Dolan Chemical Laboratory

4001 Bixby Road

Groveport, OH 43125

T: 614-836-4221, Audinet 210-4221

F: 614-836-4168, Audinet 210-4168

http://aepenv/labs

Water Analysis

Form REP-703

Rev. 0, 4/2012

Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 133312-001 Date Collected: 08/14/2013 Date Received: 8/15/2013

CPS Influent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 23.2 ug/L 0.050 0.010 DPC 08/21/2013 12:35 EPA 200.8

Arsenic, As 171 ug/L 0.10 0.030 DPC 08/21/2013 12:35 EPA 200.8

Barium, Ba 1120 ug/L 0.10 0.020 DPC 08/21/2013 12:35 EPA 200.8

Beryllium, Be < 15 ug/L U 50 15 DAM 08/26/2013 09:35 EPA 200.7

Cadmium, Cd 288 ug/L 0.050 0.010 DPC 08/21/2013 12:35 EPA 200.8

Chromium, Cr 1080 ug/L 0.20 0.040 DPC 08/21/2013 12:35 EPA 200.8

Cobalt, Co 353 ug/L 0.020 0.0040 DPC 08/21/2013 12:35 EPA 200.8

Copper, Cu 445 ug/L 0.050 0.010 DPC 08/21/2013 12:35 EPA 200.8

Lead, Pb 285 ug/L 0.010 0.0020 DPC 08/21/2013 12:35 EPA 200.8

Mercury, Hg 171000 ng/L 5000 2000 TLT 08/23/2013 EPA 1631E

Molybdenum, Mo 370 ug/L 0.050 0.010 DPC 08/21/2013 12:35 EPA 200.8

Nickel, Ni 1780 ug/L 0.20 0.050 DPC 08/21/2013 12:35 EPA 200.8

Selenium, Se 1080 ug/L 0.50 0.20 DPC 08/21/2013 12:35 EPA 200.8

Silver, Ag 0.564 ug/L 0.010 0.0020 DPC 08/21/2013 12:35 EPA 200.8

Thallium, Tl 14.8 ug/L 0.050 0.0020 DPC 08/21/2013 12:35 EPA 200.8

Tin, Sn 1030 ug/L 500 150 DAM 08/26/2013 09:35 EPA 200.7

Titanium, Ti 494 ug/L 100 15 DAM 08/26/2013 09:35 EPA 200.7

Zinc, Zn 4190 ug/L 0.50 0.10 DPC 08/21/2013 12:35 EPA 200.8

Aluminum, Al 73.8 mg/L 0.0010 0.0003 DPC 08/21/2013 12:35 EPA 200.8

Boron, B 501 mg/L 1.0 0.20 DAM 08/26/2013 09:35 EPA 200.7

Calcium, Ca 5530 mg/L 1.0 0.20 DAM 08/26/2013 09:35 EPA 200.7

Iron, Fe 311 mg/L 2.5 0.50 DAM 08/26/2013 09:35 EPA 200.7

Magnesium, Mg 4960 mg/L 0.50 0.10 DAM 08/26/2013 09:35 EPA 200.7

Manganese, Mn 91.3 mg/L 0.025 0.0050 DAM 08/26/2013 09:35 EPA 200.7

Potassium, K 104 mg/L 2.5 0.35 DAM 08/26/2013 09:34 EPA 200.7

Sodium, Na 374 mg/L 1.5 0.40 DAM 08/26/2013 09:34 EPA 200.7

Strontium, Sr 19.3 mg/L 0.050 0.015 DAM 08/26/2013 09:34 EPA 200.7

Ammonia, NH3, as N 0.20 mg/L 0.050 0.020 DMM 08/19/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 1.25 mg/L 0.50 0.10 DMM 08/21/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 42.1 mg/L 0.10 0.020 DMM 08/21/2013 SM20 4500NO3 H

Mountaineer Plant, 133312 Page 1 of 15
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 133312-001A Date Collected: 08/14/2013 Date Received: 8/15/2013

CPS Influent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.54 ug/L 0.050 0.010 DPC 08/21/2013 12:40 EPA 200.8

Arsenic, As 1.76 ug/L 0.10 0.030 DPC 08/21/2013 12:40 EPA 200.8

Barium, Ba 52.9 ug/L 0.10 0.020 DPC 08/21/2013 12:40 EPA 200.8

Beryllium, Be < 15 ug/L U 50 15 DAM 08/26/2013 09:39 EPA 200.7

Cadmium, Cd 160 ug/L 0.050 0.010 DPC 08/21/2013 12:40 EPA 200.8

Chromium, Cr 0.4 ug/L 0.20 0.040 DPC 08/21/2013 12:40 EPA 200.8

Cobalt, Co 218 ug/L 0.020 0.0040 DPC 08/21/2013 12:40 EPA 200.8

Copper, Cu 5.49 ug/L 0.050 0.010 DPC 08/21/2013 12:40 EPA 200.8

Lead, Pb 0.236 ug/L 0.010 0.0020 DPC 08/21/2013 12:40 EPA 200.8

Mercury, Hg 46.3 ng/L 10 4.0 TLT 08/23/2013 EPA 1631E

Molybdenum, Mo 143 ug/L 0.050 0.010 DPC 08/21/2013 12:40 EPA 200.8

Nickel, Ni 1080 ug/L 0.20 0.050 DPC 08/21/2013 12:40 EPA 200.8

Selenium, Se 277 ug/L 0.50 0.20 DPC 08/21/2013 12:40 EPA 200.8

Selenite, Se+4 (Hydride) 220 ug/L 20 4.0 TLT 09/04/2013 AEP Method

Silver, Ag 0.022 ug/L 0.010 0.0020 DPC 08/21/2013 12:40 EPA 200.8

Thallium, Tl 6.65 ug/L 0.050 0.0020 DPC 08/21/2013 12:40 EPA 200.8

Tin, Sn 310 ug/L 500 150 DAM 08/26/2013 09:39 EPA 200.7

Titanium, Ti < 15 ug/L U 100 15 DAM 08/26/2013 09:39 EPA 200.7

Zinc, Zn 711 ug/L 0.50 0.10 DPC 08/21/2013 12:40 EPA 200.8

Aluminum, Al 0.110 mg/L 0.0010 0.0003 DPC 08/21/2013 12:40 EPA 200.8

Boron, B 496 mg/L 1.0 0.20 DAM 08/26/2013 09:39 EPA 200.7

Calcium, Ca 687 mg/L 1.0 0.20 DAM 08/26/2013 09:39 EPA 200.7

Iron, Fe < 0.50 mg/L U 2.5 0.50 DAM 08/26/2013 09:39 EPA 200.7

Magnesium, Mg 4100 mg/L 0.50 0.10 DAM 08/26/2013 09:39 EPA 200.7

Manganese, Mn 84.8 mg/L 0.025 0.0050 DAM 08/26/2013 09:39 EPA 200.7

Potassium, K 76.3 mg/L 2.5 0.35 DAM 08/26/2013 09:37 EPA 200.7

Sodium, Na 358 mg/L 1.5 0.40 DAM 08/26/2013 09:37 EPA 200.7

Strontium, Sr 8.64 mg/L 0.050 0.015 DAM 08/26/2013 09:37 EPA 200.7

Mountaineer Plant, 133312 Page 2 of 15
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 133312-002 Date Collected: 08/14/2013 Date Received: 8/15/2013

 CPS Primary Clarifier Effluent

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.46 ug/L 0.050 0.010 DPC 08/21/2013 13:13 EPA 200.8

Arsenic, As 2.36 ug/L 0.10 0.030 DPC 08/21/2013 13:13 EPA 200.8

Barium, Ba 60.6 ug/L 0.10 0.020 DPC 08/21/2013 13:13 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/26/2013 09:43 EPA 200.7

Cadmium, Cd 0.60 ug/L 0.050 0.010 DPC 08/21/2013 13:13 EPA 200.8

Chromium, Cr 5.5 ug/L 0.20 0.040 DPC 08/21/2013 13:13 EPA 200.8

Cobalt, Co 13.7 ug/L 0.020 0.0040 DPC 08/21/2013 13:13 EPA 200.8

Copper, Cu 1.08 ug/L 0.050 0.010 DPC 08/21/2013 13:13 EPA 200.8

Lead, Pb 0.496 ug/L 0.010 0.0020 DPC 08/21/2013 13:13 EPA 200.8

Mercury, Hg 589 ng/L 250 100 TLT 08/28/2013 EPA 1631E

Molybdenum, Mo 186 ug/L 0.050 0.010 DPC 08/21/2013 13:13 EPA 200.8

Nickel, Ni 124 ug/L 0.20 0.050 DPC 08/21/2013 13:13 EPA 200.8

Selenium, Se 289 ug/L 0.50 0.20 DPC 08/21/2013 13:13 EPA 200.8

Silver, Ag 0.0060 ug/L J 0.010 0.0020 DPC 08/21/2013 13:13 EPA 200.8

Thallium, Tl 2.30 ug/L 0.050 0.0020 DPC 08/21/2013 13:13 EPA 200.8

Tin, Sn 137 ug/L 100 30 DAM 08/26/2013 09:43 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/26/2013 09:43 EPA 200.7

Zinc, Zn 12.3 ug/L 0.50 0.10 DPC 08/21/2013 13:13 EPA 200.8

Aluminum, Al 0.148 mg/L 0.0010 0.0003 DPC 08/21/2013 13:13 EPA 200.8

Boron, B 382 mg/L 0.20 0.040 DAM 08/26/2013 09:43 EPA 200.7

Calcium, Ca 765 mg/L 0.20 0.040 DAM 08/26/2013 09:43 EPA 200.7

Iron, Fe 0.44 mg/L J 0.50 0.10 DAM 08/26/2013 09:43 EPA 200.7

Magnesium, Mg 3210 mg/L 0.10 0.020 DAM 08/26/2013 09:43 EPA 200.7

Manganese, Mn 45.2 mg/L 0.0050 0.0010 DAM 08/26/2013 09:43 EPA 200.7

Potassium, K 62.7 mg/L 0.50 0.070 DAM 08/26/2013 09:41 EPA 200.7

Sodium, Na 301 mg/L 0.30 0.080 DAM 08/26/2013 09:41 EPA 200.7

Strontium, Sr 7.07 mg/L 0.010 0.0030 DAM 08/26/2013 09:41 EPA 200.7

Ammonia, NH3, as N 1.64 mg/L 0.050 0.020 DMM 08/19/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 8.53 mg/L 0.50 0.10 DMM 08/21/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 32.8 mg/L 0.10 0.020 DMM 08/21/2013 SM20 4500NO3 H

Mountaineer Plant, 133312 Page 3 of 15
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 133312-002A Date Collected: 08/14/2013 Date Received: 8/15/2013

 CPS Primary Clarifier Effluent Dissolved

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.24 ug/L 0.050 0.010 DPC 08/21/2013 13:18 EPA 200.8

Arsenic, As 1.99 ug/L 0.10 0.030 DPC 08/21/2013 13:18 EPA 200.8

Barium, Ba 54.4 ug/L 0.10 0.020 DPC 08/21/2013 13:18 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/26/2013 09:52 EPA 200.7

Cadmium, Cd 0.30 ug/L 0.050 0.010 DPC 08/21/2013 13:18 EPA 200.8

Chromium, Cr 3.5 ug/L 0.20 0.040 DPC 08/21/2013 13:18 EPA 200.8

Cobalt, Co 12.2 ug/L 0.020 0.0040 DPC 08/21/2013 13:18 EPA 200.8

Copper, Cu 0.42 ug/L 0.050 0.010 DPC 08/21/2013 13:18 EPA 200.8

Lead, Pb 0.040 ug/L 0.010 0.0020 DPC 08/21/2013 13:18 EPA 200.8

Mercury, Hg 11.5 ng/L 10 4.0 TLT 08/28/2013 EPA 1631E

Molybdenum, Mo 168 ug/L 0.050 0.010 DPC 08/21/2013 13:18 EPA 200.8

Nickel, Ni 113 ug/L 0.20 0.050 DPC 08/21/2013 13:18 EPA 200.8

Selenium, Se 259 ug/L 0.50 0.20 DPC 08/21/2013 13:18 EPA 200.8

Selenite, Se+4 (Hydride) 224 ug/L 20 4.0 TLT 09/04/2013 AEP Method

Silver, Ag 0.0020 ug/L J 0.010 0.0020 DPC 08/21/2013 13:18 EPA 200.8

Thallium, Tl 2.15 ug/L 0.050 0.0020 DPC 08/21/2013 13:18 EPA 200.8

Tin, Sn 118 ug/L 100 30 DAM 08/26/2013 09:52 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/26/2013 09:52 EPA 200.7

Zinc, Zn 6.7 ug/L 0.50 0.10 DPC 08/21/2013 13:18 EPA 200.8

Aluminum, Al 0.0291 mg/L 0.0010 0.0003 DPC 08/21/2013 13:18 EPA 200.8

Boron, B 390 mg/L 0.20 0.040 DAM 08/26/2013 09:52 EPA 200.7

Calcium, Ca 775 mg/L 0.20 0.040 DAM 08/26/2013 09:52 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 08/26/2013 09:52 EPA 200.7

Magnesium, Mg 3260 mg/L 0.10 0.020 DAM 08/26/2013 09:52 EPA 200.7

Manganese, Mn 45.9 mg/L 0.0050 0.0010 DAM 08/26/2013 09:52 EPA 200.7

Potassium, K 57.8 mg/L 0.50 0.070 DAM 08/26/2013 09:50 EPA 200.7

Sodium, Na 275 mg/L 0.30 0.080 DAM 08/26/2013 09:50 EPA 200.7

Strontium, Sr 6.44 mg/L 0.010 0.0030 DAM 08/26/2013 09:50 EPA 200.7

Mountaineer Plant, 133312 Page 4 of 15
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 133312-003 Date Collected: 08/14/2013 Date Received: 8/15/2013

CPS Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.20 ug/L 0.050 0.010 DPC 08/21/2013 13:23 EPA 200.8

Arsenic, As 1.95 ug/L 0.10 0.030 DPC 08/21/2013 13:23 EPA 200.8

Barium, Ba 64.5 ug/L 0.10 0.020 DPC 08/21/2013 13:23 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/26/2013 10:01 EPA 200.7

Cadmium, Cd 0.18 ug/L 0.050 0.010 DPC 08/21/2013 13:23 EPA 200.8

Chromium, Cr 3.4 ug/L 0.20 0.040 DPC 08/21/2013 13:23 EPA 200.8

Cobalt, Co 1.11 ug/L 0.020 0.0040 DPC 08/21/2013 13:23 EPA 200.8

Copper, Cu 0.65 ug/L 0.050 0.010 DPC 08/21/2013 13:23 EPA 200.8

Lead, Pb 0.136 ug/L 0.010 0.0020 DPC 08/21/2013 13:23 EPA 200.8

Mercury, Hg 115 ng/L 20 8.0 TLT 08/28/2013 EPA 1631E

Molybdenum, Mo 195 ug/L 0.050 0.010 DPC 08/21/2013 13:23 EPA 200.8

Nickel, Ni 24.3 ug/L 0.20 0.050 DPC 08/21/2013 13:23 EPA 200.8

Selenium, Se 229 ug/L 0.50 0.20 DPC 08/21/2013 13:23 EPA 200.8

Silver, Ag 0.0020 ug/L J 0.010 0.0020 DPC 08/21/2013 13:23 EPA 200.8

Thallium, Tl 0.91 ug/L 0.050 0.0020 DPC 08/21/2013 13:23 EPA 200.8

Tin, Sn 90 ug/L 100 30 DAM EPA 200.7

The dissolved result is significantly higher than the total recoverable result, indicating that there is a matrix interference present.

08/26/2013 10:01

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/26/2013 10:01 EPA 200.7

Zinc, Zn 3.4 ug/L 0.50 0.10 DPC 08/21/2013 13:23 EPA 200.8

Aluminum, Al 0.0971 mg/L 0.0010 0.0003 DPC 08/21/2013 13:23 EPA 200.8

Boron, B 310 mg/L 0.20 0.040 DAM 08/26/2013 10:01 EPA 200.7

Calcium, Ca 667 mg/L 0.20 0.040 DAM 08/26/2013 10:01 EPA 200.7

Iron, Fe 0.11 mg/L J 0.50 0.10 DAM 08/26/2013 10:01 EPA 200.7

Magnesium, Mg 2610 mg/L 0.10 0.020 DAM 08/26/2013 10:01 EPA 200.7

Manganese, Mn 34.9 mg/L 0.0050 0.0010 DAM 08/26/2013 10:01 EPA 200.7

Potassium, K 48.6 mg/L 0.50 0.070 DAM 08/26/2013 09:59 EPA 200.7

Sodium, Na 235 mg/L 0.30 0.080 DAM 08/26/2013 09:59 EPA 200.7

Strontium, Sr 5.84 mg/L 0.010 0.0030 DAM 08/26/2013 09:59 EPA 200.7

Ammonia, NH3, as N 1.22 mg/L 0.050 0.020 DMM 08/19/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 7.37 mg/L 0.50 0.10 DMM 08/21/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 27.5 mg/L 0.10 0.020 DMM 08/21/2013 SM20 4500NO3 H

Mountaineer Plant, 133312 Page 5 of 15
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 133312-003A Date Collected: 08/14/2013 Date Received: 8/15/2013

CPS Effluent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.15 ug/L 0.050 0.010 DPC 08/21/2013 13:28 EPA 200.8

Arsenic, As 1.74 ug/L 0.10 0.030 DPC 08/21/2013 13:28 EPA 200.8

Barium, Ba 58.6 ug/L 0.10 0.020 DPC 08/21/2013 13:28 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/26/2013 10:07 EPA 200.7

Cadmium, Cd 0.010 ug/L J 0.050 0.010 DPC 08/21/2013 13:28 EPA 200.8

Chromium, Cr 2.7 ug/L 0.20 0.040 DPC 08/21/2013 13:28 EPA 200.8

Cobalt, Co 0.320 ug/L 0.020 0.0040 DPC 08/21/2013 13:28 EPA 200.8

Copper, Cu 0.30 ug/L 0.050 0.010 DPC 08/21/2013 13:28 EPA 200.8

Lead, Pb 0.0050 ug/L J 0.010 0.0020 DPC 08/21/2013 13:28 EPA 200.8

Mercury, Hg 3.1 ng/L 2.0 0.80 TLT 08/28/2013 EPA 1631E

Molybdenum, Mo 178 ug/L 0.050 0.010 DPC 08/21/2013 13:28 EPA 200.8

Nickel, Ni 14.7 ug/L 0.20 0.050 DPC 08/21/2013 13:28 EPA 200.8

Selenium, Se 209 ug/L 0.50 0.20 DPC 08/21/2013 13:28 EPA 200.8

Selenite, Se+4 (Hydride) 164 ug/L 20 4.0 TLT 09/04/2013 AEP Method

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 08/21/2013 13:28 EPA 200.8

Thallium, Tl 0.66 ug/L 0.050 0.0020 DPC 08/21/2013 13:28 EPA 200.8

Tin, Sn 111 ug/L 100 30 DAM EPA 200.7

The dissolved result is significantly higher than the total recoverable result, indicating that there is a matrix interference present.

08/26/2013 10:07

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/26/2013 10:07 EPA 200.7

Zinc, Zn 3.7 ug/L 0.50 0.10 DPC 08/21/2013 13:28 EPA 200.8

Aluminum, Al 0.0328 mg/L 0.0010 0.0003 DPC 08/21/2013 13:28 EPA 200.8

Boron, B 314 mg/L 0.20 0.040 DAM 08/26/2013 10:07 EPA 200.7

Calcium, Ca 674 mg/L 0.20 0.040 DAM 08/26/2013 10:07 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 08/26/2013 10:07 EPA 200.7

Magnesium, Mg 2630 mg/L 0.10 0.020 DAM 08/26/2013 10:07 EPA 200.7

Manganese, Mn 35.2 mg/L 0.0050 0.0010 DAM 08/26/2013 10:07 EPA 200.7

Potassium, K 48.7 mg/L 0.50 0.070 DAM 08/26/2013 10:05 EPA 200.7

Sodium, Na 236 mg/L 0.30 0.080 DAM 08/26/2013 10:05 EPA 200.7

Strontium, Sr 5.86 mg/L 0.010 0.0030 DAM 08/26/2013 10:05 EPA 200.7

Mountaineer Plant, 133312 Page 6 of 15
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 133312-004 Date Collected: 08/14/2013 Date Received: 8/15/2013

Landfill Leachate 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 10.2 ug/L 0.050 0.010 DPC 08/21/2013 13:33 EPA 200.8

Arsenic, As 37.8 ug/L 0.10 0.030 DPC 08/21/2013 13:33 EPA 200.8

Barium, Ba 33.3 ug/L 0.10 0.020 DPC 08/21/2013 13:33 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/26/2013 10:11 EPA 200.7

Cadmium, Cd 1.20 ug/L 0.050 0.010 DPC 08/21/2013 13:33 EPA 200.8

Chromium, Cr 0.16 ug/L J 0.20 0.040 DPC 08/21/2013 13:33 EPA 200.8

Cobalt, Co 1.81 ug/L 0.020 0.0040 DPC 08/21/2013 13:33 EPA 200.8

Copper, Cu 0.30 ug/L 0.050 0.010 DPC 08/21/2013 13:33 EPA 200.8

Lead, Pb 0.027 ug/L 0.010 0.0020 DPC 08/21/2013 13:33 EPA 200.8

Mercury, Hg 39.0 ng/L 10 4.0 TLT 08/28/2013 EPA 1631E

Molybdenum, Mo 6390 ug/L 0.050 0.010 DPC 08/21/2013 13:33 EPA 200.8

Nickel, Ni 6.83 ug/L 0.20 0.050 DPC 08/21/2013 13:33 EPA 200.8

Selenium, Se 204 ug/L 0.50 0.20 DPC 08/21/2013 13:33 EPA 200.8

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 08/21/2013 13:33 EPA 200.8

Thallium, Tl 2.44 ug/L 0.050 0.0020 DPC 08/21/2013 13:33 EPA 200.8

Tin, Sn 98 ug/L 100 30 DAM 08/26/2013 10:11 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/26/2013 10:11 EPA 200.7

Zinc, Zn 2.0 ug/L 0.50 0.10 DPC 08/21/2013 13:33 EPA 200.8

Aluminum, Al 0.0163 mg/L 0.0010 0.0003 DPC 08/21/2013 13:33 EPA 200.8

Boron, B 54.5 mg/L 0.20 0.040 DAM 08/26/2013 10:11 EPA 200.7

Calcium, Ca 421 mg/L 0.20 0.040 DAM 08/26/2013 10:11 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 08/26/2013 10:11 EPA 200.7

Magnesium, Mg 391 mg/L 0.10 0.020 DAM 08/26/2013 10:11 EPA 200.7

Manganese, Mn 1.32 mg/L 0.0050 0.0010 DAM 08/26/2013 10:11 EPA 200.7

Potassium, K 112 mg/L 0.50 0.070 DAM 08/26/2013 10:09 EPA 200.7

Sodium, Na 1850 mg/L 0.30 0.080 DAM 08/26/2013 10:09 EPA 200.7

Strontium, Sr 5.69 mg/L 0.010 0.0030 DAM 08/26/2013 10:09 EPA 200.7

Ammonia, NH3, as N 0.76 mg/L 0.050 0.020 DMM 08/19/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 2.02 mg/L 0.50 0.10 DMM 08/21/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 2.53 mg/L 0.10 0.020 DMM 08/21/2013 SM20 4500NO3 H

Mountaineer Plant, 133312 Page 7 of 15
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 133312-004A Date Collected: 08/14/2013 Date Received: 8/15/2013

Landfill Leachate Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 8.79 ug/L 0.050 0.010 DPC 08/21/2013 13:37 EPA 200.8

Arsenic, As 31.8 ug/L 0.10 0.030 DPC 08/21/2013 13:37 EPA 200.8

Barium, Ba 28.7 ug/L 0.10 0.020 DPC 08/21/2013 13:37 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/26/2013 10:15 EPA 200.7

Cadmium, Cd 0.89 ug/L 0.050 0.010 DPC 08/21/2013 13:37 EPA 200.8

Chromium, Cr 0.057 ug/L J 0.20 0.040 DPC 08/21/2013 13:37 EPA 200.8

Cobalt, Co 1.42 ug/L 0.020 0.0040 DPC 08/21/2013 13:37 EPA 200.8

Copper, Cu 0.15 ug/L 0.050 0.010 DPC 08/21/2013 13:37 EPA 200.8

Lead, Pb 0.025 ug/L 0.010 0.0020 DPC 08/21/2013 13:37 EPA 200.8

Mercury, Hg 6.6 ng/L 2.0 0.80 TLT 08/28/2013 EPA 1631E

Molybdenum, Mo 5550 ug/L 0.050 0.010 DPC 08/21/2013 13:37 EPA 200.8

Nickel, Ni 5.42 ug/L 0.20 0.050 DPC 08/21/2013 13:37 EPA 200.8

Selenium, Se 149 ug/L 0.50 0.20 DPC 08/21/2013 13:37 EPA 200.8

Selenite, Se+4 (Hydride) 83.0 ug/L 20 4.0 TLT 09/04/2013 AEP Method

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 08/21/2013 13:37 EPA 200.8

Thallium, Tl 2.07 ug/L 0.050 0.0020 DPC 08/21/2013 13:37 EPA 200.8

Tin, Sn 87 ug/L 100 30 DAM 08/26/2013 10:15 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/26/2013 10:15 EPA 200.7

Zinc, Zn 2.2 ug/L 0.50 0.10 DPC 08/21/2013 13:37 EPA 200.8

Aluminum, Al 0.0059 mg/L 0.0010 0.0003 DPC 08/21/2013 13:37 EPA 200.8

Boron, B 52.1 mg/L 0.20 0.040 DAM 08/26/2013 10:15 EPA 200.7

Calcium, Ca 399 mg/L 0.20 0.040 DAM 08/26/2013 10:15 EPA 200.7

Iron, Fe < 0.10 mg/L U 0.50 0.10 DAM 08/26/2013 10:15 EPA 200.7

Magnesium, Mg 368 mg/L 0.10 0.020 DAM 08/26/2013 10:15 EPA 200.7

Manganese, Mn 1.23 mg/L 0.0050 0.0010 DAM 08/26/2013 10:15 EPA 200.7

Potassium, K 101 mg/L 0.50 0.070 DAM 08/26/2013 10:13 EPA 200.7

Sodium, Na 1660 mg/L 0.30 0.080 DAM 08/26/2013 10:13 EPA 200.7

Strontium, Sr 5.06 mg/L 0.010 0.0030 DAM 08/26/2013 10:13 EPA 200.7

Mountaineer Plant, 133312 Page 8 of 15
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 133312-005 Date Collected: 08/14/2013 Date Received: 8/15/2013

1st Stage Feed 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 5.06 ug/L 0.050 0.010 DPC 08/21/2013 13:42 EPA 200.8

Arsenic, As 16.7 ug/L 0.10 0.030 DPC 08/21/2013 13:42 EPA 200.8

Barium, Ba 50.8 ug/L 0.10 0.020 DPC 08/21/2013 13:42 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/26/2013 10:18 EPA 200.7

Cadmium, Cd 0.48 ug/L 0.050 0.010 DPC 08/21/2013 13:42 EPA 200.8

Chromium, Cr 2.8 ug/L 0.20 0.040 DPC 08/21/2013 13:42 EPA 200.8

Cobalt, Co 1.90 ug/L 0.020 0.0040 DPC 08/21/2013 13:42 EPA 200.8

Copper, Cu 1.02 ug/L 0.050 0.010 DPC 08/21/2013 13:42 EPA 200.8

Lead, Pb 0.088 ug/L 0.010 0.0020 DPC 08/21/2013 13:42 EPA 200.8

Mercury, Hg 86.7 ng/L 10 4.0 TLT 08/28/2013 EPA 1631E

Molybdenum, Mo 3050 ug/L 0.050 0.010 DPC 08/21/2013 13:42 EPA 200.8

Nickel, Ni 20.4 ug/L 0.20 0.050 DPC 08/21/2013 13:42 EPA 200.8

Selenium, Se 208 ug/L 0.50 0.20 DPC 08/21/2013 13:42 EPA 200.8

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 08/21/2013 13:42 EPA 200.8

Thallium, Tl 1.66 ug/L 0.050 0.0020 DPC 08/21/2013 13:42 EPA 200.8

Tin, Sn 73 ug/L 100 30 DAM EPA 200.7

The dissolved result is significantly higher than the total recoverable result, indicating that there is a matrix interference present.

08/26/2013 10:19

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/26/2013 10:19 EPA 200.7

Zinc, Zn 3.0 ug/L 0.50 0.10 DPC 08/21/2013 13:42 EPA 200.8

Aluminum, Al 0.0834 mg/L 0.0010 0.0003 DPC 08/21/2013 13:42 EPA 200.8

Boron, B 201 mg/L 0.20 0.040 DAM 08/26/2013 10:18 EPA 200.7

Calcium, Ca 565 mg/L 0.20 0.040 DAM 08/26/2013 10:18 EPA 200.7

Iron, Fe 1.58 mg/L 0.50 0.10 DAM 08/26/2013 10:19 EPA 200.7

Magnesium, Mg 1640 mg/L 0.10 0.020 DAM 08/26/2013 10:18 EPA 200.7

Manganese, Mn 20.6 mg/L 0.0050 0.0010 DAM 08/26/2013 10:18 EPA 200.7

Potassium, K 77.0 mg/L 0.50 0.070 DAM 08/26/2013 10:17 EPA 200.7

Sodium, Na 924 mg/L 0.30 0.080 DAM 08/26/2013 10:17 EPA 200.7

Strontium, Sr 5.81 mg/L 0.010 0.0030 DAM 08/26/2013 10:17 EPA 200.7

Ammonia, NH3, as N 0.89 mg/L 0.050 0.020 DMM 08/19/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 4.13 mg/L 0.50 0.10 DMM 08/21/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 15.6 mg/L 0.10 0.020 DMM 08/21/2013 SM20 4500NO3 H

Mountaineer Plant, 133312 Page 9 of 15
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 133312-005A Date Collected: 08/14/2013 Date Received: 8/15/2013

1st Stage Feed Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 4.88 ug/L 0.050 0.010 DPC 08/21/2013 13:47 EPA 200.8

Arsenic, As 7.94 ug/L 0.10 0.030 DPC 08/21/2013 13:47 EPA 200.8

Barium, Ba 46.3 ug/L 0.10 0.020 DPC 08/21/2013 13:47 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/26/2013 10:27 EPA 200.7

Cadmium, Cd 0.50 ug/L 0.050 0.010 DPC 08/21/2013 13:47 EPA 200.8

Chromium, Cr 0.050 ug/L J 0.20 0.040 DPC 08/21/2013 13:47 EPA 200.8

Cobalt, Co 1.92 ug/L 0.020 0.0040 DPC 08/21/2013 13:47 EPA 200.8

Copper, Cu 0.31 ug/L 0.050 0.010 DPC 08/21/2013 13:47 EPA 200.8

Lead, Pb 0.0040 ug/L J 0.010 0.0020 DPC 08/21/2013 13:47 EPA 200.8

Mercury, Hg 3.4 ng/L 2.0 0.80 TLT 08/28/2013 EPA 1631E

Molybdenum, Mo 2980 ug/L 0.050 0.010 DPC 08/21/2013 13:47 EPA 200.8

Nickel, Ni 19.4 ug/L 0.20 0.050 DPC 08/21/2013 13:47 EPA 200.8

Selenium, Se 132 ug/L 0.50 0.20 DPC 08/21/2013 13:47 EPA 200.8

Selenite, Se+4 (Hydride) 49.4 ug/L 20 4.0 TLT 09/04/2013 AEP Method

Silver, Ag 0.0020 ug/L J 0.010 0.0020 DPC 08/21/2013 13:47 EPA 200.8

Thallium, Tl 1.90 ug/L 0.050 0.0020 DPC 08/21/2013 13:47 EPA 200.8

Tin, Sn 177 ug/L 100 30 DAM EPA 200.7

The dissolved result is significantly higher than the total recoverable result, indicating that there is a matrix interference present.

08/26/2013 10:28

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/26/2013 10:28 EPA 200.7

Zinc, Zn 2.1 ug/L 0.50 0.10 DPC 08/21/2013 13:47 EPA 200.8

Aluminum, Al 0.0151 mg/L 0.0010 0.0003 DPC 08/21/2013 13:47 EPA 200.8

Boron, B 201 mg/L 0.20 0.040 DAM 08/26/2013 10:27 EPA 200.7

Calcium, Ca 562 mg/L 0.20 0.040 DAM 08/26/2013 10:27 EPA 200.7

Iron, Fe 0.855 mg/L 0.50 0.10 DAM 08/26/2013 10:28 EPA 200.7

Magnesium, Mg 1640 mg/L 0.10 0.020 DAM 08/26/2013 10:27 EPA 200.7

Manganese, Mn 21.4 mg/L 0.0050 0.0010 DAM 08/26/2013 10:27 EPA 200.7

Potassium, K 72.0 mg/L 0.50 0.070 DAM 08/26/2013 10:26 EPA 200.7

Sodium, Na 881 mg/L 0.30 0.080 DAM 08/26/2013 10:26 EPA 200.7

Strontium, Sr 5.53 mg/L 0.010 0.0030 DAM 08/26/2013 10:26 EPA 200.7

Mountaineer Plant, 133312 Page 10 of 15
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 133312-006 Date Collected: 08/14/2013 Date Received: 8/15/2013

Bioreactor Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.08 ug/L 0.050 0.010 DPC 08/21/2013 13:52 EPA 200.8

Arsenic, As 0.30 ug/L 0.10 0.030 DPC 08/21/2013 13:52 EPA 200.8

Barium, Ba 53.5 ug/L 0.10 0.020 DPC 08/21/2013 13:52 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/26/2013 10:49 EPA 200.7

Cadmium, Cd 0.027 ug/L J 0.050 0.010 DPC 08/21/2013 13:52 EPA 200.8

Chromium, Cr 0.7 ug/L 0.20 0.040 DPC 08/21/2013 13:52 EPA 200.8

Cobalt, Co 0.055 ug/L 0.020 0.0040 DPC 08/21/2013 13:52 EPA 200.8

Copper, Cu 0.14 ug/L 0.050 0.010 DPC 08/21/2013 13:52 EPA 200.8

Lead, Pb 0.010 ug/L 0.010 0.0020 DPC 08/21/2013 13:52 EPA 200.8

Mercury, Hg 1.8 ng/L 1.0 0.40 TLT 08/28/2013 EPA 1631E

Molybdenum, Mo 239 ug/L 0.050 0.010 DPC 08/21/2013 13:52 EPA 200.8

Nickel, Ni 1.68 ug/L 0.20 0.050 DPC 08/21/2013 13:52 EPA 200.8

Selenium, Se 1.1 ug/L 0.50 0.20 DPC 08/21/2013 13:52 EPA 200.8

Silver, Ag < 0.0020 ug/L U 0.010 0.0020 DPC 08/21/2013 13:52 EPA 200.8

Thallium, Tl 0.031 ug/L J 0.050 0.0020 DPC 08/21/2013 13:52 EPA 200.8

Tin, Sn 168 ug/L 100 30 DAM EPA 200.7

The dissolved result is significantly higher than the total recoverable result, indicating that there is a matrix interference present.

08/26/2013 10:50

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/26/2013 10:50 EPA 200.7

Zinc, Zn 0.5 ug/L 0.50 0.10 DPC 08/21/2013 13:52 EPA 200.8

Aluminum, Al 0.993 mg/L 0.0010 0.0003 DPC 08/21/2013 13:52 EPA 200.8

Boron, B 131 mg/L 0.20 0.040 DAM 08/26/2013 10:49 EPA 200.7

Calcium, Ca 569 mg/L 0.20 0.040 DAM 08/26/2013 10:49 EPA 200.7

Iron, Fe 0.27 mg/L J 0.50 0.10 DAM 08/26/2013 10:50 EPA 200.7

Magnesium, Mg 1330 mg/L 0.10 0.020 DAM 08/26/2013 10:49 EPA 200.7

Manganese, Mn 10.6 mg/L 0.0050 0.0010 DAM 08/26/2013 10:49 EPA 200.7

Potassium, K 71.5 mg/L 0.50 0.070 DAM 08/26/2013 10:48 EPA 200.7

Sodium, Na 891 mg/L 0.30 0.080 DAM 08/26/2013 10:48 EPA 200.7

Strontium, Sr 6.07 mg/L 0.010 0.0030 DAM 08/26/2013 10:48 EPA 200.7

Ammonia, NH3, as N 3.04 mg/L 0.050 0.020 DMM 08/19/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 6.31 mg/L 0.50 0.10 DMM 08/21/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N < 0.020 mg/L U 0.10 0.020 DMM 08/21/2013 SM20 4500NO3 H

Mountaineer Plant, 133312 Page 11 of 15
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 133312-006A Date Collected: 08/14/2013 Date Received: 8/15/2013

Bioreactor Effluent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.05 ug/L 0.050 0.010 DPC 08/21/2013 14:25 EPA 200.8

Arsenic, As 0.25 ug/L 0.10 0.030 DPC 08/21/2013 14:25 EPA 200.8

Barium, Ba 46.9 ug/L 0.10 0.020 DPC 08/21/2013 14:25 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/26/2013 10:53 EPA 200.7

Cadmium, Cd 0.021 ug/L J 0.050 0.010 DPC 08/21/2013 14:25 EPA 200.8

Chromium, Cr 0.6 ug/L 0.20 0.040 DPC 08/21/2013 14:25 EPA 200.8

Cobalt, Co 0.046 ug/L 0.020 0.0040 DPC 08/21/2013 14:25 EPA 200.8

Copper, Cu 0.036 ug/L J 0.050 0.010 DPC 08/21/2013 14:25 EPA 200.8

Lead, Pb 0.012 ug/L 0.010 0.0020 DPC 08/21/2013 14:25 EPA 200.8

Mercury, Hg 1.1 ng/L 0.50 0.20 TLT 08/28/2013 EPA 1631E

Molybdenum, Mo 208 ug/L 0.050 0.010 DPC 08/21/2013 14:25 EPA 200.8

Nickel, Ni 1.40 ug/L 0.20 0.050 DPC 08/21/2013 14:25 EPA 200.8

Selenium, Se 0.9 ug/L 0.50 0.20 DPC 08/21/2013 14:25 EPA 200.8

Selenite, Se+4 (Hydride) < 0.080 ug/L U 0.40 0.080 TLT 09/04/2013 AEP Method

Silver, Ag 0.0030 ug/L J 0.010 0.0020 DPC 08/21/2013 14:25 EPA 200.8

Thallium, Tl 0.06 ug/L 0.050 0.0020 DPC 08/21/2013 14:25 EPA 200.8

Tin, Sn 206 ug/L 100 30 DAM EPA 200.7

The dissolved result is significantly higher than the total recoverable result, indicating that there is a matrix interference present.

08/26/2013 10:54

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/26/2013 10:54 EPA 200.7

Zinc, Zn 1.1 ug/L 0.50 0.10 DPC 08/21/2013 14:25 EPA 200.8

Aluminum, Al 0.839 mg/L 0.0010 0.0003 DPC 08/21/2013 14:25 EPA 200.8

Boron, B 132 mg/L 0.20 0.040 DAM 08/26/2013 10:53 EPA 200.7

Calcium, Ca 567 mg/L 0.20 0.040 DAM 08/26/2013 10:53 EPA 200.7

Iron, Fe 0.24 mg/L J 0.50 0.10 DAM 08/26/2013 10:54 EPA 200.7

Magnesium, Mg 1320 mg/L 0.10 0.020 DAM 08/26/2013 10:53 EPA 200.7

Manganese, Mn 10.6 mg/L 0.0050 0.0010 DAM 08/26/2013 10:53 EPA 200.7

Potassium, K 70.7 mg/L 0.50 0.070 DAM 08/26/2013 10:52 EPA 200.7

Sodium, Na 865 mg/L 0.30 0.080 DAM 08/26/2013 10:52 EPA 200.7

Strontium, Sr 5.87 mg/L 0.010 0.0030 DAM 08/26/2013 10:52 EPA 200.7

Mountaineer Plant, 133312 Page 12 of 15
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 133312-007 Date Collected: 08/14/2013 Date Received: 8/15/2013

2nd Stage Feed 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 11.5 ug/L 0.050 0.010 DPC 08/21/2013 14:30 EPA 200.8

Arsenic, As 19.0 ug/L 0.10 0.030 DPC 08/21/2013 14:30 EPA 200.8

Barium, Ba 49.7 ug/L 0.10 0.020 DPC 08/21/2013 14:30 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/26/2013 10:57 EPA 200.7

Cadmium, Cd 0.40 ug/L 0.050 0.010 DPC 08/21/2013 14:30 EPA 200.8

Chromium, Cr 1.3 ug/L 0.20 0.040 DPC 08/21/2013 14:30 EPA 200.8

Cobalt, Co 2.32 ug/L 0.020 0.0040 DPC 08/21/2013 14:30 EPA 200.8

Copper, Cu 0.17 ug/L 0.050 0.010 DPC 08/21/2013 14:30 EPA 200.8

Lead, Pb 0.025 ug/L 0.010 0.0020 DPC 08/21/2013 14:30 EPA 200.8

Mercury, Hg 13.0 ng/L 10 4.0 TLT 08/28/2013 EPA 1631E

Molybdenum, Mo 3010 ug/L 0.050 0.010 DPC 08/21/2013 14:30 EPA 200.8

Nickel, Ni 12.1 ug/L 0.20 0.050 DPC 08/21/2013 14:30 EPA 200.8

Selenium, Se 25.7 ug/L 0.50 0.20 DPC 08/21/2013 14:30 EPA 200.8

Silver, Ag 0.0050 ug/L J 0.010 0.0020 DPC 08/21/2013 14:30 EPA 200.8

Thallium, Tl 1.16 ug/L 0.050 0.0020 DPC 08/21/2013 14:30 EPA 200.8

Tin, Sn 102 ug/L 100 30 DAM 08/26/2013 10:58 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/26/2013 10:58 EPA 200.7

Zinc, Zn 1.0 ug/L 0.50 0.10 DPC 08/21/2013 14:30 EPA 200.8

Aluminum, Al 0.544 mg/L 0.0010 0.0003 DPC 08/21/2013 14:30 EPA 200.8

Boron, B 172 mg/L 0.20 0.040 DAM 08/26/2013 10:57 EPA 200.7

Calcium, Ca 573 mg/L 0.20 0.040 DAM 08/26/2013 10:57 EPA 200.7

Iron, Fe 0.674 mg/L 0.50 0.10 DAM 08/26/2013 10:58 EPA 200.7

Magnesium, Mg 1580 mg/L 0.10 0.020 DAM 08/26/2013 10:57 EPA 200.7

Manganese, Mn 16.5 mg/L 0.0050 0.0010 DAM 08/26/2013 10:57 EPA 200.7

Potassium, K 69.9 mg/L 0.50 0.070 DAM 08/26/2013 10:56 EPA 200.7

Sodium, Na 831 mg/L 0.30 0.080 DAM 08/26/2013 10:56 EPA 200.7

Strontium, Sr 5.77 mg/L 0.010 0.0030 DAM 08/26/2013 10:56 EPA 200.7

Ammonia, NH3, as N 2.00 mg/L 0.050 0.020 DMM 08/19/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 6.18 mg/L 0.50 0.10 DMM 08/21/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 0.17 mg/L 0.10 0.020 DMM 08/21/2013 SM20 4500NO3 H

Mountaineer Plant, 133312 Page 13 of 15
Location: Mountaineer Plant Report Date: 9/9/2013

Sample Number: 133312-007A Date Collected: 08/14/2013 Date Received: 8/15/2013

2nd Stage Feed Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 10.1 ug/L 0.050 0.010 DPC 08/21/2013 14:35 EPA 200.8

Arsenic, As 15.8 ug/L 0.10 0.030 DPC 08/21/2013 14:35 EPA 200.8

Barium, Ba 43.7 ug/L 0.10 0.020 DPC 08/21/2013 14:35 EPA 200.8

Beryllium, Be < 3.0 ug/L U 10 3.0 DAM 08/26/2013 11:01 EPA 200.7

Cadmium, Cd 0.28 ug/L 0.050 0.010 DPC 08/21/2013 14:35 EPA 200.8

Chromium, Cr 0.9 ug/L 0.20 0.040 DPC 08/21/2013 14:35 EPA 200.8

Cobalt, Co 2.16 ug/L 0.020 0.0040 DPC 08/21/2013 14:35 EPA 200.8

Copper, Cu 0.11 ug/L 0.050 0.010 DPC 08/21/2013 14:35 EPA 200.8

Lead, Pb 0.019 ug/L 0.010 0.0020 DPC 08/21/2013 14:35 EPA 200.8

Mercury, Hg 3.8 ng/L 2.0 0.80 TLT 08/28/2013 EPA 1631E

Molybdenum, Mo 2670 ug/L 0.050 0.010 DPC 08/21/2013 14:35 EPA 200.8

Nickel, Ni 10.7 ug/L 0.20 0.050 DPC 08/21/2013 14:35 EPA 200.8

Selenium, Se 11.2 ug/L 0.50 0.20 DPC 08/21/2013 14:35 EPA 200.8

Selenite, Se+4 (Hydride) 1.9 ug/L 5.0 1.0 TLT AEP Method

lower than expected matrix spike recovery for Se+4 (70%, 74% rec).

J 09/04/2013

Silver, Ag 0.0020 ug/L J 0.010 0.0020 DPC 08/21/2013 14:35 EPA 200.8

Thallium, Tl 0.92 ug/L 0.050 0.0020 DPC 08/21/2013 14:35 EPA 200.8

Tin, Sn 68 ug/L 100 30 DAM 08/26/2013 11:02 EPA 200.7

Titanium, Ti < 3.0 ug/L U 20 3.0 DAM 08/26/2013 11:02 EPA 200.7

Zinc, Zn 1.6 ug/L 0.50 0.10 DPC 08/21/2013 14:35 EPA 200.8

Aluminum, Al 0.461 mg/L 0.0010 0.0003 DPC 08/21/2013 14:35 EPA 200.8

Boron, B 174 mg/L 0.20 0.040 DAM 08/26/2013 11:01 EPA 200.7

Calcium, Ca 578 mg/L 0.20 0.040 DAM 08/26/2013 11:01 EPA 200.7

Iron, Fe 0.503 mg/L 0.50 0.10 DAM 08/26/2013 11:02 EPA 200.7

Magnesium, Mg 1600 mg/L 0.10 0.020 DAM 08/26/2013 11:01 EPA 200.7

Manganese, Mn 16.7 mg/L 0.0050 0.0010 DAM 08/26/2013 11:01 EPA 200.7

Potassium, K 73.9 mg/L 0.50 0.070 DAM 08/26/2013 11:00 EPA 200.7

Sodium, Na 872 mg/L 0.30 0.080 DAM 08/26/2013 11:00 EPA 200.7

Strontium, Sr 6.09 mg/L 0.010 0.0030 DAM 08/26/2013 11:00 EPA 200.7

Sample Number: 133312-008 Date Collected: 08/14/2013 Date Received: 8/15/2013

Field Blank 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Mercury, Hg 0.23 ng/L J 0.50 0.20 TLT 08/28/2013 EPA 1631E

Sample Number: 133312-009 Date Collected: 08/15/2013 Date Received: 8/15/2013

 Filter Blank

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Mercury, Hg 0.28 ng/L J 0.50 0.20 TLT 08/28/2013 EPA 1631E

Mountaineer Plant, 133312 Page 14 of 15
Location: Mountaineer Plant Report Date: 9/9/2013

THIS TEST REPORT RELATES ONLY TO THE ITEMS TESTED AND SHALL NOT BE REPRODUCED EXCEPT IN FULL WITHOUT WRITTEN 

APPROVAL OF THE LABORATORY. ALL TEST RESULTS MEET ALL OF THE REQUIREMENTS OF THE ACCREDITING AUTHORITY, 

UNLESS OTHERWISE NOTED.

U: Analyte was analyzed and not detected at or above adjusted Method Detection Limit

J: Analyte was positively identified, though the quantitation was below Reporting Limit.

Brian Snyder, Chemist II

Email bssnyder@aep.com Tel. 614-836-4224

Fax 614-836-4168 Audinet 210-4224

Mountaineer Plant, 133312 Page 15 of 15