# ANALYTICAL REPORT Job Number: 500-53491-1 Job Description: John Deere Des Moines Works (JDDMW) For: Project Integration, Inc 1097 Highway 101 South Suite D-16 Greer, SC 29651 Attention: Mr. Robert Stevens

_____________________________________________Approved for release. Donna L Ingersoll Project Manager II 1/9/2013 2:46 PM 

# Donna L Ingersoll Project Manager II donna.ingersoll@testamericainc.com

01/09/2013

cc:Mr. David Kirby Mr. Robert Malcomson 

## These test results meet all the requirements of NELAC for accredited parameters. The Lab Certification ID# is 100201.
All questions regarding this test report should be directed to the TestAmerica Project Manager whose signature appears on this report. All pages of this report are integral parts of the analytical data. Therefore, this report should be reproduced only in its entirety.
Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable.
TestAmerica Laboratories, Inc. TestAmerica Chicago 2417 Bond Street, University Park, IL 60484 Tel (708) 534-5200 Fax (708) 534-5211www.testamericainc.com 

## 01/09/2013 Page 1 of 384

# Table of Contents

Cover Title Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 Data Summaries . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 Report Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 5 Manual Integration Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 6 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 8 Executive Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 9 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 11 Method / Analyst Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 13 Sample Datasheets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 14 Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 30 QC Data Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 33 Data Qualifiers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 58 QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 59 Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 67 Reagent Traceability . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 75 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 111 Organic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .112 GC/MS VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 112 Method 8260B . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 112 Method 8260B QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 113 Method 8260B Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 135 Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 141 Method 8260B ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 141 Method 8260B CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 175 Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 196 Method 8260B Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 196

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# Table of Contents
Method 8260B LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 199 Method 8260B Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 203 Method 8260B Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 209 Inorganic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .212 Metals Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 212 Met Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 213 Met Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 214 Met QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 219 Met ICV/CCV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 219 Met CRQL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 227 Met Blanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 231 Met ICSA/ICSAB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 246 Met MS/MSD/PDS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 250 Met Dup/Trip . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 251 Met LCS/LCSD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 252 Met MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 258 Met Linear Ranges . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 270 Met Preparation Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 274 Met Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 280 Met Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 289 General Chemistry Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 297 Gen Chem Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 298 Gen Chem Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 299 Gen Chem QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 304 Gen Chem ICV/CCV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 304 Gen Chem Blanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 308

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# Table of Contents
Gen Chem MS/MSD/PDS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 309 Gen Chem LCS/LCSD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 313 Gen Chem MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 315 Gen Chem Preparation Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 333 Gen Chem Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 341 Gen Chem Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 356 Shipping and Receiving Documents . . . . . . . . . . . . . . . . . . . . . . . . . . .378 Client Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 383 Sample Receipt Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 384

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### Job Narrative 500-53491-1 Comments 

### No additional comments. Receipt 

### The samples were received on 12/22/ 201211:30 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 1.3o C. Except: Cr+6 past hold time. GC/MS VOA 

### No analytical or quality issues were noted. Metals 

### No analytical or quality issues were noted. General Chemistry 

### Method(s) 9071B: The oil and grease matrix spike / matrix spike duplicate (MS/MSD) recoveries for sample 500-53491-1 in batch 174372 were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria. No other analytical or quality issues were noted.



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### Lab Name: Job No.: SDG No.: GC/MS VOA MANUAL INTEGRATION SUMMARY
TestAmerica Chicago 500-53491-1

Instrument ID: Analysis Batch Number: CMS06 171819 Lab Sample ID: Client Sample ID: Date Analyzed: Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATE ANALYST REASON STD1 500-171819/2 IC 6I1204a.d 12/04/12 14:34 GC Column:DB624 ID:0.2(mm)

Trichloroethene Baseline drabekd 12/04/12 15:38 5.83 Dibromochloromethane Baseline drabekd 12/04/12 15:38 8.17 Lab Sample ID: Client Sample ID: Date Analyzed: Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATE ANALYST REASON STD5 500-171819/6 IC 6I1204e.d 12/04/12 16:33 GC Column:DB624 ID:0.2(mm)

Chloroethane Split Peak drabekd 12/05/12 07:59 1.71 Lab Sample ID: Client Sample ID: Date Analyzed: Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATE ANALYST REASON STD1AP 500-171819/8 IC 6J1204a.d 12/04/12 17:18 GC Column:DB624 ID:0.2(mm)

Ethyl acetate Split Peak drabekd 12/05/12 08:09 4.14 n-Butyl alcohol Poor chromatography drabekd 12/05/12 08:19 5.82 2-Nitropropane Baseline drabekd 12/05/12 08:21 6.75 trans-1,4-Dichloro-2-butene Poor chromatography drabekd 12/05/12 08:28 9.94 Pentachloroethane Split Peak drabekd 12/05/12 08:10 10.41 Lab Sample ID: Client Sample ID: Date Analyzed: Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATE ANALYST REASON STD2AP 500-171819/9 IC 6J1204b.d 12/04/12 17:41 GC Column:DB624 ID:0.2(mm)

2-Nitropropane Baseline drabekd 12/05/12 08:23 6.75

8260B 

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### Lab Name: Job No.: SDG No.: GC/MS VOA MANUAL INTEGRATION SUMMARY
TestAmerica Chicago 500-53491-1

Instrument ID: Analysis Batch Number: CMS22 172615 Lab Sample ID: Client Sample ID: Date Analyzed: Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATE ANALYST REASON STD01 500-172615/2 IC 22I1211A.D 12/11/12 14:23 GC Column:DB624 ID:0.2(mm)

Trichloroethene Baseline alikpalae 12/11/12 19:50 7.55 Lab Sample ID: Client Sample ID: Date Analyzed: Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATE ANALYST REASON STD02 500-172615/3 IC 22I1211B.D 12/11/12 14:51 GC Column:DB624 ID:0.2(mm)

Bromomethane Baseline alikpalae 12/11/12 19:54 2.01 Acetonitrile Split Peak alikpalae 12/11/12 19:54 3.59 Tetrachloroethene Split Peak alikpalae 12/11/12 19:54 9.75

8260B 

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## SAMPLE SUMMARY Client: Project Integration, Inc Job Number: 500-53491-1
Client Sample ID Lab Sample ID Client Matrix Sampled Received Date/Time Date/Time
500-53491-1 FC COMPOSITE 6 Solid 12/19/2012 1430 12/22/20121130 500-53491-2 FC D COMPOSITE 6 Solid 12/19/2012 1440 12/22/20121130 500-53491-3 FC DISCRETE 6 Solid 12/19/2012 1420 12/22/20121130 500-53491-4 FC D DISCRETE 6 Solid 12/19/2012 1445 12/22/20121130 500-53491-5 FC EB 6 Water 12/19/2012 1410 12/22/20121130 500-53491-6 TRIP BLANK Water 12/19/2012 0000 12/22/20121130

TestAmerica Chicago 

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## EXECUTIVE SUMMARY- Detections Client: Project Integration, Inc Job Number: 500-53491-1

Analyte Result Reporting Limit Units Method Lab Sample ID Client Sample ID Qualifier

500-53491-1 FC COMPOSITE 6 

### 3.70 mg/Kg 6010B 643 Barium 3.70 mg/Kg 6010B 748 Copper 3.70 mg/Kg 6010B 15000 Chromium 3.70 mg/Kg 6010B 85.5 Nickel 1.85 mg/Kg 6010B 253 B Lead 1.85 mg/Kg 6010B 253 Vanadium 7.40 mg/Kg 6010B 501 Zinc 0.0605 mg/Kg 7471A 0.232 Mercury 40.0 Degrees F 1010 >176 Flashpoint 1.88 mg/Kg 9014 1.15 J Cyanide,Total 90.4 mg/Kg 9034 778 Sulfide 0.200 SU 9045C 9.79 pH 1850 mg/Kg 9071B 16600 HEM (Oil & Grease) 0.10 % Moisture 74 Percent Moisture 0.10 % Moisture 26 Percent Solids 0.100 % SM 2540G 74.0 % Moisture 0.100 % SM 2540G 26.0 Total Solids 

### TCLP 0.500 mg/L 6010B 0.0103 J Barium 0.0250 mg/L 6010B 0.442 Copper 0.0250 mg/L 6010B 0.826 Chromium 0.0250 mg/L 6010B 0.744 Nickel 0.0250 mg/L 6010B 0.0164 J Vanadium 0.100 mg/L 6010B 0.403 Zinc 0.000200 mg/L 7470A 0.000702 B Mercury

TestAmerica Chicago 

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## EXECUTIVE SUMMARY- Detections Client: Project Integration, Inc Job Number: 500-53491-1

Analyte Result Reporting Limit Units Method Lab Sample ID Client Sample ID Qualifier
500-53491-2 FC D COMPOSITE 6 

### 3.84 mg/Kg 6010B 619 Barium 3.84 mg/Kg 6010B 707 Copper 3.84 mg/Kg 6010B 15000 Chromium 3.84 mg/Kg 6010B 86.1 Nickel 1.92 mg/Kg 6010B 244 B Lead 1.92 mg/Kg 6010B 251 Vanadium 7.68 mg/Kg 6010B 499 Zinc 0.0647 mg/Kg 7471A 0.237 Mercury 40.0 Degrees F 1010 >176 Flashpoint 1.86 mg/Kg 9014 1.29 J Cyanide,Total 94.0 mg/Kg 9034 817 Sulfide 0.200 SU 9045C 9.87 pH 1950 mg/Kg 9071B 17000 HEM (Oil & Grease) 0.10 % Moisture 75 Percent Moisture 0.10 % Moisture 25 Percent Solids 0.100 % SM 2540G 75.0 % Moisture 0.100 % SM 2540G 25.0 Total Solids 

### TCLP 0.0250 mg/L 6010B 0.0547 Copper 0.0250 mg/L 6010B 0.0624 Nickel

500-53491-3 FC DISCRETE 6 

### 963 ug/Kg 8260B 7020 Acetone 19.3 ug/Kg 8260B 11.8 J 2-Butanone (MEK) 0.10 % Moisture 74 Percent Moisture 0.10 % Moisture 26 Percent Solids

500-53491-4 FC D DISCRETE 6 

### 905 ug/Kg 8260B 7150 Acetone 18.1 ug/Kg 8260B 19.5 2-Butanone (MEK) 0.10 % Moisture 72 Percent Moisture 0.10 % Moisture 28 Percent Solids

500-53491-5 FC EB 6 

### 0.0100 mg/L 6010B 0.00111 J Copper

TestAmerica Chicago 

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## METHOD SUMMARY Client: Project Integration, Inc Job Number: 500-53491-1 Preparation Method Method Lab Location Description Matrix:Solid 

### Volatile Organic Compounds(GC/MS) TAL CHI SW846 8260B Purge andTrap TAL CHI SW846 5030B Metals (ICP) TAL CHI SW846 6010B Preparation, Metals TAL CHI SW846 3050B Metals (ICP) TAL CHI SW846 6010B TCLP Extraction TAL CHI SW846 1311 Preparation,Total Metals TAL CHI SW846 3010A Mercury (CVAA) TAL CHI SW846 7470A TCLP Extraction TAL CHI SW846 1311 Preparation, Mercury TAL CHI SW846 7470A Mercury (CVAA) TAL CHI SW846 7471A Preparation, Mercury TAL CHI SW846 7471A Ignitability, Pensky-Martens Closed-Cup Method TAL CHI SW846 1010 Chromium, Hexavalent TAL CHI SW846 7196A Alkaline Digestion (Chromium, Hexavalent) TAL CHI SW846 3060A Cyanide TAL CHI SW846 9014 Cyanide, Distillation TAL CHI SW846 9010B Sulfide, Acid soluble and Insoluble (Titrimetric) TAL CHI SW846 9034 Sulfide, Distillation (Acid Soluble and Insoluble) TAL CHI SW846 9030B Sulfide, Reactive TAL CHI SW846 9034 Sulfide, Reactive TAL CHI SW846 7.3.4 pH TAL CHI SW846 9045C HEM and SGT-HEM TAL CHI SW846 9071B Preparation, HEM and SGT-HEM TAL CHI SW846 9071B Percent Moisture TAL CHI EPA Moisture Total, Fixed,andVolatile Solids TAL CHI SM SM 2540G Matrix:Water 

### Volatile Organic Compounds(GC/MS) TAL CHI SW846 8260B Purge andTrap TAL CHI SW846 5030B Metals (ICP) TAL CHI SW846 6010B Preparation,Total Metals TAL CHI SW846 3010A Mercury (CVAA) TAL CHI SW846 7470A Preparation, Mercury TAL CHI SW846 7470A HEM and SGT-HEM TAL CHI 1664A1664A HEM and SGT-HEM (SPE) TAL CHI 1664A1664A Chromium, Hexavalent TAL CHI SW846 7196A Cyanide TAL CHI SW846 9014 Cyanide, Distillation TAL CHI SW846 9010B Sulfide, Acid soluble and Insoluble (Titrimetric) TAL CHI SW846 9034 Sulfide, Reactive TAL CHI SW846 9034 Sulfide, Reactive TAL CHI SW846 7.3.4 TestAmerica Chicago 

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## METHOD SUMMARY Client: Project Integration, Inc Job Number: 500-53491-1 Preparation Method Method Lab Location Description Lab References: TAL CHI=TestAmerica Chicago 

### Method References: 1664A=EPA-821-98-002 EPA=US Environmental ProtectionAgency SM = "Standard Methods For The Examination Of Water And Wastewater " SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TestAmerica Chicago 

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## METHOD /ANALYST SUMMARY Client: Project Integration, Inc Job Number: 500-53491-1

Method Analyst Analyst ID Arndt, Brett D BDA SW846 8260B Drabek, Dave J DJD SW846 8260B Manzano, Louis LM SW846 8260B Jones, Paul PJ SW846 6010B Bills, Brandon J BJB SW846 7470A Bills, Brandon J BJB SW846 7471A Wasowicz, Andrew P APW SW846 1010 Brogan,MaryT MTB 1664A1664A Wasowicz, Andrew P APW SW846 7196A Treadwell,ElianeA EAT SW846 9014 Boyd, Cheryl L CLB SW846 9034 Moore, Colleen L CLM SW846 9034 Moore, Colleen L CLM SW846 9045C Brogan,MaryT MTB SW846 9071B Veldhuizen, Chris M CMV EPA Moisture Veldhuizen, Chris M CMV SM SM 2540G

TestAmerica Chicago 

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53491-1 Client Sample ID: 

### Lab Sample ID: FC DISCRETE 6


### Client Matrix: % Moisture: 74.1 500-53491-3 Solid Date Sampled: 12/19/2012 1420 Date Received: 12/22/20121130 8260BVolatile Organic Compounds(GC/MS)



### Dilution: 12/27/2012 1336 12/27/2012 1336 1.0 8260B

FinalWeight /Volume: InitialWeight /Volume: Lab File ID: Instrument ID: 3491-03.d 5 g 5 mL 5030B CMS06
Analysis Date: Prep Date: Analysis Batch: Prep Batch: 500-173973 N/A Analysis Method: Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL 11.8 J 19.3 6.98 2-Butanone (MEK) Surrogate %Rec Acceptance Limits Qualifier 89 70 - 134 1,2-Dichloroethane-d4 (Surr) 87 75 - 122 Toluene-d8 (Surr) 79 70 - 122 4-Bromofluorobenzene (Surr) 95 75 - 120 Dibromofluoromethane

TestAmerica Chicago 

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53491-1 Client Sample ID: 

### Lab Sample ID: FC DISCRETE 6


### Client Matrix: % Moisture: 74.1 500-53491-3 Solid Date Sampled: 12/19/2012 1420 Date Received: 12/22/20121130 8260BVolatile Organic Compounds(GC/MS)



### Dilution: 12/27/2012 1028 12/28/20121108 50 8260B

FinalWeight /Volume: InitialWeight /Volume: Lab File ID: Instrument ID: 53491-03.D 5 g 5 mL RunType: DL 5030B CMS18
Analysis Date: Prep Date: Analysis Batch: Prep Batch: 500-174064 500-173990 Analysis Method: Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL 7020 963 251 Acetone Surrogate %Rec Acceptance Limits Qualifier 97 75 - 125 1,2-Dichloroethane-d4 (Surr) 96 75 - 120 Toluene-d8 (Surr) 94 75 - 120 4-Bromofluorobenzene (Surr) 93 75 - 120 Dibromofluoromethane

TestAmerica Chicago 

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53491-1 Client Sample ID: 

### Lab Sample ID: FC D DISCRETE 6


### Client Matrix: % Moisture: 72.4 500-53491-4 Solid Date Sampled: 12/19/2012 1445 Date Received: 12/22/20121130 8260BVolatile Organic Compounds(GC/MS)



### Dilution: 12/27/2012 1359 12/27/2012 1359 1.0 8260B

FinalWeight /Volume: InitialWeight /Volume: Lab File ID: Instrument ID: 3491-04.d 5 g 5 mL 5030B CMS06
Analysis Date: Prep Date: Analysis Batch: Prep Batch: 500-173973 N/A Analysis Method: Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL 19.5 18.1 6.55 2-Butanone (MEK) Surrogate %Rec Acceptance Limits Qualifier 91 70 - 134 1,2-Dichloroethane-d4 (Surr) 89 75 - 122 Toluene-d8 (Surr) 75 70 - 122 4-Bromofluorobenzene (Surr) 90 75 - 120 Dibromofluoromethane

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53491-1 Client Sample ID: 

### Lab Sample ID: FC D DISCRETE 6


### Client Matrix: % Moisture: 72.4 500-53491-4 Solid Date Sampled: 12/19/2012 1445 Date Received: 12/22/20121130 8260BVolatile Organic Compounds(GC/MS)



### Dilution: 12/27/2012 1028 12/28/20121131 50 8260B

FinalWeight /Volume: InitialWeight /Volume: Lab File ID: Instrument ID: 53491-04.D 5 g 5 mL RunType: DL 5030B CMS18
Analysis Date: Prep Date: Analysis Batch: Prep Batch: 500-174064 500-173990 Analysis Method: Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL 7150 905 235 Acetone Surrogate %Rec Acceptance Limits Qualifier 105 75 - 125 1,2-Dichloroethane-d4 (Surr) 101 75 - 120 Toluene-d8 (Surr) 100 75 - 120 4-Bromofluorobenzene (Surr) 96 75 - 120 Dibromofluoromethane

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53491-1 Client Sample ID: 

### Lab Sample ID: FC EB 6


### Client Matrix: 500-53491-5 Water Date Sampled: 12/19/2012 1410 Date Received: 12/22/20121130 8260BVolatile Organic Compounds(GC/MS)



### Dilution: 12/27/2012 1554 12/27/2012 1554 1.0 8260B

FinalWeight /Volume: InitialWeight /Volume: Lab File ID: Instrument ID: 53491-05.D 5 mL 5 mL 5030B CMS22
Analysis Date: Prep Date: Analysis Batch: Prep Batch: 500-173987 N/A Analysis Method: Prep Method:

Analyte Result (ug/L) Qualifier MDL RL <5.00 5.00 1.29 Acetone <5.00 5.00 1.47 2-Butanone (MEK) Surrogate %Rec Acceptance Limits Qualifier 88 75 - 125 1,2-Dichloroethane-d4 (Surr) 94 75 - 120 Toluene-d8 (Surr) 88 75 - 120 4-Bromofluorobenzene (Surr) 90 75 - 120 Dibromofluoromethane

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53491-1 Client Sample ID: 

### Lab Sample ID: TRIP BLANK


### Client Matrix: 500-53491-6 Water Date Sampled: 12/19/2012 0000 Date Received: 12/22/20121130 8260BVolatile Organic Compounds(GC/MS)



### Dilution: 12/27/2012 1528 12/27/2012 1528 1.0 8260B

FinalWeight /Volume: InitialWeight /Volume: Lab File ID: Instrument ID: 53491-06.D 5 mL 5 mL 5030B CMS22
Analysis Date: Prep Date: Analysis Batch: Prep Batch: 500-173987 N/A Analysis Method: Prep Method:

Analyte Result (ug/L) Qualifier MDL RL <5.00 5.00 1.29 Acetone <5.00 5.00 1.47 2-Butanone (MEK) Surrogate %Rec Acceptance Limits Qualifier 93 75 - 125 1,2-Dichloroethane-d4 (Surr) 100 75 - 120 Toluene-d8 (Surr) 93 75 - 120 4-Bromofluorobenzene (Surr) 93 75 - 120 Dibromofluoromethane

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53491-1 Client Sample ID: 

### Lab Sample ID: FC COMPOSITE 6


### Client Matrix: % Moisture: 73.5 500-53491-1 Solid Date Sampled: 12/19/2012 1430 Date Received: 12/22/20121130 6010B Metals (ICP) 

### 6010B Instrument ID: Lab File ID: P51226B Dilution: 1.0 InitialWeight /Volume: 1.0213 g 12/26/2012 2357 FinalWeight /Volume: 100 mL 12/24/2012 1500 3050B ICP5
Analysis Date: Prep Date: Analysis Batch: 500-173964 500-173848 Prep Batch: Analysis Method: Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL 643 3.70 0.440 Barium 748 3.70 1.00 Copper 15000 3.70 0.618 Chromium 85.5 3.70 0.810 Nickel 253 B 1.85 0.636 Lead 253 1.85 0.281 Vanadium 501 7.40 2.54 Zinc
6010B Metals (ICP)-TCLP 

### 6010B Instrument ID: Lab File ID: P51226B Dilution: 1.0 InitialWeight /Volume: 50 mL 12/26/2012 1841 FinalWeight /Volume: 50 mL 12/26/2012 0750 3010A ICP5
Analysis Date: Prep Date: Analysis Batch: 500-173964 500-173872 500-173838 Prep Batch: Analysis Method: Prep Method: Leach Batch:

12/24/20121150 Leach Date: Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL 0.0103 J 0.500 0.0100 Barium 0.442 0.0250 0.0100 Copper 0.826 0.0250 0.0100 Chromium 0.744 0.0250 0.0100 Nickel <0.0500 0.0500 0.00500 Lead 0.0164 J 0.0250 0.00500 Vanadium 0.403 0.100 0.0200 Zinc

7470A Mercury(CVAA)-TCLP 

### 7470A Instrument ID: Lab File ID: 122712R.CSV Dilution: 1.0 InitialWeight /Volume: 25 mL 12/27/2012 0957 FinalWeight /Volume: 25 mL 12/26/2012 1300 7470A HG6
Analysis Date: Prep Date: Analysis Batch: 500-173997 500-173909 500-173838 Prep Batch: Analysis Method: Prep Method: Leach Batch:

12/24/20121150 Leach Date: Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL 0.000702 B 0.000200 0.0000200 Mercury

7471A Mercury(CVAA)

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53491-1 Client Sample ID: 

### Lab Sample ID: FC COMPOSITE 6


### Client Matrix: % Moisture: 73.5 500-53491-1 Solid Date Sampled: 12/19/2012 1430 Date Received: 12/22/20121130 7471A Mercury(CVAA) 

### 7471A Instrument ID: Lab File ID: 122712A.PRN Dilution: 1.0 InitialWeight /Volume: 0.6259 g 12/27/2012 0855 FinalWeight /Volume: 50 mL 12/26/2012 1400 7471A HG5
Analysis Date: Prep Date: Analysis Batch: 500-173984 500-173881 Prep Batch: Analysis Method: Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL 0.232 0.0605 0.0231 Mercury

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53491-1 Client Sample ID: 

### Lab Sample ID: FC D COMPOSITE 6


### Client Matrix: % Moisture: 74.9 500-53491-2 Solid Date Sampled: 12/19/2012 1440 Date Received: 12/22/20121130 6010B Metals (ICP) 

### 6010B Instrument ID: Lab File ID: P51226B Dilution: 1.0 InitialWeight /Volume: 1.0382 g 12/27/2012 0003 FinalWeight /Volume: 100 mL 12/24/2012 1500 3050B ICP5
Analysis Date: Prep Date: Analysis Batch: 500-173964 500-173848 Prep Batch: Analysis Method: Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL 619 3.84 0.457 Barium 707 3.84 1.04 Copper 15000 3.84 0.642 Chromium 86.1 3.84 0.841 Nickel 244 B 1.92 0.661 Lead 251 1.92 0.292 Vanadium 499 7.68 2.64 Zinc
6010B Metals (ICP)-TCLP 

### 6010B Instrument ID: Lab File ID: P51226B Dilution: 1.0 InitialWeight /Volume: 50 mL 12/26/2012 1847 FinalWeight /Volume: 50 mL 12/26/2012 0750 3010A ICP5
Analysis Date: Prep Date: Analysis Batch: 500-173964 500-173872 500-173836 Prep Batch: Analysis Method: Prep Method: Leach Batch:

12/24/20121150 Leach Date: Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL <0.500 0.500 0.0100 Barium 0.0547 0.0250 0.0100 Copper <0.0250 0.0250 0.0100 Chromium 0.0624 0.0250 0.0100 Nickel <0.0500 0.0500 0.00500 Lead <0.0250 0.0250 0.00500 Vanadium <0.100 0.100 0.0200 Zinc

7470A Mercury(CVAA)-TCLP 

### 7470A Instrument ID: Lab File ID: 122712R.CSV Dilution: 1.0 InitialWeight /Volume: 25 mL 12/27/2012 0958 FinalWeight /Volume: 25 mL 12/26/2012 1300 7470A HG6
Analysis Date: Prep Date: Analysis Batch: 500-173997 500-173909 500-173836 Prep Batch: Analysis Method: Prep Method: Leach Batch:

12/24/20121150 Leach Date: Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL <0.000200 0.000200 0.0000200 Mercury

7471A Mercury(CVAA)

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53491-1 Client Sample ID: 

### Lab Sample ID: FC D COMPOSITE 6


### Client Matrix: % Moisture: 74.9 500-53491-2 Solid Date Sampled: 12/19/2012 1440 Date Received: 12/22/20121130 7471A Mercury(CVAA) 

### 7471A Instrument ID: Lab File ID: 122712A.PRN Dilution: 1.0 InitialWeight /Volume: 0.6177 g 12/27/2012 0904 FinalWeight /Volume: 50 mL 12/26/2012 1400 7471A HG5
Analysis Date: Prep Date: Analysis Batch: 500-173984 500-173881 Prep Batch: Analysis Method: Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL 0.237 0.0647 0.0247 Mercury

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53491-1 Client Sample ID: 

### Lab Sample ID: FC EB 6


### Client Matrix: 500-53491-5 Water Date Sampled: 12/19/2012 1410 Date Received: 12/22/20121130 6010B Metals (ICP) 

### 6010B Instrument ID: Lab File ID: P6122612B.asc Dilution: 1.0 InitialWeight /Volume: 50 mL 12/26/2012 1703 FinalWeight /Volume: 50 mL 12/24/2012 1430 3010A ICP6
Analysis Date: Prep Date: Analysis Batch: 500-173963 500-173849 Prep Batch: Analysis Method: Prep Method:

Analyte Result (mg/L) Qualifier MDL RL <0.0100 0.0100 0.000440 Barium 0.00111 J 0.0100 0.00106 Copper <0.0100 0.0100 0.000960 Chromium <0.0100 0.0100 0.00190 Nickel <0.00500 0.00500 0.00158 Lead <0.00500 0.00500 0.000620 Vanadium <0.0200 0.0200 0.00472 Zinc

7470A Mercury(CVAA) 

### 7470A Instrument ID: Lab File ID: 122712R.CSV Dilution: 1.0 InitialWeight /Volume: 25 mL 12/27/2012 0926 FinalWeight /Volume: 25 mL 12/26/2012 1300 7470A HG6
Analysis Date: Prep Date: Analysis Batch: 500-173997 500-173908 Prep Batch: Analysis Method: Prep Method:

Analyte Result (mg/L) Qualifier MDL RL <0.000200 0.000200 0.0000710 Mercury

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53491-1
General Chemistry Client Sample ID: 

### Lab Sample ID: FC COMPOSITE 6


### Client Matrix: 500-53491-1 Solid Date Sampled: 12/19/2012 1430 Date Received: 12/22/20121130 Analyte Result Qual Units MDL RL Dil Method Flashpoint >176 Degrees F 40.0 40.0 1.0 1010 DryWt Corrected: N Analysis Date (Start): 01/02/2013 0930 (End) 01/02/2013 1052 

### Analysis Batch: 500-174336 Chromium, hexavalent <3.75 mg/Kg 1.46 3.75 1.0 7196A DryWt Corrected: Y Analysis Date (Start): 12/27/2012 1251 (End) 12/27/2012 1251 

### Analysis Batch: 500-174027 Prep Batch: 500-173790 Prep Date: 12/22/2012 1200 Cyanide,Total 1.15 J mg/Kg 0.622 1.88 1.0 9014 DryWt Corrected: Y Analysis Date (Start): 12/28/2012 1531 (End) 12/28/2012 1531 

### Analysis Batch: 500-174173 Prep Batch: 500-174096 Prep Date: 12/28/20121120 Sulfide 778 mg/Kg 14.5 90.4 1.0 9034 DryWt Corrected: Y Analysis Date: 12/28/2012 1443 Analysis Batch: 500-174144 Prep Batch: 500-174100 Prep Date: 12/28/2012 1220 Sulfide, Reactive <48.5 mg/Kg 3.78 48.5 1.0 9034 DryWt Corrected: N Analysis Date: 12/28/2012 1258 Analysis Batch: 500-174145 Prep Batch: 500-174101 Prep Date: 12/28/20121157 pH 9.79 SU 0.200 0.200 1.0 9045C DryWt Corrected: N Analysis Date (Start): 12/26/2012 1425 (End) 12/26/2012 1427 

### Analysis Batch: 500-173936 HEM (Oil & Grease) 16600 mg/Kg 822 1850 1.0 9071B DryWt Corrected: Y Analysis Date: 01/04/2013 1013 Analysis Batch: 500-174372 Prep Batch: 500-174369 Prep Date: 01/04/2013 0535 Percent Moisture 74 % 0.10 0.10 1.0 Moisture DryWt Corrected: N Analysis Date: 12/22/2012 1324 Analysis Batch: 500-173788 Percent Solids 26 % 0.10 0.10 1.0 Moisture DryWt Corrected: N Analysis Date: 12/22/2012 1324 Analysis Batch: 500-173788 % Moisture 74.0 % 0.100 0.100 1.0 SM 2540G DryWt Corrected: N Analysis Date: 12/27/2012 0730 Analysis Batch: 500-173970 Total Solids 26.0 % 0.100 0.100 1.0 SM 2540G DryWt Corrected: N Analysis Date: 12/27/2012 0730 Analysis Batch: 500-173970

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53491-1
General Chemistry Client Sample ID: 

### Lab Sample ID: FC D COMPOSITE 6


### Client Matrix: 500-53491-2 Solid Date Sampled: 12/19/2012 1440 Date Received: 12/22/20121130 Analyte Result Qual Units MDL RL Dil Method Flashpoint >176 Degrees F 40.0 40.0 1.0 1010 DryWt Corrected: N Analysis Date (Start): 01/02/2013 1052 (End) 01/02/2013 1214 

### Analysis Batch: 500-174336 Chromium, hexavalent <3.99 mg/Kg 1.55 3.99 1.0 7196A DryWt Corrected: Y Analysis Date (Start): 12/27/2012 1253 (End) 12/27/2012 1253 

### Analysis Batch: 500-174027 Prep Batch: 500-173790 Prep Date: 12/22/2012 1200 Cyanide,Total 1.29 J mg/Kg 0.615 1.86 1.0 9014 DryWt Corrected: Y Analysis Date (Start): 12/28/2012 1531 (End) 12/28/2012 1532 

### Analysis Batch: 500-174173 Prep Batch: 500-174096 Prep Date: 12/28/20121120 Sulfide 817 mg/Kg 15.0 94.0 1.0 9034 DryWt Corrected: Y Analysis Date: 12/28/2012 1444 Analysis Batch: 500-174144 Prep Batch: 500-174100 Prep Date: 12/28/2012 1220 Sulfide, Reactive <49.3 mg/Kg 3.85 49.3 1.0 9034 DryWt Corrected: N Analysis Date: 12/28/2012 1259 Analysis Batch: 500-174145 Prep Batch: 500-174101 Prep Date: 12/28/2012 1201 pH 9.87 SU 0.200 0.200 1.0 9045C DryWt Corrected: N Analysis Date (Start): 12/26/2012 1427 (End) 12/26/2012 1430 

### Analysis Batch: 500-173936 HEM (Oil & Grease) 17000 mg/Kg 866 1950 1.0 9071B DryWt Corrected: Y Analysis Date: 01/04/2013 1056 Analysis Batch: 500-174372 Prep Batch: 500-174369 Prep Date: 01/04/2013 0535 Percent Moisture 75 % 0.10 0.10 1.0 Moisture DryWt Corrected: N Analysis Date: 12/22/2012 1324 Analysis Batch: 500-173788 Percent Solids 25 % 0.10 0.10 1.0 Moisture DryWt Corrected: N Analysis Date: 12/22/2012 1324 Analysis Batch: 500-173788 % Moisture 75.0 % 0.100 0.100 1.0 SM 2540G DryWt Corrected: N Analysis Date: 12/27/2012 0730 Analysis Batch: 500-173970 Total Solids 25.0 % 0.100 0.100 1.0 SM 2540G DryWt Corrected: N Analysis Date: 12/27/2012 0730 Analysis Batch: 500-173970

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53491-1
General Chemistry Client Sample ID: 

### Lab Sample ID: FC DISCRETE 6


### Client Matrix: 500-53491-3 Solid Date Sampled: 12/19/2012 1420 Date Received: 12/22/20121130 Analyte Result Qual Units MDL RL Dil Method Percent Moisture 74 % 0.10 0.10 1.0 Moisture DryWt Corrected: N Analysis Date: 12/28/2012 1009 Analysis Batch: 500-174071 Percent Solids 26 % 0.10 0.10 1.0 Moisture DryWt Corrected: N Analysis Date: 12/28/2012 1009 Analysis Batch: 500-174071

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53491-1
General Chemistry Client Sample ID: 

### Lab Sample ID: FC D DISCRETE 6


### Client Matrix: 500-53491-4 Solid Date Sampled: 12/19/2012 1445 Date Received: 12/22/20121130 Analyte Result Qual Units MDL RL Dil Method Percent Moisture 72 % 0.10 0.10 1.0 Moisture DryWt Corrected: N Analysis Date: 12/28/2012 1009 Analysis Batch: 500-174071 Percent Solids 28 % 0.10 0.10 1.0 Moisture DryWt Corrected: N Analysis Date: 12/28/2012 1009 Analysis Batch: 500-174071

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53491-1
General Chemistry Client Sample ID: 

### Lab Sample ID: FC EB 6


### Client Matrix: 500-53491-5 Water Date Sampled: 12/19/2012 1410 Date Received: 12/22/20121130 Analyte Result Qual Units MDL RL Dil Method HEM (Oil & Grease) <5.33 mg/L 1.55 5.33 1.0 1664A Analysis Date: 01/08/20131108 Analysis Batch: 500-174564 Prep Batch: 500-174563 Prep Date: 01/08/2013 0601 Chromium, hexavalent <0.0100 H mg/L 0.00325 0.0100 1.0 7196A Analysis Date (Start): 12/22/2012 1412 (End) 12/22/2012 1413 

### Analysis Batch: 500-173793 Cyanide,Total <0.0100 mg/L 0.00331 0.0100 1.0 9014 Analysis Date (Start): 12/27/2012 1445 (End) 12/27/2012 1445 

### Analysis Batch: 500-174042 Prep Batch: 500-173980 Prep Date: 12/27/2012 0950 Sulfide <1.00 mg/L 0.230 1.00 1.0 9034 Analysis Date (Start): 12/24/2012 1400 (End) 12/24/2012 1402 

### Analysis Batch: 500-173846 Sulfide, Reactive <1.00 mg/L 1.00 1.00 1.0 9034 Analysis Date: 12/24/2012 1351 Analysis Batch: 500-173845 Prep Batch: 500-173844 Prep Date: 12/24/2012 0845

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## 01/09/2013 Page 29 of 384

## Quality Control Results Job Number: 500-53491-1 Client: Project Integration, Inc 

## Surrogate Recovery Report 8260BVolatile Organic Compounds(GC/MS)
Client Matrix: Solid 

### Lab Sample ID Client Sample ID DBFM DCA TOL BFB %Rec %Rec %Rec %Rec 500-53491-3 FC DISCRETE 6 95 89 87 79 500-53491-4 FC D DISCRETE 6 90 91 89 75 MB 500-173973/5 90 94 96 84 LCS 500-173973/6 81 84 89 81 LCSD 500-173973/7 91 88 93 87

Surrogate Acceptance Limits DBFM = Dibromofluoromethane 75-120 DCA= 1,2-Dichloroethane-d4 (Surr) 70-134 TOL=Toluene-d8 (Surr) 75-122 BFB = 4-Bromofluorobenzene (Surr) 70-122

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## 01/09/2013 Page 30 of 384

## Quality Control Results Job Number: 500-53491-1 Client: Project Integration, Inc 

## Surrogate Recovery Report 8260BVolatile Organic Compounds(GC/MS)
Client Matrix: Solid 

### Lab Sample ID Client Sample ID DBFM DCA TOL BFB %Rec %Rec %Rec %Rec 500-53491-3 DL FC DISCRETE 6 DL 93 97 96 94 500-53491-4 DL FC D DISCRETE 6 DL 96 105 101 100 MB 500-174064/6 96 101 101 98 LCS 500-174064/4 100 95 97 97

Surrogate Acceptance Limits DBFM = Dibromofluoromethane 75-120 DCA= 1,2-Dichloroethane-d4 (Surr) 75-125 TOL=Toluene-d8 (Surr) 75-120 BFB = 4-Bromofluorobenzene (Surr) 75-120

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## 01/09/2013 Page 31 of 384

## Quality Control Results Job Number: 500-53491-1 Client: Project Integration, Inc 

## Surrogate Recovery Report 8260BVolatile Organic Compounds(GC/MS)
Client Matrix:Water 

### Lab Sample ID Client Sample ID DBFM DCA TOL BFB %Rec %Rec %Rec %Rec 500-53491-5 FC EB 6 90 88 94 88 500-53491-6 TRIP BLANK 93 93 100 93 MB 500-173987/7 97 98 103 97 LCS 500-173987/4 94 92 96 96

Surrogate Acceptance Limits DBFM = Dibromofluoromethane 75-120 DCA= 1,2-Dichloroethane-d4 (Surr) 75-125 TOL=Toluene-d8 (Surr) 75-120 BFB = 4-Bromofluorobenzene (Surr) 75-120

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## 01/09/2013 Page 32 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173973

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 6M1227.d 5 g 5 mL Units: ug/Kg 

### Method: 8260B Preparation: 5030B
CMS06 MB 500-173973/5
Analysis Date: 12/27/2012 1033 Analysis Batch: Prep Batch: Leach Batch: N/A N/A 500-173973

Prep Date: Leach Date: 12/27/2012 1033 N/A Analyte RL MDL Qual Result <5.00 5.00 2.16 Acetone <5.00 5.00 1.81 2-Butanone (MEK) Surrogate % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr) 94 70 - 134 Toluene-d8 (Surr) 96 75 - 122 4-Bromofluorobenzene (Surr) 84 70 - 122 Dibromofluoromethane 90 75 - 120

Dilution:

Dilution: 

### Lab Control Sample/ Lab Control Sample Duplicate Recovery Report - Batch: 500-173973

1.0

1.0 Solid LCS Lab Sample ID:

LCSD Lab Sample ID: Client Matrix: Units: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume:

Client Matrix: Solid Units: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: ug/Kg 6S1227.d 5 g 5 mL

6T1227.d 5 g 5 mL ug/Kg 

### Method: 8260B Preparation: 5030B

CMS06

CMS06 LCS 500-173973/6

LCSD 500-173973/7 Analysis Date: Prep Date: Leach Date: 12/27/2012 1056 12/27/2012 1056 N/A Analysis Batch: Prep Batch: Leach Batch: 500-173973 N/A N/A

Analysis Date: Prep Date: Leach Date: 12/27/20121119 12/27/20121119 N/A Analysis Batch: Prep Batch: Leach Batch: 500-173973 N/A N/A

Analyte LCSD Qual LCS Qual RPD Limit RPD Limit LCSD LCS% Rec.
110 96 50 - 138 14 30 Acetone 90 86 58 - 133 4 30 2-Butanone (MEK) Surrogate LCS % Rec LCSD % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr) 84 88 70 - 134 Toluene-d8 (Surr) 89 93 75 - 122 4-Bromofluorobenzene (Surr) 81 87 70 - 122 Dibromofluoromethane 81 91 75 - 120

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## 01/09/2013 Page 33 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Solid 12/27/2012 1056 Dilution: Dilution: 1.0 1.0 Client Matrix: LCSD Lab Sample ID: Client Matrix: Solid 

### Laboratory Control/ Laboratory Duplicate Data Report - Batch: 500-173973 Method: 8260B Preparation: 5030B

Units:ug/Kg LCS 500-173973/6 LCSD 500-173973/7 LCS Lab Sample ID:
Analysis Date: Prep Date: Leach Date: 12/27/2012 1056 Analysis Date: Prep Date: Leach Date: 12/27/20121119 12/27/20121119 N/A N/A

LCSD Result/Qual LCS Result/Qual LCSD Spike Amount LCS Spike Amount Analyte 55.07 47.98 50.0 50.0 Acetone 44.82 43.18 50.0 50.0 2-Butanone (MEK)

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## 01/09/2013 Page 34 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173987

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 22M1227.D 5 mL 5 mL Units: ug/L 

### Method: 8260B Preparation: 5030B
CMS22 MB 500-173987/7
Analysis Date: 12/27/2012 1410 Analysis Batch: Prep Batch: Leach Batch: N/A N/A 500-173987

Prep Date: Leach Date: 12/27/2012 1410 N/A Analyte RL MDL Qual Result <5.00 5.00 1.29 Acetone <5.00 5.00 1.47 2-Butanone (MEK) Surrogate % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr) 98 75 - 125 Toluene-d8 (Surr) 103 75 - 120 4-Bromofluorobenzene (Surr) 97 75 - 120 Dibromofluoromethane 97 75 - 120

Water 1.0 

### Lab Control Sample - Batch: 500-173987

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 22S1227.D 5 mL 5 mL Units: ug/L 

### Method: 8260B Preparation: 5030B
CMS22 LCS 500-173987/4
Analysis Date: 12/27/2012 1246 Analysis Batch: Prep Batch: Leach Batch: 500-173987 N/A N/A Prep Date: Leach Date: 12/27/2012 1246 N/A Analyte Qual Limit % Rec. Result SpikeAmount 50.0 53.44 107 46 - 153 Acetone 50.0 46.97 94 54 - 138 2-Butanone (MEK) Surrogate % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr) 92 75 - 125 Toluene-d8 (Surr) 96 75 - 120 4-Bromofluorobenzene (Surr) 96 75 - 120 Dibromofluoromethane 94 75 - 120

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## 01/09/2013 Page 35 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-174064

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 18M1228.D 5 mL 5 mL Units: ug/Kg 

### Method: 8260B Preparation: N/A
CMS18 MB 500-174064/6
Analysis Date: 12/28/2012 1045 Analysis Batch: Prep Batch: Leach Batch: N/A N/A 500-174064

Prep Date: Leach Date: N/A N/A Analyte RL MDL Qual Result <5.00 5.00 1.30 Acetone <5.00 5.00 1.47 2-Butanone (MEK) Surrogate % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr) 101 75 - 125 Toluene-d8 (Surr) 101 75 - 120 4-Bromofluorobenzene (Surr) 98 75 - 120 Dibromofluoromethane 96 75 - 120

Solid 1.0 

### Lab Control Sample - Batch: 500-174064

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 18S1228.D 5 mL 5 mL Units: ug/Kg 

### Method: 8260B Preparation: N/A
CMS18 LCS 500-174064/4
Analysis Date: 12/28/2012 1000 Analysis Batch: Prep Batch: Leach Batch: 500-174064 N/A N/A Prep Date: Leach Date: N/A N/A Analyte Qual Limit % Rec. Result SpikeAmount 50.0 50.53 101 46 - 153 Acetone 50.0 43.61 87 54 - 138 2-Butanone (MEK) Surrogate % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr) 95 75 - 125 Toluene-d8 (Surr) 97 75 - 120 4-Bromofluorobenzene (Surr) 97 75 - 120 Dibromofluoromethane 100 75 - 120

TestAmerica Chicago 

## 01/09/2013 Page 36 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173848

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: P51226B 1 g 100 mL Units: mg/Kg 

### Method: 6010B Preparation: 3050B
ICP5 MB 500-173848/1-A
Analysis Date: 12/26/2012 2154 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173964 500-173848
Prep Date: Leach Date: 12/24/2012 1500 N/A Analyte RL MDL Qual Result <1.00 1.00 0.119 Barium <1.00 1.00 0.271 Copper <1.00 1.00 0.167 Chromium <1.00 1.00 0.219 Nickel 0.1770 J 0.500 0.172 Lead <0.500 0.500 0.0759 Vanadium <2.00 2.00 0.686 Zinc

Solid 1.0 

### Lab Control Sample - Batch: 500-173848

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: P51226B 1 g 100 mL Units: mg/Kg 

### Method: 6010B Preparation: 3050B
ICP5 LCS 500-173848/2-A
Analysis Date: 12/26/2012 2200 Analysis Batch: Prep Batch: Leach Batch: 500-173964 500-173848 N/A Prep Date: Leach Date: 12/24/2012 1500 N/A Analyte Qual Limit % Rec. Result SpikeAmount 200 200.1 100 80 - 120 Barium 25.0 25.74 103 80 - 120 Copper 20.0 20.94 105 80 - 120 Chromium 50.0 51.09 102 80 - 120 Nickel 10.0 10.73 107 80 - 120 Lead 50.0 51.21 102 80 - 120 Vanadium 50.0 53.63 107 80 - 120 Zinc

TestAmerica Chicago 

## 01/09/2013 Page 37 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173849

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: P6122612B.asc 50 mL 50 mL Units: mg/L 

### Method: 6010B Preparation: 3010A
ICP6 MB 500-173849/1-A
Analysis Date: 12/26/2012 1635 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173963 500-173849
Prep Date: Leach Date: 12/24/2012 1430 N/A Analyte RL MDL Qual Result <0.0100 0.0100 0.000440 Barium <0.0100 0.0100 0.00106 Copper <0.0100 0.0100 0.000960 Chromium <0.0100 0.0100 0.00190 Nickel <0.00500 0.00500 0.00158 Lead <0.00500 0.00500 0.000620 Vanadium <0.0200 0.0200 0.00472 Zinc

Water 1.0 

### Lab Control Sample - Batch: 500-173849

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: P6122612B.asc 50 mL 50 mL Units: mg/L 

### Method: 6010B Preparation: 3010A
ICP6 LCS 500-173849/2-A
Analysis Date: 12/26/2012 1639 Analysis Batch: Prep Batch: Leach Batch: 500-173963 500-173849 N/A Prep Date: Leach Date: 12/24/2012 1430 N/A Analyte Qual Limit % Rec. Result SpikeAmount 2.00 1.902 95 80 - 120 Barium 0.250 0.2317 93 80 - 120 Copper 0.200 0.1856 93 80 - 120 Chromium 0.500 0.4572 91 80 - 120 Nickel 0.100 0.09439 94 80 - 120 Lead 0.500 0.4686 94 80 - 120 Vanadium 0.500 0.4470 89 80 - 120 Zinc

TestAmerica Chicago 

## 01/09/2013 Page 38 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### TCLP SPLPE Leachate Blank- Batch: 500-173872

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: P51226B 50 mL 50 mL Units: mg/L 

### Method: 6010B Preparation: 3010A TCLP ICP5 LB 500-173836/1-B
Analysis Date: 12/26/2012 1712 Analysis Batch: Prep Batch: Leach Batch: 500-173836 500-173964 500-173872
Prep Date: Leach Date: 12/26/2012 0750 12/24/20121150 Analyte RL MDL Qual Result <0.500 0.500 0.0100 Barium <0.0250 0.0250 0.0100 Copper <0.0250 0.0250 0.0100 Chromium <0.0250 0.0250 0.0100 Nickel <0.0500 0.0500 0.00500 Lead <0.0250 0.0250 0.00500 Vanadium <0.100 0.100 0.0200 Zinc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### TCLP SPLPW Leachate Blank- Batch: 500-173872

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: P51226B 50 mL 50 mL Units: mg/L 

### Method: 6010B Preparation: 3010A TCLP ICP5 LB2 500-173838/1-B
Analysis Date: 12/26/2012 1718 Analysis Batch: Prep Batch: Leach Batch: 500-173838 500-173964 500-173872
Prep Date: Leach Date: 12/26/2012 0750 12/24/20121150 Analyte RL MDL Qual Result <0.500 0.500 0.0100 Barium <0.0250 0.0250 0.0100 Copper <0.0250 0.0250 0.0100 Chromium <0.0250 0.0250 0.0100 Nickel <0.0500 0.0500 0.00500 Lead <0.0250 0.0250 0.00500 Vanadium <0.100 0.100 0.0200 Zinc

TestAmerica Chicago 

## 01/09/2013 Page 39 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Water 1.0 

### Lab Control Sample - Batch: 500-173872

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: P51226B 50 mL 50 mL Units: mg/L 

### Method: 6010B Preparation: 3010A
ICP5 LCS 500-173872/3-A
Analysis Date: 12/26/2012 1724 Analysis Batch: Prep Batch: Leach Batch: 500-173964 500-173872 N/A Prep Date: Leach Date: 12/26/2012 0750 N/A Analyte Qual Limit % Rec. Result SpikeAmount 2.00 1.928 96 80 - 120 Barium 0.250 0.2512 100 80 - 120 Copper 0.200 0.2016 101 80 - 120 Chromium 0.500 0.4930 99 80 - 120 Nickel 0.100 0.1042 104 80 - 120 Lead 0.500 0.4994 100 80 - 120 Vanadium 0.500 0.5058 101 80 - 120 Zinc

TestAmerica Chicago 

## 01/09/2013 Page 40 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173908

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 122712R.CSV 25 mL 25 mL Units: mg/L 

### Method: 7470A Preparation: 7470A
HG6 MB 500-173908/7-A
Analysis Date: 12/27/2012 0841 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173997 500-173908
Prep Date: Leach Date: 12/26/2012 1300 N/A Analyte RL MDL Qual Result <0.000200 0.000200 0.0000710 Mercury

Water 1.0 

### Lab Control Sample - Batch: 500-173908

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 122712R.CSV 25 mL 25 mL Units: mg/L 

### Method: 7470A Preparation: 7470A
HG6 LCS 500-173908/8-A
Analysis Date: 12/27/2012 0843 Analysis Batch: Prep Batch: Leach Batch: 500-173997 500-173908 N/A Prep Date: Leach Date: 12/26/2012 1300 N/A Analyte Qual Limit % Rec. Result SpikeAmount 0.00200 0.002121 106 80 - 120 Mercury

TestAmerica Chicago 

## 01/09/2013 Page 41 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173909

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 122712R.CSV 25 mL 25 mL Units: mg/L 

### Method: 7470A Preparation: 7470A
HG6 MB 500-173909/7-A
Analysis Date: 12/27/2012 0928 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173997 500-173909
Prep Date: Leach Date: 12/26/2012 1300 N/A Analyte RL MDL Qual Result 0.00003040 J 0.000200 0.0000200 Mercury

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### TCLP SPLPE Leachate Blank- Batch: 500-173909

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 122712R.CSV 25 mL 25 mL Units: mg/L 

### Method: 7470A Preparation: 7470A TCLP HG6 LB 500-173836/1-C
Analysis Date: 12/27/2012 0949 Analysis Batch: Prep Batch: Leach Batch: 500-173836 500-173997 500-173909
Prep Date: Leach Date: 12/26/2012 1300 12/24/20121150 Analyte RL MDL Qual Result 0.00003420 J 0.000200 0.0000200 Mercury

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### TCLP SPLPW Leachate Blank- Batch: 500-173909

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 122712R.CSV 25 mL 25 mL Units: mg/L 

### Method: 7470A Preparation: 7470A TCLP HG6 LB2 500-173838/1-C
Analysis Date: 12/27/2012 0951 Analysis Batch: Prep Batch: Leach Batch: 500-173838 500-173997 500-173909
Prep Date: Leach Date: 12/26/2012 1300 12/24/20121150 Analyte RL MDL Qual Result 0.00003260 J 0.000200 0.0000200 Mercury

TestAmerica Chicago 

## 01/09/2013 Page 42 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Water 1.0 

### Lab Control Sample - Batch: 500-173909

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 122712R.CSV 25 mL 25 mL Units: mg/L 

### Method: 7470A Preparation: 7470A
HG6 LCS 500-173909/8-A
Analysis Date: 12/27/2012 0930 Analysis Batch: Prep Batch: Leach Batch: 500-173997 500-173909 N/A Prep Date: Leach Date: 12/26/2012 1300 N/A Analyte Qual Limit % Rec. Result SpikeAmount 0.00200 0.002139 107 80 - 120 Mercury

Solid 1.0 

### Matrix Spike - Batch: 500-173909
Lab Sample ID: Client Matrix: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 122712R.CSV 25 mL 25 mL Units: mg/L 

### Method: 7470A Preparation: 7470A TCLP HG6 500-53491-2
Analysis Date: 12/27/2012 1002 Analysis Batch: 500-173997 Prep Batch: 500-173909 Leach Batch: 500-173836 Prep Date: Leach Date: 12/26/2012 1300 12/24/20121150 Qual Limit % Rec. Result SpikeAmount Sample Result/Qual Analyte <0.000200 0.00100 0.0007703 77 50 - 150 Mercury

mg/L Units: Solid Dilution: 1.0 

### Duplicate - Batch: 500-173909
Lab Sample ID: Client Matrix: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 122712R.CSV 25 mL 25 mL 

### Method: 7470A Preparation: 7470A TCLP HG6 500-53491-2
Analysis Date: 12/27/2012 1000 Analysis Batch: Prep Batch: Leach Batch: 500-173997 500-173909 500-173836 Prep Date: Leach Date: 12/26/2012 1300 12/24/20121150 Analyte Qual Limit RPD Result Sample Result/Qual 0.00004470 <0.000200 NC 20 J Mercury

TestAmerica Chicago 

## 01/09/2013 Page 43 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173881

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 122712A.PRN 0.6 g 50 mL Units: mg/Kg 

### Method: 7471A Preparation: 7471A
HG5 MB 500-173881/7-A
Analysis Date: 12/27/2012 0817 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173984 500-173881
Prep Date: Leach Date: 12/26/2012 1400 N/A Analyte RL MDL Qual Result <0.0167 0.0167 0.00637 Mercury

Solid 1.0 

### Lab Control Sample - Batch: 500-173881

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 122712A.PRN 0.6 g 50 mL Units: mg/Kg 

### Method: 7471A Preparation: 7471A
HG5 LCS 500-173881/8-A
Analysis Date: 12/27/2012 0819 Analysis Batch: Prep Batch: Leach Batch: 500-173984 500-173881 N/A Prep Date: Leach Date: 12/26/2012 1400 N/A Analyte Qual Limit % Rec. Result SpikeAmount 0.167 0.1600 96 80 - 120 Mercury

TestAmerica Chicago 

## 01/09/2013 Page 44 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-174563

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 1000 mL 1000 mL Units: mg/L 

### Method: 1664A Preparation: 1664A

N/A No Equipment MB 500-174563/1-A
Analysis Date: 01/08/20131100 Analysis Batch: Prep Batch: Leach Batch: N/A 500-174564 500-174563
Prep Date: Leach Date: 01/08/2013 0535 N/A Analyte RL MDL Qual Result <5.00 5.00 1.45 HEM (Oil & Grease)

Water 1.0 

### Lab Control Sample - Batch: 500-174563

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 1000 mL 1000 mL Units: mg/L 

### Method: 1664A Preparation: 1664A

N/A No Equipment LCS 500-174563/2-A
Analysis Date: 01/08/20131104 Analysis Batch: Prep Batch: Leach Batch: 500-174564 500-174563 N/A Prep Date: Leach Date: 01/08/2013 0548 N/A Analyte Qual Limit % Rec. Result SpikeAmount 40.0 32.00 80 78 -114 HEM (Oil & Grease)

TestAmerica Chicago 

## 01/09/2013 Page 45 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173790

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 2.5 g 100 mL Units: mg/Kg 

### Method: 7196A Preparation: 3060A

N/A SPEC5 MB 500-173790/1-A
Analysis Date: 12/27/2012 1241 Analysis Batch: Prep Batch: Leach Batch: N/A 500-174027 500-173790
Prep Date: Leach Date: 12/22/2012 1200 N/A Analyte RL MDL Qual Result <1.00 1.00 0.389 Chromium, hexavalent

Solid 1.0 

### Lab Control Sample - Batch: 500-173790

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 2.5 g 100 mL Units: mg/Kg 

### Method: 7196A Preparation: 3060A

N/A SPEC5 LCS 500-173790/2-A
Analysis Date: 12/27/2012 1242 Analysis Batch: Prep Batch: Leach Batch: 500-174027 500-173790 N/A Prep Date: Leach Date: 12/22/2012 1200 N/A Analyte Qual Limit % Rec. Result SpikeAmount 10.0 9.188 92 80 - 120 Chromium, hexavalent

Solid 50 

### Lab Control Sample - Batch: 500-173790

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 2.5 g 100 mL Units: mg/Kg 

### Method: 7196A Preparation: 3060A

N/A SPEC5 LCS 500-173790/3-A
Analysis Date: 12/27/2012 1242 Analysis Batch: Prep Batch: Leach Batch: 500-174027 500-173790 N/A Prep Date: Leach Date: 12/22/2012 1200 N/A Analyte Qual Limit % Rec. Result SpikeAmount 676 669.0 99 80 - 120 Chromium, hexavalent

TestAmerica Chicago 

## 01/09/2013 Page 46 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173793

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: Units: mg/L 

### Method: 7196A Preparation: N/A

N/A SPEC5 MB 500-173793/3
Analysis Date: 12/22/2012 1411 Analysis Batch: Prep Batch: Leach Batch: N/A N/A 500-173793

Prep Date: Leach Date: N/A N/A Analyte RL MDL Qual Result <0.0100 0.0100 0.00325 Chromium, hexavalent

Water 1.0 

### Lab Control Sample - Batch: 500-173793

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 100 mL 100 mL Units: mg/L 

### Method: 7196A Preparation: N/A

N/A SPEC5 LCS 500-173793/4
Analysis Date: 12/22/2012 1411 Analysis Batch: Prep Batch: Leach Batch: 500-173793 N/A N/A Prep Date: Leach Date: N/A N/A Analyte Qual Limit % Rec. Result SpikeAmount 0.250 0.2575 103 85 -115 Chromium, hexavalent

Dilution: Dilution: Water 1.0

1.0 Client Matrix: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume:

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: Client Matrix: Water 100 mL 100 mL

100 mL 100 mL 

### Method: 7196A Preparation: N/A

N/A

N/A SPEC5

SPEC5 500-53491-5

500-53491-5 MS Lab Sample ID:

MSD Lab Sample ID: 

### Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 500-173793

12/22/2012 1413 N/A N/A Analysis Date: Prep Date: Leach Date: Analysis Batch: Prep Batch: Leach Batch: 500-173793 N/A N/A

Analysis Date: Prep Date: Leach Date: 12/22/2012 1413 N/A N/A Analysis Batch: Prep Batch: Leach Batch: 500-173793 N/A N/A

Analyte RPD Limit RPD Limit % Rec. MS MSD MS Qual MSD Qual 106 102 85 -115 5 20 Chromium, hexavalent

TestAmerica Chicago 

## 01/09/2013 Page 47 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Water 12/22/2012 1413 12/22/2012 1413 Dilution: Dilution: 1.0 1.0 Client Matrix: Client Matrix: Water 

### Method: 7196A Preparation: N/A

Units:mg/L 500-53491-5 500-53491-5 MS Lab Sample ID: MSD Lab Sample ID: 

### Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 500-173793

Analysis Date: Prep Date: Leach Date: N/A N/A Analysis Date: Prep Date: Leach Date: N/A N/A

Amount Sample Analyte Result/Qual Amount Result/Qual Result/Qual MS MSD MS Spike MSD Spike
<0.0100 0.250 0.250 0.2660 0.2541 Chromium, hexavalent

TestAmerica Chicago 

## 01/09/2013 Page 48 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173980

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 50 mL 50 mL Units: mg/L 

### Method: 9014 Preparation: 9010B

N/A SPEC5 MB 500-173980/1-A
Analysis Date: 12/27/2012 1440 Analysis Batch: Prep Batch: Leach Batch: N/A 500-174042 500-173980
Prep Date: Leach Date: 12/27/2012 0950 N/A Analyte RL MDL Qual Result <0.0100 0.0100 0.00331 Cyanide,Total

Water 1.0 

### Lab Control Sample - Batch: 500-173980

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 50 mL 50 mL Units: mg/L 

### Method: 9014 Preparation: 9010B

N/A SPEC5 LCS 500-173980/2-A
Analysis Date: 12/27/2012 1440 Analysis Batch: Prep Batch: Leach Batch: 500-174042 500-173980 N/A Prep Date: Leach Date: 12/27/2012 0950 N/A Analyte Qual Limit % Rec. Result SpikeAmount 0.100 0.1066 107 80 - 120 Cyanide,Total

TestAmerica Chicago 

## 01/09/2013 Page 49 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-174096

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 1.0000 g 50 mL Units: mg/Kg 

### Method: 9014 Preparation: 9010B

N/A SPEC5 MB 500-174096/12-A
Analysis Date: 12/28/2012 1530 Analysis Batch: Prep Batch: Leach Batch: N/A 500-174173 500-174096
Prep Date: Leach Date: 12/28/20121120 N/A Analyte RL MDL Qual Result <0.500 0.500 0.165 Cyanide,Total

Solid 1.0 

### Lab Control Sample - Batch: 500-174096

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 1.0000 g 50 mL Units: mg/Kg 

### Method: 9014 Preparation: 9010B

N/A SPEC5 LCS 500-174096/13-A
Analysis Date: 12/28/2012 1530 Analysis Batch: Prep Batch: Leach Batch: 500-174173 500-174096 N/A Prep Date: Leach Date: 12/28/20121120 N/A Analyte Qual Limit % Rec. Result SpikeAmount 5.00 5.325 107 80 - 120 Cyanide,Total

Dilution: Dilution: Solid 1.0

1.0 Client Matrix: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume:

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: Client Matrix: Solid 1.0637 g 50 mL

1.0714 g 50 mL 

### Method: 9014 Preparation: 9010B

N/A

N/A SPEC5

SPEC5 500-53491-2

500-53491-2 MS Lab Sample ID:

MSD Lab Sample ID: 

### Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 500-174096

12/28/2012 1532 N/A Analysis Date: Prep Date: Leach Date: Analysis Batch: Prep Batch: Leach Batch: 500-174173 500-174096 N/A

Analysis Date: Prep Date: Leach Date: 12/28/2012 1532 12/28/20121120 N/A Analysis Batch: Prep Batch: Leach Batch: 500-174173 500-174096 N/A 12/28/20121120

Analyte RPD Limit RPD Limit % Rec. MS MSD MS Qual MSD Qual 82 92 75 - 125 9 20 Cyanide,Total

TestAmerica Chicago 

## 01/09/2013 Page 50 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Solid 12/28/2012 1532 12/28/2012 1532 Dilution: Dilution: 1.0 1.0 Client Matrix: Client Matrix: Solid 

### Method: 9014 Preparation: 9010B

Units:mg/Kg 500-53491-2 500-53491-2 MS Lab Sample ID: MSD Lab Sample ID: 

### Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 500-174096

Analysis Date: Prep Date: Leach Date: 12/28/20121120 N/A Analysis Date: Prep Date: Leach Date: 12/28/20121120 N/A

Amount Sample Analyte Result/Qual Amount Result/Qual Result/Qual MS MSD MS Spike MSD Spike
1.29 J 7.50 7.44 7.442 8.170 Cyanide,Total

TestAmerica Chicago 

## 01/09/2013 Page 51 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173844

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 250 mL 250 mL Units: mg/L 

### Method: 9034 Preparation: 7.3.4

N/A No Equipment MB 500-173844/1-A
Analysis Date: 12/24/2012 1319 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173845 500-173844
Prep Date: Leach Date: 12/24/2012 0800 N/A Analyte RL MDL Qual Result <1.00 1.00 1.00 Sulfide, Reactive

Water 1.0 

### Lab Control Sample - Batch: 500-173844

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 250 mL 250 mL Units: mg/L 

### Method: 9034 Preparation: 7.3.4

N/A No Equipment LCS 500-173844/2-A
Analysis Date: 12/24/2012 1329 Analysis Batch: Prep Batch: Leach Batch: 500-173845 500-173844 N/A Prep Date: Leach Date: 12/24/2012 0815 N/A Analyte Qual Limit % Rec. Result SpikeAmount 3.60 3.767 105 80 - 120 Sulfide, Reactive

TestAmerica Chicago 

## 01/09/2013 Page 52 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173846

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 250 mL 250 mL Units: mg/L 

### Method: 9034 Preparation: N/A

N/A No Equipment MB 500-173846/1
Analysis Date: 12/24/2012 1319 Analysis Batch: Prep Batch: Leach Batch: N/A N/A 500-173846

Prep Date: Leach Date: N/A N/A Analyte RL MDL Qual Result <1.00 1.00 0.230 Sulfide

Water 1.0 

### Lab Control Sample - Batch: 500-173846

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 250 mL 250 mL Units: mg/L 

### Method: 9034 Preparation: N/A

N/A No Equipment LCS 500-173846/2
Analysis Date: 12/24/2012 1320 Analysis Batch: Prep Batch: Leach Batch: 500-173846 N/A N/A Prep Date: Leach Date: N/A N/A Analyte Qual Limit % Rec. Result SpikeAmount 3.60 3.760 104 80 - 120 Sulfide

TestAmerica Chicago 

## 01/09/2013 Page 53 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-174100

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 10.0000 g 10 mL Units: mg/Kg 

### Method: 9034 Preparation: 9030B

N/A No Equipment MB 500-174100/1-A
Analysis Date: 12/28/2012 1435 Analysis Batch: Prep Batch: Leach Batch: N/A 500-174144 500-174100
Prep Date: Leach Date: 12/28/2012 1220 N/A Analyte RL MDL Qual Result <25.0 25.0 4.00 Sulfide

Solid 1.0 

### Lab Control Sample - Batch: 500-174100

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 10.0000 g 10 mL Units: mg/Kg 

### Method: 9034 Preparation: 9030B

N/A No Equipment LCS 500-174100/2-A
Analysis Date: 12/28/2012 1436 Analysis Batch: Prep Batch: Leach Batch: 500-174144 500-174100 N/A Prep Date: Leach Date: 12/28/2012 1220 N/A Analyte Qual Limit % Rec. Result SpikeAmount 180 173.0 96 80 - 120 Sulfide

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## 01/09/2013 Page 54 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-174101

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 10.0000 g 10 mL Units: mg/Kg 

### Method: 9034 Preparation: 7.3.4

N/A No Equipment MB 500-174101/1-A
Analysis Date: 12/28/2012 1255 Analysis Batch: Prep Batch: Leach Batch: N/A 500-174145 500-174101
Prep Date: Leach Date: 12/28/20121135 N/A Analyte RL MDL Qual Result <50.0 50.0 3.90 Sulfide, Reactive

Solid 1.0 

### Lab Control Sample - Batch: 500-174101

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 10.0000 g 10 mL Units: mg/Kg 

### Method: 9034 Preparation: 7.3.4

N/A No Equipment LCS 500-174101/2-A
Analysis Date: 12/28/2012 1255 Analysis Batch: Prep Batch: Leach Batch: 500-174145 500-174101 N/A Prep Date: Leach Date: 12/28/20121138 N/A Analyte Qual Limit % Rec. Result SpikeAmount 180 169.4 94 80 - 120 Sulfide, Reactive

TestAmerica Chicago 

## 01/09/2013 Page 55 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-174369

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 10 g 10 mL Units: mg/Kg 

### Method: 9071B Preparation: 9071B

N/A No Equipment MB 500-174369/1-A
Analysis Date: 01/04/2013 0945 Analysis Batch: Prep Batch: Leach Batch: N/A 500-174372 500-174369
Prep Date: Leach Date: 01/04/2013 0535 N/A Analyte RL MDL Qual Result <500 500 222 HEM (Oil & Grease)

Solid 1.0 

### Lab Control Sample - Batch: 500-174369

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 10 g 10 mL Units: mg/Kg 

### Method: 9071B Preparation: 9071B

N/A No Equipment LCS 500-174369/2-A
Analysis Date: 01/04/2013 0959 Analysis Batch: Prep Batch: Leach Batch: 500-174372 500-174369 N/A Prep Date: Leach Date: 01/04/2013 0535 N/A Analyte Qual Limit % Rec. Result SpikeAmount 4000 4050 101 80 - 120 HEM (Oil & Grease)

Dilution: Dilution: Solid 1.0

1.0 Client Matrix: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume:

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: Client Matrix: Solid 10.2105 g 10 mL

10.2075 g 10 mL 

### Method: 9071B Preparation: 9071B

N/A

N/A No Equipment

No Equipment 500-53491-1

500-53491-1 MS Lab Sample ID:

MSD Lab Sample ID: 

### Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 500-174369

01/04/2013 1027 N/A Analysis Date: Prep Date: Leach Date: Analysis Batch: Prep Batch: Leach Batch: 500-174372 500-174369 N/A

Analysis Date: Prep Date: Leach Date: 01/04/2013 1042 01/04/2013 0535 N/A Analysis Batch: Prep Batch: Leach Batch: 500-174372 500-174369 N/A 01/04/2013 0535

Analyte RPD Limit RPD Limit % Rec. MS MSD MS Qual MSD Qual 154 160 75 - 125 2 20 F F HEM (Oil & Grease)

TestAmerica Chicago 

## 01/09/2013 Page 56 of 384

## Quality Control Results
Job Number: 500-53491-1 Client: Project Integration, Inc

Solid 01/04/2013 1027 01/04/2013 1042 Dilution: Dilution: 1.0 1.0 Client Matrix: Client Matrix: Solid 

### Method: 9071B Preparation: 9071B

Units:mg/Kg 500-53491-1 500-53491-1 MS Lab Sample ID: MSD Lab Sample ID: 

### Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 500-174369

Analysis Date: Prep Date: Leach Date: 01/04/2013 0535 N/A Analysis Date: Prep Date: Leach Date: 01/04/2013 0535 N/A

Amount Sample Analyte Result/Qual Amount Result/Qual Result/Qual MS MSD MS Spike MSD Spike
16600 14800 14800 39400 40340 F F HEM (Oil & Grease)

TestAmerica Chicago 

## 01/09/2013 Page 57 of 384

## DATA REPORTING QUALIFIERS Client: Project Integration, Inc Job Number: 500-53491-1

Lab Section Qualifier Description 

### GC/MS VOA Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. J

Metals Compound was found in the blank and sample. B Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. J
General Chemistry MS or MSD exceeds the control limits F Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. J Sample was prepped or analyzed beyond the specified holding time H

TestAmerica Chicago 

## 01/09/2013 Page 58 of 384

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53491-1


## QCAssociation Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis GC/MS VOA Analysis Batch:500-173973 

### Lab Control Sample Solid 8260B LCS 500-173973/6 T Lab Control Sample Duplicate Solid 8260B LCSD 500-173973/7 T Method Blank Solid 8260B MB 500-173973/5 T Solid FC DISCRETE 6 8260B 500-53491-3 T Solid FC D DISCRETE 6 8260B 500-53491-4 T Analysis Batch:500-173987 

### Lab Control Sample Water 8260B LCS 500-173987/4 T Method Blank Water 8260B MB 500-173987/7 T Water FC EB 6 8260B 500-53491-5 T Water TRIP BLANK 8260B 500-53491-6 T Prep Batch: 500-173990 

### Solid FC DISCRETE 6 5030B 500-53491-3DL T Solid FC D DISCRETE 6 5030B 500-53491-4DL T Analysis Batch:500-174064 

### Lab Control Sample Solid 8260B LCS 500-174064/4 T Method Blank Solid 8260B MB 500-174064/6 T Solid 500-173990 FC DISCRETE 6 8260B 500-53491-3DL T Solid 500-173990 FC D DISCRETE 6 8260B 500-53491-4DL T
Report Basis T=Total



### TestAmerica Chicago 

## 01/09/2013 Page 59 of 384

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53491-1


## QCAssociation Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis Metals Prep Batch: 500-173836 

### TCLP SPLPE Leachate Blank Solid 1311 LB 500-173836/1-B P TCLP SPLPE Leachate Blank Solid 1311 LB 500-173836/1-C P Solid FC D COMPOSITE 6 1311 500-53491-2 P Duplicate Solid 1311 500-53491-2DU P Matrix Spike Solid 1311 500-53491-2MS P Prep Batch: 500-173838 

### TCLP SPLPW Leachate Blank Solid 1311 LB2 500-173838/1-B P TCLP SPLPW Leachate Blank Solid 1311 LB2 500-173838/1-C P Solid FC COMPOSITE 6 1311 500-53491-1 P Prep Batch: 500-173848 

### Lab Control Sample Solid 3050B LCS 500-173848/2-A T Method Blank Solid 3050B MB 500-173848/1-A T Solid FC COMPOSITE 6 3050B 500-53491-1 T Solid FC D COMPOSITE 6 3050B 500-53491-2 T Prep Batch: 500-173849 

### Lab Control Sample Water 3010A LCS 500-173849/2-A T Method Blank Water 3010A MB 500-173849/1-A T Water FC EB 6 3010A 500-53491-5 T Prep Batch: 500-173872 

### Lab Control Sample Water 3010A LCS 500-173872/3-A T TCLP SPLPE Leachate Blank Solid 500-173836 3010A LB 500-173836/1-B P TCLP SPLPW Leachate Blank Solid 500-173838 3010A LB2 500-173838/1-B P Solid 500-173838 FC COMPOSITE 6 3010A 500-53491-1 P Solid 500-173836 FC D COMPOSITE 6 3010A 500-53491-2 P Prep Batch: 500-173881 

### Lab Control Sample Solid 7471A LCS 500-173881/8-A T Method Blank Solid 7471A MB 500-173881/7-A T Solid FC COMPOSITE 6 7471A 500-53491-1 T Solid FC D COMPOSITE 6 7471A 500-53491-2 T Prep Batch: 500-173908 

### Lab Control Sample Water 7470A LCS 500-173908/8-A T Method Blank Water 7470A MB 500-173908/7-A T Water FC EB 6 7470A 500-53491-5 T

TestAmerica Chicago 

## 01/09/2013 Page 60 of 384

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53491-1


## QCAssociation Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis Metals Prep Batch: 500-173909 

### Lab Control Sample Water 7470A LCS 500-173909/8-A T Method Blank Water 7470A MB 500-173909/7-A T TCLP SPLPE Leachate Blank Solid 500-173836 7470A LB 500-173836/1-C P TCLP SPLPW Leachate Blank Solid 500-173838 7470A LB2 500-173838/1-C P Solid 500-173838 FC COMPOSITE 6 7470A 500-53491-1 P Solid 500-173836 FC D COMPOSITE 6 7470A 500-53491-2 P Duplicate Solid 500-173836 7470A 500-53491-2DU P Matrix Spike Solid 500-173836 7470A 500-53491-2MS P Analysis Batch:500-173963 

### Lab Control Sample Water 500-173849 6010B LCS 500-173849/2-A T Method Blank Water 500-173849 6010B MB 500-173849/1-A T Water 500-173849 FC EB 6 6010B 500-53491-5 T Analysis Batch:500-173964 

### Lab Control Sample Solid 500-173848 6010B LCS 500-173848/2-A T Method Blank Solid 500-173848 6010B MB 500-173848/1-A T TCLP SPLPE Leachate Blank Solid 500-173872 6010B LB 500-173836/1-B P TCLP SPLPW Leachate Blank Solid 500-173872 6010B LB2 500-173838/1-B P Lab Control Sample Water 500-173872 6010B LCS 500-173872/3-A T Solid 500-173848 FC COMPOSITE 6 6010B 500-53491-1 T Solid 500-173872 FC COMPOSITE 6 6010B 500-53491-1 P Solid 500-173848 FC D COMPOSITE 6 6010B 500-53491-2 T Solid 500-173872 FC D COMPOSITE 6 6010B 500-53491-2 P Analysis Batch:500-173984 

### Lab Control Sample Solid 500-173881 7471A LCS 500-173881/8-A T Method Blank Solid 500-173881 7471A MB 500-173881/7-A T Solid 500-173881 FC COMPOSITE 6 7471A 500-53491-1 T Solid 500-173881 FC D COMPOSITE 6 7471A 500-53491-2 T Analysis Batch:500-173997 

### Lab Control Sample Water 500-173908 7470A LCS 500-173908/8-A T Method Blank Water 500-173908 7470A MB 500-173908/7-A T TCLP SPLPE Leachate Blank Solid 500-173909 7470A LB 500-173836/1-C P TCLP SPLPW Leachate Blank Solid 500-173909 7470A LB2 500-173838/1-C P Lab Control Sample Water 500-173909 7470A LCS 500-173909/8-A T Method Blank Water 500-173909 7470A MB 500-173909/7-A T Solid 500-173909 FC COMPOSITE 6 7470A 500-53491-1 P Solid 500-173909 FC D COMPOSITE 6 7470A 500-53491-2 P Duplicate Solid 500-173909 7470A 500-53491-2DU P Matrix Spike Solid 500-173909 7470A 500-53491-2MS P Water 500-173908 FC EB 6 7470A 500-53491-5 T

TestAmerica Chicago 

## 01/09/2013 Page 61 of 384

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53491-1


## QCAssociation Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis
Report Basis P= TCLP T=Total



### TestAmerica Chicago 

## 01/09/2013 Page 62 of 384

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53491-1


## QCAssociation Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis General Chemistry Analysis Batch:500-173788 

### Solid FC COMPOSITE 6 Moisture 500-53491-1 T Solid FC D COMPOSITE 6 Moisture 500-53491-2 T Prep Batch: 500-173790 

### Lab Control Sample Solid 3060A LCS 500-173790/2-A T Lab Control Sample Solid 3060A LCS 500-173790/3-A T Method Blank Solid 3060A MB 500-173790/1-A T Solid FC COMPOSITE 6 3060A 500-53491-1 T Solid FC D COMPOSITE 6 3060A 500-53491-2 T Analysis Batch:500-173793 

### Lab Control Sample Water 7196A LCS 500-173793/4 T Method Blank Water 7196A MB 500-173793/3 T Water FC EB 6 7196A 500-53491-5 T Matrix Spike Water 7196A 500-53491-5MS T Matrix Spike Duplicate Water 7196A 500-53491-5MSD T Prep Batch: 500-173844 

### Lab Control Sample Water 7.3.4 LCS 500-173844/2-A T Method Blank Water 7.3.4 MB 500-173844/1-A T Water FC EB 6 7.3.4 500-53491-5 T Analysis Batch:500-173845 

### Lab Control Sample Water 500-173844 9034 LCS 500-173844/2-A T Method Blank Water 500-173844 9034 MB 500-173844/1-A T Water 500-173844 FC EB 6 9034 500-53491-5 T Analysis Batch:500-173846 

### Lab Control Sample Water 9034 LCS 500-173846/2 T Method Blank Water 9034 MB 500-173846/1 T Water FC EB 6 9034 500-53491-5 T Analysis Batch:500-173936 

### Solid FC COMPOSITE 6 9045C 500-53491-1 T Solid FC D COMPOSITE 6 9045C 500-53491-2 T Analysis Batch:500-173970 

### Solid FC COMPOSITE 6 SM 2540G 500-53491-1 T Solid FC D COMPOSITE 6 SM 2540G 500-53491-2 T Prep Batch: 500-173980 

### Lab Control Sample Water 9010B LCS 500-173980/2-A T Method Blank Water 9010B MB 500-173980/1-A T Water FC EB 6 9010B 500-53491-5 T

TestAmerica Chicago 

## 01/09/2013 Page 63 of 384

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53491-1


## QCAssociation Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis General Chemistry Analysis Batch:500-174027 

### Lab Control Sample Solid 500-173790 7196A LCS 500-173790/2-A T Lab Control Sample Solid 500-173790 7196A LCS 500-173790/3-A T Method Blank Solid 500-173790 7196A MB 500-173790/1-A T Solid 500-173790 FC COMPOSITE 6 7196A 500-53491-1 T Solid 500-173790 FC D COMPOSITE 6 7196A 500-53491-2 T Analysis Batch:500-174042 

### Lab Control Sample Water 500-173980 9014 LCS 500-173980/2-A T Method Blank Water 500-173980 9014 MB 500-173980/1-A T Water 500-173980 FC EB 6 9014 500-53491-5 T Analysis Batch:500-174071 

### Solid FC DISCRETE 6 Moisture 500-53491-3 T Solid FC D DISCRETE 6 Moisture 500-53491-4 T Prep Batch: 500-174096 

### Lab Control Sample Solid 9010B LCS 500-174096/13-A T Method Blank Solid 9010B MB 500-174096/12-A T Solid FC COMPOSITE 6 9010B 500-53491-1 T Solid FC D COMPOSITE 6 9010B 500-53491-2 T Matrix Spike Solid 9010B 500-53491-2MS T Matrix Spike Duplicate Solid 9010B 500-53491-2MSD T Prep Batch: 500-174100 

### Lab Control Sample Solid 9030B LCS 500-174100/2-A T Method Blank Solid 9030B MB 500-174100/1-A T Solid FC COMPOSITE 6 9030B 500-53491-1 T Solid FC D COMPOSITE 6 9030B 500-53491-2 T Prep Batch: 500-174101 

### Lab Control Sample Solid 7.3.4 LCS 500-174101/2-A T Method Blank Solid 7.3.4 MB 500-174101/1-A T Solid FC COMPOSITE 6 7.3.4 500-53491-1 T Solid FC D COMPOSITE 6 7.3.4 500-53491-2 T Analysis Batch:500-174144 

### Lab Control Sample Solid 500-174100 9034 LCS 500-174100/2-A T Method Blank Solid 500-174100 9034 MB 500-174100/1-A T Solid 500-174100 FC COMPOSITE 6 9034 500-53491-1 T Solid 500-174100 FC D COMPOSITE 6 9034 500-53491-2 T

TestAmerica Chicago 

## 01/09/2013 Page 64 of 384

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53491-1


## QCAssociation Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis General Chemistry Analysis Batch:500-174145 

### Lab Control Sample Solid 500-174101 9034 LCS 500-174101/2-A T Method Blank Solid 500-174101 9034 MB 500-174101/1-A T Solid 500-174101 FC COMPOSITE 6 9034 500-53491-1 T Solid 500-174101 FC D COMPOSITE 6 9034 500-53491-2 T Analysis Batch:500-174173 

### Lab Control Sample Solid 500-174096 9014 LCS 500-174096/13-A T Method Blank Solid 500-174096 9014 MB 500-174096/12-A T Solid 500-174096 FC COMPOSITE 6 9014 500-53491-1 T Solid 500-174096 FC D COMPOSITE 6 9014 500-53491-2 T Matrix Spike Solid 500-174096 9014 500-53491-2MS T Matrix Spike Duplicate Solid 500-174096 9014 500-53491-2MSD T Analysis Batch:500-174336 

### Solid FC COMPOSITE 6 1010 500-53491-1 T Solid FC D COMPOSITE 6 1010 500-53491-2 T Prep Batch: 500-174369 

### Lab Control Sample Solid 9071B LCS 500-174369/2-A T Method Blank Solid 9071B MB 500-174369/1-A T Solid FC COMPOSITE 6 9071B 500-53491-1 T Matrix Spike Solid 9071B 500-53491-1MS T Matrix Spike Duplicate Solid 9071B 500-53491-1MSD T Solid FC D COMPOSITE 6 9071B 500-53491-2 T Analysis Batch:500-174372 

### Lab Control Sample Solid 500-174369 9071B LCS 500-174369/2-A T Method Blank Solid 500-174369 9071B MB 500-174369/1-A T Solid 500-174369 FC COMPOSITE 6 9071B 500-53491-1 T Matrix Spike Solid 500-174369 9071B 500-53491-1MS T Matrix Spike Duplicate Solid 500-174369 9071B 500-53491-1MSD T Solid 500-174369 FC D COMPOSITE 6 9071B 500-53491-2 T Prep Batch: 500-174563 

### Lab Control Sample Water 1664A LCS 500-174563/2-A T Method Blank Water 1664A MB 500-174563/1-A T Water FC EB 6 1664A 500-53491-5 T Analysis Batch:500-174564 

### Lab Control Sample Water 500-174563 1664A LCS 500-174563/2-A T Method Blank Water 500-174563 1664A MB 500-174563/1-A T Water 500-174563 FC EB 6 1664A 500-53491-5 T

TestAmerica Chicago 

## 01/09/2013 Page 65 of 384

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53491-1


## QCAssociation Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis
Report Basis T=Total



### TestAmerica Chicago 

## 01/09/2013 Page 66 of 384

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53491-1 

## Laboratory Chronicle

12/22/201211:30 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/19/2012 14:30 500-53491-1 FC COMPOSITE 6



### P:3010A 500-53491-A-1-D 500-173964 500-173872 12/26/2012 07:50 LAH TAL CHI 1 A:6010B 500-53491-A-1-D 500-173964 500-173872 12/26/2012 18:41 PJ TAL CHI 1 P:3050B 500-53491-A-1-C 500-173964 500-173848 12/24/2012 15:00 RL TAL CHI 1 A:6010B 500-53491-A-1-C 500-173964 500-173848 12/26/2012 23:57 PJ TAL CHI 1 P:7470A 500-53491-A-1-F 500-173997 500-173909 12/26/2012 13:00 BJB TAL CHI 1 A:7470A 500-53491-A-1-F 500-173997 500-173909 12/27/2012 09:57 BJB TAL CHI 1 P:7471A 500-53491-A-1-E 500-173984 500-173881 12/26/2012 14:00 BJB TAL CHI 1 A:7471A 500-53491-A-1-E 500-173984 500-173881 12/27/2012 08:55 BJB TAL CHI 1 A:1010 500-53491-A-1 500-174336 01/02/2013 09:30 APW TAL CHI 1 P:3060A 500-53491-A-1-A 500-174027 500-173790 12/22/2012 12:00 APW TAL CHI 1 A:7196A 500-53491-A-1-A 500-174027 500-173790 12/27/2012 12:51 APW TAL CHI 1 P:9010B 500-53491-A-1-G 500-174173 500-174096 12/28/201211:20 EAT TAL CHI 1 A:9014 500-53491-A-1-G 500-174173 500-174096 12/28/2012 15:31 EAT TAL CHI 1 P:7.3.4 500-53491-A-1-I 500-174145 500-174101 12/28/201211:57 CLM TAL CHI 1 A:9034 500-53491-A-1-I 500-174145 500-174101 12/28/2012 12:58 CLM TAL CHI 1 P:9030B 500-53491-A-1-H 500-174144 500-174100 12/28/2012 12:20 CLM TAL CHI 1 A:9034 500-53491-A-1-H 500-174144 500-174100 12/28/2012 14:43 CLM TAL CHI 1 A:9045C 500-53491-A-1 500-173936 12/26/2012 14:25 CLM TAL CHI 1 P:9071B 500-53491-A-1-J 500-174372 500-174369 01/04/2013 05:35 MTB TAL CHI 1 A:9071B 500-53491-A-1-J 500-174372 500-174369 01/04/2013 10:13 MTB TAL CHI 1 A:Moisture 500-53491-A-1 500-173788 12/22/2012 13:24 CMV TAL CHI 1 A:SM 2540G 500-53491-A-1 500-173970 12/27/2012 07:30 CMV TAL CHI 1

12/22/201211:30 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/19/2012 14:30 500-53491-1 MS FC COMPOSITE 6



### P:9071B 500-53491-A-1-K MS 500-174372 500-174369 01/04/2013 05:35 MTB TAL CHI 1 A:9071B 500-53491-A-1-K MS 500-174372 500-174369 01/04/2013 10:27 MTB TAL CHI 1

12/22/201211:30 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/19/2012 14:30 500-53491-1 MSD FC COMPOSITE 6



### P:9071B 500-53491-A-1-L MSD 500-174372 500-174369 01/04/2013 05:35 MTB TAL CHI 1 A:9071B 500-53491-A-1-L MSD 500-174372 500-174369 01/04/2013 10:42 MTB TAL CHI 1

A=Analytical MethodP= Prep Method TestAmerica Chicago 

## 01/09/2013 Page 67 of 384

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53491-1 

## Laboratory Chronicle

12/22/201211:30 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/19/2012 14:40 500-53491-2 FC D COMPOSITE 6



### P:3010A 500-53491-A-2-D 500-173964 500-173872 12/26/2012 07:50 LAH TAL CHI 1 A:6010B 500-53491-A-2-D 500-173964 500-173872 12/26/2012 18:47 PJ TAL CHI 1 P:3050B 500-53491-A-2-C 500-173964 500-173848 12/24/2012 15:00 RL TAL CHI 1 A:6010B 500-53491-A-2-C 500-173964 500-173848 12/27/2012 00:03 PJ TAL CHI 1 P:7470A 500-53491-A-2-F 500-173997 500-173909 12/26/2012 13:00 BJB TAL CHI 1 A:7470A 500-53491-A-2-F 500-173997 500-173909 12/27/2012 09:58 BJB TAL CHI 1 P:7471A 500-53491-A-2-E 500-173984 500-173881 12/26/2012 14:00 BJB TAL CHI 1 A:7471A 500-53491-A-2-E 500-173984 500-173881 12/27/2012 09:04 BJB TAL CHI 1 A:1010 500-53491-A-2 500-174336 01/02/2013 10:52 APW TAL CHI 1 P:3060A 500-53491-A-2-A 500-174027 500-173790 12/22/2012 12:00 APW TAL CHI 1 A:7196A 500-53491-A-2-A 500-174027 500-173790 12/27/2012 12:53 APW TAL CHI 1 P:9010B 500-53491-A-2-I 500-174173 500-174096 12/28/201211:20 EAT TAL CHI 1 A:9014 500-53491-A-2-I 500-174173 500-174096 12/28/2012 15:31 EAT TAL CHI 1 P:7.3.4 500-53491-A-2-M 500-174145 500-174101 12/28/2012 12:01 CLM TAL CHI 1 A:9034 500-53491-A-2-M 500-174145 500-174101 12/28/2012 12:59 CLM TAL CHI 1 P:9030B 500-53491-A-2-L 500-174144 500-174100 12/28/2012 12:20 CLM TAL CHI 1 A:9034 500-53491-A-2-L 500-174144 500-174100 12/28/2012 14:44 CLM TAL CHI 1 A:9045C 500-53491-A-2 500-173936 12/26/2012 14:27 CLM TAL CHI 1 P:9071B 500-53491-A-2-N 500-174372 500-174369 01/04/2013 05:35 MTB TAL CHI 1 A:9071B 500-53491-A-2-N 500-174372 500-174369 01/04/2013 10:56 MTB TAL CHI 1 A:Moisture 500-53491-A-2 500-173788 12/22/2012 13:24 CMV TAL CHI 1 A:SM 2540G 500-53491-A-2 500-173970 12/27/2012 07:30 CMV TAL CHI 1

12/22/201211:30 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/19/2012 14:40 500-53491-2 MS FC D COMPOSITE 6



### P:7470A 500-53491-A-2-H MS 500-173997 500-173909 12/26/2012 13:00 BJB TAL CHI 1 A:7470A 500-53491-A-2-H MS 500-173997 500-173909 12/27/2012 10:02 BJB TAL CHI 1 P:9010B 500-53491-A-2-J MS 500-174173 500-174096 12/28/201211:20 EAT TAL CHI 1 A:9014 500-53491-A-2-J MS 500-174173 500-174096 12/28/2012 15:32 EAT TAL CHI 1

12/22/201211:30 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/19/2012 14:40 500-53491-2 MSD FC D COMPOSITE 6



### P:9010B 500-53491-A-2-K MSD 500-174173 500-174096 12/28/201211:20 EAT TAL CHI 1 A:9014 500-53491-A-2-K MSD 500-174173 500-174096 12/28/2012 15:32 EAT TAL CHI 1

A=Analytical MethodP= Prep Method TestAmerica Chicago 

## 01/09/2013 Page 68 of 384

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53491-1 

## Laboratory Chronicle

12/22/201211:30 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/19/2012 14:40 500-53491-2 DU FC D COMPOSITE 6



### P:7470A 500-53491-A-2-G DU 500-173997 500-173909 12/26/2012 13:00 BJB TAL CHI 1 A:7470A 500-53491-A-2-G DU 500-173997 500-173909 12/27/2012 10:00 BJB TAL CHI 1

12/22/201211:30 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/19/2012 14:20 500-53491-3 FC DISCRETE 6



### P:5030B 500-53491-A-3 500-173973 12/27/2012 13:36 DJD TAL CHI 1 A:8260B 500-53491-A-3 500-173973 12/27/2012 13:36 DJD TAL CHI 1 P:5030B 500-53491-A-3-A 500-174064 500-173990 12/27/2012 10:28 WRE TAL CHI DL 50 A:8260B 500-53491-A-3-A 500-174064 500-173990 12/28/201211:08 BDA TAL CHI DL 50 A:Moisture 500-53491-A-3 500-174071 12/28/2012 10:09 CMV TAL CHI 1

12/22/201211:30 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/19/2012 14:45 500-53491-4 FC D DISCRETE 6



### P:5030B 500-53491-A-4 500-173973 12/27/2012 13:59 DJD TAL CHI 1 A:8260B 500-53491-A-4 500-173973 12/27/2012 13:59 DJD TAL CHI 1 P:5030B 500-53491-A-4-A 500-174064 500-173990 12/27/2012 10:28 WRE TAL CHI DL 50 A:8260B 500-53491-A-4-A 500-174064 500-173990 12/28/201211:31 BDA TAL CHI DL 50 A:Moisture 500-53491-A-4 500-174071 12/28/2012 10:09 CMV TAL CHI 1

12/22/201211:30 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/19/2012 14:10 500-53491-5 FC EB 6



### P:5030B 500-53491-A-5 500-173987 12/27/2012 15:54 LM TAL CHI 1 A:8260B 500-53491-A-5 500-173987 12/27/2012 15:54 LM TAL CHI 1 P:3010A 500-53491-E-5-A 500-173963 500-173849 12/24/2012 14:30 RL TAL CHI 1 A:6010B 500-53491-E-5-A 500-173963 500-173849 12/26/2012 17:03 PJ TAL CHI 1 P:7470A 500-53491-E-5-B 500-173997 500-173908 12/26/2012 13:00 BJB TAL CHI 1 A:7470A 500-53491-E-5-B 500-173997 500-173908 12/27/2012 09:26 BJB TAL CHI 1 P:1664A 500-53491-H-5-A 500-174564 500-174563 01/08/2013 06:01 MTB TAL CHI 1 A:1664A 500-53491-H-5-A 500-174564 500-174563 01/08/201311:08 MTB TAL CHI 1 A:7196A 500-53491-F-5 500-173793 12/22/2012 14:12 APW TAL CHI 1 P:9010B 500-53491-D-5-A 500-174042 500-173980 12/27/2012 09:50 EAT TAL CHI 1 A:9014 500-53491-D-5-A 500-174042 500-173980 12/27/2012 14:45 EAT TAL CHI 1 P:7.3.4 500-53491-G-5-A 500-173845 500-173844 12/24/2012 08:45 CLB TAL CHI 1 A:9034 500-53491-G-5-A 500-173845 500-173844 12/24/2012 13:51 CLB TAL CHI 1 A:9034 500-53491-G-5 500-173846 12/24/2012 14:00 CLB TAL CHI 1
A=Analytical MethodP= Prep Method TestAmerica Chicago 

## 01/09/2013 Page 69 of 384

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53491-1 

## Laboratory Chronicle

12/22/201211:30 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/19/2012 14:10 500-53491-5 MS FC EB 6



### A:7196A 500-53491-F-5 MS 500-173793 12/22/2012 14:13 APW TAL CHI 1

12/22/201211:30 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/19/2012 14:10 500-53491-5 MSD FC EB 6



### A:7196A 500-53491-F-5 MSD 500-173793 12/22/2012 14:13 APW TAL CHI 1

12/22/201211:30 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/19/2012 00:00 500-53491-6 TRIP BLANK



### P:5030B 500-53491-A-6 500-173987 12/27/2012 15:28 LM TAL CHI 1 A:8260B 500-53491-A-6 500-173987 12/27/2012 15:28 LM TAL CHI 1

A=Analytical MethodP= Prep Method TestAmerica Chicago 

## 01/09/2013 Page 70 of 384

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53491-1 

## Laboratory Chronicle
Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: N/A Received Date/Time: N/A MB N/A



### P:5030B MB 500-173973/5 500-173973 12/27/2012 10:33 DJD TAL CHI 1 A:8260B MB 500-173973/5 500-173973 12/27/2012 10:33 DJD TAL CHI 1 P:5030B MB 500-173987/7 500-173987 12/27/2012 14:10 LM TAL CHI 1 A:8260B MB 500-173987/7 500-173987 12/27/2012 14:10 LM TAL CHI 1 A:8260B MB 500-174064/6 500-174064 12/28/2012 10:45 BDA TAL CHI 1 P:3010A MB 500-173849/1-A 500-173963 500-173849 12/24/2012 14:30 RL TAL CHI 1 A:6010B MB 500-173849/1-A 500-173963 500-173849 12/26/2012 16:35 PJ TAL CHI 1 P:3050B MB 500-173848/1-A 500-173964 500-173848 12/24/2012 15:00 RL TAL CHI 1 A:6010B MB 500-173848/1-A 500-173964 500-173848 12/26/2012 21:54 PJ TAL CHI 1 P:7470A MB 500-173908/7-A 500-173997 500-173908 12/26/2012 13:00 BJB TAL CHI 1 A:7470A MB 500-173908/7-A 500-173997 500-173908 12/27/2012 08:41 BJB TAL CHI 1 P:7470A MB 500-173909/7-A 500-173997 500-173909 12/26/2012 13:00 BJB TAL CHI 1 A:7470A MB 500-173909/7-A 500-173997 500-173909 12/27/2012 09:28 BJB TAL CHI 1 P:7471A MB 500-173881/7-A 500-173984 500-173881 12/26/2012 14:00 BJB TAL CHI 1 A:7471A MB 500-173881/7-A 500-173984 500-173881 12/27/2012 08:17 BJB TAL CHI 1 P:1664A MB 500-174563/1-A 500-174564 500-174563 01/08/2013 05:35 MTB TAL CHI 1 A:1664A MB 500-174563/1-A 500-174564 500-174563 01/08/201311:00 MTB TAL CHI 1 A:7196A MB 500-173793/3 500-173793 12/22/2012 14:11 APW TAL CHI 1 P:3060A MB 500-173790/1-A 500-174027 500-173790 12/22/2012 12:00 APW TAL CHI 1 A:7196A MB 500-173790/1-A 500-174027 500-173790 12/27/2012 12:41 APW TAL CHI 1 P:9010B MB 500-173980/1-A 500-174042 500-173980 12/27/2012 09:50 EAT TAL CHI 1 A:9014 MB 500-173980/1-A 500-174042 500-173980 12/27/2012 14:40 EAT TAL CHI 1 P:9010B MB 500-174096/12-A 500-174173 500-174096 12/28/201211:20 EAT TAL CHI 1 A:9014 MB 500-174096/12-A 500-174173 500-174096 12/28/2012 15:30 EAT TAL CHI 1 P:7.3.4 MB 500-173844/1-A 500-173845 500-173844 12/24/2012 08:00 CLB TAL CHI 1 A:9034 MB 500-173844/1-A 500-173845 500-173844 12/24/2012 13:19 CLB TAL CHI 1 A:9034 MB 500-173846/1 500-173846 12/24/2012 13:19 CLB TAL CHI 1 P:7.3.4 MB 500-174101/1-A 500-174145 500-174101 12/28/201211:35 CLM TAL CHI 1 A:9034 MB 500-174101/1-A 500-174145 500-174101 12/28/2012 12:55 CLM TAL CHI 1 P:9030B MB 500-174100/1-A 500-174144 500-174100 12/28/2012 12:20 CLM TAL CHI 1 A:9034 MB 500-174100/1-A 500-174144 500-174100 12/28/2012 14:35 CLM TAL CHI 1 P:9071B MB 500-174369/1-A 500-174372 500-174369 01/04/2013 05:35 MTB TAL CHI 1 A:9071B MB 500-174369/1-A 500-174372 500-174369 01/04/2013 09:45 MTB TAL CHI 1
Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: N/A Received Date/Time: N/A LB N/A



### P:3010A LB 500-173836/1-B 500-173964 500-173872 12/26/2012 07:50 LAH TAL CHI 1 A:6010B LB 500-173836/1-B 500-173964 500-173872 12/26/2012 17:12 PJ TAL CHI 1 P:7470A LB 500-173836/1-C 500-173997 500-173909 12/26/2012 13:00 BJB TAL CHI 1 A:7470A LB 500-173836/1-C 500-173997 500-173909 12/27/2012 09:49 BJB TAL CHI 1

A=Analytical MethodP= Prep Method TestAmerica Chicago 

## 01/09/2013 Page 71 of 384

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53491-1 

## Laboratory Chronicle
Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: N/A Received Date/Time: N/A LB2 N/A



### P:3010A LB2 500-173838/1-B 500-173964 500-173872 12/26/2012 07:50 LAH TAL CHI 1 A:6010B LB2 500-173838/1-B 500-173964 500-173872 12/26/2012 17:18 PJ TAL CHI 1 P:7470A LB2 500-173838/1-C 500-173997 500-173909 12/26/2012 13:00 BJB TAL CHI 1 A:7470A LB2 500-173838/1-C 500-173997 500-173909 12/27/2012 09:51 BJB TAL CHI 1

A=Analytical MethodP= Prep Method TestAmerica Chicago 

## 01/09/2013 Page 72 of 384

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53491-1 

## Laboratory Chronicle
Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: N/A Received Date/Time: N/A LCS N/A



### P:5030B LCS 500-173973/6 500-173973 12/27/2012 10:56 DJD TAL CHI 1 A:8260B LCS 500-173973/6 500-173973 12/27/2012 10:56 DJD TAL CHI 1 P:5030B LCS 500-173987/4 500-173987 12/27/2012 12:46 LM TAL CHI 1 A:8260B LCS 500-173987/4 500-173987 12/27/2012 12:46 LM TAL CHI 1 A:8260B LCS 500-174064/4 500-174064 12/28/2012 10:00 BDA TAL CHI 1 P:3010A LCS 500-173849/2-A 500-173963 500-173849 12/24/2012 14:30 RL TAL CHI 1 A:6010B LCS 500-173849/2-A 500-173963 500-173849 12/26/2012 16:39 PJ TAL CHI 1 P:3010A LCS 500-173872/3-A 500-173964 500-173872 12/26/2012 07:50 LAH TAL CHI 1 A:6010B LCS 500-173872/3-A 500-173964 500-173872 12/26/2012 17:24 PJ TAL CHI 1 P:3050B LCS 500-173848/2-A 500-173964 500-173848 12/24/2012 15:00 RL TAL CHI 1 A:6010B LCS 500-173848/2-A 500-173964 500-173848 12/26/2012 22:00 PJ TAL CHI 1 P:7470A LCS 500-173908/8-A 500-173997 500-173908 12/26/2012 13:00 BJB TAL CHI 1 A:7470A LCS 500-173908/8-A 500-173997 500-173908 12/27/2012 08:43 BJB TAL CHI 1 P:7470A LCS 500-173909/8-A 500-173997 500-173909 12/26/2012 13:00 BJB TAL CHI 1 A:7470A LCS 500-173909/8-A 500-173997 500-173909 12/27/2012 09:30 BJB TAL CHI 1 P:7471A LCS 500-173881/8-A 500-173984 500-173881 12/26/2012 14:00 BJB TAL CHI 1 A:7471A LCS 500-173881/8-A 500-173984 500-173881 12/27/2012 08:19 BJB TAL CHI 1 P:1664A LCS 500-174563/2-A 500-174564 500-174563 01/08/2013 05:48 MTB TAL CHI 1 A:1664A LCS 500-174563/2-A 500-174564 500-174563 01/08/201311:04 MTB TAL CHI 1 A:7196A LCS 500-173793/4 500-173793 12/22/2012 14:11 APW TAL CHI 1 P:3060A LCS 500-173790/2-A 500-174027 500-173790 12/22/2012 12:00 APW TAL CHI 1 A:7196A LCS 500-173790/2-A 500-174027 500-173790 12/27/2012 12:42 APW TAL CHI 1 P:3060A LCS 500-173790/3-A 500-174027 500-173790 12/22/2012 12:00 APW TAL CHI 50 A:7196A LCS 500-173790/3-A 500-174027 500-173790 12/27/2012 12:42 APW TAL CHI 50 P:9010B LCS 500-173980/2-A 500-174042 500-173980 12/27/2012 09:50 EAT TAL CHI 1 A:9014 LCS 500-173980/2-A 500-174042 500-173980 12/27/2012 14:40 EAT TAL CHI 1 P:9010B LCS 500-174096/13-A 500-174173 500-174096 12/28/201211:20 EAT TAL CHI 1 A:9014 LCS 500-174096/13-A 500-174173 500-174096 12/28/2012 15:30 EAT TAL CHI 1 A:9034 LCS 500-173846/2 500-173846 12/24/2012 13:20 CLB TAL CHI 1 P:7.3.4 LCS 500-173844/2-A 500-173845 500-173844 12/24/2012 08:15 CLB TAL CHI 1 A:9034 LCS 500-173844/2-A 500-173845 500-173844 12/24/2012 13:29 CLB TAL CHI 1 P:7.3.4 LCS 500-174101/2-A 500-174145 500-174101 12/28/201211:38 CLM TAL CHI 1 A:9034 LCS 500-174101/2-A 500-174145 500-174101 12/28/2012 12:55 CLM TAL CHI 1 P:9030B LCS 500-174100/2-A 500-174144 500-174100 12/28/2012 12:20 CLM TAL CHI 1 A:9034 LCS 500-174100/2-A 500-174144 500-174100 12/28/2012 14:36 CLM TAL CHI 1 P:9071B LCS 500-174369/2-A 500-174372 500-174369 01/04/2013 05:35 MTB TAL CHI 1 A:9071B LCS 500-174369/2-A 500-174372 500-174369 01/04/2013 09:59 MTB TAL CHI 1

A=Analytical MethodP= Prep Method TestAmerica Chicago 

## 01/09/2013 Page 73 of 384

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53491-1 

## Laboratory Chronicle
Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: N/A Received Date/Time: N/A LCSD N/A



### P:5030B LCSD 500-173973/7 500-173973 12/27/201211:19 DJD TAL CHI 1 A:8260B LCSD 500-173973/7 500-173973 12/27/201211:19 DJD TAL CHI 1 

### Lab References: TAL CHI=TestAmerica Chicago

A=Analytical MethodP= Prep Method TestAmerica Chicago 

## 01/09/2013 Page 74 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 04/26/13 (Purchased Reagent) HEM (Oil & Grease) 8000 mg/L Mallin / JTBaker, Lot E50600 / K19H00 1664 HEM_00060 SGT-HEM 4000 mg/L 8260 IS SK_00027 1,4-Dichlorobenzene-d4 250 ug/mL 5 mL 5 mL 12/18/1212/04/12 8260 IS WK_00384 1, Lot NA 1,4-Difluorobenzene 250 ug/mL Chlorobenzene-d5 250 ug/mL Pentafluorobenzene 250 ug/mL 08/31/14 (Purchased Reagent) 1,4-Dichlorobenzene-d4 250 ug/mL RESTEK, Lot AO88671 .8260 IS SK_00027 1,4-Difluorobenzene 250 ug/mL Chlorobenzene-d5 250 ug/mL Pentafluorobenzene 250 ug/mL 8260 IS SK_00026 1,4-Dichlorobenzene-d4 50 ug/mL 20 mL 4000 uL 12/03/1211/19/12 8260 LOW IS_00103 MEOH, Lot DA946 1,4-Difluorobenzene 50 ug/mL Chlorobenzene-d5 50 ug/mL Pentafluorobenzene 50 ug/mL 08/31/14 (Purchased Reagent) 1,4-Dichlorobenzene-d4 250 ug/mL RESTEK, Lot AO88671 .8260 IS SK_00026 1,4-Difluorobenzene 250 ug/mL Chlorobenzene-d5 250 ug/mL Pentafluorobenzene 250 ug/mL 8260 IS SK_00027 1,4-Dichlorobenzene-d4 50 ug/mL 20 mL 4000 uL 12/14/1211/30/12 8260 LOW IS_00104 MEOH, Lot DA946 1,4-Difluorobenzene 50 ug/mL Chlorobenzene-d5 50 ug/mL Pentafluorobenzene 50 ug/mL 08/31/14 (Purchased Reagent) 1,4-Dichlorobenzene-d4 250 ug/mL RESTEK, Lot AO88671 .8260 IS SK_00027 1,4-Difluorobenzene 250 ug/mL Chlorobenzene-d5 250 ug/mL Pentafluorobenzene 250 ug/mL 8260 SS SK_00031 1,2-Dichloroethane-d4 (Surr) 50 ug/mL 20 mL 4000 uL 12/03/1211/19/12 8260 LOW SS_00105 MEOH, Lot DA946 4-Bromofluorobenzene (Surr) 50 ug/mL Dibromofluoromethane 50 ug/mL Toluene-d8 (Surr) 50 ug/mL 07/31/14 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL RESTEK, Lot A088175 .8260 SS SK_00031 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 8260 SS SK_00032 1,2-Dichloroethane-d4 (Surr) 50 ug/mL 20 mL 4000 uL 12/14/1211/30/12 8260 LOW SS_00106 MEOH, Lot DA946 4-Bromofluorobenzene (Surr) 50 ug/mL Dibromofluoromethane 50 ug/mL Toluene-d8 (Surr) 50 ug/mL 07/31/14 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL RESTEK, Lot A088175 .8260 SS SK_00032 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 8260 SS SK_00032 1,2-Dichloroethane-d4 (Surr) 50 ug/mL 20 mL 4000 uL 12/27/1212/13/12 8260 LOW SS_00107 MEOH, Lot DA946 4-Bromofluorobenzene (Surr) 50 ug/mL Dibromofluoromethane 50 ug/mL 

## 01/09/2013 Page 75 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Toluene-d8 (Surr) 50 ug/mL 07/31/14 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL RESTEK, Lot A088175 .8260 SS SK_00032 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 8260 SS SK_00032 1,2-Dichloroethane-d4 (Surr) 50 ug/mL 20 mL 4000 uL 01/09/1312/26/12 8260 LOW SS_00108 MEOH, Lot DA946 4-Bromofluorobenzene (Surr) 50 ug/mL Dibromofluoromethane 50 ug/mL Toluene-d8 (Surr) 50 ug/mL 07/31/14 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL RESTEK, Lot A088175 .8260 SS SK_00032 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 8260 SS SK_00032 1,2-Dichloroethane-d4 (Surr) 250 ug/mL 5 mL 5 mL 12/18/1212/04/12 8260 SS WK_00382 1, Lot NA 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 07/31/14 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL RESTEK, Lot A088175 .8260 SS SK_00032 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 8260 STD STK_00033 1,1,1,2-Tetrachloroethane 100 ug/mL 2 mL 2 mL 12/03/1211/19/12 8260 STD WK_00212 METHANOL, Lot NA 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL 

## 01/09/2013 Page 76 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL 08/31/14 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL Restek, Lot A088677 .8260 STD STK_00033 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 

## 01/09/2013 Page 77 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL 8260 STD STK_00033 1,1,1,2-Tetrachloroethane 100 ug/mL 2 mL 2 mL 12/18/1212/04/12 8260 STD WK_00215 METHANOL, Lot NA 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 

## 01/09/2013 Page 78 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL 

## 01/09/2013 Page 79 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL 08/31/14 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL Restek, Lot A088677 .8260 STD STK_00033 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL 

## 01/09/2013 Page 80 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL 8260 STD STK_00033 1,1,1,2-Tetrachloroethane 100 ug/mL 2 mL 2 mL 12/25/1212/11/12 8260 STD WK_00216 METHANOL, Lot NA 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL 

## 01/09/2013 Page 81 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL 08/31/14 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL Restek, Lot A088677 .8260 STD STK_00033 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 

## 01/09/2013 Page 82 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL ACRNITSTDSK_00032 Acetonitrile 800 ug/mL 2 mL 2 mL 11/26/1211/19/12 ACR/NITRSTDWK_00205 METHANOL, Lot NA Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL 12/31/12 (Purchased Reagent) Acetonitrile 800 ug/mL Restek, Lot A090686 .ACRNITSTDSK_00032 Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL ACRNITSTDSK_00033 Acetonitrile 800 ug/mL 2 mL 2 mL 12/11/1212/04/12 ACR/NITRSTDWK_00210 METHANOL, Lot NA Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL 01/31/13 (Purchased Reagent) Acetonitrile 800 ug/mL Restek, Lot A091152 .ACRNITSTDSK_00033 

## 01/09/2013 Page 83 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL ACRNITSTDSK_00034 Acetonitrile 800 ug/mL 2 mL 2 mL 12/18/1212/11/12 ACR/NITRSTDWK_00212 METHANOL, Lot NA Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL 02/28/13 (Purchased Reagent) Acetonitrile 800 ug/mL Restek, Lot A091858 .ACRNITSTDSK_00034 Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL APIX STD PT_00024 2-Nitropropane 10000 ug/mL 2 mL 250 uL 12/18/1212/04/12 APIX STD WK_00110 METHANOL, Lot DG596 3-Chloro-1-propene 250 ug/mL Cyclohexanone 10000 ug/mL Ethyl acetate 1250 ug/mL Ethyl methacrylate 250 ug/mL Iodomethane 250 ug/mL Isobutyl alcohol 10000 ug/mL Methacrylonitrile 250 ug/mL Methyl methacrylate 250 ug/mL n-Butanol 10000 ug/mL Pentachloroethane 250 ug/mL trans-1,4-Dichloro-2-butene 250 ug/mL APIX STD SK_00005 2-Nitropropane 80000 ug/mL 1 mL 1 mL 02/19/1311/19/12 .APIX STD PT_00024 METHANOL, Lot NA 3-Chloro-1-propene 2000 ug/mL Cyclohexanone 80000 ug/mL Ethyl acetate 10000 ug/mL Ethyl methacrylate 2000 ug/mL Iodomethane 2000 ug/mL Isobutyl alcohol 80000 ug/mL Methacrylonitrile 2000 ug/mL Methyl methacrylate 2000 ug/mL n-Butanol 80000 ug/mL Pentachloroethane 2000 ug/mL trans-1,4-Dichloro-2-butene 2000 ug/mL 09/04/13 (Purchased Reagent) 2-Nitropropane 80000 ug/mL SUPELCO, Lot LB95279 ..APIX STD SK_00005 3-Chloro-1-propene 2000 ug/mL Cyclohexanone 80000 ug/mL Ethyl acetate 10000 ug/mL Ethyl methacrylate 2000 ug/mL Iodomethane 2000 ug/mL Isobutyl alcohol 80000 ug/mL Methacrylonitrile 2000 ug/mL Methyl methacrylate 2000 ug/mL n-Butanol 80000 ug/mL Pentachloroethane 2000 ug/mL trans-1,4-Dichloro-2-butene 2000 ug/mL 

## 01/09/2013 Page 84 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte GAS STD SK_00027 Bromomethane 100 ug/mL 2 mL 2 mL 12/26/1211/19/12 GAS STD WK RE_00245 METHANOL, Lot NA Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Dichlorofluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL 08/31/14 (Purchased Reagent) Bromomethane 100 ug/mL RESTEK, Lot A088739 .GAS STD SK_00027 Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Dichlorofluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL GAS STD SK_00028 Bromomethane 100 ug/mL 2 mL 2 mL 12/11/1212/04/12 GAS STD WK RE_00251 METHANOL, Lot NA Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Dichlorofluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL 08/31/14 (Purchased Reagent) Bromomethane 100 ug/mL RESTEK, Lot A088739 .GAS STD SK_00028 Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Dichlorofluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL GAS STD SK_00028 Bromomethane 100 ug/mL 2 mL 2 mL 12/18/1212/11/12 GAS STD WK RE_00254 METHANOL, Lot NA Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Dichlorofluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL 08/31/14 (Purchased Reagent) Bromomethane 100 ug/mL RESTEK, Lot A088739 .GAS STD SK_00028 Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Dichlorofluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL ICAL2STDSK_00023 1,3,5-Trichlorobenzene 100 ug/mL 2 mL 2 mL 12/18/1212/04/12 ICAL2++STDWK_00108 METHANOL, Lot NA 2-Chloro-1,3-butadiene 100 ug/mL 2-Methylnaphthalene 100 ug/mL Butadiene 100 ug/mL Cyclohexane 100 ug/mL 

## 01/09/2013 Page 85 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Ethyl ether 100 ug/mL Hexane 100 ug/mL Isopropyl ether 100 ug/mL Methyl acetate 100 ug/mL Methylcyclohexane 100 ug/mL n-Heptane 100 ug/mL 05/31/14 (Purchased Reagent) 1,3,5-Trichlorobenzene 100 ug/mL Restek, Lot A088737 .ICAL2STDSK_00023 2-Chloro-1,3-butadiene 100 ug/mL 2-Methylnaphthalene 100 ug/mL Butadiene 100 ug/mL Cyclohexane 100 ug/mL Ethyl ether 100 ug/mL Hexane 100 ug/mL Isopropyl ether 100 ug/mL Methyl acetate 100 ug/mL Methylcyclohexane 100 ug/mL n-Heptane 100 ug/mL 8260 SS WK_00385 1,2-Dichloroethane-d4 (Surr) 48.12 ug/L 5 mL 0.9624 uL 01/01/1312/21/12 INST6 IS/SS_00134 1, Lot NA 4-Bromofluorobenzene (Surr) 48.12 ug/L Dibromofluoromethane 48.12 ug/L Toluene-d8 (Surr) 48.12 ug/L 8260 SS SK_00032 1,2-Dichloroethane-d4 (Surr) 250 ug/mL 5 mL 5 mL 01/01/1312/18/12 .8260 SS WK_00385 1, Lot NA 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 07/31/14 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL RESTEK, Lot A088175 ..8260 SS SK_00032 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL KET/CS2 SK_00013 2-Butanone (MEK) 100 ug/mL 2 mL 2 mL 12/03/1211/19/12 KET/CS2 STDWK_00180 METHANOL, Lot NA 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL 11/30/13 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL Restek, Lot A088681 .KET/CS2 SK_00013 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL KET/CS2 SK_00013 2-Butanone (MEK) 100 ug/mL 2 mL 2 mL 12/18/1212/04/12 KET/CS2 STDWK_00183 METHANOL, Lot NA 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL 11/30/13 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL Restek, Lot A088681 .KET/CS2 SK_00013 2-Hexanone 100 ug/mL 

## 01/09/2013 Page 86 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL KET/CS2 SK_00014 2-Butanone (MEK) 100 ug/mL 2 mL 2 mL 12/25/1212/11/12 KET/CS2 STDWK_00184 METHANOL, Lot NA 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL 11/30/13 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL Restek, Lot A088681 .KET/CS2 SK_00014 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL KET/CS2 SK_00014 2-Butanone (MEK) 100 ug/mL 2 mL 2 mL 01/09/1312/26/12 KET/CS2 STDWK_00185 METHANOL, Lot NA Acetone 100 ug/mL 11/30/13 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL Restek, Lot A088681 .KET/CS2 SK_00014 Acetone 100 ug/mL level1std5ppm_00006 Benzene 0.5 ug/mL 1 mL 100 uL 12/31/1603/20/12 level 1_00011 1, Lot CY647 Ethylbenzene 0.5 ug/mL m-Xylene & p-Xylene 1 ug/mL o-Xylene 0.5 ug/mL Toluene 0.5 ug/mL Trichloroethene 0.5 ug/mL Vinyl chloride 0.5 ug/mL level18260wk_00006 Benzene 5 ug/mL 2 mL 100 uL 02/28/1203/22/11 .level1std5ppm_00006 1, Lot CY647 Ethylbenzene 5 ug/mL m-Xylene & p-Xylene 10 ug/mL o-Xylene 5 ug/mL Toluene 5 ug/mL Trichloroethene 5 ug/mL level1gaswk_00006 100 uLVinyl chloride 5 ug/mL level18260sk_00001 Benzene 100 ug/mL 1 mL 1 mL 06/30/1203/22/11 ..level18260wk_00006 1, Lot NA Ethylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL o-Xylene 100 ug/mL Toluene 100 ug/mL Trichloroethene 100 ug/mL 06/30/12 (Purchased Reagent) Benzene 100 ug/mL Restek, Lot AO67921 ...level18260sk_00001 Ethylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL o-Xylene 100 ug/mL Toluene 100 ug/mL Trichloroethene 100 ug/mL 02/28/1203/22/11 2 mLlevel1gaspt_00005 100 uLVinyl chloride 100 ug/mL ..level1gaswk_00006 1, Lot CY647 02/28/1203/22/11 1 mLlevel1gassk_00001 1 mLVinyl chloride 2000 ug/mL ...level1gaspt_00005 MEOH, Lot NA 02/28/12 (Purchased Reagent) Vinyl chloride 2000 ug/mL SUPELCO, Lot LB65254 ....level1gassk_00001 

## 01/09/2013 Page 87 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte APIX STD WK_00110 2-Nitropropane 1000 ug/mL 1 mL 100 uL 12/18/1212/04/12 LOAPIXSTDWK_00130 1, Lot DG596 3-Chloro-1-propene 25 ug/mL Cyclohexanone 1000 ug/mL Ethyl acetate 125 ug/mL Ethyl methacrylate 25 ug/mL Iodomethane 25 ug/mL Isobutyl alcohol 1000 ug/mL Methacrylonitrile 25 ug/mL Methyl methacrylate 25 ug/mL n-Butanol 1000 ug/mL Pentachloroethane 25 ug/mL trans-1,4-Dichloro-2-butene 25 ug/mL APIX STD PT_00024 2-Nitropropane 10000 ug/mL 2 mL 250 uL 12/18/1212/04/12 .APIX STD WK_00110 METHANOL, Lot DG596 3-Chloro-1-propene 250 ug/mL Cyclohexanone 10000 ug/mL Ethyl acetate 1250 ug/mL Ethyl methacrylate 250 ug/mL Iodomethane 250 ug/mL Isobutyl alcohol 10000 ug/mL Methacrylonitrile 250 ug/mL Methyl methacrylate 250 ug/mL n-Butanol 10000 ug/mL Pentachloroethane 250 ug/mL trans-1,4-Dichloro-2-butene 250 ug/mL APIX STD SK_00005 2-Nitropropane 80000 ug/mL 1 mL 1 mL 02/19/1311/19/12 ..APIX STD PT_00024 METHANOL, Lot NA 3-Chloro-1-propene 2000 ug/mL Cyclohexanone 80000 ug/mL Ethyl acetate 10000 ug/mL Ethyl methacrylate 2000 ug/mL Iodomethane 2000 ug/mL Isobutyl alcohol 80000 ug/mL Methacrylonitrile 2000 ug/mL Methyl methacrylate 2000 ug/mL n-Butanol 80000 ug/mL Pentachloroethane 2000 ug/mL trans-1,4-Dichloro-2-butene 2000 ug/mL 09/04/13 (Purchased Reagent) 2-Nitropropane 80000 ug/mL SUPELCO, Lot LB95279 ...APIX STD SK_00005 3-Chloro-1-propene 2000 ug/mL Cyclohexanone 80000 ug/mL Ethyl acetate 10000 ug/mL Ethyl methacrylate 2000 ug/mL Iodomethane 2000 ug/mL Isobutyl alcohol 80000 ug/mL Methacrylonitrile 2000 ug/mL Methyl methacrylate 2000 ug/mL n-Butanol 80000 ug/mL Pentachloroethane 2000 ug/mL trans-1,4-Dichloro-2-butene 2000 ug/mL 

## 01/09/2013 Page 88 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte ICAL2++STDWK_00108 1,3,5-Trichlorobenzene 5 ug/mL 1 mL 50 uL 12/18/1212/04/12 LOICAL2STDWK_00123 1, Lot DG596 2-Chloro-1,3-butadiene 5 ug/mL 2-Methylnaphthalene 5 ug/mL Butadiene 5 ug/mL Cyclohexane 5 ug/mL Ethyl ether 5 ug/mL Hexane 5 ug/mL Isopropyl ether 5 ug/mL Methyl acetate 5 ug/mL Methylcyclohexane 5 ug/mL n-Heptane 5 ug/mL ICAL2STDSK_00023 1,3,5-Trichlorobenzene 100 ug/mL 2 mL 2 mL 12/18/1212/04/12 .ICAL2++STDWK_00108 METHANOL, Lot NA 2-Chloro-1,3-butadiene 100 ug/mL 2-Methylnaphthalene 100 ug/mL Butadiene 100 ug/mL Cyclohexane 100 ug/mL Ethyl ether 100 ug/mL Hexane 100 ug/mL Isopropyl ether 100 ug/mL Methyl acetate 100 ug/mL Methylcyclohexane 100 ug/mL n-Heptane 100 ug/mL 05/31/14 (Purchased Reagent) 1,3,5-Trichlorobenzene 100 ug/mL Restek, Lot A088737 ..ICAL2STDSK_00023 2-Chloro-1,3-butadiene 100 ug/mL 2-Methylnaphthalene 100 ug/mL Butadiene 100 ug/mL Cyclohexane 100 ug/mL Ethyl ether 100 ug/mL Hexane 100 ug/mL Isopropyl ether 100 ug/mL Methyl acetate 100 ug/mL Methylcyclohexane 100 ug/mL n-Heptane 100 ug/mL 8260 SS WK_00382 1,2-Dichloroethane-d4 (Surr) 50 ug/mL 1 mL 200 uL 12/18/1212/04/12 LOW8260SS WK_00044 1, Lot DA057 4-Bromofluorobenzene (Surr) 50 ug/mL Dibromofluoromethane 50 ug/mL Toluene-d8 (Surr) 50 ug/mL 8260 SS SK_00032 1,2-Dichloroethane-d4 (Surr) 250 ug/mL 5 mL 5 mL 12/18/1212/04/12 .8260 SS WK_00382 1, Lot NA 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 07/31/14 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL RESTEK, Lot A088175 ..8260 SS SK_00032 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 8260 STD WK_00212 1,1,1,2-Tetrachloroethane 5 ug/mL 1 mL 50 uL 11/26/1211/20/12 LOW8260STD WK_00211 1, Lot DG596 1,1,1-Trichloroethane 5 ug/mL 

## 01/09/2013 Page 89 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 1,1,2,2-Tetrachloroethane 5 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 5 ug/mL 1,1,2-Trichloroethane 5 ug/mL 1,1-Dichloroethane 5 ug/mL 1,1-Dichloroethene 5 ug/mL 1,1-Dichloropropene 5 ug/mL 1,2,3-Trichlorobenzene 5 ug/mL 1,2,3-Trichloropropane 5 ug/mL 1,2,4-Trichlorobenzene 5 ug/mL 1,2,4-Trimethylbenzene 5 ug/mL 1,2-Dibromo-3-Chloropropane 5 ug/mL 1,2-Dichlorobenzene 5 ug/mL 1,2-Dichloroethane 5 ug/mL 1,2-Dichloropropane 5 ug/mL 1,3,5-Trimethylbenzene 5 ug/mL 1,3-Dichlorobenzene 5 ug/mL 1,3-Dichloropropane 5 ug/mL 1,4-Dichlorobenzene 5 ug/mL 1-Chlorohexane 5 ug/mL 2,2-Dichloropropane 5 ug/mL 2-Chlorotoluene 5 ug/mL 4-Chlorotoluene 5 ug/mL 4-Isopropyltoluene 5 ug/mL Benzene 5 ug/mL Bromobenzene 5 ug/mL Bromoform 5 ug/mL Carbon tetrachloride 5 ug/mL Chlorobenzene 5 ug/mL Chlorobromomethane 5 ug/mL Chlorodibromomethane 5 ug/mL Chloroform 5 ug/mL cis-1,2-Dichloroethene 5 ug/mL cis-1,3-Dichloropropene 5 ug/mL Dibromomethane 5 ug/mL Dichlorobromomethane 5 ug/mL Ethylbenzene 5 ug/mL Ethylene Dibromide 5 ug/mL Hexachlorobutadiene 5 ug/mL Isopropylbenzene 5 ug/mL m-Xylene & p-Xylene 10 ug/mL Methyl tert-butyl ether 5 ug/mL Methylene Chloride 5 ug/mL n-Butylbenzene 5 ug/mL N-Propylbenzene 5 ug/mL Naphthalene 5 ug/mL o-Xylene 5 ug/mL sec-Butylbenzene 5 ug/mL 

## 01/09/2013 Page 90 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Styrene 5 ug/mL tert-Butylbenzene 5 ug/mL Tetrachloroethene 5 ug/mL Tetrahydrofuran 5 ug/mL Toluene 5 ug/mL trans-1,2-Dichloroethene 5 ug/mL trans-1,3-Dichloropropene 5 ug/mL Trichloroethene 5 ug/mL Bromomethane 5 ug/mL GAS STD WK RE_00245 50 uLChloroethane 5 ug/mL Chloromethane 5 ug/mL Dichlorodifluoromethane 5 ug/mL Dichlorofluoromethane 5 ug/mL Trichlorofluoromethane 5 ug/mL Vinyl chloride 5 ug/mL 2-Butanone (MEK) 5 ug/mL KET/CS2 STDWK_00180 50 uL2-Hexanone 5 ug/mL 4-Methyl-2-pentanone (MIBK) 5 ug/mL Acetone 5 ug/mL Carbon disulfide 5 ug/mL 2-Chloroethyl vinyl ether 5 ug/mL VA/2CEVESTDWK_00175 50 uLVinyl acetate 5 ug/mL 8260 STD STK_00033 1,1,1,2-Tetrachloroethane 100 ug/mL 2 mL 2 mL 12/03/1211/19/12 .8260 STD WK_00212 METHANOL, Lot NA 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL 

## 01/09/2013 Page 91 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL 08/31/14 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL Restek, Lot A088677 ..8260 STD STK_00033 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 

## 01/09/2013 Page 92 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL GAS STD SK_00027 Bromomethane 100 ug/mL 2 mL 2 mL 12/26/1211/19/12 .GAS STD WK RE_00245 METHANOL, Lot NA Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Dichlorofluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL 

## 01/09/2013 Page 93 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Vinyl chloride 100 ug/mL 08/31/14 (Purchased Reagent) Bromomethane 100 ug/mL RESTEK, Lot A088739 ..GAS STD SK_00027 Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Dichlorofluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL KET/CS2 SK_00013 2-Butanone (MEK) 100 ug/mL 2 mL 2 mL 12/03/1211/19/12 .KET/CS2 STDWK_00180 METHANOL, Lot NA 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL 11/30/13 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL Restek, Lot A088681 ..KET/CS2 SK_00013 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL 2-CEVE STD PT_00023 2-Chloroethyl vinyl ether 100 ug/mL 2 mL 100 uL 11/26/1211/19/12 .VA/2CEVESTDWK_00175 METHANOL, Lot DG860 VA STD PT_00024 100 uLVinyl acetate 100 ug/mL 01/08/1310/08/12 1 mL2-CEVESTDSK_00005 1 mL2-Chloroethyl vinyl ether 2000 ug/mL ..2-CEVE STD PT_00023 METHANOL, Lot NA 11/30/16 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL Restek, Lot A085117 ...2-CEVESTDSK_00005 01/10/1310/11/12 1 mLVA STD SK_00007 1 mLVinyl acetate 2000 ug/mL ..VA STD PT_00024 METHANOL, Lot NA 03/31/14 (Purchased Reagent) Vinyl acetate 2000 ug/mL RESTEK, Lot A090525 ...VA STD SK_00007 8260 STD WK_00215 1,1,1,2-Tetrachloroethane 5 ug/mL 1 mL 50 uL 12/11/1212/04/12 LOW8260STD WK_00214 1, Lot DG860 1,1,1-Trichloroethane 5 ug/mL 1,1,2,2-Tetrachloroethane 5 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 5 ug/mL 1,1,2-Trichloroethane 5 ug/mL 1,1-Dichloroethane 5 ug/mL 1,1-Dichloroethene 5 ug/mL 1,1-Dichloropropene 5 ug/mL 1,2,3-Trichlorobenzene 5 ug/mL 1,2,3-Trichloropropane 5 ug/mL 1,2,4-Trichlorobenzene 5 ug/mL 1,2,4-Trimethylbenzene 5 ug/mL 1,2-Dibromo-3-Chloropropane 5 ug/mL 1,2-Dichlorobenzene 5 ug/mL 1,2-Dichloroethane 5 ug/mL 1,2-Dichloropropane 5 ug/mL 1,3,5-Trimethylbenzene 5 ug/mL 1,3-Dichlorobenzene 5 ug/mL 1,3-Dichloropropane 5 ug/mL 1,4-Dichlorobenzene 5 ug/mL 1-Chlorohexane 5 ug/mL 2,2-Dichloropropane 5 ug/mL 2-Chlorotoluene 5 ug/mL 

## 01/09/2013 Page 94 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 4-Chlorotoluene 5 ug/mL 4-Isopropyltoluene 5 ug/mL Benzene 5 ug/mL Bromobenzene 5 ug/mL Bromoform 5 ug/mL Carbon tetrachloride 5 ug/mL Chlorobenzene 5 ug/mL Chlorobromomethane 5 ug/mL Chlorodibromomethane 5 ug/mL Chloroform 5 ug/mL cis-1,2-Dichloroethene 5 ug/mL cis-1,3-Dichloropropene 5 ug/mL Dibromomethane 5 ug/mL Dichlorobromomethane 5 ug/mL Ethylbenzene 5 ug/mL Ethylene Dibromide 5 ug/mL Hexachlorobutadiene 5 ug/mL Isopropylbenzene 5 ug/mL m-Xylene & p-Xylene 10 ug/mL Methyl tert-butyl ether 5 ug/mL Methylene Chloride 5 ug/mL n-Butylbenzene 5 ug/mL N-Propylbenzene 5 ug/mL Naphthalene 5 ug/mL o-Xylene 5 ug/mL sec-Butylbenzene 5 ug/mL Styrene 5 ug/mL tert-Butylbenzene 5 ug/mL Tetrachloroethene 5 ug/mL Tetrahydrofuran 5 ug/mL Toluene 5 ug/mL trans-1,2-Dichloroethene 5 ug/mL trans-1,3-Dichloropropene 5 ug/mL Trichloroethene 5 ug/mL Bromomethane 5 ug/mL GAS STD WK RE_00251 50 uLChloroethane 5 ug/mL Chloromethane 5 ug/mL Dichlorodifluoromethane 5 ug/mL Dichlorofluoromethane 5 ug/mL Trichlorofluoromethane 5 ug/mL Vinyl chloride 5 ug/mL 2-Butanone (MEK) 5 ug/mL KET/CS2 STDWK_00183 50 uL2-Hexanone 5 ug/mL 4-Methyl-2-pentanone (MIBK) 5 ug/mL Acetone 5 ug/mL Carbon disulfide 5 ug/mL 2-Chloroethyl vinyl ether 5 ug/mL VA/2CEVESTDWK_00178 50 uLVinyl acetate 5 ug/mL 

## 01/09/2013 Page 95 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 8260 STD STK_00033 1,1,1,2-Tetrachloroethane 100 ug/mL 2 mL 2 mL 12/18/1212/04/12 .8260 STD WK_00215 METHANOL, Lot NA 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL 

## 01/09/2013 Page 96 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL 08/31/14 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL Restek, Lot A088677 ..8260 STD STK_00033 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL 

## 01/09/2013 Page 97 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL GAS STD SK_00028 Bromomethane 100 ug/mL 2 mL 2 mL 12/11/1212/04/12 .GAS STD WK RE_00251 METHANOL, Lot NA Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Dichlorofluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL 08/31/14 (Purchased Reagent) Bromomethane 100 ug/mL RESTEK, Lot A088739 ..GAS STD SK_00028 Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Dichlorofluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL KET/CS2 SK_00013 2-Butanone (MEK) 100 ug/mL 2 mL 2 mL 12/18/1212/04/12 .KET/CS2 STDWK_00183 METHANOL, Lot NA 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL 11/30/13 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL Restek, Lot A088681 ..KET/CS2 SK_00013 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL 2-CEVE STD PT_00024 2-Chloroethyl vinyl ether 100 ug/mL 2 mL 100 uL 12/18/1212/04/12 .VA/2CEVESTDWK_00178 METHANOL, Lot DG860 VA STD PT_00025 100 uLVinyl acetate 100 ug/mL 02/21/1311/21/12 1 mL2-CEVESTDSK_00005 1 mL2-Chloroethyl vinyl ether 2000 ug/mL ..2-CEVE STD PT_00024 METHANOL, Lot NA 11/30/16 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL Restek, Lot A085117 ...2-CEVESTDSK_00005 

## 01/09/2013 Page 98 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 02/21/1311/21/12 1 mLVA STD SK_00007 1 mLVinyl acetate 2000 ug/mL ..VA STD PT_00025 METHANOL, Lot NA 03/31/14 (Purchased Reagent) Vinyl acetate 2000 ug/mL RESTEK, Lot A090525 ...VA STD SK_00007 8260 STD WK_00216 1,1,1,2-Tetrachloroethane 5 ug/mL 1 mL 50 uL 12/18/1212/11/12 LOW8260STD WK_00215 1, Lot DG860 1,1,1-Trichloroethane 5 ug/mL 1,1,2,2-Tetrachloroethane 5 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 5 ug/mL 1,1,2-Trichloroethane 5 ug/mL 1,1-Dichloroethane 5 ug/mL 1,1-Dichloroethene 5 ug/mL 1,1-Dichloropropene 5 ug/mL 1,2,3-Trichlorobenzene 5 ug/mL 1,2,3-Trichloropropane 5 ug/mL 1,2,4-Trichlorobenzene 5 ug/mL 1,2,4-Trimethylbenzene 5 ug/mL 1,2-Dibromo-3-Chloropropane 5 ug/mL 1,2-Dichlorobenzene 5 ug/mL 1,2-Dichloroethane 5 ug/mL 1,2-Dichloropropane 5 ug/mL 1,3,5-Trimethylbenzene 5 ug/mL 1,3-Dichlorobenzene 5 ug/mL 1,3-Dichloropropane 5 ug/mL 1,4-Dichlorobenzene 5 ug/mL 1-Chlorohexane 5 ug/mL 2,2-Dichloropropane 5 ug/mL 2-Chlorotoluene 5 ug/mL 4-Chlorotoluene 5 ug/mL 4-Isopropyltoluene 5 ug/mL Benzene 5 ug/mL Bromobenzene 5 ug/mL Bromoform 5 ug/mL Carbon tetrachloride 5 ug/mL Chlorobenzene 5 ug/mL Chlorobromomethane 5 ug/mL Chlorodibromomethane 5 ug/mL Chloroform 5 ug/mL cis-1,2-Dichloroethene 5 ug/mL cis-1,3-Dichloropropene 5 ug/mL Dibromomethane 5 ug/mL Dichlorobromomethane 5 ug/mL Ethylbenzene 5 ug/mL Ethylene Dibromide 5 ug/mL Hexachlorobutadiene 5 ug/mL Isopropylbenzene 5 ug/mL m-Xylene & p-Xylene 10 ug/mL Methyl tert-butyl ether 5 ug/mL Methylene Chloride 5 ug/mL n-Butylbenzene 5 ug/mL 

## 01/09/2013 Page 99 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte N-Propylbenzene 5 ug/mL Naphthalene 5 ug/mL o-Xylene 5 ug/mL sec-Butylbenzene 5 ug/mL Styrene 5 ug/mL tert-Butylbenzene 5 ug/mL Tetrachloroethene 5 ug/mL Tetrahydrofuran 5 ug/mL Toluene 5 ug/mL trans-1,2-Dichloroethene 5 ug/mL trans-1,3-Dichloropropene 5 ug/mL Trichloroethene 5 ug/mL Bromomethane 5 ug/mL GAS STD WK RE_00254 50 uLChloroethane 5 ug/mL Chloromethane 5 ug/mL Dichlorodifluoromethane 5 ug/mL Dichlorofluoromethane 5 ug/mL Trichlorofluoromethane 5 ug/mL Vinyl chloride 5 ug/mL 2-Butanone (MEK) 5 ug/mL KET/CS2 STDWK_00184 50 uL2-Hexanone 5 ug/mL 4-Methyl-2-pentanone (MIBK) 5 ug/mL Acetone 5 ug/mL Carbon disulfide 5 ug/mL 2-Chloroethyl vinyl ether 5 ug/mL VA/2CEVESTDWK_00179 50 uLVinyl acetate 5 ug/mL 8260 STD STK_00033 1,1,1,2-Tetrachloroethane 100 ug/mL 2 mL 2 mL 12/25/1212/11/12 .8260 STD WK_00216 METHANOL, Lot NA 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 

## 01/09/2013 Page 100 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL 08/31/14 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL Restek, Lot A088677 ..8260 STD STK_00033 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 

## 01/09/2013 Page 101 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL GAS STD SK_00028 Bromomethane 100 ug/mL 2 mL 2 mL 12/18/1212/11/12 .GAS STD WK RE_00254 METHANOL, Lot NA Chloroethane 100 ug/mL 

## 01/09/2013 Page 102 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Dichlorofluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL 08/31/14 (Purchased Reagent) Bromomethane 100 ug/mL RESTEK, Lot A088739 ..GAS STD SK_00028 Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Dichlorofluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL KET/CS2 SK_00014 2-Butanone (MEK) 100 ug/mL 2 mL 2 mL 12/25/1212/11/12 .KET/CS2 STDWK_00184 METHANOL, Lot NA 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL 11/30/13 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL Restek, Lot A088681 ..KET/CS2 SK_00014 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL 2-CEVE STD PT_00024 2-Chloroethyl vinyl ether 100 ug/mL 2 mL 100 uL 12/25/1212/11/12 .VA/2CEVESTDWK_00179 METHANOL, Lot DG860 VA STD PT_00025 100 uLVinyl acetate 100 ug/mL 02/21/1311/21/12 1 mL2-CEVESTDSK_00005 1 mL2-Chloroethyl vinyl ether 2000 ug/mL ..2-CEVE STD PT_00024 METHANOL, Lot NA 11/30/16 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL Restek, Lot A085117 ...2-CEVESTDSK_00005 02/21/1311/21/12 1 mLVA STD SK_00007 1 mLVinyl acetate 2000 ug/mL ..VA STD PT_00025 METHANOL, Lot NA 03/31/14 (Purchased Reagent) Vinyl acetate 2000 ug/mL RESTEK, Lot A090525 ...VA STD SK_00007 ACR/NITRSTDWK_00205 Acetonitrile 80 ug/mL 1 mL 100 uL 11/26/1211/20/12 LOWACRSTD WK_00190 MEOH, Lot DG596 Acrolein 400 ug/mL Acrylonitrile 80 ug/mL Propionitrile 80 ug/mL ACRNITSTDSK_00032 Acetonitrile 800 ug/mL 2 mL 2 mL 11/26/1211/19/12 .ACR/NITRSTDWK_00205 METHANOL, Lot NA Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL 12/31/12 (Purchased Reagent) Acetonitrile 800 ug/mL Restek, Lot A090686 ..ACRNITSTDSK_00032 Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL ACR/NITRSTDWK_00210 Acetonitrile 80 ug/mL 1 mL 100 uL 12/11/1212/04/12 LOWACRSTD WK_00192 MEOH, Lot DG860 Acrolein 400 ug/mL Acrylonitrile 80 ug/mL Propionitrile 80 ug/mL ACRNITSTDSK_00033 Acetonitrile 800 ug/mL 2 mL 2 mL 12/11/1212/04/12 .ACR/NITRSTDWK_00210 METHANOL, Lot NA Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL 

## 01/09/2013 Page 103 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Propionitrile 800 ug/mL 01/31/13 (Purchased Reagent) Acetonitrile 800 ug/mL Restek, Lot A091152 ..ACRNITSTDSK_00033 Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL ACR/NITRSTDWK_00212 Acetonitrile 80 ug/mL 1 mL 100 uL 12/18/1212/11/12 LOWACRSTD WK_00193 MEOH, Lot DG860 Acrolein 400 ug/mL Acrylonitrile 80 ug/mL Propionitrile 80 ug/mL ACRNITSTDSK_00034 Acetonitrile 800 ug/mL 2 mL 2 mL 12/18/1212/11/12 .ACR/NITRSTDWK_00212 METHANOL, Lot NA Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL 02/28/13 (Purchased Reagent) Acetonitrile 800 ug/mL Restek, Lot A091858 ..ACRNITSTDSK_00034 Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL 05/31/17 (Purchased Reagent) Mercury 1000 ug/mL ULTRA, Lot L00365 M11FSTKHG_00001 01/01/13 (Purchased Reagent) Mercury 1000 ug/mL Inorganic Ventures, Lot E2-HG02091 M12ASTKHG_00001 M12ESTKIC_00003 As 10 ug/mL 500 mL 3 mL 05/23/1310/04/12 M12JSPKIC_00002 1, Lot N\A Lead 10 ug/mL M12ESTKIC_00006 4 mLTl 10 ug/mL M12ESTKIC_00010 2.5 mLAl 200 ug/mL M12ESTKIC_00011 50 mLBarium 200 ug/mL Ca 1000 ug/mL K 1000 ug/mL Mg 1000 ug/mL Na 1000 ug/mL As 10 ug/mL M12ESTKIC_00012 50 mLB 100 ug/mL Be 5 ug/mL Bi 50 ug/mL Cd 5 ug/mL Chromium 20 ug/mL Co 50 ug/mL Copper 25 ug/mL Fe 100 ug/mL Lead 10 ug/mL Li 50 ug/mL Mn 50 ug/mL Nickel 50 ug/mL Se 10 ug/mL Sr 100 ug/mL Tl 10 ug/mL Vanadium 50 ug/mL Zinc 50 ug/mL 

## 01/09/2013 Page 104 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Ag 5 ug/mL M12ESTKIC_00013 50 mLMo 100 ug/mL Sb 50 ug/mL Si 500 ug/mL Sn 100 ug/mL Ti 100 ug/mL M12ISTKIC_00004 4.5 mLSe 10 ug/mL 06/01/13 (Purchased Reagent) As 1000 ug/mL IV, Lot F2-AS02083 .M12ESTKIC_00003 06/01/13 (Purchased Reagent) Lead 1000 ug/mL IV, Lot F2-PB03035 .M12ESTKIC_00006 06/01/13 (Purchased Reagent) Tl 1000 ug/mL IV, Lot E2-TL01124 .M12ESTKIC_00010 05/23/13 (Purchased Reagent) Al 2000 ug/mL EE, Lot 1214205 .M12ESTKIC_00011 Barium 2000 ug/mL Ca 10000 ug/mL K 10000 ug/mL Mg 10000 ug/mL Na 10000 ug/mL 05/23/13 (Purchased Reagent) As 40 ug/mL EE, Lot 1214206 .M12ESTKIC_00012 B 1000 ug/mL Be 50 ug/mL Bi 500 ug/mL Cd 50 ug/mL Chromium 200 ug/mL Co 500 ug/mL Copper 250 ug/mL Fe 1000 ug/mL Lead 20 ug/mL Li 500 ug/mL Mn 500 ug/mL Nickel 500 ug/mL Se 10 ug/mL Sr 1000 ug/mL Tl 50 ug/mL Vanadium 500 ug/mL Zinc 500 ug/mL 05/23/13 (Purchased Reagent) Ag 50 ug/mL EE, Lot 1214331 .M12ESTKIC_00013 Mo 1000 ug/mL Sb 500 ug/mL Si 5000 ug/mL Sn 1000 ug/mL Ti 1000 ug/mL 09/01/13 (Purchased Reagent) Se 1000 ug/mL IV, Lot E2-SE02033 .M12ISTKIC_00004 M12ESTKIC_00003 As 10 ug/mL 500 mL 3 mL 05/23/1311/20/12 M12KSPKIC_00001 1, Lot N\A Lead 10 ug/mL M12ESTKIC_00006 4 mLTl 10 ug/mL M12ESTKIC_00010 2.5 mLAl 200 ug/mL M12ESTKIC_00011 50 mLBarium 200 ug/mL Ca 1000 ug/mL 

## 01/09/2013 Page 105 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte K 1000 ug/mL Mg 1000 ug/mL Na 1000 ug/mL As 10 ug/mL M12ESTKIC_00012 50 mLB 100 ug/mL Be 5 ug/mL Bi 50 ug/mL Cd 5 ug/mL Chromium 20 ug/mL Co 50 ug/mL Copper 25 ug/mL Fe 100 ug/mL Lead 10 ug/mL Li 50 ug/mL Mn 50 ug/mL Nickel 50 ug/mL Se 10 ug/mL Sr 100 ug/mL Tl 10 ug/mL Vanadium 50 ug/mL Zinc 50 ug/mL Ag 5 ug/mL M12ESTKIC_00013 50 mLMo 100 ug/mL Sb 50 ug/mL Si 500 ug/mL Sn 100 ug/mL Ti 100 ug/mL M12ISTKIC_00004 4.5 mLSe 10 ug/mL 06/01/13 (Purchased Reagent) As 1000 ug/mL IV, Lot F2-AS02083 .M12ESTKIC_00003 06/01/13 (Purchased Reagent) Lead 1000 ug/mL IV, Lot F2-PB03035 .M12ESTKIC_00006 06/01/13 (Purchased Reagent) Tl 1000 ug/mL IV, Lot E2-TL01124 .M12ESTKIC_00010 05/23/13 (Purchased Reagent) Al 2000 ug/mL EE, Lot 1214205 .M12ESTKIC_00011 Barium 2000 ug/mL Ca 10000 ug/mL K 10000 ug/mL Mg 10000 ug/mL Na 10000 ug/mL 05/23/13 (Purchased Reagent) As 40 ug/mL EE, Lot 1214206 .M12ESTKIC_00012 B 1000 ug/mL Be 50 ug/mL Bi 500 ug/mL Cd 50 ug/mL Chromium 200 ug/mL Co 500 ug/mL Copper 250 ug/mL Fe 1000 ug/mL Lead 20 ug/mL Li 500 ug/mL 

## 01/09/2013 Page 106 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Mn 500 ug/mL Nickel 500 ug/mL Se 10 ug/mL Sr 1000 ug/mL Tl 50 ug/mL Vanadium 500 ug/mL Zinc 500 ug/mL 05/23/13 (Purchased Reagent) Ag 50 ug/mL EE, Lot 1214331 .M12ESTKIC_00013 Mo 1000 ug/mL Sb 500 ug/mL Si 5000 ug/mL Sn 1000 ug/mL Ti 1000 ug/mL 09/01/13 (Purchased Reagent) Se 1000 ug/mL IV, Lot E2-SE02033 .M12ISTKIC_00004 M12GSTKIC_00002 Barium 0.5 ug/mL 1000 mL 10 mL 07/10/1312/10/12 M12LCCVIC_00001 1, Lot N/A Chromium 0.5 ug/mL Copper 0.5 ug/mL Lead 0.5 ug/mL Nickel 0.5 ug/mL Vanadium 5 ug/mL Zinc 0.5 ug/mL 07/10/13 (Purchased Reagent) Barium 50 ug/mL HP, Lot 1219103 .M12GSTKIC_00002 Chromium 50 ug/mL Copper 50 ug/mL Lead 50 ug/mL Nickel 50 ug/mL Vanadium 500 ug/mL Zinc 50 ug/mL M12ESTKIC_00002 Barium 20 ug/L 1000 mL 2 mL 06/01/1312/03/12 M12LCRIIC_00001 1, Lot NA Chromium 20 ug/L Copper 20 ug/L Lead 10 ug/L Nickel 20 ug/L Vanadium 10 ug/L Zinc 40 ug/L 06/01/13 (Purchased Reagent) Barium 10 ug/mL IV, Lot F2-MEB423074 .M12ESTKIC_00002 Chromium 10 ug/mL Copper 10 ug/mL Lead 5 ug/mL Nickel 10 ug/mL Vanadium 5 ug/mL Zinc 20 ug/mL M12GSTKIC_00002 Barium 0.4 ug/mL 1000 mL 8 mL 07/10/1312/06/12 M12LICVIC_00001 1, Lot N/A Chromium 0.4 ug/mL Copper 0.4 ug/mL Lead 0.4 ug/mL Nickel 0.4 ug/mL 

## 01/09/2013 Page 107 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Vanadium 4 ug/mL Zinc 0.4 ug/mL 07/10/13 (Purchased Reagent) Barium 50 ug/mL HP, Lot 1219103 .M12GSTKIC_00002 Chromium 50 ug/mL Copper 50 ug/mL Lead 50 ug/mL Nickel 50 ug/mL Vanadium 500 ug/mL Zinc 50 ug/mL M12KSTKIC_00003 Al 500 ug/mL 1000 mL 100 mL 12/01/1312/03/12 M12LISAIC_00001 1, Lot na Ca 500 ug/mL Fe 200 ug/mL Mg 500 ug/mL 12/01/13 (Purchased Reagent) Al 5000 ug/mL IV, Lot F2-meb414132 .M12KSTKIC_00003 Ca 5000 ug/mL Fe 2000 ug/mL Mg 5000 ug/mL M12ISTKIC_00003 Ag 0.2 ug/mL 1000 mL 10 mL 09/01/1312/03/12 M12LISBIC_00001 1, Lot B51037 As 0.1 ug/mL Barium 0.5 ug/mL Be 0.5 ug/mL Cd 1 ug/mL Chromium 0.5 ug/mL Co 0.5 ug/mL Copper 0.5 ug/mL Lead 0.05 ug/mL Mn 0.5 ug/mL Nickel 1 ug/mL Sb 0.6 ug/mL Se 0.05 ug/mL Tl 0.1 ug/mL Vanadium 0.5 ug/mL Zinc 1 ug/mL Al 500 ug/mL M12KSTKIC_00003 100 mLCa 500 ug/mL Fe 200 ug/mL Mg 500 ug/mL 09/01/13 (Purchased Reagent) Ag 20 ug/mL IV, Lot E2-MEB399019 .M12ISTKIC_00003 As 10 ug/mL Barium 50 ug/mL Be 50 ug/mL Cd 100 ug/mL Chromium 50 ug/mL Co 50 ug/mL Copper 50 ug/mL Lead 5 ug/mL Mn 50 ug/mL 

## 01/09/2013 Page 108 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Nickel 100 ug/mL Sb 60 ug/mL Se 5 ug/mL Tl 10 ug/mL Vanadium 50 ug/mL Zinc 100 ug/mL 12/01/13 (Purchased Reagent) Al 5000 ug/mL IV, Lot F2-meb414132 .M12KSTKIC_00003 Ca 5000 ug/mL Fe 2000 ug/mL Mg 5000 ug/mL 2-CEVE STD PT_00023 2-Chloroethyl vinyl ether 100 ug/mL 2 mL 100 uL 11/26/1211/19/12 VA/2CEVESTDWK_00175 METHANOL, Lot DG860 VA STD PT_00024 100 uLVinyl acetate 100 ug/mL 01/08/1310/08/12 1 mL2-CEVESTDSK_00005 1 mL2-Chloroethyl vinyl ether 2000 ug/mL .2-CEVE STD PT_00023 METHANOL, Lot NA 11/30/16 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL Restek, Lot A085117 ..2-CEVESTDSK_00005 01/10/1310/11/12 1 mLVA STD SK_00007 1 mLVinyl acetate 2000 ug/mL .VA STD PT_00024 METHANOL, Lot NA 03/31/14 (Purchased Reagent) Vinyl acetate 2000 ug/mL RESTEK, Lot A090525 ..VA STD SK_00007 2-CEVE STD PT_00024 2-Chloroethyl vinyl ether 100 ug/mL 2 mL 100 uL 12/18/1212/04/12 VA/2CEVESTDWK_00178 METHANOL, Lot DG860 VA STD PT_00025 100 uLVinyl acetate 100 ug/mL 02/21/1311/21/12 1 mL2-CEVESTDSK_00005 1 mL2-Chloroethyl vinyl ether 2000 ug/mL .2-CEVE STD PT_00024 METHANOL, Lot NA 11/30/16 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL Restek, Lot A085117 ..2-CEVESTDSK_00005 02/21/1311/21/12 1 mLVA STD SK_00007 1 mLVinyl acetate 2000 ug/mL .VA STD PT_00025 METHANOL, Lot NA 03/31/14 (Purchased Reagent) Vinyl acetate 2000 ug/mL RESTEK, Lot A090525 ..VA STD SK_00007 2-CEVE STD PT_00024 2-Chloroethyl vinyl ether 100 ug/mL 2 mL 100 uL 12/25/1212/11/12 VA/2CEVESTDWK_00179 METHANOL, Lot DG860 VA STD PT_00025 100 uLVinyl acetate 100 ug/mL 02/21/1311/21/12 1 mL2-CEVESTDSK_00005 1 mL2-Chloroethyl vinyl ether 2000 ug/mL .2-CEVE STD PT_00024 METHANOL, Lot NA 11/30/16 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL Restek, Lot A085117 ..2-CEVESTDSK_00005 02/21/1311/21/12 1 mLVA STD SK_00007 1 mLVinyl acetate 2000 ug/mL .VA STD PT_00025 METHANOL, Lot NA 03/31/14 (Purchased Reagent) Vinyl acetate 2000 ug/mL RESTEK, Lot A090525 ..VA STD SK_00007 8260ADDSPKPT_00025 2-Butanone (MEK) 50 mg/L 2 mL 50 uL 12/03/1211/19/12 VOC/THF SPK_00124 1, Lot DG596 Acetone 50 mg/L 8260ADDSPKSK_00015 2-Butanone (MEK) 2000 mg/L 1 mL 1 mL 01/19/1311/19/12 .8260ADDSPKPT_00025 1, Lot NA Acetone 2000 mg/L 01/19/13 (Purchased Reagent) 2-Butanone (MEK) 2000 mg/L ACCUSTD, Lot 212091219 ..8260ADDSPKSK_00015 Acetone 2000 mg/L 8260ADDSPKPT_00025 2-Butanone (MEK) 50 mg/L 2 mL 50 uL 12/12/1211/28/12 VOC/THF SPK_00125 1, Lot DG596 Acetone 50 mg/L 8260ADDSPKSK_00015 2-Butanone (MEK) 2000 mg/L 1 mL 1 mL 01/19/1311/19/12 .8260ADDSPKPT_00025 1, Lot NA Acetone 2000 mg/L 01/19/13 (Purchased Reagent) 2-Butanone (MEK) 2000 mg/L ACCUSTD, Lot 212091219 ..8260ADDSPKSK_00015 Acetone 2000 mg/L 8260ADDSPKPT_00025 2-Butanone (MEK) 50 mg/L 2 mL 50 uL 12/25/1212/11/12 VOC/THF SPK_00127 1, Lot DG860 Acetone 50 mg/L 8260ADDSPKSK_00015 2-Butanone (MEK) 2000 mg/L 1 mL 1 mL 01/19/1311/19/12 .8260ADDSPKPT_00025 1, Lot NA Acetone 2000 mg/L 01/19/13 (Purchased Reagent) 2-Butanone (MEK) 2000 mg/L ACCUSTD, Lot 212091219 ..8260ADDSPKSK_00015 Acetone 2000 mg/L 

## 01/09/2013 Page 109 of 384

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 8260ADDSPKPT_00025 2-Butanone (MEK) 50 mg/L 2 mL 50 uL 01/04/1312/21/12 VOC/THF SPK_00128 1, Lot DG860 Acetone 50 mg/L 8260ADDSPKSK_00015 2-Butanone (MEK) 2000 mg/L 1 mL 1 mL 01/19/1311/19/12 .8260ADDSPKPT_00025 1, Lot NA Acetone 2000 mg/L 01/19/13 (Purchased Reagent) 2-Butanone (MEK) 2000 mg/L ACCUSTD, Lot 212091219 ..8260ADDSPKSK_00015 Acetone 2000 mg/L 04/30/15 (Purchased Reagent) Chromium, hexavalent 1000 mg/L ERA, Lot 160412 WSTCR1_00008 12/29/12 (Purchased Reagent) Chromium, hexavalent 16.9 mg/L STL, Lot Lead(II)Chrom_00001 WSTCR13_00629 05/31/17 (Purchased Reagent) Chromium, hexavalent 1000 mg/L Ultra Scientific, Lot L00439 WSTCR2_00008 12/27/1212/27/12 100 mLWSTCN1_00011 1 mLCyanide, Total 10 mg/L WSTINCN1_00571 DI WATER, Lot NA 01/31/14 (Purchased Reagent) Cyanide, Total 1000 mg/L ERA, Lot 060112 .WSTCN1_00011 12/28/1212/28/12 100 mLWSTCN1_00011 1 mLCyanide, Total 10 mg/L WSTINCN1_00572 DI WATER, Lot NA 01/31/14 (Purchased Reagent) Cyanide, Total 1000 mg/L ERA, Lot 060112 .WSTCN1_00011 WSTCN2_00028 Cyanide, Amenable 10 mg/L 100 mL 1 mL 12/27/1212/27/12 WSTINCN2_00563 DI WATER, Lot NA Cyanide, Free 10 mg/L Cyanide, Reactive 10 mg/L Cyanide, Total 10 mg/L Cyanide, Weak Acid Dissociable 10 mg/L 03/31/13 (Purchased Reagent) Cyanide, Amenable 1000 mg/L RICCA, Lot 4204518 .WSTCN2_00028 Cyanide, Free 1000 mg/L Cyanide, Reactive 1000 mg/L Cyanide, Total 1000 mg/L Cyanide, Weak Acid Dissociable 1000 mg/L WSTCN2_00028 Cyanide, Amenable 10 mg/L 100 mL 1 mL 12/28/1212/28/12 WSTINCN2_00564 DI WATER, Lot NA Cyanide, Free 10 mg/L Cyanide, Reactive 10 mg/L Cyanide, Total 10 mg/L Cyanide, Weak Acid Dissociable 10 mg/L 03/31/13 (Purchased Reagent) Cyanide, Amenable 1000 mg/L RICCA, Lot 4204518 .WSTCN2_00028 Cyanide, Free 1000 mg/L Cyanide, Reactive 1000 mg/L Cyanide, Total 1000 mg/L Cyanide, Weak Acid Dissociable 1000 mg/L 11/15/13 (Purchased Reagent) Sulfide 180 mg/L NaS/1.5g/JTB/Y39592, Lot Zn0.5n/20mL WSTSF1_00036 Sulfide as H2S 209.1 mg/L Sulfide, Reactive 180 mg/L



## 01/09/2013 Page 110 of 384

# Certification Summary Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1 Project/Site:John Deere Des MoinesWorks(JDDMW)

Laboratory Authority Program EPA Region Certification ID TestAmerica Chicago 40461 State Program Alabama 4 TestAmerica Chicago 01132CA NELAP California 9 TestAmerica Chicago 939 State Program Georgia 4 TestAmerica Chicago N/A State Program Georgia 4 TestAmerica Chicago N/A State Program Hawaii 9 TestAmerica Chicago 100201 NELAP Illinois 5 TestAmerica Chicago C-IL-02 State Program Indiana 5 TestAmerica Chicago 82 State Program Iowa 7 TestAmerica Chicago E-10161 NELAP Kansas 7 TestAmerica Chicago 90023 State Program Kentucky 4 TestAmerica Chicago 66 State Program Kentucky (UST) 4 TestAmerica Chicago 30720 NELAP Louisiana 6 TestAmerica Chicago M-IL035 State Program Massachusetts 1 TestAmerica Chicago N/A State Program Mississippi 4 TestAmerica Chicago 291 State Program North Carolina DENR 4 TestAmerica Chicago R-194 State Program North Dakota 8 TestAmerica Chicago 8908 State Program Oklahoma 6 TestAmerica Chicago 77001 State Program South Carolina 4 TestAmerica Chicago T104704252-09-TX NELAP Texas 6 TestAmerica Chicago P330-12-00038 Federal USDA TestAmerica Chicago 460142 NELAP Virginia 3 TestAmerica Chicago 999580010 State Program Wisconsin 5 TestAmerica Chicago 8TMS-Q State Program Wyoming 8 Accreditation may not be offered or required for all methods and analytes reported in this package

.Please contact your project manager for the laboratory’s current list of certified methods and analytes.



### TestAmerica Chicago 

## 01/09/2013 Page 111 of 384

# Method 8260B Volatile Organic Compounds (GC/MS) by Method 8260B

01/09/2013

Page 112 of 384

### FORM II GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.:500-53491-1 SDG No.: Matrix:Solid Level:Low TestAmerica Chicago

GC Column (1):DB624 ID:0.2(mm)
# Lab Sample ID Client Sample ID # # # DBFM DCA TOL BFB 500-53491-3 FC DISCRETE 6 95 89 87 79 500-53491-4 FC D DISCRETE 6 90 91 89 75 MB 500-173973/5 90 94 96 84 LCS 500-173973/6 81 84 89 81 LCSD 500-173973/7 91 88 93 87



### QC LIMITS QC LIMITS DBFM = Dibromofluoromethane 75-120 DCA = 1,2-Dichloroethane-d4 (Surr) 70-134 TOL = Toluene-d8 (Surr) 75-122 BFB = 4-Bromofluorobenzene (Surr) 70-122

FORM II 8260B # Column to be used to flag recovery values


## 01/09/2013 Page 113 of 384

### FORM II GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.:500-53491-1 SDG No.: Matrix:Solid Level:Medium TestAmerica Chicago

GC Column (1):DB624 ID:0.2(mm)
# Lab Sample ID Client Sample ID # # # DBFM DCA TOL BFB 500-53491-3 DL FC DISCRETE 6 DL 93 97 96 94 500-53491-4 DL FC D DISCRETE 6 DL 96 105 101 100 MB 500-174064/6 96 101 101 98 LCS 500-174064/4 100 95 97 97



### QC LIMITS QC LIMITS DBFM = Dibromofluoromethane 75-120 DCA = 1,2-Dichloroethane-d4 (Surr) 75-125 TOL = Toluene-d8 (Surr) 75-120 BFB = 4-Bromofluorobenzene (Surr) 75-120

FORM II 8260B # Column to be used to flag recovery values


## 01/09/2013 Page 114 of 384

### FORM II GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.:500-53491-1 SDG No.: Matrix:Water Level:Low TestAmerica Chicago

GC Column (1):DB624 ID:0.2(mm)
# Lab Sample ID Client Sample ID # # # DBFM DCA TOL BFB 500-53491-5 FC EB 6 90 88 94 88 500-53491-6 TRIP BLANK 93 93 100 93 MB 500-173987/7 97 98 103 97 LCS 500-173987/4 94 92 96 96



### QC LIMITS QC LIMITS DBFM = Dibromofluoromethane 75-120 DCA = 1,2-Dichloroethane-d4 (Surr) 75-125 TOL = Toluene-d8 (Surr) 75-120 BFB = 4-Bromofluorobenzene (Surr) 75-120

FORM II 8260B # Column to be used to flag recovery values


## 01/09/2013 Page 115 of 384

### GC/MS VOA LAB CONTROL SAMPLE RECOVERY FORM III

Job No.: Lab Name: SDG No.: Level: Matrix: Matrix: Low 500-53491-1

Lab File ID:6S1227.d Solid Lab ID:LCS 500-173973/6 Client ID: TestAmerica Chicago

REC % REC QC LIMITS CONCENTRATION (ug/Kg) SPIKE ADDED (ug/Kg) # LCS LCS COMPOUND Acetone 50.0 47.98 50-138 96 2-Butanone (MEK) 50.0 43.18 58-133 86

FORM III 8260B # Column to be used to flag recovery and RPD values


## 01/09/2013 Page 116 of 384

### GC/MS VOA LAB CONTROL SAMPLE RECOVERY FORM III

Job No.: Lab Name: SDG No.: Level: Matrix: Matrix: Low 500-53491-1

Lab File ID:22S1227.D Water Lab ID:LCS 500-173987/4 Client ID: TestAmerica Chicago

REC % REC QC LIMITS CONCENTRATION (ug/L) SPIKE ADDED (ug/L) # LCS LCS COMPOUND Acetone 50.0 53.44 46-153 107 2-Butanone (MEK) 50.0 46.97 54-138 94

FORM III 8260B # Column to be used to flag recovery and RPD values


## 01/09/2013 Page 117 of 384

### GC/MS VOA LAB CONTROL SAMPLE RECOVERY FORM III

Job No.: Lab Name: SDG No.: Level: Matrix: Matrix: Medium 500-53491-1

Lab File ID:18S1228.D Solid Lab ID:LCS 500-174064/4 Client ID: TestAmerica Chicago

REC % REC QC LIMITS CONCENTRATION (ug/Kg) SPIKE ADDED (ug/Kg) # LCS LCS COMPOUND Acetone 50.0 50.53 46-153 101 2-Butanone (MEK) 50.0 43.61 54-138 87

FORM III 8260B # Column to be used to flag recovery and RPD values


## 01/09/2013 Page 118 of 384

### GC/MS VOA LAB CONTROL SAMPLE DUPLICATE RECOVERY FORM III

Job No.: Lab Name: SDG No.: Level: Matrix: Matrix: Low 500-53491-1

Lab File ID:6T1227.d Solid Lab ID:LCSD 500-173973/7 Client ID: TestAmerica Chicago

COMPOUND SPIKE ADDED CONCENTRATION % REC % RPD QC LIMITS
RPD REC (ug/Kg) (ug/Kg) # LCSD LCSD

50.0 55.07 30 50-138 Acetone 14 110 50.0 44.82 30 58-133 2-Butanone (MEK) 4 90

FORM III 8260B # Column to be used to flag recovery and RPD values


## 01/09/2013 Page 119 of 384

### FORM IV GC/MS VOA METHOD BLANK SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Date Analyzed: GC Column: ID: Instrument ID: 12/28/2012 10:45 DB624 N Heated Purge:(Y/N) CMS18 18M1228.D Lab File ID: Lab Sample ID:MB 500-174064/6 Solid Matrix:
0.2(mm) THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID LAB FILE ID DATE ANALYZED CLIENT SAMPLE ID 12/28/2012 10:00 18S1228.D LCS 500-174064/4 12/28/2012 11:08 53491-03.D 500-53491-3 DL FC DISCRETE 6 DL 12/28/2012 11:31 53491-04.D 500-53491-4 DL FC D DISCRETE 6 DL

FORM IV 8260B 

## 01/09/2013 Page 120 of 384

### FORM IV GC/MS VOA METHOD BLANK SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Date Analyzed: GC Column: ID: Instrument ID: 12/27/2012 10:33 DB624 Y Heated Purge:(Y/N) CMS06 6M1227.d Lab File ID: Lab Sample ID:MB 500-173973/5 Solid Matrix:
0.2(mm) THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID LAB FILE ID DATE ANALYZED CLIENT SAMPLE ID 12/27/2012 10:56 6S1227.d LCS 500-173973/6 12/27/2012 11:19 6T1227.d LCSD 500-173973/7 12/27/2012 13:36 3491-03.d 500-53491-3 FC DISCRETE 6 12/27/2012 13:59 3491-04.d 500-53491-4 FC D DISCRETE 6

FORM IV 8260B 

## 01/09/2013 Page 121 of 384

### FORM IV GC/MS VOA METHOD BLANK SUMMARY

Lab Name: SDG No.: Job No.:500-53491-1 TestAmerica Chicago

Date Analyzed: GC Column: ID: Instrument ID: 12/27/2012 14:10 DB624 N Heated Purge:(Y/N) CMS22 22M1227.D Lab File ID: Lab Sample ID:MB 500-173987/7 Water Matrix:
0.2(mm) THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID LAB FILE ID DATE ANALYZED CLIENT SAMPLE ID 12/27/2012 12:46 22S1227.D LCS 500-173987/4 12/27/2012 15:28 53491-06.D 500-53491-6 TRIP BLANK 12/27/2012 15:54 53491-05.D 500-53491-5 FC EB 6

FORM IV 8260B 

## 01/09/2013 Page 122 of 384

### FORM V BROMOFLUOROBENZENE (BFB)

Lab Name: SDG No.: Job No.:500-53491-1

Lab File ID: Instrument ID:6B1204.d CMS06 12/04/2012 14:01 BFB Injection Date: BFB Injection Time:

M/EION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.: 171819

5015.0 - 40.0 % of mass 95 33.6 7530.0 - 60.0 % of mass 95 56.3 95Base Peak, 100% relative abundance 100.0 965.0 - 9.0 % of mass 95 7.2 173Less than 2.0 % of mass 174 1.8 (1.8)1 17450.0 - 120.00 % of mass 95 98.1 1755.0 - 9.0 % of mass 174 8.3 (8.4)1 17695.0 - 101.0 % of mass 174 96.8 (98.7)1 1775.0 - 9.0 % of mass 176 7.2 (7.5)2 1-Value is % mass 174 2-Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID LAB FILE ID LAB SAMPLE ID DATE ANALYZED TIME ANALYZED 6I1204a.d 12/04/2012 14:34 STD1 500-171819/2 6I1204b.d 12/04/2012 14:57 STD2 500-171819/3 6I1204d.d 12/04/2012 15:43 STD4 500-171819/5 6I1204CC.d 12/04/2012 16:10 STD3 500-171819/16 6I1204e.d 12/04/2012 16:33 STD5 500-171819/6 6I1204f.d 12/04/2012 16:55 STD6 500-171819/7 6J1204a.d 12/04/2012 17:18 STD1AP 500-171819/8 6J1204b.d 12/04/2012 17:41 STD2AP 500-171819/9 6J1204c.d 12/04/2012 18:04 STD3AP 500-171819/10 6J1204d.d 12/04/2012 18:27 STD4AP 500-171819/11 6J1204e.d 12/04/2012 18:49 STD5AP 500-171819/12 6J1204f.d 12/04/2012 19:13 STD6AP 500-171819/13 6S1204.d 12/04/2012 19:58 ICV 500-171819/15

FORM V 8260B 

## 01/09/2013 Page 123 of 384

### FORM V BROMOFLUOROBENZENE (BFB)

Lab Name: SDG No.: Job No.:500-53491-1

Lab File ID: Instrument ID:6B1227.d CMS06 12/27/2012 08:48 BFB Injection Date: BFB Injection Time:

M/EION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.: 173973

5015.0 - 40.0 % of mass 95 28.9 7530.0 - 60.0 % of mass 95 50.2 95Base Peak, 100% relative abundance 100.0 965.0 - 9.0 % of mass 95 6.8 173Less than 2.0 % of mass 174 0.6 (0.6)1 17450.0 - 120.00 % of mass 95 92.9 1755.0 - 9.0 % of mass 174 6.6 (7.1)1 17695.0 - 101.0 % of mass 174 92.0 (99.0)1 1775.0 - 9.0 % of mass 176 5.7 (6.2)2 1-Value is % mass 174 2-Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID LAB FILE ID LAB SAMPLE ID DATE ANALYZED TIME ANALYZED 6C1227.d 12/27/2012 09:47 CCV 500-173973/3 6D1227.d 12/27/2012 10:10 CCV 500-173973/4 6M1227.d 12/27/2012 10:33 MB 500-173973/5 6S1227.d 12/27/2012 10:56 LCS 500-173973/6 6T1227.d 12/27/2012 11:19 LCSD 500-173973/7 FC DISCRETE 6 3491-03.d 12/27/2012 13:36 500-53491-3 FC D DISCRETE 6 3491-04.d 12/27/2012 13:59 500-53491-4

FORM V 8260B 

## 01/09/2013 Page 124 of 384

### FORM V BROMOFLUOROBENZENE (BFB)

Lab Name: SDG No.: Job No.:500-53491-1

Lab File ID: Instrument ID:18B1120a.D CMS18 11/20/2012 15:22 BFB Injection Date: BFB Injection Time:

M/EION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.: 170445

5015.0 - 40.0 % of mass 95 27.9 7530.0 - 60.0 % of mass 95 48.2 95Base Peak, 100% relative abundance 100.0 965.0 - 9.0 % of mass 95 7.2 173Less than 2.0 % of mass 174 0.7 (0.8)1 17450.0 - 120.00 % of mass 95 80.8 1755.0 - 9.0 % of mass 174 5.5 (6.8)1 17695.0 - 101.0 % of mass 174 79.4 (98.2)1 1775.0 - 9.0 % of mass 176 5.5 (6.9)2 1-Value is % mass 174 2-Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID LAB FILE ID LAB SAMPLE ID DATE ANALYZED TIME ANALYZED 18I1120a.D 11/20/2012 15:57 STD1 500-170445/2 18I1120b.D 11/20/2012 16:21 STD2 500-170445/3 18I1120c.D 11/20/2012 16:46 STD3 500-170445/4 18I1120d.D 11/20/2012 17:10 STD4 500-170445/5 18I1120e.D 11/20/2012 17:35 STD5 500-170445/6 18I1120f.D 11/20/2012 17:59 STD6 500-170445/7 18I1120g.D 11/20/2012 18:23 STD7 500-170445/8 18I1120h.D 11/20/2012 18:47 STD8 500-170445/9 18I1120i.D 11/20/2012 19:11 STD9 500-170445/10 18S1120.D 11/20/2012 23:15 ICV 500-170445/20

FORM V 8260B 

## 01/09/2013 Page 125 of 384

### FORM V BROMOFLUOROBENZENE (BFB)

Lab Name: SDG No.: Job No.:500-53491-1

Lab File ID: Instrument ID:18B1228a.D CMS18 12/28/2012 08:39 BFB Injection Date: BFB Injection Time:

M/EION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.: 174064

5015.0 - 40.0 % of mass 95 32.7 7530.0 - 60.0 % of mass 95 49.9 95Base Peak, 100% relative abundance 100.0 965.0 - 9.0 % of mass 95 6.5 173Less than 2.0 % of mass 174 0.0 (0.0)1 17450.0 - 120.00 % of mass 95 113.8 1755.0 - 9.0 % of mass 174 7.1 (6.2)1 17695.0 - 101.0 % of mass 174 109.4 (96.1)1 1775.0 - 9.0 % of mass 176 8.0 (7.3)2 1-Value is % mass 174 2-Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID LAB FILE ID LAB SAMPLE ID DATE ANALYZED TIME ANALYZED 18C1228.D 12/28/2012 09:14 CCV 500-174064/2 18D1228.D 12/28/2012 09:37 CCV 500-174064/3 18S1228.D 12/28/2012 10:00 LCS 500-174064/4 18M1228.D 12/28/2012 10:45 MB 500-174064/6 FC DISCRETE 6 DL 53491-03.D 12/28/2012 11:08 500-53491-3 DL FC D DISCRETE 6 DL 53491-04.D 12/28/2012 11:31 500-53491-4 DL

FORM V 8260B 

## 01/09/2013 Page 126 of 384

### FORM V BROMOFLUOROBENZENE (BFB)

Lab Name: SDG No.: Job No.:500-53491-1

Lab File ID: Instrument ID:22B1211.D CMS22 12/11/2012 13:45 BFB Injection Date: BFB Injection Time:

M/EION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.: 172615

5015.0 - 40.0 % of mass 95 22.6 7530.0 - 60.0 % of mass 95 45.2 95Base Peak, 100% relative abundance 100.0 965.0 - 9.0 % of mass 95 7.5 173Less than 2.0 % of mass 174 0.0 (0.0)1 17450.0 - 120.00 % of mass 95 86.2 1755.0 - 9.0 % of mass 174 5.9 (6.8)1 17695.0 - 101.0 % of mass 174 86.4 (100.2)1 1775.0 - 9.0 % of mass 176 4.9 (5.7)2 1-Value is % mass 174 2-Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID LAB FILE ID LAB SAMPLE ID DATE ANALYZED TIME ANALYZED 22I1211A.D 12/11/2012 14:23 STD01 500-172615/2 22I1211B.D 12/11/2012 14:51 STD02 500-172615/3 22I1211C.D 12/11/2012 15:20 STD03 500-172615/4 22I1211D.D 12/11/2012 15:48 STD04 500-172615/5 22I1211E.D 12/11/2012 16:16 STD05 500-172615/6 22I1211F.D 12/11/2012 16:44 STD06 500-172615/7 22I1211G.D 12/11/2012 17:13 STD07 500-172615/8 22I1211H.D 12/11/2012 17:41 STD08 500-172615/9 22I1211I.D 12/11/2012 18:09 STD09 500-172615/10 22S1211.D 12/12/2012 00:17 ICV 500-172615/23

FORM V 8260B 

## 01/09/2013 Page 127 of 384

### FORM V BROMOFLUOROBENZENE (BFB)

Lab Name: SDG No.: Job No.:500-53491-1

Lab File ID: Instrument ID:22B1227.D CMS22 12/27/2012 11:16 BFB Injection Date: BFB Injection Time:

M/EION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.: 173987

5015.0 - 40.0 % of mass 95 28.5 7530.0 - 60.0 % of mass 95 53.0 95Base Peak, 100% relative abundance 100.0 965.0 - 9.0 % of mass 95 6.9 173Less than 2.0 % of mass 174 1.6 (1.6)1 17450.0 - 120.00 % of mass 95 100.4 1755.0 - 9.0 % of mass 174 8.2 (8.2)1 17695.0 - 101.0 % of mass 174 97.3 (96.9)1 1775.0 - 9.0 % of mass 176 5.0 (5.1)2 1-Value is % mass 174 2-Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID LAB FILE ID LAB SAMPLE ID DATE ANALYZED TIME ANALYZED 22C1227.D 12/27/2012 11:55 CCV 500-173987/2 22D1227.D 12/27/2012 12:22 CCV 500-173987/3 22S1227.D 12/27/2012 12:46 LCS 500-173987/4 22M1227.D 12/27/2012 14:10 MB 500-173987/7 TRIP BLANK 53491-06.D 12/27/2012 15:28 500-53491-6 FC EB 6 53491-05.D 12/27/2012 15:54 500-53491-5

FORM V 8260B 

## 01/09/2013 Page 128 of 384

### GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.: SDG No.: FORM VIII

TestAmerica Chicago 500-53491-1
Sample No.:STD3 500-171819/16 Date Analyzed:12/04/2012 16:10
Lab File ID (Standard): 6I1204CC.d Instrument ID:CMS06 GC Column:DB624 ID:0.2(mm) Heated Purge: (Y/N) Y Calibration ID:10745

AREA# RT# AREA RT# AREA# RT# # PFB DFB CBZ

UPPER LIMIT LOWER LIMIT 961332 240333 341607 1366426 334952 1339808 4.64 5.52 8.71 INITIAL CALIBRATION MID-POINT 5.14 4.14 6.02 5.02 9.21 8.21 480666 683213 669904

LAB SAMPLE ID CLIENT SAMPLE ID ICV 500-171819/15 526825 733790 696556 4.65 5.52 8.70 CCV 500-173973/3 524403 730945 744845 4.65 5.52 8.71 CCV 500-173973/4 570893 773092 773457 4.64 5.52 8.70 MB 500-173973/5 564902 741762 785524 4.65 5.52 8.71 LCS 500-173973/6 645535 860713 834642 4.64 5.52 8.70 LCSD 500-173973/7 596394 810667 809211 4.64 5.52 8.70 500-53491-3 FC DISCRETE 6 342289 476748 442713 4.64 5.52 8.70 500-53491-4 FC D DISCRETE 6 386100 531388 510019 4.65 5.52 8.70



### PFB = Pentafluorobenzene DFB = 1,4-Difluorobenzene CBZ = Chlorobenzene-d5 Area Limit = 50%-200% of internal standard area RT Limit = ± 0.5 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII 8260B 

## 01/09/2013 Page 129 of 384

### GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.: SDG No.: FORM VIII

TestAmerica Chicago 500-53491-1
Sample No.:STD3 500-171819/16 Date Analyzed:12/04/2012 16:10
Lab File ID (Standard): 6I1204CC.d Instrument ID:CMS06 GC Column:DB624 ID:0.2(mm) Heated Purge: (Y/N) Y Calibration ID:10745

AREA# RT# AREA RT# AREA# RT# # DCB

UPPER LIMIT LOWER LIMIT 843448 210862 10.72 INITIAL CALIBRATION MID-POINT 11.22 10.22 421724

LAB SAMPLE ID CLIENT SAMPLE ID ICV 500-171819/15 427951 10.72 CCV 500-173973/3 446339 10.72 CCV 500-173973/4 451529 10.72 MB 500-173973/5 410551 10.72 LCS 500-173973/6 480914 10.72 LCSD 500-173973/7 484380 10.72 500-53491-3 FC DISCRETE 6 197214*10.72 500-53491-4 FC D DISCRETE 6 222254 10.72



### DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area RT Limit = ± 0.5 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII 8260B 

## 01/09/2013 Page 130 of 384

### GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.: SDG No.: FORM VIII

TestAmerica Chicago 500-53491-1
Sample No.:STD6 500-170445/7 Date Analyzed:11/20/2012 17:59
Lab File ID (Standard): 18I1120f.D Instrument ID:CMS18 GC Column:DB624 ID:0.2(mm) Heated Purge: (Y/N) N Calibration ID:10631

AREA# RT# AREA RT# AREA# RT# # PFB DFB CBZ

UPPER LIMIT LOWER LIMIT 596976 149244 211381 845522 189544 758174 5.64 6.62 9.64 INITIAL CALIBRATION MID-POINT 6.14 5.14 7.12 6.12 10.14 9.14 298488 422761 379087

LAB SAMPLE ID CLIENT SAMPLE ID ICV 500-170445/20 294287 437412 387064 5.64 6.62 9.64 CCV 500-174064/2 280225 414660 352358 5.64 6.62 9.64 CCV 500-174064/3 280433 415891 349478 5.64 6.62 9.63 LCS 500-174064/4 289268 434398 356182 5.64 6.62 9.64 MB 500-174064/6 276833 407408 370803 5.64 6.62 9.63 500-53491-3 DL FC DISCRETE 6 DL 265949 385748 345191 5.64 6.62 9.64 500-53491-4 DL FC D DISCRETE 6 DL 252764 366504 331985 5.64 6.62 9.64



### PFB = Pentafluorobenzene DFB = 1,4-Difluorobenzene CBZ = Chlorobenzene-d5 Area Limit = 50%-200% of internal standard area RT Limit = ± 0.5 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII 8260B 

## 01/09/2013 Page 131 of 384

### GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.: SDG No.: FORM VIII

TestAmerica Chicago 500-53491-1
Sample No.:STD6 500-170445/7 Date Analyzed:11/20/2012 17:59
Lab File ID (Standard): 18I1120f.D Instrument ID:CMS18 GC Column:DB624 ID:0.2(mm) Heated Purge: (Y/N) N Calibration ID:10631

AREA# RT# AREA RT# AREA# RT# # DCB

UPPER LIMIT LOWER LIMIT 435034 108759 11.63 INITIAL CALIBRATION MID-POINT 12.13 11.13 217517

LAB SAMPLE ID CLIENT SAMPLE ID ICV 500-170445/20 213606 11.63 CCV 500-174064/2 194389 11.63 CCV 500-174064/3 193721 11.63 LCS 500-174064/4 199496 11.63 MB 500-174064/6 190160 11.63 500-53491-3 DL FC DISCRETE 6 DL 180402 11.63 500-53491-4 DL FC D DISCRETE 6 DL 175640 11.63



### DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area RT Limit = ± 0.5 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII 8260B 

## 01/09/2013 Page 132 of 384

### GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.: SDG No.: FORM VIII

TestAmerica Chicago 500-53491-1
Sample No.:STD06 500-172615/7 Date Analyzed:12/11/2012 16:44
Lab File ID (Standard): 22I1211F.D Instrument ID:CMS22 GC Column:DB624 ID:0.2(mm) Heated Purge: (Y/N) N Calibration ID:10830

AREA# RT# AREA RT# AREA# RT# # PFB DFB CBZ

UPPER LIMIT LOWER LIMIT 1409738 352435 493044 1972176 417716 1670864 6.27 7.24 10.64 INITIAL CALIBRATION MID-POINT 6.77 5.77 7.74 6.74 11.14 10.14 704869 986088 835432

LAB SAMPLE ID CLIENT SAMPLE ID ICV 500-172615/23 772269 1099840 931671 6.26 7.24 10.64 CCV 500-173987/2 701736 969856 822660 6.26 7.24 10.64 CCV 500-173987/3 696904 953661 799767 6.26 7.24 10.64 LCS 500-173987/4 716951 981854 841317 6.27 7.24 10.64 MB 500-173987/7 692291 945495 811334 6.26 7.24 10.64 500-53491-6 TRIP BLANK 686301 928214 796602 6.26 7.24 10.64 500-53491-5 FC EB 6 688414 958050 814329 6.26 7.24 10.64



### PFB = Pentafluorobenzene DFB = 1,4-Difluorobenzene CBZ = Chlorobenzene-d5 Area Limit = 50%-200% of internal standard area RT Limit = ± 0.5 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII 8260B 

## 01/09/2013 Page 133 of 384

### GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.: SDG No.: FORM VIII

TestAmerica Chicago 500-53491-1
Sample No.:STD06 500-172615/7 Date Analyzed:12/11/2012 16:44
Lab File ID (Standard): 22I1211F.D Instrument ID:CMS22 GC Column:DB624 ID:0.2(mm) Heated Purge: (Y/N) N Calibration ID:10830

AREA# RT# AREA RT# AREA# RT# # DCB

UPPER LIMIT LOWER LIMIT 1003186 250797 13.08 INITIAL CALIBRATION MID-POINT 13.58 12.58 501593

LAB SAMPLE ID CLIENT SAMPLE ID ICV 500-172615/23 542063 13.08 CCV 500-173987/2 499991 13.08 CCV 500-173987/3 451307 13.08 LCS 500-173987/4 515537 13.08 MB 500-173987/7 436959 13.08 500-53491-6 TRIP BLANK 433983 13.08 500-53491-5 FC EB 6 437814 13.07



### DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area RT Limit = ± 0.5 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII 8260B 

## 01/09/2013 Page 134 of 384

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.:

FC DISCRETE 6 SDG No.: 500-53491-1
Lab Sample ID:500-53491-3 Matrix: 3491-03.d Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

12/19/2012 14:20 Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol:

74.1 1
Level: (low/med) Low 5(g)
0.2(mm) Date Analyzed:12/27/2012 13:36

ID: DB624
Analysis Batch No.: 173973 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL19.3 6.98 J 78-93-3 2-Butanone (MEK) 11.8


### %REC CAS NO. LIMITS Q SURROGATE 89 70-134 17060-07-0 1,2-Dichloroethane-d4 (Surr) 87 75-122 2037-26-5 Toluene-d8 (Surr) 79 70-122 460-00-4 4-Bromofluorobenzene (Surr) 95 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/09/2013 Page 135 of 384

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.:

FC DISCRETE 6 DL SDG No.: 500-53491-1
Lab Sample ID:500-53491-3 DL Matrix: 53491-03.D Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

12/19/2012 14:20 Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol:

74.1 50
Level: (low/med)Medium 5(g) 5 (mL) 5(mL) 0.2(mm) Date Analyzed:12/28/2012 11:08

ID: DB624
Analysis Batch No.: 174064 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL963 251 67-64-1 Acetone 7020


### %REC CAS NO. LIMITS Q SURROGATE 97 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 96 75-120 2037-26-5 Toluene-d8 (Surr) 94 75-120 460-00-4 4-Bromofluorobenzene (Surr) 93 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/09/2013 Page 136 of 384

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.:

FC D DISCRETE 6 SDG No.: 500-53491-1
Lab Sample ID:500-53491-4 Matrix: 3491-04.d Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

12/19/2012 14:45 Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol:

72.4 1
Level: (low/med) Low 5(g)
0.2(mm) Date Analyzed:12/27/2012 13:59

ID: DB624
Analysis Batch No.: 173973 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL18.1 6.55 78-93-3 2-Butanone (MEK) 19.5


### %REC CAS NO. LIMITS Q SURROGATE 91 70-134 17060-07-0 1,2-Dichloroethane-d4 (Surr) 89 75-122 2037-26-5 Toluene-d8 (Surr) 75 70-122 460-00-4 4-Bromofluorobenzene (Surr) 90 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/09/2013 Page 137 of 384

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.:

FC D DISCRETE 6 DL SDG No.: 500-53491-1
Lab Sample ID:500-53491-4 DL Matrix: 53491-04.D Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

12/19/2012 14:45 Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol:

72.4 50
Level: (low/med)Medium 5(g) 5 (mL) 5(mL) 0.2(mm) Date Analyzed:12/28/2012 11:31

ID: DB624
Analysis Batch No.: 174064 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL905 235 67-64-1 Acetone 7150


### %REC CAS NO. LIMITS Q SURROGATE 105 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 101 75-120 2037-26-5 Toluene-d8 (Surr) 100 75-120 460-00-4 4-Bromofluorobenzene (Surr) 96 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/09/2013 Page 138 of 384

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.:

FC EB 6 SDG No.: 500-53491-1
Lab Sample ID:500-53491-5 Matrix: 53491-05.D Lab File ID: Date Collected: 8260B Analysis Method: Water TestAmerica Chicago

12/19/2012 14:10 Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med) Low 5(mL)
0.2(mm) Date Analyzed:12/27/2012 15:54

ID: DB624
Analysis Batch No.: 173987 ug/L Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 1.29 67-64-1 Acetone <5.00 5.00 1.47 78-93-3 2-Butanone (MEK) <5.00


### %REC CAS NO. LIMITS Q SURROGATE 88 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 94 75-120 2037-26-5 Toluene-d8 (Surr) 88 75-120 460-00-4 4-Bromofluorobenzene (Surr) 90 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/09/2013 Page 139 of 384

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.:

TRIP BLANK SDG No.: 500-53491-1
Lab Sample ID:500-53491-6 Matrix: 53491-06.D Lab File ID: Date Collected: 8260B Analysis Method: Water TestAmerica Chicago

12/19/2012 00:00 Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med) Low 5(mL)
0.2(mm) Date Analyzed:12/27/2012 15:28

ID: DB624
Analysis Batch No.: 173987 ug/L Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 1.29 67-64-1 Acetone <5.00 5.00 1.47 78-93-3 2-Butanone (MEK) <5.00


### %REC CAS NO. LIMITS Q SURROGATE 93 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 100 75-120 2037-26-5 Toluene-d8 (Surr) 93 75-120 460-00-4 4-Bromofluorobenzene (Surr) 93 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/09/2013 Page 140 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06 Analy Batch No.:171819

10745 Calibration Start Date: Calibration End Date: 12/04/2012 14:34 Y 12/04/2012 16:55 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

Calibration Files: LEVEL: LAB SAMPLE ID: LAB FILE ID: 1 Level STD1 500-171819/2 6I1204a.d 2 Level STD2 500-171819/3 6I1204b.d 3 Level STD3 500-171819/16 6I1204CC.d 4 Level STD4 500-171819/5 6I1204d.d 5 Level STD5 500-171819/6 6I1204e.d 6 Level STD6 500-171819/7 6I1204f.d

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 Dichlorodifluoromethane 1.0174 0.8189 0.9825 0.9247 0.9868Ave 7.8 1.0041 0.0100 15.0 0.9557 Chloromethane 1.3147 1.1022 1.1622 1.0959 1.1527Ave 6.8 1.1894 0.1000 15.0 1.1695 Vinyl chloride 1.0822 0.9159 0.9643 0.9041 0.9964Ave 6.7 1.0086 0.0100 15.0 0.9786 Bromomethane 0.6561 0.5359 0.5658 0.5126 0.5451Ave 8.8 0.5620 0.0100 15.0 0.5629 Chloroethane 0.8545 0.7097 0.6734 0.6547 0.6894Ave 10.0 0.6884 0.0100 15.0 0.7117 Dichlorofluoromethane 1.6464 1.4455 1.4042 1.3446 1.4482Ave 7.1 1.5072 0.0100 15.0 1.4660 Trichlorofluoromethane 1.5425 1.2252 1.2065 1.1652 1.2634Ave 11.0 1.2709 0.0100 15.0 1.2790 Acrolein 0.0784 0.0710 0.0627 0.0681 0.0819Ave 12.0 0.0868 0.0010 15.0 0.0748 1,1-Dichloroethene 0.5725 0.5062 0.5192 0.5251 0.5481Ave 4.9 0.5649 0.0100 15.0 0.5393 1,1,2-Trichloro-1,2,2-trifluoroethane 0.8092 0.6963 0.7098 0.7022 0.7462Ave 5.9 0.7585 0.0100 15.0 0.7370 Acetone 0.1969 0.1299 0.1270 0.1372 0.1393Qua2 0.9980 0.1352 0.0100 0.9900 0.41170.11270.0001 Carbon disulfide 2.0717 1.8310 2.1228 2.1508 2.0121Ave 5.6 2.0757 0.0100 15.0 2.0440 Acetonitrile 0.0839 0.0490 0.0402 0.0399 0.0449Qua2 0.9990 0.0467 0.0010 0.9900 2.03180.0331 0 Methylene Chloride 0.6635 0.5115 0.5232 0.4834 0.5084Ave 12.0 0.5109 0.0100 15.0 0.5335 Acrylonitrile 0.1524 0.1399 0.1237 0.1280 0.1525Ave 10.0 0.1586 0.0010 15.0 0.1425



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/09/2013 Page 141 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06 Analy Batch No.:171819

10745 Calibration Start Date: Calibration End Date: 12/04/2012 14:34 Y 12/04/2012 16:55 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 trans-1,2-Dichloroethene 0.5931 0.5632 0.5531 0.5573 0.5844Ave 3.1 0.5907 0.0100 15.0 0.5736 Methyl tert-butyl ether 1.2285 1.0592 1.1026 1.1125 1.1868Ave 5.7 1.1956 0.0100 15.0 1.1475 1,1-Dichloroethane 1.2472 1.1699 1.1522 1.1622 1.2237Ave 3.3 1.2205 0.1000 15.0 1.1960 Vinyl acetate 0.7953 0.7402 0.9524 0.8603 1.0101Ave 12.0 0.9422 0.0100 15.0 0.8834 2,2-Dichloropropane 0.7034 0.6557 0.7587 0.7383 0.7741Ave 7.0 0.7995 0.0100 15.0 0.7383 cis-1,2-Dichloroethene 0.6358 0.5831 0.5511 0.5572 0.5880Ave 5.1 0.5837 0.0100 15.0 0.5831 2-Butanone (MEK) 0.1589 0.1491 0.1741 0.1929 0.1968Ave 11.0 0.1738 0.0100 15.0 0.1743 Propionitrile 0.0334 0.0304 0.0304 0.0326 0.0352Ave 6.8 0.0355 0.0010 15.0 0.0329 Bromochloromethane 0.2640 0.2242 0.2236 0.2233 0.2335Ave 6.8 0.2290 0.0100 15.0 0.2329 Tetrahydrofuran 0.0961 0.0951 0.1082 0.1023 0.1102Ave 6.0 0.1040 0.0100 15.0 0.1027 Chloroform 1.0059 0.8787 0.8887 0.9034 0.9564Ave 5.2 0.9410 0.0100 15.0 0.9290 1,1,1-Trichloroethane 0.9044 0.7493 0.8505 0.8469 0.8894Ave 7.1 0.9164 0.0100 15.0 0.8595 Carbon tetrachloride 0.5349 0.4468 0.5129 0.5549 0.5765Ave 9.3 0.5790 0.0100 15.0 0.5342 1,1-Dichloropropene 0.8028 0.7274 0.7162 0.7444 0.7869Ave 4.5 0.7698 0.0100 15.0 0.7579 Benzene 1.5710 1.4004 1.3772 1.4946 1.4972Ave 4.9 1.4498 0.0100 15.0 1.4650 1,2-Dichloroethane 0.4930 0.4329 0.4442 0.4947 0.4992Ave 6.0 0.4759 0.0100 15.0 0.4733 Trichloroethene 0.4006 0.3758 0.3459 0.3888 0.3882Ave 5.0 0.3749 0.0100 15.0 0.3790 1,2-Dichloropropane 0.4161 0.3758 0.3680 0.3901 0.3985Ave 4.4 0.3843 0.0100 15.0 0.3888 Dibromomethane 0.1879 0.1660 0.1706 0.1741 0.1782Ave 4.4 0.1703 0.0100 15.0 0.1745 Bromodichloromethane 0.4312 0.3710 0.3994 0.4425 0.4477Ave 7.0 0.4284 0.0100 15.0 0.4200



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/09/2013 Page 142 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06 Analy Batch No.:171819

10745 Calibration Start Date: Calibration End Date: 12/04/2012 14:34 Y 12/04/2012 16:55 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 2-Chloroethyl vinyl ether 0.0965 0.0874 0.0962 0.0912 0.0993Ave 4.9 0.0903 0.0100 15.0 0.0935 cis-1,3-Dichloropropene 0.4355 0.4007 0.4109 0.4604 0.4750Ave 6.7 0.4574 0.0100 15.0 0.4400 4-Methyl-2-pentanone (MIBK) 0.2970 0.2305 0.2916 0.3119 0.2711Ave 11.0 0.2599 0.0100 15.0 0.2770 Toluene 0.9196 0.8482 0.8292 0.9329 0.9557Ave 5.9 0.9478 0.0100 15.0 0.9056 trans-1,3-Dichloropropene 0.3434 0.3227 0.3622 0.3988 0.4097Ave 9.3 0.3942 0.0100 15.0 0.3718 1,1,2-Trichloroethane 0.3027 0.2869 0.2979 0.3045 0.3149Ave 3.0 0.3024 0.0100 15.0 0.3016 Tetrachloroethene 0.4527 0.4310 0.4104 0.4575 0.4682Ave 4.7 0.4474 0.0100 15.0 0.4445 1,3-Dichloropropane 0.4154 0.3684 0.3760 0.3997 0.4041Ave 5.2 0.3690 0.0100 15.0 0.3887 2-Hexanone 0.1967 0.1691 0.2179 0.2040 0.1861Ave 10.0 0.1713 0.0100 15.0 0.1909 Dibromochloromethane 0.2331 0.2226 0.2523 0.2919 0.2973Ave 13.0 0.2925 0.0100 15.0 0.2649 1,2-Dibromoethane 0.2248 0.2056 0.2134 0.2321 0.2339Ave 4.9 0.2225 0.0100 15.0 0.2221 1-Chlorohexane 0.8497 0.7609 0.7473 0.7911 0.8333Ave 5.3 0.8334 0.0100 15.0 0.8026 Chlorobenzene 1.0890 0.9951 0.9764 1.0526 1.0888Ave 4.5 1.0565 0.3000 15.0 1.0431 1,1,1,2-Tetrachloroethane 0.3070 0.2956 0.3444 0.3789 0.3844Ave 11.0 0.3846 0.0100 15.0 0.3491 Ethylbenzene 0.6292 0.5655 0.5902 0.6273 0.6313Ave 4.3 0.6103 0.0100 15.0 0.6090 m&p-Xylene 1.5498 1.4828 1.5027 1.6944 1.7904Ave 8.5 1.7779 0.0100 15.0 1.6330 o-Xylene 1.5616 1.5031 1.5609 1.7253 1.7835Ave 7.8 1.8029 0.0100 15.0 1.6562 Styrene 1.2419 1.1547 1.2173 1.3556 1.4007Ave 8.0 1.3964 0.0100 15.0 1.2944 Bromoform 0.1622 0.1390 0.1781 0.2003 0.2160Qua1 0.9960 0.2050 0.0100 0.9900 -0.2550.18200.0002 Isopropylbenzene 3.7553 3.5476 3.2918 3.7357 3.7939Ave 5.9 3.8866 0.0100 15.0 3.6685



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/09/2013 Page 143 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06 Analy Batch No.:171819

10745 Calibration Start Date: Calibration End Date: 12/04/2012 14:34 Y 12/04/2012 16:55 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 Bromobenzene 0.8820 0.7936 0.7893 0.8417 0.8388Ave 4.1 0.8341 0.0100 15.0 0.8299 1,1,2,2-Tetrachloroethane 0.5749 0.4591 0.4791 0.5044 0.4888Ave 8.3 0.4744 0.3000 15.0 0.4968 1,2,3-Trichloropropane 0.1498 0.1293 0.1370 0.1391 0.1417Ave 5.2 0.1324 0.0100 15.0 0.1382 N-Propylbenzene 4.7265 4.3209 4.0651 4.6087 4.6711Ave 6.1 4.7658 0.0100 15.0 4.5263 2-Chlorotoluene 2.5905 2.3236 2.2523 2.5084 2.4920Ave 5.3 2.5043 0.0100 15.0 2.4452 1,3,5-Trimethylbenzene 3.2230 2.9483 2.8743 3.3095 3.3561Ave 7.2 3.4447 0.0100 15.0 3.1926 4-Chlorotoluene 3.1034 2.7648 2.7354 3.0804 3.1013Ave 6.5 3.1990 0.0100 15.0 2.9974 tert-Butylbenzene 2.8702 2.6245 2.4622 2.8128 2.7935Ave 5.9 2.8542 0.0100 15.0 2.7363 1,2,4-Trimethylbenzene 3.1779 3.0257 2.9078 3.3124 3.2583Ave 5.6 3.3651 0.0100 15.0 3.1745 sec-Butylbenzene 4.3996 4.0911 3.9512 4.5490 4.4865Ave 6.3 4.6389 0.0100 15.0 4.3527 1,3-Dichlorobenzene 1.8444 1.6756 1.6762 1.8109 1.7740Ave 3.9 1.7662 0.0100 15.0 1.7579 p-Isopropyltoluene 3.6992 3.5142 3.3950 3.8768 3.8296Ave 5.7 3.9249 0.0100 15.0 3.7066 1,4-Dichlorobenzene 1.8453 1.7033 1.6813 1.8389 1.7695Ave 3.8 1.7681 0.0100 15.0 1.7677 n-Butylbenzene 3.5999 3.3917 3.2752 3.7447 3.6977Ave 5.9 3.8176 0.0100 15.0 3.5878 1,2-Dichlorobenzene 1.6272 1.4494 1.4499 1.6195 1.5470Ave 5.1 1.5535 0.0100 15.0 1.5411 1,2-Dibromo-3-Chloropropane 0.0644 0.0544 0.0635 0.0646 0.0646Ave 6.4 0.0628 0.0100 15.0 0.0624 1,2,4-Trichlorobenzene 0.8738 0.7880 0.6482 0.6991 0.6626Ave 13.0 0.6310 0.0100 15.0 0.7171 Hexachlorobutadiene 0.7242 0.6321 0.5128 0.5239 0.5065Qua2 0.9970 0.4844 0.0100 0.9900 0.88180.5560 0 Naphthalene 1.1224 1.0162 0.8640 0.9349 0.9173Ave 11.0 0.8592 0.0100 15.0 0.9523 1,2,3-Trichlorobenzene 0.5335 0.5134 0.3651 0.3979 0.3833Qua1 0.9960 0.3563 0.0100 0.9900 0.79830.4092 0



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/09/2013 Page 144 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06 Analy Batch No.:171819

10745 Calibration Start Date: Calibration End Date: 12/04/2012 14:34 Y 12/04/2012 16:55 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 Dibromofluoromethane 0.4904 0.5628 0.5010 0.4930Ave 6.1 0.4930 0.0100 15.0 0.5081 1,2-Dichloroethane-d4 (Surr) 0.3874 0.4467 0.4112 0.3741Ave 8.1 0.3671 0.0100 15.0 0.3973 Toluene-d8 (Surr) 1.2729 1.4691 1.3972 1.3024Ave 5.9 1.3175 0.0100 15.0 1.3518 4-Bromofluorobenzene (Surr) 0.5575 0.6917 0.5810 0.5502Ave 10.0 0.5574 0.0100 15.0 0.5876



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/09/2013 Page 145 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06 Analy Batch No.:171819

10745 Calibration Start Date: Calibration End Date: 12/04/2012 14:34 Y 12/04/2012 16:55 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files: LEVEL: LAB SAMPLE ID: LAB FILE ID: Level1 STD1 500-171819/2 6I1204a.d Level2 STD2 500-171819/3 6I1204b.d Level3 STD3 500-171819/16 6I1204CC.d Level4 STD4 500-171819/5 6I1204d.d Level5 STD5 500-171819/6 6I1204e.d Level6 STD6 500-171819/7 6I1204f.d

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 6 Dichlorodifluoromethane Ave PFB 43859 164141 490706 1073926 1679708 2248613 5.00 20.0 50.0 100 150 200 Chloromethane Ave PFB 56677 220923 580439 1272796 1962205 2663554 5.00 20.0 50.0 100 150 200 Vinyl chloride Ave PFB 46653 183585 481633 1050014 1696104 2258770 5.00 20.0 50.0 100 150 200 Bromomethane Ave PFB 28282 107417 282609 595324 927883 1258628 5.00 20.0 50.0 100 150 200 Chloroethane Ave PFB 36835 142247 336325 760314 1173518 1541675 5.00 20.0 50.0 100 150 200 Dichlorofluoromethane Ave PFB 70972 289717 701331 1561621 2465148 3375221 5.00 20.0 50.0 100 150 200 Trichlorofluoromethane Ave PFB 66497 245578 602597 1353271 2150522 2845976 5.00 20.0 50.0 100 150 200 Acrolein Ave PFB 135143 569612 1253481 3165925 5578027 7777706 200 800 2000 4000 6000 8000 1,1-Dichloroethene Ave PFB 24678 101449 259314 609801 933026 1265158 5.00 20.0 50.0 100 150 200 1,1,2-Trichloro-1,2,2-trifluoroetha ne Ave PFB 34883 139553 354500 815530 1270129 1698517 5.00 20.0 50.0 100 150 200 Acetone Qua2 PFB 8488 26036 63428 159396 237040 302744 5.00 20.0 50.0 100 150 200 Carbon disulfide Ave PFB 89310 366998 1060244 2497933 3425047 4648445 5.00 20.0 50.0 100 150 200 Acetonitrile Qua2 PFB 28921 78586 160428 370513 610938 837530 40.0 160 400 800 1200 1600 Methylene Chloride Ave PFB 28603 102525 261307 561434 865406 1144172 5.00 20.0 50.0 100 150 200 Acrylonitrile Ave PFB 52548 224302 494214 1189147 2077128 2841154 40.0 160 400 800 1200 1600 trans-1,2-Dichloroethene Ave PFB 25567 112884 276266 647253 994785 1322919 5.00 20.0 50.0 100 150 200


### FORM VI 8260B 

## 01/09/2013 Page 146 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06 Analy Batch No.:171819

10745 Calibration Start Date: Calibration End Date: 12/04/2012 14:34 Y 12/04/2012 16:55 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 6 Methyl tert-butyl ether Ave PFB 52959 212291 550695 1292036 2020255 2677554 5.00 20.0 50.0 100 150 200 1,1-Dichloroethane Ave PFB 53766 234491 575476 1349737 2083045 2733212 5.00 20.0 50.0 100 150 200 Vinyl acetate Ave PFB 34285 148352 475662 999099 1719478 2109968 5.00 20.0 50.0 100 150 200 2,2-Dichloropropane Ave PFB 30324 131420 378910 857516 1317709 1790526 5.00 20.0 50.0 100 150 200 cis-1,2-Dichloroethene Ave PFB 27408 116876 275255 647076 1000867 1307173 5.00 20.0 50.0 100 150 200 2-Butanone (MEK) Ave PFB 6851 29888 86946 224026 335078 389110 5.00 20.0 50.0 100 150 200 Propionitrile Ave DFB 16200 69471 172732 411907 676543 912026 40.0 160 400 800 1200 1600 Bromochloromethane Ave PFB 11382 44936 111670 259302 397439 512811 5.00 20.0 50.0 100 150 200 Tetrahydrofuran Ave PFB 4143 19066 54053 118852 187613 232821 5.00 20.0 50.0 100 150 200 Chloroform Ave PFB 43364 176118 443833 1049184 1628033 2107213 5.00 20.0 50.0 100 150 200 1,1,1-Trichloroethane Ave PFB 38986 150190 424803 983576 1514014 2052266 5.00 20.0 50.0 100 150 200 Carbon tetrachloride Ave DFB 32398 127647 364091 875825 1385434 1859754 5.00 20.0 50.0 100 150 200 1,1-Dichloropropene Ave PFB 34609 145796 357712 864573 1339558 1723958 5.00 20.0 50.0 100 150 200 Benzene Ave DFB 95155 400069 977710 2359031 3597908 4656354 5.00 20.0 50.0 100 150 200 1,2-Dichloroethane Ave DFB 29859 123680 315359 780825 1199629 1528547 5.00 20.0 50.0 100 150 200 Trichloroethene Ave DFB 24265 107361 245590 613620 932877 1204163 5.00 20.0 50.0 100 150 200 1,2-Dichloropropane Ave DFB 25204 107370 261211 615728 957640 1234177 5.00 20.0 50.0 100 150 200 Dibromomethane Ave DFB 11382 47437 121081 274875 428159 547122 5.00 20.0 50.0 100 150 200 Bromodichloromethane Ave DFB 26117 105998 283529 698367 1075922 1375882 5.00 20.0 50.0 100 150 200 2-Chloroethyl vinyl ether Ave DFB 5843 24959 68276 143987 238709 290017 5.00 20.0 50.0 100 150 200 cis-1,3-Dichloropropene Ave DFB 26379 114470 291678 726654 1141580 1469116 5.00 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/09/2013 Page 147 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06 Analy Batch No.:171819

10745 Calibration Start Date: Calibration End Date: 12/04/2012 14:34 Y 12/04/2012 16:55 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 6 4-Methyl-2-pentanone (MIBK) Ave DFB 17991 65840 206982 492342 651507 834885 5.00 20.0 50.0 100 150 200 Toluene Ave DFB 55702 242332 588642 1472497 2296683 3044010 5.00 20.0 50.0 100 150 200 trans-1,3-Dichloropropene Ave DFB 20797 92184 257094 629495 984468 1265996 5.00 20.0 50.0 100 150 200 1,1,2-Trichloroethane Ave PFB 13050 57511 148789 353643 536069 677143 5.00 20.0 50.0 100 150 200 Tetrachloroethene Ave CBZ 28476 119937 285667 702154 1081677 1408855 5.00 20.0 50.0 100 150 200 1,3-Dichloropropane Ave CBZ 26131 102508 261720 613459 933524 1161967 5.00 20.0 50.0 100 150 200 2-Hexanone Ave CBZ 12375 47063 151685 313051 429948 539493 5.00 20.0 50.0 100 150 200 Dibromochloromethane Ave CBZ 14664 61941 175595 448008 686844 921214 5.00 20.0 50.0 100 150 200 1,2-Dibromoethane Ave DFB 13617 58743 151487 366417 562095 714479 5.00 20.0 50.0 100 150 200 1-Chlorohexane Ave PFB 36630 152507 373249 918779 1418488 1866410 5.00 20.0 50.0 100 150 200 Chlorobenzene Ave CBZ 68504 276932 679643 1615604 2515651 3327094 5.00 20.0 50.0 100 150 200 1,1,1,2-Tetrachloroethane Ave CBZ 19309 82263 239696 581547 888197 1211052 5.00 20.0 50.0 100 150 200 Ethylbenzene Ave CBZ 39579 157376 410826 962827 1458623 1921882 5.00 20.0 50.0 100 150 200 m&p-Xylene Ave CBZ 194973 825287 2091960 5201484 8273064 11198115 10.0 40.0 100 200 300 400 o-Xylene Ave CBZ 98229 418294 1086530 2648158 4120572 5677570 5.00 20.0 50.0 100 150 200 Styrene Ave CBZ 78124 321323 847341 2080656 3236183 4397468 5.00 20.0 50.0 100 150 200 Bromoform Qua1 CBZ 10201 38689 123975 307486 498988 645544 5.00 20.0 50.0 100 150 200 Isopropylbenzene Ave DCB 130272 564468 1442467 3562774 5519222 7619657 5.00 20.0 50.0 100 150 200 Bromobenzene Ave DCB 30596 126275 345893 802763 1220221 1635156 5.00 20.0 50.0 100 150 200 1,1,2,2-Tetrachloroethane Ave DCB 19943 73051 209957 481053 711087 929968 5.00 20.0 50.0 100 150 200 1,2,3-Trichloropropane Ave DCB 5196 20570 60012 132626 206208 259470 5.00 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/09/2013 Page 148 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06 Analy Batch No.:171819

10745 Calibration Start Date: Calibration End Date: 12/04/2012 14:34 Y 12/04/2012 16:55 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 6 N-Propylbenzene Ave DCB 163962 687506 1781317 4395269 6795398 9343196 5.00 20.0 50.0 100 150 200 2-Chlorotoluene Ave DCB 89865 369703 986962 2392295 3625274 4909602 5.00 20.0 50.0 100 150 200 1,3,5-Trimethylbenzene Ave DCB 111807 469109 1259499 3156272 4882363 6753218 5.00 20.0 50.0 100 150 200 4-Chlorotoluene Ave DCB 107656 439914 1198655 2937794 4511715 6271477 5.00 20.0 50.0 100 150 200 tert-Butylbenzene Ave DCB 99569 417592 1078942 2682568 4063919 5595665 5.00 20.0 50.0 100 150 200 1,2,4-Trimethylbenzene Ave DCB 110242 481424 1274220 3159004 4740128 6597181 5.00 20.0 50.0 100 150 200 sec-Butylbenzene Ave DCB 152623 650935 1731399 4338355 6526887 9094371 5.00 20.0 50.0 100 150 200 1,3-Dichlorobenzene Ave DCB 63983 266610 734521 1727058 2580768 3462604 5.00 20.0 50.0 100 150 200 p-Isopropyltoluene Ave DCB 128325 559155 1487680 3697265 5571191 7694725 5.00 20.0 50.0 100 150 200 1,4-Dichlorobenzene Ave DCB 64014 271014 736764 1753770 2574188 3466362 5.00 20.0 50.0 100 150 200 n-Butylbenzene Ave DCB 124880 539658 1435179 3571282 5379380 7484397 5.00 20.0 50.0 100 150 200 1,2-Dichlorobenzene Ave DCB 56446 230617 635338 1544477 2250579 3045582 5.00 20.0 50.0 100 150 200 1,2-Dibromo-3-Chloropropane Ave DCB 2234 8654 27809 61605 93914 123129 5.00 20.0 50.0 100 150 200 1,2,4-Trichlorobenzene Ave DCB 30313 125376 284038 666706 963905 1237013 5.00 20.0 50.0 100 150 200 Hexachlorobutadiene Qua2 DCB 25123 100580 224721 499659 736880 949639 5.00 20.0 50.0 100 150 200 Naphthalene Ave DCB 38935 161681 378609 891566 1334461 1684456 5.00 20.0 50.0 100 150 200 1,2,3-Trichlorobenzene Qua1 DCB 18507 81690 160002 379519 557639 698427 5.00 20.0 50.0 100 150 200 Dibromofluoromethane Ave PFB 98301 281110 581916 839156 1103934 20.0 50.0 100 150 200 1,2-Dichloroethane-d4 (Surr) Ave DFB 110679 317143 649071 898908 1178930 20.0 50.0 100 150 200 Toluene-d8 (Surr) Ave DFB 363660 1042887 2205424 3129848 4231595 20.0 50.0 100 150 200 4-Bromofluorobenzene (Surr) Ave CBZ 155143 481503 891809 1271160 1755381 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/09/2013 Page 149 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06 Analy Batch No.:171819

10745 Calibration Start Date: Calibration End Date: 12/04/2012 14:34 Y 12/04/2012 16:55 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

Curve Type Legend: Ave = Average ISTD Qua1 = Quadratic 1/conc ISTD Qua2 = Quadratic 1/conc^2 ISTD



### FORM VI 8260B 

## 01/09/2013 Page 150 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06 Analy Batch No.:171819

10746 Calibration Start Date: Calibration End Date: 12/04/2012 17:18 Y 12/04/2012 19:13 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

Calibration Files: LEVEL: LAB SAMPLE ID: LAB FILE ID: 1 Level STD1AP 500-171819/8 6J1204a.d 2 Level STD2AP 500-171819/9 6J1204b.d 3 Level STD3AP 500-171819/10 6J1204c.d 4 Level STD4AP 500-171819/11 6J1204d.d 5 Level STD5AP 500-171819/12 6J1204e.d 6 Level STD6AP 500-171819/13 6J1204f.d

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 Butadiene 1.1704 1.2279 1.0968 1.0951 1.2079Ave 4.9 1.1968 0.0100 15.0 1.1658 Ethyl ether 0.4055 0.4456 0.4198 0.4298 0.4343Ave 4.3 0.4585 0.0100 15.0 0.4323 Iodomethane 0.8397 0.9524 0.8632 0.8823 0.9390Ave 5.3 0.9416 0.0100 15.0 0.9030 3-Chloropropene 0.2619 0.2954 0.2794 0.2819 0.3038Ave 5.8 0.3056 0.0100 15.0 0.2880 Methyl acetate 0.3659 0.3821 0.3530 0.3743 0.3937Ave 4.9 0.4044 0.0100 15.0 0.3789 Hexane 1.0003 1.1165 1.0302 1.0554 1.1162Ave 4.7 1.1125 0.0100 15.0 1.0719 Isopropyl ether 2.2067 2.4360 2.2917 2.4215 2.6213Ave 7.4 2.6764 0.0100 15.0 2.4423 2-Chloro-1,3-butadiene 1.3107 1.4329 1.3162 1.3940 1.5159Ave 6.8 1.5380 0.0100 15.0 1.4179 Ethyl acetate 0.2404 0.2813 0.2686 0.3098 0.3063Ave 11.0 0.3315 0.0100 15.0 0.2896 Methacrylonitrile 0.1777 0.2152 0.2127 0.2335 0.2315Ave 11.0 0.2515 0.0100 15.0 0.2203 Cyclohexane 1.7178 1.6284 1.4552 1.4768 1.5751Ave 6.2 1.5846 0.0100 15.0 1.5730 Isobutyl alcohol 0.0083 0.0098 0.0098 0.0102 0.0114Ave 13.0 0.0121 0.0010 15.0 0.0103 2,2,4-Trimethylpentane 2.3074 2.4860 2.3789 2.4529 2.7064Ave 6.4 2.6728 0.0100 15.0 2.5007 Heptane 0.8426 0.8469 0.7982 0.8634 0.8905Ave 3.8 0.8766 0.0100 15.0 0.8530 n-Butyl alcohol 0.0048 0.0056 0.0058 0.0059 0.0064Ave 13.0 0.0071 0.0010 15.0 0.0059



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/09/2013 Page 151 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06 Analy Batch No.:171819

10746 Calibration Start Date: Calibration End Date: 12/04/2012 17:18 Y 12/04/2012 19:13 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 Methylcyclohexane 0.7683 0.7541 0.7187 0.7323 0.7887Ave 3.4 0.7633 0.0100 15.0 0.7542 Methyl methacrylate 0.1957 0.2053 0.2090 0.2411 0.2381Ave 9.1 0.2389 0.0100 15.0 0.2214 2-Nitropropane 0.0351 0.0557 0.0721 0.1027 0.1025Qua2 0.9930 +++++ 0.0100 0.9900 -10.850.0598 0 Ethyl methacrylate 0.2333 0.2512 0.2648 0.3057 0.3063Ave 12.0 0.3124 0.0100 15.0 0.2789 Cyclohexanone 0.0920 0.0927 0.0912 0.1071 0.1152Ave 9.8 0.0978 0.0100 15.0 0.0993 trans-1,4-Dichloro-2-butene 0.0533 0.0601 0.0614 0.0784 0.0825Qua2 0.9980 0.0877 0.0100 0.9900 -0.0550.05790.0001 Pentachloroethane 0.1724 0.2179 0.2343 0.2686 0.2970Qua1 1.0000 0.3217 0.0100 0.9900 -0.4630.21620.0003 1,3,5-Trichlorobenzene 1.0853 1.1609 1.1040 1.1775 1.1901Ave 4.3 1.2094 0.0100 15.0 1.1545 2-Methylnaphthalene 0.1748 0.2149 0.2505 0.1973 0.1786Ave 15.0 0.1792 0.0100 15.0 0.1992



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/09/2013 Page 152 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06 Analy Batch No.:171819

10746 Calibration Start Date: Calibration End Date: 12/04/2012 17:18 Y 12/04/2012 19:13 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files: LEVEL: LAB SAMPLE ID: LAB FILE ID: Level1 STD1AP 500-171819/8 6J1204a.d Level2 STD2AP 500-171819/9 6J1204b.d Level3 STD3AP 500-171819/10 6J1204c.d Level4 STD4AP 500-171819/11 6J1204d.d Level5 STD5AP 500-171819/12 6J1204e.d Level6 STD6AP 500-171819/13 6J1204f.d

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 6 Butadiene Ave PFB 59711 237793 571982 1316107 2109867 2854272 5.00 20.0 50.0 100 150 200 Ethyl ether Ave PFB 20688 86288 218958 516528 758551 1093569 5.00 20.0 50.0 100 150 200 Iodomethane Ave PFB 85680 368876 900336 2120722 3280480 4491113 10.0 40.0 100 200 300 400 3-Chloropropene Ave PFB 26728 114414 291463 677502 1061303 1457750 10.0 40.0 100 200 300 400 Methyl acetate Ave PFB 18668 73994 184121 449843 687679 964469 5.00 20.0 50.0 100 150 200 Hexane Ave PFB 51033 216226 537281 1268344 1949746 2653141 5.00 20.0 50.0 100 150 200 Isopropyl ether Ave PFB 112584 471760 1195143 2910208 4578669 6382856 5.00 20.0 50.0 100 150 200 2-Chloro-1,3-butadiene Ave PFB 66870 277486 686432 1675330 2647867 3667880 5.00 20.0 50.0 100 150 200 Ethyl acetate Ave PFB 122628 544727 1400541 3723072 5350060 7905489 50.0 200 500 1000 1500 2000 Methacrylonitrile Ave PFB 18131 83366 221818 561287 808714 1199565 10.0 40.0 100 200 300 400 Cyclohexane Ave PFB 87638 315360 758916 1774856 2751328 3779005 5.00 20.0 50.0 100 150 200 Isobutyl alcohol Ave DFB 47241 215613 569014 1358590 2205141 3307499 400 1600 4000 8000 12000 16000 2,2,4-Trimethylpentane Ave DFB 163991 685120 1728564 4079936 6520240 9114501 5.00 20.0 50.0 100 150 200 Heptane Ave DFB 59885 233399 579970 1436130 2145365 2989361 5.00 20.0 50.0 100 150 200 n-Butyl alcohol Ave DFB 27396 122976 334412 783861 1241059 1940445 400 1600 4000 8000 12000 16000 Methylcyclohexane Ave DFB 54604 207825 522199 1217989 1900254 2602848 5.00 20.0 50.0 100 150 200


### FORM VI 8260B 

## 01/09/2013 Page 153 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06 Analy Batch No.:171819

10746 Calibration Start Date: Calibration End Date: 12/04/2012 17:18 Y 12/04/2012 19:13 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 6 Methyl methacrylate Ave DFB 27819 113160 303724 802035 1147404 1629272 10.0 40.0 100 200 300 400 2-Nitropropane Qua2 CBZ 201751 1223343 4064819 13015638 18258126 +++++ 400 1600 4000 8000 12000 +++++ Ethyl methacrylate Ave CBZ 33510 137818 372926 968505 1363976 1949555 10.0 40.0 100 200 300 400 Cyclohexanone Ave DCB 291150 1128500 2979450 7326382 11645121 14112174 400 1600 4000 8000 12000 16000 trans-1,4-Dichloro-2-butene Qua2 DCB 4219 18285 50159 134107 208467 316432 10.0 40.0 100 200 300 400 Pentachloroethane Qua1 CBZ 24768 119564 330026 850927 1322444 2007968 10.0 40.0 100 200 300 400 1,3,5-Trichlorobenzene Ave DCB 42917 176629 450823 1006931 1503887 2180690 5.00 20.0 50.0 100 150 200 2-Methylnaphthalene Ave DCB 6911 32696 102284 168750 225710 323153 5.00 20.0 50.0 100 150 200 Curve Type Legend: Ave = Average ISTD Qua1 = Quadratic 1/conc ISTD Qua2 = Quadratic 1/conc^2 ISTD



### FORM VI 8260B 

## 01/09/2013 Page 154 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS18 Analy Batch No.:170445

10631 Calibration Start Date: Calibration End Date: 11/20/2012 15:57 N 11/20/2012 19:11 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

Calibration Files: LEVEL: LAB SAMPLE ID: LAB FILE ID: 1 Level STD1 500-170445/2 18I1120a.D 2 Level STD2 500-170445/3 18I1120b.D 3 Level STD3 500-170445/4 18I1120c.D 4 Level STD4 500-170445/5 18I1120d.D 5 Level STD5 500-170445/6 18I1120e.D 6 Level STD6 500-170445/7 18I1120f.D 7 Level STD7 500-170445/8 18I1120g.D 8 Level STD8 500-170445/9 18I1120h.D 9 Level STD9 500-170445/10 18I1120i.D

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Dichlorodifluoromethane 0.7338 0.6750 0.7042 0.6488Ave 6.8 0.7956 0.7810 0.7176 0.7221 0.0100 15.0 0.7223 Chloromethane 1.2860 1.1580 1.1717 1.1390Ave 5.4 1.3030 1.2866 1.1921 1.1898 0.1000 15.0 1.2158 Vinyl chloride 1.1427 1.0156 0.9540 0.9692 0.9488Ave 6.5 1.0791 1.0587 0.9766 0.9852 0.0100 15.0 1.0144 Bromomethane 0.3482 0.3298 0.3321 0.2943Ave 6.5 0.3516 0.3385 0.3092 0.3044 0.0100 15.0 0.3260 Chloroethane 0.5912 0.5020 0.5201 0.4820Ave 8.5 0.5808 0.5581 0.5185 0.4684 0.0100 15.0 0.5276 Dichlorofluoromethane 1.4329 1.2045 1.2387 1.2316Ave 6.4 1.3761 1.3461 1.2456 1.2517 0.0100 15.0 1.2909 Trichlorofluoromethane 0.9993 0.9030 0.9346 0.8909Ave 5.6 1.0344 1.0178 0.9348 0.9353 0.0100 15.0 0.9563 Acrolein 0.0719 0.0591 0.0800 0.0615Ave 9.6 0.0689 0.0685 0.0645 0.0665 0.0010 15.0 0.0676 1,1-Dichloroethene 0.5297 0.4450 0.4581 0.4790Ave 6.0 0.5196 0.5052 0.4753 0.4816 0.0100 15.0 0.4867 1,1,2-Trichloro-1,2,2-trifluoroethane 0.6606 0.5974 0.5413 0.5572Ave 6.9 0.6108 0.5938 0.5501 0.5574 0.0100 15.0 0.5836 Acetone 0.1029 0.0956Ave 7.3 0.0848 0.0903 0.0873 0.0882 0.0100 15.0 0.0915 Carbon disulfide 1.5830 1.4327 1.5370 1.5837Ave 9.4 1.8591 1.8605 1.7443 1.7493 0.0100 15.0 1.6687 Acetonitrile 0.0400 0.0356 0.0512 0.0362Ave 12.0 0.0424 0.0425 0.0390 0.0428 0.0010 15.0 0.0412



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/09/2013 Page 155 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS18 Analy Batch No.:170445

10631 Calibration Start Date: Calibration End Date: 11/20/2012 15:57 N 11/20/2012 19:11 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Methylene Chloride 0.5261 0.4806Ave 4.2 0.5308 0.5188 0.4882 0.4954 0.0100 15.0 0.5067 Acrylonitrile 0.1467 0.1176 0.1594 0.1248Ave 9.9 0.1349 0.1373 0.1269 0.1301 0.0010 15.0 0.1347 trans-1,2-Dichloroethene 0.5747 0.5119 0.5545 0.5254Ave 4.6 0.5816 0.5629 0.5334 0.5335 0.0100 15.0 0.5473 Methyl tert-butyl ether 0.8852 0.8766 0.9303 0.8415Ave 4.2 0.9549 0.9472 0.9009 0.9148 0.0100 15.0 0.9064 1,1-Dichloroethane 1.3378 1.2396 1.3158 1.2700Ave 3.7 1.3899 1.3714 1.3180 1.3226 0.1000 15.0 1.3206 Vinyl acetate 0.5108 0.4714 0.5364 0.5886Ave 13.0 0.6138 0.6506 0.6565 0.6805 0.0100 15.0 0.5886 2,2-Dichloropropane 0.6695 0.6433 0.6812 0.6374Ave 5.4 0.7445 0.7127 0.6703 0.6503 0.0100 15.0 0.6761 cis-1,2-Dichloroethene 0.5502 0.5439 0.5613 0.5408Ave 3.0 0.5868 0.5834 0.5602 0.5614 0.0100 15.0 0.5610 2-Butanone (MEK) 0.1124 0.1153Ave 2.6 0.1184 0.1197 0.1182 0.1206 0.0100 15.0 0.1174 Propionitrile 0.0313 0.0268 0.0378 0.0287Ave 11.0 0.0314 0.0310 0.0285 0.0306 0.0010 15.0 0.0308 Bromochloromethane 0.1934 0.1994 0.2158 0.1978Ave 3.8 0.2104 0.2119 0.2066 0.2093 0.0100 15.0 0.2056 Tetrahydrofuran 0.0851 0.0879 0.0770Ave 5.0 0.0835 0.0801 0.0770 0.0827 0.0100 15.0 0.0819 Chloroform 0.9654 0.8255 0.8994 0.8709Ave 5.1 0.9523 0.9477 0.9158 0.9228 0.0100 15.0 0.9125 1,1,1-Trichloroethane 0.8785 0.7529 0.8420 0.8062Ave 6.8 0.9396 0.9107 0.8721 0.8712 0.0100 15.0 0.8591 1,1-Dichloropropene 0.7821 0.6377 0.7218 0.7194Ave 6.5 0.7790 0.7731 0.7571 0.7629 0.0100 15.0 0.7416 Carbon tetrachloride 0.5107 0.4412 0.5096 0.4911Ave 8.7 0.5870 0.5667 0.5374 0.5344 0.0100 15.0 0.5223 Benzene 1.4886 1.5332 1.4063 1.4138 1.3805Ave 3.5 1.5010 1.4545 1.4161 1.4307 0.0100 15.0 1.4472 1,2-Dichloroethane 0.4761 0.4439 0.4731 0.4415Ave 2.9 0.4748 0.4618 0.4547 0.4579 0.0100 15.0 0.4605 Trichloroethene 0.3207 0.3414 0.3390 0.3794 0.3544Ave 5.4 0.3779 0.3672 0.3578 0.3577 0.0100 15.0 0.3551 1,2-Dichloropropane 0.4312 0.3991 0.4136 0.4077Ave 2.9 0.4329 0.4287 0.4205 0.4243 0.0100 15.0 0.4197



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/09/2013 Page 156 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS18 Analy Batch No.:170445

10631 Calibration Start Date: Calibration End Date: 11/20/2012 15:57 N 11/20/2012 19:11 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Dibromomethane 0.1386 0.1165 0.1443 0.1342Ave 6.4 0.1439 0.1372 0.1350 0.1370 0.0100 15.0 0.1358 Bromodichloromethane 0.3362 0.3129 0.3377 0.3404Ave 10.0 0.3975 0.4057 0.3976 0.4063 0.0100 15.0 0.3668 2-Chloroethyl vinyl ether 0.1224 0.1144 0.1157Ave 3.2 0.1238 0.1221 0.1197 0.1235 0.0100 15.0 0.1202 cis-1,3-Dichloropropene 0.3678 0.3467 0.3644 0.3844Ave 8.5 0.4186 0.4256 0.4262 0.4325 0.0100 15.0 0.3958 4-Methyl-2-pentanone (MIBK) 0.1829 0.1800Ave 3.4 0.1943 0.1966 0.1871 0.1900 0.0100 15.0 0.1885 Toluene 1.1580 0.9918 0.8547 0.8677 0.8335Ave 12.0 0.8854 0.8601 0.8535 0.8547 0.0100 15.0 0.9066 trans-1,3-Dichloropropene 0.3097 0.2793 0.3328 0.3074Ave 7.1 0.3433 0.3429 0.3351 0.3401 0.0100 15.0 0.3238 1,1,2-Trichloroethane 0.2534 0.2322 0.2524 0.2286Ave 4.3 0.2516 0.2512 0.2459 0.2576 0.0100 15.0 0.2466 Tetrachloroethene 0.4492 0.4398 0.4337 0.4385Ave 2.8 0.4617 0.4681 0.4558 0.4596 0.0100 15.0 0.4508 1,3-Dichloropropane 0.3858 0.3467 0.3557 0.3562Ave 3.4 0.3656 0.3727 0.3656 0.3739 0.0100 15.0 0.3653 2-Hexanone 0.1089 0.1175 0.1401 0.1364Ave 10.0 0.1471 0.1426 0.1365 0.1408 0.0100 15.0 0.1337 Dibromochloromethane 0.1900 0.1736 0.2021 0.2205Qua1 0.9990 0.2517 0.2684 0.2695 0.2761 0.0100 0.9900 -0.1060.24380.0002 1,2-Dibromoethane 0.1644 0.1549 0.1734 0.1590Ave 5.1 0.1804 0.1757 0.1681 0.1723 0.0100 15.0 0.1685 1-Chlorohexane 0.8953 0.7648 0.7777 0.6935Ave 9.7 0.7354 0.6989 0.6812 0.6863 0.0100 15.0 0.7416 Chlorobenzene 1.1696 1.0700 1.0714 1.0376Ave 3.6 1.1112 1.1051 1.0731 1.0863 0.3000 15.0 1.0905 1,1,1,2-Tetrachloroethane 0.3171 0.3068 0.3312 0.3619Ave 12.0 0.3996 0.4084 0.3959 0.4065 0.0100 15.0 0.3659 Ethylbenzene 0.5274 0.7232 0.6150 0.6311 0.6209Ave 8.1 0.6592 0.6578 0.6419 0.6474 0.0100 15.0 0.6360 m&p-Xylene 1.6363 1.7620 1.5234 1.6457 1.6034Ave 3.9 1.6868 1.6799 1.6536 1.6749 0.0100 15.0 1.6518 o-Xylene 1.8102 1.8258 1.6028 1.7142 1.6856Ave 4.0 1.7908 1.7872 1.7297 1.7570 0.0100 15.0 1.7448 Styrene 1.1746 1.1005 1.1331 1.1639Ave 5.4 1.2785 1.2554 1.2153 1.2608 0.0100 15.0 1.1978



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/09/2013 Page 157 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS18 Analy Batch No.:170445

10631 Calibration Start Date: Calibration End Date: 11/20/2012 15:57 N 11/20/2012 19:11 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Bromoform 0.1284 0.1085 0.1145 0.1248Qua1 0.9980 0.1534 0.1612 0.1520 0.1629 0.0100 0.9900 -0.0550.14460.0001 Isopropylbenzene 4.2314 3.7736 3.9887 3.9381Ave 3.8 4.1197 4.2012 4.1587 4.0117 0.0100 15.0 4.0529 1,1,2,2-Tetrachloroethane 0.4276 0.3620 0.4007 0.3818Ave 5.3 0.4104 0.4211 0.4073 0.4017 0.3000 15.0 0.4016 Bromobenzene 0.8931 0.7685 0.7991 0.7595Ave 5.3 0.8097 0.8250 0.7902 0.7728 0.0100 15.0 0.8022 1,2,3-Trichloropropane 0.3808 0.4432 0.3768 0.3278Ave 11.0 0.3415 0.3477 0.3343 0.3316 0.0100 15.0 0.3605 N-Propylbenzene 5.1681 4.7986 4.9942 4.7379Ave 3.1 4.9793 4.9463 4.8618 4.7157 0.0100 15.0 4.9002 2-Chlorotoluene 3.0539 2.7202 2.7737 2.6873Ave 4.2 2.8228 2.7997 2.7555 2.7030 0.0100 15.0 2.7895 1,3,5-Trimethylbenzene 3.6387 3.3372 3.4450 3.3941Ave 2.9 3.5063 3.5193 3.4302 3.3558 0.0100 15.0 3.4533 4-Chlorotoluene 3.5578 3.2742 3.2260 3.1288Ave 4.5 3.2775 3.2548 3.1464 3.0856 0.0100 15.0 3.2439 tert-Butylbenzene 3.2830 3.0181 3.0684 2.9870Ave 3.6 3.0707 3.1288 3.0264 2.9090 0.0100 15.0 3.0614 1,2,4-Trimethylbenzene 3.5921 3.3337 3.4708 3.3906Ave 3.0 3.5334 3.4591 3.3609 3.2995 0.0100 15.0 3.4300 sec-Butylbenzene 4.9350 4.5273 4.7174 4.5348Ave 3.7 4.6396 4.6676 4.4654 4.3972 0.0100 15.0 4.6105 1,3-Dichlorobenzene 1.9785 1.7239 1.6892 1.6864Ave 5.9 1.7675 1.7515 1.6801 1.6615 0.0100 15.0 1.7423 p-Isopropyltoluene 3.9642 3.7212 3.9739 3.8805Ave 3.3 3.9796 3.8852 3.7249 3.6715 0.0100 15.0 3.8501 1,4-Dichlorobenzene 1.9674 1.7052 1.6790 1.6718Ave 6.4 1.7246 1.7082 1.6358 1.6171 0.0100 15.0 1.7136 n-Butylbenzene 3.9856 3.3804 3.6510 3.6521Ave 5.6 3.8154 3.6445 3.4622 3.4262 0.0100 15.0 3.6272 1,2-Dichlorobenzene 1.4901 1.3671 1.4686 1.4289Ave 3.8 1.4898 1.4439 1.3702 1.3615 0.0100 15.0 1.4275 1,2-Dibromo-3-Chloropropane 0.0460 0.0507 0.0544Ave 5.4 0.0521 0.0536 0.0525 0.0532 0.0100 15.0 0.0518 1,2,4-Trichlorobenzene 0.8532 0.8127 0.8024 0.8009Ave 9.2 0.7959 0.7068 0.6649 0.6769 0.0100 15.0 0.7642 Hexachlorobutadiene 0.8562 0.7248 0.7313 0.7212Qua1 0.9980 0.6728 0.5630 0.5015 0.4887 0.0100 0.9900 0.17310.6915-0.001



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/09/2013 Page 158 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS18 Analy Batch No.:170445

10631 Calibration Start Date: Calibration End Date: 11/20/2012 15:57 N 11/20/2012 19:11 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Naphthalene 1.0176 0.8863 0.9288 0.9698Ave 5.0 0.9721 0.9267 0.8854 0.8994 0.0100 15.0 0.9358 1,2,3-Trichlorobenzene 0.5836 0.5407 0.5545 0.5610Ave 13.0 0.4837 0.4451 0.4210 0.4262 0.0100 15.0 0.5020 Dibromofluoromethane 0.4463Ave 0.7 0.4392 0.4398 0.4390 0.4388 0.0100 15.0 0.4406 1,2-Dichloroethane-d4 (Surr) 0.3358Ave 2.3 0.3221 0.3166 0.3185 0.3211 0.0100 15.0 0.3228 Toluene-d8 (Surr) 1.2359Ave 2.0 1.2155 1.1763 1.1979 1.1868 0.0100 15.0 1.2025 4-Bromofluorobenzene (Surr) 0.5753Ave 3.3 0.5469 0.5381 0.5310 0.5349 0.0100 15.0 0.5452



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/09/2013 Page 159 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS18 Analy Batch No.:170445

10631 Calibration Start Date: Calibration End Date: 11/20/2012 15:57 N 11/20/2012 19:11 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files: LEVEL: LAB SAMPLE ID: LAB FILE ID: Level1 STD1 500-170445/2 18I1120a.D Level2 STD2 500-170445/3 18I1120b.D Level3 STD3 500-170445/4 18I1120c.D Level4 STD4 500-170445/5 18I1120d.D Level5 STD5 500-170445/6 18I1120e.D Level6 STD6 500-170445/7 18I1120f.D Level7 STD7 500-170445/8 18I1120g.D Level8 STD8 500-170445/9 18I1120h.D Level9 STD9 500-170445/10 18I1120i.D

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Dichlorodifluoromethane Ave PFB 4428 8167 21374 77652 237482 453960 660813 863594 1.00 2.00 5.00 20.0 50.0 100 150 200 Chloromethane Ave PFB 7760 14011 35565 136324 388934 747832 1097875 1422948 1.00 2.00 5.00 20.0 50.0 100 150 200 Vinyl chloride Ave PFB 1647 6128 11543 29417 113560 322098 615375 899388 1178212 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromomethane Ave PFB 2101 3990 10080 35229 104945 196730 284749 364048 1.00 2.00 5.00 20.0 50.0 100 150 200 Chloroethane Ave PFB 3567 6074 15785 57691 173373 324430 477518 560155 1.00 2.00 5.00 20.0 50.0 100 150 200 Dichlorofluoromethane Ave PFB 8646 14573 37598 147409 410750 782459 1147085 1496932 1.00 2.00 5.00 20.0 50.0 100 150 200 Trichlorofluoromethane Ave PFB 6030 10925 28367 106635 308763 591581 860858 1118561 1.00 2.00 5.00 20.0 50.0 100 150 200 Acrolein Ave PFB 17342 28579 77741 294486 822987 1593549 2377631 3182501 40.0 80.0 160 800 2000 4000 6000 8000 1,1-Dichloroethene Ave PFB 3196 5384 13905 57336 155084 293661 437758 575993 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,2-Trichloro-1,2,2-trifluoroetha ne Ave PFB 3986 7228 16431 66697 182329 345170 506637 666624 1.00 2.00 5.00 20.0 50.0 100 150 200 Acetone Ave PFB 3122 11444 25305 52491 80381 105504 5.00 20.0 50.0 100 150 200 Carbon disulfide Ave PFB 9552 17334 46652 189561 554912 1081416 1606370 2092089 1.00 2.00 5.00 20.0 50.0 100 150 200 Acetonitrile Ave PFB 1929 3447 9954 34669 101259 197646 287117 409799 8.00 16.0 32.0 160 400 800 1200 1600 Methylene Chloride Ave PFB 15967 57524 158440 301578 449566 592532 5.00 20.0 50.0 100 150 200



### FORM VI 8260B 

## 01/09/2013 Page 160 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS18 Analy Batch No.:170445

10631 Calibration Start Date: Calibration End Date: 11/20/2012 15:57 N 11/20/2012 19:11 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Acrylonitrile Ave PFB 7080 11384 30965 119456 322243 638325 934627 1244356 8.00 16.0 32.0 160 400 800 1200 1600 trans-1,2-Dichloroethene Ave PFB 3468 6194 16831 62888 173615 327201 491180 638066 1.00 2.00 5.00 20.0 50.0 100 150 200 Methyl tert-butyl ether Ave PFB 5341 10606 28238 100722 285018 550550 829648 1094110 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1-Dichloroethane Ave PFB 8072 14998 39937 152015 414855 797118 1213789 1581777 1.00 2.00 5.00 20.0 50.0 100 150 200 Vinyl acetate Ave PFB 3082 5703 16282 70452 183216 378182 604588 813877 1.00 2.00 5.00 20.0 50.0 100 150 200 2,2-Dichloropropane Ave PFB 4040 7783 20675 76289 222237 414248 617252 777686 1.00 2.00 5.00 20.0 50.0 100 150 200 cis-1,2-Dichloroethene Ave PFB 3320 6581 17037 64724 175158 339128 515903 671364 1.00 2.00 5.00 20.0 50.0 100 150 200 2-Butanone (MEK) Ave PFB 3412 13802 35344 69602 108820 144223 5.00 20.0 50.0 100 150 200 Propionitrile Ave DFB 2135 3666 10388 39240 106076 210679 309144 433017 8.00 16.0 32.0 160 400 800 1200 1600 Bromochloromethane Ave PFB 1167 2413 6549 23678 62801 123161 190248 250350 1.00 2.00 5.00 20.0 50.0 100 150 200 Tetrahydrofuran Ave PFB 1030 2669 9218 24911 46566 70932 98870 2.00 5.00 20.0 50.0 100 150 200 Chloroform Ave PFB 5825 9988 27298 104239 284237 550852 843425 1103685 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,1-Trichloroethane Ave PFB 5301 9109 25556 96492 280448 529365 803103 1041932 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1-Dichloropropene Ave PFB 4719 7715 21907 86111 232530 449389 697190 912451 1.00 2.00 5.00 20.0 50.0 100 150 200 Carbon tetrachloride Ave DFB 4360 7543 21865 83989 248145 481322 728007 946559 1.00 2.00 5.00 20.0 50.0 100 150 200 Benzene Ave DFB 3017 13088 24041 60664 236113 634552 1235303 1918162 2534344 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dichloroethane Ave DFB 4064 7589 20299 75513 200744 392237 615935 811172 1.00 2.00 5.00 20.0 50.0 100 150 200 Trichloroethene Ave DFB 650 2914 5795 16279 60619 159741 311893 484646 633687 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dichloropropane Ave DFB 3681 6823 17748 69728 183000 364055 569576 751565 1.00 2.00 5.00 20.0 50.0 100 150 200 Dibromomethane Ave DFB 1183 1992 6192 22952 60829 116511 182922 242675 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromodichloromethane Ave DFB 2870 5349 14490 58227 168039 344530 538558 719678 1.00 2.00 5.00 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/09/2013 Page 161 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS18 Analy Batch No.:170445

10631 Calibration Start Date: Calibration End Date: 11/20/2012 15:57 N 11/20/2012 19:11 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 2-Chloroethyl vinyl ether Ave DFB 2092 4907 19794 52323 103721 162181 218791 2.00 5.00 20.0 50.0 100 150 200 cis-1,3-Dichloropropene Ave DFB 3140 5927 15638 65745 176977 361449 577374 766148 1.00 2.00 5.00 20.0 50.0 100 150 200 4-Methyl-2-pentanone (MIBK) Ave DFB 7847 30778 82132 166973 253451 336514 5.00 20.0 50.0 100 150 200 Toluene Ave DFB 2347 8467 14612 37231 142550 374325 730485 1156106 1514024 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 trans-1,3-Dichloropropene Ave DFB 2644 4775 14282 52572 145145 291191 453866 602491 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,2-Trichloroethane Ave PFB 1529 2809 7662 27366 75094 145995 226443 308046 1.00 2.00 5.00 20.0 50.0 100 150 200 Tetrachloroethene Ave CBZ 3428 6819 17026 64907 175016 340834 523590 688379 1.00 2.00 5.00 20.0 50.0 100 150 200 1,3-Dichloropropane Ave CBZ 2944 5376 13966 52729 138581 271339 420026 560106 1.00 2.00 5.00 20.0 50.0 100 150 200 2-Hexanone Ave CBZ 831 1821 5499 20191 55760 103797 156763 210949 1.00 2.00 5.00 20.0 50.0 100 150 200 Dibromochloromethane Qua1 CBZ 1450 2691 7934 32638 95420 195441 309596 413567 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dibromoethane Ave DFB 1403 2648 7441 27200 76258 149204 227695 305255 1.00 2.00 5.00 20.0 50.0 100 150 200 1-Chlorohexane Ave PFB 5402 9253 23606 83008 219512 406222 627330 820810 1.00 2.00 5.00 20.0 50.0 100 150 200 Chlorobenzene Ave CBZ 8925 16590 42064 153586 421256 804594 1232828 1627111 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,1,2-Tetrachloroethane Ave CBZ 2420 4756 13003 53568 151502 297319 454804 608869 1.00 2.00 5.00 20.0 50.0 100 150 200 Ethylbenzene Ave CBZ 1001 5518 9536 24778 91915 249878 478916 737488 969682 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 m&p-Xylene Ave CBZ 6212 26890 47238 129222 474697 1278862 2446178 3799344 5017706 0.500 2.00 4.00 10.0 40.0 100 200 300 400 o-Xylene Ave CBZ 3436 13932 24851 67298 249516 678885 1301206 1987127 2631883 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 Styrene Ave CBZ 8963 17063 44487 172291 484663 914023 1396155 1888531 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromoform Qua1 CBZ 980 1683 4496 18471 58151 117392 174647 243999 1.00 2.00 5.00 20.0 50.0 100 150 200 Isopropylbenzene Ave DCB 17989 31740 85220 327893 896099 1712979 2603073 3443871 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,2,2-Tetrachloroethane Ave DCB 1818 3045 8560 31787 89262 171689 254958 344835 1.00 2.00 5.00 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/09/2013 Page 162 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS18 Analy Batch No.:170445

10631 Calibration Start Date: Calibration End Date: 11/20/2012 15:57 N 11/20/2012 19:11 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Bromobenzene Ave DCB 3797 6464 17072 63237 176130 336370 494607 663460 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2,3-Trichloropropane Ave DCB 1619 3728 8051 27297 74292 141778 209279 284640 1.00 2.00 5.00 20.0 50.0 100 150 200 N-Propylbenzene Ave DCB 21971 40362 106702 394484 1083084 2016808 3043187 4048215 1.00 2.00 5.00 20.0 50.0 100 150 200 2-Chlorotoluene Ave DCB 12983 22880 59261 223750 613999 1141536 1724760 2320390 1.00 2.00 5.00 20.0 50.0 100 150 200 1,3,5-Trimethylbenzene Ave DCB 15469 28070 73602 282593 762675 1434967 2147102 2880791 1.00 2.00 5.00 20.0 50.0 100 150 200 4-Chlorotoluene Ave DCB 15125 27540 68924 260507 712921 1327120 1969455 2648838 1.00 2.00 5.00 20.0 50.0 100 150 200 tert-Butylbenzene Ave DCB 13957 25386 65556 248701 667934 1275738 1894346 2497268 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2,4-Trimethylbenzene Ave DCB 15271 28040 74154 282303 768572 1410421 2103731 2832505 1.00 2.00 5.00 20.0 50.0 100 150 200 sec-Butylbenzene Ave DCB 20980 38080 100788 377573 1009183 1903144 2795060 3774788 1.00 2.00 5.00 20.0 50.0 100 150 200 1,3-Dichlorobenzene Ave DCB 8411 14500 36090 140409 384456 714135 1051607 1426299 1.00 2.00 5.00 20.0 50.0 100 150 200 p-Isopropyltoluene Ave DCB 16853 31300 84902 323099 865624 1584145 2331542 3151868 1.00 2.00 5.00 20.0 50.0 100 150 200 1,4-Dichlorobenzene Ave DCB 8364 14343 35872 139195 375139 696479 1023879 1388234 1.00 2.00 5.00 20.0 50.0 100 150 200 n-Butylbenzene Ave DCB 16944 28433 78005 304075 829908 1485993 2167095 2941291 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dichlorobenzene Ave DCB 6335 11499 31377 118970 324054 588746 857673 1168761 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dibromo-3-Chloropropane Ave DCB 387 1083 4527 11328 21855 32865 45663 2.00 5.00 20.0 50.0 100 150 200 1,2,4-Trichlorobenzene Ave DCB 3627 6836 17143 66682 173111 288183 416167 581056 1.00 2.00 5.00 20.0 50.0 100 150 200 Hexachlorobutadiene Qua1 DCB 3640 6096 15625 60048 146348 229558 313901 419544 1.00 2.00 5.00 20.0 50.0 100 150 200 Naphthalene Ave DCB 4326 7455 19844 80746 211438 377865 554224 772065 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2,3-Trichlorobenzene Ave DCB 2481 4548 11846 46710 105208 181470 263513 365908 1.00 2.00 5.00 20.0 50.0 100 150 200 Dibromofluoromethane Ave PFB 53419 131105 255639 404291 524736 20.0 50.0 100 150 200 1,2-Dichloroethane-d4 (Surr) Ave DFB 57434 136159 268884 431384 568730 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/09/2013 Page 163 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS18 Analy Batch No.:170445

10631 Calibration Start Date: Calibration End Date: 11/20/2012 15:57 N 11/20/2012 19:11 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Toluene-d8 (Surr) Ave DFB 211373 513882 999001 1622664 2102290 20.0 50.0 100 150 200 4-Bromofluorobenzene (Surr) Ave CBZ 85160 207318 391774 609998 801248 20.0 50.0 100 150 200 Curve Type Legend: Ave = Average ISTD Qua1 = Quadratic 1/conc ISTD



### FORM VI 8260B 

## 01/09/2013 Page 164 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS22 Analy Batch No.:172615

10830 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

Calibration Files: LEVEL: LAB SAMPLE ID: LAB FILE ID: 1 Level STD01 500-172615/2 22I1211A.D 2 Level STD02 500-172615/3 22I1211B.D 3 Level STD03 500-172615/4 22I1211C.D 4 Level STD04 500-172615/5 22I1211D.D 5 Level STD05 500-172615/6 22I1211E.D 6 Level STD06 500-172615/7 22I1211F.D 7 Level STD07 500-172615/8 22I1211G.D 8 Level STD08 500-172615/9 22I1211H.D 9 Level STD09 500-172615/10 22I1211I.D

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Dichlorodifluoromethane 0.6445 0.5310 0.4776 0.4883Ave 9.9 0.5798 0.5632 0.5150 0.5364 0.0100 15.0 0.5420 Chloromethane 0.8256 0.7243 0.6267 0.6890Ave 7.9 0.7182 0.7230 0.6810 0.7012 0.1000 15.0 0.7111 Vinyl chloride 0.6665 0.7420 0.6103 0.5612 0.6130Ave 8.0 0.6517 0.6618 0.6041 0.6323 0.0100 15.0 0.6381 Bromomethane 0.1659 0.2203 0.1716 0.1726Ave 13.0 0.2077 0.2258 0.2110 0.2234 0.0100 15.0 0.1998 Chloroethane 0.4113 0.3289 0.3175 0.3315Ave 10.0 0.3369 0.3333 0.3044 0.3069 0.0100 15.0 0.3338 Dichlorofluoromethane 1.1276 1.0357 0.9343 1.0079Ave 6.3 0.9817 1.0066 0.9437 0.9571 0.0100 15.0 0.9993 Acetone +++++ +++++ 0.0554 0.0635Ave 7.8 0.0614 0.0672 0.0690 0.0671 0.0100 15.0 0.0639 Trichlorofluoromethane 0.9712 0.8348 0.7738 0.8319Ave 7.9 0.8320 0.8249 0.7635 0.7796 0.0100 15.0 0.8265 Acrolein 0.0331 0.0421 0.0314 0.0388Ave 13.0 0.0392 0.0429 0.0450 0.0450 0.0010 15.0 0.0397 1,1-Dichloroethene 0.4212 0.4280 0.3669 0.4008Ave 4.7 0.3938 0.3925 0.3935 0.4040 0.0100 15.0 0.4001 1,1,2-Trichloro-1,2,2-trifluoroethane 0.5610 0.4940 0.4511 0.4785Ave 6.7 0.4739 0.4784 0.4696 0.4829 0.0100 15.0 0.4862 Methylene Chloride +++++ 0.4011 0.3629 0.4004Ave 4.0 0.3719 0.3777 0.3682 0.3859 0.0100 15.0 0.3812 Carbon disulfide 1.5962 1.3713 1.3219 1.4559Ave 6.5 1.5313 1.5882 1.4767 1.4979 0.0100 15.0 1.4799



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/09/2013 Page 165 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS22 Analy Batch No.:172615

10830 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Acetonitrile 0.0371 0.0333 0.0243 0.0295Ave 13.0 0.0262 0.0281 0.0299 0.0295 0.0010 15.0 0.0297 Acrylonitrile 0.0750 0.0912 0.0677 0.0823Ave 9.0 0.0764 0.0821 0.0846 0.0849 0.0010 15.0 0.0805 trans-1,2-Dichloroethene 0.4780 0.4617 0.4088 0.4560Ave 4.4 0.4456 0.4511 0.4430 0.4552 0.0100 15.0 0.4499 2-Butanone (MEK) +++++ +++++ 0.0823 0.0919Ave 6.1 0.0908 0.0953 0.0973 0.0970 0.0100 15.0 0.0924 Methyl tert-butyl ether 0.7977 0.6853 0.6794 0.7577Ave 5.4 0.7230 0.7592 0.7369 0.7564 0.0100 15.0 0.7369 Vinyl acetate +++++ 0.6129 0.5650 0.6423Ave 5.2 0.6107 0.6494 0.6338 0.6642 0.0100 15.0 0.6255 Tetrahydrofuran +++++ +++++ 0.0538 0.0611Ave 4.2 0.0583 0.0572 0.0571 0.0595 0.0100 15.0 0.0578 1,1-Dichloroethane 0.9850 0.8255 0.8099 0.9189Ave 6.2 0.8749 0.8925 0.8704 0.9084 0.1000 15.0 0.8857 2,2-Dichloropropane 0.8126 0.7184 0.6702 0.7515Ave 5.5 0.7243 0.7285 0.7200 0.7474 0.0100 15.0 0.7341 cis-1,2-Dichloroethene 0.5106 0.4202 0.4186 0.4663Ave 6.4 0.4508 0.4630 0.4488 0.4652 0.0100 15.0 0.4554 Propionitrile 0.0230 0.0200 0.0163 0.0205Ave 10.0 0.0191 0.0201 0.0217 0.0219 0.0010 15.0 0.0203 Bromochloromethane 0.2191 0.1652 0.1606 0.1825Ave 10.0 0.1747 0.1747 0.1737 0.1772 0.0100 15.0 0.1785 Chloroform 0.7988 0.7465 0.6742 0.7604Ave 4.9 0.7195 0.7370 0.7200 0.7434 0.0100 15.0 0.7375 1,1,1-Trichloroethane 0.8087 0.7248 0.6839 0.7390Ave 4.7 0.7317 0.7368 0.7320 0.7583 0.0100 15.0 0.7394 Carbon tetrachloride 0.4978 0.4990 0.4486 0.4871Ave 3.4 0.4883 0.4750 0.4767 0.4948 0.0100 15.0 0.4834 1,1-Dichloropropene 0.7318 0.5960 0.5898 0.6649Ave 6.9 0.6479 0.6478 0.6435 0.6685 0.0100 15.0 0.6488 Benzene 1.2306 1.3508 1.2179 1.1306 1.2550Ave 4.7 1.2277 1.2183 1.1975 1.2355 0.0100 15.0 1.2293 1,2-Dichloroethane 0.3835 0.3413 0.3151 0.3618Ave 5.6 0.3558 0.3552 0.3521 0.3644 0.0100 15.0 0.3536 4-Methyl-2-pentanone (MIBK) +++++ +++++ 0.1384 0.1561Ave 5.1 0.1535 0.1552 0.1604 0.1580 0.0100 15.0 0.1536 2-Hexanone +++++ +++++ 0.1035 0.1187Ave 7.3 0.1220 0.1257 0.1256 0.1271 0.0100 15.0 0.1204



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/09/2013 Page 166 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS22 Analy Batch No.:172615

10830 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Trichloroethene 0.3583 0.3824 0.3356 0.3315 0.3516Ave 4.9 0.3434 0.3325 0.3291 0.3406 0.0100 15.0 0.3450 1,2-Dichloropropane 0.3550 0.3030 0.2849 0.3264Ave 6.4 0.3130 0.3110 0.3089 0.3197 0.0100 15.0 0.3152 Dibromomethane 0.1457 0.1306 0.1153 0.1288Ave 6.9 0.1238 0.1238 0.1224 0.1261 0.0100 15.0 0.1271 Bromodichloromethane 0.3875 0.3507 0.3319 0.3726Ave 4.6 0.3533 0.3599 0.3552 0.3686 0.0100 15.0 0.3600 2-Chloroethyl vinyl ether 0.1052 0.1095 0.1020 0.1096Ave 3.2 0.1015 0.1078 0.1021 0.1054 0.0100 15.0 0.1054 cis-1,3-Dichloropropene 0.4257 0.4102 0.3731 0.4222Ave 4.1 0.4033 0.4109 0.4067 0.4210 0.0100 15.0 0.4091 Toluene 0.9341 0.8388 0.7909 0.7458 0.8161Ave 6.2 0.8023 0.8060 0.7995 0.8258 0.0100 15.0 0.8177 trans-1,3-Dichloropropene 0.3943 0.3221 0.2903 0.3412Ave 8.6 0.3304 0.3383 0.3448 0.3521 0.0100 15.0 0.3392 1,1,2-Trichloroethane 0.2014 0.1786 0.1581 0.1681Ave 7.7 0.1638 0.1667 0.1692 0.1728 0.0100 15.0 0.1723 Tetrachloroethene 0.5511 0.4482 0.4255 0.4568Ave 9.0 0.4446 0.4384 0.4251 0.4400 0.0100 15.0 0.4537 1,3-Dichloropropane 0.3703 0.3719 0.3207 0.3542Ave 4.9 0.3407 0.3413 0.3399 0.3540 0.0100 15.0 0.3491 Dibromochloromethane 0.2702 0.2371 0.2274 0.2693Ave 6.9 0.2630 0.2690 0.2675 0.2786 0.0100 15.0 0.2603 1,2-Dibromoethane 0.2035 0.1624 0.1445 0.1607Ave 10.0 0.1572 0.1634 0.1626 0.1665 0.0100 15.0 0.1651 Chlorobenzene 1.1305 1.0221 0.9605 1.0363Ave 5.3 0.9949 0.9884 0.9670 0.9960 0.3000 15.0 1.0120 1-Chlorohexane 0.7176 0.7070 0.6491 0.6984Ave 3.1 0.6765 0.6760 0.6835 0.6837 0.0100 15.0 0.6865 1,1,1,2-Tetrachloroethane 0.3425 0.3396 0.3001 0.3448Ave 5.0 0.3425 0.3461 0.3458 0.3585 0.0100 15.0 0.3400 Ethylbenzene 0.5881 0.6023 0.5743 0.5326 0.5796Ave 3.4 0.5801 0.5769 0.5619 0.5822 0.0100 15.0 0.5753 m&p-Xylene 1.4425 1.5227 1.3904 1.3052 1.4876Ave 4.5 1.4534 1.4554 1.3960 1.3942 0.0100 15.0 1.4275 o-Xylene 1.4661 1.5830 1.3934 1.2932 1.4780Ave 5.5 1.4493 1.4706 1.4590 1.5151 0.0100 15.0 1.4564 Styrene 1.1505 1.0719 0.9871 1.1405Ave 5.6 1.1318 1.1478 1.1460 1.1845 0.0100 15.0 1.1200



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/09/2013 Page 167 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS22 Analy Batch No.:172615

10830 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Bromoform 0.1602 0.1366 0.1243 0.1553Ave 10.0 0.1546 0.1600 0.1660 0.1720 0.1000 15.0 0.1536 Isopropylbenzene 3.8233 3.3535 3.0653 3.4816Ave 7.4 3.1927 3.1639 3.1360 3.2790 0.0100 15.0 3.3119 Bromobenzene 0.8632 0.7552 0.6812 0.7730Ave 8.2 0.6922 0.7028 0.6972 0.7345 0.0100 15.0 0.7374 1,1,2,2-Tetrachloroethane 0.3977 0.4200 0.3757 0.4089Ave 6.0 0.3542 0.3640 0.3676 0.3874 0.3000 15.0 0.3844 1,2,3-Trichloropropane 0.2771 0.3098 0.2652 0.3046Ave 6.1 0.2704 0.2691 0.2728 0.2923 0.0100 15.0 0.2827 N-Propylbenzene 4.4856 4.0360 3.6439 4.1493Ave 6.5 3.8858 3.8875 3.7881 3.8936 0.0100 15.0 3.9712 4-Chlorotoluene 2.5653 2.2332 2.0176 2.3065Ave 7.0 2.1662 2.2029 2.1653 2.2760 0.0100 15.0 2.2416 1,3,5-Trimethylbenzene 3.0323 2.6976 2.4978 2.9026Ave 5.8 2.6929 2.7638 2.7107 2.8237 0.0100 15.0 2.7652 2-Chlorotoluene 3.0140 2.6145 2.4222 2.7174Ave 6.4 2.5627 2.6413 2.6089 2.7193 0.0100 15.0 2.6625 tert-Butylbenzene 2.9534 2.5783 2.3626 2.6552Ave 7.3 2.4553 2.4418 2.4420 2.5773 0.0100 15.0 2.5582 1,2,4-Trimethylbenzene 2.9651 2.7353 2.3710 2.7710Ave 6.3 2.6381 2.7234 2.6840 2.8189 0.0100 15.0 2.7134 sec-Butylbenzene 4.2594 3.7758 3.5493 3.9075Ave 5.8 3.6796 3.6591 3.6577 3.7738 0.0100 15.0 3.7828 1,3-Dichlorobenzene 1.8548 1.6516 1.4214 1.5907Ave 8.4 1.4814 1.5187 1.5128 1.5667 0.0100 15.0 1.5748 p-Isopropyltoluene 3.7168 3.3643 2.9943 3.3705Ave 6.4 3.1719 3.2121 3.1807 3.2836 0.0100 15.0 3.2868 1,4-Dichlorobenzene 1.7715 1.6564 1.4603 1.5651Ave 6.9 1.4798 1.5043 1.4758 1.5340 0.0100 15.0 1.5559 1,2-Dichlorobenzene 1.4806 1.3414 1.2093 1.4033Ave 6.4 1.2786 1.2876 1.2674 1.3183 0.0100 15.0 1.3233 n-Butylbenzene 3.1126 2.8700 2.6461 2.9480Ave 4.7 2.8772 2.9149 2.9548 3.0267 0.0100 15.0 2.9188 1,2-Dibromo-3-Chloropropane 0.0631 0.0851 0.0599 0.0678Ave 12.0 0.0613 0.0622 0.0635 0.0659 0.0100 15.0 0.0661 1,2,4-Trichlorobenzene 0.9867 0.8758 0.8191 0.8999Ave 5.3 0.8675 0.9149 0.9059 0.9063 0.0100 15.0 0.8970 Hexachlorobutadiene 0.9143 0.7960 0.7318 0.7351Ave 9.3 0.7318 0.6946 0.7407 0.7100 0.0100 15.0 0.7568



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/09/2013 Page 168 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS22 Analy Batch No.:172615

10830 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Naphthalene 1.0319 0.9651 0.8910 1.0003Ave 5.7 0.9350 0.9776 1.0179 1.0659 0.0100 15.0 0.9856 1,2,3-Trichlorobenzene 0.7942 0.6905 0.6629 0.7392Ave 5.4 0.6972 0.7092 0.7197 0.7238 0.0100 15.0 0.7171 Dibromofluoromethane 0.4088Ave 3.6 0.3747 0.4105 0.3974 0.4034 0.0100 15.0 0.3990 1,2-Dichloroethane-d4 (Surr) 0.2898Ave 2.8 0.2681 0.2786 0.2783 0.2818 0.0100 15.0 0.2793 Toluene-d8 (Surr) 1.2317Ave 3.0 1.1353 1.2008 1.1689 1.1817 0.0100 15.0 1.1837 4-Bromofluorobenzene (Surr) 0.5022Ave 2.5 0.4792 0.5117 0.5010 0.5085 0.0100 15.0 0.5005



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/09/2013 Page 169 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS22 Analy Batch No.:172615

10830 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files: LEVEL: LAB SAMPLE ID: LAB FILE ID: Level1 STD01 500-172615/2 22I1211A.D Level2 STD02 500-172615/3 22I1211B.D Level3 STD03 500-172615/4 22I1211C.D Level4 STD04 500-172615/5 22I1211D.D Level5 STD05 500-172615/6 22I1211E.D Level6 STD06 500-172615/7 22I1211F.D Level7 STD07 500-172615/8 22I1211G.D Level8 STD08 500-172615/9 22I1211H.D Level9 STD09 500-172615/10 22I1211I.D

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Dichlorodifluoromethane Ave PFB 8283 14019 34084 128973 408706 762307 1110898 1572519 1.00 2.00 5.00 20.0 50.0 100 150 200 Chloromethane Ave PFB 10611 19121 44725 181982 506217 978702 1468998 2055922 1.00 2.00 5.00 20.0 50.0 100 150 200 Vinyl chloride Ave PFB 2072 9537 16111 40052 161885 459341 895799 1302949 1853836 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromomethane Ave PFB 2132 5817 12250 45578 146376 305638 455210 654905 1.00 2.00 5.00 20.0 50.0 100 150 200 Chloroethane Ave PFB 5286 8684 22657 87550 237436 451232 656528 899737 1.00 2.00 5.00 20.0 50.0 100 150 200 Dichlorofluoromethane Ave PFB 14493 27342 66676 266205 691989 1362610 2035639 2806119 1.00 2.00 5.00 20.0 50.0 100 150 200 Acetone Ave PFB +++++ +++++ 3957 16764 43292 90934 148822 196769 +++++ +++++ 5.00 20.0 50.0 100 150 200 Trichlorofluoromethane Ave PFB 12483 22039 55227 219705 586466 1116585 1646914 2285626 1.00 2.00 5.00 20.0 50.0 100 150 200 Acrolein Ave PFB 16997 44508 89671 410157 1104663 2325112 3885554 5276134 40.0 80.0 200 800 2000 4000 6000 8000 1,1-Dichloroethene Ave PFB 5414 11300 26186 105858 277562 531364 848798 1184587 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,2-Trichloro-1,2,2-trifluoroetha ne Ave PFB 7210 13042 32193 126370 334028 647515 1013020 1415755 1.00 2.00 5.00 20.0 50.0 100 150 200 Methylene Chloride Ave PFB +++++ 10588 25901 105736 262156 511318 794285 1131397 +++++ 2.00 5.00 20.0 50.0 100 150 200 Carbon disulfide Ave PFB 20516 36202 94343 384523 1079379 2149891 3185269 4391617 1.00 2.00 5.00 20.0 50.0 100 150 200 Acetonitrile Ave PFB 3815 7023 13902 62328 147511 304606 515971 692080 8.00 16.0 40.0 160 400 800 1200 1600



### FORM VI 8260B 

## 01/09/2013 Page 170 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS22 Analy Batch No.:172615

10830 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Acrylonitrile Ave PFB 7715 19252 38635 173831 430688 889127 1460725 1990459 8.00 16.0 40.0 160 400 800 1200 1600 trans-1,2-Dichloroethene Ave PFB 6143 12190 29175 120435 314119 610637 955652 1334459 1.00 2.00 5.00 20.0 50.0 100 150 200 2-Butanone (MEK) Ave PFB +++++ +++++ 5877 24272 64002 128968 209900 284336 +++++ +++++ 5.00 20.0 50.0 100 150 200 Methyl tert-butyl ether Ave PFB 10253 18092 48485 200118 509651 1027632 1589481 2217547 1.00 2.00 5.00 20.0 50.0 100 150 200 Vinyl acetate Ave PFB +++++ 16181 40320 169641 430488 879019 1367143 1947324 +++++ 2.00 5.00 20.0 50.0 100 150 200 Tetrahydrofuran Ave PFB +++++ +++++ 3843 16127 41123 77379 123251 174315 +++++ +++++ 5.00 20.0 50.0 100 150 200 1,1-Dichloroethane Ave PFB 12660 21793 57801 242674 616675 1208102 1877461 2663163 1.00 2.00 5.00 20.0 50.0 100 150 200 2,2-Dichloropropane Ave PFB 10444 18966 47829 198464 510518 986077 1552961 2191135 1.00 2.00 5.00 20.0 50.0 100 150 200 cis-1,2-Dichloroethene Ave PFB 6562 11093 29875 123154 317732 626799 968176 1363967 1.00 2.00 5.00 20.0 50.0 100 150 200 Propionitrile Ave DFB 3274 5826 13049 61580 150541 311165 533857 726579 8.00 16.0 40.0 160 400 800 1200 1600 Bromochloromethane Ave PFB 2816 4362 11462 48207 123109 236461 374570 519660 1.00 2.00 5.00 20.0 50.0 100 150 200 Chloroform Ave PFB 10267 19708 48119 200834 507134 997634 1553050 2179601 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,1-Trichloroethane Ave PFB 10394 19135 48811 195166 515733 997347 1578989 2223267 1.00 2.00 5.00 20.0 50.0 100 150 200 Carbon tetrachloride Ave DFB 8845 18161 44839 182447 481514 918644 1463204 2051034 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1-Dichloropropene Ave PFB 9406 15734 42090 175593 456667 876844 1388026 1960009 1.00 2.00 5.00 20.0 50.0 100 150 200 Benzene Ave DFB 5292 24000 44324 113004 470128 1210657 2356179 3675431 5120985 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dichloroethane Ave DFB 6813 12420 31493 135519 350802 686980 1080708 1510261 1.00 2.00 5.00 20.0 50.0 100 150 200 4-Methyl-2-pentanone (MIBK) Ave DFB +++++ +++++ 13833 58466 151375 300182 492445 654734 +++++ +++++ 5.00 20.0 50.0 100 150 200 2-Hexanone Ave CBZ +++++ +++++ 8872 37503 101953 206593 337483 453433 +++++ +++++ 5.00 20.0 50.0 100 150 200 Trichloroethene Ave DFB 1541 6794 12213 33134 131705 338598 643029 1009984 1411923 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dichloropropane Ave DFB 6308 11028 28481 122258 308626 601403 948132 1325238 1.00 2.00 5.00 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/09/2013 Page 171 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS22 Analy Batch No.:172615

10830 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Dibromomethane Ave DFB 2589 4753 11529 48251 122106 239384 375807 522887 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromodichloromethane Ave DFB 6884 12765 33178 139566 348406 696059 1090230 1527793 1.00 2.00 5.00 20.0 50.0 100 150 200 2-Chloroethyl vinyl ether Ave DFB 1869 3984 10192 41067 100134 208398 313500 436785 1.00 2.00 5.00 20.0 50.0 100 150 200 cis-1,3-Dichloropropene Ave DFB 7564 14930 37294 158135 397656 794708 1248175 1745247 1.00 2.00 5.00 20.0 50.0 100 150 200 Toluene Ave DFB 4017 14904 28786 74548 305710 791155 1558816 2453857 3422834 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 trans-1,3-Dichloropropene Ave DFB 7005 11724 29021 127802 325796 654311 1058276 1459268 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,2-Trichloroethane Ave DFB 3579 6500 15804 62968 161526 322360 519398 716065 1.00 2.00 5.00 20.0 50.0 100 150 200 Tetrachloroethene Ave CBZ 8289 14024 36478 144290 371408 720453 1142505 1570157 1.00 2.00 5.00 20.0 50.0 100 150 200 1,3-Dichloropropane Ave CBZ 5569 11637 27497 111881 284612 560890 913572 1263367 1.00 2.00 5.00 20.0 50.0 100 150 200 Dibromochloromethane Ave CBZ 4064 7418 19500 85045 219735 442108 718959 994298 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dibromoethane Ave DFB 3616 5912 14445 60214 154974 316106 499079 690159 1.00 2.00 5.00 20.0 50.0 100 150 200 Chlorobenzene Ave CBZ 17003 31983 82345 327328 831189 1624419 2599260 3554021 1.00 2.00 5.00 20.0 50.0 100 150 200 1-Chlorohexane Ave PFB 9223 18665 46324 184447 476816 915102 1474279 2004578 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,1,2-Tetrachloroethane Ave CBZ 5151 10625 25733 108914 286131 568808 929412 1279270 1.00 2.00 5.00 20.0 50.0 100 150 200 Ethylbenzene Ave CBZ 2120 9059 17971 45661 183060 484613 948132 1510230 2077566 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 m&p-Xylene Ave CBZ 10400 45804 87017 223793 939704 2428374 4783893 7504852 9950024 0.500 2.00 4.00 10.0 40.0 100 200 300 400 o-Xylene Ave CBZ 5285 23810 43602 110873 466833 1210753 2416819 3921614 5406441 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 Styrene Ave CBZ 17304 33541 84628 360216 945512 1886331 3080454 4226631 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromoform Ave CBZ 2410 4275 10660 49043 129169 263003 446109 613724 1.00 2.00 5.00 20.0 50.0 100 150 200 Isopropylbenzene Ave DCB 31324 57244 148746 610310 1601454 3109566 5106365 6881199 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromobenzene Ave DCB 7072 12892 33053 135512 347188 690763 1135272 1541345 1.00 2.00 5.00 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/09/2013 Page 172 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS22 Analy Batch No.:172615

10830 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 1,1,2,2-Tetrachloroethane Ave DCB 3258 7169 18231 71670 177658 357760 598529 812983 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2,3-Trichloropropane Ave DCB 2270 5288 12868 53399 135614 264488 444171 613409 1.00 2.00 5.00 20.0 50.0 100 150 200 N-Propylbenzene Ave DCB 36750 68894 176823 727359 1949080 3820722 6168362 8171167 1.00 2.00 5.00 20.0 50.0 100 150 200 4-Chlorotoluene Ave DCB 21017 38120 97903 404326 1086544 2165096 3525867 4776401 1.00 2.00 5.00 20.0 50.0 100 150 200 1,3,5-Trimethylbenzene Ave DCB 24843 46048 121204 508814 1350744 2716376 4413867 5925708 1.00 2.00 5.00 20.0 50.0 100 150 200 2-Chlorotoluene Ave DCB 24693 44629 117536 476349 1285442 2595965 4248167 5706737 1.00 2.00 5.00 20.0 50.0 100 150 200 tert-Butylbenzene Ave DCB 24197 44012 114646 465442 1231564 2399839 3976419 5408653 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2,4-Trimethylbenzene Ave DCB 24293 46692 115053 485753 1323232 2676625 4370483 5915680 1.00 2.00 5.00 20.0 50.0 100 150 200 sec-Butylbenzene Ave DCB 34897 64452 172232 684971 1845685 3596271 5955880 7919600 1.00 2.00 5.00 20.0 50.0 100 150 200 1,3-Dichlorobenzene Ave DCB 15196 28192 68974 278836 743079 1492625 2463360 3287950 1.00 2.00 5.00 20.0 50.0 100 150 200 p-Isopropyltoluene Ave DCB 30451 57429 145300 590843 1590983 3156888 5179163 6891004 1.00 2.00 5.00 20.0 50.0 100 150 200 1,4-Dichlorobenzene Ave DCB 14514 28274 70862 274358 742273 1478508 2403110 3219268 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dichlorobenzene Ave DCB 12130 22897 58683 245994 641352 1265519 2063725 2766492 1.00 2.00 5.00 20.0 50.0 100 150 200 n-Butylbenzene Ave DCB 25501 48990 128404 516775 1443162 2864857 4811328 6351852 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dibromo-3-Chloropropane Ave DCB 517 1453 2909 11888 30736 61117 103368 138335 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2,4-Trichlorobenzene Ave DCB 8084 14950 39749 157753 435120 899145 1475044 1901927 1.00 2.00 5.00 20.0 50.0 100 150 200 Hexachlorobutadiene Ave DCB 7491 13587 35512 128859 367053 682660 1206171 1489923 1.00 2.00 5.00 20.0 50.0 100 150 200 Naphthalene Ave DCB 8454 16474 43237 175344 469003 960821 1657420 2236810 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2,3-Trichlorobenzene Ave DCB 6507 11786 32167 129572 349729 697002 1171916 1518870 1.00 2.00 5.00 20.0 50.0 100 150 200 Dibromofluoromethane Ave PFB 107966 264099 555702 857139 1182785 20.0 50.0 100 150 200 1,2-Dichloroethane-d4 (Surr) Ave DFB 108560 264333 538799 854290 1167924 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/09/2013 Page 173 of 384

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS22 Analy Batch No.:172615

10830 Calibration Start Date: Calibration End Date: 12/11/2012 14:23 N 12/11/2012 18:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Toluene-d8 (Surr) Ave DFB 461399 1119518 2322467 3587473 4898132 20.0 50.0 100 150 200 4-Bromofluorobenzene (Surr) Ave CBZ 158632 400320 840950 1346757 1814509 20.0 50.0 100 150 200 Curve Type Legend: Ave = Average ISTD



### FORM VI 8260B 

## 01/09/2013 Page 174 of 384

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53491-1

CMS06 12/04/2012 19:58 12/04/2012 14:34 12/04/2012 16:55 ICV 500-171819/15

DB624 TestAmerica Chicago

Lab File ID:6S1204.d Heated Purge: (Y/N) Y Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dichlorodifluoromethane 0.7088 0.9557 0.0100 37.1 50.0 -25.8* 25.0 Ave Chloromethane 0.9521 1.170 0.1000 40.7 50.0 -18.6 25.0 Ave Vinyl chloride 0.9329 0.9786 0.0100 47.7 50.0 -4.7 25.0 Ave Bromomethane 0.4976 0.5629 0.0100 44.2 50.0 -11.6 25.0 Ave Chloroethane 0.6528 0.7117 0.0100 45.9 50.0 -8.3 25.0 Ave Dichlorofluoromethane 1.305 1.466 0.0100 44.5 50.0 -11.0 25.0 Ave Trichlorofluoromethane 1.164 1.279 0.0100 45.5 50.0 -9.0 25.0 Ave Acrolein 0.0708 0.0748 0.0010 1893 2000 -5.4 25.0 Ave 1,1-Dichloroethene 0.5815 0.5393 0.0100 53.9 50.0 7.8 25.0 Ave 1,1,2-Trichloro-1,2,2-triflu oroethane 0.5548 0.7370 0.0100 37.6 50.0 -24.7 25.0 Ave Acetone 0.1428 0.0100 56.0 50.0 12.0 25.0 Qua2 Carbon disulfide 2.173 2.044 0.0100 53.2 50.0 6.3 25.0 Ave Acetonitrile 0.0432 0.0010 421 400 5.1 25.0 Qua2 Methylene Chloride 0.5791 0.5335 0.0100 54.3 50.0 8.6 25.0 Ave Acrylonitrile 0.1350 0.1425 0.0010 379 400 -5.3 25.0 Ave trans-1,2-Dichloroethene 0.6549 0.5736 0.0100 57.1 50.0 14.2 25.0 Ave Methyl tert-butyl ether 0.9692 1.148 0.0100 42.2 50.0 -15.5 25.0 Ave 1,1-Dichloroethane 1.323 1.196 0.1000 55.3 50.0 10.6 25.0 Ave Vinyl acetate 0.9732 0.8834 0.0100 55.1 50.0 10.2 25.0 Ave 2,2-Dichloropropane 0.8359 0.7383 0.0100 56.6 50.0 13.2 25.0 Ave cis-1,2-Dichloroethene 0.6322 0.5831 0.0100 54.2 50.0 8.4 25.0 Ave 2-Butanone (MEK) 0.1832 0.1743 0.0100 52.6 50.0 5.1 25.0 Ave Propionitrile 0.0339 0.0329 0.0010 412 400 2.9 25.0 Ave Bromochloromethane 0.1932 0.2329 0.0100 41.5 50.0 -17.1 25.0 Ave Tetrahydrofuran 0.1200 0.1027 0.0100 58.4 50.0 16.9 25.0 Ave Chloroform 1.049 0.9290 0.0100 56.5 50.0 12.9 25.0 Ave 1,1,1-Trichloroethane 0.9754 0.8595 0.0100 56.7 50.0 13.5 25.0 Ave Carbon tetrachloride 0.5942 0.5342 0.0100 55.6 50.0 11.2 25.0 Ave 1,1-Dichloropropene 0.8236 0.7579 0.0100 54.3 50.0 8.7 25.0 Ave Benzene 1.593 1.465 0.0100 54.4 50.0 8.7 25.0 Ave 1,2-Dichloroethane 0.5360 0.4733 0.0100 56.6 50.0 13.2 25.0 Ave Trichloroethene 0.4207 0.3790 0.0100 55.5 50.0 11.0 25.0 Ave 1,2-Dichloropropane 0.4324 0.3888 0.0100 55.6 50.0 11.2 25.0 Ave Dibromomethane 0.1893 0.1745 0.0100 54.2 50.0 8.4 25.0 Ave Bromodichloromethane 0.4564 0.4200 0.0100 54.3 50.0 8.7 25.0 Ave 2-Chloroethyl vinyl ether 0.1063 0.0935 0.0100 56.8 50.0 13.7 25.0 Ave cis-1,3-Dichloropropene 0.4949 0.4400 0.0100 60.5 53.8 12.5 25.0 Ave 4-Methyl-2-pentanone (MIBK) 0.2843 0.2770 0.0100 51.3 50.0 2.6 25.0 Ave Toluene 0.9867 0.9056 0.0100 54.5 50.0 9.0 25.0 Ave trans-1,3-Dichloropropene 0.4191 0.3718 0.0100 54.8 48.6 12.7 25.0 Ave



### FORM VII 8260B 

## 01/09/2013 Page 175 of 384

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53491-1

CMS06 12/04/2012 19:58 12/04/2012 14:34 12/04/2012 16:55 ICV 500-171819/15

DB624 TestAmerica Chicago

Lab File ID:6S1204.d Heated Purge: (Y/N) Y Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

1,1,2-Trichloroethane 0.3294 0.3016 0.0100 54.6 50.0 9.2 25.0 Ave Tetrachloroethene 0.5067 0.4445 0.0100 57.0 50.0 14.0 25.0 Ave 1,3-Dichloropropane 0.4493 0.3887 0.0100 57.8 50.0 15.6 25.0 Ave 2-Hexanone 0.1976 0.1909 0.0100 51.8 50.0 3.5 25.0 Ave Dibromochloromethane 0.2994 0.2649 0.0100 56.5 50.0 13.0 25.0 Ave 1,2-Dibromoethane 0.2452 0.2221 0.0100 55.2 50.0 10.4 25.0 Ave 1-Chlorohexane 0.6673 0.8026 0.0100 41.6 50.0 -16.9 25.0 Ave Chlorobenzene 1.075 1.043 0.3000 51.5 50.0 3.1 25.0 Ave 1,1,1,2-Tetrachloroethane 0.3958 0.3491 0.0100 56.7 50.0 13.4 25.0 Ave Ethylbenzene 0.6804 0.6090 0.0100 55.9 50.0 11.7 25.0 Ave m&p-Xylene 1.717 1.633 0.0100 105 100 5.1 25.0 Ave o-Xylene 1.707 1.656 0.0100 51.5 50.0 3.1 25.0 Ave Styrene 1.386 1.294 0.0100 53.5 50.0 7.1 25.0 Ave Bromoform 0.2127 0.1000 57.0 50.0 14.0 25.0 Qua1 Isopropylbenzene 3.656 3.668 0.0100 49.8 50.0 -0.3 25.0 Ave Bromobenzene 0.9264 0.8299 0.0100 55.8 50.0 11.6 25.0 Ave 1,1,2,2-Tetrachloroethane 0.5641 0.4968 0.3000 56.8 50.0 13.5 25.0 Ave 1,2,3-Trichloropropane 0.1571 0.1382 0.0100 56.8 50.0 13.6 25.0 Ave N-Propylbenzene 4.386 4.526 0.0100 48.5 50.0 -3.1 25.0 Ave 2-Chlorotoluene 2.505 2.445 0.0100 51.2 50.0 2.5 25.0 Ave 1,3,5-Trimethylbenzene 3.418 3.193 0.0100 53.5 50.0 7.1 25.0 Ave 4-Chlorotoluene 2.955 2.997 0.0100 49.3 50.0 -1.4 25.0 Ave tert-Butylbenzene 2.718 2.736 0.0100 49.7 50.0 -0.7 25.0 Ave 1,2,4-Trimethylbenzene 3.411 3.175 0.0100 53.7 50.0 7.5 25.0 Ave sec-Butylbenzene 4.275 4.353 0.0100 49.1 50.0 -1.8 25.0 Ave 1,3-Dichlorobenzene 1.741 1.758 0.0100 49.5 50.0 -1.0 25.0 Ave p-Isopropyltoluene 3.622 3.707 0.0100 48.9 50.0 -2.3 25.0 Ave 1,4-Dichlorobenzene 1.922 1.768 0.0100 54.4 50.0 8.7 25.0 Ave n-Butylbenzene 3.662 3.588 0.0100 51.0 50.0 2.1 25.0 Ave 1,2-Dichlorobenzene 1.561 1.541 0.0100 50.7 50.0 1.3 25.0 Ave 1,2-Dibromo-3-Chloropropane 0.0666 0.0624 0.0100 53.4 50.0 6.7 25.0 Ave 1,2,4-Trichlorobenzene 0.6739 0.7171 0.0100 47.0 50.0 -6.0 25.0 Ave Hexachlorobutadiene 0.5712 0.0100 51.7 50.0 3.4 25.0 Qua2 Naphthalene 0.9576 0.9523 0.0100 50.3 50.0 0.6 25.0 Ave 1,2,3-Trichlorobenzene 0.4184 0.0100 50.8 50.0 1.7 25.0 Qua1 Dibromofluoromethane 0.4517 0.5081 0.0100 42.8 48.1 -11.1 25.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.3281 0.3973 0.0100 39.7 48.1 -17.4 25.0 Ave Toluene-d8 (Surr) 1.217 1.352 0.0100 43.3 48.1 -9.9 25.0 Ave 4-Bromofluorobenzene (Surr) 0.5156 0.5876 0.0100 42.2 48.1 -12.2 25.0 Ave



### FORM VII 8260B 

## 01/09/2013 Page 176 of 384

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53491-1

CMS06 12/04/2012 19:58 12/04/2012 17:18 12/04/2012 19:13 ICV 500-171819/15

DB624 TestAmerica Chicago

Lab File ID:6S1204.d Heated Purge: (Y/N) Y Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF
Ethyl ether 0.3545 0.4323 0.0100 41.0 50.0 -18.0 25.0 Ave Iodomethane 1.082 0.9030 0.0100 59.9 50.0 19.9 25.0 Ave Methyl acetate 0.2226 0.3789 0.0100 29.4 50.0 -41.3* 25.0 Ave Hexane 0.8633 1.072 0.0100 40.3 50.0 -19.5 25.0 Ave Cyclohexane 1.158 1.573 0.0100 36.8 50.0 -26.4* 25.0 Ave Heptane 0.6678 0.8530 0.0100 39.1 50.0 -21.7 25.0 Ave Methylcyclohexane 0.5785 0.7542 0.0100 38.4 50.0 -23.3 25.0 Ave 1,3,5-Trichlorobenzene 1.177 1.155 0.0100 51.0 50.0 1.9 25.0 Ave



### FORM VII 8260B 

## 01/09/2013 Page 177 of 384

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53491-1

CMS06 12/27/2012 09:47 12/04/2012 14:34 12/04/2012 16:55 CCV 500-173973/3

DB624 TestAmerica Chicago

Lab File ID:6C1227.d Heated Purge: (Y/N) Y Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dichlorodifluoromethane 0.9217 0.9557 0.0100 48.2 50.0 -3.6 50.0 Ave Chloromethane 1.105 1.170 0.1000 47.2 50.0 -5.5 50.0 Ave Vinyl chloride 0.9107 0.9786 0.0100 46.5 50.0 -6.9 20.0 Ave Bromomethane 0.5445 0.5629 0.0100 48.4 50.0 -3.3 50.0 Ave Chloroethane 0.6484 0.7117 0.0100 45.6 50.0 -8.9 50.0 Ave Dichlorofluoromethane 1.377 1.466 0.0100 47.0 50.0 -6.1 50.0 Ave Trichlorofluoromethane 1.234 1.279 0.0100 48.2 50.0 -3.5 50.0 Ave Acrolein 0.0852 0.0748 0.0010 2277 2000 13.9 50.0 Ave 1,1-Dichloroethene 0.5025 0.5393 0.0100 46.6 50.0 -6.8 20.0 Ave 1,1,2-Trichloro-1,2,2-triflu oroethane 0.6729 0.7370 0.0100 45.7 50.0 -8.7 50.0 Ave Acetone 0.1327 0.0100 52.1 50.0 4.1 50.0 Qua2 Carbon disulfide 1.993 2.044 0.0100 48.8 50.0 -2.5 50.0 Ave Acetonitrile 0.0473 0.0010 462 400 15.4 50.0 Qua2 Methylene Chloride 0.4644 0.5335 0.0100 43.5 50.0 -12.9 50.0 Ave Acrylonitrile 0.1483 0.1425 0.0010 416 400 4.0 50.0 Ave trans-1,2-Dichloroethene 0.5319 0.5736 0.0100 46.4 50.0 -7.3 50.0 Ave Methyl tert-butyl ether 1.048 1.148 0.0100 45.7 50.0 -8.7 50.0 Ave 1,1-Dichloroethane 1.113 1.196 0.1000 46.5 50.0 -7.0 50.0 Ave Vinyl acetate 0.6583 0.8834 0.0100 37.3 50.0 -25.5 50.0 Ave 2,2-Dichloropropane 0.7724 0.7383 0.0100 52.3 50.0 4.6 50.0 Ave cis-1,2-Dichloroethene 0.5366 0.5831 0.0100 46.0 50.0 -8.0 50.0 Ave 2-Butanone (MEK) 0.1575 0.1743 0.0100 45.2 50.0 -9.6 50.0 Ave Propionitrile 0.0348 0.0329 0.0010 423 400 5.7 50.0 Ave Bromochloromethane 0.2109 0.2329 0.0100 45.3 50.0 -9.4 50.0 Ave Tetrahydrofuran 0.0894 0.1027 0.0100 43.5 50.0 -12.9 50.0 Ave Chloroform 0.8524 0.9290 0.0100 45.9 50.0 -8.2 20.0 Ave 1,1,1-Trichloroethane 0.8614 0.8595 0.0100 50.1 50.0 0.2 50.0 Ave Carbon tetrachloride 0.5491 0.5342 0.0100 51.4 50.0 2.8 50.0 Ave 1,1-Dichloropropene 0.6809 0.7579 0.0100 44.9 50.0 -10.2 50.0 Ave Benzene 1.312 1.465 0.0100 44.8 50.0 -10.4 50.0 Ave 1,2-Dichloroethane 0.4379 0.4733 0.0100 46.3 50.0 -7.5 50.0 Ave Trichloroethene 0.3500 0.3790 0.0100 46.2 50.0 -7.7 50.0 Ave 1,2-Dichloropropane 0.3546 0.3888 0.0100 45.6 50.0 -8.8 20.0 Ave Dibromomethane 0.1563 0.1745 0.0100 44.8 50.0 -10.5 50.0 Ave Bromodichloromethane 0.3992 0.4200 0.0100 47.5 50.0 -5.0 50.0 Ave 2-Chloroethyl vinyl ether 0.0427 0.0935 0.0100 22.8 50.0 -54.3* 50.0 Ave cis-1,3-Dichloropropene 0.4072 0.4400 0.0100 46.3 50.0 -7.4 50.0 Ave 4-Methyl-2-pentanone (MIBK) 0.2777 0.2770 0.0100 50.1 50.0 0.3 50.0 Ave Toluene 0.8480 0.9056 0.0100 46.8 50.0 -6.4 20.0 Ave trans-1,3-Dichloropropene 0.3638 0.3718 0.0100 48.9 50.0 -2.1 50.0 Ave



### FORM VII 8260B 

## 01/09/2013 Page 178 of 384

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53491-1

CMS06 12/27/2012 09:47 12/04/2012 14:34 12/04/2012 16:55 CCV 500-173973/3

DB624 TestAmerica Chicago

Lab File ID:6C1227.d Heated Purge: (Y/N) Y Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

1,1,2-Trichloroethane 0.2821 0.3016 0.0100 46.8 50.0 -6.4 50.0 Ave Tetrachloroethene 0.4238 0.4445 0.0100 47.7 50.0 -4.7 50.0 Ave 1,3-Dichloropropane 0.3550 0.3887 0.0100 45.7 50.0 -8.7 50.0 Ave 2-Hexanone 0.1883 0.1909 0.0100 49.3 50.0 -1.3 50.0 Ave Dibromochloromethane 0.2640 0.2649 0.0100 49.8 50.0 -0.4 50.0 Ave 1,2-Dibromoethane 0.2196 0.2221 0.0100 49.5 50.0 -1.1 50.0 Ave 1-Chlorohexane 0.7800 0.8026 0.0100 48.6 50.0 -2.8 50.0 Ave Chlorobenzene 0.9717 1.043 0.3000 46.6 50.0 -6.8 50.0 Ave 1,1,1,2-Tetrachloroethane 0.3463 0.3491 0.0100 49.6 50.0 -0.8 50.0 Ave Ethylbenzene 0.5747 0.6090 0.0100 47.2 50.0 -5.6 20.0 Ave m&p-Xylene 1.484 1.633 0.0100 90.9 100 -9.1 50.0 Ave o-Xylene 1.529 1.656 0.0100 46.2 50.0 -7.7 50.0 Ave Styrene 1.171 1.294 0.0100 45.2 50.0 -9.6 50.0 Ave Bromoform 0.1911 0.1000 51.6 50.0 3.2 50.0 Qua1 Isopropylbenzene 3.401 3.668 0.0100 46.4 50.0 -7.3 50.0 Ave Bromobenzene 0.8184 0.8299 0.0100 49.3 50.0 -1.4 50.0 Ave 1,1,2,2-Tetrachloroethane 0.4482 0.4968 0.3000 45.1 50.0 -9.8 50.0 Ave 1,2,3-Trichloropropane 0.1338 0.1382 0.0100 48.4 50.0 -3.2 50.0 Ave N-Propylbenzene 4.159 4.526 0.0100 45.9 50.0 -8.1 50.0 Ave 2-Chlorotoluene 2.308 2.445 0.0100 47.2 50.0 -5.6 50.0 Ave 1,3,5-Trimethylbenzene 2.938 3.193 0.0100 46.0 50.0 -8.0 50.0 Ave 4-Chlorotoluene 2.723 2.997 0.0100 45.4 50.0 -9.2 50.0 Ave tert-Butylbenzene 2.535 2.736 0.0100 46.3 50.0 -7.4 50.0 Ave 1,2,4-Trimethylbenzene 2.927 3.175 0.0100 46.1 50.0 -7.8 50.0 Ave sec-Butylbenzene 3.937 4.353 0.0100 45.2 50.0 -9.5 50.0 Ave 1,3-Dichlorobenzene 1.679 1.758 0.0100 47.8 50.0 -4.5 50.0 Ave p-Isopropyltoluene 3.406 3.707 0.0100 45.9 50.0 -8.1 50.0 Ave 1,4-Dichlorobenzene 1.638 1.768 0.0100 46.3 50.0 -7.4 50.0 Ave n-Butylbenzene 3.174 3.588 0.0100 44.2 50.0 -11.5 50.0 Ave 1,2-Dichlorobenzene 1.436 1.541 0.0100 46.6 50.0 -6.8 50.0 Ave 1,2-Dibromo-3-Chloropropane 0.0615 0.0624 0.0100 49.3 50.0 -1.3 50.0 Ave 1,2,4-Trichlorobenzene 0.6962 0.7171 0.0100 48.5 50.0 -2.9 50.0 Ave Hexachlorobutadiene 0.5845 0.0100 53.0 50.0 6.0 50.0 Qua2 Naphthalene 0.8314 0.9523 0.0100 43.7 50.0 -12.7 50.0 Ave 1,2,3-Trichlorobenzene 0.4063 0.0100 49.3 50.0 -1.5 50.0 Qua1 Dibromofluoromethane 0.4959 0.5081 0.0100 47.0 48.1 -2.4 50.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.3731 0.3973 0.0100 45.2 48.1 -6.1 50.0 Ave Toluene-d8 (Surr) 1.326 1.352 0.0100 47.2 48.1 -1.9 50.0 Ave 4-Bromofluorobenzene (Surr) 0.5361 0.5876 0.0100 43.9 48.1 -8.8 50.0 Ave



### FORM VII 8260B 

## 01/09/2013 Page 179 of 384

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53491-1

CMS06 12/27/2012 10:10 12/04/2012 14:34 12/04/2012 16:55 CCV 500-173973/4

DB624 TestAmerica Chicago

Lab File ID:6D1227.d Heated Purge: (Y/N) Y Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dibromofluoromethane 0.4622 0.5081 0.0100 43.8 48.1 -9.0 50.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.3622 0.3973 0.0100 43.9 48.1 -8.8 50.0 Ave Toluene-d8 (Surr) 1.311 1.352 0.0100 46.7 48.1 -3.0 50.0 Ave 4-Bromofluorobenzene (Surr) 0.5369 0.5876 0.0100 44.0 48.1 -8.6 50.0 Ave



### FORM VII 8260B 

## 01/09/2013 Page 180 of 384

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53491-1

CMS06 12/27/2012 10:10 12/04/2012 17:18 12/04/2012 19:13 CCV 500-173973/4

DB624 TestAmerica Chicago

Lab File ID:6D1227.d Heated Purge: (Y/N) Y Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Butadiene 1.154 1.166 0.0100 49.5 50.0 -1.0 50.0 Ave Ethyl ether 0.4291 0.4323 0.0100 49.6 50.0 -0.7 50.0 Ave Iodomethane 0.6401 0.9030 0.0100 70.9 100 -29.1 50.0 Ave 3-Chloropropene 0.1957 0.2880 0.0100 68.0 100 -32.1 50.0 Ave Methyl acetate 0.3330 0.3789 0.0100 44.0 50.0 -12.1 50.0 Ave Hexane 1.103 1.072 0.0100 51.5 50.0 2.9 50.0 Ave Isopropyl ether 2.542 2.442 0.0100 52.0 50.0 4.1 50.0 Ave 2-Chloro-1,3-butadiene 1.462 1.418 0.0100 51.6 50.0 3.1 50.0 Ave Ethyl acetate 0.2117 0.2896 0.0100 365 500 -26.9 50.0 Ave Methacrylonitrile 0.1749 0.2203 0.0100 79.4 100 -20.6 50.0 Ave Cyclohexane 1.660 1.573 0.0100 52.8 50.0 5.5 50.0 Ave Isobutyl alcohol 0.0084 0.0103 0.0010 3280 4000 -18.0 50.0 Ave 2,2,4-Trimethylpentane 2.774 2.501 0.0100 55.5 50.0 10.9 50.0 Ave Heptane 0.8919 0.8530 0.0100 52.3 50.0 4.6 50.0 Ave n-Butyl alcohol 0.0048 0.0059 0.0010 3261 4000 -18.5 50.0 Ave Methylcyclohexane 0.8231 0.7542 0.0100 54.6 50.0 9.1 50.0 Ave Methyl methacrylate 0.1785 0.2214 0.0100 80.7 100 -19.4 50.0 Ave 2-Nitropropane 0.0699 0.0100 3836 4000 -4.1 50.0 Qua2 Ethyl methacrylate 0.2385 0.2789 0.0100 85.5 100 -14.5 50.0 Ave Cyclohexanone 0.0811 0.0993 0.0100 3265 4000 -18.4 50.0 Ave trans-1,4-Dichloro-2-butene 0.0564 0.0100 87.7 100 -12.3 50.0 Qua2 Pentachloroethane 0.2430 0.0100 102 100 1.7 50.0 Qua1 1,3,5-Trichlorobenzene 1.436 1.155 0.0100 62.2 50.0 24.4 50.0 Ave 2-Methylnaphthalene 0.3459 0.1992 0.0100 86.8 50.0 73.6* 50.0 Ave



### FORM VII 8260B 

## 01/09/2013 Page 181 of 384

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53491-1

CMS18 11/20/2012 23:15 11/20/2012 15:57 11/20/2012 19:11 ICV 500-170445/20

DB624 TestAmerica Chicago

Lab File ID:18S1120.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dichlorodifluoromethane 0.7475 0.7223 0.0100 51.8 50.0 3.5 25.0 Ave Chloromethane 1.196 1.216 0.1000 49.2 50.0 -1.6 25.0 Ave Vinyl chloride 1.105 1.014 0.0100 54.4 50.0 8.9 25.0 Ave Bromomethane 0.3449 0.3260 0.0100 52.9 50.0 5.8 25.0 Ave Chloroethane 0.5345 0.5276 0.0100 50.7 50.0 1.3 25.0 Ave Dichlorofluoromethane 1.203 1.291 0.0100 46.6 50.0 -6.8 25.0 Ave Trichlorofluoromethane 0.9718 0.9563 0.0100 50.8 50.0 1.6 25.0 Ave Acrolein 0.0677 0.0676 0.0010 2003 2000 0.1 25.0 Ave 1,1-Dichloroethene 0.5115 0.4867 0.0100 52.6 50.0 5.1 25.0 Ave 1,1,2-Trichloro-1,2,2-triflu oroethane 0.5264 0.5836 0.0100 45.1 50.0 -9.8 25.0 Ave Acetone 0.0848 0.0915 0.0100 46.3 50.0 -7.4 25.0 Ave Carbon disulfide 1.870 1.669 0.0100 56.0 50.0 12.1 25.0 Ave Acetonitrile 0.0429 0.0412 0.0010 416 400 4.0 25.0 Ave Methylene Chloride 0.5400 0.5067 0.0100 53.3 50.0 6.6 25.0 Ave Acrylonitrile 0.1360 0.1347 0.0010 404 400 1.0 25.0 Ave trans-1,2-Dichloroethene 0.5838 0.5473 0.0100 53.3 50.0 6.7 25.0 Ave Methyl tert-butyl ether 0.9194 0.9064 0.0100 50.7 50.0 1.4 25.0 Ave 1,1-Dichloroethane 1.396 1.321 0.1000 52.9 50.0 5.7 25.0 Ave Vinyl acetate 0.8113 0.5886 0.0100 68.9 50.0 37.8* 25.0 Ave 2,2-Dichloropropane 0.6909 0.6761 0.0100 51.1 50.0 2.2 25.0 Ave cis-1,2-Dichloroethene 0.5988 0.5610 0.0100 53.4 50.0 6.7 25.0 Ave 2-Butanone (MEK) 0.1251 0.1174 0.0100 53.3 50.0 6.5 25.0 Ave Propionitrile 0.0303 0.0308 0.0010 394 400 -1.5 25.0 Ave Bromochloromethane 0.2121 0.2056 0.0100 51.6 50.0 3.2 25.0 Ave Tetrahydrofuran 0.0827 0.0819 0.0100 50.5 50.0 1.0 25.0 Ave Chloroform 0.9567 0.9125 0.0100 52.4 50.0 4.8 25.0 Ave 1,1,1-Trichloroethane 0.9247 0.8591 0.0100 53.8 50.0 7.6 25.0 Ave 1,1-Dichloropropene 0.7561 0.7416 0.0100 51.0 50.0 1.9 25.0 Ave Carbon tetrachloride 0.5510 0.5223 0.0100 52.8 50.0 5.5 25.0 Ave Benzene 1.424 1.447 0.0100 49.2 50.0 -1.6 25.0 Ave 1,2-Dichloroethane 0.4529 0.4605 0.0100 49.2 50.0 -1.7 25.0 Ave Trichloroethene 0.3538 0.3551 0.0100 49.8 50.0 -0.4 25.0 Ave 1,2-Dichloropropane 0.4194 0.4197 0.0100 50.0 50.0 -0.0 25.0 Ave Dibromomethane 0.1373 0.1358 0.0100 50.5 50.0 1.1 25.0 Ave Bromodichloromethane 0.3674 0.3668 0.0100 50.1 50.0 0.2 25.0 Ave 2-Chloroethyl vinyl ether 0.1270 0.1202 0.0100 52.8 50.0 5.7 25.0 Ave cis-1,3-Dichloropropene 0.4173 0.3958 0.0100 56.7 53.8 5.4 25.0 Ave 4-Methyl-2-pentanone (MIBK) 0.1944 0.1885 0.0100 51.6 50.0 3.2 25.0 Ave Toluene 0.8495 0.9066 0.0100 46.9 50.0 -6.3 25.0 Ave trans-1,3-Dichloropropene 0.3398 0.3238 0.0100 51.0 48.6 4.9 25.0 Ave



### FORM VII 8260B 

## 01/09/2013 Page 182 of 384

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53491-1

CMS18 11/20/2012 23:15 11/20/2012 15:57 11/20/2012 19:11 ICV 500-170445/20

DB624 TestAmerica Chicago

Lab File ID:18S1120.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

1,1,2-Trichloroethane 0.2514 0.2466 0.0100 51.0 50.0 1.9 25.0 Ave Tetrachloroethene 0.4528 0.4508 0.0100 50.2 50.0 0.5 25.0 Ave 1,3-Dichloropropane 0.3564 0.3653 0.0100 48.8 50.0 -2.4 25.0 Ave 2-Hexanone 0.1450 0.1337 0.0100 54.2 50.0 8.5 25.0 Ave Dibromochloromethane 0.2415 0.0100 48.3 50.0 -3.4 25.0 Qua1 1,2-Dibromoethane 0.1707 0.1685 0.0100 50.7 50.0 1.3 25.0 Ave 1-Chlorohexane 0.6944 0.7416 0.0100 46.8 50.0 -6.4 25.0 Ave Chlorobenzene 1.007 1.091 0.3000 46.2 50.0 -7.7 25.0 Ave 1,1,1,2-Tetrachloroethane 0.3703 0.3659 0.0100 50.6 50.0 1.2 25.0 Ave Ethylbenzene 0.6256 0.6360 0.0100 49.2 50.0 -1.6 25.0 Ave m&p-Xylene 1.546 1.652 0.0100 93.6 100 -6.4 25.0 Ave o-Xylene 1.582 1.745 0.0100 45.3 50.0 -9.3 25.0 Ave Styrene 1.204 1.198 0.0100 50.3 50.0 0.5 25.0 Ave Bromoform 0.1477 0.1000 49.9 50.0 -0.2 25.0 Qua1 Isopropylbenzene 3.730 4.053 0.0100 46.0 50.0 -8.0 25.0 Ave 1,1,2,2-Tetrachloroethane 0.4063 0.4016 0.3000 50.6 50.0 1.2 25.0 Ave Bromobenzene 0.8016 0.8022 0.0100 50.0 50.0 -0.0 25.0 Ave 1,2,3-Trichloropropane 0.3381 0.3605 0.0100 46.9 50.0 -6.2 25.0 Ave N-Propylbenzene 4.403 4.900 0.0100 44.9 50.0 -10.1 25.0 Ave 2-Chlorotoluene 2.594 2.790 0.0100 46.5 50.0 -7.0 25.0 Ave 1,3,5-Trimethylbenzene 3.446 3.453 0.0100 49.9 50.0 -0.2 25.0 Ave 4-Chlorotoluene 2.929 3.244 0.0100 45.2 50.0 -9.7 25.0 Ave tert-Butylbenzene 2.803 3.061 0.0100 45.8 50.0 -8.4 25.0 Ave 1,2,4-Trimethylbenzene 3.370 3.430 0.0100 49.1 50.0 -1.7 25.0 Ave sec-Butylbenzene 4.214 4.611 0.0100 45.7 50.0 -8.6 25.0 Ave 1,3-Dichlorobenzene 1.556 1.742 0.0100 44.7 50.0 -10.7 25.0 Ave p-Isopropyltoluene 3.475 3.850 0.0100 45.1 50.0 -9.7 25.0 Ave 1,4-Dichlorobenzene 1.630 1.714 0.0100 47.6 50.0 -4.9 25.0 Ave n-Butylbenzene 3.410 3.627 0.0100 47.0 50.0 -6.0 25.0 Ave 1,2-Dichlorobenzene 1.319 1.428 0.0100 46.2 50.0 -7.6 25.0 Ave 1,2-Dibromo-3-Chloropropane 0.0508 0.0518 0.0100 49.1 50.0 -1.9 25.0 Ave 1,2,4-Trichlorobenzene 0.6603 0.7642 0.0100 43.2 50.0 -13.6 25.0 Ave Hexachlorobutadiene 0.5859 0.0100 45.4 50.0 -9.2 25.0 Qua1 Naphthalene 0.8737 0.9358 0.0100 46.7 50.0 -6.6 25.0 Ave 1,2,3-Trichlorobenzene 0.4327 0.5020 0.0100 43.1 50.0 -13.8 25.0 Ave Dibromofluoromethane 0.4521 0.4406 0.0100 51.3 50.0 2.6 25.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.3163 0.3228 0.0100 49.0 50.0 -2.0 25.0 Ave Toluene-d8 (Surr) 1.189 1.202 0.0100 49.4 50.0 -1.1 25.0 Ave 4-Bromofluorobenzene (Surr) 0.5291 0.5452 0.0100 48.5 50.0 -3.0 25.0 Ave



### FORM VII 8260B 

## 01/09/2013 Page 183 of 384

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53491-1

CMS18 11/20/2012 23:15 11/20/2012 19:35 11/20/2012 22:26 ICV 500-170445/20

DB624 TestAmerica Chicago

Lab File ID:18S1120.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF
Ethyl ether 0.3863 0.4336 0.0100 44.5 50.0 -10.9 25.0 Ave Iodomethane 0.9905 0.8980 0.0100 55.2 50.0 10.3 25.0 Ave Methyl acetate 0.2086 0.3161 0.0100 33.0 50.0 -34.0* 25.0 Ave Hexane 1.102 1.276 0.0100 43.2 50.0 -13.6 25.0 Ave Cyclohexane 1.765 0.0100 48.0 50.0 -4.0 25.0 Lin1 Heptane 0.7770 0.8721 0.0100 44.6 50.0 -10.9 25.0 Ave Methylcyclohexane 0.7392 0.7981 0.0100 46.3 50.0 -7.4 25.0 Ave 1,3,5-Trichlorobenzene 1.090 1.196 0.0100 45.5 50.0 -8.9 25.0 Ave



### FORM VII 8260B 

## 01/09/2013 Page 184 of 384

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53491-1

CMS18 12/28/2012 09:14 11/20/2012 15:57 11/20/2012 19:11 CCV 500-174064/2

DB624 TestAmerica Chicago

Lab File ID:18C1228.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dichlorodifluoromethane 0.8870 0.7223 0.0100 61.4 50.0 22.8 50.0 Ave Chloromethane 1.208 1.216 0.1000 49.7 50.0 -0.7 50.0 Ave Vinyl chloride 0.9707 1.014 0.0100 47.8 50.0 -4.3 20.0 Ave Bromomethane 0.3518 0.3260 0.0100 54.0 50.0 7.9 50.0 Ave Chloroethane 0.5065 0.5276 0.0100 48.0 50.0 -4.0 50.0 Ave Dichlorofluoromethane 1.356 1.291 0.0100 52.5 50.0 5.1 50.0 Ave Trichlorofluoromethane 1.076 0.9563 0.0100 56.3 50.0 12.6 50.0 Ave Acrolein 0.0307 0.0676 0.0010 909 2000 -54.5* 50.0 Ave 1,1-Dichloroethene 0.5191 0.4867 0.0100 53.3 50.0 6.7 20.0 Ave 1,1,2-Trichloro-1,2,2-triflu oroethane 0.6296 0.5836 0.0100 53.9 50.0 7.9 50.0 Ave Acetone 0.0882 0.0915 0.0100 48.2 50.0 -3.6 50.0 Ave Carbon disulfide 1.980 1.669 0.0100 59.3 50.0 18.7 50.0 Ave Acetonitrile 0.0401 0.0412 0.0010 390 400 -2.6 50.0 Ave Methylene Chloride 0.4925 0.5067 0.0100 48.6 50.0 -2.8 50.0 Ave Acrylonitrile 0.1159 0.1347 0.0010 344 400 -14.0 50.0 Ave trans-1,2-Dichloroethene 0.5547 0.5473 0.0100 50.7 50.0 1.4 50.0 Ave Methyl tert-butyl ether 0.8376 0.9064 0.0100 46.2 50.0 -7.6 50.0 Ave 1,1-Dichloroethane 1.285 1.321 0.1000 48.7 50.0 -2.7 50.0 Ave Vinyl acetate 0.6842 0.5886 0.0100 58.1 50.0 16.2 50.0 Ave 2,2-Dichloropropane 0.7431 0.6761 0.0100 55.0 50.0 9.9 50.0 Ave cis-1,2-Dichloroethene 0.5467 0.5610 0.0100 48.7 50.0 -2.5 50.0 Ave 2-Butanone (MEK) 0.1140 0.1174 0.0100 48.5 50.0 -2.9 50.0 Ave Propionitrile 0.0272 0.0308 0.0010 354 400 -11.4 50.0 Ave Bromochloromethane 0.1957 0.2056 0.0100 47.6 50.0 -4.8 50.0 Ave Tetrahydrofuran 0.0753 0.0819 0.0100 46.0 50.0 -8.0 50.0 Ave Chloroform 0.9102 0.9125 0.0100 49.9 50.0 -0.3 20.0 Ave 1,1,1-Trichloroethane 0.9230 0.8591 0.0100 53.7 50.0 7.4 50.0 Ave Carbon tetrachloride 0.5596 0.5223 0.0100 53.6 50.0 7.1 50.0 Ave 1,1-Dichloropropene 0.7711 0.7416 0.0100 52.0 50.0 4.0 50.0 Ave Benzene 1.385 1.447 0.0100 47.9 50.0 -4.3 50.0 Ave 1,2-Dichloroethane 0.4353 0.4605 0.0100 47.3 50.0 -5.5 50.0 Ave Trichloroethene 0.3615 0.3551 0.0100 50.9 50.0 1.8 50.0 Ave 1,2-Dichloropropane 0.3788 0.4197 0.0100 45.1 50.0 -9.8 20.0 Ave Dibromomethane 0.1303 0.1358 0.0100 48.0 50.0 -4.1 50.0 Ave Bromodichloromethane 0.3766 0.3668 0.0100 51.3 50.0 2.7 50.0 Ave 2-Chloroethyl vinyl ether 0.1144 0.1202 0.0100 47.6 50.0 -4.9 50.0 Ave cis-1,3-Dichloropropene 0.3931 0.3958 0.0100 49.7 50.0 -0.7 50.0 Ave 4-Methyl-2-pentanone (MIBK) 0.1831 0.1885 0.0100 48.6 50.0 -2.9 50.0 Ave Toluene 0.8345 0.9066 0.0100 46.0 50.0 -8.0 20.0 Ave trans-1,3-Dichloropropene 0.3174 0.3238 0.0100 49.0 50.0 -2.0 50.0 Ave



### FORM VII 8260B 

## 01/09/2013 Page 185 of 384

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53491-1

CMS18 12/28/2012 09:14 11/20/2012 15:57 11/20/2012 19:11 CCV 500-174064/2

DB624 TestAmerica Chicago

Lab File ID:18C1228.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

1,1,2-Trichloroethane 0.2390 0.2466 0.0100 48.5 50.0 -3.1 50.0 Ave Tetrachloroethene 0.4570 0.4508 0.0100 50.7 50.0 1.4 50.0 Ave 1,3-Dichloropropane 0.3521 0.3653 0.0100 48.2 50.0 -3.6 50.0 Ave 2-Hexanone 0.1408 0.1337 0.0100 52.6 50.0 5.3 50.0 Ave Dibromochloromethane 0.2443 0.0100 48.8 50.0 -2.3 50.0 Qua1 1,2-Dibromoethane 0.1551 0.1685 0.0100 46.0 50.0 -8.0 50.0 Ave 1-Chlorohexane 0.7200 0.7416 0.0100 48.5 50.0 -2.9 50.0 Ave Chlorobenzene 1.067 1.091 0.3000 48.9 50.0 -2.2 50.0 Ave 1,1,1,2-Tetrachloroethane 0.3935 0.3659 0.0100 53.8 50.0 7.5 50.0 Ave Ethylbenzene 0.6449 0.6360 0.0100 50.7 50.0 1.4 20.0 Ave m&p-Xylene 1.677 1.652 0.0100 102 100 1.5 50.0 Ave o-Xylene 1.751 1.745 0.0100 50.2 50.0 0.4 50.0 Ave Styrene 1.195 1.198 0.0100 49.9 50.0 -0.3 50.0 Ave Bromoform 0.1351 0.1000 45.8 50.0 -8.4 50.0 Qua1 Isopropylbenzene 4.262 4.053 0.0100 52.6 50.0 5.1 50.0 Ave 1,1,2,2-Tetrachloroethane 0.4007 0.4016 0.3000 49.9 50.0 -0.2 50.0 Ave Bromobenzene 0.7804 0.8022 0.0100 48.6 50.0 -2.7 50.0 Ave 1,2,3-Trichloropropane 0.3357 0.3605 0.0100 46.6 50.0 -6.9 50.0 Ave N-Propylbenzene 5.113 4.900 0.0100 52.2 50.0 4.3 50.0 Ave 2-Chlorotoluene 2.842 2.790 0.0100 50.9 50.0 1.9 50.0 Ave 1,3,5-Trimethylbenzene 3.578 3.453 0.0100 51.8 50.0 3.6 50.0 Ave 4-Chlorotoluene 3.306 3.244 0.0100 51.0 50.0 1.9 50.0 Ave tert-Butylbenzene 3.149 3.061 0.0100 51.4 50.0 2.8 50.0 Ave 1,2,4-Trimethylbenzene 3.504 3.430 0.0100 51.1 50.0 2.1 50.0 Ave sec-Butylbenzene 4.798 4.611 0.0100 52.0 50.0 4.1 50.0 Ave 1,3-Dichlorobenzene 1.720 1.742 0.0100 49.4 50.0 -1.3 50.0 Ave p-Isopropyltoluene 4.047 3.850 0.0100 52.6 50.0 5.1 50.0 Ave 1,4-Dichlorobenzene 1.677 1.714 0.0100 48.9 50.0 -2.1 50.0 Ave n-Butylbenzene 3.934 3.627 0.0100 54.2 50.0 8.4 50.0 Ave 1,2-Dichlorobenzene 1.410 1.428 0.0100 49.4 50.0 -1.2 50.0 Ave 1,2-Dibromo-3-Chloropropane 0.0547 0.0518 0.0100 52.9 50.0 5.7 50.0 Ave 1,2,4-Trichlorobenzene 0.7439 0.7642 0.0100 48.7 50.0 -2.7 50.0 Ave Hexachlorobutadiene 0.6482 0.0100 50.7 50.0 1.5 50.0 Qua1 Naphthalene 0.8754 0.9358 0.0100 46.8 50.0 -6.4 50.0 Ave 1,2,3-Trichlorobenzene 0.4632 0.5020 0.0100 46.1 50.0 -7.7 50.0 Ave Dibromofluoromethane 0.4400 0.4406 0.0100 49.9 50.0 -0.1 50.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.3156 0.3228 0.0100 48.9 50.0 -2.2 50.0 Ave Toluene-d8 (Surr) 1.205 1.202 0.0100 50.1 50.0 0.2 50.0 Ave 4-Bromofluorobenzene (Surr) 0.5323 0.5452 0.0100 48.8 50.0 -2.4 50.0 Ave



### FORM VII 8260B 

## 01/09/2013 Page 186 of 384

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53491-1

CMS18 12/28/2012 09:37 11/20/2012 15:57 11/20/2012 19:11 CCV 500-174064/3

DB624 TestAmerica Chicago

Lab File ID:18D1228.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dibromofluoromethane 0.4309 0.4406 0.0100 48.9 50.0 -2.2 50.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.3128 0.3228 0.0100 48.5 50.0 -3.1 50.0 Ave Toluene-d8 (Surr) 1.164 1.202 0.0100 48.4 50.0 -3.2 50.0 Ave 4-Bromofluorobenzene (Surr) 0.5299 0.5452 0.0100 48.6 50.0 -2.8 50.0 Ave



### FORM VII 8260B 

## 01/09/2013 Page 187 of 384

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53491-1

CMS18 12/28/2012 09:37 11/20/2012 19:35 11/20/2012 22:26 CCV 500-174064/3

DB624 TestAmerica Chicago

Lab File ID:18D1228.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Butadiene 1.182 1.088 0.0100 54.3 50.0 8.7 50.0 Ave Ethyl ether 0.3630 0.4336 0.0100 41.9 50.0 -16.3 50.0 Ave Iodomethane 0.9031 0.8980 0.0100 101 100 0.6 50.0 Ave 3-Chloropropene 0.3168 0.3009 0.0100 105 100 5.3 50.0 Ave Methyl acetate 0.2765 0.3161 0.0100 43.7 50.0 -12.5 50.0 Ave Hexane 1.232 1.276 0.0100 48.3 50.0 -3.4 50.0 Ave Isopropyl ether 2.279 2.477 0.0100 46.0 50.0 -8.0 50.0 Ave 2-Chloro-1,3-butadiene 1.550 1.529 0.0100 50.7 50.0 1.4 50.0 Ave Ethyl acetate 0.2034 0.2378 0.0100 428 500 -14.5 50.0 Ave Methacrylonitrile 0.1778 0.1997 0.0100 89.0 100 -11.0 50.0 Ave Cyclohexane 1.802 0.0100 49.1 50.0 -1.9 50.0 Lin1 Isobutyl alcohol 0.0086 0.0087 0.0010 3963 4000 -0.9 50.0 Ave 2,2,4-Trimethylpentane 2.803 2.944 0.0100 47.6 50.0 -4.8 50.0 Ave Heptane 0.8750 0.8721 0.0100 50.2 50.0 0.3 50.0 Ave n-Butyl alcohol 0.0058 0.0054 0.0010 4240 4000 6.0 50.0 Ave Methylcyclohexane 0.8056 0.7981 0.0100 50.5 50.0 0.9 50.0 Ave Methyl methacrylate 0.1595 0.1838 0.0100 86.8 100 -13.2 50.0 Ave 2-Nitropropane 0.0775 0.0698 0.0100 4440 4000 11.0 50.0 Ave Ethyl methacrylate 0.2332 0.2459 0.0100 94.8 100 -5.2 50.0 Ave Cyclohexanone 0.0473 0.0282 0.0100 6696 4000 67.4* 50.0 Ave trans-1,4-Dichloro-2-butene 0.0592 0.0100 91.6 100 -8.4 50.0 Lin1 Pentachloroethane 0.3019 0.2879 0.0100 105 100 4.9 50.0 Ave 1,3,5-Trichlorobenzene 1.317 1.196 0.0100 55.0 50.0 10.0 50.0 Ave 2-Methylnaphthalene 0.2716 0.0100 40.1 50.0 -19.9 50.0 Qua



### FORM VII 8260B 

## 01/09/2013 Page 188 of 384

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53491-1

CMS22 12/12/2012 00:17 12/11/2012 14:23 12/11/2012 18:09 ICV 500-172615/23

DB624 TestAmerica Chicago

Lab File ID:22S1211.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dichlorodifluoromethane 0.4239 0.5420 0.0100 39.1 50.0 -21.8 25.0 Ave Chloromethane 0.5561 0.7111 0.1000 39.1 50.0 -21.8 25.0 Ave Vinyl chloride 0.5920 0.6381 0.0100 46.4 50.0 -7.2 25.0 Ave Bromomethane 0.1541 0.1998 0.0100 38.6 50.0 -22.9 25.0 Ave Chloroethane 0.2911 0.3338 0.0100 43.6 50.0 -12.8 25.0 Ave Dichlorofluoromethane 0.8378 0.999 0.0100 41.9 50.0 -16.2 25.0 Ave Trichlorofluoromethane 0.7409 0.8265 0.0100 44.8 50.0 -10.4 25.0 Ave Acrolein 0.0406 0.0397 0.0010 2044 2000 2.2 25.0 Ave 1,1-Dichloroethene 0.3815 0.4001 0.0100 47.7 50.0 -4.7 25.0 Ave 1,1,2-Trichloro-1,2,2-triflu oroethane 0.4598 0.4862 0.0100 47.3 50.0 -5.4 25.0 Ave Acetone 0.0621 0.0639 0.0100 48.5 50.0 -2.9 25.0 Ave Carbon disulfide 1.369 1.480 0.0100 46.3 50.0 -7.5 25.0 Ave Acetonitrile 0.0292 0.0297 0.0010 393 400 -1.7 25.0 Ave Methylene Chloride 0.3602 0.3812 0.0100 47.2 50.0 -5.5 25.0 Ave Acrylonitrile 0.0797 0.0805 0.0010 396 400 -1.0 25.0 Ave trans-1,2-Dichloroethene 0.4398 0.4499 0.0100 48.9 50.0 -2.3 25.0 Ave Methyl tert-butyl ether 0.6905 0.7369 0.0100 46.9 50.0 -6.3 25.0 Ave 1,1-Dichloroethane 0.8456 0.8857 0.1000 47.7 50.0 -4.5 25.0 Ave Vinyl acetate 0.6214 0.6255 0.0100 49.7 50.0 -0.6 25.0 Ave 2,2-Dichloropropane 0.6853 0.7341 0.0100 46.7 50.0 -6.6 25.0 Ave cis-1,2-Dichloroethene 0.4436 0.4554 0.0100 48.7 50.0 -2.6 25.0 Ave 2-Butanone (MEK) 0.0837 0.0924 0.0100 45.3 50.0 -9.4 25.0 Ave Propionitrile 0.0211 0.0203 0.0010 414 400 3.5 25.0 Ave Bromochloromethane 0.1638 0.1785 0.0100 45.9 50.0 -8.2 25.0 Ave Tetrahydrofuran 0.0548 0.0578 0.0100 47.3 50.0 -5.3 25.0 Ave Chloroform 0.7135 0.7375 0.0100 48.4 50.0 -3.3 25.0 Ave 1,1,1-Trichloroethane 0.7299 0.7394 0.0100 49.4 50.0 -1.3 25.0 Ave Carbon tetrachloride 0.4652 0.4834 0.0100 48.1 50.0 -3.8 25.0 Ave 1,1-Dichloropropene 0.6138 0.6488 0.0100 47.3 50.0 -5.4 25.0 Ave Benzene 1.148 1.229 0.0100 46.7 50.0 -6.6 25.0 Ave 1,2-Dichloroethane 0.3244 0.3536 0.0100 45.9 50.0 -8.3 25.0 Ave Trichloroethene 0.3212 0.3450 0.0100 46.6 50.0 -6.9 25.0 Ave 1,2-Dichloropropane 0.2970 0.3152 0.0100 47.1 50.0 -5.8 25.0 Ave Dibromomethane 0.1149 0.1271 0.0100 45.2 50.0 -9.6 25.0 Ave Bromodichloromethane 0.3216 0.3600 0.0100 44.7 50.0 -10.7 25.0 Ave 2-Chloroethyl vinyl ether 0.0957 0.1054 0.0100 45.4 50.0 -9.2 25.0 Ave cis-1,3-Dichloropropene 0.3814 0.4091 0.0100 50.1 53.8 -6.8 25.0 Ave 4-Methyl-2-pentanone (MIBK) 0.1404 0.1536 0.0100 45.7 50.0 -8.6 25.0 Ave Toluene 0.7569 0.8177 0.0100 46.3 50.0 -7.4 25.0 Ave trans-1,3-Dichloropropene 0.3107 0.3392 0.0100 44.5 48.6 -8.4 25.0 Ave



### FORM VII 8260B 

## 01/09/2013 Page 189 of 384

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53491-1

CMS22 12/12/2012 00:17 12/11/2012 14:23 12/11/2012 18:09 ICV 500-172615/23

DB624 TestAmerica Chicago

Lab File ID:22S1211.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

1,1,2-Trichloroethane 0.1573 0.1723 0.0100 45.6 50.0 -8.7 25.0 Ave Tetrachloroethene 0.4260 0.4537 0.0100 47.0 50.0 -6.1 25.0 Ave 1,3-Dichloropropane 0.3223 0.3491 0.0100 46.2 50.0 -7.7 25.0 Ave 2-Hexanone 0.1135 0.1204 0.0100 47.1 50.0 -5.7 25.0 Ave Dibromochloromethane 0.2454 0.2603 0.0100 47.1 50.0 -5.7 25.0 Ave 1,2-Dibromoethane 0.1486 0.1651 0.0100 45.0 50.0 -10.0 25.0 Ave Chlorobenzene 0.9004 1.012 0.3000 44.5 50.0 -11.0 25.0 Ave 1-Chlorohexane 0.6546 0.6865 0.0100 47.7 50.0 -4.6 25.0 Ave 1,1,1,2-Tetrachloroethane 0.3297 0.3400 0.0100 48.5 50.0 -3.0 25.0 Ave Ethylbenzene 0.5498 0.5753 0.0100 47.8 50.0 -4.4 25.0 Ave m&p-Xylene 1.339 1.427 0.0100 93.8 100 -6.2 25.0 Ave o-Xylene 1.295 1.456 0.0100 44.5 50.0 -11.1 25.0 Ave Styrene 1.076 1.120 0.0100 48.0 50.0 -3.9 25.0 Ave Bromoform 0.1521 0.1536 0.1000 49.5 50.0 -1.0 25.0 Ave Isopropylbenzene 2.951 3.312 0.0100 44.6 50.0 -10.9 25.0 Ave Bromobenzene 0.6901 0.7374 0.0100 46.8 50.0 -6.4 25.0 Ave 1,1,2,2-Tetrachloroethane 0.3650 0.3844 0.3000 47.5 50.0 -5.1 25.0 Ave 1,2,3-Trichloropropane 0.2697 0.2827 0.0100 47.7 50.0 -4.6 25.0 Ave N-Propylbenzene 3.489 3.971 0.0100 43.9 50.0 -12.2 25.0 Ave 4-Chlorotoluene 2.042 2.242 0.0100 45.5 50.0 -8.9 25.0 Ave 1,3,5-Trimethylbenzene 2.737 2.765 0.0100 49.5 50.0 -1.0 25.0 Ave 2-Chlorotoluene 2.355 2.663 0.0100 44.2 50.0 -11.6 25.0 Ave tert-Butylbenzene 2.302 2.558 0.0100 45.0 50.0 -10.0 25.0 Ave 1,2,4-Trimethylbenzene 2.637 2.713 0.0100 48.6 50.0 -2.8 25.0 Ave sec-Butylbenzene 3.418 3.783 0.0100 45.2 50.0 -9.6 25.0 Ave 1,3-Dichlorobenzene 1.369 1.575 0.0100 43.5 50.0 -13.1 25.0 Ave p-Isopropyltoluene 2.935 3.287 0.0100 44.7 50.0 -10.7 25.0 Ave 1,4-Dichlorobenzene 1.454 1.556 0.0100 46.7 50.0 -6.6 25.0 Ave 1,2-Dichlorobenzene 1.190 1.323 0.0100 45.0 50.0 -10.1 25.0 Ave n-Butylbenzene 2.736 2.919 0.0100 46.9 50.0 -6.3 25.0 Ave 1,2-Dibromo-3-Chloropropane 0.0567 0.0661 0.0100 42.9 50.0 -14.2 25.0 Ave 1,2,4-Trichlorobenzene 0.7803 0.8970 0.0100 43.5 50.0 -13.0 25.0 Ave Hexachlorobutadiene 0.6904 0.7568 0.0100 45.6 50.0 -8.8 25.0 Ave Naphthalene 0.8667 0.9856 0.0100 44.0 50.0 -12.1 25.0 Ave 1,2,3-Trichlorobenzene 0.6586 0.7171 0.0100 45.9 50.0 -8.2 25.0 Ave Dibromofluoromethane 0.3761 0.3990 0.0100 47.1 50.0 -5.7 25.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.2556 0.2793 0.0100 45.8 50.0 -8.5 25.0 Ave Toluene-d8 (Surr) 1.117 1.184 0.0100 47.2 50.0 -5.6 25.0 Ave 4-Bromofluorobenzene (Surr) 0.4730 0.5005 0.0100 47.3 50.0 -5.5 25.0 Ave



### FORM VII 8260B 

## 01/09/2013 Page 190 of 384

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53491-1

CMS22 12/12/2012 00:17 12/11/2012 19:06 12/11/2012 23:48 ICV 500-172615/23

DB624 TestAmerica Chicago

Lab File ID:22S1211.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF
Ethyl ether 0.2517 0.2603 0.0100 48.3 50.0 -3.3 25.0 Ave Iodomethane 0.6879 0.0100 52.8 50.0 5.6 25.0 Lin1 Methyl acetate 0.1450 0.2127 0.0100 34.1 50.0 -31.8* 25.0 Ave Hexane 0.9019 0.8764 0.0100 51.5 50.0 2.9 25.0 Ave Cyclohexane 1.057 0.0100 49.4 50.0 -1.2 25.0 Lin1 Heptane 0.6922 0.7351 0.0100 47.1 50.0 -5.8 25.0 Ave Methylcyclohexane 0.6069 0.5969 0.0100 50.8 50.0 1.7 25.0 Ave 1,3,5-Trichlorobenzene 1.140 1.226 0.0100 46.5 50.0 -7.0 25.0 Ave



### FORM VII 8260B 

## 01/09/2013 Page 191 of 384

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53491-1

CMS22 12/27/2012 11:55 12/11/2012 14:23 12/11/2012 18:09 CCV 500-173987/2

DB624 TestAmerica Chicago

Lab File ID:22C1227.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dichlorodifluoromethane 0.6218 0.5420 0.0100 57.4 50.0 14.7 50.0 Ave Chloromethane 0.7065 0.7111 0.1000 49.7 50.0 -0.7 50.0 Ave Vinyl chloride 0.6748 0.6381 0.0100 52.9 50.0 5.8 20.0 Ave Bromomethane 0.2820 0.1998 0.0100 70.6 50.0 41.2 50.0 Ave Chloroethane 0.3981 0.3338 0.0100 59.6 50.0 19.3 50.0 Ave Dichlorofluoromethane 0.997 0.999 0.0100 49.9 50.0 -0.2 50.0 Ave Trichlorofluoromethane 0.8752 0.8265 0.0100 53.0 50.0 5.9 50.0 Ave Acrolein 0.0285 0.0397 0.0010 1436 2000 -28.2 50.0 Ave 1,1-Dichloroethene 0.4001 0.4001 0.0100 50.0 50.0 -0.0 20.0 Ave 1,1,2-Trichloro-1,2,2-triflu oroethane 0.4759 0.4862 0.0100 49.0 50.0 -2.1 50.0 Ave Acetone 0.0587 0.0639 0.0100 45.9 50.0 -8.2 50.0 Ave Carbon disulfide 1.472 1.480 0.0100 49.7 50.0 -0.6 50.0 Ave Acetonitrile 0.0245 0.0297 0.0010 330 400 -17.5 50.0 Ave Methylene Chloride 0.3566 0.3812 0.0100 46.8 50.0 -6.4 50.0 Ave Acrylonitrile 0.0762 0.0805 0.0010 379 400 -5.4 50.0 Ave trans-1,2-Dichloroethene 0.4317 0.4499 0.0100 48.0 50.0 -4.1 50.0 Ave Methyl tert-butyl ether 0.6671 0.7369 0.0100 45.3 50.0 -9.5 50.0 Ave 1,1-Dichloroethane 0.8438 0.8857 0.1000 47.6 50.0 -4.7 50.0 Ave Vinyl acetate 0.5267 0.6255 0.0100 42.1 50.0 -15.8 50.0 Ave 2,2-Dichloropropane 0.6289 0.7341 0.0100 42.8 50.0 -14.3 50.0 Ave cis-1,2-Dichloroethene 0.4453 0.4554 0.0100 48.9 50.0 -2.2 50.0 Ave 2-Butanone (MEK) 0.0874 0.0924 0.0100 47.3 50.0 -5.4 50.0 Ave Propionitrile 0.0196 0.0203 0.0010 386 400 -3.6 50.0 Ave Bromochloromethane 0.1670 0.1785 0.0100 46.8 50.0 -6.5 50.0 Ave Tetrahydrofuran 0.0515 0.0578 0.0100 44.5 50.0 -11.0 50.0 Ave Chloroform 0.6995 0.7375 0.0100 47.4 50.0 -5.1 20.0 Ave 1,1,1-Trichloroethane 0.6854 0.7394 0.0100 46.4 50.0 -7.3 50.0 Ave Carbon tetrachloride 0.4313 0.4834 0.0100 44.6 50.0 -10.8 50.0 Ave 1,1-Dichloropropene 0.6403 0.6488 0.0100 49.4 50.0 -1.3 50.0 Ave Benzene 1.224 1.229 0.0100 49.8 50.0 -0.4 50.0 Ave 1,2-Dichloroethane 0.3533 0.3536 0.0100 50.0 50.0 -0.0 50.0 Ave Trichloroethene 0.3490 0.3450 0.0100 50.6 50.0 1.1 50.0 Ave 1,2-Dichloropropane 0.3146 0.3152 0.0100 49.9 50.0 -0.2 20.0 Ave Dibromomethane 0.1251 0.1271 0.0100 49.2 50.0 -1.6 50.0 Ave Bromodichloromethane 0.3555 0.3600 0.0100 49.4 50.0 -1.2 50.0 Ave 2-Chloroethyl vinyl ether 0.1106 0.1054 0.0100 52.5 50.0 5.0 50.0 Ave cis-1,3-Dichloropropene 0.3925 0.4091 0.0100 48.0 50.0 -4.1 50.0 Ave 4-Methyl-2-pentanone (MIBK) 0.1479 0.1536 0.0100 48.1 50.0 -3.7 50.0 Ave Toluene 0.8087 0.8177 0.0100 49.5 50.0 -1.1 20.0 Ave trans-1,3-Dichloropropene 0.3122 0.3392 0.0100 46.0 50.0 -7.9 50.0 Ave



### FORM VII 8260B 

## 01/09/2013 Page 192 of 384

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53491-1

CMS22 12/27/2012 11:55 12/11/2012 14:23 12/11/2012 18:09 CCV 500-173987/2

DB624 TestAmerica Chicago

Lab File ID:22C1227.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

1,1,2-Trichloroethane 0.1643 0.1723 0.0100 47.7 50.0 -4.7 50.0 Ave Tetrachloroethene 0.4598 0.4537 0.0100 50.7 50.0 1.3 50.0 Ave 1,3-Dichloropropane 0.3473 0.3491 0.0100 49.8 50.0 -0.5 50.0 Ave 2-Hexanone 0.1202 0.1204 0.0100 49.9 50.0 -0.2 50.0 Ave Dibromochloromethane 0.2612 0.2603 0.0100 50.2 50.0 0.4 50.0 Ave 1,2-Dibromoethane 0.1642 0.1651 0.0100 49.7 50.0 -0.5 50.0 Ave Chlorobenzene 1.044 1.012 0.3000 51.6 50.0 3.2 50.0 Ave 1-Chlorohexane 0.7028 0.6865 0.0100 51.2 50.0 2.4 50.0 Ave 1,1,1,2-Tetrachloroethane 0.3319 0.3400 0.0100 48.8 50.0 -2.4 50.0 Ave Ethylbenzene 0.5986 0.5753 0.0100 52.0 50.0 4.1 20.0 Ave m&p-Xylene 1.517 1.427 0.0100 106 100 6.3 50.0 Ave o-Xylene 1.495 1.456 0.0100 51.3 50.0 2.7 50.0 Ave Styrene 1.174 1.120 0.0100 52.4 50.0 4.8 50.0 Ave Bromoform 0.1506 0.1536 0.1000 49.0 50.0 -2.0 50.0 Ave Isopropylbenzene 3.313 3.312 0.0100 50.0 50.0 0.0 50.0 Ave Bromobenzene 0.7245 0.7374 0.0100 49.1 50.0 -1.8 50.0 Ave 1,1,2,2-Tetrachloroethane 0.3760 0.3844 0.3000 48.9 50.0 -2.2 50.0 Ave 1,2,3-Trichloropropane 0.2682 0.2827 0.0100 47.5 50.0 -5.1 50.0 Ave N-Propylbenzene 4.091 3.971 0.0100 51.5 50.0 3.0 50.0 Ave 4-Chlorotoluene 2.248 2.242 0.0100 50.1 50.0 0.3 50.0 Ave 1,3,5-Trimethylbenzene 2.837 2.765 0.0100 51.3 50.0 2.6 50.0 Ave 2-Chlorotoluene 2.701 2.663 0.0100 50.7 50.0 1.5 50.0 Ave tert-Butylbenzene 2.540 2.558 0.0100 49.7 50.0 -0.7 50.0 Ave 1,2,4-Trimethylbenzene 2.754 2.713 0.0100 50.7 50.0 1.5 50.0 Ave sec-Butylbenzene 3.893 3.783 0.0100 51.5 50.0 2.9 50.0 Ave 1,3-Dichlorobenzene 1.592 1.575 0.0100 50.5 50.0 1.1 50.0 Ave p-Isopropyltoluene 3.392 3.287 0.0100 51.6 50.0 3.2 50.0 Ave 1,4-Dichlorobenzene 1.585 1.556 0.0100 50.9 50.0 1.9 50.0 Ave 1,2-Dichlorobenzene 1.350 1.323 0.0100 51.0 50.0 2.0 50.0 Ave n-Butylbenzene 3.071 2.919 0.0100 52.6 50.0 5.2 50.0 Ave 1,2-Dibromo-3-Chloropropane 0.0552 0.0661 0.0100 41.7 50.0 -16.6 50.0 Ave 1,2,4-Trichlorobenzene 0.8967 0.8970 0.0100 50.0 50.0 -0.0 50.0 Ave Hexachlorobutadiene 0.7691 0.7568 0.0100 50.8 50.0 1.6 50.0 Ave Naphthalene 0.9243 0.9856 0.0100 46.9 50.0 -6.2 50.0 Ave 1,2,3-Trichlorobenzene 0.7043 0.7171 0.0100 49.1 50.0 -1.8 50.0 Ave Dibromofluoromethane 0.3704 0.3990 0.0100 46.4 50.0 -7.2 50.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.2555 0.2793 0.0100 45.7 50.0 -8.5 50.0 Ave Toluene-d8 (Surr) 1.141 1.184 0.0100 48.2 50.0 -3.6 50.0 Ave 4-Bromofluorobenzene (Surr) 0.4821 0.5005 0.0100 48.2 50.0 -3.7 50.0 Ave



### FORM VII 8260B 

## 01/09/2013 Page 193 of 384

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53491-1

CMS22 12/27/2012 12:22 12/11/2012 14:23 12/11/2012 18:09 CCV 500-173987/3

DB624 TestAmerica Chicago

Lab File ID:22D1227.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dibromofluoromethane 0.3757 0.3990 0.0100 47.1 50.0 -5.8 50.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.2682 0.2793 0.0100 48.0 50.0 -4.0 50.0 Ave Toluene-d8 (Surr) 1.217 1.184 0.0100 51.4 50.0 2.8 50.0 Ave 4-Bromofluorobenzene (Surr) 0.5156 0.5005 0.0100 51.5 50.0 3.0 50.0 Ave



### FORM VII 8260B 

## 01/09/2013 Page 194 of 384

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53491-1

CMS22 12/27/2012 12:22 12/11/2012 19:06 12/11/2012 23:48 CCV 500-173987/3

DB624 TestAmerica Chicago

Lab File ID:22D1227.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Butadiene 0.7254 0.0100 44.8 50.0 -10.5 50.0 Lin1 Ethyl ether 0.2638 0.2603 0.0100 50.7 50.0 1.3 50.0 Ave Iodomethane 0.6395 0.0100 96.6 100 -3.4 50.0 Lin1 3-Chloropropene 0.2406 0.2462 0.0100 97.7 100 -2.3 50.0 Ave Methyl acetate 0.1901 0.2127 0.0100 44.7 50.0 -10.6 50.0 Ave Hexane 0.9344 0.8764 0.0100 53.3 50.0 6.6 50.0 Ave 2-Chloro-1,3-butadiene 0.9629 0.9423 0.0100 51.1 50.0 2.2 50.0 Ave Isopropyl ether 1.519 1.545 0.0100 49.2 50.0 -1.6 50.0 Ave Ethyl acetate 0.1976 0.1956 0.0100 505 500 1.0 50.0 Ave Methacrylonitrile 0.1506 0.1427 0.0100 106 100 5.6 50.0 Ave Cyclohexane 1.052 0.0100 49.1 50.0 -1.7 50.0 Lin1 Isobutyl alcohol 0.0065 0.0073 0.0010 3556 4000 -11.1 50.0 Ave 2,2,4-Trimethylpentane 1.785 1.673 0.0100 53.4 50.0 6.7 50.0 Ave Heptane 0.7687 0.7351 0.0100 52.3 50.0 4.6 50.0 Ave n-Butyl alcohol 0.0037 0.0045 0.0010 3350 4000 -16.3 50.0 Ave Methylcyclohexane 0.6334 0.5969 0.0100 53.1 50.0 6.1 50.0 Ave Methyl methacrylate 0.1732 0.1655 0.0100 105 100 4.7 50.0 Ave 2-Nitropropane 0.0767 0.0618 0.0100 4966 4000 24.2 50.0 Ave Ethyl methacrylate 0.2708 0.2528 0.0100 107 100 7.1 50.0 Ave Cyclohexanone 0.0529 0.0256 0.0100 8275 4000 106.9* 50.0 Ave trans-1,4-Dichloro-2-butene 0.0618 0.0710 0.0100 87.1 100 -12.9 50.0 Ave Pentachloroethane 0.2996 0.2758 0.0100 109 100 8.6 50.0 Ave 1,3,5-Trichlorobenzene 1.353 1.226 0.0100 55.2 50.0 10.3 50.0 Ave 2-Methylnaphthalene 0.6506 0.6831 0.0100 47.6 50.0 -4.8 50.0 Ave



### FORM VII 8260B 

## 01/09/2013 Page 195 of 384

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG No.: 500-53491-1
Lab Sample ID:MB 500-173973/5 Matrix: 6M1227.d Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med) Low 5(g)
0.2(mm) Date Analyzed:12/27/2012 10:33

ID: DB624
Analysis Batch No.: 173973 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 2.16 67-64-1 Acetone <5.00 5.00 1.81 78-93-3 2-Butanone (MEK) <5.00


### %REC CAS NO. LIMITS Q SURROGATE 94 70-134 17060-07-0 1,2-Dichloroethane-d4 (Surr) 96 75-122 2037-26-5 Toluene-d8 (Surr) 84 70-122 460-00-4 4-Bromofluorobenzene (Surr) 90 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/09/2013 Page 196 of 384

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG No.: 500-53491-1
Lab Sample ID:MB 500-173987/7 Matrix: 22M1227.D Lab File ID: Date Collected: 8260B Analysis Method: Water TestAmerica Chicago

Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med) Low 5(mL)
0.2(mm) Date Analyzed:12/27/2012 14:10

ID: DB624
Analysis Batch No.: 173987 ug/L Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 1.29 67-64-1 Acetone <5.00 5.00 1.47 78-93-3 2-Butanone (MEK) <5.00


### %REC CAS NO. LIMITS Q SURROGATE 98 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 103 75-120 2037-26-5 Toluene-d8 (Surr) 97 75-120 460-00-4 4-Bromofluorobenzene (Surr) 97 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/09/2013 Page 197 of 384

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG No.: 500-53491-1
Lab Sample ID:MB 500-174064/6 Matrix: 18M1228.D Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med)Medium 5 (mL) 0.2(mm) Date Analyzed:12/28/2012 10:45

ID: DB624
Analysis Batch No.: 174064 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 1.30 67-64-1 Acetone <5.00 5.00 1.47 78-93-3 2-Butanone (MEK) <5.00


### %REC CAS NO. LIMITS Q SURROGATE 101 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 101 75-120 2037-26-5 Toluene-d8 (Surr) 98 75-120 460-00-4 4-Bromofluorobenzene (Surr) 96 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/09/2013 Page 198 of 384

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG No.: 500-53491-1
Lab Sample ID:LCS 500-173973/6 Matrix: 6S1227.d Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med) Low 5(g)
0.2(mm) Date Analyzed:12/27/2012 10:56

ID: DB624
Analysis Batch No.: 173973 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 2.16 67-64-1 Acetone 47.98 5.00 1.81 78-93-3 2-Butanone (MEK) 43.18


### %REC CAS NO. LIMITS Q SURROGATE 84 70-134 17060-07-0 1,2-Dichloroethane-d4 (Surr) 89 75-122 2037-26-5 Toluene-d8 (Surr) 81 70-122 460-00-4 4-Bromofluorobenzene (Surr) 81 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/09/2013 Page 199 of 384

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG No.: 500-53491-1
Lab Sample ID:LCS 500-173987/4 Matrix: 22S1227.D Lab File ID: Date Collected: 8260B Analysis Method: Water TestAmerica Chicago

Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med) Low 5(mL)
0.2(mm) Date Analyzed:12/27/2012 12:46

ID: DB624
Analysis Batch No.: 173987 ug/L Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 1.29 67-64-1 Acetone 53.44 5.00 1.47 78-93-3 2-Butanone (MEK) 46.97


### %REC CAS NO. LIMITS Q SURROGATE 92 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 96 75-120 2037-26-5 Toluene-d8 (Surr) 96 75-120 460-00-4 4-Bromofluorobenzene (Surr) 94 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/09/2013 Page 200 of 384

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG No.: 500-53491-1
Lab Sample ID:LCS 500-174064/4 Matrix: 18S1228.D Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med)Medium 5 (mL) 0.2(mm) Date Analyzed:12/28/2012 10:00

ID: DB624
Analysis Batch No.: 174064 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 1.30 67-64-1 Acetone 50.53 5.00 1.47 78-93-3 2-Butanone (MEK) 43.61


### %REC CAS NO. LIMITS Q SURROGATE 95 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 97 75-120 2037-26-5 Toluene-d8 (Surr) 97 75-120 460-00-4 4-Bromofluorobenzene (Surr) 100 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/09/2013 Page 201 of 384

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG No.: 500-53491-1
Lab Sample ID:LCSD 500-173973/7 Matrix: 6T1227.d Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med) Low 5(g)
0.2(mm) Date Analyzed:12/27/2012 11:19

ID: DB624
Analysis Batch No.: 173973 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 2.16 67-64-1 Acetone 55.07 5.00 1.81 78-93-3 2-Butanone (MEK) 44.82


### %REC CAS NO. LIMITS Q SURROGATE 88 70-134 17060-07-0 1,2-Dichloroethane-d4 (Surr) 93 75-122 2037-26-5 Toluene-d8 (Surr) 87 70-122 460-00-4 4-Bromofluorobenzene (Surr) 91 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/09/2013 Page 202 of 384

### Lab Name: Job No.: SDG No.: Instrument ID: Analysis Batch Number: GC/MS VOA ANALYSIS RUN LOG

DILUTION FACTOR COLUMN ID DATE ANALYZED LAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID 

### TestAmerica Chicago 500-53491-1

CMS06 171819 Start Date: End Date:12/04/2012 19:58 12/04/2012 14:01

BFB 500-171819/1 DB624 0.2(mm) 1 12/04/2012 14:01 6B1204.d STD1 500-171819/2 IC DB624 0.2(mm) 1 12/04/2012 14:34 6I1204a.d STD2 500-171819/3 IC DB624 0.2(mm) 1 12/04/2012 14:57 6I1204b.d STD4 500-171819/5 IC DB624 0.2(mm) 1 12/04/2012 15:43 6I1204d.d STD3 500-171819/16 ICIS DB624 0.2(mm) 1 12/04/2012 16:10 6I1204CC.d STD5 500-171819/6 IC DB624 0.2(mm) 1 12/04/2012 16:33 6I1204e.d STD6 500-171819/7 IC DB624 0.2(mm) 1 12/04/2012 16:55 6I1204f.d STD1AP 500-171819/8 IC DB624 0.2(mm) 1 12/04/2012 17:18 6J1204a.d STD2AP 500-171819/9 IC DB624 0.2(mm) 1 12/04/2012 17:41 6J1204b.d STD3AP 500-171819/10 IC DB624 0.2(mm) 1 12/04/2012 18:04 6J1204c.d STD4AP 500-171819/11 IC DB624 0.2(mm) 1 12/04/2012 18:27 6J1204d.d STD5AP 500-171819/12 IC DB624 0.2(mm) 1 12/04/2012 18:49 6J1204e.d STD6AP 500-171819/13 IC DB624 0.2(mm) 1 12/04/2012 19:13 6J1204f.d ICV 500-171819/15 DB624 0.2(mm) 1 12/04/2012 19:58 6S1204.d



### 8260B 

## 01/09/2013 Page 203 of 384

### Lab Name: Job No.: SDG No.: Instrument ID: Analysis Batch Number: GC/MS VOA ANALYSIS RUN LOG

DILUTION FACTOR COLUMN ID DATE ANALYZED LAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID 

### TestAmerica Chicago 500-53491-1

CMS06 173973 Start Date: End Date:12/27/2012 13:59 12/27/2012 08:48

BFB 500-173973/1 DB624 0.2(mm) 1 12/27/2012 08:48 6B1227.d CCV 500-173973/3 DB624 0.2(mm) 1 12/27/2012 09:47 6C1227.d CCV 500-173973/4 DB624 0.2(mm) 1 12/27/2012 10:10 6D1227.d MB 500-173973/5 DB624 0.2(mm) 1 12/27/2012 10:33 6M1227.d LCS 500-173973/6 DB624 0.2(mm) 1 12/27/2012 10:56 6S1227.d LCSD 500-173973/7 DB624 0.2(mm) 1 12/27/2012 11:19 6T1227.d ZZZZZ DB624 0.2(mm) 1 12/27/2012 11:42 ZZZZZ DB624 0.2(mm) 1 12/27/2012 12:04 500-53491-3 FC DISCRETE 6 DB624 0.2(mm) 1 12/27/2012 13:36 3491-03.d 500-53491-4 FC D DISCRETE 6 DB624 0.2(mm) 1 12/27/2012 13:59 3491-04.d



### 8260B 

## 01/09/2013 Page 204 of 384

### Lab Name: Job No.: SDG No.: Instrument ID: Analysis Batch Number: GC/MS VOA ANALYSIS RUN LOG

DILUTION FACTOR COLUMN ID DATE ANALYZED LAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID 

### TestAmerica Chicago 500-53491-1

CMS18 170445 Start Date: End Date:11/20/2012 23:15 11/20/2012 15:22

BFB 500-170445/21 DB624 0.2(mm) 1 11/20/2012 15:22 18B1120a.D STD1 500-170445/2 IC DB624 0.2(mm) 1 11/20/2012 15:57 18I1120a.D STD2 500-170445/3 IC DB624 0.2(mm) 1 11/20/2012 16:21 18I1120b.D STD3 500-170445/4 IC DB624 0.2(mm) 1 11/20/2012 16:46 18I1120c.D STD4 500-170445/5 IC DB624 0.2(mm) 1 11/20/2012 17:10 18I1120d.D STD5 500-170445/6 IC DB624 0.2(mm) 1 11/20/2012 17:35 18I1120e.D STD6 500-170445/7 ICIS DB624 0.2(mm) 1 11/20/2012 17:59 18I1120f.D STD7 500-170445/8 IC DB624 0.2(mm) 1 11/20/2012 18:23 18I1120g.D STD8 500-170445/9 IC DB624 0.2(mm) 1 11/20/2012 18:47 18I1120h.D STD9 500-170445/10 IC DB624 0.2(mm) 1 11/20/2012 19:11 18I1120i.D STD2AP 500-170445/11 IC DB624 0.2(mm) 1 11/20/2012 19:35 STD3AP 500-170445/12 IC DB624 0.2(mm) 1 11/20/2012 19:59 STD4AP 500-170445/13 IC DB624 0.2(mm) 1 11/20/2012 20:24 STD5AP 500-170445/14 IC DB624 0.2(mm) 1 11/20/2012 20:48 STD6AP 500-170445/15 IC DB624 0.2(mm) 1 11/20/2012 21:13 STD7AP 500-170445/16 IC DB624 0.2(mm) 1 11/20/2012 21:37 STD8AP 500-170445/17 IC DB624 0.2(mm) 1 11/20/2012 22:01 STD9AP 500-170445/18 IC DB624 0.2(mm) 1 11/20/2012 22:26 ICV 500-170445/20 DB624 0.2(mm) 1 11/20/2012 23:15 18S1120.D



### 8260B 

## 01/09/2013 Page 205 of 384

### Lab Name: Job No.: SDG No.: Instrument ID: Analysis Batch Number: GC/MS VOA ANALYSIS RUN LOG

DILUTION FACTOR COLUMN ID DATE ANALYZED LAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID 

### TestAmerica Chicago 500-53491-1

CMS18 174064 Start Date: End Date:12/28/2012 11:31 12/28/2012 08:39

BFB 500-174064/7 DB624 0.2(mm) 1 12/28/2012 08:39 18B1228a.D CCV 500-174064/2 DB624 0.2(mm) 1 12/28/2012 09:14 18C1228.D CCV 500-174064/3 DB624 0.2(mm) 1 12/28/2012 09:37 18D1228.D LCS 500-174064/4 DB624 0.2(mm) 1 12/28/2012 10:00 18S1228.D MB 500-174064/6 DB624 0.2(mm) 1 12/28/2012 10:45 18M1228.D 500-53491-3 DL FC DISCRETE 6 DL DB624 0.2(mm) 50 12/28/2012 11:08 53491-03.D 500-53491-4 DL FC D DISCRETE 6 DL DB624 0.2(mm) 50 12/28/2012 11:31 53491-04.D



### 8260B 

## 01/09/2013 Page 206 of 384

### Lab Name: Job No.: SDG No.: Instrument ID: Analysis Batch Number: GC/MS VOA ANALYSIS RUN LOG

DILUTION FACTOR COLUMN ID DATE ANALYZED LAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID 

### TestAmerica Chicago 500-53491-1

CMS22 172615 Start Date: End Date:12/12/2012 00:17 12/11/2012 13:45

BFB 500-172615/1 DB624 0.2(mm) 1 12/11/2012 13:45 22B1211.D STD01 500-172615/2 IC DB624 0.2(mm) 1 12/11/2012 14:23 22I1211A.D STD02 500-172615/3 IC DB624 0.2(mm) 1 12/11/2012 14:51 22I1211B.D STD03 500-172615/4 IC DB624 0.2(mm) 1 12/11/2012 15:20 22I1211C.D STD04 500-172615/5 IC DB624 0.2(mm) 1 12/11/2012 15:48 22I1211D.D STD05 500-172615/6 IC DB624 0.2(mm) 1 12/11/2012 16:16 22I1211E.D STD06 500-172615/7 ICIS DB624 0.2(mm) 1 12/11/2012 16:44 22I1211F.D STD07 500-172615/8 IC DB624 0.2(mm) 1 12/11/2012 17:13 22I1211G.D STD08 500-172615/9 IC DB624 0.2(mm) 1 12/11/2012 17:41 22I1211H.D STD09 500-172615/10 IC DB624 0.2(mm) 1 12/11/2012 18:09 22I1211I.D STD02AP 500-172615/12 IC DB624 0.2(mm) 1 12/11/2012 19:06 STD05AP 500-172615/15 IC DB624 0.2(mm) 1 12/11/2012 20:30 STD06AP 500-172615/16 IC DB624 0.2(mm) 1 12/11/2012 20:59 STD07AP 500-172615/17 IC DB624 0.2(mm) 1 12/11/2012 21:27 STD08AP 500-172615/18 IC DB624 0.2(mm) 1 12/11/2012 21:55 STD09AP 500-172615/19 IC DB624 0.2(mm) 1 12/11/2012 22:24 STD03AP 500-172615/21 IC DB624 0.2(mm) 1 12/11/2012 23:20 STD04AP 500-172615/22 IC DB624 0.2(mm) 1 12/11/2012 23:48 ICV 500-172615/23 DB624 0.2(mm) 1 12/12/2012 00:17 22S1211.D



### 8260B 

## 01/09/2013 Page 207 of 384

### Lab Name: Job No.: SDG No.: Instrument ID: Analysis Batch Number: GC/MS VOA ANALYSIS RUN LOG

DILUTION FACTOR COLUMN ID DATE ANALYZED LAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID 

### TestAmerica Chicago 500-53491-1

CMS22 173987 Start Date: End Date:12/27/2012 22:00 12/27/2012 11:16

BFB 500-173987/1 DB624 0.2(mm) 1 12/27/2012 11:16 22B1227.D CCV 500-173987/2 DB624 0.2(mm) 1 12/27/2012 11:55 22C1227.D CCV 500-173987/3 DB624 0.2(mm) 1 12/27/2012 12:22 22D1227.D LCS 500-173987/4 DB624 0.2(mm) 1 12/27/2012 12:46 22S1227.D MB 500-173987/7 DB624 0.2(mm) 1 12/27/2012 14:10 22M1227.D ZZZZZ DB624 0.2(mm) 1 12/27/2012 15:02 500-53491-6 TRIP BLANK DB624 0.2(mm) 1 12/27/2012 15:28 53491-06.D 500-53491-5 FC EB 6 DB624 0.2(mm) 1 12/27/2012 15:54 53491-05.D ZZZZZ DB624 0.2(mm) 1 12/27/2012 16:21 ZZZZZ DB624 0.2(mm) 1 12/27/2012 16:47 ZZZZZ DB624 0.2(mm) 1 12/27/2012 17:13 ZZZZZ DB624 0.2(mm) 1 12/27/2012 17:39 ZZZZZ DB624 0.2(mm) 1 12/27/2012 21:34 ZZZZZ DB624 0.2(mm) 1 12/27/2012 22:00



### 8260B 

## 01/09/2013 Page 208 of 384

### Lab Name: Job No.: SDG No.: GC/MS VOA BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Estes, William R 12/27/12 10:28 173990 Batch Method: TestAmerica Chicago

5030B Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount AnalysisComment FC DISCRETE 6 5 g 5 mL MeOH from soil jar 500-53491-A-3 5030B, 8260B T FC D DISCRETE 6 5 g 5 mL MeOH from soil jar 500-53491-A-4 5030B, 8260B T

Batch Notes Balance ID C-0133 Methanol Lot Number DH247 Pipette ID C-2207
Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 8260B 

## 01/09/2013 Page 209 of 384

# 01/09/2013 Page 210 of 384

# 01/09/2013 Page 211 of 384

# METALS

01/09/2013 Page 212 of 384

### COVER PAGE

Lab Name: Job Number:

Client Sample ID Lab Sample ID METALS

Project:John Deere Des Moines Works (JDDMW) SDG No.: 500-53491-1 TestAmerica Chicago

500-53491-1 FC COMPOSITE 6 500-53491-2 FC D COMPOSITE 6 500-53491-5 FC EB 6

Comments:



## 01/09/2013 Page 213 of 384

### 1A-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53491-1

Date Received: 12/22/2012 11:30 500-53491-1 FC COMPOSITE 6

Solid 12/19/2012 14:30 Date Sampled: Reporting Basis: DRY 

### METALS

TestAmerica Chicago

% Solids: 26.5

CAS No. Analyte C Units Q Method RL MDL DIL Result
7440-39-3 Barium 643 mg/Kg 3.70 0.440 1 6010B 7440-50-8 Copper 748 mg/Kg 3.70 1.00 1 6010B 7440-47-3 Chromium 15000 mg/Kg 3.70 0.618 1 6010B 7440-02-0 Nickel 85.5 mg/Kg 3.70 0.810 1 6010B 7439-92-1 Lead 253 mg/Kg B 1.85 0.636 1 6010B 7440-62-2 Vanadium 253 mg/Kg 1.85 0.281 1 6010B 7440-66-6 Zinc 501 mg/Kg 7.40 2.54 1 6010B 7439-97-6 Mercury 0.232 mg/Kg 0.0605 0.0231 1 7471A



### FORM IA-IN 

## 01/09/2013 Page 214 of 384

### 1A-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53491-1

Date Received: 12/22/2012 11:30 500-53491-1 FC COMPOSITE 6

Solid 12/19/2012 14:30 Date Sampled: Reporting Basis: WET 

### METALS - TCLP

TestAmerica Chicago

CAS No. Analyte C Units Q Method RL MDL DIL Result
7440-39-3 Barium 0.0103 J mg/L 0.500 0.0100 1 6010B 7440-50-8 Copper 0.442 mg/L 0.0250 0.0100 1 6010B 7440-47-3 Chromium 0.826 mg/L 0.0250 0.0100 1 6010B 7440-02-0 Nickel 0.744 mg/L 0.0250 0.0100 1 6010B 7439-92-1 Lead <0.0500 mg/L 0.0500 0.00500 1 6010B 7440-62-2 Vanadium 0.0164 J mg/L 0.0250 0.00500 1 6010B 7440-66-6 Zinc 0.403 mg/L 0.100 0.0200 1 6010B 7439-97-6 Mercury 0.000702 mg/L B 0.000200 0.000020 0 1 7470A



### FORM IA-IN 

## 01/09/2013 Page 215 of 384

### 1A-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53491-2

Date Received: 12/22/2012 11:30 500-53491-1 FC D COMPOSITE 6

Solid 12/19/2012 14:40 Date Sampled: Reporting Basis: DRY 

### METALS

TestAmerica Chicago

% Solids: 25.1

CAS No. Analyte C Units Q Method RL MDL DIL Result
7440-39-3 Barium 619 mg/Kg 3.84 0.457 1 6010B 7440-50-8 Copper 707 mg/Kg 3.84 1.04 1 6010B 7440-47-3 Chromium 15000 mg/Kg 3.84 0.642 1 6010B 7440-02-0 Nickel 86.1 mg/Kg 3.84 0.841 1 6010B 7439-92-1 Lead 244 mg/Kg B 1.92 0.661 1 6010B 7440-62-2 Vanadium 251 mg/Kg 1.92 0.292 1 6010B 7440-66-6 Zinc 499 mg/Kg 7.68 2.64 1 6010B 7439-97-6 Mercury 0.237 mg/Kg 0.0647 0.0247 1 7471A



### FORM IA-IN 

## 01/09/2013 Page 216 of 384

### 1A-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53491-2

Date Received: 12/22/2012 11:30 500-53491-1 FC D COMPOSITE 6

Solid 12/19/2012 14:40 Date Sampled: Reporting Basis: WET 

### METALS - TCLP

TestAmerica Chicago

CAS No. Analyte C Units Q Method RL MDL DIL Result
7440-39-3 Barium <0.500 mg/L 0.500 0.0100 1 6010B 7440-50-8 Copper 0.0547 mg/L 0.0250 0.0100 1 6010B 7440-47-3 Chromium <0.0250 mg/L 0.0250 0.0100 1 6010B 7440-02-0 Nickel 0.0624 mg/L 0.0250 0.0100 1 6010B 7439-92-1 Lead <0.0500 mg/L 0.0500 0.00500 1 6010B 7440-62-2 Vanadium <0.0250 mg/L 0.0250 0.00500 1 6010B 7440-66-6 Zinc <0.100 mg/L 0.100 0.0200 1 6010B 7439-97-6 Mercury <0.000200 mg/L 0.000200 0.000020 0 1 7470A



### FORM IA-IN 

## 01/09/2013 Page 217 of 384

### 1A-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53491-5

Date Received: 12/22/2012 11:30 500-53491-1 FC EB 6

Water 12/19/2012 14:10 Date Sampled: Reporting Basis: WET 

### METALS

TestAmerica Chicago

CAS No. Analyte C Units Q Method RL MDL DIL Result
7440-39-3 Barium <0.0100 mg/L 0.0100 0.000440 1 6010B 7440-50-8 Copper 0.00111 J mg/L 0.0100 0.00106 1 6010B 7440-47-3 Chromium <0.0100 mg/L 0.0100 0.000960 1 6010B 7440-02-0 Nickel <0.0100 mg/L 0.0100 0.00190 1 6010B 7439-92-1 Lead <0.00500 mg/L 0.00500 0.00158 1 6010B 7440-62-2 Vanadium <0.00500 mg/L 0.00500 0.000620 1 6010B 7440-66-6 Zinc <0.0200 mg/L 0.0200 0.00472 1 6010B 7439-97-6 Mercury <0.000200 mg/L 0.000200 0.000071 0 1 7470A



### FORM IA-IN 

## 01/09/2013 Page 218 of 384

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53491-1mg/L M12LICVIC_00001 M12LCCVIC_00001

Analyte ICV 500-173964/10 12/26/2012 16:24
Found C True %R 

### CCV 500-173964/15 12/26/2012 16:59 CCV 500-173964/27 12/26/2012 18:16
Found Found C C True %R True %R 

### Barium 

### 0.3991 0.4896 0.4843 0.400 0.500 0.500 100 98 97 Chromium 

### 0.4102 0.5077 0.5167 0.400 0.500 0.500 103 102 103 Copper 

### 0.4093 0.5108 0.5088 0.400 0.500 0.500 102 102 102 Lead 

### 0.4139 0.5121 0.5208 0.400 0.500 0.500 103 102 104 Nickel 

### 0.4046 0.4993 0.5044 0.400 0.500 0.500 101 100 101 Vanadium 

### 4.027 4.995 5.070 4.00 5.00 5.00 101 100 101 Zinc 

### 0.4072 0.5029 0.5246 0.400 0.500 0.500 102 101 105

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/09/2013 Page 219 of 384

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53491-1mg/L M12LICVIC_00001 M12LCCVIC_00001

Analyte CCV 500-173964/39 12/26/2012 19:37
Found C True %R 

### CCV 500-173964/51 12/26/2012 20:54 CCV 500-173964/63 12/26/2012 22:15
Found Found C C True %R True %R 

### Barium 

### 0.4757 0.4874 0.5129 0.500 0.500 0.500 95 97 103 Chromium 

### 0.5194 0.5172 0.5343 0.500 0.500 0.500 104 103 107 Copper 

### 0.5081 0.5067 0.5309 0.500 0.500 0.500 102 101 106 Lead 

### 0.5236 0.5195 0.5403 0.500 0.500 0.500 105 104 108 Nickel 

### 0.5031 0.5051 0.5244 0.500 0.500 0.500 101 101 105 Vanadium 

### 5.075 5.049 5.208 5.00 5.00 5.00 102 101 104 Zinc 

### 0.5342 0.5299 0.5454 0.500 0.500 0.500 107 106 109

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/09/2013 Page 220 of 384

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53491-1mg/L M12LICVIC_00001 M12LCCVIC_00001

Analyte CCV 500-173964/75 12/26/2012 23:32
Found C True %R 

### CCV 500-173964/82 12/27/2012 00:15
Found Found C C True %R True %R 

### Barium 

### 0.5192 0.5209 0.500 0.500 104 104 Chromium 

### 0.5336 0.5290 0.500 0.500 107 106 Copper 

### 0.5327 0.5343 0.500 0.500 107 107 Lead 

### 0.5361 0.5317 0.500 0.500 107 106 Nickel 

### 0.5255 0.5242 0.500 0.500 105 105 Vanadium 

### 5.177 5.169 5.00 5.00 104 103 Zinc 

### 0.5393 0.5327 0.500 0.500 108 107

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/09/2013 Page 221 of 384

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53491-1mg/L M12LICVIC_00001 M12LCCVIC_00001

Analyte ICV 500-173963/6 12/26/2012 14:24
Found C True %R 

### CCV 500-173963/35 12/26/2012 16:28 CCV 500-173963/47 12/26/2012 17:18
Found Found C C True %R True %R 

### Barium 

### 0.3896 0.4910 0.4911 0.400 0.500 0.500 97 98 98 Chromium 

### 0.3889 0.4853 0.4943 0.400 0.500 0.500 97 97 99 Copper 

### 0.3897 0.4894 0.4882 0.400 0.500 0.500 97 98 98 Lead 

### 0.4010 0.4968 0.5016 0.400 0.500 0.500 100 99 100 Nickel 

### 0.3983 0.4961 0.5001 0.400 0.500 0.500 100 99 100 Vanadium 

### 3.883 4.873 4.892 4.00 5.00 5.00 97 97 98 Zinc 

### 0.4066 0.5056 0.5166 0.400 0.500 0.500 102 101 103

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/09/2013 Page 222 of 384

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53491-1ug/L M11FSTKHG_00001 M11FSTKHG_00001

Analyte ICV 500-173984/7 12/27/2012 08:12
Found C True %R 

### CCV 500-173984/19 12/27/2012 08:34 CCV 500-173984/32 12/27/2012 09:01
Found Found C C True %R True %R 

### Mercury 

### 1.910 1.000 0.9660 2.00 1.00 1.00 96 100 97

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/09/2013 Page 223 of 384

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53491-1ug/L M11FSTKHG_00001 M11FSTKHG_00001

Analyte CCV 500-173984/36 12/27/2012 09:08
Found C True %R Found Found C C True %R True %R 

### Mercury 

### 0.8410 1.00 84

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/09/2013 Page 224 of 384

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53491-1ug/L M11FSTKHG_00001 M11FSTKHG_00001

Analyte ICV 500-173997/7 12/27/2012 08:35
Found C True %R 

### CCV 500-173997/19 12/27/2012 08:58 CCV 500-173997/31 12/27/2012 09:21
Found Found C C True %R True %R 

### Mercury 

### 1.942 1.035 1.052 2.00 1.00 1.00 97 103 105 J J

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/09/2013 Page 225 of 384

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53491-1ug/L M11FSTKHG_00001 M11FSTKHG_00001

Analyte CCV 500-173997/43 12/27/2012 09:43
Found C True %R 

### CCV 500-173997/54 12/27/2012 10:04
Found Found C C True %R True %R 

### Mercury 

### 1.096 1.010 1.00 1.00 110 101 J J

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/09/2013 Page 226 of 384

### 2B-IN

Lab Name: Job No.: SDG No.: 500-53491-1 CRQL CHECK STANDARD METALS

Method:6010B Instrument ID:ICP5 TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits CRI 500-173964/12

CRQL Check Standard CRQL Check Standard Source: M12LCRIIC_00001 Concentration Units: mg/L

50-150 Barium 0.0200 0.01980 99 50-150 Copper 0.0200 0.02105 105 50-150 Chromium 0.0200 0.02759 138 50-150 Nickel 0.0200 0.02154 108 50-150 Lead 0.0100 0.01108 111 50-150 Vanadium 0.0100 0.01021 102 50-150 Zinc 0.0400 0.04175 104

FORM IIB-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/09/2013 Page 227 of 384

### 2B-IN

Lab Name: Job No.: SDG No.: 500-53491-1 CRQL CHECK STANDARD METALS

Method:6010B Instrument ID:ICP6 TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits CRI 500-173963/8

CRQL Check Standard CRQL Check Standard Source: M12LCRIIC_00001 Concentration Units: mg/L

50-150 Barium 0.0200 0.01949 97 50-150 Copper 0.0200 0.01945 97 50-150 Chromium 0.0200 0.01962 98 50-150 Nickel 0.0200 0.01956 98 50-150 Lead 0.0100 0.01013 101 50-150 Vanadium 0.0100 0.009451 95 50-150 Zinc 0.0400 0.03889 97

FORM IIB-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/09/2013 Page 228 of 384

### 2B-IN

Lab Name: Job No.: SDG No.: 500-53491-1 CRQL CHECK STANDARD METALS

Method:7470A Instrument ID:HG6 TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits CRA 500-173997/9

CRQL Check Standard CRQL Check Standard Source: M12ASTKHG_00001 Concentration Units: ug/L

50-150 Mercury 0.200 <2.00 118

FORM IIB-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/09/2013 Page 229 of 384

### 2B-IN

Lab Name: Job No.: SDG No.: 500-53491-1 CRQL CHECK STANDARD METALS

Method:7471A Instrument ID:HG5 TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits CRA 500-173984/9

CRQL Check Standard CRQL Check Standard Source: M12ASTKHG_00001 Concentration Units: ug/L

50-150 Mercury 0.200 0.2080 104

FORM IIB-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/09/2013 Page 230 of 384

### Lab Name: Job No.:

Concentration Units: SDG No.: INSTRUMENT BLANKS METALS
TestAmerica Chicago 500-53491-1 mg/L

C Found C Found C Found C Found RL 

### Analyte ICB 500-173964/11 CCB 500-173964/16 CCB 500-173964/28 CCB 500-173964/40 12/26/2012 16:32 12/26/2012 17:06 12/26/2012 18:22 12/26/2012 19:43 

### 3-IN

Barium 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Chromium 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Copper 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Lead 

### <0.00500 <0.00500 <0.00500 <0.00500 0.00500 Nickel 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Vanadium 

### <0.00500 <0.00500 <0.00500 <0.00500 0.00500 Zinc 

### <0.0200 <0.0200 <0.0200 <0.0200 0.0200

FORM III-IN Italicized analytes were not requested for this sequence. 

## 01/09/2013 Page 231 of 384

### Lab Name: Job No.:

Concentration Units: SDG No.: INSTRUMENT BLANKS METALS
TestAmerica Chicago 500-53491-1 mg/L

C Found C Found C Found C Found RL 

### Analyte CCB 500-173964/52 CCB 500-173964/64 CCB 500-173964/76 CCB 500-173964/83 12/26/2012 21:00 12/26/2012 22:21 12/26/2012 23:38 12/27/2012 00:22 

### 3-IN

Barium 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Chromium 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Copper 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Lead 

### <0.00500 0.003280 <0.00500 <0.00500 0.00500 J Nickel 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Vanadium 

### <0.00500 <0.00500 <0.00500 <0.00500 0.00500 Zinc 

### <0.0200 <0.0200 <0.0200 <0.0200 0.0200

FORM III-IN Italicized analytes were not requested for this sequence. 

## 01/09/2013 Page 232 of 384

### Lab Name: Job No.:

Concentration Units: SDG No.: INSTRUMENT BLANKS METALS
TestAmerica Chicago 500-53491-1 mg/L

C Found C Found C Found C Found RL 

### Analyte ICB 500-173963/7 CCB 500-173963/36 CCB 500-173963/48 12/26/2012 14:28 12/26/2012 16:32 12/26/2012 17:21 

### 3-IN

Barium 

### <0.0100 <0.0100 <0.0100 0.0100 Chromium 

### <0.0100 <0.0100 <0.0100 0.0100 Copper 

### <0.0100 <0.0100 <0.0100 0.0100 Lead 

### <0.00500 <0.00500 <0.00500 0.00500 Nickel 

### <0.0100 <0.0100 <0.0100 0.0100 Vanadium 

### <0.00500 <0.00500 <0.00500 0.00500 Zinc 

### <0.0200 <0.0200 <0.0200 0.0200

FORM III-IN Italicized analytes were not requested for this sequence. 

## 01/09/2013 Page 233 of 384

### Lab Name: Job No.:

Concentration Units: SDG No.: INSTRUMENT BLANKS METALS
TestAmerica Chicago 500-53491-1 ug/L

C Found C Found C Found C Found RL 

### Analyte ICB 500-173984/8 CCB 500-173984/20 CCB 500-173984/33 CCB 500-173984/37 12/27/2012 08:14 12/27/2012 08:36 12/27/2012 09:03 12/27/2012 09:10 

### 3-IN

Mercury 

### <0.200 <0.200 <0.200 <0.200 0.200

FORM III-IN Italicized analytes were not requested for this sequence. 

## 01/09/2013 Page 234 of 384

### Lab Name: Job No.:

Concentration Units: SDG No.: INSTRUMENT BLANKS METALS
TestAmerica Chicago 500-53491-1 ug/L

C Found C Found C Found C Found RL 

### Analyte ICB 500-173997/8 CCB 500-173997/20 CCB 500-173997/32 CCB 500-173997/44 12/27/2012 08:37 12/27/2012 09:00 12/27/2012 09:22 12/27/2012 09:45 

### 3-IN

Mercury 

### <2.00 <0.200 <2.00 <2.00 2.00

FORM III-IN Italicized analytes were not requested for this sequence. 

## 01/09/2013 Page 235 of 384

### Lab Name: Job No.:

Concentration Units: SDG No.: INSTRUMENT BLANKS METALS
TestAmerica Chicago 500-53491-1 ug/L

C Found C Found C Found C Found RL 

### Analyte CCB 500-173997/55 12/27/2012 10:06 

### 3-IN

Mercury 

### <2.00 2.00

FORM III-IN Italicized analytes were not requested for this sequence. 

## 01/09/2013 Page 236 of 384

### Lab Name: Job No.: SDG No.: Lab Sample ID:MB 500-173849/1-A Concentration Units: mg/L

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53491-1

Instrument Code:ICP6 METHOD BLANK METALS

173963 TestAmerica Chicago

7440-39-3 Barium <0.0100 6010B 7440-50-8 Copper <0.0100 6010B 7440-47-3 Chromium <0.0100 6010B 7440-02-0 Nickel <0.0100 6010B 7439-92-1 Lead <0.00500 6010B 7440-62-2 Vanadium <0.00500 6010B 7440-66-6 Zinc <0.0200 6010B

FORM III-IN 

## 01/09/2013 Page 237 of 384

### Lab Name: Job No.: SDG No.: Lab Sample ID:MB 500-173848/1-A Concentration Units: mg/Kg

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53491-1

Instrument Code:ICP5 METHOD BLANK METALS

173964 TestAmerica Chicago

7440-39-3 Barium <1.00 6010B 7440-50-8 Copper <1.00 6010B 7440-47-3 Chromium <1.00 6010B 7440-02-0 Nickel <1.00 6010B 7439-92-1 Lead 0.1770 J 6010B 7440-62-2 Vanadium <0.500 6010B 7440-66-6 Zinc <2.00 6010B

FORM III-IN 

## 01/09/2013 Page 238 of 384

### Lab Name: Job No.: SDG No.: Lab Sample ID:LB 500-173836/1-B Concentration Units: mg/L

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53491-1

Instrument Code:ICP5 METHOD BLANK METALS - TCLP

173964 TestAmerica Chicago

7440-39-3 Barium <0.500 6010B 7440-50-8 Copper <0.0250 6010B 7440-47-3 Chromium <0.0250 6010B 7440-02-0 Nickel <0.0250 6010B 7439-92-1 Lead <0.0500 6010B 7440-62-2 Vanadium <0.0250 6010B 7440-66-6 Zinc <0.100 6010B

FORM III-IN 

## 01/09/2013 Page 239 of 384

### Lab Name: Job No.: SDG No.: Lab Sample ID:LB2 500-173838/1-B Concentration Units: mg/L

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53491-1

Instrument Code:ICP5 METHOD BLANK METALS - TCLP

173964 TestAmerica Chicago

7440-39-3 Barium <0.500 6010B 7440-50-8 Copper <0.0250 6010B 7440-47-3 Chromium <0.0250 6010B 7440-02-0 Nickel <0.0250 6010B 7439-92-1 Lead <0.0500 6010B 7440-62-2 Vanadium <0.0250 6010B 7440-66-6 Zinc <0.100 6010B

FORM III-IN 

## 01/09/2013 Page 240 of 384

### Lab Name: Job No.: SDG No.: Lab Sample ID:MB 500-173908/7-A Concentration Units: mg/L

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53491-1

Instrument Code:HG6 METHOD BLANK METALS

173997 TestAmerica Chicago

7439-97-6 Mercury <0.000200 7470A

FORM III-IN 

## 01/09/2013 Page 241 of 384

### Lab Name: Job No.: SDG No.: Lab Sample ID:MB 500-173909/7-A Concentration Units: mg/L

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53491-1

Instrument Code:HG6 METHOD BLANK METALS

173997 TestAmerica Chicago

7439-97-6 Mercury 0.00003040 J 7470A

FORM III-IN 

## 01/09/2013 Page 242 of 384

### Lab Name: Job No.: SDG No.: Lab Sample ID:LB 500-173836/1-C Concentration Units: mg/L

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53491-1

Instrument Code:HG6 METHOD BLANK METALS - TCLP

173997 TestAmerica Chicago

7439-97-6 Mercury 0.00003420 J 7470A

FORM III-IN 

## 01/09/2013 Page 243 of 384

### Lab Name: Job No.: SDG No.: Lab Sample ID:LB2 500-173838/1-C Concentration Units: mg/L

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53491-1

Instrument Code:HG6 METHOD BLANK METALS - TCLP

173997 TestAmerica Chicago

7439-97-6 Mercury 0.00003260 J 7470A

FORM III-IN 

## 01/09/2013 Page 244 of 384

### Lab Name: Job No.: SDG No.: Lab Sample ID:MB 500-173881/7-A Concentration Units: mg/Kg

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53491-1

Instrument Code:HG5 METHOD BLANK METALS

173984 TestAmerica Chicago

7439-97-6 Mercury <0.0167 7471A

FORM III-IN 

## 01/09/2013 Page 245 of 384

### 4A-IN

Lab Name: Job No.:

Instrument ID: ICS Source: Concentration Units:

Analyte True Percent Recovery Found SDG No.:

Lab File ID:

Solution A Solution A Lab Sample ID: TestAmerica Chicago 500-53491-1
ICSA 500-173964/13 P51226Bmg/L M12LISAIC_00001 ICP5 INTERFERENCE CHECK STANDARD METALS

0.0000 Barium 0.0022 Chromium -0.0010 Copper -0.0005 Lead 0.0011 Nickel 0.0031 Vanadium 0.0075 Zinc 

### 498 Aluminum 500 100 -0.0010 Antimony 0.0009 Arsenic -0.0002 Beryllium 0.0009 Boron 0.0058 Cadmium 482 Calcium 500 96 -0.0001 Cobalt 191 Iron 200 96 531 Magnesium 500 106 0.0062 Manganese 0.0074 Molybdenum -0.0059 Potassium 0.0009 Selenium 0.0123 Silicon 0.0004 Silver 0.0169 Sodium 0.0022 Strontium 0.0020 Thallium -0.0008 Tin 0.0005 Titanium 0.0058 Total Heavy Metals



### FORM IVA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/09/2013 Page 246 of 384

### 4A-IN

Lab Name: Job No.:

Instrument ID: ICS Source: Concentration Units:

Analyte True Percent Recovery Found SDG No.:

Lab File ID:

Solution AB Solution AB Lab Sample ID: TestAmerica Chicago 500-53491-1
ICSAB 500-173964/14 P51226Bmg/L M12LISBIC_00001 ICP5 INTERFERENCE CHECK STANDARD METALS

0.498 Barium 0.500 100 0.485 Chromium 0.500 97 0.554 Copper 0.500 111 0.0507 Lead 0.0500 101 0.973 Nickel 1.00 97 0.506 Vanadium 0.500 101 0.929 Zinc 1.00 93 

### 497 Aluminum 500 99 0.597 Antimony 0.600 99 0.100 Arsenic 0.100 100 0.483 Beryllium 0.500 97 0.0007 Boron 0.949 Cadmium 1.00 95 481 Calcium 500 96 0.486 Cobalt 0.500 97 192 Iron 200 96 531 Magnesium 500 106 0.506 Manganese 0.500 101 0.0063 Molybdenum -0.0087 Potassium 0.0503 Selenium 0.0500 101 0.0124 Silicon 0.217 Silver 0.200 109 0.0133 Sodium 0.0022 Strontium 0.104 Thallium 0.100 104 0.0002 Tin 0.0005 Titanium 3.94 Total Heavy Metals 4.05 97



### FORM IVA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/09/2013 Page 247 of 384

### 4A-IN

Lab Name: Job No.:

Instrument ID: ICS Source: Concentration Units:

Analyte True Percent Recovery Found SDG No.:

Lab File ID:

Solution A Solution A Lab Sample ID: TestAmerica Chicago 500-53491-1
ICSA 500-173963/9 P6122612B.asc mg/L M12LISAIC_00001 ICP6 INTERFERENCE CHECK STANDARD METALS

0.0001 Barium 0.0022 Chromium 0.0039 Copper 0.0100 Lead -0.0011 Nickel 0.0003 Vanadium -0.0017 Zinc 

### 503 Aluminum 500 101 0.0032 Antimony 0.0034 Arsenic 0.0004 Beryllium -0.0092 Bismuth -0.0007 Boron 0.0001 Cadmium 474 Calcium 500 95 -0.0027 Cobalt 191 Iron 200 95 509 Magnesium 500 102 0.0002 Manganese -0.0004 Molybdenum 0.0024 Potassium -0.0011 Selenium -0.0032 Silicon -0.0003 Silver 0.0378 Sodium 0.0022 Strontium -0.0058 Thallium 0.0015 Tin 0.0033 Titanium



### FORM IVA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/09/2013 Page 248 of 384

### 4A-IN

Lab Name: Job No.:

Instrument ID: ICS Source: Concentration Units:

Analyte True Percent Recovery Found SDG No.:

Lab File ID:

Solution AB Solution AB Lab Sample ID: TestAmerica Chicago 500-53491-1
ICSAB 500-173963/10 P6122612B.asc mg/L M12LISBIC_00001 ICP6 INTERFERENCE CHECK STANDARD METALS

0.490 Barium 0.500 98 0.456 Chromium 0.500 91 0.524 Copper 0.500 105 0.0579 Lead 0.0500 116 0.973 Nickel 1.00 97 0.473 Vanadium 0.500 95 0.986 Zinc 1.00 99 

### 499 Aluminum 500 100 0.586 Antimony 0.600 98 0.0996 Arsenic 0.100 100 0.516 Beryllium 0.500 103 -0.0099 Bismuth 0.0003 Boron 0.989 Cadmium 1.00 99 471 Calcium 500 94 0.500 Cobalt 0.500 100 189 Iron 200 95 506 Magnesium 500 101 0.464 Manganese 0.500 93 -0.0008 Molybdenum 0.0015 Potassium 0.0482 Selenium 0.0500 96 0.0007 Silicon 0.210 Silver 0.200 105 0.0388 Sodium 0.0021 Strontium 0.0851 Thallium 0.100 85 0.0053 Tin 0.0045 Titanium



### FORM IVA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/09/2013 Page 249 of 384

### MATRIX SPIKE SAMPLE RECOVERY METALS - TCLP 5A-IN

FC D COMPOSITE 6 MS Lab Name: Job No.: SDG No.: Client ID: Lab ID:500-53491-2 MS 500-53491-1

Matrix: Concentration Units: mg/L Solid TestAmerica Chicago

% Solids:
Control Limit %R Analyte SSR C Sample Result (SR) C Spike Added (SA) %R Q Method Mercury 50-150 0.0007703 <0.000200 0.00100 77 7470A SSR = Spiked Sample Result



### FORM VA - IN Calculations are performed before rounding to avoid round-off errors in calculated results.



## 01/09/2013 Page 250 of 384

### 6-IN DUPLICATES

FC D COMPOSITE 6 DU Lab Name: Job No.: SDG No.:

Matrix: Concentration Units: mg/L

Analyte Control Limit Sample (S)CDuplicate (D)C RPD Q Method 500-53491-1

Solid METALS - TCLP

% Solids for Sample: % Solids for Duplicate: Client ID: Lab ID:500-53491-2 DU TestAmerica Chicago

Mercury 0.00004470J <0.000200 0.000200 NC 7470A

FORM VI-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/09/2013 Page 251 of 384

### 7A-IN LAB CONTROL SAMPLE METALS

Lab ID:LCS 500-173849/2-A Lab Name: Job No.:500-53491-1 Sample Matrix:Water LCS Source:M12JSPKIC_00002 TestAmerica Chicago

Analyte Water(mg/L)
True Found C %R Limits Q Method Barium 2.00 1.902 95 6010B 80 120 Copper 0.250 0.2317 93 6010B 80 120 Chromium 0.200 0.1856 93 6010B 80 120 Nickel 0.500 0.4572 91 6010B 80 120 Lead 0.100 0.09439 94 6010B 80 120 Vanadium 0.500 0.4686 94 6010B 80 120 Zinc 0.500 0.4470 89 6010B 80 120

Calculations are performed before rounding to avoid round-off errors in calculated results.


### FORM VIIA - IN



## 01/09/2013 Page 252 of 384

### 7A-IN LAB CONTROL SAMPLE METALS

Lab ID:LCS 500-173872/3-A Lab Name: Job No.:500-53491-1 Sample Matrix:Water LCS Source:M12KSPKIC_00001 TestAmerica Chicago

Analyte Water(mg/L)
True Found C %R Limits Q Method Barium 2.00 1.928 96 6010B 80 120 Copper 0.250 0.2512 100 6010B 80 120 Chromium 0.200 0.2016 101 6010B 80 120 Nickel 0.500 0.4930 99 6010B 80 120 Lead 0.100 0.1042 104 6010B 80 120 Vanadium 0.500 0.4994 100 6010B 80 120 Zinc 0.500 0.5058 101 6010B 80 120

Calculations are performed before rounding to avoid round-off errors in calculated results.


### FORM VIIA - IN



## 01/09/2013 Page 253 of 384

### 7A-IN LAB CONTROL SAMPLE METALS

Lab ID:LCS 500-173848/2-A Lab Name: Job No.:500-53491-1 Sample Matrix:Solid LCS Source:M12JSPKIC_00002 TestAmerica Chicago

Analyte Solid(mg/Kg)
True Found C %R Limits Q Method Barium 200 200.1 100 6010B 80 120 Copper 25.0 25.74 103 6010B 80 120 Chromium 20.0 20.94 105 6010B 80 120 Nickel 50.0 51.09 102 6010B 80 120 Lead 10.0 10.73 107 6010B 80 120 Vanadium 50.0 51.21 102 6010B 80 120 Zinc 50.0 53.63 107 6010B 80 120

Calculations are performed before rounding to avoid round-off errors in calculated results.


### FORM VIIA - IN



## 01/09/2013 Page 254 of 384

### 7A-IN LAB CONTROL SAMPLE METALS

Lab ID:LCS 500-173908/8-A Lab Name: Job No.:500-53491-1 Sample Matrix:Water LCS Source:M11FSTKHG_00001 TestAmerica Chicago

Analyte Water(mg/L)
True Found C %R Limits Q Method Mercury 0.00200 0.002121 106 7470A 80 120

Calculations are performed before rounding to avoid round-off errors in calculated results.


### FORM VIIA - IN



## 01/09/2013 Page 255 of 384

### 7A-IN LAB CONTROL SAMPLE METALS

Lab ID:LCS 500-173909/8-A Lab Name: Job No.:500-53491-1 Sample Matrix:Water LCS Source:M11FSTKHG_00001 TestAmerica Chicago

Analyte Water(mg/L)
True Found C %R Limits Q Method Mercury 0.00200 0.002139 107 7470A 80 120

Calculations are performed before rounding to avoid round-off errors in calculated results.


### FORM VIIA - IN



## 01/09/2013 Page 256 of 384

### 7A-IN LAB CONTROL SAMPLE METALS

Lab ID:LCS 500-173881/8-A Lab Name: Job No.:500-53491-1 Sample Matrix:Solid LCS Source:M11FSTKHG_00001 TestAmerica Chicago

Analyte Solid(mg/Kg)
True Found C %R Limits Q Method Mercury 0.167 0.1600 96 7471A 80 120

Calculations are performed before rounding to avoid round-off errors in calculated results.


### FORM VIIA - IN



## 01/09/2013 Page 257 of 384

### 9-IN

Instrument ID:ICP5 500-53491-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS
TestAmerica Chicago DETECTION LIMITS

6010B MDL Date: 02/20/2012 13:20 Method: 3050B Prep Method: Analyte Wavelength/ Mass RL MDL (mg/Kg) (mg/Kg) Barium 0.119 1 Chromium 0.167 1 Copper 0.271 1 Lead 0.172 0.5 Nickel 0.219 1 Vanadium 0.0759 0.5 Zinc 0.686 2

FORM IX - IN 

## 01/09/2013 Page 258 of 384

### 9-IN

Instrument ID:ICP5 500-53491-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

6010B XMDL Date: 05/25/2006 09:03 Method: Analyte Wavelength/ Mass XRL XMDL (mg/L) (mg/L) Barium 0.005 0.01 Chromium 0.005 0.01 Copper 0.005 0.01 Lead 0.0025 0.005 Nickel 0.005 0.01 Vanadium 0.0025 0.005 Zinc 0.01 0.02

FORM IX - IN 

## 01/09/2013 Page 259 of 384

### 9-IN

Instrument ID:ICP6 500-53491-1 Job Number:

Water Matrix: SDG Number: Lab Name: METALS
TestAmerica Chicago DETECTION LIMITS

6010B MDL Date: 02/20/2012 13:03 Method: 3010A Prep Method: Analyte Wavelength/ Mass RL MDL (mg/L) (mg/L) Barium 0.00044 0.01 Chromium 0.00096 0.01 Copper 0.00106 0.01 Lead 0.00158 0.005 Nickel 0.0019 0.01 Vanadium 0.00062 0.005 Zinc 0.00472 0.02

FORM IX - IN 

## 01/09/2013 Page 260 of 384

### 9-IN

Instrument ID:ICP6 500-53491-1 Job Number:

Water Matrix: SDG Number: Lab Name: METALS
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

6010B XMDL Date: 05/25/2006 09:07 Method: Analyte Wavelength/ Mass XRL XMDL (mg/L) (mg/L) Barium 0.005 0.01 Chromium 0.005 0.01 Copper 0.005 0.01 Lead 0.0025 0.005 Nickel 0.005 0.01 Vanadium 0.0025 0.005 Zinc 0.01 0.02

FORM IX - IN 

## 01/09/2013 Page 261 of 384

### 9-IN

Instrument ID:ICP5 500-53491-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS - TCLP
TestAmerica Chicago DETECTION LIMITS

6010B MDL Date: 11/01/2005 15:36 Method: 3010A Prep Method: 1311 Leach Method: Analyte Wavelength/ Mass RL MDL (mg/L) (mg/L) Barium 0.01 0.5 Chromium 0.01 0.025 Copper 0.01 0.025 Lead 0.005 0.05 Nickel 0.01 0.025 Vanadium 0.005 0.025 Zinc 0.02 0.1

FORM IX - IN 

## 01/09/2013 Page 262 of 384

### 9-IN

Instrument ID:ICP5 500-53491-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS - TCLP
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

6010B XMDL Date: 01/28/2008 10:37 Method: Analyte Wavelength/ Mass XRL XMDL (mg/L) (mg/L) Barium 0.01 0.01 Chromium 0.01 0.01 Copper 0.01 0.01 Lead 0.005 0.005 Nickel 0.01 0.01 Vanadium 0.005 0.005 Zinc 0.02 0.02

FORM IX - IN 

## 01/09/2013 Page 263 of 384

### 9-IN

Instrument ID:HG6 500-53491-1 Job Number:

Water Matrix: SDG Number: Lab Name: METALS
TestAmerica Chicago DETECTION LIMITS

7470A MDL Date: 08/31/2012 10:08 Method: 7470A Prep Method: Analyte Wavelength/ Mass RL MDL (ug/L) (ug/L) Mercury 0.071 0.2

FORM IX - IN 

## 01/09/2013 Page 264 of 384

### 9-IN

Instrument ID:HG6 500-53491-1 Job Number:

Water Matrix: SDG Number: Lab Name: METALS
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

7470A XMDL Date: 08/31/2012 10:08 Method: Analyte Wavelength/ Mass XRL XMDL (ug/L) (ug/L) Mercury 0.071 0.2

FORM IX - IN 

## 01/09/2013 Page 265 of 384

### 9-IN

Instrument ID:HG6 500-53491-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS - TCLP
TestAmerica Chicago DETECTION LIMITS

7470A MDL Date: 11/01/2005 11:39 Method: 7470A Prep Method: 1311 Leach Method: Analyte Wavelength/ Mass RL MDL (ug/L) (ug/L) Mercury 0.2 2

FORM IX - IN 

## 01/09/2013 Page 266 of 384

### 9-IN

Instrument ID:HG6 500-53491-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS - TCLP
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

7470A XMDL Date: 09/16/2006 08:48 Method: Analyte Wavelength/ Mass XRL XMDL (ug/L) (ug/L) Mercury 1 2

FORM IX - IN 

## 01/09/2013 Page 267 of 384

### 9-IN

Instrument ID:HG5 500-53491-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS
TestAmerica Chicago DETECTION LIMITS

7471A MDL Date: 08/31/2012 10:15 Method: 7471A Prep Method: Analyte Wavelength/ Mass RL MDL (ug/Kg) (ug/Kg) Mercury 6.37 16.7

FORM IX - IN 

## 01/09/2013 Page 268 of 384

### 9-IN

Instrument ID:HG5 500-53491-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

7471A XMDL Date: 08/31/2012 10:16 Method: Analyte Wavelength/ Mass XRL XMDL (ug/L) (ug/L) Mercury 0.071 0.2

FORM IX - IN 

## 01/09/2013 Page 269 of 384

### 11-IN

Lab Name:TestAmerica Chicago Job No:500-53491-1

Instrument ID: Date:

Analyte Integ. Time (Sec.) Concentration Method LINEAR RANGES

ICP5 SDG No.:

(mg/L) 11/19/2012 14:31 METALS

Barium 206010B Copper 206010B Chromium 506010B Nickel 506010B Lead 506010B Vanadium 1006010B Zinc 206010B

FORM XI - IN 

## 01/09/2013 Page 270 of 384

### 11-IN

Lab Name:TestAmerica Chicago Job No:500-53491-1

Instrument ID: Date:

Analyte Integ. Time (Sec.) Concentration Method LINEAR RANGES

ICP6 SDG No.:

(mg/L) 11/19/2012 14:24 METALS

Barium 206010B Copper 206010B Chromium 206010B Nickel 206010B Lead 1006010B Vanadium 206010B Zinc 206010B

FORM XI - IN 

## 01/09/2013 Page 271 of 384

### 11-IN

Lab Name:TestAmerica Chicago Job No:500-53491-1

Instrument ID: Date:

Analyte Integ. Time (Sec.) Concentration Method LINEAR RANGES

HG5 SDG No.:

(ug/L) 03/01/2008 11:18 METALS

Mercury 5.07471A

FORM XI - IN 

## 01/09/2013 Page 272 of 384

### 11-IN

Lab Name:TestAmerica Chicago Job No:500-53491-1

Instrument ID: Date:

Analyte Integ. Time (Sec.) Concentration Method LINEAR RANGES

HG6 SDG No.:

(ug/L) 11/01/2010 11:39 METALS

Mercury 5.07470A

FORM XI - IN 

## 01/09/2013 Page 273 of 384

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53491-1 METALS
TestAmerica Chicago
Prep Method:3050B
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (g) (mL) 12/24/2012 15:00 173848 MB 500-173848/1-A 100 1 12/24/2012 15:00 173848 LCS 500-173848/2-A 100 1 12/24/2012 15:00 173848 500-53491-1 100 1.0213 12/24/2012 15:00 173848 500-53491-2 100 1.0382

FORM XII-IN 

## 01/09/2013 Page 274 of 384

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53491-1 METALS
TestAmerica Chicago
Prep Method:3010A
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (mL) (mL) 12/24/2012 14:30 173849 MB 500-173849/1-A 50 50 12/24/2012 14:30 173849 LCS 500-173849/2-A 50 50 12/24/2012 14:30 173849 500-53491-5 50 50

FORM XII-IN 

## 01/09/2013 Page 275 of 384

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53491-1 METALS
TestAmerica Chicago
Prep Method:3010A
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (mL) (mL) 12/26/2012 07:50 173872 LB 500-173836/1-B 50 50 12/26/2012 07:50 173872 LB2 500-173838/1-B 50 50 12/26/2012 07:50 173872 LCS 500-173872/3-A 50 50 12/26/2012 07:50 173872 500-53491-1 50 50 12/26/2012 07:50 173872 500-53491-2 50 50

FORM XII-IN 

## 01/09/2013 Page 276 of 384

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53491-1 METALS
TestAmerica Chicago
Prep Method:7471A
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (g) (mL) 12/26/2012 14:00 173881 MB 500-173881/7-A 50 0.6 12/26/2012 14:00 173881 LCS 500-173881/8-A 50 0.6 12/26/2012 14:00 173881 500-53491-1 50 0.6259 12/26/2012 14:00 173881 500-53491-2 50 0.6177

FORM XII-IN 

## 01/09/2013 Page 277 of 384

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53491-1 METALS
TestAmerica Chicago
Prep Method:7470A
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (mL) (mL) 12/26/2012 13:00 173908 MB 500-173908/7-A 25 25 12/26/2012 13:00 173908 LCS 500-173908/8-A 25 25 12/26/2012 13:00 173908 500-53491-5 25 25

FORM XII-IN 

## 01/09/2013 Page 278 of 384

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53491-1 METALS
TestAmerica Chicago
Prep Method:7470A
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (mL) (mL) 12/26/2012 13:00 173909 MB 500-173909/7-A 25 25 12/26/2012 13:00 173909 LCS 500-173909/8-A 25 25 12/26/2012 13:00 173909 LB 500-173836/1-C 25 25 12/26/2012 13:00 173909 LB2 500-173838/1-C 25 25 12/26/2012 13:00 173909 500-53491-1 25 25 12/26/2012 13:00 173909 500-53491-2 25 25 12/26/2012 13:00 173909 500-53491-2 DU 25 25 12/26/2012 13:00 173909 500-53491-2 MS 25 25

FORM XII-IN 

## 01/09/2013 Page 279 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

ICP5 12/26/2012 15:16 12/27/2012 00:22 6010B METALS

Lab Sample ID D / F Time 

### Analytes B aC rC uN iP bVZ n T y p e 15:16 ZZZZZZ 15:23 ZZZZZZ 15:29 ZZZZZZ 15:35 ZZZZZZ 15:41 ZZZZZZ 15:54 ZZZZZZ 16:00 ZZZZZZ 16:07 ZZZZZZ 16:15 ZZZZZZ 1 16:24 XXX XXXX ICV 500-173964/10 1 16:32 XXX XXXX ICB 500-173964/11 1 16:39 XXX XXXX CRI 500-173964/12 1 16:45 XXX XXXX ICSA 500-173964/13 1 16:51 XXX XXXX ICSAB 500-173964/14 1 16:59 XXX XXXX CCV 500-173964/15 1 17:06 XXX XXXX CCB 500-173964/16 1 17:12 XXX XXXX LB 500-173836/1-B P 1 17:18 XXX XXXX LB2 500-173838/1-B P 1 17:24 XXX XXXX LCS 500-173872/3-A T 17:31 ZZZZZZ 17:37 ZZZZZZ 17:43 ZZZZZZ 17:49 ZZZZZZ 17:55 ZZZZZZ 18:01 ZZZZZZ 18:08 ZZZZZZ 1 18:16 XXX XXXX CCV 500-173964/27 1 18:22 XXX XXXX CCB 500-173964/28 18:29 ZZZZZZ 18:35 ZZZZZZ 1 18:41 XXX XXXX 500-53491-1 P 1 18:47 XXX XXXX 500-53491-2 P 18:53 ZZZZZZ 19:04 ZZZZZZ 19:10 ZZZZZZ 19:16 ZZZZZZ 19:23 ZZZZZZ 19:29 ZZZZZZ 1 19:37 XXX XXXX CCV 500-173964/39 1 19:43 XXX XXXX CCB 500-173964/40 19:50 ZZZZZZ 19:56 ZZZZZZ



### FORM XIII-IN 

## 01/09/2013 Page 280 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

ICP5 12/26/2012 15:16 12/27/2012 00:22 6010B METALS

Lab Sample ID D / F Time 

### Analytes B aC rC uN iP bVZ n T y p e 20:02 ZZZZZZ 20:08 ZZZZZZ 20:14 ZZZZZZ 20:21 ZZZZZZ 20:27 ZZZZZZ 20:33 ZZZZZZ 20:39 ZZZZZZ 20:45 ZZZZZZ 1 20:54 XXX XXXX CCV 500-173964/51 1 21:00 XXX XXXX CCB 500-173964/52 21:06 ZZZZZZ 21:13 ZZZZZZ 21:19 ZZZZZZ 21:25 ZZZZZZ 21:31 ZZZZZZ 21:37 ZZZZZZ 21:44 ZZZZZZ 1 21:54 XXX XXXX MB 500-173848/1-A T 1 22:00 XXX XXXX LCS 500-173848/2-A T 22:07 ZZZZZZ 1 22:15 XXX XXXX CCV 500-173964/63 1 22:21 XXX XXXX CCB 500-173964/64 22:28 ZZZZZZ 22:34 ZZZZZZ 22:40 ZZZZZZ 22:46 ZZZZZZ 22:53 ZZZZZZ 22:59 ZZZZZZ 23:05 ZZZZZZ 23:11 ZZZZZZ 23:17 ZZZZZZ 23:24 ZZZZZZ 1 23:32 XXX XXXX CCV 500-173964/75 1 23:38 XXX XXXX CCB 500-173964/76 23:44 ZZZZZZ 23:51 ZZZZZZ 1 23:57 XXX XXXX 500-53491-1 T 1 00:03 XXX XXXX 500-53491-2 T 00:09 ZZZZZZ 1 00:15 XXX XXXX CCV 500-173964/82 1 00:22 XXX XXXX CCB 500-173964/83



### FORM XIII-IN 

## 01/09/2013 Page 281 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

ICP5 12/26/2012 15:16 12/27/2012 00:22 6010B METALS

Prep Types P = TCLP T = Total/NA



### FORM XIII-IN 

## 01/09/2013 Page 282 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

ICP6 12/26/2012 14:04 12/26/2012 18:46 6010B METALS

Lab Sample ID D / F Time 

### Analytes B aC rC uN iP bVZ n T y p e 14:04 ZZZZZZ 14:08 ZZZZZZ 14:12 ZZZZZZ 14:16 ZZZZZZ 14:20 ZZZZZZ 1 14:24 XXX XXXX ICV 500-173963/6 1 14:28 XXX XXXX ICB 500-173963/7 1 14:32 XXX XXXX CRI 500-173963/8 1 14:36 XXX XXXX ICSA 500-173963/9 1 14:41 XXX XXXX ICSAB 500-173963/10 14:46 CCV 500-173963/11 14:50 CCB 500-173963/12 14:54 ZZZZZZ 14:58 ZZZZZZ 15:02 ZZZZZZ 15:07 ZZZZZZ 15:12 ZZZZZZ 15:17 ZZZZZZ 15:21 ZZZZZZ 15:25 ZZZZZZ 15:29 ZZZZZZ 15:33 ZZZZZZ 15:37 CCV 500-173963/23 15:41 CCB 500-173963/24 15:45 ZZZZZZ 15:49 ZZZZZZ 15:53 ZZZZZZ 15:58 ZZZZZZ 16:04 ZZZZZZ 16:08 ZZZZZZ 16:12 ZZZZZZ 16:16 ZZZZZZ 16:20 ZZZZZZ 16:24 ZZZZZZ 1 16:28 XXX XXXX CCV 500-173963/35 1 16:32 XXX XXXX CCB 500-173963/36 1 16:35 XXX XXXX MB 500-173849/1-A T 1 16:39 XXX XXXX LCS 500-173849/2-A T 16:43 ZZZZZZ 16:47 ZZZZZZ 16:51 ZZZZZZ 16:55 ZZZZZZ



### FORM XIII-IN 

## 01/09/2013 Page 283 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

ICP6 12/26/2012 14:04 12/26/2012 18:46 6010B METALS

Lab Sample ID D / F Time 

### Analytes B aC rC uN iP bVZ n T y p e 16:59 ZZZZZZ 1 17:03 XXX XXXX 500-53491-5 T 17:07 ZZZZZZ 17:13 ZZZZZZ 1 17:18 XXX XXXX CCV 500-173963/47 1 17:21 XXX XXXX CCB 500-173963/48 17:26 ZZZZZZ 17:30 ZZZZZZ 17:34 ZZZZZZ 17:38 ZZZZZZ 17:42 ZZZZZZ 17:46 ZZZZZZ 17:50 ZZZZZZ 17:54 ZZZZZZ 17:58 ZZZZZZ 18:02 ZZZZZZ 18:06 CCV 500-173963/59 18:10 CCB 500-173963/60 18:13 ZZZZZZ 18:17 ZZZZZZ 18:21 ZZZZZZ 18:25 ZZZZZZ 18:29 ZZZZZZ 18:33 ZZZZZZ 18:38 ZZZZZZ 18:42 CCV 500-173963/68 18:46 CCB 500-173963/69 Prep Types T = Total/NA



### FORM XIII-IN 

## 01/09/2013 Page 284 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

HG6 12/27/2012 08:23 12/27/2012 10:14 7470A METALS

Lab Sample ID D / F Time 

### Analytes H g T y p e 08:23 ZZZZZZ 08:25 ZZZZZZ 08:27 ZZZZZZ 08:28 ZZZZZZ 08:30 ZZZZZZ 08:32 ZZZZZZ 1 08:35 X ICV 500-173997/7 1 08:37 X ICB 500-173997/8 1 08:39 X CRA 500-173997/9 1 08:41 X MB 500-173908/7-A T 1 08:43 X LCS 500-173908/8-A T 08:45 ZZZZZZ 08:47 ZZZZZZ 08:49 ZZZZZZ 08:50 ZZZZZZ 08:53 ZZZZZZ 08:54 ZZZZZZ 08:56 ZZZZZZ 1 08:58 X CCV 500-173997/19 1 09:00 X CCB 500-173997/20 09:02 ZZZZZZ 09:04 ZZZZZZ 09:06 ZZZZZZ 09:08 ZZZZZZ 09:09 ZZZZZZ 09:11 ZZZZZZ 09:13 ZZZZZZ 09:15 ZZZZZZ 09:17 ZZZZZZ 09:19 ZZZZZZ 1 09:21 X CCV 500-173997/31 1 09:22 X CCB 500-173997/32 09:24 ZZZZZZ 1 09:26 X 500-53491-5 T 1 09:28 X MB 500-173909/7-A T 1 09:30 X LCS 500-173909/8-A T 09:32 ZZZZZZ 09:34 ZZZZZZ 09:36 ZZZZZZ 09:38 ZZZZZZ 09:40 ZZZZZZ 09:42 ZZZZZZ



### FORM XIII-IN 

## 01/09/2013 Page 285 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

HG6 12/27/2012 08:23 12/27/2012 10:14 7470A METALS

Lab Sample ID D / F Time 

### Analytes H g T y p e 1 09:43 X CCV 500-173997/43 1 09:45 X CCB 500-173997/44 09:47 ZZZZZZ 1 09:49 X LB 500-173836/1-C P 1 09:51 X LB2 500-173838/1-C P 09:53 ZZZZZZ 09:55 ZZZZZZ 1 09:57 X 500-53491-1 P 1 09:58 X 500-53491-2 P 1 10:00 X 500-53491-2 DU P 1 10:02 X 500-53491-2 MS P 1 10:04 X CCV 500-173997/54 1 10:06 X CCB 500-173997/55 10:08 ZZZZZZ 10:10 ZZZZZZ 10:12 CCV 500-173997/58 10:14 CCB 500-173997/59 Prep Types P = TCLP T = Total/NA



### FORM XIII-IN 

## 01/09/2013 Page 286 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

HG5 12/27/2012 07:59 12/27/2012 09:10 7471A METALS

Lab Sample ID D / F Time 

### Analytes H g T y p e 07:59 X STD01REP1 500-173984/1 IC 08:01 X STD02REP1 500-173984/2 IC 08:03 X STD03REP1 500-173984/3 IC 08:05 X STD04REP1 500-173984/4 IC 08:07 X STD05REP1 500-173984/5 IC 08:09 X STD06REP1 500-173984/6 IC 1 08:12 X ICV 500-173984/7 1 08:14 X ICB 500-173984/8 1 08:15 X CRA 500-173984/9 1 08:17 X MB 500-173881/7-A T 1 08:19 X LCS 500-173881/8-A T 08:21 ZZZZZZ 08:23 ZZZZZZ 08:25 ZZZZZZ 08:27 ZZZZZZ 08:28 ZZZZZZ 08:30 ZZZZZZ 08:32 ZZZZZZ 1 08:34 X CCV 500-173984/19 1 08:36 X CCB 500-173984/20 08:38 ZZZZZZ 08:40 ZZZZZZ 08:42 ZZZZZZ 08:44 ZZZZZZ 08:46 ZZZZZZ 08:48 ZZZZZZ 08:49 ZZZZZZ 08:51 ZZZZZZ 08:53 ZZZZZZ 1 08:55 X 500-53491-1 T 08:57 CCV 500-173984/31 1 09:01 X CCV 500-173984/32 1 09:03 X CCB 500-173984/33 1 09:04 X 500-53491-2 T 09:06 ZZZZZZ 1 09:08 X CCV 500-173984/36 1 09:10 X CCB 500-173984/37



### FORM XIII-IN 

## 01/09/2013 Page 287 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

HG5 12/27/2012 07:59 12/27/2012 09:10 7471A METALS

Prep Types T = Total/NA



### FORM XIII-IN 

## 01/09/2013 Page 288 of 384

### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Laird, Rebecca 12/24/12 15:30 12/24/12 15:00 173848 Batch Method: TestAmerica Chicago

3050B Lab Sample ID Client Sample IDMethod ChainBasis CalcMsg InitialAmount FinalAmount M12JSPKIC 00002 CALC NOT SET TO RUN 1 g 100 mL MB 500-173848/1 3050B, 6010B CALC NOT SET TO RUN 1 g 100 mL 1 mL LCS 500-173848/2 3050B, 6010B FC COMPOSITE 6 CALC NOT SET TO RUN 1.0213 g 100 mL 500-53491-A-1 3050B, 6010B T FC D COMPOSITE 6 CALC NOT SET TO RUN 1.0382 g 100 mL 500-53491-A-2 3050B, 6010B T

Batch Notes Analyst BL Balance ID C-1966 First End time 1530 Hydrogen peroxide lot number L08A06 Lot # of hydrochloric acid 0000013500 Lot # of Nitric Acid L10022 Hood ID or number 3 Hot Block ID number 8 Oven, Bath or Block Temperature 1 90 Degrees C Oven, Bath or Block Temperature 2 90 Degrees C Pipette ID 1628 First Start time 1500 ID number of the thermometer J59717 Digestion Tube/Cup Lot # MF06LKK01
Basis Basis Description T Total/NA



### Page 1 of 1 6010B 

## 01/09/2013 Page 289 of 384

### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Laird, Rebecca 12/24/12 15:00 12/24/12 14:30 173849 Batch Method: TestAmerica Chicago

3010A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount M12JSPKIC 00002 50 mL 50 mL MB 500-173849/1 3010A, 6010B 50 mL 50 mL 0.5 mL LCS 500-173849/2 3010A, 6010B FC EB 6 50 mL 50 mL 500-53491-E-5 3010A, 6010B T
Batch Notes First End time 1500 Lot # of hydrochloric acid 0000007153 Lot # of Nitric Acid L08022 Hot Block ID number 4 Pipette ID 1627 First Start time 1430 ID number of the thermometer J59688 Digestion Tube/Cup Lot # 20313760 Uncorrected Temperature 90 Celsius Uncorrected Temperature 2 90 Celsius
Basis Basis Description T Total/NA



### Page 1 of 1 6010B 

## 01/09/2013 Page 290 of 384

### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Hudson, Lawrence A 12/26/12 08:20 12/26/12 07:50 173872 Batch Method: TestAmerica Chicago

3010A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount M12KSPKIC 00001 AnalysisComment 50 mL 50 mL t757 LB 500-173836/1-A 3010A, 6010B 50 mL 50 mL t757 LB2 500-173838/1-A 3010A, 6010B 50 mL 50 mL 0.5 mL LCS 500-173872/3 3010A, 6010B FC COMPOSITE 6 50 mL 50 mL LB2 500-53491-A-1-B 3010A, 6010B P FC D COMPOSITE 6 50 mL 50 mL 500-53491-A-2-B 3010A, 6010B P
Batch Notes Batch Comment T-757 First End time 0820 Lot # of hydrochloric acid 0000013500 Lot # of Nitric Acid L10022 Hot Block ID number 4 Pipette ID 1627 First Start time 0750 ID number of the thermometer J59688 Digestion Tube/Cup Lot # 20313760 Uncorrected Temperature 90 Celsius Uncorrected Temperature 2 90 Celsius
Basis Basis Description P TCLP



### Page 1 of 1 6010B 

## 01/09/2013 Page 291 of 384

### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Bills, Brandon J 12/26/12 15:00 12/26/12 13:00 173908 Batch Method: TestAmerica Chicago

7470A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount M11FSTKHG 00001 25 mL 25 mL MB 500-173908/7 7470A, 7470A 25 mL 25 mL 0.00005 mL LCS 500-173908/8 7470A, 7470A FC EB 6 25 mL 25 mL 500-53491-E-5 7470A, 7470A T
Batch Notes Hydroxylamine Hydrochloride Lot 19333 Batch Comment STOCK ID: m10cstkhg_00001, m12astkhg_00001 (Curve) Sulfuric Acid Lot Number k20042 Lot # of hydrochloric acid 0000007153 Lot # of Nitric Acid L03021 Hood ID or number c0454 Hot Block ID number 6 Potassium Persulfate Lot Number k43467 Potassium Permanganate Lot Number k35621 NaCL Lot # UF30BZEMS Oven, Bath or Block Temperature 1 88 Oven, Bath or Block Temperature 2 88 Pipette ID 2240 Repittetor Volume Check OK Stannous Chloride Lot Number k21597 Temperature 88 Celsius ID number of the thermometer hb305412 Digestion Tube/Cup Lot # 1207143 Uncorrected Temperature 90 Celsius Visual ck - digestate F.V. consistency OK
Basis Basis Description T Total/NA



### Page 1 of 1 7470A 

## 01/09/2013 Page 292 of 384

### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Bills, Brandon J 12/27/12 09:30 12/27/12 07:30 173909 Batch Method: TestAmerica Chicago

7470A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount M11FSTKHG 00001 M12ASTKHG 00001 25 mL 25 mL MB 500-173909/7 7470A, 7470A 25 mL 25 mL 0.00005 mL LCS 500-173909/8 7470A, 7470A 25 mL 25 mL LB 500-173836/1-A 7470A, 7470A 25 mL 25 mL LB2 500-173838/1-A 7470A, 7470A FC COMPOSITE 6 25 mL 25 mL 500-53491-A-1-B 7470A, 7470A P FC D COMPOSITE 6 25 mL 25 mL 500-53491-A-2-B 7470A, 7470A P FC D COMPOSITE 6 25 mL 25 mL 500-53491-A-2-B DU 7470A, 7470A P FC D COMPOSITE 6 25 mL 25 mL 0.000025 mL 500-53491-A-2-B MS 7470A, 7470A P



### Page 1 of 2 7470A 

## 01/09/2013 Page 293 of 384

### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Bills, Brandon J 12/27/12 09:30 12/27/12 07:30 173909 Batch Method: TestAmerica Chicago

7470A
Batch Notes Hydroxylamine Hydrochloride Lot 19333 Batch Comment STOCK ID: m10cstkhg_00001, m12astkhg_00001 (Curve) Sulfuric Acid Lot Number k20042 Lot # of hydrochloric acid 0000007153 Lot # of Nitric Acid L03021 Hood ID or number c0454 Hot Block ID number 6 Potassium Persulfate Lot Number k43467 Potassium Permanganate Lot Number k35621 NaCL Lot # UF30BZEMS Oven, Bath or Block Temperature 1 88 Oven, Bath or Block Temperature 2 88 Pipette ID 2240 Repittetor Volume Check OK Stannous Chloride Lot Number k21597 Temperature 88 Celsius ID number of the thermometer hb305412 Digestion Tube/Cup Lot # 1207143 Uncorrected Temperature 90 Celsius Visual ck - digestate F.V. consistency OK
Basis Basis Description P TCLP



### Page 2 of 2 7470A 

## 01/09/2013 Page 294 of 384

### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Bills, Brandon J 12/26/12 14:30 12/26/12 14:00 173881 Batch Method: TestAmerica Chicago

7471A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount M11FSTKHG 00001 0.6 g 50 mL MB 500-173881/7 7471A, 7471A 0.6 g 50 mL 0.0001 mL LCS 500-173881/8 7471A, 7471A FC COMPOSITE 6 0.6259 g 50 mL 500-53491-A-1 7471A, 7471A T FC D COMPOSITE 6 0.6177 g 50 mL 500-53491-A-2 7471A, 7471A T
Batch Notes Hydroxylamine Hydrochloride Lot 19333 Balance ID c0975 Batch Comment STOCK ID: m10cstkhg_00001, m12astkhg_00001 (Curve) Blank Soil Lot Number teflon strip_00001 Filter Lot # 21782182 Sulfuric Acid Lot Number k20042 Lot # of hydrochloric acid 0000007153 Lot # of Nitric Acid L03021 Hood ID or number c0454 Hot Block ID number 2 Potassium Persulfate Lot Number k43467 Potassium Permanganate Lot Number k35621 NaCL Lot # UF30BZEMS Oven, Bath or Block Temperature 1 90 Oven, Bath or Block Temperature 2 90 Pipette ID 1631 Repittetor Volume Check OK Stannous Chloride Lot Number k21597 Syringe Lot # 1292669 ID number of the thermometer j60025 Digestion Tube/Cup Lot # 1207143 Uncorrected Temperature 90 Celsius Uncorrected Temperature 2 90 Celsius



### Page 1 of 2 7471A 

## 01/09/2013 Page 295 of 384

### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Bills, Brandon J 12/26/12 14:30 12/26/12 14:00 173881 Batch Method: TestAmerica Chicago

7471A
Basis Basis Description T Total/NA



### Page 2 of 2 7471A 

## 01/09/2013 Page 296 of 384

# GENERAL CHEMISTRY

01/09/2013 Page 297 of 384

### COVER PAGE

Lab Name: Job Number:

Client Sample ID Lab Sample ID GENERAL CHEMISTRY

Project:John Deere Des Moines Works (JDDMW) SDG No.: 500-53491-1 TestAmerica Chicago

500-53491-1 FC COMPOSITE 6 500-53491-2 FC D COMPOSITE 6 500-53491-3 FC DISCRETE 6 500-53491-4 FC D DISCRETE 6 500-53491-5 FC EB 6

Comments:



## 01/09/2013 Page 298 of 384

### 1B-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53491-1

Date Received: 12/22/2012 11:30 500-53491-1 FC COMPOSITE 6

Solid 12/19/2012 14:30 Date Sampled: Reporting Basis: DRY 

### GENERAL CHEMISTRY

TestAmerica Chicago

% Solids: 26.5

CAS No. Analyte C Units Q Method RL MDL DIL Result
18540-29-9 Chromium, hexavalent <3.75 mg/Kg 3.75 1.46 1 7196A 57-12-5 Cyanide, Total 1.15 J mg/Kg 1.88 0.622 1 9014 18496-25-8 Sulfide 778 mg/Kg 90.4 14.5 1 9034 HEM (Oil & Grease) 16600 mg/Kg 1850 822 1 9071B



### FORM IB-IN 

## 01/09/2013 Page 299 of 384

### 1B-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53491-1

Date Received: 12/22/2012 11:30 500-53491-1 FC COMPOSITE 6

Solid 12/19/2012 14:30 Date Sampled: Reporting Basis: WET 

### GENERAL CHEMISTRY

TestAmerica Chicago

CAS No. Analyte C Units Q Method RL MDL DIL Result Sulfide, Reactive <48.5 mg/Kg 48.5 3.78 1 9034 Flashpoint >176 Degrees F 40.0 40.0 1 1010 pH 9.79 SU 0.200 0.200 1 9045C % Moisture 74.0 % 0.100 0.100 1 SM 2540G Total Solids 26.0 % 0.100 0.100 1 SM 2540G



### FORM IB-IN 

## 01/09/2013 Page 300 of 384

### 1B-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53491-2

Date Received: 12/22/2012 11:30 500-53491-1 FC D COMPOSITE 6

Solid 12/19/2012 14:40 Date Sampled: Reporting Basis: DRY 

### GENERAL CHEMISTRY

TestAmerica Chicago

% Solids: 25.1

CAS No. Analyte C Units Q Method RL MDL DIL Result
18540-29-9 Chromium, hexavalent <3.99 mg/Kg 3.99 1.55 1 7196A 57-12-5 Cyanide, Total 1.29 J mg/Kg 1.86 0.615 1 9014 18496-25-8 Sulfide 817 mg/Kg 94.0 15.0 1 9034 HEM (Oil & Grease) 17000 mg/Kg 1950 866 1 9071B



### FORM IB-IN 

## 01/09/2013 Page 301 of 384

### 1B-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53491-2

Date Received: 12/22/2012 11:30 500-53491-1 FC D COMPOSITE 6

Solid 12/19/2012 14:40 Date Sampled: Reporting Basis: WET 

### GENERAL CHEMISTRY

TestAmerica Chicago

CAS No. Analyte C Units Q Method RL MDL DIL Result Sulfide, Reactive <49.3 mg/Kg 49.3 3.85 1 9034 Flashpoint >176 Degrees F 40.0 40.0 1 1010 pH 9.87 SU 0.200 0.200 1 9045C % Moisture 75.0 % 0.100 0.100 1 SM 2540G Total Solids 25.0 % 0.100 0.100 1 SM 2540G



### FORM IB-IN 

## 01/09/2013 Page 302 of 384

### 1B-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53491-5

Date Received: 12/22/2012 11:30 500-53491-1 FC EB 6

Water 12/19/2012 14:10 Date Sampled: Reporting Basis: WET 

### GENERAL CHEMISTRY

TestAmerica Chicago

CAS No. Analyte C Units Q Method RL MDL DIL Result
18540-29-9 Chromium, hexavalent <0.0100 mg/L H 0.0100 0.00325 1 7196A 57-12-5 Cyanide, Total <0.0100 mg/L 0.0100 0.00331 1 9014 Sulfide, Reactive <1.00 mg/L 1.00 1.00 1 9034 HEM (Oil & Grease) <5.33 mg/L 5.33 1.55 1 1664A 18496-25-8 Sulfide <1.00 mg/L 1.00 0.230 1 9034



### FORM IB-IN 

## 01/09/2013 Page 303 of 384

### 2-IN

Lab Name: Job No.: SDG No.: 500-53491-1
Analyst:APW Batch Start Date: 12/22/2012 Reporting Units:mg/L Analytical Batch No.: 173793 CALIBRATION QUALITY CONTROL GENERAL CHEMISTRY

Sample NumberQC Type Time Analyte Result Spike Amount(%) Recovery Limits Qual Reagent 

### TestAmerica Chicago

ICV 14:10 Chromium, hexavalent 0.2586 0.250 103 90-110 WSTCR2_00008 1ICB 14:10 Chromium, hexavalent <0.0100 2CCV 14:14 Chromium, hexavalent 0.4955 0.500 99 90-110 WSTCR1_00008 9CCB 14:14 Chromium, hexavalent <0.0100 10



### FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/09/2013 Page 304 of 384

### 2-IN

Lab Name: Job No.: SDG No.: 500-53491-1
Analyst:APW Batch Start Date: 12/27/2012 Reporting Units:mg/L Analytical Batch No.: 174027 CALIBRATION QUALITY CONTROL GENERAL CHEMISTRY

Sample NumberQC Type Time Analyte Result Spike Amount(%) Recovery Limits Qual Reagent 

### TestAmerica Chicago

ICV 12:40 Chromium, hexavalent 0.2548 0.250 102 90-110 WSTCR2_00008 1ICB 12:40 Chromium, hexavalent <0.0200 2CCV 12:46 Chromium, hexavalent 0.5130 0.500 103 90-110 WSTCR1_00008 10CCB 12:46 Chromium, hexavalent <0.0200 11CCV 12:51 Chromium, hexavalent 0.5138 0.500 103 90-110 WSTCR1_00008 18CCB 12:52 Chromium, hexavalent <0.0200 19CCV 12:57 Chromium, hexavalent 0.5169 0.500 103 90-110 WSTCR1_00008 27CCB 12:58 Chromium, hexavalent <0.0200 28



### FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/09/2013 Page 305 of 384

### 2-IN

Lab Name: Job No.: SDG No.: 500-53491-1
Analyst:EAT Batch Start Date: 12/27/2012 Reporting Units:mg/L Analytical Batch No.: 174042 CALIBRATION QUALITY CONTROL GENERAL CHEMISTRY

Sample NumberQC Type Time Analyte Result Spike Amount(%) Recovery Limits Qual Reagent 

### TestAmerica Chicago

ICV 14:40 Cyanide, Total 0.1006 0.100 101 90-110 WSTINCN2_00563 1ICB 14:40 Cyanide, Total <0.0100 2CCV 14:43 Cyanide, Total 0.1942 0.200 97 90-110 WSTINCN1_00571 13CCB 14:43 Cyanide, Total <0.0100 14CCV 14:47 Cyanide, Total 0.1938 0.200 97 90-110 WSTINCN1_00571 25CCB 14:47 Cyanide, Total <0.0100 26



### FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/09/2013 Page 306 of 384

### 2-IN

Lab Name: Job No.: SDG No.: 500-53491-1
Analyst:EAT Batch Start Date: 12/28/2012 Reporting Units:mg/L Analytical Batch No.: 174173 CALIBRATION QUALITY CONTROL GENERAL CHEMISTRY

Sample NumberQC Type Time Analyte Result Spike Amount(%) Recovery Limits Qual Reagent 

### TestAmerica Chicago

ICV 15:25 Cyanide, Total 0.1017 0.100 102 90-110 WSTINCN2_00564 1ICB 15:25 Cyanide, Total <0.0100 2CCV 15:29 Cyanide, Total 0.1954 0.200 98 90-110 WSTINCN1_00572 13CCB 15:29 Cyanide, Total <0.0100 14CCV 15:33 Cyanide, Total 0.1951 0.200 98 90-110 WSTINCN1_00572 25CCB 15:33 Cyanide, Total <0.0100 26



### FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/09/2013 Page 307 of 384

### Lab Name: Job No.: SDG No.:

Method Analyte ResultQual Dil 

### 3-IN

500-53491-1

Lab Sample ID Units 

### TestAmerica Chicago METHOD BLANK GENERAL CHEMISTRY

RL
Batch ID:174564 Date:01/08/2013 11:00 174563 Date:01/08/2013 05:35 Prep Batch: <5.00 MB 500-174563/1-A 1 5.00 mg/L HEM (Oil & Grease) 1664A Batch ID:173793 Date:12/22/2012 14:11 <0.0100 MB 500-173793/3 1 0.0100 mg/L Chromium, hexavalent 7196A Batch ID:174027 Date:12/27/2012 12:41 173790 Date:12/22/2012 12:00 Prep Batch: <1.00 MB 500-173790/1-A 1 1.00 mg/Kg Chromium, hexavalent 7196A Batch ID:174042 Date:12/27/2012 14:40 173980 Date:12/27/2012 09:50 Prep Batch:<0.0100 MB 500-173980/1-A 1 0.0100 mg/L Cyanide, Total 9014 Batch ID:174173 Date:12/28/2012 15:30 174096 Date:12/28/2012 11:20 Prep Batch:<0.500 MB 500-174096/12-A 1 0.500 mg/Kg Cyanide, Total 9014 Batch ID:173845 Date:12/24/2012 13:19 173844 Date:12/24/2012 08:00 Prep Batch: <1.00 MB 500-173844/1-A 1 1.00 mg/L Sulfide, Reactive 9034 Batch ID:173846 Date:12/24/2012 13:19 <1.00 MB 500-173846/1 1 1.00 mg/L Sulfide 9034 Batch ID:174145 Date:12/28/2012 12:55 174101 Date:12/28/2012 11:35 Prep Batch: <50.0 MB 500-174101/1-A 1 50.0 mg/Kg Sulfide, Reactive 9034 Batch ID:174144 Date:12/28/2012 14:35 174100 Date:12/28/2012 12:20 Prep Batch: <25.0 MB 500-174100/1-A 1 25.0 mg/Kg Sulfide 9034 Batch ID:174372 Date:01/04/2013 09:45 174369 Date:01/04/2013 05:35 Prep Batch: <500 MB 500-174369/1-A 1 500 mg/Kg HEM (Oil & Grease) 9071B



### FORM III-IN 

## 01/09/2013 Page 308 of 384

### Lab Name: Job No.: SDG No.: Matrix:

Analyte 

### 500-53491-1

Method Lab Sample ID Result Unit Spike Amount Pct. Rec. Limits C RPD RPD Limit Q 

### Solid 5-IN MATRIX SPIKE SAMPLE RECOVERY GENERAL CHEMISTRY
TestAmerica Chicago

Batch ID:174173 Date:12/28/2012 15:32 Prep Batch:174096 Date:12/28/2012 11:20 Cyanide, Total 9014 mg/Kg 1.29 500-53491-2 J 9014 500-53491-2 MS Cyanide, Total 7.442 mg/Kg 7.50 75-125 82 Batch ID:174372 Date:01/04/2013 10:27 Prep Batch:174369 Date:01/04/2013 05:35 HEM (Oil & Grease) 9071B mg/Kg 16600 500-53491-1 9071B 500-53491-1 MS HEM (Oil & Grease) 39400 mg/Kg 14800 75-125 154 F



### FORM V-IN Note - Results and Reporting Limits have been adjusted for dry weight. Calculations are performed before rounding to avoid round-off errors in calculated results.



## 01/09/2013 Page 309 of 384

### Lab Name: Job No.: SDG No.: Matrix:

Analyte 

### 500-53491-1

Method Lab Sample ID Result Unit Spike Amount Pct. Rec. Limits C RPD RPD Limit Q 

### Water 5-IN MATRIX SPIKE SAMPLE RECOVERY GENERAL CHEMISTRY
TestAmerica Chicago

Batch ID:173793 Date:12/22/2012 14:13 Chromium, hexavalent 7196A mg/L <0.0100 500-53491-5 H 7196A 500-53491-5 MS Chromium, hexavalent 0.2660 mg/L 0.250 85-115 106



### FORM V-IN Calculations are performed before rounding to avoid round-off errors in calculated results.



## 01/09/2013 Page 310 of 384

### Lab Name: Job No.: SDG No.: Matrix:

Analyte 

### 500-53491-1

Method Lab Sample ID Result Unit Spike Amount Pct. Rec. Limits C RPD RPD Limit Q 

### Solid 5-IN MATRIX SPIKE DUPLICATE SAMPLE RECOVERY GENERAL CHEMISTRY
TestAmerica Chicago

Batch ID:174173 Date:12/28/2012 15:32 Prep Batch:174096 Date:12/28/2012 11:20 9014 500-53491-2 MSD Cyanide, Total 8.170 mg/Kg 7.44 92 75-125 9 20 Batch ID:174372 Date:01/04/2013 10:42 Prep Batch:174369 Date:01/04/2013 05:35 9071B 500-53491-1 MSD HEM (Oil & Grease) 40340 mg/Kg 14800 160 75-125 2 20 F



### FORM V-IN Note - Results and Reporting Limits have been adjusted for dry weight. Calculations are performed before rounding to avoid round-off errors in calculated results.



## 01/09/2013 Page 311 of 384

### Lab Name: Job No.: SDG No.: Matrix:

Analyte 

### 500-53491-1

Method Lab Sample ID Result Unit Spike Amount Pct. Rec. Limits C RPD RPD Limit Q 

### Water 5-IN MATRIX SPIKE DUPLICATE SAMPLE RECOVERY GENERAL CHEMISTRY
TestAmerica Chicago

Batch ID:173793 Date:12/22/2012 14:13 7196A 500-53491-5 MSD Chromium, hexavalent 0.2541 mg/L 0.250 102 85-115 5 20



### FORM V-IN Calculations are performed before rounding to avoid round-off errors in calculated results.



## 01/09/2013 Page 312 of 384

### 7A-IN

Job No.:500-53491-1 LAB CONTROL SAMPLE GENERAL CHEMISTRY

Lab Name: SDG No.:

Q RPD Limit RPD Limits Pct. Rec. Spike Amount Unit C Result Analyte Lab Sample ID Method 

### Matrix:Solid TestAmerica Chicago

Batch ID:174027 Date:12/27/2012 12:42 173790 Date:12/22/2012 12:00 Prep Batch: LCS Source: WSTCR2_00008 10.0 92 7196A LCS 500-173790/2- A Chromium, hexavalent 9.188 mg/Kg 80-120

Batch ID:174027 Date:12/27/2012 12:42 173790 Date:12/22/2012 12:00 Prep Batch: LCS Source: WSTCR13_00629 676 99 7196A LCS 500-173790/3- A Chromium, hexavalent 669.0 mg/Kg 80-120

Batch ID:174173 Date:12/28/2012 15:30 174096 Date:12/28/2012 11:20 Prep Batch: LCS Source: WSTINCN2_00564 5.00 107 9014 LCS 500-174096/13 -A Cyanide, Total 5.325 mg/Kg 80-120

Batch ID:174145 Date:12/28/2012 12:55 174101 Date:12/28/2012 11:38 Prep Batch: LCS Source: WSTSF1_00036 180 94 9034 LCS 500-174101/2- A Sulfide, Reactive 169.4 mg/Kg 80-120

Batch ID:174144 Date:12/28/2012 14:36 174100 Date:12/28/2012 12:20 Prep Batch: LCS Source: WSTSF1_00036 180 96 9034 LCS 500-174100/2- A Sulfide 173.0 mg/Kg 80-120

Batch ID:174372 Date:01/04/2013 09:59 174369 Date:01/04/2013 05:35 Prep Batch: LCS Source: 1664 HEM_00060 4000 101 9071B LCS 500-174369/2- A HEM (Oil & Grease) 4050 mg/Kg 80-120



### FORM VIIA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/09/2013 Page 313 of 384

### 7A-IN

Job No.:500-53491-1 LAB CONTROL SAMPLE GENERAL CHEMISTRY

Lab Name: SDG No.:

Q RPD Limit RPD Limits Pct. Rec. Spike Amount Unit C Result Analyte Lab Sample ID Method 

### Matrix:Water TestAmerica Chicago

Batch ID:174564 Date:01/08/2013 11:04 174563 Date:01/08/2013 05:48 Prep Batch: LCS Source: 1664 HEM_00060 40.0 80 1664A LCS 500-174563/2- A HEM (Oil & Grease) 32.00 mg/L 78-114

Batch ID:173793 Date:12/22/2012 14:11 LCS Source: WSTCR2_00008 0.250 103 7196A LCS 500-173793/4 Chromium, hexavalent 0.2575 mg/L 85-115 Batch ID:174042 Date:12/27/2012 14:40 173980 Date:12/27/2012 09:50 Prep Batch: LCS Source: WSTINCN2_00563 0.100 107 9014 LCS 500-173980/2- A Cyanide, Total 0.1066 mg/L 80-120

Batch ID:173846 Date:12/24/2012 13:20 LCS Source: WSTSF1_00036 3.60 104 9034 LCS 500-173846/2 Sulfide 3.760 mg/L 80-120 Batch ID:173845 Date:12/24/2012 13:29 173844 Date:12/24/2012 08:15 Prep Batch: LCS Source: WSTSF1_00036 3.60 105 9034 LCS 500-173844/2- A Sulfide, Reactive 3.767 mg/L 80-120



### FORM VIIA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/09/2013 Page 314 of 384

### 9-IN

Instrument ID:SPEC5 500-53491-1 Job Number:

Water Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

7196A MDL Date: 05/29/2012 10:43 Method: Analyte Wavelength/ Mass RL MDL (mg/L) (mg/L) Chromium, hexavalent 0.00325 0.01

FORM IX - IN 

## 01/09/2013 Page 315 of 384

### 9-IN

Instrument ID:SPEC5 500-53491-1 Job Number:

Water Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

7196A XMDL Date: 05/29/2012 10:44 Method: Analyte Wavelength/ Mass XRL XMDL (mg/L) (mg/L) Chromium, hexavalent 0.00325 0.01

FORM IX - IN 

## 01/09/2013 Page 316 of 384

### 9-IN

Instrument ID:SPEC5 500-53491-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

7196A MDL Date: 05/29/2012 14:44 Method: 3060A Prep Method: Analyte Wavelength/ Mass RL MDL (mg/Kg) (mg/Kg) Chromium, hexavalent 0.389 1

FORM IX - IN 

## 01/09/2013 Page 317 of 384

### 9-IN

Instrument ID:SPEC5 500-53491-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

7196A XMDL Date: 05/29/2012 10:45 Method: Analyte Wavelength/ Mass XRL XMDL (mg/L) (mg/L) Chromium, hexavalent 0.00325 0.02

FORM IX - IN 

## 01/09/2013 Page 318 of 384

### 9-IN

Instrument ID:SPEC5 500-53491-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9014 MDL Date: 06/18/2012 16:18 Method: 9010B Prep Method: Analyte Wavelength/ Mass RL MDL (mg/Kg) (mg/Kg) Cyanide, Total 0.165 0.5

FORM IX - IN 

## 01/09/2013 Page 319 of 384

### 9-IN

Instrument ID:SPEC5 500-53491-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

9014 XMDL Date: 06/18/2012 16:19 Method: Analyte Wavelength/ Mass XRL XMDL (mg/L) (mg/L) Cyanide, Total 0.00331 0.01

FORM IX - IN 

## 01/09/2013 Page 320 of 384

### 9-IN

Instrument ID:SPEC5 500-53491-1 Job Number:

Water Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9014 MDL Date: 06/18/2012 16:22 Method: 9010B Prep Method: Analyte Wavelength/ Mass RL MDL (mg/L) (mg/L) Cyanide, Total 0.00331 0.01

FORM IX - IN 

## 01/09/2013 Page 321 of 384

### 9-IN

Instrument ID:SPEC5 500-53491-1 Job Number:

Water Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

9014 XMDL Date: 06/18/2012 16:22 Method: Analyte Wavelength/ Mass XRL XMDL (mg/L) (mg/L) Cyanide, Total 0.00331 0.01

FORM IX - IN 

## 01/09/2013 Page 322 of 384

### 9-IN

Instrument ID:NOEQUIP 500-53491-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9034 MDL Date: 05/29/2012 16:25 Method: 7.3.4 Prep Method: Analyte Wavelength/ Mass RL MDL (mg/Kg) (mg/Kg) Sulfide, Reactive 3.9 50

FORM IX - IN 

## 01/09/2013 Page 323 of 384

### 9-IN

Instrument ID:NOEQUIP 500-53491-1 Job Number:

Water Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9034 MDL Date: 01/02/2006 09:18 Method: 7.3.4 Prep Method: Analyte Wavelength/ Mass RL MDL (mg/L) (mg/L) Sulfide, Reactive 1 1

FORM IX - IN 

## 01/09/2013 Page 324 of 384

### 9-IN

Instrument ID:FP4 500-53491-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

1010 MDL Date: 11/11/2005 10:25 Method: Analyte Wavelength/ Mass RL MDL (Degrees (Degrees F) Flashpoint 40 40

FORM IX - IN 

## 01/09/2013 Page 325 of 384

### 9-IN

Instrument ID:NoEquip 500-53491-1 Job Number:

Water Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

1664A MDL Date: 05/29/2012 15:22 Method: 1664A Prep Method: Analyte Wavelength/ Mass RL MDL (mg/L) (mg/L) HEM (Oil & Grease) 1.45 5

FORM IX - IN 

## 01/09/2013 Page 326 of 384

### 9-IN

Instrument ID:NOEQUIP 500-53491-1 Job Number:

Water Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9034 MDL Date: 05/29/2012 15:57 Method: Analyte Wavelength/ Mass RL MDL (mg/L) (mg/L) Sulfide 0.23 1

FORM IX - IN 

## 01/09/2013 Page 327 of 384

### 9-IN

Instrument ID:NOEQUIP 500-53491-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9034 MDL Date: 05/29/2012 15:59 Method: 9030B Prep Method: Analyte Wavelength/ Mass RL MDL (mg/Kg) (mg/Kg) Sulfide 4 25

FORM IX - IN 

## 01/09/2013 Page 328 of 384

### 9-IN

Instrument ID:NOEQUIP 500-53491-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9045C MDL Date: 11/01/2005 06:06 Method: Analyte Wavelength/ Mass RL MDL (SU) (SU) pH 0.2 0.2

FORM IX - IN 

## 01/09/2013 Page 329 of 384

### 9-IN

Instrument ID:NOEQUIP 500-53491-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9071B MDL Date: 05/29/2012 15:24 Method: 9071B Prep Method: Analyte Wavelength/ Mass RL MDL (mg/Kg) (mg/Kg) HEM (Oil & Grease) 222 500

FORM IX - IN 

## 01/09/2013 Page 330 of 384

### 9-IN

Instrument ID:NOEQUIP 500-53491-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

Moisture MDL Date: 11/01/2005 09:02 Method: Analyte Wavelength/ Mass RL MDL (%) (%) Percent Moisture 0.1 0.1 Percent Solids 0.1 0.1

FORM IX - IN 

## 01/09/2013 Page 331 of 384

### 9-IN

Instrument ID:NOEQUIP 500-53491-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

SM 2540G MDL Date: 11/01/2005 09:02 Method: Analyte Wavelength/ Mass RL MDL (%) (%) % Moisture 0.1 0.1 Total Solids 0.1 0.1

FORM IX - IN 

## 01/09/2013 Page 332 of 384

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53491-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:3060A
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (g) (mL) 12/22/2012 12:00 173790 MB 500-173790/1-A 100 2.5 12/22/2012 12:00 173790 LCS 500-173790/2-A 100 2.5 12/22/2012 12:00 173790 LCS 500-173790/3-A 100 2.5 12/22/2012 12:00 173790 500-53491-1 100 2.5178 12/22/2012 12:00 173790 500-53491-2 100 2.5000

FORM XII-IN 

## 01/09/2013 Page 333 of 384

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53491-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:7.3.4
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (mL) (mL) 12/24/2012 08:00 173844 MB 500-173844/1-A 250 250 12/24/2012 08:15 173844 LCS 500-173844/2-A 250 250 12/24/2012 08:45 173844 500-53491-5 250 250

FORM XII-IN 

## 01/09/2013 Page 334 of 384

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53491-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:9010B
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (mL) (mL) 12/27/2012 09:50 173980 MB 500-173980/1-A 50 50 12/27/2012 09:50 173980 LCS 500-173980/2-A 50 50 12/27/2012 09:50 173980 500-53491-5 50 50

FORM XII-IN 

## 01/09/2013 Page 335 of 384

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53491-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:9010B
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (g) (mL) 12/28/2012 11:20 174096 MB 500-174096/12-A 50 1.0000 12/28/2012 11:20 174096 LCS 500-174096/13-A 50 1.0000 12/28/2012 11:20 174096 500-53491-1 50 1.0022 12/28/2012 11:20 174096 500-53491-2 50 1.0695 12/28/2012 11:20 174096 500-53491-2 MS 50 1.0637 12/28/2012 11:20 174096 500-53491-2 MSD 50 1.0714

FORM XII-IN 

## 01/09/2013 Page 336 of 384

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53491-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:7.3.4
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (g) (mL) 12/28/2012 11:35 174101 MB 500-174101/1-A 10 10.0000 12/28/2012 11:38 174101 LCS 500-174101/2-A 10 10.0000 12/28/2012 11:57 174101 500-53491-1 10 10.3048 12/28/2012 12:01 174101 500-53491-2 10 10.1362

FORM XII-IN 

## 01/09/2013 Page 337 of 384

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53491-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:9030B
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (g) (mL) 12/28/2012 12:20 174100 MB 500-174100/1-A 10 10.0000 12/28/2012 12:20 174100 LCS 500-174100/2-A 10 10.0000 12/28/2012 12:20 174100 500-53491-1 10 10.4509 12/28/2012 12:20 174100 500-53491-2 10 10.6031

FORM XII-IN 

## 01/09/2013 Page 338 of 384

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53491-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:9071B
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (g) (mL) 01/04/2013 05:35 174369 MB 500-174369/1-A 10 10 01/04/2013 05:35 174369 LCS 500-174369/2-A 10 10 01/04/2013 05:35 174369 500-53491-1 10 10.2054 01/04/2013 05:35 174369 500-53491-1 MS 10 10.2105 01/04/2013 05:35 174369 500-53491-1 MSD 10 10.2075 01/04/2013 05:35 174369 500-53491-2 10 10.2202

FORM XII-IN 

## 01/09/2013 Page 339 of 384

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53491-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:1664A
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (mL) (mL) 01/08/2013 05:35 174563 MB 500-174563/1-A 1000 1000 01/08/2013 05:48 174563 LCS 500-174563/2-A 1000 1000 01/08/2013 06:01 174563 500-53491-5 1000 938

FORM XII-IN 

## 01/09/2013 Page 340 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

SPEC5 12/22/2012 14:10 12/22/2012 14:14 7196A GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes C r 6 T y p e 1 14:10 X ICV 500-173793/1 1 14:10 X ICB 500-173793/2 1 14:11 X MB 500-173793/3 T 1 14:11 X LCS 500-173793/4 T 14:12 ZZZZZZ 1 14:12 X 500-53491-5 T 1 14:13 X 500-53491-5 MS T 1 14:13 X 500-53491-5 MSD T 1 14:14 X CCV 500-173793/9 1 14:14 X CCB 500-173793/10 Prep Types T = Total/NA



### FORM XIII-IN 

## 01/09/2013 Page 341 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

SPEC5 12/27/2012 12:40 12/27/2012 12:59 7196A GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes C r 6 T y p e 1 12:40 X ICV 500-174027/1 1 12:40 X ICB 500-174027/2 1 12:41 X MB 500-173790/1-A T 1 12:42 X LCS 500-173790/2-A T 50 12:42 X LCS 500-173790/3-A T 12:43 ZZZZZZ 12:44 ZZZZZZ 12:44 ZZZZZZ 12:45 ZZZZZZ 1 12:46 X CCV 500-174027/10 1 12:46 X CCB 500-174027/11 12:47 ZZZZZZ 12:48 ZZZZZZ 12:48 ZZZZZZ 12:49 ZZZZZZ 12:50 ZZZZZZ 1 12:51 X 500-53491-1 T 1 12:51 X CCV 500-174027/18 1 12:52 X CCB 500-174027/19 1 12:53 X 500-53491-2 T 12:53 ZZZZZZ 12:54 ZZZZZZ 12:55 ZZZZZZ 12:55 ZZZZZZ 12:56 ZZZZZZ 12:57 ZZZZZZ 1 12:57 X CCV 500-174027/27 1 12:58 X CCB 500-174027/28 12:59 ZZZZZZ Prep Types T = Total/NA



### FORM XIII-IN 

## 01/09/2013 Page 342 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

SPEC5 12/27/2012 14:40 12/27/2012 14:49 9014 GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes C N T y p e 1 14:40 X ICV 500-174042/1 1 14:40 X ICB 500-174042/2 1 14:40 X MB 500-173980/1-A T 1 14:40 X LCS 500-173980/2-A T 14:41 ZZZZZZ 14:41 ZZZZZZ 14:41 ZZZZZZ 14:42 ZZZZZZ 14:42 ZZZZZZ 14:42 ZZZZZZ 14:42 ZZZZZZ 14:43 ZZZZZZ 1 14:43 X CCV 500-174042/13 1 14:43 X CCB 500-174042/14 14:44 ZZZZZZ 14:44 ZZZZZZ 14:44 ZZZZZZ 14:44 ZZZZZZ 14:45 ZZZZZZ 1 14:45 X 500-53491-5 T 14:45 ZZZZZZ 14:46 ZZZZZZ 14:46 ZZZZZZ 14:46 ZZZZZZ 1 14:47 X CCV 500-174042/25 1 14:47 X CCB 500-174042/26 14:47 ZZZZZZ 14:47 ZZZZZZ 14:48 ZZZZZZ 14:48 ZZZZZZ 14:48 ZZZZZZ 14:49 ZZZZZZ 14:49 CCV 500-174042/33 14:49 CCB 500-174042/34 Prep Types T = Total/NA



### FORM XIII-IN 

## 01/09/2013 Page 343 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

SPEC5 12/28/2012 15:25 12/28/2012 15:34 9014 GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes C N T y p e 1 15:25 X ICV 500-174173/1 1 15:25 X ICB 500-174173/2 15:25 ZZZZZZ 15:26 ZZZZZZ 15:26 ZZZZZZ 15:26 ZZZZZZ 15:27 ZZZZZZ 15:27 ZZZZZZ 15:27 ZZZZZZ 15:28 ZZZZZZ 15:28 ZZZZZZ 15:28 ZZZZZZ 1 15:29 X CCV 500-174173/13 1 15:29 X CCB 500-174173/14 15:29 ZZZZZZ 1 15:30 X MB 500-174096/12-A T 1 15:30 X LCS 500-174096/13-A T 15:30 ZZZZZZ 15:31 ZZZZZZ 1 15:31 X 500-53491-1 T 1 15:31 X 500-53491-2 T 1 15:32 X 500-53491-2 MS T 1 15:32 X 500-53491-2 MSD T 15:32 ZZZZZZ 1 15:33 X CCV 500-174173/25 1 15:33 X CCB 500-174173/26 15:33 ZZZZZZ 15:34 ZZZZZZ 15:34 ZZZZZZ 15:34 ZZZZZZ Prep Types T = Total/NA



### FORM XIII-IN 

## 01/09/2013 Page 344 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

NOEQUIP 12/24/2012 13:19 12/24/2012 13:51 9034 GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes S 2 R e a c T y p e 1 13:19 X MB 500-173844/1-A T 1 13:29 X LCS 500-173844/2-A T 13:40 ZZZZZZ 1 13:51 X 500-53491-5 T Prep Types T = Total/NA



### FORM XIII-IN 

## 01/09/2013 Page 345 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

NOEQUIP 12/28/2012 12:55 12/28/2012 12:59 9034 GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes S 2 R e a c T y p e 1 12:55 X MB 500-174101/1-A T 1 12:55 X LCS 500-174101/2-A T 12:56 ZZZZZZ 12:56 ZZZZZZ 12:57 ZZZZZZ 12:58 ZZZZZZ 1 12:58 X 500-53491-1 T 1 12:59 X 500-53491-2 T Prep Types T = Total/NA



### FORM XIII-IN 

## 01/09/2013 Page 346 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

FP4 01/02/2013 09:30 01/02/2013 14:58 1010 GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes F P T y p e 1 09:30 X 500-53491-1 T 1 10:52 X 500-53491-2 T 12:14 ZZZZZZ 13:36 ZZZZZZ 14:58 ZZZZZZ Prep Types T = Total/NA



### FORM XIII-IN 

## 01/09/2013 Page 347 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1
NoEquip 01/08/2013 11:00 01/08/2013 12:35 1664A GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes H E M T y p e 1 11:00 X MB 500-174563/1-A T 1 11:04 X LCS 500-174563/2-A T 1 11:08 X 500-53491-5 T 11:13 ZZZZZZ 11:17 ZZZZZZ 11:21 ZZZZZZ 11:26 ZZZZZZ 11:30 ZZZZZZ 11:34 ZZZZZZ 11:39 ZZZZZZ 11:43 ZZZZZZ 11:47 ZZZZZZ 11:52 ZZZZZZ 11:56 ZZZZZZ 12:00 ZZZZZZ 12:05 ZZZZZZ 12:09 ZZZZZZ 12:13 ZZZZZZ 12:18 ZZZZZZ 12:22 ZZZZZZ 12:26 ZZZZZZ 12:31 ZZZZZZ 12:35 ZZZZZZ Prep Types T = Total/NA



### FORM XIII-IN 

## 01/09/2013 Page 348 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

NOEQUIP 12/24/2012 13:19 12/24/2012 14:00 9034 GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes S 2 T y p e 1 13:19 X MB 500-173846/1 T 1 13:20 X LCS 500-173846/2 T 13:22 ZZZZZZ 13:24 ZZZZZZ 13:26 ZZZZZZ 13:28 ZZZZZZ 13:30 ZZZZZZ 13:32 ZZZZZZ 13:33 ZZZZZZ 13:35 ZZZZZZ 13:37 ZZZZZZ 13:39 ZZZZZZ 13:41 ZZZZZZ 13:43 ZZZZZZ 13:45 ZZZZZZ 13:47 ZZZZZZ 13:48 ZZZZZZ 13:50 ZZZZZZ 13:52 ZZZZZZ 13:54 ZZZZZZ 13:56 ZZZZZZ 13:58 ZZZZZZ 1 14:00 X 500-53491-5 T Prep Types T = Total/NA



### FORM XIII-IN 

## 01/09/2013 Page 349 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

NOEQUIP 12/28/2012 14:35 12/28/2012 14:44 9034 GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes S 2 T y p e 1 14:35 X MB 500-174100/1-A T 1 14:36 X LCS 500-174100/2-A T 14:37 ZZZZZZ 14:38 ZZZZZZ 14:39 ZZZZZZ 14:40 ZZZZZZ 14:41 ZZZZZZ 14:42 ZZZZZZ 1 14:43 X 500-53491-1 T 1 14:44 X 500-53491-2 T Prep Types T = Total/NA



### FORM XIII-IN 

## 01/09/2013 Page 350 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

NOEQUIP 12/26/2012 14:15 12/26/2012 14:27 9045C GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes p H T y p e 14:15 ZZZZZZ 14:17 ZZZZZZ 14:20 ZZZZZZ 14:22 ZZZZZZ 1 14:25 X 500-53491-1 T 1 14:27 X 500-53491-2 T Prep Types T = Total/NA



### FORM XIII-IN 

## 01/09/2013 Page 351 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

NOEQUIP 01/04/2013 09:45 01/04/2013 11:10 9071B GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes H E M T y p e 1 09:45 X MB 500-174369/1-A T 1 09:59 X LCS 500-174369/2-A T 1 10:13 X 500-53491-1 T 1 10:27 X 500-53491-1 MS T 1 10:42 X 500-53491-1 MSD T 1 10:56 X 500-53491-2 T 11:10 ZZZZZZ Prep Types T = Total/NA



### FORM XIII-IN 

## 01/09/2013 Page 352 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

NOEQUIP 12/22/2012 09:29 12/22/2012 13:24 Moisture GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes % S o lM o i s t T y p e 09:29 ZZZZZZ 09:29 ZZZZZZ 09:29 ZZZZZZ 13:24 ZZZZZZ 13:24 ZZZZZZ 13:24 ZZZZZZ 1 13:24 XX 500-53491-1 T 1 13:24 XX 500-53491-2 T 13:24 ZZZZZZ 13:24 ZZZZZZ 13:24 ZZZZZZ 13:24 ZZZZZZ 13:24 ZZZZZZ 13:24 ZZZZZZ 13:24 ZZZZZZ Prep Types T = Total/NA



### FORM XIII-IN 

## 01/09/2013 Page 353 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

NOEQUIP 12/28/2012 07:50 12/28/2012 12:33 Moisture GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes % S o lM o i s t T y p e 07:50 ZZZZZZ 07:50 ZZZZZZ 07:50 ZZZZZZ 07:50 ZZZZZZ 07:50 ZZZZZZ 07:50 ZZZZZZ 07:50 ZZZZZZ 07:50 ZZZZZZ 1 10:09 XX 500-53491-3 T 1 10:09 XX 500-53491-4 T 12:33 ZZZZZZ 12:33 ZZZZZZ 12:33 ZZZZZZ 12:33 ZZZZZZ 12:33 ZZZZZZ 12:33 ZZZZZZ 12:33 ZZZZZZ 12:33 ZZZZZZ 12:33 ZZZZZZ 12:33 ZZZZZZ 12:33 ZZZZZZ 12:33 ZZZZZZ 12:33 ZZZZZZ 12:33 ZZZZZZ 12:33 ZZZZZZ 12:33 ZZZZZZ 12:33 ZZZZZZ 12:33 ZZZZZZ 12:33 ZZZZZZ Prep Types T = Total/NA



### FORM XIII-IN 

## 01/09/2013 Page 354 of 384

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53491-1

NOEQUIP 12/27/2012 07:30 12/27/2012 07:30 SM 2540G GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes M o i s tT S T y p e 1 07:30 XX 500-53491-1 T 1 07:30 XX 500-53491-2 T Prep Types T = Total/NA



### FORM XIII-IN 

## 01/09/2013 Page 355 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Wasowicz, Andrew P 12/27/12 13:00 12/22/12 12:00 173790 Batch Method: TestAmerica Chicago

3060A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount WSTCR13 00629 WSTCR2 00008 AnalysisComment 2.5 g 100 mL MB 500-173790/1 3060A, 7196A 2.5 g 100 mL 25 uL soluble LCS 500-173790/2 3060A, 7196A 2.5 g 100 mL 100 mL soluble 0.0105 LCS 500-173790/3 3060A, 7196A FC COMPOSITE 6 2.5178 g 100 mL 500-53491-A-1 3060A, 7196A T FC D COMPOSITE 6 2.5000 g 100 mL 500-53491-A-2 3060A, 7196A T
Batch Notes Alkaline Digestion Solution Reagent ID CR6digestion_00028 Batch Comment Filter Paper Lot # 100727 First End time see above Potassium Chromate Lot # K00741 Potassium Phosphate Buffer Reagent ID Pot PO4_Buff_00002 Lead Chromate Lot # 15813PE Lead Chromate Vendor ID Lead(II)Chrom_00001 Magnesium Chloride Lot Number J14N64 (MagCl_crystal_00002) Magnesium Chloride Vendor JT Baker First Start time see above Ending Temperature 90 Celsius Starting Temperature 90 Celsius
Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 7196A 

## 01/09/2013 Page 356 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Wasowicz, Andrew P 12/22/12 14:15 12/22/12 14:10 173793 Batch Method: TestAmerica Chicago

7196A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount CalcMsg WSTCR1 00008 WSTCR2 00008 100 mL 100 mL Color Resp. is Blank 25 uL ICV 500-173793/1 7196A Color Resp. is Blank ICB 500-173793/2 7196A Color Resp. is Blank MB 500-173793/3 7196A 100 mL 100 mL Color Resp. is Blank 25 uL LCS 500-173793/4 7196A FC EB 6 Color Resp. is Blank 500-53491-F-5 7196A T FC EB 6 100 mL 100 mL Color Resp. is Blank 25 uL 500-53491-F-5 MS 7196A T FC EB 6 100 mL 100 mL Color Resp. is Blank 25 uL 500-53491-F-5 MSD 7196A T 100 mL 100 mL Color Resp. is Blank 50 uL CCV 500-173793/9 7196A Color Resp. is Blank CCB 500-173793/10 7196A

Batch Notes Batch Comment filter paper lot# 100232 Spectrophotometer Cell Path Length 540NM1CM cm Color Reagent ID Number Hexa Chrome Color Reagent-00007 First End time See Start Date/Time First Start time See Start Date/Time Sulfuric Acid Reagent ID Number H2SO4 00007
Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 7196A 

## 01/09/2013 Page 357 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Wasowicz, Andrew P 12/27/12 13:00 12/27/12 12:40 174027 Batch Method: TestAmerica Chicago

7196A Lab Sample ID Client Sample IDMethod ChainBasis FinalAmount CalcMsg WSTCR1 00008 WSTCR2 00008 100 mL Color Resp. is Blank 25 uL ICV 500-174027/1 7196A Color Resp. is Blank ICB 500-174027/2 7196A Color Resp. is Blank MB 500-173790/1-A 7196A Color Resp. is Blank LCS 500-173790/2-A 7196A Color Resp. is Blank LCS 500-173790/3-A 7196A 100 mL Color Resp. is Blank 50 uL CCV 500-174027/10 7196A Color Resp. is Blank CCB 500-174027/11 7196A FC COMPOSITE 6 Color Resp. is Blank 500-53491-A-1-A 7196A T 100 mL Color Resp. is Blank 50 uL CCV 500-174027/18 7196A Color Resp. is Blank CCB 500-174027/19 7196A FC D COMPOSITE 6 Color Resp. is Blank 500-53491-A-2-A 7196A T 100 mL Color Resp. is Blank 50 uL CCV 500-174027/27 7196A Color Resp. is Blank CCB 500-174027/28 7196A

Batch Notes Spectrophotometer Cell Path Length 540NM1CM cm Color Reagent ID Number CR+6 ColorRGT_00007 Sulfuric Acid Reagent ID Number H2SO4_00007
Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 7196A 

## 01/09/2013 Page 358 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Treadwell, Eliane A 01/03/13 11:20 12/27/12 09:50 173980 Batch Method: TestAmerica Chicago

9010B Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount SulfideCheck WSTINCN2 00563 50 mL 50 mL y MB 500-173980/1 9010B, 9014 50 mL 50 mL y 500 uL LCS 500-173980/2 9010B, 9014 FC EB 6 50 mL 50 mL y 500-53491-D-5 9010B, 9014 T
Batch Notes Bismuth Nitrate Lot # BismuthNO3_00018 Ca(OCl)2 Reagent ID Number CaCL2O2_00006 Distillation Temperature REFLUXING Degrees C KI-Starch Paper Lot # 071409 Lead Acetate Lot # 121109 Methyl Red Indicator Reagent ID Meth_Red_IN_00001 Magnesium Chloride Reagent ID Number MagChloride_00010 NaAsO2 Reagent ID Number AscorbicAcid_00003 Sodium Hydroxide Reagent ID Number 0.25N NaOH_00005 Sulfamic Acid Reagent ID Number SulfamicAcid_00022 Sulfuric Acid Reagent ID Number 50%H2SO4_00007 Zinc Acetate Buffer Reagent ID Number IO8ARCN14
Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 9014 

## 01/09/2013 Page 359 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Treadwell, Eliane A 12/27/12 14:50 12/27/12 14:40 174042 Batch Method: TestAmerica Chicago

9014 Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount WSTINCN1 00571 WSTINCN2 00563 25 mL 25 mL 250 uL ICV 500-174042/1 9014 25 mL 25 mL 500 uL CCV 500-174042/13 9014 25 mL 25 mL 500 uL CCV 500-174042/25 9014

Batch Notes Buffer Reagent ID Number SPMM Buffer_00044 Chloramine-T Reagent ID Number Chloramine-T_00002 KI-Starch Paper Lot # 110510 NaOH Lot # NaOH_00005 Sodium Hydroxide Reagent ID Number 0.25N_NaOH_00015 Pyridine-Barbituric Acid Reagent ID Pyr_BarbAcid_00022 Scrubber Solution ID NaOH_00005 Sodium Phosphate Solution ID SPMM Buffer_00044 Spectrophotometer Wavelength 578NM
Basis Basis Description

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 9014 

## 01/09/2013 Page 360 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Treadwell, Eliane A 12/28/12 12:50 12/28/12 11:20 174096 Batch Method: TestAmerica Chicago

9010B Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount SulfideCheck WSTINCN2 00564 1.0000 g 50 mL y MB 500-174096/12 9010B, 9014 1.0000 g 50 mL y 500 uL LCS 500-174096/13 9010B, 9014 FC COMPOSITE 6 1.0022 g 50 mL y 500-53491-A-1 9010B, 9014 T FC D COMPOSITE 6 1.0695 g 50 mL y 500-53491-A-2 9010B, 9014 T FC D COMPOSITE 6 1.0637 g 50 mL y 200 uL 500-53491-A-2 MS 9010B, 9014 T FC D COMPOSITE 6 1.0714 g 50 mL y 200 uL 500-53491-A-2 MSD 9010B, 9014 T

Batch Notes Bismuth Nitrate Lot # BismuthNO3_00018 Ca(OCl)2 Reagent ID Number CaCL2O2_00006 Distillation Temperature REFLUXING Degrees C KI-Starch Paper Lot # 071409 Lead Acetate Lot # 121109 Methyl Red Indicator Reagent ID Meth_Red_IN_00001 Magnesium Chloride Reagent ID Number MagChloride_00010 NaAsO2 Reagent ID Number AscorbicAcid_00003 Sodium Hydroxide Reagent ID Number 0.25N NaOH_00005 Sulfamic Acid Reagent ID Number SulfamicAcid_00022 Sulfuric Acid Reagent ID Number 50%H2SO4_00007 Zinc Acetate Buffer Reagent ID Number IO8ARCN14
Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 9014 

## 01/09/2013 Page 361 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Treadwell, Eliane A 12/28/12 15:35 12/28/12 15:25 174173 Batch Method: TestAmerica Chicago

9014 Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount WSTINCN1 00572 WSTINCN2 00564 25 mL 25 mL 250 uL ICV 500-174173/1 9014 25 mL 25 mL 500 uL CCV 500-174173/13 9014 25 mL 25 mL 500 uL CCV 500-174173/25 9014

Batch Notes Buffer Reagent ID Number SPMM Buffer_00044 Chloramine-T Reagent ID Number Chloramine-T_00002 KI-Starch Paper Lot # 110510 NaOH Lot # NaOH_00005 Sodium Hydroxide Reagent ID Number 0.25N_NaOH_00015 Pyridine-Barbituric Acid Reagent ID Pyr_BarbAcid_00022 Scrubber Solution ID NaOH_00005 Sodium Phosphate Solution ID SPMM Buffer_00044 Spectrophotometer Wavelength 578NM
Basis Basis Description

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 9014 

## 01/09/2013 Page 362 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Boyd, Cheryl L 12/24/12 09:00 12/24/12 08:00 173844 Batch Method: TestAmerica Chicago

7.3.4 Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount 250 mL 250 mL MB 500-173844/1 7.3.4, 9034 250 mL 250 mL LCS 500-173844/2 7.3.4, 9034 FC EB 6 250 mL 250 mL 500-53491-G-5 7.3.4, 9034 T
Batch Notes

Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 9034 

## 01/09/2013 Page 363 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Boyd, Cheryl L 12/24/12 14:02 12/24/12 13:19 173845 Batch Method: TestAmerica Chicago

9034 Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount IodineAmount TitrantVolume1 CalcMsg FinalAmount WSTSF1 00036 250 mL 5 mL 4.91 mL OK 250 mL MB 500-173844/1-A 9034 250 mL 5 mL 2.49 mL OK 250 mL 5 mL LCS 500-173844/2-A 9034 FC EB 6 250 mL 5 mL 5.18 mL OK 250 mL 500-53491-G-5-A 9034 T
Batch Notes Normality of Iodine Solution 0.0240 N Nominal Amount Used 250 mL Perform Calculation (0=No, 1=Yes) 1 Normality of first Titrant 0.0246 N
Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 9034 

## 01/09/2013 Page 364 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Moore, Colleen L 12/28/12 12:05 12/28/12 11:35 174101 Batch Method: TestAmerica Chicago

7.3.4 Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount WSTSF1 00036 10.0000 g 10 mL MB 500-174101/1 7.3.4, 9034 10.0000 g 10 mL 10 mL LCS 500-174101/2 7.3.4, 9034 FC COMPOSITE 6 10.3048 g 10 mL 500-53491-A-1 7.3.4, 9034 T FC D COMPOSITE 6 10.1362 g 10 mL 500-53491-A-2 7.3.4, 9034 T
Batch Notes Batch Comment Balance ID # 2489
Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 9034 

## 01/09/2013 Page 365 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Moore, Colleen L 12/28/12 13:00 12/28/12 12:55 174145 Batch Method: TestAmerica Chicago

9034 Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount IodineAmount TitrantVolume1 CalcMsg FinalAmount 10 mL 5 mL 4.68 mL OK 10 mL MB 500-174101/1-A 9034 10 mL 5 mL 0.38 mL OK 10 mL LCS 500-174101/2-A 9034 FC COMPOSITE 6 10 mL 5 mL 4.76 mL OK 10 mL 500-53491-A-1-I 9034 T FC D COMPOSITE 6 10 mL 5 mL 4.73 mL OK 10 mL 500-53491-A-2-M 9034 T
Batch Notes Normality of Iodine Solution 0.0230 N Nominal Amount Used 10 g Perform Calculation (0=No, 1=Yes) 1 Normality of first Titrant 0.0246 N
Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 9034 

## 01/09/2013 Page 366 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Wasowicz, Andrew P 01/02/13 16:20 01/02/13 09:30 174336 Batch Method: TestAmerica Chicago

1010 Lab Sample ID Client Sample IDMethod ChainBasisAnalysisComment FC COMPOSITE 6 soft clay 500-53491-A-1 1010 T FC D COMPOSITE 6 soft clay 500-53491-A-2 1010 T
Batch Notes Equipment ID HFP 339
Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 1010 

## 01/09/2013 Page 367 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Brogan, Mary T 01/08/13 10:35 01/08/13 05:35 174563 Batch Method: TestAmerica Chicago

1664A Lab Sample ID Client Sample IDMethod ChainBasis GrossWeight TareWeight InitialAmount FinalAmount 1390 g 390 g 1000 mL 1000 mL MB 500-174563/1 1664A, 1664A 1390 g 390 g 1000 mL 1000 mL LCS 500-174563/2 1664A, 1664A FC EB 6 1327 g 389 g 938 mL 1000 mL 500-53491-H-5 1664A, 1664A T
Batch Notes Batch Comment phase separating filter lot # 8293623 Concentration End Time See end date/time Concentration Start Time See start date/time Person's name who did the concentration See analyst name Disk Lot Number 47mm-1507111, pf-70610210; 90mm-150381, pf-70610210 Evaporator Temperature 50 DEG. Degrees C Extraction Analyst see analyst name Sulfuric Acid Lot Number MALG35029 Hexane Lot# HEXANES_00012 Manifold ID 1851 Methanol Lot Number Methanol_00007 Na2SO4 Lot Number Na2SO4_00006 Nominal Amount Used 1000 mL Sufficient volume for MS/MSD? NO
Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 1664A 

## 01/09/2013 Page 368 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Brogan, Mary T 01/08/13 12:40 01/08/13 11:00 174564 Batch Method: TestAmerica Chicago

1664A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount RECTUBE# ReceiverTube RecTubeWExtract

1 RecTubeWExtract 2 1000 mL 1000 mL 1 2.3114 g 2.3121 g 2.3121 g MB 500-174563/1-A 1664A 1000 mL 1000 mL 2 6.2861 g 6.3180 g 6.3181 g LCS 500-174563/2-A 1664A FC EB 6 1000 mL 1000 mL 3 2.2903 g 2.2915 g 2.2915 g 500-53491-H-5-A 1664A T Lab Sample ID Client Sample IDMethod ChainBasis WeightOne%Diff Residue Residue2 1664 HEM 00060 Pass_0.0005g 0.0007000000000 00145 g 0.0007000000000 00145 g MB 500-174563/1-A 1664A Pass_0.0005g 0.0318999999999 994 g 0.032 g 5 mL LCS 500-174563/2-A 1664A FC EB 6 Pass_0.0005g 0.0012000000000 0031 g 0.0012000000000 0031 g 500-53491-H-5-A 1664A T

Batch Notes Balance ID 1634 Calibration Check After 2nd Weighing 0.0019 / 1.0000 g Calibration Check Before 1st Weighing 0.0020 / 0.9999 g Person's name who did the concentration see analyst name Evaporator Temperature 50 Degrees C Hexane Lot# Hexanes_00012 Methanol Lot Number Methanol_00006 Na2SO4 Lot Number Na2SO4_00006 Silica Gel Lot Number Silica gel_00003 (checked in batch 157954, 7/31/12) Speedvap ID# 1564 Weight Set ID 1144 / 2495
Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 1664A 

## 01/09/2013 Page 369 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Boyd, Cheryl L 12/24/12 14:02 12/24/12 13:19 173846 Batch Method: TestAmerica Chicago

9034 Lab Sample ID Client Sample IDMethod ChainBasis TitrantVolume1 IodineAmount InitialAmount FinalAmount CalcMsg WSTSF1 00036 4.91 mL 5 mL 250 mL 250 mL OK MB 500-173846/1 9034 2.49 mL 5 mL 250 mL 250 mL OK 5 mL LCS 500-173846/2 9034 FC EB 6 5.18 mL 5 mL 250 mL 250 mL OK 500-53491-G-5 9034 T
Batch Notes First End time 14:02 Iodine Lot Number 0.25NIODINE00005 Iodine Vendor INHOUSE Normality of Iodine Solution 0.0240 N Sodium Thiosulfate Lot Number NO2S2O300008 Sodium Thiosulfate Vendor INHOUSE Nominal Amount Used 250 mL Perform Calculation (0=No, 1=Yes) 1 Starch Lot Number STARCHIND00004 Starch Vendor VWR First Start time 13:19 Sulfuric Acid Reagent ID Number 6NHCL00006 Normality of first Titrant 0.0246 N Titrant Standardization Date 11/21/12
Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 9034 

## 01/09/2013 Page 370 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Moore, Colleen L 12/28/12 13:50 12/28/12 12:20 174100 Batch Method: TestAmerica Chicago

9030B Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount WSTSF1 00036 10.0000 g 10 mL MB 500-174100/1 9030B, 9034 10.0000 g 10 mL 10 mL LCS 500-174100/2 9030B, 9034 FC COMPOSITE 6 10.4509 g 10 mL 500-53491-A-1 9030B, 9034 T FC D COMPOSITE 6 10.6031 g 10 mL 500-53491-A-2 9030B, 9034 T
Batch Notes Batch Comment BAlance ID #2489 Distillation Temperature 70 Degrees C Sodium Hydroxide Reagent ID Number 0.25N NaOH_00014 Sulfuric Acid Reagent ID Number 20% H2SO4_00003 Zinc Acetate Buffer Reagent ID Number 0.5M ZnAcetate_00005
Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 9034 

## 01/09/2013 Page 371 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Moore, Colleen L 12/28/12 14:45 12/28/12 14:35 174144 Batch Method: TestAmerica Chicago

9034 Lab Sample ID Client Sample IDMethod ChainBasis FinalAmount IodineAmount TitrantVolume1 CalcMsg 10 mL 5 mL 4.67 mL OK MB 500-174100/1-A 9034 10 mL 5 mL 0.28 mL OK LCS 500-174100/2-A 9034 FC COMPOSITE 6 10 mL 10 mL 3.88 mL OK 500-53491-A-1-H 9034 T FC D COMPOSITE 6 10 mL 10 mL 3.83 mL OK 500-53491-A-2-L 9034 T
Batch Notes HCl Concentration 6N Lot # of hydrochloric acid 6NHCL00006 Iodine Lot Number 0.25NIODINE00005 Iodine Vendor INHOUSE Normality of Iodine Solution 0.0230 N Sodium Thiosulfate Reagent ID Number NO2S2O300008 Perform Calculation (0=No, 1=Yes) 1 Starch Lot Number STARCHIND00004 Starch Vendor VWR Normality of first Titrant 0.0246 N Zinc Acetate Buffer Reagent ID Number 0.5MZNACETAT00005
Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 9034 

## 01/09/2013 Page 372 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Brogan, Mary T 01/04/13 07:40 01/04/13 05:35 174369 Batch Method: TestAmerica Chicago

9071B Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount 1664 HEM 00060 10 g 10 mL MB 500-174369/1 9071B, 9071B 10 g 10 mL 5 mL LCS 500-174369/2 9071B, 9071B FC COMPOSITE 6 10.2054 g 10 mL 500-53491-A-1 9071B, 9071B T FC COMPOSITE 6 10.2105 g 10 mL 5 mL 500-53491-A-1 MS 9071B, 9071B T FC COMPOSITE 6 10.2075 g 10 mL 5 mL 500-53491-A-1 MSD 9071B, 9071B T FC D COMPOSITE 6 10.2202 g 10 mL 500-53491-A-2 9071B, 9071B T
Batch Notes Acid used for pH adjust Lot # J23A13 Balance ID 1634 Concentration End Time See end date / time Concentration Start Time See start date / time Evaporator Temperature 50 DEG. C Filter Paper Lot Number 8293623 Hexane Lot# HEXANES_00012 Na2SO4 Lot Number Na2SO4_00006
Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 9071B 

## 01/09/2013 Page 373 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Brogan, Mary T 01/04/13 11:25 01/04/13 09:45 174372 Batch Method: TestAmerica Chicago

9071B Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount RECTUBE# ReceiverTube RecTubeWExtract

1 RecTubeWExtract 2 10 mL 10 mL 02 2.2548 g 2.2560 g 2.2558 g MB 500-174369/1-A 9071B 10 mL 10 mL 03 2.2560 g 2.2967 g 2.2965 g LCS 500-174369/2-A 9071B FC COMPOSITE 6 10 mL 10 mL 09 2.3010 g 2.3458 g 2.3458 g 500-53491-A-1-J 9071B T FC COMPOSITE 6 10 mL 10 mL 12 2.3005 g 2.4074 g 2.4070 g 500-53491-A-1-K MS 9071B T FC COMPOSITE 6 10 mL 10 mL 66 2.3495 g 2.4586 g 2.4585 g 500-53491-A-1-L MSD 9071B T FC D COMPOSITE 6 10 mL 10 mL 79 2.2391 g 2.2830 g 2.2827 g 500-53491-A-2-N 9071B T Lab Sample ID Client Sample IDMethod ChainBasis WeightOne%Diff Residue Residue2 Pass_0.0005g 0.0011999999999 9987 g 0.0009999999999 9989 g MB 500-174369/1-A 9071B Pass_0.0005g 0.0407000000000 002 g 0.0405000000000 002 g LCS 500-174369/2-A 9071B FC COMPOSITE 6 Pass_0.0005g 0.0448 g 0.0448 g 500-53491-A-1-J 9071B T FC COMPOSITE 6 Pass_0.0005g 0.1069 g 0.1065 g 500-53491-A-1-K MS 9071B T FC COMPOSITE 6 Pass_0.0005g 0.1091 g 0.109 g 500-53491-A-1-L MSD 9071B T FC D COMPOSITE 6 Pass_0.0005g 0.0438999999999 998 g 0.0436000000000 001 g 500-53491-A-2-N 9071B T

Batch Notes Balance ID 1634 Calibration Check After 2nd Weighing 0.0020 / 1.0000 Calibration Check Before 1st Weighing 0.0020 / 1.0001 Evaporator Temperature 50 Celsius Filter Paper Lot # 8293623
Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 9071B 

## 01/09/2013 Page 374 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Veldhuizen, Chris M 12/22/12 09:29 173788 Batch Method: TestAmerica Chicago

Moisture Lab Sample ID Client Sample IDMethod ChainBasis DISH# DishWeight SampleMassWet SampleMassDry FC COMPOSITE 6 7 1.27 g 11.28 g 3.92 g 500-53491-A-1 Moisture T FC D COMPOSITE 6 8 1.27 g 11.32 g 3.79 g 500-53491-A-2 Moisture T
Batch Notes Balance ID 971 No Unit Date samples were placed in the oven 12/22/12 Oven Temp when samples are put in oven 105 Degrees C Time samples were place in the oven 0935 Date samples were removed from oven 12/24/12 Oven Temp when samples removed from oven 105 Degrees C Oven ID 776 ID number of the thermometer c-1966
Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 Moisture 

## 01/09/2013 Page 375 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Veldhuizen, Chris M 12/28/12 07:50 174071 Batch Method: TestAmerica Chicago

Moisture Lab Sample ID Client Sample IDMethod ChainBasis DISH# DishWeight SampleMassWet SampleMassDry FC DISCRETE 6 9 1.28 g 11.30 g 3.88 g 500-53491-A-3 Moisture T FC D DISCRETE 6 10 1.27 g 11.33 g 4.05 g 500-53491-A-4 Moisture T
Batch Notes Balance ID 971 No Unit Date samples were placed in the oven 12/28/12 Oven Temp when samples are put in oven 105 Degrees C Time samples were place in the oven 0800 Date samples were removed from oven 12/29/12 Oven Temp when samples removed from oven 105 Degrees C Time Samples were removed from oven 0845 Oven ID 776 ID number of the thermometer c-1966
Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 Moisture 

## 01/09/2013 Page 376 of 384

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Veldhuizen, Chris M 12/27/12 07:30 173970 Batch Method: TestAmerica Chicago

SM 2540G Lab Sample ID Client Sample IDMethod ChainBasis CalcMsg FC COMPOSITE 6 Not Calculated. RunCalculation is NULL 500-53491-A-1 SM 2540G T
FC D COMPOSITE 6 Not Calculated. RunCalculation is NULL 500-53491-A-2 SM 2540G T

Batch Notes

Basis Basis Description T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for this reagent. 

### Page 1 of 1 SM 2540G 

## 01/09/2013 Page 377 of 384

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## Login Sample Receipt Checklist
Client: Project Integration, Inc Job Number: 500-53491-1 Login Number: 53491

Question Answer Comment Creator: Lunt, Jeff T List Source:TestAmerica Chicago List Number: 1



### True Radioactivity wasn't checked or is </= background as measured by a survey meter. True The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or tampered with. True Samples were received on ice. 1.3 True Cooler Temperature is acceptable

. True Cooler Temperature is recorded

. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. False Samples are received within HoldingTime

. True Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample PreservationVerified

. True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs True Containers requiring zero headspace have no headspace or bubble is <6mm (1/4"). True Multiphasic samples are not present. True Samples do not require splitting or compositing. N/A Residual Chlorine Checked.

TestAmerica Chicago 

## 01/09/2013 Page 384 of 384

# ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Chicago 2417 Bond Street University Park, IL 60484 Tel:(708)534-5200 TestAmerica Job ID: 500-53491-1 Client Project/Site: John Deere Des Moines Works (JDDMW) For: Project Integration, Inc 1097 Highway 101 South Suite D-16 Greer, South Carolina 29651 Attn: Mr. Robert Stevens
Authorized for release by: 1/9/2013 2:45:21 PM Donna Ingersoll Project Manager II donna.ingersoll@testamericainc.com

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. 

# 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15

# Table of Contents Client: Project Integration, Inc Project/Site: John Deere Des Moines Works (JDDMW) TestAmerica Job ID: 500-53491-1



## Page 2 of 36 TestAmerica Chicago 

## 1/9/2013 

# Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 

# Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2 

# Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3 

# Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4 

# Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6 

# Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7 

# Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8 

# Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14 

# QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15 

# Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .21 

# QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .22 

# Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .31 

# Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .34 

# Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .35 

# Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .36 

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