## west virginia department of environmental protection

Division of Water and Waste Management Earl Ray Tomblin, Governor 601 57th Street SE Randy 

## C.Huñinan, Cabinet Secretary Charleston, West Virginia 25304-2345 

### www.dep.wv.gov Phone: 304-926-0495 Fax: 304-926-0496 

## ANDREW JKICINSKI, PRESIDENT September 

## 25,2012 RESERVE ENVIRONMENTAL SERVICES OHIO COUNTY WV LLC 99 PENINSULA ST 91 7199 9991 7031 5500 0092 WHEELING, WV 26003

CERTIFIED RETURN RECEIPT REQUESTED
Dear Permittee:
Enclosed please 

## find WV/NPDES Permit Number 

## WV0116441 dated September 

## 25,2012.

Please note that 

## aDischarge 

## Monitoring Report 

## (DMR) is to be completed and submitted to 

## this Division each quarter.


## Finally note that copies 

## ofall future correspondence regarding the permit must be forwarded to the 

## Field Inspector 

## and Field Supervisor 

## atthe 

## following address:



## Also, please note the attachment to 

## this permit 

## which describes the 

## annual permit fee 

## requirement. If you have 

## any questions, please contact 

## John Lockhart, 

## P.E.of this Division at 

## (304) 926-0499 at extension 

## 1028.

Sincerely,



## o Patel, 

## P.E. Chief Engineer 

## YP:jl Enclosures



## Prornoting a healthy environrnent

### Permit Number: 

## WV0116441

Permittee: 

## RESERVE ENVIRONMENTAL SERVICES OHIO O

ce: 

## Env. Insp. Supv. Env. Insp.

### STATE OFWEST VIRGINIA DEPARTMENT OF ENVIRONMENTAL PROTECTION DIVISION OF WATER AND WASTE MANAGEMENT

601 57TH STREET SE CHARLESTON, WV 25304-2345


### NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM

WATER POLLUTION CONTROL PERMIT 

### NPDES PERMIT 

## NO.:WV0116441 ISSUE DATE: September 25,2012 SUBJECT: Industrial Waste EFFECTIVE DATE 

## :November 01, 2012 

### EXPIRATION DATE: 

### September 24, 2017 

### SUPERSEDES:N/A

LOCATION: 

## WHEELING Ohio Upper Ohio River 2

(City) (County) 

### (Drainage Basin) See the next page for a list of Outlets. TO WHOM IT 

### MAYCONCERN: 

## This isto certify 

## that: RESERVE ENVIRONMENTAL SERVICES 

## OHIO COUNTY 

## WV LLC 99 

## PENINSULA ST WHEELING, WV 26003 

## is hereby granted 

## aWest Virginia 

## NPDES Water 

## Pollution Control Permit 

## to: acquire, construct, install, operate 

## and maintain 

## azero discharge wastewater treatment system and best management practices 

## consisting of sedimentation, neutralization, chemical precipitation, flocculation, and 

## coal filtration operations designed to treat 

## oil andgas industry 

## drilling, development, and produced wastewater from offsite sources 

## for return 

## and/or reuse by 

## theoil and gas 

## industry. acquire, construct, install, operate 

## and maintain 

## adisposal system 

## andbest management practices 

## for the direct discharge 

## of untreated storm water 

## via Outlet 001; to Wheeling 

## Creek, atributary 

## of the 

## Ohio River approximately 

## 2.2miles from its mouth. This permit is subject to the following terms and conditions 

## : The 

## information submitted on and 

## with Permit 

## Application No. WV0116441 dated the 4th day 

## ofApril, 2012, is 

## all hereby made terms 

## and conditions of this Permit with 

## like effect as

## if all such permit application information were set forth herein and 

## with other 

## conditions set forth 

## in Sections 

## A, B, Cand Appendix 

## A.

The 

## validity of this permit 

## iscontingent 

## upon the payment 

## of the applicable annual permit 

## fee, as required 

## by Chapter 

## 22,Article 

## 11,Section 

## 10of the Code of West 

## Virginia.

# Page No.:2of11 Permit No. :WV0116441 nspectable Unit 

### Latitude Longitude 

### Receiving Stream 

## Dist.to Stream Milepost Mouth (in Mile) 

## 001 40°04'41" 80°43'07" WHEELING 

## CK 2.2 N/A

### A.001 DISCHARGE LIMITATIONS AND MONITORING REQUIREMENTS: 

### Final Limitations Year Round

During the period beginning 11/1/2012 and lasting through midnight 9/24/2017 

### the permittee isauthorized to discharge from Outlet Number(s) 001 (Storm Water 

### Runoff)
Such discharges shall be 

### limited and monitored by the permittee as specified below: Monitoring Requirements Effluent Discharge Limitations Measurement Sample Characteristic Quantity 

### Unus Other Units 

### Unia Freguency 

### Tym Flow,in Conduit or thru 

### plant N/A N/A N/A N/A Rpt Only Rpt Only mgd 1/quarter Estimated (Year Round) (ML-1) Avg. Monthly Max. Daily 

### BOD, 5-Day 20 

### Deg.C N/A N/A N/A N/A RptOnly Rpt Only mg/I 1/quarter Grab (Year Round) (ML-1) Avg. Monthly Max. Daily


### Total Suspended Solids N/A N/A N/A N/A RptOnly Rpt Only mg/I 1/quarter Grab (Year Round) (ML-1) Avg. Monthly Max. Daily 

### pH N/A N/A N/A Rpt Only N/A Rpt Only S.U. 1/quarter Grab (Year Round) (ML-1) inst. Min. Inst. Max. 

### Nitrogen, Total (as N) N/A N/A N/A N/A Rpt Only Rpt Only mg/l 1/quarter Grab (Year Round) (ML-1) Avg. Monthly Max. Daily 

### Aluminum, Total Recoverable N/A N/A N/A N/A Rpt Only RptOnly mg/I 1/quarter Grab (Year Round) (ML-1) Avg. Monthly Max. Daily
Chloride 

### (as Cl) N/A N/A N/A N/A Rpt Only RptOnly mg/I 1/quarter Grab (Year Round) (ML-1) Avg. Monthly Max. Daily 

### Fluoride, Total N/A N/A N/A N/A Rpt Only RptOnly mg/l 1/quarter Grab (Year Round) (ML-1) Avg. Monthly Max. Daily


### TotalToxic Organics (TTO) N/A N/A N/A N/A Rpt Only RptOnly mg/l 

### 1/6 months Grab (Year Round) (ML-1) Avg. Monthly Max. Daily

Samples taken in compliance with the monitoring requirements specified above shall betaken atthe following location(s): Outlet 001: 

### 12"castinplace concrete 

### pipe.
This discharge shall not cause violation ofTitle 47, Series 

### 2,Section 

### 3,of the West Virginia Legislative Rules issued pursuant to Chapter 22B, Article 

## 3. Page No.: 3 

### of 11 

### Permit 

## No.: WV0116441

# A.001

DISCHARGE LIMITATIONS AND MONITORING REQUIREMENTS: 

### Final Limitations Year Round

During the period beginning 11/1/2012 and 

### lasting through midnight 9/24/2017 the permittee isauthorized to discharge from Outlet Number(s) 001 (Storm Water Runoff)
Such discharges shall be limited and monitored by the 

### permittee as specified below: Monitoring Requirements Effluent Discharge Limitations Measurement Sample Characteristic Quantity Ung Other Units Freauency Tyge 

### Iron, Total (as Fe) N/A N/A N/A N/A Rpt Only RptOnly mg/I 1/quarter Grab (Year Round) (ML-1) Avg. Monthly Max. Daily


### Sulfate N/A N/A N/A N/A Rpt Only RptOnly mg/I 

### 1/quarter Grab (Year Round) (ML-1) Avg. Monthly Max. Daily


### Chem. Oxygen Demand N/A N/A N/A N/A Rpt Only Rpt Only mg/l 1/quarter Grab (Year Round) (ML-1) Avg. Monthly
. Max. Daily 

### Oliand Grease, Hexane EXTR. N/A N/A N/A N/A Rpt Only RptOnly mg/I 1/quarter Grab (Year Round) (ML-1) Avg. Monthly Max. Daily
Total 

### Dissolved Solids (TDS) N/A N/A N/A N/A Rpt Only RptOnly mg/I 1/quarter Grab (Year Round) (ML-1) Avg. Monthly Max. Daily 

### Radiation, Gross Alpha N/A N/A N/A N/A Rpt Only RptOnly pCi/L 

### 1/quarter Grab (Year Round) (ML-1) Avg. Monthly Max. Daily 

### Radiation, Gross Beta N/A N/A N/A N/A Rpt Only RptOnly pCi/L 

### 1/quarter Grab (Year Round) (ML-1) Avg. Monthly Max. Daily 

### Radium 226 and 

### 228, Totai N/A N/A N/A N/A Rpt Only Rpt Only pCi/L 1/quarter Grab (Year Round) (ML-1) Avg. Monthly Max. Daily 

### Strontium, Total (as Sr) N/A N/A N/A N/A RptOnly Rpt Only mg/I 1/quarter Grab (Year Round) (ML-1) Avg. Monthly Max. Daily

Samples taken in compliance with the monitoring requirements specified above shall betaken atthe following location(s): Outlet 001: 12" cast in place concrete pipe.
This discharge shall not cause violation of Title 47, Series 

### 2,Section 

### 3,ofthe West Virginia Legislative Rules issued pursuant to Chapter 

### 22B,Article 

## 3. Page 

## No.:4of 11 Permit 

## No.:WV0116441

# A.001

DISCHARGE LIMITATIONS AND MONITORING REQUIREMENTS: 

### Final Limitations Year Round

During the period beginning 11/1/2012 and 

### lasting through midnight 9/24/2017 the permittee isauthorized to discharge 

### from Outlet Number(s) 001 (Storm Water Runoff) Such discharges shall be limited and monitored by the 

### permittee as specified below: Monitorinq Requirements Effluent Discharge Limitations Measurement Sample Characteristic Quantity Units_ Other Units Freguency Tyge 

### Lithium, Total (as Li) N/A N/A N/A N/A Rpt Only RptOnly mg/I 1/quarter 

### Grab (Year Round) (ML-1) Avg. Monthly Max. Daily 

### Bromide N/A N/A N/A N/A Rpt Only RptOnly mg/l 1/quarter Grab (Year Round) (ML-1) Avg. Monthly Max. Daily

Samples taken in compliance with the monitoring requirements specified above shall be taken 

### atthe following location(s): Outlet 001: 

### 12"castinplace concrete 

### pipe. This discharge shall not cause violation ofTitle 47, Series 

## 2,Section 

### 3,of the West Virginia Legislative Rules issued pursuant to Chapter 22B, Article 

## 3. Page No.: 5 of 11 Permit 

## No.:WV0116441

# Page No.:6of 11 Permit No.: WV0116441 

# B. SCHEDULE OF COMPLIANCE 1. The permitee shall achieve compliance with the provisions for waste treatment and the monitoring requirements specified in the permit in accordance with the following schedule : Effective date ofpermit.
2. Reports of compliance or non-compliance 

### with, and progress reports on interim and final requirements contained in the above compliance schedule, if 

### any, shall bepostmarked no later than 14days following each schedule 

## date.

### Page 

## No.: 7of 11 Permit No.: WV0116441



## Section C

- 

## Other Requirements 01. Thepermittee shall practice good housekeeping including maintaining the facility grounds. There shall beno scattered parts, equipment, debris, etc. Any andall drums shall beeither stored in acovered areaor kept upon pallets andproperly sealed. 

## 02. Theissuance ofthis permit shall not relieve the permittee ofthe obligation to comply with any other 

### federal, state 

### orlocal 

## laws. Compliance with this permit does not relieve the permittee from the 

### obligation of Section 311 of the 

### Clean Water 

## Act. This permit doesnot authorize spills of hazardous substances/wastes from anypermitted outlet into waters ofthe 

### State. Such incidents aretobereported in accordance with Sections 

## IV.1 and 

## IV.2 of Appendix A ofthis permit. Specifically, the 

### permittee must 

### evaluate if the wastewater being collected 

### atthe treatment 

### facility isahazardous waste 

### (for instance acharacteristic waste 

### under 40 CFR 

## 261.24). If the wastewater 

### isahazardous waste, the 

### permittee must evaluate whether it

### qualifies asapermit by rule facility under 40 CFR 270.60(c) and meet 

### notification, manifest, and reporting requirements 

### including any more stringent state 

### hazardous waste 

### requirements. 

## 03.Upon review of information submitted 

### under terms 

### and conditions ofthis permit, thepermit may bemodified to 

### require additional effluent limitations/monitoring requirements and/or improved best 

### management practices. 

## 04.The permittee shall notify the Division of Water and Waste 

### luanagement immediately when it becomes aware of anymigration of anypollutant from any unpermitted 

### source (such ascontaminated groundwater 

### and/or storm water) into surface waters ofthe State. 

## 05.The permittee may accept wastewater 

### from treatment 

### and disposal orrecycle from the Oil & Gasindustry. The wastewater 

### approved for acceptance from all sources isnatural gaswell development andproduction water 

## only. No otherwastewater types may beaccepted without prior approval from the 

### agency. Without prior approval from theagency, the permittee 

### shall not 

### accept and treat 

### wastewater from anyother facility. 

## 06.The permittee shall submit eachquarter according to the enclosed format, aDischarge Monitoring Report 

### (DMR) indicating in terms of concentration and/or quantities the 

### values ofthe constituents listed in Section A analytically determined to beinthe plant effluent(s). Additional information pertaining toeffluent monitoring and reporting can befound in Section III ofAppendix 

## A. 07.The required DMRs shall bereceived bythe agency no later than 20daysfollowing the end of thereporting period in accordance with the following requirements. The agency isnow requiring the permittee toutilize ourelectronic discharge monitoring report (eDMR) system 

### which isnow mandatory. Thepermittee is not 

### required to submit hard copies ofthe DMRs tothe addresses listed below when using 

## eDMR. Special circumstances may result inthe agency granting anexemption toeDMR and areconsidered on casebycase

## basis. If the permittee was exempted by the 

### agency from using the eDMR system, thenthe permittee 

### isrequired tosend hard copies to 

### the addresses 

## below. The permittee may contact the agency for more information about the 

### eDMR system 

### and potential exemptions from using 

## it. Regardless, in accordance with Appendix 

## A, Section 

## III.6 ofthis permit, thepermittee shall maintain copies of DMRs (either 

### hard copies or electronic 

### copies) atthe 

### plant site 

### andthe 

### DMRs shall be madereadily available upon request for DEP personnel. 

## a. Director Division of Water and Waste Management 601 57th Street, SE Charleston, West Virginia 25304 Attn: Permitting Branch

Department of Environmental Protection Environmental Enforcement 131 A Peninsula Street Wheeling, West Virginia 26003

### Page No.: 8of 11 

### Permit 

## No.:WV0116441



## Section C

-

## Other Requirements 08. Any 

## "notdetected 

## (ND)" results by the 

### permittee must be

## "ND" atthe method 

### detection limit (MDL) for the test method used for that parameter and must 

### be reported 

### aslessthanthe MDL 

## used. The permittee may not report the 

### result aszero, 

## "ND", or report theresult aslessthan aminimum level (ML), reporting limit 

## (RL), or practical quantitation limit 

## (PQL). When averaging values of analytical results for DMR reporting purposes for monthly averages, the 

### permittee should useactual analytical results when these results aregreater than 

### orequal tothe MDL and should usezero (0) when these results are lessthan the

## MDL. If all analytical results are non-detect 

### atthe MDL 

## (<MDL), thenthe permittee should usethe actual MDL in thecalculation for averaging andreport the 

### result aslessthan the 

### average calculation. 

## 09. In incidences where aspecific test 

### method isnot defined, the permittee shall utilize an EPA approved method 

### with a method detection limit 

### (MDL) sensitive enough to 

### confirm compliance with the 

### permit effluent limit 

### for that 

### parameter. If aMDL is not 

### sensitive enough to confirm 

### compliance, themost sensitive approved method must 

### be 

## used. If amore sensitive EPA approved method 

### becomes available, that method 

### shall be

## used. Should the current 

### and/or new method not be sensitive enough to 

### confirm compliance with the permitted 

### effluent 

## limit, analytical results reported 

### as

## "notdetected" at 

### theMDL ofthe most 

### sensitive method available will bedeemed compliant for purposes ofpermit compliance. Results shall be reported 

### ontheDischarge Monitoring Reports asanumeric value lessthanthe 

## MDL. 10.The permittee 

### shall not 

### usealternate 

### DMRs without prior approval from this Agency. 

## 11.The Groundwater Protection 

### Plan (GPP) shall bemaintained at

### theplant site 

### and shall beavailable for inspection by the 

### Division of Water 

### andWaste 

### Management personnel. 

## 12.The permittee shall implement andmaintain itsexisting 

### storm water pollution prevention plan (SWPPP) for the site. The SWPPP shall beimplemented in accordance with good engineering practices. The SWPPP shall identify potential sources ofpollution which may reasonably beexpected to affect the quality of storm 

### water discharges associated with the industrial activity. In addition, the plan shall describe and ensurethe implementation of practices which areto 

### be usedto reduce the pollutants in storm water discharges associated with the 

### industrial activity atthe 

### facility and toassurecompliance with the terms and conditions ofthis permit. A copy of this document shall beretained atthesite for review upon request. 

## 13.The following storm water requirements apply to 

### Outlet 001: 

## a. Samples shall becollected from the discharge resulting from astorm 

### event that isgreater than 

## 0.1 inches in magnitude and that 

### occurs atleast 72hours from the 

### previously measurable (greater than 

## 0.1 inch rainfall) storm event. Samples shall betaken during the first thirty 

### (30) minutes, or assoon thereafter aspracticable, of the storm event. 

## b. Each outlet 

### shall bemonitored separately. C. Pollutant Benchmark Value Biological oxygen Deman 30 mg/l Chemical oxygen Demand 120 mg/1 Total Suspended Solids 100 mg/l Total Nitrogen 5 mg/1 oil and Grease 15 mg/1 Chloride 860 mg/l Iron 1 mg/1 Aluminum 0.75 mg/1 Radiation, Gross Beta 1000 pCi/1 Radiation, Gross Alpha 3 pCi/1 Radium 226 + 228 5 pCi/1 Total Toxic organics 1 mg/1 Fluoride 

## 1. 8 mg/l Bromide (as Br) 0.052 mg/l* Lithium 0.065 mg/l* Strontium 

## 9.6 mg/l* pH 

### 6.0 to 

### 9.0 

## S.U.

* 1/10 Lowest LC50 (EPA ECoToX)

### Page 

## No.:9of 11 

### Permit 

## No.:WV0116441



## Section C

-

## Other Requirements 13.c. When the concentration results from aminimum of four consecutive 

### samples of apollutant areall lessthan the corresponding benchmark value for the pollutant, additional monitoring for the pollutant isnot required (all pH values ofthe samplesmust bewithin therange 

## 6.0to

## 9.0S.U.). The facility shall submit, each

## year,to the 

### Division of Water and Waste Management, in lieu ofthe monitoring data, acertification (form will be provided upon request) that 

### there hasnot beenasignificant change inthe industrial activity orthe pollution prevention measures in the areaofthe facility that 

### drains tothe outlet for which sampling isto 

### be

## waived. If theconcentration 

### of apollutant exceeds the corresponding benchmark concentration or apH value isnot within the 

### rangeof 

## 6.0to

## 9.0S.U.,monitoring shall becontinued and storm water pollution prevention practices shall berevised and implemented. A letter stating therevised and implemented storm water pollution prevention practices shall besubmitted to 

### the Division of Water 

### and Waste Management atthe address listed in Section 

## C.07. 14.Ifthere isevidence indicating potential or realized impacts on water quality 

### dueto any storm 

### water discharge 

### associated with industrial activity covered by this permit, the permit 

### may bepromptly modified and/or reissued to include effluent limitations and/or other requirements tocontrol such 

### storm water 

### discharges. 

## 15.Thepermittee shall utilize EPA Method 

## No. 1664A (gravimetric analysis using the hexane extractable method [HEM]) for the analysis of oil and grease. 

## 16.There shall be nodischarge ofany process wastewater 

### from any outlet. 

## 17.Ifanyportion of the 

### Permittee's discharge that 

### isidentified asbeing subject to 

### Federal Effluent Guideline(s) and the 

### new orrevised requirements ofthe Federal Effluent Guideline(s) arenot currently inthis permit, the Director 

### may reopen or reissue this permit to 

### incorporate additional, more stringent requirements or limitations. 

## 18.Thepermittee shall dispose of any solid waste generated by the wastewater treatment 

### plant in accordance with all applicable disposal regulations. 

## 19.Effluent monitoring for the following pollutants shall beconducted using the most sensitive methods and detection levels commercially available and economically feasible. The following methods aretobeusedunless the permittee desires touseanEPA Approved Test Method with alisted lower method detection 

## level. Regardless, it is recognized that 

### detection levels canvary from analysis to 

### analysis andthat non-detect 

### results atadifferent MDL for the specified test method would not constitute 

## apermit violation. Parameter EPA Method 

### No. Method Detection Level (ug/1)

Gross Alpha Radiation 900.0 

### 1.0 (pCi/1) Gross Beta Radiation 900.0 

## 4.0 (pCi/1) Radium 226 903.1 

## 0.1 (pci/1) Radium 228 904.0 

## 1.0 (pCi/1) Lithium 200.7 

### 1.0 Bromide 300.1 14 

## 20. The permittee 

### shall not accept 

### anydrilling or development wastewater 

### from offsite sources that contain 

### measurable amounts of Technically Enhanced 

### Natural Occurring Radioactive Materials (TENORM) above background concentrations (asdefined by 64CSR 23 ofthe West 

### Virginia Legislative Rules) without prior certification from theWV Department 

### ofHuman 

## Health. The permittee must modify this permit upon certification to accept 

### TENORM wastewater. Thepermittee shall not accept anydrilling or development wastewater 

### from offsite sources that contain more than one-twentieth 

### of onepercent 

## (0.05%) ofuranium, thorium, or anycombination thereof (Source Material) without prior certification from the Nuclear Regulatory Commission. The permittee must modify this permit upon certification to accept Source Material wastewater.

# Page No.: 10 

### of 11 Permit No.: WV0116441



## Section C
- Other Requirements 21.The permittee 

### shall perform and submit tothe agency the 

### results of routine radiation surveys onatleastaonce per year

## basis.The first radiation survey shall beperformed onof before 6months after theacceptance and treatment of oil andgaswastewater begins. Theradiation survey shall beperformed by aprofessional radiation specialist or a health physicist. The survey, ataminimum, shall beconducted by utilizing radiation survey meters, integrated radiation measuring devices to determine potential exposure over time, and sampling ofunit operation equipment, wastes,and wastewater via laboratory analysis focusing on radium, uranium, thorium, and potassium aswell astheir radioactive daughter decay products. Upon identification ofany radioactively contaminated equipment the permittee shall immediately initiate amonitoring program, establish aworker radiation safety and education program, and decontaminate buildings, equipment, and/or facilities.

# Page No.: 11of 11 Permit 

## No.: WV0116441

The herein-described 

### activity istobeextended, modified, added

## to, made, enlarged, acquired, constructed 

### or installed, and operated, used andmaintained strictly in accordance with the terms and conditions of this 

## permit, with theplans and specifications submitted with Permit 

### Application 

## No.WV0116441; with the plan ofmaintenance and method of operation thereof submitted with suchapplication(s); and with any applicable rules andregulations promulgated by the 

### Environmental Quality Board andthe Secretary of the Department 

### ofEnvironmental Protection. Failure to 

### comply with the terms and 

### conditions of this 

### permit, with 

### the plans andspecifications submitted 

### with Permit Application 

## No.WV0116441; and with 

### the plan ofmaintenance and method 

### ofoperation thereof submitted with 

### suchapplication(s) shall constitute grounds for the revocation or suspension of this 

### permit and the 

### invocation of all theenforcement 

### procedures set

### forth in Chapter 

## 22,Article 

## 11,or 15of the Code of West 

### Virginia. This permit is issued in accordance with 

### theprovisions of Chapter 

## 22, Article 11 and 

### 12and/or 15of the 

### Code of West 

### Virginia andistransferable under the 

### terms of Section 11 ofArticle 

## 11.

Scott 

## G.Mandirola, Director

## Appendix 

# A 

# I. MANAGEMENT CONDITIONS: 

## 1. Duty to Comply

a) The permittee must comply with all conditions of this permit. Permit noncompliance constitutes aviolation of the CWA and State Act and is

grounds for enforcement action; for permit modification, revocation and reissuance, suspension or revocation; orfor denial of a permit renewal application, b) The permittee shall comply with all effluent standards orprohibitions established under Section 307(a) of the CWA for toxic pollutants within

the time provided in the regulations that establish these standards or prohibitions, even if the permit hasnot yet been modified to incorporate the requirement. 

## 2. Duty to Reapply

If the permittee wishes to continue anactivity regulated by this permit after the expiration date of this permit, the permittee must apply for a new permit at least 180days prior toexpiration of the permit. 

## 3. Duty to Mitigate

The permittee shall takeall reasonable stepsto minimize orprevent any discharge inviolation of this permit, which has areasonable likelihood of adversely affecting human health orthe environment. 

## 4. Permit Actions

This permit may be modified, revoked and reissued, suspended, or revoked for cause. The filing of arequest by the permittee for permit modification, revocation and reissuance, or revocation, oranotification of planned changes or anticipated noncompliance, does not stay any permit condition. 

## 5. Property Rights

This permit does not convey any property rights of any sort or any exclusive privilege. 

## 6. Signatory Requirements

All applications, reports, or information submitted to the Director shall be signed and certified as required in Title 47, Series 10 

### ,Section 4.6 of the West Virginia Legislative Rules. 

## 7. TransfersThis permit is not transferrable to any person except after notice to the Director. The Director may require modification or revocation and reissuance of the

permit to change the name of the permittee and incorporate such other requirements as may benecessary. 

## 8. Duty to Provide Information

The permittee shall furnish to the Director, within a reasonable specified time, any information which the Director may request to determine whether cause exists for modifying, revoking and reissuing, suspending, or revoking this permit, orto determine compliance with this permit. The permittee shall also furnish to the Director, upon request, copies of records required to bekept bythis permit. 

## 9. Other Information

Where the permittee becomes aware that it failed to submit any relevant facts in apermit application, or submitted incorrect information in a permit application or in any report to the Director, it shall promptly submit such facts orinformation. 

### 10. Inspection and Entry

The permittee shall allow the Director, oranauthorized representative, upon the presentation of credentials and other documents as may be required by law, to: a) Enter upon the permittee's premises inwhich aneffluent source or activity is located, or where records must bekept under the conditions of this

permit; b) Have access to and copy atreasonable times, any records that must be kept under the conditions of this permit; c) Inspect at reasonable times any facilities, equipment (including monitoring and control equipment), practices, or operations regulated or

required under this permit; and d) Sample ormonitor at reasonable times, for the purposes of assuring permit compliance or asotherwise authorized by the State Act, any

substances orparameters at any location. 

### 11.Permit Modification

This permit may bemodified, suspended, or revoked in whole or in part during its term inaccordance with the provisions of Chapter 22-11-12 of the Code of West Virginia. 

### 12.Water Quality

Subject to 47 WV CSR 10.3.4.a, the effluent or effluents covered by this permit are to beof such quality soasnot to cause violation of applicable water quality standards. 

## 13.Outlet Markers

A permanent marker atthe establishment shall be posted in accordance with Title 47, Series 11, Section 9of the West Virginia Legislative Rules. 

### 14.Liabilities

a) Any person who violates a permit condition implementing sections 301, 302, 306, 307, 308, 318, or 405 of the Clean Water Act issubject to a

civil penalty not to exceed $25,000 per day of such violation. Any person who willfully or negligently violates permit conditions implementing sections 301, 302,306,307, 308 or405 of the Clean Water Act issubject to afine of not less than $2,500 nor more than $25,000 per day of violation, orby imprisonment for not more than 1year, orboth. b) Any person who falsifies, tampers with, orknowingly renders inaccurate any monitoring device or method required to bemaintained under

this permit shall, upon conviction, bepunished by afine of not more than $10,000 per violation, orby imprisonment for not more than 2 years, orbyboth. c) Any person who knowingly makes any false statement, representation, or certification in any record orother document submitted or required to

bemaintained under this permit, including monitoring reports or reports of compliance ornoncompliance shall, upon conviction, be punished by afine of not more than $10,000 per violation, or by imprisonment for not more than 2years, or byboth, d) Nothing in I.14a), b),and c) shall beconstrued to limit or prohibit any other authority the Director may have under the State Water Pollution

Control Act, Chapter 22, Article 

### 11.

## II. OPERATION AND MAINTENANCE: 

## 1. Proper Operation and Maintenance

The permittee shall at all times properly operate and maintain all facilities and systems of treatment and control (and related appurtenances) which are installed orused bythe permittee toachieve compliance with the conditions of this permit Proper operation and maintenance also includes adequate laboratory controls, andappropriate quality assurance procedures. Unless otherwise required by Federal orState law, this provision requires the operation of back-up auxiliary facilities orsimilar systems which areinstalled bythe permittee only when the operation is necessary to achieve compliance with the conditions ofthe permit. For domestic waste treatment facilities, waste treatment operators asclassified bythe WV Bureau of Public Health Laws,

## W.Va. Code Chapter 16-1, will berequired except that incircumstances where thedomestic waste treatment facility is receiving any type of industrial waste, the Director may require a more highly skilled operator. 

## 2. Need to Halt or Reduce Activity Not a Defense

Itshall not beadefense for a permittee in an enforcement action that it would have been necessary to halt or reduce the permitted activity in order to maintain compliance with the conditions of thepermit. 

## 3.Bypass a) Definitions (1) "Bypass" means the intentional diversion of waste streams from any portion of atreatment facility; and (2) "Severe property damage" means substantial physical damage to property, damage to the treatment facilities which causes them to

become inoperable, or substantial and permanent loss of natural resources which can reasonably be expected to occur in the absence of abypass. Severe property damage does not mean economic loss caused bydelays in production. b) Bypass not exceeding limitations. The permittee may allow any bypass to occur which does not cause effluent limitations to be exceeded, but

only ifit also isfor essential maintenance to assure efficient operation. These bypasses are not subject to the provision of II.3.c) and II.3.d) of this permit. c) (1) If the permittee knows in advance of the need for a bypass, it shall submit prior notice, if possible atleast ten (10) days before the date of the bypass; (2) If the permittee does not know in advance of the needfor bypass, notice shall besubmitted as required in IV.2.b) of this permit. d) Prohibition of bypass

(1) Bypass is permitted only under the following conditions, and the Director may take enforcement action against a permittee for a bypass, unless; (A) Bypass was unavoidable to prevent lossof life, personal injury, orsevere property damage; (B) There were no feasible alternatives tothe bypass, such asthe use of auxiliary treatment facilities, retention of untreated

wastes, or maintenance during normal periods of equipment downtime. This condition is not satisfied if adequate backup equipment should have been installed in the exercise of reasonable engineering judgement to prevent abypass which occurred during normal periods of equipment downtime or preventative maintenance; and (C) The permittee submitted notices as required under II.3.c) of this permit. (2) The Director may approve an anticipated bypass, after considering its adverse effects, ifthe Director determines that it will meet the

three conditions listed in II.3.d.(1) of this permit. 

## 4. Upset a) Definition. "Upset" means an exceptional incident in which there is unintentional and temporary noncompliance with technology-based permit effluent limitations because of factors beyond the reasonable control of the permittee. An upset does not include noncompliance to the extent caused by operational error, improperly designed treatment facilities, inadequate treatment facilities lack of preventative maintenance, or careless or improper operation. b) Effect of an upset. An upset constitutes anaffirmative defense to anaction brought for noncompliance with such technology-based permit

effluent limitation if the requirements of II.4.c) aremet. No determination made during administrative review of claims that noncompliance was caused by upset, and before anaction for noncompliance, isfinal administrative action subject tojudicial review. c) Conditions necessary for ademonstration of upset. A permittee who wishes to establish the affirmative defense of upset shall demonstrate,

through properly signed, contemporaneous operating logs, or other relevant evidence that: (1) An upset occurred and that the permittee can identify the cause(s) of the upset; (2) The permitted facility was at thetime being properly operated; (3) The permittee submitted notice of the upset as required in IV.2.b) of this permit. (4) The permittee complied with any remedial measures required under I.3.of this permit. d) Burden ofproof. In any enforcement proceeding the permittee seeking to establish theoccurrence of an upset hasthe burden ofproof. 

## 5. Removed Substances

Where removed substances arenot otherwise covered bytheterms and conditions of this permit or other existing permit bythe Director, any solids, sludges, filter backwash orother pollutants (removed in the course of treatment orcontrol of wastewaters) and which are intended for disposal within the State, shall be disposed of only in a manner and at asite subject tothe approval bythe Director. If such substances are intended for disposal outSide the State or for reuse, 

## i.e.,asamaterial used for making another product, which inturn hasanother use, the permittee shall notify the Director in writing of the proposed disposal or use of such substances, the identity of the prospective disposer or users, and the intended place of disposal or use, asappropriate.

## III. MONITORING AND REPORTING 

## 1. Representative Sampling

Samples and measurements taken for the purpose of monitoring shall berepresentative of the monitored activity. 

## 2. Reportinga) Permittee shall submit, according tothe enclosed format, a Discharge Monitoring Report (DMR) indicating in terms of concentration, and/or quantities, thevalues of the constituents listed in Part A analytically determined to bein the plant effluent(s). DMR submissions shall bemade in accordance with theterms contained in Section C of this permit. b) Enter reported average and maximum values under "Quantity" and "Concentration" in the units specified for each parameter, asappropriate. c) Specify the number of analyzed samples that exceed the allowable permit conditions inthe columns labeled 

### "N.E."(i.e., number exceeding). d) Specify frequency of analysis for each parameter as number of analyses/specified period (e.g.,3/month is equivalent to 3analyses performed

every calendar month). If continuous, enter "Cont.". The frequency listed on format isthe minimum required. 

## 3. Test Procedures

Samples shall betaken, preserved and analyzed in accordance with the latest edition of40CFR Part 136, unless other test procedures have been specified elsewhere in this permit. 

## 4. Recording of Results

For each measurement orsample taken pursuant to the permit, the permittee shall record the following information. a) The date, exact place, and time of sampling or measurement; b) The date(s) analyses were performed; c) The individual(s) who performed the sampling or measurement; d) The individual(s) who performed the analyses; if acommercial laboratory is used, the name and address of the laboratory; e) The analytical techniques ormethods used, and f) The results of such analyses. Information not required by the DMR form is not to besubmitted to this agency, but isto beretained as required

in III.6. 

## 5. Additional Monitoring by Permittee

Ifthe permittee monitors any pollutant at any monitoring point specified inthis permit more frequently than required bythis permit, using approved test procedures orothers asspecified in this permit, the results of this monitoring shall be included inthe calculation and reporting of the data submitted in the Discharge Monitoring Report Form. Such increased frequency shall also be indicated. Calculations for all limitations which require averaging of measurements shall utilize anarithmetic mean unless otherwise specified in the permit. 

## 6. Records Retention

The permittee shall retain records of all monitoring information, including all calibration and maintenance records and all original chart recordings for continuous monitoring instrumentation, copies of all reports required by this permit, and records of all data used to complete the application for the perrnit, for a period of at least three (3) years from the date of the sample, measurement, report or application. This period may be extended by request of the Director at any time. 

## 7. Definitions

a) "Daily discharge" means thedischarge of apollutant measured during acalendar day or within any specified period that reasonably represents

the calendar day for purposes of sampling. For pollutants with limitations expressed insnits of mass, the daily discharge is calculated asthe total massof the pollutant discharged over the day. For pollutants with limitations expressed in other units of measurement, the daily discharge is calculated asthe average measurement of the pollutant over the day. b) "Average monthly discharge limitation" means the highest allowable average of daily discharges over acalendar month, calculated asthe sum

of all daily discharges measured during acalendar month divided by the number of daily discharges measured during that month. c) "Maximum daily discharge limitation" means the highest allowable daily discharge. d) "Composite Sample" isacombination of individual samples obtained at regular intervals over atime period. Either the volume of each

individual sample is proportional to discharge flow rates orthesampling interval (for constant volume samples) is proportional to the flow rates over the time period used to produce the composite. The maximum time period between individual samples shall betwo hours. e) "Grab Sample" isan individual sample collected in lessthan 15minutes. f) 

### "is"= immersion stabilization

-acalibrated device is immersed in the effluent stream until the reading is stabilized. g) The "daily average temperature" means thearithmetic average of temperature measurements made on an hourly basis, or the mean value plot of

the record of acontinuous automated temperature recording instrument, either during acalendar month, orduring the operating month if flows areof shorter duration. h) The "daily maximum temperature" means the highest arithmetic average of thetemperatures observed for any two (2) consecutive hours during

a24 hour day,or during the operating day if flows are of shorter duration. i) The "monthly average fecal coliform" bacteria isthe geometric average of all samples collected during the month. j) "Measured Flow" means any method of liquid volume measurement, the accuracy of which has been previously demonstrated in engineering

practice, orwhich arelationship to absolute volume has been obtained. k) "Estimate" means to bebased on atechnical evaluation of thesources contributing to the discharge including, but not limited to pump

capabilities, water meters and batch discharge volumes. 1) "Non-contact cooling Water" means the water that is contained in a leak-free system, 

### i.e.,no contact with any gas, liquid, orsolid other than the

container fortransport; the water shall have nonet poundage addition of any pollutant over intake water levels, exclusive of approved antifouling agents.

## IV. OTHER REPORTING 

## 1. Reporting Spills and Accidental Discharges

Nothing in this permit shall beconstrued to preclude the institution of any legal action or relieve the permittee from any responsibilities, liabilities or penalties established pursuant toTitle 47, Series 11,Section 2 of the West Virginia Legislative Rules promulgated pursuant to Chapter 22, Article 11. Attached isacopy of the West Virginia Spill Alert System for use in complying with Title 47, Series 11, Section 2 of the Legislative rules asthey pertain to the reporting of spills and accidental discharges. 

## 2. Immediate Reporting

a) The permittee shall report anynoncompliance which may endanger health orthe environment immediately after becoming aware of the

circumstances by using theAgency's designated spill alert telephone number. A written submission shall be provided within five (5) days of the time the permittee becomes aware of the circumstances. The written submission shall contain adescription of the noncompliance and its cause; the period of noncompliance, including exact dates and times, and if the noncompliance has not been corrected, the anticipated time it is expected tocontinue; and stepstaken or planned to reduce, eliminate, and prevent recurrence of the noncompliance. b) The following shall also bereported immediately:

(1) Any unanticipated bypass which exceeds any effluent limitation in the permit; (2) Any upset which exceeds any effluent limitation in the permit; and (3) Violation of a maximum daily discharge limitation for any of the pollutants listed bythe Director inthe permit to be reported

immediately. This list shall include anytoxic pollutant or hazardous substance, or any pollutant specifically identified asthe method to control atoxic pollutant or hazardous substance. c) The Director may waive thewritten report on a case-by-case basis if the oral report hasbeen received in accordance with the above. d) Compliance with the requirements of IV.2 of this section, shall not relieve aperson of compliance with Title 47, Series 11, Section 2. 

## 3. Reporting Requirements

a) Planned changes. The permittee shall give notice to the Director of any planned physical alterations or additions tothe permitted facility ivhich

may affect the nature orquantity of the discharge. Notice is required when: (1) The alteration oraddition to a permitted facility may meet one of the criteria for determining whether afacility isa new source in

Section 

### 13.7.b

of Series 10, Title 47; or (2) The alteration oraddition could significantly change the nature or increase the quantity of pollutants discharged. This notification

applies topollutants which are subject neither to effluent limitations in the permit, nor to notification requirements under IV.2 of this section. b) Anticipated noncompliance. The permittee shall give advance notice to the Director of any planned changes in the permitted facility oractivity

which may result in noncompliance with permit requirements. c) In addition to the above reporting requirements, all existing manufacturing, commercial, and silvicultural discharges must notify the Director in writing assoon asthey know or have reason to believe: (1) That any activity hasoccurred orwill occur which would result in the discharge, on a routine or frequent basis, or any toxic

pollutant which is not limited in the permit, if that discharge will exceed the highest of thefollowing "notification levels": (A) One hundred micrograms per liter (100 ug/l); (B) Two hundred micrograms per liter (200 ug/l) for acrolein and acrylonitrile; five hundred micrograms per liter (500 ug/l)

for 2,4-dinitro phenol; and for 2-methyl 4,6-dinitrophenol; and one milligram per liter (1 mg/l) for antimony; (C) Five(5)times the maximum concentration value reported forthat pollutant in the permit application in accordance with

Section 

### 4.4.b.9of Series10, Title 47. (D) The level established by the Director in accordance with Section 6.3.gof Series 10,Title 47; (2) That any activity hasoccurred or will occur which would result in any discharge (on anon-routine or infrequent basis) of atoxic

which is not limited inthe permit, ifthat discharge will exceed the highest of the following "notification levels": (A) Five hundred micrograms per liter (500 ug/l); (B) One milligram per liter (1 mg/l) for antimony; (C) Ten (10) times the maximum concentration value reported for that pollutant in the permit application in accordance with

Section 

### 4.4.b.7of Series 10, Title 47; (D) The level established by the Director in accordance with Section 6.3.g of Series 10,Title 47. (3) That they have begun or expect to begin to use or manufacture asan intermediate orfinal product or by-product of any toxic

pollutant which was not reported in the permit application under Section 

### 4.4.b.9of Series 10, Title 47 and which will result inthe discharge on a routine orfrequent basis of that toxic pollutant at levels which exceed five times the detection limit for that pollutant under approved analytical procedure. (4) That they have begun or expect to begin to use or manufacture asan intermediate orfinal product orby-product of any toxic

pollutant which was not reported in the permit application under Section 

### 4.4.b.9of Series 10, Title 47 and which will result in the discharge on a non-routine or infrequent basis of that toxic pollutant at levels which exceed ten times the detection limit for that pollutant under approved analytical procedure. 

## 4. Other Noncompliance

The permittee shall report all instances of noncompliance not reported under theabove paragraphs atthe time monitoring reports are submitted. The reports shall contain the information listed in 

### IV.2.a). Should other applicable noncompliance reporting be required, these terms and conditions will be found in Section C of this permit.WRD 2A-82 

### STATE OF WEST VIRGINIA Final Limitations 

### NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM 

## YearRound

DISCHARGE MONITORING REPORT FACILITY NAME: (Reserve 

### Environmental Services LLC) RESERVE ENVIRONMENTA 

### CERTIFIED LABORATORY NAME: LOCATION OF FACILIT': WHEELING; Ohio County CERTIFIED LABORATORY ADDRESS: 

### PERMIT NO.: WV0116 241 OUTLET 

### NO.: 001 WASTELOAD FOR THE MONTH OF: INDIVIDUAL PERFORMING ANALYSIS: Quantity_ Other Units Mcasurement Sample 

### Parameter Units 

## N.E. CEL* Units 

## N.E. Frequency 

### Type 50050 (ML-1) RF-B Reported Flow,in Conduit orthru plant N/A N/A N/A Rpt Only Rpt Only N/A mgd 1/quarter Estimated Year Round Permit Limits Avg. Monthly Max. Daily 00310 (ML-1) RF-B Reported BoD, 5-Day 20 Deg.C N N/A Rpt Only RptOnly N/A mg/l 

### 1/quarter Grab Year Round Permit LimitS Avg. Monthly Max. Daily 00530 (ML-1) RF-B Reported Total Suspended Solids N/A Rpt Only RptOnly N/A mg/I 

### 1/quarter Grab Year Round Permit LimitS Avg. Monthly Max. Daily 00400 (ML-1) RF-B Reported pH N/A N/A RptOnly N/A Rpt Only N/A 

### S.U. 1/quarter Grab Year Round Permit Limits inst. Min. Inst. Max. 00600 (ML-1) RF-B Reported Nitrogen, Total (as N) N/A N/A N/A RptOnly Rpt Only N/A mg/l 1/quarter 

### Grab Year Round Permit LimitS Avg. Monthly Max. Daily 01104 (ML-1) RF-B Reported Aluminum, Total Recoverable N/A N/A N/A RptOnly Rpt Only N/A mg/l 1/quarter Grab Year Round Permit Limits Avg. Monthly Max. Daily 00940 (ML-1) RF-B Reported Chloride (as CI) N/A N/A N/A RptOnly Rpt Only N/A mg/l 

### 1/quarter Grab Year Round Permit LimitS Avg. Monthly Max. Daily 00951 (ML-1) RF-B Reported Fluoride, Total N/A N/A N/A Rpt Only Rpt Only N/A mg/I 1/quarter Grab Year Round Permit LimitS Avg. Monthly Max. Daily



### *CEL 

### =Compliance Evalual on Level 

### Name of 

### Principal Executive Officer Icertify under 

### penalty oflaw thatthis document and all attachments were prepared Date Completed unides lily datuullusi ùiaupefviölull its aCGoidaiaC6 voith 

## a oyhtnaïs dò¿lýiind tù aë¿uió that 

### qualified personnel properly gather and evaluate the information submitted. 

## Base_d on Signature of Principal Executive Officer or myinquiry ofthe 

### person or persons who manage the system, orthose persons directly 

# . Title ofOfficer responsible for gathering the information, the information submitted 

## is,tothe best ofmy Authonzed Agent 

# Iknc..icdge

and belief, 

## true,accurate,and

## complete. Iamawarethattherearesignificant penalties forsubmitting false information including the possibility of

## afine and imprisonment for 

### knowing violations.WRD 2A-82 

### STATE OF WEST VIRGINIA Final Limitations NATIONAL POLLUTANT DISCHARGE 

## ELIMINATIONSYSTEM 

## YearRound

DISCHARGE MONITORING REPORT FACILITY NAME: (Reserve 

### Environmental Services LLC) RESERVE ENVIRONMENTA 

### CERTIFIED LABORATORY 

### NAME: LOCATION OF FACILITY: WHEELING; Ohio County CERTIFIED LABORATORY ADDRESS: 

### PERMIT 

## NO.: WV0116441 OUTLET 

### NO.: 001 

### WASTELOAD FOR THE MONTH 

### OF: INDIVIDUAL 

### PERFORMING ANALYSIS:



## ._ .. . Quantity

.

## __ _ .

## _ _ Otoer Units.- Mcasurement Sample 

### Parameter Units 

## N.E. CEL* Units 

## N.E. Frequency Type 78141 (ML-1) RF-C Reported Total Toxic Organics (TTo) N/A N/A N/A Rpt Only Rpt Only N/A mg/l 1/6 months Grab Year Round Permit LimitS Avg. Monthly Max Daily 01045 (ML-1) RF-B Reported Iron,Total (as Fe) N/A N/A N/A RptOnly Rpt Only N/A mg/l 1/quarter Grab Year Round Permit LimitS Avg. Monthly Max. Daily 81020 (ML-1) RF-B Reported sulfate N/A RptOnly Rpt Only N/A mg/l 

### 1/quarter Grab Year Round Permit LimitS Avg. Monthly Max. Daily 81017 (ML-1) RF-B Reported Chem. Oxygen Demand N/A N/A N/A Rpt Only Rpt Only N/A mg/l 1/quarter Grab Year Round Permit LimitS Avg. Monthly Max. Daily 00552 (ML-1) RF-B Reported oil and Grease, Hexane EXTR. N/A N/A N/A Rpt Only Rpt Only N/A mg/I 1/quarter 

### Grab Year Round Permit LimitS Avg. Monthly Max. Daily 70298 (ML-1) RF-B Reported Total Dissolved solids (TDS) N/A N/A N/A Rpt Only RptOnly N/A mg/l 

### 1/quarter Grab Year Round Permit LimitS Avg. Monthly Max. Daily 82077 (ML-1) RF-B Reported Radiation, Gross Alpha N/A N/A N/A Rpt Only RptOnly N/A pCi/L 

### 1/quarter Grab Year Round Permit LimitS Avg. Monthly Max. Daily 03520 (ML-1) RF-B Reported Radiation, Gross Beta N/A N/A N/A Rpt Only RptOnly N/A pCi/L 

### 1/quarter Grab Year Round Permit LimitS Avg. Monthly Max. Daily

* CEL

### =Compliance Evaluai on Level Name of Principai Executive Officer Icertify under penalty of 

### law that this document 

### and all attachments were prepared 

## DateCompleted unidos lify diteuliuti ui huisäiviöiùii iii aúüùidailue Willi 

## a ¿yötálfs dáöiýiled 10 aööuin liial 

## qualifiedpersonnel properly gather and evaluate the information submitted. Based 

## on my inquiry of the 

### person or persons who manage the system, orthose persons directly Siugtnhat 

## reedokPrinntcipal

Executive Officer 

## or Title ofOfficer responsible for gathering the information, the information submitted 

## is,tothe best ofmy knowledge and 

### belief, true, accurate, and complete. Iam aware that there are significant penalties for submitting 

### false information including the possibility ofafine and imprisonment for 

### knowing vioiations.WRD 2A-82 

### STATE OFWEST VIRGINIA Final Limitations NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM 

## YearRound

DiSCHARGE MONITORING REPORT
FACILITY 

### NAME: (Reserve 

### Environmental Services LLC) RESERVE ENVIRONMENTA CERTIFIED LABORATORY NAME: 

### LOCATION OF FACILIT": WHEELING; Ohio County CERTIFIED LABORATORY ADDRESS: 

### PERMIT 

## NO.: WV0116e 41 OUTLET 

### NO.: 001 WASTELOAD 

### FOR THE MONTH OF: INDlVIDUAL 

### PERFORMING ANALYSIS:



## __ Quantity



## _ 

# _____

# _ _ . Otitet_Qniis_

.... Measurement Sample 

### Parameter Units 

## N.E. CEL* Units 

## N.E. Frequency Type 11503 (ML-1) RF-B Reported Radium 226 and 228, Total N/A N/A N/A Rpt Only Rpt Only N/A pCi/L 1/quarter Grab Year Round Permit LimitS Avg. Monthly Max. Daily 01082 (ML-1) RF-B Reported Strontium, Total (as Sr) N/A N/A N/A RptOnly Rpt Only N/A mg/I 

### 1/quarter Grab Year Round Permit LimitS Avg. Monthly Max. Daily 01132 (ML-1) RF-B Reported Lithium, Total (as Li) N/A N/A N/A Rpt Only Rpt Only N/A mg/I 1/quarter Grab Year Round Permit LimitS Avg. Monthly Max. Daily 71870 (ML-1) RF-B Reported Bromide N/A N/A N/A RptOnly Rpt Only N/A mg/l 

### 1/quarter Grab Year Round Permit LimitS Avg. Monthly Max. Daily
N/A

N/A

N/A

N/A



### *CEL

### =Compliance Evaluation Level 

### Name of Principal Executive Officer Icertify under penalty oflaw that this document and

## allattachmentswereprepared Date 

## Completed qualified personnei properly gather and evaluate the information submitted. Based on Signature ofPrincipal Executive Officer or my inquiry 

### ofthe person or persons who manage the 

### system, orthose persons directly Authorized A ent Title of 

### Officer responsible for gathering the information, the information submitted 

## is,tothe best of my 9 knowledge and belief, true, 

## accurate,and complete. 

## Iamaware thatthere are significant penalties for submitting faise information inciuding the possibility of

## afine and imprisonment for 

### knowing vioiations.

## WV/NPDES Permit 

## No.: WV0116441

NOTICE TO 

## PERMIT TEES

The 

## 1999regular session 

## ofthe West 

## Virginia legislature revised 

## the Water 

## Pollution Control Act, Chapter 

## 22, Article 

## 11, Section 10of the Code 

## of West Virginia 

## relating to fees 

## associated with 

## permits. This section ofthe Code requires 

## all holders 

## of aState 

## water pollution control permit oranational 

## pollutant discharge 

## elimination system permit to be assessed 

## anannual permit 

## fee, based upon 

## rules promulgated 

## bythe Secretary 

## ofthe Department 

## of Environmental 

## Protection. The Secretary 

## has promulgated 

## afinal rule in accordance 

## with the code revision 

## tothis effect 

## andthese rules were effective May 

## 4,2000. The rules establish 

## anannual permit fee based upon the relative potential to degrade the waters 

## of the State 

## which, in most 

## instances, relate to volume of discharge. However, 

## for sewage facilities, the 

## annual permit fee 

## is based upon the number 

## ofcustomers served 

## by the 

## facility. You may contact the Secretary 

## of State'sOffice, State Capitol 

## Building, Charleston, WV 25305, to obtain a

## copy of the 

## rules. The reference is

## Title 47, Legislative 

## Rules, Department 

## of Environmental 

## Protection, Division 

## of Water 

## Resources, Series 

## 26 Water 

## Pollution Control Permit Fee 

## Schedules.
Based upon the volume 

## of discharge 

## forwhich your facility 

## iscurrently permitted, the number of customers served 

## byyour facility 

## orfor the category 

## you fall within, pursuant to Section 

## 7of Title 

## 47, Series 

## 26, your annual permit fee 

## is$500.00. This fee 

## isdue no later than the anniversary date 

## of permit issuance 

## in each year 

## of the term 

## of the permit 

## orin the case 

## ofcoverage under 

## ageneral 

## permit, the fee 

## is due no later than the anniversary date 

## ofyour coverage under the general 

## permit. You 

## will be invoiced 

## by this agency 

## atthe appropriate time 

## for the 

## fee. Failure to submit the 

## annual fee within 

## ninety(90) days of the due date 

## will render your permit 

## void upon the date 

## you are mailed 

## acertified written notice to that 

## effect.

### EMERGENCY RESPONSE SPILL ALERT SYSTEM WEST VIRGINIA DEPARTMENT OF ENVIRONMENTAL PROTECTION REQUIREMENTS:

Title 

## 47, Series 

## 11,Section 2 of the WestVirginia Legislative Rules, Environmental Protection, Water Resources

- 

### Waste Management, Effective July 

## 1,1994. RESPONSIBILITY FOR REPORTING:

Each and every person who may causeorberesponsible for anyspill or accidental discharge ofpollutants into thewaters ofthe Stateshall give immediate notification to 

### theDivision of Water 

### and Waste Management's Emergency Notification Number, 1-800-642-3074. 

### Such notification shall set

### forth insofar aspossible and assoon thereafter aspractical thetime and place of suchspill or discharge, type ortypes and quantity orquantities of the material or materials therein, action or actions takento stop such spill or discharge andtominimize thepolluting effect thereof, the measure ormeasures taken ortobetaken in order toprevent arecurrence of any suchspill or discharge and suchadditional information asmay berequested by the 

### Division of Water and Waste 

### Management. This also applies to 

### spills tothewaters ofthe State 

### resulting from accidents 

### to common carriers by highway, rail and water.
It 

### shall bethe responsibility of each industrial establishment 

### or other entity 

### discharging directly to 

### a stream to 

### have available the following information pertaining to those substances 

### that areemployed orhandled in its operation in sufficiently large amounts asto constitute ahazard in caseof anaccidental spill or discharge into a public stream: (1) Potential toxicity inwater to 

### man, animals and aquatic life; (2) Details on analytical procedures for the quantitative 

### estimation of such substances in water and (3) Suggestions onsafeguards or other precautionary measures tonullify thetoxic effects of asubstance 

### once it has gotten 

### into astream.

Failure to furnish suchinformation asrequired by Section 

## 14,Article 

## 11,Chapter 

## 22,Code ofWest Virginia may bepunishable under Section 

## 24,Article 

## 11,Chapter 

## 22,and/or Section 

## 22,Article 

## 11,Chapter 

## 22, Code ofWest Virginia.

Itshall bethe responsibility of any person who causes or contributes in anywayto the 

### spill oraccidental discharge ofanypollutant orpollutants into State waters 

### to immediately take any andall measures necessary to contain suchspill or discharge. It shall further bethe 

### responsibility ofsuch person totake any and all measures necessary toclean-up, remove and otherwise render such spill or discharge harmless to thewaters ofthe 

### State.

When theDiréâtor determines it necessary for the 

### effective containment andabatement 

### of spills and accidental discharges, the 

### Director may require theperson or persons responsible for suchspill or discharge to 

### monitor affected waters in amanner prescribed bythe Director until 

### the possibility of anyadverse effect on the waters 

### of the State 

### no longer exists. VOLUNTARY REPORTING BY LAW OFFICERS, 

## U.S.COAST 

## GUARD, LOCK MASTERS AND OTHERS:In casesinvolving river and highway accidents where the 

### responsible party may or may not beavailable to 

### report the incident, law officers, 

## U. S.Coast Guard, Lock Masters and other interested person(s) should make the 

### report. WHO TO CONTACT: Notify the following number: 1-800-642-3074 

### INFORMATION NEEDED:

- 

### Source ofspill or discharge

- 

### Personnel at

### the scene

- 

### Location of incident

-

### Actions initiated

- 

### Time of incident

- 

### Shipper/Manufacturer identification

- 

### Material spilled or discharged

- 

### Railcar/Truck identification number

- 

### Amount spilled or discharged

-

### Container type

- Toxicity 

### ofmaterial spilled or discharged

## RIGHT 

# OF APPEAL

Notice is hereby given of your right to appeal the terms and conditions of this permit which you are aggrieved by to the Environmental Quality Board by filing a NOTICE 

# OF APPEAL on the form prescribed by such Board for this 

# purpose, with the 

# Board, in accordance with the provisions of Section 

# 21, Article 

# 11,Chapter 22 of the Code of West Virginia within thirty 

# (30) days after the date of receipt of the above 

# permit.

# STATEOFWESTVIRGINIA DIVISIONOFENVIRONMENTALPROTECTION DIVISIONOFWATERANDWASTEMANAGEMENT

BASISFORLIMITATIONS Reserve Environmental 

## Services, LLC

WV00116441
Reserve Environmental Services 

## (RES) proposes to treat wastewater from natural 

## gaswell drilling and development 

## operations. The 

## facility reported 

## SIC 1389 (Oil and Gas Field 

## Services, Not Elsewhere 

## Classified) in the permit 

## application. The permit application indicates that 

## RES will receive 

## drilling and development wastewater and treat the wastewater 

## for return back to the natural 

## gaswell drilling companies or others 

## in the case 

## of surplus. The proposed discharge 

## from the facility 

## isstorm water runoff 

## only. General Information
Sources of water: Natural Gas 

## Well Drilling well 

## drilling and development water Discharge Location/Basin:

(Outlet 

## 001

- 

### storm water runoff only) Wheeling 

## Creek, atributary 

## of the 

## Ohio River Estimated 

## flow

-

## 0.0037 MGD Antidegradation Since the facility proposes to discharge storm runoff 

## only, Tier 

## I protection 

## isprovided. Compliance evaluation 

## N/A

- 

### Proposed Facility
Outlet 

## 001 (stormwater) 

## Flow

-- 

### Monitor 

## (BPJ)

- 

## This discharge 

## isstorm water 

## andthus variable 

## in nature. Monitoring 

## is proposed to generate a

## database.
Parameters of concern 

## include pollutants detected 

## in elevated concentrations 

## inraw water samples from well drilling development wastewater accepted by the proposed facility and/or similar 

## facilities previously permitted by the agency. Monitoring will ensure proposed BMPs are 

## followed and will generate 

## a database for comparison with stormwater benchmarks.
Other Requirements Due to the nature 

## ofthe raw wastewater accepted 

## by the permittee 

## and itspotential to 

## contain either 

## Technically Enhanced 

## Naturally Occurring 

## Radiological Material (TENORM) or Source Material 

## (SM) Section 

## C.21 has been added 

## tothe 

## permit. TENORM isregulated 

## bythe West 

## Virginia Department 

## of Human Health 

## (WVDHH) per 

## 64 CSR23 and 

## SM (uranium and 

## thorium) is regulated 

## by the Nuclear Regulatory 

## Commission. This requirement requires 

## approval by either respective regulatory authority 

## prior to receiving, 

## possessing, using, transferring, ordelivering either 

## TENORM orSM. In 

## addition, the permit requires yearly radiation surveys (Section 

## C.22) toverify that accumulation 

## of scaleand waste management activities do not 

## result in environmental 

## impacts.Regular Addition 

## NPDES Permit Rating Work Sheet Discretionary Addition scorechange,butno NPDESNo.:WIV O 1 1 6 4 4 1 statuschange Deletion Facility Name: R|e|sjejr v e E n v i r o n m e n t a I S e r v i c e s City: 

## |W| h 

## | e e i i n g Receiving Water: W h e e I i n g C r e e k
Reach Number: 0 5 0 3 0 1 0 6

isthisfacility asteam electric power piant (SiC=4911) isthis permit for amunicipai separate storm sewer with one or more ofthefoiiowing characteristics? serving apopuiation greater than100,000? 

### 1.Power output 500 MW orgreater (not using a cooling pond/lake) 

### 2.A nuclear power plant Yes; score is700 (stop here) 

### 3.Cooling water discharge greater than 25% of the receiving stream's 7010 flow rate No
Yes; score is600 (stop here) No (Continue)

FACTOR 1:Toxic Pollutant Potential
PCSSICCode: 1 3 8 9 Primary SICCode: 

## | 1| 3 

## | 8 

## | 9 

## |
Other Sic Codes: 

## | | | | | | | | | | | | | | |
Industrial SubCategory Code: 

## | 0 0 

## | 0 

## | (Code 000 if no category) 40 CFR CFR Subpart (if applicable)
Determine the Toxicity potential from Appendix 

### A.Besure to usethe Total toxicity potential column and check one Toxicity Group Code Points Toxicity Group Code Points Toxicity Group Code Points
No process 0 0 

### 3. 3 15 

### 7. 7 35 wastestreams 

### 4. 4 20 

### 8. 8 40 

# 61. 1 5 

### 5. 5 25 

### 9. 9 45 

### 2. 2 10 

### 6. 6 30 10. 10 50 Code Number Checked:| 0 

## | 0 

## | Total Points Factor 1:| 0 

## | 0 

## |

FACTOR2: Flow/Stream Flow Volume (complete either Section Aor Section B;check only one) Section A

-Wastewater Flow Only Considered Section B

-Wastewater and Streamflow Considered

Wastewater Type Code Points Wastewater Type Percent of instream Code Points (See Instructions) (See Instructions) Wastewater ConcenType 1: Flow <5 MGD 11 0 tration at Receiving NCCW Flow 5to 10 MGD 12 10 Stream Low Flow

Flow >10 to 50 MGD 13 20 Flow >50 MGD 14 30 Type l/lil: <10 % 41 0 >=10%to<=50% 42 10 Typell: Flow<1MGD 21 10 >=50% 43 20 Process Flow1to5MGD 22 20 CCW Flow>5to10MGD 23 30

Flow >10 MGD 24 50 Type ll: <10% 51 0 >=10%to<=50% 52 20 Type Ill: Flow <1 MGD 31 0 >= 50% 53 30 Other Flow1to5MGD 32 10 SW Runoff Flow >5 to 10 MGD 33 20

Flow >10 MGD 34 30
Code Number Checked:| 3 

## | 1 

## |
Total Points Factor 2:| 0 

## | 0 

## |

# NPDES PermitRatingWorkSheet

FACTOR3: Conventional Pollutants NPDES No.: W V 0 1 

## | 1 

# I 6 4 4 1 (only when limited bythe permit) 

### A.Oxygen Demanding Pollutant (check one): (BOD COD Other:
Code Points
Permit Umits (check one) X <100 lbds/day 1 0 100 to 1000 lbs/day 2 5 >1000 to 3000 lbs/day 3 15 >3000 lbs/day 4 25 Code Number Checked: 0 1
Points Scored: 0 0 

### B.Total Suspended Solids (check one): Code Points
Permit Limits (check one) <100 lbds/day 1 0 100 to 1000 lbs/day 2 5 >1000 to 5000 ibs/day 3 15 >5000 1bs/day 4 20 Code Number Checked: 0 1
Points Scored: 0 0 

### C.Nitrogen Pollutants (check one): Ammonia 00ther:

Code Points
Permit Limits (Check one) X <300 lbds/day 1 0 300 to 1000 lbs/day 2 5 >1000 to 3000 lbs/day 3 15 >3000 lbs/day 4 25 Code Number Checked: 0 1
Points Scored: 0 0
Total Points Factor 3: 0 0

FACTOR 4: Public Health Impact isthere a public drinking water supply located within 50 miles downstream of the effluent discharge (this includes any body of water to which the receiving stream isatributary)? A public water supply may include infiltration galleries, orother methods of conveyance that ultimately get water from the above referenced supply.
X Yes (if yes, check toxicity potential number below) No(if no, go to Factor 5)

Determine the human health toxicity potential from Appendix 

### A.Usethe same SiCcode and subcategory references asin Factor 

### 1.(Be sure to usethe human health toxicity group column

- check one below) Toxicity Group Code Points Toxicity Group Code Points Toxicity Group Code Points
No process 0 0 

## } 3. 3 0 

### 7. 7 15 

# 6wastestreams



# _ 4. 4 0 

### 8. 8 20 

## . 1 0 

### 5. 5 5 

### 9. 9 25



## . 2 0 

## } 6. 6 10 10. 10 30 Code Number Checked: 0 0
Total Points Factor 4: 0 0

## NPDES Permit Rating Work Sheet

FACTOR 5: Water Quality Factors NPDESNo.: 

## |W| V O 1 1 6 4 4 1


### A.Is(or will) one or more of the effluent discharge limits based on water quality factors of the receiving stream (rather than technology-based federal guidelines, ortechnology-based state effluent guidelines); or has awasteload allocation been assigned to the discharge?

Code Points
Yes 1 10 No 2 0


### B.Isthe receiving water in compliance with applicable water quality standards for pollutants that are water quality limited in the permit?

Code Points
Yes 1 0 No 2 5


### C.Does the effluent discharged from this facility exhibit the reasonable potential to violate water quality standards due to whole effluent toxicity?

Code Points

Code Number Checked: A: B: 

## } C:
Total Points Factor 5: A: 0 0 

## | B: 

## | 0 0 

## | C: 0 0 = 

## | 0 0 |Total
FACTOR 6: Proximity to Coastal Waters 

### A.Base Score: Enter Flow Code Here (from Factor 2): 

## | 3 1 

## | Enter the multiplication factor that corresponds to the flow code: 

## | 0 

## | 0 

## | 0 

## | Check appropriate facility HPRICode (from PCS): 

## | 0 4 

## |
HPRI # Code HPRI Score Flow Code Multiplication Factor
1 1 20 11,31, or41 0.00 2 2 0 12,32, or42 0.05 3 3 30 13,33, or 43 0.10 X 4 4 0 14or 34 0.15

5 5 20 21 or 51 0.10 22 or 52 0.30 HPRI code checked: 23 or 53 0.60 24 1.00

BaseScore: (HPRI Score) 0 0 x (Multiplication Factor) 

### O. 0 0 = 0 (Total Points)


### B.Addiitonal Points

- NEP Program 

### C.Additional Points

- Great Lakes Area of Concern For afacility that hasan HPRI Code of3,does the facility For afacility that hasan HPRI Code of5,does the facility discharge to one of the estuaries enrolled in the National discharge any of the pollutants of concern into one ofthe Estuary Protection (NEP) program (see instructions) or Great Lakes' 31areas of concern (see instructions)? the Chesapeake Bay?

Code Points Code Points

Yes 1 10 Yes 1 10 No 2 0 No 2 0

Code Number Checked: A: B: C:

# å

Totai Points Factor 5: A: 0 0 

## | B: 0 0

# I C: 

## | 0 0 = 

# I O O Total

## NPDES Permit Rating Work Sheet

SCORESUMMARY NPDESNo.: W V O 1 1 6 4 4 1

Factor Description Total Points
1 Toxic Pollutant Potential 0 0 2 Flow/Stream Flow Volume 0 0 3 Conventional Pollutants 0 0 4 Pubilic Health impacts 0 0 5 Water Quality Factors 0 0 6 Proximity to Near Coastal Waters 0 0

TOTAL (Factors 1through 6) 0 0 0

S1.Isthe total score equal to orgreater than 80? 

### QYes (facility isa major) No

S2.Ifthe answer to the above question is no, would you like this facility to beadiscretionary major?

YNeos (Add 500 points to the above score and provide reason below):
Reason:

NEW SCORE: 0 0 0

OLD SCORE: 

# /Å

Pe It Re ewer's Name

Phone Number

Date