EMISSIONS TESTING FOR THE 

WOOL FIBERGLASS MANUFACTURING MACT ICR 

ON THE 

MELT FURNACE (EU 002) 

OWENS CORNING INSULATING SYSTEMS, LLC 

DECEMBER 20-22, 2011 

PROJECT NO.: 511250 

Prepared for 

OWENS CORNING SCIENCE AND TECHNOLOGY, LLC 

2222 West Bella Vista Street 

Lakeland, Florida 33810-0601 

ENTEC SERVICES, INC.

30 Monroe Drive 

Pelham, Alabama 35124 

(205) 358-1011 
Owens Corning Insulating Systems, LLC Project No. 511250 

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EMISSIONS TESTING FOR THE 

WOOL FIBERGLASS MANUFACTURING MACT ICR 

ON THE 

MELT FURNACE (EU 002) 

OWENS CORNING INSULATING SYSTEMS, LLC 

DECEMBER 20-22, 2011 

PROJECT NO.: 511250 

I certify that I have personally examined and am familiar with the information 

contained herein. Based on my inquiries of the individuals immediately responsible for 

obtaining the information, I believe the contents of this report deliverable to be true, 

accurate, and complete, to the best of my knowledge. 

Entec Project No. 511250 Report Submitted: February 1, 2012 

Completed By: Reviewed By: 

_________________________ __________________________ 

W. Keith Poole 

Manager, Reporting Division 

Troy Burrows 

QA / QC Manager 
Owens Corning Insulating Systems, LLC Project No. 511250 

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TABLE OF CONTENTS 

SECTION PAGE

1.0 EXECUTIVE SUMMARY ....................................................................................... 6 

2.0 SUMMARY OF TEST RESULTS .......................................................................... 7 

 2.1 SAMPLING ISSUES AND METHOD DEVIATIONS .................................. 7 

3.0 PROCESS DESCRIPTION ................................................................................. 10 

4.0 REFERENCE METHOD TEST PROCEDURES ................................................. 11 

4.1 US EPA REFERENCE TEST METHOD 1 

 -TRAVERSE POINT LAYOUT ................................................................ 11 

4.2 US EPA REFERENCE TEST METHOD 2 – VELOCITY ......................... 11 

4.3 US EPA REFERENCE TEST METHOD 3 – DRY GAS MOLECULAR 

 WEIGHT (CARBON DIOXIDE) ................................................................ 11 

4.4 US EPA REFERENCE TEST METHOD 4 – MOISTURE CONTENT ..... 12 

4.5 US EPA REFERENCE TEST METHOD 5 WITH 29- PARTICULATE 

 AND METALS. ......................................................................................... 12 

4.6 SW-846 DETERMINATION OF HEXAVALENT CHROMIUM 

 EMISSIONS FROM STATIONARY SOURCES ...................................... 13 

 

5.0 QA / QC PROCEDURES..................................................................................... 18 

 

6.0 CALIBRATION PROCEDURES .......................................................................... 20 
Owens Corning Insulating Systems, LLC Project No. 511250 

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LIST OF APPENDICES 

APPENDIX PAGE

A RAW TEST DATA AND EMISSION CALCULATIONS 

 MELT FURNACE (EU 002) – US EPA METHODS 1 – 4, 5/29 AND 0061 ........... 1 

 A.1 US EPA METHODS 1 - 4, 5/29 .................................................................... 2 

 A.2 US EPA METHOD 0061 ............................................................................ 19 

B QA/QC DOCUMENTS AND CHECKLISTS ......................................................... 36 

C LABORATORY DATA ......................................................................................... 50 

 C.1 ENTHALPY REPORT #1211-69 – 

 METHOD 5 MULTIPLE METALS AND PM ......................................................... 51 

 C.2 ELEMENT ONE REPORT #18035 – 

 METHOD 29 CHROMIUM ................................................................................... 66 

 C.3 ELEMENT ONE REPORT #17933 – METHOD 0061 – 

 TOTAL CHROMIUM AND HEXAVALENT CHROMIUM ..................................... 95 

D CALIBRATION DATA ........................................................................................ 135 

E QSTI CERTIFICATIONS ................................................................................... 140 

F SAMPLE CALCULATIONS AND NOMENCLATURE ........................................ 145 

G EPA ICR DOCUMENTS .................................................................................... 149 

 G.1 EPA LETTER AND ENCLOSURES 1 AND 2 ........................................ 150 

H CONFIDENTIAL PRODUCTION DATA (submitted separately by CD) ................... 
Owens Corning Insulating Systems, LLC Project No. 511250 

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LIST OF TABLES

TABLE PAGE

2-1 EMISSIONS SUMMARY – METHOD 29 ............................................................... 8 

2-2 EMISSIONS SUMMARY – METHOD 0061 ........................................................... 9 

LIST OF FIGURES

FIGURE PAGE

4-1 TRAVERSE POINT LAYOUT .............................................................................. 15 

4-2 METHOD 5 / 29 SAMPLE TRAIN DIAGRAM ...................................................... 16 

4-3 METHOD 0061 SAMPLE TRAIN DIAGRAM ....................................................... 17 
Owens Corning Insulating Systems, LLC Project No. 511250 

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1.0 EXECUTIVE SUMMARY

In October of 2011 the U. S. Environmental Protection Agency (US EPA) issued an 

Information Collection Request (ICR) to Owens Corning Insulating Systems, LLC. Within the 

Fiberglass Manufacturing ICR, Enclosure 2 specified the emission sources and pollutants that 

were required to be tested. Table 1.2 presented a Summary of Wool Fiberglass Manufacturing 

Source Test Methods and Alternate Methods and specified the test methods and parameters for 

each pollutant to be tested. These enclosures are included as attachments to this report and can 

be located in Appendix G. 

 Testing was conducted at Owens Corning Insulation LLC, Lakeland facility on December 

20-22, 2011 by Mr. Stewart Meadows, Mr. Flavel Smith (Gabby), Mr. Andrew Imes and Mr. Ed 

Brown of Entec Services, Inc. Representing OCIS was Mr. Rick Cooper who coordinated testing 

with plant production personnel. 
Owens Corning Insulating Systems, LLC Project No. 511250 

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2.0 SUMMARY OF TEST RESULTS

 Emission testing was conducted on the furnace stack for filterable particulate and total 

chromium per US EPA Methods 1, 2, 3, 3a, 4, 5 and 29 of 40 CFR 60, Appendix A. Method 

0061 of “Test Methods for Evaluating Solid Waste, Physical/Chemical Methods” was utilized to 

quantify Hexavalent chromium (CR+6) and total chromium. 

2.1 SAMPLING ISSUES AND METHOD DEVIATIONS 

 In section 7.4 of Method 0061, it states that the sample should be filtered through a 0.45 

micron acetate filter immediately following recovery to remove any insoluble material. This 

procedure was inadvertently not done by the field crew but was completed in the lab. The 

samples were received cold and basic by Element One. 

 No difficulties or problems were encountered during sampling on the furnace stack. The 

emissions test summaries on the following pages provide a detailed summary of each test. 
Owens Corning Insulating Systems, LLC Project No. 511250 

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Test Performed For: Testing Performed By:

Carolinas Division

Source(s) Tested: Project Manager:

Test Condition: Flavel Smith

Test(s) Performed:

Run Number Run 1 Run 2 Run 3 Average

Date of Run 12/20/11 12/21/11 12/22/11 -

Emission Test Run Time Began - Ended 1253-1713 1320-1737 1225-1632 -

102.04 97.84 100.13 100.00

122 129 125 125

2.53 2.74 2.67 2.65

45.78 47.32 47.05 46.72

3,960 4,004 4,012 3,992

4,330 4,475 4,450 4,418

3,859 3,894 3,905 3,886

Particulate Concentration gr/dscf 1.26E-03 2.74E-03 9.42E-04 1.65E-03

Particulate Concentration mg/m3 2.88 6.27 2.16 3.77

Particulate Concentration mg/m3 @ 7% O2 57.14 124.53 42.82 74.83

Particulate Emissions Lbs/Hr 4.16E-02 9.15E-02 3.15E-02 5.49E-02

Vaporous Chromium Concentration gr/dscf 1.59E-07 8.77E-08 4.98E-08 9.88E-08

Vaporous Chromium Concentration mg/m3 3.64E-04 2.01E-04 1.14E-04 2.26E-04

Vaporous Chromium Concentration mg/m3 @ 7% O2 7.22E-03 3.98E-03 2.26E-03 4.49E-03

Vaporous Chromium Emissions Lbs/Hr 5.26E-06 2.93E-06 1.67E-06 3.28E-06

Filterable Chromium Concentration gr/dscf 2.79E-07 1.72E-07 1.41E-07 1.97E-07

Filterable Chromium Concentration mg/m3 6.38E-04 3.93E-04 3.23E-04 4.52E-04

Filterable Chromium Concentration mg/m3 @ 7% O2 1.27E-02 7.81E-03 6.42E-03 8.97E-03

Filterable Chromium Emissions Lbs/Hr 9.22E-06 5.73E-06 4.73E-06 6.56E-06

Total Chromium Concentration gr/dscf 4.38E-07 2.59E-07 1.91E-07 2.97E-07

Total Chromium Concentration mg/m3 1.00E-03 5.94E-04 4.37E-04 6.79E-04

Total Chromium Concentration mg/m3 @ 7% O2 1.99E-02 1.18E-02 8.69E-03 1.35E-02

Total Chromium Emissions Lbs/Hr 1.45E-05 8.66E-06 6.40E-06 9.88E-06

Stack Gas Flow, ACFM

Stack Temperature, o

F

Stack Gas Flow, SCFM

Stack Gas Velocity, F/S

Moisture Content, % volume

Table 2-1

Emissions Summary

Volumetric Flow Rate, DSCFM

Owens Corning Lakeland Plant

Lakeland, FL

Section 114 Testing

Melt Furnace (EU 002)

Method 29 Total Chromium and Filterable Particulate

Isokinetic Sampling Rate, %
Owens Corning Insulating Systems, LLC Project No. 51125

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Test Performed For: Testing Performed B

Carolinas Division

Source(s) Tested: Project Manager:Test Condition: Flavel SmithTest(s) Performed:

Run Number Run 1 Run 2 Run 3 Average

Date of Run 12/20/11 12/21/11 12/22/11 -

Emission Test Run Time Began - Ended 0810-1215 0751-1223 0747-1153 -

102.99 102.49 103.04 102.84

111 127 126 121

4.54 5.42 7.53 5.83

45.58 46.04 46.85 46.164,019 3,913 3,985 3,9724,311 4,354 4,431 4,3653,836 3,701 3,685 3,741

Hexavalent Chromium Concentration gr/dscf 2.42E-07 1.20E-06 1.20E-07 5.20E-07

Hexavalent Chromium Concentration mg/m3 5.54E-04 2.74E-03 2.74E-04 1.19E-03

Hexavalent Chromium Concentration mg/m3 @ 7% O2 1.15E-02 4.89E-02 7.20E-03 2.25E-02

Hexavalent Chromium Emissions Lbs/Hr 7.95E-06 1.05E-06 4.60E-07 3.16E-06Total Chromium Concentration gr/dscf 2.65E-06 1.20E-06 1.20E-07 1.32E-06

Total Chromium Concentration mg/m3 6.07E-03 2.74E-03 2.74E-04 3.03E-03

Total Chromium Concentration mg/m3 @ 7% O2 1.26E-01 4.89E-02 7.20E-03 6.07E-02

Total Chromium Emissions Lbs/Hr 8.72E-05 3.80E-05 3.79E-06 4.30E-05

=DLL (detection level limited)

Table 2-2

Emissions Summary

FurnaceHex/Total Chrome per method 0061

Isokinetic Sampling Rate, %Volumetric Flow Rate, DSCFM

Owens Corning Lakeland PlantLakeland, FLSection 114 Testing

Stack Temperature, oFStack Gas Flow, SCFMStack Gas Velocity, F/SMoisture Content, % volumeStack Gas Flow, ACFM
Owens Corning Insulating Systems, LLC Project No. 511250 

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3.0 PROCESS DESCRIPTION 

Raw Material Handling (Emission Unit (EU) 001)

Raw materials are delivered via rail car or truck for large volume supplies and in 

drums or bags for smaller volume supplies. Pneumatic and vibrator/gravity systems are 

used to unload the bulk raw materials to silos, with two common bin vent fabric filters. Bulk 

raw materials are gravity-fed through a fabric tube to a weigh station and then dropped to a 

mixer for blending. These operations take place inside the manufacturing building. 

Particulate matter (PM/PM10) emissions from raw material handling operations (EU 

001) are controlled by two Model No. 49S-8-20-TR-B Mikropul–Mikro-Pulsaire Bin Vent 

fabric filter baghouses each with a design gas flow rate of 2,800 acfm; and one (1) Model 

16AVS6 AirLanco Bin Vent fabric filter baghouse with a design gas flow rate of 1,250 acfm. 

Melting (EU 002) – Melting Furnace

After weighing and mixing, the raw materials are conveyed pneumatically to the two 

(2) cold top electric melting furnaces where molten glass is formed. The molten glass leaves 

the furnace and passes through the enclosed riser and the forehearth where it is cooled to 

the proper temperature for forming. 

Particulate matter (PM/PM10) emissions from raw material transfer to and operation 

of the two (2) melting furnaces (EU 002) are controlled by two (2) Model No. 64S-8-20-TR-B 

Mikropul–Mikro-Pulsaire high temperature fabric filter baghouses (one for each furnace), 

each with a design gas flow rate of 3,600 acfm. 
Owens Corning Insulating Systems, LLC Project No. 511250 

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4.0 REFERENCE METHOD TEST PROCEDURES 

 Emission rates were determined using US EPA Reference Test Methods 1, 2, 3, 4, 5 

and 29 of US EPA 40 CFR 60, Appendix A and Test Methods for Evaluating Solid Waste, 

Physical/Chemical Methods Method 0061. Calibration and quality assurance procedures of US 

EPA 40 CFR Part 60, Appendix A and the “Quality Assurance Handbook for Air Pollution 

Measurement System” Volume III Stationary Source-Specific Methods were followed throughout 

the duration of field and laboratory testing for all methods. The most current version for each 

method (as described in the Federal Register) was used. 

 

4.1 US EPA REFERENCE TEST METHOD 1 - TRAVERSE POINT LAYOUT 

For Information on stack dimensions, traverse points, distance to disturbance and other 

relevant data, refer to the drawing presented in Figure 4-1, “Stack Drawing and Traverse Point 

Location”. 

 

4.2 US EPA REFERENCE TEST METHOD 2 – VELOCITY 

The velocity of the gas stream was determined according to US EPA Reference Method 

2 by reading the instantaneous velocity head with an inclined manometer at each sampling point 

with a calibrated S-type pitot. The stack pressure was measured with the static side of an Stype pitot tube. A calibrated pyrometer was used to measure stack temperature at each 

sampling point. All test data, worksheets, and spreadsheets presenting the calculations are 

included in Appendix A. Calibration procedures for the velocity equipment are located in 

Section 6.0 of this report. Pitot tube, thermocouple, and other measurement device calibration 

worksheets used for the test series are presented in Appendix D. 

4.3 US EPA REFERENCE TEST METHOD 3 - DRY GAS MOLECULAR WEIGHT-CARBON 

 DIOXIDE 

Dry Gas molecular weight (carbon dioxide) was determined using US EPA Reference 

Test Method 3 (Fyrite Method). A sample of the flue gas was extracted from the gas stream 

during each test. These samples were analyzed with a Fyrite gas analyzer. The molecular 

weight of the gas was calculated using the moisture, oxygen and carbon dioxide content, and 

the measured stack gas temperature. 
Owens Corning Insulating Systems, LLC Project No. 511250 

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4.4 US EPA REFERENCE TEST METHOD 4 - MOISTURE CONTENT 

The moisture content used for calculating the gas stream flow rate was determined by 

measuring the moisture in a series of glass impingers and silica gel impinger gravimetrically with 

an analytical balance with a tolerance of 0.1 g. The volume of gas drawn was corrected to dry 

standard conditions. The dry gas meter and thermocouple calibration forms are contained in 

Appendix I. 

4.5 US EPA REFERENCE TEST METHOD 5 WITH METHOD 29 – PARTICULATE AND 

METALS DETERMINATION 

 The particulate/multiple metals sample train consisted of a heated stainless steel sample 

probe with a glass liner equipped with an S-type pitot tube and thermocouple. The probe was 

attached to a sample module consisting of a heated filter compartment, which houses the in-line 

filter holder equipped with a pre-weighed quartz filter for the collection of the particulate, and a 

series of glass impingers to collect metals and determine moisture. The sample module was 

connected to a control module by means of an umbilical cord. The control module consisted of a 

dry gas meter, calibrated orifice, leak free pump, two inclined manometers, and temperature 

controllers for the heated filter compartment, the probe, and a thermocouple indicator to monitor 

the required temperatures during the testing. 

 Gas samples were collected as follows: the sample gas was drawn through the sampling 

probe isokinetically and passed through a 3-inch quartz filter on to which particulate matter was 

deposited. The sample gas was then passed through a series of ice-cooled impingers. The first 

and second impingers contained exactly 100 ml each of an absorbing solution (5% HNO3 10% 

H2O2). The third impinger was empty. The fourth impinger contained exactly 250 g of silica gel, 

which absorbed any remaining moisture. These impingers were placed in an ice-bath to 

maintain a maximum exit temperature of < 68o

 F. The sample gas then passed through a 

vacuum pump followed by a dry gas meter. The dry gas meter integrated the sample gas flow 

throughout the duration of the test. A calibrated orifice attached to the outlet of the dry gas 

meter provided real time flow rate data. 

 A representative gas sample was acquired by sampling for equal periods of time at the 

centroid of a number of equal area regions in the exhaust stack. The sampling rate was 

adjusted at each test point maintaining an isokinetic sampling condition. 
Owens Corning Insulating Systems, LLC Project No. 511250 

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 After the sampling was complete, the filter was removed and placed in a storage 

container. The nozzle, probe liner, and inlet side of the filter holder were quantitatively washed 

with exactly 100 ml of reagent grade acetone and stored in a marked and sealed container. The 

nozzle, probe liner, and inlet side of the filter holder were rinsed again with 0.1N HNO3 and 

placed into another marked and sealed container. The nozzle and probe liner were then rinsed 

with DI water and followed by another acetone rinse. These rinses were not retained and were 

a QA/QC step to ensure clean glassware prior to starting another run. The liquids from the first 

and second impingers were weighed and added to a third marked and sealed container. The 

back half of the filter holder and these two impingers were rinsed with exactly 100 ml of 0.1N 

HNO3 and the rinses were added to the same container. The contents of the third impinger were 

weighed and then rinsed with exactly 100 ml of 0.1N HNO3 and the rinses were placed in a 

fourth marked and sealed container. All the samples were shipped to Enthalpy Analytical for 

particulate analysis. Enthalpy sub-contracted the metals analysis to Element One of 

Wilmington, NC for metals analysis. The fourth impinger was weighed to determine moisture 

catch of the silica gel. 

4.6 SW-846 DETERMINATION OF HEXAVALENT CHROMIUM EMISSIONS FROM 

STATIONARY SOURCES 

SCOPE AND APPLICATION 

 This method provides procedures for the determination of hexavalent chromium (Cr+6) 

emissions from hazardous waste incinerators, municipal waste incinerators, municipal waste 

combustors, and sewage sludge incinerators. With the approval of the Administrator, this 

method may also be used to measure total chromium. The sampling train, constructed of Teflon 

components, has only been evaluated at temperatures of less than 300o

F. Trains constructed of 

other materials, for testing at higher temperatures, are currently being evaluated. 

 Range: If employing a preconcentration procedure, the lower limit of the detection 

range can be extended to 16 nanograms per dry standard cubic meter (ng/dscm) with a 3 dscm 

gas sample (0.1 ppb in solution). With sample dilution, there is no upper limit. Follow your 

manufacturer's specific instructions on employing the preconcentration procedure for these 

analyses. 
Owens Corning Insulating Systems, LLC Project No. 511250 

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SUMMARY OF METHOD 

 For incinerators and combustors, the Cr+6 emissions are collected isokinetically from 

the source: To eliminate the possibility of Cr+6 reduction between the nozzle and impinger, the 

emission samples are collected with a recirculatory train where the impinger reagent is 

continuously recirculated to the nozzle. Recovery procedures include a post-sampling purge 

and filtration. The impinger train samples are analyzed for Cr+6 by an ion chromatograph 

equipped with a post-column reactor and a visible wavelength detector. The IC/PCR separates 

the Cr+6 as chromate (CrO4

=

) from other diphenylcarbazide reactions that occur in the postcolumn reactor. To increase sensitivity for trace levels of chromium, a preconcentration system 

may also be used in conjunction with the IC/PCR. 

INTERFERENCES 

 Components in the sample matrix may cause Cr+6 to convert to trivalent chromium 

(Cr+3) or cause Cr+3 to convert to Cr+6. A post-sampling nitrogen purge and sample filtration are 

included to eliminate many of these interferences. 

 The chromatographic separation of Cr+6 using ion chromatography reduces the 

potential for other metals to interfere with the post-column reaction. For the IC/PCR analysis, 

only compounds that coelute with Cr+6 and affect the diphenylcarbazide reaction will cause 

interference. 

 Sample cross-contamination that can occur when high-level and low-level samples 

or standards are analyzed alternately is eliminated by thorough purging of the sample loop. 

Purging can easily be obtained by increasing the injection volume of the samples to ten times 

the size of the sample loop. 
Owens Corning Insulating Systems, LLC Project No. 511250 

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Client: Job No. :

Source: Input By:

P Port Type Nipple Port Diameter

17

80

Inches

Duct 

Diameters

154.0 9.06

240.0 14.12 4 4

Point No.

1 1.1 7.1

2 4.3 10.3

3 12.8 18.8

4 15.9 21.9

 

* Adjusted points diameter > 24" no point closer than 1.0 inch

* Adjusted points diameter < 24" no point closer than 0.5 inch

Stack Diameters between 12-24 inches minimum points are 8 ; 

4 points per port if the 8 / 2 diameters downstream and

upstream criteria is met.

Furnace

Distance "A"

Distance "B"

2

6.00

Total Number of Traverse Points:

Number of Points per port / traverse:

Number of Ports:

Length of Port, inches:

Inches

Inside Stack Outside Nipple

Inches

8

Figure 4-1

Entec Services, Inc

30 Monroe Dr. Pelham, AL 35124

Stack Area, Ft2 Stack Diameter, inches: :

Stack Properties:

Type of Traverse: Velocity (V) or Particulate (P):

STACK DRAWING & TRAVERSE POINT LOCATION

511250

Stewart 

Meadows

4

1.576

Owens Corning Lakeland Plant

Stack Height, feet:

Upstream From Flow Disturbance (A):

Downstream From Flow Disturbance (B):

INCHES

17.0 INCHES

INCHES

240.0

154.0
Owens Corning Insulating Systems, LLC Project No. 511250 

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Owens Corning Insulating Systems, LLC Project No. 511250 

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Owens Corning Insulating Systems, LLC Project No. 511250 

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5.0 QA / QC PROCEDURES 

Specific Quality Assurance / Quality Control (QA / QC) procedures were adhered to 

during this test project to provide valid and scientifically defensible data. For any environmental 

field and laboratory measurement, a degree of uncertainty exists in the data due to inherent 

limitations of the measurement systems employed. Entec Services, Inc. objective of the QA / 

QC program is to produce data of known precision, accuracy, representation, completeness, 

and comparability. Special Entec-designed QA/QC checklists are contained in Appendix B. 

For purposes of the ICR, US EPA outlined procedures for quantifying measured values 

below the detection limit in Enclosure 2, Section 2.2. 

Identify the status of measured values relative to detection levels on the spreadsheet or 

in the ERT using the following descriptions: 

• BDL (below detection level) – all analytical values used to calculate and report an instack emissions value are less than the laboratory’s reported detection level(s); 

• DLL (detection level limited) – at least one but not all values used to calculate and 

report an in-stack emissions value are less than the laboratory’s reported detection level(s); or 

• ADL (above detection level) – all analytical values used to calculate and report an instack emissions value are greater than the laboratory’s reported detection level(s). 

For each reported emissions value, insert the appropriate flag (BDL, DLL, or ADL) in the 

Notes line of Excel emission test spreadsheet template or in the Comments line of the 

Electronic Reporting Tool (ERT). 

 When reporting and calculating individual test run data: 

• For analytical data reported from the lab as “nondetect” or “below detection level;” 

− Include a brief description of the procedures used to determine the analytical detection 

 and in-stack detection levels: 

 o In the Notes line of Excel emission test spreadsheet template; or 

 o In the Comments line of Lab Data tab in the Run Data Details in the ERT. 

− Describe these procedures completely in a separate attachment including the 

 measurements made, the standards used, and the statistical procedures applied. 

− Calculate in-stack emissions rate for any analytical measurement below detection level 

 using the relevant detection level as the “real” value. 

− Report the calculated emissions concentration or rate result: 
Owens Corning Insulating Systems, LLC Project No. 511250 

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 o As a bracketed “less than” detection level value (e.g., [<0.0105]) in the Excel emission 

 test spreadsheet template and include the appropriate flag in the Notes line; or 

 o As a “real” value in the ERT with the appropriate flag in the Comments line. 

− Report as “real” values (i.e., no brackets or < symbol) any analytical data measured 

 above the detection level including any data between the analytical detection level and a 

 laboratory-specific reporting or quantification level (i.e., flag as ADL). 

• For pollutant measurements composed of multiple components or fractions (e.g., Hg 

 and other metals sampling trains) when the result for the value for any component is 

 measured below the analytical detection level: 

− Calculate in-stack emissions rate or concentrations as outlined above for each 

 component or fraction; 

− Sum the measured and detection level values as outlined above using the in-stack 

 emissions rate or concentrations for all of the components or fractions; and 

− Report the sum of all components or fractions: 

 o As a bracketed “less than” detection level value (e.g., [<0.0105]) in the Excel emission 

 test spreadsheet template and include the appropriate flag in the Notes line; or 

 o As a “real” value in the ERT with the appropriate flag in the Comments line. 

− Report also the individual component or fraction values for each run if the Excel 

 emission test spreadsheet template or ERT format allows; if not (i.e., the format allows 

 reporting only a single sum value): 

 o For the Excel emission test spreadsheet template, next to the sum reported as above 

 report in the Notes line the appropriate flag along with the values for the measured or 

 detection level value for each component or fraction as used in the calculations (e.g., 

 0.036, [<0.069], 1.239, [<0.945] for a four fraction sample). 

 o For the ERT, next to the sum reported as above, report on the Comments line the 

 appropriate flag and the measured or detection level value for each 
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6.0 CALIBRATION PROCEDURES 

 All of the emission testing equipment used was calibrated according to the procedures 

outlined in the EPA 40 CFR Part 60 Appendix “A” and the Quality Assurance Handbook for Air 

Pollution Measurement Systems, Volume III, EPA-600/4-94-038b. Complete calibration records 

are located in the appendix of this report. 
APPENDIX A 

RAW TEST DATA AND EMISSIONS CALCULATIONS 

MELT FURNACE (EU 002) 

US EPA METHODS 1-4, 5/29 AND 0061 

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 1 of 167
APPENDIX A.1 

RAW TEST DATA AND EMISSIONS CALCULATIONS 

MELT FURNACE (EU 002) 

US EPA METHODS 1-4, 5/29 

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 2 of 167
EPA Method 1

EPA Method 2

EPA Method 3

EPA Method 4

EPA Method 5/29

12/20/11 12/21/11 12/22/11

SOURCE OVERVIEW

Sample Location

0.1N NaOH

PM & Metals (Total Cr)

SOURCE(S) SHAPE: Circular

Entec Services, Inc.

SOURCE OWNER:

PLANT LOCATION:

SOURCE(S) CONDITION:

Owens Corning Lakeland Plant

Section 114 Testing

Lakeland, FL

SOURCE(S) NAME(S): Furnace

Rick Cooper

REFERENCE METHOD TESTS:

Moisture Content

Molecular Weight

Florida Department of Environmental Protection (FDEP)

OWNER'S REPRESENTATIVE:

ENVIRONMENTAL ANALYST - ASSISTANT Kyle Vaughan

ENTEC PROJECT NUMBER:

DATES TESTS CONDUCTED:

511250

RULING AGENCY :

ENVIRONMENTAL ANALYST - ASSISTANT Stewart Meadows

PROBE WASH CHEMICAL:

Volumetric Flow

PROJECT MANAGER Flavel Smith

TEST PERFORMED: Method 29 Total Chromium

ADDITIONAL TEST REQUIREMENTS: Minimum Run Time (240 minutes) 

SOURCE PERMIT NUMBER: FDEP 1050375-006-AO

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 3 of 167
Client: 

Source:

Symbol Units

- - 1 2 3AVERAGE

- - 12/20/11 12/21/11 12/22/11

- Military Time 1253-1713 1320-1737 1225-1632

 minutes 240 240 240 240

As Ft2 1.576 1.576 1.576

Pbar in. Hg 30.22 29.91 29.91 30.01

Pg in. H20 -0.37 -0.37 -0.37 -0.37

Pitot Tube Correction factor Cp - 0.84 0.84 0.84 0.84

Meter Correction Factor Y - 0.937 0.937 0.937 0.937

H@ in. H20 2.002 2.002 2.002 2.002

Dn inches 0.220 0.220 0.220 0.220

Vm dcf 173.663 170.940 175.499 173.367

tm

o

F 90.0 93.9 94.1 92.7

H in. H20 1.49 1.53 1.55 1.52

Wimp grams 55.0 65.0 65.0 61.7

Wsg grams 32.4 26.5 26.4 28.4

O2 % 20.2 20.2 20.2 20.2

CO2 % 0.7 0.9 1.0 0.9

(sqrt P)avg (in. H20)1/2 0.777 0.794 0.793 0.788

ts

o

F 122.4 129.1 124.6 125.4

Cr mgCr 0.0045 0.0026 0.0019 0.0030

mn mg 12.9 27.2 9.6 16.6

ENTEC Services, Inc.

INPUT TEST DATA

Field Data Test Data

Data Input By:

511250

Stewart Meadows

Job No.:

Emission Test Run Time Began - Ended

Sampling Time

Owens Corning Lakeland Plant

Furnace

Stack Area

Run Number

Test Date

Meter Volume

Meter Temperature

Avg. Orifice Delta H

Impingers Weight Gain (Moisture)

Barometric Pressure

Stack Static Pressure

Meter Delta H @

Nozzle Diameter

Total Chromium Collected

Silica Gel Impinger Weight Gain (Moisture)

Oxygen Concentration, dry basis

Carbon Dioxide Concentration, dry basis

30 Monroe Dr. Pelham, AL 35124

Filterable Particulate Collected

Avg. Sq. Rt. of Delta P

Stack Temperature

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 4 of 167
Client: Owens Corning Lakeland Plant 511250

Source: Furnace

Formulas Symbol Units

- - 1 2 3AVERAGE

- - 12/20/11 12/21/11 12/22/11

- Military Time 1253-1713 1320-1737 1225-1632

1. Stack Pressure = Pbar + Pg / 13.6 Ps in. Hg 30.19 29.88 29.88 29.99

2. Meter Pressure = Pbar + H / 13.6 Pm in. Hg 30.33 30.02 30.02 30.13

3. Standard Meter Volume = 17.64* Y* (Vm/Tm)* (Pbar + H / 13.6) Vm(std) dscf 158.287 153.150 157.184 156.207

4a. Standard Volume of Water Vapor Condensed =0.04706*Wimp Vwc(std) scf 2.588 3.059 3.059 2.902

4b. Standard Volume of Water Collected in Silica Gel =0.04715*Wsg Vwsg(std) scf 1.528 1.249 1.245 1.341

5. Moisture Fraction =(Vwc(std) + Vwsg(std))/(Vwc(std) + Vwsg(std) + Vm(std)) Bws fraction 0.0253 0.0274 0.0267 0.0265

6. Moisture Fraction @ Saturation (Theoretical) =10[6.37-(2827/(ts+460-95.2)]/Ps TBws fraction 0.1223 0.1483 0.1313 0.1340

7. Standard Water Volume @ Saturation (Theoretical) =Vm(std) * (TBws)/(1-TBws) TVW(std) scf 22.063 26.659 23.767 24.163

8. Volume of Water @ Saturation (Theoretical) =TVw(std)/0.04707 TVlc ml 468.7 566.4 504.9 513.3

9. Molecular Weight Of Stack Gas, dry basis = 0.32*(O2)+ 0.44*(CO2)+0.28*(100-(O2)-(CO2)) Md g/g-mole 28.920 28.952 28.968 28.947

10. Molecular Weight Of Stack Gas, wet basis = Md*(1-Bws)+18.0*(Bws) Ms g/g-mole 28.643 28.652 28.676 28.657

11. Average Stack Gas Velocity = 85.49*Cp*(sqrt P)avg*SQRT((Ts) / (Ps*Mw)) vs ft/s 45.78 47.32 47.05 46.717

12. Stack Gas Flow @ Stack Conditions = 60*vs*As Qa acfm 4,330 4,475 4,450 4,418

13. Stack Gas Flow @ Standard Conditions = Qa*(Tstd/Ts)*(Ps/Pstd) Qs scfm 3,960 4,004 4,012 3,992

14. Stack Gas Flow @ Dry Standard Conditions = Qa*(1-Bws)*(Tstd/Ts)*(Ps/Pstd) Qstd dscfm 3,859 3,894 3,905 3,886

15. Total Chromium concentration @ Std. Conditions =0.01543*mCr/Vm(std) csCr gr/dscf 4.38E-07 2.61E-07 1.91E-07 2.97E-07

15. Particulate concentration @ Std. Conditions, Filterable =0.01543*mn/Vm(std) cs gr/dscf 1.26E-03 2.74E-03 9.42E-04 1.65E-03

21. Total Chromium emissions = (60/7000)*csCrl*Qsd PMRCr lb/hr 0.00 0.00 0.00 0.00

21. Particulate emissions, Filterable = (60/7000)*cs*Qsd PMR lb/hr 0.04 0.09 0.03 0.05

22. Volume collected through nozzle =Ts/Ps*[0.002669*Vlc+ Vm*Y*Pm/Tm] Vn acf 177.587 175.976 179.100 177.554

23. Particulate concentration, @ actual conditions =0.01543*mn/Vn ca gr/acf 0.0011 0.0024 0.0008 0.0014

24. Isokinetic Sampling Rate, Percent = 100*Vn / (60*vs*An*) I % 102.04 97.84 100.13 100.00

Post Meter Orifice Cal. (EMC ALT-009 Yqa) yqa 0.9073 0.9426 0.9246 0.9248

% Difference, (Calibration must be within 5% of original Y-factor) 1.30%

Description Calculated Data

Run Number

Test Date

Emission Test Run Time Began - Ended

Data Input By: Stewart Meadows

Job No.:

ENTEC Services, Inc.

30 Monroe Dr. Pelham, AL 35124

CALCULATED TEST DATA

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 5 of 167
tems, LLC 

Project No. 511250

ICR Furnace Test December 20-21, 2011

Report Appendix Page 6 of 167
Client: Test Date: 12/20/2011

Source: Run Number: 1

Traverse Point Delta P Sq. Rt. Delta P Delta H Stack Temp. (°F) Meter Temp. (°F)

1-1 0.68 0.8246 1.66 128 84

1-1 0.71 0.8426 1.73 121 84

1-1 0.72 0.8485 1.76 119 84

1-2 0.72 0.8485 1.76 126 85

1-2 0.72 0.8485 1.76 126 86

1-2 0.71 0.8426 1.73 129 87

1-3 0.55 0.7416 1.34 128 88

1-3 0.55 0.7416 1.34 129 89

1-3 0.55 0.7416 1.34 126 90

1-4 0.44 0.6633 1.07 123 90

1-4 0.43 0.6557 1.05 121 91

1-4 0.43 0.6557 1.05 118 91

2-1 0.71 0.8426 1.73 121 91

2-1 0.73 0.8544 1.78 119 92

2-1 0.73 0.8544 1.78 119 92

2-2 0.74 0.8602 1.81 120 92

2-2 0.71 0.8426 1.73 124 93

2-2 0.71 0.8426 1.73 126 93

2-3 0.59 0.7681 1.44 129 93

2-3 0.59 0.7681 1.44 127 93

2-3 0.59 0.7681 1.44 126 93

2-4 0.40 0.6325 0.98 108 93

2-4 0.45 0.6708 1.10 114 92

2-4 0.47 0.6856 1.15 117 92

116 92

K-Factor

2.44 0.61 0.7769 1.49 122.4 90.0

ENTEC Services, Inc.

Owens Corning Lakeland Plant

PARTICULATE FIELD DATA, EPA METHOD 5/29

Furnace

30 Monroe Dr. Pelham, AL 35124

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 7 of 167
tems, LLC 

Project No. 511250

ICR Furnace Test December 20-21, 2011

Report Appendix Page 8 of 167
Client: Test Date: 12/21/2011

Source: Run Number: 2

Traverse Point Delta P Sq. Rt. Delta P Delta H Stack Temp. (°F) Meter Temp. (°F)

1-1 0.68 0.8246 1.65 140 85

1-1 0.69 0.8307 1.67 139 86

1-1 0.67 0.8185 1.62 132 87

1-2 0.66 0.8124 1.60 131 88

1-2 0.67 0.8185 1.62 130 89

1-2 0.67 0.8185 1.62 133 90

1-3 0.58 0.7616 1.40 131 91

1-3 0.58 0.7616 1.40 133 92

1-3 0.58 0.7616 1.40 135 93

1-4 0.54 0.7348 1.31 123 93

1-4 0.53 0.7280 1.28 122 94

1-4 0.53 0.7280 1.28 122 94

2-1 0.72 0.8485 1.74 122 95

2-1 0.72 0.8485 1.74 131 95

2-1 0.72 0.8485 1.74 130 96

2-2 0.69 0.8307 1.67 129 97

2-2 0.69 0.8307 1.67 131 97

2-2 0.67 0.8185 1.62 140 98

2-3 0.63 0.7937 1.52 129 99

2-3 0.63 0.7937 1.52 122 99

2-3 0.63 0.7937 1.52 120 99

2-4 0.58 0.7616 1.40 120 99

2-4 0.56 0.7483 1.36 124 99

2-4 0.56 0.7483 1.36 130 98

K-Factor

2.42 0.63 0.7943 1.53 129.1 93.9

ENTEC Services, Inc.

Owens Corning Lakeland Plant

PARTICULATE FIELD DATA, EPA METHOD 5/29

30 Monroe Dr. Pelham, AL 35124

Furnace

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 9 of 167
tems, LLC 

Project No. 511250

ICR Furnace Test December 20-21, 2011

Report Appendix Page 10 of 167
Client: Test Date: 12/22/2011

Source: Run Number: 3

Traverse Point Delta P Sq. Rt. Delta P Delta H Stack Temp. (°F) Meter Temp. (°F)

1-1 0.71 0.8426 1.75 117 88

1-1 0.71 0.8426 1.75 114 89

1-1 0.72 0.8485 1.77 115 90

1-2 0.69 0.8307 1.70 124 90

1-2 0.69 0.8307 1.70 129 91

1-2 0.70 0.8367 1.72 134 92

1-3 0.60 0.7746 1.48 124 92

1-3 0.62 0.7874 1.53 121 93

1-3 0.62 0.7874 1.53 123 93

1-4 0.51 0.7141 1.25 130 94

1-4 0.52 0.7211 1.28 125 94

1-4 0.50 0.7071 1.23 124 95

2-1 0.69 0.8307 1.70 127 95

2-1 0.68 0.8246 1.67 126 95

2-1 0.70 0.8367 1.72 124 95

2-2 0.69 0.8307 1.70 121 96

2-2 0.66 0.8124 1.62 123 97

2-2 0.67 0.8185 1.65 123 97

2-3 0.61 0.7810 1.50 128 97

2-3 0.60 0.7746 1.48 126 97

2-3 0.61 0.7810 1.50 125 97

2-4 0.56 0.7483 1.38 128 97

2-4 0.55 0.7416 1.35 127 97

2-4 0.54 0.7348 1.33 133 97

K-Factor

2.46 0.63 0.7933 1.55 124.6 94.1

ENTEC Services, Inc.

Owens Corning Lakeland Plant

PARTICULATE FIELD DATA, EPA METHOD 5/29

30 Monroe Dr. Pelham, AL 35124

Furnace

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 11 of 167
Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 12 of 167
Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250

Report Appendix Page 13 of 167
Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250

Report Appendix Page 14 of 167
Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250

Report Appendix Page 15 of 167
Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250

Report Appendix Page 16 of 167
Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250

Report Appendix Page 17 of 167
Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250

Report Appendix Page 18 of 167
APPENDIX A.2 

RAW TEST DATA AND EMISSIONS CALCULATIONS 

MELT FURNACE (EU 002) 

US EPA METHODS 0061 

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 19 of 167
EPA Method 1

EPA Method 2

EPA Method 3

EPA Method 4

SW846 Method 0061

12/20/11 12/21/11 12/22/11

PROBE WASH CHEMICAL:

Volumetric Flow

PROJECT MANAGER Flavel Smith

TEST PERFORMED: Hex/Total Chrome per method 0061

ADDITIONAL TEST REQUIREMENTS: Minimum Run Time (240 minutes) 

SOURCE PERMIT NUMBER: FDEP 1050375-006-AO

ENVIRONMENTAL ANALYST - ASSISTANT Stewart Meadows

ENTEC PROJECT NUMBER:

DATES TESTS CONDUCTED:

511250

RULING AGENCY :

Rick Cooper

REFERENCE METHOD TESTS:

Moisture Content

Molecular Weight

Florida Department of Environmental Protection (FDEP)

OWNER'S REPRESENTATIVE:

ENVIRONMENTAL ANALYST - ASSISTANT Kyle Vaughan

PLANT LOCATION:

SOURCE(S) CONDITION:

Owens Corning Lakeland Plant

Section 114 Testing

Lakeland, FL

SOURCE(S) NAME(S): Furnace

Circular

Entec Services, Inc.

SOURCE OWNER:

SOURCE OVERVIEW

Sample Location

0.1N NaOH

Hex/Total Chrome

SOURCE(S) SHAPE:

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 20 of 167
Client: 

Source:

Symbol Units

- - 1 2 3AVERAGE

- - 12/20/11 12/21/11 12/22/11

- Military Time 0810-1215 0751-1223 0747-1153

 minutes 240 240 240 240

As Ft2 1.576 1.576 1.576

Pbar in. Hg 30.22 29.91 29.91 30.01

Pg in. H20 -0.37 -0.37 -0.37 -0.37

Pitot Tube Correction factor Cp - 0.84 0.84 0.84 0.84

Meter Correction Factor Y - 0.937 0.937 0.937 0.937

H@ in. H20 2.002 2.002 2.002 2.002

Dn inches 0.220 0.220 0.220 0.220

Vm dcf 170.066 165.361 166.378 167.268

tm

o

F 76.8 78.1 80.9 78.6

ENTEC Services, Inc.

INPUT TEST DATA

Field Data Test Data

Data Input By:

511250

Ben Rogers

Job No.:

Emission Test Run Time Began - Ended

Sampling Time

Owens Corning Lakeland Plant

Furnace

Stack Area

Run Number

Test Date

Meter Volume

Meter Temperature

Barometric Pressure

Stack Static Pressure

Meter Delta H @

Nozzle Diameter

30 Monroe Dr. Pelham, AL 35124

H in. H20 1.47 1.41 1.48 1.45

Wimp grams 55.0 147.0 137.0 113.0

Wsg grams 105.4 38.5 127.0 90.3

O2 % 20.23 20.12 20.37 20.24

CO2 % 0.52 0.92 0.82 0.75

Chromium (VI) mass detected CrVI ugCrVI 2.49 0.33 0.14 0.99

Total Chromium in 0.1 M HNO3 CrHNO3 ugCrHNO3 0.81 9.79 0.36 3.65

Total Chromium in 0.5 M KOH CrKOH ugCrKOH 24.00 1.72 0.685 8.80

Crtotal ugCrtotal 27.304 11.838 1.186 13.4

= non-detect

=DLL (detection level limited)

Avg. Orifice Delta H

Impingers Weight Gain (Moisture)

Silica Gel Impinger Weight Gain (Moisture)

Oxygen Concentration, dry basis

Carbon Dioxide Concentration, dry basis

Total Chromium mass detected

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 21 of 167
Client: Owens Corning Lakeland Plant 511250

Source: Furnace

Formulas Symbol Units

- - 1 2 3AVERAGE

- - 12/20/11 12/21/11 12/22/11

- Military Time 0810-1215 0751-1223 0747-1153

1. Stack Pressure = Pbar + Pg / 13.6 Ps in. Hg 30.19 29.88 29.88 29.99

2. Meter Pressure = Pbar + H / 13.6 Pm in. Hg 30.33 30.01 30.02 30.12

3. Standard Meter Volume = 17.64* Y* (Vm/Tm)* (Pbar + H / 13.6) Vm(std) dscf 158.815 152.456 152.613 154.628

4a. Standard Volume of Water Vapor Condensed =0.04706*Wimp Vwc(std) scf 2.588 6.918 6.447 5.318

4b. Standard Volume of Water Collected in Silica Gel =0.04715*Wsg Vwsg(std) scf 4.970 1.815 5.988 4.258

5. Moisture Fraction =(Vwc(std) + Vwsg(std))/(Vwc(std) + Vwsg(std) + Vm(std)) Bws fraction 0.0454 0.0542 0.0753 0.0583

6. Moisture Fraction @ Saturation (Theoretical) =10[6.37-(2827/(ts+460-95.2)]/Ps TBws fraction 0.0896 0.1385 0.1366 0.1216

7. Standard Water Volume @ Saturation (Theoretical) =Vm(std) * (TBws)/(1-TBws) TVW(std) scf 15.625 24.509 24.153 21.429

8. Volume of Water @ Saturation (Theoretical) =TVw(std)/0.04707 TVlc ml 331.9 520.7 513.1 455.3

9. Molecular Weight Of Stack Gas, dry basis = 0.32*(O2)+ 0.44*(CO2)+0.28*(100-(O2)-(CO2)) Md g/g-mole 28.892 28.952 28.946 28.930

10. Molecular Weight Of Stack Gas, wet basis = Md*(1-Bws)+18.0*(Bws) Ms g/g-mole 28.398 28.359 28.121 28.293

11. Average Stack Gas Velocity = 85.49*Cp*(sqrt P)avg*SQRT((Ts) / (Ps*Mw)) vs ft/s 45.58 46.04 46.85 46.156

12. Stack Gas Flow @ Stack Conditions = 60*vs*As Qa acfm 4,311 4,354 4,431 4,365

13. Stack Gas Flow @ Standard Conditions = Qa*(Tstd/Ts)*(Ps/Pstd) Qs scfm 4,019 3,913 3,985 3,972

14. Stack Gas Flow @ Dry Standard Conditions = Qa*(1-Bws)*(Tstd/Ts)*(Ps/Pstd) Qstd dscfm 3,836 3,701 3,685 3,741

15 Chromium (VI) concentration @ Std Conditions =0 00001543*ugC VI/V ( td) c C VI gr/dscf 2 42E-07 3 31E-08 1 46E-08 9 65E-08

Description Calculated Data

Run Number

Test Date

Emission Test Run Time Began - Ended

Data Input By: Ben Rogers

Job No.:

ENTEC Services, Inc.

30 Monroe Dr. Pelham, AL 35124

CALCULATED TEST DATA

15. Chromium (VI) concentration @ Std. Conditions =0.00001543 ugCrVI/Vm(std) csCrVI gr/dscf 2.42E 07 3.31E 08 1.46E 08 9.65E 08

15. Total Chromium concentration @ Std. Conditions =0.00001543*ugCr/Vm(std) cCr gr/dscf 2.65E-06 1.20E-06 1.20E-07 1.32E-06

21. Chromium (VI) emissions = (60/7000)*csCR(VI)*Qsd PMRCR(VI) lb/hr 7.95E-06 1.05E-06 4.60E-07 3.16E-06

21. Total Chromium emissions = (60/7000)*csCr*Qsd PMRBH lb/hr 8.72E-05 3.80E-05 3.79E-06 4.30E-05

22. Volume collected through nozzle =Ts/Ps*[0.002669*Vlc+ Vm*Y*Pm/Tm] Vn acf 178.453 179.369 183.500 180.441

23. Chromium (VI) concentration, @ actual conditions =0.00001543*mn/Vn ca gr/acf 2.15E-07 1.02E-06 9.97E-08 4.44E-07

24. Isokinetic Sampling Rate, Percent = 100*Vn / (60*vs*An*) I % 102.99 102.49 103.04 102.84

Post Meter Orifice Cal. (EMC ALT-009 Yqa) yqa 0.9094 0.9232 0.9397 0.9241

1.38%

=DLL (detection level limited)

% Difference, (Calibration must be within 5% of original Y-factor)

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 22 of 167
tems, LLC 

Project No. 511250

ICR Furnace Test December 20-21, 2011

Report Appendix Page 23 of 167
Client: Test Date: 12/20/2011

Source: Run Number: 1

Traverse Point Delta P Sq. Rt. Delta P Delta H Stack Temp. (°F) Meter Temp. (°F)

1-1 0.67 0.8185 1.61 106 61

1-1 0.70 0.8367 1.69 105 62

1-1 0.70 0.8367 1.69 105 64

1-2 0.72 0.8485 1.74 107 67

1-2 0.70 0.8367 1.69 108 69

1-2 0.70 0.8367 1.69 111 71

1-3 0.60 0.7746 1.45 111 72

1-3 0.58 0.7616 1.40 110 74

1-3 0.56 0.7483 1.35 113 75

1-4 0.45 0.6708 1.08 112 76

1-4 0.45 0.6708 1.08 110 78

1-4 0.44 0.6633 1.06 110 78

2-1 0.67 0.8185 1.61 111 79

2-1 0.67 0.8185 1.61 113 80

2-1 0.67 0.8185 1.61 116 81

2-2 0.70 0.8367 1.69 115 82

2-2 0.71 0.8426 1.71 113 83

2-2 0.70 0.8367 1.69 117 83

2-3 0.60 0.7746 1.45 114 84

2-3 0.60 0.7746 1.45 112 84

2-3 0.60 0.7746 1.45 114 84

2-4 0.46 0.6782 1.11 112 85

2-4 0.50 0.7071 1.21 113 85

2-4 0.46 0.6782 1.11 113 86

K-Factor

2.41 0.61 0.7776 1.47 111.3 76.8

ENTEC Services, Inc.

Owens Corning Lakeland Plant

PARTICULATE FIELD DATA, EPA METHOD 0061

Furnace

30 Monroe Dr. Pelham, AL 35124

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 24 of 167
tems, LLC 

Project No. 511250

ICR Furnace Test December 20-21, 2011

Report Appendix Page 25 of 167
Client: Test Date: 12/21/2011

Source: Run Number: 2

Traverse Point Delta P Sq. Rt. Delta P Delta H Stack Temp. (°F) Meter Temp. (°F)

1-1 0.65 0.8062 1.54 124 63

1-1 0.67 0.8185 1.59 118 64

1-1 0.67 0.8185 1.59 118 65

1-2 0.64 0.8000 1.52 129 67

1-2 0.65 0.8062 1.54 124 69

1-2 0.63 0.7937 1.49 129 71

1-3 0.53 0.7280 1.26 131 73

1-3 0.53 0.7280 1.26 129 75

1-3 0.55 0.7416 1.30 122 76

1-4 0.45 0.6708 1.07 118 78

1-4 0.45 0.6708 1.07 118 79

1-4 0.45 0.6708 1.07 118 80

2-1 0.66 0.8124 1.56 117 81

2-1 0.68 0.8246 1.61 121 82

2-1 0.68 0.8246 1.61 123 83

2-2 0.67 0.8185 1.59 122 84

2-2 0.69 0.8307 1.64 122 84

2-2 0.68 0.8246 1.61 124 85

2-3 0.64 0.8000 1.52 120 86

2-3 0.63 0.7937 1.49 130 86

2-3 0.50 0.7071 1.19 174 86

2-4 0.52 0.7211 1.23 143 85

2-4 0.54 0.7348 1.28 133 86

2-4 0.56 0.7483 1.33 131 86

K-Factor

2.37 0.60 0.7706 1.41 126.6 78.1

ENTEC Services, Inc.

Owens Corning Lakeland Plant

PARTICULATE FIELD DATA, EPA METHOD 0061

30 Monroe Dr. Pelham, AL 35124

Furnace

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 26 of 167
tems, LLC 

Project No. 511250

ICR Furnace Test December 20-21, 2011

Report Appendix Page 27 of 167
Client: Test Date: 12/21/2011

Source: Run Number: 3

Traverse Point Delta P Sq. Rt. Delta P Delta H Stack Temp. (°F) Meter Temp. (°F)

1-1 0.68 0.8246 1.64 125 66

1-1 0.70 0.8367 1.69 117 66

1-1 0.69 0.8307 1.66 115 68

1-2 0.69 0.8307 1.66 114 69

1-2 0.66 0.8124 1.59 125 71

1-2 0.66 0.8124 1.59 133 73

1-3 0.57 0.7550 1.37 131 75

1-3 0.55 0.7416 1.33 136 77

1-3 0.57 0.7550 1.37 137 78

1-4 0.51 0.7141 1.23 138 80

1-4 0.51 0.7141 1.23 124 82

1-4 0.51 0.7141 1.23 120 83

2-1 0.67 0.8185 1.61 124 84

2-1 0.65 0.8062 1.57 125 85

2-1 0.67 0.8185 1.61 127 86

2-2 0.65 0.8062 1.57 127 87

2-2 0.65 0.8062 1.57 135 88

2-2 0.65 0.8062 1.57 129 88

2-3 0.62 0.7874 1.49 128 88

2-3 0.63 0.7937 1.52 125 89

2-3 0.63 0.7937 1.52 123 89

2-4 0.53 0.7280 1.28 122 90

2-4 0.52 0.7211 1.25 120 90

2-4 0.52 0.7211 1.25 126 90

K-Factor

2.41 0.61 0.7812 1.48 126.1 80.9

ENTEC Services, Inc.

Owens Corning Lakeland Plant

PARTICULATE FIELD DATA, EPA METHOD 006

30 Monroe Dr. Pelham, AL 35124

Furnace

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APPENDIX B 

QA/QC DOCUMENTS AND CHECKLISTS 

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Deg. Rankin 537.0

1.249

Date:

0.753

Equation: 10/(Volume)*SQRT((0.0319*(Tm/Pbar))

10/Volume= SQRT((0.0319*(Tm/Pbar))=

Y = 0.940

Meter Calibration % Difference -0.35%

Meter Volume: 8.007 Average Temperature: 77.0

Final Volume: 205.007 Final Meter Temperature: 78.0

Initial Volume: 197.000 Initial Meter Temperature: 76.0

Calibration Date: 12/20/2010 Original Y Factor: 0.937

Meter Box: C#2887 Original Delta H @: 2.002

Source: Furnace Job Number: 511250

Client: Owens Corning Lakeland Plant Location: Lakeland, FL

ENTEC Services, Inc.

Initial Meter Box 10 Minute Calibration

30 Monroe Dr. Pelham, AL 35124

Signature: W. Stewart Meadows 12/19/2011

Barometric Pressure: 30.22

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Client: Job No. :

Source: Input By:

P Port Type Nipple Port Diameter

17

80

Inches

Duct 

Diameters

154.0 9.06

240.0 14.12 4 4

Point No.

1 1.1 7.1

2 4.3 10.3

3 12.8 18.8

4 15.9 21.9

 

* Adjusted points diameter > 24" no point closer than 1.0 inch

* Adjusted points diameter < 24" no point closer than 0.5 inch

Stack Diameters between 12-24 inches minimum points are 8 ; 

4 points per port if the 8 / 2 diameters downstream and

upstream criteria is met.

Furnace

Distance "A"

Distance "B"

2

6.00

Total Number of Traverse Points:

Number of Points per port / traverse:

Number of Ports:

Length of Port, inches:

Inches

Inside Stack Outside Nipple

Inches

8

Figure 4-1

Entec Services, Inc

30 Monroe Dr. Pelham, AL 35124

Stack Area, Ft2 Stack Diameter, inches: :

Stack Properties:

Type of Traverse: Velocity (V) or Particulate (P):

STACK DRAWING & TRAVERSE POINT LOCATION

511250

Stewart 

Meadows

4

1.576

Owens Corning Lakeland Plant

Stack Height, feet:

Upstream From Flow Disturbance (A):

Downstream From Flow Disturbance (B):

INCHES

17.0 INCHES

INCHES

240.0

154.0

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December 20-21, 2011

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Client:

Source:

Traverse Point Delta P Sq. Rt. Delta P Stack 

1-1 0.65 0.8062 1-2 0.65 0.8062 1-3 0.61 0.7810 1-4 0.47 0.6856 2-1 0.69 0.8307 2-2 0.75 0.8660 2-3 0.57 0.7550 2-4 0.46 0.6782 

Average 0.61 0.7761 

Note: Based on the preliminary traverse the flow is not considered cyclonic 

8.63

15

ENTEC Services, Inc.

Test Date:

Run No.:

12/20/11Preliminary Test

Preliminary Traverse & Cyclonic Flow Verification

Furnace

30 Monroe Dr. Pelham, AL 35124

Null Reading (Angle)

15

5356

10

Owens Corning Lakeland Plant

10

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Lakeland, FL

Project No. 511250

Report Appendix Page 47 of 167
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APPENDIX C 

LABORATORY DATA 

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APPENDIX C.1 

ENTHALPY REPORT #1211-69 

METHOD 5 MULTIPLE METALS AND PM 

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APPENDIX C.2 

ELEMENT ONE REPORT #18035 

METHOD 29 CHROMIUM 

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December 20-21, 2011

Report Appendix Page 66 of 167
Enthalpy 

800 Capitola Dr., Ste. 1 

Durham, NC 27713 

Project Number: 511250 

Chromium 

 

EPA Method 29 Analysis 

 

Analytical Report 

18035

Element One, Inc. 

5022-C Wrightsville Av., Wilmington, NC 28403 el1 910-793-0128 FAX: 910-792-6853 e1lab@e1lab.com

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elementOne 

18035 Enthalpy M29 Report Packet 

Page 3 of 22

SUMMARY OF RESULTS 

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18035 Enthalpy M29 Report Packet 

Page 4 of 22 

Summary of Analysis 

Front Half - Summary of Method 29 Metals Analysis 

Run 1 Run 2 Run 2 Run 3 Blank 

e18035-1FH e18035-2FH e18035-2FH dup e18035-3FH e18035-4FH 

Element Total μg Total μg Total μg Total μg Total μg ----------------- --------------- --------------- --------------- --------------- --------------- 

Chromium 2.86 1.71 1.70 1.44 1.74 

Back Half - Summary of Method 29 Metals Analysis 

Run 1 Run 2 Run 2 Run 3 Blank 

e18035-1BH e18035-2BH e18035-2BH dup e18035-3BH e18035-4BH 

Element Total μg Total μg Total μg Total μg Total μg ----------------- --------------- --------------- --------------- --------------- --------------- 

Chromium 1.63 0.881 0.859 0.507 0.861 

 

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18035 Enthalpy M29 Report Packet 

Page 5 of 22 

ANALYTICAL NARRATIVE 

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18035 Enthalpy M29 Report Packet 

Page 6 of 22 

Element One Analytical Narrative 

Client: Enthalpy Element One #: 18035 

Client ID: 511250/OC – Lakeland Analyst: DBW 

Method: Method 29 Dates Received: 01/17/12 

Analytes: Cr Dates Analyzed: 01/19/12 

Summary of Analysis 

The Method 29 samples were digested, prepared, and analyzed according to 

Method 29 protocol. Samples were analyzed for total chromium on a 

PerkinElmer ELAN 6100 ICP-MS. 

Detection Limits 

The ICP-MS instrument reporting limit was 1.0μg/L for total chromium. 

Analysis QA/QC 

Duplicate analyses relative percent difference (RPD), spike sample recovery, and 

second source calibration verification data are summarized in the Quality Control 

Section. All QA/QC data was within the criteria of the method. 

Additional Comments 

The reported results have not been corrected for any blank values or spike 

recovery values. The ICP analysis of the Blank samples revealed detectable 

concentrations of chromium.

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18035 Enthalpy M29 Report Packet 

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QUALITY CONTROL SUMMARY

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18035 Enthalpy M29 Report Packet 

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Summary of Quality Control Data 

Metals Duplicate Analysis RPD 

(Method 29 QC limits: < 20% for RPD)

Run 2 

Front Half 

Run 2 

Back Half 

Element RPD RPD ------------------ ----------------- ----------------- 

Chromium 0.6% 2.5% 

Metals Analysis Spike Recoveries 

(Method 29 QC limits: ±25% for Spike Recoveries)

Run 3 

Front Half 

Run 3 

Back Half 

Element Recovery Recovery ------------------ ----------------- ----------------- 

Chromium 124% 105% 

*See Analytical Narrative, page 12. 

Second Source Calibration Check Recoveries 

(Method 29 QC limits: ±10% for Second Source Continuing Check Standard*) 

Element 1 ppb 50 ppb 100 ppb* 250 ppb ----------------- ----------------- ----------------- ----------------- ----------------- 

Chromium 116% 103% 101% 99% 

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18035 Enthalpy M29 Report Packet 

Page 9 of 22 

SAMPLE CUSTODY

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18035 Enthal 18035 Enthalpy M29 Report Packet 

Page 10 of 22 

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18035 Enthalpy M29 Report Packet 

Page 11 of 22 

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18035 Enthalpy M29 Report Packet 

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ANALYTICAL DATA 

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18035 Enthalpy M29 Report Packet 

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Analytical Calculations 

MetalsElement Results (μg) =ICP Results (μg/L)*Dilution*Final Volume (L) 

WhereICP Results= Raw sample concentration (ppb)--ICP-Data Sheet

Dilution= Diluted Volume--ICP-MS Run Sheet

Aliquot 

Final Volume=FH=Final Volume (FV)--Sample Submission

 BH=Received Volume (BV).*Final Volume (FV)--Sample Submission

Aliquot (Used) 

 Combined Results=FH+BH 

MercuryMercury Results (μg) =CVAA Results (μg) *Final Volume (ml) 

 Aliquot (ml) 

WhereCVAA Results= Raw sample reading (μg)--Hg-Data Sheet

Aliquot= Sample Aliquot (Alq.)--Hg-Data Sheet

 

Final Volume=Final Volume (FV)*--Sample Submission

* With the exception of the BH fraction where- 

=Received Volume (BV)--Sample Submission

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Analytical Calculations

Spike RecoverySpike (%) = (Spiked Result (μg/L) – Sample Result (μg/L)) X100 

 Spike Amount (μg/L)

WhereSpike Result = Raw sample concentration (ppb)--ICP-Data Sheet 

Sample Result = Raw sample concentration (ppb)--ICP-Data Sheet

Spike Amount--ICP-MS Spike Table

Duplicate Analysis RPDRPD (%) = (Duplicate Result (μg/L) - Sample Result (μg/L)) X100 

 Average (μg/L)

WhereSample Result and Duplicate Results=Raw sample concentration (ppb)--ICP-Data 

Sheet

Average=(Duplicate + Sample Results)

 2

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18035 Enthalpy M29 Report Packet 

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18035 Enthalpy M29 Report Packet 

Page 16 of 22 

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18035 Enthalpy M29 Report Packet 

Page 17 of 22 

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18035 Enthalpy M29 Report Packet 

Page 18 of 22 

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18035 Enthalpy M29 Report Packet 

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18035 Enthalpy M29 Report Packet 

Page 20 of 22 

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18035 Enthal 18035 Enthalpy M29 Report Packet 

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s n

s n

s n

103 1170324 6

s n

s n

Method 6020 & 200.8 Metals Summary Report

Sample ID: Blank

Sample DatThursday, January 19, 2012 09:32:02

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 140709.3 ppb

|- Sc 45 506153.1 ppb

| Cr 52 26563.1 ppb

| Cr 53 38935.2 ppb

|> Rh 103 1108623.8 ppb

 Ho 165 1830420.4 ppb

 Kr 83 222.3 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: Standard 1

Sample DatThursday, January 19, 2012 09:33:13

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 148541.8 ppb

|- Sc 45 537253.7 ppb

| Cr 52 48967.9 1.0759 ppb

| Cr 53 44384.1 1.2297 ppb

|> Rh 103 1182176.2 ppb

 Ho 165 1938280 ppb

 Kr 83 -178.4 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: Standard 2

Sample DatThursday, January 19, 2012 09:34:23

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 147510.2 ppb

|- Sc 45 534745.8 ppb

| Cr 52 1945179.1 100.9631 ppb

| Cr 53 274407 100.6365 ppb

|> Rh 103 1170324.6 ppb

 Ho 165 1934981 ppb

 Kr 83 -33837.3 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: Standard 3

Sample DatThursday, January 19, 2012 09:35:34

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 132134.2 ppb

|- Sc 45 517907.1 ppb

| Cr 52 9013217.2 499.8072 ppb

| Cr 53 1136070.9 499.8722 ppb

|> Rh 103 1108129.6 ppb

 Ho 165 1861296.4 ppb

 Kr 83 -165009.6 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: QC Std 1

Sample DatThursday, January 19, 2012 09:36:44

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 132269.6 ppb

|- Sc 45 502821.9 ppb

| Cr 52 30031.4 0.17486 ppb

| Cr 53 41795.6 1.1064 ppb

|> Rh 103 1120004.5 ppb

 Ho 165 1807601.2 ppb

 Kr 83 210.1 mg/L

Owens Corning Insulating Systems, LLC 

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December 20-21, 2011

Report Appendix Page 88 of 167
s n

s n

s n

103

s n

s n

Method 6020 & 200.8 Metals Summary Report

Sample ID: QC Std 2

Sample DatThursday, January 19, 2012 09:37:55

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 146878.3 ppb

|- Sc 45 548221.3 ppb

| Cr 52 50545.2 1.16122 ppb

| Cr 53 46307.4 2.0712 ppb

|> Rh 103 1180618.4 ppb

 Ho 165 1933719 ppb

 Kr 83 -155.5 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: QC Std 3

Sample DatThursday, January 19, 2012 09:39:06

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 128581.5 ppb

|- Sc 45 499699.7 ppb

| Cr 52 4348975.3 246.6691 ppb

| Cr 53 557112.2 242.7049 ppb

|> Rh 103 1079896.2 ppb

 Ho 165 1808368.1 ppb

 Kr 83 -76656.6 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: QC Std 4

Sample DatThursday, January 19, 2012 09:40:17

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 143836.2 ppb

|- Sc 45 538950.9 ppb

| Cr 52 1969264 100.5613 ppb

| Cr 53 281939.5 101.9599 ppb

|> Rh 103 1189223 ppb

 Ho 165 1945932.2 ppb

 Kr 83 -34795.1 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: QC Std 5

Sample DatThursday, January 19, 2012 09:41:29

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 137093.9 ppb

|- Sc 45 525156 ppb

| Cr 52 970513.5 51.56261 ppb

| Cr 53 156445.3 52.31851 ppb

|> Rh 103 1127492.7 ppb

 Ho 165 1853456.9 ppb

 Kr 83 212.1 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: QC Std 7

Sample DatThursday, January 19, 2012 09:42:40

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 156822.2 ppb

|- Sc 45 622547.3 ppb

| Cr 52 265569.2 11.88387 ppb

| Cr 53 67623.1 10.1391 ppb

|> Rh 103 1224854.3 ppb

 Ho 165 2028980.8 ppb

 Kr 83 98.2 mg/L

Owens Corning Insulating Systems, LLC 

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Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 89 of 167
s n

s n

s n

103 1216509 2

s n

s n

Method 6020 & 200.8 Metals Summary Report

Sample ID: QC Std 2

Sample DatThursday, January 19, 2012 09:43:51

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 144225.6 ppb

|- Sc 45 543443.6 ppb

| Cr 52 53978.2 1.26158 ppb

| Cr 53 54771.5 5.03318 ppb

|> Rh 103 1214735.6 ppb

 Ho 165 1954746.3 ppb

 Kr 83 -181.2 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: LRB FH

Sample DatThursday, January 19, 2012 09:45:03

Sample De Enthalpy

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 153946.1 ppb

|- Sc 45 596280.4 ppb

| Cr 52 95224.3 3.2471 ppb

| Cr 53 26107.6 -7.12532 ppb

|> Rh 103 1242210.2 ppb

 Ho 165 2009366.7 ppb

 Kr 83 146.2 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: LRB FH

Sample DatThursday, January 19, 2012 09:46:13

Sample De Enthalpy

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 164127.2 ppb

|- Sc 45 625801.4 ppb

| Cr 52 1145417 56.5413 ppb

| Cr 53 147396.5 43.43688 ppb

|> Rh 103 1216509.2 ppb

 Ho 165 2044334.1 ppb

 Kr 83 141.9 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: 18035-1 FH

Sample DatThursday, January 19, 2012 09:47:23

Sample De Enthalpy

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 164903.9 ppb

|- Sc 45 753148.9 ppb

| Cr 52 531266.3 28.6431 ppb

| Cr 53 73255.3 16.29204 ppb

|> Rh 103 1086762.7 ppb

 Ho 165 1969906.8 ppb

 Kr 83 -4911.9 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: 18035-2 FH

Sample DatThursday, January 19, 2012 09:48:34

Sample De Enthalpy

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 160947.2 ppb

|- Sc 45 826288.6 ppb

| Cr 52 294321.7 17.12587 ppb

| Cr 53 45028.3 5.58341 ppb

|> Rh 103 974935 ppb

 Ho 165 1898400.9 ppb

 Kr 83 -6749.5 mg/L

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 90 of 167
s n

s n

s n

103 1092614 2

s n

s n

Method 6020 & 200.8 Metals Summary Report

Sample ID: 18035-2 FH

Sample DatThursday, January 19, 2012 09:49:44

Sample De Enthalpy

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 172578.8 ppb

|- Sc 45 869150.6 ppb

| Cr 52 311135.7 17.02263 ppb

| Cr 53 46356.2 4.85373 ppb

|> Rh 103 1036341.8 ppb

 Ho 165 1948980.2 ppb

 Kr 83 -7154.6 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: 18035-3 FH

Sample DatThursday, January 19, 2012 09:50:54

Sample De Enthalpy

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 170383.4 ppb

|- Sc 45 940116.1 ppb

| Cr 52 268198.3 14.43129 ppb

| Cr 53 43154.2 3.24105 ppb

|> Rh 103 1038852.5 ppb

 Ho 165 1938710.6 ppb

 Kr 83 -4352.1 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: 18035-3 FH

Sample DatThursday, January 19, 2012 09:52:05

Sample De Enthalpy

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 172903 ppb

|- Sc 45 960055.8 ppb

| Cr 52 1377502.5 76.216 ppb

| Cr 53 173696.7 62.53274 ppb

|> Rh 103 1092614.2 ppb

 Ho 165 1993662.6 ppb

 Kr 83 -4473.2 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: 18035-4 FH

Sample DatThursday, January 19, 2012 09:53:15

Sample De Enthalpy

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 183870.2 ppb

|- Sc 45 974372.3 ppb

| Cr 52 354491.5 17.39613 ppb

| Cr 53 55442.2 6.45239 ppb

|> Rh 103 1157432.3 ppb

 Ho 165 2134297.9 ppb

 Kr 83 -1390.3 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: LRB BH

Sample DatThursday, January 19, 2012 09:54:26

Sample De Enthalpy

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 176769.9 ppb

|- Sc 45 640798.3 ppb

| Cr 52 52124.4 1.15457 ppb

| Cr 53 17493.3 -10.50206 ppb

|> Rh 103 1220714.1 ppb

 Ho 165 2112425.1 ppb

 Kr 83 120.5 mg/L

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December 20-21, 2011

Report Appendix Page 91 of 167
s n

s n

s n

103 1250624 5

s n

s n

Method 6020 & 200.8 Metals Summary Report

Sample ID: LRB BH

Sample DatThursday, January 19, 2012 09:55:36

Sample De Enthalpy

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 177042.1 ppb

|- Sc 45 658284 ppb

| Cr 52 1203308.6 57.06276 ppb

| Cr 53 150575.2 42.28071 ppb

|> Rh 103 1266697.5 ppb

 Ho 165 2167348.8 ppb

 Kr 83 158.1 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: QC Std 1

Sample DatThursday, January 19, 2012 09:56:49

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 134017.1 ppb

|- Sc 45 511075.9 ppb

| Cr 52 22953.3 -0.2861 ppb

| Cr 53 39733.6 -0.84531 ppb

|> Rh 103 1188105.2 ppb

 Ho 165 1965279.6 ppb

 Kr 83 273.9 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: QC Std 4

Sample DatThursday, January 19, 2012 09:58:00

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 141292.3 ppb

|- Sc 45 545424.2 ppb

| Cr 52 2066259.6 100.3314 ppb

| Cr 53 294910 101.3139 ppb

|> Rh 103 1250624.5 ppb

 Ho 165 1987134.6 ppb

 Kr 83 -37142 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: 18035-1 BH

Sample DatThursday, January 19, 2012 09:59:13

Sample De Enthalpy

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 126394.8 ppb

|- Sc 45 317581.6 ppb

| Cr 52 349040.6 16.31131 ppb

| Cr 53 56519.9 5.85769 ppb

|> Rh 103 1209144.2 ppb

 Ho 165 1968891.9 ppb

 Kr 83 -1161.3 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: 18035-2 BH

Sample DatThursday, January 19, 2012 10:00:23

Sample De Enthalpy

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 129125.9 ppb

|- Sc 45 506503.5 ppb

| Cr 52 205141.6 8.80964 ppb

| Cr 53 36449.7 -2.76127 ppb

|> Rh 103 1228923.8 ppb

 Ho 165 1953583.2 ppb

 Kr 83 -1212.9 mg/L

Owens Corning Insulating Systems, LLC 

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Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 92 of 167
s n

s n

s n

103 1197041 2

s n

s n

Method 6020 & 200.8 Metals Summary Report

Sample ID: 18035-2 BH

Sample DatThursday, January 19, 2012 10:01:34

Sample De Enthalpy

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 129189.3 ppb

|- Sc 45 491072.2 ppb

| Cr 52 200371 8.59431 ppb

| Cr 53 35427.6 -3.1434 ppb

|> Rh 103 1225962.4 ppb

 Ho 165 1952599.3 ppb

 Kr 83 -1200.1 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: 18035-3 BH

Sample DatThursday, January 19, 2012 10:02:44

Sample De Enthalpy

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 124464.8 ppb

|- Sc 45 462006 ppb

| Cr 52 130401.5 5.07442 ppb

| Cr 53 27007.8 -6.61776 ppb

|> Rh 103 1226513.2 ppb

 Ho 165 1970931.6 ppb

 Kr 83 -811.7 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: 18035-3 BH

Sample DatThursday, January 19, 2012 10:03:55

Sample De Enthalpy

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 122797.6 ppb

|- Sc 45 454135.7 ppb

| Cr 52 1148108.3 57.6244 ppb

| Cr 53 146638.7 44.11051 ppb

|> Rh 103 1197041.2 ppb

 Ho 165 1951398.9 ppb

 Kr 83 -813.2 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: 18035-4 BH

Sample DatThursday, January 19, 2012 10:05:05

Sample De Enthalpy

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 122557.6 ppb

|- Sc 45 482921.1 ppb

| Cr 52 160590.3 8.61261 ppb

| Cr 53 29332.7 -2.6354 ppb

|> Rh 103 980860.9 ppb

 Ho 165 1696805.4 ppb

 Kr 83 -131.7 mg/L

Method 6020 & 200.8 Metals Summary Report

Sample ID: QC Std 1

Sample DatThursday, January 19, 2012 10:06:17

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 128537 ppb

|- Sc 45 496150.2 ppb

| Cr 52 24056.1 -0.22352 ppb

| Cr 53 46914.1 2.29111 ppb

|> Rh 103 1183246.5 ppb

 Ho 165 1945873 ppb

 Kr 83 241.9 mg/L

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 93 of 167
s n

Method 6020 & 200.8 Metals Summary Report

Sample ID: QC Std 4

Sample DatThursday, January 19, 2012 10:07:28

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten Conc. Mea Report Unit

 Li 6 133121.4 ppb

|- Sc 45 522147.8 ppb

| Cr 52 2011929.1 98.86711 ppb

| Cr 53 285273.1 98.8326 ppb

|> Rh 103 1235353 ppb

 Ho 165 1962113.3 ppb

 Kr 83 -36679 mg/L

Owens Corning Insulating Systems, LLC 

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December 20-21, 2011

Report Appendix Page 94 of 167
APPENDIX C.3 

ELEMENT ONE REPORT #17933 

METHOD 0061 TOTAL CHROMIUM AND HEXAVALENT CHROMIUM 

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Report Appendix Page 95 of 167
Enthalpy Analytical, Inc. 

800 Capitola Dr., Ste. 1 

Durham, NC 27713 

Project No: 511250

Total Chromium and Hexavalent Chromium 

EPA Method 0061 Analysis 

Analytical Report 

17933 

Element One, Inc. 

5022-C Wrightsville Av., Wilmington, NC 28403 el1 910-793-0128 FAX: 910-792-6853 e1lab@e1lab.com

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Report Appendix Page 96 of 167
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Report Appendix Page 97 of 167
elementOne 

17933 Enthalpy M0061 TCr and Cr6 Report Packet.doc 

Page 3 of 30

SUMMARY OF RESULTS 

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elementOne 

17933 Enthalpy M0061 TCr and Cr6 Report Packet.doc 

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Summary of Analysis 

Fibertek Furnace - Summary of Chromium (VI) Analysis 

Run 1 Run 2 Run 2 Run 3 

e17933-5 e17933-6 e17933-6 dup e17933-7

Element Total μg Total μg Total μg Total μg ----------------- --------------- --------------- --------------- --------------- 

Chromium(VI) 2.49 0.317 0.338 0.144 

Duplicate RPD, % 0.5% 0.0% 8.4% 9.5% 

Spike Recovery, % ------------ ------------ ------------ 99% 

0.5M KOH RB 

e17933-8

Element Total μg ----------------- --------------- 

Chromium(VI) < 0.128 

Duplicate RPD, % NA 

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elementOne 

17933 Enthalpy M0061 TCr and Cr6 Report Packet.doc 

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Summary of Analysis

0.1M HNO3 Rinse - Summary of Method 0061 Total Chromium Analysis 

Run 1 Run 2 Run 2 Run 3 Reagent Blank 

e1 Sample ID e17933-1 e17933-2 e17933-2 dup e17933-3 e17933-4 

Element Total μg Total μg Total μg Total μg Total μg ----------------- --------------- --------------- --------------- --------------- --------------- 

Total Chromium 0.814 9.67 9.91 0.357 < 0.24 

0.5M KOH - Summary of Method 0061 Total Chromium Analysis 

Run 1 Run 2 Run 2 Run 3 Reagent Blank 

e1 Sample ID e17933-5 e17933-6 e17933-6 dup e17933-7 e17933-8 

Element Total μg Total μg Total μg Total μg Total μg ----------------- --------------- --------------- --------------- --------------- --------------- 

Total Chromium 24.0 1.69 1.75 < 0.685 < 0.255 

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17933 Enthalpy M0061 TCr and Cr6 Report Packet.doc 

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ANALYTICAL NARRATIVE 

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Element One Analytical Narrative 

Client: Enthalpy Analytical, Inc. Element One #: 17933 

Client ID: 511250/O.C. Lakeland Analyst: DBW & LAL 

Method: M0061 Dates Received: 12/15/11 

Analytes: Total Chromium & Chromium (VI) Dates Analyzed: 12/16-20/11, 01/04-06/12 

Summary of Analysis

For Total Chromium analysis the Method 0061 samples were acidified with trace 

metals grade concentrated nitric acid and digested on a hotplate according to 

method protocol. Samples were analyzed for total chromium on a PerkinElmer 

ELAN 6100 ICP-MS. 

For Chromium VI analysis the samples were prepared and analyzed according to 

SW-846 Method 0061 protocol. Samples were analyzed for chromium (VI) using 

a Shimadzu 2010 HPLC unit and a Timberline RDR-1 Reaction Module. 

Detection Limits

The ICP-MS instrument reporting limit was 1.0μg/L for total chromium. 

The Shimadzu 2010 HPLC instrument reporting limit for chromium (VI) was 

0.1μg/L. 

Analysis QA/QC 

For Total Chromium analysis duplicate analysis relative percent difference 

(RPD), spike sample recovery and second source calibration verification data are 

summarized in the Quality Control Summary. 

For Chromium VI analysis, duplicate analyses relative percent difference (RPD) 

and spike sample recovery data are summarized with the results. 

All other QA/QC data was within the criteria of the method. 

Additional Comments 

The reported results have not been corrected for any blank values or spike 

recovery values. Due to matrix interferences it was necessary to analyze all 

samples at a minimum two-fold dilution. 

Per the client’s request the 0.5M KOH samples were analyzed for both chromium 

(VI) and total chromium. 

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elementOne 

17933 Enthalpy M0061 TCr and Cr6 Report Packet.doc 

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QUALITY CONTROL SUMMARY

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17933 Enthalpy M0061 TCr and Cr6 Report Packet.doc 

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Summary of Quality Control Data 

Metals Duplicate Analysis RPD 

(Method 0061 QC limits: < 10% for RPD)

0.1M HNO3 Run 2 0.5M KOH Run 2 

Element RPD RPD ------------------ ----------------- ----------------- 

Total Chromium 2.5% 3.3% 

 

Metals Analysis Spike Recoveries 

(Method 0061 QC limits: ± 25% for Spike Recoveries.)

0.1M HNO3 Run 3 0.5M KOH Run 3 

Element Recovery Recovery ------------------ ----------------- ----------------- 

Total Chromium 102% 90% 

Second Source Calibration Check Recoveries 

(Method 0061 QC limits: ±10% for Second Source Continuing Check Standard*) 

Element 1 ppb 50 ppb 100 ppb* 250 ppb ----------------- ----------------- ----------------- ----------------- ----------------- 

Total Chromium 95% 98% 100% 99% 

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elementOne 

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SAMPLE CUSTODY

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elementOne 

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Page 11 of 30 

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elementOne 

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ANALYTICAL DATA 

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Analytical Calculations 

MetalsElement Results (μg) =ICP Results (μg/L)*Dilution*Beginning Volume (L) 

WhereICP Results= Raw sample concentration (ppb)--ICP-Data Sheet

Dilution= Diluted Volume--ICP-MS Run Sheet

Aliquot 

Beginning Volume= (BV)--Sample Submission

Cr (VI)- 

Total Cr+6 (ug) =Cr+6 Results (μg/L)*Dilution*Final Volume (mL)/1000 

WhereCr+6 Results= Raw sample concentration (ppb)—HPLC Data Sheet

Dilution= Diluted Volume—HPLC Data Sheet

Aliquot 

Final Volume--Sample Submission 

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Analytical Calculations

Spike RecoverySpike (%) = (Spiked Result (μg/L) – Sample Result (μg/L)) X100 

 Spike Amount (μg/L)

WhereSpike Result = Raw sample concentration (ppb)--ICP-Data Sheet 

Sample Result = Raw sample concentration (ppb)--ICP-Data Sheet

Spike Amount--ICP-MS Spike Table

Duplicate Analysis RPDRPD (%) = (Duplicate Result (μg/L) - Sample Result (μg/L)) X100 

 Average (μg/L)

WhereSample Result and Duplicate Results=Raw sample concentration (ppb)--ICP-Data 

Sheet

Average=(Duplicate + Sample Results)

 2

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elementOne 

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Page 15 of 30 

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Report Appendix Page 110 of 167
elementOne 

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Page 16 of 30 

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elementOne 

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Page 17 of 30 

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Report Appendix Page 112 of 167
elementOne 

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Page 18 of 30 

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Report Appendix Page 113 of 167
elementOne 

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Page 19 of 30 

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elementOne 

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Page 20 of 30 

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Report Appendix Page 115 of 167
elementOne 

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Page 21 of 30 

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Report Appendix Page 116 of 167
elementOne 

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Page 22 of 30 

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Report Appendix Page 117 of 167
elementOne 

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Page 23 of 30 

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Report Appendix Page 118 of 167
elementOne 

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Page 24 of 30 

Owens Corning Insulating Systems, LLC 

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Report Appendix Page 119 of 167
elementOne 

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Page 25 of 30 

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Report Appendix Page 120 of 167
elementOne 

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Page 26 of 30 

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elementOne 

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Page 27 of 30 

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elementOne 

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Page 28 of 30 

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elementOne 

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Page 29 of 30 

Owens Corning Insulating Systems, LLC 

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Report Appendix Page 124 of 167
PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report

Sample ID: Blank

Sample DatFriday, December 30, 2011 10:54:25

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 11692.5 ppb

|- Sc 45 104340 ppb

| Cr 52 6723.2 ppb

| Cr 53 18304.4 ppb

|> Rh 103 452268.8 ppb

 Ho 165 999886.2 ppb

 Kr 83 60.1 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: Standard 1

Sample Da

tFriday, December 30, 2011 10:55:35

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 13333.5 ppb

|- Sc 45 112713.9 ppb

| Cr 52 12860.8 1.1573 ppb

| Cr 53 18857.6 -0.98413 ppb

|> Rh 103 479969.6 ppb

 Ho 165 1060348.1 ppb

 Kr 83 -70.5 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: Standard 2

Sample Da

tFriday, December 30, 2011 10:56:46

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 11957.2 ppb

|- Sc 45 105092.4 ppb

| Cr 52 484964.4 101.20494 ppb

| Cr 53 73357.8 98.84085 ppb

|> Rh 103 458475 ppb

 Ho 165 1036019.8 ppb

 Kr 83 -12175.3 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: Standard 3

Sample Da

tFriday, December 30, 2011 10:57:56

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 10443.5 ppb

|- Sc 45 96361.8 ppb

| Cr 52 2150458.8 499.7587 ppb

| Cr 53 268690.8 500.2358 ppb

|> Rh 103 416266.3 ppb

 Ho 165 976412.5 ppb

 Kr 83 -57161.4 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 1

Sample Da

tFriday, December 30, 2011 10:59:07

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 12892.9 ppb

|- Sc 45 112415.3 ppb

| Cr 52 6161.4 -0.20214 ppb

| Cr 53 15754.3 -6.44112 ppb

|> Rh 103 482058.6 ppb

 Ho 165 1081338.7 ppb

 Kr 83 61.2 mg/L

ICP-Data 1 of 10

elementOne e 17933-Metals 30.1

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Report Appendix Page 125 of 167
PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report

Sample ID: QC Std 2

Sample Da

tFriday, December 30, 2011 11:00:18

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 10787.5 ppb

|- Sc 45 96133 ppb

| Cr 52 9487.9 0.71713 ppb

| Cr 53 15454.8 -3.48913 ppb

|> Rh 103 426293 ppb

 Ho 165 956521.3 ppb

 Kr 83 -58 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 3

Sample Da

tFriday, December 30, 2011 11:01:28

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 12355.6 ppb

|- Sc 45 112438.1 ppb

| Cr 52 1223987.5 247.04918 ppb

| Cr 53 164413.4 250.98926 ppb

|> Rh 103 477905.1 ppb

 Ho 165 1093345.5 ppb

 Kr 83 -31915.4 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 4

Sample Da

tFriday, December 30, 2011 11:02:40

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 11395.9 ppb

|- Sc 45 101765.4 ppb

| Cr 52 465396.6 99.89192 ppb

| Cr 53 69777.5 96.00467 ppb

|> Rh 103 445603.8 ppb

 Ho 165 996959.9 ppb

 Kr 83 -11912 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 5

Sample Da

tFriday, December 30, 2011 11:03:51

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 11392.2 ppb

|- Sc 45 102113.4 ppb

| Cr 52 229873.4 48.92653 ppb

| Cr 53 41552.8 44.11998 ppb

|> Rh 103 442891.3 ppb

 Ho 165 997924.8 ppb

 Kr 83 78.4 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 6

Sample Da

tFriday, December 30, 2011 11:05:01

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 17624.2 ppb

|- Sc 45 161079.1 ppb

| Cr 52 11301 0.29091 ppb

| Cr 53 14102.6 -15.03856 ppb

|> Rh 103 632748.7 ppb

 Ho 165 1513800.8 ppb

 Kr 83 84.8 mg/L

ICP-Data 2 of 10

elementOne e 17933-Metals 30.2

Owens Corning Insulating Systems, LLC 

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December 20-21, 2011

Report Appendix Page 126 of 167
PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report

Sample ID: QC Std 7

Sample Da

tFriday, December 30, 2011 11:06:12

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 17179.2 ppb

|- Sc 45 149891.4 ppb

| Cr 52 72241.3 10.39686 ppb

| Cr 53 20550.6 -4.76575 ppb

|> Rh 103 592025.8 ppb

 Ho 165 1423130.9 ppb

 Kr 83 45.8 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 9

Sample Da

tFriday, December 30, 2011 11:07:23

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 11633.9 ppb

|- Sc 45 89008.6 ppb

| Cr 52 8162.7 0.45904 ppb

| Cr 53 9524.7 -14.56183 ppb

|> Rh 103 416184.6 ppb

 Ho 165 946396 ppb

 Kr 83 52.8 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 10

Sample Da

tFriday, December 30, 2011 11:08:33

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 14301.3 ppb

|- Sc 45 111481.7 ppb

| Cr 52 236642.4 45.99996 ppb

| Cr 53 35394.8 27.01939 ppb

|> Rh 103 484067.2 ppb

 Ho 165 1093256.2 ppb

 Kr 83 28.3 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 2

Sample Da

tFriday, December 30, 2011 11:09:45

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 12466.8 ppb

|- Sc 45 97717.1 ppb

| Cr 52 10563.1 0.94614 ppb

| Cr 53 14700.6 -5.13881 ppb

|> Rh 103 429092.9 ppb

 Ho 165 965683.3 ppb

 Kr 83 -75.2 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: 17933-1

Sample Da

tFriday, December 30, 2011 11:10:56

Sample DesEnthalpy

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 12013.4 ppb

|- Sc 45 72700.3 ppb

| Cr 52 21311.3 3.25475 ppb

| Cr 53 10459.7 -13.82125 ppb

|> Rh 103 440207.8 ppb

 Ho 165 991059.9 ppb

 Kr 83 -53.3 mg/L

ICP-Data 3 of 10

elementOne e 17933-Metals 30.3

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 127 of 167
PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report

Sample ID: 17933-2

Sample Da

tFriday, December 30, 2011 11:12:07

Sample DesEnthalpy

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 13835.6 ppb

|- Sc 45 110347 ppb

| Cr 52 187035.5 38.6834 ppb

| Cr 53 29458.4 20.39599 ppb

|> Rh 103 452256.5 ppb

 Ho 165 1039709.3 ppb

 Kr 83 -222.2 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: 17933-2

Sample Da

tFriday, December 30, 2011 11:13:17

Sample DesEnthalpy

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 15276.8 ppb

|- Sc 45 125029.6 ppb

| Cr 52 213354 39.64801 ppb

| Cr 53 31902.2 18.8994 ppb

|> Rh 103 503755.3 ppb

 Ho 165 1157595.2 ppb

 Kr 83 -253.1 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: 17933-3

Sample Da

tFriday, December 30, 2011 11:14:27

Sample DesEnthalpy

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 15389.7 ppb

|- Sc 45 124695.5 ppb

| Cr 52 15623.4 1.42864 ppb

| Cr 53 8303.8 -20.45798 ppb

|> Rh 103 527945.2 ppb

 Ho 165 1177797.1 ppb

 Kr 83 -116.4 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: 17933-3

Sample Da

tFriday, December 30, 2011 11:15:38

Sample DesEnthalpy

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 12392.2 ppb

|- Sc 45 103870.1 ppb

| Cr 52 251279 52.25205 ppb

| Cr 53 36732.4 33.42513 ppb

|> Rh 103 454039.9 ppb

 Ho 165 1017689.8 ppb

 Kr 83 -88.3 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: 17933-4

Sample Da

tFriday, December 30, 2011 11:16:48

Sample DesEnthalpy

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 15389.8 ppb

|- Sc 45 126704.9 ppb

| Cr 52 10004.2 0.37461 ppb

| Cr 53 7616.5 -21.6823 ppb

|> Rh 103 534253.8 ppb

 Ho 165 1178942.3 ppb

 Kr 83 0.4 mg/L

ICP-Data 4 of 10

elementOne e 17933-Metals 30.4

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 128 of 167
PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report

Sample ID: QC Std 1

Sample Da

tFriday, December 30, 2011 11:18:01

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 12679.2 ppb

|- Sc 45 103917.9 ppb

| Cr 52 7282.2 0.10595 ppb

| Cr 53 15737.3 -4.95189 ppb

|> Rh 103 456394.9 ppb

 Ho 165 999280.1 ppb

 Kr 83 58.9 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 4

Sample Da

tFriday, December 30, 2011 11:19:11

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 12330.3 ppb

|- Sc 45 104715.3 ppb

| Cr 52 484127.7 101.53648 ppb

| Cr 53 72406.6 97.78586 ppb

|> Rh 103 456109.3 ppb

 Ho 165 1016086.9 ppb

 Kr 83 -12129.7 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: Blank

Sample DatWednesday, January 04, 2012 14:23:35

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 7562 ppb

|- Sc 45 50003.2 ppb

| Cr 52 3844.8 ppb

| Cr 53 9461.6 ppb

|> Rh 103 221790 ppb

 Ho 165 581640.1 ppb

 Kr 83 38.7 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: Standard 1

Sample Da

tWednesday, January 04, 2012 14:24:45

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 7253.1 ppb

|- Sc 45 45870.4 ppb

| Cr 52 6112.4 1.19937 ppb

| Cr 53 9212.3 1.00888 ppb

|> Rh 103 210142.8 ppb

 Ho 165 552459.4 ppb

 Kr 83 -24.9 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: Standard 2

Sample Da

tWednesday, January 04, 2012 14:25:56

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 7446.1 ppb

|- Sc 45 46958 ppb

| Cr 52 230422.5 109.99531 ppb

| Cr 53 35291.1 107.31661 ppb

|> Rh 103 210414.7 ppb

 Ho 165 566131.5 ppb

 Kr 83 -5821.3 mg/L

ICP-Data 5 of 10

elementOne e 17933-Metals 30.5

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 129 of 167
PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report

Sample ID: Standard 3

Sample Da

tWednesday, January 04, 2012 14:27:06

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 7662 ppb

|- Sc 45 48429.3 ppb

| Cr 52 1094598.6 498.00054 ppb

| Cr 53 139383.6 498.53666 ppb

|> Rh 103 223529 ppb

 Ho 165 627354 ppb

 Kr 83 -29503.6 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 1

Sample Da

tWednesday, January 04, 2012 14:28:17

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 7584.2 ppb

|- Sc 45 47865.7 ppb

| Cr 52 3278.9 -0.23254 ppb

| Cr 53 7536.8 -6.90836 ppb

|> Rh 103 217742.9 ppb

 Ho 165 571824.7 ppb

 Kr 83 28.7 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 2

Sample Da

tWednesday, January 04, 2012 14:29:28

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 7469.7 ppb

|- Sc 45 47623.8 ppb

| Cr 52 5665.4 0.95687 ppb

| Cr 53 7893.4 -4.66458 ppb

|> Rh 103 212050.9 ppb

 Ho 165 558104.1 ppb

 Kr 83 -30.9 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 3

Sample Da

tWednesday, January 04, 2012 14:30:38

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 6940.7 ppb

|- Sc 45 43800.9 ppb

| Cr 52 508835.2 257.30324 ppb

| Cr 53 68269.5 255.68198 ppb

|> Rh 103 200452.2 ppb

 Ho 165 546763.2 ppb

 Kr 83 -13186.7 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 4

Sample Da

tWednesday, January 04, 2012 14:31:50

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 7590.2 ppb

|- Sc 45 49217.2 ppb

| Cr 52 242176.7 110.36421 ppb

| Cr 53 36120.6 104.02877 ppb

|> Rh 103 220406.7 ppb

 Ho 165 590310.2 ppb

 Kr 83 -6094.2 mg/L

ICP-Data 6 of 10

elementOne e 17933-Metals 30.6

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 130 of 167
PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report

Sample ID: QC Std 5

Sample Da

tWednesday, January 04, 2012 14:33:01

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 8179.3 ppb

|- Sc 45 53318.9 ppb

| Cr 52 124081.1 53.37283 ppb

| Cr 53 21749.7 44.6569 ppb

|> Rh 103 229661.7 ppb

 Ho 165 618003.2 ppb

 Kr 83 21.3 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 7

Sample Da

tWednesday, January 04, 2012 14:34:12

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 10.3 ppb

|- Sc 45 254.3 ppb

| Cr 52 1906.9 14003.895 ppb

| Cr 53 3859.2 258739.85 ppb

|> Rh 103 20 ppb

 Ho 165 47.7 ppb

 Kr 83 210.2 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: 17933-5

Sample Da

tWednesday, January 04, 2012 14:36:36

Sample DesEnthalpy

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 7075 ppb

|- Sc 45 57727.9 ppb

| Cr 52 113318.7 42.09263 ppb

| Cr 53 17254.4 19.55689 ppb

|> Rh 103 263661.1 ppb

 Ho 165 679605.8 ppb

 Kr 83 -97.9 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: 17933-7

Sample Da

tWednesday, January 04, 2012 14:40:07

Sample DesEnthalpy

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 8477 ppb

|- Sc 45 62115.8 ppb

| Cr 52 6732.2 0.73757 ppb

| Cr 53 2947.1 -27.38322 ppb

|> Rh 103 274091.2 ppb

 Ho 165 720592.7 ppb

 Kr 83 -237.2 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: 17933-7

Sample Da

tWednesday, January 04, 2012 14:41:17

Sample DesEnthalpy

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 8931.2 ppb

|- Sc 45 65379.6 ppb

| Cr 52 136426.9 45.1477 ppb

| Cr 53 19044.6 18.46084 ppb

|> Rh 103 296760.3 ppb

 Ho 165 779079 ppb

 Kr 83 -270.8 mg/L

ICP-Data 7 of 10

elementOne e 17933-Metals 30.7

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 131 of 167
PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report

Sample ID: 17933-8

Sample Da

tWednesday, January 04, 2012 14:42:28

Sample DesEnthalpy

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 6125.3 ppb

|- Sc 45 49946.9 ppb

| Cr 52 4508.8 0.54219 ppb

| Cr 53 2194.9 -27.16255 ppb

|> Rh 103 199080.9 ppb

 Ho 165 571235.9 ppb

 Kr 83 -48.1 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 1

Sample Da

tWednesday, January 04, 2012 14:47:12

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 13284.2 ppb

|- Sc 45 66871.8 ppb

| Cr 52 3547.7 -0.65796 ppb

| Cr 53 3570.4 -27.20741 ppb

|> Rh 103 325846.8 ppb

 Ho 165 802467.1 ppb

 Kr 83 49.1 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 4

Sample Da

tWednesday, January 04, 2012 14:48:23

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 12912.3 ppb

|- Sc 45 64058.3 ppb

| Cr 52 303833.3 97.40979 ppb

| Cr 53 40107.3 73.47831 ppb

|> Rh 103 312665.7 ppb

 Ho 165 784411 ppb

 Kr 83 -8504.2 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 1

Sample Da

tWednesday, January 04, 2012 15:13:13

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 13066.2 ppb

|- Sc 45 54019 ppb

| Cr 52 2983.8 -0.61845 ppb

| Cr 53 3166.6 -26.34665 ppb

|> Rh 103 264652.3 ppb

 Ho 165 644876.8 ppb

 Kr 83 38.4 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 4

Sample Da

tWednesday, January 04, 2012 15:14:23

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 11566.1 ppb

|- Sc 45 48297.6 ppb

| Cr 52 229647.5 96.209 ppb

| Cr 53 30275.7 72.01401 ppb

|> Rh 103 239206 ppb

 Ho 165 599111.9 ppb

 Kr 83 -6558.7 mg/L

ICP-Data 8 of 10

elementOne e 17933-Metals 30.8

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 132 of 167
PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report

Sample ID: 17933-6

Sample Da

tThursday, January 05, 2012 09:29:35

Sample DesEnthalpy

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 4741 ppb

|- Sc 45 33986.1 ppb

| Cr 52 7218.9 2.52983 ppb

| Cr 53 3053.2 -21.31877 ppb

|> Rh 103 171391.7 ppb

 Ho 165 438893 ppb

 Kr 83 -231.8 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 1

Sample Da

tThursday, January 05, 2012 10:31:03

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 11092.4 ppb

|- Sc 45 68658.6 ppb

| Cr 52 5109.4 -0.18639 ppb

| Cr 53 7501.8 -17.0675 ppb

|> Rh 103 329455.2 ppb

 Ho 165 767095.6 ppb

 Kr 83 23.8 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 4

Sample Da

tThursday, January 05, 2012 10:32:14

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 10792.8 ppb

|- Sc 45 68115.2 ppb

| Cr 52 308275.6 93.38726 ppb

| Cr 53 41968.3 72.32628 ppb

|> Rh 103 330651.9 ppb

 Ho 165 767071.6 ppb

 Kr 83 -8656.1 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 1

Sample Da

tThursday, January 05, 2012 10:44:03

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 14874.5 ppb

|- Sc 45 72640.8 ppb

| Cr 52 4390.1 -0.41898 ppb

| Cr 53 4152.6 -25.87464 ppb

|> Rh 103 331975.7 ppb

 Ho 165 784485.7 ppb

 Kr 83 12.7 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 4

Sample Da

tThursday, January 05, 2012 10:45:13

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 13321.7 ppb

|- Sc 45 64274.4 ppb

| Cr 52 293612.6 96.68435 ppb

| Cr 53 39068.1 73.5435 ppb

|> Rh 103 304377.9 ppb

 Ho 165 736773.7 ppb

 Kr 83 -8274.5 mg/L

ICP-Data 9 of 10

elementOne e 17933-Metals 30.9

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 133 of 167
PerkinElmer ELAN 6100 ICP-MS

Method 6020 & 200.8 Metals Summary Report

Sample ID: LRB

Sample Da

tThursday, January 05, 2012 14:18:49

Sample DesEnthalpy

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 11495.8 ppb

|- Sc 45 71169.8 ppb

| Cr 52 5989.3 0.10369 ppb

| Cr 53 7591.2 -16.6446 ppb

|> Rh 103 326369.5 ppb

 Ho 165 927662.1 ppb

 Kr 83 36.9 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: LRB

Sample Da

tThursday, January 05, 2012 14:20:00

Sample DesEnthalpy

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 11965.9 ppb

|- Sc 45 73724.7 ppb

| Cr 52 206979.8 60.59096 ppb

| Cr 53 31004.1 41.9387 ppb

|> Rh 103 338745.8 ppb

 Ho 165 957016.7 ppb

 Kr 83 39.8 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: 17933-6

Sample Da

tThursday, January 05, 2012 14:21:10

Sample DesEnthalpy

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 6265.5 ppb

|- Sc 45 43669.6 ppb

| Cr 52 7973.5 2.44684 ppb

| Cr 53 4111.6 -18.32476 ppb

|> Rh 103 193025.8 ppb

 Ho 165 556747.2 ppb

 Kr 83 -268.4 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 1

Sample Da

tThursday, January 05, 2012 14:30:36

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 13398.9 ppb

|- Sc 45 71679.5 ppb

| Cr 52 3386.3 -0.76334 ppb

| Cr 53 4210.3 -26.09429 ppb

|> Rh 103 343589.4 ppb

 Ho 165 876993.2 ppb

 Kr 83 41.9 mg/L

Method 6020 & 200.8 Metals Summary Repor

t

Sample ID: QC Std 4

Sample Da

tThursday, January 05, 2012 14:31:46

Sample Description:

Concentration Results

 Analyte Mass Meas. Inten

sConc. MeanReport Unit

 Li 6 14648.7 ppb

|- Sc 45 79211.6 ppb

| Cr 52 372160.2 100.84963 ppb

| Cr 53 49634.5 78.47497 ppb

|> Rh 103 370128.5 ppb

 Ho 165 954451.2 ppb

 Kr 83 -10131.8 mg/L

ICP-Data 10 of 10

elementOne e 17933-Metals 30.10

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 134 of 167
APPENDIX D 

CALIBRATION DATA 

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 135 of 167
Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250

Report Appendix Page 136 of 167
TYPE S PITOT TUBE INSPECTION DATA SHEET

Certification 

I certify that the Type S pitot tube/probe ID # NC-PA-25-A meets or exceeds all 

specifications, criteria and/or applicable design features and is hereby assigned a pitot tube 

calibration factor Cp of 0.84. NIST traceable digital thermometer serial number 111483849 

was used as reference temperature. 

Certified and Calibrated By: Ed Brown 

 

 Date Certified: 10 Jan.2012 

 Annual Calibration 

Parameter Value Allowable Range 

Assembly Level? YES Yes 

Holes Damaged? NO No 

Obstructed? NO No 

1 0 -10 < 1 < +10

2 0 -10 < 2 < +10

1 0 -5 < 1 < +5

2 0 -5 < 2 < +5

 0 

 0 

A 0.933 for 1/4” OD, 0.526 to 0.750 

for 3/8” OD, 0.788 to 1.125 

Z = A sin  0 Z =  0.125” 

W = A sin  0 W =  0.031” 

PA 0.467 for 1/4” OD, 0.263 to 0.375 

for 3/8” OD, 0.394 to 0.563 

PB 0.467 for 1/4” OD, 0.263 to 0.375 

for 3/8” OD, 0.394 to 0.563 

PA - PB 0 -0.063 to 0.063” 

DT 0.373 0.188 to 0.375” 

Thermocouple Cal. 64.2 Reference temp. 

Thermocouple Cal. 63.7 Probe Thermocouple 

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 137 of 167
Calibration Date: 8/4/2011 Calibrated by: Lalan Kirby

\

Entec Services Temperature **Reference Thermocouple Difference Within

ID Number Source Temperature Temperature Degrees F Tolerance

TC-1 ambient 68 68 0 Yes

TC-2 ambient 68 67 1 Yes

TC-6 ambient 68 68 0 Yes

TC-8 ambient 70 68 2 Yes

TC-9 ambient 69 69 0 Yes

TC-11 ambient 69 70 1 Yes

TC-14 ambient 68 67 1 Yes

TC-15 ambient 69 68 1 Yes

TC-16 ambient 69 68 1 Yes

TC-17 ambient 70 68 2 Yes

TC-20 ambient 69 69 0 Yes

TC-22 ambient 69 69 0 Yes

TC-23 ambient 67 67 0 Yes

TCS - 3 ambient 67 68 1 Yes

TCS - 4 ambient 67 68 1 Yes

TCS - 5 ambient 67 69 2 Yes

TSC -8 ambient 68 68 0 Yes

Fluke Hand Held 1 ambient 68 69 1 Yes

Fluke Hand Held 2 ambient 68 68 0 Yes

TCG - 001 ambient 69 69 0 Yes

TCG - 002 ambient 69 68 1 Yes

TCG - 003 ambient 70 70 0 Yes

TCG - 004 ambient 70 70 0 Yes

TCG - 005 ambient 69 70 1 Yes

TCG - 006 ambient 69 69 0 Yes

TCG - 007 ambient 69 68 1 Yes

TCG - 008 ambient 69 69 0 Yes

TCG - 009 ambient 69 69 0 Yes

TCG - 011 ambient 68 69 1 Yes

TCG - 012 ambient 68 68 0 Yes

TCG - 013 ambient 68 68 0 Yes

TCG - 014 ambient 68 68 0 Yes

TCG - 015 ambient 69 69 0 Yes

TCG - 016 ambient 69 69 0 Yes

TCG - 017 ambient 69 69 0 Yes

2947 ambient 68 68 0 Yes

2948 ambient 68 68 0 Yes

2958 ambient 68 67 1 Yes

3917 ambient 69 70 1 Yes

3918 ambient 69 70 1 Yes

3920 ambient 69 69 0 Yes

3923 ambient 69 69 0 Yes

3926 ambient 69 69 0 Yes

3927 ambient 69 69 0 Yes

3932 ambient 69 69 0 Yes

3933 ambient 69 69 0 Yes

3936 ambient 69 69 0 Yes

3938 ambient 69 69 0 Yes

Temperature tolerance within +/- 2 0 F of acceptable ranges for all thermocouples.

** Note: NIST Traceable Digital Thermometer Serial Number 101826260 was used as reference temperature

ENTEC Services, Inc.

30 Monroe Drive - Pelham, Al 35124

Annual Thermocouple Calibrations

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 138 of 167
Calibration Date: 8/4/2011 Calibrated by: Lalan Kirby

\

Entec Services Temperature **Reference Thermocouple Difference Within

ID Number Source Temperature Temperature Degrees F Tolerance

GN-1 ambient 67 67 0 Yes

GN-2 ambient 67 67 0 Yes

GN-3 ambient 67 67 0 Yes

GN-4 ambient 67 67 0 Yes

GN-5 ambient 67 67 0 Yes

GN-6 ambient 67 67 0 Yes

GN-7 ambient 67 67 0 Yes

GN-8 ambient 67 67 0 Yes

GN-9 ambient 67 67 0 Yes

GN-11 ambient 67 67 0 Yes

GN-13 ambient 66 66 0 Yes

GN-14 ambient 67 65 2 Yes

GN-15 (Mini HB ambient 67 65 2 Yes

GN-16 (Mini HB) ambient 67 68 -1 Yes

GN-17 ambient 67 67 0 Yes

GN-18 (Mini HB) ambient 67 67 0 Yes

GN-21 ambient 67 65 2 Yes

GN-22 (Mini HB) ambient 67 67 0 Yes

GN-23 ambient 67 67 0 Yes

GN-24 ambient 67 67 0 Yes

GN-26 ambient 67 66 1 Yes

GN-27 ambient 67 67 0 Yes

GN-28 ambient 67 67 0 Yes

GN-29 ambient 67 66 1 Yes

GN-30 ambient 66 66 0 Yes

** Note: NIST Traceable Digital Thermometer Serial Number 101826260 was used as reference temperature

ENTEC Services, Inc.

30 Monroe Drive - Pelham, Al 35124

Annual Gooseneck Thermocouple Calibrations

Temperature tolerance within +/- 2 0 F of acceptable ranges for all thermocouples.

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Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

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APPENDIX E 

QSTI CERTIFICATIONS 

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APPENDIX F 

SAMPLE CALCULATIONS AND NOMENCLATURE 

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Report Appendix Page 145 of 167
NOMENCLATURE 

As Cross-sectional area of stack, square feet 

An Cross-sectional area of nozzle, square feet 

ACFM Actual cubic feet of gas per minute at stack conditions 

Bws Proportion by volume of water vapor in gas stream 

Cs Particulate concentration in stack gas, gr/dscf 

Ca Particulate concentration in stack gas, gr/acf 

Cp Pitot tube coefficient 

∆ H Pressure drop across orifice meter, inches water 

∆ P Velocity head of stack gas, inches water 

dscf Cubic feet of dry gas corrected to standard conditions 

EA Excess Air 

E/Btu Particulate Emission Rate, pounds/mmBtu 

F F-factor, 9640 dscf/MMBTU's of heat input 

Kp Constant (85.49) 

Mn Total particulate matter collected, mg 

Md Molecular weight of stack gas; dry basis, lb/lb-mole 

Ms Molecular weight of stack gas; wet basis, lb/lb-mole 

I Percent of isokinetic sampling 

Pbar Barometric pressure, inches mercury 

Pg Stack static pressure, inches of water 

Pm Barometric pressure of dry gas meter, in. mercury 

PMR Particulate mass rate, pounds/hour 

Ps Absolute stack gas pressure, inches mercury 

Pstd Barometric pressure, standard conditions, 29.92 inches Hg 

Qa Volumetric flow rate, actual conditions, ACF/min 

Qs Volumetric flow rate, standard conditions, scf/min 

Qstd Volumetric flow rate, dry standard conditions, dscf/min 

TBws Theoretical water vapor in the gas stream based on saturated stack conditions, proportion by 

volume (dimensionless) 

TVlc Theoretical volume of water collected based on saturated stack conditions, ml 

TVwstd Theoretical volume of water vapor in the gas sample based on saturated stack conditions, 

corrected to standard temperature and pressure, scf

Tm Absolute average dry gas meter temperature, degree R (460) 

Ts Absolute average stack gas temperature, degree R (460) 

Tstd Absolute temperature at standard conditions, 528 R 

Ө Total sampling time, minutes 

Vlc Total volume collected in impingers and silica gel, gr 

Vm Volume of gas sampled through gas meter, cubic feet 

Vn Volume collected at stack conditions through nozzle, ACF 

Vma Stack gas volume sampled, ACF 

Vmstd Volume of gas sampled through gas meter, cubic feet 

Vs Average stack gas velocity, feet/sec 

Vwcstd Volume of water vapor in gas sampled from impingers, standard cubic feet 

Vwsgstd Volume of water vapor in gas sampled from silica gel, standard cubic feet 

Wimp Total volume collected in impingers, gr 

Wsg Total volume collected in silica gel, gr 

Y Dry gas meter calibration factor 

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 146 of 167
TEST CALCULATIONS

Owens Corning Lakeland Plant

Lakeland, FL

Melt Furnace (EU 002)

Run No. 1

Equations Equation Components Results

1 Ps = Pbar + (Pg/13.6) Pbar Pg Ps

(in. Hg) (in. H2O) (in. Hg)

30.22 -0.37 30.19

2 Pm = Pbar + (∆H/13.6) Pbar ∆H Pm

(in. Hg) (in. H2O) (in. Hg)

30.22 1.49 30.329

3 Vmstd = 17.647 * Vm * Y * (Pm/Tm) Vm Y Pm Tm Vmstd

(ft3) (in. Hg) (oR) (std. ft3)

173.663 0.937 30.33 550.00 158.287

4a Vwc(std) = 0.04706 * Wimp Wimp Vwc(std)

(grams) (std. ft3)

55 2.588

4b Vwsg(std) = 0.04715 * Wsg Wsg Vwsg(std)

(grams) (std. ft3)

32.4 1.528

5 Bws = Vwstd/(Vmstd + Vwstd) Vwstd Vmstd Bws

(std. ft3) (std. ft3) (fraction)

4.12 158.29 0.0253

9 Md = (0.44*%CO2) + (0.32*%O2) + (0.28*((100-(%CO2 + %O2))) CO2 O2 Md

(%) (%) (g/g-mole)

0.70 20.20 28.920

10 Ms = Md * (1-Bws) + 18* Bws Md Bws TBws Ms

g/g-mole (fraction) % (g/g-mole)

28.92 0.0253 7.0385 28.643

11 Vs = 85.49 * Cp * (∆pavg)^1/2 * (Ts/Ps*Ms)^1/2 Cp (∆pavg)1/2 Ts Ps Ms Vs

(in. H2O) (oR) (in. Hg) (g/g-mole) (ft/sec)

0.84 0.777 582.4 30.19 28.64 45.78

12 Qa = Vs * As * 60 Vs As Qa

(ft/sec) (ft2) (acf/min)

45.78 1.576 4,330

13 Qs = Qa * (528/Ts) * (Ps/29.92) Qa Ts Ps Qs

(acf/min) (oR) (in. Hg) (scf/min)

4,330 582.4 30.19 3,961

14 Qstd = Qa * (1-Bws)*(528/Ts)*(Ps/29.92) Qa Bws Ts Ps Qstd

(acf/min) (fraction) (oR) (in. Hg) (dscf/min)

4,330 0.0253 582.4 30.19 3,861

15 Cs = 0.00001543 * (Mn/Vmstd) Mn Vmstd Cs

(mg) (ft3) (gr/scfd)

12.900 158.287 1.26E-03

18 PMR = Cs * Qstd * (60/7000) Cs Qstd PMR

(gr/scfd) (dscf/min) (lbs/hr)

1.26E-03 3,861 0.042

19 Vn = Ts/Ps * {(0.002669) * Vlc + (Vm * Y * Pm)/Tm)} Ts Ps Vlc Vm Y Vn

(oR) (in. Hg) (gr) (ft3) (acf)

582.4 30.193 87.40 173.663 0.937 177.587

Pm Tm

(in. Hg) (oR)

30.329 550.00

Owens Corning Insulating Systems, LLC 

Lakeland, FL

Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 147 of 167
TEST CALCULATIONS

Owens Corning Lakeland Plant

Lakeland, FL

Melt Furnace (EU 002)

Run No. 1

Equations Equation Components Results

21 I = Vn * 100/(60 * Θ * Vs * An) Vn Vs An Θ I

(acf) (ft/sec) (ft2) (min) (%)

177.587 45.782 0.000264 240 102.04

Equations for Metals Emissions Calculations

22 CCr = 0.001 mg/ug * ug / dscm Meter Vol. CCr

Filterable Chromiuim concentration at standard conditions dscm mg/dscm

4.482 6.38E-04

Chromiuim Mass

ug

2.86

23 CCr-7%=CCr * ((20.9-7)/(20.9-%O2)) CCr O2 CCr-7%

Filterable Chromium concentration at 7% oxygen mg/dscm (%) mg/dscm @ 7% O2

6.38E-04 20.20 1.27E-02

24 Crkg/hr= 0.000001 kg/mg * CCr mg/dscm *Qsd m3/min * 60 min/hr CCr Qstd Crkg/hr

Hourly Filterable Chromium emissions mg/dscm (dscm/min) kg/hr

6.38E-04 112 4.29E-06

Cr lbs/hr

9.47E-06

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Project No. 511250 ICR Furnace Test 

December 20-21, 2011

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APPENDIX G 

ICR DOCUMENTS 

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December 20-21, 2011

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APPENDIX G.1 

EPA LETTER AND ENCLOSURES 1 AND 2 

 

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APPENDIX H 

CONFIDENTIAL PRODUCTION DATA 

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Project No. 511250 ICR Furnace Test 

December 20-21, 2011

Report Appendix Page 165 of 167
Process information will be submitted electronically

separately as Confidential Business Information (CBI).

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Project No. 511250 ICR Furnace Test 

December 20-21, 2011

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This is the last page of

this report.

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Report Appendix Page 167 of 167