S507501 

Test Report 

Measurement of the molecular weights 

”S-2033”

TORAY RESEARCH CENTER, INC. 

3-3-7 Sonoyama㧘Otsu City㧘Shiga 520-8567㧘

JAPAN

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ޤSummaryޣ

The measurements of the average molecular weights and the contents of components having 

molecular weight of less than 2000 of the test sample “S-2033” were carried out using 

GPC-MALS. The results are shown in Tables A and B. 

Table A Average molecular weights 

Polydispersity 

Sample Mn *1 Mw *2 Mz *3 

Mw/Mn Mz/Mw

Lot.MMS2033 A1 108000 234000 493000 2.17 2.11 

Lot.MMS2033 A2 108000 231000 474000 2.14 2.05 

Lot.MMS2033 A3 112000 238000 506000 2.13 2.13 

*1 Number Average Molecular Weight 

*2 Weight Average Molecular Weight 

*3 Z Average Molecular Weight 

Table B Contents of components less than MW 2000 

Sample Content of component 

<MW 2000 (%) 

Lot.MMS2033 A1 0.005 

Lot.MMS2033 A2 0.000 

Lot.MMS2033 A3 0.000 

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1. Sponsor 

Name Daikin Industries, LTD. 

Address 1-1, Nishi-Hitotsuya, Settsu, Osaka 566-8585, Japan 

2. Test Laboratory 

Name Toray Reserch Center, Inc. 

Address 3-3-7 Sonoyama, Otsu City, Shiga, 520-8567, Japan 

3. Objective 

The objective of this measurement is to obtain the average molecular weights and content of 

components having molecular weight of less than 2000 of S-2033. 

4. Sample 

࡮S-2033 Lot.MMS2033 A1 

࡮S-2033 Lot.MMS2033 A2 

࡮S-2033 Lot.MMS2033 A3 

5. Experimental 

The measurements of molecular weights, a molecular weight distribution, and a content of 

components less than MW2000 were attempted by GPC-MALS. 

5.1 Measurement Parameters 

Apparatus Gel Permeation Chromatograph (GPC- 14)

Detector Differential refractive index detector Waters 2414 (Waters) 

Multi Angle laser Light Scattering DWAN DSP (Wyatt Tchnology)

Column set HFIP-LG (Column No.A104205) (Shodex) 

HFIP-806M (Column No.A205211) (Shodex) 

HFIP-806M (Column No. A205212) (Shodex)

Mobile Phase Hexafluoroisopropanol (5mM sodium trifluroacetate)

Flow rate 0.494 mL/min 

Sample Concentration 0.10% (wt/vol) 

Filtration 0.45 Pm-Millex-LH (Millipore) 

Injection volume 0.200 mL 

Temperature 40͠

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Solubility Soluble

Filter 0.45 Pm-JH OMNIPORE (Millipore) 

Data Processing system ASTRA (Wyatt Technology) 

5.2 Analytical method 

The test substance (0.010g) of as received product (see item 1) was dissolved into 

hexafluoroisopropanol (10mL) to give a 0.10% solution. And the solution was subjected to the 

analysis. 

Instrumental constant of GPC-MALS was obtained by standard sample. Absolute molecular 

weight and molecular weight distribution of the test substance were calculated by the software 

for GPC-MALS analysis. 

6. Results 

6.1 GPC-MALS Curves 

GPC-MALS curves of the sample are shown in Figs.1 to 3. In these figures, the upsides 

curve is MALS curve, and the downsides curve is RI curve. The signal of the sample was 

detected from about 29 min. to 50 min. in the RI curve. The peaks detected after about 50 min. of 

the elution time were the solvent-composition-change, solvent-impurity and/or the system peak 

(It was confirmed by the GPC measurement of the solvent. See Fig.4). 

6.2 Calibration curve of molecular weight 

The absolute molecular weight (Mw) of the sample was calculated by the Eqs. (1) and (2). 

 ¦ ¦

   

/ (2)

2 (1) 1

w

2

i i i

i

i i

i

M c M c

A c

R M

K c 

T

where, Mw : Absolute weight average molecular weight 

 Mi : Weight average molecular weight of each elution time 

K : Constant = 

 instrument constant(refractive index of the solvent)2

 (specific refractive index increment)2

RTi : Excess Rayleigh ratio of each elution time 

 A2 : Second virial coefficient 

 ci : Concentration of each elution time 

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 In the right side of Eq. (1), the second term is negligibly small compared with the first term. 

Therefore the second term was neglected. The absolute molecular weight of the sample was 

234000. 

6.3 Determination of specific refractive index increment (dn/dc)

Determination of specific refractive index increment(dn/dc) was calculated by the use of 

GPC-MALS curve of sample(Fig.1) and that of the standard Polymethyl methacrylate(PMMA) 

(M-21(Shodex)㧦Mw = 20600)(Fig.9) according to the following equation. The dn/dc of sample 

was 0.0965 mL/g. 

 dn/dc(sample) = dn/dc(PMMA(0.183 mg/L))Asample / APMMA (3) 

where, Asample and APMMA were the peak area values of the sample and the standard 

PMMA, respectively. 

6.4 Calibration curve of molecular weight 

The calibration curve is shown in Fig.5. This calibration curve was obtained by the method 

that showed as follows.

1. Calibration curve was obtained from the relationship between the elution time (ti) and 

the molecular weight (Mi) of the standard Polymethyl methacrylates(PMMAs) and 

3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl acrylate(C6SFA) measured under the same 

GPC-MALS condition. 

2. The calibration curve was adjusted by such a way as the weight average molecular 

weight of the sample coincides with the absolute weight average molecular weight 

(234000) by GPC-MALS. 

3

3

2

0 1 2 log M A  A  t  A  t  A  t (4) 

where, M : Molecular weight 

t : Elution time 

Ai : Coefficients 

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6.5 Calculation of MWD and average molecular weights 

The MWDs were originated by the RI curves of the sample (Figs.1 to 3) and the calibration 

curve (Fig.5) using GPC data processing system. The MWD curves and the average molecular 

weights are shown in Figs.6 to 8 and Table A. 

The notations of the symbols in the Table A were as follows: 

Mn : Number average molecular weight 

 Mw : Weight average molecular weight 

 Mz : Z average molecular weight 

 Mw / Mn : Polydispersity 

 Mz / Mw : Polydispersity 

6.6 Content of the components having molecular weight <2000 

The MWD data are shown in Tables 1 to 3. The contents of the components having the 

molecular weight of less than MW 2000 are shown in Table B. 

7. Conclusion 

The measurements of the average molecular weights and the content of components 

molecular weight of less than 2000 of S-2033 were carried out using GPC-MALS. The content of 

the components having molecular weight of less than 2000 was less than 0.017%. 

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㪊㪎㪅㪍㪌 㪉㪍㪊㪍㪈 㪇㪅㪇㪉㪎 㪇㪅㪇㪎㪋 㪈㪅㪊㪍㪌

㪊㪎㪅㪏㪌 㪉㪋㪈㪇㪐 㪇㪅㪇㪉㪈 㪇㪅㪇㪌㪎 㪈㪅㪈㪈㪌

㪊㪏㪅㪇㪌 㪉㪉㪇㪍㪉 㪇㪅㪇㪈㪍 㪇㪅㪇㪋㪋 㪇㪅㪐㪉㪉

㪊㪏㪅㪉㪌 㪉㪇㪈㪐㪐 㪇㪅㪇㪈㪊 㪇㪅㪇㪊㪌 㪇㪅㪎㪎㪋

㪊㪏㪅㪋㪌 㪈㪏㪌㪇㪊 㪇㪅㪇㪈㪇 㪇㪅㪇㪉㪎 㪇㪅㪍㪌㪏

㪊㪏㪅㪍㪌 㪈㪍㪐㪌㪐 㪇㪅㪇㪇㪏 㪇㪅㪇㪉㪉 㪇㪅㪌㪍㪍

㪊㪏㪅㪏㪌 㪈㪌㪌㪌㪉 㪇㪅㪇㪇㪍 㪇㪅㪇㪈㪏 㪇㪅㪋㪐㪈

㪊㪐㪅㪇㪌 㪈㪋㪉㪎㪇 㪇㪅㪇㪇㪌 㪇㪅㪇㪈㪌 㪇㪅㪋㪊㪇

㪊㪐㪅㪉㪌 㪈㪊㪈㪇㪈 㪇㪅㪇㪇㪋 㪇㪅㪇㪈㪊 㪇㪅㪊㪎㪐

㪊㪐㪅㪋㪌 㪈㪉㪇㪊㪋 㪇㪅㪇㪇㪋 㪇㪅㪇㪈㪈 㪇㪅㪊㪊㪌

㪊㪐㪅㪍㪌 㪈㪈㪇㪍㪈 㪇㪅㪇㪇㪊 㪇㪅㪇㪈㪇 㪇㪅㪉㪐㪎

㪊㪐㪅㪏㪌 㪈㪇㪈㪎㪉 㪇㪅㪇㪇㪊 㪇㪅㪇㪈㪇 㪇㪅㪉㪍㪉

㪋㪇㪅㪇㪌 㪐㪊㪍㪇 㪇㪅㪇㪇㪊 㪇㪅㪇㪇㪏 㪇㪅㪉㪊㪇

㪋㪇㪅㪉㪌 㪏㪍㪈㪏 㪇㪅㪇㪇㪊 㪇㪅㪇㪇㪏 㪇㪅㪉㪇㪇

㪋㪇㪅㪋㪌 㪎㪐㪊㪐 㪇㪅㪇㪇㪉 㪇㪅㪇㪇㪎 㪇㪅㪈㪎㪊

㪋㪇㪅㪍㪌 㪎㪊㪈㪐 㪇㪅㪇㪇㪉 㪇㪅㪇㪇㪍 㪇㪅㪈㪌㪇

㪋㪇㪅㪏㪌 㪍㪎㪌㪈 㪇㪅㪇㪇㪉 㪇㪅㪇㪇㪌 㪇㪅㪈㪊㪈

㪋㪈㪅㪇㪌 㪍㪉㪊㪇 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪋 㪇㪅㪈㪈㪋

㪋㪈㪅㪉㪌 㪌㪎㪌㪋 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪋 㪇㪅㪈㪇㪈

㪋㪈㪅㪋㪌 㪌㪊㪈㪎 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪊 㪇㪅㪇㪏㪐

㪋㪈㪅㪍㪌 㪋㪐㪈㪍 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪊 㪇㪅㪇㪎㪏

㪋㪈㪅㪏㪌 㪋㪌㪋㪐 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪊 㪇㪅㪇㪍㪏

㪋㪉㪅㪇㪌 㪋㪉㪈㪉 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪋 㪇㪅㪇㪌㪎

㪋㪉㪅㪉㪌 㪊㪐㪇㪉 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪊 㪇㪅㪇㪋㪍

㪋㪉㪅㪋㪌 㪊㪍㪈㪎 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪊 㪇㪅㪇㪊㪎

㪋㪉㪅㪍㪌 㪊㪊㪌㪌 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪉 㪇㪅㪇㪉㪐

㪋㪉㪅㪏㪌 㪊㪈㪈㪌 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪉 㪇㪅㪇㪉㪊

㪋㪊㪅㪇㪌 㪉㪏㪐㪊 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪈 㪇㪅㪇㪈㪏

㪋㪊㪅㪉㪌 㪉㪍㪏㪐 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪈 㪇㪅㪇㪈㪋

㪋㪊㪅㪋㪌 㪉㪌㪇㪈 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪈 㪇㪅㪇㪈㪈

㪋㪊㪅㪍㪌 㪉㪊㪉㪏 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪉 㪇㪅㪇㪇㪏

㪋㪊㪅㪏㪌 㪉㪈㪍㪐 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪍

㪋㪋㪅㪇㪌 㪉㪇㪉㪈 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪌

㪋㪋㪅㪉㪌 㪈㪏㪏㪌 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪊

㪋㪋㪅㪋㪌 㪈㪎㪍㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪈

㪋㪋㪅㪍㪌 㪈㪍㪋㪋 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪋㪅㪏㪌 㪈㪌㪊㪍 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪌㪅㪇㪌 㪈㪋㪊㪎 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪌㪅㪉㪌 㪈㪊㪋㪌 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪌㪅㪋㪌 㪈㪉㪍㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪌㪅㪍㪌 㪈㪈㪏㪈 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪌㪅㪏㪌 㪈㪈㪇㪏 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪍㪅㪇㪌 㪈㪇㪋㪈 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪍㪅㪉㪌 㪐㪎㪏 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪍㪅㪋㪌 㪐㪉㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪍㪅㪍㪌 㪏㪍㪌 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪍㪅㪏㪌 㪏㪈㪌 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪎㪅㪇㪌 㪎㪍㪏 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪎㪅㪉㪌 㪎㪉㪋 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪎㪅㪋㪌 㪍㪏㪋 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪎㪅㪍㪌 㪍㪋㪍 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪎㪅㪏㪌 㪍㪈㪈 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪏㪅㪇㪌 㪌㪎㪏 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪏㪅㪉㪌 㪌㪋㪏 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪏㪅㪋㪌 㪌㪈㪐 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪫㪸㪹㫃㪼㩷㪈㪄㩷㪉

㪫㪪㪄㪜㪇㪎㪎㪢㪡 㪘㫋㫋㪸㪺㪿㫄㪼㫅㫋㩷㪎

Page 9/25
㪫㪸㪹㫃㪼㩷㪈㩷㩷㩷㩷㩷㩷㩷㪤㫆㫃㪼㪺㫌㫃㪸㫉㩷㪮㪼㫀㪾㪿㫋㩷㪛㪸㫋㪸 㪪㪌㪇㪎㪌㪇㪈

㪜㫃㫀㫋㫌㫀㫆㫅㩷㪫㫀㫄㪼

㩿㫄㫀㫅㪀

㪤㫆㫃㪼㪺㫌㫃㪸㫉

㪮㪼㫀㪾㪿㫋

㪠㫅㫋㪼㫅㫊㫀㫋㫐

㩿㫄㪭㪀

㪻㩿㪮㪼㫀㪾㪿㫋㪀

㪆㪻㪣㫆㪾㩿㪤㪮㪀 㪮㪼㫀㪾㪿㫋㩷㩼

㪋㪏㪅㪍㪌 㪋㪐㪉 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪏㪅㪏㪌 㪋㪍㪎 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪐㪅㪇㪌 㪋㪋㪋 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪐㪅㪉㪌 㪋㪉㪉 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪐㪅㪋㪌 㪋㪇㪉 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪐㪅㪍㪌 㪊㪏㪊 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪫㪸㪹㫃㪼㩷㪈㪄㩷㪊

㪫㪪㪄㪜㪇㪎㪎㪢㪡 㪘㫋㫋㪸㪺㪿㫄㪼㫅㫋㩷㪎

Page 10/25
㪫㪸㪹㫃㪼㩷㪉㩷㩷㩷㩷㩷㩷㩷㪤㫆㫃㪼㪺㫌㫃㪸㫉㩷㪮㪼㫀㪾㪿㫋㩷㪛㪸㫋㪸 㪪㪌㪇㪎㪌㪇㪈

㪪㪸㫄㫇㫃㪼 䋺㩷㪣㫆㫋㪅㩷㪤㪤㪪㪉㪇㪊㪊䇭㪘㪉 㪤㫅 䋺㩷㪈㪇㪏㪇㪇㪇

㪦㫇㪼㫉㪸㫋㫆㫉 䋺㩷㪘㪢㪘㪪㪘㪢㪘 㪤㫎 䋺㩷㪉㪊㪈㪇㪇㪇

㪛㪸㫋㪼 䋺㩷㪉㪇㪈㪊㪅㪉㪅㪉㪇 㪤㫑 䋺㩷㪋㪎㪋㪇㪇㪇

㪤㫎㪆㪤㫅 䋺㩷㪉㪅㪈㪋

㪤㫑㪆㪤㫎 䋺㩷㪉㪅㪇㪌

㪜㫃㫀㫋㫌㫀㫆㫅㩷㪫㫀㫄㪼

㩿㫄㫀㫅㪀

㪤㫆㫃㪼㪺㫌㫃㪸㫉

㪮㪼㫀㪾㪿㫋

㪠㫅㫋㪼㫅㫊㫀㫋㫐

㩿㫄㪭㪀

㪻㩿㪮㪼㫀㪾㪿㫋㪀

㪆㪻㪣㫆㪾㩿㪤㪮㪀 㪮㪼㫀㪾㪿㫋㩷㩼

㪉㪏㪅㪇㪍 㪊㪈㪎㪇㪍㪍㪊 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪈㪇㪇㪅㪇㪇㪇

㪉㪏㪅㪉㪍 㪉㪏㪋㪍㪏㪐㪌 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪈 㪐㪐㪅㪐㪐㪐

㪉㪏㪅㪋㪍 㪉㪌㪌㪍㪏㪉㪊 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪉 㪐㪐㪅㪐㪐㪌

㪉㪏㪅㪍㪍 㪉㪉㪐㪍㪏㪐㪋 㪇㪅㪇㪇㪉 㪇㪅㪇㪇㪋 㪐㪐㪅㪐㪏㪈

㪉㪏㪅㪏㪍 㪉㪇㪍㪊㪐㪉㪍 㪇㪅㪇㪇㪋 㪇㪅㪇㪇㪐 㪐㪐㪅㪐㪋㪏

㪉㪐㪅㪇㪍 㪈㪏㪌㪌㪇㪏㪈 㪇㪅㪇㪇㪏 㪇㪅㪇㪈㪏 㪐㪐㪅㪏㪏㪍

㪉㪐㪅㪉㪌 㪈㪍㪍㪎㪏㪉㪌 㪇㪅㪇㪈㪊 㪇㪅㪇㪉㪐 㪐㪐㪅㪎㪎㪎

㪉㪐㪅㪋㪌 㪈㪋㪐㪐㪏㪏㪌 㪇㪅㪇㪉㪇 㪇㪅㪇㪋㪌 㪐㪐㪅㪍㪇㪌

㪉㪐㪅㪍㪌 㪈㪊㪋㪐㪉㪊㪐 㪇㪅㪇㪉㪐 㪇㪅㪇㪍㪌 㪐㪐㪅㪊㪌㪈

㪉㪐㪅㪏㪌 㪈㪉㪈㪋㪇㪎㪍 㪇㪅㪇㪊㪐 㪇㪅㪇㪏㪏 㪐㪏㪅㪐㪐㪐

㪊㪇㪅㪇㪌 㪈㪇㪐㪉㪎㪎㪌 㪇㪅㪇㪌㪈 㪇㪅㪈㪈㪌 㪐㪏㪅㪌㪊㪊

㪊㪇㪅㪉㪌 㪐㪏㪊㪏㪏㪐 㪇㪅㪇㪍㪋 㪇㪅㪈㪋㪋 㪐㪎㪅㪐㪊㪐

㪊㪇㪅㪋㪌 㪏㪏㪍㪈㪉㪌 㪇㪅㪇㪎㪐 㪇㪅㪈㪎㪎 㪐㪎㪅㪉㪇㪊

㪊㪇㪅㪍㪌 㪎㪐㪏㪊㪉㪋 㪇㪅㪇㪐㪌 㪇㪅㪉㪈㪋 㪐㪍㪅㪊㪈㪇

㪊㪇㪅㪏㪌 㪎㪈㪐㪋㪌㪉 㪇㪅㪈㪈㪊 㪇㪅㪉㪌㪌 㪐㪌㪅㪉㪋㪊

㪊㪈㪅㪇㪌 㪍㪋㪏㪌㪏㪉 㪇㪅㪈㪊㪉 㪇㪅㪊㪇㪇 㪐㪊㪅㪐㪏㪎

㪊㪈㪅㪉㪌 㪌㪏㪋㪏㪏㪍 㪇㪅㪈㪌㪊 㪇㪅㪊㪋㪏 㪐㪉㪅㪌㪉㪍

㪊㪈㪅㪋㪌 㪌㪉㪎㪍㪉㪉 㪇㪅㪈㪎㪋 㪇㪅㪊㪐㪐 㪐㪇㪅㪏㪋㪎

㪊㪈㪅㪍㪌 㪋㪎㪍㪈㪉㪎 㪇㪅㪈㪐㪎 㪇㪅㪋㪌㪊 㪏㪏㪅㪐㪊㪎

㪊㪈㪅㪏㪌 㪋㪉㪐㪏㪇㪎 㪇㪅㪉㪉㪈 㪇㪅㪌㪇㪐 㪏㪍㪅㪎㪐㪇

㪊㪉㪅㪇㪌 㪊㪏㪏㪈㪊㪇 㪇㪅㪉㪋㪌 㪇㪅㪌㪍㪎 㪏㪋㪅㪊㪐㪎

㪊㪉㪅㪉㪌 㪊㪌㪇㪍㪉㪇 㪇㪅㪉㪎㪇 㪇㪅㪍㪉㪍 㪏㪈㪅㪎㪌㪊

㪊㪉㪅㪋㪌 㪊㪈㪍㪏㪌㪇 㪇㪅㪉㪐㪌 㪇㪅㪍㪏㪍 㪎㪏㪅㪏㪌㪍

㪊㪉㪅㪍㪌 㪉㪏㪍㪋㪊㪐 㪇㪅㪊㪈㪐 㪇㪅㪎㪋㪎 㪎㪌㪅㪎㪇㪍

㪊㪉㪅㪏㪌 㪉㪌㪐㪇㪋㪊 㪇㪅㪊㪋㪋 㪇㪅㪏㪇㪍 㪎㪉㪅㪊㪇㪌

㪊㪊㪅㪇㪌 㪉㪊㪋㪊㪌㪏 㪇㪅㪊㪍㪎 㪇㪅㪏㪍㪌 㪍㪏㪅㪍㪌㪐

㪊㪊㪅㪉㪌 㪉㪈㪉㪈㪇㪎 㪇㪅㪊㪐㪇 㪇㪅㪐㪉㪈 㪍㪋㪅㪎㪎㪐

㪊㪊㪅㪋㪌 㪈㪐㪉㪇㪋㪊 㪇㪅㪋㪈㪇 㪇㪅㪐㪎㪊 㪍㪇㪅㪍㪏㪊

㪊㪊㪅㪍㪌 㪈㪎㪊㪐㪋㪎 㪇㪅㪋㪉㪏 㪈㪅㪇㪈㪐 㪌㪍㪅㪊㪐㪊

㪊㪊㪅㪏㪌 㪈㪌㪎㪍㪉㪇 㪇㪅㪋㪋㪉 㪈㪅㪇㪌㪎 㪌㪈㪅㪐㪊㪐

㪊㪋㪅㪇㪌 㪈㪋㪉㪏㪏㪋 㪇㪅㪋㪌㪉 㪈㪅㪇㪏㪍 㪋㪎㪅㪊㪍㪊

㪊㪋㪅㪉㪌 㪈㪉㪐㪌㪎㪐 㪇㪅㪋㪌㪎 㪈㪅㪈㪇㪉 㪋㪉㪅㪎㪈㪉

㪊㪋㪅㪋㪌 㪈㪈㪎㪌㪍㪊 㪇㪅㪋㪌㪌 㪈㪅㪈㪇㪊 㪊㪏㪅㪇㪋㪎

㪊㪋㪅㪍㪌 㪈㪇㪍㪎㪇㪎 㪇㪅㪋㪋㪍 㪈㪅㪇㪏㪍 㪊㪊㪅㪋㪊㪏

㪊㪋㪅㪏㪌 㪐㪍㪏㪐㪌 㪇㪅㪋㪉㪐 㪈㪅㪇㪋㪐 㪉㪏㪅㪐㪍㪌

㪊㪌㪅㪇㪌 㪏㪏㪇㪉㪋 㪇㪅㪋㪇㪋 㪇㪅㪐㪐㪉 㪉㪋㪅㪎㪈㪋

㪊㪌㪅㪉㪌 㪏㪇㪇㪇㪇 㪇㪅㪊㪎㪈 㪇㪅㪐㪈㪌 㪉㪇㪅㪎㪍㪋

㪊㪌㪅㪋㪌 㪎㪉㪎㪋㪈 㪇㪅㪊㪊㪉 㪇㪅㪏㪉㪋 㪈㪎㪅㪈㪏㪌

㪊㪌㪅㪍㪌 㪍㪍㪈㪎㪈 㪇㪅㪉㪐㪇 㪇㪅㪎㪉㪊 㪈㪋㪅㪇㪉㪇

㪊㪌㪅㪏㪌 㪍㪇㪉㪉㪈 㪇㪅㪉㪋㪏 㪇㪅㪍㪉㪇 㪈㪈㪅㪉㪐㪇

㪊㪍㪅㪇㪌 㪌㪋㪏㪊㪊 㪇㪅㪉㪇㪍 㪇㪅㪌㪈㪏 㪏㪅㪐㪐㪉

㪊㪍㪅㪉㪌 㪋㪐㪐㪌㪇 㪇㪅㪈㪍㪎 㪇㪅㪋㪉㪉 㪎㪅㪈㪇㪎

㪊㪍㪅㪋㪌 㪋㪌㪌㪉㪋 㪇㪅㪈㪊㪉 㪇㪅㪊㪊㪎 㪌㪅㪌㪐㪎

㪊㪍㪅㪍㪌 㪋㪈㪌㪈㪇 㪇㪅㪈㪇㪊 㪇㪅㪉㪍㪋 㪋㪅㪋㪈㪇

㪊㪍㪅㪏㪌 㪊㪎㪏㪍㪏 㪇㪅㪇㪎㪐 㪇㪅㪉㪇㪋 㪊㪅㪋㪐㪈

㪊㪎㪅㪇㪌 㪊㪋㪌㪍㪊 㪇㪅㪇㪍㪈 㪇㪅㪈㪌㪎 㪉㪅㪎㪏㪎

㪊㪎㪅㪉㪌 㪊㪈㪌㪍㪊 㪇㪅㪇㪋㪍 㪇㪅㪈㪉㪇 㪉㪅㪉㪌㪇

㪊㪎㪅㪋㪌 㪉㪏㪏㪊㪎 㪇㪅㪇㪊㪌 㪇㪅㪇㪐㪉 㪈㪅㪏㪋㪈

㪫㪸㪹㫃㪼㩷㪉㪄㩷㪈

㪫㪪㪄㪜㪇㪎㪎㪢㪡 㪘㫋㫋㪸㪺㪿㫄㪼㫅㫋㩷㪎

Page 11/25

  CBI    CBI 
㪫㪸㪹㫃㪼㩷㪉㩷㩷㩷㩷㩷㩷㩷㪤㫆㫃㪼㪺㫌㫃㪸㫉㩷㪮㪼㫀㪾㪿㫋㩷㪛㪸㫋㪸 㪪㪌㪇㪎㪌㪇㪈

㪜㫃㫀㫋㫌㫀㫆㫅㩷㪫㫀㫄㪼

㩿㫄㫀㫅㪀

㪤㫆㫃㪼㪺㫌㫃㪸㫉

㪮㪼㫀㪾㪿㫋

㪠㫅㫋㪼㫅㫊㫀㫋㫐

㩿㫄㪭㪀

㪻㩿㪮㪼㫀㪾㪿㫋㪀

㪆㪻㪣㫆㪾㩿㪤㪮㪀 㪮㪼㫀㪾㪿㫋㩷㩼

㪊㪎㪅㪍㪌 㪉㪍㪊㪍㪈 㪇㪅㪇㪉㪎 㪇㪅㪇㪎㪈 㪈㪅㪌㪉㪐

㪊㪎㪅㪏㪌 㪉㪋㪈㪇㪐 㪇㪅㪇㪉㪈 㪇㪅㪇㪌㪌 㪈㪅㪉㪏㪎

㪊㪏㪅㪇㪌 㪉㪉㪇㪍㪉 㪇㪅㪇㪈㪍 㪇㪅㪇㪋㪋 㪈㪅㪇㪐㪐

㪊㪏㪅㪉㪌 㪉㪇㪈㪐㪐 㪇㪅㪇㪈㪊 㪇㪅㪇㪊㪌 㪇㪅㪐㪌㪇

㪊㪏㪅㪋㪌 㪈㪏㪌㪇㪊 㪇㪅㪇㪈㪈 㪇㪅㪇㪉㪐 㪇㪅㪏㪊㪇

㪊㪏㪅㪍㪌 㪈㪍㪐㪌㪐 㪇㪅㪇㪇㪐 㪇㪅㪇㪉㪋 㪇㪅㪎㪊㪇

㪊㪏㪅㪏㪌 㪈㪌㪌㪌㪉 㪇㪅㪇㪇㪏 㪇㪅㪇㪉㪈 㪇㪅㪍㪋㪌

㪊㪐㪅㪇㪌 㪈㪋㪉㪎㪇 㪇㪅㪇㪇㪎 㪇㪅㪇㪈㪏 㪇㪅㪌㪎㪋

㪊㪐㪅㪉㪌 㪈㪊㪈㪇㪈 㪇㪅㪇㪇㪍 㪇㪅㪇㪈㪍 㪇㪅㪌㪈㪈

㪊㪐㪅㪋㪌 㪈㪉㪇㪊㪋 㪇㪅㪇㪇㪌 㪇㪅㪇㪈㪌 㪇㪅㪋㪌㪌

㪊㪐㪅㪍㪌 㪈㪈㪇㪍㪈 㪇㪅㪇㪇㪌 㪇㪅㪇㪈㪋 㪇㪅㪋㪇㪋

㪊㪐㪅㪏㪌 㪈㪇㪈㪎㪉 㪇㪅㪇㪇㪌 㪇㪅㪇㪈㪊 㪇㪅㪊㪌㪎

㪋㪇㪅㪇㪌 㪐㪊㪍㪇 㪇㪅㪇㪇㪋 㪇㪅㪇㪈㪉 㪇㪅㪊㪈㪈

㪋㪇㪅㪉㪌 㪏㪍㪈㪏 㪇㪅㪇㪇㪋 㪇㪅㪇㪈㪈 㪇㪅㪉㪍㪐

㪋㪇㪅㪋㪌 㪎㪐㪊㪐 㪇㪅㪇㪇㪊 㪇㪅㪇㪈㪇 㪇㪅㪉㪊㪇

㪋㪇㪅㪍㪌 㪎㪊㪈㪐 㪇㪅㪇㪇㪊 㪇㪅㪇㪈㪇 㪇㪅㪈㪐㪌

㪋㪇㪅㪏㪌 㪍㪎㪌㪈 㪇㪅㪇㪇㪊 㪇㪅㪇㪇㪐 㪇㪅㪈㪍㪊

㪋㪈㪅㪇㪌 㪍㪉㪊㪇 㪇㪅㪇㪇㪊 㪇㪅㪇㪇㪏 㪇㪅㪈㪊㪋

㪋㪈㪅㪉㪌 㪌㪎㪌㪋 㪇㪅㪇㪇㪊 㪇㪅㪇㪇㪏 㪇㪅㪈㪇㪎

㪋㪈㪅㪋㪌 㪌㪊㪈㪎 㪇㪅㪇㪇㪉 㪇㪅㪇㪇㪎 㪇㪅㪇㪏㪊

㪋㪈㪅㪍㪌 㪋㪐㪈㪍 㪇㪅㪇㪇㪉 㪇㪅㪇㪇㪍 㪇㪅㪇㪍㪉

㪋㪈㪅㪏㪌 㪋㪌㪋㪐 㪇㪅㪇㪇㪉 㪇㪅㪇㪇㪌 㪇㪅㪇㪋㪌

㪋㪉㪅㪇㪌 㪋㪉㪈㪉 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪋 㪇㪅㪇㪊㪇

㪋㪉㪅㪉㪌 㪊㪐㪇㪉 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪊 㪇㪅㪇㪈㪐

㪋㪉㪅㪋㪌 㪊㪍㪈㪎 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪉 㪇㪅㪇㪈㪈

㪋㪉㪅㪍㪌 㪊㪊㪌㪌 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪉 㪇㪅㪇㪇㪋

㪋㪉㪅㪏㪌 㪊㪈㪈㪌 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪈

㪋㪊㪅㪇㪌 㪉㪏㪐㪊 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪊㪅㪉㪌 㪉㪍㪏㪐 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪊㪅㪋㪌 㪉㪌㪇㪈 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪊㪅㪍㪌 㪉㪊㪉㪏 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪊㪅㪏㪌 㪉㪈㪍㪐 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪋㪅㪇㪌 㪉㪇㪉㪈 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪋㪅㪉㪌 㪈㪏㪏㪌 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪋㪅㪋㪌 㪈㪎㪍㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪋㪅㪍㪌 㪈㪍㪋㪋 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪋㪅㪏㪌 㪈㪌㪊㪍 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪌㪅㪇㪌 㪈㪋㪊㪎 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪌㪅㪉㪌 㪈㪊㪋㪌 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪌㪅㪋㪌 㪈㪉㪍㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪌㪅㪍㪌 㪈㪈㪏㪈 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪌㪅㪏㪌 㪈㪈㪇㪏 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪍㪅㪇㪌 㪈㪇㪋㪈 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪍㪅㪉㪌 㪐㪎㪏 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪍㪅㪋㪌 㪐㪉㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪍㪅㪍㪌 㪏㪍㪌 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪍㪅㪏㪌 㪏㪈㪌 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪎㪅㪇㪌 㪎㪍㪏 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪎㪅㪉㪌 㪎㪉㪋 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪎㪅㪋㪌 㪍㪏㪋 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪎㪅㪍㪌 㪍㪋㪍 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪎㪅㪏㪌 㪍㪈㪈 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪏㪅㪇㪌 㪌㪎㪏 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪏㪅㪉㪌 㪌㪋㪏 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪏㪅㪋㪌 㪌㪈㪐 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪫㪸㪹㫃㪼㩷㪉㪄㩷㪉

㪫㪪㪄㪜㪇㪎㪎㪢㪡 㪘㫋㫋㪸㪺㪿㫄㪼㫅㫋㩷㪎

Page 12/25
㪫㪸㪹㫃㪼㩷㪉㩷㩷㩷㩷㩷㩷㩷㪤㫆㫃㪼㪺㫌㫃㪸㫉㩷㪮㪼㫀㪾㪿㫋㩷㪛㪸㫋㪸 㪪㪌㪇㪎㪌㪇㪈

㪜㫃㫀㫋㫌㫀㫆㫅㩷㪫㫀㫄㪼

㩿㫄㫀㫅㪀

㪤㫆㫃㪼㪺㫌㫃㪸㫉

㪮㪼㫀㪾㪿㫋

㪠㫅㫋㪼㫅㫊㫀㫋㫐

㩿㫄㪭㪀

㪻㩿㪮㪼㫀㪾㪿㫋㪀

㪆㪻㪣㫆㪾㩿㪤㪮㪀 㪮㪼㫀㪾㪿㫋㩷㩼

㪋㪏㪅㪍㪌 㪋㪐㪉 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪏㪅㪏㪌 㪋㪍㪎 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪐㪅㪇㪌 㪋㪋㪋 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪐㪅㪉㪌 㪋㪉㪉 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪐㪅㪋㪌 㪋㪇㪉 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪐㪅㪍㪌 㪊㪏㪊 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪫㪸㪹㫃㪼㩷㪉㪄㩷㪊

㪫㪪㪄㪜㪇㪎㪎㪢㪡 㪘㫋㫋㪸㪺㪿㫄㪼㫅㫋㩷㪎

Page 13/25
㪫㪸㪹㫃㪼㩷㪊㩷㩷㩷㩷㩷㩷㩷㪤㫆㫃㪼㪺㫌㫃㪸㫉㩷㪮㪼㫀㪾㪿㫋㩷㪛㪸㫋㪸 㪪㪌㪇㪎㪌㪇㪈

㪪㪸㫄㫇㫃㪼 䋺㩷㪣㫆㫋㪅㩷㪤㪤㪪㪉㪇㪊㪊䇭㪘㪊 㪤㫅 䋺㩷㪈㪈㪉㪇㪇㪇

㪦㫇㪼㫉㪸㫋㫆㫉 䋺㩷㪘㪢㪘㪪㪘㪢㪘 㪤㫎 䋺㩷㪉㪊㪏㪇㪇㪇

㪛㪸㫋㪼 䋺㩷㪉㪇㪈㪊㪅㪉㪅㪉㪇 㪤㫑 䋺㩷㪌㪇㪍㪇㪇㪇

㪤㫎㪆㪤㫅 䋺㩷㪉㪅㪈㪊

㪤㫑㪆㪤㫎 䋺㩷㪉㪅㪈㪊

㪜㫃㫀㫋㫌㫀㫆㫅㩷㪫㫀㫄㪼

㩿㫄㫀㫅㪀

㪤㫆㫃㪼㪺㫌㫃㪸㫉

㪮㪼㫀㪾㪿㫋

㪠㫅㫋㪼㫅㫊㫀㫋㫐

㩿㫄㪭㪀

㪻㩿㪮㪼㫀㪾㪿㫋㪀

㪆㪻㪣㫆㪾㩿㪤㪮㪀 㪮㪼㫀㪾㪿㫋㩷㩼

㪉㪏㪅㪇㪍 㪊㪈㪎㪇㪍㪍㪊 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪈㪇㪇㪅㪇㪇㪇

㪉㪏㪅㪉㪍 㪉㪏㪋㪍㪏㪐㪌 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪈 㪐㪐㪅㪐㪐㪏

㪉㪏㪅㪋㪍 㪉㪌㪌㪍㪏㪉㪊 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪊 㪐㪐㪅㪐㪐㪇

㪉㪏㪅㪍㪍 㪉㪉㪐㪍㪏㪐㪋 㪇㪅㪇㪇㪊 㪇㪅㪇㪇㪎 㪐㪐㪅㪐㪍㪏

㪉㪏㪅㪏㪍 㪉㪇㪍㪊㪐㪉㪍 㪇㪅㪇㪇㪍 㪇㪅㪇㪈㪊 㪐㪐㪅㪐㪉㪈

㪉㪐㪅㪇㪍 㪈㪏㪌㪌㪇㪏㪈 㪇㪅㪇㪈㪈 㪇㪅㪇㪉㪋 㪐㪐㪅㪏㪊㪌

㪉㪐㪅㪉㪌 㪈㪍㪍㪎㪏㪉㪌 㪇㪅㪇㪈㪎 㪇㪅㪇㪊㪏 㪐㪐㪅㪍㪐㪈

㪉㪐㪅㪋㪌 㪈㪋㪐㪐㪏㪏㪌 㪇㪅㪇㪉㪌 㪇㪅㪇㪌㪍 㪐㪐㪅㪋㪎㪈

㪉㪐㪅㪍㪌 㪈㪊㪋㪐㪉㪊㪐 㪇㪅㪇㪊㪌 㪇㪅㪇㪎㪐 㪐㪐㪅㪈㪌㪏

㪉㪐㪅㪏㪌 㪈㪉㪈㪋㪇㪎㪍 㪇㪅㪇㪋㪍 㪇㪅㪈㪇㪋 㪐㪏㪅㪎㪊㪌

㪊㪇㪅㪇㪌 㪈㪇㪐㪉㪎㪎㪌 㪇㪅㪇㪌㪏 㪇㪅㪈㪊㪉 㪐㪏㪅㪈㪐㪈

㪊㪇㪅㪉㪌 㪐㪏㪊㪏㪏㪐 㪇㪅㪇㪎㪈 㪇㪅㪈㪍㪊 㪐㪎㪅㪌㪈㪌

㪊㪇㪅㪋㪌 㪏㪏㪍㪈㪉㪌 㪇㪅㪇㪏㪌 㪇㪅㪈㪐㪍 㪐㪍㪅㪍㪐㪍

㪊㪇㪅㪍㪌 㪎㪐㪏㪊㪉㪋 㪇㪅㪈㪇㪈 㪇㪅㪉㪊㪉 㪐㪌㪅㪎㪉㪈

㪊㪇㪅㪏㪌 㪎㪈㪐㪋㪌㪉 㪇㪅㪈㪈㪎 㪇㪅㪉㪎㪉 㪐㪋㪅㪌㪎㪎

㪊㪈㪅㪇㪌 㪍㪋㪏㪌㪏㪉 㪇㪅㪈㪊㪍 㪇㪅㪊㪈㪌 㪐㪊㪅㪉㪋㪐

㪊㪈㪅㪉㪌 㪌㪏㪋㪏㪏㪍 㪇㪅㪈㪌㪌 㪇㪅㪊㪍㪈 㪐㪈㪅㪎㪉㪊

㪊㪈㪅㪋㪌 㪌㪉㪎㪍㪉㪉 㪇㪅㪈㪎㪍 㪇㪅㪋㪈㪇 㪏㪐㪅㪐㪏㪐

㪊㪈㪅㪍㪌 㪋㪎㪍㪈㪉㪎 㪇㪅㪈㪐㪎 㪇㪅㪋㪍㪉 㪏㪏㪅㪇㪊㪍

㪊㪈㪅㪏㪌 㪋㪉㪐㪏㪇㪎 㪇㪅㪉㪈㪐 㪇㪅㪌㪈㪌 㪏㪌㪅㪏㪌㪎

㪊㪉㪅㪇㪌 㪊㪏㪏㪈㪊㪇 㪇㪅㪉㪋㪈 㪇㪅㪌㪍㪐 㪏㪊㪅㪋㪋㪐

㪊㪉㪅㪉㪌 㪊㪌㪇㪍㪉㪇 㪇㪅㪉㪍㪊 㪇㪅㪍㪉㪋 㪏㪇㪅㪏㪇㪍

㪊㪉㪅㪋㪌 㪊㪈㪍㪏㪌㪇 㪇㪅㪉㪏㪍 㪇㪅㪍㪏㪈 㪎㪎㪅㪐㪉㪍

㪊㪉㪅㪍㪌 㪉㪏㪍㪋㪊㪐 㪇㪅㪊㪇㪐 㪇㪅㪎㪊㪎 㪎㪋㪅㪏㪈㪇

㪊㪉㪅㪏㪌 㪉㪌㪐㪇㪋㪊 㪇㪅㪊㪊㪈 㪇㪅㪎㪐㪊 㪎㪈㪅㪋㪍㪇

㪊㪊㪅㪇㪌 㪉㪊㪋㪊㪌㪏 㪇㪅㪊㪌㪉 㪇㪅㪏㪋㪎 㪍㪎㪅㪏㪏㪉

㪊㪊㪅㪉㪌 㪉㪈㪉㪈㪇㪎 㪇㪅㪊㪎㪊 㪇㪅㪐㪇㪇 㪍㪋㪅㪇㪏㪍

㪊㪊㪅㪋㪌 㪈㪐㪉㪇㪋㪊 㪇㪅㪊㪐㪈 㪇㪅㪐㪋㪏 㪍㪇㪅㪇㪏㪐

㪊㪊㪅㪍㪌 㪈㪎㪊㪐㪋㪎 㪇㪅㪋㪇㪎 㪇㪅㪐㪐㪉 㪌㪌㪅㪐㪈㪇

㪊㪊㪅㪏㪌 㪈㪌㪎㪍㪉㪇 㪇㪅㪋㪉㪈 㪈㪅㪇㪉㪏 㪌㪈㪅㪌㪎㪐

㪊㪋㪅㪇㪌 㪈㪋㪉㪏㪏㪋 㪇㪅㪋㪊㪇 㪈㪅㪇㪌㪍 㪋㪎㪅㪈㪊㪇

㪊㪋㪅㪉㪌 㪈㪉㪐㪌㪎㪐 㪇㪅㪋㪊㪌 㪈㪅㪇㪎㪊 㪋㪉㪅㪍㪇㪍

㪊㪋㪅㪋㪌 㪈㪈㪎㪌㪍㪊 㪇㪅㪋㪊㪌 㪈㪅㪇㪎㪍 㪊㪏㪅㪇㪍㪈

㪊㪋㪅㪍㪌 㪈㪇㪍㪎㪇㪎 㪇㪅㪋㪉㪎 㪈㪅㪇㪍㪊 㪊㪊㪅㪌㪌㪐

㪊㪋㪅㪏㪌 㪐㪍㪏㪐㪌 㪇㪅㪋㪈㪊 㪈㪅㪇㪊㪈 㪉㪐㪅㪈㪎㪊

㪊㪌㪅㪇㪌 㪏㪏㪇㪉㪋 㪇㪅㪊㪐㪈 㪇㪅㪐㪏㪈 㪉㪋㪅㪐㪏㪈

㪊㪌㪅㪉㪌 㪏㪇㪇㪇㪇 㪇㪅㪊㪍㪈 㪇㪅㪐㪈㪈 㪉㪈㪅㪇㪍㪈

㪊㪌㪅㪋㪌 㪎㪉㪎㪋㪈 㪇㪅㪊㪉㪎 㪇㪅㪏㪉㪏 㪈㪎㪅㪋㪎㪎

㪊㪌㪅㪍㪌 㪍㪍㪈㪎㪈 㪇㪅㪉㪏㪐 㪇㪅㪎㪊㪌 㪈㪋㪅㪉㪎㪐

㪊㪌㪅㪏㪌 㪍㪇㪉㪉㪈 㪇㪅㪉㪋㪏 㪇㪅㪍㪊㪍 㪈㪈㪅㪋㪐㪉

㪊㪍㪅㪇㪌 㪌㪋㪏㪊㪊 㪇㪅㪉㪇㪐 㪇㪅㪌㪊㪍 㪐㪅㪈㪉㪋

㪊㪍㪅㪉㪌 㪋㪐㪐㪌㪇 㪇㪅㪈㪎㪈 㪇㪅㪋㪋㪈 㪎㪅㪈㪍㪋

㪊㪍㪅㪋㪌 㪋㪌㪌㪉㪋 㪇㪅㪈㪊㪎 㪇㪅㪊㪌㪌 㪌㪅㪌㪏㪇

㪊㪍㪅㪍㪌 㪋㪈㪌㪈㪇 㪇㪅㪈㪇㪎 㪇㪅㪉㪏㪇 㪋㪅㪊㪉㪌

㪊㪍㪅㪏㪌 㪊㪎㪏㪍㪏 㪇㪅㪇㪏㪊 㪇㪅㪉㪈㪎 㪊㪅㪊㪋㪐

㪊㪎㪅㪇㪌 㪊㪋㪌㪍㪊 㪇㪅㪇㪍㪊 㪇㪅㪈㪍㪏 㪉㪅㪌㪐㪏

㪊㪎㪅㪉㪌 㪊㪈㪌㪍㪊 㪇㪅㪇㪋㪏 㪇㪅㪈㪉㪏 㪉㪅㪇㪉㪌

㪊㪎㪅㪋㪌 㪉㪏㪏㪊㪎 㪇㪅㪇㪊㪎 㪇㪅㪇㪐㪏 㪈㪅㪌㪐㪈

㪫㪸㪹㫃㪼㩷㪊㪄㩷㪈

㪫㪪㪄㪜㪇㪎㪎㪢㪡 㪘㫋㫋㪸㪺㪿㫄㪼㫅㫋㩷㪎

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  CBI    CBI 
㪫㪸㪹㫃㪼㩷㪊㩷㩷㩷㩷㩷㩷㩷㪤㫆㫃㪼㪺㫌㫃㪸㫉㩷㪮㪼㫀㪾㪿㫋㩷㪛㪸㫋㪸 㪪㪌㪇㪎㪌㪇㪈

㪜㫃㫀㫋㫌㫀㫆㫅㩷㪫㫀㫄㪼

㩿㫄㫀㫅㪀

㪤㫆㫃㪼㪺㫌㫃㪸㫉

㪮㪼㫀㪾㪿㫋

㪠㫅㫋㪼㫅㫊㫀㫋㫐

㩿㫄㪭㪀

㪻㩿㪮㪼㫀㪾㪿㫋㪀

㪆㪻㪣㫆㪾㩿㪤㪮㪀 㪮㪼㫀㪾㪿㫋㩷㩼

㪊㪎㪅㪍㪌 㪉㪍㪊㪍㪈 㪇㪅㪇㪉㪏 㪇㪅㪇㪎㪌 㪈㪅㪉㪍㪈

㪊㪎㪅㪏㪌 㪉㪋㪈㪇㪐 㪇㪅㪇㪉㪈 㪇㪅㪇㪌㪎 㪈㪅㪇㪈㪈

㪊㪏㪅㪇㪌 㪉㪉㪇㪍㪉 㪇㪅㪇㪈㪍 㪇㪅㪇㪋㪋 㪇㪅㪏㪉㪇

㪊㪏㪅㪉㪌 㪉㪇㪈㪐㪐 㪇㪅㪇㪈㪉 㪇㪅㪇㪊㪋 㪇㪅㪍㪎㪋

㪊㪏㪅㪋㪌 㪈㪏㪌㪇㪊 㪇㪅㪇㪈㪇 㪇㪅㪇㪉㪎 㪇㪅㪌㪍㪈

㪊㪏㪅㪍㪌 㪈㪍㪐㪌㪐 㪇㪅㪇㪇㪏 㪇㪅㪇㪉㪈 㪇㪅㪋㪎㪉

㪊㪏㪅㪏㪌 㪈㪌㪌㪌㪉 㪇㪅㪇㪇㪍 㪇㪅㪇㪈㪎 㪇㪅㪋㪇㪈

㪊㪐㪅㪇㪌 㪈㪋㪉㪎㪇 㪇㪅㪇㪇㪌 㪇㪅㪇㪈㪋 㪇㪅㪊㪋㪋

㪊㪐㪅㪉㪌 㪈㪊㪈㪇㪈 㪇㪅㪇㪇㪋 㪇㪅㪇㪈㪉 㪇㪅㪉㪐㪎

㪊㪐㪅㪋㪌 㪈㪉㪇㪊㪋 㪇㪅㪇㪇㪋 㪇㪅㪇㪈㪈 㪇㪅㪉㪌㪌

㪊㪐㪅㪍㪌 㪈㪈㪇㪍㪈 㪇㪅㪇㪇㪋 㪇㪅㪇㪈㪇 㪇㪅㪉㪈㪎

㪊㪐㪅㪏㪌 㪈㪇㪈㪎㪉 㪇㪅㪇㪇㪊 㪇㪅㪇㪇㪐 㪇㪅㪈㪏㪉

㪋㪇㪅㪇㪌 㪐㪊㪍㪇 㪇㪅㪇㪇㪊 㪇㪅㪇㪇㪏 㪇㪅㪈㪌㪇

㪋㪇㪅㪉㪌 㪏㪍㪈㪏 㪇㪅㪇㪇㪉 㪇㪅㪇㪇㪎 㪇㪅㪈㪉㪊

㪋㪇㪅㪋㪌 㪎㪐㪊㪐 㪇㪅㪇㪇㪉 㪇㪅㪇㪇㪌 㪇㪅㪈㪇㪈

㪋㪇㪅㪍㪌 㪎㪊㪈㪐 㪇㪅㪇㪇㪉 㪇㪅㪇㪇㪌 㪇㪅㪇㪏㪉

㪋㪇㪅㪏㪌 㪍㪎㪌㪈 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪋 㪇㪅㪇㪍㪍

㪋㪈㪅㪇㪌 㪍㪉㪊㪇 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪋 㪇㪅㪇㪌㪉

㪋㪈㪅㪉㪌 㪌㪎㪌㪋 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪊 㪇㪅㪇㪋㪇

㪋㪈㪅㪋㪌 㪌㪊㪈㪎 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪊 㪇㪅㪇㪊㪇

㪋㪈㪅㪍㪌 㪋㪐㪈㪍 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪉 㪇㪅㪇㪉㪈

㪋㪈㪅㪏㪌 㪋㪌㪋㪐 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪉 㪇㪅㪇㪈㪌

㪋㪉㪅㪇㪌 㪋㪉㪈㪉 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪉 㪇㪅㪇㪇㪐

㪋㪉㪅㪉㪌 㪊㪐㪇㪉 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪌

㪋㪉㪅㪋㪌 㪊㪍㪈㪎 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪈 㪇㪅㪇㪇㪈

㪋㪉㪅㪍㪌 㪊㪊㪌㪌 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪉㪅㪏㪌 㪊㪈㪈㪌 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪊㪅㪇㪌 㪉㪏㪐㪊 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪊㪅㪉㪌 㪉㪍㪏㪐 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪊㪅㪋㪌 㪉㪌㪇㪈 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪊㪅㪍㪌 㪉㪊㪉㪏 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪊㪅㪏㪌 㪉㪈㪍㪐 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪋㪅㪇㪌 㪉㪇㪉㪈 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪋㪅㪉㪌 㪈㪏㪏㪌 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪋㪅㪋㪌 㪈㪎㪍㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪋㪅㪍㪌 㪈㪍㪋㪋 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪋㪅㪏㪌 㪈㪌㪊㪍 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪌㪅㪇㪌 㪈㪋㪊㪎 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪌㪅㪉㪌 㪈㪊㪋㪌 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪌㪅㪋㪌 㪈㪉㪍㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪌㪅㪍㪌 㪈㪈㪏㪈 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪌㪅㪏㪌 㪈㪈㪇㪏 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪍㪅㪇㪌 㪈㪇㪋㪈 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪍㪅㪉㪌 㪐㪎㪏 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪍㪅㪋㪌 㪐㪉㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪍㪅㪍㪌 㪏㪍㪌 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪍㪅㪏㪌 㪏㪈㪌 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪎㪅㪇㪌 㪎㪍㪏 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪎㪅㪉㪌 㪎㪉㪋 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪎㪅㪋㪌 㪍㪏㪋 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪎㪅㪍㪌 㪍㪋㪍 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪎㪅㪏㪌 㪍㪈㪈 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪏㪅㪇㪌 㪌㪎㪏 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪏㪅㪉㪌 㪌㪋㪏 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪏㪅㪋㪌 㪌㪈㪐 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪫㪸㪹㫃㪼㩷㪊㪄㩷㪉

㪫㪪㪄㪜㪇㪎㪎㪢㪡 㪘㫋㫋㪸㪺㪿㫄㪼㫅㫋㩷㪎

Page 15/25
㪫㪸㪹㫃㪼㩷㪊㩷㩷㩷㩷㩷㩷㩷㪤㫆㫃㪼㪺㫌㫃㪸㫉㩷㪮㪼㫀㪾㪿㫋㩷㪛㪸㫋㪸 㪪㪌㪇㪎㪌㪇㪈

㪜㫃㫀㫋㫌㫀㫆㫅㩷㪫㫀㫄㪼

㩿㫄㫀㫅㪀

㪤㫆㫃㪼㪺㫌㫃㪸㫉

㪮㪼㫀㪾㪿㫋

㪠㫅㫋㪼㫅㫊㫀㫋㫐

㩿㫄㪭㪀

㪻㩿㪮㪼㫀㪾㪿㫋㪀

㪆㪻㪣㫆㪾㩿㪤㪮㪀 㪮㪼㫀㪾㪿㫋㩷㩼

㪋㪏㪅㪍㪌 㪋㪐㪉 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪏㪅㪏㪌 㪋㪍㪎 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪐㪅㪇㪌 㪋㪋㪋 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪐㪅㪉㪌 㪋㪉㪉 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪐㪅㪋㪌 㪋㪇㪉 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪋㪐㪅㪍㪌 㪊㪏㪊 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇 㪇㪅㪇㪇㪇

㪫㪸㪹㫃㪼㩷㪊㪄㩷㪊

㪫㪪㪄㪜㪇㪎㪎㪢㪡 㪘㫋㫋㪸㪺㪿㫄㪼㫅㫋㩷㪎

Page 16/25
10 20 30 40 50 60

-0.4-0.6-0.8-1.0-1.2-1.4-1.6-1.8-2.0

504540353025201510

Date :

Sample : Solvent :Concentration : Flow Rate :Injection Volume : Detector :Apparatus : Temperature :Column : Operator :

2013.2.20

Shodex HFIP-LG(1), HFIP-806M(2) AKASAKAGPC(14) 40.0°C

MMS2023 A1 0.100 % 0.494 mL/min0.200 mL RI-2414 (256X), LS 

HFIP(5mM NaTFA)

Fig . 1 Gel Permeation Chromatogram

Toray Research Center Inc.

File: A14

Retention Time (min)

V

m

y

ti

s

n

e

t

n

II

R

V

m

y

ti

s

n

e

t

n

I

S

L

LS Curve

RI Curve

㪫㪪㪄㪜㪇㪎㪎㪢㪡 㪘㫋㫋㪸㪺㪿㫄㪼㫅㫋㩷㪎

Page 17/25

CBI

CBI
10 20 30 40 50 60

-0.4-0.6-0.8-1.0-1.2-1.4-1.6-1.8-2.0

504540353025201510

Date :

Sample : Solvent :Concentration : Flow Rate :Injection Volume : Detector :Apparatus : Temperature :Column : Operator :

2013.2.20

Shodex HFIP-LG(1), HFIP-806M(2) AKASAKAGPC(14) 40.0°C

MMS2023 A2 0.101 % 0.494 mL/min0.200 mL RI-2414 (256X), LS 

HFIP(5mM NaTFA)

Fig . 2 Gel Permeation Chromatogram

Toray Research Center Inc.

File: A09

Retention Time (min)

V

m

y

ti

s

n

e

t

n

II

R

V

m

y

ti

s

n

e

t

n

I

S

L

RI Curve

LS Curve

㪫㪪㪄㪜㪇㪎㪎㪢㪡 㪘㫋㫋㪸㪺㪿㫄㪼㫅㫋㩷㪎

Page 18/25

CBI

CBI
10 20 30 40 50 60

-0.4-0.6-0.8-1.0-1.2-1.4-1.6-1.8-2.0

504540353025201510

Date :

Sample : Solvent :Concentration : Flow Rate :Injection Volume : Detector :Apparatus : Temperature :Column : Operator :

2013.2.20

Shodex HFIP-LG(1), HFIP-806M(2) AKASAKAGPC(14) 40.0°C

MMS2023 A3 0.103 % 0.494 mL/min0.200 mL RI-2414 (256X), LS 

HFIP(5mM NaTFA)

Fig . 3 Gel Permeation Chromatogram

Toray Research Center Inc.

File: A10

Retention Time (min)

V

m

y

ti

s

n

e

t

n

II

R

V

m

y

ti

s

n

e

t

n

I

S

L

LS Curve

RI Curve

㪫㪪㪄㪜㪇㪎㪎㪢㪡 㪘㫋㫋㪸㪺㪿㫄㪼㫅㫋㩷㪎

Page 19/25

CBI

CBI
10 20 30 40 50 60

-0.4-0.6-0.8-1.0-1.2-1.4-1.6-1.8-2.0

504540353025201510

Date :

Sample : Solvent :Concentration : Flow Rate :Injection Volume : Detector :Apparatus : Temperature :Column : Operator :

2013.2.20

Shodex HFIP-LG(1), HFIP-806M(2) AKASAKAGPC(14) 40.0°C

-0.200 mL RI-2414 (256X), LS 

0.494 mL/min

Blank HFIP(5mM NaTFA)

Fig . 4 Gel Permeation Chromatogram

Toray Research Center Inc.

File: A12

Retention Time (min)

V

m

y

ti

s

n

e

t

n

II

R

V

m

y

ti

s

n

e

t

n

I

S

L

LS Curve

RI Curve

㪫㪪㪄㪜㪇㪎㪎㪢㪡 㪘㫋㫋㪸㪺㪿㫄㪼㫅㫋㩷㪎

Page 20/25

CBI
28 30 32 34 36 38 40 42 44 46 48 50

9876543210

10

Sample : Detector :Apparatus : Temperature :Column : Operator :Solvent : Date :Flow Rate :

GPC(14) 40.0Shodex HFIP-LG(1), HFIP-806M(2) AKASAKAHFIP(5mM NaTFA) 2013.2.200.494 mL/min

°C

PMMA (S-2033) RI-2414 (256X), LS

Fig . 5 Calibration Curve

Toray Research Center Inc.

File: CC-9.BXX

Log(MW) = A(0) + A(1)T + A(2)T2+ A(3)T3+ ・・・ Coefficient(Order: 3) A(0) : 13.36413 A(1) : -0.2194237 A(2) : -2.118073E-03 A(3) : 4.348887E-05 Molecular Weight Data RT(min) MW 30.04 1109389 31.14 640404

33.05 22838835.14 7623938.18 2127240.97 699844.92 187546.28 85846.78 65049.60 418

Retention Time (min)

th

g

i

eW

ra

l

uce

l

o

M

g

o

L

㪫㪪㪄㪜㪇㪎㪎㪢㪡 㪘㫋㫋㪸㪺㪿㫄㪼㫅㫋㩷㪎

Page 21/25

CBI

CBI
102 103 104 105 106 107 108

2.01.81.61.41.21.00.80.60.40.20.0

Mn : Mv : Operator :Mw : Mw/Mn : Date :Mz : Mz/Mw :

 108000 AKASAKA 234000 2.17 2013.2.20 493000 2.11

Sample: MMS2023 A1

Fig . 6 Molecular Weight Distribution Curve

File: A14(A1).MWD

Toray Research Center Inc. Molecular Weight

M

g

o

L

d

/

W

d

㪫㪪㪄㪜㪇㪎㪎㪢㪡 㪘㫋㫋㪸㪺㪿㫄㪼㫅㫋㩷㪎

Page 22/25

CBI

CBI CBI

CBI
102 103 104 105 106 107 108

2.01.81.61.41.21.00.80.60.40.20.0

Mn : Mv : Operator :Mw : Mw/Mn : Date :Mz : Mz/Mw :

 108000 AKASAKA 231000 2.14 2013.2.20 474000 2.05

Sample: MMS2023 A2

Fig . 7 Molecular Weight Distribution Curve

File: A09(A2).MWD

Toray Research Center Inc. Molecular Weight

M

g

o

L

d

/

W

d

㪫㪪㪄㪜㪇㪎㪎㪢㪡 㪘㫋㫋㪸㪺㪿㫄㪼㫅㫋㩷㪎

Page 23/25

CBI

CBI

CBI

CBI
102 103 104 105 106 107 108

2.01.81.61.41.21.00.80.60.40.20.0

Mn : Mv : Operator :Mw : Mw/Mn : Date :Mz : Mz/Mw :

 112000 AKASAKA 238000 2.13 2013.2.20 506000 2.13

Sample: MMS2023 A3

Fig . 8 Molecular Weight Distribution Curve

File: A10(A3).MWD

Toray Research Center Inc. Molecular Weight

M

g

o

L

d

/

W

d

㪫㪪㪄㪜㪇㪎㪎㪢㪡 㪘㫋㫋㪸㪺㪿㫄㪼㫅㫋㩷㪎

Page 24/25

CBI CBI

CBI

CBI
10 20 30 40 50 60

0.0

-0.2-0.4-0.6-0.8-1.0-1.2

0.40.20.0

504540353025201510

Date :

Sample : Solvent :Concentration : Flow Rate :Injection Volume : Detector :Apparatus : Temperature :Column : Operator :

2013.2.20

Shodex HFIP-LG(1), HFIP-806M(2) AKASAKAGPC(14) 40.0°C

PMMA (20600) 0.100 % 0.494 mL/min0.200 mL RI-2414 (64X), LS 

HFIP(5mM NaTFA)

Fig . 9 Gel Permeation Chromatogram

Toray Research Center Inc.

File: A01

Retention Time (min)

V

m

y

ti

s

n

e

t

n

II

R

V

m

y

ti

s

n

e

t

n

I

S

L

LS Curve

RI Curve

㪫㪪㪄㪜㪇㪎㪎㪢㪡 㪘㫋㫋㪸㪺㪿㫄㪼㫅㫋㩷㪎

Page 25/25

CBI