Instructionsfor completing the Fuel Material AnalysisInform

This Information Collection Request (ICR) spreadsheet is intended to collect information ab

used fossil fuel burning power plants.  Constituents of concern are:  mercury, chlorine, fluor

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium.  T

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analys

number of analyses would coincide with one boiler where emissions testing for all 4 HAP

Data for multiple boilers should be handled by using separate spreadsheets.   Fields that a

required fields.  Green highlighted cells should be filled using the drop‐down boxes, include

filled from other fields.

Please name each resulting spreadsheet with the following naming convention:   

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls  (example:  8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1.  Please enter the  EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boile

2.  Please enter the test date on the Boiler Information worksheet.

3.  Please choose the type of fuel being sampled using the drop‐down in the fuel column of

worksheet.  If you choose "other", please provide a description of the fuel in the Other Fuel

4.  Please provide the analysis method for each constituent in the Analysis Methods worksh

04".

5.  Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist works

measure that you plan to report are not found in the Units of measure table, please fill them

highlighted, cell in each table.  This allows you to choose the units of measure in the Fuels S

6.  Select the HAPs Test Group (i.e., HAP surrogate)  for which the tab's data reflects (orang

7 P id th S l N b d S l D t th F l S l R lt kh t Y

Instructionsfor completing the Fuel Material AnalysisInform

This Information Collection Request (ICR) spreadsheet is intended to collect information ab

used fossil fuel burning power plants.  Constituents of concern are:  mercury, chlorine, fluor

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium.  T

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analys

number of analyses would coincide with one boiler where emissions testing for all 4 HAP

Data for multiple boilers should be handled by using separate spreadsheets.   Fields that a

required fields.  Green highlighted cells should be filled using the drop‐down boxes, include

filled from other fields.

Please name each resulting spreadsheet with the following naming convention:   

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls  (example:  8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1.  Please enter the  EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boile

2.  Please enter the test date on the Boiler Information worksheet.

3.  Please choose the type of fuel being sampled using the drop‐down in the fuel column of

worksheet.  If you choose "other", please provide a description of the fuel in the Other Fuel

4.  Please provide the analysis method for each constituent in the Analysis Methods worksh

04".

5.  Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist works

measure that you plan to report are not found in the Units of measure table, please fill them

highlighted, cell in each table.  This allows you to choose the units of measure in the Fuels S

6.  Select the HAPs Test Group (i.e., HAP surrogate)  for which the tab's data reflects (orang

7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet.  Yo

composite samples consisting of 3 combined grab samples each, but you are not limited to

more.

8.  Provide the results of the analyses for each constituent requested.  Use the drop‐down b

measure.
mation

bout chemical analyses of fuels

rine, and metals, such as

This spreadsheet is intended to

ses at that specific boiler.  This

surrogates were being tested.

are highlighted in yellow are

ed.   Gray fields are automatically

er Information worksheet.

f the Boiler Information

l Description column.

heet.  For example:  "ASTM D5865‐

sheet (orange tab).  If the units of

m in the blank, orange

Sample Results worksheet.

ge highlighted cell).

t id i i f 3

mation

bout chemical analyses of fuels

rine, and metals, such as

This spreadsheet is intended to

ses at that specific boiler.  This

surrogates were being tested.

are highlighted in yellow are

ed.   Gray fields are automatically

er Information worksheet.

f the Boiler Information

l Description column.

heet.  For example:  "ASTM D5865‐

sheet (orange tab).  If the units of

m in the blank, orange

Sample Results worksheet.

ge highlighted cell).

ou must provide a minimum of 3

that number if you have collected

boxes to fill in the units of
EIA Facility Code Facility Name Boiler ID Fuel Type 1

860 Duck Creek 1 subbituminous
Fuel Type 2 Fuel Type 3 Other Fuel Description
EIA Facility Code Facility Name Boiler ID Basis Analyte

860 Duck Creek 1 As Received Higher Heating Value

860 Duck Creek 1 As Received % Moisture

860 Duck Creek 1 As Received % Ash

860 Duck Creek 1 As Received % Sulfur

860 Duck Creek 1 Dry basis Higher Heating Value

860 Duck Creek 1 Dry basis % Ash

860 Duck Creek 1 Dry basis % Sulfur

860 Duck Creek 1 Dry basis Antimony

860 Duck Creek 1 Dry basis Arsenic

860 Duck Creek 1 Dry basis Beryllium

860 Duck Creek 1 Dry basis Cadmium

860 Duck Creek 1 Dry basis Chlorine

860 Duck Creek 1 Dry basis Chromium

860 Duck Creek 1 Dry basis Cobalt

860 Duck Creek 1 Dry basis Fluorine

860 Duck Creek 1 Dry basis Lead

860 Duck Creek 1 Dry basis Manganese

860 Duck Creek 1 Dry basis Mercury

860 Duck Creek 1 Dry basis Nickel

860 Duck Creek 1 Dry basis Selenium
Analysis Method for each Analyte 

(example: ASTM D5865-04)

ASTM D5865

ASTM D5142

ASTM D5142

ASTM D4239

ASTM D5865

ASTM D5142

ASTM D5142

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D6722

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357
EIA Facility Code Facility Name Boiler ID HAPs Test Group

860 Duck Creek 1 Mercury and non‐mercury metalic HAP

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating Value 

(HHV)

(as received) HHV Units

Run 1 06/08/2010 06/08/2010 9131.06

Run 2 06/09/2010 06/09/2010 9145.17

Run 3 06/10/2010 06/10/2010 9156.45

 Fuel Testing Results
Ps

% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

25.29 6.36 1.24 12222.00 Btu/lb 8.51 1.66

24.32 6.55 1.26 12084.00 Btu/lb 8.65 1.66

24.57 7.01 1.37 12139.00 Btu/lb 9.29 1.82
Chlorine

(Dry Basis)

Chlorine 

Units

Mercury 

(Dry Basis)

Mercury 

Units

Antimony 

(Dry Basis)

Antimony 

Units

Arsenic (Dry 

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

0.0274 % 0.056 μg/g 0.184 μg/g 1.08 μg/g 0.592

0.0265 % 0.047 μg/g 0.182 μg/g 1.18 μg/g 0.533

0.0262 % 0.043 μg/g 0.193 μg/g 1.11 μg/g 0.573
Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry 

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

μg/g 0.0969 μg/g 6.92 μg/g 6.07 μg/g 18.50 μg/g

μg/g 0.1340 μg/g 6.58 μg/g 2.79 μg/g 19.10 μg/g

μg/g 0.1120 μg/g 6.82 μg/g 2.20 μg/g 19.40 μg/g
Nickel (Dry 

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry 

Basis) Cobalt Units Total Moisture

6.57 μg/g [<1] μg/g 55 μg/g 1.82 μg/g 25.29

5.47 μg/g [<1] μg/g 57 μg/g 1.86 μg/g 24.32

5.70 μg/g [<1] μg/g 59.3 μg/g 1.90 μg/g 24.57

Pr
Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

42.9 8.51 48.59 69.96 4.8 1.16 1.66

42.66 8.65 48.69 68.76 4.78 1.11 1.66

42.62 9.29 48.09 69.33 4.77 1.13 1.82

roximate Analyses, % by wt Ultimate Analyses, % by wt
Oxygen

13.88

15.01

13.63
EIA Facility Code Facility Name Boiler ID HAPs Test Group

860 Duck Creek 1 Acid gas HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

Run 1 06/08/2010 06/08/2010 9131.06 Btu/lb

Run 2 06/09/2010 06/09/2010 9145.17 Btu/lb

Run 3 06/10/2010 06/10/2010 9156.45 Btu/lb

 Fuel Testing Results
% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

25.29 6.36 1.24 12222.00 Btu/lb 8.51 1.66

24.32 6.55 1.26 12084.00 Btu/lb 8.65 1.66

24.57 7.01 1.37 12139.00 Btu/lb 9.29 1.82
Chlorine

(Dry Basis)

Chlorine 

Units

Mercury 

(Dry Basis)

Mercury 

Units

Antimony 

(Dry Basis)

Antimony 

Units

Arsenic (Dry 

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

0.0274 % 0.056 μg/g 0.184 μg/g 1.08 μg/g 0.592 μg/g

0.0265 % 0.047 μg/g 0.182 μg/g 1.18 μg/g 0.533 μg/g

0.0262 % 0.043 μg/g 0.193 μg/g 1.11 μg/g 0.573 μg/g
Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry 

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry 

Basis) Nickel Units

0.0969 μg/g 6.92 μg/g 6.07 μg/g 18.50 μg/g 6.57 μg/g

0.1340 μg/g 6.58 μg/g 2.79 μg/g 19.10 μg/g 5.47 μg/g

0.1120 μg/g 6.82 μg/g 2.20 μg/g 19.40 μg/g 5.70 μg/g
Note the P

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry 

Basis) Cobalt Units Total Moisture Volatiles

[<1] μg/g 55 μg/g 1.82 μg/g 25.29 42.9

[<1] μg/g 57 μg/g 1.86 μg/g 24.32 42.66

[<1] μg/g 59.3 μg/g 1.90 μg/g 24.57 42.62

Proximate Analyses, %
roximate/Ultimate data below should be recorded on a dry basis (including ash).

Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

8.51 48.59 69.96 4.8 1.16 1.66 13.88

8.65 48.69 68.76 4.78 1.11 1.66 15.01

9.29 48.09 69.33 4.77 1.13 1.82 13.63

% by wt Ultimate Analyses, % by wt
EIA Facility Code Facility Name Boiler ID HAPs Test Group

860 Duck Creek 1

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher 

Heating 

Value (HHV)

(as 

received) HHV Units

 Fuel Testing Results
% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)
Chlorine

(Dry Basis)

Chlorine 

Units

Mercury 

(Dry Basis)

Mercury 

Units

Antimony 

(Dry Basis)

Antimony 

Units

Arsenic (Dry 

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units
Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry 

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry 

Basis) Nickel Units
Note the Proximate/U

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry 

Basis) Cobalt Units Total Moisture Volatiles Ash

Proximate Analyses, % by wt
ltimate data below should be recorded on a dry basis (including ash).

Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

Ultimate Analyses, % by wt
EIA Facility Code Facility Name Boiler ID HAPs Test Group

860 Duck Creek 1

Sample Number 

 Fuel Testing Results

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units
Higher 

% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)
Chlorine

(Dry Basis)

Chlorine 

Units

Mercury 

(Dry Basis)

Mercury 

Units

Antimony 

(Dry Basis)

Antimony 

Units

Arsenic (Dry 

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units
Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry 

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry 

Basis) Nickel Units
Note the Proximate/U

Proximate Analyses, % by w

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry 

Basis) Cobalt Units Total Moisture Volatiles Ash
ltimate data below should be recorded on a dry basis (including ash).

wt Ultimate Analyses, % by wt

Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen
Units of Measure Tables: Please do not modify these tables, except to add your own unit of measu

Fuel Units of Measure - HHV

anthracite Btu/lb

bituminous Btu/gallon

subbituminous

lignite

coal refuse (culm or gob)

No.2 Fuel Oil (distillate)

No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals

synfuel mg/g

petroleum coke μg/g

other mg/Kg
re to the orange hightlighted cell, if necessary.

Units of Measure - Cl, Fl

%

ppm