InstructionsforcompletingtheFuelMaterialAnalysisInformationThisInformationCollectionRequest(ICR)spreadsheetisintendedtocollectinformationaboutchemicalanalysesoffuelsusedfossilfuelburningpowerplants.Constituentsofconcernare:mercury,chlorine,fluorine,andmetals,suchasantimony,beryllium,cadmium,chromium,cobalt,lead,manganese,nickel,andselenium.ThisspreadsheetisintendedtoInstructionsforcompletingtheFuelMaterialAnalysisInformationThisInformationCollectionRequest(ICR)spreadsheetisintendedtocollectinformationaboutchemicalanalysesoffuelsusedfossilfuelburningpowerplants.Constituentsofconcernare:mercury,chlorine,fluorine,andmetals,suchasantimony,beryllium,cadmium,chromium,cobalt,lead,manganese,nickel,andselenium.Thisspreadsheetisintendedtobeusedforoneboilerofonefacilitybutisdesignedtoallowmultiple(upto4)fuelanalysesatthatspecificboiler.Thisnumberofanalyseswouldcoincidewithoneboilerwhereemissionstestingforall4HAPsurrogateswerebeingtested.Dataformultipleboilersshouldbehandledbyusingseparatespreadsheets.Fieldsthatarehighlightedinyellowarerequiredfields.Greenhighlightedcellsshouldbefilledusingthedrop‐downboxes,included.Grayfieldsareautomaticallyfilledfromotherfields.InstructionsforcompletingtheFuelMaterialAnalysisInformationThisInformationCollectionRequest(ICR)spreadsheetisintendedtocollectinformationaboutchemicalanalysesoffuelsusedfossilfuelburningpowerplants.Constituentsofconcernare:mercury,chlorine,fluorine,andmetals,suchasantimony,beryllium,cadmium,chromium,cobalt,lead,manganese,nickel,andselenium.Thisspreadsheetisintendedtobeusedforoneboilerofonefacilitybutisdesignedtoallowmultiple(upto4)fuelanalysesatthatspecificboiler.Thisnumberofanalyseswouldcoincidewithoneboilerwhereemissionstestingforall4HAPsurrogateswerebeingtested.Dataformultipleboilersshouldbehandledbyusingseparatespreadsheets.Fieldsthatarehighlightedinyellowarerequiredfields.Greenhighlightedcellsshouldbefilledusingthedrop‐downboxes,included.Grayfieldsareautomaticallyfilledfromotherfields.Pleasenameeachresultingspreadsheetwiththefollowingnamingconvention:[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls(example:8100_Unit_2_Fuels_Testing.xls).Pleaserefertothefollowingstepswhenusingthesespreadsheets.InstructionsforcompletingtheFuelMaterialAnalysisInformationThisInformationCollectionRequest(ICR)spreadsheetisintendedtocollectinformationaboutchemicalanalysesoffuelsusedfossilfuelburningpowerplants.Constituentsofconcernare:mercury,chlorine,fluorine,andmetals,suchasantimony,beryllium,cadmium,chromium,cobalt,lead,manganese,nickel,andselenium.Thisspreadsheetisintendedtobeusedforoneboilerofonefacilitybutisdesignedtoallowmultiple(upto4)fuelanalysesatthatspecificboiler.Thisnumberofanalyseswouldcoincidewithoneboilerwhereemissionstestingforall4HAPsurrogateswerebeingtested.Dataformultipleboilersshouldbehandledbyusingseparatespreadsheets.Fieldsthatarehighlightedinyellowarerequiredfields.Greenhighlightedcellsshouldbefilledusingthedrop‐downboxes,included.Grayfieldsareautomaticallyfilledfromotherfields.Pleasenameeachresultingspreadsheetwiththefollowingnamingconvention:[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls(example:8100_Unit_2_Fuels_Testing.xls).Pleaserefertothefollowingstepswhenusingthesespreadsheets.1.PleaseentertheEIAFacilityCode,FacilityNameandBoilerIDofyourboilerontheBoilerInformationworksheet.2.PleaseenterthetestdateontheBoilerInformationworksheet.3.Pleasechoosethetypeoffuelbeingsampledusingthedrop‐downinthefuelcolumnoftheBoilerInformationworksheetIfyouchoose"other"pleaseprovideadescriptionofthefuelintheOtherFuelDescriptioncolumnInstructionsforcompletingtheFuelMaterialAnalysisInformationThisInformationCollectionRequest(ICR)spreadsheetisintendedtocollectinformationaboutchemicalanalysesoffuelsusedfossilfuelburningpowerplants.Constituentsofconcernare:mercury,chlorine,fluorine,andmetals,suchasantimony,beryllium,cadmium,chromium,cobalt,lead,manganese,nickel,andselenium.Thisspreadsheetisintendedtobeusedforoneboilerofonefacilitybutisdesignedtoallowmultiple(upto4)fuelanalysesatthatspecificboiler.Thisnumberofanalyseswouldcoincidewithoneboilerwhereemissionstestingforall4HAPsurrogateswerebeingtested.Dataformultipleboilersshouldbehandledbyusingseparatespreadsheets.Fieldsthatarehighlightedinyellowarerequiredfields.Greenhighlightedcellsshouldbefilledusingthedrop‐downboxes,included.Grayfieldsareautomaticallyfilledfromotherfields.Pleasenameeachresultingspreadsheetwiththefollowingnamingconvention:[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls(example:8100_Unit_2_Fuels_Testing.xls).Pleaserefertothefollowingstepswhenusingthesespreadsheets.1.PleaseentertheEIAFacilityCode,FacilityNameandBoilerIDofyourboilerontheBoilerInformationworksheet.2.PleaseenterthetestdateontheBoilerInformationworksheet.3.Pleasechoosethetypeoffuelbeingsampledusingthedrop‐downinthefuelcolumnoftheBoilerInformationworksheet.Ifyouchoose"other",pleaseprovideadescriptionofthefuelintheOtherFuelDescriptioncolumn.4.PleaseprovidetheanalysismethodforeachconstituentintheAnalysisMethodsworksheet.Forexample:"ASTMD5865‐04".5.PleasechecktheUnitsofMeasuretablesforHHV,Metals,andCl/FlinthePicklistworksheet(orangetab).Iftheunits ofmeasurethatyouplantoreportarenotfoundintheUnitsofmeasuretable,pleasefillthemintheblank,orangehighlighted,cellineachtable.ThisallowsyoutochoosetheunitsofmeasureintheFuelsSampleResultsworksheet.InstructionsforcompletingtheFuelMaterialAnalysisInformationThisInformationCollectionRequest(ICR)spreadsheetisintendedtocollectinformationaboutchemicalanalysesoffuelsusedfossilfuelburningpowerplants.Constituentsofconcernare:mercury,chlorine,fluorine,andmetals,suchasantimony,beryllium,cadmium,chromium,cobalt,lead,manganese,nickel,andselenium.Thisspreadsheetisintendedtobeusedforoneboilerofonefacilitybutisdesignedtoallowmultiple(upto4)fuelanalysesatthatspecificboiler.Thisnumberofanalyseswouldcoincidewithoneboilerwhereemissionstestingforall4HAPsurrogateswerebeingtested.Dataformultipleboilersshouldbehandledbyusingseparatespreadsheets.Fieldsthatarehighlightedinyellowarerequiredfields.Greenhighlightedcellsshouldbefilledusingthedrop‐downboxes,included.Grayfieldsareautomaticallyfilledfromotherfields.Pleasenameeachresultingspreadsheetwiththefollowingnamingconvention:[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls(example:8100_Unit_2_Fuels_Testing.xls).Pleaserefertothefollowingstepswhenusingthesespreadsheets.1.PleaseentertheEIAFacilityCode,FacilityNameandBoilerIDofyourboilerontheBoilerInformationworksheet.2.PleaseenterthetestdateontheBoilerInformationworksheet.3.Pleasechoosethetypeoffuelbeingsampledusingthedrop‐downinthefuelcolumnoftheBoilerInformationworksheet.Ifyouchoose"other",pleaseprovideadescriptionofthefuelintheOtherFuelDescriptioncolumn.4.PleaseprovidetheanalysismethodforeachconstituentintheAnalysisMethodsworksheet.Forexample:"ASTMD5865‐04".5.PleasechecktheUnitsofMeasuretablesforHHV,Metals,andCl/FlinthePicklistworksheet(orangetab).Iftheunits ofmeasurethatyouplantoreportarenotfoundintheUnitsofmeasuretable,pleasefillthemintheblank,orangehighlighted,cellineachtable.ThisallowsyoutochoosetheunitsofmeasureintheFuelsSampleResultsworksheet.6.SelecttheHAPsTestGroup(i.e.,HAPsurrogate)forwhichthetab'sdatareflects(orangehighlightedcell).7.ProvidetheSampleNumberandSampleDateontheFuelsSampleResultsworksheet.Youmustprovideaminimumof3compositesamplesconsistingof3combinedgrabsampleseach,butyouarenotlimitedtothatnumberifyouhavecollectedmore.8.Providetheresultsoftheanalysesforeachconstituentrequested.Usethedrop‐downboxestofillintheunitsofInstructionsforcompletingtheFuelMaterialAnalysisInformationThisInformationCollectionRequest(ICR)spreadsheetisintendedtocollectinformationaboutchemicalanalysesoffuelsusedfossilfuelburningpowerplants.Constituentsofconcernare:mercury,chlorine,fluorine,andmetals,suchasantimony,beryllium,cadmium,chromium,cobalt,lead,manganese,nickel,andselenium.Thisspreadsheetisintendedtobeusedforoneboilerofonefacilitybutisdesignedtoallowmultiple(upto4)fuelanalysesatthatspecificboiler.Thisnumberofanalyseswouldcoincidewithoneboilerwhereemissionstestingforall4HAPsurrogateswerebeingtested.Dataformultipleboilersshouldbehandledbyusingseparatespreadsheets.Fieldsthatarehighlightedinyellowarerequiredfields.Greenhighlightedcellsshouldbefilledusingthedrop‐downboxes,included.Grayfieldsareautomaticallyfilledfromotherfields.Pleasenameeachresultingspreadsheetwiththefollowingnamingconvention:[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls(example:8100_Unit_2_Fuels_Testing.xls).Pleaserefertothefollowingstepswhenusingthesespreadsheets.1.PleaseentertheEIAFacilityCode,FacilityNameandBoilerIDofyourboilerontheBoilerInformationworksheet.2.PleaseenterthetestdateontheBoilerInformationworksheet.3.Pleasechoosethetypeoffuelbeingsampledusingthedrop‐downinthefuelcolumnoftheBoilerInformationworksheet.Ifyouchoose"other",pleaseprovideadescriptionofthefuelintheOtherFuelDescriptioncolumn.4.PleaseprovidetheanalysismethodforeachconstituentintheAnalysisMethodsworksheet.Forexample:"ASTMD5865‐04".5.PleasechecktheUnitsofMeasuretablesforHHV,Metals,andCl/FlinthePicklistworksheet(orangetab).Iftheunits ofmeasurethatyouplantoreportarenotfoundintheUnitsofmeasuretable,pleasefillthemintheblank,orangehighlighted,cellineachtable.ThisallowsyoutochoosetheunitsofmeasureintheFuelsSampleResultsworksheet.6.SelecttheHAPsTestGroup(i.e.,HAPsurrogate)forwhichthetab'sdatareflects(orangehighlightedcell).7.ProvidetheSampleNumberandSampleDateontheFuelsSampleResultsworksheet.Youmustprovideaminimumof3compositesamplesconsistingof3combinedgrabsampleseach,butyouarenotlimitedtothatnumberifyouhavecollectedmore.8.Providetheresultsoftheanalysesforeachconstituentrequested.Usethedrop‐downboxestofillintheunitsofmeasure.

# EIA Facility Code Facility Name Boiler ID Fuel Type 1

8102 Gavin 2 

# bituminous

# Fuel Type 2 Fuel Type 3 Other Fuel Description

# EIA Facility Code Facility Name Boiler ID Basis Analyte



# 8102 Gavin 2 As Received Higher Heating Value



# 8102 Gavin 2 As Received % Moisture



# 8102 Gavin 2 As Received % Ash



# 8102 Gavin 2 As Received % Sulfur



# 8102 Gavin 2 Dry basis Higher Heating Value



# 8102 Gavin 2 Dry basis % Ash



# 8102 Gavin 2 Dry basis % Sulfur



# 8102 Gavin 2 Dry basis Antimony



# 8102 Gavin 2 Dry basis Arsenic



# 8102 Gavin 2 Dry basis Beryllium



# 8102 Gavin 2 Dry basis Cadmium



# 8102 Gavin 2 Dry basis Chlorine



# 8102 Gavin 2 Dry basis Chromium



# 8102 Gavin 2 Dry basis Cobalt



# 8102 Gavin 2 Dry basis Fluorine



# 8102 Gavin 2 Dry basis Lead



# 8102 Gavin 2 Dry basis Manganese



# 8102 Gavin 2 Dry basis Mercury



# 8102 Gavin 2 Dry basis Nickel



# 8102 Gavin 2 Dry basis Selenium

# A na l ys i s M e th o d f or eac h A na l y t e

(example: ASTM D5865-04)



# ASTM D5865

ASTM D3302

ASTM D3174

ASTM D4239 Method B

ASTM D5865

ASTM D3174

ASTM D4239 Method B

ASTM D4208

ASTM D3761

# EIA Facility Code Facility Name Boiler ID 

# HAPs Test Group



# 8102 Gavin 2

Sample Number

(minimum of 3

composite

samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV)

(as received) HHV Units 

# Fuel Testing Results

# % Moisture

(as

received) % Ash

(as

received) % Sulfur

(as

received) Higher

Heating

Value (HHV)

(Dry Basis) HHV Units % Ash

(Dry Basis) % Sulfur

(Dry Basis)

# Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units A rsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units

# Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese

(Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units

# Note the P

Selenium

(Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Proximate Analyses, %

# roximate/Ultimate data below should be recorded on a dry basis (including ash).

Ash Fixed Carbo n Carbon Hydrogen Nitrogen Total Sulfur Oxygen % by w t Ultimate Analyses, % by wt

# EIA Facility Code Facility Name Boiler ID 

# HAPs Test Group



# 8102 Gavin 2

Sample Number

(minimum of 3

composite

samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher

Heating

Value (HHV)

(as

received) HHV Units 

# Fuel Testing Results

# % Moisture

(as

received) % Ash

(as

received) % Sulfur

(as

received) Higher

Heating

Value (HHV)

(Dry Basis) HHV Units % Ash

(Dry Basis) % Sulfur

(Dry Basis)

# Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units A rsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units

# Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese

(Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units

# Note the Proximate/U

Selenium

(Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash Proximate Analyses, % by wt

# ltimate data below should be recorded on a dry basis (including ash).

Fixed Carbo n Carbon Hydrogen Nitrogen Total Sulfur Oxygen Ultimate Analyses, % by wt

# EIA Facility Code Facility Name Boiler ID 

# HAPs Test Group



# 8102 Gavin 2

Sample Number

(minimum of 3

composite

samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV)

(as received) HHV Units 

# Fuel Testing Results

# % Moisture

(as

received) % Ash

(as

received) % Sulfur

(as

received) Higher

Heating

Value (HHV)

(Dry Basis) HHV Units % Ash

(Dry Basis) % Sulfur

(Dry Basis)

# Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units A rsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units

# Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese

(Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units

# Note the Proximate/U

Selenium

(Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash Proximate Analyses, % by w

# ltimate data below should be recorded on a dry basis (including ash).

Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen wt Ultimate Analyses, % by wt

# EIA Facility Code Facility Name Boiler ID



# 8102 Gavin 2

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value

(HHV)

(as received)



# Unit 2 Test 1 Coal Composite 

# 3/11/2010 3/11/2010 11230.00

Unit 2 Test 2 Coal Composite 

# 3/11/2010 3/11/2010 11419.00

Unit 2 Test 3 Coal Composite 

# 3/11/2010 3/11/2010 11085.00 Fuel Testing Results

# HAPs Test Group



# Acid gas HAPs

HHV Units % Moisture

(as

received) % Ash

(as

received) % Sulfur

(as

received) Higher

Heating

Value (HHV)

(Dry Basis)



# Btu/lb 12.4 10.13 2.9 12819

Btu/lb 12.27 9.3 3 13017

Btu/lb 14.23 8.47 2.44 12900

# HHV Units % Ash

(Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units



# Btu/lb 11.57 3.31 0.07 %

Btu/lb 10.6 3.42 0.05 %

Btu/lb 9.88 2.85 0.02 %

# Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis)

# Chromium

Units Lead (Dry

Basis) Lead Units Manganese

(Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium

(Dry Basis) Selenium

Units

# Note the Proximate/Ultimate data belo w

Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon



# 87 ug/g 12.4 39.11 11.57 49.32

86 ug/g 12.27 39.4 10.6 50

84 ug/g 14.23 39.93 9.88 50.19 Proximate Analyses, % by wt

# w should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen



# 71.02 5.38 2.01 3.31 6.71

72.18 5.5 2.05 3.42 6.25

72.11 5.52 2.09 2.85 7.55 Ultimate Analyses, % by wt

# Units of Measure Tables: Please do not modify these tables, except to add your own unit of measu

Fuel Units of Measure - HHV

anthracite Btu/lb

bituminous Btu/gallon

subbituminous

lignite

coal refuse (culm or gob)

No.2 Fuel Oil (distillate)

No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals

synfuel mg/g

petroleum coke μ g/g

othe r mg/Kg

# re to the orange hightlighted cell, if necessary.

Units of Measure - Cl, Fl

%

ppm