# • cargIll 

# '" ." Sioux City, IA Emission Test**R~port** 

# December 2005 

# •

- Thompson Environmental Consulting, Inc. "

a member of THE COMPUI\NCE GROUP 

# •
Environmental Engineering. Permi.tting and 

### Compliance Services

## -

# .•

EMISSION TEST REPORT for Cargill Incorporated

. located in 

### Sioux City, Iowa on December 12-15,2005



### Conducted by 

### Comprehensive Emission**Services~** 

# me. P.O. Box 

### 910 Waukee, Iowa 

### 50263 (515) 987-0200 Project No. 11805


# •

# • . TABLE OF CONTENTS

CONTENTS
Preface
....................................................................... :.................................................2 Introduction
................................................................................................................ 3 Swnmary of Results
............................................................................................... :.... 

### 4 Sampling and Analytical Procedures
......................................................................... 

### 6 Ml7 Sampling Apparatus
.......................................................................................... 7 Test Results
................................................................................................................. 8
Appendix A

- Example Calculations Appendix 

### B**~** 

### Laboratory Data Forms AppendixC -Field Data Forms Appendix D - Pretest Calibrations Appendix E - Postiest Calibrations Appendix F

- Process Data
. Appendix 

### G - Opacity Certification 

### TABLES
Table 1, Swnmruy of Test Results for the Bean Dust Bagfilter (EP 2)
.................... 

### .4 Table 2, Summary ofTest Results for the West Grain Filter (EP 1)
......................... 5 Table 3, Test Results for the Bean Dust Bagfilter (EP 2)
.......................................... 8 Table 4, Test Results for the West Grain Filter (EP 1)
.............................................. 9



### FIGURES
Figure 

### 1, M17 Sampling Apparatus
........ , ..................................................................7 

# •

# • PREFACE
This report summarizes the results of the data collected for compliance testing performed at the Cargill Incorporated facility in Sioux City, Iowa; To the best of our knowledge, the data 

### in this report 

## are accurate and complete. Any questions concerning this report should be directed to 

### Mr. Tim Titus or 

### Mr. Jay Titus. They may be reached by phone at 

### (515) 987-0200. 

# ---------_.. , 

### Jay 

### Titus Test Leader'.



# tit De,cember 

### 27, 2005

2

# • INTRODUCTION
An 

### emission test was conducted by Comprehensive Emission Services on the Bean Dust

. Bagfilter (EP 2) and the West Grain Filter (EP 1) at the Cargill Incorporated facility in

Sioux City, Iowa. Three Method 17 with 202 backhalfparticulate sampling runs and three Method 9, Opacity runs were performed. PMlO emissions wiUhave to be derived from the PM samples for this source. The iesting fulfills the requirements for testing in the IDNR Permit**#95~A·324-S8** 

### and #95-A-323-S8. The testing was performed on December 12-15,2005.
Coordinating the field tests: Tim Titus

- Comprehensive Emission Services, Inc. Matt Pearson

- Cargill Incorporated Lisa Schmidt

- Thompson Environmental Consulting) Inc. Conducting the field tests: Jay Titus

- Comprehensive Emission Services, Inc. Mason Woltz

- Comprehensive Emission Services, Inc. Witnessing the field tests:
Mark Stone

- Iowa Department of Natural Resources

The appendices to this report contain the followip.g information and data: Appendix A: Example Calculations Appendix B: Laboratory Data Forms Appendix C: Field Data Forms

. Appendix D: Pretest Calibrations

Appendix E: Posttest Calibrations Appendix F: Process Data Appendix G: Opacity Certification 

# •

3

### SUMMARY OF RESULTS
In 

### accordance with current IDNR protocol, when .less than 10 mg of sample is collected, 10 mg of sample catch is used for calculations. Sources with 

### sample collections less than 10 mg are shown with a '<'symbol in the following tables to indicate that actual samples

. were less than the assumed 10 mg catch. Both the actual and the assumed emission rates can be found in Appendix C:


### Table 1 summarizes the test results for testing performed on the Bean Dust Bagfilter (EP 2). Three Method 17 with 202 backhalf particulate sampling runs and three Method 9, Opacity runs were performed. PM lO 

### emissions will have to be derived from the PM samples for this source. The testing fulfills the requirements for testing in the IDNR Perniit #95-A-324-S8. The testing was performed on December 12-14,2005. 

### The allowable limit for PMIO is 0.76 lblhr, The allowable limit Opacity is 0%.
No blank corrections were performed. Table 1 

### Summary of 

### Test Results Bean Dust Bagfilter (EP 2) 

### units Run 1 Run 2 Run 3 PM Net Weight g 

### <0.0100 <0.0100 <0.0100

PM Emission gr/dscf <0.0009 <0.0009 <0.0009 PM Emission Rate lblhr <0.22 : <0.22 <0.22 Flow Rate acfm 28,086 27,533 28,031 Flow Rate dscfm 27,986 27,239 27,845 I 

### Isokinetics % 

### 98.6 99.1 98.7 Start Time HH:MM 15:21-7:55 10:18 14:49-7:53 Stop Time HH:MM 

### 17:21-9:55 14:26 16:49-9:53 Run Date mm/dd/yr 12/12&13/05 12/13/05 12/13&14105 

### units Run 1 Run 2 Run 3 Opacity % 

### 0.0 0.0 0.0 Start Time HH:MM 

### 15:30 8:00 10:20 Stop Time HH:MM·· 

### 16:30 9:00 11:20 Run Date mmlddlyr 12112/05 .12/13/05 12/13/05

4 

## I

### Table 2 summarizes the test results for testing performed on the West Grain Filter (EP 1). 

# e. Three Method 17 with 202 backhalfparticulate sampling runs were performed. PMlO emissions will have to be derived from the PM samples for this source. Opacity could not be performed on this source do to steam from another source that interfered with the Opacity reader's ability to see the stack clearly. The Opacity requirement in the permit was waived in the field by Mr. Mark Stone of the IDNR. The testing fulfills the
.

.requirements for testing in 

### the IDNR Permit #95-A-323-S8. The testing was performed on December 14 and 15,2005.
The allowable limit for PM lO 

### 0.60 lblhr.

Table 2 Summary 

### of Test Results West Grain Cleaner 

### PI PM Net Wei ht

PM Emission PM Emission Rate Flow Rate FiowRate Isokinetic8 Start Time Time Run Date units

acfm dscfm

% HH:MM 

### HH:MM mmlddlyr Run 1 <0.0100
. <0.0009

<0.17 21,367 21,518

99.3 12:09 16:12 12/14/05 

### R1lll2 <0.0100 <0.0009

<0.17 21,198 21,830

99.0 7:53 12:07 12/15/05 

### 17:22 12/15/05 

# e



# •

5

# • SAMPLING AND ANALYTICAL PROCEDURES 

### Sampling Procedures
Particulate emissions were deterrp.ined by U.S. Environmental :protection Agency (EPA)

.Methods 1, 2, 3, 4, 17, 202 and 9. These Methods are titled;
Method 1 • "Sample and Velocity Traverse for Stationary Sources" Method 2 - "Determination of Stack Gas Velocity and Volumetric Flow Rate" Method 3 - "Gas Analysis for Carbon Dioxide, Oxygen, Excess Air and Dry
. Molecular Weight" Method 4 - "Determfuation tor Moisture Content in Stack Gases" Method 17

- "Determination of Particulate Emissions from Stationary Sources (In-Stack Filtration Method)" Method 202 '. "Condensible Particulate Emissions" Method 9 - "Detennination of Visual Emissions from Stationary Sources"
These methods appear in detail inTitle 40, Code of Federal Regulations (CFR). Part 60,

. Appendix A.


### The Sampling Apparatus is shown in Figure 1 on Page 6. All equipment was calibrated at Comprehensive Emission Services' office prior 

### to shipment to the test site.
. 

### Sampling Locations A total of 24 sample points were used to determine particulate emissions. The sample time per point was 10 minutes, for a total sampling time of 240 minutes per test run. The stack sampling point locations canbe found along with the field data sheets 

### in Appendix 

### C. Analytical Procedures The particulate emission rate 

### was detennined following procedures detailed 

### in EPA' Methods 17 and 202. Particulate samples collected on Whatman glass fiber fllters were analyzed gravimetrically. The probe and nozzles were rinsed with acetone. The rinse 

### was transferred to tarred beakers and evaporated to dryness. The back-half water was· collected and separated into organic and in-organic parts. The samples were then transferred to tarred beakers and evaporated to dryness:

6

# • Table 3 Particulate Emission Results

Bean Dust Basrfilter (EP 21 

### Parameters PM Emissions Weight Collected Actual Emission Rate Stack Flow Rates Velocity

Actual Standard Conditions t"I 

### -" n 

### Isokinetics Sample Volume Ave. Stack Temperature

-

Ave. Square Root AP Ave. ilH 

### Ave. Meter Temperature Oxygen Carbon Dioxide Moisture Collected Moisture Start Time Stop Time " Run Date Sampling Time

s 

### Opacity Start Time Stop Time Run Date Sampling Time Units Run 1 g <0.0100 gr/dscf <0.0009



### Ib/hr <0.22 ftlmiti 7,064 

### acfm 28,086 dscfm 27,9-86

# ~6 100

of 66**inchesH~O** 

### 2.0985 inches H20 

### 1.62 of 7.6 % 

### 21.00 % 

### 0.00 

### m1 35".0 % 

### H20 

### 1.0 HH:MM 

### 15:21-7:55 HH:MM 

### "17:21-9:55 mmldd/yr" 12112&13/05

minutes 240

Units 1



### % 

### .0 HH:MM 

### 15:30 mmlddlyr "12/12/05

minutes 60 Run 2 Run 3 

## , <0.0100 <0.0100

<0.0009 <0.0009

<0.22 <0.22 6,925 7,050 27,533 28,031 27,239 27,845

99.1 98.7 162.468 165.330 69 67 2.0504
_ 2.09i.U

1.56 1.61 53.9 48.9 21.00 21.00 0.00 0.00 37.0 36.0 ""

1.1 1.0 10:18 14:49-7:53 14:26**16:49~9:53** 

### 12/13105 12/13&14/05 240 240 Run 2 Run 3

0.0 0.0 8:00 9:00 11:20 12/13105 12/13/05
. 60 60 

# •

8

### Table 4 Particulate 

### Emission Results West Grain Cleaner (EP 1) Parameters 

### Units Run 

### 1 Run 

### 2 Run 3 PM Emissions Weight Collected g 

### <0..0.10.0. <0..0.10.0. <0..010.0 ACtual gr/dscf 

### <0..00.0.9 <0..0.0.0.9 <0..0.0.0.9 Emission Rate 

### Iblhr <0.17 

### <0..17
. <0..17**S~ck** 

### Flow Rates Velocity
. ftlmin 

### 2,941 2,917 21,198 

### 21,830. 

# Ai=**21;64~** . Actual acfm 

### 21,367 Standard Conditions dscfm 

### 21,518 Sampling Results Isokinetics % 

### 993 

### 99.0. 99.1 

### Sample Volume 'dscf 

### 165.461 

### 167.310. 166.0.84 Ave. Stack Temperature OF 

### 53 43 ·43

Ave. Square Root AP inches H2O 

### 0..8780. 0..880.9 0..8736 Ave. 

### Ali inches H 2

### 0 

### 1.70. 1.71 1.71 Ave. Meter Temperature OF 

### 61.6 54.9 61.5 Oxygen % 

### 21.0.0. 21.0.0. 21.QD Carbon Dioxide % 

### 0.0.0. 0..0.0. 0..0.0. Moisture Collected 

### m1 32.0. 41.0. 39.5 Moisture % 

### H20 

### 0..9 0..9 0..9 Run Start Time HH:MM 

### 12:0.9 7:53 12:35 Run Stop Time 

### I HH:MM 

### 16:12 

### 12:0.7 17:22 Run Dat.e mmlddlyr


### . 12114/0.5 12/15/0.5 12115/0.5 Sampling Time minutes 

### 240. 240 

### 240.

9

# • Appendix A Example Calculations 

# •

•

### Symbol 

### Qa As Bws Cp Cstd Dn dscfm g gr/dscfm 

### ID 

### Md Ms Qstd Pb Ps 

# .- SP Tm 

### Ts Vi Vf Vm Vmstd Vs We Wtgain y 

# e .%&0

% C02 %02 %1 

### AH bP 

## NOMENCLATURE Description Actual cubic feet per minute Area of stack Percent water Pitot tube calibration coefficient Concetration ofparticulate dry basis, standard conditions Diameter ofnozzle 

### Dry standard cubic feet per minute Grams Grains per 

### dry standard cubic feet per minute Inside diameter of stack MolecUlar weight, 

### dry stack gas Molecular weight, stack gas Stack flow rate, 

### dry standard conditions Barometric Pressure Stack pressure Static pressure Average meter temperature Temperature of stack gas Initial meter reading Final mete:t;' reading Volume meter, 

### actual Vohune meter, standard conditions Average stack gas velocity Total moisture collected Total particulate matter collected Meter condition factor Sampling time Percent moisture by volume Percent carbon dioxide by volume, 

### dry Percent oxygen by volume, 

### dry Percent isokinetic • Pressure drop across orifice meter

Gas velocity pressure

### ------- "- .'-"_.-.-'--'


### PARTICULATE CALCULATION EQUATIONS 

### Runl 

# • 1. Volume of meter



# v,,, =(807.004-647.700)xO.999 

# v., = 159.145 

### ft3
2. Volume of meter, standard conditions (68' ,29.92 

### in.Hg)

_ T", +460

-	 ' ( 1.62) 17.65x159.145x 29.90+­ 

## V
_**13~**

",(sid)

- 

### 47.6+460
Vm{std) 

## = 166.100 ft3 3. 

### Percent moisture by 

### volume 100 X 

### 0.4707 X 

### We**B~==-------~**


### B

ws 

### B",_, 

### 4. 0.04707 X 

### We + V,1I{.,'ld)

== 

### 100 X 

### 0.4707 X 

### 35.0 0.04707 X 

### 35.0 + 166.100

== 

### 1.0 % 

### Molecular weight, dry 

### stack 

### gas

MtI 

### ==0.16xO.00+21.00+28.0

### 5. Molecular weight, stack g 

# • M == 

### M 

# X(l Bws 

# )+18X(1- Bw .,) s d 

### 100 100

. (. 1.0) (1.0 ) 

### M ==28.84x 1-- +18x 1-­ s . 

### 100 100 

### M .• 

## = 28.73 

### 6. Stack Pressure 

## SP P 

### =P. 

## +-.

·t b 

### 13.6


### P = 

### 29.90+ 1.30



### .. 13.6 

## P.. = 

### 30.00 

### inch. 

### Hg 

# • 7. Velocity of stack gas


### + 460 

# (JA::\ v.. == 

### 60 x 85.349 xC

### p x 

### P + M x '\j 

### /!.p 

### J""g**.~** .r 

### 66+460

. V.= 

### 60x85.349.xO.84x x 

### 2.0985 30.00 

### + 28.73 

### Vs == 7,064 

### ftlmin



### . 8. Percent isokinetic 100x 

### %I == 

### 24 

# • % 

### I 

## =

____ . _10_O_x-,(6_6_+_4_6"",",0

### ),--x_l_66_.l_0_0_~_--:: 17.65 x 240x 7,064 x 30.00x 

# (1- 1.0)x 

### 7t:X (0.135)2 100. 24'**----~,:.-----'-'---''----** 

### 17.65xBxV s 

### xP( 

# X(I- Bws)x7t:x(Dn)2.

. 100

%1 == 

### 98.6

### 9. Area of stack 

# • IDJ2 A 

### == 1CX 

# (

­



### " 24·.
A. 

## = 1C 

### X(27.00J2

, 24

10. 

### Stack volumetric flow rate actual conditions



### Qa = 7,064x3.98 

### Qa 

## = 28,086 acfm 11. Stack volumetric flowrate, standard conditions (68 0 ,29.92 

### in.Hg) 

# • 17.65 x 

### Vs x 

### As x 

### P a X 

### (1 -'- 

### Bws)

. 100 QSld 

## = 

# ----r-. -+-4-6-0---'----'­

. 1--'­ 17.65x7,064x3.98x30.00x (10) 100
. 

### Qstd == 

### -----6-6-+-4-60---'--------'--­
Q'.ld 

### = 27,986 dscfm 12. Grains per dry 

### standard cubic feet 15.43 x Wt gain 

### C s1d 

### == V;1I(std}


### C 

### 15.43x 0.0072

Sld 

### == 

### 166.100 

# • :::: 0 .0007 gr/dscf C l1d

### 13. Emission rate 

# • lb 60x Wtgain x. Qstd == 

### hr 453.5924x Vm(std) 

### lb 60x 0.0072 x 27,986 == 

### hr 453.5924 x 166.100 Ib 

## = 0.16Ib/hr hr


# •

•

# AppendixB Laboratory Data Forms.**~** 

# ..

# • Project Number: ,..-.

## ...J.j1l1.lo~6'-ro_7_"- _____ 

### Plant Name:

### ~C:.:a;...I",t...;I;....;' I..;..l

______ 

### Date:. 

### /i?-/I.; -():5 Analysis Type: 

### J2? 

## /1-/2 J2



# •

Identification

. F= 3 inch filter P = 47mm filter B = 150ml Beaker 

## c = 250ml Beaker D = 400ml Beaker·

Run! Type Identification Final Tare Net Number Weight Weight Weight Filter 

## P)ft; 

# 15**z·~S" ~·56lt,!.{**  

## . ,1)0 

## I 

# t Probe Rinse ( ml) 

# f,"57-95 

# 1-B.?9;L/ 1B. 

# <J<JZ(, ItJOO{5 Front HalfWeight 

## .OOr<jOrganic. ( ml) 

# e 'io l/D IO'/5tJ3$' /0£/ 

# sen J 

## OD 

# '2- 2..
. Inorganic 

# o 38g2. 

# /f{o. 

# eN1- 

# /1t.o. 

# firl (P 

## flD 

## 3 

## I Total Net Weight 

## .DDi-Z. Rw2 Type Identification Final Tare Net Number Weight Weight Weight Filter' 

# f /& 

## 19'**2.51/~** 

## :;;·5"11:;- ,!lDO 0 Probe Rinse ( ml) 

## B 57--9& 

# &'1· 89(lL 

# !P1-. 

# B9"3**~o()O** C Front Half Weight 

# , ou c 0 Organic ( ml) 

### t 

## L/tJ,/

# I 

# JIJIt,. 0·-'; iz3 

# It/ft,· t?15$ I 

## 000'5 Inorganic 

# 1> 3t3S3 

# /31.**~5~** 

## I 

# /3'1. 

# 5S3S I 

### poZ(P

. Total Net Weight 

### .OD3 ( Run 3 Type Identification Final Tare Net Number Weight Weight Weight Filter 

# f /&20 

# 2.. 

# &ct./J :J. (po 

## 1./**~** I , 

### 0000

# I~ ml) 

# B3 }--97-

## {P1./f.t-~ 

## to1;. 

## (1-50 t 

### 0000 Front HalfWeight 

## DODD c Organic ( ml) 

## C qO'-/L 

# /01. 

# S'oL{9= fIJI. 501 

# e, .00 

## t \ Inorganic 

## D 

# 3&tlLf 

# I r8. 3l'1;f 

# l?-ro·32-Q\ ·,OOOt./ Total Net Weight 

### ;OO'S'

### Project NlImber: 

### --L./L..;/ B;;....,

### _11_5.---.;

____ Plant Name:**~C=4.c....:Mr:.!.:-:-'** f.J.-/

______ 

### Date: t;;J-lfR-<7 

## > , Analysis 

### Type: 

## 1/1/7- 

## /Za ;'2 Run 1 Type Identification Final Tare Net Number Weight Weight Weight 

# .! Filter 

# p**l#6~'f** 

# 2· &t;1-? 

# d· {;;51"1 "OOO;{ Probe Rinse ( mI) 

## B 37-96 

# (//. 13039 

# w¥. 80,/0 ,0000 Fr.ont HalfWeight 

### , Od 

### O**~** Organic ( mI) 

## C. 

# 1./(1£/3 

# JP;J39v9

# ~.39S'.i ' ,oDoD Inorganic 

## D 3i?65 

# /37 

# z,z,oS 139- 2/'11­ I 

### oc; 

## 13 Total Net Weight 

## ,OUIS RUN 2 Type Identification Final Tare Net Number Weight Weight Weight Filter 

## PI5B7­ 

## Z· 

# &.L/Cf1­ 

# /).**~tJr** 

# I • {)/)O{p

, Probe Rinse ( ml) 

# B 379'J**7-~.** 0111

### '1-~. 

## OilY d)()OO, Front HalfWeight I 

### DOC**~** Organic ( mI) 

# e.. /lOt/I{**IO~.Ol/fO** 

## //}&>. oi.{ft; 0 

## ,&0/0 Inorganic 

## P 

# 36 Bfa 

# //t; Z. fJ..pz,o 

# lID 2,**B~W** 

## .0 00 0 Total NetWeight 

### .001 

## \0

, Run 3 Type Identification Final Tare Net Number Weight Weight Weight Filtex: 

# p /S89; 

## 2.&532­**d·~S3S** 0000 ,. Probe Rinse ( ml) 

# 8 3 

## goo (p 

# 1-. 051-"1­ {P 

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### (

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## lODD'lIdentification F= 3 inch filter P := 47mmfilter B = 150m! Beaker C 250m! Beaker D :;; 400ml Beaker

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# - TARE WEIGHT 

# WEIGHING SHEET
Time Date. Analyst

Check Weight Weighing (grams) 

### 4 5



# S'd0 

# 3**Iw~.** 

# :J01£{



# ::. C CoMPREHENSIVE 

# E EMISSION

## ~ 

# S SERVICES

# . Appendix C

.

Field Data FormsRun No. Location: Cargill (EP 2) Date: .roject# 

### % Isokinetic= Initial Meter Volume (Cubic Feet)= Final Meter Volume (Cubic Feet)= Meter Factor- Final Leak Rate (cu Ftlmin)= Net meter Volume (Cubic Feet)::: Gas Volume (Dry Std Cubic Feet 68 Deg)= Barometric Pressure (in Hg) :: Static Pressure (Inches H20)= Stack Pressure (in Hg)= Percent Oxygen ::: Percent Carbon Dioxide= Moisture Collected(ml)= Percent Water- Average Meter Temperature (F);;; Average Delta H ( in H20);;; Average Delta P (inches H20)=**Averag~** Stack Temp (F)=

. • ry Molecular Weight::: 

### ...,et Molecular Weight= Sampling Time (Minutes)= Nozzle Diameter(lnches)= Stack Round or Square::: Stack Dimention A (Inches)=· Stack Qimention B (Inches)= Equivilent Diameter (inches)'" Stack Area (Square Feet) = Pltot Coefficient:: Average Square Root of Delta P (inches H20)= Stack Velocity (Actual, ftlmin)= Flow Rate (Actual, Cubic ftlmin)= Flow Rate (Std, Dry, Cubic ftlmin 68 Deg)= Particulate Loading - Front Half Particulate Weight Net (g)'"

. Paticulate Loading, Dry Std. 68 Deg (grlscf)=

.

Emission Rate (Iblhr)= Particulate Loading - Total Catch Including Impingers

_ articulate Weight Net (g)= articulate Loading. Dry. Std. 68 Deg (grlscf)= Emission Rate (Ib/hr)=

. Percent Impinger Catch= 1, assumed 10mg Dec 12&13,2005 11805

98.6 647.700 807.004 0.999 0.002 159.145 166.100

29.90

1.30 30.00 21.00

0.00 35.0

1.0 47.6 1.62 4.4167 66 28.84 28.73 240.0 0.135 Round 27.00 27.00 30.47

3.98 0.84. 2.0985

7,064 28,086 27.986

0.0019 0.0002 0.04

0.0100 0.0009 0.22 81.00Run No. Location: Cargill (EP 2) Date: .roject# % Isokineti.c= Initial Meter Volume (Cubic Feet):: Final Meter Volume (Cubic Feet)= Meter Factor= Final.Leak Rate (cu Ftlmin)= Net meter Volume (Cubic Feet)= Gas Volume (Dry Std Cubic Feet 68 Oeg)= Barometric Pressure (in Hg) 

# = Static Pressure (Inches H20)= Stack Pressure (in Hg)= Percent Oxygen = Percent Carbon Dioxide= Moisture Collected(ml)= Percent Water- Average Meter Temperature (F)= Average Delta H ( in H20)=

. Average Delta P (inches H20)=

Average Stack Temp (F)=

.

. Dry Molecular Weight=



# "et Molecular Weight= Sampling Time (Minutes)= Nozzle Diameter(lnches)= Stack Round or Square= Stack Dimention A (lnches)= Stack Dimention B (Inches)= Equivilent Diameter (inches)= Stack Area (Square Feet) = 

### Pilot Coefficient=

. Average Square Root of Delta P (inches H20)= Stack Velocity (Actual, ftlmin)= Flow Rate (Actual, Cubic ftlmin)= Flow Rate (Std, Dry, Cubic ftlmin 68 Deg)= Particulate Loading - Front Half Particulate Weight Net (g)= Paticulate Loading, Dry Std. 68 Deg (grlscf)= Emission Rate (Iblhr)= Particulate Loading - Total Catch Including Impingers

_ articulate Weight Net (g)= articulate Loading, Dry Std. 68 Deg (grlscf)= Emission Rate (lb/hr)= Percent Impinger Catch=, 1 Dec 12&13, 2005 11805

98.6 647.700 ' 807.004 0.999 0.002 159.145 166.100

29.90

1.30 30.00 21.00

0.00 35.0

1.0 47.6 1.62 4.4167 66 28.84 28.73 240.0 0.135 Round 27.00 27.00 30.47

3.9a 

### 0.84 2.0985

7,064 28,086 27,986

0.0019 0.0002 0.04

0.0072 0.0007 0.16 73.6'1Run No. Location: Cargill (EP 2) Date: .roject.# 

### % Isokinetic= Initial Meter Volume (Cubic Feet):::: Final· Meter Volume (Cubic Feet)::: Meter Factor::: Final Leak Rate (cu FUmin)= Net meter Volume (Cubic Feet);; Gas Volume (Dry Std Cubic Feet 

### 68 D6g)= Barometric Pressure (in Hg) = Static Pressure (Inches H20)= Stack Pressure (in Hg)= Percent Oxygen ::: Percent Carbon Dioxide= Moisture Collected(ml)= Percent Water= Average Meter Temperature (F)= Average Delta H ( in H20)= Average Delta P (inches H20)= Average Stack Temp (F)=



# .. r;; Molecular Weight= 

### .,vet Molecular Weight:::: Sampling Time (Minutes)= Nozzle Diameter(lnches)= Stack Round or SqLiare: Stack Dimention A (Inches)= Stack Dimentlon B (lnches)= Equlvilent Diameter (inches)= Stack Area (Square Feet) = Pitot Coefficient= Average Square Root of Delta P (inches H20)= Stack Velocity (Actual, ftlmin)= Flow Rate (Actual, Cubic ftlmin)= Flow Rate (Std. Dry. Cubic ftlmin 

### 68 Deg)= Particulate Loading - Front Half Particulate Weight Net (g)= Paticulate Loading, Dry Std. 

### 68 Deg (grfscf)= Emission Rate (Ib/hr)= Particulate Loading - Total Catch Including Impingers A>articulate Weight Net (g)= .-particulate Loading, Dry Std. 

### 68 Deg (grfscf)= Emission Rate (Ib/hr)= Percent Impinger Catch= 

### 2, assumed 10mg Dec 

### 13, 2005 11805

99.1 808.000 965.794 0.999 0.000 151.636 

### 162.468

29.90

1.30 30.00 21.00

0.00 37-.0

1.1 53.9 

### 1:56 4.2208 

### 69 28.84 

### 28.72 240.0 0.135 Round 

### 27.00 27.00 30.47

3.98 0.84 2.0504

6,925 

### 27,533 27,239

0.0000 0.0000 0.00

0.0100 0.0009 0.22 100.00Run No. Location: Cargill (EP 2) Date: tfroject# 

### % Isol<;inetic= Initial Meter Volume (Cubic Feet)::; Final Meter Volume (Cubic Feet)= Meter Factor= Final Leak Rate (cu Ftlmin)= Net meter Volume (Cubic Feet)= Gas Volume (Dry Std Cubi.c Feet 

### 68 Deg)= Barometric Pressure (in Hg) ­ Static Pressure (Inches H20)= Stack Pressure (in Hg)= Percent Oxygen ::: Percent Carbon Dioxide=
. Moisture Collected(rnl)= Percent Water= Average Meter Temperature (F)= Average Delta H ( in H20)=
· Average Delta P (inches H20)=

.

Average Stack Temp (F)=

. Dry Molecular Weight::: 

# evet Molecular Weight= Sampling Time (Minutes)= Nozzle Diameter(lnches)= Stack Round or Square=
· Stack Dimention A (Inches)";;;

Stack Dimention B (Inches)­ Equivilent Diameter (inches)= Stack Area (Square Feet) ;; Pitot Coefficient= Average Square Root of Delta P (inches H20)= Stack Velocity (Actual, ftlmin)= Flow Rate (Actual, Cubic ftlmln)=
· Flow Rate (Std, Dry, Cubic ft/min 68 Deg)=

Particulate Loading;.. Front Half Particulate Weight Net (g)=. Paticulate Loading. Dry**St~.** 68 Deg (grlscf)= Emission Rate (Ib/hr)= Particulate Loading - Total Catch Including Impingers

articulate Weight Net (9)= • articulate Loading, Dry Std. 

### 68 Deg (gr/5cf)= Emission Rate (Ib/hr)= Percent Impinger Catch= 

### 2 Dec 

### 13. 2005 11805

99.1 

### 808.000 965.794 0.999 

### 0.000 157.636 162.468



### 29.90

1.30 30.00 21.00

0.00 37.0

1.1 53.9 1.56 4.2208 69 

### 28.84 28.72 240.0 

### 0.135 R.ound 

### 27.00 27.00 30.47

3.98 0:84 

### 2.0504

6,925 27,533 27,239

0.0000 0.0000 0.00
.

0.0031 0.0003 0.07 100.00Run No. Location: Cargill (EP 2) Date: tfroject# % Isokinetic= Initial Meter Volume (Cubic Feet)= Final Meter Volume (Cubic Feet)= Meter Factor: Final Leak Rate (cu Ftlmin)= Net meter Volume (Cubic Feet)= Gas Volume (Dry Std Cubic Feet 

### 68 Deg)= Barometric Pressure (in Hg) = Static p'ressure (Inches H20)= Stack Pressure (in Hg)= Percent Oxygen: Percent Carbon Dioxide;:; 

### Moisture Collected(mJ)= PercentWater= Average Meter: Temperature (F)= Average Delta H (in H20)= Average Delta P.(inches H20)= Average Stack Temp (F)=**~7** Molecular Weight= , •• et Molecular Welght= Sampling Time (Minutes): Nozzle Diameter(lnches)== Stack Round or Square= Stack Dimention A (Inches)= Stack Dimention B (Inches)= '. Equivilent Diameter (inches)=

, Stack Area (Square Feet) ==

Pitot Coefficient= Average Square Root of De(ta P (inches H20)= Stack Velocity (Actual, fUmin)= Flow Rate (Actual, Cubic fUmin)= Flow Rate (Std, Dry, Cubic fUmin 68 Deg)= Particulate Loading - Front Half Particulate Weight Net (g)= Paticulate Loading, Dry Std. 68 Deg (grlscf)= Emission Rate (Ib/hr)= Particulate Loading - Total Catch Including Impingers

_ articulate Weight Net (g)= artIculate Loading, Dry Std. 

### 68 Deg (gr/8cf)= Emission Rate (Iblhr)= Percent Impinger Catch= 3, assumed 10mg Dec 13&14, 2005 11805

98.7 966.200 1125.172 0.999 6.000 158.813 165.330

29.90

1.30 30.00 21.00

0.00 36.0

1.0 48.9 1.61 4.3792 67 28.84 28.73 240.0 0.135 Round 27.00 27.00 30.47

,3.98 0.84 2.0914

7,050 28,031 27,845

0.0000 0.0000 0.00

0.0100 0.0009 0.22 100.00Run No. Location: Cargill (EP 2) Date: .,roject# 

### % Isokinetic= Initial Meter Volume (Cubic Feet)= Final Meter Volume (Cubic Feet)::::: Meter Factor= Final leak Rate (cu FUmin)=

. Net meter Volume (Cubic Feet)=

Gas Volume (Dry Std Cubic Feet 68 Deg)= Barometric Pressure (in Hg) ::; Static Pressure (Inches H20)::: stack Pressure (in Hg):::: Percent Oxygen ::; Percent Carbon Dioxide= Moisture Collected(ml)= Percent Water-
. Average Meter Temperature (F)= Average Delta.H (in H20)= Average Delta P (inches H20)= Average Stack Temp (F)=

. Dry Molecular Weight=



# .et
Molecular Weight:: Sampling Time (Minutes)= Nozzle Diameter(lnches)= Stack Round or Square= Stack Dimention A (Inches)= Stack Dimention B (Inches)= Equivilent Diameter (inches)= Stack Area (Square Feet) = Pitot Coefficient= Average Square Root of DeitaP (inches H20)= StackVelocity (Actual, ftlmin)= Flow Rate (Actual, Cubic fUmin)= Flow Rate (Std; Dry, Cubic ftlmin 88 Deg)= Particulate Loading - Front Half Particulate Weight Net (g)= Paticulate Loading, Dry Std. 88Deg (grlscf)= Emission Rate (lb/hr)= Particulate Loading - Total Catch Including Impingers

_ articulate Weight Net (g)= articulate Loading, Dry Std. 680eg (gr{scf)=

. Emission Rate (Iblhr)= Percent Impinger Catch= 

### 3 Dec 13&14, 2005 11805 ·98.7 988.200 

### 1125.172 0.999 0.000 

### 158.813 185.330

29.90

1.30 

### 30.00 21.00

0.00 36.0

1.0 48.9 

### 1.61 4.3792 

### 67 28.84 28.73 

### 240.0
. 

### 0.135 Round 27.00 

### 27.00
. 30.47

3.98 

### 0.84 2.0914



### 7,050 28,031 27,845



### 0.0000 0.0000 0.00

0.0015 0.0001 

### 0.03 100.00Run No. Location: Cargill (EP 1) Date: .roject#
. % Isokinetic= " Initial Meter Volume (Cubic Feet)= Final Meter Volume (Cubic Feet)= Meter Factor- Final Leak Rate (cu Ftlmin)= Net meter Volume (Cubic Feet)= Gas Volume (Dry Std Cubic Feet 68 Deg)= Barometric Pressure (in Hg) = Static Pressure (Inches H20)= Stack Pressure (in Hg)= Percent Oxygen = Percent Carbon Dioxide= Moisture Gollected(ml)= Percent Water= Average Meter Temperature (F)= Average Delta H 

### (in H20)=' Average Delta P (inches H20)= Average Stack Temp (F)= Dry Molecular Weight= 

# .et
Molecular vveight= Sampling Time (Minutes)= Nozzle Diameter(lnches)= Stack Round or Square= Stack Dimention A (Inches)"" Stack Dimention B (Inches)= Equivilent Diameter (inches)= Stack Area (Square Feet) = Pitot Coefficient= Average Square Root of Delta P (inches H20)=

.. Stack Velocity (Actual, ftlmin)= Flow Rate (Actual, Cubic ftlmin)= Flow Hate (Std, Dry, Cubic ftlmin 68 Oeg)=

. Particulate Loading - Front Half PartiCUlate Weight Net (g)= Paticulate Loading,· Dry Std. 68 Deg (grlscf)= Emission Rate (Iblhr)= Particulate Loading - Total Catch Including Impingers

articulate Weight Net (g)=

. • artiCUlate Loading, DrY Std, 68 

### Oeg (grlscf)= Emission Rate (Iblhr)= Percent Impinger Catch= 1, assumed 10mg Dec 14, 2005 11805

99.3 125.900 291.135
. 0.999 0.003 165.070 165.461

29.50

0.58 29.54 21.00

0.00 32.0

0.9 61.6 1.70 0.7938 53 28.84 28.74 240.0 0.207 Round' 36.60 36.50 41.19

7.27 0.84 0.8780

2,941 21,367 21,518

0.0002 0.0000 0.00

0.0100 0.0009 0.17 98.00Run No. Location: Cargill (EP 1) Date: .roject# % Isokinetic= Initial Meter Volume (Cubic Feet)= Final Meter Volume (Cubic Feet)= Meter Factor= Final Leak Rate (cu Ftlmin)= Net meter Volume (Cubic Feet)= Gas Volume (Dry Std Cubic Feet 68 Deg)= Barometric Pressure (in Hg) = Static Pressure (Inches H20)= Stack Pressure (in Hg)= Percent Oxygen = Percent Carbon Dioxide::: Moisture Collected{ml)= Percent Water"" Average Meter Temperature (F)= Average Delta H (in H20)= Average Delta P (inches H20)=

. Average Stack Temp (F)=

. Dry Molecular Weight= 

# evet Molecular Weight= Sampling Time (Minutes)= Nozzle Diameter(lnches)= Stack Round or Square= Stack Dimention 

### A (Inches)= Stack Dimention S·(lnches)= EquivilentDiameter (inches)= Stack Area (Square Feet) = Pitot Coefficient= Average Square Root of Delta P (inches H20)= Stack Velocity (Actual, ftlmin)= Flow Rate (Actual, Cubic ftlmin)= Flow Rate (Std. Dry, Cubic ftlmin 68 Deg)= Particulate Loading - Front Half Particulate Weight Net (g)= Patlculate Loading, Dry Std. 68 Deg (grlscf)= Emission Rate (Ib/hr)= Particulate Loading - Total Catch Including Impingers
.•artiCUlate Weight Net (g)=

. articulate Loading, Dry Std. 68 Deg (grlscf)= Emission Rate (Iblhr)= Percent Impinger Catch= 1 Dec 14, 2005
. 11805

99.3 125.900 291.135 0.999 0.003 165.070 165.461

29.50

0.58 29.54 21.00

0.00 32.0

0.9 61·.6 1.70 0.7938 53 28.84 28.74 240.0· 0.207 Round 36.50 36.50 41.19

7.27 0.84 0.8780

2.941 21,367 21,518

·0.0002

0.0000 0.00

0.0015
. 0.0001 0.03 86.67Run No. Location: Cargill (EP 1) Date: 4froject# % Isokinetic= Initial Meter Volume (Cubic Feet)= Final Meter Volume (Cubic Feet)= Meter Factor= Final Leak Rate (cu Ftlmin)= Net meter Volume (Cubic Feet)= Gas Volume (Dry Std Cubic Feet 68 Deg)= Barometric Pressure (in Hg) = Static Pressure (Inches H20)= Stack Pressure (in Hg)= Percent Oxygen = Percent Carbon Dioxide= Moisture Collected(ml)= Percent Water= Average Meter Temperature (F)= Average Delta H ( in H20)= Average Delta P (inches H20)= Average Stack Temp (F)= Dry Molecular Weight=

. • et Molecular Weight= Sampling Time (Minutes)= Nozzle Diameter(lnches)= Stack Round or Square= Stack Dlmention A (Inches)= Stack Dimention 

### B (lnches)= Equivilent Diameter (inches)= Stack Area' (Square Feet) 

### = Pitot Coefficient= Average Square Root of Delta P (inches H20)= Stack Velocity (Actual, ftlmin)= Flow Rate (Actual, Cubic ftlmin)= Flow Rate (Std. Dry, Cubic ftlmin 68 Oeg)= Particulate Loading - FrontHalf Particulate Weight Net (g)= Paticulate Loading, Dry Std. 68 Deg (grlscf)= Emission Rate (Ib/hr)= Particulate Loading - Total Catch Including Impingers

. _articulate Weight Net (g)= , articulate Loading. Dry Std. 

### 68 Deg (grlscf)= Emission Rate (Ib/hr)= Percent Impinger Catch= 2, assumed 10mg Dec 

### 15.2005 11805



### 99.0 291.500 456.164 

### 0.999 0.002 164.499 167.310

29.55



### 0.58 29.59 

### 21.00

0.00 41.0



### 0.9 54.9 1.71 0.7908 43 

### 28.84 28.74 240.0 0.207 Round 

### 36.50 36.50
. 41.19

7.27 0.84 0.8809

2.917 21,198 

### 21,830

0.0006 0.0001 0.0:1



### 0.0100 0.0009 0.17 94.00Run No. Location: Cargill (EP 1) Date: .roject# % Isokinetic= Initial Meter Volume (Cubic Feet)= Final Meter Volume (Cubic Feet)= Meter Factor= Final Leak Rate(cu Ftlmin)= Net meter Volume (Cubic Feet);::: Gas Volume (Dry Std Cubic Feet 68 Deg)= Barometric Pressure (in Hg) :::

. Static Pressure (Inches H20)=

Stack Pressure (in Hg)= Percent Oxygen = Percent Carbon Dioxide= Moisture Collected(ml)= Percent Water= Average Meter Temperature (F)=

.Average Delta H ( in H20):::: Average Delta P (inches H20)= Average Stack Temp (F)= Dry Molecular Weight::;

### ~et Molecular Weight: Sampling Time (Minutes)= Nozzle Diameter(lnches)= Stack Round or Square: Stack Dimention A (Inches): Stack Dimention B (Inches)= Equivilent Diameter (inches)::::: Stack Area (Square Feet) = . Pitot Coefficient:;;: Average Square Root of Delta P (inches H20)= Stack Velocity (Actual. ftlmin)= Flow Rate (Actual, Cubic ftlmin)::: Flow Rate (Std. Dry, Cubic ftlmin 68 Deg)= Particulate Loading Front Half Particulate Weight Net (g)= Paticulate Loading, Dry Std. 68 Deg (grlscf)= Emission Rate (Ib/hr)= Particulate Loading - Total Catch Including Impingers AParticulate WeIght Net (g)= Wparticulate Loading, Dry Std. 68 Deg (grlscf)= Emission Rate (tb/hr);;:: Percent Impinger Catch::::: 

### 2 Dec 15, 2005 11805

99.0 291.500 456.164

'0.999 0.002 164.499. 167.310

29.55

0.58 29.59 21.00

0.00 41.0

0.9 54.9 1.71 0.7908 43 28.84 28.74 240.0 0.207 Round 36.50 36.50 41.19

7.27 0.84 0.8809

2,917 21,198 21,830

0.0006 0.0001 0.01

0.0016. 0.0001 0.03 62.50

# ---------_. -_.­
Run No. Location: Cargill (EP 1) Date: .roject# . % Isokinetic= Initial Meter Volume (Cubic Feet)= Final Meter Volume (Cubic Feet)= Meter Factor= Final Leak Rate (cu FUmin)= l\Iet meter Volume (Cubic Feet)= Gas Volume (Dry Std Cubic Feet 68 Deg)= Barometric Pressure (in Hg) = Static Pressure (Inches H20)= Stack Pressure (in Hg)= Percent Oxygen = Percent Carbon Dioxide= Moisture Collected(ml)= Percent Water= Average Meter Temperature (F)= Average Delta H ( In H20)= Average Delta P (inches H20)= Average Stack Temp (F)= Dry Molecular Weight= 

# evet Molecular Weight= Sampling Time (Minutes)= Nozzle Diaineter(1 nches)= Stack Round or Square= Stack DimentionA (Inches)= Stack Dimention B (Inches)= Equivilent Diameter (inches)= Stack Area (Square Feet) = Pitot Coefficient= Average Square Root of Delta P (inches H20)= Stack Velocity (Actual, ftlmin)= Flow Rate (Actual, Cubic ftlmin)= Flow Rate (Std, Dry, Cubic ftlmin 68 Deg)= Particulate Loading - Front Half Particulate Weight Net (g)= Paticulate Loading, Dry Std. 68 Deg (grlscf)= Emission Rate (Ib/hr)= Particulate Loading - Total Catch Including Impingers

_ articulate Weight Net (g)= articulate Loading, Dry Std. 68 Deg (grlscf)= Emission Rate (lblhr)= Percent Impinger Catch= 3, assumed 10mg Dec 15, 2005 11805

99.1 456.600 622.164 0.999 0.004 165.398 166.084

29.55

0.58 29.59 21.00

0.00 39.5

0.9 61.5 1.71 0.7763 43 28.84 28.74 240.0' 0.207 Round 36.50 36.50 41.19

7.27. 0.84 0.8736

2,894 21,025 21,649

0.0000 0;0000 0.00

0.0100 0.0009 0.17 100.00Run No. Location: Cargill (EP 1) Date: 4froject# 

### % Isokinetic= Initial Meter Volume (Cubic Feet): Final Meter Volume (CubiC Feet)= Meter Factor= Final Leak Rate (cu Ftlmin)= Net meter Volume (Cubic Feet)= Gas Volume (Dry Std Cubic Feet 68 Deg)= Barometric Pressure (in Hg) 

### = Static Pressure (Inches H20)= Stack Pressure (in Hg)=

. Percent Oxygen 

### = Percent Carbon Dioxide= Moisture Collected(ml)= Percent Water=
. . Average Meter Temperature (F)= Average Delta H ( in H20)'" Average Delta P (inches H20)= Average Stack Temp (F)=



# .**~7** Molecular Weight:::: 

### ,.,.et Molecular Weight= Sampling Time (Minutes)= Nozzle Diameter(lnches)= Stack Round or Square: Stack Dlmention A (lnches)= Stack Dimention B (Inches)= Equivilent Diameter (inches)= Stack Area (Square Feet) ::: Pitot Coefficient= Average Square Root of Delta P (inches H20)'" Stack Velocity (Actual, ftlmin)= Flow Rate (Actual, Cubic ftlmin)= Flow Rate (Std, Dry, Cubic ftlmin 88 Deg)= Particulate Loading- Front Half PartiCUlate Weight Net (g)= Paticulate Loading, Dry Std. 68 Deg (grlscf)= Emission Rate (Iblhr)= Particulate Loading - Total Catch Including Impingers

_ articulate Weight Net (g)= articulate Loading, Dry Std. 

### 68 Deg (grlscf)= Emission Rate (Ib/hr)= Percent Impinger Catch= 

### 3 Dec 15,2005 11805

99
.. 1 456.600 622.164 

### 0.999 0.004 165.398 166.084



### 29.55

0.58 

### 29.59 21.00

0.00 

### 39.5

0.9 81.5 

### 1.71 0.7763 43 28.84 28.74 240.0 0.207 Round 

### 36.50 36.50 41.19



### 7.27 0.84 0.8736

2,894 

### 21,025 21,649

0.0000 0.0000 0.00

0.0007 0.0001 0.01 100.00

## - 

# --
- -



# - - 

# -- - 

# -- - '- 

# -c - --­ -':: 

# -- COMPREHENSIVE



# - -


# - 

# =E=

- -



# ­ - 

# - EMISSION



# - S­

-- 

# - - SERVICES.

• "

__ 1.. J

# It;: 1/;:;­ Project NUl.lWer_---'_
.......... w...:.()_,

__________ RunNumber

__.l..I

________ Date 

# _---!-.:::/**J~/,-,-/.::..;:,.6.,-J...:...::1** ]--f-.1./(jL-5:.z....-
__ Sample Type J 

# Ij) fI). Plant 

## Cu r 

# 91 J( 

## ff'2
. Location**_~:....-** __ ______ 

# 2 ;7 Assumed Moisture % . Meter Number**_~~** Minutes Per Point (min.) Oven Number 

# VA­**S~pling** Time (min.) ). 

# Y 

# 0 Umbilical Number
. 

### I

# Sr/ Meter Factor Y Pitot Number 

# <7,9 , 

# ? ) Meter

# ~H@ 

# If?' V Probe Number 

# J Pitot Coefficient Cp Probe Length 

# O.

# ((~ 

# J I ) ' t ) L Stack Axis 1 (inch.). 1 Nozzle Type
_ ......... Z<--_ 

## )- '1"' Stack Axis 2 (mob.) """';;'--'-_ 

# 'CIPU Barometric Pressure (in. Hg)**--=:;;....J._..::..J.l~_** , .) Static Pressure (in. IIzOJ

__;...:./'..;::.J
__ Nozzle Diameter (inch.)

__ 

## 0_,1-1
..... 

## 3...;..)''--_

Orsat Project Leader

# _~J~CI**+-y~1r-J/'-'-J....;..l!"-~----­** Meter Operator

# --"J""·.!!.~+y.....Jr'-!j..J..'t...!l.V...;:S---- LabPerson

___________ SUpPOrt Personnel

Schematic ofTesting Location

Impingers 

# 1**~** 

## C**I---'";;;;;;..;;...=.;..:;.;;;;.....~==.t...-.-~~~--=-z~~--I** 

## frvl,bf!J

Pitot Leak Check 

### RECOVERY 

### DATA

Trial %C02 %C02+%02 %02

1 A 2

# !~**~** 

# hfen I 3 I 

### ... Avg Final Initial Difference Impinger 1 . 

## j£.')S 

# I Of)**~.** Impinger2 

### ItO 

# il/U 

# 0 Impinger 3 

### lOt) 

## 1f)1J 0

. Impinger 4 

# /'7'3 

# 7 L 

# I3 '3° Condition/coior Total 

# 3;; 

# • Notes: Filter Number:

## Field Data Sheet

# - -- - 

# --

- 

# --

- 

# -

-- - 

# -C­ -'. 

# -- COMPREHENSIVE 

# =E= EMISSION 

# -S:::::, SERVICES



# -- .
Project 

### Number_..:../oI..-l

## ~",-,(I,-I 21-'

_____ Project Leader

__

## J~'u7_,;,. 

# _______ Run Number

__)=:;;..;...,

_____-'--

___ Meter Operator 

### _....:J::;..:...c, ...L,

_______ Date 

## J)!Jjj(J), Lab Person

__---'-

________ i , Sample Type 

# I 

# 7:f2: d 

# '< Support Personnel

### --LN...:.J,~IvIW/r..._ 

### ______ Plant 

# CU'1f (f Location 

## e:f;2. 

# 1 Assumed Moisture % Meter Number 

### t.7­ Minutes Per Peint (min.)
. 

# L Oven Number 

# AlA**S~1ing** Time (min.)
. ). 

# 'fa Umbilical Number 

# JJrL Meter Factor Y

# ~ Pitot Number 

## J Meter 

# tlli@tiif**I)t~robe** Number _..;..)
__ Pitot Coefficient Cp 

## (/11'1 Probe Length ) , ") 'Ttl C; '­ Stack Axis 1 (inch.) / 

### !. Nozzle Type**_...:./....:J~_** Schematic ofTesting Location , ) ,.<1 Stack Axis 2 (inch.) --"_-'_'-_ Barometric Pressure (in. Hg) 

## ').q, 

# b Static Pressure (in. H20)

__J...l....
__ Nozzle Diameter (inch.) 

### _--..;;(J-Io!""'ll
....... 

# 1'_ Leak Rate Before Leak Rate After Pitot Leak Check 

### RECOVERY DATA Orsat Impingers Final Initial DifI:erence Impinger I 

# 10'] I Of; 

# !7 Impinger2 

# IOI) {C/O 

# 0 Impinger3 

# i(fO 

# 11{l (/ Impinger4

### '1~( 

# 711**:>~** Condition/Color Total 

# j't-
. Trial %CO

1 2 3 Avg Notes: Filter Number: 

# P**J~/1**

## Field Data Sheet Run No

## -...;;2~ 

# _____

_ Project No.

## -L!...lI-v--rJ~{J-1-)--
.., Location 

## E 

# f 2 Date J

# )..;'3/t' 

# 5 /. I Operator .), 

# ttl H,**~i.** " Start Time" 

# li#j I ().

# J~ Stop Time

## :f)-;+~ 

# ILj; 

# 1**~**

§.. 

## C . 

# --== COMPREBENSIVE 

## = E 

## = EMISSION 

## S**~** SERVICES

## - 

# -- - --



# -- - 

# -- -

Final Initial Difference

Total 

# -c ­ =:.: 

## -==== COMPREHENSIVE 

# =E EMISSION 

# • - S=

-- 

# - SERVICES

Project

## Number--ll:..J./...l.i~;';;;'[;...I.)f ______ Project Leader 

### _.::..J,:;,I.

# ,+'I...L.,------- RuriNumber

__ 

## J

____

# -=-

______ Meter Operator

__ J_,-,-'J..:.....(

_______**ubPe~n** _____________ Date 

# ))"/IJJ:/Lj/flf J Support Personnel _'

## 11...::.,~lv:........:..... _______ Plant 

## Gicutfl Sial/V 

# tt"'"y Location Sample Type 

## -.t...'J..1;I-'/A:....;·

### ~(} .....______- ..... 

# E



# pd.

Assumed Moisture % Meter Number 

### X 

# 5" Minutes Per Point (min.) Oven Number 

### N,4 Sampling Time (min.) 

# 2'ttl Umbilical Number

## ~ Meter Factor Y 

# 0,'1 

# r Pitot Number ) Meter AH@

__

# Cf;...~~9.L..· _ Probe Number 

# _...."J,..,...._ ..:;..I

;...1 

# • . Pitot Coefficient Cp 

## rJ I 

# Y

# ~ Probe Length

__

# )~/_ 

# ::2 11 

# >5 Stack Axis I (inch.)**~~~I__** Nozzle Type

____ Schematic ofTesting Location 

### ;l 

# t I[ Stack Axis 2 (inch.)
. Barometric Pressure (in. Hg)

## :;2~. 

# 11 Static Pressure (in. H20) 

### _-.:-11.,;,1..:;.)"...£
__ Nozzle Diameter (inch.) _. __ 

## rl_I

__ {

# l
........

f_ Pitot Leak Check 

### RECOVERY DATA Orsat Impingers

Trial**%CO~** %C02+o/00 Z %02

1 \ 2 

# _H f1 

# )2, 

# en t 3 I Ayg Impinger 1 Impinger2 Impinger3 Imp' Condition/Color 

# p 

# I**~;).tJ** Notes: Filter Number:

## Field Data Sheet Run No
............... 

# 5_--'-

___ Project No. --</LL/-tL!f£/}<......;' S,--'
__ • Location 

# tf.2, _, Date

## J)J/~ .J.JLfJpj I , • Operator ' 

## J 

# .l

# '* /1. W, Start Time 

# 14 : t{f - 

# 7;)} 

# JI**~L.lCi_a:** 

### (;'3 Stop Time

__**.:....::fI~. "2-1-.../...~I--",.I-** 

# - -- 

# Preliminary Velocity 

# e Plant Project No. 

# Jl (! 

# I' Date /) 

# ---/)---11

# ~ tfd-... Location 

# N ).1,1 Staok 

### 1.0. Pitot 

### Cp 

# O·t l Statio Pressure in 

### H2 

### O 

# I, 

# 2 Barometer Pressure in. Hg 

# 2.',2fL 

# tJ Start Time $top Time 

# 4 Operators

. SCHEMATfCOFTRAVERSEPOINTLAYOLn" Final Pitot Leak Check at <2:3" 

### HlP P 

### I F Traverse Velocity stack Cyclonic Flow

Point Head Temp. D eterminatron Number 

### AP OF

, in.H 2 Q AP at 0° Angle Whioh Reference**Y~lds** III NuHllP 

# Ad 1? (; 1 J. 

# ':J.b '& 

# 1 'J

### '1/~ 

## }(; 

# '1**~i-** 

## '1-11 

# 5 ).] 

# 1-'(;**~.** 

# 9(; :/(j 

# ,1­ 

# !.L :J 

# 10 Vi 

# ).4 'J.-.() 

# 9 )1 

## f 

# +0 lO**~I** 

# +0 t) 

## )',0 

# *V IL 

# T<:)**~** 

## &,**~** Traverse Point Number Velocity Head 

### AP in.H:p Stack: Temp

, OF Cycfonlc FlOW Determination 6P atO G 'Referenoe A:ngle Which YieldS aNuH AP 

### lff 

## 1./} 

# 7fJ

::< l.f. 

# I 

# 7-0 J**Lt~9** 

# t1J t.t It. )' 

# 1-fJ )'

## ~I**~** 

# 1-0**~** I:f 

# C 'Hi 

# t '1**~q** 

# 10 t( 

# )'1 

# +0 '1 

# G 

# . 

# , J.-(j 10

## ~/~ '1{) , / 

# , '1**~** 

# &Y t) 

### '1,) 

# itt Notes: 

# :::;. C -===, --:--" --= COMPREHENSIVE



# - - - 

# E-

-- -­ - - EWSSrON 

# ==- S**~** :SERVICESTotal Number of Points(8, 12, 16,20,24)= " 24 EP 2 Stack Diameter or Length(inches)= 27 Round Square 

### _oint Distance 1 0,6 1 0.6 

### 2 1.8 

### 2 1.7 3 3.2 3 

### 2.8 4 4.8 4 3.9 5 6.8 5 5.1 6 9,6 6 6.2 7 17.4 7 7.3 8 20.3 8 8.4 9 22.2 9 

### 9.6 10 23.8 10 10,7 11 25.2 11 11.8 12 26.4 12 12.9 If stack diameter is less than 24 inches each point must be greater than 0.5 inches from wall if stack diameter is greater than 24 inches each point must be greater than 1.0 inches from wall 

# •

•

# -------

I . .1lIlo_ 

# _ .. 

### _ ..


## EPA

# EMISSIO':OBS~VATION FORM 1 . 

# FJ&Jl1 n 1 111- , 1**I~** 

# j21 1 

# I

Of .JdLFm n'

## ~!\:J6IIlon I 

## :3JLFeiT '" I0bsGtvaft00 DaIs



## . )).:rJ· rJ('**~,,%or\Q ~**  

# r t
·

### C(lA!~I'tII~'>; 30 rnG

## i6 

## :3(j**~** Q 15 <lO -45 cornmm\!l 1 

# 0 0 0 0 2 

# 0 {; 

# a 0 s (J 

# 0 0 

# tl 4 

## 0 

# 0 

# 0 !J II 

### () 

# rJ 0 

# 10 <Ii 

# 0 

# 0 

# 0 {} 7 

## (J 

# 0-- If 

# 0 , .... " 9 

# 0 

# 0 () (j 9 

## () 

# 0 0 0 

# 0 

# 0 f) 11 

# 0 0 () 

## 0 12 

# 0 

# 0 0 0 13 

# 0 0 0 

# tJ 14 

## 0 

# 0 

# a () 16 

# 0 

# 0 

# 10 10 16 

## 0 

# 0 

# 0 

# 10
17 

# rJ 

# 0 10 0 18 

# 0 0 () 

### ()­

. 19 

# D () () 

## 0 120 

## 0 () () 

### (j

21 

### () 

## 0 

# 0 0 22 

# 0 0 () f) 23 

# 0 

# 0 

# a 0 24­ 

## 0 

# 0 0 

# 10 - 26 

# 0 0 

## 0 0 26 

# 0 0 

# /J .'0 

### () 

## 0 

# 0

28 

### (J 

# a () 29 

## 0 {; 

# IJ (} so 

# 0 

# 0 

# 0 0

VEOF 1. 

### 1

# Ot...ILL

.... 0 

# . I o:n::"", 

# I • • 

# -- 0I:>s9Ml1I0n DaIB**Tr-i3~t7)-**

## ~ 0 11; 1 

### () () 2 

### (. 

# 0 3 

## (j 

# 0
4 

# 0 () 5 

## () 

# 0 6. 

## () 

# 0
7 

### () 

### () 8 

## () 

# D \I 

# 0 () 10 

## () 

## .() II 

# V 0 12 

# n 0 13 

## () 

## () 14 

# 0 0 15 

# cJ 0 16 

# rJ 0 17 

# a 0 18 

### (j 

# O·
1'1 

## () 

# 0 20. 

# a (j 21 

# ·0 0 22 

### r) 

# 0 2a 

### ( ) 

# 0 24 

### ( ') 

# 0 25 

# C 

# 0 26 

# 0 

# 0

. 27 

# a ()

28 

# rJ 

# t/
29 

### () 

# 0 31) 

# a () lirria Z<:rno 

## "&",1',..41**l~linllr:llfJ** 

### IOndltM 

## q**~DD**

30 45 COIl'orr'IInll 

## f) 

# 0 

# 7J /J 

## 0 

# 0 () 

# 75 IJ 0 () (]. 

## () 

# 0 () () 

# 10· 0

(). 

### () 

# n () f) 

# 7i O· 

# 0 0 

# iJ .. 

### f) 

## [} () 

# 0 

# 0 {J 

# 0 O· 

# 0 0 (/ (j. 

## 0 (; f) 

### (J 

# 0 (J 

## () 

# CI () 

# 7J () 

# d 

# 0 fJ (j 

## (; () 

# 7J 

# 0 

# 0

# Ot JtLmr n 

### .1

## ~I'm I

.**~.** to



# ....

# ­ EPA 

## SIBLE

# EMISSION""OBS~VATION FORM 1 

# F=jE!¥¥' '}[- I to 

# t4 t 

# I.

.. 140'

### ---~-----~------~----- SI.K\ 1.OOOIkln t.i1e
.



### VEOFl.l**~1alD<D** ...

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### I1maL~fd 

## i stQf1liYe 

### ifl 

## i).d IOrdltN /f 

# ;JfJ**~** a

### ~5**~ ~ .~~**  1 

## (J () () 

# 0 2 

# 0 

# 0 1; (j 3 

### [t) () 

# -0 0 4 

# £:to () 

## () 6 

### () 

### () 

## 0 /I 

# o I> 6 15 7 

# rJ 7J (f 

# iJ B 

## (J 

# () 

# 0 () 

# , 

# rJ 

# 0 (j. 

# 0 10 

# a ·0 (J. 

# 0 11 

# C' 

# %+1) {J 12 

### (J 

# 0 () 18 

# Ll

# E~ 14 

# 0 15 

# t1 () 

# o 0

. 16 

# 0 0 

# /J 0

17 

## (J (J 

## /7 

# o· 18 

## -() 

## O· 

# tJ O·
19 

# r;- 0 

# ?J 0

# ~v (j 

# 0 rJ· ...... 21 

# 0 

# "rJ (j () 22 

# o· 0 

# 0 0 .­ 2-' 

# 0 () 

# -0 0

.. 24 

# 0 0 

# rJ 0

25 

### () 

# iJ (j 

# iJ 25 

# 0 

# 0 

# 75 0 27 

# 0 () () 

# 0
28 

# a () 

## 0 

# D 29 

## CJ 0· 

# 0 {J 30 

### () 

# (1 () 

# 0

### - 

# -

- - 

# •

• - 

# -c - -­ -' 

# - 

# -- COMPRE:HENSIVE



# -

- - 

# =E=

- - ­ - - EMISSION



# - - -- 

# S-

- ­ 

# -- 

# -- - 

# - SERVICES

Project

# Number·----=J_/.::..~.:;..O.:...? ______

## R~NmOOer ____ '

__

## ~~ __________ Date 

# f

# ~ntlj~ Sample Type 

## 11#/12. , Plant 

# Cq rir fI hOVX 

# [(1'1 Location _t.",;,P...,J/:,...-

__________
Assumed Moisture % 

# I,)" Minutes Per Point (min.)

## ~ SampliugTime (min.) ). 

### Ll/)

Stack Axis 2 (inch.)**---.:;/...lI~r.t-_ ~**  MeterFactorY
. 

# D,911 Meter AH@ ( , 

# 7 

# t**~** Pitot Coefficient Cp 

# 0 t 

# r**~f** Stack Axis 1 (inch.) 

# 3 ',('-(1 V ) '21.rll Meter Number )' Oven Number 

# 1\1 A Umbilical Number 

# .!.:ilL PitotNumber 

# l/I Probe Number 

# 'i Probe Length

## ~_y~l_ '}1. Nozzle Type**_..,f;.<....£/~.** 

### _ Project Lea4er _J......,.'''::''';'&\-+.Y,,-/;!....-t

# ~_fJ_) ____ Meter Operator

# ----=**J:...!(j~t~r.Lt .:...{**  T:.-{j,:->..,;..

_____ LabPerson

_____________ Support Personnel _.s.../1...l0W:):....l!(/..uH---:.;..W,."Lfi,-'-:....!Tft;==-
__

Schematic ofTesting Location
Barometric Pressure (in. Hg) 

# 29.')& Static Pressure (in. H2 0)

## _-,(fL.:~,-,-f...;.~~ Leak Rate Before ' Leak Rate After • Pitot Leak Check '" 15 in_ H Nozzle

# Diamet~r (inch.)

# _---.,;..(J...;,~.:...;)..;;,.{I...l.f_ in.H After 

## RECOVERY DATA Orsat Impingers

Trial %C0 2 %C0 2+%02 %02 1 A 2 

# AI**~~t** 

# en 

# i 3 !­ ) Avg Final Initial Difference Impinge! I 

# /OtJ 

# 100 0 Impinger2 

# 100 100 

# 0

.. Impinger3 

## i()() 

# lOO , 

# 0 Impinger4 

# :JIG ·.7f'1lf 

# 32 Condition/Color Total 

# 3A 

# • P 15,fl Notes:

# )qve~ Q5

# ~CGPlfl.{f Filter Number:

## Field Data Sheet Run No ..........J..

______

_

## Proj~ct No:

## ....J/f...!...'iL!:.r{!~'**)~--­**
,., LocatIon 

### £,f 

# f .

, Date, 

# IJ-II't/fJ5" Operator 

# J. 

# r rJ 

# It W. Start Time 

### J 

# l: 0 

# 1 1(; 

# ;J:l., Stop Time _---..:..-::...L;_ ;....;;......-­**'",.,.~** .

# =.,C

# E

# S. 

# C OMPREHENSlVE EMISSION SERVICES

Project

# Number~}..L/.JL.r..;;..(}~7 ______

# J'~/. Project Leader 

# --"""T"""..I..-.:..------­ Run

## Number_....:2::::::::...~~ 

## ______ Meter Operator

__

# J_~...;.r...l.( ___- __ 

### LWhnoo

____________________ Date

__**-:..::.:..::-.--=.;::~::;;.......:..** ______ 

# 11- 

# is-fl,­ Sample Type 

# I 

# W (j 

# 2 , Support Personnel

__

### tf...,;.:.(..;,lv~! _____ PJam 

# c._crt tI >1 flVX eaf'f, Location

# ~ll I**~** 

# 7', Assumed Moisture %**~** 

## L Meter Number _--"_ 

# • MinutesPerPoint(min.) 

# .1L OvenNumber 

# IVA- Sampling Time (min.)

## )~a UmbilicalNumher 

# lJt/ MeterFactorY ,(/, 

# Yf1 PitotNumher 

# 4 Meter AH@ 

# I. 

# ? '1 Probe Number 

# '1 Pitot Coefficient Cp 

# 0,**r~** Probe Length 

# Y , 

# Jr. ,'1 )5 Stack Axis 1 (inch.) 

### !l L Nozzle Type
. ____....,.-_ Schematic ofTesting Location 

# 3

/



# ,5' {/ Stack Axis 2 (inch.)**_..;:..f(~_** Barometric Pressure (in. Hg) 

# 29. S' 

# S'" Static Pressure (in.

## ~O)**_---.,;():....:,~7_;-g** __

## Nozrl.~ Diameter (inch.)

__ {/..;....;I

## ).~(/ ... ]._


### RECOVERY DATA Orsat Impingers Leak Rate After i Pitot Leak Check**~** 15

Trial %C0 2 %C02 +%02 %02 1 '2 

# 11 (.Qf1' ,

3 

# I \ V I V Avg 

### Final Initial Difference Impinger 1 

# lOO 100 

# a Impinger2 

# lOb I 

# (Jp 0 Impinger 3 

# lOO I{J 

# 0 0 Impinger4 

# 't12 13/ if) Condition/Color Total 

# vl1

• Notes: Filter Number: 

# ...... 

# _______ _ ,-'-f_/_5**·~--'7**

## Field Data Sheet Run No

## ~;2_....--~ 

## ___

_ Project No.

## --L!IIJL8j~l}-"-1? --­ • Location 

# Er I Date 

## 1,2**~/5'-{j)** Operator 

## J,r J 

# H, 

# W
.. Start 

### Time 

# r; rJ li:Of Stop Time _-..:..!::,.;,t.....::....::::....!.---­

### - 

# - - - - 

# -- -



### -- - 

### -- 

## - 

# :.

- 

# -

- 

# c-

-- -- -­ -' 

# -- COMPREHENSIVE



# - 

# =E-==

- -- EMISSION



# - S­

-- 

# -- - - SERVICES



### . 

# J, 

# /r Project 

### Nwnber---lJ..J,.'I...::,YI...:Il_"..:..,l

_______ Project Leader

____,.;".-

______**R~Number** ___ 

## J

____________ 

# J.7'. eter erator

__---.,;.,-..:.-

_______ M Op Date 

## _----.,;J;",.:;..)_-f:....Lr......:-**(I~5"** 

# ____ Lab Person

____-,-..

________ Sample Type 

## I 

# 'J!).fl2 Support Personnel

__ /:.../.:.....:....'

## _U-:.

_____ Plant 

### LCI, 

# 1'1' (I Location 

## _---=-e....!.f--:...i

________
Assumed Moisture % " )' Meter Number 

# 9 Minutes Per Point (min.) 

# -.iL.. Oven Number 

## IV} Sampling Time (min.) 

# 110 Umbilical Number

# ~ MeterFactorY
. PitotNumber 

### I..f 

## O. 

# '1r (j 

# /'1 J I Meter .6H@

__....;...,:.....r.L....:::U:-_ProbeNumber_ 

## Lf ..;...._ Pitot Coefficient Cp 

## 0/ 

## /,1 Probe Length 

### Lf I . Stack Axis 1 (inch.) 

# llt,S'1 NozzleType 

## .5} Schematic ofTesting Location**J(,~{f** 

## . Stack Axis 2 (inch.)**_~",z..._** Barometric Pressure (in. Hg) 

## 2 

# 9, 

# ST (Z 

# rg Static Pressure (in. HP) -.........;;..;....<.)...:;....-­ Nozzle Diaffieter (inch.)

__ 

### (/,_'.:-}....:;(/_1-,--­ Leak R8te Before 

### Leak: Rate After Pitot Leak Check**~** 15 in. H in.H After 

### RECOVERY DATA ·Orsat Impingers

Trial %C0 2 %C0 2+%02 %02

I 2 I I 

### .... 3

### -~ 

# 'Pre hI Avg Final Initial Difference Impinger 1 

# /00 !(f{) (/ Impinger2 

## ft/{; 

# (dO 

# 0 Impinger3 

# ;O{) /(10 

# 6 Impinger4

## 7)~,Y 

# ct«9 3Cf,} Condition/Color Total 

## 5'1,$" 

# P!J,tl· Filter Number: Notes: 

# S q v( 

# J Q,S 

# c r; (I 

# f{3 

# e

## Field Data Sheet Run No 

# ----=------­

.. Project 

### No. --L.f./I..Ji..[.l<:-U

# 1-!--

___

., Location {; 

# f f Date 

## I**).-/7~Q** 

## 9**operator,--..:.J~~ J!......-:-J.-~M.:.:..** **~rv"-** 

# __ .. Start Time _--IL._:"j. •**..£..,.!-=-~**

### I)

## :~:"'\ -'[',4 

# 2. Stop Time _--L...!._ /**r~-----=-** 

## __**~CEC** 

## COMPREHENSIVE



## - SE EMISSION 

# === '= SERVICES

# • Preliminary Velocity
Plant prOject.No

..

# ,~II~r'-.,;t~)..;...)'_~ __ Date 

# 1)/ / If

## if)" Location 

# £1'7 r '''I 

### c:: i {

### Staokl.D·'--;)..Jlr~~ 4./.(,------- 

### Pitot Cp
. (It 

# y, Statio Pressure in H:p,

______ 

### Barometer Pressure 

### in.

## Hg,......;.-:;......L2,~>].K.-_ Start Tlme!

___**..,---~--** 

### $top Timea.

______-

____ Operator$;

__....;.·

_______**~**

. SCHEMATIC OF TRAVERSE POINT LAYOUT Rnal PitQt .Leak Cheek at ;:a:3" H:oP P 

### I F Travers!' Velocity Staok Cyclonie Flow



### Point He-ad Temp, DetermInation**Numb~r** AP 

### OF .·In.H,p tiP at O· Angle Which Reference Yields a NullAP 

# 41 . . 't ( ?b 

# 1 

# , rt't­ 1'-1 .7 

# J I

## ~7 

# !if 

# '1 I 

# )J
. iJl t;' I

### ~2 

# ,.2 & 

# 1'.2 ?.2 :f.­ 

# ,&3 9") 

## f{ 1**1-~** 

# ..**?~** 

# q 

# 11b ,) 

# It 

# L3 5) I( 

## I, ) 

# 51 

# h 1,2 I{q Notes: Traverse Velocity Stack Cyclonic FloW Point Number 

# /}1

2­ 3 

# li·**~' -~**  

# .1­**~**

### ~ I{J 

## Il 

# 11 Head Temp Determination 

### AP OF AP at·O· 

### iri. H 2O Angle Which Reference Yields a Null AP

### 11~ 

# ".'" ."T I



## . ./52**~** 

# &**~** 

# f)

I 

## y'f 5".2 

# ,')7 

# ')1



# . .)1**s~** I

### )-~ 

# 52 .-:tP 

# ,1


# ,**r~** 

### I)) 

## }, f· )'".2­ 

## II 

# b C)J 

# \ ,2**~y** ..

## ~c**~** COMPREHENSIVE 

# = - 

# E-=

-­ - 

# - EMISSION'**~** 

## -=



# -**S~** SERVICESTotal Number of Points(8,12,16,20,24)= 24 EP 1 Stack Diameter or Length{inches)'" 36.5

. Round Square _oint Distance 1 0.8 1 0.8 2 

### 2.4 2 2.3 3 4.3 3 3.8 4 

### 6.5 4 ( 5.3 5 9.1 5 6.8 6 13.0 6 8.4 7 23.5 7 9.9 8 27.4 8 11.4 9 30.0 9 12.9 10 32.2 10 14.4 11 34.1 11 16.0 12 35.7 12 17.5 If stack diameter is less than 24 inches each point must be greater than 0.5 inches from wall if stack diameter is greater than 24 inches each point must be greater than 1.0 inches from wall**~Ncrne** FadIlYNamo**.BIraGI~** 

## ,star. Clti

### I~ I'\'CICaI$ 

### 1\Wt#**I~Mod& ~--a~** **I~Mod&**
IlleeI:IIl:e
....••.... '

Het#of £mIsr. Pl. ReI.loOi::lfilllMlf Haltt o1l!mt1s. PI. 61af End End 61af ' IJ6iIQ1c9to Elrist. pt,**~"'!i.I'nIII&.I'I"~1** stat End 61af End

# ~~ Jrng lone stat11mCo 

### IErd1\TlQ
III 30 4S Comrt!fInII 1 2 3 <4

.. I; /I '1 B 9 III n

## ~ 13 14 11:1 16 17 111 19

, ' 20

### ,'~ .. '

-, 2T 22 28 24 25 20 27 28 29 SO

... /f"I!1l!**~I ~"Q'laII.r8**  

# It>a

CEri!IecI Bv 

# rom VEOF1.l

# AppendixD Pretest-C alibrationsMETER CAUBRA TION Operator M.W. K Factor 0.6274

ate December 

### 2, 2005 Meter Number 

### 5 • revious Y Factor 1.001 Orifice Number 23

RUN 1 RUN2 Meter Volume Final Cubic Feet 626.399 632.020 Initial Cubic Feet 620.800 626.400

Net Cubic Feet 5.599 5.620 Meter Temperature Inlet Initial Oeg.F 53.0 55.0 Final Oeg.F 55.0**57~0** Outlet Initial Deg.F 53.0 54.0 Final Deg.F 54.0 56.0 Avg. lVIeter Temp Oeg. F 53.8 55.5 Time sec 

### 420.0 420.0 Meter Delta H inches H2O 2.30 2.30 Barometric Pressure inchesHg 30.05 30.05 

# "oom Temperature. Initial Oeg. F 56.0 57.0 Final Oeg. F 57.0 59.0 Avg.Room Temperature Oeg.F 56.5 58.0 Pump Vacuum inches Hg 15 15 Vcr {std} dscf 5.807 5.799 Vm (std) dscf 5.810 5.811 Y Factor 1.000 0.998 Delta H@ 1.969 1.959 AverageY 0.999 Average Delta H@ 1.964 +/- 2% Criteria Percent of Avg Y 0.09 PASS +/- 5% Criteria Percent of Final Y 0.23 PASS 

# e·

# -- - CONSOLE WORK SHEET

# G,f1~ Operator: J..-:.M..s.:.
. ....lI.\J,;-.- ._'-.,...-

___ 

### K Factor: ' 

### Date: 

# I t - 'J-. 

# -O? Meter 

### tD. 

# -=- 

# t{

________ Previous 

## Y Factor: 

# \.0 V\ Orifice Number:

# .;,..~_) ______
Run Number METER VOLUME ' Units 2 

### 1 ft3 Final

## ')..(,·J~1 

# J:: 3**;2,O~** 0 , ffl' Initial 

## C, 

## :In. gOo 

# ' (;2'. 

# tICJD Meter Temperature INLET Initial 

### of 

# S-)'**~J** of 

# • Final' 

## ')S' 

# '5'7 OUTLET Initial 

### of

## ~.3 

# 51 of Final 

## I 

# :;-t./**S-~** sec Time 

# 'l;;1. U 

# ' 112 t) in. H 2 O MeterLlH 

# 2. -;**:J~** 

## ') Barometric Pressure in. Hg 

# 3t>
.. D)**·~O** 

# OS Room Temperature Initial 

### of

. of

# ~t: 

# 57 

# ?7 Final 

# .('9 in. Hg Pump Vacuum 

### /t.;"""" 

# /.5 

# • -

- 

# - - --



# -

­ -, 

# =-c­

- - COMPREHENSIVE



# - 

# =E= --'



# - - 

# - - EMISSION 

## = =::::... . 

# 'S-= ":::



# -- - SERVICESORIFICE BRACKETING M.W. BRACKET ORIFICES: Operator December 2, 2005 Orifice No. 1 23 .ate K Factor 0.6274 

### 5 Orifice No.2 20 Meter Number 0.999 K Factor 0.5409 Meter Y Factor ORIFICE #1 ORIFICE #2 Meter Volume Final Cubic Feet 637.745 643.340 Initial Cubic Feet 632.100 637.800

Net Cubic Feet 5.645 5.540 Meter Temperature Inlet Initial Oeg.F 61.0 61.0 Final Oeg. F 61.0 61.0 Outlet Initial Oeg.F 58.0 59.0 Final Oeg.F 59.0 60.0 Avg: Meter Temp Oeg. F 59.8 60.3
sec 420.0 480.0 Time Meter Delta H inches H2O 2.30 1.60 Barometric Pressure inches Hg 30.05 30.05

.. oom Temperature Initial Deg.F 59.0 59.0 Final Oeg.F 59.0 59.0 Avg.Room Temperature Oeg.F 59.0 59.0

. Pump Vacuum inches Hg 15 16 Vcr (std) dscf 5.793 5.708 5.667 Vm (std) dscf 5.790 1.001 1.007 Y Factor (brackets) +1- 2% Criteria Percent ofY 0.16 0.82 PASS PASS

### - -

- 

# -- - 

# -
- 

## -

- 

## -

-- 

# - -- -- 

# - -- - 

## . BRACKETING WORK SHEET Operator: 

# fI/1, tJ·
. 1

:2-J..-/}? Date: 

# -=--

______----'-_ f)at! Current Y Factor • 

## 7 1 

# I ../ 

## ) Meter 1.0. 

## ---=-

____...--

____ . I 

# 1L}.
» 

### K Factor No.

## 1·--=(p:......:~~~--- K Factor No.

# 2~}**f_V.-;.O_I.-,-l_~** __


# • Units 1 2 METER VOLUME '')1> 

### '1"-l( Final 

## G,'-{3. 

## y';D tr 

## C/) J-.**jt)~** Initial 

## tr 

## 3/, 

# dnO Meter Temperature INLET Initial 

### G,I· OF Final 

# GI ro/ of
. 

## Col

OUTLET of Initial 

# 0 0**~y** OF· Final 

# S1 Co 

## I sec Time 

# 4:J. C 

# t-/<7J{) I,G in. H 2O MeterAH 

# J..·3 ,)2),0) 

# Jc),**D~** Barometric Pressure in
.. Hg Room Temperature Initial of 

# s-q -jet of Final 

# 5--1 

# 51 PumpVacuum in. Hg

### I~

### I~



# =- .-= 

# =-c­ =-E--":""

-



# - _. 

# S-

­ 

# C OMPREHENSNE 

### EMISSION SERVICES

# Appendix E·



# .. Post-test Calibrations

e.METER CALIBRATION Operator M.W. K Factor 0.6274 December 16,2005 Meter Number 

### 5 

# e ate revious Y Factor 0.999 Orifice Number 23

RUN 1 RUN2 Meter Volume Final Cubic Feet 628.415 634.118 Initial Cubic Feet 622.800 628.500

Net Cubic Feet 5.615 5.618 Meter Temperature Inlet Initial Oeg.F 54.0 56.0 Final Deg.F 56.0 56.0 Outlet Initial Deg.F 54.0 '54.0 Final Deg.F 54.0 55.0 Avg. Meter Temp Deg. F 54.5 55.3
sec 420.0 420.0 Time Meter Delta H inches H2O 2.20 2.20 Barometric Pressure inches Hg 29.75 29.75 

# _oom Temperature Initial Deg.F 56.0 57.0 Final Deg.F 57.0 57.0 Avg.Room Temperature Deg.F 56'.5 57.0 Pump Vacuum inches Hg 16 16 Vcr (std) dscf 5.749 5.746 Vm (std) dscf 5.758 5.753 Y Factor 0.998 0.999 Delta H@ 1.889 1.888 Average Y 0.999 Average Delta H@ 1.889 +/- 2% Criteria Percent of Avg Y 0.02 PASS +/- 5% Criteria Percent of Final Y 0.04 

# • PASS

# -- - 

# • CONSOLE WORK SHEET

. . 111 K Factor: 

## _"-:;C,=-)_·_I..!...--

______ 

## I '7

## ~ 

# \f.t;- 0

## ~ Operator: 

### ...LM---.l...

# .....::V...;:l.~~.**_~** __ 

### Date: ;,..... 

# v'-_...:..------- Meter LD. 

# _<5

___..:..-

____ Previous Y Factor:
.......

# -I-q.+-q---11i~-- Orifice Number:

# -=~:........,.cJ=-- _____
Run Number METER VOLUME Units 2 1 

### 'ff! Final 

# c,J.. L £/ 

# IS­ 

# &-:/-/'/1<1 Initial 

### ff! 

## (,J)..-**~** 

### 0 (.1

## ~~t·)OO Meter Temperature INLET. Initial 

### of 

# :;-!**~L/** of Final 

# :;-b sC;

.. OUTLET Initial 

### of 

# 0 sf. of 

# 5-4 Final 

# ))
sec Time 

## 7"';20 

# iJ':JJJ in. H 2 O Meter ilH 

## :;2.;2.

## --;;~:z. 

# . Barometric Pressure in. Hg 

# 2'1.7S .29, 

# '1r· Room Temperature Initial

## ~7 Final 

# S-7 in. Hg 

## . j Pump Vacuum 

## i(;; "F 

### of 

# S-C;

. 

# .>7**~c** COMPREH.ENSIVE
.



# - --' 

# =E=

­ - 

# - EMISSION' .::::::=.. ' 

# -= 

# -. - - 

# S-

­ 

# -- -. 

# -- - SERVICES.

# •

## BRACKETING WORK SHEET



# . ftA W' Meter 1.0.

# _s=~ 

# __.......-

____ Operator: L.....lo.l......;· ._'

_______ 

### Date: 

# l2: -lo-.O ( K Factor No. 

### 1 ...L'

# ..::.Cu~)-=-JI-~_' ----.;.

___ Current Y Factor ' 

### K Factor No.2 ....:. • ...i£..),.......:4...;...O...L.Q

____ 

# q 

# q1

METER VOLUME Final Initial Meter Temperature INL.ET Initial Final OUTLET Initial Final

. Time MeterAH Barometric Pressure Room Temperature Initial Final Pump Vacuum Units 

## te te

of of
QF QF sec in. H2O ·in.Hg


### of OF

. in. Hg 1

## G31.1/~**~3L./\)QO ~(**  

# 6--Z

.**~S** 

# S-7 

# 4:2 D 2 .., . 

## .,.....**~1, 1S~**  

# S--'? <,-1 

# f(P I


## -', =. 

# C ·E

. S-::::: .==.. 

## .-=



# -­ - .. 2 

# tt-frJftft c,t./ 0
. i.1 0 {) 

# <f (,1

.. 

# 5"7 

# S'"! 

# '-I ;JD 

# I.t**~1.?5"** 

# !:7' 

# S7 17

COMPREHENSIVE E:MISSION SERVICES

# AppendixF Process Data



# •**Rece~V&d:** '1 61 6 2.40PM; 7122791225 .> Thompson Envir**Cns~t;** Page 2 01/05/2006 

### 14:36 FAX 7122191235 CARGILL SC CRUSH @002



### Compliance Emission Test Operating Data Owner;Cargill. Sioux City 

### Date: December 

### 12-!S.200S Source: West Gmid**Clearl~1'** 

### PermIt #: 95-A·'23-B8

Maximum Continuous Pl'oC8SS Rate (Manufacturer'l&**Rating)'.-;;;~..;.;43:;...t;.;o;,;;nslhr=_~** ________ HistoriC<ll Average Process**AatEl,_--.:..N~A-,--** ___________________ Historical Maximum PrOCs5$ Rate,

__ N..;.A

...._________.....**_-~--_~** ........__ Types and Sources ( If any) of fuels normally Bumed

__N

__

A

____-

_______**~** Type of Fuel Bumed During t\'Il$ test,--_ N;.;;A:.:.-

_________**---_~** ___ 

### If Fuel is used Approximate QUl;ultities of each listed above bumea AnnuaJly._N...;A;..;....

___ __ 

# I , Recycling Capability No 

# X
I Rooyclfng io Progress No 

## X Procc!jS**QilLRl~** ing Run!

# ~ Process Rate (gaUhr, IbJhr, tanslhr, etc•.. ) Process Flat$ Wet Percent Moisture (%)

How Process Rate wa$ Determined 

### RUn 1 Run 2
.. Run 3 

# 23"f,...y/r 3" fp... 

### r/)".. 

## :.z.3. -fr,.nG/I ,..



# r,;, 

# k t,&v./:$
Pnon Re$ponsib;;-'l**?~att P~arson**  Signature 

# 1/ {r,t;fC

# ~,~, TltleJPosJtlanCruSh Plaot S"'perintencient "' Please indicate 

## m the ;;tame /lnits 

## as your 

### bjMp&.aI informatioo

# ~ j 

### 1**R~ce1ved:** 1/ 5/ 6 3:41PM; 7122791235 -> Thompson Snv1r Cns1t; Page a 01/05/2006 14:37 FAX 7122791235 CARGILL SC CRUSH 

### IaJ 003

'/
J, 

### A.I:R POLLlJT10N CONIllOL EQWMENT OPElUTlNG 

### DATA



### , PIaw: Cargill. Sioux City 

### Loe:u:iou Sioux City, IA Soum:Type West Grain Cie'aner. Rated Pf(ldm;tion _2_4_3_to ..................________ Il!Ihr 

# •

DatI:**O~C;** 12-/S, 2Q()S**T~** ____ Ad:\all'tod-u.ctton • 

### AirPtowData

____________



### __________ __--------­**~N~** 

# ------------------ MecM1I7c:ll Collector: Tube'Dia. in... Number ofTulIe:i Design Ap

___

### in. HiO 

### Gas Temp _,_"i! 4p i:a**~** ])e:rip d'mItube @ 6.p @ 

### "F Fan Rated RP. OpttaI:ia, Volts Opcr.Wn: Amps

____­



# - . : l'Tt :ioiUltOT F'lCldNo. Primary 

### Prim;uy**S~ODdasy** Ser.:ondary Spark Ram Voltage (volts) Cur.rent (amps) Voltage (J{)I) CwrC!1t (ma) (per min) 

# I**.~** 

# ,
, 

## i I

# !
,**~** 

# I ; ·1 r ! Op=r;ting AJ:nps ---- Ap 

### inH.O Opeming VolU

____ Pl:rSol'l R:spomil:lle fer D9tI .:.;M;;.:::lt;:;;;tt.;;.P.;;.;I:lIlllil=OI1=-

_________**Si~** 

### _______________________**~~** 

### ________ Tltie.ifasitiaEl Ct\1.Sh Plant SUEenntec.de-p.t

LOReceivedo 1/ 5/ 6 3:41PM; 7122791235 -> Thompson Envir**Cns~t;** Page 4 01/05/2006 14:37 FAX 7122791235 CARGILL SC CRUSH 

### I4J 004 

# I**~.** 

# •

1· 

### Cotnpliance Emission Test Operating Data

OWner: Cargill • Sioux City gate: December 12.15,2005 Source: EP 2, Bean Dust Bllg Filter Permit #: 95-A-!l24-S8

Maximum Continuous Proce:ss**R~e** (Manufacturer's Rating),

___ 1.-87_
.... 5
....

tOD=sIh,r;;...f

_________ Historical Average Process**Rate:..-----'-Nc.;..A-"----~** ____**~~~---** ________ Hialorical Maximum Process**~te.** __ N
....

A:.o.-

___-

___ __**~-_~~~_~** Types and Sources ( 

### if any ) of Fuels normally Bumed._.:...;N:...,:A---'-

____________ Type of Fuel Burned During this test'---;..:.N::..:A=----

________**-~** ________ If fuel Is UlJed Approximate Quantities of eacll listed above burned AnI'1Ui;llly_
...**N_A~** ___**~-** Recycling Capability No 

## X

, Recycling in Progress No 

## X I
I 

# •

Proc:t$$ Rate (gallhr, Iblhr. tonslhr. etc.•. ) Proc;ess Rate Wet 

### Peroe"t Moisture ("/.'**Pro~ess** Rate 

### Dry How Proc&$S Rate was Detennined 

### Run 1 Run 2" RunS I 

## Y7.S**~r/J.** 

# .. 

# rr-7. t(**Ip....~,..** 

### 1'77.)-A-f/).
..



# .**p~c.e(,.S ~cJ.1.**  p....,n ...

### ~"""**Slghature~** 

# , Title/PDsitionCI1.llJh Plant St;pcrintendent

ow Plsase jndicat, 

### in the same !wit§. 

### as your Iljstprica/ information 

# • IRace.i.ved: 1/ 5/ IS 3:41 PM; 7122791235 -> Thompson Env.i.r**CnB~t;** Page S 01/05/2006 14:37 FAX 7122791235 CARGILL SC CRlTSH 

### I4J 005



### AIR POU.unON 

### CONnOL EQUlP:MENT OPERATING DATA
Plant 

### C:Ulill- Sioux. City,.
. L.rx:;:u,ioilSiQUX City, IA 

### Soun;c 

### type EP 2, Beall Dust Bag FIlter R.a1cd. Prgd.ul;tion 1 B 7.5 tonslhr Actu.al**I'roductiQn---------~-** DaI:c**D~~** 12.IS,**:z()O~ r~**  

# ___"'--**~No.** 

## _____________________ JJ: Pto-w Oam

_____.-_--_ Mcebapi!ljl! Cl'tntetor: 

### T. Dia. in.. 

### Number oiTIibes Dc:rigrt**~p** ___**~-,in.** 

### HiO (]as Temp

__ -......_"" 0b$c:ver:l6p
. in H10**Dm~** dlnItube@ Observed Ap • @ " Fan 

### Rated H.P.
_ Opcr4I:iDs Volf!l Operadll.S' A.lt\ps

________ '1: Prtcil:ritator F'JdI1NQ. Pr.ima.ry Pri.m.aty Sc::aud.a.ry 

### Set;ondiuy 

### SFkP.atc VottaSC: (volts) CUITeDC (alPPS) VQIr.ap: (KV) Current (ma) (per min) 

# -

ScrubCcr: T1)'C _.**-...,,~** _______-::-**Ap(~sc;mbbu) _~._~**  _____ .in 

### HzO· Fa RlJ.tl'ld liP Operating Volts _---:____ Operating.Amps

___**~_** L1quid. Cltt'Ulalion Rale gal/min. % .Ma.Icc-up
___ BlowdoWl1

____ gpm SribWgWam 

### Chal3S'= tnwva.I
_ .....__________________..- Stttllilg Tank Cle:uting lnrerva.l

Ap _.. inHtO Diameter

___........**~-** 

### Fa.n R.:1ted f.l'p**_~** _____ Opentin8 Volts
_____ OpmJ,tillg Amps

___......,,... 

### Puson**P.~nsible** for 

### Dm .;;..Ma;;:..:....It_Pe.;;.....ar;;;.::s;.oion.,;......

___........**~~** ___ Signatm'l:l

__________**~~** ______ T1IItlPasir:ion Crusb Plant SuperinttndeQL Cvc:!one; 

### Type:**~=-** 

# ________

to

# Appendix G Opacity Certification­



# ·e

# VISIBLE EMISSIONS EVALUATOR
This is to certify that 

# Jay 

# Titus

met the specifications ofFederal Reference Method 9 (40 CFR Part 60, Appendix A, Method 9) and qualified as a visible emissions evaluator. Maximum deviation on white and black smoke did not exceed 7.5% opacity and no single error exceeding 15% opacity was incurred during the certification test conducted 

# by Opaque Smoke School, LLC of Overland Park, Kansas. This certificate is valid for six months from date of issue. '

Des Moines, lA October] 1, 2005 6036



### Location 

### Date of Issue Certificate Number

Presideni/Director of Training