Instructions for completing the Fuel Material Analysis Inform

This Information Collection Request (ICR) spreadsheet is intended to collect information ab

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluo r antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. T
be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analy s number of analyses would coincide with one boiler where emissions testing for all 4 HAP

Data for multiple boilers should be handled by using separate spreadsheets. Fields that a required fields. Green highlighted cells should be filled using the drop

‐ down boxes, includ e filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boil e
2. Please enter the test date on the Boiler Information worksheet.

3. Please choose the type of fuel being sampled using the drop

‐ down in the fuel column of

worksheet. If you choose "other", please provide a description of the fuel in the Other Fue l

4. Please provide the analysis method for each constituent in the Analysis Methods works h

04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist works

measure that you plan to report are not found in the Units of measure table, please fill the m highlighted, cell in each table. This allows you to choose the units of measure in the Fuels S

6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orang

7 P id th S l N b d S l D t th F l S l R lt kh t Y Instructions for completing the Fuel Material Analysis Inform

This Information Collection Request (ICR) spreadsheet is intended to collect information ab

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluo r antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. T
be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analy s number of analyses would coincide with one boiler where emissions testing for all 4 HAP

Data for multiple boilers should be handled by using separate spreadsheets. Fields that a required fields. Green highlighted cells should be filled using the drop

‐ down boxes, includ e filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boil e
2. Please enter the test date on the Boiler Information worksheet.

3. Please choose the type of fuel being sampled using the drop

‐ down in the fuel column of

worksheet. If you choose "other", please provide a description of the fuel in the Other Fue l

4. Please provide the analysis method for each constituent in the Analysis Methods works h

04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist works

measure that you plan to report are not found in the Units of measure table, please fill the m highlighted, cell in each table. This allows you to choose the units of measure in the Fuels S

6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orang

7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. Y o composite samples consisting of 3 combined grab samples each, but you are not limited to

more.
8. Provide the results of the analyses for each constituent requested. Use the drop

‐ down b

measure.m ation

b out chemical analyses of fuels

rine, and metals, such as This spreadsheet is intended to

ses at that specific boiler. This
surrogates were being tested.

a re highlighted in yellow are

e d. Gray fields are automatically

e r Information worksheet.

f the Boiler Information

l Description column.

h eet. For example: "ASTM D5865

‐

s heet (orange tab). If the units of

m in the blank, orange
S ample Results worksheet.

g e highlighted cell).

t id i i f 3 m ation

b out chemical analyses of fuels

rine, and metals, such as This spreadsheet is intended to

ses at that specific boiler. This
surrogates were being tested.

a re highlighted in yellow are

e d. Gray fields are automatically

e r Information worksheet.

f the Boiler Information

l Description column.

h eet. For example: "ASTM D5865

‐

s heet (orange tab). If the units of

m in the blank, orange
S ample Results worksheet.

g e highlighted cell).

ou must provide a minimum of 3
that number if you have collected

b oxes to fill in the units ofEIA Facility Code Facility Name Boiler ID Fuel Type 1

860 Duck Creek 1 subbituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA Facility Code Facility Name Boiler ID Basis Analyte

860 Duck Creek 1 As Received Higher Heating Value

860 Duck Creek 1 As Received % Moisture

860 Duck Creek 1 As Received % Ash

860 Duck Creek 1 As Received % Sulfur

860 Duck Creek 1 Dry basis Higher Heating Value

860 Duck Creek 1 Dry basis % Ash

860 Duck Creek 1 Dry basis % Sulfur

860 Duck Creek 1 Dry basis Antimony

860 Duck Creek 1 Dry basis Arsenic

860 Duck Creek 1 Dry basis Beryllium

860 Duck Creek 1 Dry basis Cadmium

860 Duck Creek 1 Dry basis Chlorine

860 Duck Creek 1 Dry basis Chromium

860 Duck Creek 1 Dry basis Cobalt

860 Duck Creek 1 Dry basis Fluorine

860 Duck Creek 1 Dry basis Lead

860 Duck Creek 1 Dry basis Manganese

860 Duck Creek 1 Dry basis Mercury

860 Duck Creek 1 Dry basis Nickel

860 Duck Creek 1 Dry basis SeleniumA na l ys i s M e th o d f or eac h A na l y t e (example: ASTM D5865-04)

ASTM D5865

ASTM D5142

ASTM D5142

ASTM D4239

ASTM D5865

ASTM D5142

ASTM D5142

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D6722

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357EIA Facility Code Facility Name Boiler ID HAPs Test Group

860 Duck Creek 1 Mercury and non

‐ mercury metalic HA P

Sample Number (minimum of 3

composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units

Run 1 06/08/2010 06/08/2010 9131.06

Run 2 06/09/2010 06/09/2010 9145.17

Run 3 06/10/2010 06/10/2010 9156.45 Fuel Testing ResultsP s

% Moisture (as received) % Ash (as received) % Sulfur (as received) Higher Heating Value (HHV) (Dry Basis) HHV Units % Ash (Dry Basis) % Sulfur (Dry Basis) 25.29 6.36 1.24 12222.00 Btu/lb 8.51 1.66 24.32 6.55 1.26 12084.00 Btu/lb 8.65 1.66 24.57 7.01 1.37 12139.00 Btu/lb 9.29 1.82Chlorine (Dry Basis) Chlorine

Units Mercury (Dry Basis) Mercury

Units Antimony (Dry Basis) Antimony

Units A rsenic (Dry Basis) Arsenic

Units Beryllium (Dry Basis)

0.0274 % 0.056 μ g/g 0.184 μ g/g 1.08 μ g/g 0.592

0.0265 % 0.047 μ g/g 0.182 μ g/g 1.18 μ g/g 0.533

0.0262 % 0.043 μ g/g 0.193 μ g/g 1.11 μ g/g 0.573Beryllium

Units Cadmium (Dry Basis) Cadmium

Units Chromium (Dry Basis) Chromium

Units Lead (Dry Basis) Lead Units Manganese (Dry Basis) Manganese

Units

μ g/g 0.0969 μ g/g 6.92 μ g/g 6.07 μ g/g 18.50 μ g/g

μ g/g 0.1340 μ g/g 6.58 μ g/g 2.79 μ g/g 19.10 μ g/g

μ g/g 0.1120 μ g/g 6.82 μ g/g 2.20 μ g/g 19.40 μ g/gNickel (Dry Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry Basis) Cobalt Units Total Moisture

6.57 μ g/g [<1] μ g/g 55 μ g/g 1.82 μ g/g 25.29

5.47 μ g/g [<1] μ g/g 57 μ g/g 1.86 μ g/g 24.32

5.70 μ g/g [<1] μ g/g 59.3 μ g/g 1.90 μ g/g 24.57 P rNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

42.9 8.51 48.59 69.96 4.8 1.16 1.66

42.66 8.65 48.69 68.76 4.78 1.11 1.66

42.62 9.29 48.09 69.33 4.77 1.13 1.82 r oximate Analyses, % by w t Ultimate Analyses, % by wtOxygen

13.88

15.01

13.63EIA Facility Code Facility Name Boiler ID HAPs Test Group

860 Duck Creek 1 Acid gas HAPs

Sample Number (minimum of 3

composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units

Run 1 06/08/2010 06/08/2010 9131.06 Btu/lb

Run 2 06/09/2010 06/09/2010 9145.17 Btu/lb

Run 3 06/10/2010 06/10/2010 9156.45 Btu/lb Fuel Testing Results% Moisture (as received) % Ash (as received) % Sulfur (as received) Higher Heating Value (HHV) (Dry Basis) HHV Units % Ash (Dry Basis) % Sulfur (Dry Basis) 25.29 6.36 1.24 12222.00 Btu/lb 8.51 1.66 24.32 6.55 1.26 12084.00 Btu/lb 8.65 1.66 24.57 7.01 1.37 12139.00 Btu/lb 9.29 1.82Chlorine (Dry Basis) Chlorine

Units Mercury (Dry Basis) Mercury
Units Antimony (Dry Basis) Antimony
Units A rsenic (Dry Basis) Arsenic
Units Beryllium (Dry Basis) Beryllium
Units

0.0274 % 0.056 μ g/g 0.184 μ g/g 1.08 μ g/g 0.592 μ g/g

0.0265 % 0.047 μ g/g 0.182 μ g/g 1.18 μ g/g 0.533 μ g/g

0.0262 % 0.043 μ g/g 0.193 μ g/g 1.11 μ g/g 0.573 μ g/gCadmium (Dry Basis) Cadmium

Units Chromium (Dry Basis) Chromium

Units Lead (Dry Basis) Lead Units Manganese (Dry Basis) Manganese
Units Nickel (Dry Basis) Nickel Units

0.0969 μ g/g 6.92 μ g/g 6.07 μ g/g 18.50 μ g/g 6.57 μ g/g

0.1340 μ g/g 6.58 μ g/g 2.79 μ g/g 19.10 μ g/g 5.47 μ g/g

0.1120 μ g/g 6.82 μ g/g 2.20 μ g/g 19.40 μ g/g 5.70 μ g/gNote the P

Selenium (Dry Basis) Selenium

Units Fluorine (Dry Basis) Fluorine
Units Cobalt (Dry Basis) Cobalt Units Total Moisture Volatiles [<1] μ g/g 55 μ g/g 1.82 μ g/g 25.29 42.9
[<1] μ g/g 57 μ g/g 1.86 μ g/g 24.32 42.66
[<1] μ g/g 59.3 μ g/g 1.90 μ g/g 24.57 42.62 Proximate Analyses, %roximate/Ultimate data below should be recorded on a dry basis (including ash).

Ash Fixed Carbo n Carbon Hydrogen Nitrogen Total Sulfur Oxygen

8.51 48.59 69.96 4.8 1.16 1.66 13.88

8.65 48.69 68.76 4.78 1.11 1.66 15.01

9.29 48.09 69.33 4.77 1.13 1.82 13.63 % by w t Ultimate Analyses, % by wtEIA Facility Code Facility Name Boiler ID HAPs Test Group

860 Duck Creek 1

Sample Number (minimum of 3

composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture (as received) % Ash (as received) % Sulfur (as received) Higher Heating Value (HHV) (Dry Basis) HHV Units % Ash (Dry Basis) % Sulfur (Dry Basis)Chlorine (Dry Basis) Chlorine

Units Mercury (Dry Basis) Mercury
Units Antimony (Dry Basis) Antimony
Units A rsenic (Dry Basis) Arsenic
Units Beryllium (Dry Basis) Beryllium
UnitsCadmium (Dry Basis) Cadmium

Units Chromium (Dry Basis) Chromium

Units Lead (Dry Basis) Lead Units Manganese (Dry Basis) Manganese
Units Nickel (Dry Basis) Nickel UnitsNote the Proximate/U

Selenium (Dry Basis) Selenium

Units Fluorine (Dry Basis) Fluorine
Units Cobalt (Dry Basis) Cobalt Units Total Moisture Volatiles Ash Proximate Analyses, % by wtltimate data below should be recorded on a dry basis (including ash).

Fixed Carbo n Carbon Hydrogen Nitrogen Total Sulfur Oxygen Ultimate Analyses, % by wtEIA Facility Code Facility Name Boiler ID HAPs Test Group

860 Duck Creek 1

Sample Number Fuel Testing Results

(minimum of 3

composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV UnitsHigher
% Moisture (as received) % Ash (as received) % Sulfur (as received) Heating Value (HHV) (Dry Basis) HHV Units % Ash (Dry Basis) % Sulfur (Dry Basis)Chlorine (Dry Basis) Chlorine

Units Mercury (Dry Basis) Mercury
Units Antimony (Dry Basis) Antimony
Units A rsenic (Dry Basis) Arsenic
Units Beryllium (Dry Basis) Beryllium
UnitsCadmium (Dry Basis) Cadmium

Units Chromium (Dry Basis) Chromium

Units Lead (Dry Basis) Lead Units Manganese (Dry Basis) Manganese
Units Nickel (Dry Basis) Nickel UnitsNote the Proximate/U

Proximate Analyses, % by w

Selenium (Dry Basis) Selenium

Units Fluorine (Dry Basis) Fluorine
Units Cobalt (Dry Basis) Cobalt Units Total Moisture Volatiles Ashltimate data below should be recorded on a dry basis (including ash).

wt Ultimate Analyses, % by wt

Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur OxygenUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measu

Fuel Units of Measure - HHV
anthracite Btu/lb bituminous Btu/gallon
subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μ g/g
othe r mg/Kgre to the orange hightlighted cell, if necessary.

Units of Measure - Cl, Fl
%

ppm