01/19/2012 15:49 Page 01 from 02

Batch number 

Inspection lot

Material

Customer

Inspection lot creation date : 01/18/2012

ICAP METALS SCREEN

ANALYTE

Silver

Aluminum

Arsenic

Barium

~~[ylli .u,m Ismutn Calcium

Cadmium Cobalt Chromium

iCroopper n

Potassium

Magnesium Manganese

Moly’~denum

Sodium

Nickel

Lead

Antimony

TS~N~enium

Thallium

Vanadium

Zinc

AA METAL SCREEN

ANALYTE

Mercury

ANION SCREEN

ANALYTE

Fluoride

Chloride

Phosphate

PHYSICAL ANALYSIS

ANALYTE

Ash Ash Character

PHpidity.I as H2SO4 )

]scos~[y temperature Spindle size

Sbeed Water % Heat of Combustion Sediment

~4ensit~.. eavy ~weta s

RESULT LIMIT (HO/BR)

<1 (15/20)

(500/NA)  ̄ 6<1 (8.0110)

< 1 (836/1000)

<1 (38/500) <t

11

<1 (22t27) <1

(215/260) 2<1 (33140) 6

3 (2000/NA) 13

<1

218 (5001NA) 802 (2000/2000) 1187/105) <1 (209/380)

<1 (19/40)

2 (1.0/8.0) 3

<I (141500) <1

1 (430/400)

UNITS

RESULT L1MIT HOI~QL~ UNITS

<0.100 (1.0/0.5) mglkg

gESULT L1MI~T ~ UNITS

< 10 (1501150) mg/kg 0.55 (30/NA) %w/~fi <50 (2001500) mg/kg

RESULT LIM tq_" HO~H~L~J UNITS

0.05 (10/4.9) %wlw Adherent

7.0 (3-11 )I(4-9)

599 (1000/1500) cP 160 °F LV4

60 R/min 1.9 %w/w 13051 BTU/tb <1 %.(V) 1.150 g/ml <500 mg/kg
01/19/2012

Inspection lot

15:49 Page 02 from 02

Flashpoint >200 °F

VISUAl. INSPECTION

ANALYTE RESULT LIMIT (NO/BE) UNITS

Gas Evolution No Number of phases 1 Color (Visual) Black Opaqueness Yes Suspended solids Yes SEPARATED PHASES No

COMBUSTION PARAMETERS

ANALYTE

Carbon

Hydrogen ~Nftrogen ~ulfur

RESULT LIMIT ~ UNITS

ORGANIC SCREEN

ANALYTE

PCB

Benzene

RESULT LIMI~,~ UNITS_

<5 mg/kg

RESULT LIMIT~ H O~EQ~B~) UNITS

Yes

No

No

COMMENTS

ANALYTE

TEST BURN

MPDS MSDS

Usage decision : Recertification sample received from MPDS and MSDS pulled from Lotus CHN and S data not available due to Instrument down.

Viscous material. Viscosity exceeds review limit (see profile)

Temp.(deg. F) Viscosity(cps)

71 >10000 110 79OO 130 233O 150 1130 160 599 170 36O

,~ompatibility issues: void contact with caustics, strong oxidizers, strong acids and acid anhydrides.

Approved by

Date:
0

0

0

0

o

0

%Transmittance
0i/21/2011 00:54 Page 01 from 02

Inspection lot creation date : 01/20/2011

ICAP METALS SCREEN-

~ _RESULT LIMIT ~IOiBR)

Silver <1 (15120) AJumlnum - 4<1 (500/NA) Arsenic (8.0/10) Badum <1 (836/1000) Ben/ilium Bis~ut~ :l’ (361500)

Cal~lum 3

0baltadmlum ~t

(22/27),

hromlum 3 (2151260) opper <t (33/40) 3n  ̄ 13 ~0tasslum 3 (2000/NA) ~a~neslum

N~up k75

,ead <1 2 )

_An.tim.ony. <1 (19140)

~e~emum 2 (1.0/8.0) TN 3

Tha iUm Vanadium :I (141500)

Zinc 9 (4301400)

LrNITS

m

AA METAL SCREEN

Mercury <0~100 (1.0/0.5) mg/kg

"ANION SCREEN  ̄

~YTE ~ LIMIT (HO~BR) . ~N-I T S.

C~i00~ldeFI O’ e <10 (1501150) mg/kfl 0.72 (30/NA) %W/v7 Phosphate <60 (2001500) mg/kg

PHYSICAL ANALYSIS

AN~Y~ g~ESULT LIMIT (HO/BR) ; .LrNITS

Ash 0.10 (10/4.9) %w/w

~ Chattier Adherent ’

8.0 (3-11)/(4-9) .A.cid~.( as H2SO4 ) wscosmty 3:[3~0 (100011500) cP ~mp~..ra~re °F _~pmdi.e s~ze

 ̄ _60_ R/rain

Heat of Combustion :~,D13531 %WIW BTU/Ib S_edi~ent <1 %~/~

.u.ens~... 1.233 g/~nl" rteaW Me~a~s <500 mg/kg
01/21/2011 00:54 Page 02 from 02

O~:~

Flashpoint 130 oF

VISUAL INSPECTION

~ RESULT LIMIT ~ _UNITS Gas Evolution No ~Nu.m~r of p,h, ases 1

~olor (visual) Black

~upaque,nes.s . . Yes. ~usoenaea solids Yes SEPARATED PHASES No

COMBUSTION PARAMETERS

~ RESUL~T LIMIT (’HO/BR) UNITS Carbon Hydrogen 61,20 %w/w

Ni’tn:~n 8.30 %w~v 2.50 %wAy Su~T 8.80 %w/w

ORGANIC SCREEN

PCB

Be~ene

COMMENTS

I~EST BURN Yes .oNo

LIMIT ~ ~

~s~ge deeblon : vts¢ous material(Profile given be ow)

TemP.(deg.F) Viscosity(cps)

68  ̄ 80 :~10800

50

.Co ~ [~ati biJity.iss...u, e s: . P, volo contact wjm caustics, strong oxtdlzem, strong acids and acid anhydrides.

~ApaPmVed by re:
%Transmittance

ol