Instructionsfor completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls(example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet.If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of

measure.Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet.If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

1385 Dale 3 bituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis Analyte

1385 Dale 3 As Received Higher Heating Value 1385 Dale 3 As Received % Moisture 1385 Dale 3 As Received % Ash 1385 Dale 3 As Received % Sulfur 1385 Dale 3 Dry basis Higher Heating Value 1385 Dale 3 Dry basis % Ash 1385 Dale 3 Dry basis % Sulfur 1385 Dale 3 Dry basis Antimony 1385 Dale 3 Dry basis Arsenic 1385 Dale 3 Dry basis Beryllium 1385 Dale 3 Dry basis Cadmium 1385 Dale 3 Dry basis Chlorine 1385 Dale 3 Dry basis Chromium 1385 Dale 3 Dry basis Cobalt 1385 Dale 3 Dry basis Fluorine 1385 Dale 3 Dry basis Lead 1385 Dale 3 Dry basis Manganese 1385 Dale 3 Dry basis Mercury 1385 Dale 3 Dry basis Nickel 1385 Dale 3 Dry basis SeleniumAnalysis Method for each Analyte

(example: ASTM D5865-04) ASTM D5865-04 ASTM D3302-05 ASTM D3174-04 ASTM D4239-05 C ASTM D5865-04 ASTM D3174-04 ASTM D4239-05 C ASTM D6357-04 B ASTM D6357-04 B ASTM D6357-04 B ASTM D6357-04 B ASTM D4208-02 ASTM D6357-04 B ASTM D6357-04 B ASTM D3761-96 ASTM D6357-04 B ASTM D6357-04 B ASTM D6357-04 B ASTM D6357-04 B ASTM D6357-04 CEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 1385 Dale 3 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 1 4/5/2010 4/5/2010 12845.00 Btu/lb 2 4/6/2010 4/6/2010 12762.00 Btu/lb 3 4/6/2010 4/6/2010 12811.00 Btu/lb 1 4/6/2010 4/6/2010 12762.00 Btu/lb 2 4/6/2010 4/6/2010 12811.00 Btu/lb 3 4/7/2010 4/7/2010 12780.00 Btu/lb 1 4/7/2010 4/7/2010 12780.00 Btu/lb 2 4/7/2010 4/7/2010 12776.00 Btu/lb 3 4/8/2010 4/8/2010 13062.00 Btu/lb Fuel Testing ResultsMercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 6.09 7.66 0.9 13678 Btu/lb 8.16 0.96 6.3 8.1 0.83 13620 Btu/lb 8.64 0.89 6.69 7.61 0.81 13730 Btu/lb 8.16 0.87 6.3 8.1 0.83 13620 Btu/lb 8.64 0.89 6.69 7.61 0.81 13730 Btu/lb 8.16 0.87 6.94 8.18 0.85 13733 Btu/lb 8.79 0.91 6.94 8.18 0.85 13733 Btu/lb 8.79 0.91 5.49 8.96 0.9 13518 Btu/lb 9.48 0.95 5.19 7.69 0.86 13777 Btu/lb 8.11 0.91Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 1894 ppm 0.05 μg/g 0.78 μg/g 4.64 μg/g 2.04 2000 ppm 0.05 μg/g 0.85 μg/g 4.33 μg/g 2.25 2082 ppm 0.05 μg/g 0.85 μg/g 4.35 μg/g 2.58 2000 ppm 0.05 μg/g 0.85 μg/g 4.33 μg/g 2.25 2082 ppm 0.05 μg/g 0.85 μg/g 4.35 μg/g 2.58 2017 ppm 0.04 μg/g 0.88 μg/g 4.47 μg/g 2.31 2017 ppm 0.04 μg/g 0.88 μg/g 4.47 μg/g 2.31 1692 ppm 0.09 μg/g 0.86 μg/g 4.71 μg/g 2.5 1906 ppm 0.05 μg/g 0.76 μg/g 4.63 μg/g 2.24Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units μg/g 0.01 μg/g 14.2 μg/g 4.27 μg/g 10.25 μg/g μg/g 0.01 μg/g 14.78 μg/g 5.01 μg/g 9.55 μg/g μg/g 0.01 μg/g 14.7 μg/g 5.03 μg/g 9.75 μg/g μg/g 0.01 μg/g 14.78 μg/g 5.01 μg/g 9.55 μg/g μg/g 0.01 μg/g 14.7 μg/g 5.03 μg/g 9.75 μg/g μg/g 0.01 μg/g 15.9 μg/g 4.55 μg/g 10.03 μg/g μg/g 0.01 μg/g 15.9 μg/g 4.55 μg/g 10.03 μg/g μg/g 0.01 μg/g 15.79 μg/g 5.17 μg/g 9.22 μg/g μg/g 0.01 μg/g 13.81 μg/g 3.94 μg/g 9.36 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 13.59 μg/g 4.2 μg/g 54 ppm 7.09 μg/g N/A 14.03 μg/g 4.23 μg/g 46 ppm 7.21 μg/g N/A 14.18 μg/g 4.08 μg/g 38 ppm 7.28 μg/g N/A 14.03 μg/g 4.23 μg/g 46 ppm 7.21 μg/g N/A 14.18 μg/g 4.08 μg/g 38 ppm 7.28 μg/g N/A 14.67 μg/g 2.63 μg/g 39 ppm 7.67 μg/g N/A 14.67 μg/g 2.63 μg/g 39 ppm 7.67 μg/g N/A 13.97 μg/g 4.52 μg/g 44 ppm 7.56 μg/g N/A 13.61 μg/g 3.89 μg/g 39 ppm 7.09 μg/g N/A Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 37.21 8.16 54.63 75.63 5.1 1.44 0.96 37.7 8.64 53.66 75.48 5.1 1.44 0.89 37.77 8.16 54.07 75.75 5.13 1.46 0.87 37.7 8.64 53.66 75.48 5.1 1.44 0.89 37.77 8.16 54.07 75.75 5.13 1.46 0.87 37.22 8.79 53.99 75.45 5.04 1.48 0.91 37.22 8.79 53.99 75.45 5.04 1.48 0.91 37.7 9.48 52.82 74.46 5.02 1.47 0.95 38.42 8.11 53.47 75.61 5.14 1.47 0.91 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen

8.71 8.45 8.63 8.45 8.63 8.33 8.33 8.62 8.76EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 1385 Dale 3 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 1 3/31/2010 3/31/2010 12969.00 Btu/lb 2 3/31/2010 3/31/2010 12877.00 Btu/lb 3 4/1/2010 4/1/2010 12906.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 6.12 7.56 0.92 13814 Btu/lb 8.05 0.98 6.5 7.58 0.85 13772 Btu/lb 8.11 0.91 5.4 7.62 0.88 13643 Btu/lb 8.05 0.93Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/ABeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/ANickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units N/A N/A 45 ppm N/A N/A N/A 36 ppm N/A N/A N/A 40 ppm N/ANote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur N/A 37.99 8.05 53.96 75.84 5.15 1.48 0.98 N/A 37.54 8.11 54.35 76.13 5.16 1.49 0.91 N/A 38.16 8.05 53.79 75.89 5.13 1.48 0.93 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 8.5 8.2 8.52EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 1385 Dale 3 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 1 4/1/2010 4/1/2010 12791.00 Btu/lb 2 4/1/2010 4/1/2010 12683.00 Btu/lb 3 4/2/2010 4/2/2010 12537.00 Btu/lb 1 4/2/2010 4/2/2010 12852.00 Btu/lb 2 4/2/2010 4/2/2010 12580.00 Btu/lb 3 4/2/2010 4/2/2010 12704.00 Btu/lb 1 4/8/2010 4/8/2010 12944.00 Btu/lb 2 4/8/2010 4/8/2010 12886.00 Btu/lb 3 4/8/2010 4/8/2010 12780.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 5.55 8.22 0.87 13543 Btu/lb 8.7 0.92 6.54 8.62 0.88 13570 Btu/lb 9.22 0.94 6.29 9.57 0.88 13378 Btu/lb 10.21 0.94 5.61 8.01 0.92 13616 Btu/lb 8.49 0.97 5.57 9.93 0.9 13322 Btu/lb 10.52 0.95 5.99 8.47 0.92 13513 Btu/lb 9.01 0.98 5.95 7.55 0.9 13763 Btu/lb 8.03 0.96 6.18 7.32 0.91 13735 Btu/lb 7.8 0.97 6.1 7.93 0.89 13610 Btu/lb 8.45 0.95Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/ABeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/ANickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A 36 ppm N/A N/A N/A N/A 44 ppm N/A N/A N/A N/A 40 ppm N/A N/A Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 37.94 8.7 53.36 75.02 5.05 1.45 0.92 8.86 36.89 9.22 53.89 74.85 5.07 1.46 0.94 8.46 36.96 10.21 52.83 73.43 4.99 1.42 0.94 9.01 37.26 8.49 54.25 74.6 5.08 1.45 0.97 9.41 37.44 10.52 52.04 74.43 5.12 1.41 0.95 7.57 38.74 9.01 52.25 74.84 5.09 1.45 0.98 8.63 37.03 8.03 54.94 75.69 5.12 1.48 0.96 8.72 38.52 7.8 53.68 75.7 5.12 1.43 0.97 8.98 38.06 8.45 53.49 75 5.12 1.45 0.95 9.03 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 1385 Dale 3

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bituminous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm