URS Corporation 

1600 Perimeter Park Dr. 

Morrisville, NC 27560

AES ICR Test 

Guayama, PR 

Project # 39682175 

PO # 226013.US

Analytical Report 

(0310-96)

EPA CTM-033

Hydrogen Cyanide 

EPA OTM-028 

Condensible Particulate Matter 

EPA Method 26A 

Hydrogen Chloride 

Hydrogen Fluoride

Enthalpy Analytical, Inc. 

Phone: (919) 850 - 4392 / Fax: (919) 850 - 9012 / www.enthalpy.com 

2202 Ellis Road Durham, NC 27703 - 5518 
I certify that to the best of my knowledge all analytical data presented in this report: 

 Have been checked for completeness 

 Are accurate, error-free, and legible 

 Have been conducted in accordance with approved protocol, and that all deviations and analytical 

problems are summarized in the appropriate narrative(s) 

This analytical report was prepared in Portable Document Format (.PDF) and contains  pages. 

EA# 0310-96 Page 2 of 236
Summary of Results

EA# 0310-96 Page 3 of 236
Compound Sample ID / Catch Weight (ug)

Unit 1 Run 1 Unit 1 Run 2 Unit 1 Run 3

Hydrogen Cyanide 2,261 1,887 2,253 

Unit 2 Run 1 Unit 2 Run 2 Unit 2 Run 3

Hydrogen Cyanide 2,751 2,497 2,475 

NaOH FS Pb Ace FB 3/8/10 NaOH FB 3/8/10

Hydrogen Cyanide 594 12.4 ND 16.3 ND

NaOH RB 3/11/10 Pb Ace RB 3/6/10 Pb Ace RB2 3/14/10

Hydrogen Cyanide 13.3 ND 6.59 ND 9.36 ND

H2O RB 3/6/10

Hydrogen Cyanide 10.2 ND

Company

Analyst

Parameters

# Samples

URS Corp. - RTP

KHB

EPA CTM-033

6 Runs, 6 Blanks

Client #

Job #

PO #

Report Date

39682175

0310-96

226013.US

4/8/2010

0310-96 res ctm033 4/9/2010

EA# 0310-96 Page 4 of 236
Compound Sample ID / Catch Weight (ug)

Unit 1 Run 1 Unit 1 Run 2 Unit 1 Run 3

Hydrogen Fluoride 384 ND 320 ND 315 ND

Hydrogen Chloride 375 ND 313 ND 307 ND

Unit 2 Run 1 Unit 2 Run 2 Unit 2 Run 3

Hydrogen Fluoride 305 ND 331 ND 354 ND

Hydrogen Chloride 297 ND 323 ND 345 ND

Field Blank RB H2SO4

Hydrogen Fluoride 210 ND 63.0 ND 0 ND

Hydrogen Chloride 205 ND 61.5 ND 0 ND

Company

Analyst

Parameters

# Samples

URS Corp. - RTP

EO

EPA Method 26A

6 Runs, 2 Blanks

Client #

Job #

PO #

Report Date

39682175

0310-96

226013.US

3/31/2010

0310-96 res m26a 4/9/2010

EA# 0310-96 Page 5 of 236
Compound Sample ID / Condensible Particulate Matter (CPM) Weight (mg)

Unit 1 Run 1 Unit 1 Run 2 Unit 1 Run 3

Net Organic Catch 20.3 15.0 13.0

Corrected Inorganic 330.8 220.4 336.4

FB Corrected CPM 349.1 233.5 347.4

Unit 2 Run 1 Unit 2 Run 2 Unit 2 Run 3

Net Organic Catch 13.9 12.7 10.9

Corrected Inorganic 159.2 176.6 234.3

FB Corrected CPM 171.1 187.3 243.2

Filter Blank Run 8 Run 9

Net Organic Catch 2.9 0.0 0.0

Corrected Inorganic 10.3 0.0 0.0

FB Corrected CPM 11.2 -2.0 -2.0

Field Blank

Organic Catch 8.3 If Train Blank Corrected CPM is >2.0 mg,

Inorganic Catch 6.3 then sample correction is 2.0 mg.

CPM 14.6

Company

Analyst

Parameters

# Samples

URS Corp. - RTP

ARM

EPA OTM-028

6 Runs, Blanks

Client #

Job #

PO #

Report Date

39682175

0310-96

226013.US

3/31/2010

0310-96 res OTM-028 4/9/2010

EA# 0310-96 Page 6 of 236
Results

EA# 0310-96 Page 7 of 236
MDL 0.0143 (ug/mL) Lower Curve Limit 0.104 (ug/mL)

LOQ 0.104 (ug/mL) Upper Curve Limit 2.08 (ug/mL)

Compound

Sample

ID

Lab ID

 # 1

Lab ID

 # 2

Analysis

Method

Ret 

Time 

(min)

Ret 

Time 

(min)

% Diff

Ret

Conc

# 1

(ug/mL)

Conc

# 2

(ug/mL)

% Diff

Conc

Avg

Conc

(ug/mL)

U1-Pb-R1 036-4901.D 036-4902.D 0310-96C.M NA NA NA 0.0143 0.0143 0.0 0.0143 

U1-NaOH-R1 037-5001.D 037-5002.D 0310-96C.M 8.22 8.25 0.4 1.33 1.31 0.6 1.32 

U1-Pb-R2 038-5101.D 038-5102.D 0310-96C.M NA NA NA 0.0143 0.0143 0.0 0.0143 

U1-NaOH-R2 039-5201.D 039-5202.D 0310-96C.M 8.26 8.30 0.5 0.887 0.908 1.1 0.897 

U1-Pb-R3 040-5301.D 040-5302.D 0310-96C.M NA NA NA 0.0143 0.0143 0.0 0.0143 

U1-NaOH-R3 041-5601.D 041-5602.D 0310-96C.M 8.31 8.31 0.0 0.972 0.981 0.5 0.977 

U2-Pb-R1 042-5701.D 042-5702.D 0310-96C.M NA NA NA 0.0143 0.0143 0.0 0.0143 

U2-NaOH-R1 043-5801.D 043-5802.D 0310-96C.M 8.23 8.20 0.3 1.35 1.39 1.3 1.37 

U2-Pb-R2 044-5901.D 044-5902.D 0310-96C.M NA NA NA 0.0143 0.0143 0.0 0.0143 

U2-NaOH-R2 045-6001.D 045-6002.D 0310-96C.M 8.16 8.14 0.2 1.15 1.16 0.6 1.15 

U2-Pb-R3 046-6301.D 046-6302.D 0310-96C.M NA NA NA 0.0143 0.0143 0.0 0.0143 

U2-NaOH-R3 047-6401.D 047-6402.D 0310-96C.M 8.02 8.03 0.2 1.16 1.19 1.2 1.17 

Hydrogen Cyanide

Company

Analyst

Parameters

# Samples

URS Corp. - RTPKHBEPA CTM-0336 Runs, 6 Blanks

Client #

Job #

PO #

Report Date

396821750310-96226013.US4/8/2010

0310-96 res ctm033 

EA# 0310-96 Page 8 of 236
MDL 0.0143 (ug/mL) Lower Curve Limit 0.104 (ug/mL)

LOQ 0.104 (ug/mL) Upper Curve Limit 2.08 (ug/mL)

Compound

Sample

ID

Lab ID

 # 1

Lab ID

 # 2

Analysis

Method

Ret 

Time 

(min)

Ret 

Time 

(min)

% Diff

Ret

Conc

# 1

(ug/mL)

Conc

# 2

(ug/mL)

% Diff

Conc

Avg

Conc

(ug/mL)

Hydrogen Cyanide

Company

Analyst

Parameters

# Samples

URS Corp. - RTPKHBEPA CTM-0336 Runs, 6 Blanks

Client #

Job #

PO #

Report Date

396821750310-96226013.US4/8/2010

LD / U2-NaOH-R1 062-2301.D 062-2302.D 0310-96D.M 8.19 8.22 0.5 1.48 1.50 0.6 1.49 

NaOH FS 050-6701.D 050-6702.D 0310-96C.M 8.01 8.02 0.2 0.843 0.829 0.9 0.836 

NaOH FB 3/8/10 048-6501.D 048-6502.D 0310-96C.M NA NA NA 0.0143 0.0143 0.0 0.0143 

NaOH RB 3/11/10 049-6601.D 049-6602.D 0310-96C.M NA NA NA 0.0143 0.0143 0.0 0.0143 

Pb Ace FB 3/8/10 051-0801.D 051-0802.D 0310-96D.M NA NA NA 0.0143 0.0143 0.0 0.0143 

Pb Ace RB 3/6/10 052-0901.D 052-0902.D 0310-96D.M NA NA NA 0.0143 0.0143 0.0 0.0143 

Pb Ace RB2 3/14/10 053-1001.D 053-1002.D 0310-96D.M NA NA NA 0.0143 0.0143 0.0 0.0143 

H2O RB 3/6/10 054-1101.D 054-1102.D 0310-96D.M NA NA NA 0.0143 0.0143 0.0 0.0143 

0.1N NaOH - RB 007-0801.D 007-0802.D 0310-96C.M NA NA NA 0.0143 0.0143 0.0 0.0143 0.1N NaOH - RB 007-0701.D 007-0702.D 0310-96D.M NA NA NA 0.0143 0.0143 0.0 0.0143 0.1N NaOH - RB 007-0801.D 007-0802.D 0310-96G.M NA NA NA 0.0143 0.0143 0.0 0.0143 

0310-96 res ctm033 

EA# 0310-96 Page 9 of 236
MDL 0.0143 (ug/mL) Lower Curve Limit 0.104 (ug/mL)

LOQ 0.104 (ug/mL) Upper Curve Limit 2.08 (ug/mL)

Compound

Sample

ID

Lab ID

 # 1

Lab ID

 # 2

Analysis

Method

Ret 

Time 

(min)

Ret 

Time 

(min)

% Diff

Ret

Conc

# 1

(ug/mL)

Conc

# 2

(ug/mL)

% Diff

Conc

Avg

Conc

(ug/mL)

Hydrogen Cyanide

Company

Analyst

Parameters

# Samples

URS Corp. - RTPKHBEPA CTM-0336 Runs, 6 Blanks

Client #

Job #

PO #

Report Date

396821750310-96226013.US4/8/2010

MS / U2-NaOH-R1 015-1101.D 015-1102.D 0310-96G.M 8.39 8.39 0.0 1.19 1.18 0.3 1.18 

Spike 

Native 

Spike R

MSD / U2-NaOH-R1 016-1201.D 016-1202.D 0310-96G.M 8.38 8.39 0.0 1.17 1.18 0.3 1.18 

Spike 

Native 

Spike R

LCS #1 055-1201.D 055-1202.D 0310-96D.M 8.00 8.02 0.2 1.16 1.17 0.4 1.16 

Spike 

Spike R

LCS #2 056-1501.D 056-1502.D 0310-96D.M 7.97 7.98 0.1 1.15 1.19 1.8 1.17 

Spike 

Spike R

0310-96 res ctm033 

EA# 0310-96 Page 10 of 236
MDL 0.0200 (ug/mL) Lower Curve Limit 0.100 (ug/mL)

LOQ 0.100 (ug/mL) Upper Curve Limit 14.8 (ug/mL)

Compound

Sample

ID

Lab ID

 # 1

Lab ID

 # 2

Analysis

Method

Ret 

Time 

(min)

Ret 

Time 

(min)

% Diff

Ret

Conc

# 1

(ug/mL)

Conc

# 2

(ug/mL)

% Diff

Conc

Avg

Conc

(ug/mL)

Acid 

Correct

Facto

Unit 1 Run 1 025-2801.D 025-2802.D HPLC51PG56.M NA NA NA 0.0200 0.0200 0.0 0.0200 1.053 Unit 1 Run 2 028-3501.D 028-3502.D HPLC51PG56.M NA NA NA 0.0200 0.0200 0.0 0.0200 1.053 Unit 1 Run 3 029-3601.D 029-3602.D HPLC51PG56.M NA NA NA 0.0200 0.0200 0.0 0.0200 1.053 Unit 2 Run 1 030-3701.D 030-3702.D HPLC51PG56.M NA NA NA 0.0200 0.0200 0.0 0.0200 1.053 Unit 2 Run 2 031-3801.D 031-3802.D HPLC51PG56.M NA NA NA 0.0200 0.0200 0.0 0.0200 1.053 Unit 2 Run 3 032-3901.D 032-3902.D HPLC51PG56.M NA NA NA 0.0200 0.0200 0.0 0.0200 1.053 

Field Blank 033-4001.D 033-4002.D HPLC51PG56.M NA NA NA 0.0200 0.0200 0.0 0.0200 1.053 RB H2SO4 034-4301.D 034-4302.D HPLC51PG56.M NA NA NA 0.0200 0.0200 0.0 0.0200 1.053 

0.01N H2SO4/NaOH Blank 007-0801.D 007-0802.D HPLC51PG56.M NA NA NA 0.0200 0.0200 0.0 0.0200 1.053 0.01N H2SO4/NaOH Blank 093-3201.D 093-3202.D HPLC51PG56.M NA NA NA 0.0200 0.0200 0.0 0.0200 1.053 

Hydrogen Fluoride as Fluoride

Company

Analyst

Parameters

# Samples

URS Corp. - RTPEOEPA Method 26A6 Runs, 2 Blanks

Client #

Job #

PO #

Report Date

396821750310-96226013.US3/31/2010

0310-96 res m26a 

EA# 0310-96 Page 11 of 236
MDL 0.0200 (ug/mL) Lower Curve Limit 0.100 (ug/mL)

LOQ 0.100 (ug/mL) Upper Curve Limit 14.8 (ug/mL)

Compound

Sample

ID

Lab ID

 # 1

Lab ID

 # 2

Analysis

Method

Ret 

Time 

(min)

Ret 

Time 

(min)

% Diff

Ret

Conc

# 1

(ug/mL)

Conc

# 2

(ug/mL)

% Diff

Conc

Avg

Conc

(ug/mL)

Acid 

Correct

Facto

Hydrogen Fluoride as Fluoride

Company

Analyst

Parameters

# Samples

URS Corp. - RTPEOEPA Method 26A6 Runs, 2 Blanks

Client #

Job #

PO #

Report Date

396821750310-96226013.US3/31/2010

MS U1 R1 026-3301.D 026-3302.D HPLC51PG56.M 2.79 2.79 0.0 3.31 3.32 0.2 3.31 1.053 

S

N

Sp

MSD U1 R1 027-3401.D 027-3402.D HPLC51PG56.M 2.80 2.79 0.0 3.32 3.31 0.1 3.31 1.053 

S

N

Sp

HPLC51pg56 #LCS 006-0701.D 006-0702.D HPLC51PG56.M 2.79 2.79 0.0 4.20 4.21 0.1 4.21 1.053 

S

Sp

HPLC51pg56 #LCS 092-3101.D 092-3102.D HPLC51PG56.M 2.80 2.80 0.0 4.23 4.23 0.1 4.23 1.053 

S

Sp

0310-96 res m26a 

EA# 0310-96 Page 12 of 236
MDL 0.0200 (ug/mL) Lower Curve Limit 0.100 (ug/mL)

LOQ 0.100 (ug/mL) Upper Curve Limit 14.8 (ug/mL)

Compound

Sample

ID

Lab ID

 # 1

Lab ID

 # 2

Analysis

Method

Ret 

Time 

(min)

Ret 

Time 

(min)

% Diff

Ret

Conc

# 1

(ug/mL)

Conc

# 2

(ug/mL)

% Diff

Conc

Avg

Conc

(ug/mL)

Acid 

Correct

Facto

Unit 1 Run 1 025-2801.D 025-2802.D HPLC51PG56.M NA NA NA 0.0200 0.0200 0.0 0.0200 1.028 Unit 1 Run 2 028-3501.D 028-3502.D HPLC51PG56.M NA NA NA 0.0200 0.0200 0.0 0.0200 1.028 Unit 1 Run 3 029-3601.D 029-3602.D HPLC51PG56.M NA NA NA 0.0200 0.0200 0.0 0.0200 1.028 Unit 2 Run 1 030-3701.D 030-3702.D HPLC51PG56.M NA NA NA 0.0200 0.0200 0.0 0.0200 1.028 Unit 2 Run 2 031-3801.D 031-3802.D HPLC51PG56.M NA NA NA 0.0200 0.0200 0.0 0.0200 1.028 Unit 2 Run 3 032-3901.D 032-3902.D HPLC51PG56.M NA NA NA 0.0200 0.0200 0.0 0.0200 1.028 

Field Blank 033-4001.D 033-4002.D HPLC51PG56.M NA NA NA 0.0200 0.0200 0.0 0.0200 1.028 RB H2SO4 034-4301.D 034-4302.D HPLC51PG56.M NA NA NA 0.0200 0.0200 0.0 0.0200 1.028 

0.01N H2SO4/NaOH Blank 007-0801.D 007-0802.D HPLC51PG56.M NA NA NA 0.0200 0.0200 0.0 0.0200 1.028 0.01N H2SO4/NaOH Blank 093-3201.D 093-3202.D HPLC51PG56.M NA NA NA 0.0200 0.0200 0.0 0.0200 1.028 

Hydrogen Chloride as Chloride

Company

Analyst

Parameters

# Samples

URS Corp. - RTPEOEPA Method 26A6 Runs, 2 Blanks

Client #

Job #

PO #

Report Date

396821750310-96226013.US3/31/2010

0310-96 res m26a 

EA# 0310-96 Page 13 of 236
MDL 0.0200 (ug/mL) Lower Curve Limit 0.100 (ug/mL)

LOQ 0.100 (ug/mL) Upper Curve Limit 14.8 (ug/mL)

Compound

Sample

ID

Lab ID

 # 1

Lab ID

 # 2

Analysis

Method

Ret 

Time 

(min)

Ret 

Time 

(min)

% Diff

Ret

Conc

# 1

(ug/mL)

Conc

# 2

(ug/mL)

% Diff

Conc

Avg

Conc

(ug/mL)

Acid 

Correct

Facto

Hydrogen Chloride as Chloride

Company

Analyst

Parameters

# Samples

URS Corp. - RTPEOEPA Method 26A6 Runs, 2 Blanks

Client #

Job #

PO #

Report Date

396821750310-96226013.US3/31/2010

MS U1 R1 026-3301.D 026-3302.D HPLC51PG56.M 3.74 3.74 0.0 2.85 2.85 0.0 2.85 1.028 

S

N

Sp

MSD U1 R1 027-3401.D 027-3402.D HPLC51PG56.M 3.74 3.74 0.0 2.85 2.85 0.1 2.85 1.028 

S

N

Sp

HPLC51pg56 #LCS 006-0701.D 006-0702.D HPLC51PG56.M 3.77 3.77 0.0 3.78 3.78 0.0 3.78 1.028 

S

Sp

HPLC51pg56 #LCS 092-3101.D 092-3102.D HPLC51PG56.M 3.74 3.74 0.0 3.80 3.80 0.0 3.80 1.028 

S

Sp

0310-96 res m26a 

EA# 0310-96 Page 14 of 236
Analysis of Condensible Particulate Recovery

Sample ID Number Field Blank Unit 1 Run 1 Unit 1 Run 2 Unit 1 Run 3

Organic

Beaker Number 3526 3520 3521 3522

Initial Acetone Volume, mL 21 83 73 38

Initial MeCl2 Volume, mL 17 165 167 142

Lab MeCl2 Volume, mL 165 Dates 165 Dates 165 Dates 165 Dates

Final Weight, g 2.6551 3/30/10 2.6819 3/30/10 2.6597 3/30/10 2.6583 3/30/1

Reweigh, Final, g 2.6550 3/31/10 2.6817 3/31/10 2.6596 3/31/10 2.6582 3/31/1

Beaker Tare, g 2.6468 3/24/10 2.6615 3/24/10 2.6446 3/24/10 2.6452 3/24/1

Net Organic Catch, mg 8.3 20.3 15.0 13.0

Inorganic

Beaker Number 3565 Dates 3559 Dates 3560 Dates 3561 Dates

Final Weight, g 2.6707 3/30/10 2.9634 3/30/10 2.8499 3/30/10 2.9662 3/30/1

Reweigh, Final, g 2.6706 3/31/10 2.9630 3/31/10 2.8498 3/31/10 2.9660 3/31/1

Beaker Tare, g 2.6642 3/26/10 2.6318 3/26/10 2.6288 3/26/10 2.6288 3/26/1

H2O FV, mL 86 534 498 503

Resuspended Volume, mL 100 100 100 100

Removed Pre-aliquot, mL 0.5 0.5 0.5 0.5

Pre-aliquot CF 1.01 1.001 1.001 1.001

Removed Post-aliquot, mL 0.5 0.5 0.5 0.5

Post-aliquot CF 1.01 1.01 1.01 1.01

Net Inorganic, mg 6.5 333.2 222.3 339.3

Ammonium Correction, mg 0.1 2.4 1.9 2.9

Corrected Inorganic, mg 6.3 330.8 220.4 336.4

Condensible Particulate Matter, mg 14.6 351.1 235.5 349.4

TB Corrected CPM, mg 349.1 233.5 347.4

-----------------------------------------------------------------Client Blank Analyses------------------------------------------------------------------

Type Blank MeCl Blank Type Blank H2O Blank Type Blank 

Beaker Number 3528 Beaker Number 3567 Beaker Number 

Tare weight, g 2.6319 Tare weight, g 2.6558 Tare weight, g 

Dry Residue Weight, g 2.6393 Dry Residue Weight, g 2.6569 Dry Residue Weight, g 

Reweigh, Final, g 2.6393 Reweigh, Final, g 2.6568 Reweigh, Final, g 

MeCl2 Residue, g 0.0074 Water Residue, g 0.0010 Acetone Residue, g 

MeCl2 Volume, mL 110 Water Volume, mL 106 Acetone Volume, mL 

Max. MeCl2 Residue, g 0.0022 Max. Water Residue, g 0.0011 Max. Acetone Residue, 

---------------------------------------------------------------In-House Blank Analyses------------------------------------------------------------------

Type Blank MeCl Blank Type Blank H2O Blank Type Blank 

Beaker Number 3529 Beaker Number 3568 Beaker Number 

Tare weight, g 2.6235 Tare weight, g 2.6607 Tare weight, g 

Dry Residue Weight, g 2.6264 Dry Residue Weight, g 2.6612 Dry Residue Weight, g 

Reweigh, Final, g 2.6264 Reweigh, Final, g 2.6611 Reweigh, Final, g 

MeCl2 Residue, g 0.0029 Water Residue, g 0.0005 Acetone Residue, g 

MeCl2 Volume, mL 225 Water Volume, mL 250 Acetone Volume, mL 

Max. MeCl2 Residue, g 0.0045 Max. Water Residue, g 0.0025 Max. Acetone Residue, 

Company

Analyst

Parameters

# Samples

URS Corp. - RTPARMEPA OTM-286 Runs, Blanks

Client #

Job #

PO #

Report Date

396821750310-96226013.US3/31/2010

EA# 0310-96 Page 15 of 236
Analysis of Condensible Particulate Recovery

Sample ID Number Field Blank Unit 2 Run 1 Unit 2 Run 2 Unit 2 Run 3

Organic

Beaker Number 3526 3523 3524 3525

Initial Acetone Volume, mL 21 54 66 16

Initial MeCl2 Volume, mL 17 127 124 80

Lab MeCl2 Volume, mL 165 Dates 165 Dates 165 Dates 165 Dates

Final Weight, g 2.6551 3/30/10 2.6698 3/30/10 2.6620 3/30/10 2.6564 3/30/1

Reweigh, Final, g 2.6550 3/31/10 2.6697 3/31/10 2.6618 3/31/10 2.6564 3/31/1

Beaker Tare, g 2.6468 3/24/10 2.6559 3/24/10 2.6492 3/24/10 2.6455 3/26/1

Net Organic Catch, mg 8.3 13.9 12.7 10.9

Inorganic

Beaker Number 3565 Dates 3562 Dates 3563 Dates 3564 Dates

Final Weight, g 2.6707 3/30/10 2.8206 3/30/10 2.8386 3/30/10 2.8928 3/30/1

Reweigh, Final, g 2.6706 3/31/10 2.8206 3/31/10 2.8385 3/31/10 2.8927 3/31/1

Beaker Tare, g 2.6642 3/26/10 2.6614 3/26/10 2.6603 3/26/10 2.6570 3/26/1

H2O FV, mL 86 559 487 525

Resuspended Volume, mL 100 100 100 100

Removed Pre-aliquot, mL 0.5 0.5 0.5 0.5

Pre-aliquot CF 1.01 1.001 1.001 1.001

Removed Post-aliquot, mL 0.5 0.5 0.5 0.5

Post-aliquot CF 1.01 1.01 1.01 1.01

Net Inorganic, mg 6.5 160.2 179.2 237.1

Ammonium Correction, mg 0.1 1.0 2.6 2.8

Corrected Inorganic, mg 6.3 159.2 176.6 234.3

Condensible Particulate Matter, mg 14.6 173.1 189.3 245.2

TB Corrected CPM, mg 171.1 187.3 243.2

-----------------------------------------------------------------Client Blank Analyses------------------------------------------------------------------

Type Blank MeCl Blank Type Blank H2O Blank Type Blank 

Beaker Number 3528 Beaker Number 3567 Beaker Number 

Tare weight, g 2.6319 Tare weight, g 2.6558 Tare weight, g 

Dry Residue Weight, g 2.6393 Dry Residue Weight, g 2.6569 Dry Residue Weight, g 

Reweigh, Final, g 2.6393 Reweigh, Final, g 2.6568 Reweigh, Final, g 

MeCl2 Residue, g 0.0074 Water Residue, g 0.0010 Acetone Residue, g 

MeCl2 Volume, mL 110 Water Volume, mL 106 Acetone Volume, mL 

Max. MeCl2 Residue, g 0.0022 Max. Water Residue, g 0.0011 Max. Acetone Residue, 

---------------------------------------------------------------In-House Blank Analyses------------------------------------------------------------------

Type Blank MeCl Blank Type Blank H2O Blank Type Blank 

Beaker Number 3529 Beaker Number 3568 Beaker Number 

Tare weight, g 2.6235 Tare weight, g 2.6607 Tare weight, g 

Dry Residue Weight, g 2.6264 Dry Residue Weight, g 2.6612 Dry Residue Weight, g 

Reweigh, Final, g 2.6264 Reweigh, Final, g 2.6611 Reweigh, Final, g 

MeCl2 Residue, g 0.0029 Water Residue, g 0.0005 Acetone Residue, g 

MeCl2 Volume, mL 225 Water Volume, mL 250 Acetone Volume, mL 

Max. MeCl2 Residue, g 0.0045 Max. Water Residue, g 0.0025 Max. Acetone Residue, 

Company

Analyst

Parameters

# Samples

URS Corp. - RTPARMEPA OTM-286 Runs, Blanks

Client #

Job #

PO #

Report Date

396821750310-96226013.US3/31/2010

EA# 0310-96 Page 16 of 236
Analysis of Condensible Particulate Recovery

Sample ID Number Field Blank Filter Blank Run 8 Run 9

Organic

Beaker Number 3526 3527

Initial Acetone Volume, mL 21 0 0 0

Initial MeCl2 Volume, mL 17 0 0 0

Lab MeCl2 Volume, mL 165 Dates 165 Dates 165 Dates 165 Dates

Final Weight, g 2.6551 3/30/10 2.6520 3/30/10

Reweigh, Final, g 2.6550 3/31/10 2.6520 3/31/10

Beaker Tare, g 2.6468 3/24/10 2.6492 3/24/10

Net Organic Catch, mg 8.3 2.9 0.0 0.0

Inorganic

Beaker Number 3565 Dates 3566 Dates Dates Dates

Final Weight, g 2.6707 3/30/10 2.6776 3/30/10

Reweigh, Final, g 2.6706 3/31/10 2.6775 3/31/10

Beaker Tare, g 2.6642 3/26/10 2.6673 3/26/10

H2O FV, mL 86 75 0 0

Resuspended Volume, mL 100 100 100.0 100.0

Removed Pre-aliquot, mL 0.5 0.5 0.5 0.5

Pre-aliquot CF 1.01 1.01 0.00 0.00

Removed Post-aliquot, mL 0.5 0.5 0.5 0.5

Post-aliquot CF 1.01 1.01 1.01 1.01

Net Inorganic, mg 6.5 10.3 0.0 0.0

Ammonium Correction, mg 0.1 0.0 0.0 0.0

Corrected Inorganic, mg 6.3 10.3 0.0 0.0

Condensible Particulate Matter, mg 14.6 13.2 0.0 0.0

TB Corrected CPM, mg 11.2 -2.0 -2.0

-----------------------------------------------------------------Client Blank Analyses------------------------------------------------------------------

Type Blank MeCl Blank Type Blank H2O Blank Type Blank 

Beaker Number 3528 Beaker Number 3567 Beaker Number 

Tare weight, g 2.6319 Tare weight, g 2.6558 Tare weight, g 

Dry Residue Weight, g 2.6393 Dry Residue Weight, g 2.6569 Dry Residue Weight, g 

Reweigh, Final, g 2.6393 Reweigh, Final, g 2.6568 Reweigh, Final, g 

MeCl2 Residue, g 0.0074 Water Residue, g 0.0010 Acetone Residue, g 

MeCl2 Volume, mL 110 Water Volume, mL 106 Acetone Volume, mL 

Max. MeCl2 Residue, g 0.0022 Max. Water Residue, g 0.0011 Max. Acetone Residue, 

---------------------------------------------------------------In-House Blank Analyses------------------------------------------------------------------

Type Blank MeCl Blank Type Blank H2O Blank Type Blank 

Beaker Number 3529 Beaker Number 3568 Beaker Number 

Tare weight, g 2.6235 Tare weight, g 2.6607 Tare weight, g 

Dry Residue Weight, g 2.6264 Dry Residue Weight, g 2.6612 Dry Residue Weight, g 

Reweigh, Final, g 2.6264 Reweigh, Final, g 2.6611 Reweigh, Final, g 

MeCl2 Residue, g 0.0029 Water Residue, g 0.0005 Acetone Residue, g 

MeCl2 Volume, mL 225 Water Volume, mL 250 Acetone Volume, mL 

Max. MeCl2 Residue, g 0.0045 Max. Water Residue, g 0.0025 Max. Acetone Residue, 

Company

Analyst

Parameters

# Samples

URS Corp. - RTPARMEPA OTM-286 Runs, Blanks

Client #

Job #

PO #

Report Date

396821750310-96226013.US3/31/2010

EA# 0310-96 Page 17 of 236
MDL 0.09 (mg Ammonium)

MDL 0.26 (mg Sulfate)

Blank titrant amount (Vtb) 0.03 [Set this equal to the In-House Blank Titration Volume and then white out this note]

NH4OH normality 0.1 Lot # Sigma Aldrich 318620

Sample ID.

Volume

Resuspended

(mL)

Titration

Aliquot

Vol (mL)

Aliquot Factor 

(mL rec'd/aliq mL)

Field Blank 100 99.5 0.10 1.01 0.34 0.12

Unit 1 Run 1 100 99.5 1.44 1.01 6.81 2.41

Unit 1 Run 2 100 99.5 1.14 1.01 5.36 1.90

Unit 1 Run 3 100 99.5 1.71 1.01 8.11 2.88

Unit 2 Run 1 100 99.5 0.62 1.01 2.85 1.01

Unit 2 Run 2 100 99.5 1.55 1.01 7.34 2.60

Unit 2 Run 3 100 99.5 1.69 1.01 8.01 2.84

Filter Blank 100 99.5 0.08 ND 1.01 0.26 ND 0.09 ND

Reagent Blank 100 99.5 0.08 ND 1.01 0.26 ND 0.09 ND

SO4 Catch

(mg)

NH4OH

Titration

Vol (mL)

Ammonium

equivalent

(mg)

Company

Analyst

Parameters

# Samples

URS Corp. - RTP

ARM

EPA OTM-28

6 Runs, Blanks

Client #

Job #

PO #

Report Date

39682175

0310-96

226013.US

3/31/2010

EA# 0310-96 Page 18 of 236
Narrative Summary

EA# 0310-96 Page 19 of 236
Enthalpy Analytical Narrative Summary 

Company URS Corp. - RTP Client # 39682175

Analyst KHB Job # 0310-96 

Parameters EPA CTM-033 PO # 226013.US 

# Samples 6 Runs, 6 Blanks Report Date April 8, 2010 

Custody Heather Tarjeft received the samples on 3/18/10 after being relinquished 

by URS Corporation of Research Triangle Park, NC. The samples were 

received at 5.2C and in good condition. The NaOH fractions were 

received at a pH of 12 or greater. Prior to, during, and after analysis, 

the samples were kept under lock with access only to authorized 

personnel by Enthalpy Analytical, Inc. 

Analysis The samples were analyzed for hydrogen cyanide using the analytical 

procedures in EPA Conditional Test Method 033, Sampling and 

Analysis for Hydrogen Cyanide Emissions from Stationary Sources. 

The samples were analyzed following the procedures in Section 11.0, 

Analytical Procedures. 

The DIONEX Model 500, High Performance Liquid Chromatograph 

("Grandmama") was equipped with a DIONEX ED40 Electrochemical 

Detector and a Dionex Ion Pac AS7, 4 x 250 mm column (S/N 012759). 

Calibration The calibration curves are located in the back of this report and 

referenced in the Analysis Method column on the Detailed Results page. 

For each calibration curve used, the first page of the curve contains all 

method specific parameters (i.e., curve type, origin, weight, etc.) used to 

quantify the samples. The calibration curve section also includes a table 

with the Retention Time (RetTime), Level (Lvl), Amount 

(corresponding units), Area, Response Factor (Amt/Area) and the 

analyte Name. The calibration table is used to identify (by retention 

time) and quantify each target compound. 

Chromatographic 

Conditions 

The acquisition method 1000.M is included in the Calibration Curve 

Chromatograms section of this report. 

QC Notes As required in Section 9.0, Quality Control, client-provided field blank, 

reagent blank and field spike were analyzed. In the laboratory the 

following QC samples were analyzed: method blank, Matrix 

Spike/Matrix Spike Duplicate, and a replicate analysis. All method 

required acceptance criteria were met. 

EA# 0310-96 Page 20 of 236
Enthalpy Analytical Narrative Summary 

(continued) 

QC Notes 

(continued) 

A matrix spike and matrix spike duplicate (MS and MSD) were 

performed on the sample U2-NaOH-R1 and exhibited recovery values 

of 106% and 107%. 

A Laboratory Duplicate (LD) analysis was performed on the sample 

U2-NaOH-R1. The result differed from the initial result by 9%. 

Prior to sample collection the laboratory prepared aqueous spikes, each 

of which contained 1,088 μg of hydrogen cyanide. Five aqueous spikes 

were sent to the client and two were retained by the laboratory for use as 

Laboratory Control Samples (LCSs). 

The LCSs were then analyzed in the same manner as the samples and 

both exhibited recovery values of 107%. 

The volumes as measured by the laboratory were used for reporting 

purposes. 

All sample preparation and analytical holding times specified in the 

method were met. In Section 11.1.2 the specified analytical holding time 

is 30 days from collection. 

Reporting Notes The results presented in this report are representative of the samples as 

provided to the laboratory. 

Enthalpy Analytical, Inc. is accredited to perform this method for 

compliance purposes by the National Environmental Laboratory 

Accreditation Conference (NELAC) through the Louisiana 

Environmental Laboratory Accreditation Program (LELAP), certificate 

number 04010. 

EA# 0310-96 Page 21 of 236
Enthalpy Analytical Narrative Summary 

Company URS Corp. - RTP Client # 39682175 

Analyst EO Job # 0310-96 

Parameters EPA Method 26A PO # 226013.US 

# Samples 6 Runs, 2 Blanks Report Date March 31, 2010 

Custody Heather Tarjeft received the samples on 3/19/10 after being relinquished 

by URS Corporation of Research Triangle Park, NC. The samples were 

received at 17.2C and in good condition. Prior to, during, and after 

analysis, the samples were kept under lock with access only to 

authorized personnel by Enthalpy Analytical, Inc. 

Analysis The samples were analyzed for hydrogen chloride (HCl) and hydrogen 

fluoride (HF) using the analytical procedures in EPA Method 26A, 

Determination of Hydrogen Halide and Halogen Emissions from 

Stationary Sources Isokinetic Method (40 CFR Part 60, Appendix A). 

The samples were analyzed following the procedures in Section 11.0, 

Analytical Procedures. All samples and standards are prepared, stored, 

and analyzed using high-density polyethylene containers. 

Samples for Unit 1 were received in two containers per run. 

Proportional aliquots were taken and combined for a single analysis. 

The Metrohm 861 Compact IC ("Smithers" S/N 1861002007189) was 

equipped with a Metrohm 861 Conductivity Detector and a Metrosep A 

Supp 5 - 110/4.0mm column (S/N # 905298). 

Calibration The calibration curve is located in the back of this report and referenced 

in the Analysis Method column on the Detailed Results page. 

The first page of the curve contains all method specific parameters (i.e., 

curve type, origin, weight, etc.) used to quantify the samples. The 

calibration curve section also includes a table with the Retention Time 

(RetTime), Level (Lvl), Amount (corresponding units), Area, Response 

Factor (Amt/Area) and the analyte Name. The calibration table is used 

to identify (by retention time) and quantify each target compound. 

Chromatographic 

Conditions 

The acquisition method Metrohm.M is included in the Calibration 

Curve Chromatograms section of this report. 

QC Notes As required in Section 7.2.2, Absorbing Solution Blanks, clientprovided field and reagent blanks were analyzed. Additionally, a 

quality control check sample was analyzed at the same time as the 

blanks and samples. All method required acceptance criteria were met. 

EA# 0310-96 Page 22 of 236
Enthalpy Analytical Narrative Summary 

(continued) 

QC Notes 

(continued) 

A matrix spike and a matrix spike duplicate sample were performed on 

the sample Unit 1 Run 1. The matrix spike samples exhibited recovery 

values of 94.9% and 95.1% for HCl and 110% and 110% for HF. 

The Laboratory Control Samples (LCS) prepared and analyzed along 

with the samples exhibited recovery values of 105% and 106% for HF 

and 94.5% and 95.0% for HCL. 

All sample preparation and analytical holding times specified in the 

method were met. Section 13.2, Sample Stability, specifies an analytical 

holding time of four weeks. 

Reporting Notes The H2SO4 matrix samples were analyzed for Cl-

 and F- but are reported 

as HCl and HF, respectively. The results were converted using an acid 

conversion factor of 1.028 for HCl and 1.053 for HF. 

The results presented in this report are representative of the samples as 

provided to the laboratory. 

Enthalpy Analytical, Inc. is accredited to perform this method for 

compliance purposes by the National Environmental Laboratory 

Accreditation Conference (NELAC) through the Louisiana 

Environmental Laboratory Accreditation Program (LELAP), certificate 

number 04010. 

EA# 0310-96 Page 23 of 236
Enthalpy Analytical Narrative Summary 

Company URS Corp. - RTP Client # 39682175

Analyst ARM Job # 0310-96 

Parameters EPA OTM-028 PO # 226013.US 

# Samples 6 Runs, Blanks Report Date March 31, 2010 

Custody Heather Tarjeft received the samples on 3/19/10 after being relinquished 

by URS Corporation of of Research Triangle Park, NC. The samples 

were received at 19.1C and in good condition. Prior to, during, and 

after analysis, the samples were kept under lock with access only to 

authorized personnel by Enthalpy Analytical, Inc. 

Analysis The samples were analyzed for Particulate Matter using the analytical 

procedures in EPA Other Test Method (OTM) 28, Dry Inpinger Method 

for Determining Condensable Particulate Emissions from Stationary 

Sources. 

All samples were weighed on a Sartorius Model ME 5-F (SN 23104965) 

certified by Precision Weighing, Inc. through the end of October 2010, 

(NIST Test Weight # 1481174). 

QC Notes A field blank, filter blank, acetone blank, water blank, and methylene 

chloride blank were received and analyzed with these samples. 

The method specifies blank corrections are accomplished by subtracting 

the particulate mass determined in the ‘Field Train Blank’ or 2 mg 

(whichever is less) from the sample weight. 

The inorganic results for the samples were corrected for the ammonium 

ions used to precipitate the sulfate, per the formula in the Method 

(Section 12.2.1). 

When the pH of the samples was measured to be 7.0 or greater with the 

pH meter, no titrant was added. 

All sample preparation and analytical holding times specified in the 

method were met. 

Reporting Notes Enthalpy Analytical, Inc. considers gravimetric analyses for OTM-028 

±0.5 mg. Therefore, negative catch weights between 0 and –0.5 mg are 

set to zero and no investigation is undertaken. Negative catch weights < 

-0.5 mg are investigated. None of the catch results for this data set were 

< -0.5 mg. 

The results presented in this report are representative of the samples as 

provided to the laboratory. 

EA# 0310-96 Page 24 of 236
General Reporting Notes 

The following are general reporting notes that are applicable to all Enthalpy Analytical, Inc. data 

reports, unless specifically noted otherwise.

 The acronym MDL represents the Minimum Detection Limit. Below this value the laboratory cannot 

determine the presence of the analyte of interest reliably. 

 The acronym LOQ represents the Limit of Quantification. Below this value the laboratory cannot 

quantitate the analyte of interest within the criteria of the method. 

 The acronym ND following a value indicates a non-detect or analytical result below the MDL. 

 The letter J following a value indicates an analytical result between the MDL and the LOQ. A J flag 

indicates that the laboratory can positively identify the analyte of interest as present, but the value 

should be considered an estimate. 

 The letter E following a value indicates an analytical result exceeding 100% of the highest calibration 

point. The associated value should be considered as an estimate. 

 The acronym DF represents Dilution Factor. This number represents dilution of the sample during the 

preparation and/or analysis process. The analytical result taken from a laboratory instrument is 

multiplied by the DF to determine the final undiluted sample results. 

 The addition of MS to the Sample ID represents a Matrix Spike. An aliquot of an actual sample is 

spiked with a known amount of analyte so that a percent recovery value can be determined. This shows 

what effect the sample matrix may have on the target analyte, i.e. whether or not anything in the sample 

matrix interferes with the analysis of the analyte(s). 

 The addition of MSD to the Sample ID represents a Matrix Spike Duplicate. Prepared in the same 

manner as an MS, the use of duplicate matrix spikes allows further confirmation of laboratory quality 

by showing the consistency of results gained by performing the same steps multiple times. 

 The addition of LD to the Sample ID represents a Laboratory Duplicate. The analyst prepares an 

additional aliquot of sample for testing and the results of the duplicate analysis are compared to the 

initial result. The result should have a difference value of within 10% of the initial result (if the results 

of the original analysis are greater than the LOQ). 

 The addition of AD to the Sample ID represents an Alternate Dilution. The analyst prepares an 

additional aliquot at a different dilution factor (usually double the initial factor). This analysis helps 

confirm that no additional compound is present and coeluting or sharing absorbance with the analyte of 

interest, as they would have a different response/absorbance than the analyte of interest. 

 The Sample ID LCS represents a Laboratory Control Sample. Clean matrix, similar to the client sample 

matrix, prepared and analyzed by the laboratory using the same reagents, spiking standards and 

procedures used for the client samples. The LCS is used to assess the control of the laboratory’s 

analytical system. Whenever spikes are prepared for our client projects, two extra spikes are prepared. 

The extras (randomly chosen) are labeled with the associated project number and kept in-house at the 

appropriate temperature conditions. When the project samples are received for analysis, the LCSs are 

analyzed to confirm that the analyte could be recovered from the media, separate from the samples 

which were used on the project and which may have been affected by source matrix, sample collection 

and/or sample transport. 

EA# 0310-96 Page 25 of 236
General Reporting Notes 

(continued) 

 Significant Figures: Where the reported value is much greater than unity (1.00) in the units expressed, 

the number is rounded to a whole number of units, rather than to 3 significant figures. For example, a 

value of 10,456.45 ug catch is rounded to 10,456 ug. There are five significant digits displayed, but no 

confidence should be placed on more than two significant digits. 

 Manual Integration: The data systems used for processing will flag manually integrated peaks with 

an “M”. There are several reasons a peak may be manually integrated. These reasons will be identified 

by the following two letter designations. The peak was not integrated by the software “NI”, the peak 

was integrated incorrectly by the software “II” or the wrong peak was integrated by the software 

“WP”. These codes will accompany the analyst’s manual integration stamp placed next to the 

compound name. 

EA# 0310-96 Page 26 of 236
Sample Custody

EA# 0310-96 Page 27 of 236
EA# 0310-96 Page 28 of 236
EA# 0310-96 Page 29 of 236
EA# 0310-96 Page 30 of 236
EA# 0310-96 Page 31 of 236
EA# 0310-96 Page 32 of 236
---------------------------

~ 

Sample 10 Code DatelTime Sample Matrix 0 :.2

:::c :E CI) Comments 

AGY-U1-27/28-IMR-1 Methylene Chloride 3/5/2010 X Unit 1 Run 1 

AGY-U1-27/28-IMR-2 Methylene Chloride 3/5/2010 X Unit 1 Run 2 

-27128-IMR-3 Methylene Chloride 3/6/2010 X Unit 1 Run 3 

Methylene Chloride 3/1312010 X Unit 2 Run 1 

Methylene Chloride 3113/2010 X Unit 2 Run 2 

MR-3 Methylene Chloride 3/14/2010 X Unit 2 Run 3 

Methylene Chloride 3/812010 X Field Blank 

Methylene Chloride 3/8/2010 X t~; Reagent Blank 

Water 3/8/2010 X 

P6~..~ ~ 3tcnho 

Remarks: Technical Contact is Jerry Workman (919) 461-1289 

Relinquished by: 

Received by: 

Relinquished by: 

Received by: 

EA# 0310-96 Page 33 of 236
EA# 0310-96 Page 34 of 236
EA# 0310-96 Page 35 of 236
EA# 0310-96 Page 36 of 236
EA# 0310-96 Page 37 of 236
S; '0 0..

Sample Matrix f! '0 :2 

G ::I: CJ) Comments

Acetone Unit 1 Run 1

Acetone Unit 1 Run 2

Acetone Unit 1 Run 3

Acetone Unit 1 Run 1

Acetone Unit 1 Run 2

Acetone Unit 1 Run 3

Acetone 

Acetone 

Acetone 

10 

EA# 0310-96 Page 38 of 236
EA# 0310-96 Page 39 of 236
EA# 0310-96 Page 40 of 236
Sample 

Chromatograms

EA# 0310-96 Page 41 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\036-4901.D)

 Area: 47.563

 1.474

 1.757

 8.358 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.358 MM 47.56303 0.00000 0.00000 Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Negative results set to zero (cal. curve intercept), (Hydrogen Cyanide)

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\036-4901.D

Sample Name: U1-Pb-1*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 49

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 2:47:50 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:00:33 AM KHB Page 1 of 1

EA# 0310-96 Page 42 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\036-4902.D)

 Area: 48.8266

 1.473

 1.753

 8.312 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.312 MM 48.82658 0.00000 0.00000 Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Negative results set to zero (cal. curve intercept), (Hydrogen Cyanide)

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\036-4902.D

Sample Name: U1-Pb-1*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 49

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 3:03:06 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:00:52 AM KHB Page 1 of 1

EA# 0310-96 Page 43 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\037-5001.D) 1.480 1.619 1.731 2.182 8.220 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.220 BB 1370.48254 9.70414e-4 1.32993 Hydrogen Cyanide 

Totals : 1.32993

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\037-5001.D

Sample Name: U1-NaOH-1*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 50

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 3:18:23 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:01:00 AM KHB Page 1 of 1

EA# 0310-96 Page 44 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\037-5002.D) 1.479 1.734 2.188 8.253 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.253 BB 1355.80103 9.69881e-4 1.31497 Hydrogen Cyanide 

Totals : 1.31497

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\037-5002.D

Sample Name: U1-NaOH-1*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 50

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 3:33:39 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:01:11 AM KHB Page 1 of 1

EA# 0310-96 Page 45 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\038-5101.D)

 Area: 63.1595

 1.477

 1.688 1.765

 8.371 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.371 MM 63.15947 0.00000 0.00000 Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Negative results set to zero (cal. curve intercept), (Hydrogen Cyanide)

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\038-5101.D

Sample Name: U1-Pb-2*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 51

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 3:48:56 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:01:26 AM KHB Page 1 of 1

EA# 0310-96 Page 46 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\038-5102.D)

 Area: 50.9545

 1.476

 1.691 1.764

 8.388 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.388 MM 50.95449 0.00000 0.00000 Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Negative results set to zero (cal. curve intercept), (Hydrogen Cyanide)

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\038-5102.D

Sample Name: U1-Pb-2*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 51

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 4:04:12 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:01:40 AM KHB Page 1 of 1

EA# 0310-96 Page 47 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\039-5201.D) 1.478 1.622 1.739 2.178 8.256 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.256 BB 936.07892 9.47596e-4 8.87025e-1 Hydrogen Cyanide 

Totals : 8.87025e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\039-5201.D

Sample Name: U1-NaOH-2*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 52

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 4:19:30 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:01:48 AM KHB Page 1 of 1

EA# 0310-96 Page 48 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\039-5202.D) 1.745 2.185 8.300 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.300 BB 956.22791 9.49113e-4 9.07568e-1 Hydrogen Cyanide 

Totals : 9.07568e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\039-5202.D

Sample Name: U1-NaOH-2*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 52

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 4:34:46 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:02:01 AM KHB Page 1 of 1

EA# 0310-96 Page 49 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\040-5301.D)

 Area: 60.0793

 1.474

 1.765

 8.367 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.367 MM 60.07925 0.00000 0.00000 Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Negative results set to zero (cal. curve intercept), (Hydrogen Cyanide)

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\040-5301.D

Sample Name: U1-Pb-3*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 53

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 4:50:02 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:02:20 AM KHB Page 1 of 1

EA# 0310-96 Page 50 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\040-5302.D)

 Area: 58.2781

 1.476

 1.771

 8.383 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.383 MM 58.27813 0.00000 0.00000 Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Negative results set to zero (cal. curve intercept), (Hydrogen Cyanide)

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\040-5302.D

Sample Name: U1-Pb-3*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 53

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 5:05:18 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:02:33 AM KHB Page 1 of 1

EA# 0310-96 Page 51 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\041-5601.D) 1.753 2.183 8.312 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.312 BB 1019.54974 9.53490e-4 9.72130e-1 Hydrogen Cyanide 

Totals : 9.72130e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\041-5601.D

Sample Name: U1-NaOH-3*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 56

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 6:21:41 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:02:42 AM KHB Page 1 of 1

EA# 0310-96 Page 52 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\041-5602.D) 1.754 2.186 8.310 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.310 BB 1028.17786 9.54044e-4 9.80927e-1 Hydrogen Cyanide 

Totals : 9.80927e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\041-5602.D

Sample Name: U1-NaOH-3*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 56

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 6:36:57 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:02:50 AM KHB Page 1 of 1

EA# 0310-96 Page 53 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\042-5701.D)

 Area: 70.7309

 1.481

 1.767

 8.374 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.374 MM 70.73090 6.68875e-5 4.73102e-3 Hydrogen Cyanide 

Totals : 4.73102e-3

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\042-5701.D

Sample Name: U2-Pb-1*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 57

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 6:52:15 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:03:06 AM KHB Page 1 of 1

EA# 0310-96 Page 54 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\042-5702.D)

 Area: 70.0303

 1.476

 1.767

 8.341 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.341 MM 70.03030 5.73567e-5 4.01670e-3 Hydrogen Cyanide 

Totals : 4.01670e-3

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\042-5702.D

Sample Name: U2-Pb-1*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 57

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 7:07:30 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:03:18 AM KHB Page 1 of 1

EA# 0310-96 Page 55 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\043-5801.D) 1.731 2.157 8.229 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.229 BB 1391.50391 9.71156e-4 1.35137 Hydrogen Cyanide 

Totals : 1.35137

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\043-5801.D

Sample Name: U2-NaOH-1*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 58

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 7:22:47 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:03:29 AM KHB Page 1 of 1

EA# 0310-96 Page 56 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\043-5802.D) 1.734 2.155 8.203 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.203 BB 1427.31409 9.72371e-4 1.38788 Hydrogen Cyanide 

Totals : 1.38788

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\043-5802.D

Sample Name: U2-NaOH-1*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 58

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 7:38:04 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:03:36 AM KHB Page 1 of 1

EA# 0310-96 Page 57 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\044-5901.D)

 Area: 47.6002

 1.481 1.607 1.764

 8.289 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.289 MM 47.60016 0.00000 0.00000 Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Negative results set to zero (cal. curve intercept), (Hydrogen Cyanide)

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\044-5901.D

Sample Name: U2-Pb-2*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 59

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 7:53:21 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:03:58 AM KHB Page 1 of 1

EA# 0310-96 Page 58 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\044-5902.D)

 Area: 47.9002

 1.478

 1.767

 8.262 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.262 MM 47.90025 0.00000 0.00000 Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Negative results set to zero (cal. curve intercept), (Hydrogen Cyanide)

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\044-5902.D

Sample Name: U2-Pb-2*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 59

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 8:08:36 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:04:11 AM KHB Page 1 of 1

EA# 0310-96 Page 59 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\045-6001.D) 1.731 2.169 8.155 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.155 BB 1189.37158 9.62926e-4 1.14528 Hydrogen Cyanide 

Totals : 1.14528

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\045-6001.D

Sample Name: U2-NaOH-2*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 60

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 8:23:53 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:04:19 AM KHB Page 1 of 1

EA# 0310-96 Page 60 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\045-6002.D) 1.734 2.170 8.136 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.136 BB 1201.94104 9.63519e-4 1.15809 Hydrogen Cyanide 

Totals : 1.15809

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\045-6002.D

Sample Name: U2-NaOH-2*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 60

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 8:39:09 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:04:25 AM KHB Page 1 of 1

EA# 0310-96 Page 61 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\046-6301.D)

 Area: 11.1265

 1.472

 1.764

 8.173 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.173 MM 11.12650 0.00000 0.00000 Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Negative results set to zero (cal. curve intercept), (Hydrogen Cyanide)

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\046-6301.D

Sample Name: U2-Pb-3*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 63

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 9:55:32 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:04:47 AM KHB Page 1 of 1

EA# 0310-96 Page 62 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\046-6302.D)

 Area: 12.0705

 1.476

 1.767

 8.181 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.181 MM 12.07053 0.00000 0.00000 Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Negative results set to zero (cal. curve intercept), (Hydrogen Cyanide)

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\046-6302.D

Sample Name: U2-Pb-3*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 63

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 10:10:49 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:05:02 AM KHB Page 1 of 1

EA# 0310-96 Page 63 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\047-6401.D) 1.727 2.153 8.019 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.019 BB 1203.38965 9.63586e-4 1.15957 Hydrogen Cyanide 

Totals : 1.15957

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\047-6401.D

Sample Name: U2-NaOH-3*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 64

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 10:26:05 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:05:11 AM KHB Page 1 of 1

EA# 0310-96 Page 64 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\047-6402.D) 1.734 2.156 8.034 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.034 BB 1230.87097 9.64837e-4 1.18759 Hydrogen Cyanide 

Totals : 1.18759

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\047-6402.D

Sample Name: U2-NaOH-3*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 64

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 10:41:21 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:05:18 AM KHB Page 1 of 1

EA# 0310-96 Page 65 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\062-2301.D) 1.731 2.132 8.186 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.186 BB 862.47913 1.72158e-3 1.48483 Hydrogen Cyanide 

Totals : 1.48483

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\062-2301.D

Sample Name: LD/U2-NaOH-1*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 23

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/3/2010 12:58:59 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 Sample Info : Lab Duplicate

 

 =====================================================================

Instrument 3 4/6/2010 8:41:27 AM KHB Page 1 of 1

EA# 0310-96 Page 66 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\062-2302.D) 1.734 2.127 8.224 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.224 BB 872.12213 1.72236e-3 1.50211 Hydrogen Cyanide 

Totals : 1.50211

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\062-2302.D

Sample Name: LD/U2-NaOH-1*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 23

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/3/2010 1:14:15 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 Sample Info : Lab Duplicate

 

 =====================================================================

Instrument 3 4/6/2010 8:41:32 AM KHB Page 1 of 1

EA# 0310-96 Page 67 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\050-6701.D) 1.476 1.747 8.005 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.005 BB 893.33582 9.44152e-4 8.43445e-1 Hydrogen Cyanide 

Totals : 8.43445e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\050-6701.D

Sample Name: NaOH FS*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 67

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 11:57:45 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:05:54 AM KHB Page 1 of 1

EA# 0310-96 Page 68 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\050-6702.D) 1.481 1.750 8.021 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.021 BB 878.99542 9.42921e-4 8.28823e-1 Hydrogen Cyanide 

Totals : 8.28823e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\050-6702.D

Sample Name: NaOH FS*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 67

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 12:13:01 AM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 10:06:00 AM KHB Page 1 of 1

EA# 0310-96 Page 69 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\048-6501.D) 1.471 1.645 1.745 2.243

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.255 - - - Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\048-6501.D

Sample Name: NaOH FB*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 65

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 10:56:39 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 Sample Info : Sample Blank

 

 =====================================================================

Instrument 3 4/3/2010 10:05:28 AM KHB Page 1 of 2

EA# 0310-96 Page 70 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\048-6502.D) 1.479 1.753 2.252

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.255 - - - Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\048-6502.D

Sample Name: NaOH FB*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 65

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 11:11:54 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 Sample Info : Sample Blank

 

 =====================================================================

Instrument 3 4/3/2010 10:05:34 AM KHB Page 1 of 2

EA# 0310-96 Page 71 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\049-6601.D) 1.477 1.756

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.255 - - - Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\049-6601.D

Sample Name: NaOH RB*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 66

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 11:27:12 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 Sample Info : Sample Blank

 

 =====================================================================

Instrument 3 4/3/2010 10:05:40 AM KHB Page 1 of 2

EA# 0310-96 Page 72 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\049-6602.D) 1.480 1.757 2.256

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.255 - - - Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\049-6602.D

Sample Name: NaOH RB*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 66

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 11:42:28 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 Sample Info : Sample Blank

 

 =====================================================================

Instrument 3 4/3/2010 10:05:47 AM KHB Page 1 of 2

EA# 0310-96 Page 73 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\051-0801.D) 1.608 1.780

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.267 - - - Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\051-0801.D

Sample Name: NaOH FB*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 8

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 8:15:44 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 Sample Info : Sample Blank

 

 =====================================================================

Instrument 3 4/6/2010 8:39:12 AM KHB Page 1 of 2

EA# 0310-96 Page 74 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\051-0802.D) 1.458 1.604 1.779

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.267 - - - Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\051-0802.D

Sample Name: NaOH FB*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 8

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 8:30:59 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 Sample Info : Sample Blank

 

 =====================================================================

Instrument 3 4/6/2010 8:39:21 AM KHB Page 1 of 2

EA# 0310-96 Page 75 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\052-0901.D) 1.613 1.790

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.267 - - - Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\052-0901.D

Sample Name: NaOH RB*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 9

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 8:46:17 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 Sample Info : Sample Blank

 

 =====================================================================

Instrument 3 4/6/2010 8:39:34 AM KHB Page 1 of 2

EA# 0310-96 Page 76 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\052-0902.D) 1.468 1.617 1.789

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.267 - - - Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\052-0902.D

Sample Name: NaOH RB*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 9

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 9:01:33 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 Sample Info : Sample Blank

 

 =====================================================================

Instrument 3 4/6/2010 8:39:40 AM KHB Page 1 of 2

EA# 0310-96 Page 77 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\053-1001.D) 1.612 1.660 1.794

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.267 - - - Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\053-1001.D

Sample Name: NaOH RB2*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 10

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 9:16:50 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 Sample Info : Sample Blank

 

 =====================================================================

Instrument 3 4/6/2010 8:39:57 AM KHB Page 1 of 2

EA# 0310-96 Page 78 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\053-1002.D) 1.604 1.655 1.795

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.267 - - - Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\053-1002.D

Sample Name: NaOH RB2*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 10

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 9:32:06 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 Sample Info : Sample Blank

 

 =====================================================================

Instrument 3 4/6/2010 8:40:06 AM KHB Page 1 of 2

EA# 0310-96 Page 79 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\054-1101.D) 1.460 1.653 1.732

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.267 - - - Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\054-1101.D

Sample Name: H2O RB*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 11

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 9:47:23 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 Sample Info : Sample Blank

 

 =====================================================================

Instrument 3 4/6/2010 8:40:18 AM KHB Page 1 of 2

EA# 0310-96 Page 80 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\054-1102.D) 1.465 1.665 1.735

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.267 - - - Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\054-1102.D

Sample Name: H2O RB*5 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 11

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 10:02:39 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 Sample Info : Sample Blank

 

 =====================================================================

Instrument 3 4/6/2010 8:40:29 AM KHB Page 1 of 2

EA# 0310-96 Page 81 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\007-0801.D)

 Area: 33.8087

 1.472

 1.670 1.741

 8.357 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.357 MM 33.80872 0.00000 0.00000 Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Negative results set to zero (cal. curve intercept), (Hydrogen Cyanide)

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\007-0801.D

Sample Name: 0.1N NaOH - RB

 =====================================================================

 Acq. Operator : KHB Seq. Line : 8

 Acq. Instrument : Grandmama Location : -

 Injection Date : 3/31/2010 5:54:58 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/6/2010 9:14:09 AM KHB Page 1 of 1

EA# 0310-96 Page 82 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\007-0802.D)

 Area: 31.4207

 1.475

 1.668 1.738

 8.358 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.358 MM 31.42074 0.00000 0.00000 Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Negative results set to zero (cal. curve intercept), (Hydrogen Cyanide)

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\007-0802.D

Sample Name: 0.1N NaOH - RB

 =====================================================================

 Acq. Operator : KHB Seq. Line : 8

 Acq. Instrument : Grandmama Location : -

 Injection Date : 3/31/2010 6:10:14 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/6/2010 9:14:23 AM KHB Page 1 of 1

EA# 0310-96 Page 83 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\007-0701.D) 1.649 1.724

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.267 - - - Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\007-0701.D

Sample Name: 0.1N NaOH - RB

 =====================================================================

 Acq. Operator : KHB Seq. Line : 7

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 7:45:11 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:27:27 AM KHB Page 1 of 2

EA# 0310-96 Page 84 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\007-0702.D) 1.668 1.737

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.267 - - - Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\007-0702.D

Sample Name: 0.1N NaOH - RB

 =====================================================================

 Acq. Operator : KHB Seq. Line : 7

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 8:00:27 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:27:35 AM KHB Page 1 of 2

EA# 0310-96 Page 85 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\007-0801.D) 1.696 1.769 2.270 8.472 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 08, 2010 4:21:55 PM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.472 BB 148.58122 0.00000 0.00000 Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Negative results set to zero (cal. curve intercept), (Hydrogen Cyanide)

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\007-0801.D

Sample Name: 0.1N NaOH - RB

 =====================================================================

 Acq. Operator : KHB Seq. Line : 8

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/8/2010 1:25:35 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 4/8/2010 9:49:36 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

 Last changed : 4/8/2010 4:21:58 PM by KHB

 =====================================================================

Instrument 3 4/8/2010 4:36:34 PM KHB Page 1 of 1

EA# 0310-96 Page 86 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\007-0802.D) 1.687 1.766 2.266 8.456 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 08, 2010 4:21:55 PM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.456 BB 150.31404 0.00000 0.00000 Hydrogen Cyanide 

Totals : 0.00000

1 Warnings or Errors :

Warning : Negative results set to zero (cal. curve intercept), (Hydrogen Cyanide)

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\007-0802.D

Sample Name: 0.1N NaOH - RB

 =====================================================================

 Acq. Operator : KHB Seq. Line : 8

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/8/2010 1:40:51 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 4/8/2010 9:49:36 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

 Last changed : 4/8/2010 4:21:58 PM by KHB

 =====================================================================

Instrument 3 4/8/2010 4:36:41 PM KHB Page 1 of 1

EA# 0310-96 Page 87 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\015-1101.D)

 Area: 1516.07

 1.758

 2.187

 8.388 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 08, 2010 4:21:55 PM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.388 MM 1516.06641 7.82306e-4 1.18603 Hydrogen Cyanide 

Totals : 1.18603

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\015-1101.D

Sample Name: MS*2/U2-NaOH-1 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 11

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/8/2010 2:57:14 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 4/8/2010 9:49:36 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

 Last changed : 4/8/2010 4:21:58 PM by KHB

 Sample Info : Matrix Spike

 

 =====================================================================

Instrument 3 4/8/2010 4:56:12 PM KHB Page 1 of 1

EA# 0310-96 Page 88 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\015-1102.D)

 Area: 1506.84

 1.758

 2.191

 8.387 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 08, 2010 4:21:55 PM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.387 MM 1506.84326 7.81755e-4 1.17798 Hydrogen Cyanide 

Totals : 1.17798

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\015-1102.D

Sample Name: MS*2/U2-NaOH-1 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 11

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/8/2010 3:12:29 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 4/8/2010 9:49:36 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

 Last changed : 4/8/2010 4:21:58 PM by KHB

 Sample Info : Matrix Spike

 

 =====================================================================

Instrument 3 4/8/2010 4:57:57 PM KHB Page 1 of 1

EA# 0310-96 Page 89 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\016-1201.D)

 Area: 1502.79

 1.759

 2.187

 8.382 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 08, 2010 4:21:55 PM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.382 MM 1502.78699 7.81510e-4 1.17444 Hydrogen Cyanide 

Totals : 1.17444

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\016-1201.D

Sample Name: MSD*2/U2-NaOH-1 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 12

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/8/2010 3:27:47 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 4/8/2010 9:49:36 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

 Last changed : 4/8/2010 4:21:58 PM by KHB

 Sample Info : Matrix Spike Duplicate

 

 =====================================================================

Instrument 3 4/8/2010 4:43:04 PM KHB Page 1 of 1

EA# 0310-96 Page 90 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\016-1202.D)

 Area: 1511.12

 1.760

 2.191

 8.386 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 08, 2010 4:21:55 PM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.386 MM 1511.12451 7.82011e-4 1.18172 Hydrogen Cyanide 

Totals : 1.18172

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\016-1202.D

Sample Name: MSD*2/U2-NaOH-1 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 12

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/8/2010 3:43:09 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 4/8/2010 9:49:36 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

 Last changed : 4/8/2010 4:21:58 PM by KHB

 Sample Info : Matrix Spike Duplicate

 

 =====================================================================

Instrument 3 4/8/2010 4:43:24 PM KHB Page 1 of 1

EA# 0310-96 Page 91 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\055-1201.D) 1.734 8.002 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.002 BB 680.45349 1.70276e-3 1.15865 Hydrogen Cyanide 

Totals : 1.15865

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\055-1201.D

Sample Name: LCS #1*100 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 12

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 10:17:56 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 Sample Info : Lab Control Sample

 

 =====================================================================

Instrument 3 4/6/2010 8:40:37 AM KHB Page 1 of 1

EA# 0310-96 Page 92 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\055-1202.D) 1.466 1.667 1.740 8.021 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.021 BB 685.77051 1.70345e-3 1.16817 Hydrogen Cyanide 

Totals : 1.16817

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\055-1202.D

Sample Name: LCS #1*100 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 12

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 10:33:12 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 Sample Info : Lab Control Sample

 

 =====================================================================

Instrument 3 4/6/2010 8:40:43 AM KHB Page 1 of 1

EA# 0310-96 Page 93 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\056-1501.D) 1.433 1.663 1.733 7.970 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 7.970 BB 673.66669 1.70186e-3 1.14649 Hydrogen Cyanide 

Totals : 1.14649

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\056-1501.D

Sample Name: LCS #2*100 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 15

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 11:49:41 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 Sample Info : Lab Control Sample

 

 =====================================================================

Instrument 3 4/6/2010 8:40:53 AM KHB Page 1 of 1

EA# 0310-96 Page 94 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\056-1502.D) 1.465 1.667 1.742 7.980 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 7.980 BB 697.71216 1.70496e-3 1.18957 Hydrogen Cyanide 

Totals : 1.18957

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\056-1502.D

Sample Name: LCS #2*100 0310-96

 =====================================================================

 Acq. Operator : KHB Seq. Line : 15

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/3/2010 12:04:57 AM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 Sample Info : Lab Control Sample

 

 =====================================================================

Instrument 3 4/6/2010 8:41:01 AM KHB Page 1 of 1

EA# 0310-96 Page 95 of 236
Calibration 

Curve Chromatograms

EA# 0310-96 Page 96 of 236
=====================================================================

 Calibration Table 

=====================================================================

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Calculate : External Standard

Based on : Peak Area

Rel. Reference Window : 10.000 %

Abs. Reference Window : 0.300 min

Rel. Non-ref. Window : 10.000 %

Abs. Non-ref. Window : 0.300 min

Use Multiplier & Dilution Factor with ISTDs

Uncalibrated Peaks : not reported

Partial Calibration : Yes, identified peaks are recalibrated

Correct All Ret. Times: No, only for identified peaks

Curve Type : Linear

Origin : Ignored

Weight : Linear (Amnt)

Recalibration Settings: 

Average Response : Average all calibrations

Average Retention Time: Floating Average New 75%

Calibration Report Options :

 Printout of recalibrations within a sequence:

 Calibration Table after Recalibration

 Normal Report after Recalibration

 If the sequence is done with bracketing:

 Results of first cycle (ending previous bracket)

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Lvl Amount Area Amt/Area Ref Grp Name 

 [min] Sig [ug/mL] 

-------|--|--|----------|----------|----------|---|--|---------------

 8.255 1 1 1.03500e-1 158.68324 6.52243e-4 Hydrogen Cyanide 

 2 5.07300e-1 599.87674 8.45674e-4 

 3 9.90500e-1 1096.56512 9.03275e-4 

 4 1.54100 1557.83539 9.89193e-4 

 5 2.08000 2039.49207 1.01986e-3 

=====================================================================

 Peak Sum Table 

=====================================================================

***No Entries in table***

=====================================================================

Method H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

Instrument 3 4/3/2010 9:40:41 AM KHB Page 1 of 2

EA# 0310-96 Page 97 of 236
=====================================================================

 Calibration Curves

=====================================================================

Amount[ug/mL]

0 1 2

Area

0

250

500

750

1000

1250

1500

1750

2000

1

2

3

4

5

Hydrogen Cyanide at exp. RT: 8.255

ADC1 A, ADC1 CHANNEL A

Correlation: 0.99859

Residual Std. Dev.: 56.86690

Formula: y = mx + b

 m: 980.79368

 b: 66.09075

 x: Amount

 y: Area

Calibration Level Weights:

 Level 1 : 1

 Level 2 : 0.204021

 Level 3 : 0.104493

 Level 4 : 0.067164

 Level 5 : 0.04976

=====================================================================

Method H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

Instrument 3 4/3/2010 9:40:41 AM KHB Page 2 of 2

EA# 0310-96 Page 98 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\001-0201.D) 1.468 1.669 1.739 8.325 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.325 BB 158.31195 5.93936e-4 9.40271e-2 Hydrogen Cyanide 

Totals : 9.40271e-2

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\001-0201.D

Sample Name: hplcprep4pg7 #1

 =====================================================================

 Acq. Operator : KHB Seq. Line : 2

 Acq. Instrument : Grandmama Location : -

 Injection Date : 3/31/2010 2:51:33 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:41:09 AM KHB Page 1 of 1

EA# 0310-96 Page 99 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\001-0202.D) 1.466 1.734 8.310 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.310 BB 159.05453 5.95923e-4 9.47842e-2 Hydrogen Cyanide 

Totals : 9.47842e-2

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\001-0202.D

Sample Name: hplcprep4pg7 #1

 =====================================================================

 Acq. Operator : KHB Seq. Line : 2

 Acq. Instrument : Grandmama Location : -

 Injection Date : 3/31/2010 3:06:49 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:41:16 AM KHB Page 1 of 1

EA# 0310-96 Page 100 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\002-0301.D) 1.466 1.665 1.735 8.302 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.302 BB 594.40326 9.06217e-4 5.38658e-1 Hydrogen Cyanide 

Totals : 5.38658e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\002-0301.D

Sample Name: hplcprep4pg7 #2

 =====================================================================

 Acq. Operator : KHB Seq. Line : 3

 Acq. Instrument : Grandmama Location : -

 Injection Date : 3/31/2010 3:22:06 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:41:20 AM KHB Page 1 of 1

EA# 0310-96 Page 101 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\002-0302.D) 1.469 1.671 1.741 8.301 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.301 BB 605.35022 9.08267e-4 5.49819e-1 Hydrogen Cyanide 

Totals : 5.49819e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\002-0302.D

Sample Name: hplcprep4pg7 #2

 =====================================================================

 Acq. Operator : KHB Seq. Line : 3

 Acq. Instrument : Grandmama Location : -

 Injection Date : 3/31/2010 3:37:22 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:41:25 AM KHB Page 1 of 1

EA# 0310-96 Page 102 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\003-0401.D) 1.463 1.660 1.728 8.240 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.240 BB 1096.14856 9.58108e-4 1.05023 Hydrogen Cyanide 

Totals : 1.05023

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\003-0401.D

Sample Name: hplcprep4pg7 #3

 =====================================================================

 Acq. Operator : KHB Seq. Line : 4

 Acq. Instrument : Grandmama Location : -

 Injection Date : 3/31/2010 3:52:39 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:41:31 AM KHB Page 1 of 1

EA# 0310-96 Page 103 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\003-0402.D) 1.470 1.732 8.272 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.272 BB 1096.98169 9.58155e-4 1.05108 Hydrogen Cyanide 

Totals : 1.05108

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\003-0402.D

Sample Name: hplcprep4pg7 #3

 =====================================================================

 Acq. Operator : KHB Seq. Line : 4

 Acq. Instrument : Grandmama Location : -

 Injection Date : 3/31/2010 4:07:55 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:41:36 AM KHB Page 1 of 1

EA# 0310-96 Page 104 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-0501.D) 1.473 1.739 8.278 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.278 BB 1515.66589 9.75123e-4 1.47796 Hydrogen Cyanide 

Totals : 1.47796

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-0501.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 5

 Acq. Instrument : Grandmama Location : -

 Injection Date : 3/31/2010 4:23:12 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:41:43 AM KHB Page 1 of 1

EA# 0310-96 Page 105 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-0502.D) 1.468 1.735 8.251 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.251 BB 1600.00488 9.77467e-4 1.56395 Hydrogen Cyanide 

Totals : 1.56395

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-0502.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 5

 Acq. Instrument : Grandmama Location : -

 Injection Date : 3/31/2010 4:38:28 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:41:50 AM KHB Page 1 of 1

EA# 0310-96 Page 106 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\005-0601.D) 1.461 1.661 1.729 8.233 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.233 BB 2090.05225 9.87342e-4 2.06360 Hydrogen Cyanide 

Totals : 2.06360

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\005-0601.D

Sample Name: hplcprep4pg7 #5

 =====================================================================

 Acq. Operator : KHB Seq. Line : 6

 Acq. Instrument : Grandmama Location : -

 Injection Date : 3/31/2010 4:53:45 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:41:57 AM KHB Page 1 of 1

EA# 0310-96 Page 107 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\005-0602.D) 1.469 1.731 8.263 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.263 BB 1988.93188 9.85702e-4 1.96050 Hydrogen Cyanide 

Totals : 1.96050

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\005-0602.D

Sample Name: hplcprep4pg7 #5

 =====================================================================

 Acq. Operator : KHB Seq. Line : 6

 Acq. Instrument : Grandmama Location : -

 Injection Date : 3/31/2010 5:09:07 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:42:04 AM KHB Page 1 of 1

EA# 0310-96 Page 108 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\006-0701.D) 1.470 1.669 1.737 8.288 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.288 BB 959.67920 9.49366e-4 9.11087e-1 Hydrogen Cyanide 

Totals : 9.11087e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\006-0701.D

Sample Name: hplcprep4pg7 #LCS

 =====================================================================

 Acq. Operator : KHB Seq. Line : 7

 Acq. Instrument : Grandmama Location : -

 Injection Date : 3/31/2010 5:24:24 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:42:11 AM KHB Page 1 of 1

EA# 0310-96 Page 109 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\006-0702.D) 1.464 1.666 1.737 8.276 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.276 BB 961.50732 9.49500e-4 9.12951e-1 Hydrogen Cyanide 

Totals : 9.12951e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\006-0702.D

Sample Name: hplcprep4pg7 #LCS

 =====================================================================

 Acq. Operator : KHB Seq. Line : 7

 Acq. Instrument : Grandmama Location : -

 Injection Date : 3/31/2010 5:39:40 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:42:18 AM KHB Page 1 of 1

EA# 0310-96 Page 110 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-1301.D) 1.468 1.664 1.733 8.134 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.134 BB 1585.77869 9.77089e-4 1.54945 Hydrogen Cyanide 

Totals : 1.54945

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-1301.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 13

 Acq. Instrument : Grandmama Location : -

 Injection Date : 3/31/2010 8:27:47 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:42:35 AM KHB Page 1 of 1

EA# 0310-96 Page 111 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-1302.D) 1.472 1.736 8.122 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.122 BB 1596.32336 9.77370e-4 1.56020 Hydrogen Cyanide 

Totals : 1.56020

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-1302.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 13

 Acq. Instrument : Grandmama Location : -

 Injection Date : 3/31/2010 8:43:03 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:42:41 AM KHB Page 1 of 1

EA# 0310-96 Page 112 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-2001.D) 1.480 1.665 1.741 8.020 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.020 BB 1608.29333 9.77684e-4 1.57240 Hydrogen Cyanide 

Totals : 1.57240

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-2001.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 20

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 12:01:39 AM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:42:49 AM KHB Page 1 of 1

EA# 0310-96 Page 113 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-2002.D) 1.472 1.669 1.740 8.019 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.019 BB 1712.51831 9.80234e-4 1.67867 Hydrogen Cyanide 

Totals : 1.67867

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-2002.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 20

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 12:16:55 AM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:43:12 AM KHB Page 1 of 1

EA# 0310-96 Page 114 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-2701.D) 1.472 1.672 1.743 8.022 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.022 BB 1647.42615 9.78679e-4 1.61230 Hydrogen Cyanide 

Totals : 1.61230

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-2701.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 27

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 3:35:31 AM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:43:21 AM KHB Page 1 of 1

EA# 0310-96 Page 115 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-2702.D) 1.468 1.732 7.982 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 7.982 BB 1625.98572 9.78140e-4 1.59044 Hydrogen Cyanide 

Totals : 1.59044

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-2702.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 27

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 3:50:47 AM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:43:28 AM KHB Page 1 of 1

EA# 0310-96 Page 116 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-3401.D) 1.483 1.673 1.745 8.261 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.261 BB 1528.44287 9.75495e-4 1.49099 Hydrogen Cyanide 

Totals : 1.49099

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-3401.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 34

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 7:09:28 AM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:43:42 AM KHB Page 1 of 1

EA# 0310-96 Page 117 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-3402.D) 1.482 1.675 1.748 8.281 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.281 BB 1560.73547 9.76407e-4 1.52391 Hydrogen Cyanide 

Totals : 1.52391

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-3402.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 34

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 7:24:44 AM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:43:49 AM KHB Page 1 of 1

EA# 0310-96 Page 118 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-4101.D) 1.479 1.668 1.738 8.264 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.264 BB 1502.43188 9.74732e-4 1.46447 Hydrogen Cyanide 

Totals : 1.46447

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-4101.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 41

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 10:43:25 AM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:43:58 AM KHB Page 1 of 1

EA# 0310-96 Page 119 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-4102.D) 1.467 1.660 1.729 8.228 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.228 BB 1501.56042 9.74706e-4 1.46358 Hydrogen Cyanide 

Totals : 1.46358

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-4102.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 41

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 10:58:42 AM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:44:04 AM KHB Page 1 of 1

EA# 0310-96 Page 120 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-4801.D) 1.470 1.672 1.746 8.275 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.275 BB 1633.78418 9.78338e-4 1.59839 Hydrogen Cyanide 

Totals : 1.59839

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-4801.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 48

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 2:17:17 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:44:14 AM KHB Page 1 of 1

EA# 0310-96 Page 121 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-4802.D) 1.471 1.666 1.736 8.250 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.250 BB 1599.92737 9.77465e-4 1.56387 Hydrogen Cyanide 

Totals : 1.56387

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-4802.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 48

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 2:32:33 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:44:24 AM KHB Page 1 of 1

EA# 0310-96 Page 122 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-5501.D) 1.479 1.676 1.746 8.313 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.313 BB 1443.40576 9.72898e-4 1.40429 Hydrogen Cyanide 

Totals : 1.40429

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-5501.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 55

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 5:51:08 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:44:44 AM KHB Page 1 of 1

EA# 0310-96 Page 123 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-5502.D) 1.474 1.672 1.743 8.289 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.289 BB 1431.87061 9.72522e-4 1.39253 Hydrogen Cyanide 

Totals : 1.39253

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-5502.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 55

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 6:06:24 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:44:56 AM KHB Page 1 of 1

EA# 0310-96 Page 124 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-6201.D) 1.472 1.666 1.738 8.074 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.074 BB 1414.13306 9.71931e-4 1.37444 Hydrogen Cyanide 

Totals : 1.37444

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-6201.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 62

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 9:24:59 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:45:05 AM KHB Page 1 of 1

EA# 0310-96 Page 125 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-6202.D) 1.473 1.669 1.738 8.066 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.066 BB 1450.10461 9.73113e-4 1.41112 Hydrogen Cyanide 

Totals : 1.41112

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\004-6202.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 62

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/1/2010 9:40:16 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:45:11 AM KHB Page 1 of 1

EA# 0310-96 Page 126 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\003-6801.D) 1.472 1.672 1.740 8.017 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.017 BB 946.83807 9.48414e-4 8.97994e-1 Hydrogen Cyanide 

Totals : 8.97994e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\003-6801.D

Sample Name: hplcprep4pg7 #3

 =====================================================================

 Acq. Operator : KHB Seq. Line : 68

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 12:28:18 AM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:45:46 AM KHB Page 1 of 1

EA# 0310-96 Page 127 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\003-6802.D)

 Area: 957.644

 1.480

 1.670 1.741

 8.023 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 01, 2010 8:37:28 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.023 MM 957.64447 9.49217e-4 9.09013e-1 Hydrogen Cyanide 

Totals : 9.09013e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96C\003-6802.D

Sample Name: hplcprep4pg7 #3

 =====================================================================

 Acq. Operator : KHB Seq. Line : 68

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 12:43:33 AM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96C.M

 Last changed : 4/2/2010 5:02:15 PM by KHB

 =====================================================================

Instrument 3 4/3/2010 9:46:00 AM KHB Page 1 of 1

EA# 0310-96 Page 128 of 236
=====================================================================

 Calibration Table 

=====================================================================

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Calculate : External Standard

Based on : Peak Area

Rel. Reference Window : 10.000 %

Abs. Reference Window : 0.300 min

Rel. Non-ref. Window : 10.000 %

Abs. Non-ref. Window : 0.300 min

Use Multiplier & Dilution Factor with ISTDs

Uncalibrated Peaks : not reported

Partial Calibration : Yes, identified peaks are recalibrated

Correct All Ret. Times: No, only for identified peaks

Curve Type : Linear

Origin : Ignored

Weight : Linear (Amnt)

Recalibration Settings: 

Average Response : Average all calibrations

Average Retention Time: Floating Average New 75%

Calibration Report Options :

 Printout of recalibrations within a sequence:

 Calibration Table after Recalibration

 Normal Report after Recalibration

 If the sequence is done with bracketing:

 Results of first cycle (ending previous bracket)

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Lvl Amount Area Amt/Area Ref Grp Name 

 [min] Sig [ug/mL] 

-------|--|--|----------|----------|----------|---|--|---------------

 8.267 1 1 1.03500e-1 91.28078 1.13386e-3 Hydrogen Cyanide 

 2 5.07300e-1 315.68977 1.60696e-3 

 3 9.90500e-1 596.65891 1.66008e-3 

 4 1.54100 892.60303 1.72641e-3 

 5 2.08000 1187.42535 1.75169e-3 

=====================================================================

 Peak Sum Table 

=====================================================================

***No Entries in table***

=====================================================================

Method H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

Instrument 3 4/6/2010 8:25:06 AM KHB Page 1 of 2

EA# 0310-96 Page 129 of 236
=====================================================================

 Calibration Curves

=====================================================================

Amount[ug/mL]

0 1 2

Area

0

200

400

600

800

1000

1

2

3

4

5

Hydrogen Cyanide at exp. RT: 8.267

ADC1 A, ADC1 CHANNEL A

Correlation: 0.99994

Residual Std. Dev.: 7.20496

Formula: y = mx + b

 m: 558.04992

 b: 33.87075

 x: Amount

 y: Area

Calibration Level Weights:

 Level 1 : 1

 Level 2 : 0.204021

 Level 3 : 0.104493

 Level 4 : 0.067164

 Level 5 : 0.04976

=====================================================================

Method H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

Instrument 3 4/6/2010 8:25:06 AM KHB Page 2 of 2

EA# 0310-96 Page 130 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\001-0101.D)

 Area: 92.914

 1.471

 1.670 1.742

 8.308 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.308 MM 92.91398 1.13872e-3 1.05803e-1 Hydrogen Cyanide 

Totals : 1.05803e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\001-0101.D

Sample Name: hplcprep4pg7 #1

 =====================================================================

 Acq. Operator : KHB Seq. Line : 1

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 4:41:48 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:25:50 AM KHB Page 1 of 1

EA# 0310-96 Page 131 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\001-0102.D)

 Area: 89.7035

 1.455

 1.652 1.723

 8.253 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.253 MM 89.70345 1.11534e-3 1.00050e-1 Hydrogen Cyanide 

Totals : 1.00050e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\001-0102.D

Sample Name: hplcprep4pg7 #1

 =====================================================================

 Acq. Operator : KHB Seq. Line : 1

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 4:57:08 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:25:21 AM KHB Page 1 of 1

EA# 0310-96 Page 132 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\002-0201.D) 1.455 1.651 1.726 8.221 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.221 BB 322.97928 1.60403e-3 5.18069e-1 Hydrogen Cyanide 

Totals : 5.18069e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\002-0201.D

Sample Name: hplcprep4pg7 #2

 =====================================================================

 Acq. Operator : KHB Seq. Line : 2

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 5:12:25 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:25:56 AM KHB Page 1 of 1

EA# 0310-96 Page 133 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\002-0202.D) 1.468 1.665 1.736 8.273 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.273 BB 308.40027 1.59515e-3 4.91944e-1 Hydrogen Cyanide 

Totals : 4.91944e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\002-0202.D

Sample Name: hplcprep4pg7 #2

 =====================================================================

 Acq. Operator : KHB Seq. Line : 2

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 5:27:41 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:26:03 AM KHB Page 1 of 1

EA# 0310-96 Page 134 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\003-0301.D) 1.464 1.666 1.737 8.232 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.232 BB 605.01593 1.69163e-3 1.02347 Hydrogen Cyanide 

Totals : 1.02347

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\003-0301.D

Sample Name: hplcprep4pg7 #3

 =====================================================================

 Acq. Operator : KHB Seq. Line : 3

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 5:42:58 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:26:08 AM KHB Page 1 of 1

EA# 0310-96 Page 135 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\003-0302.D) 1.466 1.660 1.732 8.245 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.245 BB 588.30188 1.68878e-3 9.93515e-1 Hydrogen Cyanide 

Totals : 9.93515e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\003-0302.D

Sample Name: hplcprep4pg7 #3

 =====================================================================

 Acq. Operator : KHB Seq. Line : 3

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 5:58:15 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:26:16 AM KHB Page 1 of 1

EA# 0310-96 Page 136 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\004-0401.D) 1.666 1.741 8.248 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.248 BB 875.26874 1.72261e-3 1.50775 Hydrogen Cyanide 

Totals : 1.50775

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\004-0401.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 4

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 6:13:32 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:26:25 AM KHB Page 1 of 1

EA# 0310-96 Page 137 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\004-0402.D) 1.469 1.667 1.739 8.255 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.255 BB 909.93732 1.72525e-3 1.56987 Hydrogen Cyanide 

Totals : 1.56987

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\004-0402.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 4

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 6:28:48 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:26:39 AM KHB Page 1 of 1

EA# 0310-96 Page 138 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\005-0501.D) 1.467 1.665 1.740 8.224 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.224 BB 1180.62842 1.74055e-3 2.05494 Hydrogen Cyanide 

Totals : 2.05494

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\005-0501.D

Sample Name: hplcprep4pg7 #5

 =====================================================================

 Acq. Operator : KHB Seq. Line : 5

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 6:44:05 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:26:46 AM KHB Page 1 of 1

EA# 0310-96 Page 139 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\005-0502.D) 1.458 1.658 1.730 8.206 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.206 BB 1194.22229 1.74113e-3 2.07930 Hydrogen Cyanide 

Totals : 2.07930

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\005-0502.D

Sample Name: hplcprep4pg7 #5

 =====================================================================

 Acq. Operator : KHB Seq. Line : 5

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 6:59:21 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:26:53 AM KHB Page 1 of 1

EA# 0310-96 Page 140 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\006-0601.D) 1.735 8.208 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.208 BB 517.62390 1.67470e-3 8.66864e-1 Hydrogen Cyanide 

Totals : 8.66864e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\006-0601.D

Sample Name: hplcprep4pg7 #LCS

 =====================================================================

 Acq. Operator : KHB Seq. Line : 6

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 7:14:38 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:27:06 AM KHB Page 1 of 1

EA# 0310-96 Page 141 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\006-0602.D) 1.664 1.735 8.192 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.192 BB 498.90042 1.67030e-3 8.33312e-1 Hydrogen Cyanide 

Totals : 8.33312e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\006-0602.D

Sample Name: hplcprep4pg7 #LCS

 =====================================================================

 Acq. Operator : KHB Seq. Line : 6

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 7:29:54 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:27:13 AM KHB Page 1 of 1

EA# 0310-96 Page 142 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\003-1301.D) 1.657 1.730 7.972 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 7.972 BB 635.89722 1.69651e-3 1.07880 Hydrogen Cyanide 

Totals : 1.07880

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\003-1301.D

Sample Name: hplcprep4pg7 #3

 =====================================================================

 Acq. Operator : KHB Seq. Line : 13

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 10:48:29 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:27:44 AM KHB Page 1 of 1

EA# 0310-96 Page 143 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\003-1302.D) 1.465 1.667 1.741 8.006 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.006 BB 637.61737 1.69676e-3 1.08189 Hydrogen Cyanide 

Totals : 1.08189

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\003-1302.D

Sample Name: hplcprep4pg7 #3

 =====================================================================

 Acq. Operator : KHB Seq. Line : 13

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/2/2010 11:03:51 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:27:51 AM KHB Page 1 of 1

EA# 0310-96 Page 144 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\003-2001.D) 1.663 1.735 8.208 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.208 BB 616.81616 1.69355e-3 1.04461 Hydrogen Cyanide 

Totals : 1.04461

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\003-2001.D

Sample Name: hplcprep4pg7 #3

 =====================================================================

 Acq. Operator : KHB Seq. Line : 20

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/3/2010 11:27:14 AM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:28:04 AM KHB Page 1 of 1

EA# 0310-96 Page 145 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\003-2002.D) 1.464 1.666 1.741 8.221 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.221 BB 629.77905 1.69558e-3 1.06784 Hydrogen Cyanide 

Totals : 1.06784

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\003-2002.D

Sample Name: hplcprep4pg7 #3

 =====================================================================

 Acq. Operator : KHB Seq. Line : 20

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/3/2010 11:42:30 AM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:28:10 AM KHB Page 1 of 1

EA# 0310-96 Page 146 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\003-2701.D) 1.468 1.667 1.743 8.271 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.271 BB 624.37903 1.69475e-3 1.05816 Hydrogen Cyanide 

Totals : 1.05816

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\003-2701.D

Sample Name: hplcprep4pg7 #3

 =====================================================================

 Acq. Operator : KHB Seq. Line : 27

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/3/2010 3:01:11 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:28:19 AM KHB Page 1 of 1

EA# 0310-96 Page 147 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\003-2702.D) 1.469 1.670 1.741 8.251 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.251 BB 630.06641 1.69562e-3 1.06836 Hydrogen Cyanide 

Totals : 1.06836

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\003-2702.D

Sample Name: hplcprep4pg7 #3

 =====================================================================

 Acq. Operator : KHB Seq. Line : 27

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/3/2010 3:16:27 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:28:27 AM KHB Page 1 of 1

EA# 0310-96 Page 148 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\003-3401.D) 1.675 1.746 8.291 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.291 BB 604.33838 1.69152e-3 1.02225 Hydrogen Cyanide 

Totals : 1.02225

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\003-3401.D

Sample Name: hplcprep4pg7 #3

 =====================================================================

 Acq. Operator : KHB Seq. Line : 34

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/3/2010 6:35:07 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:28:35 AM KHB Page 1 of 1

EA# 0310-96 Page 149 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\003-3402.D)

 Area: 594.341

 1.658 1.731

 8.273 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Tuesday, April 06, 2010 8:24:10 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.273 MM 594.34137 1.68983e-3 1.00434 Hydrogen Cyanide 

Totals : 1.00434

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96D\003-3402.D

Sample Name: hplcprep4pg7 #3

 =====================================================================

 Acq. Operator : KHB Seq. Line : 34

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/3/2010 6:50:24 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 3/17/2010 9:48:43 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96D.M

 Last changed : 4/6/2010 8:24:11 AM by KHB

 =====================================================================

Instrument 3 4/6/2010 8:28:55 AM KHB Page 1 of 1

EA# 0310-96 Page 150 of 236
=====================================================================

 Calibration Table 

=====================================================================

Calib. Data Modified : Thursday, April 08, 2010 4:21:55 PM

Calculate : External Standard

Based on : Peak Area

Rel. Reference Window : 10.000 %

Abs. Reference Window : 0.300 min

Rel. Non-ref. Window : 10.000 %

Abs. Non-ref. Window : 0.300 min

Use Multiplier & Dilution Factor with ISTDs

Uncalibrated Peaks : not reported

Partial Calibration : Yes, identified peaks are recalibrated

Correct All Ret. Times: No, only for identified peaks

Curve Type : Linear

Origin : Ignored

Weight : Linear (Amnt)

Recalibration Settings: 

Average Response : Average all calibrations

Average Retention Time: Floating Average New 75%

Calibration Report Options :

 Printout of recalibrations within a sequence:

 Calibration Table after Recalibration

 Normal Report after Recalibration

 If the sequence is done with bracketing:

 Results of first cycle (ending previous bracket)

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Lvl Amount Area Amt/Area Ref Grp Name 

 [min] Sig [ug/mL] 

-------|--|--|----------|----------|----------|---|--|---------------

 8.520 1 1 1.03500e-1 255.03889 4.05820e-4 Hydrogen Cyanide 

 2 5.07300e-1 827.54083 6.13021e-4 

 3 9.90500e-1 1407.16968 7.03895e-4 

 4 1.54100 1860.77960 8.28148e-4 

 5 2.08000 2418.35120 8.60090e-4 

=====================================================================

 Peak Sum Table 

=====================================================================

***No Entries in table***

=====================================================================

Method H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

Instrument 3 4/8/2010 4:22:05 PM KHB Page 1 of 2

EA# 0310-96 Page 151 of 236
=====================================================================

 Calibration Curves

=====================================================================

Amount[ug/mL]

0 1 2

Area

0

500

1000

1500

2000

2500

1

2

3

4

5

Hydrogen Cyanide at exp. RT: 8.520

ADC1 A, ADC1 CHANNEL A

Correlation: 0.99525

Residual Std. Dev.: 116.32524

Formula: y = mx + b

 m: 1146.38235

 b: 156.42553

 x: Amount

 y: Area

Calibration Level Weights:

 Level 1 : 1

 Level 2 : 0.204021

 Level 3 : 0.104493

 Level 4 : 0.067164

 Level 5 : 0.04976

=====================================================================

Method H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

Instrument 3 4/8/2010 4:22:05 PM KHB Page 2 of 2

EA# 0310-96 Page 152 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\001-0201.D)

 Area: 253.135

 1.686 1.765

 2.272

 8.505 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 08, 2010 4:21:55 PM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.505 FM 253.13521 3.33264e-4 8.43608e-2 Hydrogen Cyanide 

Totals : 8.43608e-2

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\001-0201.D

Sample Name: hplcprep4pg7 #1

 =====================================================================

 Acq. Operator : KHB Seq. Line : 2

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/8/2010 10:22:16 AM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 4/8/2010 9:49:36 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

 Last changed : 4/8/2010 4:21:58 PM by KHB

 =====================================================================

Instrument 3 4/8/2010 4:29:35 PM KHB Page 1 of 1

EA# 0310-96 Page 153 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\001-0202.D)

 Area: 256.958

 1.698 1.773

 2.286

 8.525 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 08, 2010 4:21:55 PM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.525 MM 256.95786 3.41283e-4 8.76953e-2 Hydrogen Cyanide 

Totals : 8.76953e-2

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\001-0202.D

Sample Name: hplcprep4pg7 #1

 =====================================================================

 Acq. Operator : KHB Seq. Line : 2

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/8/2010 10:37:33 AM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 4/8/2010 9:49:36 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

 Last changed : 4/8/2010 4:21:58 PM by KHB

 =====================================================================

Instrument 3 4/8/2010 4:22:22 PM KHB Page 1 of 1

EA# 0310-96 Page 154 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\002-0301.D) 1.682 1.760 2.268 8.467 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 08, 2010 4:21:55 PM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.467 BB 839.83075 7.09834e-4 5.96141e-1 Hydrogen Cyanide 

Totals : 5.96141e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\002-0301.D

Sample Name: hplcprep4pg7 #2

 =====================================================================

 Acq. Operator : KHB Seq. Line : 3

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/8/2010 10:52:49 AM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 4/8/2010 9:49:36 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

 Last changed : 4/8/2010 4:21:58 PM by KHB

 =====================================================================

Instrument 3 4/8/2010 4:29:45 PM KHB Page 1 of 1

EA# 0310-96 Page 155 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\002-0302.D) 1.686 1.767 2.273 8.491 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 08, 2010 4:21:55 PM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.491 BB 815.25092 7.04936e-4 5.74700e-1 Hydrogen Cyanide 

Totals : 5.74700e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\002-0302.D

Sample Name: hplcprep4pg7 #2

 =====================================================================

 Acq. Operator : KHB Seq. Line : 3

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/8/2010 11:08:06 AM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 4/8/2010 9:49:36 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

 Last changed : 4/8/2010 4:21:58 PM by KHB

 =====================================================================

Instrument 3 4/8/2010 4:29:50 PM KHB Page 1 of 1

EA# 0310-96 Page 156 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\003-0401.D) 1.695 1.775 2.283 8.460 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 08, 2010 4:21:55 PM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.460 BB 1401.60974 7.74956e-4 1.08619 Hydrogen Cyanide 

Totals : 1.08619

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\003-0401.D

Sample Name: hplcprep4pg7 #3

 =====================================================================

 Acq. Operator : KHB Seq. Line : 4

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/8/2010 11:23:23 AM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 4/8/2010 9:49:36 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

 Last changed : 4/8/2010 4:21:58 PM by KHB

 =====================================================================

Instrument 3 4/8/2010 4:29:55 PM KHB Page 1 of 1

EA# 0310-96 Page 157 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\003-0402.D) 1.699 1.777 2.286 8.475 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 08, 2010 4:21:55 PM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.475 BB 1412.72961 7.75722e-4 1.09589 Hydrogen Cyanide 

Totals : 1.09589

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\003-0402.D

Sample Name: hplcprep4pg7 #3

 =====================================================================

 Acq. Operator : KHB Seq. Line : 4

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/8/2010 11:38:38 AM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 4/8/2010 9:49:36 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

 Last changed : 4/8/2010 4:21:58 PM by KHB

 =====================================================================

Instrument 3 4/8/2010 4:30:00 PM KHB Page 1 of 1

EA# 0310-96 Page 158 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\004-0501.D) 1.696 1.777 2.283 8.458 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 08, 2010 4:21:55 PM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.458 BB 1902.18762 8.00575e-4 1.52284 Hydrogen Cyanide 

Totals : 1.52284

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\004-0501.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 5

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/8/2010 11:53:55 AM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 4/8/2010 9:49:36 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

 Last changed : 4/8/2010 4:21:58 PM by KHB

 =====================================================================

Instrument 3 4/8/2010 4:30:09 PM KHB Page 1 of 1

EA# 0310-96 Page 159 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\004-0502.D) 1.688 1.768 2.271 8.453 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 08, 2010 4:21:55 PM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.453 BB 1819.37158 7.97310e-4 1.45060 Hydrogen Cyanide 

Totals : 1.45060

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\004-0502.D

Sample Name: hplcprep4pg7 #4

 =====================================================================

 Acq. Operator : KHB Seq. Line : 5

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/8/2010 12:09:12 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 4/8/2010 9:49:36 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

 Last changed : 4/8/2010 4:21:58 PM by KHB

 =====================================================================

Instrument 3 4/8/2010 4:30:15 PM KHB Page 1 of 1

EA# 0310-96 Page 160 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\005-0601.D) 1.690 1.769 2.272 8.433 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 08, 2010 4:21:55 PM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.433 BB 2389.64868 8.15208e-4 1.94806 Hydrogen Cyanide 

Totals : 1.94806

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\005-0601.D

Sample Name: hplcprep4pg7 #5

 =====================================================================

 Acq. Operator : KHB Seq. Line : 6

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/8/2010 12:24:29 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 4/8/2010 9:49:36 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

 Last changed : 4/8/2010 4:21:58 PM by KHB

 =====================================================================

Instrument 3 4/8/2010 4:30:21 PM KHB Page 1 of 1

EA# 0310-96 Page 161 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\005-0602.D) 1.698 1.775 2.284 8.435 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 08, 2010 4:21:55 PM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.435 BB 2447.05371 8.16548e-4 1.99814 Hydrogen Cyanide 

Totals : 1.99814

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\005-0602.D

Sample Name: hplcprep4pg7 #5

 =====================================================================

 Acq. Operator : KHB Seq. Line : 6

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/8/2010 12:39:45 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 4/8/2010 9:49:36 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

 Last changed : 4/8/2010 4:21:58 PM by KHB

 =====================================================================

Instrument 3 4/8/2010 4:30:29 PM KHB Page 1 of 1

EA# 0310-96 Page 162 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\006-0701.D)

 Area: 1170.18

 1.689 1.769

 2.275

 8.430 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 08, 2010 4:21:55 PM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.430 MM 1170.18103 7.55702e-4 8.84308e-1 Hydrogen Cyanide 

Totals : 8.84308e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\006-0701.D

Sample Name: hplcprep4pg7 #LCS

 =====================================================================

 Acq. Operator : KHB Seq. Line : 7

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/8/2010 12:55:01 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 4/8/2010 9:49:36 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

 Last changed : 4/8/2010 4:21:58 PM by KHB

 =====================================================================

Instrument 3 4/8/2010 4:31:04 PM KHB Page 1 of 1

EA# 0310-96 Page 163 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\006-0702.D)

 Area: 1120.76

 1.687 1.764

 2.268

 8.425 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 08, 2010 4:21:55 PM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.425 MM 1120.75830 7.50560e-4 8.41196e-1 Hydrogen Cyanide 

Totals : 8.41196e-1

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\006-0702.D

Sample Name: hplcprep4pg7 #LCS

 =====================================================================

 Acq. Operator : KHB Seq. Line : 7

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/8/2010 1:10:18 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 4/8/2010 9:49:36 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

 Last changed : 4/8/2010 4:21:58 PM by KHB

 =====================================================================

Instrument 3 4/8/2010 4:31:20 PM KHB Page 1 of 1

EA# 0310-96 Page 164 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\003-1301.D)

 Area: 1343.49

 1.689 1.769

 2.275

 8.383 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 08, 2010 4:21:55 PM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.383 MM 1343.49377 7.70745e-4 1.03549 Hydrogen Cyanide 

Totals : 1.03549

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\003-1301.D

Sample Name: hplcprep4pg7 #3

 =====================================================================

 Acq. Operator : KHB Seq. Line : 13

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/8/2010 3:58:32 PM Inj : 1

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 4/8/2010 9:49:36 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

 Last changed : 4/8/2010 4:21:58 PM by KHB

 =====================================================================

Instrument 3 4/8/2010 4:32:25 PM KHB Page 1 of 1

EA# 0310-96 Page 165 of 236
0 2 4 6 8 10 12 min

nC

50

100

150

200

250

300

350

400

 ADC1 A, ADC1 CHANNEL A (H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\003-1302.D) 1.689 1.769 2.274 8.388 - Hydrogen Cyanide

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Thursday, April 08, 2010 4:21:55 PM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [nC*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 8.388 BB 1379.40637 7.73389e-4 1.06682 Hydrogen Cyanide 

Totals : 1.06682

=====================================================================

 *** End of Report ***

Data File H:\HPLC2010Q1\GRANDMAM\DATA\MAR\0310-96G\003-1302.D

Sample Name: hplcprep4pg7 #3

 =====================================================================

 Acq. Operator : KHB Seq. Line : 13

 Acq. Instrument : Grandmama Location : -

 Injection Date : 4/8/2010 4:13:48 PM Inj : 2

 Acq. Method : H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Last changed : 4/8/2010 9:49:36 AM by KHB

 Analysis Method : H:\HPLC2010Q1\GRANDMAM\METHODS\0310-96G.M

 Last changed : 4/8/2010 4:21:58 PM by KHB

 =====================================================================

Instrument 3 4/8/2010 4:32:42 PM KHB Page 1 of 1

EA# 0310-96 Page 166 of 236
 Method Information

 Method: H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

 Modified: 3/17/2010 at 9:48:43 AM

 Column: Dionex Ionpac AS7 4 X 250mm

 Eluent: 0.5M Sodium Acetate/0.1M NaOH/0.5% v/v Ethylenediamine

 Flow rate: 1.0 mL/min

=========================================================================

 ANALOG DIGITAL CONVERTER

=========================================================================

 Signal 1

 ---------------------

Description: ADC1 CHANNEL A

Source: Signal

Unit: nC

Units/Volt: 1000.000

Peakwidth (Data Rate): 0.133 Min (2.00 Hz)

Stop Time: 14.01 Min

Data Storage: All

Start Signal Source: External Device Will Start 35900

Timed Event Table:

 <no events>

 method: H:\HPLC2010Q1\GRANDMAM\METHODS\1000.M

Modified on: 3/17/2010 at 9:48:43 AM

Grandmama 3/17/2010 9:49:42 AM KHB Page 1 of 1

EA# 0310-96 Page 167 of 236
Sequence Table:

 Method and Injection Info Part:

 Line Location SampleName Method Inj SampleType InjVolume

 DataFile AutoBalance LimsID

 ==== ======== ==================== ==================== ======== ========== =========

 1 Vial 7 0.1N NaOH - RB 1000 2 Sample 

 

 2 Vial 1 hplcprep4pg7 #1 1000 2 Sample 

 3 Vial 2 hplcprep4pg7 #2 1000 2 Sample 

 4 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

 5 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

 6 Vial 5 hplcprep4pg7 #5 1000 2 Sample 

 7 Vial 6 hplcprep4pg7 #LCS 1000 2 Sample 

 8 Vial 7 0.1N NaOH - RB 1000 2 Sample 

 9 Vial 8 T5 Run 1*5 0310-127 1000 2 Sample 

 10 Vial 9 T5 Run 2*5 0310-127 1000 2 Sample 

 11 Vial 10 T5 Run 3*5 0310-127 1000 2 Sample 

 12 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

 13 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

 14 Vial 11 Blank*5 0310-127 1000 2 Sample 

 15 Vial 12 Unit 1 R3*5 0310-126 1000 2 Sample 

 16 Vial 13 Unit 1 R4*5 0310-126 1000 2 Sample 

 17 Vial 14 Unit 1 R5*5 0310-126 1000 2 Sample 

 18 Vial 15 Unit 2 R4*5 0310-126 1000 2 Sample 

 19 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

 20 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

 21 Vial 16 Unit 2 R5*5 0310-126 1000 2 Sample 

 22 Vial 17 Unit 2 R6*5 0310-126 1000 2 Sample 

 23 Vial 18 Blank*5 0310-126 1000 2 Sample 

 24 Vial 19 U9-R1-C3*5 0210-93 1000 2 Sample 

 25 Vial 20 U9-R1-C4*5 0210-93 1000 2 Sample 

 26 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

 27 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

Sequence: H:\HPLC2010Q1\GRANDMAM\SEQUENCE\0210-96C.S

Instrument 3 4/6/2010 9:16:38 AM KHB Page 1 of 4

EA# 0310-96 Page 168 of 236
 Line Location SampleName Method Inj SampleType InjVolume

 DataFile AutoBalance LimsID

 ==== ======== ==================== ==================== ======== ========== =========

 28 Vial 21 U9-R2-C3*5 0210-93 1000 2 Sample 

 

 29 Vial 22 U9-R2-C4*5 0210-93 1000 2 Sample 

 30 Vial 23 U9-R3-C3*5 0210-93 1000 2 Sample 

 31 Vial 24 U9-R3-C4*5 0210-93 1000 2 Sample 

 32 Vial 25 U10-R1-C3*5 0210-93 1000 2 Sample 

 33 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

 34 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

 35 Vial 26 U10-R1-C4*5 0210-93 1000 2 Sample 

 36 Vial 27 U10-R2-C3*5 0210-93 1000 2 Sample 

 37 Vial 28 U10-R2-C4*5 0210-93 1000 2 Sample 

 38 Vial 29 U10-R3-C3*5 0210-93 1000 2 Sample 

 39 Vial 30 U10-R3-C4*5 0210-93 1000 2 Sample 

 40 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

 41 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

 42 Vial 31 FB Spk*5 0210-93 1000 2 Sample 

 43 Vial 32 U10-FB-C3*5 0210-93 1000 2 Sample 

 44 Vial 33 U10-FB-C4*5 0210-93 1000 2 Sample 

 45 Vial 34 U10-RB-4N NaOH*5 0210-93 1000 2 Sample 

 46 Vial 35 U10-RB-Pb Ace*5 0210-93 1000 2 Sample 

 47 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

 48 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

 49 Vial 36 U1-Pb-1*5 0310-96 1000 2 Sample 

 50 Vial 37 U1-NaOH-1*5 0310-96 1000 2 Sample 

 51 Vial 38 U1-Pb-2*5 0310-96 1000 2 Sample 

 52 Vial 39 U1-NaOH-2*5 0310-96 1000 2 Sample 

 53 Vial 40 U1-Pb-3*5 0310-96 1000 2 Sample 

 54 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

 55 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

 56 Vial 41 U1-NaOH-3*5 0310-96 1000 2 Sample 

 57 Vial 42 U2-Pb-1*5 0310-96 1000 2 Sample 

Sequence: H:\HPLC2010Q1\GRANDMAM\SEQUENCE\0210-96C.S

Instrument 3 4/6/2010 9:16:38 AM KHB Page 2 of 4

EA# 0310-96 Page 169 of 236
 Line Location SampleName Method Inj SampleType InjVolume

 DataFile AutoBalance LimsID

 ==== ======== ==================== ==================== ======== ========== =========

 58 Vial 43 U2-NaOH-1*5 0310-96 1000 2 Sample 

 

 59 Vial 44 U2-Pb-2*5 0310-96 1000 2 Sample 

 60 Vial 45 U2-NaOH-2*5 0310-96 1000 2 Sample 

 61 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

 62 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

 63 Vial 46 U2-Pb-3*5 0310-96 1000 2 Sample 

 64 Vial 47 U2-NaOH-3*5 0310-96 1000 2 Sample 

 65 Vial 48 NaOH FB*5 0310-96 1000 2 Sample 

 66 Vial 49 NaOH RB*5 0310-96 1000 2 Sample 

 67 Vial 50 NaOH FS*5 0310-96 1000 2 Sample 

 68 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

 69 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

 70 Vial 51 NaOH FB*5 0310-96 1000 2 Sample 

 71 Vial 52 NaOH RB*5 0310-96 1000 2 Sample 

 72 Vial 53 NaOH RB2*5 0310-96 1000 2 Sample 

 73 Vial 54 H2O RB*5 0310-96 1000 2 Sample 

 74 Vial 55 LCS #1*100 0310-96 1000 2 Sample 

 75 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

 76 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

 77 Vial 56 LCS #2*100 0310-96 1000 2 Sample 

 78 Vial 57 LCS #1*100 0210-93 1000 2 Sample 

 79 Vial 58 LCS #2*100 0210-93 1000 2 Sample 

 80 Vial 59 LD/U9-R1-C4*5 0210-93 1000 2 Sample 

 81 Vial 60 MS/U9-R1-C4 0210-93 1000 2 Sample 

 82 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

 83 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

 84 Vial 61 MSD/U9-R1-C4 0210-93 1000 2 Sample 

 85 Vial 62 LD/U2-NaOH-1*5 0310-96 1000 2 Sample 

 86 Vial 63 MS/U2-NaOH-1 0310-96 1000 2 Sample 

 87 Vial 64 MSD/U2-NaOH-1 0310-96 1000 2 Sample 

Sequence: H:\HPLC2010Q1\GRANDMAM\SEQUENCE\0210-96C.S

Instrument 3 4/6/2010 9:16:38 AM KHB Page 3 of 4

EA# 0310-96 Page 170 of 236
 Line Location SampleName Method Inj SampleType InjVolume

 DataFile AutoBalance LimsID

 ==== ======== ==================== ==================== ======== ========== =========

 88 Vial 65 LD/Unit 1 R4*5 0310-126 1000 2 Sample 

 

 89 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

 90 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

 91 Vial 66 MS/Unit 1 R4 0310-126 1000 2 Sample 

 92 Vial 67 MSD/Unit 1 R4 0310-126 1000 2 Sample 

 93 Vial 68 LD/T5 Run 1*5 0310-127 1000 2 Sample 

 94 Vial 69 MS/T5 Run 1 0310-127 1000 2 Sample 

 95 Vial 70 MSD/T5 Run 1 0310-127 1000 2 Sample 

 96 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

 97 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

Sequence: H:\HPLC2010Q1\GRANDMAM\SEQUENCE\0210-96C.S

Instrument 3 4/6/2010 9:16:38 AM KHB Page 4 of 4

EA# 0310-96 Page 171 of 236
Sequence Table:

 Method and Injection Info Part:

 Line Location SampleName Method Inj SampleType InjVolume

 DataFile AutoBalance LimsID

 ==== ======== ==================== ==================== ======== ========== =========

 1 Vial 1 hplcprep4pg7 #1 1000 2 Sample 

 

 2 Vial 2 hplcprep4pg7 #2 1000 2 Sample 

 3 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

 4 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

 5 Vial 5 hplcprep4pg7 #5 1000 2 Sample 

 6 Vial 6 hplcprep4pg7 #LCS 1000 2 Sample 

 7 Vial 7 0.1N NaOH - RB 1000 2 Sample 

 8 Vial 51 NaOH FB*5 0310-96 1000 2 Sample 

 9 Vial 52 NaOH RB*5 0310-96 1000 2 Sample 

 10 Vial 53 NaOH RB2*5 0310-96 1000 2 Sample 

 11 Vial 54 H2O RB*5 0310-96 1000 2 Sample 

 12 Vial 55 LCS #1*100 0310-96 1000 2 Sample 

 13 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

 14 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

 15 Vial 56 LCS #2*100 0310-96 1000 2 Sample 

 16 Vial 57 LCS #1*100 0210-93 1000 2 Sample 

 17 Vial 58 LCS #2*100 0210-93 1000 2 Sample 

 18 Vial 59 LD/U9-R1-C4*5 0210-93 1000 2 Sample 

 19 Vial 60 MS/U9-R1-C4 0210-93 1000 2 Sample 

 20 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

 21 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

 22 Vial 61 MSD/U9-R1-C4 0210-93 1000 2 Sample 

 23 Vial 62 LD/U2-NaOH-1*5 0310-96 1000 2 Sample 

 24 Vial 63 MS/U2-NaOH-1 0310-96 1000 2 Sample 

 25 Vial 64 MSD/U2-NaOH-1 0310-96 1000 2 Sample 

 26 Vial 65 LD/Unit 1 R4*5 0310-126 1000 2 Sample 

 27 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

Sequence: H:\HPLC2010Q1\GRANDMAM\SEQUENCE\0210-96D.S

Instrument 3 4/6/2010 9:16:45 AM KHB Page 1 of 2

EA# 0310-96 Page 172 of 236
 Line Location SampleName Method Inj SampleType InjVolume

 DataFile AutoBalance LimsID

 ==== ======== ==================== ==================== ======== ========== =========

 28 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

 

 29 Vial 66 MS/Unit 1 R4 0310-126 1000 2 Sample 

 30 Vial 67 MSD/Unit 1 R4 0310-126 1000 2 Sample 

 31 Vial 68 LD/T5 Run 1*5 0310-127 1000 2 Sample 

 32 Vial 69 MS/T5 Run 1 0310-127 1000 2 Sample 

 33 Vial 70 MSD/T5 Run 1 0310-127 1000 2 Sample 

 34 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

 35 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

Sequence: H:\HPLC2010Q1\GRANDMAM\SEQUENCE\0210-96D.S

Instrument 3 4/6/2010 9:16:45 AM KHB Page 2 of 2

EA# 0310-96 Page 173 of 236
Sequence Table:

 Method and Injection Info Part:

 Line Location SampleName Method Inj SampleType InjVolume

 DataFile AutoBalance LimsID

 ==== ======== ==================== ==================== ======== ========== =========

 1 Vial 7 0.1N NaOH - RB 1000 2 Sample 

 

 2 Vial 1 hplcprep4pg7 #1 1000 2 Sample 

 3 Vial 2 hplcprep4pg7 #2 1000 2 Sample 

 4 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

 5 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

 6 Vial 5 hplcprep4pg7 #5 1000 2 Sample 

 7 Vial 6 hplcprep4pg7 #LCS 1000 2 Sample 

 8 Vial 7 0.1N NaOH - RB 1000 2 Sample 

 9 Vial 11 MS/U2-NaOH-1 0310-96 1000 2 Sample 

 10 Vial 12 MSD/U2-NaOH-1 0310-96 1000 2 Sample 

 11 Vial 15 MS*2/U2-NaOH-1 0310-96 1000 2 Sample 

 12 Vial 16 MSD*2/U2-NaOH-1 0310-96 1000 2 Sample 

 13 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

 14 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

 15 Vial 13 MS*10/T5 Run 1 0310-127 1000 2 Sample 

 16 Vial 14 MSD*10/T5 Run 1 0310-127 1000 2 Sample 

 17 Vial 3 hplcprep4pg7 #3 1000 2 Sample 

 18 Vial 4 hplcprep4pg7 #4 1000 2 Sample 

Sequence: H:\HPLC2010Q1\GRANDMAM\SEQUENCE\0210-96G.S

Instrument 3 4/8/2010 5:01:55 PM KHB Page 1 of 1

EA# 0310-96 Page 174 of 236
Sample 

Chromatograms

EA# 0310-96 Page 175 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 28

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 12:32:07 AM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\025-2801.D)

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.806 - - - Fluoride 

 3.775 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\025-2801.D

Sample Name: U1 R1 *20 0310-96

Instrument 1 3/24/2010 1:51:32 PM ARM Page 1 of 2

EA# 0310-96 Page 176 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 28

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 12:42:56 AM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\025-2802.D) 5.802

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.806 - - - Fluoride 

 3.775 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\025-2802.D

Sample Name: U1 R1 *20 0310-96

Instrument 1 3/24/2010 1:51:43 PM ARM Page 1 of 2

EA# 0310-96 Page 177 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 35

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 3:03:17 AM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\028-3501.D) 3.449

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.806 - - - Fluoride 

 3.775 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\028-3501.D

Sample Name: U1 R2 *20 0310-96

Instrument 1 3/24/2010 1:54:30 PM ARM Page 1 of 2

EA# 0310-96 Page 178 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 35

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 3:14:05 AM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\028-3502.D) 3.450

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.806 - - - Fluoride 

 3.775 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\028-3502.D

Sample Name: U1 R2 *20 0310-96

Instrument 1 3/24/2010 1:54:39 PM ARM Page 1 of 2

EA# 0310-96 Page 179 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 36

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 3:24:53 AM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\029-3601.D) 3.451 4.506 5.804

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.806 - - - Fluoride 

 3.775 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\029-3601.D

Sample Name: U1 R3 *20 0310-96

Instrument 1 3/24/2010 1:55:23 PM ARM Page 1 of 2

EA# 0310-96 Page 180 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 36

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 3:35:41 AM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\029-3602.D) 3.451

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.806 - - - Fluoride 

 3.775 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\029-3602.D

Sample Name: U1 R3 *20 0310-96

Instrument 1 3/24/2010 1:55:35 PM ARM Page 1 of 2

EA# 0310-96 Page 181 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 37

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 3:46:28 AM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\030-3701.D) 3.451 4.505 5.788

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.806 - - - Fluoride 

 3.775 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\030-3701.D

Sample Name: U2 R1 *20 0310-96

Instrument 1 3/24/2010 1:56:01 PM ARM Page 1 of 2

EA# 0310-96 Page 182 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 37

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 3:57:16 AM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\030-3702.D) 3.512 4.560 5.850

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.806 - - - Fluoride 

 3.775 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\030-3702.D

Sample Name: U2 R1 *20 0310-96

Instrument 1 3/24/2010 1:56:13 PM ARM Page 1 of 2

EA# 0310-96 Page 183 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 38

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 4:08:04 AM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\031-3801.D) 3.451 4.499

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.806 - - - Fluoride 

 3.775 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\031-3801.D

Sample Name: U2 R2 *20 0310-96

Instrument 1 3/24/2010 1:56:29 PM ARM Page 1 of 2

EA# 0310-96 Page 184 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 38

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 4:18:51 AM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\031-3802.D) 3.450 4.503

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.806 - - - Fluoride 

 3.775 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\031-3802.D

Sample Name: U2 R2 *20 0310-96

Instrument 1 3/24/2010 1:57:22 PM ARM Page 1 of 2

EA# 0310-96 Page 185 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 39

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 4:29:40 AM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\032-3901.D) 3.449 4.501

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.806 - - - Fluoride 

 3.775 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\032-3901.D

Sample Name: U2 R3 *20 0310-96

Instrument 1 3/24/2010 1:57:33 PM ARM Page 1 of 2

EA# 0310-96 Page 186 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 39

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 4:40:27 AM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\032-3902.D) 3.447 4.503

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.806 - - - Fluoride 

 3.775 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\032-3902.D

Sample Name: U2 R3 *20 0310-96

Instrument 1 3/24/2010 1:57:44 PM ARM Page 1 of 2

EA# 0310-96 Page 187 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 40

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 4:51:16 AM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\033-4001.D)

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.806 - - - Fluoride 

 3.775 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\033-4001.D

Sample Name: FB *20 0310-96

Instrument 1 3/24/2010 1:58:06 PM ARM Page 1 of 2

EA# 0310-96 Page 188 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 40

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 5:02:04 AM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\033-4002.D)

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.806 - - - Fluoride 

 3.775 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\033-4002.D

Sample Name: FB *20 0310-96

Instrument 1 3/24/2010 1:58:19 PM ARM Page 1 of 2

EA# 0310-96 Page 189 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 43

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 5:56:02 AM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\034-4301.D)

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.806 - - - Fluoride 

 3.775 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\034-4301.D

Sample Name: RB H2SO4 *20 0310-96

Instrument 1 3/24/2010 1:59:07 PM ARM Page 1 of 2

EA# 0310-96 Page 190 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 43

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 6:06:50 AM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\034-4302.D)

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.806 - - - Fluoride 

 3.775 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\034-4302.D

Sample Name: RB H2SO4 *20 0310-96

Instrument 1 3/24/2010 1:59:16 PM ARM Page 1 of 2

EA# 0310-96 Page 191 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 8

Acq. Instrument : Smithers Location : -

Injection Date : 3/23/2010 5:20:15 PM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\007-0801.D)

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.806 - - - Fluoride 

 3.775 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\007-0801.D

Sample Name: 0.01N H2SO4/NaOH Blank

Instrument 1 3/24/2010 1:50:34 PM ARM Page 1 of 2

EA# 0310-96 Page 192 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 8

Acq. Instrument : Smithers Location : -

Injection Date : 3/23/2010 5:31:02 PM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\007-0802.D)

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.806 - - - Fluoride 

 3.775 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\007-0802.D

Sample Name: 0.01N H2SO4/NaOH Blank

Instrument 1 3/24/2010 1:50:45 PM ARM Page 1 of 2

EA# 0310-96 Page 193 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 32

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 1:58:30 AM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\093-3201.D)

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.806 - - - Fluoride 

 3.775 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\093-3201.D

Sample Name: 0.01N H2SO4/NaOH Blank

Instrument 1 3/24/2010 1:53:11 PM ARM Page 1 of 2

EA# 0310-96 Page 194 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 32

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 2:09:18 AM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\093-3202.D)

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.806 - - - Fluoride 

 3.775 - - - Chloride 

Totals : 0.00000

1 Warnings or Errors :

Warning : Calibrated compound(s) not found

=====================================================================

=====================================================================

 Area Percent Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\093-3202.D

Sample Name: 0.01N H2SO4/NaOH Blank

Instrument 1 3/24/2010 1:53:21 PM ARM Page 1 of 2

EA# 0310-96 Page 195 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 33

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 2:20:06 AM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\026-3301.D) 2.794 - Fluoride 3.743 - Chloride 5.086 5.763 6.233

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.794 BB 213.10400 1.55139e-2 3.30608 Fluoride 

 3.743 BB 110.73000 2.57113e-2 2.84702 Chloride 

Totals : 6.15310

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\026-3301.D

Sample Name: MS U1 R1 *20 0310-96

Instrument 1 3/24/2010 1:53:38 PM ARM Page 1 of 1

EA# 0310-96 Page 196 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 33

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 2:30:54 AM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\026-3302.D) 2.793 - Fluoride 3.742 - Chloride 5.085 5.762 6.232

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.793 BB 213.78407 1.55141e-2 3.31667 Fluoride 

 3.742 BB 110.83074 2.57110e-2 2.84957 Chloride 

Totals : 6.16624

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\026-3302.D

Sample Name: MS U1 R1 *20 0310-96

Instrument 1 3/24/2010 1:53:48 PM ARM Page 1 of 1

EA# 0310-96 Page 197 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 34

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 2:41:42 AM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\027-3401.D) 2.795 - Fluoride 3.743 - Chloride 5.087 5.763 6.233

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.795 BB 213.85445 1.55141e-2 3.31776 Fluoride 

 3.743 BB 110.87465 2.57109e-2 2.85069 Chloride 

Totals : 6.16845

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\027-3401.D

Sample Name: MSD U1 R1 *20 0310-96

Instrument 1 3/24/2010 1:54:09 PM ARM Page 1 of 1

EA# 0310-96 Page 198 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 34

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 2:52:29 AM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\027-3402.D) 2.794 - Fluoride 3.744 - Chloride 5.087 5.765 6.233

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.794 BB 213.30302 1.55140e-2 3.30918 Fluoride 

 3.744 BB 110.98945 2.57105e-2 2.85360 Chloride 

Totals : 6.16278

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\027-3402.D

Sample Name: MSD U1 R1 *20 0310-96

Instrument 1 3/24/2010 1:54:18 PM ARM Page 1 of 1

EA# 0310-96 Page 199 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 7

Acq. Instrument : Smithers Location : -

Injection Date : 3/23/2010 4:58:39 PM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\006-0701.D) 2.794 - Fluoride 3.769 - Chloride

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.794 BB 270.79840 1.55243e-2 4.20394 Fluoride 

 3.769 BB 147.50558 2.56262e-2 3.78001 Chloride 

Totals : 7.98396

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\006-0701.D

Sample Name: HPLC51pg56 #LCS

Instrument 1 3/24/2010 1:50:16 PM ARM Page 1 of 1

EA# 0310-96 Page 200 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 7

Acq. Instrument : Smithers Location : -

Injection Date : 3/23/2010 5:09:27 PM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\006-0702.D) 2.794 - Fluoride 3.768 - Chloride

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.794 BB 271.25171 1.55243e-2 4.21100 Fluoride 

 3.768 BB 147.51759 2.56262e-2 3.78032 Chloride 

Totals : 7.99132

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\006-0702.D

Sample Name: HPLC51pg56 #LCS

Instrument 1 3/24/2010 1:50:24 PM ARM Page 1 of 1

EA# 0310-96 Page 201 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 31

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 1:36:54 AM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\092-3101.D) 2.797 - Fluoride 3.744 - Chloride

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.797 BB 272.30817 1.55245e-2 4.22744 Fluoride 

 3.744 BB 148.21523 2.56250e-2 3.79802 Chloride 

Totals : 8.02546

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\092-3101.D

Sample Name: HPLC51pg56 #LCS

Instrument 1 3/24/2010 1:52:52 PM ARM Page 1 of 1

EA# 0310-96 Page 202 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 31

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 1:47:43 AM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\092-3102.D) 2.797 - Fluoride 3.743 - Chloride

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.797 BB 272.62543 1.55245e-2 4.23238 Fluoride 

 3.743 BB 148.30034 2.56249e-2 3.80017 Chloride 

Totals : 8.03255

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\092-3102.D

Sample Name: HPLC51pg56 #LCS

Instrument 1 3/24/2010 1:53:02 PM ARM Page 1 of 1

EA# 0310-96 Page 203 of 236
Calibration 

Curve Chromatograms

EA# 0310-96 Page 204 of 236
=====================================================================

 Calibration Table 

=====================================================================

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Calculate : External Standard

Based on : Peak Area

Rel. Reference Window : 10.000 %

Abs. Reference Window : 0.000 min

Rel. Non-ref. Window : 10.000 %

Abs. Non-ref. Window : 0.000 min

Use Multiplier & Dilution Factor with ISTDs

Uncalibrated Peaks : not reported

Partial Calibration : Yes, identified peaks are recalibrated

Correct All Ret. Times: No, only for identified peaks

Curve Type : Linear

Origin : Connected

Weight : Linear (Amnt)

Recalibration Settings: 

Average Response : Average all calibrations

Average Retention Time: Floating Average New 75%

Calibration Report Options :

 Printout of recalibrations within a sequence:

 Calibration Table after Recalibration

 Normal Report after Recalibration

 If the sequence is done with bracketing:

 Results of first cycle (ending previous bracket)

Signal 1: ADC1 B, ADC1 B, Metrohm

Signal 2: ADC1 A, ADC1 CHANNEL A

RetTime Lvl Amount Area Amt/Area Ref Grp Name 

 [min] Sig [ug/mL] 

-------|--|--|----------|----------|----------|---|--|---------------

 2.806 2 1 1.00000e-1 6.11878 1.63431e-2 Fluoride 

 2 9.99000e-1 70.82605 1.41050e-2 

 3 5.07600 354.18941 1.43313e-2 

 4 9.10000 597.66461 1.52259e-2 

 5 14.80000 907.06418 1.63164e-2 

 3.775 2 1 1.00000e-1 2.87020 3.48408e-2 Chloride 

 2 9.99000e-1 33.95667 2.94198e-2 

 3 5.07600 194.73593 2.60661e-2 

 4 9.10000 357.45839 2.54575e-2 

 5 14.80000 588.98598 2.51279e-2 

=====================================================================

 Peak Sum Table 

=====================================================================

***No Entries in table***

=====================================================================

Method U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Instrument 1 3/24/2010 1:26:45 PM ARM Page 1 of 2

EA# 0310-96 Page 205 of 236
=====================================================================

 Calibration Curves

=====================================================================

Amount[ug/mL]

0 10

Area

0

200

400

600

800

1

2

3

4

5

Fluoride at exp. RT: 2.806

ADC1 A, ADC1 CHANNEL A

Correlation: 0.99851

Residual Std. Dev.: 31.22675

Formula: y = mx + b

 m: 64.25766

 b: 6.62762e-1 

 x: Amount

 y: Area

Calibration Level Weights:

 Level 1 : 1

 Level 2 : 0.1001

 Level 3 : 0.019701

 Level 4 : 0.010989

 Level 5 : 0.006757

Amount[ug/mL]

0 10

Area

0

100

200

300

400

500

1

2

3

4

5

Chloride at exp. RT: 3.775

ADC1 A, ADC1 CHANNEL A

Correlation: 0.99973

Residual Std. Dev.: 5.19853

Formula: y = mx + b

 m: 39.41669

 b: -1.48998

 x: Amount

 y: Area

Calibration Level Weights:

 Level 1 : 1

 Level 2 : 0.1001

 Level 3 : 0.019701

 Level 4 : 0.010989

 Level 5 : 0.006757

=====================================================================

Method U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Instrument 1 3/24/2010 1:26:45 PM ARM Page 2 of 2

EA# 0310-96 Page 206 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 2

Acq. Instrument : Smithers Location : -

Injection Date : 3/23/2010 3:10:41 PM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\001-0201.D) 2.791 - Fluoride 3.771 - Chloride

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.791 BB 6.09814 1.41073e-2 8.60283e-2 Fluoride 

 3.771 BB 2.84644 3.86500e-2 1.10015e-1 Chloride 

Totals : 1.96043e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\001-0201.D

Sample Name: HPLC51pg56 #1

Instrument 1 3/24/2010 1:47:13 PM ARM Page 1 of 1

EA# 0310-96 Page 207 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 2

Acq. Instrument : Smithers Location : -

Injection Date : 3/23/2010 3:21:29 PM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\001-0202.D) 2.793 - Fluoride 3.773 - Chloride

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.793 BB 6.15458 1.41073e-2 8.68244e-2 Fluoride 

 3.773 BB 2.84985 3.86341e-2 1.10101e-1 Chloride 

Totals : 1.96926e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\001-0202.D

Sample Name: HPLC51pg56 #1

Instrument 1 3/24/2010 1:47:21 PM ARM Page 1 of 1

EA# 0310-96 Page 208 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 44

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 6:17:38 AM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\001-4401.D) 2.791 - Fluoride 3.761 - Chloride

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.791 BB 6.08988 1.41073e-2 8.59117e-2 Fluoride 

 3.761 BB 2.91406 3.83418e-2 1.11731e-1 Chloride 

Totals : 1.97642e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\001-4401.D

Sample Name: HPLC51pg56 #1

Instrument 1 3/24/2010 1:47:29 PM ARM Page 1 of 1

EA# 0310-96 Page 209 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 44

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 6:28:26 AM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\001-4402.D) 2.793 - Fluoride 3.766 - Chloride

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.793 BB 6.13252 1.41073e-2 8.65133e-2 Fluoride 

 3.766 BB 2.87045 3.85389e-2 1.10624e-1 Chloride 

Totals : 1.97137e-1

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\001-4402.D

Sample Name: HPLC51pg56 #1

Instrument 1 3/24/2010 1:47:37 PM ARM Page 1 of 1

EA# 0310-96 Page 210 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 3

Acq. Instrument : Smithers Location : -

Injection Date : 3/23/2010 3:32:16 PM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\002-0301.D) 2.789 - Fluoride 3.771 - Chloride 5.166 5.913 6.181

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.789 BB 70.84959 1.54168e-2 1.09227 Fluoride 

 3.771 BB 33.76752 2.64894e-2 8.94481e-1 Chloride 

Totals : 1.98675

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\002-0301.D

Sample Name: HPLC51pg56 #2

Instrument 1 3/24/2010 1:47:50 PM ARM Page 1 of 1

EA# 0310-96 Page 211 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 3

Acq. Instrument : Smithers Location : -

Injection Date : 3/23/2010 3:43:05 PM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\002-0302.D) 2.788 - Fluoride 3.768 - Chloride 5.162 5.909 6.183

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.788 BB 71.08764 1.54173e-2 1.09598 Fluoride 

 3.768 BB 33.87715 2.64858e-2 8.97263e-1 Chloride 

Totals : 1.99324

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\002-0302.D

Sample Name: HPLC51pg56 #2

Instrument 1 3/24/2010 1:47:58 PM ARM Page 1 of 1

EA# 0310-96 Page 212 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 45

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 6:39:13 AM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\002-4501.D) 2.790 - Fluoride 3.767 - Chloride 5.165 5.891 6.185

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.790 BB 70.53569 1.54161e-2 1.08739 Fluoride 

 3.767 BB 34.09715 2.64786e-2 9.02844e-1 Chloride 

Totals : 1.99023

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\002-4501.D

Sample Name: HPLC51pg56 #2

Instrument 1 3/24/2010 1:48:06 PM ARM Page 1 of 1

EA# 0310-96 Page 213 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 45

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 6:50:01 AM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\002-4502.D) 2.789 - Fluoride 3.768 - Chloride 5.172 5.904 6.172

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.789 BB 70.83129 1.54167e-2 1.09199 Fluoride 

 3.768 BB 34.08488 2.64790e-2 9.02533e-1 Chloride 

Totals : 1.99452

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\002-4502.D

Sample Name: HPLC51pg56 #2

Instrument 1 3/24/2010 1:48:15 PM ARM Page 1 of 1

EA# 0310-96 Page 214 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 4

Acq. Instrument : Smithers Location : -

Injection Date : 3/23/2010 3:53:53 PM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\003-0401.D) 2.795 - Fluoride 3.767 - Chloride 5.137 5.879 6.189

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.795 BB 351.93832 1.55330e-2 5.46667 Fluoride 

 3.767 BB 192.98418 2.55658e-2 4.93380 Chloride 

Totals : 10.40047

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\003-0401.D

Sample Name: HPLC51pg56 #3

Instrument 1 3/24/2010 1:48:24 PM ARM Page 1 of 1

EA# 0310-96 Page 215 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 4

Acq. Instrument : Smithers Location : -

Injection Date : 3/23/2010 4:04:41 PM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\003-0402.D) 2.841 - Fluoride 3.822 - Chloride 5.197 5.944 6.249

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.841 BB 357.80850 1.55335e-2 5.55803 Fluoride 

 3.822 BB 195.88971 2.55629e-2 5.00752 Chloride 

Totals : 10.56554

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\003-0402.D

Sample Name: HPLC51pg56 #3

Instrument 1 3/24/2010 1:48:32 PM ARM Page 1 of 1

EA# 0310-96 Page 216 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 46

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 7:00:50 AM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\003-4601.D) 2.795 - Fluoride 3.770 - Chloride 5.158 5.895 6.171

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.795 BB 353.74982 1.55332e-2 5.49486 Fluoride 

 3.770 BB 195.05389 2.55638e-2 4.98631 Chloride 

Totals : 10.48117

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\003-4601.D

Sample Name: HPLC51pg56 #3

Instrument 1 3/24/2010 1:48:41 PM ARM Page 1 of 1

EA# 0310-96 Page 217 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 46

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 7:11:37 AM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\003-4602.D) 2.794 - Fluoride 3.771 - Chloride 5.166 5.906 6.160

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.794 BB 353.26099 1.55331e-2 5.48726 Fluoride 

 3.771 BB 195.01593 2.55638e-2 4.98535 Chloride 

Totals : 10.47260

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\003-4602.D

Sample Name: HPLC51pg56 #3

Instrument 1 3/24/2010 1:48:49 PM ARM Page 1 of 1

EA# 0310-96 Page 218 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 5

Acq. Instrument : Smithers Location : -

Injection Date : 3/23/2010 4:15:29 PM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\004-0501.D) 2.800 - Fluoride 3.766 - Chloride 5.125 5.868 6.189

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.800 BB 597.61945 1.55451e-2 9.29005 Fluoride 

 3.766 BB 356.49597 2.54760e-2 9.08209 Chloride 

Totals : 18.37214

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\004-0501.D

Sample Name: HPLC51pg56 #4

Instrument 1 3/24/2010 1:48:57 PM ARM Page 1 of 1

EA# 0310-96 Page 219 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 5

Acq. Instrument : Smithers Location : -

Injection Date : 3/23/2010 4:26:16 PM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\004-0502.D) 2.800 - Fluoride 3.768 - Chloride 5.131 5.874 6.190

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.800 BB 596.18506 1.55450e-2 9.26772 Fluoride 

 3.768 BB 356.59222 2.54760e-2 9.08453 Chloride 

Totals : 18.35226

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\004-0502.D

Sample Name: HPLC51pg56 #4

Instrument 1 3/24/2010 1:49:06 PM ARM Page 1 of 1

EA# 0310-96 Page 220 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 47

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 7:22:24 AM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\004-4701.D) 2.799 - Fluoride 3.771 - Chloride 5.160 5.904 6.157

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.799 BB 598.91089 1.55451e-2 9.31014 Fluoride 

 3.771 BB 358.35028 2.54754e-2 9.12913 Chloride 

Totals : 18.43928

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\004-4701.D

Sample Name: HPLC51pg56 #4

Instrument 1 3/24/2010 1:49:17 PM ARM Page 1 of 1

EA# 0310-96 Page 221 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 47

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 7:33:13 AM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\004-4702.D) 2.800 - Fluoride 3.774 - Chloride 5.169 5.915 6.147

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.800 BB 597.94305 1.55451e-2 9.29508 Fluoride 

 3.774 BB 358.39508 2.54754e-2 9.13027 Chloride 

Totals : 18.42535

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\004-4702.D

Sample Name: HPLC51pg56 #4

Instrument 1 3/24/2010 1:49:26 PM ARM Page 1 of 1

EA# 0310-96 Page 222 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 6

Acq. Instrument : Smithers Location : -

Injection Date : 3/23/2010 4:37:04 PM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\005-0601.D) 2.808 - Fluoride 3.768 - Chloride 5.865 6.191

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.808 BB 904.42017 1.55509e-2 14.06459 Fluoride 

 3.768 BB 587.19165 2.54343e-2 14.93483 Chloride 

Totals : 28.99942

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\005-0601.D

Sample Name: HPLC51pg56 #5

Instrument 1 3/24/2010 1:49:35 PM ARM Page 1 of 1

EA# 0310-96 Page 223 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 6

Acq. Instrument : Smithers Location : -

Injection Date : 3/23/2010 4:47:52 PM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\005-0602.D) 2.807 - Fluoride 3.766 - Chloride 5.118 5.861 6.194

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.807 BB 905.61633 1.55510e-2 14.08320 Fluoride 

 3.766 BB 588.26648 2.54342e-2 14.96210 Chloride 

Totals : 29.04530

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\005-0602.D

Sample Name: HPLC51pg56 #5

Instrument 1 3/24/2010 1:49:46 PM ARM Page 1 of 1

EA# 0310-96 Page 224 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 48

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 7:44:01 AM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\005-4801.D) 2.807 - Fluoride 3.775 - Chloride 5.162 5.912 6.148

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.807 BB 908.30072 1.55510e-2 14.12498 Fluoride 

 3.775 BB 590.09827 2.54340e-2 15.00857 Chloride 

Totals : 29.13355

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\005-4801.D

Sample Name: HPLC51pg56 #5

Instrument 1 3/24/2010 1:49:54 PM ARM Page 1 of 1

EA# 0310-96 Page 225 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 48

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 7:54:49 AM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\005-4802.D) 2.806 - Fluoride 3.775 - Chloride 5.167 5.919 6.139

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.806 BB 909.91949 1.55510e-2 14.15017 Fluoride 

 3.775 BB 590.38751 2.54340e-2 15.01591 Chloride 

Totals : 29.16608

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\005-4802.D

Sample Name: HPLC51pg56 #5

Instrument 1 3/24/2010 1:50:06 PM ARM Page 1 of 1

EA# 0310-96 Page 226 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 17

Acq. Instrument : Smithers Location : -

Injection Date : 3/23/2010 8:34:36 PM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\090-1701.D) 2.795 - Fluoride 3.755 - Chloride 5.089 5.818 6.204

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.795 BB 353.08353 1.55331e-2 5.48449 Fluoride 

 3.755 BB 193.78250 2.55650e-2 4.95406 Chloride 

Totals : 10.43855

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\090-1701.D

Sample Name: HPLC51pg56 #3

Instrument 1 3/24/2010 1:51:05 PM ARM Page 1 of 1

EA# 0310-96 Page 227 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 17

Acq. Instrument : Smithers Location : -

Injection Date : 3/23/2010 8:45:23 PM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\090-1702.D) 2.796 - Fluoride 3.754 - Chloride 5.808 6.209

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.796 BB 352.39661 1.55331e-2 5.47380 Fluoride 

 3.754 BB 193.77600 2.55650e-2 4.95389 Chloride 

Totals : 10.42769

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\090-1702.D

Sample Name: HPLC51pg56 #3

Instrument 1 3/24/2010 1:51:17 PM ARM Page 1 of 1

EA# 0310-96 Page 228 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 29

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 12:53:43 AM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\090-2901.D) 2.796 - Fluoride 3.741 - Chloride 5.036 5.742 6.225

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.796 BB 353.42969 1.55332e-2 5.48988 Fluoride 

 3.741 BB 194.13525 2.55647e-2 4.96300 Chloride 

Totals : 10.45289

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\090-2901.D

Sample Name: HPLC51pg56 #3

Instrument 1 3/24/2010 1:52:06 PM ARM Page 1 of 1

EA# 0310-96 Page 229 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 29

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 1:04:31 AM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\090-2902.D) 2.797 - Fluoride 3.742 - Chloride 5.037 5.744 6.227

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.797 BB 352.92029 1.55331e-2 5.48195 Fluoride 

 3.742 BB 194.20056 2.55646e-2 4.96466 Chloride 

Totals : 10.44662

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\090-2902.D

Sample Name: HPLC51pg56 #3

Instrument 1 3/24/2010 1:52:16 PM ARM Page 1 of 1

EA# 0310-96 Page 230 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 41

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 5:12:51 AM Inj : 1

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\100-4101.D) 2.795 - Fluoride 3.740 - Chloride 5.044 5.746 6.220

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.795 BB 352.20810 1.55331e-2 5.47087 Fluoride 

 3.740 BB 194.22064 2.55646e-2 4.96517 Chloride 

Totals : 10.43604

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\100-4101.D

Sample Name: HPLC51pg56 #3

Instrument 1 3/24/2010 1:58:31 PM ARM Page 1 of 1

EA# 0310-96 Page 231 of 236
=====================================================================

Acq. Operator : EO Seq. Line : 41

Acq. Instrument : Smithers Location : -

Injection Date : 3/24/2010 5:23:39 AM Inj : 2

Acq. Method : H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Last changed : 2/23/2010 8:12:27 AM by mgb

Analysis Method : U:\HPLC2010Q1\SMITHERS\METHODS\HPLC51PG56.M

Last changed : 3/24/2010 11:55:00 AM by ARM

2 3 4 5 6 7 8 min

μS/cm

0

20

40

60

80

100

 ADC1 A, ADC1 CHANNEL A (U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\100-4102.D) 2.796 - Fluoride 3.742 - Chloride 5.047 5.749 6.223

=====================================================================

 External Standard Report 

=====================================================================

Sorted By : Signal

Calib. Data Modified : Wednesday, March 24, 2010 11:54:54 AM

Multiplier : 1.0000

Dilution : 1.0000

Use Multiplier & Dilution Factor with ISTDs

Signal 1: ADC1 A, ADC1 CHANNEL A

RetTime Type Area Amt/Area Amount Grp Name

 [min] [μS/cm*s] [ug/mL] 

-------|------|----------|----------|----------|--|------------------

 2.796 BB 351.85950 1.55330e-2 5.46545 Fluoride 

 3.742 BB 194.21121 2.55646e-2 4.96493 Chloride 

Totals : 10.43038

=====================================================================

 *** End of Report ***

Data File U:\HPLC2010Q1\SMITHERS\DATA\MAR\HPLC51PG56\100-4102.D

Sample Name: HPLC51pg56 #3

Instrument 1 3/24/2010 1:58:39 PM ARM Page 1 of 1

EA# 0310-96 Page 232 of 236
 Method Information

 Method: H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

 Modified: 2/23/2010 at 8:12:27 AM

=========================================================================

 ANALOG DIGITAL CONVERTER

=========================================================================

 Signal 1

 ---------------------

Description: ADC1 CHANNEL A

Source: Signal

Unit: μS/cm

Units/Volt: 100.000

Peakwidth (Data Rate): 0.027 Min (10.00 Hz)

Stop Time: No Limit

Data Storage: All

Start Signal Source: External Device Will Start 35900

Timed Event Table:

 <no events>

 method: H:\HPLC2010Q1\SMITHERS\METHODS\METROHM.M

Modified on: 2/23/2010 at 8:12:27 AM

Smithers 3/16/2010 1:54:21 PM KHB/EO Page 1 of 1

EA# 0310-96 Page 233 of 236
Sequence Table:

 Method and Injection Info Part:

 Line Location SampleName Method Inj SampleType InjVolume

 DataFile AutoBalance LimsID

 ==== ======== ==================== ==================== ======== ========== =========

 1 Vial 127 DI Rinse METROHM 4 Sample 

 

 2 Vial 1 HPLC51pg56 #1 METROHM 2 Sample 

 3 Vial 2 HPLC51pg56 #2 METROHM 2 Sample 

 4 Vial 3 HPLC51pg56 #3 METROHM 2 Sample 

 5 Vial 4 HPLC51pg56 #4 METROHM 2 Sample 

 6 Vial 5 HPLC51pg56 #5 METROHM 2 Sample 

 7 Vial 6 HPLC51pg56 #LCS METROHM 2 Sample 

 8 Vial 7 0.01N H2SO4/NaOH Blank METROHM 2 Sample 

 9 Vial 8 KR-031810-11 *20 0310-117 METROHM 2 Sample 

 10 Vial 9 MS KR-031810-11 *20 0310-117 METROHM 2 Sample 

 11 Vial 10 MSD KR-031810-11 *20 0310-117 METROHM 2 Sample 

 12 Vial 11 KR-031810-12 *20 0310-117 METROHM 2 Sample 

 13 Vial 12 KR-031810-13 *20 0310-117 METROHM 2 Sample 

 14 Vial 13 KR-031810-14 *20 0310-117 METROHM 2 Sample 

 15 Vial 14 U9 R1 *20 0210-93 METROHM 2 Sample 

 16 Vial 15 MS U9 R1 *20 0210-93 METROHM 2 Sample 

 17 Vial 90 HPLC51pg56 #3 METROHM 2 Sample 

 18 Vial 91 HPLC51pg56 #4 METROHM 2 Sample 

 19 Vial 16 MSD U9 R1 *20 0210-93 METROHM 2 Sample 

 20 Vial 17 U9 R2 *20 0210-93 METROHM 2 Sample 

 21 Vial 18 U9 R3 *20 0210-93 METROHM 2 Sample 

 22 Vial 19 U10 R1 *20 0210-93 METROHM 2 Sample 

 23 Vial 20 U10 R2 *20 0210-93 METROHM 2 Sample 

 24 Vial 21 U10 R3 *20 0210-93 METROHM 2 Sample 

 25 Vial 22 RB DI H2O 0210-93 METROHM 2 Sample 

 26 Vial 23 RB H2SO4 *20 0210-93 METROHM 2 Sample 

 27 Vial 24 FB *20 0210-93 METROHM 2 Sample 

Sequence: U:\HPLC2010Q1\SMITHERS\SEQUENCE\HPLC51PG56.S

Instrument 1 3/24/2010 2:03:12 PM ARM Page 1 of 2

EA# 0310-96 Page 234 of 236
 Line Location SampleName Method Inj SampleType InjVolume

 DataFile AutoBalance LimsID

 ==== ======== ==================== ==================== ======== ========== =========

 28 Vial 25 U1 R1 *20 0310-96 METROHM 2 Sample 

 

 29 Vial 90 HPLC51pg56 #3 METROHM 2 Sample 

 30 Vial 91 HPLC51pg56 #4 METROHM 2 Sample 

 31 Vial 92 HPLC51pg56 #LCS METROHM 2 Sample 

 32 Vial 93 0.01N H2SO4/NaOH Blank METROHM 2 Sample 

 33 Vial 26 MS U1 R1 *20 0310-96 METROHM 2 Sample 

 34 Vial 27 MSD U1 R1 *20 0310-96 METROHM 2 Sample 

 35 Vial 28 U1 R2 *20 0310-96 METROHM 2 Sample 

 36 Vial 29 U1 R3 *20 0310-96 METROHM 2 Sample 

 37 Vial 30 U2 R1 *20 0310-96 METROHM 2 Sample 

 38 Vial 31 U2 R2 *20 0310-96 METROHM 2 Sample 

 39 Vial 32 U2 R3 *20 0310-96 METROHM 2 Sample 

 40 Vial 33 FB *20 0310-96 METROHM 2 Sample 

 41 Vial 100 HPLC51pg56 #3 METROHM 2 Sample 

 42 Vial 101 HPLC51pg56 #4 METROHM 2 Sample 

 43 Vial 34 RB H2SO4 *20 0310-96 METROHM 2 Sample 

 44 Vial 1 HPLC51pg56 #1 METROHM 2 Sample 

 45 Vial 2 HPLC51pg56 #2 METROHM 2 Sample 

 46 Vial 3 HPLC51pg56 #3 METROHM 2 Sample 

 47 Vial 4 HPLC51pg56 #4 METROHM 2 Sample 

 48 Vial 5 HPLC51pg56 #5 METROHM 2 Sample 

Sequence: U:\HPLC2010Q1\SMITHERS\SEQUENCE\HPLC51PG56.S

Instrument 1 3/24/2010 2:03:12 PM ARM Page 2 of 2

EA# 0310-96 Page 235 of 236
This Is The Last Page

Of This Report.

EA# 0310-96 Page 236 of 236