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Batch number Inspection lot Material Customer

Inspection lot creation date : 01/18/2012

ICAP METALS SCREEN ANALYTE Silver Aluminum Arsenic Barium ~~[ylli .u,m Ismutn Calcium Cadmium Cobalt Chromium iCroopper n Potassium Magnesium Manganese Moly’~denum Sodium Nickel Lead Antimony TS~N~enium Thallium Vanadium Zinc AA METAL SCREEN ANALYTE Mercury ANION SCREEN ANALYTE Fluoride Chloride Phosphate PHYSICAL ANALYSIS ANALYTE Ash Ash Character PH pidity.I as H2SO4 ) ]scos~[y temperature Spindle size Sbeed Water % Heat of Combustion Sediment ~4ensit~.. eavy ~weta s RESULT LIMIT (HO/BR) <1 (15/20)

(500/NA)  ̄ 6<1 (8.0110) < 1 (836/1000) <1 (38/500) <t 11 <1 (22t27) <1 (215/260) 2<1 (33140) 6 3 (2000/NA) 13 <1 218 (5001NA) 802 (2000/2000)

1187/105) <1 (209/380) <1 (19/40) 2 (1.0/8.0) 3 <I (141500) <1 1 (430/400) UNITS

RESULT L1MIT HOI~QL~ UNITS <0.100 (1.0/0.5) mglkg
gESULT L1MI~T ~ UNITS < 10 (1501150) mg/kg 0.55 (30/NA) %w/~fi <50 (2001500) mg/kg

RESULT LIM tq_" HO~H~L~JUNITS 0.05 (10/4.9) %wlw Adherent 7.0 (3-11 )I(4-9) 599 (1000/1500) cP 160 °F LV4 60 R/min 1.9 %w/w 13051 BTU/tb 

## <1 %.(V) 1.150 g/ml <500 mg/kg

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Inspection lot15:49 Page 02 from 02

Flashpoint >200 °F VISUAl. INSPECTION ANALYTE RESULT LIMIT (NO/BE) UNITS Gas Evolution No Number of phases 1 Color (Visual) Black Opaqueness Yes Suspended solids Yes SEPARATED PHASES No COMBUSTION PARAMETERS ANALYTE Carbon Hydrogen ~Nftrogen ~ulfur RESULTLIMIT ~UNITS

ORGANIC SCREEN ANALYTE PCB Benzene RESULT LIMI~,~ UNITS_ <5 mg/kg

RESULT LIMIT~ H O~EQ~B~) UNITS Yes No No COMMENTS ANALYTE TEST BURN MPDS MSDS Usage decision : Recertification sample received from MPDS and MSDS pulled from Lotus CHN and S data not available due to Instrument down. Viscous material. Viscosity exceeds review limit (see profile) Temp.(deg. F) Viscosity(cps) 71 >10000 110 79OO 130 233O 150 1130 160 599 170 36O ,~ompatibility issues: void contact with caustics, strong oxidizers, strong acids and acid anhydrides.

Approved by Date:0

0 0

0 o 0 

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### 0i/21/2011 00:54 Page 01 from 02

Inspection lot creation date : 01/20/2011

ICAP METALS SCREEN-

~ _RESULTLIMIT ~IOiBR) 

### Silver <1 (15120) AJumlnum - 4<1 (500/NA) Arsenic (8.0/10) Badum <1 (836/1000) Ben/ilium 

# Bis~ut~ :l’ (361500) Cal~lum 3 0baltadmlum ~t (22/27), hromlum 3 (2151260) opper <t (33/40) 3n  ̄ 13 ~0tasslum 3 (2000/NA) ~a~neslum 

# N~up k75 ,ead <1 2 ) _An.tim.ony. <1 (19140) ~e~emum 2 (1.0/8.0) TN 3 Tha iUm 

# Vanadium :I (141500) Zinc 9 (4301400) LrNITS

m

AA METAL SCREEN Mercury <0~100 (1.0/0.5) mg/kg "ANION SCREEN  ̄ ~YTE

~ LIMIT (HO~BR). ~N-I T S. C~i00~ldeFI O’ e <10 (1501150) mg/kfl 0.72 (30/NA) %W/v7 Phosphate <60 (2001500) mg/kg PHYSICAL ANALYSIS AN~Y~ g~ESULTLIMIT (HO/BR) ;.LrNITS 

### Ash 0.10 (10/4.9) %w/w ~ Chattier Adherent ’ 8.0 (3-11)/(4-9) .A.cid~.( as H2SO4 ) wscosmty 3:[3~0 (100011500) cP ~mp~..ra~re °F _~pmdi.e s~ze

 ̄ _60_ R/rain Heat of Combustion :~,D13531 %WIW BTU/Ib S_edi~ent <1 %~/~ .u.ens~... 1.233 g/~nl" rteaWMe~a~s <500 mg/kg

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O~:~

Flashpoint 130 oF VISUAL INSPECTION

~ RESULTLIMIT ~ _UNITS Gas Evolution No ~Nu.m~r of p,h, ases 1 ~olor (visual) Black ~upaque,nes.s . . Yes. ~usoenaea solids Yes SEPARATED PHASES No COMBUSTION PARAMETERS

~ RESUL~TLIMIT (’HO/BR)UNITS Carbon 61,20 %w/w Hydrogen 8.30 %w~v Ni’tn:~n 2.50 %wAy Su~T 8.80 %w/w 

### ORGANIC SCREEN
PCB Be~ene COMMENTS

I~EST BURN Yes



# .o No LIMIT ~ ~



### ~s~ge deeblon : vts¢ous material(Profile given be ow) TemP.(deg.F) Viscosity(cps) 68 :~10800  ̄80 50 .Co ~ [~ati biJity.iss...u, e s: . P, volo contact wjm caustics, strong oxtdlzem, strong acids and acid anhydrides. ~ApaPmVed by re:

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