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/ Dakota-3 E&P Company, LLC. NSR Synthetic Minor Application WEP211324 

# ATTACHMENT C: FLASHING EMISSIONS CALCULATIONS

• E&P Tanks Emission Summary

• E&P Tanks Linear Relationship (Emission Factor)Mandaree Field 1000 BOPD wt%

****************************************************************************************** * Project Setup Information *
****************************************************************************************** Project File : Y:\Projects\Williams Exploration & Production WEP\WEP211324 Ft. Berthold IR Well Work\E&P Tanks\Mandaree Field 1000 BOPD.ept Flowsheet Selection : Oil Tank with Separator Calculation Method : RVP Distillation Control Efficiency : 100.0% Known Separator Stream : Low Pressure Oil Entering Air Composition : No
Filed Name : Mandaree Well Name : Cross 2-13H and Patricia Charging 4-15H Averages Permit Number : Dakota-3 E&P Company, LLC Date : 9/24/2010

****************************************************************************************** * Data Input *
****************************************************************************************** Separator Pressure : 51.00[psig] Separator Temperature : 82.50[F] Ambient Pressure : 14.70[psia] Ambient Temperature : 70.00[F] C10+ SG : 0.8000 C10+ MW : 235.14
-- Low Pressure Oil ---------------------------------------------------------------------- No. Component wt % 1 H2S 0.0014 2 O2 0.0000 3 CO2 0.0042 4 N2 0.0015 5 C1 0.0320 6 C2 0.3654 7 C3 1.2089 8 i-C4 0.3443 9 n-C4 1.5191 10 i-C5 0.6508 11 n-C5 1.2185 12 C6 1.3933 13 C7 6.7524 14 C8 15.9338 15 C9 14.3170 16 C10+ 53.7971 17 Benzene 0.0479 18 Toluene 0.0997 19 E-Benzene 0.0600 20 Xylenes 0.3998 21 n-C6 1.4864 22 224Trimethylp 0.3663
-- Sales Oil ----------------------------------------------------------------------------- Production Rate : 1000[bbl/day] Days of Annual Operation : 365 [days/year] API Gravity : 41.85 Reid Vapor Pressure : 5.90[psia]

****************************************************************************************** * Calculation Results *
****************************************************************************************** -- Emission Summary ---------------------------------------------------------------------- Item Uncontrolled Uncontrolled [ton/yr] [lb/hr] Page 1---------------------------------------------------------------- E&P TANK
Total HAPs 8.550 1.952 Total HC 812.744 185.558 VOCs, C2+ 796.480 181.845 VOCs, C3+ 612.595 139.862 Page 1Mandaree Field 1000 BOPD wt% Uncontrolled Recovery Info. Vapor 40.2300 [MSCFD] HC Vapor 40.0300 [MSCFD] GOR 40.23 [SCF/bbl] -- Emission Composition ------------------------------------------------------------------ No Component Uncontrolled Uncontrolled [ton/yr] [lb/hr] 1 H2S 0.689 0.157 2 O2 0.000 0.000 3 CO2 2.160 0.493 4 N2 0.786 0.179 5 C1 16.264 3.713 6 C2 183.886 41.983 7 C3 375.375 85.702 8 i-C4 37.149 8.482 9 n-C4 112.787 25.750 10 i-C5 17.863 4.078 11 n-C5 24.862 5.676 12 C6 8.648 1.974 13 C7 13.803 3.151 14 C8 10.281 2.347 15 C9 3.270 0.747 16 C10+ 0.004 0.001 17 Benzene 0.234 0.053 18 Toluene 0.136 0.031 19 E-Benzene 0.027 0.006 20 Xylenes 0.156 0.036 21 n-C6 7.394 1.688 22 224Trimethylp 0.604 0.138 Total 816.378 186.388

-- Stream Data --------------------------------------------------------------------------- No. Component MW LP Oil Flash Oil Sale Oil Flash Gas W&S Gas Total Emissions wt % wt % wt % wt % wt % wt % 1 H2S 34.80 0.0014 0.0010 0.0000 0.0873 0.0856 0.0861 2 O2 32.00 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 3 CO2 44.01 0.0042 0.0020 0.0000 0.4818 0.1765 0.2642 4 N2 28.01 0.0015 0.0001 0.0000 0.3044 0.0123 0.0962 5 C1 16.04 0.0320 0.0079 0.0000 5.2226 0.6866 1.9891 6 C2 30.07 0.3654 0.2356 0.0039 28.3624 20.1288 22.4930 7 C3 44.10 1.2089 1.0468 0.4786 36.1613 49.8497 45.9192 8 i-C4 58.12 0.3443 0.3257 0.2757 4.3503 4.6218 4.5438 9 n-C4 58.12 1.5191 1.4623 1.3185 13.7647 13.8076 13.7953 10 i-C5 72.15 0.6508 0.6432 0.6257 2.2771 2.1480 2.1850 11 n-C5 72.15 1.2185 1.2094 1.1888 3.1795 2.9854 3.0410 12 C6 86.16 1.3933 1.3945 1.3984 1.1369 1.0640 1.0850 13 C7 100.20 6.7524 6.7753 6.8342 1.8207 1.7133 1.7442 14 C8 114.23 15.9338 16.0015 16.1730 1.3430 1.2744 1.2941 15 C9 128.28 14.3170 14.3815 14.5440 0.4133 0.4189 0.4174 16 C10+ 235.14 53.7971 54.0465 54.6758 0.0006 0.0005 0.0006 17 Benzene 78.11 0.0479 0.0480 0.0483 0.0298 0.0281 0.0285 18 Toluene 92.13 0.0997 0.1001 0.1011 0.0174 0.0165 0.0166 19 E-Benzene 106.17 0.0600 0.0603 0.0610 0.0035 0.0032 0.0033 20 Xylenes 106.17 0.3998 0.4016 0.4059 0.0196 0.0187 0.0191 21 n-C6 86.18 1.4864 1.4889 1.4959 0.9466 0.8874 0.9045 22 224Trimethylp 114.24 0.3663 0.3677 0.3711 0.0772 0.0726 0.0739
MW 143.08 144.90 148.98 39.02 43.55 42.14 Stream Mole Ratio 1.0000 0.9829 0.9448 0.0171 0.0381 0.0552 Heating Value [BTU/SCF] 2225.52 2481.29 2401.97 Gas Gravity [Gas/Air] 1.35 1.50 1.45 Bubble Pt. @ 100F [psia] 32.28 20.39 7.37 Page 2---------------------------------------------------------------- E&P TANK RVP @ 100F [psia] 15.35 12.04 6.01 Spec. Gravity @ 100F 0.677 0.678 0.680

Page 2Emission estimates are based on using the E&P TANK V2.0 Model, RVP Distillation Column As shown below, the E&P Tanks summary output has a linear relationship with the production rate of the oil with the given inputs listed below.


### Inputs: Low pressure oil from average of 2 representative Mandaree Field Dakota-3 Wells Separator: 51 psig, 83 degF Flash Valve: 13.7 psia, 50 degF Sales Oil: API Gravity 41.9, Reid Vapor Pressure 5.90 psia, 365 days/year
Outputs: Oil Production Rates (bbl/day) (P) 0 50 100 300 1000 Emission (tons/yr) Total HC 0 40.6372 81.2744 243.8232 812.744 VOCs, C3+ 0 30.62975 61.2595 183.7785 612.595 Total HAPs 0 0.4275 0.855 2.565 8.55
VOC (C3+) Emission Factor: 0.6126 tpy/BOPD HAP Emission Factor: 0.00855 tpy/BOPD Oil Storage Tank Flashing Emissions Calculation Methodology E&P Tanks Linear Relation between Production (bbls/day) and Emissions (tons/yr)

y = 0.00855x R 2 = 1.00000 y = 0.6126x R 2 = 1

0 100 200 300 400 500 600 700

0 500 1000 1500tons/year



### bbl/day 

### Tank Emissions by Production Rate

Total HAPs VOCs, C3+ Linear (Total HAPs) Linear (VOCs, C3+)Dakota-3 E&P Company, LLC. NSR Synthetic Minor Application WEP211324 

# ATTACHMENT D: REPRESENTATIVE LOW PRESSURE OIL ANALYTICAL DATA

### Company

.................... ZENERGY 

### Lab Number

................ CR

Ͳ 10330 Study Number.......... CR

Ͳ 2 Date Sampled

.............. 7

Ͳ 15

Ͳ 2010 Date Tested............. 7

Ͳ 23

Ͳ 2010

S l Id tifi ti CROSS 2 13 H CRUDE OIL 

### EXTENDED HYDROCARBON (GLYCALC) LIQUID STUDY

Samp l e I d enti f ication

.................... C R OSS 2-13 H C RUDE O IL



### Sample Location .......... MONTANA. Sample Pressure ......... 22 PSIG Sample Temperature.... 95 F Type Sample ............... SPOT County...................... DUNN Test method ................ 

### GPA

Ͳ 2286 Sampling Method........ YZ PISTON

Components Mole % Weight % Liq. Vol. % Hydrogen Sulfide

.......... 0.003 0.001 0.001 

### Oxygen

...................... 0.000 0.000 0.000 

### Carbon Dioxide

............ 0.013 0.004 0.004 

### Nitrogen

..................... 0.007 0.001 0.001 

### Methane 0 180 0 021 0 050



### ..................... . . . 

### Ethane

....................... 1.602 0.342 0.709 

### Propane

..................... 4.036 1.264 1.839 

### iso

Ͳ Butane

.................. 0.855 0.353 0.463



### n
Ͳ Butane

.................... 3.974 1.640 2.072 

### iso

Ͳ Pentane

................ 1.378 0.706 0.833



### n
Ͳ Pentane

................... 2.569 1.316 1.540 

### H 2 510 1 536 1 707 

### exanes

..................... . . . 

### Heptanes

.................... 10.694 7.610 8.159 

### Octanes

..................... 19.351 15.699 16.394 

### Nonanes

..................... 17.072 15.551 15.886 

### Decanes+

................... 31.435 51.099 47.376 

### Benzene...................... 0.093 0.052 0.043 

### Toluene....................... 0.166 0.109 0.092 

### Ethylbenzene............... 0.104 0.078 0.066 

### Xylenes....................... 0.618 0.466 0.397



### n
Ͳ Hexane

.................... 2.798 1.712 1.903 

### 2,2,4

Ͳ Trimethylpentane... 0.542 0.440 0.466 

### TOTALS

..................... 100.000 100.000 100.000ADDITIONAL BETX DATA



### Components Mole % Weight % Liq. Vol. % 2-Methylpentane 1.486 0.910 1.011 3-Methylpentane 1 024 0 627 0 696 3

- Methylpentane

. . . n-Hexane 2.798 1.712 1.903 2,2,4-Trimethylpentane 0.542 0.440 0.466
Benzene 0.093 0.052 0.043
Toluene 0.166 0.109 0.092 Ethylbenzene 0.104 0.078 0.066 m-Xylene 0.066 0.050 0.042 p-Xylene 0.436 0.329 0.280 o-Xylene 0.116 0.087 0.074

API GRAVITY AT 60/60 F, calculated........................................................................ 60.3 SPECIFIC GRAVITY AT 60/60 F, calculated.............................................................. 0.7378 RELATIVE SPECIFIC GRAVITY OF DECANES+ (C10+) FRACTION ............................... 0.7958 AVERAGE MOLECULAR WEIGHT .......................................................................... 140.803 AVERAGE MOLECULAR WEIGHT OF DECANES+ (C10+) FRACTION .......................... 228.881 TRUE VAPOR PRESSURE AT 100 F PSIA calculated 33 400 TRUE VAPOR PRESSURE AT 100 F
, PSIA
, calculated

................................................ . AVERAGE BOILING POINT, F, ................................................................................ 299.063 CUBIC FEET OF GAS / GALLON OF LIQUID, as Ideal Gas .......................................... 19.106 BTU / GALLON OF LIQUID AT 14.73 PSIA, calculated ................................................. 122456.887 LBS / GALLON OF LIQUID, calculated ...................................................................... 6.152

NOTATION: ALL CALCULATIONS PERFORMED USING PHYSICAL CONSTANTS FROM GPA 2145-09, THE TABLES
OF PHYSICAL CONSTANTS FOR HYDROCARBONS AND OTHER COMPOUNDS OF INTEREST
TO THE NATURAL GAS INDUSTRY.

### EXTENDED HYDROCARBON LIQUID STUDIES



## CERTIFICATE OF ANALYSIS

Company................ PRECISION ANALYSIS

L bN b CR 10330 St d N b a umer............. CR-10330 Study Number............ CR-2B Date Sampled............. 7-15-2010 Date Tested.............. 7-22-2010

Sample Identification................ ZENERGY - CROSS 2-13 H CRUDE OIL

Sample Location......... MONTANA. Sample Pressure.......... N/A Sample Temperature.... N/A Flowrate................... N/A County..................... DUNN

Test Method.............. VARIOUS Sample Container........ 1-QUART BOTTLE

TEST PERFORMED RESULTS

A PI GRAVITY AT 60/60 F (ASTM D-287), observed...................... 42.5 / ( ),

SPECIFIC GRAVITY AT 60/60 F (ASTM D-1657), calculated.......... 0.8132

REID VAPOR PRESSURE (ASTM D-323), PSIG AT 100 F.............. 5.2 PSIG

TOTAL SULFUR CONTENT (ASTM D-5453), PPMW.................. 658.98 PPMW

TRUE VAPOR PRESSURE (ASTM D-2889), PSIA AT 100 F ........... N/A

BASIC SEDIMENT AND WATER CONTENT, % BY VOLUME.... N/A

COPPER STRIP CORROSION (ASTM D-130), 1 HOUR AT 100 F........... N/A

FREE WATER, observed......................................................... N/A

NOTATION : ALL TESTING PROVIDED ABOVE WAS PERFORMED IN ACCORDANCE TO METHODOLOGY OUTLINED BY THE AMERICAN SOCIETY FOR TESTING AND MATERIALS (ASTM).

### 5HSRUW5HSRUW(GLWRU

Chromatogram Cross 2-13H C:\GCsolution\DRO\DRO Data\08-2010\08-01-2010\Cross 2-13H.gcd - Channel 1min Intensity 0.0

2.5

5.0

7.5

10.0

12.5

15.0

17.5

20.0

22.5

25.0

27.5

30.0 0 50000 100000 150000 200000 250000

1.055 / 1.137 / 1.306 / 1.405 / 1.552 / 1.668 / 1.729 / 1.901 / 1.979 / 2.039 / 2.109 / 2.280 / 2.417 / 2.565 / 2.667 / 2.854 / 2.949 / 3.034 / 3.092 / 3.213 / 3.342 / 3.420 / 3.539 / 3.632 / 3.773 / 3.862 / 3.965 / 4.069 / 4.148 / 4.335 / 4.448 / 4.508 / 4.583 / 4.692 / 4.751 / 4.901 / 5.021 / 5.164 / 5.365 / 5.508 / 5.608 / Decane (C10) 5.816 / 5.947 / 6.069 / 6.188 / 6.286 / 6.393 / 6.509 / 6.569 / 6.657 / 6.714 / 6.777 / 6.896 / 7.083 /

7.220 / 7.323 / 7.381 / 7.455 / 7.559 / 7.632 / 7.703 / 7.769 / 7.836 / 7.907 /

7.967 / 8.056 / 8.184 / 8.268 / 8.329 / 8.452 / 8.540 / 8.633 /

8.744 / 8.808 /

8.998 / 9.128 /

9.270 / 9.380 / 9.467 / 9.526 / 9.596 / 9.724 / 9.862 / 9.939 / 10.055 / 10.150 / 10.257 / 10.332 / 10.427 / 10.487 / 10.568 / 10.638 / 10.766 /

10.828 / 10.911 / 11.051 / 11.216 / 11.469 /

11.613 / 11.706 / 11.785 / 12.031 /

12.128 / 12.182 / 12.302 / 12.409 / 12.463 / 12.536 / 12.607 / 12.700 / 12.822 / 13.004 / 13.088 / 13.203 / 13.305 / 13.372 / 13.447 / 13.582 / 13.674 / 13.803 / 13.929 / 14.089 / 14.146 / 14.316 / 14.427 /

14.515 / 14.592 / 14.691 / 14.773 / 14.896 / 15.041 / 15.129 / 15.249 / 15.300 /

15.369 / 15.430 / 15.566 / 15.620 / 15.691 / 15.787 / 15.947 / o-terphenyl 16.113 / 16.187 / 16.339 / 16.456 / 16.570 / 16.661 / 16.813 / 16.894 / 16.979 / 17.143 /

17.306 / 17.449 / 17.519 / 17.642 / 17.787 / 17.954 / 18.052 / 18.153 / 18.222 / 18.292 / 18.434 / 18.549 / 18.723 / 18.887 / 18.991 / 19.197 / 19.331 / 19.474 / 19.663 / 19.724 / 19.785 / 19.850 / 19.927 / 19.995 / 20.077 / 20.182 / 20.222 / 20.345 / 20.443 / 20.634 / 20.789 / 20.871 / 20.945 / 21.059 / 21.134 / 21.205 / 21.310 / 21.542 / 21.695 / 21.795 / 21.855 / 21.905 / 21.966 / 22.073 / 22.181 / 22.367 / 22.425 /

22.599 / Octacosane (C28) 22.737 / 22.808 / 22.879 / 23.003 / 23.058 / 23.117 /

23.217 / 23.351 / 23.418 / 23.678 /

23.816 / 23.905 / 24.027 / 24.086 / 24.202 / 24.264 / 24.400 / 24.521 / 24.587 / 24.651 / 24.765 / 24.809 / 24.874 / 24.981 / 25.069 / 25.142 / 25.201 / 25.273 / 25.334 / 25.401 / 25.462 / 25.568 / 25.705 / 25.765 / 25.966 / 26.056 / 26.229 / 26.397 / 26.487 / 26.575 / 26.665 / 26.758 / 26.958 / 27.073 / 27.191 / 27.327 / 27.441 / 27.561 / 27.668 / 27.798 / 27.952 / 28.073 / 28.297 / 28.467 / 28.689 / 28.833 / 28.995 / 29.193 / 29.393 / 29.601 /

### Company

.................... ZENERGY 

### Lab Number

................ CR

Ͳ 10330 Study Number.......... CR

Ͳ 3 Date Sampled

.............. 7

Ͳ 15

Ͳ 2010 Date Tested............. 7

Ͳ 23

Ͳ 2010

S l Id tifi ti PATRICIA CHARGING 4 15 H CRUDE OIL 

### EXTENDED HYDROCARBON (GLYCALC) LIQUID STUDY

Samp l e I d enti f ication

.................... PATRI C IA C HAR G IN G 4-15 H C RUDE O IL



### Sample Location .......... MONTANA. Sample Pressure ......... 80 PSIG Sample Temperature.... 70 F Type Sample ............... SPOT County...................... DUNN Test method ................ 

### GPA

Ͳ 2286 Sampling Method........ YZ PISTON

Components Mole % Weight % Liq. Vol. % Hydrogen Sulfide

.......... 0.008 0.002 0.002 

### Oxygen

...................... 0.000 0.000 0.000 

### Carbon Dioxide

............ 0.014 0.004 0.004 

### Nitrogen

..................... 0.008 0.001 0.001 

### Methane 0 398 0 043 0 107



### ..................... . . . 

### Ethane

....................... 1.921 0.387 0.811 

### Propane

..................... 3.914 1.155 1.702 

### iso

Ͳ Butane

.................. 0.862 0.335 0.445



### n
Ͳ Butane

.................... 3.606 1.403 1.795 

### iso

Ͳ Pentane

................ 1.238 0.598 0.715



### n
Ͳ Pentane

................... 2.329 1.125 1.333 

### H 2 180 1 257 1 415 

### exanes

..................... . . . 

### Heptanes

.................... 8.849 5.934 6.445 

### Octanes

..................... 21.103 16.133 17.068 

### Nonanes

..................... 15.296 13.130 13.589 

### Decanes+

................... 34.917 56.412 52.378 

### Benzene...................... 0.085 0.044 0.038 

### Toluene....................... 0.148 0.091 0.078 

### Ethylbenzene............... 0.060 0.043 0.037 

### Xylenes....................... 0.473 0.336 0.290



### n
Ͳ Hexane

.................... 2.204 1.271 1.431 

### 2,2,4

Ͳ Trimethylpentane... 0.387 0.296 0.317 

### TOTALS

..................... 100.000 100.000 100.000ADDITIONAL BETX DATA



### Components Mole % Weight % Liq. Vol. % 2-Methylpentane 1.272 0.734 0.826 3-Methylpentane 0 908 0 524 0 590 3

- Methylpentane

. . . n-Hexane 2.204 1.271 1.431 2,2,4-Trimethylpentane 0.387 0.296 0.317
Benzene 0.085 0.044 0.038
Toluene 0.148 0.091 0.078 Ethylbenzene 0.060 0.043 0.037 m-Xylene 0.058 0.041 0.036 p-Xylene 0.298 0.212 0.183 o-Xylene 0.117 0.083 0.072

API GRAVITY AT 60/60 F, calculated........................................................................ 57.8 SPECIFIC GRAVITY AT 60/60 F, calculated.............................................................. 0.7475 RELATIVE SPECIFIC GRAVITY OF DECANES+ (C10+) FRACTION ............................... 0.8050 AVERAGE MOLECULAR WEIGHT .......................................................................... 149.417 AVERAGE MOLECULAR WEIGHT OF DECANES+ (C10+) FRACTION .......................... 241.399 TRUE VAPOR PRESSURE AT 100 F PSIA calculated 46 319 TRUE VAPOR PRESSURE AT 100 F
, PSIA
, calculated

................................................ . AVERAGE BOILING POINT, F, ................................................................................ 314.836 CUBIC FEET OF GAS / GALLON OF LIQUID, as Ideal Gas .......................................... 18.857 BTU / GALLON OF LIQUID AT 14.73 PSIA, calculated ................................................. 122700.693 LBS / GALLON OF LIQUID, calculated ...................................................................... 6.232

NOTATION: ALL CALCULATIONS PERFORMED USING PHYSICAL CONSTANTS FROM GPA 2145-09, THE TABLES
OF PHYSICAL CONSTANTS FOR HYDROCARBONS AND OTHER COMPOUNDS OF INTEREST
TO THE NATURAL GAS INDUSTRY.

### EXTENDED HYDROCARBON LIQUID STUDIES



## CERTIFICATE OF ANALYSIS

Company................ ZENERGY

L bN b CR 10330 St d N b a umer............. CR-10330 Study Number............ CR-3B Date Sampled............. 7-15-2010 Date Tested.............. 7-22-2010

Sample Identification................ PATRICIA CHARGING 4-15 H CRUDE OIL

Sample Location......... MONTANA. Sample Pressure.......... N/A Sample Temperature.... N/A Flowrate................... N/A County..................... DUNN

Test Method.............. VARIOUS Sample Container........ 1-QUART BOTTLE

TEST PERFORMED RESULTS

A PI GRAVITY AT 60/60 F (ASTM D-287), observed...................... 41.2 / ( ),

SPECIFIC GRAVITY AT 60/60 F (ASTM D-1657), calculated.......... 0.8193

REID VAPOR PRESSURE (ASTM D-323), PSIG AT 100 F.............. 6.6 PSIG

TOTAL SULFUR CONTENT (ASTM D-5453), PPMW.................. 940.25 PPMW

TRUE VAPOR PRESSURE (ASTM D-2889), PSIA AT 100 F ........... N/A

BASIC SEDIMENT AND WATER CONTENT, % BY VOLUME.... N/A

COPPER STRIP CORROSION (ASTM D-130), 1 HOUR AT 100 F........... N/A

FREE WATER, observed......................................................... N/A

NOTATION : ALL TESTING PROVIDED ABOVE WAS PERFORMED IN ACCORDANCE TO METHODOLOGY OUTLINED BY THE AMERICAN SOCIETY FOR TESTING AND MATERIALS (ASTM).

### 5HSRUW5HSRUW(GLWRU

Chromatogram PC 4-15 1-100 C:\GCsolution\DRO\DRO Data\08-2010\08-01-2010\PC 4-15 1-100.gcd - Channel 1min Intensity 0.0

2.5

5.0

7.5

10.0

12.5

15.0

17.5

20.0

22.5

25.0

27.5

30.0 0 50000 100000 150000 200000 250000

1.054 / 1.137 / 1.407 / 1.593 / 1.670 / 1.730 / 1.902 / 2.040 / 2.109 / 2.280 / 2.363 /

2.418 / 2.566 / 2.667 / 2.855 / 2.950 / 3.035 / 3.136 /

3.214 / 3.343 / 3.421 / 3.540 / 3.635 / 3.773 / 3.863 / 3.967 / 4.070 / 4.149 / 4.335 / 4.509 / 4.584 / 4.694 / 4.750 / 4.901 / 5.022 / 5.166 / 5.366 / 5.510 / 5.610 / Decane (C10) 5.818 / 5.949 / 6.070 / 6.190 / 6.288 / 6.397 / 6.512 / 6.564 / 6.660 / 6.714 / 6.780 / 6.901 / 7.016 / 7.084 / 7.156 / 7.221 /

7.326 / 7.384 / 7.457 / 7.561 / 7.634 / 7.747 / 7.836 / 7.908 /

7.969 / 8.059 / 8.184 / 8.270 / 8.331 / 8.453 / 8.542 / 8.634 / 8.745 / 8.812 / 9.000 / 9.129 /

9.271 / 9.381 / 9.469 / 9.529 / 9.597 / 9.725 / 9.863 / 9.942 / 10.057 / 10.149 / 10.260 / 10.334 / 10.429 /

10.488 / 10.570 / 10.640 / 10.768 /

10.830 / 10.913 /

11.059 / 11.220 / 11.472 / 11.615 / 11.787 / 12.031 / 12.130 / 12.184 / 12.318 / 12.414 / 12.470 / 12.541 / 12.606 / 12.706 / 12.826 / 13.005 / 13.088 / 13.306 / 13.376 / 13.450 / 13.583 / 13.673 / 13.728 / 13.934 / 14.091 / 14.148 / 14.319 / 14.445 /

14.516 / 14.595 / 14.692 / 14.779 / 14.896 / 15.042 / 15.130 / 15.246 /

15.373 / 15.431 / 15.568 / 15.621 / 15.658 / 15.775 /

15.883 / 15.950 / o-terphenyl 16.056 / 16.118 / 16.191 / 16.341 / 16.460 / 16.573 / 16.667 / 16.814 / 16.894 / 16.987 / 17.144 / 17.313 / 17.452 / 17.528 / 17.644 / 17.796 / 17.963 / 18.087 / 18.144 / 18.226 / 18.292 / 18.436 / 18.558 / 18.723 / 18.924 / 18.986 / 19.083 / 19.198 / 19.272 / 19.329 / 19.473 / 19.627 / 19.786 / 19.849 / 19.928 / 20.077 / 20.180 / 20.244 / 20.372 / 20.431 / 20.488 / 20.634 / 20.798 / 20.870 / 20.952 / 21.027 / 21.131 / 21.218 / 21.313 / 21.422 / 21.538 / 21.594 / 21.705 / 21.795 / 21.845 / 21.966 / 22.068 / 22.188 / 22.368 / 22.426 / 22.604 / Octacosane (C28) 22.717 / 22.799 / 22.997 / 23.054 /

23.217 / 23.347 / 23.408 / 23.605 / 23.663 /

23.817 / 24.040 / 24.163 / 24.292 / 24.402 / 24.498 / 24.572 / 24.634 / 24.695 / 24.758 / 24.836 / 24.977 / 25.088 / 25.178 / 25.438 / 25.504 / 25.571 / 25.721 / 25.797 / 26.044 / 26.117 / 26.208 / 26.366 / 26.438 / 26.526 / 26.626 / 26.733 / 26.830 / 26.947 / 27.166 / 27.448 / 27.552 / 27.669 / 27.776 / 27.974 / 28.293 / 28.432 / 28.616 / 28.720 / 28.944 / 29.074 / 29.336 / 29.688 / 29 920 /Dakota-3 E&P Company, LLC. NSR Synthetic Minor Application WEP211324 

# ATTACHMENT E: REPRESENTATIVE GAS ANALYSIS

## 	

	



 	
  
      
    
   
    
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01 ( 54  4  545 55  4  4  46 4 5 5 45 45  46  4  4  54  54  54  545  54 5 54  545 5  554 45  6 4 #'

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(!!*/.
	### Client: BISON ENGINEERING 

### Analysis Date: 10/11/2011



### Sample ID: ALISIA FOX 16

Ͳ 9 

### Date Sampled: 10/11/2011



### Unique #: Purpose:

Sample Temperature: 62 DEG F 

### Sample Pressure: 20 PSI



### Sampled By: TC 

### Type Sample: ONLINE



### County: DUNN

Components Mole % Weight % Liq. Vol. % Carbon Dioxide............. 0.677 1.161 0.551 

### Hydrogen Sulfide........... 0.000 0.000 0.000 

### Nitrogen...................... 3.323 3.626 

### 1.742 Methane...................... 58.464 36.543 

### 47.240 Ethane........................ 21.074 24.689 

### 26.862 Propane....................... 10.662 18.317 

### 13.999 iso

Ͳ Butane................... 0.861 1.949 

### 1.342

n
Ͳ Butane...................... 2.523 5.713 

### 3.791 iso

Ͳ Pentane.................. 0.389 1.092 

### 0.677

n
Ͳ Pentane.................... 0.599 1.684 

### 1.035 Cyclopentane............... 0.028 0.075 

### 0.039

n
Ͳ Hexane..................... 0.196 0.657 

### 0.384 Cyclohexane................ 0.196 0.642 

### 0.317 Other Hexanes ............. 0.147 0.492 0.287 

### Heptanes..................... 0.338 1.321 0.744 

### Methylcyclohexane........ 0.129 0.493 0.247 

### 2,2,4

Ͳ Trimethylpentane... 0.001 0.004 0.002 

### Benzene...................... 0.085 0.257 0.113 

### Toluene....................... 0.073 0.264 0.117 

### Ethylbenzene............... 0.003 0.014 0.006 

### Xylenes....................... 0.112 0.462 0.206 

### C8+ Heavies................ 0.122 0.545 

### 0.299 Totals

........................ 100.000 100.000 

### 100.000ADDITIONAL BETX DATA



### Components Mole % Weight % Liq. Vol. % Cyclopentane 0.028 0.075 0.039 Cyclohexane 0.196 0.642 0.317 2-Methylpentane 0.092 0.310 0.181 3-Methylpentane 0.054 0.182 0.106
n-Hexane 0.196 0.657 0.384 Methylcyclohexane 0.129 0.493 0.247 2,2,4-Trimethylpentane 0.001 0.004 0.002
Benzene 0.085 0.257 0.113
Toluene 0.073 0.264 0.117 Ethylbenzene 0.003 0.014 0.006 0 018 0 073 0 033 m-Xylene . . . p-Xylene 0.076 0.313 0.139 o-Xylene 0.018 0.076 0.034

SPECIFIC GRAVITY @ 60/60 F l l t d 0 8862 SPECIFIC GRAVITY @ 60 / 60 F, calculated................................................... . TOTAL GPM (Ethane Inclusive)................................................................. 10.561 CALCULATED BTU / REAL CF @ 14.73 PSIA, dry basis.................................. 1462.236 CALCULATED BTU / REAL CF @ 14.73 PSIA, wet basis.................................. 1437.527 AVERAGE MOLECULAR WEIGHT............................................................ 25.666 MOLAR MASS RATIO.............................................................................. 0.8862 RELATIVE DENSITY ( G x Z (Air) / Z ), calculated........................................ 0.8911 IDEAL GROSS HEATING VALUE BTU / IDEAL CF @ 14 696 PSIA 1450 907 IDEAL GROSS HEATING VALUE , BTU / IDEAL CF @ 14

. 696 PSIA

.................. 1450

. 907 COMPRESSIBILITY FACTOR (Z).............................................................. 0.99453

PROPANE GPM ..................................................................................... 2.9297 BUTANE GPM ....................................................................................... 1.0743 GASOLINE GPM (PENTANE AND HEAVIER) ........................................... 0.9357

NOTATION: ALL CALCULATIONS PERFORMED USING PHYSICAL CONSTANTS FROM GPA 2145-09, THE TABLES
OF PHYSICAL CONSTANTS FOR HYDROCARBONS AND OTHER COMPOUNDS OF INTEREST
TO THE NATURAL GAS INDUSTRY.

### Client: BISON ENGINEERING 

### Analysis Date: 10/11/2011



### Sample ID: HIGH HAWK 4

Ͳ 9 

### Date Sampled: 10/11/2011



### Unique #: Purpose:

Sample Temperature: 59 DEG F 

### Sample Pressure: 25 PSI



### Sampled By: TC 

### Type Sample: ONLINE



### County: DUNN

Components Mole % Weight % Liq. Vol. % Carbon Dioxide............. 0.517 0.681 0.356 

### Hydrogen Sulfide........... 0.000 0.000 0.000 

### Nitrogen...................... 0.562 0.471 

### 0.249 Methane...................... 28.060 13.456 

### 19.176 Ethane........................ 34.433 30.949 

### 37.122 Propane....................... 25.191 33.204 

### 27.977 iso

Ͳ Butane................... 2.180 3.787 

### 2.875

n
Ͳ Butane...................... 6.332 11.001 

### 8.047 iso

Ͳ Pentane.................. 0.795 1.714 

### 1.172

n
Ͳ Pentane.................... 1.017 2.194 

### 1.487 Cyclopentane............... 0.037 0.079 

### 0.045

n
Ͳ Hexane..................... 0.146 0.375 

### 0.242 Cyclohexane................ 0.047 0.119 

### 0.065 Other Hexanes ............. 0.291 0.749 0.482 

### Heptanes..................... 0.084 0.252 0.157 

### Methylcyclohexane........ 0.025 0.073 0.040 

### 2,2,4

Ͳ Trimethylpentane... 0.000 0.000 0.000 

### Benzene...................... 0.018 0.043 0.021 

### Toluene....................... 0.069 0.190 0.093 

### Ethylbenzene............... 0.004 0.011 0.005 

### Xylenes....................... 0.015 0.049 0.024 

### C8+ Heavies................ 0.177 0.605 

### 0.366 Totals

........................ 100.000 100.000 

### 100.000ADDITIONAL BETX DATA



### Components Mole % Weight % Liq. Vol. % Cyclopentane 0.037 0.079 0.045 Cyclohexane 0.047 0.119 0.065 2-Methylpentane 0.183 0.471 0.303 3-Methylpentane 0.108 0.278 0.179
n-Hexane 0.146 0.375 0.242 Methylcyclohexane 0.025 0.073 0.040 2,2,4-Trimethylpentane 0.000 0.000 0.000
Benzene 0.018 0.043 0.021
Toluene 0.069 0.190 0.093 Ethylbenzene 0.004 0.011 0.005 0 002 0 008 0 004 m-Xylene . . . p-Xylene 0.010 0.033 0.016 o-Xylene 0.003 0.008 0.004

SPECIFIC GRAVITY @ 60/60 F l l t d 1 1551 SPECIFIC GRAVITY @ 60 / 60 F, calculated................................................... . TOTAL GPM (Ethane Inclusive)................................................................. 19.847 CALCULATED BTU / REAL CF @ 14.73 PSIA, dry basis.................................. 1945.085 CALCULATED BTU / REAL CF @ 14.73 PSIA, wet basis.................................. 1911.926 AVERAGE MOLECULAR WEIGHT............................................................ 33.454 MOLAR MASS RATIO.............................................................................. 1.1551 RELATIVE DENSITY ( G x Z (Air) / Z ), calculated........................................ 1.1668 IDEAL GROSS HEATING VALUE BTU / IDEAL CF @ 14 696 PSIA 1921 067 IDEAL GROSS HEATING VALUE , BTU / IDEAL CF @ 14

. 696 PSIA

.................. 1921

. 067 COMPRESSIBILITY FACTOR (Z).............................................................. 0.98992

PROPANE GPM ..................................................................................... 6.9222 BUTANE GPM ....................................................................................... 2.7025 GASOLINE GPM (PENTANE AND HEAVIER) ........................................... 1.0377

NOTATION: ALL CALCULATIONS PERFORMED USING PHYSICAL CONSTANTS FROM GPA 2145-09, THE TABLES
OF PHYSICAL CONSTANTS FOR HYDROCARBONS AND OTHER COMPOUNDS OF INTEREST
TO THE NATURAL GAS INDUSTRY.

### Client: BISON ENGINEERING 

### Analysis Date: 10/11/2011 WILLIAMS 

### Sample ID: NATHAN HALE 3

Ͳ 18 

### Date Sampled: 10/11/2011



### Unique #: Purpose:

Sample Temperature: 59 DEG F 

### Sample Pressure: 15 PSI



### Sampled By: TC 

### Type Sample: ONLINE



### County: DUNN

Components Mole % Weight % Liq. Vol. % Carbon Dioxide............. 0.561 0.873 0.443 

### Hydrogen Sulfide........... 0.000 0.000 0.000 

### Nitrogen...................... 3.504 3.471 

### 1.784 Methane...................... 56.578 32.094 

### 44.375 Ethane........................ 15.797 16.795 

### 19.545 Propane....................... 11.394 17.765 

### 14.522 iso

Ͳ Butane................... 1.536 3.156 

### 2.325

n
Ͳ Butane...................... 5.735 11.786 

### 8.364 iso

Ͳ Pentane.................. 1.045 2.666 

### 1.768

n
Ͳ Pentane.................... 1.419 3.619 

### 2.379 Cyclopentane............... 0.102 0.252 

### 0.139

n
Ͳ Hexane..................... 0.461 1.405 

### 0.877 Cyclohexane................ 0.304 0.903 

### 0.478 Other Hexanes ............. 0.333 1.015 0.634 

### Heptanes..................... 0.692 2.453 1.478 

### Methylcyclohexane........ 0.242 0.842 0.451 

### 2,2,4

Ͳ Trimethylpentane... 0.001 0.002 0.001 

### Benzene...................... 0.192 0.530 0.248 

### Toluene....................... 0.066 0.215 0.102 

### Ethylbenzene............... 0.003 0.010 0.005 

### Xylenes....................... 0.010 0.038 0.018 

### C8+ Heavies................ 0.027 0.109 

### 0.064 Totals

........................ 100.000 100.000 

### 100.000ADDITIONAL BETX DATA



### Components Mole % Weight % Liq. Vol. % Cyclopentane 0.102 0.252 0.139 Cyclohexane 0.304 0.903 0.478 2-Methylpentane 0.210 0.639 0.399 3-Methylpentane 0.123 0.376 0.235
n-Hexane 0.461 1.405 0.877 Methylcyclohexane 0.242 0.842 0.451 2,2,4-Trimethylpentane 0.001 0.002 0.001
Benzene 0.192 0.530 0.248
Toluene 0.066 0.215 0.102 Ethylbenzene 0.003 0.010 0.005 0 002 0 006 0 003 m-Xylene . . . p-Xylene 0.007 0.026 0.012 o-Xylene 0.002 0.006 0.003

SPECIFIC GRAVITY @ 60/60 F l l t d 0 9765 SPECIFIC GRAVITY @ 60 / 60 F, calculated................................................... . TOTAL GPM (Ethane Inclusive)................................................................. 11.511 CALCULATED BTU / REAL CF @ 14.73 PSIA, dry basis.................................. 1602.761 CALCULATED BTU / REAL CF @ 14.73 PSIA, wet basis.................................. 1575.593 AVERAGE MOLECULAR WEIGHT............................................................ 28.281 MOLAR MASS RATIO.............................................................................. 0.9765 RELATIVE DENSITY ( G x Z (Air) / Z ), calculated........................................ 0.9832 IDEAL GROSS HEATING VALUE BTU / IDEAL CF @ 14 696 PSIA 1588 143 IDEAL GROSS HEATING VALUE , BTU / IDEAL CF @ 14

. 696 PSIA

.................. 1588

. 143 COMPRESSIBILITY FACTOR (Z).............................................................. 0.99316

PROPANE GPM ..................................................................................... 3.1309 BUTANE GPM ....................................................................................... 2.3045 GASOLINE GPM (PENTANE AND HEAVIER) ........................................... 1.8621

NOTATION: ALL CALCULATIONS PERFORMED USING PHYSICAL CONSTANTS FROM GPA 2145-09, THE TABLES
OF PHYSICAL CONSTANTS FOR HYDROCARBONS AND OTHER COMPOUNDS OF INTEREST
TO THE NATURAL GAS INDUSTRY.

### Client: BISON ENGINEERING 

### Analysis Date: 10/11/2011 WILLIAMS 

### Sample ID: SKUNK CREEK 1

Ͳ 12 

### Date Sampled: 10/11/2011



### Unique #: Purpose:

Sample Temperature: 78 DEG F 

### Sample Pressure: 30 PSI



### Sampled By: TC 

### Type Sample: ONLINE



### County: DUNN

Components Mole % Weight % Liq. Vol. % Carbon Dioxide............. 0.596 0.893 0.454 

### Hydrogen Sulfide........... 0.000 0.000 0.000 

### Nitrogen...................... 3.717 3.545 

### 1.828 Methane...................... 46.514 25.407 

### 35.242 Ethane........................ 22.053 22.578 

### 26.359 Propane....................... 16.952 25.451 

### 20.872 iso

Ͳ Butane................... 1.718 3.399 

### 2.512

n
Ͳ Butane...................... 5.657 11.195 

### 7.971 iso

Ͳ Pentane.................. 0.829 2.037 

### 1.355

n
Ͳ Pentane.................... 1.021 2.507 

### 1.654 Cyclopentane............... 0.070 0.167 

### 0.092

n
Ͳ Hexane..................... 0.263 0.771 

### 0.483 Cyclohexane................ 0.077 0.222 

### 0.118 Other Hexanes ............. 0.061 0.178 0.112 

### Heptanes..................... 0.231 0.789 0.477 

### Methylcyclohexane........ 0.034 0.115 0.062 

### 2,2,4

Ͳ Trimethylpentane... 0.000 0.000 0.000 

### Benzene...................... 0.015 0.040 0.019 

### Toluene....................... 0.044 0.137 0.065 

### Ethylbenzene............... 0.004 0.016 0.008 

### Xylenes....................... 0.018 0.066 0.032 

### C8+ Heavies................ 0.125 0.487 

### 0.287 Totals

........................ 100.000 100.000 

### 100.000ADDITIONAL BETX DATA



### Components Mole % Weight % Liq. Vol. % Cyclopentane 0.070 0.167 0.092 Cyclohexane 0.077 0.222 0.118 2-Methylpentane 0.038 0.112 0.070 3-Methylpentane 0.023 0.066 0.041
n-Hexane 0.263 0.771 0.483 Methylcyclohexane 0.034 0.115 0.062 2,2,4-Trimethylpentane 0.000 0.000 0.000
Benzene 0.015 0.040 0.019
Toluene 0.044 0.137 0.065 Ethylbenzene 0.004 0.016 0.008 0 003 0 011 0 005 m-Xylene . . . p-Xylene 0.012 0.045 0.021 o-Xylene 0.003 0.011 0.005

SPECIFIC GRAVITY @ 60/60 F l l t d 1 0141 SPECIFIC GRAVITY @ 60 / 60 F, calculated................................................... . TOTAL GPM (Ethane Inclusive)................................................................. 13.943 CALCULATED BTU / REAL CF @ 14.73 PSIA, dry basis.................................. 1663.548 CALCULATED BTU / REAL CF @ 14.73 PSIA, wet basis.................................. 1635.316 AVERAGE MOLECULAR WEIGHT............................................................ 29.370 MOLAR MASS RATIO.............................................................................. 1.0141 RELATIVE DENSITY ( G x Z (Air) / Z ), calculated........................................ 1.0215 IDEAL GROSS HEATING VALUE BTU / IDEAL CF @ 14 696 PSIA 1647 712 IDEAL GROSS HEATING VALUE , BTU / IDEAL CF @ 14

. 696 PSIA

.................. 1647

. 712 COMPRESSIBILITY FACTOR (Z).............................................................. 0.99276

PROPANE GPM ..................................................................................... 4.6583 BUTANE GPM ....................................................................................... 2.3395 GASOLINE GPM (PENTANE AND HEAVIER) ........................................... 1.0627

NOTATION: ALL CALCULATIONS PERFORMED USING PHYSICAL CONSTANTS FROM GPA 2145-09, THE TABLES
OF PHYSICAL CONSTANTS FOR HYDROCARBONS AND OTHER COMPOUNDS OF INTEREST
TO THE NATURAL GAS INDUSTRY.

### Client: BISON ENGINEERING 

### Analysis Date: 10/11/2011 WILLIAMS 

### Sample ID: TAT 2

Ͳ 1 

### Date Sampled: 10/11/2011



### Unique #: Purpose:

Sample Temperature: 117 DEG F 

### Sample Pressure: 17 PSI



### Sampled By: TC 

### Type Sample: ONLINE



### County: DUNN

Components Mole % Weight % Liq. Vol. % Carbon Dioxide............. 0.644 0.870 0.462 

### Hydrogen Sulfide........... 0.000 0.000 0.000 

### Nitrogen...................... 1.573 1.352 

### 0.727 Methane...................... 39.023 19.208 

### 27.788 Ethane........................ 23.624 21.796 

### 26.538 Propane....................... 20.193 27.321 

### 23.368 iso

Ͳ Butane................... 2.557 4.559 

### 3.514

n
Ͳ Butane...................... 7.945 14.169 

### 10.521 iso

Ͳ Pentane.................. 1.185 2.623 

### 1.820

n
Ͳ Pentane.................... 1.596 3.532 

### 2.430 Cyclopentane............... 0.101 0.217 

### 0.125

n
Ͳ Hexane..................... 0.369 0.975 

### 0.637 Cyclohexane................ 0.172 0.445 

### 0.246 Other Hexanes ............. 0.417 1.101 0.720 

### Heptanes..................... 0.393 1.209 0.762 

### Methylcyclohexane........ 0.099 0.299 0.168 

### 2,2,4

Ͳ Trimethylpentane... 0.001 0.002 0.001 

### Benzene...................... 0.031 0.075 0.037 

### Toluene....................... 0.034 0.097 0.048 

### Ethylbenzene............... 0.002 0.007 0.004 

### Xylenes....................... 0.007 0.021 0.011 

### C8+ Heavies................ 0.035 0.121 

### 0.074 Totals

........................ 100.000 100.000 

### 100.000ADDITIONAL BETX DATA



### Components Mole % Weight % Liq. Vol. % Cyclopentane 0.101 0.217 0.125 Cyclohexane 0.172 0.445 0.246 2-Methylpentane 0.262 0.693 0.453 3-Methylpentane 0.154 0.408 0.267
n-Hexane 0.369 0.975 0.637 Methylcyclohexane 0.099 0.299 0.168 2,2,4-Trimethylpentane 0.001 0.002 0.001
Benzene 0.031 0.075 0.037
Toluene 0.034 0.097 0.048 Ethylbenzene 0.002 0.007 0.004 0 001 0 003 0 002 m-Xylene . . . p-Xylene 0.004 0.014 0.007 o-Xylene 0.001 0.003 0.002

SPECIFIC GRAVITY @ 60/60 F l l t d 1 1253 SPECIFIC GRAVITY @ 60 / 60 F, calculated................................................... . TOTAL GPM (Ethane Inclusive)................................................................. 16.864 CALCULATED BTU / REAL CF @ 14.73 PSIA, dry basis.................................. 1874.169 CALCULATED BTU / REAL CF @ 14.73 PSIA, wet basis.................................. 1842.251 AVERAGE MOLECULAR WEIGHT............................................................ 32.591 MOLAR MASS RATIO.............................................................................. 1.1253 RELATIVE DENSITY ( G x Z (Air) / Z ), calculated........................................ 1.1360 IDEAL GROSS HEATING VALUE BTU / IDEAL CF @ 14 696 PSIA 1852 257 IDEAL GROSS HEATING VALUE , BTU / IDEAL CF @ 14

. 696 PSIA

.................. 1852

. 257 COMPRESSIBILITY FACTOR (Z).............................................................. 0.99058

PROPANE GPM ..................................................................................... 5.5490 BUTANE GPM ....................................................................................... 3.3329 GASOLINE GPM (PENTANE AND HEAVIER) ........................................... 1.6803

NOTATION: ALL CALCULATIONS PERFORMED USING PHYSICAL CONSTANTS FROM GPA 2145-09, THE TABLES
OF PHYSICAL CONSTANTS FOR HYDROCARBONS AND OTHER COMPOUNDS OF INTEREST
TO THE NATURAL GAS INDUSTRY.

### Client: BISON ENGINEERING 

### Analysis Date: 10/11/2011 WILLIAMS 

### Sample ID: WELL 32

Ͳ 29 

### Date Sampled: 10/11/2011



### Unique #: Purpose:

Sample Temperature: 66 DEG F 

### Sample Pressure: 20 PSI



### Sampled By: TC 

### Type Sample: ONLINE



### County: DUNN

Components Mole % Weight % Liq. Vol. % Carbon Dioxide............. 0.512 0.724 0.372 

### Hydrogen Sulfide........... 0.000 0.000 0.000 

### Nitrogen...................... 1.570 1.414 

### 0.735 Methane...................... 39.457 20.353 

### 28.475 Ethane........................ 27.369 26.461 

### 31.158 Propane....................... 20.271 28.740 

### 23.773 iso

Ͳ Butane................... 2.013 3.763 

### 2.805

n
Ͳ Butane...................... 5.884 10.995 

### 7.896 iso

Ͳ Pentane.................. 0.765 1.776 

### 1.192

n
Ͳ Pentane.................... 1.021 2.368 

### 1.575 Cyclopentane............... 0.054 0.123 

### 0.069

n
Ͳ Hexane..................... 0.193 0.536 

### 0.339 Cyclohexane................ 0.066 0.180 

### 0.096 Other Hexanes ............. 0.261 0.724 0.457 

### Heptanes..................... 0.240 0.773 0.471 

### Methylcyclohexane........ 0.081 0.254 0.138 

### 2,2,4

Ͳ Trimethylpentane... 0.000 0.000 0.000 

### Benzene...................... 0.015 0.038 0.018 

### Toluene....................... 0.073 0.216 0.104 

### Ethylbenzene............... 0.004 0.014 0.007 

### Xylenes....................... 0.015 0.050 0.024 

### C8+ Heavies................ 0.136 0.498 

### 0.296 Totals

........................ 100.000 100.000 

### 100.000ADDITIONAL BETX DATA



### Components Mole % Weight % Liq. Vol. % Cyclopentane 0.054 0.123 0.069 Cyclohexane 0.066 0.180 0.096 2-Methylpentane 0.164 0.455 0.288 3-Methylpentane 0.097 0.268 0.169
n-Hexane 0.193 0.536 0.339 Methylcyclohexane 0.081 0.254 0.138 2,2,4-Trimethylpentane 0.000 0.000 0.000
Benzene 0.015 0.038 0.018
Toluene 0.073 0.216 0.104 Ethylbenzene 0.004 0.014 0.007 0 002 0 008 0 004 m-Xylene . . . p-Xylene 0.010 0.034 0.016 o-Xylene 0.002 0.008 0.004

SPECIFIC GRAVITY @ 60/60 F l l t d 1 0738 SPECIFIC GRAVITY @ 60 / 60 F, calculated................................................... . TOTAL GPM (Ethane Inclusive)................................................................. 16.499 CALCULATED BTU / REAL CF @ 14.73 PSIA, dry basis.................................. 1796.792 CALCULATED BTU / REAL CF @ 14.73 PSIA, wet basis.................................. 1766.229 AVERAGE MOLECULAR WEIGHT............................................................ 31.101 MOLAR MASS RATIO.............................................................................. 1.0738 RELATIVE DENSITY ( G x Z (Air) / Z ), calculated........................................ 1.0830 IDEAL GROSS HEATING VALUE BTU / IDEAL CF @ 14 696 PSIA 1777 412 IDEAL GROSS HEATING VALUE , BTU / IDEAL CF @ 14

. 696 PSIA

.................. 1777

. 412 COMPRESSIBILITY FACTOR (Z).............................................................. 0.99149

PROPANE GPM ..................................................................................... 5.5702 BUTANE GPM ....................................................................................... 2.5073 GASOLINE GPM (PENTANE AND HEAVIER) ........................................... 1.1204

NOTATION: ALL CALCULATIONS PERFORMED USING PHYSICAL CONSTANTS FROM GPA 2145-09, THE TABLES
OF PHYSICAL CONSTANTS FOR HYDROCARBONS AND OTHER COMPOUNDS OF INTEREST
TO THE NATURAL GAS INDUSTRY.

### Client: BISON ENGINEERING 

### Analysis Date: 10/11/2011 WILLIAMS 

### Sample ID: WOLF 27

Ͳ 34 

### Date Sampled: 10/11/2011



### Unique #: Purpose:

Sample Temperature: 60 DEG F 

### Sample Pressure: 30 PSI



### Sampled By: TC 

### Type Sample: ONLINE



### County: DUNN

Components Mole % Weight % Liq. Vol. % Carbon Dioxide............. 0.514 0.836 0.406 

### Hydrogen Sulfide........... 0.000 0.000 0.000 

### Nitrogen...................... 2.455 2.541 

### 1.250 Methane...................... 55.961 33.170 

### 43.916 Ethane........................ 21.138 23.484 

### 26.169 Propane....................... 11.397 18.569 

### 14.535 iso

Ͳ Butane................... 1.184 2.543 

### 1.794

n
Ͳ Butane...................... 3.503 7.523 

### 5.113 iso

Ͳ Pentane.................. 0.833 2.219 

### 1.409

n
Ͳ Pentane.................... 1.363 3.634 

### 2.287 Cyclopentane............... 0.097 0.250 

### 0.132

n
Ͳ Hexane..................... 0.357 1.138 

### 0.680 Cyclohexane................ 0.150 0.467 

### 0.236 Other Hexanes ............. 0.456 1.453 0.868 

### Heptanes..................... 0.400 1.481 0.854 

### Methylcyclohexane........ 0.082 0.299 0.153 

### 2,2,4

Ͳ Trimethylpentane... 0.000 0.000 0.000 

### Benzene...................... 0.030 0.085 0.038 

### Toluene....................... 0.032 0.110 0.050 

### Ethylbenzene............... 0.002 0.006 0.003 

### Xylenes....................... 0.007 0.026 0.012 

### C8+ Heavies................ 0.039 0.166 

### 0.093 Totals

........................ 100.000 100.000 

### 100.000ADDITIONAL BETX DATA



### Components Mole % Weight % Liq. Vol. % Cyclopentane 0.097 0.250 0.132 Cyclohexane 0.150 0.467 0.236 2-Methylpentane 0.287 0.914 0.547 3-Methylpentane 0.169 0.538 0.322
n-Hexane 0.357 1.138 0.680 Methylcyclohexane 0.082 0.299 0.153 2,2,4-Trimethylpentane 0.000 0.000 0.000
Benzene 0.030 0.085 0.038
Toluene 0.032 0.110 0.050 Ethylbenzene 0.002 0.006 0.003 0 001 0 004 0 002 m-Xylene . . . p-Xylene 0.005 0.018 0.008 o-Xylene 0.001 0.004 0.002

SPECIFIC GRAVITY @ 60/60 F l l t d 0 9345 SPECIFIC GRAVITY @ 60 / 60 F, calculated................................................... . TOTAL GPM (Ethane Inclusive)................................................................. 11.726 CALCULATED BTU / REAL CF @ 14.73 PSIA, dry basis.................................. 1558.098 CALCULATED BTU / REAL CF @ 14.73 PSIA, wet basis.................................. 1531.712 AVERAGE MOLECULAR WEIGHT............................................................ 27.065 MOLAR MASS RATIO.............................................................................. 0.9345 RELATIVE DENSITY ( G x Z (Air) / Z ), calculated........................................ 0.9403 IDEAL GROSS HEATING VALUE BTU / IDEAL CF @ 14 696 PSIA 1544 831 IDEAL GROSS HEATING VALUE , BTU / IDEAL CF @ 14

. 696 PSIA

.................. 1544

. 831 COMPRESSIBILITY FACTOR (Z).............................................................. 0.99377

PROPANE GPM ..................................................................................... 3.1318 BUTANE GPM ....................................................................................... 1.4882 GASOLINE GPM (PENTANE AND HEAVIER) ........................................... 1.4675

NOTATION: ALL CALCULATIONS PERFORMED USING PHYSICAL CONSTANTS FROM GPA 2145-09, THE TABLES
OF PHYSICAL CONSTANTS FOR HYDROCARBONS AND OTHER COMPOUNDS OF INTEREST
TO THE NATURAL GAS INDUSTRY.Dakota-3 E&P Company, LLC. NSR Synthetic Minor Application WEP211324 

# ATTACHMENT F: ENGINE MANUFACTURER’S SPECS

# This section of the document has been redacted because it contains copyrighted information. The redacted information

can be viewed from the hard copy of the docket, which is available at the EPA Region 8 Office upon request.Dakota-3 E&P Company, LLC. NSR Synthetic Minor Application WEP211324 

# ATTACHMENT G: EMISSION CONTROL DEVICE MANUFACTURER’S SPECS	

 	





  

#  
 
 

### TYPICAL MANDAREE AREA **FOUR WELL PAD FACILITY PLOT PLAN Dakota-3 E&P Company, LLC**  **FBIR, North Dakota**

**NOT TO SCALE**

12’d x 20’h 12’d x 20’h 12’d x 20’h

**Recycle Pump Chemicals** 

**(4)Wellheads**

**Tank Vent line**

Utility F lare **LACT Gas to sales**  **Gas Meter**

12’d x 20’h 12’d x 20’h 12’d x 20’h

12’d x 20’h 400 bbl oil 12’d x 20’h 400 bbl oil 12’d x 20’h 400 bbl Prod. H2O

12’d x 20’h 400 bbl oil 12’d x 20’h 400 bbl oil 12’d x 20’h 400 bbl oil Enclosed Combustor

**Recycle Pump**  **Recycle Pump** 

**Recycle Pump**  **LACT Unit** 

**LACT Unit** 

**LACT Unit**  12’d x 20’h 400 bbl oil

12’d x 20’h

12’d x 20’h 400 bbl oil

12’d x 20’h 400 bbl H2O 12’d x 20’h

12’d x 20’h

12’d x 20’h 400 bbl oil

12’d x 20’h 400 bbl oil **Valve**

**Valve**

**Valve Valve** 

**Recycle Line** 6’d x 20’h vertical treater Separator 30” d by 10’ h Gas Meter **(4) Gensets Genset** 

**Oil Pipeline Water**  **Pipeline** 24 bbl Diesel

Legend

Berms Water Line Crude Line Flowline Buried Recycle Lines Gas Sales Line Tank Vapor Line Flared Gas Line 6’d x 20’h vertical treater Separator 30” d by 10’ h Gas Meter

6’d x 20’h vertical treater Separator 30” d by 10’ h

6’d x 20’h vertical treater Separator 30” d by 10’ h	

 	





  

#   

Dakota-3 E&P Company, LLC. NSR Synthetic Minor Application WEP211324 

# ATTACHMENT J: DIESEL TANK EPA TANKS 4.09D **E MISSIONS SUMMARY** 

### TANKS 4.0.9d Emissions Report - Detail Format Tank Indentification and Physical Characteristics

Identification User Identification: 1000 gallon diesel tank City: Williston State: North Dakota Company: Williams E&P, LLC Type of Tank: Horizontal Tank Description: 1,000 gallon diesel tank to fuel onsite diesel generators. Tank throughput is based on engine fuel consumption.

Tank Dimensions Shell Length (ft): 10.00 Diameter (ft): 4.16 Volume (gallons): 1,000.00 Turnovers: 2,244.31 Net Throughput(gal/yr): 2,244,312.00 Is Tank Heated (y/n): N Is Tank Underground (y/n): N

Paint Characteristics Shell Color/Shade: Gray/Medium Shell Condition Good

Breather Vent Settings Vacuum Settings (psig): -0.03 Pressure Settings (psig) 0.03

Meterological Data used in Emissions Calculations: Bismarck, North Dakota (Avg Atmospheric Pressure = 13.86 psia) 

### Page 1 of 6 TANKS 4.0 Report

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### 1000 gallon diesel tank - Horizontal Tank Williston, North Dakota 

### T ANKS 4.0.9d Emissions Report - Detail Format Liquid Contents of Storage Tank

Daily Liquid Surf. Temperature (deg F) Liquid Bulk Temp Vapor Pressure (psia) Vapor Mol. Liquid Mass Vapor Mass Mol. Basis for Vapor Pressure Mixture/Component Month Avg. Min. Max. (deg F) Avg. Min. Max. Weight. Fract. Fract. Weight Calculations

Distillate fuel oil no. 2 All 50.18 39.72 60.64 44.68 0.0045 0.0031 0.0067 130.0000 188.00 Option 1: VP50 = .0045 VP60 = .0065 

### Page 2 of 6 TANKS 4.0 Report

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### 1000 gallon diesel tank - Horizontal Tank Williston, North Dakota 

### T ANKS 4.0.9d Emissions Report - Detail Format Detail Calculations (AP-42)

Annual Emission Calcaulations

Standing Losses (lb): 0.2654 Vapor Space Volume (cu ft): 86.5719 Vapor Density (lb/cu ft): 0.0001 Vapor Space Expansion Factor: 0.0780 Vented Vapor Saturation Factor: 0.9995
Tank Vapor Space Volume: Vapor Space Volume (cu ft): 86.5719 Tank Diameter (ft): 4.1600 Effective Diameter (ft): 7.2797 Vapor Space Outage (ft): 2.0800 Tank Shell Length (ft): 10.0000
Vapor Density Vapor Density (lb/cu ft): 0.0001 Vapor Molecular Weight (lb/lb-mole): 130.0000 Vapor Pressure at Daily Average Liquid Surface Temperature (psia): 0.0045 Daily Avg. Liquid Surface Temp. (deg. R): 509.8466 Daily Average Ambient Temp. (deg. F): 41.5958 Ideal Gas Constant R (psia cuft / (lb-mol-deg R)): 10.731 Liquid Bulk Temperature (deg. R): 504.3458 Tank Paint Solar Absorptance (Shell): 0.6800 Daily Total Solar Insulation Factor (Btu/sqft day): 1,276.2450
Vapor Space Expansion Factor Vapor Space Expansion Factor: 0.0780 Daily Vapor Temperature Range (deg. R): 41.8377 Daily Vapor Pressure Range (psia): 0.0036 Breather Vent Press. Setting Range(psia): 0.0600 Vapor Pressure at Daily Average Liquid Surface Temperature (psia): 0.0045 Vapor Pressure at Daily Minimum Liquid Surface Temperature (psia): 0.0031 Vapor Pressure at Daily Maximum Liquid Surface Temperature (psia): 0.0067 Daily Avg. Liquid Surface Temp. (deg R): 509.8466 Daily Min. Liquid Surface Temp. (deg R): 499.3872 Daily Max. Liquid Surface Temp. (deg R): 520.3060 Daily Ambient Temp. Range (deg. R): 24.3583
Vented Vapor Saturation Factor Vented Vapor Saturation Factor: 0.9995 Vapor Pressure at Daily Average Liquid: Surface Temperature (psia): 0.0045 Vapor Space Outage (ft): 2.0800

Working Losses (lb): 5.6720 Vapor Molecular Weight (lb/lb-mole): 130.0000 Vapor Pressure at Daily Average Liquid Surface Temperature (psia): 0.0045 Annual Net Throughput (gal/yr.): 2,244,312.0000 

### Page 3 of 6 TANKS 4.0 Report

9/29/2011 file://C:\Program Files\Tanks409d\summarydisplay.htmAnnual Turnovers: 2,244.3120 Turnover Factor: 0.1800 Tank Diameter (ft): 4.1600 Working Loss Product Factor: 1.0000

Total Losses (lb): 5.9375 

### Page 4 of 6 TANKS 4.0 Report

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### Emissions Report for: Annual

1000 gallon diesel tank - Horizontal Tank Williston, North Dakota 

### T ANKS 4.0.9d Emissions Report - Detail Format Individual Tank Emission Totals

Losses(lbs) Components Working Loss Breathing Loss Total Emissions Distillate fuel oil no. 2 5.67 0.27 5.94 

### Page 5 of 6 TANKS 4.0 Report

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### Page 6 of 6 TANKS 4.0 Report

9/29/2011 file://C:\Program Files\Tanks409d\summarydisplay.htm