November 8, 2012 CAA Section 114 - Polyvinyl Chloride and Copolymers (PVC) Production Pro

PVC General Company and Facility Information

Instructions

Please complete this worksheet for your parent company and PVC production facility.

Parent Company General Information

Parent Company Name:

Address:

City:

Country: USA

Size of Company (approximate number of employees including all subsidiaries, branches, and related establishments 

PVC Production Facility General Information

Facility Name:

Facility Address:

Facility City:

Facility Technical Contact Name:

Technical Contact Telephone Number:

Technical Contact Email:

Number of employees attached to the PVC production facility: 145

115 Perimeter Place, Suite 460

Axiall Corporation

662-369-3590

jason.darnell@axiall.com

Aberdeen

PO Box 91

Aberdeen

Jason Darnell

Atlanta
ers (PVC) Production Process Wastewater

State: GA Zip Code: 30346

hes, and related establishments owned): 5848

State: MS Zip Code: 39730
November 8, 2012 CAA Section 114 - Polyvinyl Chloride and Copolymers (PVC) Production Pro

PVC Production Process Wastewater Treatment System Information Update

Instructions

2. Also complete the additional supplemental questions to Form C-1-c.

FORM C-1-c

PROCESS EQUIPMENT - WASTEWATER STEAM STRIPPER

Process Unit ID: 1

Process Equipment ID: U-60/61

Wastewater Feed Rate (lb/hr): 10500

Feed Temperature (°F): 80

Feed Inlet Pressure (psia): 20

Liquid Loading Rate (liters/m2):

Steam Feed Rate (lb/hr): 3000

Steam to Feed Ratio (kg steam/liter of wastewater):

Operating Temperature (°F): 200

Operating Pressure (psig): 0

Total Number of Stages: 1

Overall Calculated Tray Efficiency: 100

Stripping Factor:

Flow configuration (countercurrent, cocurrent): Batch

Number of Actual Trays: 0

Column Height (meters):

Year Equipment Installed: 2004

Equipment Currently Regulated Under (cite regulations): 40 CFR 61 Subparts A and F, 40 CFR 63 Subpart 

1. A copy of your facility's responses on Form C-1-c of the August 21, 2009 CAA section 114 request were included w

below.
mers (PVC) Production Process Wastewater

Form C-1-c Supplemental Questions

Please also provide the stripper feed rate in liters per hour, or liters for batch strippers:

If the above stripper feed rate or capacity does not equal the maximum design rate or capacity, plea

parts A and F, 40 CFR 63 Subpart J

ection 114 request were included with the CAA Section 114 request letter dated November XX, 2012. Please review those previous respons
 batch strippers: liters/hour

15000 liters

m design rate or capacity, please provide those values:

 liters/hour (max design)

 liters (max design)

eview those previous responses and update if necessary
November 8, 2012 CAA Section 114 - Polyvinyl Chloride and Copolymers (PVC) Production Pro

PVC Production Process Wastewater Stream Information

Instructions

1. Complete a row in Table 1 below for each PVC process wastewater stream generated within the PVC production fa

2. Complete a row in Table 2 below for each PVC process wastewater stream that exits a PVC production process wa

3. In Table 4, please provide the source, flow rates, and the ID of the PVC process wastewater treatment system for e

Table 1. Process Wastewater Streams Not Treated by a PVC Process Wastewater Treatment System

1 3

PVC Process 

Wastewater 

Stream ID

PVC Process 

Unit ID Name of PVC Process Wastewater Stream

2
Table 2. Process Wastewater Streams Exiting a PVC Process Wastewater Treatment System

1 2 3 4 5 6

Min

1 U-60/61 Steam Stripping Batch 16000

Table 3. PVC Process Wastewater Destination Codes Table

Wastewater treatment system

Discharge without treatment by pipeline, sewer, or other conveyance to surface water

Discharge to POTW, no treatment

Discharge to PrOTW, no treatment

Zero discharge or alternative disposal method

Recycle to process

Other

Table 4. Non-PVC Production Process Wastewater Streams Entering a PVC Process Wastewater Treatment S

2 3

Min Max

Is this 

process 

wastewater 

treatment 

system batch 

or continuous 

operation?

Process Wastewater Stream Flow Rate 

(gallons per day)

Type of Process 

Wastewater 

Treatment System

Source of Process Wastewater Stream

1

PVC Process Wastewate

Destination Description

PVC Process 

Wastewater 

Treatment 

System ID

PVC Process 

Unit ID

PVC Process 

Wastewater 

Stream ID

VC) Production Process Wastewater

hin the PVC production facility that exits a piece of PVC production process equipment and is not treated by a PVC production process waste

VC production process wastewater treatment system.

ter treatment system for each stream that enters a PVC process wastewater treatment system but that does not originate from the PVC prod

tment System

4 5 6 7 8

Min Max Average

PVC Process Wastewater Stream Flow Rate 

(gallons per day) Operating Days Per 

Year

Flow Rate 

Determination 

Method
7 8 9 10 11

Max Average

24000 20000 Estimated 350 WWT

Code

WWT Provide name of the wastewater treatment system

SW Provide name of outfall

POTWRAW Provide name of POTW

PrOTWRAW Provide name of PrOTW

ZEROALT Describe method

RECYC Describe where in the process the stream is recycled

OTHER Describe

Wastewater Treatment System

4 5 6 7

Average

Flow Rate 

Determination 

Method

Operating Days 

Per Year

water Stream Flow Rate 

ons per day)

PVC Process 

Wastewater Stream 

Destination Code

(Refer to Table 3 below)

VC Process Wastewater Stream Flow Rate 

(gallons per day)

Flow Rate 

Determination 

Method

PVC Process 

Wastewater 

Treatment 

System ID

Operating Days 

Per Year

Process Wastewater Destination D

eated by a PVC production process wastewater treatment system.

hat does not originate from the PVC production facility.

9 10

Originating PVC Process 

Equipment ID

Originating PVC Process 

Equipment Description
12 13

City of Aberdeen POTW Yes

e of the wastewater treatment system

ere in the process the stream is recycled

Associated Destination 

Information

(Refer to Table 3 below)

Process Wastewater Destination Details to Provide in Column 12 of Table 1 and Column 11 of Table 2

Is this PVC process wastewater 

stream exposed to the atmosphere 

at any point between the outlet of 

the PVC process wastewater 

treatment system and its 

destination?

11 12

Associated Destination Information

PVC Process Wastewater Stream 

Destination Code

(Refer to Table 3 below)
If your response in Column 3 is "Other" then please provide a description of the process wastewaetr 

treatment system

14

able 1 and Column 11 of Table 2

13

Is this PVC process wastewater 

stream exposed to the atmosphere 

at any point between the 

originating PVC process equipment 

and its destination?
de a description of the process wastewaetr 
November 8, 2012 CAA Section 114 - Polyvinyl Chloride and Copolymers (PVC) Production Pro

PVC Production Process Wastewater Sampling and Analysis Data

Instructions

1. Complete the table below for each PVC process wastewater steam exiting a process wastewater treatment system 

2. Enter the PVC process wastewater treatment system ID for the stream that was sampled and analyzed. The ID mu

3. Complete columns 1 through 30. Enter the sample date, resin type, stream flow rate, basis for flow rate determinat

4. Enter any other HAP expected to be present (that are not listed in Table 10 to Subpart HHHHHHH of Part 63) in the 

4. For compounds that were not detected, indicate as such in the "Non-Detect?" column and provide the method dete

5. Enter any notes or additional information relevant to the sampling or analysis.

Company

Facility

PVC Process Wastewater Treatment System ID

CAS No. HAP

107211 Ethylene glycol

67561 Methanol

75070 Acetaldehyde

50000 Formaldehyde

51285 2,4-dinitrophenol

98862 Acetophenone

117817 Bis(2-ethylhexyl) phthalate (DEHP)

123319 Hydroquinone

108952 Phenol

79345 1,1,2,2-tetrachloroethane

106990 1,3-butadiene

540841 2,2,4-trimethylpentane

71432 Benzene

108907 Chlorobenzene

67663 Chloroform

126998 Chloroprene

98828 Cumene

75003 Ethyl chloride (Chloroethane)

100414 Ethylbenzene

107062 Ethylene dichloride (1,2-Dichloroethane)

75343 Ethylidene dichloride (1,1-Dichloroethane)

74873 Methyl chloride (Chloromethane)

75092 Methylene chloride

110543 n-Hexane

Resin Type (suspension, dispersion, bulk, etc.) -->
108883 Toluene

71556 Methyl chloroform (1,1,1-Trichloroethane)

79005 1,1,2-Trichloroethane

108054 Vinyl acetate

593602 Vinyl bromide

75014 Vinyl chloride

75354 Vinylidene chloride (1,1-Dichloroethylene)

1330207 Xylenes (isomers and mixtures)
 Chloride and Copolymers (PVC) Production Process Wastewater

g and Analysis Data

stewater steam exiting a process wastewater treatment system that was sampled and analyzed. Complete one worksheet for each single st

m ID for the stream that was sampled and analyzed. The ID must match the IDs listed in Table 2 of the "Stream Info" worksheet.

date, resin type, stream flow rate, basis for flow rate determination, stream temperature, sample type, analysis date, lab report ID, and lab sa

re not listed in Table 10 to Subpart HHHHHHH of Part 63) in the table below.

such in the "Non-Detect?" column and provide the method detection limit, in ppmw, in the "Concentration (ppmw)" column.

 the sampling or analysis.

Axiall Corporation

Aberdeen

Analysis Method Concentration 

(ppmw) Non-Detect?

SW-846-8015C 0.6 Non-detect

SW-846-8015C 0.2 Non-detect

SW-846-8315A 6.53

SW-846-8315A 0.975

SW-846-8270D 0.0876 Non-detect

SW-846-8270D 15.8

SW-846-8270D 0.143 Non-detect

SW-846-8270D 0.370 Non-detect

SW-846-8270D 0.485 Non-detect

SW-846-8260B 0.00465 Non-detect

SW-846-8260B 0.012 Non-detect

SW-846-8260B 0.0225 Non-detect

SW-846-8260B 0.00239 Non-detect

SW-846-8260B 0.00232 Non-detect

SW-846-8260B 0.00545 Non-detect

SW-846-8260B 0.0165 Non-detect

SW-846-8260B 0.00287 Non-detect

SW-846-8260B 0.0271

SW-846-8260B 0.00291 Non-detect

SW-846-8260B 0.0140 Non-detect

SW-846-8260B 0.00580 Non-detect

SW-846-8260B 0.049

SW-846-8260B 0.0209 Non-detect

SW-846-8260B 0.0835 Non-detect

Stream Temperature (degrees F) -->

Sample Date -->

Stream Flow Rate (gallons per minute) -->

Resin Type (suspension, dispersion, bulk, etc.) --> Suspension

200

01/14/13

Stripper Bottoms Wastewater

13-015-0215

01/16/13

41

Lab Report ID -->

Flow Rate Determination Method -->

Analysis Date -->

Lab Sample ID -->

Estimated
SW-846-8260B 0.00250 Non-detect

SW-846-8260B 0.00690 Non-detect

SW-846-8260B 0.00223 Non-detect

SW-846-8260B 0.00337 Non-detect

SW-846-8260B NOT FOUND Non-detect

EPA Method 107 0.869

SW-846-8260B 0.00287 Non-detect

SW-846-8260B 0.0036 Non-detect
and analyzed. Complete one worksheet for each single stream (make copies of this worksheet if necessary).

sted in Table 2 of the "Stream Info" worksheet.

ature, sample type, analysis date, lab report ID, and lab sample ID. Enter the concentration results for each HAP listed.

, in the "Concentration (ppmw)" column.

Note(s) Concentration 

(ppmw) Non-Detect? Note(s)

0.6 Non-detect

0.2 Non-detect

11.600

Detected in blank 1.21

0.0928 Non-detect

14.800

0.152 Non-detect

0.400 Non-detect

0.513 Non-detect

0.00465 Non-detect

0.012 Non-detect

0.0225 Non-detect

0.00239 Non-detect

0.00232 Non-detect

0.00545 Non-detect

0.0165 Non-detect

0.00287 Non-detect

Estimated Value 0.0533

0.00291 Non-detect

0.0140 Non-detect

0.00580 Non-detect

Estimated Value 0.128

0.0209 Non-detect

0.0835 Non-detect

1

Suspension

Estimated

Stripper Bottoms Wastewater

Estimated

01/18/13

37.4

13-017-0225

01/15/13

200

2
0.00250 Non-detect

0.00690 Non-detect

0.00223 Non-detect

0.00337 Non-detect

NOT FOUND Non-detect

1.780

0.00358 Non-detect

0.0036 Non-detect
Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

0.6 Non-detect 0.6 Non-detect

0.2 Non-detect 0.2 Non-detect

7.32 7.97

1.32 1.66

0.0770 Non-detect 0.0686 Non-detect

18.5 17.9

0.126 Non-detect 0.112 Non-detect

0.435 Non-detect 0.429 Non-detect

0.426 Non-detect 0.0379 Non-detect

0.00465 Non-detect 0.00186 Non-detect

0.0120 Non-detect 0.00480 Non-detect

0.0225 Non-detect 0.00900 Non-detect

0.00239 Non-detect 0.00095 Non-detect

0.00232 Non-detect 0.00092 Non-detect

0.00545 Non-detect 0.00218 Non-detect

0.0165 Non-detect 0.0066 Non-detect

0.00287 Non-detect 0.00115 Non-detect

0.00625 Non-detect 0.0242

0.00291 Non-detect 0.00116 Non-detect

0.0140 Non-detect 0.00560 Non-detect

0.00580 Non-detect 0.00232 Non-detect

0.0651 0.0826

0.0209 Non-detect 0.00836 Non-detect

0.0835 Non-detect 0.0334 Non-detect

200

41

Estimated

Stripper Bottoms Wastewater

01/18/13

39.2

Estimated

13-017-0226 13-021-0234

01/21/13

Stripper Bottoms Wastewater

200

3

01/16/13 01/17/13

Suspension Suspension
0.00250 Non-detect 0.00099 Non-detect

0.00690 Non-detect 0.00276 Non-detect

0.00223 Non-detect 0.00089 Non-detect

0.00337 Non-detect 0.00135 Non-detect

NOT FOUND Non-detect NOT FOUND Non-detect

1.17 1.86

0.00358 Non-detect 0.00143 Non-detect

0.0036 Non-detect 0.0014 Non-detect
Note(s) Concentration 

(ppmw) Non-Detect? Note(s)

0.6 Non-detect

0.2 Non-detect

5.55

1.40

0.0853 Non-detect

16.8

0.139 Non-detect

0.316 Non-detect

0.0472 Non-detect

0.00186 Non-detect

0.00480 Non-detect

0.00900 Non-detect

0.00095 Non-detect

0.00092 Non-detect

0.00218 Non-detect

0.00660 Non-detect

0.00115 Non-detect

0.0740

0.00116 Non-detect

0.00560 Non-detect

0.00232 Non-detect

0.211

0.00836 Non-detect

0.0334 Non-detect

35.6

Estimated Estimated

13-021-0235

01/21/13

Stripper Bottoms Wastewater

Suspension

200

4 5

01/18/13
0.00099 Non-detect

0.00276 Non-detect

0.00089 Non-detect

0.00135 Non-detect

NOT FOUND Non-detect

2.700

0.00143 Non-detect

0.0014 Non-detect
Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

65.9 Non-detect 6.5 Non-detect

1650 790

4.77 5.99

1.61 1.2

0.0789 Non-detect 0.0631 Non-detect

15.400 14.7

0.129 Non-detect 0.103 Non-detect

0.380 Non-detect 0.0316 Non-detect

0.0436 Non-detect 0.0349 Non-detect

0.00465 Non-detect 0.00465 Non-detect

0.0120 Non-detect 0.0120 Non-detect

0.0225 Non-detect 0.0225 Non-detect

0.00239 Non-detect 0.00239 Non-detect

0.00232 Non-detect 0.00232 Non-detect

0.00545 Non-detect 0.00545 Non-detect

0.0165 Non-detect 0.0165 Non-detect

0.00287 Non-detect 0.00287 Non-detect

0.127 0.00625 Non-detect

0.00291 Non-detect 0.00291 Non-detect

0.0682 0.386

0.00580 Non-detect 0.00580 Non-detect

0.197 0.0362

0.0209 Non-detect 0.0209 Non-detect

0.0835 Non-detect 0.0835 Non-detect

01/19/13 01/20/13

01/22/13

13-021-0263

Estimated

Stripper Bottoms Wastewater Stripper Bottoms Wastewater

39.2

13-021-0264

01/22/13

Estimated

39.2

6

200 200

Suspension Suspension
0.00250 Non-detect 0.00250 Non-detect

0.00690 Non-detect 0.00690 Non-detect

0.00223 Non-detect 0.00223 Non-detect

0.00337 Non-detect 0.00337 Non-detect

NOT FOUND Non-detect NOT FOUND Non-detect

5.350 0.766

0.00358 Non-detect 0.00358 Non-detect

0.0036 Non-detect 0.0036 Non-detect
Note(s) Concentration 

(ppmw) Non-Detect? Note(s)

6.5 Non-detect

673

4.70

1.08

0.0657 Non-detect

24.0

0.107 Non-detect

0.0316 Non-detect

0.0364 Non-detect

0.00186 Non-detect

0.00480 Non-detect

0.00900 Non-detect

0.00095 Non-detect

0.00092 Non-detect

0.00218 Non-detect

0.00660 Non-detect

0.00115 Non-detect

0.0322

0.00116 Non-detect

Estimated value 0.0380

0.00232 Non-detect

Estimated value 0.107

0.00836 Non-detect

0.0334 Non-detect

Suspension

Estimated

200

01/21/13

7 8

Estimated

41

Stripper Bottoms Wastewater

13-021-0265

01/22/13
0.00099 Non-detect

0.00276 Non-detect

0.00089 Non-detect

0.00135 Non-detect

NOT FOUND Non-detect

1.250

0.00143 Non-detect

0.0014 Non-detect
Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

0.8 Estimated value/detected in blank 1.0

1250 910

32.4 2.42

4.37 0.381

0.0678 Non-detect 0.0678 Non-detect

21.5 19.7

0.111 Non-detect 0.111 Non-detect

0.319 Non-detect 0.306 Non-detect

0.0375 Non-detect 0.0375 Non-detect

0.00186 Non-detect 0.00092 Non-detect

0.00480 Non-detect 0.00240 Non-detect

0.00900 Non-detect 0.00450 Non-detect

0.00095 Non-detect 0.00047 Non-detect

0.00092 Non-detect 0.00046 Non-detect

0.00218 Non-detect 0.00109 Non-detect

0.00660 Non-detect 0.00330 Non-detect

0.00115 Non-detect 0.00335

0.0643 0.112

0.00116 Non-detect 0.00058 Non-detect

0.00560 Non-detect 0.406

0.00232 Non-detect 0.00116 Non-detect

0.144 0.259

0.00836 Non-detect 0.00418 Non-detect

0.0334 Non-detect 0.0167 Non-detect

Suspension

200 200

9

01/22/13 01/23/13

Suspension

01/25/13

37.4

Estimated Estimated

39.2

Stripper Bottoms Wastewater Stripper Bottoms Wastewater

13-024-0209 13-024-0210

01/25/13
0.00099 Non-detect 0.00049 Non-detect

0.00276 Non-detect 0.00044 Non-detect

0.00089 Non-detect 0.00138 Non-detect

0.00135 Non-detect 0.00067 Non-detect

NOT FOUND Non-detect NOT FOUND Non-detect

1.82 3.37

0.00143 Non-detect 0.00071 Non-detect

0.00115 Non-detect 0.0007 Non-detect
Note(s) Concentration 

(ppmw) Non-Detect? Note(s)

Detected in blank 10.4 Detected in blank

901

2.16

Estimated Value 0.223

0.0760 Non-detect

30.8

0.124 Non-detect

0.300 Non-detect

0.0420 Non-detect

0.00186 Non-detect

0.00240 Non-detect

0.00450 Non-detect

0.00095 Non-detect

0.00092 Non-detect

0.00218 Non-detect

0.00660 Non-detect

Estimated Value 0.00115 Non-detect

0.0358

0.00116 Non-detect

0.0382

0.00232 Non-detect

0.0859

0.0265 Estimated value

0.0334 Non-detect

01/24/13

Suspension

10 11

200

33.8

01/28/13

Estimated Estimated

Stripper Bottoms Wastewater

13-028-0205
0.00099 Non-detect

0.00276 Non-detect

0.00089 Non-detect

0.00135 Non-detect

NOT FOUND Non-detect

0.934

0.00143 Non-detect

0.0014 Non-detect
Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

19.7 Detected in blank 3.9

2210 2300

4.63 5.79

0.419 0.987

0.0686 Non-detect 0.0751 Non-detect

38.1 38.2

0.112 Non-detect 0.123 Non-detect

0.357 Non-detect 0.361 Non-detect

0.0379 Non-detect 0.0415 Non-detect

0.00186 Non-detect 0.00009 Non-detect

0.00480 Non-detect 0.00024 Non-detect

0.00900 Non-detect 0.00045 Non-detect

0.00095 Non-detect 0.00004 Non-detect

0.00092 Non-detect 0.00004 Non-detect

0.00412 Estimated value 0.00010 Non-detect

0.00660 Non-detect 0.00033 Non-detect

0.00115 Non-detect 0.00081

0.0694 0.0359

0.00116 Non-detect 0.00005 Non-detect

0.107 0.0369

0.00232 Non-detect 0.00011 Non-detect

0.218 0.123

0.0303 Estimated value 0.00041 Non-detect

0.0334 Non-detect 0.00167 Non-detect

01/25/13 01/26/13

Suspension Suspension

12

200

37.4 39.2

200

Estimated Estimated

13-028-0206 13-028-0301

01/28/13 01/29/13

Stripper Bottoms Wastewater Stripper Bottoms Wastewater
0.00099 Non-detect 0.00004 Non-detect

0.00276 Non-detect 0.00013 Non-detect

0.00089 Non-detect 0.00075

0.00135 Non-detect 0.0006 Non-detect

NOT FOUND Non-detect NOT FOUND Non-detect

1.59 1.01

0.00143 Non-detect 0.00007 Non-detect

0.0014 Non-detect 0.00007 Non-detect
Note(s) Concentration 

(ppmw) Non-Detect? Note(s)

Detected in blank 3.6 Detected in blank

1710

5.59

0.918

0.0631 Non-detect

39.9

0.103 Non-detect

0.345 Non-detect

0.0349 Non-detect

0.00009 Non-detect

0.00024 Non-detect

0.00045 Non-detect

0.00004 Non-detect

0.00004 Non-detect

0.00010 Non-detect

0.00033 Non-detect

Estimated value 0.00129

0.0755

0.00005 Non-detect

0.0521

0.00011 Non-detect

0.245

0.00041 Non-detect

0.00167 Non-detect

Suspension

13 14

01/27/13

200

33.8

Estimated Estimated

01/29/13

13-028-0302

Stripper Bottoms Wastewater
0.00004 Non-detect

0.00013 Non-detect

Estimated value 0.00128

0.00006 Non-detect

NOT FOUND Non-detect

1.54

0.00007 Non-detect

0.00007 Non-detect
Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

3.2 Detected in blank 0.6 Non-detect

1580 201

4.25 4.26

0.978 0.496

0.0742 Non-detect 0.0631 Non-detect

16.8 10.7

0.121 Non-detect 0.103 Non-detect

0.385 Non-detect 0.300 Non-detect

0.0411 Non-detect 0.0349 Non-detect

0.00009 Non-detect 0.00929 Non-detect

0.00024 Non-detect 0.0240 Non-detect

0.00045 Non-detect 0.0450 Non-detect

0.00004 Non-detect 0.00478 Non-detect

0.00004 Non-detect 0.00463 Non-detect

0.00010 Non-detect 0.0109 Non-detect

0.00033 Non-detect 0.0330 Non-detect

0.00157 0.00573 Non-detect

0.0609 0.0125 Non-detect

0.00005 Non-detect 0.00581 Non-detect

0.0448 0.0280 Non-detect

0.00011 Non-detect 0.0116 Non-detect

0.170 0.0538

0.00041 Non-detect 0.179

0.00167 Non-detect 0.167 Non-detect

Suspension Suspension

01/28/13 01/29/13

15

39.2

Estimated

200 200

41

Estimated

13-028-0303

Stripper Bottoms Wastewater Stripper Bottoms Wastewater

13-031-0227

01/29/13 02/01/13
0.00004 Non-detect 0.00499 Non-detect

0.00013 Non-detect 0.0138 Non-detect

0.00106 0.00445 Non-detect

0.00006 Non-detect 0.00674 Non-detect

NOT FOUND Non-detect NOT FOUND Non-detect

1.32 0.718

0.00007 Non-detect 0.00716 Non-detect

0.00007 Non-detect 0.0072 Non-detect
Note(s) Concentration 

(ppmw) Non-Detect? Note(s)

0.6 Non-detect

71.5

4.39

0.653

0.0701 Non-detect

14.4

0.115 Non-detect

0.333 Non-detect

0.0388 Non-detect

0.00186 Non-detect

0.00480 Non-detect

0.00900 Non-detect

0.00095 Non-detect

0.00092 Non-detect

0.00218 Non-detect

0.00660 Non-detect

0.00115 Non-detect

0.101

0.00116 Non-detect

0.0786

0.00232 Non-detect

Estimated value 0.250

Estimated value 0.0329 Estimated value

0.0334 Non-detect

Suspension

16 17

01/30/13

Estimated Estimated

200

02/01/13

Stripper Bottoms Wastewater

13-031-0228

37.4
0.00099 Non-detect

0.00276 Non-detect

0.00089 Non-detect

0.00135 Non-detect

NOT FOUND Non-detect

2.92

0.00143 Non-detect

0.0014 Non-detect
Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

0.6 Non-detect 0.6 Non-detect

97.0 175

3.28 6.59

1.29 1.15

0.0709 Non-detect 0.0678 Non-detect

22.4 28.0

0.116 Non-detect 0.111 Non-detect

0.361 Non-detect 0.357 Non-detect

0.0392 Non-detect 0.0375 Non-detect

0.00465 Non-detect 0.00465 Non-detect

0.0120 Non-detect 0.0120 Non-detect

0.0225 Non-detect 0.0225 Non-detect

0.00239 Non-detect 0.00239 Non-detect

0.00232 Non-detect 0.00232 Non-detect

0.00545 Non-detect 0.00545 Non-detect

0.0165 Non-detect 0.0165 Non-detect

0.00287 Non-detect 0.00287 Non-detect

0.0466 Estimated value 0.224

0.00291 Non-detect 0.00291 Non-detect

0.0798 0.235

0.00580 Non-detect 0.00580 Non-detect

0.141 0.396

0.0209 Non-detect 0.0209 Non-detect

0.0835 Non-detect 0.0835 Non-detect

Suspension Suspension

01/31/13 02/01/13

18

Estimated Estimated

200 200

02/04/13 02/04/13

Stripper Bottoms Wastewater Stripper Bottoms Wastewater

39.2

13-035-0213

37.4

13-035-0214
0.00250 Non-detect 0.00250 Non-detect

0.00690 Non-detect 0.00690 Non-detect

0.00223 Non-detect 0.00223 Non-detect

0.00337 Non-detect 0.00337 Non-detect

NOT FOUND Non-detect NOT FOUND Non-detect

1.26 3.00

0.00358 Non-detect 0.00358 Non-detect

0.0036 Non-detect 0.0036 Non-detect
Note(s) Concentration 

(ppmw) Non-Detect? Note(s)

0.6 Non-detect

116

3.50

0.912

0.0760 Non-detect

20.8

0.0124 Non-detect

0.349 Non-detect

0.0420 Non-detect

0.00465 Non-detect

0.0518

0.0225 Non-detect

0.00239 Non-detect

0.00232 Non-detect

0.00545 Non-detect

0.0165 Non-detect

0.00287 Non-detect

0.117

0.00291 Non-detect

0.0140 Non-detect

0.00580 Non-detect

0.305

0.0209 Non-detect

0.0835 Non-detect

02/02/13

Suspension

19 20

Estimated Estimated

200

39.2

02/06/13

13-035-0304

Stripper Bottoms Wastewater
0.00250 Non-detect

0.00690 Non-detect

0.00223 Non-detect

0.00337 Non-detect

NOT FOUND Non-detect

2.79

0.00358 Non-detect

0.00358 Non-detect
Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

0.6 Non-detect 0.6 Non-detect

216 120

3.63 4.02

1.16 1.22

0.0734 Non-detect 0.0779 Non-detect

20.4 26.6

0.120 Non-detect 0.127 Non-detect

0.357 Non-detect 0.437

0.0406 Non-detect 0.0431 Non-detect

0.00465 Non-detect 0.00465 Non-detect

0.0470 Estimated Value 0.0120 Non-detect

0.0225 Non-detect 0.0225 Non-detect

0.00239 Non-detect 0.00239 Non-detect

0.00232 Non-detect 0.00232 Non-detect

0.00545 Non-detect 0.00545 Non-detect

0.0165 Non-detect 0.0165 Non-detect

0.00287 Non-detect 0.00287 Non-detect

0.0957 0.0447

0.00291 Non-detect 0.00291 Non-detect

0.109 0.0705

0.00580 Non-detect 0.00580 Non-detect

0.211 0.111

0.0209 Non-detect 0.0209 Non-detect

0.0835 Non-detect 0.0835 Non-detect

02/03/13 02/04/13

Suspension

21

35.6

200

Estimated

02/06/13

Stripper Bottoms Wastewater

200

Suspension

Estimated

13-035-0305 13-035-0306

02/06/13

Stripper Bottoms Wastewater

37.4
0.00250 Non-detect 0.00250 Non-detect

0.00690 Non-detect 0.00690 Non-detect

0.00223 Non-detect 0.00223 Non-detect

0.00337 Non-detect 0.00337 Non-detect

NOT FOUND Non-detect NOT FOUND Non-detect

1.54 1.15

0.00358 Non-detect 0.00358 Non-detect

0.0036 Non-detect 0.0036 Non-detect
Note(s) Concentration 

(ppmw) Non-Detect? Note(s)

0.6 Non-detect

111

3.66

1.97

0.0657 Non-detect

18.3

0.107 Non-detect

Estimated value 0.333 Non-detect

0.0364 Non-detect

0.00092 Non-detect

0.00240 Non-detect

0.00450 Non-detect

0.00047 Non-detect

0.00046 Non-detect

0.0141

0.00330 Non-detect

0.00057 Non-detect

Estimated value 0.101

0.00058 Non-detect

0.00280 Non-detect

0.00116 Non-detect

0.385

0.00418 Non-detect

0.0167 Non-detect

22

02/05/13

Suspension

Estimated

13-038-0264

41

200

Estimated

02/08/13

Stripper Bottoms Wastewater

23
0.00049 Non-detect

0.00138 Non-detect

0.00044 Non-detect

0.00067 Non-detect

NOT FOUND Non-detect

1.68

0.00071 Non-detect

0.0007 Non-detect
Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

2.0 3.3

242 273

3.65 2.92

1.11 0.960

0.0725 Non-detect 0.0742 Non-detect

17.8 21.8

0.119 Non-detect 0.121 Non-detect

0.341 Non-detect 0.323 Non-detect

0.0401 Non-detect 0.0411 Non-detect

0.00465 Non-detect 0.00092 Non-detect

0.0120 Non-detect 0.00240 Non-detect

0.0225 Non-detect 0.00450 Non-detect

0.00239 Non-detect 0.00047 Non-detect

0.00232 Non-detect 0.00046 Non-detect

0.00545 Non-detect 0.00109 Non-detect

0.0165 Non-detect 0.00330 Non-detect

0.00287 Non-detect 0.00057 Non-detect

0.191 0.0453

0.00291 Non-detect 0.00394

0.132 0.0467

0.00580 Non-detect 0.00116 Non-detect

0.449 0.124

0.0209 Non-detect 0.00418 Non-detect

0.0835 Non-detect 0.0167 Non-detect

02/06/13 02/07/13

Suspension Suspension

200 200

Estimated

13-042-0203

39.2. 39.2

02/08/13

Estimated

02/12/13

Stripper Bottoms Wastewater

13-038-0265

Stripper Bottoms Wastewater

24
0.00250 Non-detect 0.00049 Non-detect

0.00690 Non-detect 0.00138 Non-detect

0.0223 Non-detect 0.00044 Non-detect

0.00337 Non-detect 0.00067 Non-detect

NOT FOUND Non-detect NOT FOUND Non-detect

3.11 0.976

0.00358 Non-detect 0.00071 Non-detect

0.0036 Non-detect 0.0007 Non-detect
Note(s) Concentration 

(ppmw) Non-Detect? Note(s)

Detected in blank 0.6 Non-detect

149

3.47

1.25

0.077 Non-detect

23.4

0.126 Non-detect

0.390 Non-detect

0.0426 Non-detect

0.00092 Non-detect

0.00240 Non-detect

0.00450 Non-detect

0.00047 Non-detect

0.00046 Non-detect

0.00109 Non-detect

0.00330 Non-detect

0.00057 Non-detect

0.11

Estimated value; detected in blank 0.00269 Estimated value; detected in blank

0.0684

0.00116 Non-detect

0.230

0.00418 Non-detect

0.0167 Non-detect

Estimated

Stripper Bottoms Wastewater

25 26

37.4

02/12/13

Suspension

200

02/08/13

13-042-0204

Estimated
0.00049 Non-detect

0.00138 Non-detect

0.00044 Non-detect

0.00067 Non-detect

NOT FOUND Non-detect

2.95

0.00071 Non-detect

0.0007 Non-detect
Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

0.6 Non-detect 0.6 Non-detect

153 162

4.34 4.82

0.775 0.798

0.0760 Non-detect 0.0631 Non-detect

21.8 37

0.124 Non-detect 0.103 Non-detect

0.323 Non-detect 0.323 Non-detect

0.0420 Non-detect 0.0349 Non-detect

0.00092 Non-detect 0.00465 Non-detect

0.00240 Non-detect 0.0120 Non-detect

0.00450 Non-detect 0.02250 Non-detect

0.00047 Non-detect 0.00239 Non-detect

0.00046 Non-detect 0.00232 Non-detect

0.00109 Non-detect 0.00545 Non-detect

0.00330 Non-detect 0.01650 Non-detect

0.00057 Non-detect 0.00287 Non-detect

0.0182 0.0516

0.00058 Non-detect 0.00291 Non-detect

0.0155 0.124

0.00116 Non-detect 0.00580

0.0299 0.112

0.00418 Non-detect 0.0938

0.0167 Non-detect 0.0835 Non-detect

Stripper Bottoms Wastewater Stripper Bottoms Wastewater

27

02/13/13

Estimated

200

02/09/13

Suspension Suspension

02/13/13

41 39.2

13-042-0292 13-042-0293

Estimated

200

02/10/13
0.00049 Non-detect 0.00250 Non-detect

0.00138 Non-detect 0.00690 Non-detect

0.00044 Non-detect 0.00223 Non-detect

0.00067 Non-detect 0.00337 Non-detect

NOT FOUND Non-detect NOT FOUND Non-detect

0.406 1.12

0.00071 Non-detect 0.00906

0.0007 Non-detect 0.0007 Non-detect
Note(s) Concentration 

(ppmw) Non-Detect? Note(s)

0.6 Non-detect

169

4.11

1.69

0.0686 Non-detect

29.5

0.112 Non-detect

0.333 Non-detect

0.0379 Non-detect

0.00465 Non-detect

0.0120 Non-detect

0.0225 Non-detect

0.00239 Non-detect

0.00232 Non-detect

0.00545 Non-detect

0.0165 Non-detect

0.00287 Non-detect

0.0654

0.00291 Non-detect

0.0900

Estimated value 0.00580 Non-detect

0.139

Estimated value 0.0822 Estimated value

0.0835 Non-detect

Stripper Bottoms Wastewater

02/13/13

Suspension

Estimated

28

13-042-0294

39.2

Estimated

200

02/11/13

29
0.00250 Non-detect

0.00690 Non-detect

0.00223 Non-detect

0.00337 Non-detect

NOT FOUND Non-detect

1.08

Estimated value 0.00358 Non-detect

0.0036 Non-detect
Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

0.6 Non-detect

117

3.75

0.973

0.0686 Non-detect

27.3

0.112 Non-detect

0.337 Non-detect

0.0379 Non-detect

0.00465 Non-detect

0.0120 Non-detect

0.0225 Non-detect

0.00239 Non-detect

0.00232 Non-detect

0.00545 Non-detect

0.0165 Non-detect

0.00287 Non-detect

0.00625 Non-detect

0.00291 Non-detect

0.0535

0.00580 Non-detect

0.0604

0.0209 Non-detect

0.0835 Non-detect

Stripper Bottoms Wastewater

Suspension

02/12/13

37.4

02/18/13

Estimated

13-044-0236

200

30
0.00250 Non-detect

0.00690 Non-detect

0.00223 Non-detect

0.00337 Non-detect

NOT FOUND Non-detect

0.391

0.00358 Non-detect

0.0036 Non-detect
Note(s) Concentration 

(ppmw) Non-Detect? Note(s)

31 32

Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

33

Note(s) Concentration 

(ppmw) Non-Detect? Note(s)

34 35

Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

36

Note(s) Concentration 

(ppmw) Non-Detect? Note(s)

37 38

Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

39

Note(s) Concentration 

(ppmw) Non-Detect? Note(s)

40 41

Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

42

Note(s) Concentration 

(ppmw) Non-Detect? Note(s)

43 44

Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

45

Note(s) Concentration 

(ppmw) Non-Detect? Note(s)

46 47

Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

48

Note(s) Concentration 

(ppmw) Non-Detect? Note(s)

49 50

Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

51

Note(s) Concentration 

(ppmw) Non-Detect? Note(s)

52 53

Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

54

Note(s) Concentration 

(ppmw) Non-Detect? Note(s)

55 56

Concentration 

(ppmw) Non-Detect? Note(s) Concentration (ppmw) Non-Detect?

57

Note(s) Concentration 

(ppmw) Non-Detect? Note(s)

58 59

Concentration 

(ppmw) Non-Detect? Note(s)

60