bean Dust Bagfilter (EP 2) ..........................................8 


Table 4, Test Results for the West Grain Filter (EP 1) ..............................................9 


FIGURES 

Figure 1, M17 Sampling Apparatus ........ , .................................................................. 7 


• 

• PREFACE 

This report summarizes the results ofthe data collected for compliance testing performed 

at the Cargill Incorporated facility in Sioux City, Iowa; To the best ofour knowledge, the 

data in this report are accurate and complete. Any questions concerning this report 

should be directed to Mr. Tim Titus or Mr. Jay Titus. They may be reached by phone at 

(515) 987-0200. 

---------_.. , 

Jay Titus 

Test Leader'. 

tit De,cember 27, 2005 

2 
• INTRODUCTION 

An emission test was conducted by Comprehensive Emission Services on the Bean Dust 

. Bagfilter (EP 2) and the West Grain Filter (EP 1) at the Cargill Incorporated facility in 

Sioux City, Iowa. Three Method 17 with 202 backhalfparticulate sampling runs and 

three Method 9, Opacity runs were performed. PMlO emissions wiUhave to be derived 

from the PM samples for this source. The iesting fulfills the requirements for testing in 

the IDNR Permit #95~A·324-S8 and #95-A-323-S8. The testing was performed on 

December 12-15,2005. 

Coordinating the field tests: 

Tim Titus - Comprehensive Emission Services, Inc. 


Matt Pearson - Cargill Incorporated 


Lisa Schmidt - Thompson Environmental Consulting) Inc. 


Conducting the field tests: 

Jay Titus - Comprehensive Emission Services, Inc. 

Mason Woltz - Comprehensive Emission Services, Inc. 

Witnessing the field tests: 

Mark Stone - Iowa Department ofNatural Resources 

The appendices to this report contain the followip.g information and data: 

Appendix A: Example Calculations 

Appendix B: Laboratory Data Forms 

Appendix C: Field Data Forms 

. Appendix D: Pretest Calibrations 

Appendix E: Posttest Calibrations 

Appendix F: Process Data 

Appendix G: Opacity Certification 

• 

3 
SUMMARY OF RESULTS 


In accordance with current IDNR protocol, when .less than 10 mg ofsample is collected, 

10 mg of sample catch is used for calculations. Sources with sample collections less than 

10 mg are shown with a '<'symbol in the following tables to indicate that actual samples 

. were less than the assumed 10 mg catch. Both the actual and the assumed emission rates 

can be found in Appendix C: 

Table 1 summarizes the test results for testing performed on the Bean Dust Bagfilter (EP 

2). Three Method 17 with 202 backhalf particulate sampling runs and three Method 9, 

Opacity runs were performed. PMlO emissions will have to be derived from the PM 

samples for this source. The testing fulfills the requirements for testing in the IDNR 

Perniit #95-A-324-S8. The testing was performed on December 12-14,2005. 

The allowable limit for PMIO is 0.76 lblhr, 

The allowable limit Opacity is 0%. 

No blank corrections were performed. 

Table 1 


Summary of Test Results 


Bean Dust Bagfilter (EP 2) 


units Run 1 Run 2 Run 3 

PM Net Weight g <0.0100 <0.0100 <0.0100 

PM Emission gr/dscf <0.0009 <0.0009 <0.0009 

PM Emission Rate lblhr <0.22 : <0.22 <0.22 

Flow Rate acfm 28,086 27,533 28,031 

Flow Rate dscfm 27,986 27,239 27,845 I Isokinetics % 98.6 99.1 98.7 

Start Time HH:MM 15:21-7:55 10:18 14:49-7:53 

Stop Time HH:MM 17:21-9:55 14:26 16:49-9:53 

Run Date mm/dd/yr 12/12&13/05 12/13/05 12/13&14105 

units Run 1 Run 2 Run 3 

Opacity % 0.0 0.0 0.0 

Start Time HH:MM 15:30 8:00 10:20 

Stop Time HH:MM·· 16:30 9:00 11:20 

Run Date mmlddlyr 12112/05 .12/13/05 12/13/05 

4 

I 
Table 2 summarizes the test results for testing performed on the West Grain Filter (EP 1). e. Three Method 17 with 202 backhalf particulate sampling runs were performed. PMlO 

emissions will have to be derived from the PM samples for this source. Opacity could 

not be performed on this source do to steam from another source that interfered with the 

Opacity reader's ability to see the stack clearly. The Opacity requirement in the permit 


was waived in the field by Mr. Mark Stone of the IDNR. The testing fulfills the . 


. requirements for testing in the IDNR Permit #95-A-323-S8. The testing was performed 


on December 14 and 15,2005. 

The allowable limit for PMlO 0.60 lblhr. 

Table 2 


Summary of Test Results 


West Grain Cleaner PI 


PM Net Wei ht 

PM Emission 

PM Emission Rate 

Flow Rate 

FiowRate 

Isokinetic8 

Start Time 

Time 

Run Date 

units 

acfm 

dscfm 

% 

HH:MM 

HH:MM 

mmlddlyr 

Run 1 

<0.0100 . 

<0.0009 

<0.17 

21,367 

21,518 

99.3 

12:09 

16:12 

12/14/05 

R1lll2 

<0.0100 

<0.0009 

<0.17 

21,198 

21,830 

99.0 

7:53 

12:07 

12/15/05 

17:22 

12/15/05 

e 


• 


5 

• SAMPLING AND ANALYTICAL PROCEDURES 

Sampling Procedures 

Particulate emissions were deterrp.ined by U.S. Environmental :protection Agency (EPA) 

. Methods 1, 2, 3, 4, 17, 202 and 9. These Methods are titled; 

Method 1 • "Sample and Velocity Traverse for Stationary Sources" 

Method 2 - "Determination ofStack Gas Velocity and Volumetric Flow Rate" 

Method 3 - "Gas Analysis for Carbon Dioxide, Oxygen, Excess Air and Dry . 

Molecular Weight" 

Method 4 - "Determfuation tor Moisture Content in Stack Gases" 

Method 17 - "Determination ofParticulate Emissions from Stationary 

Sources (In-Stack Filtration Method)" 

Method 202 '. "Condensible Particulate Emissions" 

Method 9 - "Detennination ofVisual Emissions from Stationary 

Sources" 

These methods appear in detail inTitle 40, Code ofFederal Regulations (CFR). Part 60, 

.Appendix A. 

The Sampling Apparatus is shown in Figure 1 on Page 6. All equipment was calibrated 

at Comprehensive Emission Services' office prior to shipment to the test site. . 

Sampling Locations 

A total of 24 sample points were used to determine particulate emissions. The sample 

time per point was 10 minutes, for a total sampling time of 240 minutes per test run. The 

stack sampling point locations canbe found along with the field data sheets in Appendix 

C. 

Analytical Procedures 

The particulate emission rate was detennined following procedures detailed in EPA' 

Methods 17 and 202. Particulate samples collected on Whatman glass fiber fllters were 

analyzed gravimetrically. The probe and nozzles were rinsed with acetone. The rinse 

was transferred to tarred beakers and evaporated to dryness. The back-half water was· 

collected and separated into organic and in-organic parts. The samples were then 

transferred to tarred beakers and evaporated to dryness: 

6 
• 
 Table 3 


Particulate Emission Results 


Bean Dust Basrfilter (EP 21 


Parameters 

PM Emissions 

Weight Collected 

Actual 

Emission Rate 

Stack Flow Rates 

Velocity 

Actual 

Standard Conditions t"I -" n 

Isokinetics 

Sample Volume 

Ave. Stack Temperature -

Ave. Square Root AP 

Ave. ilH 

Ave. Meter Temperature 

Oxygen 

Carbon Dioxide 

Moisture Collected 

Moisture 

Start Time 

Stop Time 

" Run Date 

Sampling Time 

s 

Opacity 

Start Time 

Stop Time 

Run Date 

Sampling Time 

Units Run 1 

g <0.0100 

gr/dscf <0.0009 

Ib/hr <0.22 

ftlmiti 7,064 

acfm 28,086 

dscfm 27,9-86 

~6100 

of 66 

inchesH~O 2.0985 

inches H20 1.62 

of 7.6 

% 21.00 

% 0.00 

m1 35".0 

% H20 1.0 

HH:MM 15:21-7:55 

HH:MM "17:21-9:55 

mmldd/yr" 12112&13/05 

minutes 240 

Units 1 

% .0 

HH:MM 15:30 

mmlddlyr " 12/12/05 

minutes 60 

Run 2 Run 3 , 

<0.0100 <0.0100 

<0.0009 <0.0009 

<0.22 <0.22 

6,925 7,050 

27,533 28,031 

27,239 27,845 

99.1 98.7 

162.468 165.330 

69 67 

2.0504 _ 2.09i.U 

1.56 1.61 

53.9 48.9 

21.00 21.00 

0.00 0.00 

37.0 36.0 "" 

1.1 1.0 

10:18 14:49-7:53 

14:26 16:49~9:53 

12/13105 12/13&14/05 

240 240 

Run 2 Run 3 

0.0 0.0 

8:00 

9:00 11:20 

12/13105 12/13/05 . 

60 60 

• 


8 
Table 4 


Particulate Emission Results 


West Grain Cleaner (EP 1) 


Parameters Units Run 1 Run 2 Run 3 

PM Emissions 

Weight Collected g <0..0.10.0. <0..0.10.0. <0..010.0 

ACtual gr/dscf <0..00.0.9 <0..0.0.0.9 <0..0.0.0.9 

Emission Rate Iblhr <0.17 <0..17 . <0..17 

S~ck Flow Rates 

Velocity . ftlmin 2,941 2,917 

21,198 

21,830. Ai=21;64~ . 

Actual acfm 21,367 

Standard Conditions dscfm 21,518 

Sampling Results 

Isokinetics % 993 99.0. 99.1 

Sample Volume 'dscf 165.461 167.310. 166.0.84 

Ave. Stack Temperature OF 53 43 ·43 

Ave. Square Root AP inches H2O 0..8780. 0..880.9 0..8736 

Ave. Ali inches H20 1.70. 1.71 1.71 

Ave. Meter Temperature OF 61.6 54.9 61.5 

Oxygen % 21.0.0. 21.0.0. 21.QD 

Carbon Dioxide % 0.0.0. 0..0.0. 0..0.0. 

Moisture Collected m1 32.0. 41.0. 39.5 

Moisture % H20 0..9 0..9 0..9 

Run Start Time HH:MM 12:0.9 7:53 12:35 

Run Stop Time I HH:MM 16:12 12:0.7 17:22 

Run Dat.e mmlddlyr . 12114/0.5 12/15/0.5 12115/0.5 

Sampling Time minutes 240. 240 240. 

9 
• 


Appendix A 


Example Calculations 


• 

• 
Symbol 

Qa 

As 

Bws 

Cp 

Cstd 

Dn 

dscfm 

g 

gr/dscfm 

ID 

Md 

Ms 

Qstd 

Pb 

Ps 

.-

SP 

Tm 

Ts 

Vi 

Vf 

Vm 

Vmstd 

Vs 

We 

Wtgain 

y 

e 

.%&0 

% C02 

%02 

%1 

AH 

bP 

NOMENCLATURE 

Description 

Actual cubic feet per minute 

Area ofstack 

Percent water 

Pitot tube calibration coefficient 

Concetration ofparticulate dry basis, standard conditions 

Diameter ofnozzle 

Dry standard cubic feet per minute 

Grams 

Grains per dry standard cubic feet per minute 

Inside diameter of stack 

MolecUlar weight, dry stack gas 

Molecular weight, stack gas 

Stack flow rate, dry standard conditions 

Barometric Pressure 

Stack pressure 

Static pressure 

Average meter temperature 

Temperature ofstack gas 

Initial meter reading 

Final mete:t;' reading 

Volume meter, actual 

Vohune meter, standard conditions 

Average stack gas velocity 

Total moisture collected 

Total particulate matter collected 

Meter condition factor 

Sampling time 

Percent moisture by volume 

Percent carbon dioxide by volume, dry 

Percent oxygen by volume, dry 


Percent isokinetic 


• Pressure drop across orifice meter 

Gas velocity pressure 
------- "- .'-"_.-.-'--' 

PARTICULATE CALCULATION EQUATIONS 


Runl 


• 

1. Volume of meter 

v,,, =(807.004-647.700)xO.999 

v., = 159.145 ft3 

2. Volume of meter, standard conditions (68' ,29.92 in.Hg) 

_ T", +460 

-	 ' ( 1.62) 17.65x159.145x 29.90+­

V _ 13~ 

",(sid) - 47.6+460 

Vm{std) =166.100 ft3 

3. 	 Percent moisture by volume 

100 X 0.4707 X We B~==-------~

B 

ws 

B",_, 

4. 

0.04707 X We + V,1I{.,'ld) 

== 100 X 0.4707 X 35.0 

0.04707 X 35.0 + 166.100 

== 1.0 % 

Molecular weight, dry stack gas 

MtI ==0.16xO.00+21.00+28.0 
5. Molecular weight, stack g 

• 

M == M X(l Bws )+18X(1- Bw.,) s d 100 100 

M ==28.84x . (. 1--1.0) +18x (1.0 1-­) s . 100 100 

M.• = 28.73 

6. Stack Pressure 

SP P =P. +-. ·t b 13.6 

P = 29.90+ 1.30 .. 13.6 

P.. = 30.00 inch. Hg 

• 7. Velocity of stack gas 

+ 460 (JA::\ v.. == 60 x 85.349 xCp x P + M x '\j /!.p J""g .~ .r 

66+460 . V.= 60x85.349.xO.84x x 2.0985 

30.00 + 28.73 

Vs == 7,064 ftlmin 

.8. Percent isokinetic 


100x
 %I == 

24 

• 

%I = ____. _10_O_x-,(6_6_+_4_6"",",0),--x_l_66_.l_0_0_~_--::

17.65 x 240x 7,064 x 30.00x (1- 1.0)x 7t:X (0.135)2

100. 24' 

----~,:.-----'-'---''----

17.65xBxVs xP( X(I- Bws)x7t:x(Dn)2. . 100 

%1 == 98.6 

9. Area of stack 

• 

IDJ2 A == 1CX 

" (­24·. 

A. = 1C X(27.00J2 , 24 

10. Stack volumetric flow rate actual conditions 

Qa =7,064x3.98 


Qa = 28,086 acfm 


11. Stack volumetric flowrate, standard conditions (68 0 ,29.92 in.Hg) 

• 17.65 x Vs x As x PaX (1 -'- Bws) . 100 


QSld = ----r-.

17.65x7,064x3.98x30.00x 

-+-4-6-0---'----'­. (10) 1--'­

100 . Qstd == -----6-6-+-4-60---'--------'--­

Q'.ld = 27,986 dscfm 

12. Grains per dry standard cubic feet 

15.43 x Wt gain

Cs1d == 
 V;1I(std} 


C 15.43x 0.0072 
 Sld == 
 166.100 


• C :::: 0 .0007 gr/dscf
 l1d 
13. Emission rate 

• 

lb 60x Wtgain x. Qstd 

== hr 453.5924x Vm(std) 

lb 60x 0.0072 x 27,986 == hr 453.5924 x 166.100 

Ib = 0.16Ib/hr 

hr 

• 


• 

AppendixB 

Laboratory Data Forms. ~ .. 
• 

Project Number: ,..-....J.j1l1.lo~6'-ro_7_"-_____ 

Plant Name: ~C:.:a;...I",t...;I;....;'I..;..l______ 

Date:. /i?-/I.; -():5 

Analysis Type: J2? /1-/2J2 

• 

Identification 

. F= 3 inch filter P = 47mm filter B = 150ml Beaker c = 250ml Beaker D = 400ml Beaker· 

Run! 

Type Identification Final Tare Net 

Number Weight Weight Weight 

Filter P)ft; 15 z·~S" ~·56lt,!.{ . ,1)0 I t 

Probe Rinse ( ml) f,"57-95 1-B.?9;L/ 1B.<J<JZ(, ItJOO{5 

Front HalfWeight .OOr<jOrganic. ( ml) e 'io l/D IO'/5tJ3$' /0£/ sen J OD '2- 2.. . 

Inorganic o38g2. /f{o. eN1- /1t.o. firl(P flD 3 I 

Total Net Weight .DDi-Z. 

Rw2 

Type Identification Final Tare Net 

Number Weight Weight Weight 

Filter' f /& 19' 2.51/~ :;;·5"11:;- ,!lDO 0 

Probe Rinse ( ml) B 57--9& &'1· 89(lL !P1-. B9"3 ~o()O C 

Front Half Weight , ou c 0 

Organic ( ml) t L/tJ,/I JIJIt,. 0·-'; iz3 It/ft,· t?15$ I 000'5 

Inorganic 1> 3t3S3 /31. ~5~ I /3'1. 5S3S I poZ(P 

. Total Net Weight .OD3 ( 

Run 3 

Type Identification Final Tare Net 

Number Weight Weight Weight 

Filter f /&20 2.. &ct./J :J. (po 1./ ~ I , 0000 

I~ ml) B3 }--97- {P1./f.t-~ to1;. (1-50 t 0000 

Front HalfWeight DODD c 

Organic ( ml) C qO'-/L /01. S'oL{9= fIJI. 501 e, .00 t \ 

Inorganic D 3&tlLf I r8. 3l'1;f l?-ro·32-Q\ ·,OOOt./ 

Total NetWeight ;OO'S' 
Project NlImber: --L./L..;/B;;....,_11_5.---.;____ 


Plant Name: ~C=4.c....:Mr:.!.:-:-'f.J.-/______ 


Date: t;;J-lfR-<7> , 


Analysis Type: 1/1/7- /Za ;'2 


Run 1 

Type Identification Final Tare Net 

Number Weight Weight Weight .! 

Filter p l#6~'f 2· &t;1-? d· {;;51"1 "OOO;{ 

Probe Rinse ( mI) B 37-96 (//. 13039 w¥. 80,/0 ,0000 

Fr.ont HalfWeight , Od O ~ 

Organic ( mI) C. 1./(1£/3 JP;J39v9 ~.39S'.i ' ,oDoD 

Inorganic D 3i?65 /37 z,z,oS 139- 2/'11­I oc; 13 

Total Net Weight ,OUIS 

RUN 2 

Type Identification Final Tare Net 

Number Weight Weight Weight 

Filter PI5B7­Z· &.L/Cf1­/). ~tJr I • {)/)O{p 

, Probe Rinse ( ml) B 379'J 7-~. 0111 '1-~. OilY d)()OO, 

Front HalfWeight I DOC ~ 

Organic ( mI) e.. /lOt/I{ IO~.Ol/fO //}&>. oi.{ft; 0 ,&0/0 

Inorganic P 36 Bfa //t;Z. fJ..pz,o lID 2, B~W .0 00 0 

Total NetWeight .001 \0 , 

Run 3 

Type Identification Final Tare Net 

Number Weight Weight Weight 

Filtex: p /S89; 2.&532­ d·~S3S 0000 ,. 

Probe Rinse ( ml) 8 3 goo (p 1-. 051-"1­{P1-·D)+£f .1.0000 

FrontHalf Weight .0000 

Organic ( , mI) ,t l.{o45 ' jOi).·l/813 j 0::;, ~8;;~ 100D5 

Inorganic [) 3B'Of­A'.R1· ~1'o/t- 1~ 9· 'fLf l/~ ',I DOD;;J.. 

Total Net Weight lODD'lIdentification 

F= 3 inch filter P := 47mmfilter B = 150m! Beaker C 250m! Beaker D :;; 400ml Beaker 
It e e 


FINAL WEIGHT . 


WEIGHING SHEET 


Time 

Date 

A,nalyst 

IDNo. .Run 

o')~'1rZ . 

4~' 

~~.'1 

//~ 5 

IS~L6 

I ~<r) 

Check Weight 

Check Weight 

Check Weight 

Weighiug (grams) 

1 234 5 

Tare 

Weight Weight 

~c COMPREHENSIVE 

E .EMISSION 

. S­ . SERVICES 
- - -- --

-- - -- -

c 

'ttJ 1:/$ 

Check Weight 

e e 

FINAL WEIGHT 


• ,WEIGHING SHEET 


, I ' 

Time 

Date 

,ADalyst 

Average I Final 

Tare 

'lDNo. Weigbt I Ru·i tdgh~W-1 ; 1 2 .. 5 

=C COMPREHENSIVE =E= - ­ -- . --­ EMISSION

--_. S-­ -- - SERVICES 
• 
 ~ 

"" 

'..,j 

~ .~ f'. 

e <.,,!l> 

~ '...9 ~ (1 

~ a I~ 

­ ~ 

C'< 

~ ~ 

~ I~ ~ ~ '1.3 -< '-.9 \l \.l "-..9 '-.9 " r,.9 ~ '~ 1.0 . n{ • ~" ("( ~ \\ /;'{ (~ t'. ~ '" ('< \1' 

V) 

..., 

i 

f 

.!9 

.Ef C") 

j 

. 

.~ ~ r­ iJ !'\'­ ...s )"t­ t: \i.... l':s ~ ~ It N Fl 

~ N ~ ~ - IN Q () .~ N) N) \.A

N) ~ N 

I~ ::r' ::.:t­ .~ r<) ~ ::r !'i­ '::l­ \n 0 

I • \ ~ ~ ~ ~ ~ -3 ....:J ~ ~ ~ ..j)

0­ ~ I~ I~ lei . l'i .\fl cc ~ c'i, \0 ~ ~ 

~ ~~ ('f\ <:r­ ~ <;) ~ I~ f'I­ ~ ~ C) M .~ . 

~ 

~ G1­ N ~ ~ ~ N ~ ~ C; \r. 

N ., S ~ :::r­ ::r. ~ t'<) ~ ~ ~ :::r­ 'Q

.c\.) \ .~ ....3 

i~ ~ ~ ~ 

i~ ...,:) . ~ ~ ~. ~ .~ l'li i\:"($ .~ i~ ri ~ V\ 

~ i - :J. ~ 'il . ~ .!l ~ e = ."iii \r., \ <:::l "'­

~ ~ 

:~ '-9 ~ V<:. 

.~ E= t "'" l:::c ~ 9 '-..1\ 

"" S!: -.. ~ ...... ~ 

- ~ ~ ~ ~ :.I) ~ 0 i'( --......... ........ ~: v 
'.. " 

IUl ~ 

I::

:a.111 

I---l,.----,--!~~f__+__+__+_,_+__+__+___!___I___'_I____+__+__I'----I_:_+__I 

-io 

l 4.l 4l ~. 'Q3 

~ .... 

- ~ ~ '" Q ~ ...... 

Q ~.

0 
e e' ­

TARE WEIGHT 


WEIGHING SHEET 


, . !, 

. Time I 9:/'1 

Date I II-:;;).J -05 

Analyst' I JJA It1. 

ill No. 

'. I 

nfo 

1 J--9'1 

:r7BS 

Check Weight 

Weighing (grams) 

. , 2 ,3 . 4 5 

:.c 

-­- E­--­ COMPREHENSIVE 

EMISSION 

, S~ SERVICES 
e e 'e 

TARE WEIGHT 

, WEIGHING SHEET 

Time , I 

Date 

AnaJyst 


Weighing (gr:ams) 
 Average 

ID NQ. 

1 2. 3 4 5 

61. if~q S 

61-, \'}~ I ' 

6~. "d'~!.f I 

Check Weight 

::}5.0( I ~ 

fl1-.o'5 

1-'b .f} '2 (; 0 

C011PREHENSIVE 

EMISSION' 

SERVICES 
e e
 • 

TARE WEIGHT 


WEIGHING SHEET 


Time 

Date 

Analyst 

IDNo. 

1 

e 

Check Weight 

Weighing (grams) 

2 3. 4 5 

CoMPREHENSIVE 

EMISSION 

SERVICES· 
e
 e e 

TARE.WEIGHT 


WEIGHING SHEET 


I _ 

Time 


Date 


Analyst 
 I 

Weighing (grams) 

ID No. . r 

1 2 3 .. 4 5 

. Check Weight II +0.0:3'j.$ It:ta· 01 <7'f 

~ C CoMPREHENSIVE 

E EMISSION 

S~ SERVICES 
tit tit

-

TARE WEIGHT 


WEIGHING SHEET 


Time 

Date. 

Analyst 

Check Weight 

Weighing (grams) 

4 5 

S'd0 3 

Iw~. :J01£{ 

::. C CoMPREHENSIVE 

E EMISSION 

~ S SERVICES 
. Appendix C 


. Field Data Forms 

Run No. 


Location: Cargill (EP 2) 


Date: 


.roject# 


% Isokinetic= 

Initial Meter Volume (Cubic Feet)= 


Final Meter Volume (Cubic Feet)= 


Meter Factor-


Final Leak Rate (cu Ftlmin)= 


Net meter Volume (Cubic Feet)::: 


Gas Volume (Dry Std Cubic Feet 68 Deg)= 


Barometric Pressure (in Hg) :: 


Static Pressure (Inches H20)= 


Stack Pressure (in Hg)= 


Percent Oxygen ::: 


Percent Carbon Dioxide= 


Moisture Collected(ml)= 


Percent Water-


Average Meter Temperature (F);;; 


Average Delta H ( in H20);;; 


Average Delta P (inches H20)= 


Averag~ Stack Temp (F)= 


. • ry Molecular Weight::: 

...,et Molecular Weight= 

Sampling Time (Minutes)= 


Nozzle Diameter(lnches)= 


Stack Round or Square::: 


Stack Dimention A (Inches)=· 


Stack Qimention B (Inches)= 


Equivilent Diameter (inches)'" 


Stack Area (Square Feet) = 


Pltot Coefficient:: 


Average Square Root of Delta P (inches H20)= 


Stack Velocity (Actual, ftlmin)= 


Flow Rate (Actual, Cubic ftlmin)= 


Flow Rate (Std, Dry, Cubic ftlmin 68 Deg)= 


Particulate Loading - Front Half 

Particulate Weight Net (g)'" 


. Paticulate Loading, Dry Std. 68 Deg (grlscf)= . 


Emission Rate (Iblhr)= 


Particulate Loading - Total Catch Including Impingers 

_ articulate Weight Net (g)= 

articulate Loading. Dry. Std. 68 Deg (grlscf)= 

Emission Rate (Ib/hr)= . 

Percent Impinger Catch= 

1, assumed 10mg 

Dec 12&13,2005 

11805 

98.6 

647.700 

807.004 

0.999 

0.002 

159.145 

166.100 

29.90 

1.30 

30.00 

21.00 

0.00 

35.0 

1.0 

47.6 

1.62 

4.4167 

66 

28.84 

28.73 

240.0 

0.135 

Round 

27.00 

27.00 

30.47 

3.98 

0.84. 

2.0985 

7,064 

28,086 

27.986 

0.0019 

0.0002 

0.04 

0.0100 

0.0009 

0.22 

81.00 
Run No. 


Location: Cargill (EP 2) 


Date: 


.roject# 

% Isokineti.c= 

Initial Meter Volume (Cubic Feet):: 


Final Meter Volume (Cubic Feet)= 


Meter Factor= 


Final.Leak Rate (cu Ftlmin)= 


Net meter Volume (Cubic Feet)= 


Gas Volume (Dry Std Cubic Feet 68 Oeg)= 


Barometric Pressure (in Hg) = 


Static Pressure (Inches H20)= 


Stack Pressure (in Hg)= 


Percent Oxygen = 


Percent Carbon Dioxide= 


Moisture Collected(ml)= 


Percent Water-


Average Meter Temperature (F)= 

Average Delta H ( in H20)= 

. Average Delta P (inches H20)= 

Average Stack Temp (F)= . 

. Dry Molecular Weight= "et Molecular Weight= 

Sampling Time (Minutes)= 


Nozzle Diameter(lnches)= 


Stack Round or Square= 


Stack Dimention A (lnches)= 


Stack Dimention B (Inches)= 


Equivilent Diameter (inches)= 


Stack Area (Square Feet) = 


Pilot Coefficient= . 


Average Square Root of Delta P (inches H20)= 


Stack Velocity (Actual, ftlmin)= 


Flow Rate (Actual, Cubic ftlmin)= 


Flow Rate (Std, Dry, Cubic ftlmin 68 Deg)= 


Particulate Loading - Front Half 


Particulate Weight Net (g)= 


Paticulate Loading, Dry Std. 68 Deg (grlscf)= 


Emission Rate (Iblhr)= 


Particulate Loading - Total Catch Including Impingers 


_ articulate Weight Net (g)= 

articulate Loading, Dry Std. 68 Deg (grlscf)= 

Emission Rate (lb/hr)= 

Percent Impinger Catch=, 

1 

Dec 12&13, 2005 

11805 

98.6 

647.700 ' 

807.004 

0.999 

0.002 

159.145 

166.100 

29.90 

1.30 

30.00 

21.00 

0.00 

35.0 

1.0 

47.6 

1.62 

4.4167 

66 

28.84 

28.73 

240.0 

0.135 

Round 

27.00 

27.00 

30.47 

3.9a 

0.84 

2.0985 

7,064 

28,086 

27,986 

0.0019 

0.0002 

0.04 

0.0072 

0.0007 

0.16 

73.6'1 
Run No. 


Location: Cargill (EP 2) 


Date: 


.roject.# 

% Isokinetic= 

Initial Meter Volume (Cubic Feet):::: 


Final· Meter Volume (Cubic Feet)::: 


Meter Factor::: 


Final Leak Rate (cu FUmin)= 


Net meter Volume (Cubic Feet);; 


Gas Volume (Dry Std Cubic Feet 68 D6g)= 


Barometric Pressure (in Hg) = 


Static Pressure (Inches H20)= 


Stack Pressure (in Hg)= 


Percent Oxygen ::: 


Percent Carbon Dioxide= 


Moisture Collected(ml)= 


Percent Water= 


Average Meter Temperature (F)= 


Average Delta H ( in H20)= 


Average Delta P (inches H20)= 


Average Stack Temp (F)= 


..r;; Molecular Weight= 

.,vet Molecular Weight:::: 

Sampling Time (Minutes)= 


Nozzle Diameter(lnches)= 


Stack Round or SqLiare: 


Stack Dimention A (Inches)= 


Stack Dimentlon B (lnches)= 


Equlvilent Diameter (inches)= 


Stack Area (Square Feet) = 


Pitot Coefficient= 


Average Square Root of Delta P (inches H20)= 


Stack Velocity (Actual, ftlmin)= 


Flow Rate (Actual, Cubic ftlmin)= 


Flow Rate (Std. Dry. Cubic ftlmin 68 Deg)= 


Particulate Loading - Front Half 

Particulate Weight Net (g)= 


Paticulate Loading, Dry Std. 68 Deg (grfscf)= 


Emission Rate (Ib/hr)= 


Particulate Loading - Total Catch Including Impingers 

A>articulate Weight Net (g)= 

.-particulate Loading, Dry Std. 68 Deg (grfscf)= 

Emission Rate (Ib/hr)= 

Percent Impinger Catch= 

2, assumed 10mg 

Dec 13, 2005 

11805 

99.1 

808.000 

965.794 

0.999 

0.000 

151.636 

162.468 

29.90 

1.30 

30.00 

21.00 

0.00 

37-.0 

1.1 

53.9 

1:56 

4.2208 

69 

28.84 

28.72 

240.0 

0.135 

Round 

27.00 

27.00 

30.47 

3.98 

0.84 

2.0504 

6,925 

27,533 

27,239 

0.0000 

0.0000 

0.00 

0.0100 

0.0009 

0.22 

100.00 
Run No. 


Location: Cargill (EP 2) 


Date: 


tfroject# 

% Isol<;inetic= 

Initial Meter Volume (Cubic Feet)::; 


Final Meter Volume (Cubic Feet)= 


Meter Factor= 


Final Leak Rate (cu Ftlmin)= 


Net meter Volume (Cubic Feet)= 


Gas Volume (Dry Std Cubi.c Feet 68 Deg)= 


Barometric Pressure (in Hg) ­

Static Pressure (Inches H20)= 


Stack Pressure (in Hg)= 


Percent Oxygen ::: 


Percent Carbon Dioxide= . 


Moisture Collected(rnl)= 


Percent Water= 


Average Meter Temperature (F)= 

Average Delta H ( in H20)= 

· Average Delta P (inches H20)= . 

Average Stack Temp (F)= 

. Dry Molecular Weight::: evet Molecular Weight= 

Sampling Time (Minutes)= 


Nozzle Diameter(lnches)= 


Stack Round or Square= 


· Stack Dimention A (Inches)";;; 


Stack Dimention B (Inches)­


Equivilent Diameter (inches)= 


Stack Area (Square Feet) ;; 


Pitot Coefficient= 


Average Square Root of Delta P (inches H20)= 


Stack Velocity (Actual, ftlmin)= 


Flow Rate (Actual, Cubic ftlmln)= 


· Flow Rate (Std, Dry, Cubic ft/min 68 Deg)= 


Particulate Loading;.. Front Half 

Particulate Weight Net (g)=. 


Paticulate Loading. Dry St~. 68 Deg (grlscf)= 


Emission Rate (Ib/hr)= 


Particulate Loading - Total Catch Including Impingers 

articulate Weight Net (9)= 

•	 articulate Loading, Dry Std. 68 Deg (gr/5cf)= 

Emission Rate (Ib/hr)= 

Percent Impinger Catch= 

2 

Dec 13. 2005 

11805 

99.1 

808.000 

965.794 

0.999 

0.000 

157.636 

162.468 

29.90 

1.30 

30.00 

21.00 

0.00 

37.0 

1.1 

53.9 

1.56 

4.2208 

69 

28.84 

28.72 

240.0 

0.135 

R.ound 

27.00 

27.00 

30.47 

3.98 

0:84 

2.0504 

6,925 

27,533 

27,239 

0.0000 

0.0000 

0.00 . 

0.0031 

0.0003 

0.07 

100.00 
Run No. 

Location: Cargill (EP 2) 

Date: 

tfroject# 

% Isokinetic= 

Initial Meter Volume (Cubic Feet)= 


Final Meter Volume (Cubic Feet)= 


Meter Factor: 


Final Leak Rate (cu Ftlmin)= 


Net meter Volume (Cubic Feet)= 


Gas Volume (Dry Std Cubic Feet 68 Deg)= 


Barometric Pressure (in Hg) = 


Static p'ressure (Inches H20)= 


Stack Pressure (in Hg)= 


Percent Oxygen: 


Percent Carbon Dioxide;:; 


Moisture Collected(mJ)= 


PercentWater= 


Average Meter: Temperature (F)= 


Average Delta H (in H20)= 


Average Delta P.(inches H20)= 


Average Stack Temp (F)= 


~7 Molecular Weight= , 

••et Molecular Welght= 

Sampling Time (Minutes): 


Nozzle Diameter(lnches)== 


Stack Round or Square= 


Stack Dimention A (Inches)= 


Stack Dimention B (Inches)= '. 


Equivilent Diameter (inches)= 


, Stack Area (Square Feet) == 


Pitot Coefficient= 


Average Square Root of De(ta P (inches H20)= 


Stack Velocity (Actual, fUmin)= 


Flow Rate (Actual, Cubic fUmin)= 


Flow Rate (Std, Dry, Cubic fUmin 68 Deg)= 


Particulate Loading - Front Half 

Particulate Weight Net (g)= 


Paticulate Loading, Dry Std. 68 Deg (grlscf)= 


Emission Rate (Ib/hr)= 


Particulate Loading - Total Catch Including Impingers 

_ articulate Weight Net (g)= 

artIculate Loading, Dry Std. 68 Deg (gr/8cf)= 

Emission Rate (Iblhr)= 

Percent Impinger Catch= 

3, assumed 10mg 

Dec 13&14, 2005 

11805 

98.7 

966.200 


1125.172 


0.999 

6.000 

158.813 

165.330 

29.90 

1.30 

30.00 

21.00 

0.00 

36.0 

1.0 

48.9 

1.61 

4.3792 

67 

28.84 

28.73 

240.0 

0.135 

Round 

27.00 

27.00 

30.47 

,3.98 

0.84 

2.0914 

7,050 

28,031 

27,845 

0.0000 

0.0000 

0.00 

0.0100 

0.0009 

0.22 

100.00 
Run No. 


Location: Cargill (EP 2) 


Date: 


.,roject# 


% Isokinetic= 

Initial Meter Volume (Cubic Feet)= 


Final Meter Volume (Cubic Feet)::::: 


Meter Factor= 


Final leak Rate (cu FUmin)= 


. 	Net meter Volume (Cubic Feet)= 


Gas Volume (Dry Std Cubic Feet 68 Deg)= 


Barometric Pressure (in Hg) ::; 


Static Pressure (Inches H20)::: 


stack Pressure (in Hg):::: 


Percent Oxygen ::; 


Percent Carbon Dioxide= 


Moisture Collected(ml)= 


Percent Water- . 


Average Meter Temperature (F)= 


Average Delta.H (in H20)= 


Average Delta P (inches H20)= 


Average Stack Temp (F)= 


. Dry Molecular Weight= .et Molecular Weight:: 

Sampling Time (Minutes)= 


Nozzle Diameter(lnches)= 


Stack Round or Square= 


Stack Dimention A (Inches)= 


Stack Dimention B (Inches)= 


Equivilent Diameter (inches)= 


Stack Area (Square Feet) = 


Pitot Coefficient= 


Average Square Root of DeitaP (inches H20)= 


StackVelocity (Actual, ftlmin)= 


Flow Rate (Actual, Cubic fUmin)= 


Flow Rate (Std; Dry, Cubic ftlmin 88 Deg)= 


Particulate Loading - Front Half 


Particulate Weight Net (g)= 


Paticulate Loading, Dry Std. 88Deg (grlscf)= 


Emission Rate (lb/hr)= 


Particulate Loading - Total Catch Including Impingers 


_ articulate Weight Net (g)= 

articulate Loading, Dry Std. 680eg (gr{scf)= . 

Emission Rate (Iblhr)= 

Percent Impinger Catch= 

3 

Dec 13&14, 2005 

11805 

·98.7 

988.200 

1125.172 

0.999 

0.000 

158.813 

185.330 

29.90 

1.30 

30.00 

21.00 

0.00 

36.0 

1.0 

48.9 

1.61 

4.3792 

67 

28.84 

28.73 

240.0 . 

0.135 

Round 

27.00 

27.00 . 

30.47 

3.98 

0.84 

2.0914 

7,050 

28,031 

27,845 

0.0000 

0.0000 

0.00 

0.0015 

0.0001 

0.03 

100.00 
Run No. 


Location: Cargill (EP 1) 


Date: 


.roject# . 

% Isokinetic= 

" 

Initial Meter Volume (Cubic Feet)= 


Final Meter Volume (Cubic Feet)= 


Meter Factor-


Final Leak Rate (cu Ftlmin)= 


Net meter Volume (Cubic Feet)= 


Gas Volume (Dry Std Cubic Feet 68 Deg)= 


Barometric Pressure (in Hg) = 


Static Pressure (Inches H20)= 


Stack Pressure (in Hg)= 


Percent Oxygen = 


Percent Carbon Dioxide= 


Moisture Gollected(ml)= 


Percent Water= 


Average Meter Temperature (F)= 


Average Delta H (in H20)=' 


Average Delta P (inches H20)= 


Average Stack Temp (F)= 


Dry Molecular Weight= 
 .et Molecular vveight= 

Sampling Time (Minutes)= 


Nozzle Diameter(lnches)= 


Stack Round or Square= 


Stack Dimention A (Inches)"" 


Stack Dimention B (Inches)= 


Equivilent Diameter (inches)= 


Stack Area (Square Feet) = 


Pitot Coefficient= 


Average Square Root of Delta P (inches H20)= .. 


Stack Velocity (Actual, ftlmin)= 


Flow Rate (Actual, Cubic ftlmin)= 


Flow Hate (Std, Dry, Cubic ftlmin 68 Oeg)= . 


Particulate Loading - Front Half 

PartiCUlate Weight Net (g)= 


Paticulate Loading,· Dry Std. 68 Deg (grlscf)= 


Emission Rate (Iblhr)= 


Particulate Loading - Total Catch Including Impingers 

articulate Weight Net (g)= 	 . 

•	 artiCUlate Loading, DrY Std, 68 Oeg (grlscf)= 

Emission Rate (Iblhr)= 

Percent Impinger Catch= 

1, assumed 10mg 

Dec 14, 2005 

11805 

99.3 

125.900 

291.135 . 

0.999 

0.003 

165.070 

165.461 

29.50 

0.58 

29.54 

21.00 

0.00 

32.0 

0.9 

61.6 

1.70 

0.7938 

53 

28.84 

28.74 

240.0 

0.207 

Round' 

36.60 

36.50 

41.19 

7.27 

0.84 

0.8780 

2,941 

21,367 

21,518 

0.0002 

0.0000 

0.00 

0.0100 

0.0009 

0.17 

98.00 
Run No. 


Location: Cargill (EP 1) 


Date: 


.roject# 

% Isokinetic= 

Initial Meter Volume (Cubic Feet)= 


Final Meter Volume (Cubic Feet)= 


Meter Factor= 


Final Leak Rate (cu Ftlmin)= 


Net meter Volume (Cubic Feet)= 


Gas Volume (Dry Std Cubic Feet 68 Deg)= 


Barometric Pressure (in Hg) = 


Static Pressure (Inches H20)= 


Stack Pressure (in Hg)= 


Percent Oxygen = 


Percent Carbon Dioxide::: 


Moisture Collected{ml)= 


Percent Water"" 


Average Meter Temperature (F)= 


Average Delta H (in H20)= 


Average Delta P (inches H20)= 


. Average Stack Temp (F)= 

. Dry Molecular Weight= evet Molecular Weight= 

Sampling Time (Minutes)= 


Nozzle Diameter(lnches)= 


Stack Round or Square= 


Stack Dimention A (Inches)= 


Stack Dimention S·(lnches)= 


EquivilentDiameter (inches)= 


Stack Area (Square Feet) = 


Pitot Coefficient= 


Average Square Root of Delta P (inches H20)= 


Stack Velocity (Actual, ftlmin)= 


Flow Rate (Actual, Cubic ftlmin)= 


Flow Rate (Std. Dry, Cubic ftlmin 68 Deg)= 


Particulate Loading - Front Half 


Particulate Weight Net (g)= 


Patlculate Loading, Dry Std. 68 Deg (grlscf)= 


Emission Rate (Ib/hr)= 


Particulate Loading - Total Catch Including Impingers 


.•artiCUlate Weight Net (g)= 

. articulate Loading, Dry Std. 68 Deg (grlscf)= 


Emission Rate (Iblhr)= 


Percent Impinger Catch= 


1 

Dec 14, 2005 . 

11805 

99.3 

125.900 

291.135 

0.999 

0.003 

165.070 

165.461 

29.50 

0.58 

29.54 

21.00 

0.00 

32.0 

0.9 

61·.6 

1.70 

0.7938 

53 

28.84 

28.74 

240.0· 

0.207 

Round 

36.50 

36.50 

41.19 

7.27 

0.84 

0.8780 

2.941 

21,367 

21,518 

·0.0002 

0.0000 

0.00 

0.0015 . 

0.0001 

0.03 

86.67 
Run No. 


Location: Cargill (EP 1) 


Date: 


4froject# 


% Isokinetic= 

Initial Meter Volume (Cubic Feet)= 


Final Meter Volume (Cubic Feet)= 


Meter F actor= 


Final Leak Rate (cu Ftlmin)= 


Net meter Volume (Cubic Feet)= 


Gas Volume (Dry Std Cubic Feet 68 Deg)= 


Barometric Pressure (in Hg) = 


Static Pressure (Inches H20)= 


Stack Pressure (in Hg)= 


Percent Oxygen = 


Percent Carbon Dioxide= 


Moisture Collected(ml)= 


Percent Water= 


Average Meter Temperature (F)= 


Average Delta H ( in H20)= 


Average Delta P (inches H20)= 


Average Stack Temp (F)= 


Dry Molecular Weight= 


. • et Molecular Weight= 

Sampling Time (Minutes)= 


Nozzle Diameter(lnches)= 


Stack Round or Square= 


Stack Dlmention A (Inches)= 


Stack Dimention B (lnches)= 


Equivilent Diameter (inches)= 


Stack Area' (Square Feet) = 


Pitot Coefficient= 


Average Square Root of Delta P (inches H20)= 


Stack Velocity (Actual, ftlmin)= 


Flow Rate (Actual, Cubic ftlmin)= 


Flow Rate (Std. Dry, Cubic ftlmin 68 Oeg)= 


Particulate Loading - FrontHalf 


Particulate Weight Net (g)= 


Paticulate Loading, Dry Std. 68 Deg (grlscf)= 


Emission Rate (Ib/hr)= 


Particulate Loading - Total Catch Including Impingers 


. _articulate Weight Net (g)= , 

articulate Loading. Dry Std. 68 Deg (grlscf)= 

Emission Rate (Ib/hr)= 

Percent Impinger Catch= 

2, assumed 10mg 

Dec 15.2005 

11805 

99.0 

291.500 

456.164 

0.999 

0.002 

164.499 

167.310 

29.55 

0.58 

29.59 

21.00 

0.00 

41.0 

0.9 

54.9 

1.71 

0.7908 

43 

28.84 

28.74 

240.0 

0.207 

Round 

36.50 

36.50 . 

41.19 

7.27 

0.84 

0.8809 

2.917 

21,198 

21,830 

0.0006 

0.0001 

0.0:1 

0.0100 

0.0009 

0.17 

94.00 
Run No. 

Location: Cargill (EP 1) 

Date: 

.roject# 

% Isokinetic= 

Initial Meter Volume (Cubic Feet)= 


Final Meter Volume (Cubic Feet)= 


Meter Factor= 


Final Leak Rate(cu Ftlmin)= 


Net meter Volume (Cubic Feet);::: 


Gas Volume (Dry Std Cubic Feet 68 Deg)= 


Barometric Pressure (in Hg) ::: 


. Static Pressure (Inches H20)= 


Stack Pressure (in Hg)= 


Percent Oxygen = 


Percent Carbon Dioxide= 


Moisture Collected(ml)= 


Percent Water= 


Average Meter Temperature (F)= 

. Average Delta H ( in H20):::: 


Average Delta P (inches H20)= 


Average Stack Temp (F)= 


Dry Molecular Weight::; 


~et Molecular Weight: 

Sampling Time (Minutes)= 


Nozzle Diameter(lnches)= 


Stack Round or Square: 


Stack Dimention A (Inches): 


Stack Dimention B (Inches)= 


Equivilent Diameter (inches)::::: 


Stack Area (Square Feet) = . 


Pitot Coefficient:;;: 


Average Square Root of Delta P (inches H20)= 


Stack Velocity (Actual. ftlmin)= 


FlowRate (Actual, Cubic ftlmin)::: 


Flow Rate (Std. Dry, Cubic ftlmin 68 Deg)= 


Particulate Loading Front Half 


Particulate Weight Net (g)= 


Paticulate Loading, Dry Std. 68 Deg (grlscf)= 


Emission Rate (Ib/hr)= 


Particulate Loading - Total Catch Including Impingers 


AParticulate WeIght Net (g)= 

Wparticulate Loading, Dry Std. 68 Deg (grlscf)= 

Emission Rate (tb/hr);;:: 

Percent Impinger Catch::::: 

2 

Dec 15, 2005 

11805 

99.0 

291.500 

456.164 

'0.999 

0.002 

164.499. 

167.310 

29.55 

0.58 

29.59 

21.00 

0.00 

41.0 

0.9 

54.9 

1.71 

0.7908 

43 

28.84 

28.74 

240.0 

0.207 

Round 

36.50 

36.50 

41.19 

7.27 

0.84 

0.8809 

2,917 

21,198 

21,830 

0.0006 

0.0001 

0.01 

0.0016. 

0.0001 

0.03 

62.50 
---------_.-_.­

Run No. 


Location: Cargill (EP 1) 


Date: 


.roject# 


. % Isokinetic= 


Initial Meter Volume (Cubic Feet)= 


Final Meter Volume (Cubic Feet)= 


Meter Factor= 


Final Leak Rate (cu FUmin)= 


l\Iet meter Volume (Cubic Feet)= 


Gas Volume (Dry Std Cubic Feet 68 Deg)= 


Barometric Pressure (in Hg) = 


Static Pressure (Inches H20)= 


Stack Pressure (in Hg)= 


Percent Oxygen = 


Percent Carbon Dioxide= 


Moisture Collected(ml)= 


Percent Water= 


Average Meter Temperature (F)= 


Average Delta H ( In H20)= 


Average Delta P (inches H20)= 


Average Stack Temp (F)= 


Dry Molecular Weight= 
 evet Molecular Weight= 

Sampling Time (Minutes)= 


Nozzle Diaineter(1 nches)= 


Stack Round or Square= 


Stack DimentionA (Inches)= 


Stack Dimention B (Inches)= 


Equivilent Diameter (inches)= 


Stack Area (Square Feet) = 


Pitot Coefficient= 


Average Square Root of Delta P (inches H20)= 


Stack Velocity (Actual, ftlmin)= 


Flow Rate (Actual, Cubic ftlmin)= 


Flow Rate (Std, Dry, Cubic ftlmin 68 Deg)= 


Particulate Loading - Front Half 


Particulate Weight Net (g)= 


Paticulate Loading, Dry Std. 68 Deg (grlscf)= 


Emission Rate (Ib/hr)= 


Particulate Loading - Total Catch Including Impingers 


_ articulate Weight Net (g)= 

articulate Loading, Dry Std. 68 Deg (grlscf)= 

Emission Rate (lblhr)= 

Percent Impinger Catch= 

3, assumed 10mg 

Dec 15, 2005 

11805 

99.1 

456.600 

622.164 

0.999 

0.004 

165.398 

166.084 

29.55 

0.58 

29.59 

21.00 

0.00 

39.5 

0.9 

61.5 

1.71 

0.7763 

43 

28.84 

28.74 

240.0' 

0.207 

Round 

36.50 

36.50 

41.19 

7.27. 

0.84 

0.8736 

2,894 

21,025 

21,649 

0.0000 

0;0000 

0.00 

0.0100 

0.0009 

0.17 

100.00 
Run No. 


Location: Cargill (EP 1) 


Date: 


4froject# 


% Isokinetic= 

Initial Meter Volume (Cubic Feet): 


Final Meter Volume (CubiC Feet)= 


Meter Factor= 


Final Leak Rate (cu Ftlmin)= 


Net meter Volume (Cubic Feet)= 


Gas Volume (Dry Std Cubic Feet 68 Deg)= 


Barometric Pressure (in Hg) = 


Static Pressure (Inches H20)= 


Stack Pressure (in Hg)= . 


Percent Oxygen = 


Percent Carbon Dioxide= 


Moisture Collected(ml)= 


Percent Water= . . 


Average Meter Temperature (F)= 


Average Delta H ( in H20)'" 


Average Delta P (inches H20)= 


Average Stack Temp (F)= 


.	~7Molecular Weight:::: 

,.,.et Molecular Weight= 

Sampling Time (Minutes)= 


Nozzle Diameter(lnches)= 


Stack Round or Square: 


Stack Dlmention A (lnches)= 


Stack Dimention B (Inches)= 


Equivilent Diameter (inches)= 


Stack Area (Square Feet) ::: 


Pitot Coefficient= 


Average Square Root of Delta P (inches H20)'" 


Stack Velocity (Actual, ftlmin)= 


Flow Rate (Actual, Cubic ftlmin)= 


Flow Rate (Std, Dry, Cubic ftlmin 88 Deg)= 


Particulate Loading- Front Half 


PartiCUlate Weight Net (g)= 


Paticulate Loading, Dry Std. 68 Deg (grlscf)= 


Emission Rate (Iblhr)= 


Particulate Loading - Total Catch Including Impingers 


_ articulate Weight Net (g)= 

articulate Loading, Dry Std. 68 Deg (grlscf)= 

Emission Rate (Ib/hr)= 

Percent Impinger Catch= 

3 

Dec 15,2005 

11805 

99.. 1 

456.600 

622.164 

0.999 

0.004 

165.398 

166.084 

29.55 

0.58 

29.59 

21.00 

0.00 

39.5 

0.9 

81.5 

1.71 

0.7763 

43 

28.84 

28.74 

240.0 

0.207 

Round 

36.50 

36.50 

41.19 

7.27 

0.84 

0.8736 

2,894 

21,025 

21,649 

0.0000 

0.0000 

0.00 

0.0007 

0.0001 

0.01 

100.00 
- -- - -

- - ---- --

'--':: 

-c ---­ -- COMPREHENSIVE 

-

-

-

=E=--

­ - - EMISSION 

- S­ -- -- SERVICES. 

Project • NUl.lWer_---'_ "__1.. J.......... It;: w...:.()_, 1/;:;­__________ 


RunNumber__.l..I________ 

Date _---!-.:::/J~/,-,-/.::..;:,.6.,-J...:...::1 ]--f-.1./(jL-5:.z....-__ 

Sample Type J Ij)fI). 

Plant Cu r 91 J( ff'2 . Location _~:....-__ ______ 

2 ;7 Assumed Moisture % . Meter Number _~~ 

Minutes Per Point (min.) Oven Number VA­ S~pling Time (min.) ).Y0 Umbilical Number . ISr/ 

Meter Factor Y <7,9 , ? Pitot Number ) 

Meter ~H@ If?' V Probe Number J 

Pitot Coefficient Cp O. ((~ Probe Length JI 

) ' t ) L Stack Axis 1 (inch.). 1 Nozzle Type _ .........Z<--_ 


)-'1"' Stack Axis 2 (mob.) """';;'--'-_ 

Barometric Pressure (in. Hg) --=:;;....J._..::..J.l~_ 'CIPU

, .) 

Static Pressure (in. IIzOJ __;...:./'..;::.J__ 

Nozzle Diameter (inch.) __0_,1-1..... 3...;..)''--_ 

Orsat 

Project Leader _~J~CI+-y~1r-J/'-'-J....;..l!"-~----­ Meter Operator --"J""·.!!.~+y.....Jr'-!j..J..'t...!l.V...;:S---- LabPerson ___________ 

SUpPOrt Personnel 

Schematic ofTesting Location 

Impingers 

1~ C 

I---'";;;;;;..;;...=.;..:;.;;;;.....~==.t...-.-~~~--=-z~~--I frvl,bf!J 

Pitot Leak Check 

RECOVERY DATA 


Trial %C02 %C02+%02 %02 

1 A 

2 !~ ~ hfen I 

3 

I ... 

Avg 

Final Initial Difference 

Impinger 1 . j£.')S IOf) ~. 

Impinger2 ItO il/U 0 

Impinger 3 lOt) 1f)1J 0 

. Impinger 4 /'7'3 7L

I3 '3° 

Condition/coior Total 3;; 

•

Notes: Filter Number: 
Field Data Sheet 
-- ---- - -- - -

-- -

-C­ -'. -- COMPREHENSIVE =E= EMISSION 

--

-S:::::, SERVICES . 

Project Number_..:../oI..-l~",-,(I,-I21-'_____ Project Leader __J~'u7_,;,._______ 

Run Number__)=:;;..;...,_____-'--___ Meter Operator _....:J::;..:...c,...L,_______ 

Date J)!Jjj(J), Lab Person __---'-________ i , 

Sample Type I 7:f2:d'< Support Personnel --LN...:.J,~IvIW/r..._______ 


Plant CU'1f (f 


Location e:f;2. 


Assumed Moisture % 1 Meter Number t.7­

Minutes Per Peint (min.) . L Oven Number AlA S~1ing Time (min.) . ).'fa Umbilical Number JJrL 

Meter Factor Y ~ Pitot Number J 

Meter tlli@tiifI)t~robe Number _..;..) __ 

Pitot Coefficient Cp (/11'1 Probe Length ) , 

") 'Ttl C; '­

Stack Axis 1 (inch.) / !. Nozzle Type _...:./....:J~_ Schematic ofTesting Location 

, ) ,.<1 Stack Axis 2 (inch.) --"_-'_'-_ 

Barometric Pressure (in. Hg) ').q, b 

Static Pressure (in. H20) __J...l....__ 

Nozzle Diameter (inch.) _--..;;(J-Io!""'ll....... 1'_ 
 Leak Rate Before 

Leak Rate After 

Pitot Leak Check 

RECOVERY DATA 


Orsat Impingers 


Final Initial DifI:erence 

Impinger I 10'] I Of; !7 

Impinger2 IOI) {C/O 0 

Impinger3 i(fO 11{l (/ 

Impinger4 '1~( 711 :>~ 

Condition/Color Total j't- . 

Trial %CO 

1 

2 

3 

Avg 

Notes: Filter Number: PJ~/1 
Field Data Sheet 

Run No -...;;2~_____ _ Project No. -L!...lI-v--rJ~{J-1-)--

.., Location Ef 2 

Date J)..;'3/t'5 /. I 

Operator .), ttl H, ~i. " 

Start Time" li#j I(). J~ Stop Time :f)-;+~ ILj;1 ~ 

§.. C . --== COMPREBENSIVE 

= E = EMISSION 

S~ SERVICES 
-

- ----

-- - -- -

Final Initial Difference 

Total 

-c ­ =:.: -==== COMPREHENSIVE =E EMISSION

• --- S=- SERVICES 

Project Number--ll:..J./...l.i~;';;;'[;...I.)f ______ Project Leader _.::..J,:;,I.,+'I...L.,-------

RuriNumber__J____-=-______ Meter Operator __J_,-,-'J..:.....(_______ 

Date ubPe~n _____________ ))"/IJJ:/Lj/flf J 

Support Personnel _'11...::.,~lv:........:....._______ 

Plant Gicutfl Sial/V tt"'"y 

Location 

Sample Type -.t...'J..1;I-'/A:....;·~(}.....______- ..... 

Epd. 

Assumed Moisture % Meter Number X 5" 


Minutes Per Point (min.) Oven Number N,4 


Sampling Time (min.) 2'ttl Umbilical Number ~ 

Meter Factor Y 0,'1 r Pitot Number ) 


Meter AH@ __ ..:;..I;...1 Cf;...~~9.L..·_ Probe Number _...."J,..,...._


• 

. Pitot Coefficient Cp rJ I Y~ Probe Length __)~/_ ::2 11 

Stack Axis >5
 I (inch.) ~~~I__ Nozzle Type ____ Schematic ofTesting Location 

;l t I[

Stack Axis 2 (inch.) . 

Barometric Pressure (in. Hg) :;2~. 11 


Static Pressure (in. H20) _-.:-11.,;,1..:;.)"...£__ 


Nozzle Diameter (inch.) _.__rl_I__{l........ f_ 


Pitot Leak Check 

RECOVERY DATA 

Orsat Impingers 

Trial %CO~ %C02+o/00Z %02 

1 \ 

2 _H f1 )2, en t 

3 I 

Ayg 

Impinger 1 

Impinger2 

Impinger3 

Imp' 

Condition/Color 

Notes: Filter Number: pI~;).tJ
Field Data Sheet 

Run No ............... 5_--'-___ 
 Project No. --</LL/-tL!f£/}<......;'S,--' __ 

• 	 Location tf.2, _, Date J)J/~ .J.JLfJpj I , • 

Operator ' J .l'*/1. W, 

Start Time 14 :t{f - 7;)} JI ~L.lCi_a: (;'3 Stop Time __.:....::fI~."2-1-.../...~I--",.I-
- --

Preliminary Velocity 


e 

Plant Project No. Jl (! I' 

Date /) ---/)---11 ~ tfd-... Location ).1,1 N

Staok 1.0. 


Pitot Cp O·tl 


Statio Pressure in H2O I, 2 


Barometer Pressure in. Hg 2.',2fL tJ 


Start Time 


$top Time 
 4 

Operators 

. SCHEMATfCOFTRAVERSEPOINTLAYOLn" 

Final Pitot Leak Check at <2:3" HlP P I F 

Traverse Velocity stack Cyclonic Flow 

Point Head Temp. Determinatron 

Number AP OF 

, in.H2Q AP at 0° Angle Whioh 

Reference Y~lds 

III NuHllP 

Ad 1? (; 1 

J. ':J.b '& 1 

'J '1/~ }(; 

'1 ~i- '1-11 

5 ).] 1-'(; 

~. 9(; :/(j 

,1­ !.L :J 10 

Vi ).4 'J.-.() 

9 )1 f +0 

lO ~I +0 

t) )',0 *V 

IL T<:) ~ &, ~ 

Traverse 

Point 

Number 

Velocity 

Head 

AP 

in.H:p 

Stack: 

Temp 

, OF 

Cycfonlc FlOW 

Determination 

6P atOG 

'Referenoe 

A:ngle Which 

YieldS 

aNuH AP 

lff 1./} 7fJ 

::< l.f. I 7-0 

J Lt~9 t1J 

t.t It. )' 1-fJ 

)' ~I ~ 1-0 

~ I:f C 'Hi 

t '1 ~q 10 

t( )'1 +0 

'1 G., J.-(j 

10 ~/~ '1{) , 

/ , '1 ~ &Y 

t) '1,) itt 

Notes: 

:::;. C -===, --:--" --= COMPREHENSIVE 

--- E----­ - - EWSSrON 

==- S ~ :SERVICES 
Total Number of Points(8, 12, 16,20,24)= " 24 EP 2 


Stack Diameter or Length(inches)= 27 


Round Square 

_oint Distance 

1 0,6 1 0.6 

2 1.8 2 1.7 

3 3.2 3 2.8 

4 4.8 4 3.9 

5 6.8 5 5.1 


6 9,6 6 6.2 


7 17.4 7 7.3 

8 20.3 8 8.4 

9 22.2 9 9.6 


10 23.8 10 10,7 


11 25.2 11 11.8 


12 26.4 12 12.9 


If stack diameter is less than 24 inches each point must be greater than 0.5 inches from wall 

if stack diameter is greater than 24 inches each point must be greater than 1.0 inches from wall 

• 


• 

-------

I . 

.1lIlo_ 

_ .. _.. 

EPA 

EMISSIO':OBS~VATION FORM 1 . FJ&Jl1n1111- , 1 I~ j21 1I 


Of .JdLFm n' 

~!\:J6IIlon I :3JLFeiT '" I0bsGtvaft00 DaIs

. )).:rJ· rJ(' ~,,%or\Q ~ r t · C(lA!~I'tII~'>; 30 rnGi6 :3(j 

~ Q 15 <lO -45 cornmm\!l 

1 0 0 0 0 2 0 {; a 0 s (J 0 0 tl 4 0 0 0 !J II () rJ 0 10 <Ii 0 0 0 {} 

7 (J 0-- If 0 ,.... " 

9 0 0 () (j 

9 () 0 0 0 

0 0 f) 

11 0 0 () 0 12 0 0 0 0 13 0 0 0 tJ 14 0 0 a () 

16 0 0 10 10 

16 0 0 0 10 17 rJ 0 10 0 18 0 0 () ()­

. 19 D () () 0 

120 0 () () (j 21 () 0 0 0 22 0 0 () f) 

23 0 0 a 0 24­ 0 0 0 10 -

26 0 0 0 0 26 0 0 /J 

.'0 () 0 0 28 (J a () 

29 0 {; IJ (} 

so 0 0 0 0 

VEOF1.1 

Ot...ILL.... 0 

. I o:n::"", I • •

--

0I:>s9Ml1I0n DaIB 

Tr-i3~t7)-

~ 0 11; 

1 () () 

2 (. 0 3 (j 0 4 0 () 5 () 0 6. () 0 7 () () 

8 () D 

\I 0 () 

10 () .() 

II V 0 

12 n 0 13 () () 

14 0 0 

15 cJ 0 

16 rJ 0 

17 a 0 18 (j O· 1'1 () 0 

20. a (j 

21 ·0 0 22 r) 0 2a ( ) 0 

24 ( ') 0 

25 C 0 26 0 0 . 27 a () 

28 rJ t/ 29 () 0 

31) a () 

lirria Z<:rno "&",1',..41 l~linllr:llfJ IOndltM 

q~DD 

30 45 COIl'orr'IInll 

f) 0 

7J /J 

0 0 

() 75 

IJ 0 

() (]. 

() 0 

() () 

10· 0 

(). () 

n () 

f) 7i 

O· 0 

0 iJ .. 

f) [} 

() 0 

0 {J 

0 O· 

0 0 

(/ (j. 

0 (; 

f) (J 

0 (J 

() CI 

() 7J 

() d 

0 fJ 

(j (; 

() 7J 

0 0 
Ot JtLmr n 

.1 ~I'm I . ~. to 

....­

EPA 

SIBLE EMISSION""OBS~VATION FORM 1 F=jE!¥¥' '}[- I to t4 t I. 

.. 140' 

---~-----~------~----- SI.K\ 1.OOOIkln t.i1e . 

VEOFl.l 

~1alD<D ... - '-U"I I1maL~fd i stQf1liYeifl i).d IOrdltN/f ;JfJ 

~ a ~5 ~ ~ .~~ 

1 (J () () 0 

2 0 0 1; (j 

3 [t) () -0 0 4 £:to () () 6 () () 0 /I o I> 6 15 7 rJ 7J (f iJ B (J () 0 () , rJ 0 (j. 0 10 a ·0 (J. 0 

11 C' %+1) {J 12 (J 0 () 18 Ll 

15 

14 0 E~ t1 () o 0 . 16 0 0 /J 0 17 (J (J /7 o· 18 -() O· tJ O· 

19 r;- 0 ?J 0 

~v (j 0 rJ· ...... 

21 0 "rJ (j () 

22 o· 0 0 0 .­

2-' 0 () -0 0 .. 24 0 0 rJ 0 25 () iJ (j iJ 25 0 0 75 0 27 0 () () 0 28 a () 0 D 

29 CJ 0· 0 {J 30 () (1 () 0 
- -

- -

• 


• 


-c - --­ -' - -- COMPRE:HENSIVE 

-

-

-

=E=-- - -­ EMISSION 

--

-- S-- -- ­ -- -

- SERVICES 

Project Number·----=J_/.::..~.:;..O.:...?______ 

R~NmOOer____' __~~__________ 

Date f~ntlj~ 

Sample Type 11#/12. , 


Plant Cq rir fI hOVX [(1'1 


Location _t.",;,P...,J/:,...-__________ 


Assumed Moisture % I,)" 


Minutes Per Point (min.) ~ 

SampliugTime (min.) ).Ll/) 


Stack Axis 2 (inch.) ---.:;/...lI~r.t-_~ 

MeterFactorY . D,911 

Meter AH@ ( , 7t ~ 

Pitot Coefficient Cp 0t r~f 

Stack Axis 1 (inch.) 3',('-(1 V ) 

'21.rll 

Meter Number )' 

Oven Number 1\1A 

Umbilical Number .!.:ilL 

PitotNumber l/I 

Probe Number 'i 

Probe Length ~_y~l_ '}1. 

Nozzle Type _..,f;.<....£/~._ 

Project Lea4er _J......,.'''::''';'&\-+.Y,,-/;!....-t~_fJ_)____ 


Meter Operator ----=J:...!(j~t~r.Lt.:...{T:.-{j,:->..,;.._____ 


LabPerson _____________ 


Support Personnel _.s.../1...l0W:):....l!(/..uH---:.;..W,."Lfi,-'-:....!Tft;==-__ 


Schematic ofTesting Location 

Barometric Pressure (in. Hg) 29.')& 

Static Pressure (in. H20) _-,(fL.:~,-,-f...;.~~ Leak Rate Before ' 

Leak Rate After • 

Pitot Leak Check 

'" 15 in_ H 

Nozzle Diamet~r (inch.) _---.,;..(J...;,~.:...;)..;;,.{I...l.f_ in.H 

After 

RECOVERY DATA 

Orsat Impingers 

Trial %C02 %C02+%02 %02 

1 A 

2 AI~~t eni 

3 

!­ ) 

Avg 

Final Initial Difference 

Impinge! I /OtJ 100 0 

Impinger2 100 100 0 .. Impinger3 i()() lOO , 0 

Impinger4 :JIG ·.7f'1lf 32 

Condition/Color Total 3A 

• 

P 15,fl Notes: )qve~ Q5 ~CGPlfl.{f Filter Number: 
Field Data Sheet 

Run No ..........J..______ 


_ Proj~ct No: ....J/f...!...'iL!:.r{!~')~--­

,.,LocatIon £,f f . 

, Date, IJ-II't/fJ5" 

Operator J.rrJ ItW. 

Start Time Jl:01 

1(; ;J:l., Stop Time _---..:..-::...L;_;....;;......-­

'",.,.~ . 
=.,C 

E 

S. 

COMPREHENSlVE 

EMISSION 

SERVICES 

Project Number~}..L/.JL.r..;;..(}~7______ J'~/. Project Leader --"""T"""..I..-.:..------­

Run Number_....:2::::::::...~~______ Meter Operator __J_~...;.r...l.(___- __ 


LWhnoo ____________________
 Date __-:..::.:..::-.--=.;::~::;;.......:.. 11- is-fl,­______


Sample Type IW (j2 , Support Personnel __tf...,;.:.(..;,lv~!_____ 


PJam c._crt tI >1 flVX eaf'f, 


Location 
 ~ll 

I ~ 7', Assumed Moisture % ~ L Meter Number _--"_ 

• 

MinutesPerPoint(min.) .1L OvenNumber IVA-


Sampling Time (min.) )~a UmbilicalNumher lJt/ 


MeterFactorY ,(/, Yf1 PitotNumher 4 


Meter AH@ I. ? '1 Probe Number '1 


Pitot Coefficient Cp 0,r~ Probe Length Y , 
 Jr. ,'1 )5 Stack Axis 1 (inch.) !l L Nozzle Type .____....,.-_ Schematic ofTesting Location 3/,5' {/ Stack Axis 2 (inch.) _..;:..f(~_ 

Barometric Pressure (in. Hg) 29. S' S'" 


Static Pressure (in. ~O) _---.,;():....:,~7_;-g __ 


Nozrl.~ Diameter (inch.) __{/..;....;I).~(/...]._ 


RECOVERY DATA 

Orsat Impingers 

Leak Rate After i 

Pitot Leak Check 

~ 15 

Trial %C02 %C02+%02 %02 

1 

'2 11 (.Qf1' , 

3 I \ VI V 

Avg 

Final Initial Difference 

Impinger 1 lOO 100 a 

Impinger2 lOb I (Jp 0 

Impinger 3 lOO I{J 0 0 

Impinger4 't12 13/ if) 

Condition/Color Total vl1 

• Notes: 

Filter Number: ,-'-f_/_5...... ·~--'7________
Field Data Sheet 

Run No ~;2_....--~___ 

_ Project No. --L!IIJL8j~l}-"-1?--­

• 	 Location Er I 

Date 1,2 ~/5'-{j) 

Operator J,rJ H, W.. 
 Start Time 
 r; rJ 

li:Of Stop Time _-..:..!::,.;,t.....::....::::....!.---­
- - - --- -- ---- -

-

:.-

-

- c------­ -' -- COMPREHENSIVE 

-

-

=E-==-- EMISSION 

--

- S­ -- -

- SERVICES . 

J, /r Project Nwnber---lJ..J,.'I...::,YI...:Il_"..:..,l_______ Project Leader ____,.;".-______ 

R~Number___J____________ M eter erator __---.,;.,-..:.- J.7'._______ Op 

Date _----.,;J;",.:;..)_-f:....Lr......:-(I~5"____ Lab Person ____-,-..________ 

Sample Type I 'J!).fl2 Support Personnel __/:.../.:.....:....'_U-:._____ 

Plant LCI, 1'1' (I 

Location _---=-e....!.f--:...i________ 

Assumed Moisture % " )' Meter Number 9 

Minutes Per Point (min.) -.iL.. Oven Number IV} 

Sampling Time (min.) 110 Umbilical Number ~ 

MeterFactorY . O. '1r PitotNumber I..f

(j /'1

Meter .6H@ __....;...,:.....r.L....:::U:-_ProbeNumber_ JI Lf ..;...._ 

Pitot Coefficient Cp 0/ /,1 Probe Length Lf I . 


Stack Axis 1 (inch.) llt,S'1 NozzleType .5} Schematic ofTesting Location 


J(,~{f . Stack Axis 2 (inch.) _~",z..._ 

Barometric Pressure (in. Hg) 2 9, ST 

(Z rg Static Pressure (in. HP) -.........;;..;....<.)...:;....-­

Nozzle Diaffieter (inch.) __(/,_'.:-}....:;(/_1-,--­

Leak R8te Before 

Leak: Rate After 

Pitot Leak Check 

~ 15 in. H 

in.H 

After 

RECOVERY DATA 


·Orsat Impingers 


Trial %C02 %C02+%02 %02 

I 

2 I I .... 

3 -~ 'Pre hI 

Avg 

Final Initial Difference 

Impinger 1 /00 !(f{) (/ 

Impinger2 ft/{; (dO 0 

Impinger3 ;O{) /(10 6 

Impinger4 7)~,Y ct«9 3Cf,} 

Condition/Color Total 5'1,$" 

P!J,tl· Notes: Sqv(J Q,S cr;(If{3 Filter Number: 

e 
Field Data Sheet 

Run No ----=------­ ..Project No. --L.f./I..Ji..[.l<:-U1-!--___ 

.,	Location {;f f 

Date I ).-/7~Q 9 

operator,--..:.J~~J!......-:-J.-~M.:.:..~rv"- .. __ Start Time _--IL._:"j. I) •

:~:"'\ ..£..,.!-=-~

-'[',4 	 2. Stop Time _--L...!._/ r~-----=-__ 

~CEC COMPREHENSIVE - SE EMISSION 

=== '= SERVICES 
• 

Preliminary Velocity 

Plant prOject.No..,~II~r'-.,;t~)..;...)'_~__ 

Date 1)//Ifif)" 

Location £1'7 r 

'''I c:: i {

Staokl.D·'--;)..Jlr~~4./.(,-------

Pitot Cp . (It y, 


Statio Pressure in H:p, ______ 


Barometer Pressure in. Hg,......;.-:;......L2,~>].K.-_ 

Start Tlme!___..,---~--

$top Timea.______- ____ 

Operator$;__....;.·_______~ 

. SCHEMATIC OF TRAVERSE POINT LAYOUT 

Rnal PitQt .Leak Cheek at ;:a:3" H:oP P I F 

Travers!' Velocity Staok Cyclonie Flow 

Point He-ad Temp, DetermInation 

Numb~r AP OF 

.·In.H,p tiP at O· Angle Which 

Reference Yields 

a NullAP 

41 . . 't ( ?b 

1 ,rt't­ 1'-1 .7 

J I ~7 !if 

'1 I )J . iJl 

t;' I ~2 ,.2 

& 1'.2 ?.2 

:f.­ ,&3 9") 

f{ 1 1-~ .. ?~ 

q 11b ,) 

It L3 5) 

I( I, ) 51 

h 1,2 I{q 

Notes: 

Traverse Velocity Stack Cyclonic FloW 

Point 

Number 

/}1 

2­

3 

li· 

~' -~ 

.1­

~ 

~ 

I{J 

Il 

11 

Head Temp Determination 

AP OF 

AP at·O· iri. H2O Angle Which 

Reference Yields 

a Null AP 

11~ 

."T I . ".'"./52 

~ &~ f) 

I y'f 5".2 

,')7 ')1 

..)1 s~ 

I )-~ 52 

.-:tP ,1 

, r~ I)) 

}, f· )'".2­

II b C)J 

\,2 ~y 

.. 

~c ~ COMPREHENSIVE 

-

=

~ 

- E-=-­- EMISSION' -= 

- S~ SERVICES 
Total Number of Points(8,12,16,20,24)= 24 EP 1 


Stack Diameter or Length{inches)'" 36.5 


. Round Square 

_oint Distance 

1 0.8 1 0.8 

2 2.4 2 2.3 

3 4.3 3 3.8 

4 6.5 4 ( 5.3 

5 9.1 5 6.8 

6 13.0 6 8.4 

7 23.5 7 9.9 

8 27.4 8 11.4 

9 30.0 9 12.9 


10 32.2 10 14.4 


11 34.1 11 16.0 


12 35.7 12 17.5 


If stack diameter is less than 24 inches each point must be greater than 0.5 inches from wall 

if stack diameter is greater than 24 inches each point must be greater than 1.0 inches from wall 
~Ncrne 

FadIlYNamo 

.BIraGI~ 

,star. Clti I~ 

I'\'CICaI$ 1\Wt# I~Mod& 

~--a~ I~Mod& 

IlleeI:IIl:e....••....' 

Haltt o1l!mt1s. PI. Het#of £mIsr. Pl. ReI.loOi::lfilllMlf

End 61af End 61af ' IJ6iIQ1c9to Elrist. pt, ~"'!i.I'nIII&.I'I"~1 

61af End stat End

~~ Jrng lone stat11mCo IErd1\TlQ 

III 30 4S Comrt!fInII 

1 

2 

3 

<4 .. 

I; 

/I 

'1 

B 

9 

III 

n 

~ 13 

14 

11:1 

16 

17 

111 

19 , ' 

20 ,'~ ..' 

-, 

2T 

22 

28 

24 

25 

20 

27 

28 

29 

SO 

.../f"I!1l! 

~I~"Q'laII.r8 It>a 

CEri!IecI Bv rom 

VEOF1.l 
AppendixD 


Pretest-Ca lib rations 

METER CAUBRA TION 

Operator M.W. K Factor 0.6274 

ate December 2, 2005 Meter Number 5 

• revious Y Factor 1.001 Orifice Number 23 

RUN 1 RUN2 


Meter Volume 


Final Cubic Feet 626.399 632.020 

Initial Cubic Feet 620.800 626.400 

Net Cubic Feet 5.599 5.620 

Meter Temperature 


Inlet 


Initial Oeg.F 53.0 55.0 

Final Oeg.F 55.0 57~0 

Outlet 

Initial Deg.F 53.0 54.0 

Final Deg.F 54.0 56.0 

Avg. lVIeter Temp Oeg. F 53.8 55.5 

Time sec 420.0 420.0 


Meter Delta H inches H2O 2.30 2.30 


Barometric Pressure inchesHg 30.05 30.05 


"oom Temperature. 

Initial Oeg. F 56.0 57.0 


Final Oeg. F 57.0 59.0 


Avg.Room Temperature Oeg.F 56.5 58.0 


Pump Vacuum inches Hg 15 15 

Vcr {std} dscf 5.807 5.799 


Vm (std) dscf 5.810 5.811 


Y Factor 1.000 0.998 


Delta H@ 1.969 1.959 


AverageY 0.999 

Average Delta H@ 1.964 

+/- 2% Criteria 


Percent of Avg Y 0.09 


PASS 


+/- 5% Criteria 


Percent of Final Y 0.23 


PASS 


e· 

-- -

CONSOLE WORK SHEET 

Operator: J..-:.M..s.:......lI.\J,;-.-._'-.,...-___ K Factor: ' G,f1~

Date: It -'J-. -O? Meter tD. -=- t{________ 

Previous Y Factor: \.0V\ Orifice Number: .;,..~_)______ 

Run Number 

METER VOLUME ' Units 1 2

Final ft3 ')..(,·J~1 J:: 3;2,O~ 0 , 

ffl' Initial C, :In. gOo ' (;2'. tICJD 

Meter Temperature 


INLET 


Initial 
 of ~J S-)'

of 

• 


Final' 
 ')S' '5'7 

OUTLET 


Initial 
 of ~.3 51 

Final of I :;-t./ S-~ 

Time sec 'l;;1. U ' 112 t) 

MeterLlH in. H2O 2. -; :J~ ') 

Barometric Pressure in. Hg ·~O OS 3t> .. D)

Room Temperature 


Initial 
 of 

. of 

~t: 

57 

?7 

Final .('9 

Pump Vacuum in. Hg /.5 /t.;""""

• -

-

- ----

­

-,-

=-c­- COMPREHENSIVE =E= - --' -- -- EMISSION 

==::::... .'S-="::: -- - SERVICES 
ORIFICE BRACKETING 

Operator M.W. BRACKET ORIFICES: 

December 2, 2005 Orifice No. 1 23 

.ate K Factor 0.6274 

Meter 5 Orifice No.2 20 Number 

Meter 0.999 K Factor 0.5409 Y Factor 

ORIFICE #1 ORIFICE #2 

Meter Volume 

Final Cubic Feet 637.745 643.340 

Initial Cubic Feet 632.100 637.800 

Net Cubic Feet 5.645 5.540 

Meter Temperature 

Inlet 

Initial Oeg.F 61.0 61.0 

Final Oeg. F 61.0 61.0 

Outlet 

Initial Oeg.F 58.0 59.0 

Final Oeg.F 59.0 60.0 

Avg: Meter Temp Oeg. F 59.8 60.3 

sec 420.0 480.0 Time 

Meter Delta H inches H2O 2.30 1.60 

Barometric Pressure inches Hg 30.05 30.05 

..oom Temperature 

Initial Deg.F 59.0 59.0 

Final Oeg.F 59.0 59.0 

Avg.Room Temperature Oeg.F 59.0 59.0 

. Pump Vacuum inches Hg 15 16 

Vcr (std) dscf 5.793 5.708 

5.667 Vm (std) dscf 5.790 

Y 1.001 1.007 Factor (brackets) 

+1- 2% Criteria 


Percent ofY 
 0.16 0.82 

PASS PASS 
- -

-

- ----- - - ---- - --

-- --

. BRACKETING WORK SHEET 


Operator: fI/1, tJ· . 

Date: -=-- 1:2-J..-/}? ______----'-_ 

f)at! 

Current Y Factor • 7 1 I 

../

Meter 1.0. ) ---=-____...--____ 

. I » 1L}. K Factor No. 1·--=(p:......:~~~---

K Factor No. 2~}f_V.-;.O_I.-,-l_~__ 

• 


METER VOLUME Units 1 2

Final tr '')1> '1"-l( G,'-{3. y';D

Initial tr C/) J-. jt)~ 3/, dnO 

Meter Temperature 


INLET 


Initial 
 G,I· 

Final OF GI ro/ 

of . Col 

OUTLET 

of Initial ~y 00

Final OF· S1 Co I 

Time sec 4:J. C t-/<7J{) 

MeterAH in. H2O J..·3 I,G

Barometric Pressure in..Hg Jc), D~ ,)2),0)

Room Temperature 


Initial 
 of s-q -jet 

Final of 5--1 51 

PumpVacuum in. Hg I~ I~

=-c­ =- .-=

=-E--":""


-

-

_. S-­

COMPREHENSNE 


EMISSION 


SERVICES 
Appendix E· 

.. Post-test Calibrations 

e. 

METER CALIBRATION 

Operator 	 M.W. K Factor 0.6274 

December 16,2005 Meter Number 5

eate 

revious Y Factor 0.999 Orifice Number 	 23 

RUN 1 RUN2 

Meter Volume 


Final Cubic Feet 628.415 634.118 


Initial Cubic Feet 622.800 628.500 


Net Cubic Feet 5.615 5.618 


Meter Temperature 

Inlet 

Initial Oeg.F 54.0 56.0 

Final Deg.F 56.0 56.0 

Outlet 

Initial Deg.F 54.0 '54.0 

Final Deg.F 54.0 55.0 

Avg. Meter Temp Deg. F 	 54.5 55.3 

Time 
 sec 	 420.0 420.0

Meter Delta H inches H2O 2.20 2.20 


Barometric Pressure inches Hg 29.75 29.75 


_oom Temperature 

Initial Deg.F 56.0 57.0 

Final Deg.F 57.0 57.0 

Avg.Room Temperature Deg.F 	 56'.5 57.0 

Pump Vacuum 	 inches Hg 16 16 

Vcr (std) dscf 5.749 5.746 


Vm (std) dscf 5.758 5.753 


Y Factor 
 0.998 0.999 


Delta H@ 1.889 1.888 


Average Y 0.999 


Average Delta H@ 1.889 


+/- 2% Criteria 


Percent of Avg Y 0.02 


PASS 


+/- 5% Criteria 


Percent of Final Y 0.04 


• 	

PASS 
-- -

• CONSOLE WORK SHEET 

. . 111 

K Factor: _"-:;C,=-)_·_I..!...--______ 

I '7 ~ \f.t;- 0 ~ 

Operator: ...LM---.l........::V...;:l.~~._~__ 

Date: ;,.....v'-_...:..------- Meter LD. _<5___..:..-____ 

Previous Y Factor: .......-I-q.+-q---11i~-- Orifice Number: -=~:........,.cJ=--_____ 


Run Number 


METER VOLUME 
 Units 1 2

Final 'ff! c,J.. L £/ IS­ &-:/-/'/1<1 

Initial ff! (,J)..- ~ 0 (.1 ~~t·)OO 

Meter Temperature 

INLET. 

Initial of ~L/ :;-!

Final .. of sC; :;-b

OUTLET 


Initial 
 of sf. 0

Final of 5-4 )) 

Time sec 7"';20 iJ':JJJ 

Meter ilH in. H2O :;2.;2. --;;~:z. . Barometric Pressure in. Hg 2'1.7S .29, '1r· 

Room Temperature 


Initial 
 ~7 

Final S-7 

Pump Vacuum in. Hg . j i(;; 

"F 

of 

S-C; . 

.>7 

~c COMPREH.ENSIVE . 

-

=E=--'

­ - - EMISSION' .::::::=.. '-= 

-.

-

-

S-­ ---- -.- SERVICES. 
• 

BRACKETING WORK SHEET 


. ftA W' Operator: L.....lo.l......;·._'_______ Meter 1.0. _s=~__.......-____


Date: l2: -lo-.O ( K Factor No. 1 ...L'..::.Cu~)-=-JI-~_'----.;.___ 

Current Y Factor ' qq1 K Factor No.2 ....:.•...i£..),.......:4...;...O...L.Q____


METER VOLUME 

Final 

Initial 

Meter Temperature 

INL.ET 

Initial 

Final 

OUTLET 

Initial 

Final 

. Time 

MeterAH 

Barometric Pressure 

Room Temperature 

Initial 

Final 

Pump Vacuum 

Units 

te 

te 

of 

of 

QF 

QF 

sec 

in. H2O 

·in.Hg 

of 

OF 

. in. Hg 

1 

G31.1/~ 

~3L./\)QO 

~( 

6--Z 

.~SS-7 

4:2 D 

2 . .,..... ..,

~1, 1S~ 

S--'? 

<,-1 

f(P 

I 

-', =. C 

·E 

. S-::::: .==.. .-= -­ -

.. 2 

tt-frJftft 

c,t./0.i.1 0 {) 

<f 

(,1 

.. 

5"7 

S'"! 

'-I ;JD 

I.t 

~1.?5" 

!:7' 

S7 

17 

COMPREHENSIVE 


E:MISSION 


SERVICES 
AppendixF 


Process Data 


• 
Rece~V&d: '1 61 6 2.40PM; 7122791225 .> Thompson Envir Cns~t; Page 2 

01/05/2006 14:36 FAX 7122191235 CARGILL SC CRUSH @002 

Compliance Emission Test 

Operating Data 

Owner;Cargill. Sioux City Date: December 12-!S.200S 

Source: West Gmid Clearl~1' PermIt #: 95-A·'23-B8 

Maximum Continuous Pl'oC8SS Rate (Manufacturer'l& Rating)'.-;;;~..;.;43:;...t;.;o;,;;nslhr=_~________ 

HistoriC<ll Average Process AatEl,_--.:..N~A-,--___________________ 

Historical Maximum PrOCs5$ Rate,__N..;.A...._________....._-~--_~........__ 


Types and Sources ( If any) of fuels normally Bumed__N__A____- _______~ 

Type of Fuel Bumed During t\'Il$ test,--_N;.;;A:.:.-_________---_~___ 

If Fuel is used Approximate QUl;ultities of each listed above bumea AnnuaJly._N...;A;..;....___ __ 

I 

, 

Recycling Capability No X I Rooyclfng io Progress No X 

Procc!jS QilLRl~ ing Run! 

~ Process Rate 

(gaUhr, IbJhr, tanslhr, etc•.. ) 

Process Flat$ Wet 

Percent Moisture (%) 

How Process Rate wa$ 

Determined 

RUn 1 Run 2.. Run 3 

23"f,...y/r 3" fp... r/)".. :.z.3. -fr,.nG/I,.. 

r,;,k t,&v./:$ 

Pnon Re$ponsib;;-'l ?~att P~arson 

Signature 1/{r,t;fC ~,~, 

TltleJPosJtlanCruSh Plaot S"'perintencient 

"' Please indicate mthe ;;tame /lnits as your bjMp&.aI informatioo 

~ j 

1 
R~ce1ved: 1/ 5/ 6 3:41PM; 7122791235 -> Thompson Snv1r Cns1t; Page a 

01/05/2006 14:37 FAX 7122791235 CARGILL SC CRUSH IaJ 003 

'/ 

J 

, A.I:R POLLlJT10N CONIllOL EQWMENT OPElUTlNG DATA 

, PIaw: Cargill. Sioux City Loe:u:iou Sioux City, IA 
 • Soum:Type West Grain Cie'aner. Rated Pf(ldm;tion _2_4_3_to...... Il!Ihr ............________


DatI: O~C; 12-/S, 2Q()S T~ ____ Ad:\all'tod-u.ctton • AirPtowData ____________ ~N~ __________ ------------------ __--------­

MecM1I7c:ll Collector: 


Tube'Dia. in... Number ofTulIe:i Design Ap ___in. HiO Gas Temp _,_"i! 


4p i:a ~ ])e:rip d'mItube @ 6.p @ "F 


Fan Rated RP. OpttaI:ia, Volts Opcr.Wn: Amps ____­

- . : l'Tt :ioiUltOT 

F'lCldNo. Primary Prim;uy S~ODdasy Ser.:ondary SparkRam 

Voltage (volts) Cur.rent (amps) Voltage (J{)I) CwrC!1t (ma) (per min) 

I 


.~ , 

, 

i 

I 

, 

!

~ 

I 

; 

·1 

r 

! 

Op=r;ting AJ:nps ----

Ap inH.O 

Opeming VolU ____ 

Pl:rSol'l R:spomil:lle fer D9tI .:.;M;;.:::lt;:;;;tt.;;.P.;;.;I:lIlllil=OI1=-_________ 

Si~ _______________________~~________ 

Tltie.ifasitiaEl Ct\1.Sh Plant SUEenntec.de-p.t 

LO 
Receivedo 1/ 5/ 6 3:41PM; 7122791235 -> Thompson Envir Cns~t; Page 4 

01/05/2006 14:37 FAX 7122791235 CARGILL SC CRUSH I4J 004 

I ~. 

•

1· 

Cotnpliance Emission Test 

Operating Data 

OWner: Cargill • Sioux City gate: December 12.15,2005 

Source: EP 2, Bean Dust Bllg Filter Permit #: 95-A-!l24-S8 

Maximum Continuous Proce:ss R~e (Manufacturer's Rating),___1.-87_.... 5....tOD=sIh,r;;...f_________ 

Historical Average Process Rate:..-----'-Nc.;..A-"----~____~~~---________ 

Hialorical Maximum Process ~te.__N....A:.o.-___- ___ __~-_~~~_~

Types and Sources ( if any ) of Fuels normally Bumed._.:...;N:...,:A---'-____________ 

Type of Fuel Burned During this test'---;..:.N::..:A=----________-~________ 

If fuel Is UlJed Approximate Quantities of eacll listed above burned AnI'1Ui;llly_... N_A~___~-

Recycling Capability No X , Recycling in Progress No X 

I 

• I

Proc:t$$ Rate 


(gallhr, Iblhr. tonslhr. etc .•. ) 


Proc;ess Rate Wet 


Peroe"t Moisture ("/.' 

Pro~ess Rate Dry 

How Proc&$S Rate was 


Detennined 


Run 1 Run 2" RunS 

I Y7.S ~r/J... rr-7. t(Ip....~,.. 1'77.)-A-f/)... 

. 

p~c.e(,.S ~cJ.1. 

p....,n ...~""" 

Slghature~ , 

Title/PDsitionCI1.llJh Plant St;pcrintendent 

ow Plsase jndicat, in the same !wit§. as your Iljstprica/ information 

• 
 I 
Race.i.ved: 1/ 5/ IS 3:41 PM; 7122791235 -> Thompson Env.i.r CnB~t; Page S 01/05/2006 14:37 FAX 7122791235 CARGILL SC CRlTSH I4J 005 

AIR POU.unON CONnOL EQUlP:MENT OPERATING DATA 

Plant C:Ulill- Sioux. City,. . L.rx:;:u,ioilSiQUX City, IA 

Soun;c type EP 2, Beall Dust Bag FIlter R.a1cd. Prgd.ul;tion 1 B 7.5 tonslhr 

Actu.al I'roductiQn---------~- DaI:c D~~ 12.IS, :z()O~ r~ ___"'-- ~No. _____________________ JJ: Pto-w Oam _____.-_--_ 

Mcebapi!ljl! Cl'tntetor: 

T.Dia. in.. Number oiTIibes Dc:rigrt ~p ___~-,in. HiO (]as Temp __-......_"" 

0b$c:ver:l6p . in H10 Dm~ dlnItube@ Observed Ap • @ " 

Fan Rated H.P. _ Opcr4I:iDs Volf!l Operadll.S' A.lt\ps ________ 

'1: Prtcil:ritator 

F'JdI1NQ. Pr.ima.ry Pri.m.aty Sc::aud.a.ry Set;ondiuy SFkP.atc 

VottaSC: (volts) CUITeDC (alPPS) VQIr.ap: (KV) Current (ma) (per min) 

-

ScrubCcr: 

T1)'C _.-...,,~_______-::- Ap(~sc;mbbu) _~._~_____ .in HzO· 

FaRlJ.tl'ld liP Operating Volts _---:____ Operating.Amps ___~_ 

L1quid. Cltt'Ulalion Rale gal/min. % .Ma.Icc-up ___ BlowdoWl1 ____ gpm SribWgWam Chal3S'= tnwva.I _ .....__________________..-

Stttllilg Tank Cle:uting lnrerva.l 

Ap _.. inHtO Diameter ___........~-

Fa.n R.:1ted f.l'p _~_____ Opentin8 Volts _____ OpmJ,tillg Amps ___......,,... 

Puson P.~nsible for Dm .;;..Ma;;:..:....It_Pe.;;.....ar;;;.::s;.oion.,;......___........~~___ 


Signatm'l:l __________~~______ 

T1IItlPasir:ion Crusb Plant SuperinttndeQL 

Cvc:!one;

Type: ~=-________ 

to 
Appendix G 

Opacity Certification­

·e 

VISIBLE EMISSIONS EVALUATOR 


This is to certify that 

Jay Titus 


met the specifications ofFederal Reference Method 9 (40 CFR Part 60, Appendix 

A, Method 9) and qualified as a visible emissions evaluator. Maximum deviation 

on white and black smoke did not exceed 7.5% opacity and no single error exceeding 15% opacity was incurred during the certification test conducted by Opaque 

Smoke School, LLC ofOverland Park, Kansas. This certificate is valid for six 

months from date of issue. ' 

Des Moines, lA October] 1, 2005 6036 

Location Date ofIssue Certificate Number 

Presideni/Director of Training