ANALYTICAL REPORT

Job Number: 500-53491-1

Job Description: John Deere Des Moines Works (JDDMW)

For:

Project Integration, Inc

1097 Highway 101 South

Suite D-16

Greer, SC 29651

Attention: Mr. Robert Stevens

_____________________________________________

Approved for release.

Donna L Ingersoll

Project Manager II

1/9/2013 2:46 PM

Donna L Ingersoll

Project Manager II

donna.ingersoll@testamericainc.com

01/09/2013

cc: Mr. David Kirby

Mr. Robert Malcomson

These test results meet all the requirements of NELAC for accredited parameters.

The Lab Certification ID# is 100201.

All questions regarding this test report should be directed to the TestAmerica Project Manager whose signature appears

on this report. All pages of this report are integral parts of the analytical data. Therefore, this report should be

reproduced only in its entirety.

Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable.

TestAmerica Laboratories, Inc.

TestAmerica Chicago 2417 Bond Street, University Park, IL 60484

Tel (708) 534-5200 Fax (708) 534-5211 www.testamericainc.com

Page 1 of 384 01/09/2013
Table of Contents

Cover Title Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Data Summaries . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Report Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Manual Integration Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Executive Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

Method / Analyst Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

Sample Datasheets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30

QC Data Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33

Data Qualifiers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58

QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59

Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 67

Reagent Traceability . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 75

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 111

Organic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 112

GC/MS VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 112

Method 8260B . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 112

Method 8260B QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 113

Method 8260B Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 135

Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 141

Method 8260B ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 141

Method 8260B CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 175

Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 196

Method 8260B Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 196

Page 2 of 384 01/09/2013
Table of Contents

Method 8260B LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 199

Method 8260B Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 203

Method 8260B Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 209

Inorganic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 212

Metals Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 212

Met Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 213

Met Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 214

Met QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 219

Met ICV/CCV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 219

Met CRQL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 227

Met Blanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 231

Met ICSA/ICSAB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 246

Met MS/MSD/PDS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 250

Met Dup/Trip . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 251

Met LCS/LCSD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 252

Met MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 258

Met Linear Ranges . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 270

Met Preparation Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 274

Met Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 280

Met Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 289

General Chemistry Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 297

Gen Chem Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 298

Gen Chem Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 299

Gen Chem QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 304

Gen Chem ICV/CCV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 304

Gen Chem Blanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 308

Page 3 of 384 01/09/2013
Table of Contents

Gen Chem MS/MSD/PDS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 309

Gen Chem LCS/LCSD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 313

Gen Chem MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 315

Gen Chem Preparation Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 333

Gen Chem Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 341

Gen Chem Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 356

Shipping and Receiving Documents . . . . . . . . . . . . . . . . . . . . . . . . . . . 378

Client Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 383

Sample Receipt Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 384

Page 4 of 384 01/09/2013
Job Narrative

500-53491-1

Comments

No additional comments. 

Receipt 

The samples were received on 12/22/2012 11:30 AM; the samples arrived in good condition, properly preserved and, where required, on 

ice. The temperature of the cooler at receipt was 1.3o C.

Except:

Cr+6 past hold time.

GC/MS VOA 

No analytical or quality issues were noted.

Metals 

No analytical or quality issues were noted.

General Chemistry 

Method(s) 9071B: The oil and grease matrix spike / matrix spike duplicate (MS/MSD) recoveries for sample 500-53491-1 in batch 174372 

were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria.

No other analytical or quality issues were noted.

Page 5 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GC/MS VOA MANUAL INTEGRATION SUMMARY

TestAmerica Chicago 500-53491-1

Instrument ID: CMS06 Analysis Batch Number: 171819

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD1 500-171819/2 IC

12/04/12 14:34 6I1204a.d GC Column: DB624 ID: 0.2(mm)

Trichloroethene 5.83 Baseline drabekd 12/04/12 15:38

Dibromochloromethane 8.17 Baseline drabekd 12/04/12 15:38

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD5 500-171819/6 IC

12/04/12 16:33 6I1204e.d GC Column: DB624 ID: 0.2(mm)

Chloroethane 1.71 Split Peak drabekd 12/05/12 07:59

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD1AP 500-171819/8 IC

12/04/12 17:18 6J1204a.d GC Column: DB624 ID: 0.2(mm)

Ethyl acetate 4.14 Split Peak drabekd 12/05/12 08:09

n-Butyl alcohol 5.82 Poor chromatography drabekd 12/05/12 08:19

2-Nitropropane 6.75 Baseline drabekd 12/05/12 08:21

trans-1,4-Dichloro-2-butene 9.94 Poor chromatography drabekd 12/05/12 08:28

Pentachloroethane 10.41 Split Peak drabekd 12/05/12 08:10

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD2AP 500-171819/9 IC

12/04/12 17:41 6J1204b.d GC Column: DB624 ID: 0.2(mm)

2-Nitropropane 6.75 Baseline drabekd 12/05/12 08:23

8260B

Page 6 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GC/MS VOA MANUAL INTEGRATION SUMMARY

TestAmerica Chicago 500-53491-1

Instrument ID: CMS22 Analysis Batch Number: 172615

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD01 500-172615/2 IC

12/11/12 14:23 22I1211A.D GC Column: DB624 ID: 0.2(mm)

Trichloroethene 7.55 Baseline alikpalae 12/11/12 19:50

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD02 500-172615/3 IC

12/11/12 14:51 22I1211B.D GC Column: DB624 ID: 0.2(mm)

Bromomethane 2.01 Baseline alikpalae 12/11/12 19:54

Acetonitrile 3.59 Split Peak alikpalae 12/11/12 19:54

Tetrachloroethene 9.75 Split Peak alikpalae 12/11/12 19:54

8260B

Page 7 of 384 01/09/2013
SAMPLE SUMMARY

Client: Project Integration, Inc Job Number: 500-53491-1

Lab Sample ID Client Sample ID Client Matrix Sampled Received

Date/Time Date/Time

500-53491-1 FC COMPOSITE 6 Solid 12/19/2012 1430 12/22/2012 1130

500-53491-2 FC D COMPOSITE 6 Solid 12/19/2012 1440 12/22/2012 1130

500-53491-3 FC DISCRETE 6 Solid 12/19/2012 1420 12/22/2012 1130

500-53491-4 FC D DISCRETE 6 Solid 12/19/2012 1445 12/22/2012 1130

500-53491-5 FC EB 6 Water 12/19/2012 1410 12/22/2012 1130

500-53491-6 TRIP BLANK Water 12/19/2012 0000 12/22/2012 1130

TestAmerica Chicago Page 8 of 384 01/09/2013
EXECUTIVE SUMMARY - Detections

Client: Project Integration, Inc Job Number: 500-53491-1

Analyte Result

Reporting 

Limit Units Method

Lab Sample ID Client Sample ID

Qualifier

500-53491-1 FC COMPOSITE 6

Barium 643 3.70 mg/Kg 6010B

Copper 748 3.70 mg/Kg 6010B

Chromium 15000 3.70 mg/Kg 6010B

Nickel 85.5 3.70 mg/Kg 6010B

Lead 253 B 1.85 mg/Kg 6010B

Vanadium 253 1.85 mg/Kg 6010B

Zinc 501 7.40 mg/Kg 6010B

Mercury 0.232 0.0605 mg/Kg 7471A

Flashpoint >176 40.0 Degrees F 1010

Cyanide, Total 1.15 J 1.88 mg/Kg 9014

Sulfide 778 90.4 mg/Kg 9034

pH 9.79 0.200 SU 9045C

HEM (Oil & Grease) 16600 1850 mg/Kg 9071B

Percent Moisture 74 0.10 % Moisture

Percent Solids 26 0.10 % Moisture

% Moisture 74.0 0.100 % SM 2540G

Total Solids 26.0 0.100 % SM 2540G

TCLP

Barium 0.0103 J 0.500 mg/L 6010B

Copper 0.442 0.0250 mg/L 6010B

Chromium 0.826 0.0250 mg/L 6010B

Nickel 0.744 0.0250 mg/L 6010B

Vanadium 0.0164 J 0.0250 mg/L 6010B

Zinc 0.403 0.100 mg/L 6010B

Mercury 0.000702 B 0.000200 mg/L 7470A

TestAmerica Chicago Page 9 of 384 01/09/2013
EXECUTIVE SUMMARY - Detections

Client: Project Integration, Inc Job Number: 500-53491-1

Analyte Result

Reporting 

Limit Units Method

Lab Sample ID Client Sample ID

Qualifier

500-53491-2 FC D COMPOSITE 6

Barium 619 3.84 mg/Kg 6010B

Copper 707 3.84 mg/Kg 6010B

Chromium 15000 3.84 mg/Kg 6010B

Nickel 86.1 3.84 mg/Kg 6010B

Lead 244 B 1.92 mg/Kg 6010B

Vanadium 251 1.92 mg/Kg 6010B

Zinc 499 7.68 mg/Kg 6010B

Mercury 0.237 0.0647 mg/Kg 7471A

Flashpoint >176 40.0 Degrees F 1010

Cyanide, Total 1.29 J 1.86 mg/Kg 9014

Sulfide 817 94.0 mg/Kg 9034

pH 9.87 0.200 SU 9045C

HEM (Oil & Grease) 17000 1950 mg/Kg 9071B

Percent Moisture 75 0.10 % Moisture

Percent Solids 25 0.10 % Moisture

% Moisture 75.0 0.100 % SM 2540G

Total Solids 25.0 0.100 % SM 2540G

TCLP

Copper 0.0547 0.0250 mg/L 6010B

Nickel 0.0624 0.0250 mg/L 6010B

500-53491-3 FC DISCRETE 6

Acetone 7020 963 ug/Kg 8260B

2-Butanone (MEK) 11.8 J 19.3 ug/Kg 8260B

Percent Moisture 74 0.10 % Moisture

Percent Solids 26 0.10 % Moisture

500-53491-4 FC D DISCRETE 6

Acetone 7150 905 ug/Kg 8260B

2-Butanone (MEK) 19.5 18.1 ug/Kg 8260B

Percent Moisture 72 0.10 % Moisture

Percent Solids 28 0.10 % Moisture

500-53491-5 FC EB 6

Copper 0.00111 J 0.0100 mg/L 6010B

TestAmerica Chicago Page 10 of 384 01/09/2013
METHOD SUMMARY

Client: Project Integration, Inc Job Number: 500-53491-1

Description Lab Location Method Preparation Method

Matrix: Solid

Volatile Organic Compounds (GC/MS) TAL CHI SW846 8260B

Purge and Trap TAL CHI SW846 5030B

Metals (ICP) TAL CHI SW846 6010B

Preparation, Metals TAL CHI SW846 3050B

Metals (ICP) TAL CHI SW846 6010B

TCLP Extraction TAL CHI SW846 1311

Preparation, Total Metals TAL CHI SW846 3010A

Mercury (CVAA) TAL CHI SW846 7470A

TCLP Extraction TAL CHI SW846 1311

Preparation, Mercury TAL CHI SW846 7470A

Mercury (CVAA) TAL CHI SW846 7471A

Preparation, Mercury TAL CHI SW846 7471A

Ignitability, Pensky-Martens Closed-Cup Method TAL CHI SW846 1010

Chromium, Hexavalent TAL CHI SW846 7196A

Alkaline Digestion (Chromium, Hexavalent) TAL CHI SW846 3060A

Cyanide TAL CHI SW846 9014

Cyanide, Distillation TAL CHI SW846 9010B

Sulfide, Acid soluble and Insoluble (Titrimetric) TAL CHI SW846 9034

Sulfide, Distillation (Acid Soluble and Insoluble) TAL CHI SW846 9030B

Sulfide, Reactive TAL CHI SW846 9034

Sulfide, Reactive TAL CHI SW846 7.3.4

pH TAL CHI SW846 9045C

HEM and SGT-HEM TAL CHI SW846 9071B

Preparation, HEM and SGT-HEM TAL CHI SW846 9071B

Percent Moisture TAL CHI EPA Moisture

Total, Fixed, and Volatile Solids TAL CHI SM SM 2540G

Matrix: Water

Volatile Organic Compounds (GC/MS) TAL CHI SW846 8260B

Purge and Trap TAL CHI SW846 5030B

Metals (ICP) TAL CHI SW846 6010B

Preparation, Total Metals TAL CHI SW846 3010A

Mercury (CVAA) TAL CHI SW846 7470A

Preparation, Mercury TAL CHI SW846 7470A

HEM and SGT-HEM TAL CHI 1664A 1664A

HEM and SGT-HEM (SPE) TAL CHI 1664A 1664A

Chromium, Hexavalent TAL CHI SW846 7196A

Cyanide TAL CHI SW846 9014

Cyanide, Distillation TAL CHI SW846 9010B

Sulfide, Acid soluble and Insoluble (Titrimetric) TAL CHI SW846 9034

Sulfide, Reactive TAL CHI SW846 9034

Sulfide, Reactive TAL CHI SW846 7.3.4

TestAmerica Chicago Page 11 of 384 01/09/2013
METHOD SUMMARY

Client: Project Integration, Inc Job Number: 500-53491-1

Description Lab Location Method Preparation Method

Lab References:

TAL CHI = TestAmerica Chicago

Method References:

1664A = EPA-821-98-002

EPA = US Environmental Protection Agency

SM = "Standard Methods For The Examination Of Water And Wastewater" SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TestAmerica Chicago Page 12 of 384 01/09/2013
METHOD / ANALYST SUMMARY

Client: Project Integration, Inc Job Number: 500-53491-1

Method Analyst Analyst ID

SW846 8260B Arndt, Brett D BDA

SW846 8260B Drabek, Dave J DJD

SW846 8260B Manzano, Louis LM

SW846 6010B Jones, Paul PJ

SW846 7470A Bills, Brandon J BJB

SW846 7471A Bills, Brandon J BJB

SW846 1010 Wasowicz, Andrew P APW

1664A 1664A Brogan, Mary T MTB

SW846 7196A Wasowicz, Andrew P APW

SW846 9014 Treadwell, Eliane A EAT

SW846 9034 Boyd, Cheryl L CLB

SW846 9034 Moore, Colleen L CLM

SW846 9045C Moore, Colleen L CLM

SW846 9071B Brogan, Mary T MTB

EPA Moisture Veldhuizen, Chris M CMV

SM SM 2540G Veldhuizen, Chris M CMV

TestAmerica Chicago

Page 13 of 384 01/09/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53491-1

Client Sample ID:

Lab Sample ID:

FC DISCRETE 6

Client Matrix: % Moisture: 74.1

500-53491-3

Solid

Date Sampled: 12/19/2012 1420

Date Received: 12/22/2012 1130

8260B Volatile Organic Compounds (GC/MS)

Dilution:

12/27/2012 1336

12/27/2012 1336

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume: Lab File ID:

Instrument ID:

3491-03.d

5 g

5 mL

5030B

CMS06

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

500-173973

N/A

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

2-Butanone (MEK) 11.8 J 6.98 19.3

Surrogate %Rec Qualifier Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 89 70 - 134

Toluene-d8 (Surr) 87 75 - 122

4-Bromofluorobenzene (Surr) 79 70 - 122

Dibromofluoromethane 95 75 - 120

TestAmerica Chicago Page 14 of 384 01/09/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53491-1

Client Sample ID:

Lab Sample ID:

FC DISCRETE 6

Client Matrix: % Moisture: 74.1

500-53491-3

Solid

Date Sampled: 12/19/2012 1420

Date Received: 12/22/2012 1130

8260B Volatile Organic Compounds (GC/MS)

Dilution:

12/27/2012 1028

12/28/2012 1108

50

8260B

Final Weight/Volume:

Initial Weight/Volume: Lab File ID:

Instrument ID:

53491-03.D

5 g

Run Type: DL 5 mL

5030B

CMS18

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

500-174064

500-173990

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

Acetone 7020 251 963

Surrogate %Rec Qualifier Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 97 75 - 125

Toluene-d8 (Surr) 96 75 - 120

4-Bromofluorobenzene (Surr) 94 75 - 120

Dibromofluoromethane 93 75 - 120

TestAmerica Chicago Page 15 of 384 01/09/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53491-1

Client Sample ID:

Lab Sample ID:

FC D DISCRETE 6

Client Matrix: % Moisture: 72.4

500-53491-4

Solid

Date Sampled: 12/19/2012 1445

Date Received: 12/22/2012 1130

8260B Volatile Organic Compounds (GC/MS)

Dilution:

12/27/2012 1359

12/27/2012 1359

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume: Lab File ID:

Instrument ID:

3491-04.d

5 g

5 mL

5030B

CMS06

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

500-173973

N/A

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

2-Butanone (MEK) 19.5 6.55 18.1

Surrogate %Rec Qualifier Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 91 70 - 134

Toluene-d8 (Surr) 89 75 - 122

4-Bromofluorobenzene (Surr) 75 70 - 122

Dibromofluoromethane 90 75 - 120

TestAmerica Chicago Page 16 of 384 01/09/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53491-1

Client Sample ID:

Lab Sample ID:

FC D DISCRETE 6

Client Matrix: % Moisture: 72.4

500-53491-4

Solid

Date Sampled: 12/19/2012 1445

Date Received: 12/22/2012 1130

8260B Volatile Organic Compounds (GC/MS)

Dilution:

12/27/2012 1028

12/28/2012 1131

50

8260B

Final Weight/Volume:

Initial Weight/Volume: Lab File ID:

Instrument ID:

53491-04.D

5 g

Run Type: DL 5 mL

5030B

CMS18

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

500-174064

500-173990

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

Acetone 7150 235 905

Surrogate %Rec Qualifier Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 105 75 - 125

Toluene-d8 (Surr) 101 75 - 120

4-Bromofluorobenzene (Surr) 100 75 - 120

Dibromofluoromethane 96 75 - 120

TestAmerica Chicago Page 17 of 384 01/09/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53491-1

Client Sample ID:

Lab Sample ID:

FC EB 6

Client Matrix:

500-53491-5

Water

Date Sampled: 12/19/2012 1410

Date Received: 12/22/2012 1130

8260B Volatile Organic Compounds (GC/MS)

Dilution:

12/27/2012 1554

12/27/2012 1554

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume: Lab File ID:

Instrument ID:

53491-05.D

5 mL

5 mL

5030B

CMS22

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

500-173987

N/A

Analysis Method:

Prep Method:

Analyte Result (ug/L) Qualifier MDL RL

Acetone <5.00 1.29 5.00

2-Butanone (MEK) <5.00 1.47 5.00

Surrogate %Rec Qualifier Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 88 75 - 125

Toluene-d8 (Surr) 94 75 - 120

4-Bromofluorobenzene (Surr) 88 75 - 120

Dibromofluoromethane 90 75 - 120

TestAmerica Chicago Page 18 of 384 01/09/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53491-1

Client Sample ID:

Lab Sample ID:

TRIP BLANK

Client Matrix:

500-53491-6

Water

Date Sampled: 12/19/2012 0000

Date Received: 12/22/2012 1130

8260B Volatile Organic Compounds (GC/MS)

Dilution:

12/27/2012 1528

12/27/2012 1528

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume: Lab File ID:

Instrument ID:

53491-06.D

5 mL

5 mL

5030B

CMS22

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

500-173987

N/A

Analysis Method:

Prep Method:

Analyte Result (ug/L) Qualifier MDL RL

Acetone <5.00 1.29 5.00

2-Butanone (MEK) <5.00 1.47 5.00

Surrogate %Rec Qualifier Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 93 75 - 125

Toluene-d8 (Surr) 100 75 - 120

4-Bromofluorobenzene (Surr) 93 75 - 120

Dibromofluoromethane 93 75 - 120

TestAmerica Chicago Page 19 of 384 01/09/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53491-1

Client Sample ID:

Lab Sample ID:

FC COMPOSITE 6

Client Matrix: % Moisture: 73.5

500-53491-1

Solid

Date Sampled: 12/19/2012 1430

Date Received: 12/22/2012 1130

6010B Metals (ICP)

6010B Instrument ID:

Lab File ID: P51226B

Dilution: 1.0 Initial Weight/Volume: 1.0213 g

12/26/2012 2357 Final Weight/Volume: 100 mL

12/24/2012 1500

3050B

ICP5

Analysis Date:

Prep Date:

Analysis Batch: 500-173964

Prep Batch: 500-173848

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL

Barium 643 0.440 3.70

Copper 748 1.00 3.70

Chromium 15000 0.618 3.70

Nickel 85.5 0.810 3.70

Lead 253 B 0.636 1.85

Vanadium 253 0.281 1.85

Zinc 501 2.54 7.40

6010B Metals (ICP)-TCLP

6010B Instrument ID:

Lab File ID: P51226B

Dilution: 1.0 Initial Weight/Volume: 50 mL

12/26/2012 1841 Final Weight/Volume: 50 mL

12/26/2012 0750

3010A

ICP5

Analysis Date:

Prep Date:

Analysis Batch: 500-173964

500-173872

500-173838

Prep Batch:

Analysis Method:

Prep Method:

Leach Batch:

Leach Date: 12/24/2012 1150

Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL

Barium 0.0103 J 0.0100 0.500

Copper 0.442 0.0100 0.0250

Chromium 0.826 0.0100 0.0250

Nickel 0.744 0.0100 0.0250

Lead <0.0500 0.00500 0.0500

Vanadium 0.0164 J 0.00500 0.0250

Zinc 0.403 0.0200 0.100

7470A Mercury (CVAA)-TCLP

7470A Instrument ID:

Lab File ID: 122712R.CSV

Dilution: 1.0 Initial Weight/Volume: 25 mL

12/27/2012 0957 Final Weight/Volume: 25 mL

12/26/2012 1300

7470A

HG6

Analysis Date:

Prep Date:

Analysis Batch: 500-173997

500-173909

500-173838

Prep Batch:

Analysis Method:

Prep Method:

Leach Batch:

Leach Date: 12/24/2012 1150

Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL

Mercury 0.000702 B 0.0000200 0.000200

7471A Mercury (CVAA)

TestAmerica Chicago Page 20 of 384 01/09/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53491-1

Client Sample ID:

Lab Sample ID:

FC COMPOSITE 6

Client Matrix: % Moisture: 73.5

500-53491-1

Solid

Date Sampled: 12/19/2012 1430

Date Received: 12/22/2012 1130

7471A Mercury (CVAA)

7471A Instrument ID:

Lab File ID: 122712A.PRN

Dilution: 1.0 Initial Weight/Volume: 0.6259 g

12/27/2012 0855 Final Weight/Volume: 50 mL

12/26/2012 1400

7471A

HG5

Analysis Date:

Prep Date:

Analysis Batch: 500-173984

Prep Batch: 500-173881

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL

Mercury 0.232 0.0231 0.0605

TestAmerica Chicago Page 21 of 384 01/09/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53491-1

Client Sample ID:

Lab Sample ID:

FC D COMPOSITE 6

Client Matrix: % Moisture: 74.9

500-53491-2

Solid

Date Sampled: 12/19/2012 1440

Date Received: 12/22/2012 1130

6010B Metals (ICP)

6010B Instrument ID:

Lab File ID: P51226B

Dilution: 1.0 Initial Weight/Volume: 1.0382 g

12/27/2012 0003 Final Weight/Volume: 100 mL

12/24/2012 1500

3050B

ICP5

Analysis Date:

Prep Date:

Analysis Batch: 500-173964

Prep Batch: 500-173848

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL

Barium 619 0.457 3.84

Copper 707 1.04 3.84

Chromium 15000 0.642 3.84

Nickel 86.1 0.841 3.84

Lead 244 B 0.661 1.92

Vanadium 251 0.292 1.92

Zinc 499 2.64 7.68

6010B Metals (ICP)-TCLP

6010B Instrument ID:

Lab File ID: P51226B

Dilution: 1.0 Initial Weight/Volume: 50 mL

12/26/2012 1847 Final Weight/Volume: 50 mL

12/26/2012 0750

3010A

ICP5

Analysis Date:

Prep Date:

Analysis Batch: 500-173964

500-173872

500-173836

Prep Batch:

Analysis Method:

Prep Method:

Leach Batch:

Leach Date: 12/24/2012 1150

Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL

Barium <0.500 0.0100 0.500

Copper 0.0547 0.0100 0.0250

Chromium <0.0250 0.0100 0.0250

Nickel 0.0624 0.0100 0.0250

Lead <0.0500 0.00500 0.0500

Vanadium <0.0250 0.00500 0.0250

Zinc <0.100 0.0200 0.100

7470A Mercury (CVAA)-TCLP

7470A Instrument ID:

Lab File ID: 122712R.CSV

Dilution: 1.0 Initial Weight/Volume: 25 mL

12/27/2012 0958 Final Weight/Volume: 25 mL

12/26/2012 1300

7470A

HG6

Analysis Date:

Prep Date:

Analysis Batch: 500-173997

500-173909

500-173836

Prep Batch:

Analysis Method:

Prep Method:

Leach Batch:

Leach Date: 12/24/2012 1150

Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL

Mercury <0.000200 0.0000200 0.000200

7471A Mercury (CVAA)

TestAmerica Chicago Page 22 of 384 01/09/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53491-1

Client Sample ID:

Lab Sample ID:

FC D COMPOSITE 6

Client Matrix: % Moisture: 74.9

500-53491-2

Solid

Date Sampled: 12/19/2012 1440

Date Received: 12/22/2012 1130

7471A Mercury (CVAA)

7471A Instrument ID:

Lab File ID: 122712A.PRN

Dilution: 1.0 Initial Weight/Volume: 0.6177 g

12/27/2012 0904 Final Weight/Volume: 50 mL

12/26/2012 1400

7471A

HG5

Analysis Date:

Prep Date:

Analysis Batch: 500-173984

Prep Batch: 500-173881

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL

Mercury 0.237 0.0247 0.0647

TestAmerica Chicago Page 23 of 384 01/09/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53491-1

Client Sample ID:

Lab Sample ID:

FC EB 6

Client Matrix:

500-53491-5

Water

Date Sampled: 12/19/2012 1410

Date Received: 12/22/2012 1130

6010B Metals (ICP)

6010B Instrument ID:

Lab File ID: P6122612B.asc

Dilution: 1.0 Initial Weight/Volume: 50 mL

12/26/2012 1703 Final Weight/Volume: 50 mL

12/24/2012 1430

3010A

ICP6

Analysis Date:

Prep Date:

Analysis Batch: 500-173963

Prep Batch: 500-173849

Analysis Method:

Prep Method:

Analyte Result (mg/L) Qualifier MDL RL

Barium <0.0100 0.000440 0.0100

Copper 0.00111 J 0.00106 0.0100

Chromium <0.0100 0.000960 0.0100

Nickel <0.0100 0.00190 0.0100

Lead <0.00500 0.00158 0.00500

Vanadium <0.00500 0.000620 0.00500

Zinc <0.0200 0.00472 0.0200

7470A Mercury (CVAA)

7470A Instrument ID:

Lab File ID: 122712R.CSV

Dilution: 1.0 Initial Weight/Volume: 25 mL

12/27/2012 0926 Final Weight/Volume: 25 mL

12/26/2012 1300

7470A

HG6

Analysis Date:

Prep Date:

Analysis Batch: 500-173997

Prep Batch: 500-173908

Analysis Method:

Prep Method:

Analyte Result (mg/L) Qualifier MDL RL

Mercury <0.000200 0.0000710 0.000200

TestAmerica Chicago Page 24 of 384 01/09/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53491-1

General Chemistry

Client Sample ID:

Lab Sample ID:

FC COMPOSITE 6

Client Matrix:

500-53491-1

Solid

Date Sampled: 12/19/2012 1430

Date Received: 12/22/2012 1130

Analyte Result Qual Units MDL RL Dil Method

Flashpoint >176 Degrees F 40.0 40.0 1.0 1010

Analysis Batch: 500-174336 Analysis Date (Start): 01/02/2013 0930 (End) 01/02/2013 1052 DryWt Corrected: N

Chromium, hexavalent <3.75 mg/Kg 1.46 3.75 1.0 7196A

Analysis Batch: 500-174027 Analysis Date (Start): 12/27/2012 1251 (End) 12/27/2012 1251 DryWt Corrected: Y

Prep Batch: 500-173790 Prep Date: 12/22/2012 1200

Cyanide, Total 1.15 J mg/Kg 0.622 1.88 1.0 9014

Analysis Batch: 500-174173 Analysis Date (Start): 12/28/2012 1531 (End) 12/28/2012 1531 DryWt Corrected: Y

Prep Batch: 500-174096 Prep Date: 12/28/2012 1120

Sulfide 778 mg/Kg 14.5 90.4 1.0 9034

Analysis Batch: 500-174144 Analysis Date: 12/28/2012 1443 DryWt Corrected: Y

Prep Batch: 500-174100 Prep Date: 12/28/2012 1220

Sulfide, Reactive <48.5 mg/Kg 3.78 48.5 1.0 9034

Analysis Batch: 500-174145 Analysis Date: 12/28/2012 1258 DryWt Corrected: N

Prep Batch: 500-174101 Prep Date: 12/28/2012 1157

pH 9.79 SU 0.200 0.200 1.0 9045C

Analysis Batch: 500-173936 Analysis Date (Start): 12/26/2012 1425 (End) 12/26/2012 1427 DryWt Corrected: N

HEM (Oil & Grease) 16600 mg/Kg 822 1850 1.0 9071B

Analysis Batch: 500-174372 Analysis Date: 01/04/2013 1013 DryWt Corrected: Y

Prep Batch: 500-174369 Prep Date: 01/04/2013 0535

Percent Moisture 74 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-173788 Analysis Date: 12/22/2012 1324 DryWt Corrected: N

Percent Solids 26 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-173788 Analysis Date: 12/22/2012 1324 DryWt Corrected: N

% Moisture 74.0 % 0.100 0.100 1.0 SM 2540G

Analysis Batch: 500-173970 Analysis Date: 12/27/2012 0730 DryWt Corrected: N

Total Solids 26.0 % 0.100 0.100 1.0 SM 2540G

Analysis Batch: 500-173970 Analysis Date: 12/27/2012 0730 DryWt Corrected: N

TestAmerica Chicago Page 25 of 384 01/09/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53491-1

General Chemistry

Client Sample ID:

Lab Sample ID:

FC D COMPOSITE 6

Client Matrix:

500-53491-2

Solid

Date Sampled: 12/19/2012 1440

Date Received: 12/22/2012 1130

Analyte Result Qual Units MDL RL Dil Method

Flashpoint >176 Degrees F 40.0 40.0 1.0 1010

Analysis Batch: 500-174336 Analysis Date (Start): 01/02/2013 1052 (End) 01/02/2013 1214 DryWt Corrected: N

Chromium, hexavalent <3.99 mg/Kg 1.55 3.99 1.0 7196A

Analysis Batch: 500-174027 Analysis Date (Start): 12/27/2012 1253 (End) 12/27/2012 1253 DryWt Corrected: Y

Prep Batch: 500-173790 Prep Date: 12/22/2012 1200

Cyanide, Total 1.29 J mg/Kg 0.615 1.86 1.0 9014

Analysis Batch: 500-174173 Analysis Date (Start): 12/28/2012 1531 (End) 12/28/2012 1532 DryWt Corrected: Y

Prep Batch: 500-174096 Prep Date: 12/28/2012 1120

Sulfide 817 mg/Kg 15.0 94.0 1.0 9034

Analysis Batch: 500-174144 Analysis Date: 12/28/2012 1444 DryWt Corrected: Y

Prep Batch: 500-174100 Prep Date: 12/28/2012 1220

Sulfide, Reactive <49.3 mg/Kg 3.85 49.3 1.0 9034

Analysis Batch: 500-174145 Analysis Date: 12/28/2012 1259 DryWt Corrected: N

Prep Batch: 500-174101 Prep Date: 12/28/2012 1201

pH 9.87 SU 0.200 0.200 1.0 9045C

Analysis Batch: 500-173936 Analysis Date (Start): 12/26/2012 1427 (End) 12/26/2012 1430 DryWt Corrected: N

HEM (Oil & Grease) 17000 mg/Kg 866 1950 1.0 9071B

Analysis Batch: 500-174372 Analysis Date: 01/04/2013 1056 DryWt Corrected: Y

Prep Batch: 500-174369 Prep Date: 01/04/2013 0535

Percent Moisture 75 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-173788 Analysis Date: 12/22/2012 1324 DryWt Corrected: N

Percent Solids 25 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-173788 Analysis Date: 12/22/2012 1324 DryWt Corrected: N

% Moisture 75.0 % 0.100 0.100 1.0 SM 2540G

Analysis Batch: 500-173970 Analysis Date: 12/27/2012 0730 DryWt Corrected: N

Total Solids 25.0 % 0.100 0.100 1.0 SM 2540G

Analysis Batch: 500-173970 Analysis Date: 12/27/2012 0730 DryWt Corrected: N

TestAmerica Chicago Page 26 of 384 01/09/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53491-1

General Chemistry

Client Sample ID:

Lab Sample ID:

FC DISCRETE 6

Client Matrix:

500-53491-3

Solid

Date Sampled: 12/19/2012 1420

Date Received: 12/22/2012 1130

Analyte Result Qual Units MDL RL Dil Method

Percent Moisture 74 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-174071 Analysis Date: 12/28/2012 1009 DryWt Corrected: N

Percent Solids 26 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-174071 Analysis Date: 12/28/2012 1009 DryWt Corrected: N

TestAmerica Chicago Page 27 of 384 01/09/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53491-1

General Chemistry

Client Sample ID:

Lab Sample ID:

FC D DISCRETE 6

Client Matrix:

500-53491-4

Solid

Date Sampled: 12/19/2012 1445

Date Received: 12/22/2012 1130

Analyte Result Qual Units MDL RL Dil Method

Percent Moisture 72 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-174071 Analysis Date: 12/28/2012 1009 DryWt Corrected: N

Percent Solids 28 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-174071 Analysis Date: 12/28/2012 1009 DryWt Corrected: N

TestAmerica Chicago Page 28 of 384 01/09/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53491-1

General Chemistry

Client Sample ID:

Lab Sample ID:

FC EB 6

Client Matrix:

500-53491-5

Water

Date Sampled: 12/19/2012 1410

Date Received: 12/22/2012 1130

Analyte Result Qual Units MDL RL Dil Method

HEM (Oil & Grease) <5.33 mg/L 1.55 5.33 1.0 1664A

Analysis Batch: 500-174564 Analysis Date: 01/08/2013 1108

Prep Batch: 500-174563 Prep Date: 01/08/2013 0601

Chromium, hexavalent <0.0100 H mg/L 0.00325 0.0100 1.0 7196A

Analysis Batch: 500-173793 Analysis Date (Start): 12/22/2012 1412 (End) 12/22/2012 1413

Cyanide, Total <0.0100 mg/L 0.00331 0.0100 1.0 9014

Analysis Batch: 500-174042 Analysis Date (Start): 12/27/2012 1445 (End) 12/27/2012 1445

Prep Batch: 500-173980 Prep Date: 12/27/2012 0950

Sulfide <1.00 mg/L 0.230 1.00 1.0 9034

Analysis Batch: 500-173846 Analysis Date (Start): 12/24/2012 1400 (End) 12/24/2012 1402

Sulfide, Reactive <1.00 mg/L 1.00 1.00 1.0 9034

Analysis Batch: 500-173845 Analysis Date: 12/24/2012 1351

Prep Batch: 500-173844 Prep Date: 12/24/2012 0845

TestAmerica Chicago Page 29 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Surrogate Recovery Report

8260B Volatile Organic Compounds (GC/MS)

Client Matrix: Solid

Lab Sample ID Client Sample ID

DBFM DCA TOL BFB

%Rec %Rec %Rec %Rec

500-53491-3 FC DISCRETE 6 95 89 87 79

500-53491-4 FC D DISCRETE 6 90 91 89 75

MB 500-173973/5 90 94 96 84

LCS 500-173973/6 81 84 89 81

LCSD 500-173973/7 91 88 93 87

Surrogate Acceptance Limits

DBFM = Dibromofluoromethane 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 70-134

TOL = Toluene-d8 (Surr) 75-122

BFB = 4-Bromofluorobenzene (Surr) 70-122

TestAmerica Chicago

Page 30 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Surrogate Recovery Report

8260B Volatile Organic Compounds (GC/MS)

Client Matrix: Solid

Lab Sample ID Client Sample ID

DBFM DCA TOL BFB

%Rec %Rec %Rec %Rec

500-53491-3 DL FC DISCRETE 6 DL 93 97 96 94

500-53491-4 DL FC D DISCRETE 6 

DL

96 105 101 100

MB 500-174064/6 96 101 101 98

LCS 500-174064/4 100 95 97 97

Surrogate Acceptance Limits

DBFM = Dibromofluoromethane 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 75-125

TOL = Toluene-d8 (Surr) 75-120

BFB = 4-Bromofluorobenzene (Surr) 75-120

TestAmerica Chicago

Page 31 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Surrogate Recovery Report

8260B Volatile Organic Compounds (GC/MS)

Client Matrix: Water

Lab Sample ID Client Sample ID

DBFM DCA TOL BFB

%Rec %Rec %Rec %Rec

500-53491-5 FC EB 6 90 88 94 88

500-53491-6 TRIP BLANK 93 93 100 93

MB 500-173987/7 97 98 103 97

LCS 500-173987/4 94 92 96 96

Surrogate Acceptance Limits

DBFM = Dibromofluoromethane 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 75-125

TOL = Toluene-d8 (Surr) 75-120

BFB = 4-Bromofluorobenzene (Surr) 75-120

TestAmerica Chicago

Page 32 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173973

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 6M1227.d5 g

Units: ug/Kg 5 mL

Method: 8260B

Preparation: 5030B

MB 500-173973/5 CMS06

Analysis Date: 12/27/2012 1033

Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

500-173973

Prep Date:

Leach Date:

12/27/2012 1033

N/A

Analyte Result Qual MDL RL

Acetone <5.00 2.16 5.00

2-Butanone (MEK) <5.00 1.81 5.00

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 94 70 - 134

Toluene-d8 (Surr) 96 75 - 122

4-Bromofluorobenzene (Surr) 84 70 - 122

Dibromofluoromethane 90 75 - 120

Dilution:

Dilution:

Lab Control Sample/

Lab Control Sample Duplicate Recovery Report - Batch: 500-173973

1.0

1.0

Solid

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: Client Matrix: Solid

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume:

ug/Kg

6S1227.d

5 g

5 mL

6T1227.d

5 g

ug/Kg 5 mL

Method: 8260B

Preparation: 5030B

CMS06

CMS06

LCS 500-173973/6

LCSD 500-173973/7

Analysis Date:

Prep Date:

Leach Date:

12/27/2012 1056

12/27/2012 1056

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

500-173973

N/A

N/A

Analysis Date:

Prep Date:

Leach Date:

12/27/2012 1119

12/27/2012 1119

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

500-173973

N/A

N/A

Analyte LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qual

% Rec.

Acetone 96 110 50 - 138 14 30

2-Butanone (MEK) 86 90 58 - 133 4 30

Surrogate LCS % Rec LCSD % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 84 88 70 - 134

Toluene-d8 (Surr) 89 93 75 - 122

4-Bromofluorobenzene (Surr) 81 87 70 - 122

Dibromofluoromethane 81 91 75 - 120

TestAmerica Chicago Page 33 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Solid

12/27/2012 1056

Dilution: 1.0 Dilution: 1.0

Client Matrix:

LCSD Lab Sample ID:

Client Matrix: Solid

Laboratory Control/

Laboratory Duplicate Data Report - Batch: 500-173973

Method: 8260B

Preparation: 5030B

LCS Lab Sample ID: LCS 500-173973/6 Units: ug/Kg LCSD 500-173973/7

Analysis Date:

Prep Date:

Leach Date:

12/27/2012 1056

Analysis Date:

Prep Date:

Leach Date:

12/27/2012 1119

12/27/2012 1119

N/A N/A

LCSD 

Result/Qual

LCS 

Result/Qual

LCSD Spike 

Amount

LCS Spike 

Amount Analyte

Acetone 50.0 50.0 47.98 55.07

2-Butanone (MEK) 50.0 50.0 43.18 44.82

TestAmerica Chicago Page 34 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173987

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 22M1227.D5 mL

Units: ug/L 5 mL

Method: 8260B

Preparation: 5030B

MB 500-173987/7 CMS22

Analysis Date: 12/27/2012 1410

Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

500-173987

Prep Date:

Leach Date:

12/27/2012 1410

N/A

Analyte Result Qual MDL RL

Acetone <5.00 1.29 5.00

2-Butanone (MEK) <5.00 1.47 5.00

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 98 75 - 125

Toluene-d8 (Surr) 103 75 - 120

4-Bromofluorobenzene (Surr) 97 75 - 120

Dibromofluoromethane 97 75 - 120

Water

1.0

Lab Control Sample - Batch: 500-173987

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 22S1227.D5 mL

Units: ug/L 5 mL

Method: 8260B

Preparation: 5030B

LCS 500-173987/4 CMS22

Analysis Date: 12/27/2012 1246

Analysis Batch:

Prep Batch:

Leach Batch:

500-173987

N/A

N/A

Prep Date:

Leach Date:

12/27/2012 1246

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Acetone 50.0 53.44 107 46 - 153

2-Butanone (MEK) 50.0 46.97 94 54 - 138

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 92 75 - 125

Toluene-d8 (Surr) 96 75 - 120

4-Bromofluorobenzene (Surr) 96 75 - 120

Dibromofluoromethane 94 75 - 120

TestAmerica Chicago Page 35 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-174064

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 18M1228.D5 mL

Units: ug/Kg 5 mL

Method: 8260B

Preparation: N/A

MB 500-174064/6 CMS18

Analysis Date: 12/28/2012 1045

Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

500-174064

Prep Date:

Leach Date:

N/A

N/A

Analyte Result Qual MDL RL

Acetone <5.00 1.30 5.00

2-Butanone (MEK) <5.00 1.47 5.00

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 101 75 - 125

Toluene-d8 (Surr) 101 75 - 120

4-Bromofluorobenzene (Surr) 98 75 - 120

Dibromofluoromethane 96 75 - 120

Solid

1.0

Lab Control Sample - Batch: 500-174064

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 18S1228.D5 mL

Units: ug/Kg 5 mL

Method: 8260B

Preparation: N/A

LCS 500-174064/4 CMS18

Analysis Date: 12/28/2012 1000

Analysis Batch:

Prep Batch:

Leach Batch:

500-174064

N/A

N/A

Prep Date:

Leach Date:

N/A

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Acetone 50.0 50.53 101 46 - 153

2-Butanone (MEK) 50.0 43.61 87 54 - 138

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 95 75 - 125

Toluene-d8 (Surr) 97 75 - 120

4-Bromofluorobenzene (Surr) 97 75 - 120

Dibromofluoromethane 100 75 - 120

TestAmerica Chicago Page 36 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173848

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51226B1 g

Units: mg/Kg 100 mL

Method: 6010B

Preparation: 3050B

MB 500-173848/1-A ICP5

Analysis Date: 12/26/2012 2154

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173964

500-173848

Prep Date:

Leach Date:

12/24/2012 1500

N/A

Analyte Result Qual MDL RL

Barium <1.00 0.119 1.00

Copper <1.00 0.271 1.00

Chromium <1.00 0.167 1.00

Nickel <1.00 0.219 1.00

Lead 0.1770 J 0.172 0.500

Vanadium <0.500 0.0759 0.500

Zinc <2.00 0.686 2.00

Solid

1.0

Lab Control Sample - Batch: 500-173848

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51226B1 g

Units: mg/Kg 100 mL

Method: 6010B

Preparation: 3050B

LCS 500-173848/2-A ICP5

Analysis Date: 12/26/2012 2200

Analysis Batch:

Prep Batch:

Leach Batch:

500-173964

500-173848

N/A

Prep Date:

Leach Date:

12/24/2012 1500

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Barium 200 200.1 100 80 - 120

Copper 25.0 25.74 103 80 - 120

Chromium 20.0 20.94 105 80 - 120

Nickel 50.0 51.09 102 80 - 120

Lead 10.0 10.73 107 80 - 120

Vanadium 50.0 51.21 102 80 - 120

Zinc 50.0 53.63 107 80 - 120

TestAmerica Chicago Page 37 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173849

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P6122612B.asc50 mL

Units: mg/L 50 mL

Method: 6010B

Preparation: 3010A

MB 500-173849/1-A ICP6

Analysis Date: 12/26/2012 1635

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173963

500-173849

Prep Date:

Leach Date:

12/24/2012 1430

N/A

Analyte Result Qual MDL RL

Barium <0.0100 0.000440 0.0100

Copper <0.0100 0.00106 0.0100

Chromium <0.0100 0.000960 0.0100

Nickel <0.0100 0.00190 0.0100

Lead <0.00500 0.00158 0.00500

Vanadium <0.00500 0.000620 0.00500

Zinc <0.0200 0.00472 0.0200

Water

1.0

Lab Control Sample - Batch: 500-173849

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P6122612B.asc50 mL

Units: mg/L 50 mL

Method: 6010B

Preparation: 3010A

LCS 500-173849/2-A ICP6

Analysis Date: 12/26/2012 1639

Analysis Batch:

Prep Batch:

Leach Batch:

500-173963

500-173849

N/A

Prep Date:

Leach Date:

12/24/2012 1430

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Barium 2.00 1.902 95 80 - 120

Copper 0.250 0.2317 93 80 - 120

Chromium 0.200 0.1856 93 80 - 120

Nickel 0.500 0.4572 91 80 - 120

Lead 0.100 0.09439 94 80 - 120

Vanadium 0.500 0.4686 94 80 - 120

Zinc 0.500 0.4470 89 80 - 120

TestAmerica Chicago Page 38 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

TCLP SPLPE Leachate Blank - Batch: 500-173872

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51226B50 mL

Units: mg/L 50 mL

Method: 6010B

Preparation: 3010A

TCLP

LB 500-173836/1-B ICP5

Analysis Date: 12/26/2012 1712

Analysis Batch:

Prep Batch:

Leach Batch: 500-173836

500-173964

500-173872

Prep Date:

Leach Date:

12/26/2012 0750

12/24/2012 1150

Analyte Result Qual MDL RL

Barium <0.500 0.0100 0.500

Copper <0.0250 0.0100 0.0250

Chromium <0.0250 0.0100 0.0250

Nickel <0.0250 0.0100 0.0250

Lead <0.0500 0.00500 0.0500

Vanadium <0.0250 0.00500 0.0250

Zinc <0.100 0.0200 0.100

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

TCLP SPLPW Leachate Blank - Batch: 500-173872

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51226B50 mL

Units: mg/L 50 mL

Method: 6010B

Preparation: 3010A

TCLP

LB2 500-173838/1-B ICP5

Analysis Date: 12/26/2012 1718

Analysis Batch:

Prep Batch:

Leach Batch: 500-173838

500-173964

500-173872

Prep Date:

Leach Date:

12/26/2012 0750

12/24/2012 1150

Analyte Result Qual MDL RL

Barium <0.500 0.0100 0.500

Copper <0.0250 0.0100 0.0250

Chromium <0.0250 0.0100 0.0250

Nickel <0.0250 0.0100 0.0250

Lead <0.0500 0.00500 0.0500

Vanadium <0.0250 0.00500 0.0250

Zinc <0.100 0.0200 0.100

TestAmerica Chicago Page 39 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Water

1.0

Lab Control Sample - Batch: 500-173872

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51226B50 mL

Units: mg/L 50 mL

Method: 6010B

Preparation: 3010A

LCS 500-173872/3-A ICP5

Analysis Date: 12/26/2012 1724

Analysis Batch:

Prep Batch:

Leach Batch:

500-173964

500-173872

N/A

Prep Date:

Leach Date:

12/26/2012 0750

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Barium 2.00 1.928 96 80 - 120

Copper 0.250 0.2512 100 80 - 120

Chromium 0.200 0.2016 101 80 - 120

Nickel 0.500 0.4930 99 80 - 120

Lead 0.100 0.1042 104 80 - 120

Vanadium 0.500 0.4994 100 80 - 120

Zinc 0.500 0.5058 101 80 - 120

TestAmerica Chicago Page 40 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173908

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 122712R.CSV25 mL

Units: mg/L 25 mL

Method: 7470A

Preparation: 7470A

MB 500-173908/7-A HG6

Analysis Date: 12/27/2012 0841

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173997

500-173908

Prep Date:

Leach Date:

12/26/2012 1300

N/A

Analyte Result Qual MDL RL

Mercury <0.000200 0.0000710 0.000200

Water

1.0

Lab Control Sample - Batch: 500-173908

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 122712R.CSV25 mL

Units: mg/L 25 mL

Method: 7470A

Preparation: 7470A

LCS 500-173908/8-A HG6

Analysis Date: 12/27/2012 0843

Analysis Batch:

Prep Batch:

Leach Batch:

500-173997

500-173908

N/A

Prep Date:

Leach Date:

12/26/2012 1300

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Mercury 0.00200 0.002121 106 80 - 120

TestAmerica Chicago Page 41 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173909

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 122712R.CSV25 mL

Units: mg/L 25 mL

Method: 7470A

Preparation: 7470A

MB 500-173909/7-A HG6

Analysis Date: 12/27/2012 0928

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173997

500-173909

Prep Date:

Leach Date:

12/26/2012 1300

N/A

Analyte Result Qual MDL RL

Mercury 0.00003040 J 0.0000200 0.000200

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

TCLP SPLPE Leachate Blank - Batch: 500-173909

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 122712R.CSV25 mL

Units: mg/L 25 mL

Method: 7470A

Preparation: 7470A

TCLP

LB 500-173836/1-C HG6

Analysis Date: 12/27/2012 0949

Analysis Batch:

Prep Batch:

Leach Batch: 500-173836

500-173997

500-173909

Prep Date:

Leach Date:

12/26/2012 1300

12/24/2012 1150

Analyte Result Qual MDL RL

Mercury 0.00003420 J 0.0000200 0.000200

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

TCLP SPLPW Leachate Blank - Batch: 500-173909

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 122712R.CSV25 mL

Units: mg/L 25 mL

Method: 7470A

Preparation: 7470A

TCLP

LB2 500-173838/1-C HG6

Analysis Date: 12/27/2012 0951

Analysis Batch:

Prep Batch:

Leach Batch: 500-173838

500-173997

500-173909

Prep Date:

Leach Date:

12/26/2012 1300

12/24/2012 1150

Analyte Result Qual MDL RL

Mercury 0.00003260 J 0.0000200 0.000200

TestAmerica Chicago Page 42 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Water

1.0

Lab Control Sample - Batch: 500-173909

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 122712R.CSV25 mL

Units: mg/L 25 mL

Method: 7470A

Preparation: 7470A

LCS 500-173909/8-A HG6

Analysis Date: 12/27/2012 0930

Analysis Batch:

Prep Batch:

Leach Batch:

500-173997

500-173909

N/A

Prep Date:

Leach Date:

12/26/2012 1300

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Mercury 0.00200 0.002139 107 80 - 120

Solid

1.0

Matrix Spike - Batch: 500-173909

Lab Sample ID:

Client Matrix:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 122712R.CSV25 mL

Units: mg/L 25 mL

Method: 7470A

Preparation: 7470A

TCLP

500-53491-2 HG6

Analysis Date: 12/27/2012 1002

Analysis Batch: 500-173997

Prep Batch: 500-173909

Leach Batch: 500-173836

Prep Date:

Leach Date:

12/26/2012 1300

12/24/2012 1150

Analyte Sample Result/Qual Spike Amount Result % Rec. Limit Qual

Mercury <0.000200 0.00100 0.0007703 77 50 - 150

Units: mg/L

Solid

Dilution: 1.0

Duplicate - Batch: 500-173909

Lab Sample ID:

Client Matrix:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 122712R.CSV25 mL

25 mL

Method: 7470A

Preparation: 7470A

TCLP

500-53491-2 HG6

Analysis Date: 12/27/2012 1000

Analysis Batch:

Prep Batch:

Leach Batch:

500-173997

500-173909

500-173836

Prep Date:

Leach Date:

12/26/2012 1300

12/24/2012 1150

Analyte Sample Result/Qual Result RPD Limit Qual

Mercury <0.000200 0.00004470 NC 20 J

TestAmerica Chicago Page 43 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173881

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 122712A.PRN0.6 g

Units: mg/Kg 50 mL

Method: 7471A

Preparation: 7471A

MB 500-173881/7-A HG5

Analysis Date: 12/27/2012 0817

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173984

500-173881

Prep Date:

Leach Date:

12/26/2012 1400

N/A

Analyte Result Qual MDL RL

Mercury <0.0167 0.00637 0.0167

Solid

1.0

Lab Control Sample - Batch: 500-173881

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 122712A.PRN0.6 g

Units: mg/Kg 50 mL

Method: 7471A

Preparation: 7471A

LCS 500-173881/8-A HG5

Analysis Date: 12/27/2012 0819

Analysis Batch:

Prep Batch:

Leach Batch:

500-173984

500-173881

N/A

Prep Date:

Leach Date:

12/26/2012 1400

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Mercury 0.167 0.1600 96 80 - 120

TestAmerica Chicago Page 44 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-174563

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 1000 mL

Units: mg/L 1000 mL

Method: 1664A

Preparation: 1664A

N/A

MB 500-174563/1-A No Equipment 

Analysis Date: 01/08/2013 1100

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-174564

500-174563

Prep Date:

Leach Date:

01/08/2013 0535

N/A

Analyte Result Qual MDL RL

HEM (Oil & Grease) <5.00 1.45 5.00

Water

1.0

Lab Control Sample - Batch: 500-174563

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 1000 mL

Units: mg/L 1000 mL

Method: 1664A

Preparation: 1664A

N/A

LCS 500-174563/2-A No Equipment 

Analysis Date: 01/08/2013 1104

Analysis Batch:

Prep Batch:

Leach Batch:

500-174564

500-174563

N/A

Prep Date:

Leach Date:

01/08/2013 0548

N/A

Analyte Spike Amount Result % Rec. Limit Qual

HEM (Oil & Grease) 40.0 32.00 80 78 - 114

TestAmerica Chicago Page 45 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173790

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 2.5 g

Units: mg/Kg 100 mL

Method: 7196A

Preparation: 3060A

N/A

MB 500-173790/1-A SPEC5

Analysis Date: 12/27/2012 1241

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-174027

500-173790

Prep Date:

Leach Date:

12/22/2012 1200

N/A

Analyte Result Qual MDL RL

Chromium, hexavalent <1.00 0.389 1.00

Solid

1.0

Lab Control Sample - Batch: 500-173790

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 2.5 g

Units: mg/Kg 100 mL

Method: 7196A

Preparation: 3060A

N/A

LCS 500-173790/2-A SPEC5

Analysis Date: 12/27/2012 1242

Analysis Batch:

Prep Batch:

Leach Batch:

500-174027

500-173790

N/A

Prep Date:

Leach Date:

12/22/2012 1200

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Chromium, hexavalent 10.0 9.188 92 80 - 120

Solid

50

Lab Control Sample - Batch: 500-173790

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 2.5 g

Units: mg/Kg 100 mL

Method: 7196A

Preparation: 3060A

N/A

LCS 500-173790/3-A SPEC5

Analysis Date: 12/27/2012 1242

Analysis Batch:

Prep Batch:

Leach Batch:

500-174027

500-173790

N/A

Prep Date:

Leach Date:

12/22/2012 1200

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Chromium, hexavalent 676 669.0 99 80 - 120

TestAmerica Chicago Page 46 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173793

Instrument ID:

Lab File ID:

Initial Weight/Volume: Units: mg/L Final Weight/Volume:

Method: 7196A

Preparation: N/A

N/A

MB 500-173793/3 SPEC5

Analysis Date: 12/22/2012 1411

Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

500-173793

Prep Date:

Leach Date:

N/A

N/A

Analyte Result Qual MDL RL

Chromium, hexavalent <0.0100 0.00325 0.0100

Water

1.0

Lab Control Sample - Batch: 500-173793

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 100 mL

Units: mg/L 100 mL

Method: 7196A

Preparation: N/A

N/A

LCS 500-173793/4 SPEC5

Analysis Date: 12/22/2012 1411

Analysis Batch:

Prep Batch:

Leach Batch:

500-173793

N/A

N/A

Prep Date:

Leach Date:

N/A

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Chromium, hexavalent 0.250 0.2575 103 85 - 115

Dilution:

Dilution:

Water

1.0

1.0

Client Matrix:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: Client Matrix: Water

100 mL

100 mL

100 mL

100 mL

Method: 7196A

Preparation: N/A

N/A

N/A

SPEC5

SPEC5

500-53491-5

500-53491-5

MS Lab Sample ID:

MSD Lab Sample ID:

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-173793

12/22/2012 1413

N/A

N/A

Analysis Date:

Prep Date:

Leach Date:

Analysis Batch:

Prep Batch:

Leach Batch:

500-173793

N/A

N/A

Analysis Date:

Prep Date:

Leach Date:

12/22/2012 1413

N/A

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

500-173793

N/A

N/A

Analyte Limit RPD RPD Limit

% Rec.

MS MSD MS Qual MSD Qual

Chromium, hexavalent 106 102 85 - 115 5 20

TestAmerica Chicago Page 47 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Water

12/22/2012 1413 12/22/2012 1413

Dilution: 1.0 Dilution: 1.0

Client Matrix: Client Matrix: Water

Method: 7196A

Preparation: N/A

MS Lab Sample ID: 500-53491-5 Units: mg/L MSD Lab Sample ID: 500-53491-5

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-173793

Analysis Date:

Prep Date:

Leach Date:

N/A

N/A

Analysis Date:

Prep Date:

Leach Date:

N/A

N/A

Amount

Sample

Analyte Result/Qual Amount Result/Qual Result/Qual

MS Spike MSD Spike MS MSD

Chromium, hexavalent <0.0100 0.250 0.250 0.2660 0.2541

TestAmerica Chicago Page 48 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173980

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 50 mL

Units: mg/L 50 mL

Method: 9014

Preparation: 9010B

N/A

MB 500-173980/1-A SPEC5

Analysis Date: 12/27/2012 1440

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-174042

500-173980

Prep Date:

Leach Date:

12/27/2012 0950

N/A

Analyte Result Qual MDL RL

Cyanide, Total <0.0100 0.00331 0.0100

Water

1.0

Lab Control Sample - Batch: 500-173980

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 50 mL

Units: mg/L 50 mL

Method: 9014

Preparation: 9010B

N/A

LCS 500-173980/2-A SPEC5

Analysis Date: 12/27/2012 1440

Analysis Batch:

Prep Batch:

Leach Batch:

500-174042

500-173980

N/A

Prep Date:

Leach Date:

12/27/2012 0950

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Cyanide, Total 0.100 0.1066 107 80 - 120

TestAmerica Chicago Page 49 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-174096

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 1.0000 g

Units: mg/Kg 50 mL

Method: 9014

Preparation: 9010B

N/A

MB 500-174096/12-A SPEC5

Analysis Date: 12/28/2012 1530

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-174173

500-174096

Prep Date:

Leach Date:

12/28/2012 1120

N/A

Analyte Result Qual MDL RL

Cyanide, Total <0.500 0.165 0.500

Solid

1.0

Lab Control Sample - Batch: 500-174096

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 1.0000 g

Units: mg/Kg 50 mL

Method: 9014

Preparation: 9010B

N/A

LCS 500-174096/13-A SPEC5

Analysis Date: 12/28/2012 1530

Analysis Batch:

Prep Batch:

Leach Batch:

500-174173

500-174096

N/A

Prep Date:

Leach Date:

12/28/2012 1120

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Cyanide, Total 5.00 5.325 107 80 - 120

Dilution:

Dilution:

Solid

1.0

1.0

Client Matrix:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: Client Matrix: Solid

1.0637 g

50 mL

1.0714 g

50 mL

Method: 9014

Preparation: 9010B

N/A

N/A

SPEC5

SPEC5

500-53491-2

500-53491-2

MS Lab Sample ID:

MSD Lab Sample ID:

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-174096

12/28/2012 1532

N/A

Analysis Date:

Prep Date:

Leach Date:

Analysis Batch:

Prep Batch:

Leach Batch:

500-174173

500-174096

N/A

Analysis Date:

Prep Date:

Leach Date:

12/28/2012 1532

12/28/2012 1120

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

500-174173

500-174096

N/A

12/28/2012 1120

Analyte Limit RPD RPD Limit

% Rec.

MS MSD MS Qual MSD Qual

Cyanide, Total 82 92 75 - 125 9 20

TestAmerica Chicago Page 50 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Solid

12/28/2012 1532 12/28/2012 1532

Dilution: 1.0 Dilution: 1.0

Client Matrix: Client Matrix: Solid

Method: 9014

Preparation: 9010B

MS Lab Sample ID: 500-53491-2 Units: mg/Kg MSD Lab Sample ID: 500-53491-2

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-174096

Analysis Date:

Prep Date:

Leach Date:

12/28/2012 1120

N/A

Analysis Date:

Prep Date:

Leach Date:

12/28/2012 1120

N/A

Amount

Sample

Analyte Result/Qual Amount Result/Qual Result/Qual

MS Spike MSD Spike MS MSD

Cyanide, Total 1.29 J 7.50 7.44 7.442 8.170

TestAmerica Chicago Page 51 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173844

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 250 mL

Units: mg/L 250 mL

Method: 9034

Preparation: 7.3.4

N/A

MB 500-173844/1-A No Equipment 

Analysis Date: 12/24/2012 1319

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173845

500-173844

Prep Date:

Leach Date:

12/24/2012 0800

N/A

Analyte Result Qual MDL RL

Sulfide, Reactive <1.00 1.00 1.00

Water

1.0

Lab Control Sample - Batch: 500-173844

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 250 mL

Units: mg/L 250 mL

Method: 9034

Preparation: 7.3.4

N/A

LCS 500-173844/2-A No Equipment 

Analysis Date: 12/24/2012 1329

Analysis Batch:

Prep Batch:

Leach Batch:

500-173845

500-173844

N/A

Prep Date:

Leach Date:

12/24/2012 0815

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Sulfide, Reactive 3.60 3.767 105 80 - 120

TestAmerica Chicago Page 52 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173846

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 250 mL

Units: mg/L 250 mL

Method: 9034

Preparation: N/A

N/A

MB 500-173846/1 No Equipment 

Analysis Date: 12/24/2012 1319

Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

500-173846

Prep Date:

Leach Date:

N/A

N/A

Analyte Result Qual MDL RL

Sulfide <1.00 0.230 1.00

Water

1.0

Lab Control Sample - Batch: 500-173846

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 250 mL

Units: mg/L 250 mL

Method: 9034

Preparation: N/A

N/A

LCS 500-173846/2 No Equipment 

Analysis Date: 12/24/2012 1320

Analysis Batch:

Prep Batch:

Leach Batch:

500-173846

N/A

N/A

Prep Date:

Leach Date:

N/A

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Sulfide 3.60 3.760 104 80 - 120

TestAmerica Chicago Page 53 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-174100

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10.0000 g

Units: mg/Kg 10 mL

Method: 9034

Preparation: 9030B

N/A

MB 500-174100/1-A No Equipment 

Analysis Date: 12/28/2012 1435

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-174144

500-174100

Prep Date:

Leach Date:

12/28/2012 1220

N/A

Analyte Result Qual MDL RL

Sulfide <25.0 4.00 25.0

Solid

1.0

Lab Control Sample - Batch: 500-174100

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10.0000 g

Units: mg/Kg 10 mL

Method: 9034

Preparation: 9030B

N/A

LCS 500-174100/2-A No Equipment 

Analysis Date: 12/28/2012 1436

Analysis Batch:

Prep Batch:

Leach Batch:

500-174144

500-174100

N/A

Prep Date:

Leach Date:

12/28/2012 1220

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Sulfide 180 173.0 96 80 - 120

TestAmerica Chicago Page 54 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-174101

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10.0000 g

Units: mg/Kg 10 mL

Method: 9034

Preparation: 7.3.4

N/A

MB 500-174101/1-A No Equipment 

Analysis Date: 12/28/2012 1255

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-174145

500-174101

Prep Date:

Leach Date:

12/28/2012 1135

N/A

Analyte Result Qual MDL RL

Sulfide, Reactive <50.0 3.90 50.0

Solid

1.0

Lab Control Sample - Batch: 500-174101

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10.0000 g

Units: mg/Kg 10 mL

Method: 9034

Preparation: 7.3.4

N/A

LCS 500-174101/2-A No Equipment 

Analysis Date: 12/28/2012 1255

Analysis Batch:

Prep Batch:

Leach Batch:

500-174145

500-174101

N/A

Prep Date:

Leach Date:

12/28/2012 1138

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Sulfide, Reactive 180 169.4 94 80 - 120

TestAmerica Chicago Page 55 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-174369

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10 g

Units: mg/Kg 10 mL

Method: 9071B

Preparation: 9071B

N/A

MB 500-174369/1-A No Equipment 

Analysis Date: 01/04/2013 0945

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-174372

500-174369

Prep Date:

Leach Date:

01/04/2013 0535

N/A

Analyte Result Qual MDL RL

HEM (Oil & Grease) <500 222 500

Solid

1.0

Lab Control Sample - Batch: 500-174369

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10 g

Units: mg/Kg 10 mL

Method: 9071B

Preparation: 9071B

N/A

LCS 500-174369/2-A No Equipment 

Analysis Date: 01/04/2013 0959

Analysis Batch:

Prep Batch:

Leach Batch:

500-174372

500-174369

N/A

Prep Date:

Leach Date:

01/04/2013 0535

N/A

Analyte Spike Amount Result % Rec. Limit Qual

HEM (Oil & Grease) 4000 4050 101 80 - 120

Dilution:

Dilution:

Solid

1.0

1.0

Client Matrix:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: Client Matrix: Solid

10.2105 g

10 mL

10.2075 g

10 mL

Method: 9071B

Preparation: 9071B

N/A

N/A

No Equipment 

No Equipment 

500-53491-1

500-53491-1

MS Lab Sample ID:

MSD Lab Sample ID:

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-174369

01/04/2013 1027

N/A

Analysis Date:

Prep Date:

Leach Date:

Analysis Batch:

Prep Batch:

Leach Batch:

500-174372

500-174369

N/A

Analysis Date:

Prep Date:

Leach Date:

01/04/2013 1042

01/04/2013 0535

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

500-174372

500-174369

N/A

01/04/2013 0535

Analyte Limit RPD RPD Limit

% Rec.

MS MSD MS Qual MSD Qual

HEM (Oil & Grease) 154 160 75 - 125 2 20 F F

TestAmerica Chicago Page 56 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Solid

01/04/2013 1027 01/04/2013 1042

Dilution: 1.0 Dilution: 1.0

Client Matrix: Client Matrix: Solid

Method: 9071B

Preparation: 9071B

MS Lab Sample ID: 500-53491-1 Units: mg/Kg MSD Lab Sample ID: 500-53491-1

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-174369

Analysis Date:

Prep Date:

Leach Date:

01/04/2013 0535

N/A

Analysis Date:

Prep Date:

Leach Date:

01/04/2013 0535

N/A

Amount

Sample

Analyte Result/Qual Amount Result/Qual Result/Qual

MS Spike MSD Spike MS MSD

HEM (Oil & Grease) 16600 14800 14800 39400 F 40340 F

TestAmerica Chicago Page 57 of 384 01/09/2013
DATA REPORTING QUALIFIERS

Client: Project Integration, Inc Job Number: 500-53491-1

Lab Section Qualifier Description

GC/MS VOA

Result is less than the RL but greater than or equal to the MDL and the 

concentration is an approximate value.

J

Metals

B Compound was found in the blank and sample.

Result is less than the RL but greater than or equal to the MDL and the 

concentration is an approximate value.

J

General Chemistry

F MS or MSD exceeds the control limits

Result is less than the RL but greater than or equal to the MDL and the 

concentration is an approximate value.

J

H Sample was prepped or analyzed beyond the specified holding time

TestAmerica Chicago Page 58 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

GC/MS VOA

Analysis Batch:500-173973

LCS 500-173973/6 Lab Control Sample T Solid 8260B

LCSD 500-173973/7 Lab Control Sample Duplicate T Solid 8260B

MB 500-173973/5 Method Blank T Solid 8260B

500-53491-3 FC DISCRETE 6 T Solid 8260B

500-53491-4 FC D DISCRETE 6 T Solid 8260B

Analysis Batch:500-173987

LCS 500-173987/4 Lab Control Sample T Water 8260B

MB 500-173987/7 Method Blank T Water 8260B

500-53491-5 FC EB 6 T Water 8260B

500-53491-6 TRIP BLANK T Water 8260B

Prep Batch: 500-173990

500-53491-3DL FC DISCRETE 6 T Solid 5030B

500-53491-4DL FC D DISCRETE 6 T Solid 5030B

Analysis Batch:500-174064

LCS 500-174064/4 Lab Control Sample T Solid 8260B

MB 500-174064/6 Method Blank T Solid 8260B

500-53491-3DL FC DISCRETE 6 T Solid 8260B 500-173990

500-53491-4DL FC D DISCRETE 6 T Solid 8260B 500-173990

Report Basis

T = Total

TestAmerica Chicago

Page 59 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

Metals

Prep Batch: 500-173836

LB 500-173836/1-B TCLP SPLPE Leachate Blank P Solid 1311

LB 500-173836/1-C TCLP SPLPE Leachate Blank P Solid 1311

500-53491-2 FC D COMPOSITE 6 P Solid 1311

500-53491-2DU Duplicate P Solid 1311

500-53491-2MS Matrix Spike P Solid 1311

Prep Batch: 500-173838

LB2 500-173838/1-B TCLP SPLPW Leachate Blank P Solid 1311

LB2 500-173838/1-C TCLP SPLPW Leachate Blank P Solid 1311

500-53491-1 FC COMPOSITE 6 P Solid 1311

Prep Batch: 500-173848

LCS 500-173848/2-A Lab Control Sample T Solid 3050B

MB 500-173848/1-A Method Blank T Solid 3050B

500-53491-1 FC COMPOSITE 6 T Solid 3050B

500-53491-2 FC D COMPOSITE 6 T Solid 3050B

Prep Batch: 500-173849

LCS 500-173849/2-A Lab Control Sample T Water 3010A

MB 500-173849/1-A Method Blank T Water 3010A

500-53491-5 FC EB 6 T Water 3010A

Prep Batch: 500-173872

LCS 500-173872/3-A Lab Control Sample T Water 3010A

LB 500-173836/1-B TCLP SPLPE Leachate Blank P Solid 3010A 500-173836

LB2 500-173838/1-B TCLP SPLPW Leachate Blank P Solid 3010A 500-173838

500-53491-1 FC COMPOSITE 6 P Solid 3010A 500-173838

500-53491-2 FC D COMPOSITE 6 P Solid 3010A 500-173836

Prep Batch: 500-173881

LCS 500-173881/8-A Lab Control Sample T Solid 7471A

MB 500-173881/7-A Method Blank T Solid 7471A

500-53491-1 FC COMPOSITE 6 T Solid 7471A

500-53491-2 FC D COMPOSITE 6 T Solid 7471A

Prep Batch: 500-173908

LCS 500-173908/8-A Lab Control Sample T Water 7470A

MB 500-173908/7-A Method Blank T Water 7470A

500-53491-5 FC EB 6 T Water 7470A

TestAmerica Chicago

Page 60 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

Metals

Prep Batch: 500-173909

LCS 500-173909/8-A Lab Control Sample T Water 7470A

MB 500-173909/7-A Method Blank T Water 7470A

LB 500-173836/1-C TCLP SPLPE Leachate Blank P Solid 7470A 500-173836

LB2 500-173838/1-C TCLP SPLPW Leachate Blank P Solid 7470A 500-173838

500-53491-1 FC COMPOSITE 6 P Solid 7470A 500-173838

500-53491-2 FC D COMPOSITE 6 P Solid 7470A 500-173836

500-53491-2DU Duplicate P Solid 7470A 500-173836

500-53491-2MS Matrix Spike P Solid 7470A 500-173836

Analysis Batch:500-173963

LCS 500-173849/2-A Lab Control Sample T Water 6010B 500-173849

MB 500-173849/1-A Method Blank T Water 6010B 500-173849

500-53491-5 FC EB 6 T Water 6010B 500-173849

Analysis Batch:500-173964

LCS 500-173848/2-A Lab Control Sample T Solid 6010B 500-173848

MB 500-173848/1-A Method Blank T Solid 6010B 500-173848

LB 500-173836/1-B TCLP SPLPE Leachate Blank P Solid 6010B 500-173872

LB2 500-173838/1-B TCLP SPLPW Leachate Blank P Solid 6010B 500-173872

LCS 500-173872/3-A Lab Control Sample T Water 6010B 500-173872

500-53491-1 FC COMPOSITE 6 T Solid 6010B 500-173848

500-53491-1 FC COMPOSITE 6 P Solid 6010B 500-173872

500-53491-2 FC D COMPOSITE 6 T Solid 6010B 500-173848

500-53491-2 FC D COMPOSITE 6 P Solid 6010B 500-173872

Analysis Batch:500-173984

LCS 500-173881/8-A Lab Control Sample T Solid 7471A 500-173881

MB 500-173881/7-A Method Blank T Solid 7471A 500-173881

500-53491-1 FC COMPOSITE 6 T Solid 7471A 500-173881

500-53491-2 FC D COMPOSITE 6 T Solid 7471A 500-173881

Analysis Batch:500-173997

LCS 500-173908/8-A Lab Control Sample T Water 7470A 500-173908

MB 500-173908/7-A Method Blank T Water 7470A 500-173908

LB 500-173836/1-C TCLP SPLPE Leachate Blank P Solid 7470A 500-173909

LB2 500-173838/1-C TCLP SPLPW Leachate Blank P Solid 7470A 500-173909

LCS 500-173909/8-A Lab Control Sample T Water 7470A 500-173909

MB 500-173909/7-A Method Blank T Water 7470A 500-173909

500-53491-1 FC COMPOSITE 6 P Solid 7470A 500-173909

500-53491-2 FC D COMPOSITE 6 P Solid 7470A 500-173909

500-53491-2DU Duplicate P Solid 7470A 500-173909

500-53491-2MS Matrix Spike P Solid 7470A 500-173909

500-53491-5 FC EB 6 T Water 7470A 500-173908

TestAmerica Chicago

Page 61 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

Report Basis

P = TCLP

T = Total

TestAmerica Chicago

Page 62 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

General Chemistry

Analysis Batch:500-173788

500-53491-1 FC COMPOSITE 6 T Solid Moisture

500-53491-2 FC D COMPOSITE 6 T Solid Moisture

Prep Batch: 500-173790

LCS 500-173790/2-A Lab Control Sample T Solid 3060A

LCS 500-173790/3-A Lab Control Sample T Solid 3060A

MB 500-173790/1-A Method Blank T Solid 3060A

500-53491-1 FC COMPOSITE 6 T Solid 3060A

500-53491-2 FC D COMPOSITE 6 T Solid 3060A

Analysis Batch:500-173793

LCS 500-173793/4 Lab Control Sample T Water 7196A

MB 500-173793/3 Method Blank T Water 7196A

500-53491-5 FC EB 6 T Water 7196A

500-53491-5MS Matrix Spike T Water 7196A

500-53491-5MSD Matrix Spike Duplicate T Water 7196A

Prep Batch: 500-173844

LCS 500-173844/2-A Lab Control Sample T Water 7.3.4

MB 500-173844/1-A Method Blank T Water 7.3.4

500-53491-5 FC EB 6 T Water 7.3.4

Analysis Batch:500-173845

LCS 500-173844/2-A Lab Control Sample T Water 9034 500-173844

MB 500-173844/1-A Method Blank T Water 9034 500-173844

500-53491-5 FC EB 6 T Water 9034 500-173844

Analysis Batch:500-173846

LCS 500-173846/2 Lab Control Sample T Water 9034

MB 500-173846/1 Method Blank T Water 9034

500-53491-5 FC EB 6 T Water 9034

Analysis Batch:500-173936

500-53491-1 FC COMPOSITE 6 T Solid 9045C

500-53491-2 FC D COMPOSITE 6 T Solid 9045C

Analysis Batch:500-173970

500-53491-1 FC COMPOSITE 6 T Solid SM 2540G

500-53491-2 FC D COMPOSITE 6 T Solid SM 2540G

Prep Batch: 500-173980

LCS 500-173980/2-A Lab Control Sample T Water 9010B

MB 500-173980/1-A Method Blank T Water 9010B

500-53491-5 FC EB 6 T Water 9010B

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QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

General Chemistry

Analysis Batch:500-174027

LCS 500-173790/2-A Lab Control Sample T Solid 7196A 500-173790

LCS 500-173790/3-A Lab Control Sample T Solid 7196A 500-173790

MB 500-173790/1-A Method Blank T Solid 7196A 500-173790

500-53491-1 FC COMPOSITE 6 T Solid 7196A 500-173790

500-53491-2 FC D COMPOSITE 6 T Solid 7196A 500-173790

Analysis Batch:500-174042

LCS 500-173980/2-A Lab Control Sample T Water 9014 500-173980

MB 500-173980/1-A Method Blank T Water 9014 500-173980

500-53491-5 FC EB 6 T Water 9014 500-173980

Analysis Batch:500-174071

500-53491-3 FC DISCRETE 6 T Solid Moisture

500-53491-4 FC D DISCRETE 6 T Solid Moisture

Prep Batch: 500-174096

LCS 500-174096/13-A Lab Control Sample T Solid 9010B

MB 500-174096/12-A Method Blank T Solid 9010B

500-53491-1 FC COMPOSITE 6 T Solid 9010B

500-53491-2 FC D COMPOSITE 6 T Solid 9010B

500-53491-2MS Matrix Spike T Solid 9010B

500-53491-2MSD Matrix Spike Duplicate T Solid 9010B

Prep Batch: 500-174100

LCS 500-174100/2-A Lab Control Sample T Solid 9030B

MB 500-174100/1-A Method Blank T Solid 9030B

500-53491-1 FC COMPOSITE 6 T Solid 9030B

500-53491-2 FC D COMPOSITE 6 T Solid 9030B

Prep Batch: 500-174101

LCS 500-174101/2-A Lab Control Sample T Solid 7.3.4

MB 500-174101/1-A Method Blank T Solid 7.3.4

500-53491-1 FC COMPOSITE 6 T Solid 7.3.4

500-53491-2 FC D COMPOSITE 6 T Solid 7.3.4

Analysis Batch:500-174144

LCS 500-174100/2-A Lab Control Sample T Solid 9034 500-174100

MB 500-174100/1-A Method Blank T Solid 9034 500-174100

500-53491-1 FC COMPOSITE 6 T Solid 9034 500-174100

500-53491-2 FC D COMPOSITE 6 T Solid 9034 500-174100

TestAmerica Chicago

Page 64 of 384 01/09/2013
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Client: Project Integration, Inc Job Number: 500-53491-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

General Chemistry

Analysis Batch:500-174145

LCS 500-174101/2-A Lab Control Sample T Solid 9034 500-174101

MB 500-174101/1-A Method Blank T Solid 9034 500-174101

500-53491-1 FC COMPOSITE 6 T Solid 9034 500-174101

500-53491-2 FC D COMPOSITE 6 T Solid 9034 500-174101

Analysis Batch:500-174173

LCS 500-174096/13-A Lab Control Sample T Solid 9014 500-174096

MB 500-174096/12-A Method Blank T Solid 9014 500-174096

500-53491-1 FC COMPOSITE 6 T Solid 9014 500-174096

500-53491-2 FC D COMPOSITE 6 T Solid 9014 500-174096

500-53491-2MS Matrix Spike T Solid 9014 500-174096

500-53491-2MSD Matrix Spike Duplicate T Solid 9014 500-174096

Analysis Batch:500-174336

500-53491-1 FC COMPOSITE 6 T Solid 1010

500-53491-2 FC D COMPOSITE 6 T Solid 1010

Prep Batch: 500-174369

LCS 500-174369/2-A Lab Control Sample T Solid 9071B

MB 500-174369/1-A Method Blank T Solid 9071B

500-53491-1 FC COMPOSITE 6 T Solid 9071B

500-53491-1MS Matrix Spike T Solid 9071B

500-53491-1MSD Matrix Spike Duplicate T Solid 9071B

500-53491-2 FC D COMPOSITE 6 T Solid 9071B

Analysis Batch:500-174372

LCS 500-174369/2-A Lab Control Sample T Solid 9071B 500-174369

MB 500-174369/1-A Method Blank T Solid 9071B 500-174369

500-53491-1 FC COMPOSITE 6 T Solid 9071B 500-174369

500-53491-1MS Matrix Spike T Solid 9071B 500-174369

500-53491-1MSD Matrix Spike Duplicate T Solid 9071B 500-174369

500-53491-2 FC D COMPOSITE 6 T Solid 9071B 500-174369

Prep Batch: 500-174563

LCS 500-174563/2-A Lab Control Sample T Water 1664A

MB 500-174563/1-A Method Blank T Water 1664A

500-53491-5 FC EB 6 T Water 1664A

Analysis Batch:500-174564

LCS 500-174563/2-A Lab Control Sample T Water 1664A 500-174563

MB 500-174563/1-A Method Blank T Water 1664A 500-174563

500-53491-5 FC EB 6 T Water 1664A 500-174563

TestAmerica Chicago

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QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

Report Basis

T = Total

TestAmerica Chicago

Page 66 of 384 01/09/2013
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Laboratory Chronicle

12/22/2012 11:30

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/19/2012 14:30 Received Date/Time: 500-53491-1 FC COMPOSITE 6

P:3010A 500-53491-A-1-D 500-173964 500-173872 12/26/2012 07:50 1 TAL CHI LAH

A:6010B 500-53491-A-1-D 500-173964 500-173872 12/26/2012 18:41 1 TAL CHI PJ

P:3050B 500-53491-A-1-C 500-173964 500-173848 12/24/2012 15:00 1 TAL CHI RL

A:6010B 500-53491-A-1-C 500-173964 500-173848 12/26/2012 23:57 1 TAL CHI PJ

P:7470A 500-53491-A-1-F 500-173997 500-173909 12/26/2012 13:00 1 TAL CHI BJB

A:7470A 500-53491-A-1-F 500-173997 500-173909 12/27/2012 09:57 1 TAL CHI BJB

P:7471A 500-53491-A-1-E 500-173984 500-173881 12/26/2012 14:00 1 TAL CHI BJB

A:7471A 500-53491-A-1-E 500-173984 500-173881 12/27/2012 08:55 1 TAL CHI BJB

A:1010 500-53491-A-1 500-174336 01/02/2013 09:30 1 TAL CHI APW

P:3060A 500-53491-A-1-A 500-174027 500-173790 12/22/2012 12:00 1 TAL CHI APW

A:7196A 500-53491-A-1-A 500-174027 500-173790 12/27/2012 12:51 1 TAL CHI APW

P:9010B 500-53491-A-1-G 500-174173 500-174096 12/28/2012 11:20 1 TAL CHI EAT

A:9014 500-53491-A-1-G 500-174173 500-174096 12/28/2012 15:31 1 TAL CHI EAT

P:7.3.4 500-53491-A-1-I 500-174145 500-174101 12/28/2012 11:57 1 TAL CHI CLM

A:9034 500-53491-A-1-I 500-174145 500-174101 12/28/2012 12:58 1 TAL CHI CLM

P:9030B 500-53491-A-1-H 500-174144 500-174100 12/28/2012 12:20 1 TAL CHI CLM

A:9034 500-53491-A-1-H 500-174144 500-174100 12/28/2012 14:43 1 TAL CHI CLM

A:9045C 500-53491-A-1 500-173936 12/26/2012 14:25 1 TAL CHI CLM

P:9071B 500-53491-A-1-J 500-174372 500-174369 01/04/2013 05:35 1 TAL CHI MTB

A:9071B 500-53491-A-1-J 500-174372 500-174369 01/04/2013 10:13 1 TAL CHI MTB

A:Moisture 500-53491-A-1 500-173788 12/22/2012 13:24 1 TAL CHI CMV

A:SM 2540G 500-53491-A-1 500-173970 12/27/2012 07:30 1 TAL CHI CMV

12/22/2012 11:30

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/19/2012 14:30 Received Date/Time: 500-53491-1 MS FC COMPOSITE 6

P:9071B 500-53491-A-1-K MS 500-174372 500-174369 01/04/2013 05:35 1 TAL CHI MTB

A:9071B 500-53491-A-1-K MS 500-174372 500-174369 01/04/2013 10:27 1 TAL CHI MTB

12/22/2012 11:30

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/19/2012 14:30 Received Date/Time: 500-53491-1 MSD FC COMPOSITE 6

P:9071B 500-53491-A-1-L 

MSD

500-174372 500-174369 01/04/2013 05:35 1 TAL CHI MTB

A:9071B 500-53491-A-1-L 

MSD

500-174372 500-174369 01/04/2013 10:42 1 TAL CHI MTB

TestAmerica Chicago A = Analytical Method P = Prep Method 

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Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/19/2012 14:40 Received Date/Time: 500-53491-2 FC D COMPOSITE 6

P:3010A 500-53491-A-2-D 500-173964 500-173872 12/26/2012 07:50 1 TAL CHI LAH

A:6010B 500-53491-A-2-D 500-173964 500-173872 12/26/2012 18:47 1 TAL CHI PJ

P:3050B 500-53491-A-2-C 500-173964 500-173848 12/24/2012 15:00 1 TAL CHI RL

A:6010B 500-53491-A-2-C 500-173964 500-173848 12/27/2012 00:03 1 TAL CHI PJ

P:7470A 500-53491-A-2-F 500-173997 500-173909 12/26/2012 13:00 1 TAL CHI BJB

A:7470A 500-53491-A-2-F 500-173997 500-173909 12/27/2012 09:58 1 TAL CHI BJB

P:7471A 500-53491-A-2-E 500-173984 500-173881 12/26/2012 14:00 1 TAL CHI BJB

A:7471A 500-53491-A-2-E 500-173984 500-173881 12/27/2012 09:04 1 TAL CHI BJB

A:1010 500-53491-A-2 500-174336 01/02/2013 10:52 1 TAL CHI APW

P:3060A 500-53491-A-2-A 500-174027 500-173790 12/22/2012 12:00 1 TAL CHI APW

A:7196A 500-53491-A-2-A 500-174027 500-173790 12/27/2012 12:53 1 TAL CHI APW

P:9010B 500-53491-A-2-I 500-174173 500-174096 12/28/2012 11:20 1 TAL CHI EAT

A:9014 500-53491-A-2-I 500-174173 500-174096 12/28/2012 15:31 1 TAL CHI EAT

P:7.3.4 500-53491-A-2-M 500-174145 500-174101 12/28/2012 12:01 1 TAL CHI CLM

A:9034 500-53491-A-2-M 500-174145 500-174101 12/28/2012 12:59 1 TAL CHI CLM

P:9030B 500-53491-A-2-L 500-174144 500-174100 12/28/2012 12:20 1 TAL CHI CLM

A:9034 500-53491-A-2-L 500-174144 500-174100 12/28/2012 14:44 1 TAL CHI CLM

A:9045C 500-53491-A-2 500-173936 12/26/2012 14:27 1 TAL CHI CLM

P:9071B 500-53491-A-2-N 500-174372 500-174369 01/04/2013 05:35 1 TAL CHI MTB

A:9071B 500-53491-A-2-N 500-174372 500-174369 01/04/2013 10:56 1 TAL CHI MTB

A:Moisture 500-53491-A-2 500-173788 12/22/2012 13:24 1 TAL CHI CMV

A:SM 2540G 500-53491-A-2 500-173970 12/27/2012 07:30 1 TAL CHI CMV

12/22/2012 11:30

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/19/2012 14:40 Received Date/Time: 500-53491-2 MS FC D COMPOSITE 6

P:7470A 500-53491-A-2-H MS 500-173997 500-173909 12/26/2012 13:00 1 TAL CHI BJB

A:7470A 500-53491-A-2-H MS 500-173997 500-173909 12/27/2012 10:02 1 TAL CHI BJB

P:9010B 500-53491-A-2-J MS 500-174173 500-174096 12/28/2012 11:20 1 TAL CHI EAT

A:9014 500-53491-A-2-J MS 500-174173 500-174096 12/28/2012 15:32 1 TAL CHI EAT

12/22/2012 11:30

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/19/2012 14:40 Received Date/Time: 500-53491-2 MSD FC D COMPOSITE 6

P:9010B 500-53491-A-2-K 

MSD

500-174173 500-174096 12/28/2012 11:20 1 TAL CHI EAT

A:9014 500-53491-A-2-K 

MSD

500-174173 500-174096 12/28/2012 15:32 1 TAL CHI EAT

TestAmerica Chicago A = Analytical Method P = Prep Method 

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Laboratory Chronicle

12/22/2012 11:30

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/19/2012 14:40 Received Date/Time: 500-53491-2 DU FC D COMPOSITE 6

P:7470A 500-53491-A-2-G DU 500-173997 500-173909 12/26/2012 13:00 1 TAL CHI BJB

A:7470A 500-53491-A-2-G DU 500-173997 500-173909 12/27/2012 10:00 1 TAL CHI BJB

12/22/2012 11:30

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/19/2012 14:20 Received Date/Time: 500-53491-3 FC DISCRETE 6

P:5030B 500-53491-A-3 500-173973 12/27/2012 13:36 1 TAL CHI DJD

A:8260B 500-53491-A-3 500-173973 12/27/2012 13:36 1 TAL CHI DJD

P:5030B 500-53491-A-3-A DL 500-174064 500-173990 12/27/2012 10:28 50 TAL CHI WRE

A:8260B 500-53491-A-3-A DL 500-174064 500-173990 12/28/2012 11:08 50 TAL CHI BDA

A:Moisture 500-53491-A-3 500-174071 12/28/2012 10:09 1 TAL CHI CMV

12/22/2012 11:30

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/19/2012 14:45 Received Date/Time: 500-53491-4 FC D DISCRETE 6

P:5030B 500-53491-A-4 500-173973 12/27/2012 13:59 1 TAL CHI DJD

A:8260B 500-53491-A-4 500-173973 12/27/2012 13:59 1 TAL CHI DJD

P:5030B 500-53491-A-4-A DL 500-174064 500-173990 12/27/2012 10:28 50 TAL CHI WRE

A:8260B 500-53491-A-4-A DL 500-174064 500-173990 12/28/2012 11:31 50 TAL CHI BDA

A:Moisture 500-53491-A-4 500-174071 12/28/2012 10:09 1 TAL CHI CMV

12/22/2012 11:30

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/19/2012 14:10 Received Date/Time: 500-53491-5 FC EB 6

P:5030B 500-53491-A-5 500-173987 12/27/2012 15:54 1 TAL CHI LM

A:8260B 500-53491-A-5 500-173987 12/27/2012 15:54 1 TAL CHI LM

P:3010A 500-53491-E-5-A 500-173963 500-173849 12/24/2012 14:30 1 TAL CHI RL

A:6010B 500-53491-E-5-A 500-173963 500-173849 12/26/2012 17:03 1 TAL CHI PJ

P:7470A 500-53491-E-5-B 500-173997 500-173908 12/26/2012 13:00 1 TAL CHI BJB

A:7470A 500-53491-E-5-B 500-173997 500-173908 12/27/2012 09:26 1 TAL CHI BJB

P:1664A 500-53491-H-5-A 500-174564 500-174563 01/08/2013 06:01 1 TAL CHI MTB

A:1664A 500-53491-H-5-A 500-174564 500-174563 01/08/2013 11:08 1 TAL CHI MTB

A:7196A 500-53491-F-5 500-173793 12/22/2012 14:12 1 TAL CHI APW

P:9010B 500-53491-D-5-A 500-174042 500-173980 12/27/2012 09:50 1 TAL CHI EAT

A:9014 500-53491-D-5-A 500-174042 500-173980 12/27/2012 14:45 1 TAL CHI EAT

P:7.3.4 500-53491-G-5-A 500-173845 500-173844 12/24/2012 08:45 1 TAL CHI CLB

A:9034 500-53491-G-5-A 500-173845 500-173844 12/24/2012 13:51 1 TAL CHI CLB

A:9034 500-53491-G-5 500-173846 12/24/2012 14:00 1 TAL CHI CLB

TestAmerica Chicago A = Analytical Method P = Prep Method 

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Laboratory Chronicle

12/22/2012 11:30

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/19/2012 14:10 Received Date/Time: 500-53491-5 MS FC EB 6

A:7196A 500-53491-F-5 MS 500-173793 12/22/2012 14:13 1 TAL CHI APW

12/22/2012 11:30

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/19/2012 14:10 Received Date/Time: 500-53491-5 MSD FC EB 6

A:7196A 500-53491-F-5 MSD 500-173793 12/22/2012 14:13 1 TAL CHI APW

12/22/2012 11:30

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/19/2012 00:00 Received Date/Time: 500-53491-6 TRIP BLANK

P:5030B 500-53491-A-6 500-173987 12/27/2012 15:28 1 TAL CHI LM

A:8260B 500-53491-A-6 500-173987 12/27/2012 15:28 1 TAL CHI LM

TestAmerica Chicago A = Analytical Method P = Prep Method 

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Laboratory Chronicle

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: N/A Received Date/Time: N/A

MB N/A

P:5030B MB 500-173973/5 500-173973 12/27/2012 10:33 1 TAL CHI DJD

A:8260B MB 500-173973/5 500-173973 12/27/2012 10:33 1 TAL CHI DJD

P:5030B MB 500-173987/7 500-173987 12/27/2012 14:10 1 TAL CHI LM

A:8260B MB 500-173987/7 500-173987 12/27/2012 14:10 1 TAL CHI LM

A:8260B MB 500-174064/6 500-174064 12/28/2012 10:45 1 TAL CHI BDA

P:3010A MB 500-173849/1-A 500-173963 500-173849 12/24/2012 14:30 1 TAL CHI RL

A:6010B MB 500-173849/1-A 500-173963 500-173849 12/26/2012 16:35 1 TAL CHI PJ

P:3050B MB 500-173848/1-A 500-173964 500-173848 12/24/2012 15:00 1 TAL CHI RL

A:6010B MB 500-173848/1-A 500-173964 500-173848 12/26/2012 21:54 1 TAL CHI PJ

P:7470A MB 500-173908/7-A 500-173997 500-173908 12/26/2012 13:00 1 TAL CHI BJB

A:7470A MB 500-173908/7-A 500-173997 500-173908 12/27/2012 08:41 1 TAL CHI BJB

P:7470A MB 500-173909/7-A 500-173997 500-173909 12/26/2012 13:00 1 TAL CHI BJB

A:7470A MB 500-173909/7-A 500-173997 500-173909 12/27/2012 09:28 1 TAL CHI BJB

P:7471A MB 500-173881/7-A 500-173984 500-173881 12/26/2012 14:00 1 TAL CHI BJB

A:7471A MB 500-173881/7-A 500-173984 500-173881 12/27/2012 08:17 1 TAL CHI BJB

P:1664A MB 500-174563/1-A 500-174564 500-174563 01/08/2013 05:35 1 TAL CHI MTB

A:1664A MB 500-174563/1-A 500-174564 500-174563 01/08/2013 11:00 1 TAL CHI MTB

A:7196A MB 500-173793/3 500-173793 12/22/2012 14:11 1 TAL CHI APW

P:3060A MB 500-173790/1-A 500-174027 500-173790 12/22/2012 12:00 1 TAL CHI APW

A:7196A MB 500-173790/1-A 500-174027 500-173790 12/27/2012 12:41 1 TAL CHI APW

P:9010B MB 500-173980/1-A 500-174042 500-173980 12/27/2012 09:50 1 TAL CHI EAT

A:9014 MB 500-173980/1-A 500-174042 500-173980 12/27/2012 14:40 1 TAL CHI EAT

P:9010B MB 500-174096/12-A 500-174173 500-174096 12/28/2012 11:20 1 TAL CHI EAT

A:9014 MB 500-174096/12-A 500-174173 500-174096 12/28/2012 15:30 1 TAL CHI EAT

P:7.3.4 MB 500-173844/1-A 500-173845 500-173844 12/24/2012 08:00 1 TAL CHI CLB

A:9034 MB 500-173844/1-A 500-173845 500-173844 12/24/2012 13:19 1 TAL CHI CLB

A:9034 MB 500-173846/1 500-173846 12/24/2012 13:19 1 TAL CHI CLB

P:7.3.4 MB 500-174101/1-A 500-174145 500-174101 12/28/2012 11:35 1 TAL CHI CLM

A:9034 MB 500-174101/1-A 500-174145 500-174101 12/28/2012 12:55 1 TAL CHI CLM

P:9030B MB 500-174100/1-A 500-174144 500-174100 12/28/2012 12:20 1 TAL CHI CLM

A:9034 MB 500-174100/1-A 500-174144 500-174100 12/28/2012 14:35 1 TAL CHI CLM

P:9071B MB 500-174369/1-A 500-174372 500-174369 01/04/2013 05:35 1 TAL CHI MTB

A:9071B MB 500-174369/1-A 500-174372 500-174369 01/04/2013 09:45 1 TAL CHI MTB

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: N/A Received Date/Time: N/A

LB N/A

P:3010A LB 500-173836/1-B 500-173964 500-173872 12/26/2012 07:50 1 TAL CHI LAH

A:6010B LB 500-173836/1-B 500-173964 500-173872 12/26/2012 17:12 1 TAL CHI PJ

P:7470A LB 500-173836/1-C 500-173997 500-173909 12/26/2012 13:00 1 TAL CHI BJB

A:7470A LB 500-173836/1-C 500-173997 500-173909 12/27/2012 09:49 1 TAL CHI BJB

TestAmerica Chicago A = Analytical Method P = Prep Method 

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Sample Date/Time: N/A Received Date/Time: N/A

LB2 N/A

P:3010A LB2 500-173838/1-B 500-173964 500-173872 12/26/2012 07:50 1 TAL CHI LAH

A:6010B LB2 500-173838/1-B 500-173964 500-173872 12/26/2012 17:18 1 TAL CHI PJ

P:7470A LB2 500-173838/1-C 500-173997 500-173909 12/26/2012 13:00 1 TAL CHI BJB

A:7470A LB2 500-173838/1-C 500-173997 500-173909 12/27/2012 09:51 1 TAL CHI BJB

TestAmerica Chicago A = Analytical Method P = Prep Method 

Page 72 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Laboratory Chronicle

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: N/A Received Date/Time: N/A

LCS N/A

P:5030B LCS 500-173973/6 500-173973 12/27/2012 10:56 1 TAL CHI DJD

A:8260B LCS 500-173973/6 500-173973 12/27/2012 10:56 1 TAL CHI DJD

P:5030B LCS 500-173987/4 500-173987 12/27/2012 12:46 1 TAL CHI LM

A:8260B LCS 500-173987/4 500-173987 12/27/2012 12:46 1 TAL CHI LM

A:8260B LCS 500-174064/4 500-174064 12/28/2012 10:00 1 TAL CHI BDA

P:3010A LCS 500-173849/2-A 500-173963 500-173849 12/24/2012 14:30 1 TAL CHI RL

A:6010B LCS 500-173849/2-A 500-173963 500-173849 12/26/2012 16:39 1 TAL CHI PJ

P:3010A LCS 500-173872/3-A 500-173964 500-173872 12/26/2012 07:50 1 TAL CHI LAH

A:6010B LCS 500-173872/3-A 500-173964 500-173872 12/26/2012 17:24 1 TAL CHI PJ

P:3050B LCS 500-173848/2-A 500-173964 500-173848 12/24/2012 15:00 1 TAL CHI RL

A:6010B LCS 500-173848/2-A 500-173964 500-173848 12/26/2012 22:00 1 TAL CHI PJ

P:7470A LCS 500-173908/8-A 500-173997 500-173908 12/26/2012 13:00 1 TAL CHI BJB

A:7470A LCS 500-173908/8-A 500-173997 500-173908 12/27/2012 08:43 1 TAL CHI BJB

P:7470A LCS 500-173909/8-A 500-173997 500-173909 12/26/2012 13:00 1 TAL CHI BJB

A:7470A LCS 500-173909/8-A 500-173997 500-173909 12/27/2012 09:30 1 TAL CHI BJB

P:7471A LCS 500-173881/8-A 500-173984 500-173881 12/26/2012 14:00 1 TAL CHI BJB

A:7471A LCS 500-173881/8-A 500-173984 500-173881 12/27/2012 08:19 1 TAL CHI BJB

P:1664A LCS 500-174563/2-A 500-174564 500-174563 01/08/2013 05:48 1 TAL CHI MTB

A:1664A LCS 500-174563/2-A 500-174564 500-174563 01/08/2013 11:04 1 TAL CHI MTB

A:7196A LCS 500-173793/4 500-173793 12/22/2012 14:11 1 TAL CHI APW

P:3060A LCS 500-173790/2-A 500-174027 500-173790 12/22/2012 12:00 1 TAL CHI APW

A:7196A LCS 500-173790/2-A 500-174027 500-173790 12/27/2012 12:42 1 TAL CHI APW

P:3060A LCS 500-173790/3-A 500-174027 500-173790 12/22/2012 12:00 50 TAL CHI APW

A:7196A LCS 500-173790/3-A 500-174027 500-173790 12/27/2012 12:42 50 TAL CHI APW

P:9010B LCS 500-173980/2-A 500-174042 500-173980 12/27/2012 09:50 1 TAL CHI EAT

A:9014 LCS 500-173980/2-A 500-174042 500-173980 12/27/2012 14:40 1 TAL CHI EAT

P:9010B LCS 500-174096/13-A 500-174173 500-174096 12/28/2012 11:20 1 TAL CHI EAT

A:9014 LCS 500-174096/13-A 500-174173 500-174096 12/28/2012 15:30 1 TAL CHI EAT

A:9034 LCS 500-173846/2 500-173846 12/24/2012 13:20 1 TAL CHI CLB

P:7.3.4 LCS 500-173844/2-A 500-173845 500-173844 12/24/2012 08:15 1 TAL CHI CLB

A:9034 LCS 500-173844/2-A 500-173845 500-173844 12/24/2012 13:29 1 TAL CHI CLB

P:7.3.4 LCS 500-174101/2-A 500-174145 500-174101 12/28/2012 11:38 1 TAL CHI CLM

A:9034 LCS 500-174101/2-A 500-174145 500-174101 12/28/2012 12:55 1 TAL CHI CLM

P:9030B LCS 500-174100/2-A 500-174144 500-174100 12/28/2012 12:20 1 TAL CHI CLM

A:9034 LCS 500-174100/2-A 500-174144 500-174100 12/28/2012 14:36 1 TAL CHI CLM

P:9071B LCS 500-174369/2-A 500-174372 500-174369 01/04/2013 05:35 1 TAL CHI MTB

A:9071B LCS 500-174369/2-A 500-174372 500-174369 01/04/2013 09:59 1 TAL CHI MTB

TestAmerica Chicago A = Analytical Method P = Prep Method 

Page 73 of 384 01/09/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53491-1

Laboratory Chronicle

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: N/A Received Date/Time: N/A

LCSD N/A

P:5030B LCSD 500-173973/7 500-173973 12/27/2012 11:19 1 TAL CHI DJD

A:8260B LCSD 500-173973/7 500-173973 12/27/2012 11:19 1 TAL CHI DJD

Lab References:

TAL CHI = TestAmerica Chicago

TestAmerica Chicago A = Analytical Method P = Prep Method 

Page 74 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1664 HEM_00060 04/26/13 Mallin / JTBaker, Lot E50600 / K19H00 (Purchased Reagent) HEM (Oil & Grease) 8000 mg/L

SGT-HEM 4000 mg/L

8260 IS WK_00384 12/18/12 12/04/12 1, Lot NA 5 mL 8260 IS SK_00027 5 mL 1,4-Dichlorobenzene-d4 250 ug/mL

1,4-Difluorobenzene 250 ug/mL

Chlorobenzene-d5 250 ug/mL

Pentafluorobenzene 250 ug/mL

.8260 IS SK_00027 08/31/14 RESTEK, Lot AO88671 (Purchased Reagent) 1,4-Dichlorobenzene-d4 250 ug/mL

1,4-Difluorobenzene 250 ug/mL

Chlorobenzene-d5 250 ug/mL

Pentafluorobenzene 250 ug/mL

8260 LOW IS_00103 12/03/12 11/19/12 MEOH, Lot DA946 20 mL 8260 IS SK_00026 4000 uL 1,4-Dichlorobenzene-d4 50 ug/mL

1,4-Difluorobenzene 50 ug/mL

Chlorobenzene-d5 50 ug/mL

Pentafluorobenzene 50 ug/mL

.8260 IS SK_00026 08/31/14 RESTEK, Lot AO88671 (Purchased Reagent) 1,4-Dichlorobenzene-d4 250 ug/mL

1,4-Difluorobenzene 250 ug/mL

Chlorobenzene-d5 250 ug/mL

Pentafluorobenzene 250 ug/mL

8260 LOW IS_00104 12/14/12 11/30/12 MEOH, Lot DA946 20 mL 8260 IS SK_00027 4000 uL 1,4-Dichlorobenzene-d4 50 ug/mL

1,4-Difluorobenzene 50 ug/mL

Chlorobenzene-d5 50 ug/mL

Pentafluorobenzene 50 ug/mL

.8260 IS SK_00027 08/31/14 RESTEK, Lot AO88671 (Purchased Reagent) 1,4-Dichlorobenzene-d4 250 ug/mL

1,4-Difluorobenzene 250 ug/mL

Chlorobenzene-d5 250 ug/mL

Pentafluorobenzene 250 ug/mL

8260 LOW SS_00105 12/03/12 11/19/12 MEOH, Lot DA946 20 mL 8260 SS SK_00031 4000 uL 1,2-Dichloroethane-d4 (Surr) 50 ug/mL

4-Bromofluorobenzene (Surr) 50 ug/mL

Dibromofluoromethane 50 ug/mL

Toluene-d8 (Surr) 50 ug/mL

.8260 SS SK_00031 07/31/14 RESTEK, Lot A088175 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

8260 LOW SS_00106 12/14/12 11/30/12 MEOH, Lot DA946 20 mL 8260 SS SK_00032 4000 uL 1,2-Dichloroethane-d4 (Surr) 50 ug/mL

4-Bromofluorobenzene (Surr) 50 ug/mL

Dibromofluoromethane 50 ug/mL

Toluene-d8 (Surr) 50 ug/mL

.8260 SS SK_00032 07/31/14 RESTEK, Lot A088175 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

8260 LOW SS_00107 12/27/12 12/13/12 MEOH, Lot DA946 20 mL 8260 SS SK_00032 4000 uL 1,2-Dichloroethane-d4 (Surr) 50 ug/mL

4-Bromofluorobenzene (Surr) 50 ug/mL

Dibromofluoromethane 50 ug/mL

Page 75 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Toluene-d8 (Surr) 50 ug/mL

.8260 SS SK_00032 07/31/14 RESTEK, Lot A088175 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

8260 LOW SS_00108 01/09/13 12/26/12 MEOH, Lot DA946 20 mL 8260 SS SK_00032 4000 uL 1,2-Dichloroethane-d4 (Surr) 50 ug/mL

4-Bromofluorobenzene (Surr) 50 ug/mL

Dibromofluoromethane 50 ug/mL

Toluene-d8 (Surr) 50 ug/mL

.8260 SS SK_00032 07/31/14 RESTEK, Lot A088175 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

8260 SS WK_00382 12/18/12 12/04/12 1, Lot NA 5 mL 8260 SS SK_00032 5 mL 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

.8260 SS SK_00032 07/31/14 RESTEK, Lot A088175 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

8260 STD WK_00212 12/03/12 11/19/12 METHANOL, Lot NA 2 mL 8260 STD STK_00033 2 mL 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Page 76 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

.8260 STD STK_00033 08/31/14 Restek, Lot A088677 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

Page 77 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

8260 STD WK_00215 12/18/12 12/04/12 METHANOL, Lot NA 2 mL 8260 STD STK_00033 2 mL 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

Page 78 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Page 79 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

.8260 STD STK_00033 08/31/14 Restek, Lot A088677 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Page 80 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

8260 STD WK_00216 12/25/12 12/11/12 METHANOL, Lot NA 2 mL 8260 STD STK_00033 2 mL 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

Page 81 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

.8260 STD STK_00033 08/31/14 Restek, Lot A088677 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

Page 82 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

ACR/NITRSTDWK_00205 11/26/12 11/19/12 METHANOL, Lot NA 2 mL ACRNITSTDSK_00032 2 mL Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

.ACRNITSTDSK_00032 12/31/12 Restek, Lot A090686 (Purchased Reagent) Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

ACR/NITRSTDWK_00210 12/11/12 12/04/12 METHANOL, Lot NA 2 mL ACRNITSTDSK_00033 2 mL Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

.ACRNITSTDSK_00033 01/31/13 Restek, Lot A091152 (Purchased Reagent) Acetonitrile 800 ug/mL

Page 83 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

ACR/NITRSTDWK_00212 12/18/12 12/11/12 METHANOL, Lot NA 2 mL ACRNITSTDSK_00034 2 mL Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

.ACRNITSTDSK_00034 02/28/13 Restek, Lot A091858 (Purchased Reagent) Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

APIX STD WK_00110 12/18/12 12/04/12 METHANOL, Lot DG596 2 mL APIX STD PT_00024 250 uL 2-Nitropropane 10000 ug/mL

3-Chloro-1-propene 250 ug/mL

Cyclohexanone 10000 ug/mL

Ethyl acetate 1250 ug/mL

Ethyl methacrylate 250 ug/mL

Iodomethane 250 ug/mL

Isobutyl alcohol 10000 ug/mL

Methacrylonitrile 250 ug/mL

Methyl methacrylate 250 ug/mL

n-Butanol 10000 ug/mL

Pentachloroethane 250 ug/mL

trans-1,4-Dichloro-2-butene 250 ug/mL

.APIX STD PT_00024 02/19/13 11/19/12 METHANOL, Lot NA 1 mL APIX STD SK_00005 1 mL 2-Nitropropane 80000 ug/mL

3-Chloro-1-propene 2000 ug/mL

Cyclohexanone 80000 ug/mL

Ethyl acetate 10000 ug/mL

Ethyl methacrylate 2000 ug/mL

Iodomethane 2000 ug/mL

Isobutyl alcohol 80000 ug/mL

Methacrylonitrile 2000 ug/mL

Methyl methacrylate 2000 ug/mL

n-Butanol 80000 ug/mL

Pentachloroethane 2000 ug/mL

trans-1,4-Dichloro-2-butene 2000 ug/mL

..APIX STD SK_00005 09/04/13 SUPELCO, Lot LB95279 (Purchased Reagent) 2-Nitropropane 80000 ug/mL

3-Chloro-1-propene 2000 ug/mL

Cyclohexanone 80000 ug/mL

Ethyl acetate 10000 ug/mL

Ethyl methacrylate 2000 ug/mL

Iodomethane 2000 ug/mL

Isobutyl alcohol 80000 ug/mL

Methacrylonitrile 2000 ug/mL

Methyl methacrylate 2000 ug/mL

n-Butanol 80000 ug/mL

Pentachloroethane 2000 ug/mL

trans-1,4-Dichloro-2-butene 2000 ug/mL

Page 84 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

GAS STD WK RE_00245 12/26/12 11/19/12 METHANOL, Lot NA 2 mL GAS STD SK_00027 2 mL Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

.GAS STD SK_00027 08/31/14 RESTEK, Lot A088739 (Purchased Reagent) Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

GAS STD WK RE_00251 12/11/12 12/04/12 METHANOL, Lot NA 2 mL GAS STD SK_00028 2 mL Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

.GAS STD SK_00028 08/31/14 RESTEK, Lot A088739 (Purchased Reagent) Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

GAS STD WK RE_00254 12/18/12 12/11/12 METHANOL, Lot NA 2 mL GAS STD SK_00028 2 mL Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

.GAS STD SK_00028 08/31/14 RESTEK, Lot A088739 (Purchased Reagent) Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

ICAL2++STDWK_00108 12/18/12 12/04/12 METHANOL, Lot NA 2 mL ICAL2STDSK_00023 2 mL 1,3,5-Trichlorobenzene 100 ug/mL

2-Chloro-1,3-butadiene 100 ug/mL

2-Methylnaphthalene 100 ug/mL

Butadiene 100 ug/mL

Cyclohexane 100 ug/mL

Page 85 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Ethyl ether 100 ug/mL

Hexane 100 ug/mL

Isopropyl ether 100 ug/mL

Methyl acetate 100 ug/mL

Methylcyclohexane 100 ug/mL

n-Heptane 100 ug/mL

.ICAL2STDSK_00023 05/31/14 Restek, Lot A088737 (Purchased Reagent) 1,3,5-Trichlorobenzene 100 ug/mL

2-Chloro-1,3-butadiene 100 ug/mL

2-Methylnaphthalene 100 ug/mL

Butadiene 100 ug/mL

Cyclohexane 100 ug/mL

Ethyl ether 100 ug/mL

Hexane 100 ug/mL

Isopropyl ether 100 ug/mL

Methyl acetate 100 ug/mL

Methylcyclohexane 100 ug/mL

n-Heptane 100 ug/mL

5 mL 8260 SS WK_00385 0.9624 1,2-Dichloroethane-d4 (Surr) 48.12 ug/L

uL

INST6 IS/SS_00134 01/01/13 12/21/12 1, Lot NA

4-Bromofluorobenzene (Surr) 48.12 ug/L

Dibromofluoromethane 48.12 ug/L

Toluene-d8 (Surr) 48.12 ug/L

.8260 SS WK_00385 01/01/13 12/18/12 1, Lot NA 5 mL 8260 SS SK_00032 5 mL 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

..8260 SS SK_00032 07/31/14 RESTEK, Lot A088175 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

KET/CS2 STDWK_00180 12/03/12 11/19/12 METHANOL, Lot NA 2 mL KET/CS2 SK_00013 2 mL 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

.KET/CS2 SK_00013 11/30/13 Restek, Lot A088681 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

KET/CS2 STDWK_00183 12/18/12 12/04/12 METHANOL, Lot NA 2 mL KET/CS2 SK_00013 2 mL 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

.KET/CS2 SK_00013 11/30/13 Restek, Lot A088681 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

Page 86 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

KET/CS2 STDWK_00184 12/25/12 12/11/12 METHANOL, Lot NA 2 mL KET/CS2 SK_00014 2 mL 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

.KET/CS2 SK_00014 11/30/13 Restek, Lot A088681 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

KET/CS2 STDWK_00185 01/09/13 12/26/12 METHANOL, Lot NA 2 mL KET/CS2 SK_00014 2 mL 2-Butanone (MEK) 100 ug/mL

Acetone 100 ug/mL

.KET/CS2 SK_00014 11/30/13 Restek, Lot A088681 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL

Acetone 100 ug/mL

level 1_00011 12/31/16 03/20/12 1, Lot CY647 1 mL level1std5ppm_00006 100 uL Benzene 0.5 ug/mL

Ethylbenzene 0.5 ug/mL

m-Xylene & p-Xylene 1 ug/mL

o-Xylene 0.5 ug/mL

Toluene 0.5 ug/mL

Trichloroethene 0.5 ug/mL

Vinyl chloride 0.5 ug/mL

.level1std5ppm_00006 02/28/12 03/22/11 1, Lot CY647 2 mL level18260wk_00006 100 uL Benzene 5 ug/mL

Ethylbenzene 5 ug/mL

m-Xylene & p-Xylene 10 ug/mL

o-Xylene 5 ug/mL

Toluene 5 ug/mL

Trichloroethene 5 ug/mL

level1gaswk_00006 100 uL Vinyl chloride 5 ug/mL

..level18260wk_00006 06/30/12 03/22/11 1, Lot NA 1 mL level18260sk_00001 1 mL Benzene 100 ug/mL

Ethylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

o-Xylene 100 ug/mL

Toluene 100 ug/mL

Trichloroethene 100 ug/mL

...level18260sk_00001 06/30/12 Restek, Lot AO67921 (Purchased Reagent) Benzene 100 ug/mL

Ethylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

o-Xylene 100 ug/mL

Toluene 100 ug/mL

Trichloroethene 100 ug/mL

..level1gaswk_00006 02/28/12 03/22/11 1, Lot CY647 2 mL level1gaspt_00005 100 uL Vinyl chloride 100 ug/mL

...level1gaspt_00005 02/28/12 03/22/11 MEOH, Lot NA 1 mL level1gassk_00001 1 mL Vinyl chloride 2000 ug/mL

....level1gassk_00001 02/28/12 SUPELCO, Lot LB65254 (Purchased Reagent) Vinyl chloride 2000 ug/mL

Page 87 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

LOAPIXSTDWK_00130 12/18/12 12/04/12 1, Lot DG596 1 mL APIX STD WK_00110 100 uL 2-Nitropropane 1000 ug/mL

3-Chloro-1-propene 25 ug/mL

Cyclohexanone 1000 ug/mL

Ethyl acetate 125 ug/mL

Ethyl methacrylate 25 ug/mL

Iodomethane 25 ug/mL

Isobutyl alcohol 1000 ug/mL

Methacrylonitrile 25 ug/mL

Methyl methacrylate 25 ug/mL

n-Butanol 1000 ug/mL

Pentachloroethane 25 ug/mL

trans-1,4-Dichloro-2-butene 25 ug/mL

.APIX STD WK_00110 12/18/12 12/04/12 METHANOL, Lot DG596 2 mL APIX STD PT_00024 250 uL 2-Nitropropane 10000 ug/mL

3-Chloro-1-propene 250 ug/mL

Cyclohexanone 10000 ug/mL

Ethyl acetate 1250 ug/mL

Ethyl methacrylate 250 ug/mL

Iodomethane 250 ug/mL

Isobutyl alcohol 10000 ug/mL

Methacrylonitrile 250 ug/mL

Methyl methacrylate 250 ug/mL

n-Butanol 10000 ug/mL

Pentachloroethane 250 ug/mL

trans-1,4-Dichloro-2-butene 250 ug/mL

..APIX STD PT_00024 02/19/13 11/19/12 METHANOL, Lot NA 1 mL APIX STD SK_00005 1 mL 2-Nitropropane 80000 ug/mL

3-Chloro-1-propene 2000 ug/mL

Cyclohexanone 80000 ug/mL

Ethyl acetate 10000 ug/mL

Ethyl methacrylate 2000 ug/mL

Iodomethane 2000 ug/mL

Isobutyl alcohol 80000 ug/mL

Methacrylonitrile 2000 ug/mL

Methyl methacrylate 2000 ug/mL

n-Butanol 80000 ug/mL

Pentachloroethane 2000 ug/mL

trans-1,4-Dichloro-2-butene 2000 ug/mL

...APIX STD SK_00005 09/04/13 SUPELCO, Lot LB95279 (Purchased Reagent) 2-Nitropropane 80000 ug/mL

3-Chloro-1-propene 2000 ug/mL

Cyclohexanone 80000 ug/mL

Ethyl acetate 10000 ug/mL

Ethyl methacrylate 2000 ug/mL

Iodomethane 2000 ug/mL

Isobutyl alcohol 80000 ug/mL

Methacrylonitrile 2000 ug/mL

Methyl methacrylate 2000 ug/mL

n-Butanol 80000 ug/mL

Pentachloroethane 2000 ug/mL

trans-1,4-Dichloro-2-butene 2000 ug/mL

Page 88 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

LOICAL2STDWK_00123 12/18/12 12/04/12 1, Lot DG596 1 mL ICAL2++STDWK_00108 50 uL 1,3,5-Trichlorobenzene 5 ug/mL

2-Chloro-1,3-butadiene 5 ug/mL

2-Methylnaphthalene 5 ug/mL

Butadiene 5 ug/mL

Cyclohexane 5 ug/mL

Ethyl ether 5 ug/mL

Hexane 5 ug/mL

Isopropyl ether 5 ug/mL

Methyl acetate 5 ug/mL

Methylcyclohexane 5 ug/mL

n-Heptane 5 ug/mL

.ICAL2++STDWK_00108 12/18/12 12/04/12 METHANOL, Lot NA 2 mL ICAL2STDSK_00023 2 mL 1,3,5-Trichlorobenzene 100 ug/mL

2-Chloro-1,3-butadiene 100 ug/mL

2-Methylnaphthalene 100 ug/mL

Butadiene 100 ug/mL

Cyclohexane 100 ug/mL

Ethyl ether 100 ug/mL

Hexane 100 ug/mL

Isopropyl ether 100 ug/mL

Methyl acetate 100 ug/mL

Methylcyclohexane 100 ug/mL

n-Heptane 100 ug/mL

..ICAL2STDSK_00023 05/31/14 Restek, Lot A088737 (Purchased Reagent) 1,3,5-Trichlorobenzene 100 ug/mL

2-Chloro-1,3-butadiene 100 ug/mL

2-Methylnaphthalene 100 ug/mL

Butadiene 100 ug/mL

Cyclohexane 100 ug/mL

Ethyl ether 100 ug/mL

Hexane 100 ug/mL

Isopropyl ether 100 ug/mL

Methyl acetate 100 ug/mL

Methylcyclohexane 100 ug/mL

n-Heptane 100 ug/mL

LOW8260SS WK_00044 12/18/12 12/04/12 1, Lot DA057 1 mL 8260 SS WK_00382 200 uL 1,2-Dichloroethane-d4 (Surr) 50 ug/mL

4-Bromofluorobenzene (Surr) 50 ug/mL

Dibromofluoromethane 50 ug/mL

Toluene-d8 (Surr) 50 ug/mL

.8260 SS WK_00382 12/18/12 12/04/12 1, Lot NA 5 mL 8260 SS SK_00032 5 mL 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

..8260 SS SK_00032 07/31/14 RESTEK, Lot A088175 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

LOW8260STD WK_00211 11/26/12 11/20/12 1, Lot DG596 1 mL 8260 STD WK_00212 50 uL 1,1,1,2-Tetrachloroethane 5 ug/mL

1,1,1-Trichloroethane 5 ug/mL

Page 89 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1,1,2,2-Tetrachloroethane 5 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

5 ug/mL

1,1,2-Trichloroethane 5 ug/mL

1,1-Dichloroethane 5 ug/mL

1,1-Dichloroethene 5 ug/mL

1,1-Dichloropropene 5 ug/mL

1,2,3-Trichlorobenzene 5 ug/mL

1,2,3-Trichloropropane 5 ug/mL

1,2,4-Trichlorobenzene 5 ug/mL

1,2,4-Trimethylbenzene 5 ug/mL

1,2-Dibromo-3-Chloropropane 5 ug/mL

1,2-Dichlorobenzene 5 ug/mL

1,2-Dichloroethane 5 ug/mL

1,2-Dichloropropane 5 ug/mL

1,3,5-Trimethylbenzene 5 ug/mL

1,3-Dichlorobenzene 5 ug/mL

1,3-Dichloropropane 5 ug/mL

1,4-Dichlorobenzene 5 ug/mL

1-Chlorohexane 5 ug/mL

2,2-Dichloropropane 5 ug/mL

2-Chlorotoluene 5 ug/mL

4-Chlorotoluene 5 ug/mL

4-Isopropyltoluene 5 ug/mL

Benzene 5 ug/mL

Bromobenzene 5 ug/mL

Bromoform 5 ug/mL

Carbon tetrachloride 5 ug/mL

Chlorobenzene 5 ug/mL

Chlorobromomethane 5 ug/mL

Chlorodibromomethane 5 ug/mL

Chloroform 5 ug/mL

cis-1,2-Dichloroethene 5 ug/mL

cis-1,3-Dichloropropene 5 ug/mL

Dibromomethane 5 ug/mL

Dichlorobromomethane 5 ug/mL

Ethylbenzene 5 ug/mL

Ethylene Dibromide 5 ug/mL

Hexachlorobutadiene 5 ug/mL

Isopropylbenzene 5 ug/mL

m-Xylene & p-Xylene 10 ug/mL

Methyl tert-butyl ether 5 ug/mL

Methylene Chloride 5 ug/mL

n-Butylbenzene 5 ug/mL

N-Propylbenzene 5 ug/mL

Naphthalene 5 ug/mL

o-Xylene 5 ug/mL

sec-Butylbenzene 5 ug/mL

Page 90 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Styrene 5 ug/mL

tert-Butylbenzene 5 ug/mL

Tetrachloroethene 5 ug/mL

Tetrahydrofuran 5 ug/mL

Toluene 5 ug/mL

trans-1,2-Dichloroethene 5 ug/mL

trans-1,3-Dichloropropene 5 ug/mL

Trichloroethene 5 ug/mL

GAS STD WK RE_00245 50 uL Bromomethane 5 ug/mL

Chloroethane 5 ug/mL

Chloromethane 5 ug/mL

Dichlorodifluoromethane 5 ug/mL

Dichlorofluoromethane 5 ug/mL

Trichlorofluoromethane 5 ug/mL

Vinyl chloride 5 ug/mL

KET/CS2 STDWK_00180 50 uL 2-Butanone (MEK) 5 ug/mL

2-Hexanone 5 ug/mL

4-Methyl-2-pentanone (MIBK) 5 ug/mL

Acetone 5 ug/mL

Carbon disulfide 5 ug/mL

VA/2CEVESTDWK_00175 50 uL 2-Chloroethyl vinyl ether 5 ug/mL

Vinyl acetate 5 ug/mL

.8260 STD WK_00212 12/03/12 11/19/12 METHANOL, Lot NA 2 mL 8260 STD STK_00033 2 mL 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Page 91 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

..8260 STD STK_00033 08/31/14 Restek, Lot A088677 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

Page 92 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

.GAS STD WK RE_00245 12/26/12 11/19/12 METHANOL, Lot NA 2 mL GAS STD SK_00027 2 mL Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Page 93 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Vinyl chloride 100 ug/mL

..GAS STD SK_00027 08/31/14 RESTEK, Lot A088739 (Purchased Reagent) Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

.KET/CS2 STDWK_00180 12/03/12 11/19/12 METHANOL, Lot NA 2 mL KET/CS2 SK_00013 2 mL 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

..KET/CS2 SK_00013 11/30/13 Restek, Lot A088681 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

.VA/2CEVESTDWK_00175 11/26/12 11/19/12 METHANOL, Lot DG860 2 mL 2-CEVE STD PT_00023 100 uL 2-Chloroethyl vinyl ether 100 ug/mL

VA STD PT_00024 100 uL Vinyl acetate 100 ug/mL

..2-CEVE STD PT_00023 01/08/13 10/08/12 METHANOL, Lot NA 1 mL 2-CEVESTDSK_00005 1 mL 2-Chloroethyl vinyl ether 2000 ug/mL

...2-CEVESTDSK_00005 11/30/16 Restek, Lot A085117 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL

..VA STD PT_00024 01/10/13 10/11/12 METHANOL, Lot NA 1 mL VA STD SK_00007 1 mL Vinyl acetate 2000 ug/mL

...VA STD SK_00007 03/31/14 RESTEK, Lot A090525 (Purchased Reagent) Vinyl acetate 2000 ug/mL

LOW8260STD WK_00214 12/11/12 12/04/12 1, Lot DG860 1 mL 8260 STD WK_00215 50 uL 1,1,1,2-Tetrachloroethane 5 ug/mL

1,1,1-Trichloroethane 5 ug/mL

1,1,2,2-Tetrachloroethane 5 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

5 ug/mL

1,1,2-Trichloroethane 5 ug/mL

1,1-Dichloroethane 5 ug/mL

1,1-Dichloroethene 5 ug/mL

1,1-Dichloropropene 5 ug/mL

1,2,3-Trichlorobenzene 5 ug/mL

1,2,3-Trichloropropane 5 ug/mL

1,2,4-Trichlorobenzene 5 ug/mL

1,2,4-Trimethylbenzene 5 ug/mL

1,2-Dibromo-3-Chloropropane 5 ug/mL

1,2-Dichlorobenzene 5 ug/mL

1,2-Dichloroethane 5 ug/mL

1,2-Dichloropropane 5 ug/mL

1,3,5-Trimethylbenzene 5 ug/mL

1,3-Dichlorobenzene 5 ug/mL

1,3-Dichloropropane 5 ug/mL

1,4-Dichlorobenzene 5 ug/mL

1-Chlorohexane 5 ug/mL

2,2-Dichloropropane 5 ug/mL

2-Chlorotoluene 5 ug/mL

Page 94 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

4-Chlorotoluene 5 ug/mL

4-Isopropyltoluene 5 ug/mL

Benzene 5 ug/mL

Bromobenzene 5 ug/mL

Bromoform 5 ug/mL

Carbon tetrachloride 5 ug/mL

Chlorobenzene 5 ug/mL

Chlorobromomethane 5 ug/mL

Chlorodibromomethane 5 ug/mL

Chloroform 5 ug/mL

cis-1,2-Dichloroethene 5 ug/mL

cis-1,3-Dichloropropene 5 ug/mL

Dibromomethane 5 ug/mL

Dichlorobromomethane 5 ug/mL

Ethylbenzene 5 ug/mL

Ethylene Dibromide 5 ug/mL

Hexachlorobutadiene 5 ug/mL

Isopropylbenzene 5 ug/mL

m-Xylene & p-Xylene 10 ug/mL

Methyl tert-butyl ether 5 ug/mL

Methylene Chloride 5 ug/mL

n-Butylbenzene 5 ug/mL

N-Propylbenzene 5 ug/mL

Naphthalene 5 ug/mL

o-Xylene 5 ug/mL

sec-Butylbenzene 5 ug/mL

Styrene 5 ug/mL

tert-Butylbenzene 5 ug/mL

Tetrachloroethene 5 ug/mL

Tetrahydrofuran 5 ug/mL

Toluene 5 ug/mL

trans-1,2-Dichloroethene 5 ug/mL

trans-1,3-Dichloropropene 5 ug/mL

Trichloroethene 5 ug/mL

GAS STD WK RE_00251 50 uL Bromomethane 5 ug/mL

Chloroethane 5 ug/mL

Chloromethane 5 ug/mL

Dichlorodifluoromethane 5 ug/mL

Dichlorofluoromethane 5 ug/mL

Trichlorofluoromethane 5 ug/mL

Vinyl chloride 5 ug/mL

KET/CS2 STDWK_00183 50 uL 2-Butanone (MEK) 5 ug/mL

2-Hexanone 5 ug/mL

4-Methyl-2-pentanone (MIBK) 5 ug/mL

Acetone 5 ug/mL

Carbon disulfide 5 ug/mL

VA/2CEVESTDWK_00178 50 uL 2-Chloroethyl vinyl ether 5 ug/mL

Vinyl acetate 5 ug/mL

Page 95 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

.8260 STD WK_00215 12/18/12 12/04/12 METHANOL, Lot NA 2 mL 8260 STD STK_00033 2 mL 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

Page 96 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

..8260 STD STK_00033 08/31/14 Restek, Lot A088677 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Page 97 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

.GAS STD WK RE_00251 12/11/12 12/04/12 METHANOL, Lot NA 2 mL GAS STD SK_00028 2 mL Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

..GAS STD SK_00028 08/31/14 RESTEK, Lot A088739 (Purchased Reagent) Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

.KET/CS2 STDWK_00183 12/18/12 12/04/12 METHANOL, Lot NA 2 mL KET/CS2 SK_00013 2 mL 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

..KET/CS2 SK_00013 11/30/13 Restek, Lot A088681 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

.VA/2CEVESTDWK_00178 12/18/12 12/04/12 METHANOL, Lot DG860 2 mL 2-CEVE STD PT_00024 100 uL 2-Chloroethyl vinyl ether 100 ug/mL

VA STD PT_00025 100 uL Vinyl acetate 100 ug/mL

..2-CEVE STD PT_00024 02/21/13 11/21/12 METHANOL, Lot NA 1 mL 2-CEVESTDSK_00005 1 mL 2-Chloroethyl vinyl ether 2000 ug/mL

...2-CEVESTDSK_00005 11/30/16 Restek, Lot A085117 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL

Page 98 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

..VA STD PT_00025 02/21/13 11/21/12 METHANOL, Lot NA 1 mL VA STD SK_00007 1 mL Vinyl acetate 2000 ug/mL

...VA STD SK_00007 03/31/14 RESTEK, Lot A090525 (Purchased Reagent) Vinyl acetate 2000 ug/mL

LOW8260STD WK_00215 12/18/12 12/11/12 1, Lot DG860 1 mL 8260 STD WK_00216 50 uL 1,1,1,2-Tetrachloroethane 5 ug/mL

1,1,1-Trichloroethane 5 ug/mL

1,1,2,2-Tetrachloroethane 5 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

5 ug/mL

1,1,2-Trichloroethane 5 ug/mL

1,1-Dichloroethane 5 ug/mL

1,1-Dichloroethene 5 ug/mL

1,1-Dichloropropene 5 ug/mL

1,2,3-Trichlorobenzene 5 ug/mL

1,2,3-Trichloropropane 5 ug/mL

1,2,4-Trichlorobenzene 5 ug/mL

1,2,4-Trimethylbenzene 5 ug/mL

1,2-Dibromo-3-Chloropropane 5 ug/mL

1,2-Dichlorobenzene 5 ug/mL

1,2-Dichloroethane 5 ug/mL

1,2-Dichloropropane 5 ug/mL

1,3,5-Trimethylbenzene 5 ug/mL

1,3-Dichlorobenzene 5 ug/mL

1,3-Dichloropropane 5 ug/mL

1,4-Dichlorobenzene 5 ug/mL

1-Chlorohexane 5 ug/mL

2,2-Dichloropropane 5 ug/mL

2-Chlorotoluene 5 ug/mL

4-Chlorotoluene 5 ug/mL

4-Isopropyltoluene 5 ug/mL

Benzene 5 ug/mL

Bromobenzene 5 ug/mL

Bromoform 5 ug/mL

Carbon tetrachloride 5 ug/mL

Chlorobenzene 5 ug/mL

Chlorobromomethane 5 ug/mL

Chlorodibromomethane 5 ug/mL

Chloroform 5 ug/mL

cis-1,2-Dichloroethene 5 ug/mL

cis-1,3-Dichloropropene 5 ug/mL

Dibromomethane 5 ug/mL

Dichlorobromomethane 5 ug/mL

Ethylbenzene 5 ug/mL

Ethylene Dibromide 5 ug/mL

Hexachlorobutadiene 5 ug/mL

Isopropylbenzene 5 ug/mL

m-Xylene & p-Xylene 10 ug/mL

Methyl tert-butyl ether 5 ug/mL

Methylene Chloride 5 ug/mL

n-Butylbenzene 5 ug/mL

Page 99 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

N-Propylbenzene 5 ug/mL

Naphthalene 5 ug/mL

o-Xylene 5 ug/mL

sec-Butylbenzene 5 ug/mL

Styrene 5 ug/mL

tert-Butylbenzene 5 ug/mL

Tetrachloroethene 5 ug/mL

Tetrahydrofuran 5 ug/mL

Toluene 5 ug/mL

trans-1,2-Dichloroethene 5 ug/mL

trans-1,3-Dichloropropene 5 ug/mL

Trichloroethene 5 ug/mL

GAS STD WK RE_00254 50 uL Bromomethane 5 ug/mL

Chloroethane 5 ug/mL

Chloromethane 5 ug/mL

Dichlorodifluoromethane 5 ug/mL

Dichlorofluoromethane 5 ug/mL

Trichlorofluoromethane 5 ug/mL

Vinyl chloride 5 ug/mL

KET/CS2 STDWK_00184 50 uL 2-Butanone (MEK) 5 ug/mL

2-Hexanone 5 ug/mL

4-Methyl-2-pentanone (MIBK) 5 ug/mL

Acetone 5 ug/mL

Carbon disulfide 5 ug/mL

VA/2CEVESTDWK_00179 50 uL 2-Chloroethyl vinyl ether 5 ug/mL

Vinyl acetate 5 ug/mL

.8260 STD WK_00216 12/25/12 12/11/12 METHANOL, Lot NA 2 mL 8260 STD STK_00033 2 mL 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

Page 100 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

..8260 STD STK_00033 08/31/14 Restek, Lot A088677 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

Page 101 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

.GAS STD WK RE_00254 12/18/12 12/11/12 METHANOL, Lot NA 2 mL GAS STD SK_00028 2 mL Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Page 102 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

..GAS STD SK_00028 08/31/14 RESTEK, Lot A088739 (Purchased Reagent) Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

.KET/CS2 STDWK_00184 12/25/12 12/11/12 METHANOL, Lot NA 2 mL KET/CS2 SK_00014 2 mL 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

..KET/CS2 SK_00014 11/30/13 Restek, Lot A088681 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

.VA/2CEVESTDWK_00179 12/25/12 12/11/12 METHANOL, Lot DG860 2 mL 2-CEVE STD PT_00024 100 uL 2-Chloroethyl vinyl ether 100 ug/mL

VA STD PT_00025 100 uL Vinyl acetate 100 ug/mL

..2-CEVE STD PT_00024 02/21/13 11/21/12 METHANOL, Lot NA 1 mL 2-CEVESTDSK_00005 1 mL 2-Chloroethyl vinyl ether 2000 ug/mL

...2-CEVESTDSK_00005 11/30/16 Restek, Lot A085117 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL

..VA STD PT_00025 02/21/13 11/21/12 METHANOL, Lot NA 1 mL VA STD SK_00007 1 mL Vinyl acetate 2000 ug/mL

...VA STD SK_00007 03/31/14 RESTEK, Lot A090525 (Purchased Reagent) Vinyl acetate 2000 ug/mL

LOWACRSTD WK_00190 11/26/12 11/20/12 MEOH, Lot DG596 1 mL ACR/NITRSTDWK_00205 100 uL Acetonitrile 80 ug/mL

Acrolein 400 ug/mL

Acrylonitrile 80 ug/mL

Propionitrile 80 ug/mL

.ACR/NITRSTDWK_00205 11/26/12 11/19/12 METHANOL, Lot NA 2 mL ACRNITSTDSK_00032 2 mL Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

..ACRNITSTDSK_00032 12/31/12 Restek, Lot A090686 (Purchased Reagent) Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

LOWACRSTD WK_00192 12/11/12 12/04/12 MEOH, Lot DG860 1 mL ACR/NITRSTDWK_00210 100 uL Acetonitrile 80 ug/mL

Acrolein 400 ug/mL

Acrylonitrile 80 ug/mL

Propionitrile 80 ug/mL

.ACR/NITRSTDWK_00210 12/11/12 12/04/12 METHANOL, Lot NA 2 mL ACRNITSTDSK_00033 2 mL Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Page 103 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Propionitrile 800 ug/mL

..ACRNITSTDSK_00033 01/31/13 Restek, Lot A091152 (Purchased Reagent) Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

LOWACRSTD WK_00193 12/18/12 12/11/12 MEOH, Lot DG860 1 mL ACR/NITRSTDWK_00212 100 uL Acetonitrile 80 ug/mL

Acrolein 400 ug/mL

Acrylonitrile 80 ug/mL

Propionitrile 80 ug/mL

.ACR/NITRSTDWK_00212 12/18/12 12/11/12 METHANOL, Lot NA 2 mL ACRNITSTDSK_00034 2 mL Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

..ACRNITSTDSK_00034 02/28/13 Restek, Lot A091858 (Purchased Reagent) Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

M11FSTKHG_00001 05/31/17 ULTRA, Lot L00365 (Purchased Reagent) Mercury 1000 ug/mL

M12ASTKHG_00001 01/01/13 Inorganic Ventures, Lot E2-HG02091 (Purchased Reagent) Mercury 1000 ug/mL

M12JSPKIC_00002 05/23/13 10/04/12 1, Lot N\A 500 mL M12ESTKIC_00003 3 mL As 10 ug/mL

M12ESTKIC_00006 4 mL Lead 10 ug/mL

M12ESTKIC_00010 2.5 mL Tl 10 ug/mL

M12ESTKIC_00011 50 mL Al 200 ug/mL

Barium 200 ug/mL

Ca 1000 ug/mL

K 1000 ug/mL

Mg 1000 ug/mL

Na 1000 ug/mL

M12ESTKIC_00012 50 mL As 10 ug/mL

B 100 ug/mL

Be 5 ug/mL

Bi 50 ug/mL

Cd 5 ug/mL

Chromium 20 ug/mL

Co 50 ug/mL

Copper 25 ug/mL

Fe 100 ug/mL

Lead 10 ug/mL

Li 50 ug/mL

Mn 50 ug/mL

Nickel 50 ug/mL

Se 10 ug/mL

Sr 100 ug/mL

Tl 10 ug/mL

Vanadium 50 ug/mL

Zinc 50 ug/mL

Page 104 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

M12ESTKIC_00013 50 mL Ag 5 ug/mL

Mo 100 ug/mL

Sb 50 ug/mL

Si 500 ug/mL

Sn 100 ug/mL

Ti 100 ug/mL

M12ISTKIC_00004 4.5 mL Se 10 ug/mL

.M12ESTKIC_00003 06/01/13 IV, Lot F2-AS02083 (Purchased Reagent) As 1000 ug/mL

.M12ESTKIC_00006 06/01/13 IV, Lot F2-PB03035 (Purchased Reagent) Lead 1000 ug/mL

.M12ESTKIC_00010 06/01/13 IV, Lot E2-TL01124 (Purchased Reagent) Tl 1000 ug/mL

.M12ESTKIC_00011 05/23/13 EE, Lot 1214205 (Purchased Reagent) Al 2000 ug/mL

Barium 2000 ug/mL

Ca 10000 ug/mL

K 10000 ug/mL

Mg 10000 ug/mL

Na 10000 ug/mL

.M12ESTKIC_00012 05/23/13 EE, Lot 1214206 (Purchased Reagent) As 40 ug/mL

B 1000 ug/mL

Be 50 ug/mL

Bi 500 ug/mL

Cd 50 ug/mL

Chromium 200 ug/mL

Co 500 ug/mL

Copper 250 ug/mL

Fe 1000 ug/mL

Lead 20 ug/mL

Li 500 ug/mL

Mn 500 ug/mL

Nickel 500 ug/mL

Se 10 ug/mL

Sr 1000 ug/mL

Tl 50 ug/mL

Vanadium 500 ug/mL

Zinc 500 ug/mL

.M12ESTKIC_00013 05/23/13 EE, Lot 1214331 (Purchased Reagent) Ag 50 ug/mL

Mo 1000 ug/mL

Sb 500 ug/mL

Si 5000 ug/mL

Sn 1000 ug/mL

Ti 1000 ug/mL

.M12ISTKIC_00004 09/01/13 IV, Lot E2-SE02033 (Purchased Reagent) Se 1000 ug/mL

M12KSPKIC_00001 05/23/13 11/20/12 1, Lot N\A 500 mL M12ESTKIC_00003 3 mL As 10 ug/mL

M12ESTKIC_00006 4 mL Lead 10 ug/mL

M12ESTKIC_00010 2.5 mL Tl 10 ug/mL

M12ESTKIC_00011 50 mL Al 200 ug/mL

Barium 200 ug/mL

Ca 1000 ug/mL

Page 105 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

K 1000 ug/mL

Mg 1000 ug/mL

Na 1000 ug/mL

M12ESTKIC_00012 50 mL As 10 ug/mL

B 100 ug/mL

Be 5 ug/mL

Bi 50 ug/mL

Cd 5 ug/mL

Chromium 20 ug/mL

Co 50 ug/mL

Copper 25 ug/mL

Fe 100 ug/mL

Lead 10 ug/mL

Li 50 ug/mL

Mn 50 ug/mL

Nickel 50 ug/mL

Se 10 ug/mL

Sr 100 ug/mL

Tl 10 ug/mL

Vanadium 50 ug/mL

Zinc 50 ug/mL

M12ESTKIC_00013 50 mL Ag 5 ug/mL

Mo 100 ug/mL

Sb 50 ug/mL

Si 500 ug/mL

Sn 100 ug/mL

Ti 100 ug/mL

M12ISTKIC_00004 4.5 mL Se 10 ug/mL

.M12ESTKIC_00003 06/01/13 IV, Lot F2-AS02083 (Purchased Reagent) As 1000 ug/mL

.M12ESTKIC_00006 06/01/13 IV, Lot F2-PB03035 (Purchased Reagent) Lead 1000 ug/mL

.M12ESTKIC_00010 06/01/13 IV, Lot E2-TL01124 (Purchased Reagent) Tl 1000 ug/mL

.M12ESTKIC_00011 05/23/13 EE, Lot 1214205 (Purchased Reagent) Al 2000 ug/mL

Barium 2000 ug/mL

Ca 10000 ug/mL

K 10000 ug/mL

Mg 10000 ug/mL

Na 10000 ug/mL

.M12ESTKIC_00012 05/23/13 EE, Lot 1214206 (Purchased Reagent) As 40 ug/mL

B 1000 ug/mL

Be 50 ug/mL

Bi 500 ug/mL

Cd 50 ug/mL

Chromium 200 ug/mL

Co 500 ug/mL

Copper 250 ug/mL

Fe 1000 ug/mL

Lead 20 ug/mL

Li 500 ug/mL

Page 106 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Mn 500 ug/mL

Nickel 500 ug/mL

Se 10 ug/mL

Sr 1000 ug/mL

Tl 50 ug/mL

Vanadium 500 ug/mL

Zinc 500 ug/mL

.M12ESTKIC_00013 05/23/13 EE, Lot 1214331 (Purchased Reagent) Ag 50 ug/mL

Mo 1000 ug/mL

Sb 500 ug/mL

Si 5000 ug/mL

Sn 1000 ug/mL

Ti 1000 ug/mL

.M12ISTKIC_00004 09/01/13 IV, Lot E2-SE02033 (Purchased Reagent) Se 1000 ug/mL

M12LCCVIC_00001 07/10/13 12/10/12 1, Lot N/A 1000 mL M12GSTKIC_00002 10 mL Barium 0.5 ug/mL

Chromium 0.5 ug/mL

Copper 0.5 ug/mL

Lead 0.5 ug/mL

Nickel 0.5 ug/mL

Vanadium 5 ug/mL

Zinc 0.5 ug/mL

.M12GSTKIC_00002 07/10/13 HP, Lot 1219103 (Purchased Reagent) Barium 50 ug/mL

Chromium 50 ug/mL

Copper 50 ug/mL

Lead 50 ug/mL

Nickel 50 ug/mL

Vanadium 500 ug/mL

Zinc 50 ug/mL

M12LCRIIC_00001 06/01/13 12/03/12 1, Lot NA 1000 mL M12ESTKIC_00002 2 mL Barium 20 ug/L

Chromium 20 ug/L

Copper 20 ug/L

Lead 10 ug/L

Nickel 20 ug/L

Vanadium 10 ug/L

Zinc 40 ug/L

.M12ESTKIC_00002 06/01/13 IV, Lot F2-MEB423074 (Purchased Reagent) Barium 10 ug/mL

Chromium 10 ug/mL

Copper 10 ug/mL

Lead 5 ug/mL

Nickel 10 ug/mL

Vanadium 5 ug/mL

Zinc 20 ug/mL

M12LICVIC_00001 07/10/13 12/06/12 1, Lot N/A 1000 mL M12GSTKIC_00002 8 mL Barium 0.4 ug/mL

Chromium 0.4 ug/mL

Copper 0.4 ug/mL

Lead 0.4 ug/mL

Nickel 0.4 ug/mL

Page 107 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Vanadium 4 ug/mL

Zinc 0.4 ug/mL

.M12GSTKIC_00002 07/10/13 HP, Lot 1219103 (Purchased Reagent) Barium 50 ug/mL

Chromium 50 ug/mL

Copper 50 ug/mL

Lead 50 ug/mL

Nickel 50 ug/mL

Vanadium 500 ug/mL

Zinc 50 ug/mL

M12LISAIC_00001 12/01/13 12/03/12 1, Lot na 1000 mL M12KSTKIC_00003 100 mL Al 500 ug/mL

Ca 500 ug/mL

Fe 200 ug/mL

Mg 500 ug/mL

.M12KSTKIC_00003 12/01/13 IV, Lot F2-meb414132 (Purchased Reagent) Al 5000 ug/mL

Ca 5000 ug/mL

Fe 2000 ug/mL

Mg 5000 ug/mL

M12LISBIC_00001 09/01/13 12/03/12 1, Lot B51037 1000 mL M12ISTKIC_00003 10 mL Ag 0.2 ug/mL

As 0.1 ug/mL

Barium 0.5 ug/mL

Be 0.5 ug/mL

Cd 1 ug/mL

Chromium 0.5 ug/mL

Co 0.5 ug/mL

Copper 0.5 ug/mL

Lead 0.05 ug/mL

Mn 0.5 ug/mL

Nickel 1 ug/mL

Sb 0.6 ug/mL

Se 0.05 ug/mL

Tl 0.1 ug/mL

Vanadium 0.5 ug/mL

Zinc 1 ug/mL

M12KSTKIC_00003 100 mL Al 500 ug/mL

Ca 500 ug/mL

Fe 200 ug/mL

Mg 500 ug/mL

.M12ISTKIC_00003 09/01/13 IV, Lot E2-MEB399019 (Purchased Reagent) Ag 20 ug/mL

As 10 ug/mL

Barium 50 ug/mL

Be 50 ug/mL

Cd 100 ug/mL

Chromium 50 ug/mL

Co 50 ug/mL

Copper 50 ug/mL

Lead 5 ug/mL

Mn 50 ug/mL

Page 108 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Nickel 100 ug/mL

Sb 60 ug/mL

Se 5 ug/mL

Tl 10 ug/mL

Vanadium 50 ug/mL

Zinc 100 ug/mL

.M12KSTKIC_00003 12/01/13 IV, Lot F2-meb414132 (Purchased Reagent) Al 5000 ug/mL

Ca 5000 ug/mL

Fe 2000 ug/mL

Mg 5000 ug/mL

VA/2CEVESTDWK_00175 11/26/12 11/19/12 METHANOL, Lot DG860 2 mL 2-CEVE STD PT_00023 100 uL 2-Chloroethyl vinyl ether 100 ug/mL

VA STD PT_00024 100 uL Vinyl acetate 100 ug/mL

.2-CEVE STD PT_00023 01/08/13 10/08/12 METHANOL, Lot NA 1 mL 2-CEVESTDSK_00005 1 mL 2-Chloroethyl vinyl ether 2000 ug/mL

..2-CEVESTDSK_00005 11/30/16 Restek, Lot A085117 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL

.VA STD PT_00024 01/10/13 10/11/12 METHANOL, Lot NA 1 mL VA STD SK_00007 1 mL Vinyl acetate 2000 ug/mL

..VA STD SK_00007 03/31/14 RESTEK, Lot A090525 (Purchased Reagent) Vinyl acetate 2000 ug/mL

VA/2CEVESTDWK_00178 12/18/12 12/04/12 METHANOL, Lot DG860 2 mL 2-CEVE STD PT_00024 100 uL 2-Chloroethyl vinyl ether 100 ug/mL

VA STD PT_00025 100 uL Vinyl acetate 100 ug/mL

.2-CEVE STD PT_00024 02/21/13 11/21/12 METHANOL, Lot NA 1 mL 2-CEVESTDSK_00005 1 mL 2-Chloroethyl vinyl ether 2000 ug/mL

..2-CEVESTDSK_00005 11/30/16 Restek, Lot A085117 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL

.VA STD PT_00025 02/21/13 11/21/12 METHANOL, Lot NA 1 mL VA STD SK_00007 1 mL Vinyl acetate 2000 ug/mL

..VA STD SK_00007 03/31/14 RESTEK, Lot A090525 (Purchased Reagent) Vinyl acetate 2000 ug/mL

VA/2CEVESTDWK_00179 12/25/12 12/11/12 METHANOL, Lot DG860 2 mL 2-CEVE STD PT_00024 100 uL 2-Chloroethyl vinyl ether 100 ug/mL

VA STD PT_00025 100 uL Vinyl acetate 100 ug/mL

.2-CEVE STD PT_00024 02/21/13 11/21/12 METHANOL, Lot NA 1 mL 2-CEVESTDSK_00005 1 mL 2-Chloroethyl vinyl ether 2000 ug/mL

..2-CEVESTDSK_00005 11/30/16 Restek, Lot A085117 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL

.VA STD PT_00025 02/21/13 11/21/12 METHANOL, Lot NA 1 mL VA STD SK_00007 1 mL Vinyl acetate 2000 ug/mL

..VA STD SK_00007 03/31/14 RESTEK, Lot A090525 (Purchased Reagent) Vinyl acetate 2000 ug/mL

VOC/THF SPK_00124 12/03/12 11/19/12 1, Lot DG596 2 mL 8260ADDSPKPT_00025 50 uL 2-Butanone (MEK) 50 mg/L

Acetone 50 mg/L

.8260ADDSPKPT_00025 01/19/13 11/19/12 1, Lot NA 1 mL 8260ADDSPKSK_00015 1 mL 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

..8260ADDSPKSK_00015 01/19/13 ACCUSTD, Lot 212091219 (Purchased Reagent) 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

VOC/THF SPK_00125 12/12/12 11/28/12 1, Lot DG596 2 mL 8260ADDSPKPT_00025 50 uL 2-Butanone (MEK) 50 mg/L

Acetone 50 mg/L

.8260ADDSPKPT_00025 01/19/13 11/19/12 1, Lot NA 1 mL 8260ADDSPKSK_00015 1 mL 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

..8260ADDSPKSK_00015 01/19/13 ACCUSTD, Lot 212091219 (Purchased Reagent) 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

VOC/THF SPK_00127 12/25/12 12/11/12 1, Lot DG860 2 mL 8260ADDSPKPT_00025 50 uL 2-Butanone (MEK) 50 mg/L

Acetone 50 mg/L

.8260ADDSPKPT_00025 01/19/13 11/19/12 1, Lot NA 1 mL 8260ADDSPKSK_00015 1 mL 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

..8260ADDSPKSK_00015 01/19/13 ACCUSTD, Lot 212091219 (Purchased Reagent) 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

Page 109 of 384 01/09/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

VOC/THF SPK_00128 01/04/13 12/21/12 1, Lot DG860 2 mL 8260ADDSPKPT_00025 50 uL 2-Butanone (MEK) 50 mg/L

Acetone 50 mg/L

.8260ADDSPKPT_00025 01/19/13 11/19/12 1, Lot NA 1 mL 8260ADDSPKSK_00015 1 mL 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

..8260ADDSPKSK_00015 01/19/13 ACCUSTD, Lot 212091219 (Purchased Reagent) 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

WSTCR1_00008 04/30/15 ERA, Lot 160412 (Purchased Reagent) Chromium, hexavalent 1000 mg/L

WSTCR13_00629 12/29/12 STL, Lot Lead(II)Chrom_00001 (Purchased Reagent) Chromium, hexavalent 16.9 mg/L

WSTCR2_00008 05/31/17 Ultra Scientific, Lot L00439 (Purchased Reagent) Chromium, hexavalent 1000 mg/L

WSTINCN1_00571 12/27/12 12/27/12 DI WATER, Lot NA 100 mL WSTCN1_00011 1 mL Cyanide, Total 10 mg/L

.WSTCN1_00011 01/31/14 ERA, Lot 060112 (Purchased Reagent) Cyanide, Total 1000 mg/L

WSTINCN1_00572 12/28/12 12/28/12 DI WATER, Lot NA 100 mL WSTCN1_00011 1 mL Cyanide, Total 10 mg/L

.WSTCN1_00011 01/31/14 ERA, Lot 060112 (Purchased Reagent) Cyanide, Total 1000 mg/L

WSTINCN2_00563 12/27/12 12/27/12 DI WATER, Lot NA 100 mL WSTCN2_00028 1 mL Cyanide, Amenable 10 mg/L

Cyanide, Free 10 mg/L

Cyanide, Reactive 10 mg/L

Cyanide, Total 10 mg/L

Cyanide, Weak Acid Dissociable 10 mg/L

.WSTCN2_00028 03/31/13 RICCA, Lot 4204518 (Purchased Reagent) Cyanide, Amenable 1000 mg/L

Cyanide, Free 1000 mg/L

Cyanide, Reactive 1000 mg/L

Cyanide, Total 1000 mg/L

Cyanide, Weak Acid Dissociable 1000 mg/L

WSTINCN2_00564 12/28/12 12/28/12 DI WATER, Lot NA 100 mL WSTCN2_00028 1 mL Cyanide, Amenable 10 mg/L

Cyanide, Free 10 mg/L

Cyanide, Reactive 10 mg/L

Cyanide, Total 10 mg/L

Cyanide, Weak Acid Dissociable 10 mg/L

.WSTCN2_00028 03/31/13 RICCA, Lot 4204518 (Purchased Reagent) Cyanide, Amenable 1000 mg/L

Cyanide, Free 1000 mg/L

Cyanide, Reactive 1000 mg/L

Cyanide, Total 1000 mg/L

Cyanide, Weak Acid Dissociable 1000 mg/L

WSTSF1_00036 11/15/13 NaS/1.5g/JTB/Y39592, Lot Zn0.5n/20mL (Purchased Reagent) Sulfide 180 mg/L

Sulfide as H2S 209.1 mg/L

Sulfide, Reactive 180 mg/L

Page 110 of 384 01/09/2013
Certification Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Laboratory Authority Program EPA Region Certification ID

TestAmerica Chicago Alabama State Program 4 40461

TestAmerica Chicago California NELAP 9 01132CA

TestAmerica Chicago Georgia State Program 4 939

TestAmerica Chicago Georgia State Program 4 N/A

TestAmerica Chicago Hawaii State Program 9 N/A

TestAmerica Chicago Illinois NELAP 5 100201

TestAmerica Chicago Indiana State Program 5 C-IL-02

TestAmerica Chicago Iowa State Program 7 82

TestAmerica Chicago Kansas NELAP 7 E-10161

TestAmerica Chicago Kentucky State Program 4 90023

TestAmerica Chicago Kentucky (UST) State Program 4 66

TestAmerica Chicago Louisiana NELAP 6 30720

TestAmerica Chicago Massachusetts State Program 1 M-IL035

TestAmerica Chicago Mississippi State Program 4 N/A

TestAmerica Chicago North Carolina DENR State Program 4 291

TestAmerica Chicago North Dakota State Program 8 R-194

TestAmerica Chicago Oklahoma State Program 6 8908

TestAmerica Chicago South Carolina State Program 4 77001

TestAmerica Chicago Texas NELAP 6 T104704252-09-TX

TestAmerica Chicago USDA Federal P330-12-00038

TestAmerica Chicago Virginia NELAP 3 460142

TestAmerica Chicago Wisconsin State Program 5 999580010

TestAmerica Chicago Wyoming State Program 8 8TMS-Q

Accreditation may not be offered or required for all methods and analytes reported in this package. Please contact your project manager for the laboratory’s 

current list of certified methods and analytes.

Page 111 of 384 TestAmerica Chicago 01/09/2013
Method 8260B

Volatile Organic Compounds (GC/MS) 

by Method 8260B

Page 112 of 384 01/09/2013
FORM II

GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.: 500-53491-1

SDG No.:

Matrix: Solid Level: Low

TestAmerica Chicago

GC Column (1): DB624 ID: 0.2 (mm)

Client Sample ID Lab Sample ID DBFM # DCA # TOL # BFB #

FC DISCRETE 6 500-53491-3 95 89 87 79

FC D DISCRETE 6 500-53491-4 90 91 89 75

MB 500-173973/5 90 94 96 84

LCS 500-173973/6 81 84 89 81

LCSD 

500-173973/7

91 88 93 87

QC LIMITS

DBFM = Dibromofluoromethane QC LIMITS 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 70-134

TOL = Toluene-d8 (Surr) 75-122

BFB = 4-Bromofluorobenzene (Surr) 70-122

FORM II 8260B

# Column to be used to flag recovery values

Page 113 of 384 01/09/2013
FORM II

GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.: 500-53491-1

SDG No.:

Matrix: Solid Level: Medium

TestAmerica Chicago

GC Column (1): DB624 ID: 0.2 (mm)

Client Sample ID Lab Sample ID DBFM # DCA # TOL # BFB #

FC DISCRETE 6 DL 500-53491-3 DL 93 97 96 94

FC D DISCRETE 6 DL 500-53491-4 DL 96 105 101 100

MB 500-174064/6 96 101 101 98

LCS 500-174064/4 100 95 97 97

QC LIMITS

DBFM = Dibromofluoromethane QC LIMITS 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 75-125

TOL = Toluene-d8 (Surr) 75-120

BFB = 4-Bromofluorobenzene (Surr) 75-120

FORM II 8260B

# Column to be used to flag recovery values

Page 114 of 384 01/09/2013
FORM II

GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.: 500-53491-1

SDG No.:

Matrix: Water Level: Low

TestAmerica Chicago

GC Column (1): DB624 ID: 0.2 (mm)

Client Sample ID Lab Sample ID DBFM # DCA # TOL # BFB #

FC EB 6 500-53491-5 90 88 94 88

TRIP BLANK 500-53491-6 93 93 100 93

MB 500-173987/7 97 98 103 97

LCS 500-173987/4 94 92 96 96

QC LIMITS

DBFM = Dibromofluoromethane QC LIMITS 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 75-125

TOL = Toluene-d8 (Surr) 75-120

BFB = 4-Bromofluorobenzene (Surr) 75-120

FORM II 8260B

# Column to be used to flag recovery values

Page 115 of 384 01/09/2013
GC/MS VOA LAB CONTROL SAMPLE RECOVERY

FORM III

Lab Name: Job No.:

SDG No.:

Matrix: Level:

Matrix:

Low

500-53491-1

Solid Lab File ID: 6S1227.d

Lab ID: LCS 500-173973/6 Client ID:

TestAmerica Chicago

REC 

%

REC

QC

CONCENTRATION LIMITS

(ug/Kg)

SPIKE

ADDED

(ug/Kg)

#

LCS LCS

COMPOUND

Acetone 50.0 47.98 96 50-138

2-Butanone (MEK) 50.0 43.18 86 58-133

FORM III 8260B

# Column to be used to flag recovery and RPD values

Page 116 of 384 01/09/2013
GC/MS VOA LAB CONTROL SAMPLE RECOVERY

FORM III

Lab Name: Job No.:

SDG No.:

Matrix: Level:

Matrix:

Low

500-53491-1

Water Lab File ID: 22S1227.D

Lab ID: LCS 500-173987/4 Client ID:

TestAmerica Chicago

REC 

%

REC

QC

CONCENTRATION LIMITS

(ug/L)

SPIKE

ADDED

(ug/L)

#

LCS LCS

COMPOUND

Acetone 50.0 53.44 107 46-153

2-Butanone (MEK) 50.0 46.97 94 54-138

FORM III 8260B

# Column to be used to flag recovery and RPD values

Page 117 of 384 01/09/2013
GC/MS VOA LAB CONTROL SAMPLE RECOVERY

FORM III

Lab Name: Job No.:

SDG No.:

Matrix: Level:

Matrix:

Medium

500-53491-1

Solid Lab File ID: 18S1228.D

Lab ID: LCS 500-174064/4 Client ID:

TestAmerica Chicago

REC 

%

REC

QC

CONCENTRATION LIMITS

(ug/Kg)

SPIKE

ADDED

(ug/Kg)

#

LCS LCS

COMPOUND

Acetone 50.0 50.53 101 46-153

2-Butanone (MEK) 50.0 43.61 87 54-138

FORM III 8260B

# Column to be used to flag recovery and RPD values

Page 118 of 384 01/09/2013
GC/MS VOA LAB CONTROL SAMPLE DUPLICATE RECOVERY

FORM III

Lab Name: Job No.:

SDG No.:

Matrix: Level:

Matrix:

Low

500-53491-1

Solid Lab File ID: 6T1227.d

Lab ID: LCSD 500-173973/7 Client ID:

TestAmerica Chicago

COMPOUND

SPIKE

ADDED CONCENTRATION %

REC

%

RPD

QC LIMITS

(ug/Kg) (ug/Kg) RPD REC 

#

LCSD LCSD

Acetone 50.0 55.07 110 14 30 50-138

2-Butanone (MEK) 50.0 44.82 90 4 30 58-133

FORM III 8260B

# Column to be used to flag recovery and RPD values

Page 119 of 384 01/09/2013
FORM IV

GC/MS VOA METHOD BLANK SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Date Analyzed:

GC Column: ID:

Instrument ID: 12/28/2012 10:45

DB624

Heated Purge:(Y/N) N

CMS18

Lab File ID: 18M1228.D Lab Sample ID: MB 500-174064/6

Matrix: Solid

0.2(mm)

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID

LAB

CLIENT SAMPLE ID FILE ID DATE ANALYZED

LCS 500-174064/4 18S1228.D 12/28/2012 10:00

FC DISCRETE 6 DL 500-53491-3 DL 53491-03.D 12/28/2012 11:08

FC D DISCRETE 6 DL 500-53491-4 DL 53491-04.D 12/28/2012 11:31

FORM IV 8260B

Page 120 of 384 01/09/2013
FORM IV

GC/MS VOA METHOD BLANK SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Date Analyzed:

GC Column: ID:

Instrument ID: 12/27/2012 10:33

DB624

Heated Purge:(Y/N) Y

CMS06

Lab File ID: 6M1227.d Lab Sample ID: MB 500-173973/5

Matrix: Solid

0.2(mm)

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID

LAB

CLIENT SAMPLE ID FILE ID DATE ANALYZED

LCS 500-173973/6 6S1227.d 12/27/2012 10:56

LCSD 500-173973/7 6T1227.d 12/27/2012 11:19

FC DISCRETE 6 500-53491-3 3491-03.d 12/27/2012 13:36

FC D DISCRETE 6 500-53491-4 3491-04.d 12/27/2012 13:59

FORM IV 8260B

Page 121 of 384 01/09/2013
FORM IV

GC/MS VOA METHOD BLANK SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53491-1

Date Analyzed:

GC Column: ID:

Instrument ID: 12/27/2012 14:10

DB624

Heated Purge:(Y/N) N

CMS22

Lab File ID: 22M1227.D Lab Sample ID: MB 500-173987/7

Matrix: Water

0.2(mm)

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID

LAB

CLIENT SAMPLE ID FILE ID DATE ANALYZED

LCS 500-173987/4 22S1227.D 12/27/2012 12:46

TRIP BLANK 500-53491-6 53491-06.D 12/27/2012 15:28

FC EB 6 500-53491-5 53491-05.D 12/27/2012 15:54

FORM IV 8260B

Page 122 of 384 01/09/2013
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53491-1

Lab File ID:

Instrument ID:

6B1204.d

CMS06

12/04/2012

14:01

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 171819

50 15.0 - 40.0 % of mass 95 33.6 

75 30.0 - 60.0 % of mass 95 56.3 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 7.2 

173 Less than 2.0 % of mass 174 1.8 (1.8)1

174 50.0 - 120.00 % of mass 95 98.1 

175 5.0 - 9.0 % of mass 174 8.3 (8.4)1

176 95.0 - 101.0 % of mass 174 96.8 (98.7)1

177 5.0 - 9.0 % of mass 176 7.2 (7.5)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

STD1 500-171819/2 6I1204a.d 12/04/2012 14:34

STD2 500-171819/3 6I1204b.d 12/04/2012 14:57

STD4 500-171819/5 6I1204d.d 12/04/2012 15:43

STD3 500-171819/16 6I1204CC.d 12/04/2012 16:10

STD5 500-171819/6 6I1204e.d 12/04/2012 16:33

STD6 500-171819/7 6I1204f.d 12/04/2012 16:55

STD1AP 500-171819/8 6J1204a.d 12/04/2012 17:18

STD2AP 500-171819/9 6J1204b.d 12/04/2012 17:41

STD3AP 6J1204c.d 12/04/2012 18:04

500-171819/10

STD4AP 6J1204d.d 12/04/2012 18:27

500-171819/11

STD5AP 6J1204e.d 12/04/2012 18:49

500-171819/12

STD6AP 6J1204f.d 12/04/2012 19:13

500-171819/13

ICV 500-171819/15 6S1204.d 12/04/2012 19:58

FORM V 8260B Page 123 of 384 01/09/2013
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53491-1

Lab File ID:

Instrument ID:

6B1227.d

CMS06

12/27/2012

08:48

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 173973

50 15.0 - 40.0 % of mass 95 28.9 

75 30.0 - 60.0 % of mass 95 50.2 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 6.8 

173 Less than 2.0 % of mass 174 0.6 (0.6)1

174 50.0 - 120.00 % of mass 95 92.9 

175 5.0 - 9.0 % of mass 174 6.6 (7.1)1

176 95.0 - 101.0 % of mass 174 92.0 (99.0)1

177 5.0 - 9.0 % of mass 176 5.7 (6.2)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

CCV 500-173973/3 6C1227.d 12/27/2012 09:47

CCV 500-173973/4 6D1227.d 12/27/2012 10:10

MB 500-173973/5 6M1227.d 12/27/2012 10:33

LCS 500-173973/6 6S1227.d 12/27/2012 10:56

LCSD 500-173973/7 6T1227.d 12/27/2012 11:19

FC DISCRETE 6 500-53491-3 3491-03.d 12/27/2012 13:36

FC D DISCRETE 6 500-53491-4 3491-04.d 12/27/2012 13:59

FORM V 8260B Page 124 of 384 01/09/2013
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53491-1

Lab File ID:

Instrument ID:

18B1120a.D

CMS18

11/20/2012

15:22

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 170445

50 15.0 - 40.0 % of mass 95 27.9 

75 30.0 - 60.0 % of mass 95 48.2 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 7.2 

173 Less than 2.0 % of mass 174 0.7 (0.8)1

174 50.0 - 120.00 % of mass 95 80.8 

175 5.0 - 9.0 % of mass 174 5.5 (6.8)1

176 95.0 - 101.0 % of mass 174 79.4 (98.2)1

177 5.0 - 9.0 % of mass 176 5.5 (6.9)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

STD1 500-170445/2 18I1120a.D 11/20/2012 15:57

STD2 500-170445/3 18I1120b.D 11/20/2012 16:21

STD3 500-170445/4 18I1120c.D 11/20/2012 16:46

STD4 500-170445/5 18I1120d.D 11/20/2012 17:10

STD5 500-170445/6 18I1120e.D 11/20/2012 17:35

STD6 500-170445/7 18I1120f.D 11/20/2012 17:59

STD7 500-170445/8 18I1120g.D 11/20/2012 18:23

STD8 500-170445/9 18I1120h.D 11/20/2012 18:47

STD9 500-170445/10 18I1120i.D 11/20/2012 19:11

ICV 500-170445/20 18S1120.D 11/20/2012 23:15

FORM V 8260B Page 125 of 384 01/09/2013
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53491-1

Lab File ID:

Instrument ID:

18B1228a.D

CMS18

12/28/2012

08:39

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 174064

50 15.0 - 40.0 % of mass 95 32.7 

75 30.0 - 60.0 % of mass 95 49.9 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 6.5 

173 Less than 2.0 % of mass 174 0.0 (0.0)1

174 50.0 - 120.00 % of mass 95 113.8 

175 5.0 - 9.0 % of mass 174 7.1 (6.2)1

176 95.0 - 101.0 % of mass 174 109.4 (96.1)1

177 5.0 - 9.0 % of mass 176 8.0 (7.3)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

CCV 500-174064/2 18C1228.D 12/28/2012 09:14

CCV 500-174064/3 18D1228.D 12/28/2012 09:37

LCS 500-174064/4 18S1228.D 12/28/2012 10:00

MB 500-174064/6 18M1228.D 12/28/2012 10:45

FC DISCRETE 6 DL 500-53491-3 DL 53491-03.D 12/28/2012 11:08

FC D DISCRETE 6 DL 500-53491-4 DL 53491-04.D 12/28/2012 11:31

FORM V 8260B Page 126 of 384 01/09/2013
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53491-1

Lab File ID:

Instrument ID:

22B1211.D

CMS22

12/11/2012

13:45

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 172615

50 15.0 - 40.0 % of mass 95 22.6 

75 30.0 - 60.0 % of mass 95 45.2 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 7.5 

173 Less than 2.0 % of mass 174 0.0 (0.0)1

174 50.0 - 120.00 % of mass 95 86.2 

175 5.0 - 9.0 % of mass 174 5.9 (6.8)1

176 95.0 - 101.0 % of mass 174 86.4 (100.2)1

177 5.0 - 9.0 % of mass 176 4.9 (5.7)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

STD01 500-172615/2 22I1211A.D 12/11/2012 14:23

STD02 500-172615/3 22I1211B.D 12/11/2012 14:51

STD03 500-172615/4 22I1211C.D 12/11/2012 15:20

STD04 500-172615/5 22I1211D.D 12/11/2012 15:48

STD05 500-172615/6 22I1211E.D 12/11/2012 16:16

STD06 500-172615/7 22I1211F.D 12/11/2012 16:44

STD07 500-172615/8 22I1211G.D 12/11/2012 17:13

STD08 500-172615/9 22I1211H.D 12/11/2012 17:41

STD09 500-172615/10 22I1211I.D 12/11/2012 18:09

ICV 500-172615/23 22S1211.D 12/12/2012 00:17

FORM V 8260B Page 127 of 384 01/09/2013
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53491-1

Lab File ID:

Instrument ID:

22B1227.D

CMS22

12/27/2012

11:16

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 173987

50 15.0 - 40.0 % of mass 95 28.5 

75 30.0 - 60.0 % of mass 95 53.0 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 6.9 

173 Less than 2.0 % of mass 174 1.6 (1.6)1

174 50.0 - 120.00 % of mass 95 100.4 

175 5.0 - 9.0 % of mass 174 8.2 (8.2)1

176 95.0 - 101.0 % of mass 174 97.3 (96.9)1

177 5.0 - 9.0 % of mass 176 5.0 (5.1)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

CCV 500-173987/2 22C1227.D 12/27/2012 11:55

CCV 500-173987/3 22D1227.D 12/27/2012 12:22

LCS 500-173987/4 22S1227.D 12/27/2012 12:46

MB 500-173987/7 22M1227.D 12/27/2012 14:10

TRIP BLANK 500-53491-6 53491-06.D 12/27/2012 15:28

FC EB 6 500-53491-5 53491-05.D 12/27/2012 15:54

FORM V 8260B Page 128 of 384 01/09/2013
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53491-1

Sample No.: STD3 500-171819/16 Date Analyzed: 12/04/2012 16:10

Lab File ID (Standard): 6I1204CC.d

Instrument ID: CMS06 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) Y

Calibration ID: 10745

AREA # RT # AREA # RT # AREA # RT #

PFB DFB CBZ

UPPER LIMIT

LOWER LIMIT

961332

240333 341607

1366426

334952

1339808

INITIAL CALIBRATION MID-POINT 4.64 5.52 8.71

5.14

4.14

6.02

5.02

9.21

8.21

480666 683213 669904

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-171819/15 526825 4.65 733790 5.52 696556 8.70

CCV 500-173973/3 524403 4.65 730945 5.52 744845 8.71

CCV 500-173973/4 570893 4.64 773092 5.52 773457 8.70

MB 500-173973/5 564902 4.65 741762 5.52 785524 8.71

LCS 500-173973/6 645535 4.64 860713 5.52 834642 8.70

LCSD 500-173973/7 596394 4.64 810667 5.52 809211 8.70

500-53491-3 FC DISCRETE 6 342289 4.64 476748 5.52 442713 8.70

500-53491-4 FC D DISCRETE 6 386100 4.65 531388 5.52 510019 8.70

PFB = Pentafluorobenzene

DFB = 1,4-Difluorobenzene

CBZ = Chlorobenzene-d5

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 129 of 384 01/09/2013
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53491-1

Sample No.: STD3 500-171819/16 Date Analyzed: 12/04/2012 16:10

Lab File ID (Standard): 6I1204CC.d

Instrument ID: CMS06 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) Y

Calibration ID: 10745

AREA # RT # AREA # RT # AREA # RT #

DCB

UPPER LIMIT

LOWER LIMIT

843448

210862

INITIAL CALIBRATION MID-POINT 10.72

11.22

10.22

421724

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-171819/15 427951 10.72

CCV 500-173973/3 446339 10.72

CCV 500-173973/4 451529 10.72

MB 500-173973/5 410551 10.72

LCS 500-173973/6 480914 10.72

LCSD 500-173973/7 484380 10.72

500-53491-3 FC DISCRETE 6 197214* 10.72

500-53491-4 FC D DISCRETE 6 222254 10.72

DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 130 of 384 01/09/2013
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53491-1

Sample No.: STD6 500-170445/7 Date Analyzed: 11/20/2012 17:59

Lab File ID (Standard): 18I1120f.D

Instrument ID: CMS18 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) N

Calibration ID: 10631

AREA # RT # AREA # RT # AREA # RT #

PFB DFB CBZ

UPPER LIMIT

LOWER LIMIT

596976

149244 211381

845522

189544

758174

INITIAL CALIBRATION MID-POINT 5.64 6.62 9.64

6.14

5.14

7.12

6.12

10.14

9.14

298488 422761 379087

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-170445/20 294287 5.64 437412 6.62 387064 9.64

CCV 500-174064/2 280225 5.64 414660 6.62 352358 9.64

CCV 500-174064/3 280433 5.64 415891 6.62 349478 9.63

LCS 500-174064/4 289268 5.64 434398 6.62 356182 9.64

MB 500-174064/6 276833 5.64 407408 6.62 370803 9.63

500-53491-3 DL FC DISCRETE 6 DL 265949 5.64 385748 6.62 345191 9.64

500-53491-4 DL FC D DISCRETE 6 DL 252764 5.64 366504 6.62 331985 9.64

PFB = Pentafluorobenzene

DFB = 1,4-Difluorobenzene

CBZ = Chlorobenzene-d5

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 131 of 384 01/09/2013
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53491-1

Sample No.: STD6 500-170445/7 Date Analyzed: 11/20/2012 17:59

Lab File ID (Standard): 18I1120f.D

Instrument ID: CMS18 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) N

Calibration ID: 10631

AREA # RT # AREA # RT # AREA # RT #

DCB

UPPER LIMIT

LOWER LIMIT

435034

108759

INITIAL CALIBRATION MID-POINT 11.63

12.13

11.13

217517

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-170445/20 213606 11.63

CCV 500-174064/2 194389 11.63

CCV 500-174064/3 193721 11.63

LCS 500-174064/4 199496 11.63

MB 500-174064/6 190160 11.63

500-53491-3 DL FC DISCRETE 6 DL 180402 11.63

500-53491-4 DL FC D DISCRETE 6 DL 175640 11.63

DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 132 of 384 01/09/2013
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53491-1

Sample No.: STD06 500-172615/7 Date Analyzed: 12/11/2012 16:44

Lab File ID (Standard): 22I1211F.D

Instrument ID: CMS22 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) N

Calibration ID: 10830

AREA # RT # AREA # RT # AREA # RT #

PFB DFB CBZ

UPPER LIMIT

LOWER LIMIT

1409738

352435 493044

1972176

417716

1670864

INITIAL CALIBRATION MID-POINT 6.27 7.24 10.64

6.77

5.77

7.74

6.74

11.14

10.14

704869 986088 835432

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-172615/23 772269 6.26 1099840 7.24 931671 10.64

CCV 500-173987/2 701736 6.26 969856 7.24 822660 10.64

CCV 500-173987/3 696904 6.26 953661 7.24 799767 10.64

LCS 500-173987/4 716951 6.27 981854 7.24 841317 10.64

MB 500-173987/7 692291 6.26 945495 7.24 811334 10.64

500-53491-6 TRIP BLANK 686301 6.26 928214 7.24 796602 10.64

500-53491-5 FC EB 6 688414 6.26 958050 7.24 814329 10.64

PFB = Pentafluorobenzene

DFB = 1,4-Difluorobenzene

CBZ = Chlorobenzene-d5

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 133 of 384 01/09/2013
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53491-1

Sample No.: STD06 500-172615/7 Date Analyzed: 12/11/2012 16:44

Lab File ID (Standard): 22I1211F.D

Instrument ID: CMS22 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) N

Calibration ID: 10830

AREA # RT # AREA # RT # AREA # RT #

DCB

UPPER LIMIT

LOWER LIMIT

1003186

250797

INITIAL CALIBRATION MID-POINT 13.08

13.58

12.58

501593

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-172615/23 542063 13.08

CCV 500-173987/2 499991 13.08

CCV 500-173987/3 451307 13.08

LCS 500-173987/4 515537 13.08

MB 500-173987/7 436959 13.08

500-53491-6 TRIP BLANK 433983 13.08

500-53491-5 FC EB 6 437814 13.07

DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 134 of 384 01/09/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

FC DISCRETE 6

SDG No.:

500-53491-1

Lab Sample ID: 500-53491-3

Matrix: Lab File ID: 3491-03.d

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

12/19/2012 14:20

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor:

74.1

1

Level: (low/med) Low

5(g)

0.2(mm)

Date Analyzed: 12/27/2012 13:36

DB624 ID:

Analysis Batch No.: 173973 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

78-93-3 2-Butanone (MEK) 11.8 J 19.3 6.98

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 89 70-134

2037-26-5 Toluene-d8 (Surr) 87 75-122

460-00-4 4-Bromofluorobenzene (Surr) 79 70-122

1868-53-7 Dibromofluoromethane 95 75-120

FORM I 8260B

Page 135 of 384 01/09/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

FC DISCRETE 6 DL

SDG No.:

500-53491-1

Lab Sample ID: 500-53491-3 DL

Matrix: Lab File ID: 53491-03.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

12/19/2012 14:20

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor:

74.1

50

Level: (low/med) Medium

5(g)

5 (mL)

5(mL) 0.2(mm)

Date Analyzed: 12/28/2012 11:08

DB624 ID:

Analysis Batch No.: 174064 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 7020 963 251

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 97 75-125

2037-26-5 Toluene-d8 (Surr) 96 75-120

460-00-4 4-Bromofluorobenzene (Surr) 94 75-120

1868-53-7 Dibromofluoromethane 93 75-120

FORM I 8260B

Page 136 of 384 01/09/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

FC D DISCRETE 6

SDG No.:

500-53491-1

Lab Sample ID: 500-53491-4

Matrix: Lab File ID: 3491-04.d

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

12/19/2012 14:45

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor:

72.4

1

Level: (low/med) Low

5(g)

0.2(mm)

Date Analyzed: 12/27/2012 13:59

DB624 ID:

Analysis Batch No.: 173973 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

78-93-3 2-Butanone (MEK) 19.5 18.1 6.55

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 91 70-134

2037-26-5 Toluene-d8 (Surr) 89 75-122

460-00-4 4-Bromofluorobenzene (Surr) 75 70-122

1868-53-7 Dibromofluoromethane 90 75-120

FORM I 8260B

Page 137 of 384 01/09/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

FC D DISCRETE 6 DL

SDG No.:

500-53491-1

Lab Sample ID: 500-53491-4 DL

Matrix: Lab File ID: 53491-04.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

12/19/2012 14:45

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor:

72.4

50

Level: (low/med) Medium

5(g)

5 (mL)

5(mL) 0.2(mm)

Date Analyzed: 12/28/2012 11:31

DB624 ID:

Analysis Batch No.: 174064 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 7150 905 235

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 105 75-125

2037-26-5 Toluene-d8 (Surr) 101 75-120

460-00-4 4-Bromofluorobenzene (Surr) 100 75-120

1868-53-7 Dibromofluoromethane 96 75-120

FORM I 8260B

Page 138 of 384 01/09/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

FC EB 6

SDG No.:

500-53491-1

Lab Sample ID: 500-53491-5

Matrix: Lab File ID: 53491-05.D

Analysis Method: 8260B Date Collected:

Water

TestAmerica Chicago

12/19/2012 14:10

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(mL)

0.2(mm)

Date Analyzed: 12/27/2012 15:54

DB624 ID:

Analysis Batch No.: 173987 Units: ug/L

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone <5.00 5.00 1.29

78-93-3 2-Butanone (MEK) <5.00 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 88 75-125

2037-26-5 Toluene-d8 (Surr) 94 75-120

460-00-4 4-Bromofluorobenzene (Surr) 88 75-120

1868-53-7 Dibromofluoromethane 90 75-120

FORM I 8260B

Page 139 of 384 01/09/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

TRIP BLANK

SDG No.:

500-53491-1

Lab Sample ID: 500-53491-6

Matrix: Lab File ID: 53491-06.D

Analysis Method: 8260B Date Collected:

Water

TestAmerica Chicago

12/19/2012 00:00

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(mL)

0.2(mm)

Date Analyzed: 12/27/2012 15:28

DB624 ID:

Analysis Batch No.: 173987 Units: ug/L

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone <5.00 5.00 1.29

78-93-3 2-Butanone (MEK) <5.00 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 93 75-125

2037-26-5 Toluene-d8 (Surr) 100 75-120

460-00-4 4-Bromofluorobenzene (Surr) 93 75-120

1868-53-7 Dibromofluoromethane 93 75-120

FORM I 8260B

Page 140 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06

Analy Batch No.: 171819

Calibration Start Date: 12/04/2012 14:34 Calibration End Date: 10745

Y

12/04/2012 16:55

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD1 500-171819/2 6I1204a.d

Level 2 STD2 500-171819/3 6I1204b.d

Level 3 STD3 500-171819/16 6I1204CC.d

Level 4 STD4 500-171819/5 6I1204d.d

Level 5 STD5 500-171819/6 6I1204e.d

Level 6 STD6 500-171819/7 6I1204f.d

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

Dichlorodifluoromethane 1.0174 0.8189 0.9825 0.9247 0.9868 Ave 7.8

1.0041

0.9557 0.0100 15.0

Chloromethane 1.3147 1.1022 1.1622 1.0959 1.1527 Ave 6.8

1.1894

1.1695 0.1000 15.0

Vinyl chloride 1.0822 0.9159 0.9643 0.9041 0.9964 Ave 6.7

1.0086

0.9786 0.0100 15.0

Bromomethane 0.6561 0.5359 0.5658 0.5126 0.5451 Ave 8.8

0.5620

0.5629 0.0100 15.0

Chloroethane 0.8545 0.7097 0.6734 0.6547 0.6894 Ave 10.0

0.6884

0.7117 0.0100 15.0

Dichlorofluoromethane 1.6464 1.4455 1.4042 1.3446 1.4482 Ave 7.1

1.5072

1.4660 0.0100 15.0

Trichlorofluoromethane 1.5425 1.2252 1.2065 1.1652 1.2634 Ave 11.0

1.2709

1.2790 0.0100 15.0

Acrolein 0.0784 0.0710 0.0627 0.0681 0.0819 Ave 12.0

0.0868

0.0748 0.0010 15.0

1,1-Dichloroethene 0.5725 0.5062 0.5192 0.5251 0.5481 Ave 4.9

0.5649

0.5393 0.0100 15.0

1,1,2-Trichloro-1,2,2-trifluoroethane 0.8092 0.6963 0.7098 0.7022 0.7462 Ave 5.9

0.7585

0.7370 0.0100 15.0

Acetone 0.1969 0.1299 0.1270 0.1372 0.1393 Qua2 0.9980

0.1352

0.4117 0.1127 0.0001 0.0100 0.9900

Carbon disulfide 2.0717 1.8310 2.1228 2.1508 2.0121 Ave 5.6

2.0757

2.0440 0.0100 15.0

Acetonitrile 0.0839 0.0490 0.0402 0.0399 0.0449 Qua2 0.9990

0.0467

2.0318 0.0331 0 0.0010 0.9900

Methylene Chloride 0.6635 0.5115 0.5232 0.4834 0.5084 Ave 12.0

0.5109

0.5335 0.0100 15.0

Acrylonitrile 0.1524 0.1399 0.1237 0.1280 0.1525 Ave 10.0

0.1586

0.1425 0.0010 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 141 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06

Analy Batch No.: 171819

Calibration Start Date: 12/04/2012 14:34 Calibration End Date: 10745

Y

12/04/2012 16:55

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

trans-1,2-Dichloroethene 0.5931 0.5632 0.5531 0.5573 0.5844 Ave 3.1

0.5907

0.5736 0.0100 15.0

Methyl tert-butyl ether 1.2285 1.0592 1.1026 1.1125 1.1868 Ave 5.7

1.1956

1.1475 0.0100 15.0

1,1-Dichloroethane 1.2472 1.1699 1.1522 1.1622 1.2237 Ave 3.3

1.2205

1.1960 0.1000 15.0

Vinyl acetate 0.7953 0.7402 0.9524 0.8603 1.0101 Ave 12.0

0.9422

0.8834 0.0100 15.0

2,2-Dichloropropane 0.7034 0.6557 0.7587 0.7383 0.7741 Ave 7.0

0.7995

0.7383 0.0100 15.0

cis-1,2-Dichloroethene 0.6358 0.5831 0.5511 0.5572 0.5880 Ave 5.1

0.5837

0.5831 0.0100 15.0

2-Butanone (MEK) 0.1589 0.1491 0.1741 0.1929 0.1968 Ave 11.0

0.1738

0.1743 0.0100 15.0

Propionitrile 0.0334 0.0304 0.0304 0.0326 0.0352 Ave 6.8

0.0355

0.0329 0.0010 15.0

Bromochloromethane 0.2640 0.2242 0.2236 0.2233 0.2335 Ave 6.8

0.2290

0.2329 0.0100 15.0

Tetrahydrofuran 0.0961 0.0951 0.1082 0.1023 0.1102 Ave 6.0

0.1040

0.1027 0.0100 15.0

Chloroform 1.0059 0.8787 0.8887 0.9034 0.9564 Ave 5.2

0.9410

0.9290 0.0100 15.0

1,1,1-Trichloroethane 0.9044 0.7493 0.8505 0.8469 0.8894 Ave 7.1

0.9164

0.8595 0.0100 15.0

Carbon tetrachloride 0.5349 0.4468 0.5129 0.5549 0.5765 Ave 9.3

0.5790

0.5342 0.0100 15.0

1,1-Dichloropropene 0.8028 0.7274 0.7162 0.7444 0.7869 Ave 4.5

0.7698

0.7579 0.0100 15.0

Benzene 1.5710 1.4004 1.3772 1.4946 1.4972 Ave 4.9

1.4498

1.4650 0.0100 15.0

1,2-Dichloroethane 0.4930 0.4329 0.4442 0.4947 0.4992 Ave 6.0

0.4759

0.4733 0.0100 15.0

Trichloroethene 0.4006 0.3758 0.3459 0.3888 0.3882 Ave 5.0

0.3749

0.3790 0.0100 15.0

1,2-Dichloropropane 0.4161 0.3758 0.3680 0.3901 0.3985 Ave 4.4

0.3843

0.3888 0.0100 15.0

Dibromomethane 0.1879 0.1660 0.1706 0.1741 0.1782 Ave 4.4

0.1703

0.1745 0.0100 15.0

Bromodichloromethane 0.4312 0.3710 0.3994 0.4425 0.4477 Ave 7.0

0.4284

0.4200 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 142 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06

Analy Batch No.: 171819

Calibration Start Date: 12/04/2012 14:34 Calibration End Date: 10745

Y

12/04/2012 16:55

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

2-Chloroethyl vinyl ether 0.0965 0.0874 0.0962 0.0912 0.0993 Ave 4.9

0.0903

0.0935 0.0100 15.0

cis-1,3-Dichloropropene 0.4355 0.4007 0.4109 0.4604 0.4750 Ave 6.7

0.4574

0.4400 0.0100 15.0

4-Methyl-2-pentanone (MIBK) 0.2970 0.2305 0.2916 0.3119 0.2711 Ave 11.0

0.2599

0.2770 0.0100 15.0

Toluene 0.9196 0.8482 0.8292 0.9329 0.9557 Ave 5.9

0.9478

0.9056 0.0100 15.0

trans-1,3-Dichloropropene 0.3434 0.3227 0.3622 0.3988 0.4097 Ave 9.3

0.3942

0.3718 0.0100 15.0

1,1,2-Trichloroethane 0.3027 0.2869 0.2979 0.3045 0.3149 Ave 3.0

0.3024

0.3016 0.0100 15.0

Tetrachloroethene 0.4527 0.4310 0.4104 0.4575 0.4682 Ave 4.7

0.4474

0.4445 0.0100 15.0

1,3-Dichloropropane 0.4154 0.3684 0.3760 0.3997 0.4041 Ave 5.2

0.3690

0.3887 0.0100 15.0

2-Hexanone 0.1967 0.1691 0.2179 0.2040 0.1861 Ave 10.0

0.1713

0.1909 0.0100 15.0

Dibromochloromethane 0.2331 0.2226 0.2523 0.2919 0.2973 Ave 13.0

0.2925

0.2649 0.0100 15.0

1,2-Dibromoethane 0.2248 0.2056 0.2134 0.2321 0.2339 Ave 4.9

0.2225

0.2221 0.0100 15.0

1-Chlorohexane 0.8497 0.7609 0.7473 0.7911 0.8333 Ave 5.3

0.8334

0.8026 0.0100 15.0

Chlorobenzene 1.0890 0.9951 0.9764 1.0526 1.0888 Ave 4.5

1.0565

1.0431 0.3000 15.0

1,1,1,2-Tetrachloroethane 0.3070 0.2956 0.3444 0.3789 0.3844 Ave 11.0

0.3846

0.3491 0.0100 15.0

Ethylbenzene 0.6292 0.5655 0.5902 0.6273 0.6313 Ave 4.3

0.6103

0.6090 0.0100 15.0

m&p-Xylene 1.5498 1.4828 1.5027 1.6944 1.7904 Ave 8.5

1.7779

1.6330 0.0100 15.0

o-Xylene 1.5616 1.5031 1.5609 1.7253 1.7835 Ave 7.8

1.8029

1.6562 0.0100 15.0

Styrene 1.2419 1.1547 1.2173 1.3556 1.4007 Ave 8.0

1.3964

1.2944 0.0100 15.0

Bromoform 0.1622 0.1390 0.1781 0.2003 0.2160 Qua1 0.9960

0.2050

-0.255 0.1820 0.0002 0.0100 0.9900

Isopropylbenzene 3.7553 3.5476 3.2918 3.7357 3.7939 Ave 5.9

3.8866

3.6685 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 143 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06

Analy Batch No.: 171819

Calibration Start Date: 12/04/2012 14:34 Calibration End Date: 10745

Y

12/04/2012 16:55

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

Bromobenzene 0.8820 0.7936 0.7893 0.8417 0.8388 Ave 4.1

0.8341

0.8299 0.0100 15.0

1,1,2,2-Tetrachloroethane 0.5749 0.4591 0.4791 0.5044 0.4888 Ave 8.3

0.4744

0.4968 0.3000 15.0

1,2,3-Trichloropropane 0.1498 0.1293 0.1370 0.1391 0.1417 Ave 5.2

0.1324

0.1382 0.0100 15.0

N-Propylbenzene 4.7265 4.3209 4.0651 4.6087 4.6711 Ave 6.1

4.7658

4.5263 0.0100 15.0

2-Chlorotoluene 2.5905 2.3236 2.2523 2.5084 2.4920 Ave 5.3

2.5043

2.4452 0.0100 15.0

1,3,5-Trimethylbenzene 3.2230 2.9483 2.8743 3.3095 3.3561 Ave 7.2

3.4447

3.1926 0.0100 15.0

4-Chlorotoluene 3.1034 2.7648 2.7354 3.0804 3.1013 Ave 6.5

3.1990

2.9974 0.0100 15.0

tert-Butylbenzene 2.8702 2.6245 2.4622 2.8128 2.7935 Ave 5.9

2.8542

2.7363 0.0100 15.0

1,2,4-Trimethylbenzene 3.1779 3.0257 2.9078 3.3124 3.2583 Ave 5.6

3.3651

3.1745 0.0100 15.0

sec-Butylbenzene 4.3996 4.0911 3.9512 4.5490 4.4865 Ave 6.3

4.6389

4.3527 0.0100 15.0

1,3-Dichlorobenzene 1.8444 1.6756 1.6762 1.8109 1.7740 Ave 3.9

1.7662

1.7579 0.0100 15.0

p-Isopropyltoluene 3.6992 3.5142 3.3950 3.8768 3.8296 Ave 5.7

3.9249

3.7066 0.0100 15.0

1,4-Dichlorobenzene 1.8453 1.7033 1.6813 1.8389 1.7695 Ave 3.8

1.7681

1.7677 0.0100 15.0

n-Butylbenzene 3.5999 3.3917 3.2752 3.7447 3.6977 Ave 5.9

3.8176

3.5878 0.0100 15.0

1,2-Dichlorobenzene 1.6272 1.4494 1.4499 1.6195 1.5470 Ave 5.1

1.5535

1.5411 0.0100 15.0

1,2-Dibromo-3-Chloropropane 0.0644 0.0544 0.0635 0.0646 0.0646 Ave 6.4

0.0628

0.0624 0.0100 15.0

1,2,4-Trichlorobenzene 0.8738 0.7880 0.6482 0.6991 0.6626 Ave 13.0

0.6310

0.7171 0.0100 15.0

Hexachlorobutadiene 0.7242 0.6321 0.5128 0.5239 0.5065 Qua2 0.9970

0.4844

0.8818 0.5560 0 0.0100 0.9900

Naphthalene 1.1224 1.0162 0.8640 0.9349 0.9173 Ave 11.0

0.8592

0.9523 0.0100 15.0

1,2,3-Trichlorobenzene 0.5335 0.5134 0.3651 0.3979 0.3833 Qua1 0.9960

0.3563

0.7983 0.4092 0 0.0100 0.9900

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 144 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06

Analy Batch No.: 171819

Calibration Start Date: 12/04/2012 14:34 Calibration End Date: 10745

Y

12/04/2012 16:55

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

Dibromofluoromethane 0.4904 0.5628 0.5010 0.4930 Ave 6.1

0.4930

0.5081 0.0100 15.0

1,2-Dichloroethane-d4 (Surr) 0.3874 0.4467 0.4112 0.3741 Ave 8.1

0.3671

0.3973 0.0100 15.0

Toluene-d8 (Surr) 1.2729 1.4691 1.3972 1.3024 Ave 5.9

1.3175

1.3518 0.0100 15.0

4-Bromofluorobenzene (Surr) 0.5575 0.6917 0.5810 0.5502 Ave 10.0

0.5574

0.5876 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 145 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06

Analy Batch No.: 171819

Calibration Start Date: 12/04/2012 14:34 Calibration End Date: 10745

Y

12/04/2012 16:55

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD1 500-171819/2 6I1204a.d

Level 2 STD2 500-171819/3 6I1204b.d

Level 3 STD3 500-171819/16 6I1204CC.d

Level 4 STD4 500-171819/5 6I1204d.d

Level 5 STD5 500-171819/6 6I1204e.d

Level 6 STD6 500-171819/7 6I1204f.d

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 6

Dichlorodifluoromethane PFB Ave 43859 164141 490706 1073926 1679708

2248613

5.00 20.0 50.0 100 150

200

Chloromethane PFB Ave 56677 220923 580439 1272796 1962205

2663554

5.00 20.0 50.0 100 150

200

Vinyl chloride PFB Ave 46653 183585 481633 1050014 1696104

2258770

5.00 20.0 50.0 100 150

200

Bromomethane PFB Ave 28282 107417 282609 595324 927883

1258628

5.00 20.0 50.0 100 150

200

Chloroethane PFB Ave 36835 142247 336325 760314 1173518

1541675

5.00 20.0 50.0 100 150

200

Dichlorofluoromethane PFB Ave 70972 289717 701331 1561621 2465148

3375221

5.00 20.0 50.0 100 150

200

Trichlorofluoromethane PFB Ave 66497 245578 602597 1353271 2150522

2845976

5.00 20.0 50.0 100 150

200

Acrolein PFB Ave 135143 569612 1253481 3165925 5578027

7777706

200 800 2000 4000 6000

8000

1,1-Dichloroethene PFB Ave 24678 101449 259314 609801 933026

1265158

5.00 20.0 50.0 100 150

200

1,1,2-Trichloro-1,2,2-trifluoroetha

ne

PFB Ave 34883 139553 354500 815530 1270129

1698517

5.00 20.0 50.0 100 150

200

Acetone PFB Qua2 8488 26036 63428 159396 237040

302744

5.00 20.0 50.0 100 150

200

Carbon disulfide PFB Ave 89310 366998 1060244 2497933 3425047

4648445

5.00 20.0 50.0 100 150

200

Acetonitrile PFB Qua2 28921 78586 160428 370513 610938

837530

40.0 160 400 800 1200

1600

Methylene Chloride PFB Ave 28603 102525 261307 561434 865406

1144172

5.00 20.0 50.0 100 150

200

Acrylonitrile PFB Ave 52548 224302 494214 1189147 2077128

2841154

40.0 160 400 800 1200

1600

trans-1,2-Dichloroethene PFB Ave 25567 112884 276266 647253 994785

1322919

5.00 20.0 50.0 100 150

200

FORM VI 8260B Page 146 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06

Analy Batch No.: 171819

Calibration Start Date: 12/04/2012 14:34 Calibration End Date: 10745

Y

12/04/2012 16:55

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 6

Methyl tert-butyl ether PFB Ave 52959 212291 550695 1292036 2020255

2677554

5.00 20.0 50.0 100 150

200

1,1-Dichloroethane PFB Ave 53766 234491 575476 1349737 2083045

2733212

5.00 20.0 50.0 100 150

200

Vinyl acetate PFB Ave 34285 148352 475662 999099 1719478

2109968

5.00 20.0 50.0 100 150

200

2,2-Dichloropropane PFB Ave 30324 131420 378910 857516 1317709

1790526

5.00 20.0 50.0 100 150

200

cis-1,2-Dichloroethene PFB Ave 27408 116876 275255 647076 1000867

1307173

5.00 20.0 50.0 100 150

200

2-Butanone (MEK) PFB Ave 6851 29888 86946 224026 335078

389110

5.00 20.0 50.0 100 150

200

Propionitrile DFB Ave 16200 69471 172732 411907 676543

912026

40.0 160 400 800 1200

1600

Bromochloromethane PFB Ave 11382 44936 111670 259302 397439

512811

5.00 20.0 50.0 100 150

200

Tetrahydrofuran PFB Ave 4143 19066 54053 118852 187613

232821

5.00 20.0 50.0 100 150

200

Chloroform PFB Ave 43364 176118 443833 1049184 1628033

2107213

5.00 20.0 50.0 100 150

200

1,1,1-Trichloroethane PFB Ave 38986 150190 424803 983576 1514014

2052266

5.00 20.0 50.0 100 150

200

Carbon tetrachloride DFB Ave 32398 127647 364091 875825 1385434

1859754

5.00 20.0 50.0 100 150

200

1,1-Dichloropropene PFB Ave 34609 145796 357712 864573 1339558

1723958

5.00 20.0 50.0 100 150

200

Benzene DFB Ave 95155 400069 977710 2359031 3597908

4656354

5.00 20.0 50.0 100 150

200

1,2-Dichloroethane DFB Ave 29859 123680 315359 780825 1199629

1528547

5.00 20.0 50.0 100 150

200

Trichloroethene DFB Ave 24265 107361 245590 613620 932877

1204163

5.00 20.0 50.0 100 150

200

1,2-Dichloropropane DFB Ave 25204 107370 261211 615728 957640

1234177

5.00 20.0 50.0 100 150

200

Dibromomethane DFB Ave 11382 47437 121081 274875 428159

547122

5.00 20.0 50.0 100 150

200

Bromodichloromethane DFB Ave 26117 105998 283529 698367 1075922

1375882

5.00 20.0 50.0 100 150

200

2-Chloroethyl vinyl ether DFB Ave 5843 24959 68276 143987 238709

290017

5.00 20.0 50.0 100 150

200

cis-1,3-Dichloropropene DFB Ave 26379 114470 291678 726654 1141580

1469116

5.00 20.0 50.0 100 150

200

FORM VI 8260B Page 147 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06

Analy Batch No.: 171819

Calibration Start Date: 12/04/2012 14:34 Calibration End Date: 10745

Y

12/04/2012 16:55

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 6

4-Methyl-2-pentanone (MIBK) DFB Ave 17991 65840 206982 492342 651507

834885

5.00 20.0 50.0 100 150

200

Toluene DFB Ave 55702 242332 588642 1472497 2296683

3044010

5.00 20.0 50.0 100 150

200

trans-1,3-Dichloropropene DFB Ave 20797 92184 257094 629495 984468

1265996

5.00 20.0 50.0 100 150

200

1,1,2-Trichloroethane PFB Ave 13050 57511 148789 353643 536069

677143

5.00 20.0 50.0 100 150

200

Tetrachloroethene CBZ Ave 28476 119937 285667 702154 1081677

1408855

5.00 20.0 50.0 100 150

200

1,3-Dichloropropane CBZ Ave 26131 102508 261720 613459 933524

1161967

5.00 20.0 50.0 100 150

200

2-Hexanone CBZ Ave 12375 47063 151685 313051 429948

539493

5.00 20.0 50.0 100 150

200

Dibromochloromethane CBZ Ave 14664 61941 175595 448008 686844

921214

5.00 20.0 50.0 100 150

200

1,2-Dibromoethane DFB Ave 13617 58743 151487 366417 562095

714479

5.00 20.0 50.0 100 150

200

1-Chlorohexane PFB Ave 36630 152507 373249 918779 1418488

1866410

5.00 20.0 50.0 100 150

200

Chlorobenzene CBZ Ave 68504 276932 679643 1615604 2515651

3327094

5.00 20.0 50.0 100 150

200

1,1,1,2-Tetrachloroethane CBZ Ave 19309 82263 239696 581547 888197

1211052

5.00 20.0 50.0 100 150

200

Ethylbenzene CBZ Ave 39579 157376 410826 962827 1458623

1921882

5.00 20.0 50.0 100 150

200

m&p-Xylene CBZ Ave 194973 825287 2091960 5201484 8273064

11198115

10.0 40.0 100 200 300

400

o-Xylene CBZ Ave 98229 418294 1086530 2648158 4120572

5677570

5.00 20.0 50.0 100 150

200

Styrene CBZ Ave 78124 321323 847341 2080656 3236183

4397468

5.00 20.0 50.0 100 150

200

Bromoform CBZ Qua1 10201 38689 123975 307486 498988

645544

5.00 20.0 50.0 100 150

200

Isopropylbenzene DCB Ave 130272 564468 1442467 3562774 5519222

7619657

5.00 20.0 50.0 100 150

200

Bromobenzene DCB Ave 30596 126275 345893 802763 1220221

1635156

5.00 20.0 50.0 100 150

200

1,1,2,2-Tetrachloroethane DCB Ave 19943 73051 209957 481053 711087

929968

5.00 20.0 50.0 100 150

200

1,2,3-Trichloropropane DCB Ave 5196 20570 60012 132626 206208

259470

5.00 20.0 50.0 100 150

200

FORM VI 8260B Page 148 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06

Analy Batch No.: 171819

Calibration Start Date: 12/04/2012 14:34 Calibration End Date: 10745

Y

12/04/2012 16:55

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 6

N-Propylbenzene DCB Ave 163962 687506 1781317 4395269 6795398

9343196

5.00 20.0 50.0 100 150

200

2-Chlorotoluene DCB Ave 89865 369703 986962 2392295 3625274

4909602

5.00 20.0 50.0 100 150

200

1,3,5-Trimethylbenzene DCB Ave 111807 469109 1259499 3156272 4882363

6753218

5.00 20.0 50.0 100 150

200

4-Chlorotoluene DCB Ave 107656 439914 1198655 2937794 4511715

6271477

5.00 20.0 50.0 100 150

200

tert-Butylbenzene DCB Ave 99569 417592 1078942 2682568 4063919

5595665

5.00 20.0 50.0 100 150

200

1,2,4-Trimethylbenzene DCB Ave 110242 481424 1274220 3159004 4740128

6597181

5.00 20.0 50.0 100 150

200

sec-Butylbenzene DCB Ave 152623 650935 1731399 4338355 6526887

9094371

5.00 20.0 50.0 100 150

200

1,3-Dichlorobenzene DCB Ave 63983 266610 734521 1727058 2580768

3462604

5.00 20.0 50.0 100 150

200

p-Isopropyltoluene DCB Ave 128325 559155 1487680 3697265 5571191

7694725

5.00 20.0 50.0 100 150

200

1,4-Dichlorobenzene DCB Ave 64014 271014 736764 1753770 2574188

3466362

5.00 20.0 50.0 100 150

200

n-Butylbenzene DCB Ave 124880 539658 1435179 3571282 5379380

7484397

5.00 20.0 50.0 100 150

200

1,2-Dichlorobenzene DCB Ave 56446 230617 635338 1544477 2250579

3045582

5.00 20.0 50.0 100 150

200

1,2-Dibromo-3-Chloropropane DCB Ave 2234 8654 27809 61605 93914

123129

5.00 20.0 50.0 100 150

200

1,2,4-Trichlorobenzene DCB Ave 30313 125376 284038 666706 963905

1237013

5.00 20.0 50.0 100 150

200

Hexachlorobutadiene DCB Qua2 25123 100580 224721 499659 736880

949639

5.00 20.0 50.0 100 150

200

Naphthalene DCB Ave 38935 161681 378609 891566 1334461

1684456

5.00 20.0 50.0 100 150

200

1,2,3-Trichlorobenzene DCB Qua1 18507 81690 160002 379519 557639

698427

5.00 20.0 50.0 100 150

200

Dibromofluoromethane PFB Ave 98301 281110 581916 839156

1103934

20.0 50.0 100 150

200

1,2-Dichloroethane-d4 (Surr) DFB Ave 110679 317143 649071 898908

1178930

20.0 50.0 100 150

200

Toluene-d8 (Surr) DFB Ave 363660 1042887 2205424 3129848

4231595

20.0 50.0 100 150

200

4-Bromofluorobenzene (Surr) CBZ Ave 155143 481503 891809 1271160

1755381

20.0 50.0 100 150

200

FORM VI 8260B Page 149 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06

Analy Batch No.: 171819

Calibration Start Date: 12/04/2012 14:34 Calibration End Date: 10745

Y

12/04/2012 16:55

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

Curve Type Legend:

Ave = Average ISTD

Qua1 = Quadratic 1/conc ISTD

Qua2 = Quadratic 1/conc^2 ISTD

FORM VI 8260B Page 150 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06

Analy Batch No.: 171819

Calibration Start Date: 12/04/2012 17:18 Calibration End Date: 10746

Y

12/04/2012 19:13

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD1AP 500-171819/8 6J1204a.d

Level 2 STD2AP 500-171819/9 6J1204b.d

Level 3 STD3AP 500-171819/10 6J1204c.d

Level 4 STD4AP 500-171819/11 6J1204d.d

Level 5 STD5AP 500-171819/12 6J1204e.d

Level 6 STD6AP 500-171819/13 6J1204f.d

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

Butadiene 1.1704 1.2279 1.0968 1.0951 1.2079 Ave 4.9

1.1968

1.1658 0.0100 15.0

Ethyl ether 0.4055 0.4456 0.4198 0.4298 0.4343 Ave 4.3

0.4585

0.4323 0.0100 15.0

Iodomethane 0.8397 0.9524 0.8632 0.8823 0.9390 Ave 5.3

0.9416

0.9030 0.0100 15.0

3-Chloropropene 0.2619 0.2954 0.2794 0.2819 0.3038 Ave 5.8

0.3056

0.2880 0.0100 15.0

Methyl acetate 0.3659 0.3821 0.3530 0.3743 0.3937 Ave 4.9

0.4044

0.3789 0.0100 15.0

Hexane 1.0003 1.1165 1.0302 1.0554 1.1162 Ave 4.7

1.1125

1.0719 0.0100 15.0

Isopropyl ether 2.2067 2.4360 2.2917 2.4215 2.6213 Ave 7.4

2.6764

2.4423 0.0100 15.0

2-Chloro-1,3-butadiene 1.3107 1.4329 1.3162 1.3940 1.5159 Ave 6.8

1.5380

1.4179 0.0100 15.0

Ethyl acetate 0.2404 0.2813 0.2686 0.3098 0.3063 Ave 11.0

0.3315

0.2896 0.0100 15.0

Methacrylonitrile 0.1777 0.2152 0.2127 0.2335 0.2315 Ave 11.0

0.2515

0.2203 0.0100 15.0

Cyclohexane 1.7178 1.6284 1.4552 1.4768 1.5751 Ave 6.2

1.5846

1.5730 0.0100 15.0

Isobutyl alcohol 0.0083 0.0098 0.0098 0.0102 0.0114 Ave 13.0

0.0121

0.0103 0.0010 15.0

2,2,4-Trimethylpentane 2.3074 2.4860 2.3789 2.4529 2.7064 Ave 6.4

2.6728

2.5007 0.0100 15.0

Heptane 0.8426 0.8469 0.7982 0.8634 0.8905 Ave 3.8

0.8766

0.8530 0.0100 15.0

n-Butyl alcohol 0.0048 0.0056 0.0058 0.0059 0.0064 Ave 13.0

0.0071

0.0059 0.0010 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 151 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06

Analy Batch No.: 171819

Calibration Start Date: 12/04/2012 17:18 Calibration End Date: 10746

Y

12/04/2012 19:13

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

Methylcyclohexane 0.7683 0.7541 0.7187 0.7323 0.7887 Ave 3.4

0.7633

0.7542 0.0100 15.0

Methyl methacrylate 0.1957 0.2053 0.2090 0.2411 0.2381 Ave 9.1

0.2389

0.2214 0.0100 15.0

2-Nitropropane 0.0351 0.0557 0.0721 0.1027 0.1025 Qua2 0.9930

+++++

-10.85 0.0598 0 0.0100 0.9900

Ethyl methacrylate 0.2333 0.2512 0.2648 0.3057 0.3063 Ave 12.0

0.3124

0.2789 0.0100 15.0

Cyclohexanone 0.0920 0.0927 0.0912 0.1071 0.1152 Ave 9.8

0.0978

0.0993 0.0100 15.0

trans-1,4-Dichloro-2-butene 0.0533 0.0601 0.0614 0.0784 0.0825 Qua2 0.9980

0.0877

-0.055 0.0579 0.0001 0.0100 0.9900

Pentachloroethane 0.1724 0.2179 0.2343 0.2686 0.2970 Qua1 1.0000

0.3217

-0.463 0.2162 0.0003 0.0100 0.9900

1,3,5-Trichlorobenzene 1.0853 1.1609 1.1040 1.1775 1.1901 Ave 4.3

1.2094

1.1545 0.0100 15.0

2-Methylnaphthalene 0.1748 0.2149 0.2505 0.1973 0.1786 Ave 15.0

0.1792

0.1992 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 152 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06

Analy Batch No.: 171819

Calibration Start Date: 12/04/2012 17:18 Calibration End Date: 10746

Y

12/04/2012 19:13

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD1AP 500-171819/8 6J1204a.d

Level 2 STD2AP 500-171819/9 6J1204b.d

Level 3 STD3AP 500-171819/10 6J1204c.d

Level 4 STD4AP 500-171819/11 6J1204d.d

Level 5 STD5AP 500-171819/12 6J1204e.d

Level 6 STD6AP 500-171819/13 6J1204f.d

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 6

Butadiene PFB Ave 59711 237793 571982 1316107 2109867

2854272

5.00 20.0 50.0 100 150

200

Ethyl ether PFB Ave 20688 86288 218958 516528 758551

1093569

5.00 20.0 50.0 100 150

200

Iodomethane PFB Ave 85680 368876 900336 2120722 3280480

4491113

10.0 40.0 100 200 300

400

3-Chloropropene PFB Ave 26728 114414 291463 677502 1061303

1457750

10.0 40.0 100 200 300

400

Methyl acetate PFB Ave 18668 73994 184121 449843 687679

964469

5.00 20.0 50.0 100 150

200

Hexane PFB Ave 51033 216226 537281 1268344 1949746

2653141

5.00 20.0 50.0 100 150

200

Isopropyl ether PFB Ave 112584 471760 1195143 2910208 4578669

6382856

5.00 20.0 50.0 100 150

200

2-Chloro-1,3-butadiene PFB Ave 66870 277486 686432 1675330 2647867

3667880

5.00 20.0 50.0 100 150

200

Ethyl acetate PFB Ave 122628 544727 1400541 3723072 5350060

7905489

50.0 200 500 1000 1500

2000

Methacrylonitrile PFB Ave 18131 83366 221818 561287 808714

1199565

10.0 40.0 100 200 300

400

Cyclohexane PFB Ave 87638 315360 758916 1774856 2751328

3779005

5.00 20.0 50.0 100 150

200

Isobutyl alcohol DFB Ave 47241 215613 569014 1358590 2205141

3307499

400 1600 4000 8000 12000

16000

2,2,4-Trimethylpentane DFB Ave 163991 685120 1728564 4079936 6520240

9114501

5.00 20.0 50.0 100 150

200

Heptane DFB Ave 59885 233399 579970 1436130 2145365

2989361

5.00 20.0 50.0 100 150

200

n-Butyl alcohol DFB Ave 27396 122976 334412 783861 1241059

1940445

400 1600 4000 8000 12000

16000

Methylcyclohexane DFB Ave 54604 207825 522199 1217989 1900254

2602848

5.00 20.0 50.0 100 150

200

FORM VI 8260B Page 153 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS06

Analy Batch No.: 171819

Calibration Start Date: 12/04/2012 17:18 Calibration End Date: 10746

Y

12/04/2012 19:13

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 6

Methyl methacrylate DFB Ave 27819 113160 303724 802035 1147404

1629272

10.0 40.0 100 200 300

400

2-Nitropropane CBZ Qua2 201751 1223343 4064819 13015638 18258126

+++++

400 1600 4000 8000 12000

+++++

Ethyl methacrylate CBZ Ave 33510 137818 372926 968505 1363976

1949555

10.0 40.0 100 200 300

400

Cyclohexanone DCB Ave 291150 1128500 2979450 7326382 11645121

14112174

400 1600 4000 8000 12000

16000

trans-1,4-Dichloro-2-butene DCB Qua2 4219 18285 50159 134107 208467

316432

10.0 40.0 100 200 300

400

Pentachloroethane CBZ Qua1 24768 119564 330026 850927 1322444

2007968

10.0 40.0 100 200 300

400

1,3,5-Trichlorobenzene DCB Ave 42917 176629 450823 1006931 1503887

2180690

5.00 20.0 50.0 100 150

200

2-Methylnaphthalene DCB Ave 6911 32696 102284 168750 225710

323153

5.00 20.0 50.0 100 150

200

Curve Type Legend:

Ave = Average ISTD

Qua1 = Quadratic 1/conc ISTD

Qua2 = Quadratic 1/conc^2 ISTD

FORM VI 8260B Page 154 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS18

Analy Batch No.: 170445

Calibration Start Date: 11/20/2012 15:57 Calibration End Date: 10631

N

11/20/2012 19:11

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD1 500-170445/2 18I1120a.D

Level 2 STD2 500-170445/3 18I1120b.D

Level 3 STD3 500-170445/4 18I1120c.D

Level 4 STD4 500-170445/5 18I1120d.D

Level 5 STD5 500-170445/6 18I1120e.D

Level 6 STD6 500-170445/7 18I1120f.D

Level 7 STD7 500-170445/8 18I1120g.D

Level 8 STD8 500-170445/9 18I1120h.D

Level 9 STD9 500-170445/10 18I1120i.D

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Dichlorodifluoromethane 0.7338 0.6750 0.7042 0.6488 Ave 6.8

0.7956 0.7810 0.7176 0.7221

0.7223 0.0100 15.0

Chloromethane 1.2860 1.1580 1.1717 1.1390 Ave 5.4

1.3030 1.2866 1.1921 1.1898

1.2158 0.1000 15.0

Vinyl chloride 1.1427 1.0156 0.9540 0.9692 0.9488 Ave 6.5

1.0791 1.0587 0.9766 0.9852

1.0144 0.0100 15.0

Bromomethane 0.3482 0.3298 0.3321 0.2943 Ave 6.5

0.3516 0.3385 0.3092 0.3044

0.3260 0.0100 15.0

Chloroethane 0.5912 0.5020 0.5201 0.4820 Ave 8.5

0.5808 0.5581 0.5185 0.4684

0.5276 0.0100 15.0

Dichlorofluoromethane 1.4329 1.2045 1.2387 1.2316 Ave 6.4

1.3761 1.3461 1.2456 1.2517

1.2909 0.0100 15.0

Trichlorofluoromethane 0.9993 0.9030 0.9346 0.8909 Ave 5.6

1.0344 1.0178 0.9348 0.9353

0.9563 0.0100 15.0

Acrolein 0.0719 0.0591 0.0800 0.0615 Ave 9.6

0.0689 0.0685 0.0645 0.0665

0.0676 0.0010 15.0

1,1-Dichloroethene 0.5297 0.4450 0.4581 0.4790 Ave 6.0

0.5196 0.5052 0.4753 0.4816

0.4867 0.0100 15.0

1,1,2-Trichloro-1,2,2-trifluoroethane 0.6606 0.5974 0.5413 0.5572 Ave 6.9

0.6108 0.5938 0.5501 0.5574

0.5836 0.0100 15.0

Acetone 0.1029 0.0956 Ave 7.3

0.0848 0.0903 0.0873 0.0882

0.0915 0.0100 15.0

Carbon disulfide 1.5830 1.4327 1.5370 1.5837 Ave 9.4

1.8591 1.8605 1.7443 1.7493

1.6687 0.0100 15.0

Acetonitrile 0.0400 0.0356 0.0512 0.0362 Ave 12.0

0.0424 0.0425 0.0390 0.0428

0.0412 0.0010 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 155 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS18

Analy Batch No.: 170445

Calibration Start Date: 11/20/2012 15:57 Calibration End Date: 10631

N

11/20/2012 19:11

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Methylene Chloride 0.5261 0.4806 Ave 4.2

0.5308 0.5188 0.4882 0.4954

0.5067 0.0100 15.0

Acrylonitrile 0.1467 0.1176 0.1594 0.1248 Ave 9.9

0.1349 0.1373 0.1269 0.1301

0.1347 0.0010 15.0

trans-1,2-Dichloroethene 0.5747 0.5119 0.5545 0.5254 Ave 4.6

0.5816 0.5629 0.5334 0.5335

0.5473 0.0100 15.0

Methyl tert-butyl ether 0.8852 0.8766 0.9303 0.8415 Ave 4.2

0.9549 0.9472 0.9009 0.9148

0.9064 0.0100 15.0

1,1-Dichloroethane 1.3378 1.2396 1.3158 1.2700 Ave 3.7

1.3899 1.3714 1.3180 1.3226

1.3206 0.1000 15.0

Vinyl acetate 0.5108 0.4714 0.5364 0.5886 Ave 13.0

0.6138 0.6506 0.6565 0.6805

0.5886 0.0100 15.0

2,2-Dichloropropane 0.6695 0.6433 0.6812 0.6374 Ave 5.4

0.7445 0.7127 0.6703 0.6503

0.6761 0.0100 15.0

cis-1,2-Dichloroethene 0.5502 0.5439 0.5613 0.5408 Ave 3.0

0.5868 0.5834 0.5602 0.5614

0.5610 0.0100 15.0

2-Butanone (MEK) 0.1124 0.1153 Ave 2.6

0.1184 0.1197 0.1182 0.1206

0.1174 0.0100 15.0

Propionitrile 0.0313 0.0268 0.0378 0.0287 Ave 11.0

0.0314 0.0310 0.0285 0.0306

0.0308 0.0010 15.0

Bromochloromethane 0.1934 0.1994 0.2158 0.1978 Ave 3.8

0.2104 0.2119 0.2066 0.2093

0.2056 0.0100 15.0

Tetrahydrofuran 0.0851 0.0879 0.0770 Ave 5.0

0.0835 0.0801 0.0770 0.0827

0.0819 0.0100 15.0

Chloroform 0.9654 0.8255 0.8994 0.8709 Ave 5.1

0.9523 0.9477 0.9158 0.9228

0.9125 0.0100 15.0

1,1,1-Trichloroethane 0.8785 0.7529 0.8420 0.8062 Ave 6.8

0.9396 0.9107 0.8721 0.8712

0.8591 0.0100 15.0

1,1-Dichloropropene 0.7821 0.6377 0.7218 0.7194 Ave 6.5

0.7790 0.7731 0.7571 0.7629

0.7416 0.0100 15.0

Carbon tetrachloride 0.5107 0.4412 0.5096 0.4911 Ave 8.7

0.5870 0.5667 0.5374 0.5344

0.5223 0.0100 15.0

Benzene 1.4886 1.5332 1.4063 1.4138 1.3805 Ave 3.5

1.5010 1.4545 1.4161 1.4307

1.4472 0.0100 15.0

1,2-Dichloroethane 0.4761 0.4439 0.4731 0.4415 Ave 2.9

0.4748 0.4618 0.4547 0.4579

0.4605 0.0100 15.0

Trichloroethene 0.3207 0.3414 0.3390 0.3794 0.3544 Ave 5.4

0.3779 0.3672 0.3578 0.3577

0.3551 0.0100 15.0

1,2-Dichloropropane 0.4312 0.3991 0.4136 0.4077 Ave 2.9

0.4329 0.4287 0.4205 0.4243

0.4197 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 156 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS18

Analy Batch No.: 170445

Calibration Start Date: 11/20/2012 15:57 Calibration End Date: 10631

N

11/20/2012 19:11

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Dibromomethane 0.1386 0.1165 0.1443 0.1342 Ave 6.4

0.1439 0.1372 0.1350 0.1370

0.1358 0.0100 15.0

Bromodichloromethane 0.3362 0.3129 0.3377 0.3404 Ave 10.0

0.3975 0.4057 0.3976 0.4063

0.3668 0.0100 15.0

2-Chloroethyl vinyl ether 0.1224 0.1144 0.1157 Ave 3.2

0.1238 0.1221 0.1197 0.1235

0.1202 0.0100 15.0

cis-1,3-Dichloropropene 0.3678 0.3467 0.3644 0.3844 Ave 8.5

0.4186 0.4256 0.4262 0.4325

0.3958 0.0100 15.0

4-Methyl-2-pentanone (MIBK) 0.1829 0.1800 Ave 3.4

0.1943 0.1966 0.1871 0.1900

0.1885 0.0100 15.0

Toluene 1.1580 0.9918 0.8547 0.8677 0.8335 Ave 12.0

0.8854 0.8601 0.8535 0.8547

0.9066 0.0100 15.0

trans-1,3-Dichloropropene 0.3097 0.2793 0.3328 0.3074 Ave 7.1

0.3433 0.3429 0.3351 0.3401

0.3238 0.0100 15.0

1,1,2-Trichloroethane 0.2534 0.2322 0.2524 0.2286 Ave 4.3

0.2516 0.2512 0.2459 0.2576

0.2466 0.0100 15.0

Tetrachloroethene 0.4492 0.4398 0.4337 0.4385 Ave 2.8

0.4617 0.4681 0.4558 0.4596

0.4508 0.0100 15.0

1,3-Dichloropropane 0.3858 0.3467 0.3557 0.3562 Ave 3.4

0.3656 0.3727 0.3656 0.3739

0.3653 0.0100 15.0

2-Hexanone 0.1089 0.1175 0.1401 0.1364 Ave 10.0

0.1471 0.1426 0.1365 0.1408

0.1337 0.0100 15.0

Dibromochloromethane 0.1900 0.1736 0.2021 0.2205 Qua1 0.9990

0.2517 0.2684 0.2695 0.2761

-0.106 0.2438 0.0002 0.0100 0.9900

1,2-Dibromoethane 0.1644 0.1549 0.1734 0.1590 Ave 5.1

0.1804 0.1757 0.1681 0.1723

0.1685 0.0100 15.0

1-Chlorohexane 0.8953 0.7648 0.7777 0.6935 Ave 9.7

0.7354 0.6989 0.6812 0.6863

0.7416 0.0100 15.0

Chlorobenzene 1.1696 1.0700 1.0714 1.0376 Ave 3.6

1.1112 1.1051 1.0731 1.0863

1.0905 0.3000 15.0

1,1,1,2-Tetrachloroethane 0.3171 0.3068 0.3312 0.3619 Ave 12.0

0.3996 0.4084 0.3959 0.4065

0.3659 0.0100 15.0

Ethylbenzene 0.5274 0.7232 0.6150 0.6311 0.6209 Ave 8.1

0.6592 0.6578 0.6419 0.6474

0.6360 0.0100 15.0

m&p-Xylene 1.6363 1.7620 1.5234 1.6457 1.6034 Ave 3.9

1.6868 1.6799 1.6536 1.6749

1.6518 0.0100 15.0

o-Xylene 1.8102 1.8258 1.6028 1.7142 1.6856 Ave 4.0

1.7908 1.7872 1.7297 1.7570

1.7448 0.0100 15.0

Styrene 1.1746 1.1005 1.1331 1.1639 Ave 5.4

1.2785 1.2554 1.2153 1.2608

1.1978 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 157 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS18

Analy Batch No.: 170445

Calibration Start Date: 11/20/2012 15:57 Calibration End Date: 10631

N

11/20/2012 19:11

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Bromoform 0.1284 0.1085 0.1145 0.1248 Qua1 0.9980

0.1534 0.1612 0.1520 0.1629

-0.055 0.1446 0.0001 0.0100 0.9900

Isopropylbenzene 4.2314 3.7736 3.9887 3.9381 Ave 3.8

4.1197 4.2012 4.1587 4.0117

4.0529 0.0100 15.0

1,1,2,2-Tetrachloroethane 0.4276 0.3620 0.4007 0.3818 Ave 5.3

0.4104 0.4211 0.4073 0.4017

0.4016 0.3000 15.0

Bromobenzene 0.8931 0.7685 0.7991 0.7595 Ave 5.3

0.8097 0.8250 0.7902 0.7728

0.8022 0.0100 15.0

1,2,3-Trichloropropane 0.3808 0.4432 0.3768 0.3278 Ave 11.0

0.3415 0.3477 0.3343 0.3316

0.3605 0.0100 15.0

N-Propylbenzene 5.1681 4.7986 4.9942 4.7379 Ave 3.1

4.9793 4.9463 4.8618 4.7157

4.9002 0.0100 15.0

2-Chlorotoluene 3.0539 2.7202 2.7737 2.6873 Ave 4.2

2.8228 2.7997 2.7555 2.7030

2.7895 0.0100 15.0

1,3,5-Trimethylbenzene 3.6387 3.3372 3.4450 3.3941 Ave 2.9

3.5063 3.5193 3.4302 3.3558

3.4533 0.0100 15.0

4-Chlorotoluene 3.5578 3.2742 3.2260 3.1288 Ave 4.5

3.2775 3.2548 3.1464 3.0856

3.2439 0.0100 15.0

tert-Butylbenzene 3.2830 3.0181 3.0684 2.9870 Ave 3.6

3.0707 3.1288 3.0264 2.9090

3.0614 0.0100 15.0

1,2,4-Trimethylbenzene 3.5921 3.3337 3.4708 3.3906 Ave 3.0

3.5334 3.4591 3.3609 3.2995

3.4300 0.0100 15.0

sec-Butylbenzene 4.9350 4.5273 4.7174 4.5348 Ave 3.7

4.6396 4.6676 4.4654 4.3972

4.6105 0.0100 15.0

1,3-Dichlorobenzene 1.9785 1.7239 1.6892 1.6864 Ave 5.9

1.7675 1.7515 1.6801 1.6615

1.7423 0.0100 15.0

p-Isopropyltoluene 3.9642 3.7212 3.9739 3.8805 Ave 3.3

3.9796 3.8852 3.7249 3.6715

3.8501 0.0100 15.0

1,4-Dichlorobenzene 1.9674 1.7052 1.6790 1.6718 Ave 6.4

1.7246 1.7082 1.6358 1.6171

1.7136 0.0100 15.0

n-Butylbenzene 3.9856 3.3804 3.6510 3.6521 Ave 5.6

3.8154 3.6445 3.4622 3.4262

3.6272 0.0100 15.0

1,2-Dichlorobenzene 1.4901 1.3671 1.4686 1.4289 Ave 3.8

1.4898 1.4439 1.3702 1.3615

1.4275 0.0100 15.0

1,2-Dibromo-3-Chloropropane 0.0460 0.0507 0.0544 Ave 5.4

0.0521 0.0536 0.0525 0.0532

0.0518 0.0100 15.0

1,2,4-Trichlorobenzene 0.8532 0.8127 0.8024 0.8009 Ave 9.2

0.7959 0.7068 0.6649 0.6769

0.7642 0.0100 15.0

Hexachlorobutadiene 0.8562 0.7248 0.7313 0.7212 Qua1 0.9980

0.6728 0.5630 0.5015 0.4887

0.1731 0.6915 -0.001 0.0100 0.9900

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 158 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS18

Analy Batch No.: 170445

Calibration Start Date: 11/20/2012 15:57 Calibration End Date: 10631

N

11/20/2012 19:11

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Naphthalene 1.0176 0.8863 0.9288 0.9698 Ave 5.0

0.9721 0.9267 0.8854 0.8994

0.9358 0.0100 15.0

1,2,3-Trichlorobenzene 0.5836 0.5407 0.5545 0.5610 Ave 13.0

0.4837 0.4451 0.4210 0.4262

0.5020 0.0100 15.0

Dibromofluoromethane 0.4463 Ave 0.7

0.4392 0.4398 0.4390 0.4388

0.4406 0.0100 15.0

1,2-Dichloroethane-d4 (Surr) 0.3358 Ave 2.3

0.3221 0.3166 0.3185 0.3211

0.3228 0.0100 15.0

Toluene-d8 (Surr) 1.2359 Ave 2.0

1.2155 1.1763 1.1979 1.1868

1.2025 0.0100 15.0

4-Bromofluorobenzene (Surr) 0.5753 Ave 3.3

0.5469 0.5381 0.5310 0.5349

0.5452 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 159 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS18

Analy Batch No.: 170445

Calibration Start Date: 11/20/2012 15:57 Calibration End Date: 10631

N

11/20/2012 19:11

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD1 500-170445/2 18I1120a.D

Level 2 STD2 500-170445/3 18I1120b.D

Level 3 STD3 500-170445/4 18I1120c.D

Level 4 STD4 500-170445/5 18I1120d.D

Level 5 STD5 500-170445/6 18I1120e.D

Level 6 STD6 500-170445/7 18I1120f.D

Level 7 STD7 500-170445/8 18I1120g.D

Level 8 STD8 500-170445/9 18I1120h.D

Level 9 STD9 500-170445/10 18I1120i.D

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Dichlorodifluoromethane PFB Ave 4428 8167 21374 77652

237482 453960 660813 863594

1.00 2.00 5.00 20.0

50.0 100 150 200

Chloromethane PFB Ave 7760 14011 35565 136324

388934 747832 1097875 1422948

1.00 2.00 5.00 20.0

50.0 100 150 200

Vinyl chloride PFB Ave 1647 6128 11543 29417 113560

322098 615375 899388 1178212

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

Bromomethane PFB Ave 2101 3990 10080 35229

104945 196730 284749 364048

1.00 2.00 5.00 20.0

50.0 100 150 200

Chloroethane PFB Ave 3567 6074 15785 57691

173373 324430 477518 560155

1.00 2.00 5.00 20.0

50.0 100 150 200

Dichlorofluoromethane PFB Ave 8646 14573 37598 147409

410750 782459 1147085 1496932

1.00 2.00 5.00 20.0

50.0 100 150 200

Trichlorofluoromethane PFB Ave 6030 10925 28367 106635

308763 591581 860858 1118561

1.00 2.00 5.00 20.0

50.0 100 150 200

Acrolein PFB Ave 17342 28579 77741 294486

822987 1593549 2377631 3182501

40.0 80.0 160 800

2000 4000 6000 8000

1,1-Dichloroethene PFB Ave 3196 5384 13905 57336

155084 293661 437758 575993

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,2-Trichloro-1,2,2-trifluoroetha

ne

PFB Ave 3986 7228 16431 66697

182329 345170 506637 666624

1.00 2.00 5.00 20.0

50.0 100 150 200

Acetone PFB Ave 3122 11444

25305 52491 80381 105504

5.00 20.0

50.0 100 150 200

Carbon disulfide PFB Ave 9552 17334 46652 189561

554912 1081416 1606370 2092089

1.00 2.00 5.00 20.0

50.0 100 150 200

Acetonitrile PFB Ave 1929 3447 9954 34669

101259 197646 287117 409799

8.00 16.0 32.0 160

400 800 1200 1600

Methylene Chloride PFB Ave 15967 57524

158440 301578 449566 592532

5.00 20.0

50.0 100 150 200

FORM VI 8260B Page 160 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS18

Analy Batch No.: 170445

Calibration Start Date: 11/20/2012 15:57 Calibration End Date: 10631

N

11/20/2012 19:11

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Acrylonitrile PFB Ave 7080 11384 30965 119456

322243 638325 934627 1244356

8.00 16.0 32.0 160

400 800 1200 1600

trans-1,2-Dichloroethene PFB Ave 3468 6194 16831 62888

173615 327201 491180 638066

1.00 2.00 5.00 20.0

50.0 100 150 200

Methyl tert-butyl ether PFB Ave 5341 10606 28238 100722

285018 550550 829648 1094110

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1-Dichloroethane PFB Ave 8072 14998 39937 152015

414855 797118 1213789 1581777

1.00 2.00 5.00 20.0

50.0 100 150 200

Vinyl acetate PFB Ave 3082 5703 16282 70452

183216 378182 604588 813877

1.00 2.00 5.00 20.0

50.0 100 150 200

2,2-Dichloropropane PFB Ave 4040 7783 20675 76289

222237 414248 617252 777686

1.00 2.00 5.00 20.0

50.0 100 150 200

cis-1,2-Dichloroethene PFB Ave 3320 6581 17037 64724

175158 339128 515903 671364

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Butanone (MEK) PFB Ave 3412 13802

35344 69602 108820 144223

5.00 20.0

50.0 100 150 200

Propionitrile DFB Ave 2135 3666 10388 39240

106076 210679 309144 433017

8.00 16.0 32.0 160

400 800 1200 1600

Bromochloromethane PFB Ave 1167 2413 6549 23678

62801 123161 190248 250350

1.00 2.00 5.00 20.0

50.0 100 150 200

Tetrahydrofuran PFB Ave 1030 2669 9218

24911 46566 70932 98870

2.00 5.00 20.0

50.0 100 150 200

Chloroform PFB Ave 5825 9988 27298 104239

284237 550852 843425 1103685

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,1-Trichloroethane PFB Ave 5301 9109 25556 96492

280448 529365 803103 1041932

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1-Dichloropropene PFB Ave 4719 7715 21907 86111

232530 449389 697190 912451

1.00 2.00 5.00 20.0

50.0 100 150 200

Carbon tetrachloride DFB Ave 4360 7543 21865 83989

248145 481322 728007 946559

1.00 2.00 5.00 20.0

50.0 100 150 200

Benzene DFB Ave 3017 13088 24041 60664 236113

634552 1235303 1918162 2534344

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichloroethane DFB Ave 4064 7589 20299 75513

200744 392237 615935 811172

1.00 2.00 5.00 20.0

50.0 100 150 200

Trichloroethene DFB Ave 650 2914 5795 16279 60619

159741 311893 484646 633687

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichloropropane DFB Ave 3681 6823 17748 69728

183000 364055 569576 751565

1.00 2.00 5.00 20.0

50.0 100 150 200

Dibromomethane DFB Ave 1183 1992 6192 22952

60829 116511 182922 242675

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromodichloromethane DFB Ave 2870 5349 14490 58227

168039 344530 538558 719678

1.00 2.00 5.00 20.0

50.0 100 150 200

FORM VI 8260B Page 161 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS18

Analy Batch No.: 170445

Calibration Start Date: 11/20/2012 15:57 Calibration End Date: 10631

N

11/20/2012 19:11

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

2-Chloroethyl vinyl ether DFB Ave 2092 4907 19794

52323 103721 162181 218791

2.00 5.00 20.0

50.0 100 150 200

cis-1,3-Dichloropropene DFB Ave 3140 5927 15638 65745

176977 361449 577374 766148

1.00 2.00 5.00 20.0

50.0 100 150 200

4-Methyl-2-pentanone (MIBK) DFB Ave 7847 30778

82132 166973 253451 336514

5.00 20.0

50.0 100 150 200

Toluene DFB Ave 2347 8467 14612 37231 142550

374325 730485 1156106 1514024

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

trans-1,3-Dichloropropene DFB Ave 2644 4775 14282 52572

145145 291191 453866 602491

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,2-Trichloroethane PFB Ave 1529 2809 7662 27366

75094 145995 226443 308046

1.00 2.00 5.00 20.0

50.0 100 150 200

Tetrachloroethene CBZ Ave 3428 6819 17026 64907

175016 340834 523590 688379

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3-Dichloropropane CBZ Ave 2944 5376 13966 52729

138581 271339 420026 560106

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Hexanone CBZ Ave 831 1821 5499 20191

55760 103797 156763 210949

1.00 2.00 5.00 20.0

50.0 100 150 200

Dibromochloromethane CBZ Qua1 1450 2691 7934 32638

95420 195441 309596 413567

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dibromoethane DFB Ave 1403 2648 7441 27200

76258 149204 227695 305255

1.00 2.00 5.00 20.0

50.0 100 150 200

1-Chlorohexane PFB Ave 5402 9253 23606 83008

219512 406222 627330 820810

1.00 2.00 5.00 20.0

50.0 100 150 200

Chlorobenzene CBZ Ave 8925 16590 42064 153586

421256 804594 1232828 1627111

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,1,2-Tetrachloroethane CBZ Ave 2420 4756 13003 53568

151502 297319 454804 608869

1.00 2.00 5.00 20.0

50.0 100 150 200

Ethylbenzene CBZ Ave 1001 5518 9536 24778 91915

249878 478916 737488 969682

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

m&p-Xylene CBZ Ave 6212 26890 47238 129222 474697

1278862 2446178 3799344 5017706

0.500 2.00 4.00 10.0 40.0

100 200 300 400

o-Xylene CBZ Ave 3436 13932 24851 67298 249516

678885 1301206 1987127 2631883

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

Styrene CBZ Ave 8963 17063 44487 172291

484663 914023 1396155 1888531

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromoform CBZ Qua1 980 1683 4496 18471

58151 117392 174647 243999

1.00 2.00 5.00 20.0

50.0 100 150 200

Isopropylbenzene DCB Ave 17989 31740 85220 327893

896099 1712979 2603073 3443871

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,2,2-Tetrachloroethane DCB Ave 1818 3045 8560 31787

89262 171689 254958 344835

1.00 2.00 5.00 20.0

50.0 100 150 200

FORM VI 8260B Page 162 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS18

Analy Batch No.: 170445

Calibration Start Date: 11/20/2012 15:57 Calibration End Date: 10631

N

11/20/2012 19:11

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Bromobenzene DCB Ave 3797 6464 17072 63237

176130 336370 494607 663460

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,3-Trichloropropane DCB Ave 1619 3728 8051 27297

74292 141778 209279 284640

1.00 2.00 5.00 20.0

50.0 100 150 200

N-Propylbenzene DCB Ave 21971 40362 106702 394484

1083084 2016808 3043187 4048215

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Chlorotoluene DCB Ave 12983 22880 59261 223750

613999 1141536 1724760 2320390

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3,5-Trimethylbenzene DCB Ave 15469 28070 73602 282593

762675 1434967 2147102 2880791

1.00 2.00 5.00 20.0

50.0 100 150 200

4-Chlorotoluene DCB Ave 15125 27540 68924 260507

712921 1327120 1969455 2648838

1.00 2.00 5.00 20.0

50.0 100 150 200

tert-Butylbenzene DCB Ave 13957 25386 65556 248701

667934 1275738 1894346 2497268

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,4-Trimethylbenzene DCB Ave 15271 28040 74154 282303

768572 1410421 2103731 2832505

1.00 2.00 5.00 20.0

50.0 100 150 200

sec-Butylbenzene DCB Ave 20980 38080 100788 377573

1009183 1903144 2795060 3774788

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3-Dichlorobenzene DCB Ave 8411 14500 36090 140409

384456 714135 1051607 1426299

1.00 2.00 5.00 20.0

50.0 100 150 200

p-Isopropyltoluene DCB Ave 16853 31300 84902 323099

865624 1584145 2331542 3151868

1.00 2.00 5.00 20.0

50.0 100 150 200

1,4-Dichlorobenzene DCB Ave 8364 14343 35872 139195

375139 696479 1023879 1388234

1.00 2.00 5.00 20.0

50.0 100 150 200

n-Butylbenzene DCB Ave 16944 28433 78005 304075

829908 1485993 2167095 2941291

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichlorobenzene DCB Ave 6335 11499 31377 118970

324054 588746 857673 1168761

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dibromo-3-Chloropropane DCB Ave 387 1083 4527

11328 21855 32865 45663

2.00 5.00 20.0

50.0 100 150 200

1,2,4-Trichlorobenzene DCB Ave 3627 6836 17143 66682

173111 288183 416167 581056

1.00 2.00 5.00 20.0

50.0 100 150 200

Hexachlorobutadiene DCB Qua1 3640 6096 15625 60048

146348 229558 313901 419544

1.00 2.00 5.00 20.0

50.0 100 150 200

Naphthalene DCB Ave 4326 7455 19844 80746

211438 377865 554224 772065

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,3-Trichlorobenzene DCB Ave 2481 4548 11846 46710

105208 181470 263513 365908

1.00 2.00 5.00 20.0

50.0 100 150 200

Dibromofluoromethane PFB Ave 53419

131105 255639 404291 524736

20.0

50.0 100 150 200

1,2-Dichloroethane-d4 (Surr) DFB Ave 57434

136159 268884 431384 568730

20.0

50.0 100 150 200

FORM VI 8260B Page 163 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS18

Analy Batch No.: 170445

Calibration Start Date: 11/20/2012 15:57 Calibration End Date: 10631

N

11/20/2012 19:11

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Toluene-d8 (Surr) DFB Ave 211373

513882 999001 1622664 2102290

20.0

50.0 100 150 200

4-Bromofluorobenzene (Surr) CBZ Ave 85160

207318 391774 609998 801248

20.0

50.0 100 150 200

Curve Type Legend:

Ave = Average ISTD

Qua1 = Quadratic 1/conc ISTD

FORM VI 8260B Page 164 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD01 500-172615/2 22I1211A.D

Level 2 STD02 500-172615/3 22I1211B.D

Level 3 STD03 500-172615/4 22I1211C.D

Level 4 STD04 500-172615/5 22I1211D.D

Level 5 STD05 500-172615/6 22I1211E.D

Level 6 STD06 500-172615/7 22I1211F.D

Level 7 STD07 500-172615/8 22I1211G.D

Level 8 STD08 500-172615/9 22I1211H.D

Level 9 STD09 500-172615/10 22I1211I.D

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Dichlorodifluoromethane 0.6445 0.5310 0.4776 0.4883 Ave 9.9

0.5798 0.5632 0.5150 0.5364

0.5420 0.0100 15.0

Chloromethane 0.8256 0.7243 0.6267 0.6890 Ave 7.9

0.7182 0.7230 0.6810 0.7012

0.7111 0.1000 15.0

Vinyl chloride 0.6665 0.7420 0.6103 0.5612 0.6130 Ave 8.0

0.6517 0.6618 0.6041 0.6323

0.6381 0.0100 15.0

Bromomethane 0.1659 0.2203 0.1716 0.1726 Ave 13.0

0.2077 0.2258 0.2110 0.2234

0.1998 0.0100 15.0

Chloroethane 0.4113 0.3289 0.3175 0.3315 Ave 10.0

0.3369 0.3333 0.3044 0.3069

0.3338 0.0100 15.0

Dichlorofluoromethane 1.1276 1.0357 0.9343 1.0079 Ave 6.3

0.9817 1.0066 0.9437 0.9571

0.9993 0.0100 15.0

Acetone +++++ +++++ 0.0554 0.0635 Ave 7.8

0.0614 0.0672 0.0690 0.0671

0.0639 0.0100 15.0

Trichlorofluoromethane 0.9712 0.8348 0.7738 0.8319 Ave 7.9

0.8320 0.8249 0.7635 0.7796

0.8265 0.0100 15.0

Acrolein 0.0331 0.0421 0.0314 0.0388 Ave 13.0

0.0392 0.0429 0.0450 0.0450

0.0397 0.0010 15.0

1,1-Dichloroethene 0.4212 0.4280 0.3669 0.4008 Ave 4.7

0.3938 0.3925 0.3935 0.4040

0.4001 0.0100 15.0

1,1,2-Trichloro-1,2,2-trifluoroethane 0.5610 0.4940 0.4511 0.4785 Ave 6.7

0.4739 0.4784 0.4696 0.4829

0.4862 0.0100 15.0

Methylene Chloride +++++ 0.4011 0.3629 0.4004 Ave 4.0

0.3719 0.3777 0.3682 0.3859

0.3812 0.0100 15.0

Carbon disulfide 1.5962 1.3713 1.3219 1.4559 Ave 6.5

1.5313 1.5882 1.4767 1.4979

1.4799 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 165 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Acetonitrile 0.0371 0.0333 0.0243 0.0295 Ave 13.0

0.0262 0.0281 0.0299 0.0295

0.0297 0.0010 15.0

Acrylonitrile 0.0750 0.0912 0.0677 0.0823 Ave 9.0

0.0764 0.0821 0.0846 0.0849

0.0805 0.0010 15.0

trans-1,2-Dichloroethene 0.4780 0.4617 0.4088 0.4560 Ave 4.4

0.4456 0.4511 0.4430 0.4552

0.4499 0.0100 15.0

2-Butanone (MEK) +++++ +++++ 0.0823 0.0919 Ave 6.1

0.0908 0.0953 0.0973 0.0970

0.0924 0.0100 15.0

Methyl tert-butyl ether 0.7977 0.6853 0.6794 0.7577 Ave 5.4

0.7230 0.7592 0.7369 0.7564

0.7369 0.0100 15.0

Vinyl acetate +++++ 0.6129 0.5650 0.6423 Ave 5.2

0.6107 0.6494 0.6338 0.6642

0.6255 0.0100 15.0

Tetrahydrofuran +++++ +++++ 0.0538 0.0611 Ave 4.2

0.0583 0.0572 0.0571 0.0595

0.0578 0.0100 15.0

1,1-Dichloroethane 0.9850 0.8255 0.8099 0.9189 Ave 6.2

0.8749 0.8925 0.8704 0.9084

0.8857 0.1000 15.0

2,2-Dichloropropane 0.8126 0.7184 0.6702 0.7515 Ave 5.5

0.7243 0.7285 0.7200 0.7474

0.7341 0.0100 15.0

cis-1,2-Dichloroethene 0.5106 0.4202 0.4186 0.4663 Ave 6.4

0.4508 0.4630 0.4488 0.4652

0.4554 0.0100 15.0

Propionitrile 0.0230 0.0200 0.0163 0.0205 Ave 10.0

0.0191 0.0201 0.0217 0.0219

0.0203 0.0010 15.0

Bromochloromethane 0.2191 0.1652 0.1606 0.1825 Ave 10.0

0.1747 0.1747 0.1737 0.1772

0.1785 0.0100 15.0

Chloroform 0.7988 0.7465 0.6742 0.7604 Ave 4.9

0.7195 0.7370 0.7200 0.7434

0.7375 0.0100 15.0

1,1,1-Trichloroethane 0.8087 0.7248 0.6839 0.7390 Ave 4.7

0.7317 0.7368 0.7320 0.7583

0.7394 0.0100 15.0

Carbon tetrachloride 0.4978 0.4990 0.4486 0.4871 Ave 3.4

0.4883 0.4750 0.4767 0.4948

0.4834 0.0100 15.0

1,1-Dichloropropene 0.7318 0.5960 0.5898 0.6649 Ave 6.9

0.6479 0.6478 0.6435 0.6685

0.6488 0.0100 15.0

Benzene 1.2306 1.3508 1.2179 1.1306 1.2550 Ave 4.7

1.2277 1.2183 1.1975 1.2355

1.2293 0.0100 15.0

1,2-Dichloroethane 0.3835 0.3413 0.3151 0.3618 Ave 5.6

0.3558 0.3552 0.3521 0.3644

0.3536 0.0100 15.0

4-Methyl-2-pentanone (MIBK) +++++ +++++ 0.1384 0.1561 Ave 5.1

0.1535 0.1552 0.1604 0.1580

0.1536 0.0100 15.0

2-Hexanone +++++ +++++ 0.1035 0.1187 Ave 7.3

0.1220 0.1257 0.1256 0.1271

0.1204 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 166 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Trichloroethene 0.3583 0.3824 0.3356 0.3315 0.3516 Ave 4.9

0.3434 0.3325 0.3291 0.3406

0.3450 0.0100 15.0

1,2-Dichloropropane 0.3550 0.3030 0.2849 0.3264 Ave 6.4

0.3130 0.3110 0.3089 0.3197

0.3152 0.0100 15.0

Dibromomethane 0.1457 0.1306 0.1153 0.1288 Ave 6.9

0.1238 0.1238 0.1224 0.1261

0.1271 0.0100 15.0

Bromodichloromethane 0.3875 0.3507 0.3319 0.3726 Ave 4.6

0.3533 0.3599 0.3552 0.3686

0.3600 0.0100 15.0

2-Chloroethyl vinyl ether 0.1052 0.1095 0.1020 0.1096 Ave 3.2

0.1015 0.1078 0.1021 0.1054

0.1054 0.0100 15.0

cis-1,3-Dichloropropene 0.4257 0.4102 0.3731 0.4222 Ave 4.1

0.4033 0.4109 0.4067 0.4210

0.4091 0.0100 15.0

Toluene 0.9341 0.8388 0.7909 0.7458 0.8161 Ave 6.2

0.8023 0.8060 0.7995 0.8258

0.8177 0.0100 15.0

trans-1,3-Dichloropropene 0.3943 0.3221 0.2903 0.3412 Ave 8.6

0.3304 0.3383 0.3448 0.3521

0.3392 0.0100 15.0

1,1,2-Trichloroethane 0.2014 0.1786 0.1581 0.1681 Ave 7.7

0.1638 0.1667 0.1692 0.1728

0.1723 0.0100 15.0

Tetrachloroethene 0.5511 0.4482 0.4255 0.4568 Ave 9.0

0.4446 0.4384 0.4251 0.4400

0.4537 0.0100 15.0

1,3-Dichloropropane 0.3703 0.3719 0.3207 0.3542 Ave 4.9

0.3407 0.3413 0.3399 0.3540

0.3491 0.0100 15.0

Dibromochloromethane 0.2702 0.2371 0.2274 0.2693 Ave 6.9

0.2630 0.2690 0.2675 0.2786

0.2603 0.0100 15.0

1,2-Dibromoethane 0.2035 0.1624 0.1445 0.1607 Ave 10.0

0.1572 0.1634 0.1626 0.1665

0.1651 0.0100 15.0

Chlorobenzene 1.1305 1.0221 0.9605 1.0363 Ave 5.3

0.9949 0.9884 0.9670 0.9960

1.0120 0.3000 15.0

1-Chlorohexane 0.7176 0.7070 0.6491 0.6984 Ave 3.1

0.6765 0.6760 0.6835 0.6837

0.6865 0.0100 15.0

1,1,1,2-Tetrachloroethane 0.3425 0.3396 0.3001 0.3448 Ave 5.0

0.3425 0.3461 0.3458 0.3585

0.3400 0.0100 15.0

Ethylbenzene 0.5881 0.6023 0.5743 0.5326 0.5796 Ave 3.4

0.5801 0.5769 0.5619 0.5822

0.5753 0.0100 15.0

m&p-Xylene 1.4425 1.5227 1.3904 1.3052 1.4876 Ave 4.5

1.4534 1.4554 1.3960 1.3942

1.4275 0.0100 15.0

o-Xylene 1.4661 1.5830 1.3934 1.2932 1.4780 Ave 5.5

1.4493 1.4706 1.4590 1.5151

1.4564 0.0100 15.0

Styrene 1.1505 1.0719 0.9871 1.1405 Ave 5.6

1.1318 1.1478 1.1460 1.1845

1.1200 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 167 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Bromoform 0.1602 0.1366 0.1243 0.1553 Ave 10.0

0.1546 0.1600 0.1660 0.1720

0.1536 0.1000 15.0

Isopropylbenzene 3.8233 3.3535 3.0653 3.4816 Ave 7.4

3.1927 3.1639 3.1360 3.2790

3.3119 0.0100 15.0

Bromobenzene 0.8632 0.7552 0.6812 0.7730 Ave 8.2

0.6922 0.7028 0.6972 0.7345

0.7374 0.0100 15.0

1,1,2,2-Tetrachloroethane 0.3977 0.4200 0.3757 0.4089 Ave 6.0

0.3542 0.3640 0.3676 0.3874

0.3844 0.3000 15.0

1,2,3-Trichloropropane 0.2771 0.3098 0.2652 0.3046 Ave 6.1

0.2704 0.2691 0.2728 0.2923

0.2827 0.0100 15.0

N-Propylbenzene 4.4856 4.0360 3.6439 4.1493 Ave 6.5

3.8858 3.8875 3.7881 3.8936

3.9712 0.0100 15.0

4-Chlorotoluene 2.5653 2.2332 2.0176 2.3065 Ave 7.0

2.1662 2.2029 2.1653 2.2760

2.2416 0.0100 15.0

1,3,5-Trimethylbenzene 3.0323 2.6976 2.4978 2.9026 Ave 5.8

2.6929 2.7638 2.7107 2.8237

2.7652 0.0100 15.0

2-Chlorotoluene 3.0140 2.6145 2.4222 2.7174 Ave 6.4

2.5627 2.6413 2.6089 2.7193

2.6625 0.0100 15.0

tert-Butylbenzene 2.9534 2.5783 2.3626 2.6552 Ave 7.3

2.4553 2.4418 2.4420 2.5773

2.5582 0.0100 15.0

1,2,4-Trimethylbenzene 2.9651 2.7353 2.3710 2.7710 Ave 6.3

2.6381 2.7234 2.6840 2.8189

2.7134 0.0100 15.0

sec-Butylbenzene 4.2594 3.7758 3.5493 3.9075 Ave 5.8

3.6796 3.6591 3.6577 3.7738

3.7828 0.0100 15.0

1,3-Dichlorobenzene 1.8548 1.6516 1.4214 1.5907 Ave 8.4

1.4814 1.5187 1.5128 1.5667

1.5748 0.0100 15.0

p-Isopropyltoluene 3.7168 3.3643 2.9943 3.3705 Ave 6.4

3.1719 3.2121 3.1807 3.2836

3.2868 0.0100 15.0

1,4-Dichlorobenzene 1.7715 1.6564 1.4603 1.5651 Ave 6.9

1.4798 1.5043 1.4758 1.5340

1.5559 0.0100 15.0

1,2-Dichlorobenzene 1.4806 1.3414 1.2093 1.4033 Ave 6.4

1.2786 1.2876 1.2674 1.3183

1.3233 0.0100 15.0

n-Butylbenzene 3.1126 2.8700 2.6461 2.9480 Ave 4.7

2.8772 2.9149 2.9548 3.0267

2.9188 0.0100 15.0

1,2-Dibromo-3-Chloropropane 0.0631 0.0851 0.0599 0.0678 Ave 12.0

0.0613 0.0622 0.0635 0.0659

0.0661 0.0100 15.0

1,2,4-Trichlorobenzene 0.9867 0.8758 0.8191 0.8999 Ave 5.3

0.8675 0.9149 0.9059 0.9063

0.8970 0.0100 15.0

Hexachlorobutadiene 0.9143 0.7960 0.7318 0.7351 Ave 9.3

0.7318 0.6946 0.7407 0.7100

0.7568 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 168 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Naphthalene 1.0319 0.9651 0.8910 1.0003 Ave 5.7

0.9350 0.9776 1.0179 1.0659

0.9856 0.0100 15.0

1,2,3-Trichlorobenzene 0.7942 0.6905 0.6629 0.7392 Ave 5.4

0.6972 0.7092 0.7197 0.7238

0.7171 0.0100 15.0

Dibromofluoromethane 0.4088 Ave 3.6

0.3747 0.4105 0.3974 0.4034

0.3990 0.0100 15.0

1,2-Dichloroethane-d4 (Surr) 0.2898 Ave 2.8

0.2681 0.2786 0.2783 0.2818

0.2793 0.0100 15.0

Toluene-d8 (Surr) 1.2317 Ave 3.0

1.1353 1.2008 1.1689 1.1817

1.1837 0.0100 15.0

4-Bromofluorobenzene (Surr) 0.5022 Ave 2.5

0.4792 0.5117 0.5010 0.5085

0.5005 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 169 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD01 500-172615/2 22I1211A.D

Level 2 STD02 500-172615/3 22I1211B.D

Level 3 STD03 500-172615/4 22I1211C.D

Level 4 STD04 500-172615/5 22I1211D.D

Level 5 STD05 500-172615/6 22I1211E.D

Level 6 STD06 500-172615/7 22I1211F.D

Level 7 STD07 500-172615/8 22I1211G.D

Level 8 STD08 500-172615/9 22I1211H.D

Level 9 STD09 500-172615/10 22I1211I.D

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Dichlorodifluoromethane PFB Ave 8283 14019 34084 128973

408706 762307 1110898 1572519

1.00 2.00 5.00 20.0

50.0 100 150 200

Chloromethane PFB Ave 10611 19121 44725 181982

506217 978702 1468998 2055922

1.00 2.00 5.00 20.0

50.0 100 150 200

Vinyl chloride PFB Ave 2072 9537 16111 40052 161885

459341 895799 1302949 1853836

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

Bromomethane PFB Ave 2132 5817 12250 45578

146376 305638 455210 654905

1.00 2.00 5.00 20.0

50.0 100 150 200

Chloroethane PFB Ave 5286 8684 22657 87550

237436 451232 656528 899737

1.00 2.00 5.00 20.0

50.0 100 150 200

Dichlorofluoromethane PFB Ave 14493 27342 66676 266205

691989 1362610 2035639 2806119

1.00 2.00 5.00 20.0

50.0 100 150 200

Acetone PFB Ave +++++ +++++ 3957 16764

43292 90934 148822 196769

+++++ +++++ 5.00 20.0

50.0 100 150 200

Trichlorofluoromethane PFB Ave 12483 22039 55227 219705

586466 1116585 1646914 2285626

1.00 2.00 5.00 20.0

50.0 100 150 200

Acrolein PFB Ave 16997 44508 89671 410157

1104663 2325112 3885554 5276134

40.0 80.0 200 800

2000 4000 6000 8000

1,1-Dichloroethene PFB Ave 5414 11300 26186 105858

277562 531364 848798 1184587

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,2-Trichloro-1,2,2-trifluoroetha

ne

PFB Ave 7210 13042 32193 126370

334028 647515 1013020 1415755

1.00 2.00 5.00 20.0

50.0 100 150 200

Methylene Chloride PFB Ave +++++ 10588 25901 105736

262156 511318 794285 1131397

+++++ 2.00 5.00 20.0

50.0 100 150 200

Carbon disulfide PFB Ave 20516 36202 94343 384523

1079379 2149891 3185269 4391617

1.00 2.00 5.00 20.0

50.0 100 150 200

Acetonitrile PFB Ave 3815 7023 13902 62328

147511 304606 515971 692080

8.00 16.0 40.0 160

400 800 1200 1600

FORM VI 8260B Page 170 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Acrylonitrile PFB Ave 7715 19252 38635 173831

430688 889127 1460725 1990459

8.00 16.0 40.0 160

400 800 1200 1600

trans-1,2-Dichloroethene PFB Ave 6143 12190 29175 120435

314119 610637 955652 1334459

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Butanone (MEK) PFB Ave +++++ +++++ 5877 24272

64002 128968 209900 284336

+++++ +++++ 5.00 20.0

50.0 100 150 200

Methyl tert-butyl ether PFB Ave 10253 18092 48485 200118

509651 1027632 1589481 2217547

1.00 2.00 5.00 20.0

50.0 100 150 200

Vinyl acetate PFB Ave +++++ 16181 40320 169641

430488 879019 1367143 1947324

+++++ 2.00 5.00 20.0

50.0 100 150 200

Tetrahydrofuran PFB Ave +++++ +++++ 3843 16127

41123 77379 123251 174315

+++++ +++++ 5.00 20.0

50.0 100 150 200

1,1-Dichloroethane PFB Ave 12660 21793 57801 242674

616675 1208102 1877461 2663163

1.00 2.00 5.00 20.0

50.0 100 150 200

2,2-Dichloropropane PFB Ave 10444 18966 47829 198464

510518 986077 1552961 2191135

1.00 2.00 5.00 20.0

50.0 100 150 200

cis-1,2-Dichloroethene PFB Ave 6562 11093 29875 123154

317732 626799 968176 1363967

1.00 2.00 5.00 20.0

50.0 100 150 200

Propionitrile DFB Ave 3274 5826 13049 61580

150541 311165 533857 726579

8.00 16.0 40.0 160

400 800 1200 1600

Bromochloromethane PFB Ave 2816 4362 11462 48207

123109 236461 374570 519660

1.00 2.00 5.00 20.0

50.0 100 150 200

Chloroform PFB Ave 10267 19708 48119 200834

507134 997634 1553050 2179601

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,1-Trichloroethane PFB Ave 10394 19135 48811 195166

515733 997347 1578989 2223267

1.00 2.00 5.00 20.0

50.0 100 150 200

Carbon tetrachloride DFB Ave 8845 18161 44839 182447

481514 918644 1463204 2051034

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1-Dichloropropene PFB Ave 9406 15734 42090 175593

456667 876844 1388026 1960009

1.00 2.00 5.00 20.0

50.0 100 150 200

Benzene DFB Ave 5292 24000 44324 113004 470128

1210657 2356179 3675431 5120985

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichloroethane DFB Ave 6813 12420 31493 135519

350802 686980 1080708 1510261

1.00 2.00 5.00 20.0

50.0 100 150 200

4-Methyl-2-pentanone (MIBK) DFB Ave +++++ +++++ 13833 58466

151375 300182 492445 654734

+++++ +++++ 5.00 20.0

50.0 100 150 200

2-Hexanone CBZ Ave +++++ +++++ 8872 37503

101953 206593 337483 453433

+++++ +++++ 5.00 20.0

50.0 100 150 200

Trichloroethene DFB Ave 1541 6794 12213 33134 131705

338598 643029 1009984 1411923

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichloropropane DFB Ave 6308 11028 28481 122258

308626 601403 948132 1325238

1.00 2.00 5.00 20.0

50.0 100 150 200

FORM VI 8260B Page 171 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Dibromomethane DFB Ave 2589 4753 11529 48251

122106 239384 375807 522887

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromodichloromethane DFB Ave 6884 12765 33178 139566

348406 696059 1090230 1527793

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Chloroethyl vinyl ether DFB Ave 1869 3984 10192 41067

100134 208398 313500 436785

1.00 2.00 5.00 20.0

50.0 100 150 200

cis-1,3-Dichloropropene DFB Ave 7564 14930 37294 158135

397656 794708 1248175 1745247

1.00 2.00 5.00 20.0

50.0 100 150 200

Toluene DFB Ave 4017 14904 28786 74548 305710

791155 1558816 2453857 3422834

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

trans-1,3-Dichloropropene DFB Ave 7005 11724 29021 127802

325796 654311 1058276 1459268

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,2-Trichloroethane DFB Ave 3579 6500 15804 62968

161526 322360 519398 716065

1.00 2.00 5.00 20.0

50.0 100 150 200

Tetrachloroethene CBZ Ave 8289 14024 36478 144290

371408 720453 1142505 1570157

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3-Dichloropropane CBZ Ave 5569 11637 27497 111881

284612 560890 913572 1263367

1.00 2.00 5.00 20.0

50.0 100 150 200

Dibromochloromethane CBZ Ave 4064 7418 19500 85045

219735 442108 718959 994298

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dibromoethane DFB Ave 3616 5912 14445 60214

154974 316106 499079 690159

1.00 2.00 5.00 20.0

50.0 100 150 200

Chlorobenzene CBZ Ave 17003 31983 82345 327328

831189 1624419 2599260 3554021

1.00 2.00 5.00 20.0

50.0 100 150 200

1-Chlorohexane PFB Ave 9223 18665 46324 184447

476816 915102 1474279 2004578

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,1,2-Tetrachloroethane CBZ Ave 5151 10625 25733 108914

286131 568808 929412 1279270

1.00 2.00 5.00 20.0

50.0 100 150 200

Ethylbenzene CBZ Ave 2120 9059 17971 45661 183060

484613 948132 1510230 2077566

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

m&p-Xylene CBZ Ave 10400 45804 87017 223793 939704

2428374 4783893 7504852 9950024

0.500 2.00 4.00 10.0 40.0

100 200 300 400

o-Xylene CBZ Ave 5285 23810 43602 110873 466833

1210753 2416819 3921614 5406441

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

Styrene CBZ Ave 17304 33541 84628 360216

945512 1886331 3080454 4226631

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromoform CBZ Ave 2410 4275 10660 49043

129169 263003 446109 613724

1.00 2.00 5.00 20.0

50.0 100 150 200

Isopropylbenzene DCB Ave 31324 57244 148746 610310

1601454 3109566 5106365 6881199

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromobenzene DCB Ave 7072 12892 33053 135512

347188 690763 1135272 1541345

1.00 2.00 5.00 20.0

50.0 100 150 200

FORM VI 8260B Page 172 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

1,1,2,2-Tetrachloroethane DCB Ave 3258 7169 18231 71670

177658 357760 598529 812983

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,3-Trichloropropane DCB Ave 2270 5288 12868 53399

135614 264488 444171 613409

1.00 2.00 5.00 20.0

50.0 100 150 200

N-Propylbenzene DCB Ave 36750 68894 176823 727359

1949080 3820722 6168362 8171167

1.00 2.00 5.00 20.0

50.0 100 150 200

4-Chlorotoluene DCB Ave 21017 38120 97903 404326

1086544 2165096 3525867 4776401

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3,5-Trimethylbenzene DCB Ave 24843 46048 121204 508814

1350744 2716376 4413867 5925708

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Chlorotoluene DCB Ave 24693 44629 117536 476349

1285442 2595965 4248167 5706737

1.00 2.00 5.00 20.0

50.0 100 150 200

tert-Butylbenzene DCB Ave 24197 44012 114646 465442

1231564 2399839 3976419 5408653

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,4-Trimethylbenzene DCB Ave 24293 46692 115053 485753

1323232 2676625 4370483 5915680

1.00 2.00 5.00 20.0

50.0 100 150 200

sec-Butylbenzene DCB Ave 34897 64452 172232 684971

1845685 3596271 5955880 7919600

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3-Dichlorobenzene DCB Ave 15196 28192 68974 278836

743079 1492625 2463360 3287950

1.00 2.00 5.00 20.0

50.0 100 150 200

p-Isopropyltoluene DCB Ave 30451 57429 145300 590843

1590983 3156888 5179163 6891004

1.00 2.00 5.00 20.0

50.0 100 150 200

1,4-Dichlorobenzene DCB Ave 14514 28274 70862 274358

742273 1478508 2403110 3219268

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichlorobenzene DCB Ave 12130 22897 58683 245994

641352 1265519 2063725 2766492

1.00 2.00 5.00 20.0

50.0 100 150 200

n-Butylbenzene DCB Ave 25501 48990 128404 516775

1443162 2864857 4811328 6351852

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dibromo-3-Chloropropane DCB Ave 517 1453 2909 11888

30736 61117 103368 138335

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,4-Trichlorobenzene DCB Ave 8084 14950 39749 157753

435120 899145 1475044 1901927

1.00 2.00 5.00 20.0

50.0 100 150 200

Hexachlorobutadiene DCB Ave 7491 13587 35512 128859

367053 682660 1206171 1489923

1.00 2.00 5.00 20.0

50.0 100 150 200

Naphthalene DCB Ave 8454 16474 43237 175344

469003 960821 1657420 2236810

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,3-Trichlorobenzene DCB Ave 6507 11786 32167 129572

349729 697002 1171916 1518870

1.00 2.00 5.00 20.0

50.0 100 150 200

Dibromofluoromethane PFB Ave 107966

264099 555702 857139 1182785

20.0

50.0 100 150 200

1,2-Dichloroethane-d4 (Surr) DFB Ave 108560

264333 538799 854290 1167924

20.0

50.0 100 150 200

FORM VI 8260B Page 173 of 384 01/09/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53491-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Toluene-d8 (Surr) DFB Ave 461399

1119518 2322467 3587473 4898132

20.0

50.0 100 150 200

4-Bromofluorobenzene (Surr) CBZ Ave 158632

400320 840950 1346757 1814509

20.0

50.0 100 150 200

Curve Type Legend:

Ave = Average ISTD

FORM VI 8260B Page 174 of 384 01/09/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53491-1

CMS06

12/04/2012 19:58

12/04/2012 14:34

12/04/2012 16:55

ICV 500-171819/15

DB624

TestAmerica Chicago

Lab File ID: 6S1204.d Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.9557 0.7088 0.0100 37.1 50.0 -25.8* 25.0

Chloromethane Ave 1.170 0.9521 0.1000 40.7 50.0 -18.6 25.0

Vinyl chloride Ave 0.9786 0.9329 0.0100 47.7 50.0 -4.7 25.0

Bromomethane Ave 0.5629 0.4976 0.0100 44.2 50.0 -11.6 25.0

Chloroethane Ave 0.7117 0.6528 0.0100 45.9 50.0 -8.3 25.0

Dichlorofluoromethane Ave 1.466 1.305 0.0100 44.5 50.0 -11.0 25.0

Trichlorofluoromethane Ave 1.279 1.164 0.0100 45.5 50.0 -9.0 25.0

Acrolein Ave 0.0748 0.0708 0.0010 1893 2000 -5.4 25.0

1,1-Dichloroethene Ave 0.5393 0.5815 0.0100 53.9 50.0 7.8 25.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.7370 0.5548 0.0100 37.6 50.0 -24.7 25.0

Acetone Qua2 0.1428 0.0100 56.0 50.0 12.0 25.0

Carbon disulfide Ave 2.044 2.173 0.0100 53.2 50.0 6.3 25.0

Acetonitrile Qua2 0.0432 0.0010 421 400 5.1 25.0

Methylene Chloride Ave 0.5335 0.5791 0.0100 54.3 50.0 8.6 25.0

Acrylonitrile Ave 0.1425 0.1350 0.0010 379 400 -5.3 25.0

trans-1,2-Dichloroethene Ave 0.5736 0.6549 0.0100 57.1 50.0 14.2 25.0

Methyl tert-butyl ether Ave 1.148 0.9692 0.0100 42.2 50.0 -15.5 25.0

1,1-Dichloroethane Ave 1.196 1.323 0.1000 55.3 50.0 10.6 25.0

Vinyl acetate Ave 0.8834 0.9732 0.0100 55.1 50.0 10.2 25.0

2,2-Dichloropropane Ave 0.7383 0.8359 0.0100 56.6 50.0 13.2 25.0

cis-1,2-Dichloroethene Ave 0.5831 0.6322 0.0100 54.2 50.0 8.4 25.0

2-Butanone (MEK) Ave 0.1743 0.1832 0.0100 52.6 50.0 5.1 25.0

Propionitrile Ave 0.0329 0.0339 0.0010 412 400 2.9 25.0

Bromochloromethane Ave 0.2329 0.1932 0.0100 41.5 50.0 -17.1 25.0

Tetrahydrofuran Ave 0.1027 0.1200 0.0100 58.4 50.0 16.9 25.0

Chloroform Ave 0.9290 1.049 0.0100 56.5 50.0 12.9 25.0

1,1,1-Trichloroethane Ave 0.8595 0.9754 0.0100 56.7 50.0 13.5 25.0

Carbon tetrachloride Ave 0.5342 0.5942 0.0100 55.6 50.0 11.2 25.0

1,1-Dichloropropene Ave 0.7579 0.8236 0.0100 54.3 50.0 8.7 25.0

Benzene Ave 1.465 1.593 0.0100 54.4 50.0 8.7 25.0

1,2-Dichloroethane Ave 0.4733 0.5360 0.0100 56.6 50.0 13.2 25.0

Trichloroethene Ave 0.3790 0.4207 0.0100 55.5 50.0 11.0 25.0

1,2-Dichloropropane Ave 0.3888 0.4324 0.0100 55.6 50.0 11.2 25.0

Dibromomethane Ave 0.1745 0.1893 0.0100 54.2 50.0 8.4 25.0

Bromodichloromethane Ave 0.4200 0.4564 0.0100 54.3 50.0 8.7 25.0

2-Chloroethyl vinyl ether Ave 0.0935 0.1063 0.0100 56.8 50.0 13.7 25.0

cis-1,3-Dichloropropene Ave 0.4400 0.4949 0.0100 60.5 53.8 12.5 25.0

4-Methyl-2-pentanone (MIBK) Ave 0.2770 0.2843 0.0100 51.3 50.0 2.6 25.0

Toluene Ave 0.9056 0.9867 0.0100 54.5 50.0 9.0 25.0

trans-1,3-Dichloropropene Ave 0.3718 0.4191 0.0100 54.8 48.6 12.7 25.0

FORM VII 8260B

Page 175 of 384 01/09/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53491-1

CMS06

12/04/2012 19:58

12/04/2012 14:34

12/04/2012 16:55

ICV 500-171819/15

DB624

TestAmerica Chicago

Lab File ID: 6S1204.d Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

1,1,2-Trichloroethane Ave 0.3016 0.3294 0.0100 54.6 50.0 9.2 25.0

Tetrachloroethene Ave 0.4445 0.5067 0.0100 57.0 50.0 14.0 25.0

1,3-Dichloropropane Ave 0.3887 0.4493 0.0100 57.8 50.0 15.6 25.0

2-Hexanone Ave 0.1909 0.1976 0.0100 51.8 50.0 3.5 25.0

Dibromochloromethane Ave 0.2649 0.2994 0.0100 56.5 50.0 13.0 25.0

1,2-Dibromoethane Ave 0.2221 0.2452 0.0100 55.2 50.0 10.4 25.0

1-Chlorohexane Ave 0.8026 0.6673 0.0100 41.6 50.0 -16.9 25.0

Chlorobenzene Ave 1.043 1.075 0.3000 51.5 50.0 3.1 25.0

1,1,1,2-Tetrachloroethane Ave 0.3491 0.3958 0.0100 56.7 50.0 13.4 25.0

Ethylbenzene Ave 0.6090 0.6804 0.0100 55.9 50.0 11.7 25.0

m&p-Xylene Ave 1.633 1.717 0.0100 105 100 5.1 25.0

o-Xylene Ave 1.656 1.707 0.0100 51.5 50.0 3.1 25.0

Styrene Ave 1.294 1.386 0.0100 53.5 50.0 7.1 25.0

Bromoform Qua1 0.2127 0.1000 57.0 50.0 14.0 25.0

Isopropylbenzene Ave 3.668 3.656 0.0100 49.8 50.0 -0.3 25.0

Bromobenzene Ave 0.8299 0.9264 0.0100 55.8 50.0 11.6 25.0

1,1,2,2-Tetrachloroethane Ave 0.4968 0.5641 0.3000 56.8 50.0 13.5 25.0

1,2,3-Trichloropropane Ave 0.1382 0.1571 0.0100 56.8 50.0 13.6 25.0

N-Propylbenzene Ave 4.526 4.386 0.0100 48.5 50.0 -3.1 25.0

2-Chlorotoluene Ave 2.445 2.505 0.0100 51.2 50.0 2.5 25.0

1,3,5-Trimethylbenzene Ave 3.193 3.418 0.0100 53.5 50.0 7.1 25.0

4-Chlorotoluene Ave 2.997 2.955 0.0100 49.3 50.0 -1.4 25.0

tert-Butylbenzene Ave 2.736 2.718 0.0100 49.7 50.0 -0.7 25.0

1,2,4-Trimethylbenzene Ave 3.175 3.411 0.0100 53.7 50.0 7.5 25.0

sec-Butylbenzene Ave 4.353 4.275 0.0100 49.1 50.0 -1.8 25.0

1,3-Dichlorobenzene Ave 1.758 1.741 0.0100 49.5 50.0 -1.0 25.0

p-Isopropyltoluene Ave 3.707 3.622 0.0100 48.9 50.0 -2.3 25.0

1,4-Dichlorobenzene Ave 1.768 1.922 0.0100 54.4 50.0 8.7 25.0

n-Butylbenzene Ave 3.588 3.662 0.0100 51.0 50.0 2.1 25.0

1,2-Dichlorobenzene Ave 1.541 1.561 0.0100 50.7 50.0 1.3 25.0

1,2-Dibromo-3-Chloropropane Ave 0.0624 0.0666 0.0100 53.4 50.0 6.7 25.0

1,2,4-Trichlorobenzene Ave 0.7171 0.6739 0.0100 47.0 50.0 -6.0 25.0

Hexachlorobutadiene Qua2 0.5712 0.0100 51.7 50.0 3.4 25.0

Naphthalene Ave 0.9523 0.9576 0.0100 50.3 50.0 0.6 25.0

1,2,3-Trichlorobenzene Qua1 0.4184 0.0100 50.8 50.0 1.7 25.0

Dibromofluoromethane Ave 0.5081 0.4517 0.0100 42.8 48.1 -11.1 25.0

1,2-Dichloroethane-d4 (Surr) Ave 0.3973 0.3281 0.0100 39.7 48.1 -17.4 25.0

Toluene-d8 (Surr) Ave 1.352 1.217 0.0100 43.3 48.1 -9.9 25.0

4-Bromofluorobenzene (Surr) Ave 0.5876 0.5156 0.0100 42.2 48.1 -12.2 25.0

FORM VII 8260B

Page 176 of 384 01/09/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53491-1

CMS06

12/04/2012 19:58

12/04/2012 17:18

12/04/2012 19:13

ICV 500-171819/15

DB624

TestAmerica Chicago

Lab File ID: 6S1204.d Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Ethyl ether Ave 0.4323 0.3545 0.0100 41.0 50.0 -18.0 25.0

Iodomethane Ave 0.9030 1.082 0.0100 59.9 50.0 19.9 25.0

Methyl acetate Ave 0.3789 0.2226 0.0100 29.4 50.0 -41.3* 25.0

Hexane Ave 1.072 0.8633 0.0100 40.3 50.0 -19.5 25.0

Cyclohexane Ave 1.573 1.158 0.0100 36.8 50.0 -26.4* 25.0

Heptane Ave 0.8530 0.6678 0.0100 39.1 50.0 -21.7 25.0

Methylcyclohexane Ave 0.7542 0.5785 0.0100 38.4 50.0 -23.3 25.0

1,3,5-Trichlorobenzene Ave 1.155 1.177 0.0100 51.0 50.0 1.9 25.0

FORM VII 8260B

Page 177 of 384 01/09/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53491-1

CMS06

12/27/2012 09:47

12/04/2012 14:34

12/04/2012 16:55

CCV 500-173973/3

DB624

TestAmerica Chicago

Lab File ID: 6C1227.d Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.9557 0.9217 0.0100 48.2 50.0 -3.6 50.0

Chloromethane Ave 1.170 1.105 0.1000 47.2 50.0 -5.5 50.0

Vinyl chloride Ave 0.9786 0.9107 0.0100 46.5 50.0 -6.9 20.0

Bromomethane Ave 0.5629 0.5445 0.0100 48.4 50.0 -3.3 50.0

Chloroethane Ave 0.7117 0.6484 0.0100 45.6 50.0 -8.9 50.0

Dichlorofluoromethane Ave 1.466 1.377 0.0100 47.0 50.0 -6.1 50.0

Trichlorofluoromethane Ave 1.279 1.234 0.0100 48.2 50.0 -3.5 50.0

Acrolein Ave 0.0748 0.0852 0.0010 2277 2000 13.9 50.0

1,1-Dichloroethene Ave 0.5393 0.5025 0.0100 46.6 50.0 -6.8 20.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.7370 0.6729 0.0100 45.7 50.0 -8.7 50.0

Acetone Qua2 0.1327 0.0100 52.1 50.0 4.1 50.0

Carbon disulfide Ave 2.044 1.993 0.0100 48.8 50.0 -2.5 50.0

Acetonitrile Qua2 0.0473 0.0010 462 400 15.4 50.0

Methylene Chloride Ave 0.5335 0.4644 0.0100 43.5 50.0 -12.9 50.0

Acrylonitrile Ave 0.1425 0.1483 0.0010 416 400 4.0 50.0

trans-1,2-Dichloroethene Ave 0.5736 0.5319 0.0100 46.4 50.0 -7.3 50.0

Methyl tert-butyl ether Ave 1.148 1.048 0.0100 45.7 50.0 -8.7 50.0

1,1-Dichloroethane Ave 1.196 1.113 0.1000 46.5 50.0 -7.0 50.0

Vinyl acetate Ave 0.8834 0.6583 0.0100 37.3 50.0 -25.5 50.0

2,2-Dichloropropane Ave 0.7383 0.7724 0.0100 52.3 50.0 4.6 50.0

cis-1,2-Dichloroethene Ave 0.5831 0.5366 0.0100 46.0 50.0 -8.0 50.0

2-Butanone (MEK) Ave 0.1743 0.1575 0.0100 45.2 50.0 -9.6 50.0

Propionitrile Ave 0.0329 0.0348 0.0010 423 400 5.7 50.0

Bromochloromethane Ave 0.2329 0.2109 0.0100 45.3 50.0 -9.4 50.0

Tetrahydrofuran Ave 0.1027 0.0894 0.0100 43.5 50.0 -12.9 50.0

Chloroform Ave 0.9290 0.8524 0.0100 45.9 50.0 -8.2 20.0

1,1,1-Trichloroethane Ave 0.8595 0.8614 0.0100 50.1 50.0 0.2 50.0

Carbon tetrachloride Ave 0.5342 0.5491 0.0100 51.4 50.0 2.8 50.0

1,1-Dichloropropene Ave 0.7579 0.6809 0.0100 44.9 50.0 -10.2 50.0

Benzene Ave 1.465 1.312 0.0100 44.8 50.0 -10.4 50.0

1,2-Dichloroethane Ave 0.4733 0.4379 0.0100 46.3 50.0 -7.5 50.0

Trichloroethene Ave 0.3790 0.3500 0.0100 46.2 50.0 -7.7 50.0

1,2-Dichloropropane Ave 0.3888 0.3546 0.0100 45.6 50.0 -8.8 20.0

Dibromomethane Ave 0.1745 0.1563 0.0100 44.8 50.0 -10.5 50.0

Bromodichloromethane Ave 0.4200 0.3992 0.0100 47.5 50.0 -5.0 50.0

2-Chloroethyl vinyl ether Ave 0.0935 0.0427 0.0100 22.8 50.0 -54.3* 50.0

cis-1,3-Dichloropropene Ave 0.4400 0.4072 0.0100 46.3 50.0 -7.4 50.0

4-Methyl-2-pentanone (MIBK) Ave 0.2770 0.2777 0.0100 50.1 50.0 0.3 50.0

Toluene Ave 0.9056 0.8480 0.0100 46.8 50.0 -6.4 20.0

trans-1,3-Dichloropropene Ave 0.3718 0.3638 0.0100 48.9 50.0 -2.1 50.0

FORM VII 8260B

Page 178 of 384 01/09/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53491-1

CMS06

12/27/2012 09:47

12/04/2012 14:34

12/04/2012 16:55

CCV 500-173973/3

DB624

TestAmerica Chicago

Lab File ID: 6C1227.d Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

1,1,2-Trichloroethane Ave 0.3016 0.2821 0.0100 46.8 50.0 -6.4 50.0

Tetrachloroethene Ave 0.4445 0.4238 0.0100 47.7 50.0 -4.7 50.0

1,3-Dichloropropane Ave 0.3887 0.3550 0.0100 45.7 50.0 -8.7 50.0

2-Hexanone Ave 0.1909 0.1883 0.0100 49.3 50.0 -1.3 50.0

Dibromochloromethane Ave 0.2649 0.2640 0.0100 49.8 50.0 -0.4 50.0

1,2-Dibromoethane Ave 0.2221 0.2196 0.0100 49.5 50.0 -1.1 50.0

1-Chlorohexane Ave 0.8026 0.7800 0.0100 48.6 50.0 -2.8 50.0

Chlorobenzene Ave 1.043 0.9717 0.3000 46.6 50.0 -6.8 50.0

1,1,1,2-Tetrachloroethane Ave 0.3491 0.3463 0.0100 49.6 50.0 -0.8 50.0

Ethylbenzene Ave 0.6090 0.5747 0.0100 47.2 50.0 -5.6 20.0

m&p-Xylene Ave 1.633 1.484 0.0100 90.9 100 -9.1 50.0

o-Xylene Ave 1.656 1.529 0.0100 46.2 50.0 -7.7 50.0

Styrene Ave 1.294 1.171 0.0100 45.2 50.0 -9.6 50.0

Bromoform Qua1 0.1911 0.1000 51.6 50.0 3.2 50.0

Isopropylbenzene Ave 3.668 3.401 0.0100 46.4 50.0 -7.3 50.0

Bromobenzene Ave 0.8299 0.8184 0.0100 49.3 50.0 -1.4 50.0

1,1,2,2-Tetrachloroethane Ave 0.4968 0.4482 0.3000 45.1 50.0 -9.8 50.0

1,2,3-Trichloropropane Ave 0.1382 0.1338 0.0100 48.4 50.0 -3.2 50.0

N-Propylbenzene Ave 4.526 4.159 0.0100 45.9 50.0 -8.1 50.0

2-Chlorotoluene Ave 2.445 2.308 0.0100 47.2 50.0 -5.6 50.0

1,3,5-Trimethylbenzene Ave 3.193 2.938 0.0100 46.0 50.0 -8.0 50.0

4-Chlorotoluene Ave 2.997 2.723 0.0100 45.4 50.0 -9.2 50.0

tert-Butylbenzene Ave 2.736 2.535 0.0100 46.3 50.0 -7.4 50.0

1,2,4-Trimethylbenzene Ave 3.175 2.927 0.0100 46.1 50.0 -7.8 50.0

sec-Butylbenzene Ave 4.353 3.937 0.0100 45.2 50.0 -9.5 50.0

1,3-Dichlorobenzene Ave 1.758 1.679 0.0100 47.8 50.0 -4.5 50.0

p-Isopropyltoluene Ave 3.707 3.406 0.0100 45.9 50.0 -8.1 50.0

1,4-Dichlorobenzene Ave 1.768 1.638 0.0100 46.3 50.0 -7.4 50.0

n-Butylbenzene Ave 3.588 3.174 0.0100 44.2 50.0 -11.5 50.0

1,2-Dichlorobenzene Ave 1.541 1.436 0.0100 46.6 50.0 -6.8 50.0

1,2-Dibromo-3-Chloropropane Ave 0.0624 0.0615 0.0100 49.3 50.0 -1.3 50.0

1,2,4-Trichlorobenzene Ave 0.7171 0.6962 0.0100 48.5 50.0 -2.9 50.0

Hexachlorobutadiene Qua2 0.5845 0.0100 53.0 50.0 6.0 50.0

Naphthalene Ave 0.9523 0.8314 0.0100 43.7 50.0 -12.7 50.0

1,2,3-Trichlorobenzene Qua1 0.4063 0.0100 49.3 50.0 -1.5 50.0

Dibromofluoromethane Ave 0.5081 0.4959 0.0100 47.0 48.1 -2.4 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.3973 0.3731 0.0100 45.2 48.1 -6.1 50.0

Toluene-d8 (Surr) Ave 1.352 1.326 0.0100 47.2 48.1 -1.9 50.0

4-Bromofluorobenzene (Surr) Ave 0.5876 0.5361 0.0100 43.9 48.1 -8.8 50.0

FORM VII 8260B

Page 179 of 384 01/09/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53491-1

CMS06

12/27/2012 10:10

12/04/2012 14:34

12/04/2012 16:55

CCV 500-173973/4

DB624

TestAmerica Chicago

Lab File ID: 6D1227.d Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dibromofluoromethane Ave 0.5081 0.4622 0.0100 43.8 48.1 -9.0 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.3973 0.3622 0.0100 43.9 48.1 -8.8 50.0

Toluene-d8 (Surr) Ave 1.352 1.311 0.0100 46.7 48.1 -3.0 50.0

4-Bromofluorobenzene (Surr) Ave 0.5876 0.5369 0.0100 44.0 48.1 -8.6 50.0

FORM VII 8260B

Page 180 of 384 01/09/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53491-1

CMS06

12/27/2012 10:10

12/04/2012 17:18

12/04/2012 19:13

CCV 500-173973/4

DB624

TestAmerica Chicago

Lab File ID: 6D1227.d Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Butadiene Ave 1.166 1.154 0.0100 49.5 50.0 -1.0 50.0

Ethyl ether Ave 0.4323 0.4291 0.0100 49.6 50.0 -0.7 50.0

Iodomethane Ave 0.9030 0.6401 0.0100 70.9 100 -29.1 50.0

3-Chloropropene Ave 0.2880 0.1957 0.0100 68.0 100 -32.1 50.0

Methyl acetate Ave 0.3789 0.3330 0.0100 44.0 50.0 -12.1 50.0

Hexane Ave 1.072 1.103 0.0100 51.5 50.0 2.9 50.0

Isopropyl ether Ave 2.442 2.542 0.0100 52.0 50.0 4.1 50.0

2-Chloro-1,3-butadiene Ave 1.418 1.462 0.0100 51.6 50.0 3.1 50.0

Ethyl acetate Ave 0.2896 0.2117 0.0100 365 500 -26.9 50.0

Methacrylonitrile Ave 0.2203 0.1749 0.0100 79.4 100 -20.6 50.0

Cyclohexane Ave 1.573 1.660 0.0100 52.8 50.0 5.5 50.0

Isobutyl alcohol Ave 0.0103 0.0084 0.0010 3280 4000 -18.0 50.0

2,2,4-Trimethylpentane Ave 2.501 2.774 0.0100 55.5 50.0 10.9 50.0

Heptane Ave 0.8530 0.8919 0.0100 52.3 50.0 4.6 50.0

n-Butyl alcohol Ave 0.0059 0.0048 0.0010 3261 4000 -18.5 50.0

Methylcyclohexane Ave 0.7542 0.8231 0.0100 54.6 50.0 9.1 50.0

Methyl methacrylate Ave 0.2214 0.1785 0.0100 80.7 100 -19.4 50.0

2-Nitropropane Qua2 0.0699 0.0100 3836 4000 -4.1 50.0

Ethyl methacrylate Ave 0.2789 0.2385 0.0100 85.5 100 -14.5 50.0

Cyclohexanone Ave 0.0993 0.0811 0.0100 3265 4000 -18.4 50.0

trans-1,4-Dichloro-2-butene Qua2 0.0564 0.0100 87.7 100 -12.3 50.0

Pentachloroethane Qua1 0.2430 0.0100 102 100 1.7 50.0

1,3,5-Trichlorobenzene Ave 1.155 1.436 0.0100 62.2 50.0 24.4 50.0

2-Methylnaphthalene Ave 0.1992 0.3459 0.0100 86.8 50.0 73.6* 50.0

FORM VII 8260B

Page 181 of 384 01/09/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53491-1

CMS18

11/20/2012 23:15

11/20/2012 15:57

11/20/2012 19:11

ICV 500-170445/20

DB624

TestAmerica Chicago

Lab File ID: 18S1120.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.7223 0.7475 0.0100 51.8 50.0 3.5 25.0

Chloromethane Ave 1.216 1.196 0.1000 49.2 50.0 -1.6 25.0

Vinyl chloride Ave 1.014 1.105 0.0100 54.4 50.0 8.9 25.0

Bromomethane Ave 0.3260 0.3449 0.0100 52.9 50.0 5.8 25.0

Chloroethane Ave 0.5276 0.5345 0.0100 50.7 50.0 1.3 25.0

Dichlorofluoromethane Ave 1.291 1.203 0.0100 46.6 50.0 -6.8 25.0

Trichlorofluoromethane Ave 0.9563 0.9718 0.0100 50.8 50.0 1.6 25.0

Acrolein Ave 0.0676 0.0677 0.0010 2003 2000 0.1 25.0

1,1-Dichloroethene Ave 0.4867 0.5115 0.0100 52.6 50.0 5.1 25.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.5836 0.5264 0.0100 45.1 50.0 -9.8 25.0

Acetone Ave 0.0915 0.0848 0.0100 46.3 50.0 -7.4 25.0

Carbon disulfide Ave 1.669 1.870 0.0100 56.0 50.0 12.1 25.0

Acetonitrile Ave 0.0412 0.0429 0.0010 416 400 4.0 25.0

Methylene Chloride Ave 0.5067 0.5400 0.0100 53.3 50.0 6.6 25.0

Acrylonitrile Ave 0.1347 0.1360 0.0010 404 400 1.0 25.0

trans-1,2-Dichloroethene Ave 0.5473 0.5838 0.0100 53.3 50.0 6.7 25.0

Methyl tert-butyl ether Ave 0.9064 0.9194 0.0100 50.7 50.0 1.4 25.0

1,1-Dichloroethane Ave 1.321 1.396 0.1000 52.9 50.0 5.7 25.0

Vinyl acetate Ave 0.5886 0.8113 0.0100 68.9 50.0 37.8* 25.0

2,2-Dichloropropane Ave 0.6761 0.6909 0.0100 51.1 50.0 2.2 25.0

cis-1,2-Dichloroethene Ave 0.5610 0.5988 0.0100 53.4 50.0 6.7 25.0

2-Butanone (MEK) Ave 0.1174 0.1251 0.0100 53.3 50.0 6.5 25.0

Propionitrile Ave 0.0308 0.0303 0.0010 394 400 -1.5 25.0

Bromochloromethane Ave 0.2056 0.2121 0.0100 51.6 50.0 3.2 25.0

Tetrahydrofuran Ave 0.0819 0.0827 0.0100 50.5 50.0 1.0 25.0

Chloroform Ave 0.9125 0.9567 0.0100 52.4 50.0 4.8 25.0

1,1,1-Trichloroethane Ave 0.8591 0.9247 0.0100 53.8 50.0 7.6 25.0

1,1-Dichloropropene Ave 0.7416 0.7561 0.0100 51.0 50.0 1.9 25.0

Carbon tetrachloride Ave 0.5223 0.5510 0.0100 52.8 50.0 5.5 25.0

Benzene Ave 1.447 1.424 0.0100 49.2 50.0 -1.6 25.0

1,2-Dichloroethane Ave 0.4605 0.4529 0.0100 49.2 50.0 -1.7 25.0

Trichloroethene Ave 0.3551 0.3538 0.0100 49.8 50.0 -0.4 25.0

1,2-Dichloropropane Ave 0.4197 0.4194 0.0100 50.0 50.0 -0.0 25.0

Dibromomethane Ave 0.1358 0.1373 0.0100 50.5 50.0 1.1 25.0

Bromodichloromethane Ave 0.3668 0.3674 0.0100 50.1 50.0 0.2 25.0

2-Chloroethyl vinyl ether Ave 0.1202 0.1270 0.0100 52.8 50.0 5.7 25.0

cis-1,3-Dichloropropene Ave 0.3958 0.4173 0.0100 56.7 53.8 5.4 25.0

4-Methyl-2-pentanone (MIBK) Ave 0.1885 0.1944 0.0100 51.6 50.0 3.2 25.0

Toluene Ave 0.9066 0.8495 0.0100 46.9 50.0 -6.3 25.0

trans-1,3-Dichloropropene Ave 0.3238 0.3398 0.0100 51.0 48.6 4.9 25.0

FORM VII 8260B

Page 182 of 384 01/09/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53491-1

CMS18

11/20/2012 23:15

11/20/2012 15:57

11/20/2012 19:11

ICV 500-170445/20

DB624

TestAmerica Chicago

Lab File ID: 18S1120.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

1,1,2-Trichloroethane Ave 0.2466 0.2514 0.0100 51.0 50.0 1.9 25.0

Tetrachloroethene Ave 0.4508 0.4528 0.0100 50.2 50.0 0.5 25.0

1,3-Dichloropropane Ave 0.3653 0.3564 0.0100 48.8 50.0 -2.4 25.0

2-Hexanone Ave 0.1337 0.1450 0.0100 54.2 50.0 8.5 25.0

Dibromochloromethane Qua1 0.2415 0.0100 48.3 50.0 -3.4 25.0

1,2-Dibromoethane Ave 0.1685 0.1707 0.0100 50.7 50.0 1.3 25.0

1-Chlorohexane Ave 0.7416 0.6944 0.0100 46.8 50.0 -6.4 25.0

Chlorobenzene Ave 1.091 1.007 0.3000 46.2 50.0 -7.7 25.0

1,1,1,2-Tetrachloroethane Ave 0.3659 0.3703 0.0100 50.6 50.0 1.2 25.0

Ethylbenzene Ave 0.6360 0.6256 0.0100 49.2 50.0 -1.6 25.0

m&p-Xylene Ave 1.652 1.546 0.0100 93.6 100 -6.4 25.0

o-Xylene Ave 1.745 1.582 0.0100 45.3 50.0 -9.3 25.0

Styrene Ave 1.198 1.204 0.0100 50.3 50.0 0.5 25.0

Bromoform Qua1 0.1477 0.1000 49.9 50.0 -0.2 25.0

Isopropylbenzene Ave 4.053 3.730 0.0100 46.0 50.0 -8.0 25.0

1,1,2,2-Tetrachloroethane Ave 0.4016 0.4063 0.3000 50.6 50.0 1.2 25.0

Bromobenzene Ave 0.8022 0.8016 0.0100 50.0 50.0 -0.0 25.0

1,2,3-Trichloropropane Ave 0.3605 0.3381 0.0100 46.9 50.0 -6.2 25.0

N-Propylbenzene Ave 4.900 4.403 0.0100 44.9 50.0 -10.1 25.0

2-Chlorotoluene Ave 2.790 2.594 0.0100 46.5 50.0 -7.0 25.0

1,3,5-Trimethylbenzene Ave 3.453 3.446 0.0100 49.9 50.0 -0.2 25.0

4-Chlorotoluene Ave 3.244 2.929 0.0100 45.2 50.0 -9.7 25.0

tert-Butylbenzene Ave 3.061 2.803 0.0100 45.8 50.0 -8.4 25.0

1,2,4-Trimethylbenzene Ave 3.430 3.370 0.0100 49.1 50.0 -1.7 25.0

sec-Butylbenzene Ave 4.611 4.214 0.0100 45.7 50.0 -8.6 25.0

1,3-Dichlorobenzene Ave 1.742 1.556 0.0100 44.7 50.0 -10.7 25.0

p-Isopropyltoluene Ave 3.850 3.475 0.0100 45.1 50.0 -9.7 25.0

1,4-Dichlorobenzene Ave 1.714 1.630 0.0100 47.6 50.0 -4.9 25.0

n-Butylbenzene Ave 3.627 3.410 0.0100 47.0 50.0 -6.0 25.0

1,2-Dichlorobenzene Ave 1.428 1.319 0.0100 46.2 50.0 -7.6 25.0

1,2-Dibromo-3-Chloropropane Ave 0.0518 0.0508 0.0100 49.1 50.0 -1.9 25.0

1,2,4-Trichlorobenzene Ave 0.7642 0.6603 0.0100 43.2 50.0 -13.6 25.0

Hexachlorobutadiene Qua1 0.5859 0.0100 45.4 50.0 -9.2 25.0

Naphthalene Ave 0.9358 0.8737 0.0100 46.7 50.0 -6.6 25.0

1,2,3-Trichlorobenzene Ave 0.5020 0.4327 0.0100 43.1 50.0 -13.8 25.0

Dibromofluoromethane Ave 0.4406 0.4521 0.0100 51.3 50.0 2.6 25.0

1,2-Dichloroethane-d4 (Surr) Ave 0.3228 0.3163 0.0100 49.0 50.0 -2.0 25.0

Toluene-d8 (Surr) Ave 1.202 1.189 0.0100 49.4 50.0 -1.1 25.0

4-Bromofluorobenzene (Surr) Ave 0.5452 0.5291 0.0100 48.5 50.0 -3.0 25.0

FORM VII 8260B

Page 183 of 384 01/09/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53491-1

CMS18

11/20/2012 23:15

11/20/2012 19:35

11/20/2012 22:26

ICV 500-170445/20

DB624

TestAmerica Chicago

Lab File ID: 18S1120.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Ethyl ether Ave 0.4336 0.3863 0.0100 44.5 50.0 -10.9 25.0

Iodomethane Ave 0.8980 0.9905 0.0100 55.2 50.0 10.3 25.0

Methyl acetate Ave 0.3161 0.2086 0.0100 33.0 50.0 -34.0* 25.0

Hexane Ave 1.276 1.102 0.0100 43.2 50.0 -13.6 25.0

Cyclohexane Lin1 1.765 0.0100 48.0 50.0 -4.0 25.0

Heptane Ave 0.8721 0.7770 0.0100 44.6 50.0 -10.9 25.0

Methylcyclohexane Ave 0.7981 0.7392 0.0100 46.3 50.0 -7.4 25.0

1,3,5-Trichlorobenzene Ave 1.196 1.090 0.0100 45.5 50.0 -8.9 25.0

FORM VII 8260B

Page 184 of 384 01/09/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53491-1

CMS18

12/28/2012 09:14

11/20/2012 15:57

11/20/2012 19:11

CCV 500-174064/2

DB624

TestAmerica Chicago

Lab File ID: 18C1228.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.7223 0.8870 0.0100 61.4 50.0 22.8 50.0

Chloromethane Ave 1.216 1.208 0.1000 49.7 50.0 -0.7 50.0

Vinyl chloride Ave 1.014 0.9707 0.0100 47.8 50.0 -4.3 20.0

Bromomethane Ave 0.3260 0.3518 0.0100 54.0 50.0 7.9 50.0

Chloroethane Ave 0.5276 0.5065 0.0100 48.0 50.0 -4.0 50.0

Dichlorofluoromethane Ave 1.291 1.356 0.0100 52.5 50.0 5.1 50.0

Trichlorofluoromethane Ave 0.9563 1.076 0.0100 56.3 50.0 12.6 50.0

Acrolein Ave 0.0676 0.0307 0.0010 909 2000 -54.5* 50.0

1,1-Dichloroethene Ave 0.4867 0.5191 0.0100 53.3 50.0 6.7 20.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.5836 0.6296 0.0100 53.9 50.0 7.9 50.0

Acetone Ave 0.0915 0.0882 0.0100 48.2 50.0 -3.6 50.0

Carbon disulfide Ave 1.669 1.980 0.0100 59.3 50.0 18.7 50.0

Acetonitrile Ave 0.0412 0.0401 0.0010 390 400 -2.6 50.0

Methylene Chloride Ave 0.5067 0.4925 0.0100 48.6 50.0 -2.8 50.0

Acrylonitrile Ave 0.1347 0.1159 0.0010 344 400 -14.0 50.0

trans-1,2-Dichloroethene Ave 0.5473 0.5547 0.0100 50.7 50.0 1.4 50.0

Methyl tert-butyl ether Ave 0.9064 0.8376 0.0100 46.2 50.0 -7.6 50.0

1,1-Dichloroethane Ave 1.321 1.285 0.1000 48.7 50.0 -2.7 50.0

Vinyl acetate Ave 0.5886 0.6842 0.0100 58.1 50.0 16.2 50.0

2,2-Dichloropropane Ave 0.6761 0.7431 0.0100 55.0 50.0 9.9 50.0

cis-1,2-Dichloroethene Ave 0.5610 0.5467 0.0100 48.7 50.0 -2.5 50.0

2-Butanone (MEK) Ave 0.1174 0.1140 0.0100 48.5 50.0 -2.9 50.0

Propionitrile Ave 0.0308 0.0272 0.0010 354 400 -11.4 50.0

Bromochloromethane Ave 0.2056 0.1957 0.0100 47.6 50.0 -4.8 50.0

Tetrahydrofuran Ave 0.0819 0.0753 0.0100 46.0 50.0 -8.0 50.0

Chloroform Ave 0.9125 0.9102 0.0100 49.9 50.0 -0.3 20.0

1,1,1-Trichloroethane Ave 0.8591 0.9230 0.0100 53.7 50.0 7.4 50.0

Carbon tetrachloride Ave 0.5223 0.5596 0.0100 53.6 50.0 7.1 50.0

1,1-Dichloropropene Ave 0.7416 0.7711 0.0100 52.0 50.0 4.0 50.0

Benzene Ave 1.447 1.385 0.0100 47.9 50.0 -4.3 50.0

1,2-Dichloroethane Ave 0.4605 0.4353 0.0100 47.3 50.0 -5.5 50.0

Trichloroethene Ave 0.3551 0.3615 0.0100 50.9 50.0 1.8 50.0

1,2-Dichloropropane Ave 0.4197 0.3788 0.0100 45.1 50.0 -9.8 20.0

Dibromomethane Ave 0.1358 0.1303 0.0100 48.0 50.0 -4.1 50.0

Bromodichloromethane Ave 0.3668 0.3766 0.0100 51.3 50.0 2.7 50.0

2-Chloroethyl vinyl ether Ave 0.1202 0.1144 0.0100 47.6 50.0 -4.9 50.0

cis-1,3-Dichloropropene Ave 0.3958 0.3931 0.0100 49.7 50.0 -0.7 50.0

4-Methyl-2-pentanone (MIBK) Ave 0.1885 0.1831 0.0100 48.6 50.0 -2.9 50.0

Toluene Ave 0.9066 0.8345 0.0100 46.0 50.0 -8.0 20.0

trans-1,3-Dichloropropene Ave 0.3238 0.3174 0.0100 49.0 50.0 -2.0 50.0

FORM VII 8260B

Page 185 of 384 01/09/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53491-1

CMS18

12/28/2012 09:14

11/20/2012 15:57

11/20/2012 19:11

CCV 500-174064/2

DB624

TestAmerica Chicago

Lab File ID: 18C1228.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

1,1,2-Trichloroethane Ave 0.2466 0.2390 0.0100 48.5 50.0 -3.1 50.0

Tetrachloroethene Ave 0.4508 0.4570 0.0100 50.7 50.0 1.4 50.0

1,3-Dichloropropane Ave 0.3653 0.3521 0.0100 48.2 50.0 -3.6 50.0

2-Hexanone Ave 0.1337 0.1408 0.0100 52.6 50.0 5.3 50.0

Dibromochloromethane Qua1 0.2443 0.0100 48.8 50.0 -2.3 50.0

1,2-Dibromoethane Ave 0.1685 0.1551 0.0100 46.0 50.0 -8.0 50.0

1-Chlorohexane Ave 0.7416 0.7200 0.0100 48.5 50.0 -2.9 50.0

Chlorobenzene Ave 1.091 1.067 0.3000 48.9 50.0 -2.2 50.0

1,1,1,2-Tetrachloroethane Ave 0.3659 0.3935 0.0100 53.8 50.0 7.5 50.0

Ethylbenzene Ave 0.6360 0.6449 0.0100 50.7 50.0 1.4 20.0

m&p-Xylene Ave 1.652 1.677 0.0100 102 100 1.5 50.0

o-Xylene Ave 1.745 1.751 0.0100 50.2 50.0 0.4 50.0

Styrene Ave 1.198 1.195 0.0100 49.9 50.0 -0.3 50.0

Bromoform Qua1 0.1351 0.1000 45.8 50.0 -8.4 50.0

Isopropylbenzene Ave 4.053 4.262 0.0100 52.6 50.0 5.1 50.0

1,1,2,2-Tetrachloroethane Ave 0.4016 0.4007 0.3000 49.9 50.0 -0.2 50.0

Bromobenzene Ave 0.8022 0.7804 0.0100 48.6 50.0 -2.7 50.0

1,2,3-Trichloropropane Ave 0.3605 0.3357 0.0100 46.6 50.0 -6.9 50.0

N-Propylbenzene Ave 4.900 5.113 0.0100 52.2 50.0 4.3 50.0

2-Chlorotoluene Ave 2.790 2.842 0.0100 50.9 50.0 1.9 50.0

1,3,5-Trimethylbenzene Ave 3.453 3.578 0.0100 51.8 50.0 3.6 50.0

4-Chlorotoluene Ave 3.244 3.306 0.0100 51.0 50.0 1.9 50.0

tert-Butylbenzene Ave 3.061 3.149 0.0100 51.4 50.0 2.8 50.0

1,2,4-Trimethylbenzene Ave 3.430 3.504 0.0100 51.1 50.0 2.1 50.0

sec-Butylbenzene Ave 4.611 4.798 0.0100 52.0 50.0 4.1 50.0

1,3-Dichlorobenzene Ave 1.742 1.720 0.0100 49.4 50.0 -1.3 50.0

p-Isopropyltoluene Ave 3.850 4.047 0.0100 52.6 50.0 5.1 50.0

1,4-Dichlorobenzene Ave 1.714 1.677 0.0100 48.9 50.0 -2.1 50.0

n-Butylbenzene Ave 3.627 3.934 0.0100 54.2 50.0 8.4 50.0

1,2-Dichlorobenzene Ave 1.428 1.410 0.0100 49.4 50.0 -1.2 50.0

1,2-Dibromo-3-Chloropropane Ave 0.0518 0.0547 0.0100 52.9 50.0 5.7 50.0

1,2,4-Trichlorobenzene Ave 0.7642 0.7439 0.0100 48.7 50.0 -2.7 50.0

Hexachlorobutadiene Qua1 0.6482 0.0100 50.7 50.0 1.5 50.0

Naphthalene Ave 0.9358 0.8754 0.0100 46.8 50.0 -6.4 50.0

1,2,3-Trichlorobenzene Ave 0.5020 0.4632 0.0100 46.1 50.0 -7.7 50.0

Dibromofluoromethane Ave 0.4406 0.4400 0.0100 49.9 50.0 -0.1 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.3228 0.3156 0.0100 48.9 50.0 -2.2 50.0

Toluene-d8 (Surr) Ave 1.202 1.205 0.0100 50.1 50.0 0.2 50.0

4-Bromofluorobenzene (Surr) Ave 0.5452 0.5323 0.0100 48.8 50.0 -2.4 50.0

FORM VII 8260B

Page 186 of 384 01/09/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53491-1

CMS18

12/28/2012 09:37

11/20/2012 15:57

11/20/2012 19:11

CCV 500-174064/3

DB624

TestAmerica Chicago

Lab File ID: 18D1228.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dibromofluoromethane Ave 0.4406 0.4309 0.0100 48.9 50.0 -2.2 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.3228 0.3128 0.0100 48.5 50.0 -3.1 50.0

Toluene-d8 (Surr) Ave 1.202 1.164 0.0100 48.4 50.0 -3.2 50.0

4-Bromofluorobenzene (Surr) Ave 0.5452 0.5299 0.0100 48.6 50.0 -2.8 50.0

FORM VII 8260B

Page 187 of 384 01/09/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53491-1

CMS18

12/28/2012 09:37

11/20/2012 19:35

11/20/2012 22:26

CCV 500-174064/3

DB624

TestAmerica Chicago

Lab File ID: 18D1228.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Butadiene Ave 1.088 1.182 0.0100 54.3 50.0 8.7 50.0

Ethyl ether Ave 0.4336 0.3630 0.0100 41.9 50.0 -16.3 50.0

Iodomethane Ave 0.8980 0.9031 0.0100 101 100 0.6 50.0

3-Chloropropene Ave 0.3009 0.3168 0.0100 105 100 5.3 50.0

Methyl acetate Ave 0.3161 0.2765 0.0100 43.7 50.0 -12.5 50.0

Hexane Ave 1.276 1.232 0.0100 48.3 50.0 -3.4 50.0

Isopropyl ether Ave 2.477 2.279 0.0100 46.0 50.0 -8.0 50.0

2-Chloro-1,3-butadiene Ave 1.529 1.550 0.0100 50.7 50.0 1.4 50.0

Ethyl acetate Ave 0.2378 0.2034 0.0100 428 500 -14.5 50.0

Methacrylonitrile Ave 0.1997 0.1778 0.0100 89.0 100 -11.0 50.0

Cyclohexane Lin1 1.802 0.0100 49.1 50.0 -1.9 50.0

Isobutyl alcohol Ave 0.0087 0.0086 0.0010 3963 4000 -0.9 50.0

2,2,4-Trimethylpentane Ave 2.944 2.803 0.0100 47.6 50.0 -4.8 50.0

Heptane Ave 0.8721 0.8750 0.0100 50.2 50.0 0.3 50.0

n-Butyl alcohol Ave 0.0054 0.0058 0.0010 4240 4000 6.0 50.0

Methylcyclohexane Ave 0.7981 0.8056 0.0100 50.5 50.0 0.9 50.0

Methyl methacrylate Ave 0.1838 0.1595 0.0100 86.8 100 -13.2 50.0

2-Nitropropane Ave 0.0698 0.0775 0.0100 4440 4000 11.0 50.0

Ethyl methacrylate Ave 0.2459 0.2332 0.0100 94.8 100 -5.2 50.0

Cyclohexanone Ave 0.0282 0.0473 0.0100 6696 4000 67.4* 50.0

trans-1,4-Dichloro-2-butene Lin1 0.0592 0.0100 91.6 100 -8.4 50.0

Pentachloroethane Ave 0.2879 0.3019 0.0100 105 100 4.9 50.0

1,3,5-Trichlorobenzene Ave 1.196 1.317 0.0100 55.0 50.0 10.0 50.0

2-Methylnaphthalene Qua 0.2716 0.0100 40.1 50.0 -19.9 50.0

FORM VII 8260B

Page 188 of 384 01/09/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53491-1

CMS22

12/12/2012 00:17

12/11/2012 14:23

12/11/2012 18:09

ICV 500-172615/23

DB624

TestAmerica Chicago

Lab File ID: 22S1211.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.5420 0.4239 0.0100 39.1 50.0 -21.8 25.0

Chloromethane Ave 0.7111 0.5561 0.1000 39.1 50.0 -21.8 25.0

Vinyl chloride Ave 0.6381 0.5920 0.0100 46.4 50.0 -7.2 25.0

Bromomethane Ave 0.1998 0.1541 0.0100 38.6 50.0 -22.9 25.0

Chloroethane Ave 0.3338 0.2911 0.0100 43.6 50.0 -12.8 25.0

Dichlorofluoromethane Ave 0.999 0.8378 0.0100 41.9 50.0 -16.2 25.0

Trichlorofluoromethane Ave 0.8265 0.7409 0.0100 44.8 50.0 -10.4 25.0

Acrolein Ave 0.0397 0.0406 0.0010 2044 2000 2.2 25.0

1,1-Dichloroethene Ave 0.4001 0.3815 0.0100 47.7 50.0 -4.7 25.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.4862 0.4598 0.0100 47.3 50.0 -5.4 25.0

Acetone Ave 0.0639 0.0621 0.0100 48.5 50.0 -2.9 25.0

Carbon disulfide Ave 1.480 1.369 0.0100 46.3 50.0 -7.5 25.0

Acetonitrile Ave 0.0297 0.0292 0.0010 393 400 -1.7 25.0

Methylene Chloride Ave 0.3812 0.3602 0.0100 47.2 50.0 -5.5 25.0

Acrylonitrile Ave 0.0805 0.0797 0.0010 396 400 -1.0 25.0

trans-1,2-Dichloroethene Ave 0.4499 0.4398 0.0100 48.9 50.0 -2.3 25.0

Methyl tert-butyl ether Ave 0.7369 0.6905 0.0100 46.9 50.0 -6.3 25.0

1,1-Dichloroethane Ave 0.8857 0.8456 0.1000 47.7 50.0 -4.5 25.0

Vinyl acetate Ave 0.6255 0.6214 0.0100 49.7 50.0 -0.6 25.0

2,2-Dichloropropane Ave 0.7341 0.6853 0.0100 46.7 50.0 -6.6 25.0

cis-1,2-Dichloroethene Ave 0.4554 0.4436 0.0100 48.7 50.0 -2.6 25.0

2-Butanone (MEK) Ave 0.0924 0.0837 0.0100 45.3 50.0 -9.4 25.0

Propionitrile Ave 0.0203 0.0211 0.0010 414 400 3.5 25.0

Bromochloromethane Ave 0.1785 0.1638 0.0100 45.9 50.0 -8.2 25.0

Tetrahydrofuran Ave 0.0578 0.0548 0.0100 47.3 50.0 -5.3 25.0

Chloroform Ave 0.7375 0.7135 0.0100 48.4 50.0 -3.3 25.0

1,1,1-Trichloroethane Ave 0.7394 0.7299 0.0100 49.4 50.0 -1.3 25.0

Carbon tetrachloride Ave 0.4834 0.4652 0.0100 48.1 50.0 -3.8 25.0

1,1-Dichloropropene Ave 0.6488 0.6138 0.0100 47.3 50.0 -5.4 25.0

Benzene Ave 1.229 1.148 0.0100 46.7 50.0 -6.6 25.0

1,2-Dichloroethane Ave 0.3536 0.3244 0.0100 45.9 50.0 -8.3 25.0

Trichloroethene Ave 0.3450 0.3212 0.0100 46.6 50.0 -6.9 25.0

1,2-Dichloropropane Ave 0.3152 0.2970 0.0100 47.1 50.0 -5.8 25.0

Dibromomethane Ave 0.1271 0.1149 0.0100 45.2 50.0 -9.6 25.0

Bromodichloromethane Ave 0.3600 0.3216 0.0100 44.7 50.0 -10.7 25.0

2-Chloroethyl vinyl ether Ave 0.1054 0.0957 0.0100 45.4 50.0 -9.2 25.0

cis-1,3-Dichloropropene Ave 0.4091 0.3814 0.0100 50.1 53.8 -6.8 25.0

4-Methyl-2-pentanone (MIBK) Ave 0.1536 0.1404 0.0100 45.7 50.0 -8.6 25.0

Toluene Ave 0.8177 0.7569 0.0100 46.3 50.0 -7.4 25.0

trans-1,3-Dichloropropene Ave 0.3392 0.3107 0.0100 44.5 48.6 -8.4 25.0

FORM VII 8260B

Page 189 of 384 01/09/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53491-1

CMS22

12/12/2012 00:17

12/11/2012 14:23

12/11/2012 18:09

ICV 500-172615/23

DB624

TestAmerica Chicago

Lab File ID: 22S1211.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

1,1,2-Trichloroethane Ave 0.1723 0.1573 0.0100 45.6 50.0 -8.7 25.0

Tetrachloroethene Ave 0.4537 0.4260 0.0100 47.0 50.0 -6.1 25.0

1,3-Dichloropropane Ave 0.3491 0.3223 0.0100 46.2 50.0 -7.7 25.0

2-Hexanone Ave 0.1204 0.1135 0.0100 47.1 50.0 -5.7 25.0

Dibromochloromethane Ave 0.2603 0.2454 0.0100 47.1 50.0 -5.7 25.0

1,2-Dibromoethane Ave 0.1651 0.1486 0.0100 45.0 50.0 -10.0 25.0

Chlorobenzene Ave 1.012 0.9004 0.3000 44.5 50.0 -11.0 25.0

1-Chlorohexane Ave 0.6865 0.6546 0.0100 47.7 50.0 -4.6 25.0

1,1,1,2-Tetrachloroethane Ave 0.3400 0.3297 0.0100 48.5 50.0 -3.0 25.0

Ethylbenzene Ave 0.5753 0.5498 0.0100 47.8 50.0 -4.4 25.0

m&p-Xylene Ave 1.427 1.339 0.0100 93.8 100 -6.2 25.0

o-Xylene Ave 1.456 1.295 0.0100 44.5 50.0 -11.1 25.0

Styrene Ave 1.120 1.076 0.0100 48.0 50.0 -3.9 25.0

Bromoform Ave 0.1536 0.1521 0.1000 49.5 50.0 -1.0 25.0

Isopropylbenzene Ave 3.312 2.951 0.0100 44.6 50.0 -10.9 25.0

Bromobenzene Ave 0.7374 0.6901 0.0100 46.8 50.0 -6.4 25.0

1,1,2,2-Tetrachloroethane Ave 0.3844 0.3650 0.3000 47.5 50.0 -5.1 25.0

1,2,3-Trichloropropane Ave 0.2827 0.2697 0.0100 47.7 50.0 -4.6 25.0

N-Propylbenzene Ave 3.971 3.489 0.0100 43.9 50.0 -12.2 25.0

4-Chlorotoluene Ave 2.242 2.042 0.0100 45.5 50.0 -8.9 25.0

1,3,5-Trimethylbenzene Ave 2.765 2.737 0.0100 49.5 50.0 -1.0 25.0

2-Chlorotoluene Ave 2.663 2.355 0.0100 44.2 50.0 -11.6 25.0

tert-Butylbenzene Ave 2.558 2.302 0.0100 45.0 50.0 -10.0 25.0

1,2,4-Trimethylbenzene Ave 2.713 2.637 0.0100 48.6 50.0 -2.8 25.0

sec-Butylbenzene Ave 3.783 3.418 0.0100 45.2 50.0 -9.6 25.0

1,3-Dichlorobenzene Ave 1.575 1.369 0.0100 43.5 50.0 -13.1 25.0

p-Isopropyltoluene Ave 3.287 2.935 0.0100 44.7 50.0 -10.7 25.0

1,4-Dichlorobenzene Ave 1.556 1.454 0.0100 46.7 50.0 -6.6 25.0

1,2-Dichlorobenzene Ave 1.323 1.190 0.0100 45.0 50.0 -10.1 25.0

n-Butylbenzene Ave 2.919 2.736 0.0100 46.9 50.0 -6.3 25.0

1,2-Dibromo-3-Chloropropane Ave 0.0661 0.0567 0.0100 42.9 50.0 -14.2 25.0

1,2,4-Trichlorobenzene Ave 0.8970 0.7803 0.0100 43.5 50.0 -13.0 25.0

Hexachlorobutadiene Ave 0.7568 0.6904 0.0100 45.6 50.0 -8.8 25.0

Naphthalene Ave 0.9856 0.8667 0.0100 44.0 50.0 -12.1 25.0

1,2,3-Trichlorobenzene Ave 0.7171 0.6586 0.0100 45.9 50.0 -8.2 25.0

Dibromofluoromethane Ave 0.3990 0.3761 0.0100 47.1 50.0 -5.7 25.0

1,2-Dichloroethane-d4 (Surr) Ave 0.2793 0.2556 0.0100 45.8 50.0 -8.5 25.0

Toluene-d8 (Surr) Ave 1.184 1.117 0.0100 47.2 50.0 -5.6 25.0

4-Bromofluorobenzene (Surr) Ave 0.5005 0.4730 0.0100 47.3 50.0 -5.5 25.0

FORM VII 8260B

Page 190 of 384 01/09/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53491-1

CMS22

12/12/2012 00:17

12/11/2012 19:06

12/11/2012 23:48

ICV 500-172615/23

DB624

TestAmerica Chicago

Lab File ID: 22S1211.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Ethyl ether Ave 0.2603 0.2517 0.0100 48.3 50.0 -3.3 25.0

Iodomethane Lin1 0.6879 0.0100 52.8 50.0 5.6 25.0

Methyl acetate Ave 0.2127 0.1450 0.0100 34.1 50.0 -31.8* 25.0

Hexane Ave 0.8764 0.9019 0.0100 51.5 50.0 2.9 25.0

Cyclohexane Lin1 1.057 0.0100 49.4 50.0 -1.2 25.0

Heptane Ave 0.7351 0.6922 0.0100 47.1 50.0 -5.8 25.0

Methylcyclohexane Ave 0.5969 0.6069 0.0100 50.8 50.0 1.7 25.0

1,3,5-Trichlorobenzene Ave 1.226 1.140 0.0100 46.5 50.0 -7.0 25.0

FORM VII 8260B

Page 191 of 384 01/09/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53491-1

CMS22

12/27/2012 11:55

12/11/2012 14:23

12/11/2012 18:09

CCV 500-173987/2

DB624

TestAmerica Chicago

Lab File ID: 22C1227.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.5420 0.6218 0.0100 57.4 50.0 14.7 50.0

Chloromethane Ave 0.7111 0.7065 0.1000 49.7 50.0 -0.7 50.0

Vinyl chloride Ave 0.6381 0.6748 0.0100 52.9 50.0 5.8 20.0

Bromomethane Ave 0.1998 0.2820 0.0100 70.6 50.0 41.2 50.0

Chloroethane Ave 0.3338 0.3981 0.0100 59.6 50.0 19.3 50.0

Dichlorofluoromethane Ave 0.999 0.997 0.0100 49.9 50.0 -0.2 50.0

Trichlorofluoromethane Ave 0.8265 0.8752 0.0100 53.0 50.0 5.9 50.0

Acrolein Ave 0.0397 0.0285 0.0010 1436 2000 -28.2 50.0

1,1-Dichloroethene Ave 0.4001 0.4001 0.0100 50.0 50.0 -0.0 20.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.4862 0.4759 0.0100 49.0 50.0 -2.1 50.0

Acetone Ave 0.0639 0.0587 0.0100 45.9 50.0 -8.2 50.0

Carbon disulfide Ave 1.480 1.472 0.0100 49.7 50.0 -0.6 50.0

Acetonitrile Ave 0.0297 0.0245 0.0010 330 400 -17.5 50.0

Methylene Chloride Ave 0.3812 0.3566 0.0100 46.8 50.0 -6.4 50.0

Acrylonitrile Ave 0.0805 0.0762 0.0010 379 400 -5.4 50.0

trans-1,2-Dichloroethene Ave 0.4499 0.4317 0.0100 48.0 50.0 -4.1 50.0

Methyl tert-butyl ether Ave 0.7369 0.6671 0.0100 45.3 50.0 -9.5 50.0

1,1-Dichloroethane Ave 0.8857 0.8438 0.1000 47.6 50.0 -4.7 50.0

Vinyl acetate Ave 0.6255 0.5267 0.0100 42.1 50.0 -15.8 50.0

2,2-Dichloropropane Ave 0.7341 0.6289 0.0100 42.8 50.0 -14.3 50.0

cis-1,2-Dichloroethene Ave 0.4554 0.4453 0.0100 48.9 50.0 -2.2 50.0

2-Butanone (MEK) Ave 0.0924 0.0874 0.0100 47.3 50.0 -5.4 50.0

Propionitrile Ave 0.0203 0.0196 0.0010 386 400 -3.6 50.0

Bromochloromethane Ave 0.1785 0.1670 0.0100 46.8 50.0 -6.5 50.0

Tetrahydrofuran Ave 0.0578 0.0515 0.0100 44.5 50.0 -11.0 50.0

Chloroform Ave 0.7375 0.6995 0.0100 47.4 50.0 -5.1 20.0

1,1,1-Trichloroethane Ave 0.7394 0.6854 0.0100 46.4 50.0 -7.3 50.0

Carbon tetrachloride Ave 0.4834 0.4313 0.0100 44.6 50.0 -10.8 50.0

1,1-Dichloropropene Ave 0.6488 0.6403 0.0100 49.4 50.0 -1.3 50.0

Benzene Ave 1.229 1.224 0.0100 49.8 50.0 -0.4 50.0

1,2-Dichloroethane Ave 0.3536 0.3533 0.0100 50.0 50.0 -0.0 50.0

Trichloroethene Ave 0.3450 0.3490 0.0100 50.6 50.0 1.1 50.0

1,2-Dichloropropane Ave 0.3152 0.3146 0.0100 49.9 50.0 -0.2 20.0

Dibromomethane Ave 0.1271 0.1251 0.0100 49.2 50.0 -1.6 50.0

Bromodichloromethane Ave 0.3600 0.3555 0.0100 49.4 50.0 -1.2 50.0

2-Chloroethyl vinyl ether Ave 0.1054 0.1106 0.0100 52.5 50.0 5.0 50.0

cis-1,3-Dichloropropene Ave 0.4091 0.3925 0.0100 48.0 50.0 -4.1 50.0

4-Methyl-2-pentanone (MIBK) Ave 0.1536 0.1479 0.0100 48.1 50.0 -3.7 50.0

Toluene Ave 0.8177 0.8087 0.0100 49.5 50.0 -1.1 20.0

trans-1,3-Dichloropropene Ave 0.3392 0.3122 0.0100 46.0 50.0 -7.9 50.0

FORM VII 8260B

Page 192 of 384 01/09/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53491-1

CMS22

12/27/2012 11:55

12/11/2012 14:23

12/11/2012 18:09

CCV 500-173987/2

DB624

TestAmerica Chicago

Lab File ID: 22C1227.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

1,1,2-Trichloroethane Ave 0.1723 0.1643 0.0100 47.7 50.0 -4.7 50.0

Tetrachloroethene Ave 0.4537 0.4598 0.0100 50.7 50.0 1.3 50.0

1,3-Dichloropropane Ave 0.3491 0.3473 0.0100 49.8 50.0 -0.5 50.0

2-Hexanone Ave 0.1204 0.1202 0.0100 49.9 50.0 -0.2 50.0

Dibromochloromethane Ave 0.2603 0.2612 0.0100 50.2 50.0 0.4 50.0

1,2-Dibromoethane Ave 0.1651 0.1642 0.0100 49.7 50.0 -0.5 50.0

Chlorobenzene Ave 1.012 1.044 0.3000 51.6 50.0 3.2 50.0

1-Chlorohexane Ave 0.6865 0.7028 0.0100 51.2 50.0 2.4 50.0

1,1,1,2-Tetrachloroethane Ave 0.3400 0.3319 0.0100 48.8 50.0 -2.4 50.0

Ethylbenzene Ave 0.5753 0.5986 0.0100 52.0 50.0 4.1 20.0

m&p-Xylene Ave 1.427 1.517 0.0100 106 100 6.3 50.0

o-Xylene Ave 1.456 1.495 0.0100 51.3 50.0 2.7 50.0

Styrene Ave 1.120 1.174 0.0100 52.4 50.0 4.8 50.0

Bromoform Ave 0.1536 0.1506 0.1000 49.0 50.0 -2.0 50.0

Isopropylbenzene Ave 3.312 3.313 0.0100 50.0 50.0 0.0 50.0

Bromobenzene Ave 0.7374 0.7245 0.0100 49.1 50.0 -1.8 50.0

1,1,2,2-Tetrachloroethane Ave 0.3844 0.3760 0.3000 48.9 50.0 -2.2 50.0

1,2,3-Trichloropropane Ave 0.2827 0.2682 0.0100 47.5 50.0 -5.1 50.0

N-Propylbenzene Ave 3.971 4.091 0.0100 51.5 50.0 3.0 50.0

4-Chlorotoluene Ave 2.242 2.248 0.0100 50.1 50.0 0.3 50.0

1,3,5-Trimethylbenzene Ave 2.765 2.837 0.0100 51.3 50.0 2.6 50.0

2-Chlorotoluene Ave 2.663 2.701 0.0100 50.7 50.0 1.5 50.0

tert-Butylbenzene Ave 2.558 2.540 0.0100 49.7 50.0 -0.7 50.0

1,2,4-Trimethylbenzene Ave 2.713 2.754 0.0100 50.7 50.0 1.5 50.0

sec-Butylbenzene Ave 3.783 3.893 0.0100 51.5 50.0 2.9 50.0

1,3-Dichlorobenzene Ave 1.575 1.592 0.0100 50.5 50.0 1.1 50.0

p-Isopropyltoluene Ave 3.287 3.392 0.0100 51.6 50.0 3.2 50.0

1,4-Dichlorobenzene Ave 1.556 1.585 0.0100 50.9 50.0 1.9 50.0

1,2-Dichlorobenzene Ave 1.323 1.350 0.0100 51.0 50.0 2.0 50.0

n-Butylbenzene Ave 2.919 3.071 0.0100 52.6 50.0 5.2 50.0

1,2-Dibromo-3-Chloropropane Ave 0.0661 0.0552 0.0100 41.7 50.0 -16.6 50.0

1,2,4-Trichlorobenzene Ave 0.8970 0.8967 0.0100 50.0 50.0 -0.0 50.0

Hexachlorobutadiene Ave 0.7568 0.7691 0.0100 50.8 50.0 1.6 50.0

Naphthalene Ave 0.9856 0.9243 0.0100 46.9 50.0 -6.2 50.0

1,2,3-Trichlorobenzene Ave 0.7171 0.7043 0.0100 49.1 50.0 -1.8 50.0

Dibromofluoromethane Ave 0.3990 0.3704 0.0100 46.4 50.0 -7.2 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.2793 0.2555 0.0100 45.7 50.0 -8.5 50.0

Toluene-d8 (Surr) Ave 1.184 1.141 0.0100 48.2 50.0 -3.6 50.0

4-Bromofluorobenzene (Surr) Ave 0.5005 0.4821 0.0100 48.2 50.0 -3.7 50.0

FORM VII 8260B

Page 193 of 384 01/09/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53491-1

CMS22

12/27/2012 12:22

12/11/2012 14:23

12/11/2012 18:09

CCV 500-173987/3

DB624

TestAmerica Chicago

Lab File ID: 22D1227.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dibromofluoromethane Ave 0.3990 0.3757 0.0100 47.1 50.0 -5.8 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.2793 0.2682 0.0100 48.0 50.0 -4.0 50.0

Toluene-d8 (Surr) Ave 1.184 1.217 0.0100 51.4 50.0 2.8 50.0

4-Bromofluorobenzene (Surr) Ave 0.5005 0.5156 0.0100 51.5 50.0 3.0 50.0

FORM VII 8260B

Page 194 of 384 01/09/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53491-1

CMS22

12/27/2012 12:22

12/11/2012 19:06

12/11/2012 23:48

CCV 500-173987/3

DB624

TestAmerica Chicago

Lab File ID: 22D1227.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Butadiene Lin1 0.7254 0.0100 44.8 50.0 -10.5 50.0

Ethyl ether Ave 0.2603 0.2638 0.0100 50.7 50.0 1.3 50.0

Iodomethane Lin1 0.6395 0.0100 96.6 100 -3.4 50.0

3-Chloropropene Ave 0.2462 0.2406 0.0100 97.7 100 -2.3 50.0

Methyl acetate Ave 0.2127 0.1901 0.0100 44.7 50.0 -10.6 50.0

Hexane Ave 0.8764 0.9344 0.0100 53.3 50.0 6.6 50.0

2-Chloro-1,3-butadiene Ave 0.9423 0.9629 0.0100 51.1 50.0 2.2 50.0

Isopropyl ether Ave 1.545 1.519 0.0100 49.2 50.0 -1.6 50.0

Ethyl acetate Ave 0.1956 0.1976 0.0100 505 500 1.0 50.0

Methacrylonitrile Ave 0.1427 0.1506 0.0100 106 100 5.6 50.0

Cyclohexane Lin1 1.052 0.0100 49.1 50.0 -1.7 50.0

Isobutyl alcohol Ave 0.0073 0.0065 0.0010 3556 4000 -11.1 50.0

2,2,4-Trimethylpentane Ave 1.673 1.785 0.0100 53.4 50.0 6.7 50.0

Heptane Ave 0.7351 0.7687 0.0100 52.3 50.0 4.6 50.0

n-Butyl alcohol Ave 0.0045 0.0037 0.0010 3350 4000 -16.3 50.0

Methylcyclohexane Ave 0.5969 0.6334 0.0100 53.1 50.0 6.1 50.0

Methyl methacrylate Ave 0.1655 0.1732 0.0100 105 100 4.7 50.0

2-Nitropropane Ave 0.0618 0.0767 0.0100 4966 4000 24.2 50.0

Ethyl methacrylate Ave 0.2528 0.2708 0.0100 107 100 7.1 50.0

Cyclohexanone Ave 0.0256 0.0529 0.0100 8275 4000 106.9* 50.0

trans-1,4-Dichloro-2-butene Ave 0.0710 0.0618 0.0100 87.1 100 -12.9 50.0

Pentachloroethane Ave 0.2758 0.2996 0.0100 109 100 8.6 50.0

1,3,5-Trichlorobenzene Ave 1.226 1.353 0.0100 55.2 50.0 10.3 50.0

2-Methylnaphthalene Ave 0.6831 0.6506 0.0100 47.6 50.0 -4.8 50.0

FORM VII 8260B

Page 195 of 384 01/09/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53491-1

Lab Sample ID: MB 500-173973/5

Matrix: Lab File ID: 6M1227.d

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(g)

0.2(mm)

Date Analyzed: 12/27/2012 10:33

DB624 ID:

Analysis Batch No.: 173973 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone <5.00 5.00 2.16

78-93-3 2-Butanone (MEK) <5.00 5.00 1.81

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 94 70-134

2037-26-5 Toluene-d8 (Surr) 96 75-122

460-00-4 4-Bromofluorobenzene (Surr) 84 70-122

1868-53-7 Dibromofluoromethane 90 75-120

FORM I 8260B

Page 196 of 384 01/09/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53491-1

Lab Sample ID: MB 500-173987/7

Matrix: Lab File ID: 22M1227.D

Analysis Method: 8260B Date Collected:

Water

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(mL)

0.2(mm)

Date Analyzed: 12/27/2012 14:10

DB624 ID:

Analysis Batch No.: 173987 Units: ug/L

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone <5.00 5.00 1.29

78-93-3 2-Butanone (MEK) <5.00 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 98 75-125

2037-26-5 Toluene-d8 (Surr) 103 75-120

460-00-4 4-Bromofluorobenzene (Surr) 97 75-120

1868-53-7 Dibromofluoromethane 97 75-120

FORM I 8260B

Page 197 of 384 01/09/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53491-1

Lab Sample ID: MB 500-174064/6

Matrix: Lab File ID: 18M1228.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Medium

5 (mL)

0.2(mm)

Date Analyzed: 12/28/2012 10:45

DB624 ID:

Analysis Batch No.: 174064 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone <5.00 5.00 1.30

78-93-3 2-Butanone (MEK) <5.00 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 101 75-125

2037-26-5 Toluene-d8 (Surr) 101 75-120

460-00-4 4-Bromofluorobenzene (Surr) 98 75-120

1868-53-7 Dibromofluoromethane 96 75-120

FORM I 8260B

Page 198 of 384 01/09/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53491-1

Lab Sample ID: LCS 500-173973/6

Matrix: Lab File ID: 6S1227.d

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(g)

0.2(mm)

Date Analyzed: 12/27/2012 10:56

DB624 ID:

Analysis Batch No.: 173973 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 47.98 5.00 2.16

78-93-3 2-Butanone (MEK) 43.18 5.00 1.81

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 84 70-134

2037-26-5 Toluene-d8 (Surr) 89 75-122

460-00-4 4-Bromofluorobenzene (Surr) 81 70-122

1868-53-7 Dibromofluoromethane 81 75-120

FORM I 8260B

Page 199 of 384 01/09/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53491-1

Lab Sample ID: LCS 500-173987/4

Matrix: Lab File ID: 22S1227.D

Analysis Method: 8260B Date Collected:

Water

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(mL)

0.2(mm)

Date Analyzed: 12/27/2012 12:46

DB624 ID:

Analysis Batch No.: 173987 Units: ug/L

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 53.44 5.00 1.29

78-93-3 2-Butanone (MEK) 46.97 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 92 75-125

2037-26-5 Toluene-d8 (Surr) 96 75-120

460-00-4 4-Bromofluorobenzene (Surr) 96 75-120

1868-53-7 Dibromofluoromethane 94 75-120

FORM I 8260B

Page 200 of 384 01/09/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53491-1

Lab Sample ID: LCS 500-174064/4

Matrix: Lab File ID: 18S1228.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Medium

5 (mL)

0.2(mm)

Date Analyzed: 12/28/2012 10:00

DB624 ID:

Analysis Batch No.: 174064 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 50.53 5.00 1.30

78-93-3 2-Butanone (MEK) 43.61 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 95 75-125

2037-26-5 Toluene-d8 (Surr) 97 75-120

460-00-4 4-Bromofluorobenzene (Surr) 97 75-120

1868-53-7 Dibromofluoromethane 100 75-120

FORM I 8260B

Page 201 of 384 01/09/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53491-1

Lab Sample ID: LCSD 500-173973/7

Matrix: Lab File ID: 6T1227.d

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(g)

0.2(mm)

Date Analyzed: 12/27/2012 11:19

DB624 ID:

Analysis Batch No.: 173973 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 55.07 5.00 2.16

78-93-3 2-Butanone (MEK) 44.82 5.00 1.81

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 88 70-134

2037-26-5 Toluene-d8 (Surr) 93 75-122

460-00-4 4-Bromofluorobenzene (Surr) 87 70-122

1868-53-7 Dibromofluoromethane 91 75-120

FORM I 8260B

Page 202 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53491-1

CMS06

171819

Start Date:

End Date: 12/04/2012 19:58

12/04/2012 14:01

BFB 500-171819/1 12/04/2012 14:01 1 6B1204.d DB624 0.2(mm)

STD1 500-171819/2 IC 12/04/2012 14:34 1 6I1204a.d DB624 0.2(mm)

STD2 500-171819/3 IC 12/04/2012 14:57 1 6I1204b.d DB624 0.2(mm)

STD4 500-171819/5 IC 12/04/2012 15:43 1 6I1204d.d DB624 0.2(mm)

STD3 500-171819/16 

ICIS

12/04/2012 16:10 1 6I1204CC.d DB624 0.2(mm)

STD5 500-171819/6 IC 12/04/2012 16:33 1 6I1204e.d DB624 0.2(mm)

STD6 500-171819/7 IC 12/04/2012 16:55 1 6I1204f.d DB624 0.2(mm)

STD1AP 500-171819/8 

IC

12/04/2012 17:18 1 6J1204a.d DB624 0.2(mm)

STD2AP 500-171819/9 

IC

12/04/2012 17:41 1 6J1204b.d DB624 0.2(mm)

STD3AP 500-171819/10 

IC

12/04/2012 18:04 1 6J1204c.d DB624 0.2(mm)

STD4AP 500-171819/11 

IC

12/04/2012 18:27 1 6J1204d.d DB624 0.2(mm)

STD5AP 500-171819/12 

IC

12/04/2012 18:49 1 6J1204e.d DB624 0.2(mm)

STD6AP 500-171819/13 

IC

12/04/2012 19:13 1 6J1204f.d DB624 0.2(mm)

ICV 500-171819/15 12/04/2012 19:58 1 6S1204.d DB624 0.2(mm)

8260B

Page 203 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53491-1

CMS06

173973

Start Date:

End Date: 12/27/2012 13:59

12/27/2012 08:48

BFB 500-173973/1 12/27/2012 08:48 1 6B1227.d DB624 0.2(mm)

CCV 500-173973/3 12/27/2012 09:47 1 6C1227.d DB624 0.2(mm)

CCV 500-173973/4 12/27/2012 10:10 1 6D1227.d DB624 0.2(mm)

MB 500-173973/5 12/27/2012 10:33 1 6M1227.d DB624 0.2(mm)

LCS 500-173973/6 12/27/2012 10:56 1 6S1227.d DB624 0.2(mm)

LCSD 500-173973/7 12/27/2012 11:19 1 6T1227.d DB624 0.2(mm)

ZZZZZ 12/27/2012 11:42 1 DB624 0.2(mm)

ZZZZZ 12/27/2012 12:04 1 DB624 0.2(mm)

500-53491-3 FC DISCRETE 6 12/27/2012 13:36 1 3491-03.d DB624 0.2(mm)

500-53491-4 FC D DISCRETE 6 12/27/2012 13:59 1 3491-04.d DB624 0.2(mm)

8260B

Page 204 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53491-1

CMS18

170445

Start Date:

End Date: 11/20/2012 23:15

11/20/2012 15:22

BFB 500-170445/21 11/20/2012 15:22 1 18B1120a.D DB624 0.2(mm)

STD1 500-170445/2 IC 11/20/2012 15:57 1 18I1120a.D DB624 0.2(mm)

STD2 500-170445/3 IC 11/20/2012 16:21 1 18I1120b.D DB624 0.2(mm)

STD3 500-170445/4 IC 11/20/2012 16:46 1 18I1120c.D DB624 0.2(mm)

STD4 500-170445/5 IC 11/20/2012 17:10 1 18I1120d.D DB624 0.2(mm)

STD5 500-170445/6 IC 11/20/2012 17:35 1 18I1120e.D DB624 0.2(mm)

STD6 500-170445/7 

ICIS

11/20/2012 17:59 1 18I1120f.D DB624 0.2(mm)

STD7 500-170445/8 IC 11/20/2012 18:23 1 18I1120g.D DB624 0.2(mm)

STD8 500-170445/9 IC 11/20/2012 18:47 1 18I1120h.D DB624 0.2(mm)

STD9 500-170445/10 

IC

11/20/2012 19:11 1 18I1120i.D DB624 0.2(mm)

STD2AP 500-170445/11 

IC

11/20/2012 19:35 1 DB624 0.2(mm)

STD3AP 500-170445/12 

IC

11/20/2012 19:59 1 DB624 0.2(mm)

STD4AP 500-170445/13 

IC

11/20/2012 20:24 1 DB624 0.2(mm)

STD5AP 500-170445/14 

IC

11/20/2012 20:48 1 DB624 0.2(mm)

STD6AP 500-170445/15 

IC

11/20/2012 21:13 1 DB624 0.2(mm)

STD7AP 500-170445/16 

IC

11/20/2012 21:37 1 DB624 0.2(mm)

STD8AP 500-170445/17 

IC

11/20/2012 22:01 1 DB624 0.2(mm)

STD9AP 500-170445/18 

IC

11/20/2012 22:26 1 DB624 0.2(mm)

ICV 500-170445/20 11/20/2012 23:15 1 18S1120.D DB624 0.2(mm)

8260B

Page 205 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53491-1

CMS18

174064

Start Date:

End Date: 12/28/2012 11:31

12/28/2012 08:39

BFB 500-174064/7 12/28/2012 08:39 1 18B1228a.D DB624 0.2(mm)

CCV 500-174064/2 12/28/2012 09:14 1 18C1228.D DB624 0.2(mm)

CCV 500-174064/3 12/28/2012 09:37 1 18D1228.D DB624 0.2(mm)

LCS 500-174064/4 12/28/2012 10:00 1 18S1228.D DB624 0.2(mm)

MB 500-174064/6 12/28/2012 10:45 1 18M1228.D DB624 0.2(mm)

500-53491-3 DL FC DISCRETE 6 DL 12/28/2012 11:08 50 53491-03.D DB624 0.2(mm)

500-53491-4 DL FC D DISCRETE 6 DL 12/28/2012 11:31 50 53491-04.D DB624 0.2(mm)

8260B

Page 206 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53491-1

CMS22

172615

Start Date:

End Date: 12/12/2012 00:17

12/11/2012 13:45

BFB 500-172615/1 12/11/2012 13:45 1 22B1211.D DB624 0.2(mm)

STD01 500-172615/2 

IC

12/11/2012 14:23 1 22I1211A.D DB624 0.2(mm)

STD02 500-172615/3 

IC

12/11/2012 14:51 1 22I1211B.D DB624 0.2(mm)

STD03 500-172615/4 

IC

12/11/2012 15:20 1 22I1211C.D DB624 0.2(mm)

STD04 500-172615/5 

IC

12/11/2012 15:48 1 22I1211D.D DB624 0.2(mm)

STD05 500-172615/6 

IC

12/11/2012 16:16 1 22I1211E.D DB624 0.2(mm)

STD06 500-172615/7 

ICIS

12/11/2012 16:44 1 22I1211F.D DB624 0.2(mm)

STD07 500-172615/8 

IC

12/11/2012 17:13 1 22I1211G.D DB624 0.2(mm)

STD08 500-172615/9 

IC

12/11/2012 17:41 1 22I1211H.D DB624 0.2(mm)

STD09 500-172615/10 

IC

12/11/2012 18:09 1 22I1211I.D DB624 0.2(mm)

STD02AP 

500-172615/12 IC

12/11/2012 19:06 1 DB624 0.2(mm)

STD05AP 

500-172615/15 IC

12/11/2012 20:30 1 DB624 0.2(mm)

STD06AP 

500-172615/16 IC

12/11/2012 20:59 1 DB624 0.2(mm)

STD07AP 

500-172615/17 IC

12/11/2012 21:27 1 DB624 0.2(mm)

STD08AP 

500-172615/18 IC

12/11/2012 21:55 1 DB624 0.2(mm)

STD09AP 

500-172615/19 IC

12/11/2012 22:24 1 DB624 0.2(mm)

STD03AP 

500-172615/21 IC

12/11/2012 23:20 1 DB624 0.2(mm)

STD04AP 

500-172615/22 IC

12/11/2012 23:48 1 DB624 0.2(mm)

ICV 500-172615/23 12/12/2012 00:17 1 22S1211.D DB624 0.2(mm)

8260B

Page 207 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53491-1

CMS22

173987

Start Date:

End Date: 12/27/2012 22:00

12/27/2012 11:16

BFB 500-173987/1 12/27/2012 11:16 1 22B1227.D DB624 0.2(mm)

CCV 500-173987/2 12/27/2012 11:55 1 22C1227.D DB624 0.2(mm)

CCV 500-173987/3 12/27/2012 12:22 1 22D1227.D DB624 0.2(mm)

LCS 500-173987/4 12/27/2012 12:46 1 22S1227.D DB624 0.2(mm)

MB 500-173987/7 12/27/2012 14:10 1 22M1227.D DB624 0.2(mm)

ZZZZZ 12/27/2012 15:02 1 DB624 0.2(mm)

500-53491-6 TRIP BLANK 12/27/2012 15:28 1 53491-06.D DB624 0.2(mm)

500-53491-5 FC EB 6 12/27/2012 15:54 1 53491-05.D DB624 0.2(mm)

ZZZZZ 12/27/2012 16:21 1 DB624 0.2(mm)

ZZZZZ 12/27/2012 16:47 1 DB624 0.2(mm)

ZZZZZ 12/27/2012 17:13 1 DB624 0.2(mm)

ZZZZZ 12/27/2012 17:39 1 DB624 0.2(mm)

ZZZZZ 12/27/2012 21:34 1 DB624 0.2(mm)

ZZZZZ 12/27/2012 22:00 1 DB624 0.2(mm)

8260B

Page 208 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GC/MS VOA BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

173990 12/27/12 10:28 Estes, William R

Batch Method:

TestAmerica Chicago

5030B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount AnalysisComment

FC DISCRETE 6 5 g 5 mL MeOH from soil 

jar

500-53491-A-3 5030B, 8260B T

FC D DISCRETE 6 5 g 5 mL MeOH from soil 

jar

500-53491-A-4 5030B, 8260B T

Batch Notes

Balance ID C-0133

Methanol Lot Number DH247

Pipette ID C-2207

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

8260B Page 1 of 1

Page 209 of 384 01/09/2013


METALS

Page 212 of 384 01/09/2013
COVER PAGE

Lab Name: Job Number: 

Client Sample ID Lab Sample ID

METALS

Project: John Deere Des Moines Works (JDDMW)

SDG No.:

TestAmerica Chicago 500-53491-1

FC COMPOSITE 6 500-53491-1 

FC D COMPOSITE 6 500-53491-2 

FC EB 6 500-53491-5 

Comments:

Page 213 of 384 01/09/2013
1A-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53491-1

Date Received: 12/22/2012 11:30

500-53491-1

FC COMPOSITE 6

Solid Date Sampled: 12/19/2012 14:30

Reporting Basis: DRY

METALS

TestAmerica Chicago

% Solids: 26.5

CAS No. Analyte Result RL MDL Units C Q DIL Method

7440-39-3 Barium 643 3.70 0.440 mg/Kg 1 6010B

7440-50-8 Copper 748 3.70 1.00 mg/Kg 1 6010B

7440-47-3 Chromium 15000 3.70 0.618 mg/Kg 1 6010B

7440-02-0 Nickel 85.5 3.70 0.810 mg/Kg 1 6010B

7439-92-1 Lead 253 1.85 0.636 mg/Kg B 1 6010B

7440-62-2 Vanadium 253 1.85 0.281 mg/Kg 1 6010B

7440-66-6 Zinc 501 7.40 2.54 mg/Kg 1 6010B

7439-97-6 Mercury 0.232 0.0605 0.0231 mg/Kg 1 7471A

FORM IA-IN Page 214 of 384 01/09/2013
1A-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53491-1

Date Received: 12/22/2012 11:30

500-53491-1

FC COMPOSITE 6

Solid Date Sampled: 12/19/2012 14:30

Reporting Basis: WET

METALS - TCLP

TestAmerica Chicago

CAS No. Analyte Result RL MDL Units C Q DIL Method

7440-39-3 Barium 0.0103 0.500 0.0100 mg/L J 1 6010B

7440-50-8 Copper 0.442 0.0250 0.0100 mg/L 1 6010B

7440-47-3 Chromium 0.826 0.0250 0.0100 mg/L 1 6010B

7440-02-0 Nickel 0.744 0.0250 0.0100 mg/L 1 6010B

7439-92-1 Lead <0.0500 0.0500 0.00500 mg/L 1 6010B

7440-62-2 Vanadium 0.0164 0.0250 0.00500 mg/L J 1 6010B

7440-66-6 Zinc 0.403 0.100 0.0200 mg/L 1 6010B

7439-97-6 Mercury 0.000702 0.000200 0.000020 mg/L B

0

1 7470A

FORM IA-IN Page 215 of 384 01/09/2013
1A-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53491-2

Date Received: 12/22/2012 11:30

500-53491-1

FC D COMPOSITE 6

Solid Date Sampled: 12/19/2012 14:40

Reporting Basis: DRY

METALS

TestAmerica Chicago

% Solids: 25.1

CAS No. Analyte Result RL MDL Units C Q DIL Method

7440-39-3 Barium 619 3.84 0.457 mg/Kg 1 6010B

7440-50-8 Copper 707 3.84 1.04 mg/Kg 1 6010B

7440-47-3 Chromium 15000 3.84 0.642 mg/Kg 1 6010B

7440-02-0 Nickel 86.1 3.84 0.841 mg/Kg 1 6010B

7439-92-1 Lead 244 1.92 0.661 mg/Kg B 1 6010B

7440-62-2 Vanadium 251 1.92 0.292 mg/Kg 1 6010B

7440-66-6 Zinc 499 7.68 2.64 mg/Kg 1 6010B

7439-97-6 Mercury 0.237 0.0647 0.0247 mg/Kg 1 7471A

FORM IA-IN Page 216 of 384 01/09/2013
1A-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53491-2

Date Received: 12/22/2012 11:30

500-53491-1

FC D COMPOSITE 6

Solid Date Sampled: 12/19/2012 14:40

Reporting Basis: WET

METALS - TCLP

TestAmerica Chicago

CAS No. Analyte Result RL MDL Units C Q DIL Method

7440-39-3 Barium <0.500 0.500 0.0100 mg/L 1 6010B

7440-50-8 Copper 0.0547 0.0250 0.0100 mg/L 1 6010B

7440-47-3 Chromium <0.0250 0.0250 0.0100 mg/L 1 6010B

7440-02-0 Nickel 0.0624 0.0250 0.0100 mg/L 1 6010B

7439-92-1 Lead <0.0500 0.0500 0.00500 mg/L 1 6010B

7440-62-2 Vanadium <0.0250 0.0250 0.00500 mg/L 1 6010B

7440-66-6 Zinc <0.100 0.100 0.0200 mg/L 1 6010B

7439-97-6 Mercury <0.000200 0.000200 0.000020 mg/L

0

1 7470A

FORM IA-IN Page 217 of 384 01/09/2013
1A-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53491-5

Date Received: 12/22/2012 11:30

500-53491-1

FC EB 6

Water Date Sampled: 12/19/2012 14:10

Reporting Basis: WET

METALS

TestAmerica Chicago

CAS No. Analyte Result RL MDL Units C Q DIL Method

7440-39-3 Barium <0.0100 0.0100 0.000440 mg/L 1 6010B

7440-50-8 Copper 0.00111 0.0100 0.00106 mg/L J 1 6010B

7440-47-3 Chromium <0.0100 0.0100 0.000960 mg/L 1 6010B

7440-02-0 Nickel <0.0100 0.0100 0.00190 mg/L 1 6010B

7439-92-1 Lead <0.00500 0.00500 0.00158 mg/L 1 6010B

7440-62-2 Vanadium <0.00500 0.00500 0.000620 mg/L 1 6010B

7440-66-6 Zinc <0.0200 0.0200 0.00472 mg/L 1 6010B

7439-97-6 Mercury <0.000200 0.000200 0.000071 mg/L

0

1 7470A

FORM IA-IN Page 218 of 384 01/09/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53491-1

M12LICVIC_00001 mg/L

M12LCCVIC_00001

Analyte

ICV 500-173964/10

12/26/2012 16:24

Found C True %R

CCV 500-173964/15

12/26/2012 16:59

CCV 500-173964/27

12/26/2012 18:16

Found C True %R Found C True %R

Barium 0.3991 0.400 100 0.4896 0.500 98 0.4843 0.500 97

Chromium 0.4102 0.400 103 0.5077 0.500 102 0.5167 0.500 103

Copper 0.4093 0.400 102 0.5108 0.500 102 0.5088 0.500 102

Lead 0.4139 0.400 103 0.5121 0.500 102 0.5208 0.500 104

Nickel 0.4046 0.400 101 0.4993 0.500 100 0.5044 0.500 101

Vanadium 4.027 4.00 101 4.995 5.00 100 5.070 5.00 101

Zinc 0.4072 0.400 102 0.5029 0.500 101 0.5246 0.500 105

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 219 of 384 01/09/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53491-1

M12LICVIC_00001 mg/L

M12LCCVIC_00001

Analyte

CCV 500-173964/39

12/26/2012 19:37

Found C True %R

CCV 500-173964/51

12/26/2012 20:54

CCV 500-173964/63

12/26/2012 22:15

Found C True %R Found C True %R

Barium 0.4757 0.500 95 0.4874 0.500 97 0.5129 0.500 103

Chromium 0.5194 0.500 104 0.5172 0.500 103 0.5343 0.500 107

Copper 0.5081 0.500 102 0.5067 0.500 101 0.5309 0.500 106

Lead 0.5236 0.500 105 0.5195 0.500 104 0.5403 0.500 108

Nickel 0.5031 0.500 101 0.5051 0.500 101 0.5244 0.500 105

Vanadium 5.075 5.00 102 5.049 5.00 101 5.208 5.00 104

Zinc 0.5342 0.500 107 0.5299 0.500 106 0.5454 0.500 109

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 220 of 384 01/09/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53491-1

M12LICVIC_00001 mg/L

M12LCCVIC_00001

Analyte

CCV 500-173964/75

12/26/2012 23:32

Found C True %R

CCV 500-173964/82

12/27/2012 00:15

Found C True %R Found C True %R

Barium 0.5192 0.500 104 0.5209 0.500 104

Chromium 0.5336 0.500 107 0.5290 0.500 106

Copper 0.5327 0.500 107 0.5343 0.500 107

Lead 0.5361 0.500 107 0.5317 0.500 106

Nickel 0.5255 0.500 105 0.5242 0.500 105

Vanadium 5.177 5.00 104 5.169 5.00 103

Zinc 0.5393 0.500 108 0.5327 0.500 107

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 221 of 384 01/09/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53491-1

M12LICVIC_00001 mg/L

M12LCCVIC_00001

Analyte

ICV 500-173963/6

12/26/2012 14:24

Found C True %R

CCV 500-173963/35

12/26/2012 16:28

CCV 500-173963/47

12/26/2012 17:18

Found C True %R Found C True %R

Barium 0.3896 0.400 97 0.4910 0.500 98 0.4911 0.500 98

Chromium 0.3889 0.400 97 0.4853 0.500 97 0.4943 0.500 99

Copper 0.3897 0.400 97 0.4894 0.500 98 0.4882 0.500 98

Lead 0.4010 0.400 100 0.4968 0.500 99 0.5016 0.500 100

Nickel 0.3983 0.400 100 0.4961 0.500 99 0.5001 0.500 100

Vanadium 3.883 4.00 97 4.873 5.00 97 4.892 5.00 98

Zinc 0.4066 0.400 102 0.5056 0.500 101 0.5166 0.500 103

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 222 of 384 01/09/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53491-1

M11FSTKHG_00001 ug/L

M11FSTKHG_00001

Analyte

ICV 500-173984/7

12/27/2012 08:12

Found C True %R

CCV 500-173984/19

12/27/2012 08:34

CCV 500-173984/32

12/27/2012 09:01

Found C True %R Found C True %R

Mercury 1.910 2.00 96 1.000 1.00 100 0.9660 1.00 97

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 223 of 384 01/09/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53491-1

M11FSTKHG_00001 ug/L

M11FSTKHG_00001

Analyte

CCV 500-173984/36

12/27/2012 09:08

Found C True %R Found C True %R Found C True %R

Mercury 0.8410 1.00 84

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 224 of 384 01/09/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53491-1

M11FSTKHG_00001 ug/L

M11FSTKHG_00001

Analyte

ICV 500-173997/7

12/27/2012 08:35

Found C True %R

CCV 500-173997/19

12/27/2012 08:58

CCV 500-173997/31

12/27/2012 09:21

Found C True %R Found C True %R

Mercury 1.942 J 2.00 97 1.035 1.00 103 1.052 J 1.00 105

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 225 of 384 01/09/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53491-1

M11FSTKHG_00001 ug/L

M11FSTKHG_00001

Analyte

CCV 500-173997/43

12/27/2012 09:43

Found C True %R

CCV 500-173997/54

12/27/2012 10:04

Found C True %R Found C True %R

Mercury 1.096 J 1.00 110 1.010 J 1.00 101

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 226 of 384 01/09/2013
2B-IN

Lab Name: Job No.:

SDG No.:

500-53491-1

CRQL CHECK STANDARD

METALS

Method: 6010B Instrument ID: ICP5

TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRI 500-173964/12

CRQL Check Standard

CRQL Check Standard Source: M12LCRIIC_00001

Concentration Units: mg/L

Barium 0.0200 0.01980 99 50-150

Copper 0.0200 0.02105 105 50-150

Chromium 0.0200 0.02759 138 50-150

Nickel 0.0200 0.02154 108 50-150

Lead 0.0100 0.01108 111 50-150

Vanadium 0.0100 0.01021 102 50-150

Zinc 0.0400 0.04175 104 50-150

FORM IIB-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 227 of 384 01/09/2013
2B-IN

Lab Name: Job No.:

SDG No.:

500-53491-1

CRQL CHECK STANDARD

METALS

Method: 6010B Instrument ID: ICP6

TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRI 500-173963/8

CRQL Check Standard

CRQL Check Standard Source: M12LCRIIC_00001

Concentration Units: mg/L

Barium 0.0200 0.01949 97 50-150

Copper 0.0200 0.01945 97 50-150

Chromium 0.0200 0.01962 98 50-150

Nickel 0.0200 0.01956 98 50-150

Lead 0.0100 0.01013 101 50-150

Vanadium 0.0100 0.009451 95 50-150

Zinc 0.0400 0.03889 97 50-150

FORM IIB-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 228 of 384 01/09/2013
2B-IN

Lab Name: Job No.:

SDG No.:

500-53491-1

CRQL CHECK STANDARD

METALS

Method: 7470A Instrument ID: HG6

TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRA 500-173997/9

CRQL Check Standard

CRQL Check Standard Source: M12ASTKHG_00001

Concentration Units: ug/L

Mercury 0.200 <2.00 118 50-150

FORM IIB-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 229 of 384 01/09/2013
2B-IN

Lab Name: Job No.:

SDG No.:

500-53491-1

CRQL CHECK STANDARD

METALS

Method: 7471A Instrument ID: HG5

TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRA 500-173984/9

CRQL Check Standard

CRQL Check Standard Source: M12ASTKHG_00001

Concentration Units: ug/L

Mercury 0.200 0.2080 104 50-150

FORM IIB-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 230 of 384 01/09/2013
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53491-1

mg/L

Analyte RL Found C Found C Found C Found C

ICB 500-173964/11 CCB 500-173964/16 CCB 500-173964/28 CCB 500-173964/40

12/26/2012 16:32 12/26/2012 17:06 12/26/2012 18:22 12/26/2012 19:43

3-IN

Barium 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Chromium 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Copper 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Lead 0.00500 <0.00500 <0.00500 <0.00500 <0.00500

Nickel 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Vanadium 0.00500 <0.00500 <0.00500 <0.00500 <0.00500

Zinc 0.0200 <0.0200 <0.0200 <0.0200 <0.0200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 231 of 384 01/09/2013
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53491-1

mg/L

Analyte RL Found C Found C Found C Found C

CCB 500-173964/52 CCB 500-173964/64 CCB 500-173964/76 CCB 500-173964/83

12/26/2012 21:00 12/26/2012 22:21 12/26/2012 23:38 12/27/2012 00:22

3-IN

Barium 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Chromium 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Copper 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Lead 0.00500 <0.00500 0.003280 J <0.00500 <0.00500

Nickel 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Vanadium 0.00500 <0.00500 <0.00500 <0.00500 <0.00500

Zinc 0.0200 <0.0200 <0.0200 <0.0200 <0.0200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 232 of 384 01/09/2013
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53491-1

mg/L

Analyte RL Found C Found C Found C Found C

ICB 500-173963/7 CCB 500-173963/36 CCB 500-173963/48

12/26/2012 14:28 12/26/2012 16:32 12/26/2012 17:21

3-IN

Barium 0.0100 <0.0100 <0.0100 <0.0100

Chromium 0.0100 <0.0100 <0.0100 <0.0100

Copper 0.0100 <0.0100 <0.0100 <0.0100

Lead 0.00500 <0.00500 <0.00500 <0.00500

Nickel 0.0100 <0.0100 <0.0100 <0.0100

Vanadium 0.00500 <0.00500 <0.00500 <0.00500

Zinc 0.0200 <0.0200 <0.0200 <0.0200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 233 of 384 01/09/2013
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53491-1

ug/L

Analyte RL Found C Found C Found C Found C

ICB 500-173984/8 CCB 500-173984/20 CCB 500-173984/33 CCB 500-173984/37

12/27/2012 08:14 12/27/2012 08:36 12/27/2012 09:03 12/27/2012 09:10

3-IN

Mercury 0.200 <0.200 <0.200 <0.200 <0.200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 234 of 384 01/09/2013
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53491-1

ug/L

Analyte RL Found C Found C Found C Found C

ICB 500-173997/8 CCB 500-173997/20 CCB 500-173997/32 CCB 500-173997/44

12/27/2012 08:37 12/27/2012 09:00 12/27/2012 09:22 12/27/2012 09:45

3-IN

Mercury 2.00 <2.00 <0.200 <2.00 <2.00

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 235 of 384 01/09/2013
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53491-1

ug/L

Analyte RL Found C Found C Found C Found C

CCB 500-173997/55

12/27/2012 10:06

3-IN

Mercury 2.00 <2.00

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 236 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/L Lab Sample ID: MB 500-173849/1-A

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53491-1

Instrument Code: ICP6

METHOD BLANK

METALS

 173963

TestAmerica Chicago

7440-39-3 Barium <0.0100 6010B

7440-50-8 Copper <0.0100 6010B

7440-47-3 Chromium <0.0100 6010B

7440-02-0 Nickel <0.0100 6010B

7439-92-1 Lead <0.00500 6010B

7440-62-2 Vanadium <0.00500 6010B

7440-66-6 Zinc <0.0200 6010B

FORM III-IN

Page 237 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/Kg Lab Sample ID: MB 500-173848/1-A

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53491-1

Instrument Code: ICP5

METHOD BLANK

METALS

 173964

TestAmerica Chicago

7440-39-3 Barium <1.00 6010B

7440-50-8 Copper <1.00 6010B

7440-47-3 Chromium <1.00 6010B

7440-02-0 Nickel <1.00 6010B

7439-92-1 Lead 0.1770 J 6010B

7440-62-2 Vanadium <0.500 6010B

7440-66-6 Zinc <2.00 6010B

FORM III-IN

Page 238 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/L Lab Sample ID: LB 500-173836/1-B

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53491-1

Instrument Code: ICP5

METHOD BLANK

METALS - TCLP

 173964

TestAmerica Chicago

7440-39-3 Barium <0.500 6010B

7440-50-8 Copper <0.0250 6010B

7440-47-3 Chromium <0.0250 6010B

7440-02-0 Nickel <0.0250 6010B

7439-92-1 Lead <0.0500 6010B

7440-62-2 Vanadium <0.0250 6010B

7440-66-6 Zinc <0.100 6010B

FORM III-IN

Page 239 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/L Lab Sample ID: LB2 500-173838/1-B

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53491-1

Instrument Code: ICP5

METHOD BLANK

METALS - TCLP

 173964

TestAmerica Chicago

7440-39-3 Barium <0.500 6010B

7440-50-8 Copper <0.0250 6010B

7440-47-3 Chromium <0.0250 6010B

7440-02-0 Nickel <0.0250 6010B

7439-92-1 Lead <0.0500 6010B

7440-62-2 Vanadium <0.0250 6010B

7440-66-6 Zinc <0.100 6010B

FORM III-IN

Page 240 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/L Lab Sample ID: MB 500-173908/7-A

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53491-1

Instrument Code: HG6

METHOD BLANK

METALS

 173997

TestAmerica Chicago

7439-97-6 Mercury <0.000200 7470A

FORM III-IN

Page 241 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/L Lab Sample ID: MB 500-173909/7-A

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53491-1

Instrument Code: HG6

METHOD BLANK

METALS

 173997

TestAmerica Chicago

7439-97-6 Mercury 0.00003040 J 7470A

FORM III-IN

Page 242 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/L Lab Sample ID: LB 500-173836/1-C

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53491-1

Instrument Code: HG6

METHOD BLANK

METALS - TCLP

 173997

TestAmerica Chicago

7439-97-6 Mercury 0.00003420 J 7470A

FORM III-IN

Page 243 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/L Lab Sample ID: LB2 500-173838/1-C

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53491-1

Instrument Code: HG6

METHOD BLANK

METALS - TCLP

 173997

TestAmerica Chicago

7439-97-6 Mercury 0.00003260 J 7470A

FORM III-IN

Page 244 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/Kg Lab Sample ID: MB 500-173881/7-A

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53491-1

Instrument Code: HG5

METHOD BLANK

METALS

 173984

TestAmerica Chicago

7439-97-6 Mercury <0.0167 7471A

FORM III-IN

Page 245 of 384 01/09/2013
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution A Solution A

Lab Sample ID:

TestAmerica Chicago 500-53491-1

ICSA 500-173964/13

P51226B

mg/L

M12LISAIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium 0.0000

Chromium 0.0022

Copper -0.0010

Lead -0.0005

Nickel 0.0011

Vanadium 0.0031

Zinc 0.0075

Aluminum 500 498 100

Antimony -0.0010

Arsenic 0.0009

Beryllium -0.0002

Boron 0.0009

Cadmium 0.0058

Calcium 500 482 96

Cobalt -0.0001

Iron 200 191 96

Magnesium 500 531 106

Manganese 0.0062

Molybdenum 0.0074

Potassium -0.0059

Selenium 0.0009

Silicon 0.0123

Silver 0.0004

Sodium 0.0169

Strontium 0.0022

Thallium 0.0020

Tin -0.0008

Titanium 0.0005

Total Heavy Metals 0.0058

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 246 of 384 01/09/2013
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution AB Solution AB

Lab Sample ID:

TestAmerica Chicago 500-53491-1

ICSAB 500-173964/14

P51226B

mg/L

M12LISBIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium 0.500 0.498 100

Chromium 0.500 0.485 97

Copper 0.500 0.554 111

Lead 0.0500 0.0507 101

Nickel 1.00 0.973 97

Vanadium 0.500 0.506 101

Zinc 1.00 0.929 93

Aluminum 500 497 99

Antimony 0.600 0.597 99

Arsenic 0.100 0.100 100

Beryllium 0.500 0.483 97

Boron 0.0007

Cadmium 1.00 0.949 95

Calcium 500 481 96

Cobalt 0.500 0.486 97

Iron 200 192 96

Magnesium 500 531 106

Manganese 0.500 0.506 101

Molybdenum 0.0063

Potassium -0.0087

Selenium 0.0500 0.0503 101

Silicon 0.0124

Silver 0.200 0.217 109

Sodium 0.0133

Strontium 0.0022

Thallium 0.100 0.104 104

Tin 0.0002

Titanium 0.0005

Total Heavy Metals 4.05 3.94 97

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 247 of 384 01/09/2013
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution A Solution A

Lab Sample ID:

TestAmerica Chicago 500-53491-1

ICSA 500-173963/9

P6122612B.asc

mg/L

M12LISAIC_00001

ICP6

INTERFERENCE CHECK STANDARD

METALS

Barium 0.0001

Chromium 0.0022

Copper 0.0039

Lead 0.0100

Nickel -0.0011

Vanadium 0.0003

Zinc -0.0017

Aluminum 500 503 101

Antimony 0.0032

Arsenic 0.0034

Beryllium 0.0004

Bismuth -0.0092

Boron -0.0007

Cadmium 0.0001

Calcium 500 474 95

Cobalt -0.0027

Iron 200 191 95

Magnesium 500 509 102

Manganese 0.0002

Molybdenum -0.0004

Potassium 0.0024

Selenium -0.0011

Silicon -0.0032

Silver -0.0003

Sodium 0.0378

Strontium 0.0022

Thallium -0.0058

Tin 0.0015

Titanium 0.0033

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 248 of 384 01/09/2013
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution AB Solution AB

Lab Sample ID:

TestAmerica Chicago 500-53491-1

ICSAB 500-173963/10

P6122612B.asc

mg/L

M12LISBIC_00001

ICP6

INTERFERENCE CHECK STANDARD

METALS

Barium 0.500 0.490 98

Chromium 0.500 0.456 91

Copper 0.500 0.524 105

Lead 0.0500 0.0579 116

Nickel 1.00 0.973 97

Vanadium 0.500 0.473 95

Zinc 1.00 0.986 99

Aluminum 500 499 100

Antimony 0.600 0.586 98

Arsenic 0.100 0.0996 100

Beryllium 0.500 0.516 103

Bismuth -0.0099

Boron 0.0003

Cadmium 1.00 0.989 99

Calcium 500 471 94

Cobalt 0.500 0.500 100

Iron 200 189 95

Magnesium 500 506 101

Manganese 0.500 0.464 93

Molybdenum -0.0008

Potassium 0.0015

Selenium 0.0500 0.0482 96

Silicon 0.0007

Silver 0.200 0.210 105

Sodium 0.0388

Strontium 0.0021

Thallium 0.100 0.0851 85

Tin 0.0053

Titanium 0.0045

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 249 of 384 01/09/2013
MATRIX SPIKE SAMPLE RECOVERY

METALS - TCLP

5A-IN

FC D COMPOSITE 6 MS

Lab Name: Job No.:

SDG No.:

Client ID: Lab ID: 500-53491-2 MS

500-53491-1

Matrix: Solid Concentration Units: mg/L

TestAmerica Chicago

% Solids:

Control

Limit

%R Analyte SSR 

C

Sample

Result (SR) 

C

Spike

Added (SA) %R Q Method

Mercury 0.0007703 <0.000200 0.00100 77 50-150 7470A

SSR = Spiked Sample Result

FORM VA - IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 250 of 384 01/09/2013
6-IN

DUPLICATES

FC D COMPOSITE 6 DU

Lab Name: Job No.:

SDG No.:

Matrix: Concentration Units: mg/L

Analyte

Control

Limit Sample (S) 

C

Duplicate (D) 

C

RPD Q Method

500-53491-1

Solid

METALS - TCLP

% Solids for Sample: % Solids for Duplicate:

Client ID: Lab ID: 500-53491-2 DU

TestAmerica Chicago

Mercury 0.000200 <0.000200 0.00004470 J NC 7470A

FORM VI-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 251 of 384 01/09/2013
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-173849/2-A 

Lab Name: Job No.: 500-53491-1

Sample Matrix: Water LCS Source: M12JSPKIC_00002

TestAmerica Chicago

Analyte

Water(mg/L)

True Found C %R Limits Q Method

Barium 2.00 1.902 95 80 120 6010B

Copper 0.250 0.2317 93 80 120 6010B

Chromium 0.200 0.1856 93 80 120 6010B

Nickel 0.500 0.4572 91 80 120 6010B

Lead 0.100 0.09439 94 80 120 6010B

Vanadium 0.500 0.4686 94 80 120 6010B

Zinc 0.500 0.4470 89 80 120 6010B

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 252 of 384 01/09/2013
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-173872/3-A 

Lab Name: Job No.: 500-53491-1

Sample Matrix: Water LCS Source: M12KSPKIC_00001

TestAmerica Chicago

Analyte

Water(mg/L)

True Found C %R Limits Q Method

Barium 2.00 1.928 96 80 120 6010B

Copper 0.250 0.2512 100 80 120 6010B

Chromium 0.200 0.2016 101 80 120 6010B

Nickel 0.500 0.4930 99 80 120 6010B

Lead 0.100 0.1042 104 80 120 6010B

Vanadium 0.500 0.4994 100 80 120 6010B

Zinc 0.500 0.5058 101 80 120 6010B

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 253 of 384 01/09/2013
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-173848/2-A 

Lab Name: Job No.: 500-53491-1

Sample Matrix: Solid LCS Source: M12JSPKIC_00002

TestAmerica Chicago

Analyte

Solid(mg/Kg)

True Found C %R Limits Q Method

Barium 200 200.1 100 80 120 6010B

Copper 25.0 25.74 103 80 120 6010B

Chromium 20.0 20.94 105 80 120 6010B

Nickel 50.0 51.09 102 80 120 6010B

Lead 10.0 10.73 107 80 120 6010B

Vanadium 50.0 51.21 102 80 120 6010B

Zinc 50.0 53.63 107 80 120 6010B

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 254 of 384 01/09/2013
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-173908/8-A 

Lab Name: Job No.: 500-53491-1

Sample Matrix: Water LCS Source: M11FSTKHG_00001

TestAmerica Chicago

Analyte

Water(mg/L)

True Found C %R Limits Q Method

Mercury 0.00200 0.002121 106 80 120 7470A

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 255 of 384 01/09/2013
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-173909/8-A 

Lab Name: Job No.: 500-53491-1

Sample Matrix: Water LCS Source: M11FSTKHG_00001

TestAmerica Chicago

Analyte

Water(mg/L)

True Found C %R Limits Q Method

Mercury 0.00200 0.002139 107 80 120 7470A

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 256 of 384 01/09/2013
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-173881/8-A 

Lab Name: Job No.: 500-53491-1

Sample Matrix: Solid LCS Source: M11FSTKHG_00001

TestAmerica Chicago

Analyte

Solid(mg/Kg)

True Found C %R Limits Q Method

Mercury 0.167 0.1600 96 80 120 7471A

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 257 of 384 01/09/2013
9-IN

Instrument ID: ICP5

Job Number: 500-53491-1

Matrix: Solid

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

DETECTION LIMITS

Method: 6010B MDL Date: 02/20/2012 13:20

Prep Method: 3050B

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

Barium 1 0.119

Chromium 1 0.167

Copper 1 0.271

Lead 0.5 0.172

Nickel 1 0.219

Vanadium 0.5 0.0759

Zinc 2 0.686

FORM IX - IN

Page 258 of 384 01/09/2013
9-IN

Instrument ID: ICP5

Job Number: 500-53491-1

Matrix: Solid

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 6010B XMDL Date: 05/25/2006 09:03

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Barium 0.01 0.005

Chromium 0.01 0.005

Copper 0.01 0.005

Lead 0.005 0.0025

Nickel 0.01 0.005

Vanadium 0.005 0.0025

Zinc 0.02 0.01

FORM IX - IN

Page 259 of 384 01/09/2013
9-IN

Instrument ID: ICP6

Job Number: 500-53491-1

Matrix: Water

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

DETECTION LIMITS

Method: 6010B MDL Date: 02/20/2012 13:03

Prep Method: 3010A

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Barium 0.01 0.00044

Chromium 0.01 0.00096

Copper 0.01 0.00106

Lead 0.005 0.00158

Nickel 0.01 0.0019

Vanadium 0.005 0.00062

Zinc 0.02 0.00472

FORM IX - IN

Page 260 of 384 01/09/2013
9-IN

Instrument ID: ICP6

Job Number: 500-53491-1

Matrix: Water

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 6010B XMDL Date: 05/25/2006 09:07

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Barium 0.01 0.005

Chromium 0.01 0.005

Copper 0.01 0.005

Lead 0.005 0.0025

Nickel 0.01 0.005

Vanadium 0.005 0.0025

Zinc 0.02 0.01

FORM IX - IN

Page 261 of 384 01/09/2013
9-IN

Instrument ID: ICP5

Job Number: 500-53491-1

Matrix: Solid

SDG Number:

Lab Name:

METALS - TCLP

TestAmerica Chicago

DETECTION LIMITS

Method: 6010B MDL Date: 11/01/2005 15:36

Prep Method: 3010A

Leach Method: 1311

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Barium 0.5 0.01

Chromium 0.025 0.01

Copper 0.025 0.01

Lead 0.05 0.005

Nickel 0.025 0.01

Vanadium 0.025 0.005

Zinc 0.1 0.02

FORM IX - IN

Page 262 of 384 01/09/2013
9-IN

Instrument ID: ICP5

Job Number: 500-53491-1

Matrix: Solid

SDG Number:

Lab Name:

METALS - TCLP

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 6010B XMDL Date: 01/28/2008 10:37

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Barium 0.01 0.01

Chromium 0.01 0.01

Copper 0.01 0.01

Lead 0.005 0.005

Nickel 0.01 0.01

Vanadium 0.005 0.005

Zinc 0.02 0.02

FORM IX - IN

Page 263 of 384 01/09/2013
9-IN

Instrument ID: HG6

Job Number: 500-53491-1

Matrix: Water

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

DETECTION LIMITS

Method: 7470A MDL Date: 08/31/2012 10:08

Prep Method: 7470A

Analyte Wavelength/

Mass

RL MDL

(ug/L) (ug/L)

Mercury 0.2 0.071

FORM IX - IN

Page 264 of 384 01/09/2013
9-IN

Instrument ID: HG6

Job Number: 500-53491-1

Matrix: Water

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 7470A XMDL Date: 08/31/2012 10:08

Analyte Wavelength/

Mass

XRL XMDL

(ug/L) (ug/L)

Mercury 0.2 0.071

FORM IX - IN

Page 265 of 384 01/09/2013
9-IN

Instrument ID: HG6

Job Number: 500-53491-1

Matrix: Solid

SDG Number:

Lab Name:

METALS - TCLP

TestAmerica Chicago

DETECTION LIMITS

Method: 7470A MDL Date: 11/01/2005 11:39

Prep Method: 7470A

Leach Method: 1311

Analyte Wavelength/

Mass

RL MDL

(ug/L) (ug/L)

Mercury 2 0.2

FORM IX - IN

Page 266 of 384 01/09/2013
9-IN

Instrument ID: HG6

Job Number: 500-53491-1

Matrix: Solid

SDG Number:

Lab Name:

METALS - TCLP

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 7470A XMDL Date: 09/16/2006 08:48

Analyte Wavelength/

Mass

XRL XMDL

(ug/L) (ug/L)

Mercury 2 1

FORM IX - IN

Page 267 of 384 01/09/2013
9-IN

Instrument ID: HG5

Job Number: 500-53491-1

Matrix: Solid

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

DETECTION LIMITS

Method: 7471A MDL Date: 08/31/2012 10:15

Prep Method: 7471A

Analyte Wavelength/

Mass

RL MDL

(ug/Kg) (ug/Kg)

Mercury 16.7 6.37

FORM IX - IN

Page 268 of 384 01/09/2013
9-IN

Instrument ID: HG5

Job Number: 500-53491-1

Matrix: Solid

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 7471A XMDL Date: 08/31/2012 10:16

Analyte Wavelength/

Mass

XRL XMDL

(ug/L) (ug/L)

Mercury 0.2 0.071

FORM IX - IN

Page 269 of 384 01/09/2013
11-IN

Lab Name: TestAmerica Chicago Job No: 500-53491-1

Instrument ID: Date:

Analyte

Integ.

Time

(Sec.)

Concentration

Method

LINEAR RANGES

ICP5

SDG No.:

(mg/L)

11/19/2012 14:31

METALS

Barium 20 6010B

Copper 20 6010B

Chromium 50 6010B

Nickel 50 6010B

Lead 50 6010B

Vanadium 100 6010B

Zinc 20 6010B

FORM XI - IN

Page 270 of 384 01/09/2013
11-IN

Lab Name: TestAmerica Chicago Job No: 500-53491-1

Instrument ID: Date:

Analyte

Integ.

Time

(Sec.)

Concentration

Method

LINEAR RANGES

ICP6

SDG No.:

(mg/L)

11/19/2012 14:24

METALS

Barium 20 6010B

Copper 20 6010B

Chromium 20 6010B

Nickel 20 6010B

Lead 100 6010B

Vanadium 20 6010B

Zinc 20 6010B

FORM XI - IN

Page 271 of 384 01/09/2013
11-IN

Lab Name: TestAmerica Chicago Job No: 500-53491-1

Instrument ID: Date:

Analyte

Integ.

Time

(Sec.)

Concentration

Method

LINEAR RANGES

HG5

SDG No.:

(ug/L)

03/01/2008 11:18

METALS

Mercury 5.0 7471A

FORM XI - IN

Page 272 of 384 01/09/2013
11-IN

Lab Name: TestAmerica Chicago Job No: 500-53491-1

Instrument ID: Date:

Analyte

Integ.

Time

(Sec.)

Concentration

Method

LINEAR RANGES

HG6

SDG No.:

(ug/L)

11/01/2010 11:39

METALS

Mercury 5.0 7470A

FORM XI - IN

Page 273 of 384 01/09/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53491-1

METALS

TestAmerica Chicago

Prep Method: 3050B

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-173848/1-A 12/24/2012 15:00 173848 1 100

LCS 500-173848/2-A 12/24/2012 15:00 173848 1 100

500-53491-1 12/24/2012 15:00 173848 1.0213 100

500-53491-2 12/24/2012 15:00 173848 1.0382 100

FORM XII-IN

Page 274 of 384 01/09/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53491-1

METALS

TestAmerica Chicago

Prep Method: 3010A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-173849/1-A 12/24/2012 14:30 173849 50 50

LCS 500-173849/2-A 12/24/2012 14:30 173849 50 50

500-53491-5 12/24/2012 14:30 173849 50 50

FORM XII-IN

Page 275 of 384 01/09/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53491-1

METALS

TestAmerica Chicago

Prep Method: 3010A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

LB 500-173836/1-B 12/26/2012 07:50 173872 50 50

LB2 500-173838/1-B 12/26/2012 07:50 173872 50 50

LCS 500-173872/3-A 12/26/2012 07:50 173872 50 50

500-53491-1 12/26/2012 07:50 173872 50 50

500-53491-2 12/26/2012 07:50 173872 50 50

FORM XII-IN

Page 276 of 384 01/09/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53491-1

METALS

TestAmerica Chicago

Prep Method: 7471A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-173881/7-A 12/26/2012 14:00 173881 0.6 50

LCS 500-173881/8-A 12/26/2012 14:00 173881 0.6 50

500-53491-1 12/26/2012 14:00 173881 0.6259 50

500-53491-2 12/26/2012 14:00 173881 0.6177 50

FORM XII-IN

Page 277 of 384 01/09/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53491-1

METALS

TestAmerica Chicago

Prep Method: 7470A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-173908/7-A 12/26/2012 13:00 173908 25 25

LCS 500-173908/8-A 12/26/2012 13:00 173908 25 25

500-53491-5 12/26/2012 13:00 173908 25 25

FORM XII-IN

Page 278 of 384 01/09/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53491-1

METALS

TestAmerica Chicago

Prep Method: 7470A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-173909/7-A 12/26/2012 13:00 173909 25 25

LCS 500-173909/8-A 12/26/2012 13:00 173909 25 25

LB 500-173836/1-C 12/26/2012 13:00 173909 25 25

LB2 500-173838/1-C 12/26/2012 13:00 173909 25 25

500-53491-1 12/26/2012 13:00 173909 25 25

500-53491-2 12/26/2012 13:00 173909 25 25

500-53491-2 DU 12/26/2012 13:00 173909 25 25

500-53491-2 MS 12/26/2012 13:00 173909 25 25

FORM XII-IN

Page 279 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

ICP5

12/26/2012 15:16 12/27/2012 00:22

6010B

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

B

a

C

r

C

u

N

i

P

b

V Z

n

T

y

p

e

ZZZZZZ 15:16

ZZZZZZ 15:23

ZZZZZZ 15:29

ZZZZZZ 15:35

ZZZZZZ 15:41

ZZZZZZ 15:54

ZZZZZZ 16:00

ZZZZZZ 16:07

ZZZZZZ 16:15

ICV 500-173964/10 1 16:24 X X X X X X X

ICB 500-173964/11 1 16:32 X X X X X X X

CRI 500-173964/12 1 16:39 X X X X X X X

ICSA 500-173964/13 1 16:45 X X X X X X X

ICSAB 500-173964/14 1 16:51 X X X X X X X

CCV 500-173964/15 1 16:59 X X X X X X X

CCB 500-173964/16 1 17:06 X X X X X X X

LB 500-173836/1-B 1 P 17:12 X X X X X X X

LB2 500-173838/1-B 1 P 17:18 X X X X X X X

LCS 500-173872/3-A 1 T 17:24 X X X X X X X

ZZZZZZ 17:31

ZZZZZZ 17:37

ZZZZZZ 17:43

ZZZZZZ 17:49

ZZZZZZ 17:55

ZZZZZZ 18:01

ZZZZZZ 18:08

CCV 500-173964/27 1 18:16 X X X X X X X

CCB 500-173964/28 1 18:22 X X X X X X X

ZZZZZZ 18:29

ZZZZZZ 18:35

500-53491-1 1 P 18:41 X X X X X X X

500-53491-2 1 P 18:47 X X X X X X X

ZZZZZZ 18:53

ZZZZZZ 19:04

ZZZZZZ 19:10

ZZZZZZ 19:16

ZZZZZZ 19:23

ZZZZZZ 19:29

CCV 500-173964/39 1 19:37 X X X X X X X

CCB 500-173964/40 1 19:43 X X X X X X X

ZZZZZZ 19:50

ZZZZZZ 19:56

FORM XIII-IN Page 280 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

ICP5

12/26/2012 15:16 12/27/2012 00:22

6010B

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

B

a

C

r

C

u

N

i

P

b

V Z

n

T

y

p

e

ZZZZZZ 20:02

ZZZZZZ 20:08

ZZZZZZ 20:14

ZZZZZZ 20:21

ZZZZZZ 20:27

ZZZZZZ 20:33

ZZZZZZ 20:39

ZZZZZZ 20:45

CCV 500-173964/51 1 20:54 X X X X X X X

CCB 500-173964/52 1 21:00 X X X X X X X

ZZZZZZ 21:06

ZZZZZZ 21:13

ZZZZZZ 21:19

ZZZZZZ 21:25

ZZZZZZ 21:31

ZZZZZZ 21:37

ZZZZZZ 21:44

MB 500-173848/1-A 1 T 21:54 X X X X X X X

LCS 500-173848/2-A 1 T 22:00 X X X X X X X

ZZZZZZ 22:07

CCV 500-173964/63 1 22:15 X X X X X X X

CCB 500-173964/64 1 22:21 X X X X X X X

ZZZZZZ 22:28

ZZZZZZ 22:34

ZZZZZZ 22:40

ZZZZZZ 22:46

ZZZZZZ 22:53

ZZZZZZ 22:59

ZZZZZZ 23:05

ZZZZZZ 23:11

ZZZZZZ 23:17

ZZZZZZ 23:24

CCV 500-173964/75 1 23:32 X X X X X X X

CCB 500-173964/76 1 23:38 X X X X X X X

ZZZZZZ 23:44

ZZZZZZ 23:51

500-53491-1 1 T 23:57 X X X X X X X

500-53491-2 1 T 00:03 X X X X X X X

ZZZZZZ 00:09

CCV 500-173964/82 1 00:15 X X X X X X X

CCB 500-173964/83 1 00:22 X X X X X X X FORM XIII-IN Page 281 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

ICP5

12/26/2012 15:16 12/27/2012 00:22

6010B

METALS

Prep Types

P = TCLP

T = Total/NA

FORM XIII-IN Page 282 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

ICP6

12/26/2012 14:04 12/26/2012 18:46

6010B

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

B

a

C

r

C

u

N

i

P

b

V Z

n

T

y

p

e

ZZZZZZ 14:04

ZZZZZZ 14:08

ZZZZZZ 14:12

ZZZZZZ 14:16

ZZZZZZ 14:20

ICV 500-173963/6 1 14:24 X X X X X X X

ICB 500-173963/7 1 14:28 X X X X X X X

CRI 500-173963/8 1 14:32 X X X X X X X

ICSA 500-173963/9 1 14:36 X X X X X X X

ICSAB 500-173963/10 1 14:41 X X X X X X X

CCV 500-173963/11 14:46

CCB 500-173963/12 14:50

ZZZZZZ 14:54

ZZZZZZ 14:58

ZZZZZZ 15:02

ZZZZZZ 15:07

ZZZZZZ 15:12

ZZZZZZ 15:17

ZZZZZZ 15:21

ZZZZZZ 15:25

ZZZZZZ 15:29

ZZZZZZ 15:33

CCV 500-173963/23 15:37

CCB 500-173963/24 15:41

ZZZZZZ 15:45

ZZZZZZ 15:49

ZZZZZZ 15:53

ZZZZZZ 15:58

ZZZZZZ 16:04

ZZZZZZ 16:08

ZZZZZZ 16:12

ZZZZZZ 16:16

ZZZZZZ 16:20

ZZZZZZ 16:24

CCV 500-173963/35 1 16:28 X X X X X X X

CCB 500-173963/36 1 16:32 X X X X X X X

MB 500-173849/1-A 1 T 16:35 X X X X X X X

LCS 500-173849/2-A 1 T 16:39 X X X X X X X

ZZZZZZ 16:43

ZZZZZZ 16:47

ZZZZZZ 16:51

ZZZZZZ 16:55

FORM XIII-IN Page 283 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

ICP6

12/26/2012 14:04 12/26/2012 18:46

6010B

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

B

a

C

r

C

u

N

i

P

b

V Z

n

T

y

p

e

ZZZZZZ 16:59

500-53491-5 1 T 17:03 X X X X X X X

ZZZZZZ 17:07

ZZZZZZ 17:13

CCV 500-173963/47 1 17:18 X X X X X X X

CCB 500-173963/48 1 17:21 X X X X X X X

ZZZZZZ 17:26

ZZZZZZ 17:30

ZZZZZZ 17:34

ZZZZZZ 17:38

ZZZZZZ 17:42

ZZZZZZ 17:46

ZZZZZZ 17:50

ZZZZZZ 17:54

ZZZZZZ 17:58

ZZZZZZ 18:02

CCV 500-173963/59 18:06

CCB 500-173963/60 18:10

ZZZZZZ 18:13

ZZZZZZ 18:17

ZZZZZZ 18:21

ZZZZZZ 18:25

ZZZZZZ 18:29

ZZZZZZ 18:33

ZZZZZZ 18:38

CCV 500-173963/68 18:42

CCB 500-173963/69 18:46

Prep Types

T = Total/NA

FORM XIII-IN Page 284 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

HG6

12/27/2012 08:23 12/27/2012 10:14

7470A

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

H

g

T

y

p

e

ZZZZZZ 08:23

ZZZZZZ 08:25

ZZZZZZ 08:27

ZZZZZZ 08:28

ZZZZZZ 08:30

ZZZZZZ 08:32

ICV 500-173997/7 1 08:35 X

ICB 500-173997/8 1 08:37 X

CRA 500-173997/9 1 08:39 X

MB 500-173908/7-A 1 T 08:41 X

LCS 500-173908/8-A 1 T 08:43 X

ZZZZZZ 08:45

ZZZZZZ 08:47

ZZZZZZ 08:49

ZZZZZZ 08:50

ZZZZZZ 08:53

ZZZZZZ 08:54

ZZZZZZ 08:56

CCV 500-173997/19 1 08:58 X

CCB 500-173997/20 1 09:00 X

ZZZZZZ 09:02

ZZZZZZ 09:04

ZZZZZZ 09:06

ZZZZZZ 09:08

ZZZZZZ 09:09

ZZZZZZ 09:11

ZZZZZZ 09:13

ZZZZZZ 09:15

ZZZZZZ 09:17

ZZZZZZ 09:19

CCV 500-173997/31 1 09:21 X

CCB 500-173997/32 1 09:22 X

ZZZZZZ 09:24

500-53491-5 1 T 09:26 X

MB 500-173909/7-A 1 T 09:28 X

LCS 500-173909/8-A 1 T 09:30 X

ZZZZZZ 09:32

ZZZZZZ 09:34

ZZZZZZ 09:36

ZZZZZZ 09:38

ZZZZZZ 09:40

ZZZZZZ 09:42

FORM XIII-IN Page 285 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

HG6

12/27/2012 08:23 12/27/2012 10:14

7470A

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

H

g

T

y

p

e

CCV 500-173997/43 1 09:43 X

CCB 500-173997/44 1 09:45 X

ZZZZZZ 09:47

LB 500-173836/1-C 1 P 09:49 X

LB2 500-173838/1-C 1 P 09:51 X

ZZZZZZ 09:53

ZZZZZZ 09:55

500-53491-1 1 P 09:57 X

500-53491-2 1 P 09:58 X

500-53491-2 DU 1 P 10:00 X

500-53491-2 MS 1 P 10:02 X

CCV 500-173997/54 1 10:04 X

CCB 500-173997/55 1 10:06 X

ZZZZZZ 10:08

ZZZZZZ 10:10

CCV 500-173997/58 10:12

CCB 500-173997/59 10:14

Prep Types

P = TCLP

T = Total/NA

FORM XIII-IN Page 286 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

HG5

12/27/2012 07:59 12/27/2012 09:10

7471A

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

H

g

T

y

p

e

STD01REP1 07:59 X

500-173984/1 IC 

STD02REP1 08:01 X

500-173984/2 IC 

STD03REP1 08:03 X

500-173984/3 IC 

STD04REP1 08:05 X

500-173984/4 IC 

STD05REP1 08:07 X

500-173984/5 IC 

STD06REP1 08:09 X

500-173984/6 IC 

ICV 500-173984/7 1 08:12 X

ICB 500-173984/8 1 08:14 X

CRA 500-173984/9 1 08:15 X

MB 500-173881/7-A 1 T 08:17 X

LCS 500-173881/8-A 1 T 08:19 X

ZZZZZZ 08:21

ZZZZZZ 08:23

ZZZZZZ 08:25

ZZZZZZ 08:27

ZZZZZZ 08:28

ZZZZZZ 08:30

ZZZZZZ 08:32

CCV 500-173984/19 1 08:34 X

CCB 500-173984/20 1 08:36 X

ZZZZZZ 08:38

ZZZZZZ 08:40

ZZZZZZ 08:42

ZZZZZZ 08:44

ZZZZZZ 08:46

ZZZZZZ 08:48

ZZZZZZ 08:49

ZZZZZZ 08:51

ZZZZZZ 08:53

500-53491-1 1 T 08:55 X

CCV 500-173984/31 08:57

CCV 500-173984/32 1 09:01 X

CCB 500-173984/33 1 09:03 X

500-53491-2 1 T 09:04 X

ZZZZZZ 09:06

CCV 500-173984/36 1 09:08 X

CCB 500-173984/37 1 09:10 X FORM XIII-IN Page 287 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

HG5

12/27/2012 07:59 12/27/2012 09:10

7471A

METALS

Prep Types

T = Total/NA

FORM XIII-IN Page 288 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Laird, Rebecca

12/24/12 15:30

173848 12/24/12 15:00

Batch Method:

TestAmerica Chicago

3050B

Lab Sample ID Client Sample ID Method Chain Basis CalcMsg InitialAmount FinalAmount M12JSPKIC 00002

CALC NOT SET TO 

RUN

MB 500-173848/1 3050B, 6010B 1 g 100 mL

CALC NOT SET TO 

RUN

LCS 1 g 100 mL 1 mL

500-173848/2

3050B, 6010B

FC COMPOSITE 6 CALC NOT SET TO 

RUN

500-53491-A-1 3050B, 6010B T 1.0213 g 100 mL

FC D COMPOSITE 6 CALC NOT SET TO 

RUN

500-53491-A-2 3050B, 6010B T 1.0382 g 100 mL

Batch Notes

Analyst BL

Balance ID C-1966

First End time 1530

Hydrogen peroxide lot number L08A06

Lot # of hydrochloric acid 0000013500

Lot # of Nitric Acid L10022

Hood ID or number 3

Hot Block ID number 8

Oven, Bath or Block Temperature 1 90 Degrees C

Oven, Bath or Block Temperature 2 90 Degrees C

Pipette ID 1628

First Start time 1500

ID number of the thermometer J59717

Digestion Tube/Cup Lot # MF06LKK01

Basis Basis Description

T Total/NA

6010B Page 1 of 1

Page 289 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Laird, Rebecca

12/24/12 15:00

173849 12/24/12 14:30

Batch Method:

TestAmerica Chicago

3010A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount M12JSPKIC 00002

MB 500-173849/1 3010A, 6010B 50 mL 50 mL

LCS 50 mL 50 mL 0.5 mL

500-173849/2

3010A, 6010B

500-53491-E-5 FC EB 6 3010A, 6010B T 50 mL 50 mL

Batch Notes

First End time 1500

Lot # of hydrochloric acid 0000007153

Lot # of Nitric Acid L08022

Hot Block ID number 4

Pipette ID 1627

First Start time 1430

ID number of the thermometer J59688

Digestion Tube/Cup Lot # 20313760

Uncorrected Temperature 90 Celsius

Uncorrected Temperature 2 90 Celsius

Basis Basis Description

T Total/NA

6010B Page 1 of 1

Page 290 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Hudson, Lawrence A

12/26/12 08:20

173872 12/26/12 07:50

Batch Method:

TestAmerica Chicago

3010A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount M12KSPKIC 00001 AnalysisComment

LB 50 mL 50 mL t757

500-173836/1-A

3010A, 6010B

LB2 50 mL 50 mL t757

500-173838/1-A

3010A, 6010B

LCS 50 mL 50 mL 0.5 mL

500-173872/3

3010A, 6010B

500-53491-A-1-B FC COMPOSITE 6 3010A, 6010B P 50 mL 50 mL LB2

500-53491-A-2-B FC D COMPOSITE 6 3010A, 6010B P 50 mL 50 mL

Batch Notes

Batch Comment T-757

First End time 0820

Lot # of hydrochloric acid 0000013500

Lot # of Nitric Acid L10022

Hot Block ID number 4

Pipette ID 1627

First Start time 0750

ID number of the thermometer J59688

Digestion Tube/Cup Lot # 20313760

Uncorrected Temperature 90 Celsius

Uncorrected Temperature 2 90 Celsius

Basis Basis Description

P TCLP

6010B Page 1 of 1

Page 291 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Bills, Brandon J

12/26/12 15:00

173908 12/26/12 13:00

Batch Method:

TestAmerica Chicago

7470A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount M11FSTKHG 00001

MB 500-173908/7 7470A, 7470A 25 mL 25 mL

LCS 25 mL 25 mL 0.00005 mL

500-173908/8

7470A, 7470A

500-53491-E-5 FC EB 6 7470A, 7470A T 25 mL 25 mL

Batch Notes

Hydroxylamine Hydrochloride Lot 19333

Batch Comment STOCK ID: m10cstkhg_00001, m12astkhg_00001 

(Curve)

Sulfuric Acid Lot Number k20042

Lot # of hydrochloric acid 0000007153

Lot # of Nitric Acid L03021

Hood ID or number c0454

Hot Block ID number 6

Potassium Persulfate Lot Number k43467

Potassium Permanganate Lot Number k35621

NaCL Lot # UF30BZEMS

Oven, Bath or Block Temperature 1 88

Oven, Bath or Block Temperature 2 88

Pipette ID 2240

Repittetor Volume Check OK

Stannous Chloride Lot Number k21597

Temperature 88 Celsius

ID number of the thermometer hb305412

Digestion Tube/Cup Lot # 1207143

Uncorrected Temperature 90 Celsius

Visual ck - digestate F.V. consistency OK

Basis Basis Description

T Total/NA

7470A Page 1 of 1

Page 292 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Bills, Brandon J

12/27/12 09:30

173909 12/27/12 07:30

Batch Method:

TestAmerica Chicago

7470A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount M11FSTKHG 00001 M12ASTKHG 00001

MB 500-173909/7 7470A, 7470A 25 mL 25 mL

LCS 25 mL 25 mL 0.00005 mL

500-173909/8

7470A, 7470A

LB 25 mL 25 mL

500-173836/1-A

7470A, 7470A

LB2 25 mL 25 mL

500-173838/1-A

7470A, 7470A

500-53491-A-1-B FC COMPOSITE 6 7470A, 7470A P 25 mL 25 mL

500-53491-A-2-B FC D COMPOSITE 6 7470A, 7470A P 25 mL 25 mL

500-53491-A-2-B FC D COMPOSITE 6 25 mL 25 mL

DU

7470A, 7470A P

500-53491-A-2-B FC D COMPOSITE 6 25 mL 25 mL 0.000025 mL

MS

7470A, 7470A P

7470A Page 1 of 2

Page 293 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Bills, Brandon J

12/27/12 09:30

173909 12/27/12 07:30

Batch Method:

TestAmerica Chicago

7470A

Batch Notes

Hydroxylamine Hydrochloride Lot 19333

Batch Comment STOCK ID: m10cstkhg_00001, m12astkhg_00001 

(Curve)

Sulfuric Acid Lot Number k20042

Lot # of hydrochloric acid 0000007153

Lot # of Nitric Acid L03021

Hood ID or number c0454

Hot Block ID number 6

Potassium Persulfate Lot Number k43467

Potassium Permanganate Lot Number k35621

NaCL Lot # UF30BZEMS

Oven, Bath or Block Temperature 1 88

Oven, Bath or Block Temperature 2 88

Pipette ID 2240

Repittetor Volume Check OK

Stannous Chloride Lot Number k21597

Temperature 88 Celsius

ID number of the thermometer hb305412

Digestion Tube/Cup Lot # 1207143

Uncorrected Temperature 90 Celsius

Visual ck - digestate F.V. consistency OK

Basis Basis Description

P TCLP

7470A Page 2 of 2

Page 294 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Bills, Brandon J

12/26/12 14:30

173881 12/26/12 14:00

Batch Method:

TestAmerica Chicago

7471A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount M11FSTKHG 00001

MB 500-173881/7 7471A, 7471A 0.6 g 50 mL

LCS 0.6 g 50 mL 0.0001 mL

500-173881/8

7471A, 7471A

500-53491-A-1 FC COMPOSITE 6 7471A, 7471A T 0.6259 g 50 mL

500-53491-A-2 FC D COMPOSITE 6 7471A, 7471A T 0.6177 g 50 mL

Batch Notes

Hydroxylamine Hydrochloride Lot 19333

Balance ID c0975

Batch Comment STOCK ID: m10cstkhg_00001, m12astkhg_00001 

(Curve)

Blank Soil Lot Number teflon strip_00001

Filter Lot # 21782182

Sulfuric Acid Lot Number k20042

Lot # of hydrochloric acid 0000007153

Lot # of Nitric Acid L03021

Hood ID or number c0454

Hot Block ID number 2

Potassium Persulfate Lot Number k43467

Potassium Permanganate Lot Number k35621

NaCL Lot # UF30BZEMS

Oven, Bath or Block Temperature 1 90

Oven, Bath or Block Temperature 2 90

Pipette ID 1631

Repittetor Volume Check OK

Stannous Chloride Lot Number k21597

Syringe Lot # 1292669

ID number of the thermometer j60025

Digestion Tube/Cup Lot # 1207143

Uncorrected Temperature 90 Celsius

Uncorrected Temperature 2 90 Celsius

7471A Page 1 of 2

Page 295 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Bills, Brandon J

12/26/12 14:30

173881 12/26/12 14:00

Batch Method:

TestAmerica Chicago

7471A

Basis Basis Description

T Total/NA

7471A Page 2 of 2

Page 296 of 384 01/09/2013
GENERAL CHEMISTRY

Page 297 of 384 01/09/2013
COVER PAGE

Lab Name: Job Number: 

Client Sample ID Lab Sample ID

GENERAL CHEMISTRY

Project: John Deere Des Moines Works (JDDMW)

SDG No.:

TestAmerica Chicago 500-53491-1

FC COMPOSITE 6 500-53491-1 

FC D COMPOSITE 6 500-53491-2 

FC DISCRETE 6 500-53491-3 

FC D DISCRETE 6 500-53491-4 

FC EB 6 500-53491-5 

Comments:

Page 298 of 384 01/09/2013
1B-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53491-1

Date Received: 12/22/2012 11:30

500-53491-1

FC COMPOSITE 6

Solid Date Sampled: 12/19/2012 14:30

Reporting Basis: DRY

GENERAL CHEMISTRY

TestAmerica Chicago

% Solids: 26.5

CAS No. Analyte Result RL MDL Units C Q DIL Method

18540-29-9 Chromium, hexavalent <3.75 3.75 1.46 mg/Kg 1 7196A

57-12-5 Cyanide, Total 1.15 1.88 0.622 mg/Kg J 1 9014

18496-25-8 Sulfide 778 90.4 14.5 mg/Kg 1 9034

HEM (Oil & Grease) 16600 1850 822 mg/Kg 1 9071B

FORM IB-IN Page 299 of 384 01/09/2013
1B-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53491-1

Date Received: 12/22/2012 11:30

500-53491-1

FC COMPOSITE 6

Solid Date Sampled: 12/19/2012 14:30

Reporting Basis: WET

GENERAL CHEMISTRY

TestAmerica Chicago

CAS No. Analyte Result RL MDL Units C Q DIL Method

Sulfide, Reactive <48.5 48.5 3.78 mg/Kg 1 9034

Flashpoint >176 Degrees 

F

40.0 40.0 1 1010

pH 9.79 0.200 0.200 SU 1 9045C

% Moisture 74.0 0.100 0.100 % 1 SM 2540G

Total Solids 26.0 0.100 0.100 % 1 SM 2540G

FORM IB-IN Page 300 of 384 01/09/2013
1B-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53491-2

Date Received: 12/22/2012 11:30

500-53491-1

FC D COMPOSITE 6

Solid Date Sampled: 12/19/2012 14:40

Reporting Basis: DRY

GENERAL CHEMISTRY

TestAmerica Chicago

% Solids: 25.1

CAS No. Analyte Result RL MDL Units C Q DIL Method

18540-29-9 Chromium, hexavalent <3.99 3.99 1.55 mg/Kg 1 7196A

57-12-5 Cyanide, Total 1.29 1.86 0.615 mg/Kg J 1 9014

18496-25-8 Sulfide 817 94.0 15.0 mg/Kg 1 9034

HEM (Oil & Grease) 17000 1950 866 mg/Kg 1 9071B

FORM IB-IN Page 301 of 384 01/09/2013
1B-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53491-2

Date Received: 12/22/2012 11:30

500-53491-1

FC D COMPOSITE 6

Solid Date Sampled: 12/19/2012 14:40

Reporting Basis: WET

GENERAL CHEMISTRY

TestAmerica Chicago

CAS No. Analyte Result RL MDL Units C Q DIL Method

Sulfide, Reactive <49.3 49.3 3.85 mg/Kg 1 9034

Flashpoint >176 Degrees 

F

40.0 40.0 1 1010

pH 9.87 0.200 0.200 SU 1 9045C

% Moisture 75.0 0.100 0.100 % 1 SM 2540G

Total Solids 25.0 0.100 0.100 % 1 SM 2540G

FORM IB-IN Page 302 of 384 01/09/2013
1B-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53491-5

Date Received: 12/22/2012 11:30

500-53491-1

FC EB 6

Water Date Sampled: 12/19/2012 14:10

Reporting Basis: WET

GENERAL CHEMISTRY

TestAmerica Chicago

CAS No. Analyte Result RL MDL Units C Q DIL Method

18540-29-9 Chromium, hexavalent <0.0100 0.0100 0.00325 mg/L H 1 7196A

57-12-5 Cyanide, Total <0.0100 0.0100 0.00331 mg/L 1 9014

Sulfide, Reactive <1.00 1.00 1.00 mg/L 1 9034

HEM (Oil & Grease) <5.33 5.33 1.55 mg/L 1 1664A

18496-25-8 Sulfide <1.00 1.00 0.230 mg/L 1 9034

FORM IB-IN Page 303 of 384 01/09/2013
2-IN

Lab Name: Job No.:

SDG No.:

500-53491-1

Analyst: APW Batch Start Date: 12/22/2012

Reporting Units: mg/L Analytical Batch No.: 173793

CALIBRATION QUALITY CONTROL

GENERAL CHEMISTRY

Sample

Number

QC 

Type Time Analyte Result

Spike

Amount

(%)

Recovery Limits Qual Reagent

TestAmerica Chicago

 1 ICV 14:10 Chromium, hexavalent 0.2586 0.250 103 90-110 WSTCR2_00008

 2 ICB 14:10 Chromium, hexavalent <0.0100

 9 CCV 14:14 Chromium, hexavalent 0.4955 0.500 99 90-110 WSTCR1_00008

 10 CCB 14:14 Chromium, hexavalent <0.0100

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 304 of 384 01/09/2013
2-IN

Lab Name: Job No.:

SDG No.:

500-53491-1

Analyst: APW Batch Start Date: 12/27/2012

Reporting Units: mg/L Analytical Batch No.: 174027

CALIBRATION QUALITY CONTROL

GENERAL CHEMISTRY

Sample

Number

QC 

Type Time Analyte Result

Spike

Amount

(%)

Recovery Limits Qual Reagent

TestAmerica Chicago

 1 ICV 12:40 Chromium, hexavalent 0.2548 0.250 102 90-110 WSTCR2_00008

 2 ICB 12:40 Chromium, hexavalent <0.0200

 10 CCV 12:46 Chromium, hexavalent 0.5130 0.500 103 90-110 WSTCR1_00008

 11 CCB 12:46 Chromium, hexavalent <0.0200

 18 CCV 12:51 Chromium, hexavalent 0.5138 0.500 103 90-110 WSTCR1_00008

 19 CCB 12:52 Chromium, hexavalent <0.0200

 27 CCV 12:57 Chromium, hexavalent 0.5169 0.500 103 90-110 WSTCR1_00008

 28 CCB 12:58 Chromium, hexavalent <0.0200

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 305 of 384 01/09/2013
2-IN

Lab Name: Job No.:

SDG No.:

500-53491-1

Analyst: EAT Batch Start Date: 12/27/2012

Reporting Units: mg/L Analytical Batch No.: 174042

CALIBRATION QUALITY CONTROL

GENERAL CHEMISTRY

Sample

Number

QC 

Type Time Analyte Result

Spike

Amount

(%)

Recovery Limits Qual Reagent

TestAmerica Chicago

 1 ICV 14:40 Cyanide, Total 0.1006 0.100 101 90-110 WSTINCN2_00563

 2 ICB 14:40 Cyanide, Total <0.0100

 13 CCV 14:43 Cyanide, Total 0.1942 0.200 97 90-110 WSTINCN1_00571

 14 CCB 14:43 Cyanide, Total <0.0100

 25 CCV 14:47 Cyanide, Total 0.1938 0.200 97 90-110 WSTINCN1_00571

 26 CCB 14:47 Cyanide, Total <0.0100

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 306 of 384 01/09/2013
2-IN

Lab Name: Job No.:

SDG No.:

500-53491-1

Analyst: EAT Batch Start Date: 12/28/2012

Reporting Units: mg/L Analytical Batch No.: 174173

CALIBRATION QUALITY CONTROL

GENERAL CHEMISTRY

Sample

Number

QC 

Type Time Analyte Result

Spike

Amount

(%)

Recovery Limits Qual Reagent

TestAmerica Chicago

 1 ICV 15:25 Cyanide, Total 0.1017 0.100 102 90-110 WSTINCN2_00564

 2 ICB 15:25 Cyanide, Total <0.0100

 13 CCV 15:29 Cyanide, Total 0.1954 0.200 98 90-110 WSTINCN1_00572

 14 CCB 15:29 Cyanide, Total <0.0100

 25 CCV 15:33 Cyanide, Total 0.1951 0.200 98 90-110 WSTINCN1_00572

 26 CCB 15:33 Cyanide, Total <0.0100

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 307 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

Method Analyte Result Qual Dil

3-IN

500-53491-1

Lab Sample ID Units

TestAmerica Chicago

METHOD BLANK

GENERAL CHEMISTRY

RL

Batch ID: 174564 Date: 01/08/2013 11:00 Prep Batch: 174563 Date: 01/08/2013 05:35

1664A MB 500-174563/1-A HEM (Oil & Grease) <5.00 mg/L 5.00 1

Batch ID: 173793 Date: 12/22/2012 14:11

7196A MB 500-173793/3 Chromium, hexavalent <0.0100 mg/L 0.0100 1

Batch ID: 174027 Date: 12/27/2012 12:41 Prep Batch: 173790 Date: 12/22/2012 12:00

7196A MB 500-173790/1-A Chromium, hexavalent <1.00 mg/Kg 1.00 1

Batch ID: 174042 Date: 12/27/2012 14:40 Prep Batch: 173980 Date: 12/27/2012 09:50

9014 MB 500-173980/1-A Cyanide, Total <0.0100 mg/L 0.0100 1

Batch ID: 174173 Date: 12/28/2012 15:30 Prep Batch: 174096 Date: 12/28/2012 11:20

MB <0.500

500-174096/12-A

9014 Cyanide, Total mg/Kg 0.500 1

Batch ID: 173845 Date: 12/24/2012 13:19 Prep Batch: 173844 Date: 12/24/2012 08:00

9034 MB 500-173844/1-A Sulfide, Reactive <1.00 mg/L 1.00 1

Batch ID: 173846 Date: 12/24/2012 13:19

9034 MB 500-173846/1 Sulfide <1.00 mg/L 1.00 1

Batch ID: 174145 Date: 12/28/2012 12:55 Prep Batch: 174101 Date: 12/28/2012 11:35

9034 MB 500-174101/1-A Sulfide, Reactive <50.0 mg/Kg 50.0 1

Batch ID: 174144 Date: 12/28/2012 14:35 Prep Batch: 174100 Date: 12/28/2012 12:20

9034 MB 500-174100/1-A Sulfide <25.0 mg/Kg 25.0 1

Batch ID: 174372 Date: 01/04/2013 09:45 Prep Batch: 174369 Date: 01/04/2013 05:35

9071B MB 500-174369/1-A HEM (Oil & Grease) <500 mg/Kg 500 1

FORM III-IN

Page 308 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

Matrix:

Analyte

500-53491-1

Method Lab Sample ID Result Unit

Spike

Amount

Pct.

Rec. C Limits RPD

RPD

Limit Q

Solid

5-IN

MATRIX SPIKE SAMPLE RECOVERY

GENERAL CHEMISTRY

TestAmerica Chicago

Batch ID: 174173 Date: 12/28/2012 15:32 Prep Batch: 174096 Date: 12/28/2012 11:20

9014 500-53491-2 Cyanide, Total 1.29 J mg/Kg

9014 500-53491-2 

MS 

Cyanide, Total 7.442 mg/Kg 7.50 82 75-125

Batch ID: 174372 Date: 01/04/2013 10:27 Prep Batch: 174369 Date: 01/04/2013 05:35

9071B 500-53491-1 HEM (Oil & Grease) 16600 mg/Kg

9071B 500-53491-1 

MS 

HEM (Oil & Grease) 39400 mg/Kg 14800 154 75-125 F

FORM V-IN

Note - Results and Reporting Limits have been adjusted for dry weight.

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 309 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

Matrix:

Analyte

500-53491-1

Method Lab Sample ID Result Unit

Spike

Amount

Pct.

Rec. C Limits RPD

RPD

Limit Q

Water

5-IN

MATRIX SPIKE SAMPLE RECOVERY

GENERAL CHEMISTRY

TestAmerica Chicago

Batch ID: 173793 Date: 12/22/2012 14:13

7196A 500-53491-5 Chromium, hexavalent <0.0100 mg/L H

7196A 500-53491-5 

MS 

Chromium, hexavalent 0.2660 mg/L 0.250 106 85-115

FORM V-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 310 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

Matrix:

Analyte

500-53491-1

Method Lab Sample ID Result Unit

Spike

Amount

Pct.

Rec. C Limits RPD

RPD

Limit Q

Solid

5-IN

MATRIX SPIKE DUPLICATE SAMPLE RECOVERY

GENERAL CHEMISTRY

TestAmerica Chicago

Batch ID: 174173 Date: 12/28/2012 15:32 Prep Batch: 174096 Date: 12/28/2012 11:20

9014 500-53491-2 

MSD 

Cyanide, Total 8.170 mg/Kg 7.44 92 75-125 9 20

Batch ID: 174372 Date: 01/04/2013 10:42 Prep Batch: 174369 Date: 01/04/2013 05:35

9071B 500-53491-1 

MSD 

HEM (Oil & Grease) 40340 mg/Kg 14800 160 75-125 2 20 F

FORM V-IN

Note - Results and Reporting Limits have been adjusted for dry weight.

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 311 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

Matrix:

Analyte

500-53491-1

Method Lab Sample ID Result Unit

Spike

Amount

Pct.

Rec. C Limits RPD

RPD

Limit Q

Water

5-IN

MATRIX SPIKE DUPLICATE SAMPLE RECOVERY

GENERAL CHEMISTRY

TestAmerica Chicago

Batch ID: 173793 Date: 12/22/2012 14:13

7196A 500-53491-5 

MSD 

Chromium, hexavalent 0.2541 mg/L 0.250 102 85-115 5 20

FORM V-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 312 of 384 01/09/2013
7A-IN

Job No.: 500-53491-1

LAB CONTROL SAMPLE

GENERAL CHEMISTRY

Lab Name:

SDG No.:

Q

RPD

Limit Limits RPD

Pct.

Rec.

Spike

Amount Method Lab Sample ID Analyte Result C Unit

Matrix: Solid

TestAmerica Chicago

Batch ID: 174027 Date: 12/27/2012 12:42 Prep Batch: 173790 Date: 12/22/2012 12:00

LCS Source: WSTCR2_00008

7196A LCS 10.0 92

500-173790/2-

A

Chromium, hexavalent 9.188 mg/Kg 80-120

Batch ID: 174027 Date: 12/27/2012 12:42 Prep Batch: 173790 Date: 12/22/2012 12:00

LCS Source: WSTCR13_00629

7196A LCS 676 99

500-173790/3-

A

Chromium, hexavalent 669.0 mg/Kg 80-120

Batch ID: 174173 Date: 12/28/2012 15:30 Prep Batch: 174096 Date: 12/28/2012 11:20

LCS Source: WSTINCN2_00564

9014 LCS 5.00 107

500-174096/13

-A

Cyanide, Total 5.325 mg/Kg 80-120

Batch ID: 174145 Date: 12/28/2012 12:55 Prep Batch: 174101 Date: 12/28/2012 11:38

LCS Source: WSTSF1_00036

9034 LCS 180 94

500-174101/2-

A

Sulfide, Reactive 169.4 mg/Kg 80-120

Batch ID: 174144 Date: 12/28/2012 14:36 Prep Batch: 174100 Date: 12/28/2012 12:20

LCS Source: WSTSF1_00036

9034 LCS 180 96

500-174100/2-

A

Sulfide 173.0 mg/Kg 80-120

Batch ID: 174372 Date: 01/04/2013 09:59 Prep Batch: 174369 Date: 01/04/2013 05:35

LCS Source: 1664 HEM_00060

9071B LCS 4000 101

500-174369/2-

A

HEM (Oil & Grease) 4050 mg/Kg 80-120

FORM VIIA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 313 of 384 01/09/2013
7A-IN

Job No.: 500-53491-1

LAB CONTROL SAMPLE

GENERAL CHEMISTRY

Lab Name:

SDG No.:

Q

RPD

Limit Limits RPD

Pct.

Rec.

Spike

Amount Method Lab Sample ID Analyte Result C Unit

Matrix: Water

TestAmerica Chicago

Batch ID: 174564 Date: 01/08/2013 11:04 Prep Batch: 174563 Date: 01/08/2013 05:48

LCS Source: 1664 HEM_00060

1664A LCS 40.0 80

500-174563/2-

A

HEM (Oil & Grease) 32.00 mg/L 78-114

Batch ID: 173793 Date: 12/22/2012 14:11

LCS Source: WSTCR2_00008

7196A LCS 0.250 103

500-173793/4

Chromium, hexavalent 0.2575 mg/L 85-115

Batch ID: 174042 Date: 12/27/2012 14:40 Prep Batch: 173980 Date: 12/27/2012 09:50

LCS Source: WSTINCN2_00563

9014 LCS 0.100 107

500-173980/2-

A

Cyanide, Total 0.1066 mg/L 80-120

Batch ID: 173846 Date: 12/24/2012 13:20

LCS Source: WSTSF1_00036

9034 LCS 3.60 104

500-173846/2

Sulfide 3.760 mg/L 80-120

Batch ID: 173845 Date: 12/24/2012 13:29 Prep Batch: 173844 Date: 12/24/2012 08:15

LCS Source: WSTSF1_00036

9034 LCS 3.60 105

500-173844/2-

A

Sulfide, Reactive 3.767 mg/L 80-120

FORM VIIA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 314 of 384 01/09/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53491-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 7196A MDL Date: 05/29/2012 10:43

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Chromium, hexavalent 0.01 0.00325

FORM IX - IN

Page 315 of 384 01/09/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53491-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 7196A XMDL Date: 05/29/2012 10:44

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Chromium, hexavalent 0.01 0.00325

FORM IX - IN

Page 316 of 384 01/09/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53491-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 7196A MDL Date: 05/29/2012 14:44

Prep Method: 3060A

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

Chromium, hexavalent 1 0.389

FORM IX - IN

Page 317 of 384 01/09/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53491-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 7196A XMDL Date: 05/29/2012 10:45

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Chromium, hexavalent 0.02 0.00325

FORM IX - IN

Page 318 of 384 01/09/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53491-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9014 MDL Date: 06/18/2012 16:18

Prep Method: 9010B

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

Cyanide, Total 0.5 0.165

FORM IX - IN

Page 319 of 384 01/09/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53491-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 9014 XMDL Date: 06/18/2012 16:19

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Cyanide, Total 0.01 0.00331

FORM IX - IN

Page 320 of 384 01/09/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53491-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9014 MDL Date: 06/18/2012 16:22

Prep Method: 9010B

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Cyanide, Total 0.01 0.00331

FORM IX - IN

Page 321 of 384 01/09/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53491-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 9014 XMDL Date: 06/18/2012 16:22

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Cyanide, Total 0.01 0.00331

FORM IX - IN

Page 322 of 384 01/09/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53491-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9034 MDL Date: 05/29/2012 16:25

Prep Method: 7.3.4

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

Sulfide, Reactive 50 3.9

FORM IX - IN

Page 323 of 384 01/09/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53491-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9034 MDL Date: 01/02/2006 09:18

Prep Method: 7.3.4

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Sulfide, Reactive 1 1

FORM IX - IN

Page 324 of 384 01/09/2013
9-IN

Instrument ID: FP4

Job Number: 500-53491-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 1010 MDL Date: 11/11/2005 10:25

Analyte Wavelength/

Mass

RL MDL

(Degrees (Degrees F)

Flashpoint 40 40

FORM IX - IN

Page 325 of 384 01/09/2013
9-IN

Instrument ID: NoEquip

Job Number: 500-53491-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 1664A MDL Date: 05/29/2012 15:22

Prep Method: 1664A

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

HEM (Oil & Grease) 5 1.45

FORM IX - IN

Page 326 of 384 01/09/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53491-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9034 MDL Date: 05/29/2012 15:57

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Sulfide 1 0.23

FORM IX - IN

Page 327 of 384 01/09/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53491-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9034 MDL Date: 05/29/2012 15:59

Prep Method: 9030B

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

Sulfide 25 4

FORM IX - IN

Page 328 of 384 01/09/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53491-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9045C MDL Date: 11/01/2005 06:06

Analyte Wavelength/

Mass

RL MDL

(SU) (SU)

pH 0.2 0.2

FORM IX - IN

Page 329 of 384 01/09/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53491-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9071B MDL Date: 05/29/2012 15:24

Prep Method: 9071B

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

HEM (Oil & Grease) 500 222

FORM IX - IN

Page 330 of 384 01/09/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53491-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: Moisture MDL Date: 11/01/2005 09:02

Analyte Wavelength/

Mass

RL MDL

(%) (%)

Percent Moisture 0.1 0.1

Percent Solids 0.1 0.1

FORM IX - IN

Page 331 of 384 01/09/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53491-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: SM 2540G MDL Date: 11/01/2005 09:02

Analyte Wavelength/

Mass

RL MDL

(%) (%)

% Moisture 0.1 0.1

Total Solids 0.1 0.1

FORM IX - IN

Page 332 of 384 01/09/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53491-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 3060A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-173790/1-A 12/22/2012 12:00 173790 2.5 100

LCS 500-173790/2-A 12/22/2012 12:00 173790 2.5 100

LCS 500-173790/3-A 12/22/2012 12:00 173790 2.5 100

500-53491-1 12/22/2012 12:00 173790 2.5178 100

500-53491-2 12/22/2012 12:00 173790 2.5000 100

FORM XII-IN

Page 333 of 384 01/09/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53491-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 7.3.4

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-173844/1-A 12/24/2012 08:00 173844 250 250

LCS 500-173844/2-A 12/24/2012 08:15 173844 250 250

500-53491-5 12/24/2012 08:45 173844 250 250

FORM XII-IN

Page 334 of 384 01/09/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53491-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 9010B

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-173980/1-A 12/27/2012 09:50 173980 50 50

LCS 500-173980/2-A 12/27/2012 09:50 173980 50 50

500-53491-5 12/27/2012 09:50 173980 50 50

FORM XII-IN

Page 335 of 384 01/09/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53491-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 9010B

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-174096/12-A 12/28/2012 11:20 174096 1.0000 50

LCS 500-174096/13-A 12/28/2012 11:20 174096 1.0000 50

500-53491-1 12/28/2012 11:20 174096 1.0022 50

500-53491-2 12/28/2012 11:20 174096 1.0695 50

500-53491-2 MS 12/28/2012 11:20 174096 1.0637 50

500-53491-2 MSD 12/28/2012 11:20 174096 1.0714 50

FORM XII-IN

Page 336 of 384 01/09/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53491-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 7.3.4

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-174101/1-A 12/28/2012 11:35 174101 10.0000 10

LCS 500-174101/2-A 12/28/2012 11:38 174101 10.0000 10

500-53491-1 12/28/2012 11:57 174101 10.3048 10

500-53491-2 12/28/2012 12:01 174101 10.1362 10

FORM XII-IN

Page 337 of 384 01/09/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53491-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 9030B

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-174100/1-A 12/28/2012 12:20 174100 10.0000 10

LCS 500-174100/2-A 12/28/2012 12:20 174100 10.0000 10

500-53491-1 12/28/2012 12:20 174100 10.4509 10

500-53491-2 12/28/2012 12:20 174100 10.6031 10

FORM XII-IN

Page 338 of 384 01/09/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53491-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 9071B

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-174369/1-A 01/04/2013 05:35 174369 10 10

LCS 500-174369/2-A 01/04/2013 05:35 174369 10 10

500-53491-1 01/04/2013 05:35 174369 10.2054 10

500-53491-1 MS 01/04/2013 05:35 174369 10.2105 10

500-53491-1 MSD 01/04/2013 05:35 174369 10.2075 10

500-53491-2 01/04/2013 05:35 174369 10.2202 10

FORM XII-IN

Page 339 of 384 01/09/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53491-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 1664A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-174563/1-A 01/08/2013 05:35 174563 1000 1000

LCS 500-174563/2-A 01/08/2013 05:48 174563 1000 1000

500-53491-5 01/08/2013 06:01 174563 938 1000

FORM XII-IN

Page 340 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

SPEC5

12/22/2012 14:10 12/22/2012 14:14

7196A

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

C

r

6 T

y

p

e

ICV 500-173793/1 1 14:10 X

ICB 500-173793/2 1 14:10 X

MB 500-173793/3 1 T 14:11 X

LCS 500-173793/4 1 T 14:11 X

ZZZZZZ 14:12

500-53491-5 1 T 14:12 X

500-53491-5 MS 1 T 14:13 X

500-53491-5 MSD 1 T 14:13 X

CCV 500-173793/9 1 14:14 X

CCB 500-173793/10 1 14:14 X

Prep Types

T = Total/NA

FORM XIII-IN Page 341 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

SPEC5

12/27/2012 12:40 12/27/2012 12:59

7196A

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

C

r

6 T

y

p

e

ICV 500-174027/1 1 12:40 X

ICB 500-174027/2 1 12:40 X

MB 500-173790/1-A 1 T 12:41 X

LCS 500-173790/2-A 1 T 12:42 X

LCS 500-173790/3-A 50 T 12:42 X

ZZZZZZ 12:43

ZZZZZZ 12:44

ZZZZZZ 12:44

ZZZZZZ 12:45

CCV 500-174027/10 1 12:46 X

CCB 500-174027/11 1 12:46 X

ZZZZZZ 12:47

ZZZZZZ 12:48

ZZZZZZ 12:48

ZZZZZZ 12:49

ZZZZZZ 12:50

500-53491-1 1 T 12:51 X

CCV 500-174027/18 1 12:51 X

CCB 500-174027/19 1 12:52 X

500-53491-2 1 T 12:53 X

ZZZZZZ 12:53

ZZZZZZ 12:54

ZZZZZZ 12:55

ZZZZZZ 12:55

ZZZZZZ 12:56

ZZZZZZ 12:57

CCV 500-174027/27 1 12:57 X

CCB 500-174027/28 1 12:58 X

ZZZZZZ 12:59

Prep Types

T = Total/NA

FORM XIII-IN Page 342 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

SPEC5

12/27/2012 14:40 12/27/2012 14:49

9014

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

C

N

T

y

p

e

ICV 500-174042/1 1 14:40 X

ICB 500-174042/2 1 14:40 X

MB 500-173980/1-A 1 T 14:40 X

LCS 500-173980/2-A 1 T 14:40 X

ZZZZZZ 14:41

ZZZZZZ 14:41

ZZZZZZ 14:41

ZZZZZZ 14:42

ZZZZZZ 14:42

ZZZZZZ 14:42

ZZZZZZ 14:42

ZZZZZZ 14:43

CCV 500-174042/13 1 14:43 X

CCB 500-174042/14 1 14:43 X

ZZZZZZ 14:44

ZZZZZZ 14:44

ZZZZZZ 14:44

ZZZZZZ 14:44

ZZZZZZ 14:45

500-53491-5 1 T 14:45 X

ZZZZZZ 14:45

ZZZZZZ 14:46

ZZZZZZ 14:46

ZZZZZZ 14:46

CCV 500-174042/25 1 14:47 X

CCB 500-174042/26 1 14:47 X

ZZZZZZ 14:47

ZZZZZZ 14:47

ZZZZZZ 14:48

ZZZZZZ 14:48

ZZZZZZ 14:48

ZZZZZZ 14:49

CCV 500-174042/33 14:49

CCB 500-174042/34 14:49

Prep Types

T = Total/NA

FORM XIII-IN Page 343 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

SPEC5

12/28/2012 15:25 12/28/2012 15:34

9014

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

C

N

T

y

p

e

ICV 500-174173/1 1 15:25 X

ICB 500-174173/2 1 15:25 X

ZZZZZZ 15:25

ZZZZZZ 15:26

ZZZZZZ 15:26

ZZZZZZ 15:26

ZZZZZZ 15:27

ZZZZZZ 15:27

ZZZZZZ 15:27

ZZZZZZ 15:28

ZZZZZZ 15:28

ZZZZZZ 15:28

CCV 500-174173/13 1 15:29 X

CCB 500-174173/14 1 15:29 X

ZZZZZZ 15:29

MB 500-174096/12-A 1 T 15:30 X

LCS 500-174096/13-A 1 T 15:30 X

ZZZZZZ 15:30

ZZZZZZ 15:31

500-53491-1 1 T 15:31 X

500-53491-2 1 T 15:31 X

500-53491-2 MS 1 T 15:32 X

500-53491-2 MSD 1 T 15:32 X

ZZZZZZ 15:32

CCV 500-174173/25 1 15:33 X

CCB 500-174173/26 1 15:33 X

ZZZZZZ 15:33

ZZZZZZ 15:34

ZZZZZZ 15:34

ZZZZZZ 15:34

Prep Types

T = Total/NA

FORM XIII-IN Page 344 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

NOEQUIP

12/24/2012 13:19 12/24/2012 13:51

9034

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

S

2

R

e

a

c

T

y

p

e

MB 500-173844/1-A 1 T 13:19 X

LCS 500-173844/2-A 1 T 13:29 X

ZZZZZZ 13:40

500-53491-5 1 T 13:51 X

Prep Types

T = Total/NA

FORM XIII-IN Page 345 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

NOEQUIP

12/28/2012 12:55 12/28/2012 12:59

9034

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

S

2

R

e

a

c

T

y

p

e

MB 500-174101/1-A 1 T 12:55 X

LCS 500-174101/2-A 1 T 12:55 X

ZZZZZZ 12:56

ZZZZZZ 12:56

ZZZZZZ 12:57

ZZZZZZ 12:58

500-53491-1 1 T 12:58 X

500-53491-2 1 T 12:59 X

Prep Types

T = Total/NA

FORM XIII-IN Page 346 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

FP4

01/02/2013 09:30 01/02/2013 14:58

1010

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

F

P

T

y

p

e

500-53491-1 1 T 09:30 X

500-53491-2 1 T 10:52 X

ZZZZZZ 12:14

ZZZZZZ 13:36

ZZZZZZ 14:58

Prep Types

T = Total/NA

FORM XIII-IN Page 347 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

NoEquip

01/08/2013 11:00 01/08/2013 12:35

1664A

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

H

E

M T

y

p

e

MB 500-174563/1-A 1 T 11:00 X

LCS 500-174563/2-A 1 T 11:04 X

500-53491-5 1 T 11:08 X

ZZZZZZ 11:13

ZZZZZZ 11:17

ZZZZZZ 11:21

ZZZZZZ 11:26

ZZZZZZ 11:30

ZZZZZZ 11:34

ZZZZZZ 11:39

ZZZZZZ 11:43

ZZZZZZ 11:47

ZZZZZZ 11:52

ZZZZZZ 11:56

ZZZZZZ 12:00

ZZZZZZ 12:05

ZZZZZZ 12:09

ZZZZZZ 12:13

ZZZZZZ 12:18

ZZZZZZ 12:22

ZZZZZZ 12:26

ZZZZZZ 12:31

ZZZZZZ 12:35

Prep Types

T = Total/NA

FORM XIII-IN Page 348 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

NOEQUIP

12/24/2012 13:19 12/24/2012 14:00

9034

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

S

2

T

y

p

e

MB 500-173846/1 1 T 13:19 X

LCS 500-173846/2 1 T 13:20 X

ZZZZZZ 13:22

ZZZZZZ 13:24

ZZZZZZ 13:26

ZZZZZZ 13:28

ZZZZZZ 13:30

ZZZZZZ 13:32

ZZZZZZ 13:33

ZZZZZZ 13:35

ZZZZZZ 13:37

ZZZZZZ 13:39

ZZZZZZ 13:41

ZZZZZZ 13:43

ZZZZZZ 13:45

ZZZZZZ 13:47

ZZZZZZ 13:48

ZZZZZZ 13:50

ZZZZZZ 13:52

ZZZZZZ 13:54

ZZZZZZ 13:56

ZZZZZZ 13:58

500-53491-5 1 T 14:00 X

Prep Types

T = Total/NA

FORM XIII-IN Page 349 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

NOEQUIP

12/28/2012 14:35 12/28/2012 14:44

9034

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

S

2

T

y

p

e

MB 500-174100/1-A 1 T 14:35 X

LCS 500-174100/2-A 1 T 14:36 X

ZZZZZZ 14:37

ZZZZZZ 14:38

ZZZZZZ 14:39

ZZZZZZ 14:40

ZZZZZZ 14:41

ZZZZZZ 14:42

500-53491-1 1 T 14:43 X

500-53491-2 1 T 14:44 X

Prep Types

T = Total/NA

FORM XIII-IN Page 350 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

NOEQUIP

12/26/2012 14:15 12/26/2012 14:27

9045C

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

p

H

T

y

p

e

ZZZZZZ 14:15

ZZZZZZ 14:17

ZZZZZZ 14:20

ZZZZZZ 14:22

500-53491-1 1 T 14:25 X

500-53491-2 1 T 14:27 X

Prep Types

T = Total/NA

FORM XIII-IN Page 351 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

NOEQUIP

01/04/2013 09:45 01/04/2013 11:10

9071B

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

H

E

M T

y

p

e

MB 500-174369/1-A 1 T 09:45 X

LCS 500-174369/2-A 1 T 09:59 X

500-53491-1 1 T 10:13 X

500-53491-1 MS 1 T 10:27 X

500-53491-1 MSD 1 T 10:42 X

500-53491-2 1 T 10:56 X

ZZZZZZ 11:10

Prep Types

T = Total/NA

FORM XIII-IN Page 352 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

NOEQUIP

12/22/2012 09:29 12/22/2012 13:24

Moisture

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

%

S

o

l

M

o

i

s

t

T

y

p

e

ZZZZZZ 09:29

ZZZZZZ 09:29

ZZZZZZ 09:29

ZZZZZZ 13:24

ZZZZZZ 13:24

ZZZZZZ 13:24

500-53491-1 1 T 13:24 X X

500-53491-2 1 T 13:24 X X

ZZZZZZ 13:24

ZZZZZZ 13:24

ZZZZZZ 13:24

ZZZZZZ 13:24

ZZZZZZ 13:24

ZZZZZZ 13:24

ZZZZZZ 13:24

Prep Types

T = Total/NA

FORM XIII-IN Page 353 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

NOEQUIP

12/28/2012 07:50 12/28/2012 12:33

Moisture

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

%

S

o

l

M

o

i

s

t

T

y

p

e

ZZZZZZ 07:50

ZZZZZZ 07:50

ZZZZZZ 07:50

ZZZZZZ 07:50

ZZZZZZ 07:50

ZZZZZZ 07:50

ZZZZZZ 07:50

ZZZZZZ 07:50

500-53491-3 1 T 10:09 X X

500-53491-4 1 T 10:09 X X

ZZZZZZ 12:33

ZZZZZZ 12:33

ZZZZZZ 12:33

ZZZZZZ 12:33

ZZZZZZ 12:33

ZZZZZZ 12:33

ZZZZZZ 12:33

ZZZZZZ 12:33

ZZZZZZ 12:33

ZZZZZZ 12:33

ZZZZZZ 12:33

ZZZZZZ 12:33

ZZZZZZ 12:33

ZZZZZZ 12:33

ZZZZZZ 12:33

ZZZZZZ 12:33

ZZZZZZ 12:33

ZZZZZZ 12:33

ZZZZZZ 12:33

Prep Types

T = Total/NA

FORM XIII-IN Page 354 of 384 01/09/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53491-1

NOEQUIP

12/27/2012 07:30 12/27/2012 07:30

SM 2540G

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

M

o

i

s

t

T

S

T

y

p

e

500-53491-1 1 T 07:30 X X

500-53491-2 1 T 07:30 X X

Prep Types

T = Total/NA

FORM XIII-IN Page 355 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Wasowicz, Andrew P

12/27/12 13:00

173790 12/22/12 12:00

Batch Method:

TestAmerica Chicago

3060A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount WSTCR13 00629 WSTCR2 00008 AnalysisComment

MB 500-173790/1 3060A, 7196A 2.5 g 100 mL

LCS 2.5 g 100 mL 25 uL soluble

500-173790/2

3060A, 7196A

LCS 2.5 g 100 mL 100 mL soluble 0.0105

500-173790/3

3060A, 7196A

500-53491-A-1 FC COMPOSITE 6 3060A, 7196A T 2.5178 g 100 mL

500-53491-A-2 FC D COMPOSITE 6 3060A, 7196A T 2.5000 g 100 mL

Batch Notes

Alkaline Digestion Solution Reagent ID CR6digestion_00028

Batch Comment Filter Paper Lot # 100727

First End time see above

Potassium Chromate Lot # K00741

Potassium Phosphate Buffer Reagent ID Pot PO4_Buff_00002

Lead Chromate Lot # 15813PE

Lead Chromate Vendor ID Lead(II)Chrom_00001

Magnesium Chloride Lot Number J14N64 (MagCl_crystal_00002)

Magnesium Chloride Vendor JT Baker

First Start time see above

Ending Temperature 90 Celsius

Starting Temperature 90 Celsius

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

7196A Page 1 of 1

Page 356 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Wasowicz, Andrew P

12/22/12 14:15

173793 12/22/12 14:10

Batch Method:

TestAmerica Chicago

7196A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount CalcMsg WSTCR1 00008 WSTCR2 00008

100 mL 100 mL Color Resp. is 

Blank

ICV 25 uL

500-173793/1

7196A

Color Resp. is 

Blank

ICB 

500-173793/2

7196A

Color Resp. is 

Blank

MB 500-173793/3 7196A

100 mL 100 mL Color Resp. is 

Blank

LCS 25 uL

500-173793/4

7196A

FC EB 6 Color Resp. is 

Blank

500-53491-F-5 7196A T

FC EB 6 100 mL 100 mL Color Resp. is 

Blank

500-53491-F-5 25 uL

MS

7196A T

FC EB 6 100 mL 100 mL Color Resp. is 

Blank

500-53491-F-5 25 uL

MSD

7196A T

100 mL 100 mL Color Resp. is 

Blank

CCV 50 uL

500-173793/9

7196A

Color Resp. is 

Blank

CCB 

500-173793/10

7196A

Batch Notes

Batch Comment filter paper lot# 100232

Spectrophotometer Cell Path Length 540NM1CM cm

Color Reagent ID Number Hexa Chrome Color Reagent-00007

First End time See Start Date/Time

First Start time See Start Date/Time

Sulfuric Acid Reagent ID Number H2SO4 00007

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

7196A Page 1 of 1

Page 357 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Wasowicz, Andrew P

12/27/12 13:00

174027 12/27/12 12:40

Batch Method:

TestAmerica Chicago

7196A

Lab Sample ID Client Sample ID Method Chain Basis FinalAmount CalcMsg WSTCR1 00008 WSTCR2 00008

100 mL Color Resp. is 

Blank

ICV 25 uL

500-174027/1

7196A

Color Resp. is 

Blank

ICB 

500-174027/2

7196A

Color Resp. is 

Blank

MB 

500-173790/1-A

7196A

Color Resp. is 

Blank

LCS 

500-173790/2-A

7196A

Color Resp. is 

Blank

LCS 

500-173790/3-A

7196A

100 mL Color Resp. is 

Blank

CCV 50 uL

500-174027/10

7196A

Color Resp. is 

Blank

CCB 

500-174027/11

7196A

FC COMPOSITE 6 Color Resp. is 

Blank

500-53491-A-1-A 7196A T

100 mL Color Resp. is 

Blank

CCV 50 uL

500-174027/18

7196A

Color Resp. is 

Blank

CCB 

500-174027/19

7196A

FC D COMPOSITE 6 Color Resp. is 

Blank

500-53491-A-2-A 7196A T

100 mL Color Resp. is 

Blank

CCV 50 uL

500-174027/27

7196A

Color Resp. is 

Blank

CCB 

500-174027/28

7196A

Batch Notes

Spectrophotometer Cell Path Length 540NM1CM cm

Color Reagent ID Number CR+6 ColorRGT_00007

Sulfuric Acid Reagent ID Number H2SO4_00007

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

7196A Page 1 of 1

Page 358 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Treadwell, Eliane A

01/03/13 11:20

173980 12/27/12 09:50

Batch Method:

TestAmerica Chicago

9010B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount SulfideCheck WSTINCN2 00563

MB 500-173980/1 9010B, 9014 50 mL 50 mL y

LCS 50 mL 50 mL y 500 uL

500-173980/2

9010B, 9014

500-53491-D-5 FC EB 6 9010B, 9014 T 50 mL 50 mL y

Batch Notes

Bismuth Nitrate Lot # BismuthNO3_00018

Ca(OCl)2 Reagent ID Number CaCL2O2_00006

Distillation Temperature REFLUXING Degrees C

KI-Starch Paper Lot # 071409

Lead Acetate Lot # 121109

Methyl Red Indicator Reagent ID Meth_Red_IN_00001

Magnesium Chloride Reagent ID Number MagChloride_00010

NaAsO2 Reagent ID Number AscorbicAcid_00003

Sodium Hydroxide Reagent ID Number 0.25N NaOH_00005

Sulfamic Acid Reagent ID Number SulfamicAcid_00022

Sulfuric Acid Reagent ID Number 50%H2SO4_00007

Zinc Acetate Buffer Reagent ID Number IO8ARCN14

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

9014 Page 1 of 1

Page 359 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Treadwell, Eliane A

12/27/12 14:50

174042 12/27/12 14:40

Batch Method:

TestAmerica Chicago

9014

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount WSTINCN1 00571 WSTINCN2 00563

ICV 25 mL 25 mL 250 uL

500-174042/1

9014

CCV 25 mL 25 mL 500 uL

500-174042/13

9014

CCV 25 mL 25 mL 500 uL

500-174042/25

9014

Batch Notes

Buffer Reagent ID Number SPMM Buffer_00044

Chloramine-T Reagent ID Number Chloramine-T_00002

KI-Starch Paper Lot # 110510

NaOH Lot # NaOH_00005

Sodium Hydroxide Reagent ID Number 0.25N_NaOH_00015

Pyridine-Barbituric Acid Reagent ID Pyr_BarbAcid_00022

Scrubber Solution ID NaOH_00005

Sodium Phosphate Solution ID SPMM Buffer_00044

Spectrophotometer Wavelength 578NM

Basis Basis Description

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

9014 Page 1 of 1

Page 360 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Treadwell, Eliane A

12/28/12 12:50

174096 12/28/12 11:20

Batch Method:

TestAmerica Chicago

9010B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount SulfideCheck WSTINCN2 00564

MB 1.0000 g 50 mL y

500-174096/12

9010B, 9014

LCS 1.0000 g 50 mL y 500 uL

500-174096/13

9010B, 9014

500-53491-A-1 FC COMPOSITE 6 9010B, 9014 T 1.0022 g 50 mL y

500-53491-A-2 FC D COMPOSITE 6 9010B, 9014 T 1.0695 g 50 mL y

500-53491-A-2 FC D COMPOSITE 6 1.0637 g 50 mL y 200 uL

MS

9010B, 9014 T

500-53491-A-2 FC D COMPOSITE 6 1.0714 g 50 mL y 200 uL

MSD

9010B, 9014 T

Batch Notes

Bismuth Nitrate Lot # BismuthNO3_00018

Ca(OCl)2 Reagent ID Number CaCL2O2_00006

Distillation Temperature REFLUXING Degrees C

KI-Starch Paper Lot # 071409

Lead Acetate Lot # 121109

Methyl Red Indicator Reagent ID Meth_Red_IN_00001

Magnesium Chloride Reagent ID Number MagChloride_00010

NaAsO2 Reagent ID Number AscorbicAcid_00003

Sodium Hydroxide Reagent ID Number 0.25N NaOH_00005

Sulfamic Acid Reagent ID Number SulfamicAcid_00022

Sulfuric Acid Reagent ID Number 50%H2SO4_00007

Zinc Acetate Buffer Reagent ID Number IO8ARCN14

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

9014 Page 1 of 1

Page 361 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Treadwell, Eliane A

12/28/12 15:35

174173 12/28/12 15:25

Batch Method:

TestAmerica Chicago

9014

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount WSTINCN1 00572 WSTINCN2 00564

ICV 25 mL 25 mL 250 uL

500-174173/1

9014

CCV 25 mL 25 mL 500 uL

500-174173/13

9014

CCV 25 mL 25 mL 500 uL

500-174173/25

9014

Batch Notes

Buffer Reagent ID Number SPMM Buffer_00044

Chloramine-T Reagent ID Number Chloramine-T_00002

KI-Starch Paper Lot # 110510

NaOH Lot # NaOH_00005

Sodium Hydroxide Reagent ID Number 0.25N_NaOH_00015

Pyridine-Barbituric Acid Reagent ID Pyr_BarbAcid_00022

Scrubber Solution ID NaOH_00005

Sodium Phosphate Solution ID SPMM Buffer_00044

Spectrophotometer Wavelength 578NM

Basis Basis Description

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

9014 Page 1 of 1

Page 362 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Boyd, Cheryl L

12/24/12 09:00

173844 12/24/12 08:00

Batch Method:

TestAmerica Chicago

7.3.4

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount

MB 500-173844/1 7.3.4, 9034 250 mL 250 mL

LCS 250 mL 250 mL

500-173844/2

7.3.4, 9034

500-53491-G-5 FC EB 6 7.3.4, 9034 T 250 mL 250 mL

Batch Notes

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

9034 Page 1 of 1

Page 363 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Boyd, Cheryl L

12/24/12 14:02

173845 12/24/12 13:19

Batch Method:

TestAmerica Chicago

9034

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount IodineAmount TitrantVolume1 CalcMsg FinalAmount WSTSF1 00036

MB 250 mL 5 mL 4.91 mL OK 250 mL

500-173844/1-A

9034

LCS 250 mL 5 mL 2.49 mL OK 250 mL 5 mL

500-173844/2-A

9034

500-53491-G-5-A FC EB 6 9034 T 250 mL 5 mL 5.18 mL OK 250 mL

Batch Notes

Normality of Iodine Solution 0.0240 N

Nominal Amount Used 250 mL

Perform Calculation (0=No, 1=Yes) 1

Normality of first Titrant 0.0246 N

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

9034 Page 1 of 1

Page 364 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Moore, Colleen L

12/28/12 12:05

174101 12/28/12 11:35

Batch Method:

TestAmerica Chicago

7.3.4

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount WSTSF1 00036

MB 500-174101/1 7.3.4, 9034 10.0000 g 10 mL

LCS 10.0000 g 10 mL 10 mL

500-174101/2

7.3.4, 9034

500-53491-A-1 FC COMPOSITE 6 7.3.4, 9034 T 10.3048 g 10 mL

500-53491-A-2 FC D COMPOSITE 6 7.3.4, 9034 T 10.1362 g 10 mL

Batch Notes

Batch Comment Balance ID # 2489

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

9034 Page 1 of 1

Page 365 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Moore, Colleen L

12/28/12 13:00

174145 12/28/12 12:55

Batch Method:

TestAmerica Chicago

9034

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount IodineAmount TitrantVolume1 CalcMsg FinalAmount

MB 10 mL 5 mL 4.68 mL OK 10 mL

500-174101/1-A

9034

LCS 10 mL 5 mL 0.38 mL OK 10 mL

500-174101/2-A

9034

500-53491-A-1-I FC COMPOSITE 6 9034 T 10 mL 5 mL 4.76 mL OK 10 mL

500-53491-A-2-M FC D COMPOSITE 6 9034 T 10 mL 5 mL 4.73 mL OK 10 mL

Batch Notes

Normality of Iodine Solution 0.0230 N

Nominal Amount Used 10 g

Perform Calculation (0=No, 1=Yes) 1

Normality of first Titrant 0.0246 N

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

9034 Page 1 of 1

Page 366 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Wasowicz, Andrew P

01/02/13 16:20

174336 01/02/13 09:30

Batch Method:

TestAmerica Chicago

1010

Lab Sample ID Client Sample ID Method Chain Basis AnalysisComment

500-53491-A-1 FC COMPOSITE 6 1010 T soft clay

500-53491-A-2 FC D COMPOSITE 6 1010 T soft clay

Batch Notes

Equipment ID HFP 339

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

1010 Page 1 of 1

Page 367 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Brogan, Mary T

01/08/13 10:35

174563 01/08/13 05:35

Batch Method:

TestAmerica Chicago

1664A

Lab Sample ID Client Sample ID Method Chain Basis GrossWeight TareWeight InitialAmount FinalAmount

MB 500-174563/1 1664A, 1664A 1390 g 390 g 1000 mL 1000 mL

LCS 1390 g 390 g 1000 mL 1000 mL

500-174563/2

1664A, 1664A

500-53491-H-5 FC EB 6 1664A, 1664A T 1327 g 389 g 938 mL 1000 mL

Batch Notes

Batch Comment phase separating filter lot # 8293623

Concentration End Time See end date/time

Concentration Start Time See start date/time

Person's name who did the concentration See analyst name

Disk Lot Number 47mm-1507111, pf-70610210; 90mm-150381, 

pf-70610210

Evaporator Temperature 50 DEG. Degrees C

Extraction Analyst see analyst name

Sulfuric Acid Lot Number MALG35029

Hexane Lot# HEXANES_00012

Manifold ID 1851

Methanol Lot Number Methanol_00007

Na2SO4 Lot Number Na2SO4_00006

Nominal Amount Used 1000 mL

Sufficient volume for MS/MSD? NO

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

1664A Page 1 of 1

Page 368 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Brogan, Mary T

01/08/13 12:40

174564 01/08/13 11:00

Batch Method:

TestAmerica Chicago

1664A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount RECTUBE# ReceiverTube RecTubeWExtract

1

RecTubeWExtract

2

MB 1000 mL 1000 mL 1 2.3114 g 2.3121 g 2.3121 g

500-174563/1-A

1664A

LCS 1000 mL 1000 mL 2 6.2861 g 6.3180 g 6.3181 g

500-174563/2-A

1664A

500-53491-H-5-A FC EB 6 1664A T 1000 mL 1000 mL 3 2.2903 g 2.2915 g 2.2915 g

Lab Sample ID Client Sample ID Method Chain Basis WeightOne%Diff Residue Residue2 1664 HEM 00060

Pass_0.0005g 0.0007000000000

00145 g

0.0007000000000

00145 g

MB 

500-174563/1-A

1664A

Pass_0.0005g 0.0318999999999

994 g

LCS 0.032 g 5 mL

500-174563/2-A

1664A

FC EB 6 Pass_0.0005g 0.0012000000000

0031 g

0.0012000000000

0031 g

500-53491-H-5-A 1664A T

Batch Notes

Balance ID 1634

Calibration Check After 2nd Weighing 0.0019 / 1.0000 g

Calibration Check Before 1st Weighing 0.0020 / 0.9999 g

Person's name who did the concentration see analyst name

Evaporator Temperature 50 Degrees C

Hexane Lot# Hexanes_00012

Methanol Lot Number Methanol_00006

Na2SO4 Lot Number Na2SO4_00006

Silica Gel Lot Number Silica gel_00003 (checked in batch 157954, 

7/31/12)

Speedvap ID# 1564

Weight Set ID 1144 / 2495

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

1664A Page 1 of 1

Page 369 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Boyd, Cheryl L

12/24/12 14:02

173846 12/24/12 13:19

Batch Method:

TestAmerica Chicago

9034

Lab Sample ID Client Sample ID Method Chain Basis TitrantVolume1 IodineAmount InitialAmount FinalAmount CalcMsg WSTSF1 00036

MB 500-173846/1 9034 4.91 mL 5 mL 250 mL 250 mL OK

LCS 2.49 mL 5 mL 250 mL 250 mL OK 5 mL

500-173846/2

9034

500-53491-G-5 FC EB 6 9034 T 5.18 mL 5 mL 250 mL 250 mL OK

Batch Notes

First End time 14:02

Iodine Lot Number 0.25NIODINE00005

Iodine Vendor INHOUSE

Normality of Iodine Solution 0.0240 N

Sodium Thiosulfate Lot Number NO2S2O300008

Sodium Thiosulfate Vendor INHOUSE

Nominal Amount Used 250 mL

Perform Calculation (0=No, 1=Yes) 1

Starch Lot Number STARCHIND00004

Starch Vendor VWR

First Start time 13:19

Sulfuric Acid Reagent ID Number 6NHCL00006

Normality of first Titrant 0.0246 N

Titrant Standardization Date 11/21/12

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

9034 Page 1 of 1

Page 370 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Moore, Colleen L

12/28/12 13:50

174100 12/28/12 12:20

Batch Method:

TestAmerica Chicago

9030B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount WSTSF1 00036

MB 500-174100/1 9030B, 9034 10.0000 g 10 mL

LCS 10.0000 g 10 mL 10 mL

500-174100/2

9030B, 9034

500-53491-A-1 FC COMPOSITE 6 9030B, 9034 T 10.4509 g 10 mL

500-53491-A-2 FC D COMPOSITE 6 9030B, 9034 T 10.6031 g 10 mL

Batch Notes

Batch Comment BAlance ID #2489

Distillation Temperature 70 Degrees C

Sodium Hydroxide Reagent ID Number 0.25N NaOH_00014

Sulfuric Acid Reagent ID Number 20% H2SO4_00003

Zinc Acetate Buffer Reagent ID Number 0.5M ZnAcetate_00005

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

9034 Page 1 of 1

Page 371 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Moore, Colleen L

12/28/12 14:45

174144 12/28/12 14:35

Batch Method:

TestAmerica Chicago

9034

Lab Sample ID Client Sample ID Method Chain Basis FinalAmount IodineAmount TitrantVolume1 CalcMsg

MB 10 mL 5 mL 4.67 mL OK

500-174100/1-A

9034

LCS 10 mL 5 mL 0.28 mL OK

500-174100/2-A

9034

500-53491-A-1-H FC COMPOSITE 6 9034 T 10 mL 10 mL 3.88 mL OK

500-53491-A-2-L FC D COMPOSITE 6 9034 T 10 mL 10 mL 3.83 mL OK

Batch Notes

HCl Concentration 6N

Lot # of hydrochloric acid 6NHCL00006

Iodine Lot Number 0.25NIODINE00005

Iodine Vendor INHOUSE

Normality of Iodine Solution 0.0230 N

Sodium Thiosulfate Reagent ID Number NO2S2O300008

Perform Calculation (0=No, 1=Yes) 1

Starch Lot Number STARCHIND00004

Starch Vendor VWR

Normality of first Titrant 0.0246 N

Zinc Acetate Buffer Reagent ID Number 0.5MZNACETAT00005

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

9034 Page 1 of 1

Page 372 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Brogan, Mary T

01/04/13 07:40

174369 01/04/13 05:35

Batch Method:

TestAmerica Chicago

9071B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount 1664 HEM 00060

MB 500-174369/1 9071B, 9071B 10 g 10 mL

LCS 10 g 10 mL 5 mL

500-174369/2

9071B, 9071B

500-53491-A-1 FC COMPOSITE 6 9071B, 9071B T 10.2054 g 10 mL

500-53491-A-1 FC COMPOSITE 6 10.2105 g 10 mL 5 mL

MS

9071B, 9071B T

500-53491-A-1 FC COMPOSITE 6 10.2075 g 10 mL 5 mL

MSD

9071B, 9071B T

500-53491-A-2 FC D COMPOSITE 6 9071B, 9071B T 10.2202 g 10 mL

Batch Notes

Acid used for pH adjust Lot # J23A13

Balance ID 1634

Concentration End Time See end date / time

Concentration Start Time See start date / time

Evaporator Temperature 50 DEG. C

Filter Paper Lot Number 8293623

Hexane Lot# HEXANES_00012

Na2SO4 Lot Number Na2SO4_00006

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

9071B Page 1 of 1

Page 373 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Brogan, Mary T

01/04/13 11:25

174372 01/04/13 09:45

Batch Method:

TestAmerica Chicago

9071B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount RECTUBE# ReceiverTube RecTubeWExtract

1

RecTubeWExtract

2

MB 10 mL 10 mL 02 2.2548 g 2.2560 g 2.2558 g

500-174369/1-A

9071B

LCS 10 mL 10 mL 03 2.2560 g 2.2967 g 2.2965 g

500-174369/2-A

9071B

500-53491-A-1-J FC COMPOSITE 6 9071B T 10 mL 10 mL 09 2.3010 g 2.3458 g 2.3458 g

500-53491-A-1-K FC COMPOSITE 6 10 mL 10 mL 12 2.3005 g 2.4074 g 2.4070 g

MS

9071B T

500-53491-A-1-L FC COMPOSITE 6 10 mL 10 mL 66 2.3495 g 2.4586 g 2.4585 g

MSD

9071B T

500-53491-A-2-N FC D COMPOSITE 6 9071B T 10 mL 10 mL 79 2.2391 g 2.2830 g 2.2827 g

Lab Sample ID Client Sample ID Method Chain Basis WeightOne%Diff Residue Residue2

Pass_0.0005g 0.0011999999999

9987 g

0.0009999999999

9989 g

MB 

500-174369/1-A

9071B

Pass_0.0005g 0.0407000000000

002 g

0.0405000000000

002 g

LCS 

500-174369/2-A

9071B

500-53491-A-1-J FC COMPOSITE 6 9071B T Pass_0.0005g 0.0448 g 0.0448 g

500-53491-A-1-K FC COMPOSITE 6 Pass_0.0005g 0.1069 g 0.1065 g

MS

9071B T

500-53491-A-1-L FC COMPOSITE 6 Pass_0.0005g 0.1091 g 0.109 g

MSD

9071B T

FC D COMPOSITE 6 Pass_0.0005g 0.0438999999999

998 g

0.0436000000000

001 g

500-53491-A-2-N 9071B T

Batch Notes

Balance ID 1634

Calibration Check After 2nd Weighing 0.0020 / 1.0000

Calibration Check Before 1st Weighing 0.0020 / 1.0001

Evaporator Temperature 50 Celsius

Filter Paper Lot # 8293623

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

9071B Page 1 of 1

Page 374 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

173788 12/22/12 09:29 Veldhuizen, Chris M

Batch Method:

TestAmerica Chicago

Moisture

Lab Sample ID Client Sample ID Method Chain Basis DISH# DishWeight SampleMassWet SampleMassDry

500-53491-A-1 FC COMPOSITE 6 Moisture T 7 1.27 g 11.28 g 3.92 g

500-53491-A-2 FC D COMPOSITE 6 Moisture T 8 1.27 g 11.32 g 3.79 g

Batch Notes

Balance ID 971 No Unit

Date samples were placed in the oven 12/22/12

Oven Temp when samples are put in oven 105 Degrees C

Time samples were place in the oven 0935

Date samples were removed from oven 12/24/12

Oven Temp when samples removed from oven 105 Degrees C

Oven ID 776

ID number of the thermometer c-1966

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

Moisture Page 1 of 1

Page 375 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

174071 12/28/12 07:50 Veldhuizen, Chris M

Batch Method:

TestAmerica Chicago

Moisture

Lab Sample ID Client Sample ID Method Chain Basis DISH# DishWeight SampleMassWet SampleMassDry

500-53491-A-3 FC DISCRETE 6 Moisture T 9 1.28 g 11.30 g 3.88 g

500-53491-A-4 FC D DISCRETE 6 Moisture T 10 1.27 g 11.33 g 4.05 g

Batch Notes

Balance ID 971 No Unit

Date samples were placed in the oven 12/28/12

Oven Temp when samples are put in oven 105 Degrees C

Time samples were place in the oven 0800

Date samples were removed from oven 12/29/12

Oven Temp when samples removed from oven 105 Degrees C

Time Samples were removed from oven 0845

Oven ID 776

ID number of the thermometer c-1966

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

Moisture Page 1 of 1

Page 376 of 384 01/09/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53491-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

173970 12/27/12 07:30 Veldhuizen, Chris M

Batch Method:

TestAmerica Chicago

SM 2540G

Lab Sample ID Client Sample ID Method Chain Basis CalcMsg

FC COMPOSITE 6 Not Calculated. 

RunCalculation 

is NULL

500-53491-A-1 SM 2540G T

FC D COMPOSITE 6 Not Calculated. 

RunCalculation 

is NULL

500-53491-A-2 SM 2540G T

Batch Notes

Basis Basis Description

T Total/NA

The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for 

this reagent.

SM 2540G Page 1 of 1

Page 377 of 384 01/09/2013






Login Sample Receipt Checklist

Client: Project Integration, Inc Job Number: 500-53491-1

Login Number: 53491

Question Answer Comment

Creator: Lunt, Jeff T

List Source: TestAmerica Chicago

List Number: 1

Radioactivity wasn't checked or is </= background as measured by a survey True

meter.

The cooler's custody seal, if present, is intact. True

Sample custody seals, if present, are intact. True

The cooler or samples do not appear to have been compromised or True

tampered with.

Samples were received on ice. True 1.3

Cooler Temperature is acceptable. True

Cooler Temperature is recorded. True

COC is present. True

COC is filled out in ink and legible. True

COC is filled out with all pertinent information. True

Is the Field Sampler's name present on COC? True

There are no discrepancies between the containers received and the COC. True

Samples are received within Holding Time. False

Sample containers have legible labels. True

Containers are not broken or leaking. True

Sample collection date/times are provided. True

Appropriate sample containers are used. True

Sample bottles are completely filled. True

Sample Preservation Verified. True

There is sufficient vol. for all requested analyses, incl. any requested True

MS/MSDs

Containers requiring zero headspace have no headspace or bubble is True

<6mm (1/4").

Multiphasic samples are not present. True

Samples do not require splitting or compositing. True

Residual Chlorine Checked. N/A

TestAmerica Chicago Page 384 of 384 01/09/2013
ANALYTICAL REPORT

TestAmerica Laboratories, Inc.

TestAmerica Chicago

2417 Bond Street

University Park, IL 60484

Tel: (708)534-5200

TestAmerica Job ID: 500-53491-1

Client Project/Site: John Deere Des Moines Works (JDDMW)

For:

Project Integration, Inc

1097 Highway 101 South

Suite D-16

Greer, South Carolina 29651

Attn: Mr. Robert Stevens

Authorized for release by:

1/9/2013 2:45:21 PM

Donna Ingersoll

Project Manager II

donna.ingersoll@testamericainc.com

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited

parameters, exceptions are noted in this report. This report may not be reproduced except in full,

and with written approval from the laboratory. For questions please contact the Project Manager

at the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature is

intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15
Table of Contents

Client: Project Integration, Inc

Project/Site: John Deere Des Moines Works (JDDMW)

TestAmerica Job ID: 500-53491-1

Page 2 of 36

TestAmerica Chicago

1/9/2013

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22

Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15
Case Narrative

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Job ID: 500-53491-1

Laboratory: TestAmerica Chicago

Narrative

Job Narrative

500-53491-1

Comments

No additional comments. 

Receipt 

The samples were received on 12/22/2012 11:30 AM; the samples arrived in good condition, properly preserved and, where required, on 

ice. The temperature of the cooler at receipt was 1.3o C.

Except:

Cr+6 past hold time.

GC/MS VOA 

No analytical or quality issues were noted.

Metals 

No analytical or quality issues were noted.

General Chemistry 

Method(s) 9071B: The oil and grease matrix spike / matrix spike duplicate (MS/MSD) recoveries for sample 500-53491-1 in batch 174372 

were outside control limits. The associated laboratory control sample (LCS) recovery met acceptance criteria.

No other analytical or quality issues were noted.

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Detection Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC COMPOSITE 6 Lab Sample ID: 500-53491-1

Barium ☼

RL

3.70 mg/Kg

MDL

0.440

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

643 1 6010B Total/NA

Copper 748 3.70 1.00 mg/Kg 1 ☼ 6010B Total/NA

Chromium 15000 3.70 0.618 mg/Kg 1 ☼ 6010B Total/NA

Nickel 85.5 3.70 0.810 mg/Kg 1 ☼ 6010B Total/NA

Lead 253 B 1.85 0.636 mg/Kg 1 ☼ 6010B Total/NA

Vanadium 253 1.85 0.281 mg/Kg 1 ☼ 6010B Total/NA

Zinc 501 7.40 2.54 mg/Kg 1 ☼ 6010B Total/NA

Barium 0.0103 J 0.500 0.0100 mg/L 1 6010B TCLP

Copper 0.442 0.0250 0.0100 mg/L 1 6010B TCLP

Chromium 0.826 0.0250 0.0100 mg/L 1 6010B TCLP

Nickel 0.744 0.0250 0.0100 mg/L 1 6010B TCLP

Vanadium 0.0164 J 0.0250 0.00500 mg/L 1 6010B TCLP

Zinc 0.403 0.100 0.0200 mg/L 1 6010B TCLP

Mercury 0.000702 B 0.000200 0.0000200 mg/L 1 7470A TCLP

Mercury 0.232 0.0605 0.0231 mg/Kg 1 ☼ 7471A Total/NA

Flashpoint >176 40.0 40.0 Degrees F 1 1010 Total/NA

Cyanide, Total 1.15 J 1.88 0.622 mg/Kg 1 ☼ 9014 Total/NA

Sulfide 778 90.4 14.5 mg/Kg 1 ☼ 9034 Total/NA

pH 9.79 0.200 0.200 SU 1 9045C Total/NA

HEM (Oil & Grease) 16600 1850 822 mg/Kg 1 ☼ 9071B Total/NA

Total Solids 26.0 0.100 0.100 % 1 SM 2540G Total/NA

Client Sample ID: FC D COMPOSITE 6 Lab Sample ID: 500-53491-2

Barium ☼

RL

3.84 mg/Kg

MDL

0.457

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

619 1 6010B Total/NA

Copper 707 3.84 1.04 mg/Kg 1 ☼ 6010B Total/NA

Chromium 15000 3.84 0.642 mg/Kg 1 ☼ 6010B Total/NA

Nickel 86.1 3.84 0.841 mg/Kg 1 ☼ 6010B Total/NA

Lead 244 B 1.92 0.661 mg/Kg 1 ☼ 6010B Total/NA

Vanadium 251 1.92 0.292 mg/Kg 1 ☼ 6010B Total/NA

Zinc 499 7.68 2.64 mg/Kg 1 ☼ 6010B Total/NA

Copper 0.0547 0.0250 0.0100 mg/L 1 6010B TCLP

Nickel 0.0624 0.0250 0.0100 mg/L 1 6010B TCLP

Mercury 0.237 0.0647 0.0247 mg/Kg 1 ☼ 7471A Total/NA

Flashpoint >176 40.0 40.0 Degrees F 1 1010 Total/NA

Cyanide, Total 1.29 J 1.86 0.615 mg/Kg 1 ☼ 9014 Total/NA

Sulfide 817 94.0 15.0 mg/Kg 1 ☼ 9034 Total/NA

pH 9.87 0.200 0.200 SU 1 9045C Total/NA

HEM (Oil & Grease) 17000 1950 866 mg/Kg 1 ☼ 9071B Total/NA

Total Solids 25.0 0.100 0.100 % 1 SM 2540G Total/NA

Client Sample ID: FC DISCRETE 6 Lab Sample ID: 500-53491-3

2-Butanone (MEK) ☼

RL

19.3 ug/Kg

MDL

6.98

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

11.8 J 1 8260B Total/NA

Acetone - DL 7020 963 251 ug/Kg 50 ☼ 8260B Total/NA

Client Sample ID: FC D DISCRETE 6 Lab Sample ID: 500-53491-4

2-Butanone (MEK) ☼

RL

18.1 ug/Kg

MDL

6.55

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

19.5 1 8260B Total/NA

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Detection Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC D DISCRETE 6 (Continued) Lab Sample ID: 500-53491-4

Acetone - DL ☼

RL

905 ug/Kg

MDL

235

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

7150 50 8260B Total/NA

Client Sample ID: FC EB 6 Lab Sample ID: 500-53491-5

Copper

RL

0.0100 mg/L

MDL

0.00106

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

0.00111 J 1 6010B Total/NA

Client Sample ID: TRIP BLANK Lab Sample ID: 500-53491-6

 No Detections

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Method Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method Method Description Protocol Laboratory

8260B Volatile Organic Compounds (GC/MS) SW846 TAL CHI

6010B Metals (ICP) SW846 TAL CHI

7470A Mercury (CVAA) SW846 TAL CHI

7471A Mercury (CVAA) SW846 TAL CHI

1010 Ignitability, Pensky-Martens Closed-Cup Method SW846 TAL CHI

1664A HEM and SGT-HEM 1664A TAL CHI

7196A Chromium, Hexavalent SW846 TAL CHI

9014 Cyanide SW846 TAL CHI

9034 Sulfide, Acid soluble and Insoluble (Titrimetric) SW846 TAL CHI

9034 Sulfide, Reactive SW846 TAL CHI

9045C pH SW846 TAL CHI

9071B HEM and SGT-HEM SW846 TAL CHI

Moisture Percent Moisture EPA TAL CHI

SM 2540G Total, Fixed, and Volatile Solids SM TAL CHI

Protocol References:

1664A = EPA-821-98-002

EPA = US Environmental Protection Agency

SM = "Standard Methods For The Examination Of Water And Wastewater",

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200

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Sample Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Lab Sample ID Client Sample ID Matrix Collected Received

500-53491-1 FC COMPOSITE 6 Solid 12/19/12 14:30 12/22/12 11:30

500-53491-2 FC D COMPOSITE 6 Solid 12/19/12 14:40 12/22/12 11:30

500-53491-3 FC DISCRETE 6 Solid 12/19/12 14:20 12/22/12 11:30

500-53491-4 FC D DISCRETE 6 Solid 12/19/12 14:45 12/22/12 11:30

500-53491-5 FC EB 6 Water 12/19/12 14:10 12/22/12 11:30

500-53491-6 TRIP BLANK Water 12/19/12 00:00 12/22/12 11:30

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Client Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC COMPOSITE 6 Lab Sample ID: 500-53491-1

Date Collected: 12/19/12 14:30 Matrix: Solid

Date Received: 12/22/12 11:30 Percent Solids: 26.5

Method: 6010B - Metals (ICP)

RL MDL

Barium 643 3.70 0.440 mg/Kg ☼ 12/24/12 15:00 12/26/12 23:57 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper 748 3.70 1.00 mg/Kg ☼ 12/24/12 15:00 12/26/12 23:57 1

Chromium 15000 3.70 0.618 mg/Kg ☼ 12/24/12 15:00 12/26/12 23:57 1

Nickel 85.5 3.70 0.810 mg/Kg ☼ 12/24/12 15:00 12/26/12 23:57 1

Lead 253 B 1.85 0.636 mg/Kg ☼ 12/24/12 15:00 12/26/12 23:57 1

Vanadium 253 1.85 0.281 mg/Kg ☼ 12/24/12 15:00 12/26/12 23:57 1

Zinc 501 7.40 2.54 mg/Kg ☼ 12/24/12 15:00 12/26/12 23:57 1

Method: 6010B - Metals (ICP) - TCLP

RL MDL

Barium 0.0103 J 0.500 0.0100 mg/L 12/26/12 07:50 12/26/12 18:41 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper 0.442 0.0250 0.0100 mg/L 12/26/12 07:50 12/26/12 18:41 1

Chromium 0.826 0.0250 0.0100 mg/L 12/26/12 07:50 12/26/12 18:41 1

Nickel 0.744 0.0250 0.0100 mg/L 12/26/12 07:50 12/26/12 18:41 1

Lead <0.0500 0.0500 0.00500 mg/L 12/26/12 07:50 12/26/12 18:41 1

Vanadium 0.0164 J 0.0250 0.00500 mg/L 12/26/12 07:50 12/26/12 18:41 1

Zinc 0.403 0.100 0.0200 mg/L 12/26/12 07:50 12/26/12 18:41 1

Method: 7470A - Mercury (CVAA) - TCLP

RL MDL

Mercury 0.000702 B 0.000200 0.0000200 mg/L 12/26/12 13:00 12/27/12 09:57 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Method: 7471A - Mercury (CVAA)

RL MDL

Mercury 0.232 0.0605 0.0231 mg/Kg ☼ 12/26/12 14:00 12/27/12 08:55 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

General Chemistry

RL MDL

Flashpoint >176 40.0 40.0 Degrees F 01/02/13 09:30 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Chromium, hexavalent <3.75 3.75 1.46 mg/Kg ☼ 12/22/12 12:00 12/27/12 12:51 1

Cyanide, Total 1.15 J 1.88 0.622 mg/Kg ☼ 12/28/12 11:20 12/28/12 15:31 1

Sulfide 778 90.4 14.5 mg/Kg ☼ 12/28/12 12:20 12/28/12 14:43 1

Sulfide, Reactive <48.5 48.5 3.78 mg/Kg 12/28/12 11:57 12/28/12 12:58 1

pH 9.79 0.200 0.200 SU 12/26/12 14:25 1

HEM (Oil & Grease) 16600 1850 822 mg/Kg ☼ 01/04/13 05:35 01/04/13 10:13 1

Total Solids 26.0 0.100 0.100 % 12/27/12 07:30 1

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Client Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC D COMPOSITE 6 Lab Sample ID: 500-53491-2

Date Collected: 12/19/12 14:40 Matrix: Solid

Date Received: 12/22/12 11:30 Percent Solids: 25.1

Method: 6010B - Metals (ICP)

RL MDL

Barium 619 3.84 0.457 mg/Kg ☼ 12/24/12 15:00 12/27/12 00:03 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper 707 3.84 1.04 mg/Kg ☼ 12/24/12 15:00 12/27/12 00:03 1

Chromium 15000 3.84 0.642 mg/Kg ☼ 12/24/12 15:00 12/27/12 00:03 1

Nickel 86.1 3.84 0.841 mg/Kg ☼ 12/24/12 15:00 12/27/12 00:03 1

Lead 244 B 1.92 0.661 mg/Kg ☼ 12/24/12 15:00 12/27/12 00:03 1

Vanadium 251 1.92 0.292 mg/Kg ☼ 12/24/12 15:00 12/27/12 00:03 1

Zinc 499 7.68 2.64 mg/Kg ☼ 12/24/12 15:00 12/27/12 00:03 1

Method: 6010B - Metals (ICP) - TCLP

RL MDL

Barium <0.500 0.500 0.0100 mg/L 12/26/12 07:50 12/26/12 18:47 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper 0.0547 0.0250 0.0100 mg/L 12/26/12 07:50 12/26/12 18:47 1

Chromium <0.0250 0.0250 0.0100 mg/L 12/26/12 07:50 12/26/12 18:47 1

Nickel 0.0624 0.0250 0.0100 mg/L 12/26/12 07:50 12/26/12 18:47 1

Lead <0.0500 0.0500 0.00500 mg/L 12/26/12 07:50 12/26/12 18:47 1

Vanadium <0.0250 0.0250 0.00500 mg/L 12/26/12 07:50 12/26/12 18:47 1

Zinc <0.100 0.100 0.0200 mg/L 12/26/12 07:50 12/26/12 18:47 1

Method: 7470A - Mercury (CVAA) - TCLP

RL MDL

Mercury <0.000200 0.000200 0.0000200 mg/L 12/26/12 13:00 12/27/12 09:58 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Method: 7471A - Mercury (CVAA)

RL MDL

Mercury 0.237 0.0647 0.0247 mg/Kg ☼ 12/26/12 14:00 12/27/12 09:04 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

General Chemistry

RL MDL

Flashpoint >176 40.0 40.0 Degrees F 01/02/13 10:52 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Chromium, hexavalent <3.99 3.99 1.55 mg/Kg ☼ 12/22/12 12:00 12/27/12 12:53 1

Cyanide, Total 1.29 J 1.86 0.615 mg/Kg ☼ 12/28/12 11:20 12/28/12 15:31 1

Sulfide 817 94.0 15.0 mg/Kg ☼ 12/28/12 12:20 12/28/12 14:44 1

Sulfide, Reactive <49.3 49.3 3.85 mg/Kg 12/28/12 12:01 12/28/12 12:59 1

pH 9.87 0.200 0.200 SU 12/26/12 14:27 1

HEM (Oil & Grease) 17000 1950 866 mg/Kg ☼ 01/04/13 05:35 01/04/13 10:56 1

Total Solids 25.0 0.100 0.100 % 12/27/12 07:30 1

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Client Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC DISCRETE 6 Lab Sample ID: 500-53491-3

Date Collected: 12/19/12 14:20 Matrix: Solid

Date Received: 12/22/12 11:30 Percent Solids: 25.9

Method: 8260B - Volatile Organic Compounds (GC/MS)

RL MDL

2-Butanone (MEK) 11.8 J 19.3 6.98 ug/Kg ☼ 12/27/12 13:36 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

1,2-Dichloroethane-d4 (Surr) 89 70 - 134 12/27/12 13:36 1

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 87 75 - 122 12/27/12 13:36 1

4-Bromofluorobenzene (Surr) 79 70 - 122 12/27/12 13:36 1

Dibromofluoromethane 95 75 - 120 12/27/12 13:36 1

Method: 8260B - Volatile Organic Compounds (GC/MS) - DL

RL MDL

Acetone 7020 963 251 ug/Kg ☼ 12/27/12 10:28 12/28/12 11:08 50

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

1,2-Dichloroethane-d4 (Surr) 97 75 - 125 12/27/12 10:28 12/28/12 11:08 50

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 96 75 - 120 12/27/12 10:28 12/28/12 11:08 50

4-Bromofluorobenzene (Surr) 94 75 - 120 12/27/12 10:28 12/28/12 11:08 50

Dibromofluoromethane 93 75 - 120 12/27/12 10:28 12/28/12 11:08 50

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Client Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC D DISCRETE 6 Lab Sample ID: 500-53491-4

Date Collected: 12/19/12 14:45 Matrix: Solid

Date Received: 12/22/12 11:30 Percent Solids: 27.6

Method: 8260B - Volatile Organic Compounds (GC/MS)

RL MDL

2-Butanone (MEK) 19.5 18.1 6.55 ug/Kg ☼ 12/27/12 13:59 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

1,2-Dichloroethane-d4 (Surr) 91 70 - 134 12/27/12 13:59 1

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 89 75 - 122 12/27/12 13:59 1

4-Bromofluorobenzene (Surr) 75 70 - 122 12/27/12 13:59 1

Dibromofluoromethane 90 75 - 120 12/27/12 13:59 1

Method: 8260B - Volatile Organic Compounds (GC/MS) - DL

RL MDL

Acetone 7150 905 235 ug/Kg ☼ 12/27/12 10:28 12/28/12 11:31 50

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

1,2-Dichloroethane-d4 (Surr) 105 75 - 125 12/27/12 10:28 12/28/12 11:31 50

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 101 75 - 120 12/27/12 10:28 12/28/12 11:31 50

4-Bromofluorobenzene (Surr) 100 75 - 120 12/27/12 10:28 12/28/12 11:31 50

Dibromofluoromethane 96 75 - 120 12/27/12 10:28 12/28/12 11:31 50

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Client Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC EB 6 Lab Sample ID: 500-53491-5

Date Collected: 12/19/12 14:10 Matrix: Water

Date Received: 12/22/12 11:30

Method: 8260B - Volatile Organic Compounds (GC/MS)

RL MDL

Acetone <5.00 5.00 1.29 ug/L 12/27/12 15:54 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

2-Butanone (MEK) <5.00 5.00 1.47 ug/L 12/27/12 15:54 1

1,2-Dichloroethane-d4 (Surr) 88 75 - 125 12/27/12 15:54 1

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 94 75 - 120 12/27/12 15:54 1

4-Bromofluorobenzene (Surr) 88 75 - 120 12/27/12 15:54 1

Dibromofluoromethane 90 75 - 120 12/27/12 15:54 1

Method: 6010B - Metals (ICP)

RL MDL

Barium <0.0100 0.0100 0.000440 mg/L 12/24/12 14:30 12/26/12 17:03 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper 0.00111 J 0.0100 0.00106 mg/L 12/24/12 14:30 12/26/12 17:03 1

Chromium <0.0100 0.0100 0.000960 mg/L 12/24/12 14:30 12/26/12 17:03 1

Nickel <0.0100 0.0100 0.00190 mg/L 12/24/12 14:30 12/26/12 17:03 1

Lead <0.00500 0.00500 0.00158 mg/L 12/24/12 14:30 12/26/12 17:03 1

Vanadium <0.00500 0.00500 0.000620 mg/L 12/24/12 14:30 12/26/12 17:03 1

Zinc <0.0200 0.0200 0.00472 mg/L 12/24/12 14:30 12/26/12 17:03 1

Method: 7470A - Mercury (CVAA)

RL MDL

Mercury <0.000200 0.000200 0.0000710 mg/L 12/26/12 13:00 12/27/12 09:26 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

General Chemistry

RL MDL

HEM (Oil & Grease) <5.33 5.33 1.55 mg/L 01/08/13 06:01 01/08/13 11:08 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Chromium, hexavalent <0.0100 H 0.0100 0.00325 mg/L 12/22/12 14:12 1

Cyanide, Total <0.0100 0.0100 0.00331 mg/L 12/27/12 09:50 12/27/12 14:45 1

Sulfide <1.00 1.00 0.230 mg/L 12/24/12 14:00 1

Sulfide, Reactive <1.00 1.00 1.00 mg/L 12/24/12 08:45 12/24/12 13:51 1

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Client Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: TRIP BLANK Lab Sample ID: 500-53491-6

Date Collected: 12/19/12 00:00 Matrix: Water

Date Received: 12/22/12 11:30

Method: 8260B - Volatile Organic Compounds (GC/MS)

RL MDL

Acetone <5.00 5.00 1.29 ug/L 12/27/12 15:28 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

2-Butanone (MEK) <5.00 5.00 1.47 ug/L 12/27/12 15:28 1

1,2-Dichloroethane-d4 (Surr) 93 75 - 125 12/27/12 15:28 1

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 100 75 - 120 12/27/12 15:28 1

4-Bromofluorobenzene (Surr) 93 75 - 120 12/27/12 15:28 1

Dibromofluoromethane 93 75 - 120 12/27/12 15:28 1

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Definitions/Glossary

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Qualifiers

GC/MS VOA

Qualifier Description

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Qualifier

Metals

Qualifier Description

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Qualifier

B Compound was found in the blank and sample.

General Chemistry

Qualifier Description

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Qualifier

F MS or MSD exceeds the control limits

H Sample was prepped or analyzed beyond the specified holding time

Glossary

These commonly used abbreviations may or may not be present in this report.

☼ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

DL, RA, RE, IN Indicates a Dilution, Reanalysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

EDL Estimated Detection Limit

EPA United States Environmental Protection Agency

MDA Minimum detectable activity

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

GC/MS VOA

Analysis Batch: 173973

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-3 FC DISCRETE 6 Total/NA Solid 8260B

500-53491-4 FC D DISCRETE 6 Total/NA Solid 8260B

LCS 500-173973/6 Lab Control Sample Total/NA Solid 8260B

LCSD 500-173973/7 Lab Control Sample Dup Total/NA Solid 8260B

MB 500-173973/5 Method Blank Total/NA Solid 8260B

Analysis Batch: 173987

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-5 FC EB 6 Total/NA Water 8260B

500-53491-6 TRIP BLANK Total/NA Water 8260B

LCS 500-173987/4 Lab Control Sample Total/NA Water 8260B

MB 500-173987/7 Method Blank Total/NA Water 8260B

Prep Batch: 173990

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-3 - DL FC DISCRETE 6 Total/NA Solid 5030B

500-53491-4 - DL FC D DISCRETE 6 Total/NA Solid 5030B

Analysis Batch: 174064

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-3 - DL FC DISCRETE 6 Total/NA Solid 8260B 173990

500-53491-4 - DL FC D DISCRETE 6 Total/NA Solid 8260B 173990

LCS 500-174064/4 Lab Control Sample Total/NA Solid 8260B

MB 500-174064/6 Method Blank Total/NA Solid 8260B

Metals

Leach Batch: 173836

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-2 FC D COMPOSITE 6 TCLP Solid 1311

500-53491-2 DU FC D COMPOSITE 6 TCLP Solid 1311

500-53491-2 MS FC D COMPOSITE 6 TCLP Solid 1311

LB 500-173836/1-B LB Method Blank TCLP Solid 1311

LB 500-173836/1-C LB Method Blank TCLP Solid 1311

Leach Batch: 173838

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 TCLP Solid 1311

LB2 500-173838/1-B LB2 Method Blank TCLP Solid 1311

LB2 500-173838/1-C LB2 Method Blank TCLP Solid 1311

Prep Batch: 173848

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 Total/NA Solid 3050B

500-53491-2 FC D COMPOSITE 6 Total/NA Solid 3050B

LCS 500-173848/2-A Lab Control Sample Total/NA Solid 3050B

MB 500-173848/1-A Method Blank Total/NA Solid 3050B

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Metals (Continued)

Prep Batch: 173849

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-5 FC EB 6 Total/NA Water 3010A

LCS 500-173849/2-A Lab Control Sample Total/NA Water 3010A

MB 500-173849/1-A Method Blank Total/NA Water 3010A

Prep Batch: 173872

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 TCLP Solid 3010A 173838

500-53491-2 FC D COMPOSITE 6 TCLP Solid 3010A 173836

LB 500-173836/1-B LB Method Blank TCLP Solid 3010A 173836

LB2 500-173838/1-B LB2 Method Blank TCLP Solid 3010A 173838

LCS 500-173872/3-A Lab Control Sample Total/NA Solid 3010A

Prep Batch: 173881

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 Total/NA Solid 7471A

500-53491-2 FC D COMPOSITE 6 Total/NA Solid 7471A

LCS 500-173881/8-A Lab Control Sample Total/NA Solid 7471A

MB 500-173881/7-A Method Blank Total/NA Solid 7471A

Prep Batch: 173908

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-5 FC EB 6 Total/NA Water 7470A

LCS 500-173908/8-A Lab Control Sample Total/NA Water 7470A

MB 500-173908/7-A Method Blank Total/NA Water 7470A

Prep Batch: 173909

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 TCLP Solid 7470A 173838

500-53491-2 FC D COMPOSITE 6 TCLP Solid 7470A 173836

500-53491-2 DU FC D COMPOSITE 6 TCLP Solid 7470A 173836

500-53491-2 MS FC D COMPOSITE 6 TCLP Solid 7470A 173836

LB 500-173836/1-C LB Method Blank TCLP Solid 7470A 173836

LB2 500-173838/1-C LB2 Method Blank TCLP Solid 7470A 173838

LCS 500-173909/8-A Lab Control Sample Total/NA Solid 7470A

MB 500-173909/7-A Method Blank Total/NA Solid 7470A

Analysis Batch: 173963

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-5 FC EB 6 Total/NA Water 6010B 173849

LCS 500-173849/2-A Lab Control Sample Total/NA Water 6010B 173849

MB 500-173849/1-A Method Blank Total/NA Water 6010B 173849

Analysis Batch: 173964

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 TCLP Solid 6010B 173872

500-53491-1 FC COMPOSITE 6 Total/NA Solid 6010B 173848

500-53491-2 FC D COMPOSITE 6 TCLP Solid 6010B 173872

500-53491-2 FC D COMPOSITE 6 Total/NA Solid 6010B 173848

LB 500-173836/1-B LB Method Blank TCLP Solid 6010B 173872

LB2 500-173838/1-B LB2 Method Blank TCLP Solid 6010B 173872

LCS 500-173848/2-A Lab Control Sample Total/NA Solid 6010B 173848

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Metals (Continued)

Analysis Batch: 173964 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

LCS 500-173872/3-A Lab Control Sample Total/NA Solid 6010B 173872

MB 500-173848/1-A Method Blank Total/NA Solid 6010B 173848

Analysis Batch: 173984

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 Total/NA Solid 7471A 173881

500-53491-2 FC D COMPOSITE 6 Total/NA Solid 7471A 173881

LCS 500-173881/8-A Lab Control Sample Total/NA Solid 7471A 173881

MB 500-173881/7-A Method Blank Total/NA Solid 7471A 173881

Analysis Batch: 173997

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 TCLP Solid 7470A 173909

500-53491-2 FC D COMPOSITE 6 TCLP Solid 7470A 173909

500-53491-2 DU FC D COMPOSITE 6 TCLP Solid 7470A 173909

500-53491-2 MS FC D COMPOSITE 6 TCLP Solid 7470A 173909

500-53491-5 FC EB 6 Total/NA Water 7470A 173908

LB 500-173836/1-C LB Method Blank TCLP Solid 7470A 173909

LB2 500-173838/1-C LB2 Method Blank TCLP Solid 7470A 173909

LCS 500-173908/8-A Lab Control Sample Total/NA Water 7470A 173908

LCS 500-173909/8-A Lab Control Sample Total/NA Solid 7470A 173909

MB 500-173908/7-A Method Blank Total/NA Water 7470A 173908

MB 500-173909/7-A Method Blank Total/NA Solid 7470A 173909

General Chemistry

Analysis Batch: 173788

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 Total/NA Solid Moisture

500-53491-2 FC D COMPOSITE 6 Total/NA Solid Moisture

Prep Batch: 173790

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 Total/NA Solid 3060A

500-53491-2 FC D COMPOSITE 6 Total/NA Solid 3060A

LCS 500-173790/2-A Lab Control Sample Total/NA Solid 3060A

LCS 500-173790/3-A Lab Control Sample Total/NA Solid 3060A

MB 500-173790/1-A Method Blank Total/NA Solid 3060A

Analysis Batch: 173793

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-5 FC EB 6 Total/NA Water 7196A

500-53491-5 MS FC EB 6 Total/NA Water 7196A

500-53491-5 MSD FC EB 6 Total/NA Water 7196A

LCS 500-173793/4 Lab Control Sample Total/NA Water 7196A

MB 500-173793/3 Method Blank Total/NA Water 7196A

Prep Batch: 173844

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-5 FC EB 6 Total/NA Water 7.3.4

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

General Chemistry (Continued)

Prep Batch: 173844 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

LCS 500-173844/2-A Lab Control Sample Total/NA Water 7.3.4

MB 500-173844/1-A Method Blank Total/NA Water 7.3.4

Analysis Batch: 173845

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-5 FC EB 6 Total/NA Water 9034 173844

LCS 500-173844/2-A Lab Control Sample Total/NA Water 9034 173844

MB 500-173844/1-A Method Blank Total/NA Water 9034 173844

Analysis Batch: 173846

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-5 FC EB 6 Total/NA Water 9034

LCS 500-173846/2 Lab Control Sample Total/NA Water 9034

MB 500-173846/1 Method Blank Total/NA Water 9034

Analysis Batch: 173936

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 Total/NA Solid 9045C

500-53491-2 FC D COMPOSITE 6 Total/NA Solid 9045C

Analysis Batch: 173970

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 Total/NA Solid SM 2540G

500-53491-2 FC D COMPOSITE 6 Total/NA Solid SM 2540G

Prep Batch: 173980

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-5 FC EB 6 Total/NA Water 9010B

LCS 500-173980/2-A Lab Control Sample Total/NA Water 9010B

MB 500-173980/1-A Method Blank Total/NA Water 9010B

Analysis Batch: 174027

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 Total/NA Solid 7196A 173790

500-53491-2 FC D COMPOSITE 6 Total/NA Solid 7196A 173790

LCS 500-173790/2-A Lab Control Sample Total/NA Solid 7196A 173790

LCS 500-173790/3-A Lab Control Sample Total/NA Solid 7196A 173790

MB 500-173790/1-A Method Blank Total/NA Solid 7196A 173790

Analysis Batch: 174042

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-5 FC EB 6 Total/NA Water 9014 173980

LCS 500-173980/2-A Lab Control Sample Total/NA Water 9014 173980

MB 500-173980/1-A Method Blank Total/NA Water 9014 173980

Analysis Batch: 174071

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-3 FC DISCRETE 6 Total/NA Solid Moisture

500-53491-4 FC D DISCRETE 6 Total/NA Solid Moisture

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

General Chemistry (Continued)

Prep Batch: 174096

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 Total/NA Solid 9010B

500-53491-2 FC D COMPOSITE 6 Total/NA Solid 9010B

500-53491-2 MS FC D COMPOSITE 6 Total/NA Solid 9010B

500-53491-2 MSD FC D COMPOSITE 6 Total/NA Solid 9010B

LCS 500-174096/13-A Lab Control Sample Total/NA Solid 9010B

MB 500-174096/12-A Method Blank Total/NA Solid 9010B

Prep Batch: 174100

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 Total/NA Solid 9030B

500-53491-2 FC D COMPOSITE 6 Total/NA Solid 9030B

LCS 500-174100/2-A Lab Control Sample Total/NA Solid 9030B

MB 500-174100/1-A Method Blank Total/NA Solid 9030B

Prep Batch: 174101

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 Total/NA Solid 7.3.4

500-53491-2 FC D COMPOSITE 6 Total/NA Solid 7.3.4

LCS 500-174101/2-A Lab Control Sample Total/NA Solid 7.3.4

MB 500-174101/1-A Method Blank Total/NA Solid 7.3.4

Analysis Batch: 174144

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 Total/NA Solid 9034 174100

500-53491-2 FC D COMPOSITE 6 Total/NA Solid 9034 174100

LCS 500-174100/2-A Lab Control Sample Total/NA Solid 9034 174100

MB 500-174100/1-A Method Blank Total/NA Solid 9034 174100

Analysis Batch: 174145

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 Total/NA Solid 9034 174101

500-53491-2 FC D COMPOSITE 6 Total/NA Solid 9034 174101

LCS 500-174101/2-A Lab Control Sample Total/NA Solid 9034 174101

MB 500-174101/1-A Method Blank Total/NA Solid 9034 174101

Analysis Batch: 174173

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 Total/NA Solid 9014 174096

500-53491-2 FC D COMPOSITE 6 Total/NA Solid 9014 174096

500-53491-2 MS FC D COMPOSITE 6 Total/NA Solid 9014 174096

500-53491-2 MSD FC D COMPOSITE 6 Total/NA Solid 9014 174096

LCS 500-174096/13-A Lab Control Sample Total/NA Solid 9014 174096

MB 500-174096/12-A Method Blank Total/NA Solid 9014 174096

Analysis Batch: 174336

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 Total/NA Solid 1010

500-53491-2 FC D COMPOSITE 6 Total/NA Solid 1010

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

General Chemistry (Continued)

Prep Batch: 174369

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 Total/NA Solid 9071B

500-53491-1 MS FC COMPOSITE 6 Total/NA Solid 9071B

500-53491-1 MSD FC COMPOSITE 6 Total/NA Solid 9071B

500-53491-2 FC D COMPOSITE 6 Total/NA Solid 9071B

LCS 500-174369/2-A Lab Control Sample Total/NA Solid 9071B

MB 500-174369/1-A Method Blank Total/NA Solid 9071B

Analysis Batch: 174372

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-1 FC COMPOSITE 6 Total/NA Solid 9071B 174369

500-53491-1 MS FC COMPOSITE 6 Total/NA Solid 9071B 174369

500-53491-1 MSD FC COMPOSITE 6 Total/NA Solid 9071B 174369

500-53491-2 FC D COMPOSITE 6 Total/NA Solid 9071B 174369

LCS 500-174369/2-A Lab Control Sample Total/NA Solid 9071B 174369

MB 500-174369/1-A Method Blank Total/NA Solid 9071B 174369

Prep Batch: 174563

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-5 FC EB 6 Total/NA Water 1664A

LCS 500-174563/2-A Lab Control Sample Total/NA Water 1664A

MB 500-174563/1-A Method Blank Total/NA Water 1664A

Analysis Batch: 174564

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53491-5 FC EB 6 Total/NA Water 1664A 174563

LCS 500-174563/2-A Lab Control Sample Total/NA Water 1664A 174563

MB 500-174563/1-A Method Blank Total/NA Water 1664A 174563

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Surrogate Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 8260B - Volatile Organic Compounds (GC/MS)

Matrix: Solid Prep Type: Total/NA

Lab Sample ID Client Sample ID (70-134) (75-122) (70-122) (75-120)

12DCE TOL BFB DBFM

500-53491-3 89 87 79 95

Percent Surrogate Recovery (Acceptance Limits)

FC DISCRETE 6

500-53491-4 FC D DISCRETE 6 91 89 75 90

LCS 500-173973/6 Lab Control Sample 84 89 81 81

LCSD 500-173973/7 Lab Control Sample Dup 88 93 87 91

MB 500-173973/5 Method Blank 94 96 84 90

Surrogate Legend

12DCE = 1,2-Dichloroethane-d4 (Surr)

TOL = Toluene-d8 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

DBFM = Dibromofluoromethane

Method: 8260B - Volatile Organic Compounds (GC/MS)

Matrix: Solid Prep Type: Total/NA

Lab Sample ID Client Sample ID (75-125) (75-120) (75-120) (75-120)

12DCE DBFM TOL BFB

500-53491-3 - DL 97 93 96 94

Percent Surrogate Recovery (Acceptance Limits)

FC DISCRETE 6

500-53491-4 - DL FC D DISCRETE 6 105 96 101 100

LCS 500-174064/4 Lab Control Sample 95 100 97 97

MB 500-174064/6 Method Blank 101 96 101 98

Surrogate Legend

12DCE = 1,2-Dichloroethane-d4 (Surr)

DBFM = Dibromofluoromethane

TOL = Toluene-d8 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

Method: 8260B - Volatile Organic Compounds (GC/MS)

Matrix: Water Prep Type: Total/NA

Lab Sample ID Client Sample ID (75-125) (75-120) (75-120) (75-120)

12DCE TOL BFB DBFM

500-53491-5 88 94 88 90

Percent Surrogate Recovery (Acceptance Limits)

FC EB 6

500-53491-6 TRIP BLANK 93 100 93 93

LCS 500-173987/4 Lab Control Sample 92 96 96 94

MB 500-173987/7 Method Blank 98 103 97 97

Surrogate Legend

12DCE = 1,2-Dichloroethane-d4 (Surr)

TOL = Toluene-d8 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

DBFM = Dibromofluoromethane

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 8260B - Volatile Organic Compounds (GC/MS)

Lab Sample ID: MB 500-173973/5 Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173973

RL MDL

Acetone <5.00 5.00 2.16 ug/Kg 12/27/12 10:33 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

2-Butanone (MEK) <5.00 5.00 1.81 ug/Kg 12/27/12 10:33 1

1,2-Dichloroethane-d4 (Surr) 94 70 - 134 12/27/12 10:33 1

MB MB

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 96 75 - 122 12/27/12 10:33 1

4-Bromofluorobenzene (Surr) 84 70 - 122 12/27/12 10:33 1

Dibromofluoromethane 90 75 - 120 12/27/12 10:33 1

Lab Sample ID: LCS 500-173973/6 Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173973

Acetone 50.0 47.98 ug/Kg 96 50 - 138

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

2-Butanone (MEK) 50.0 43.18 ug/Kg 86 58 - 133

1,2-Dichloroethane-d4 (Surr) 70 - 134

Surrogate

84

LCS LCS

%Recovery Qualifier Limits

Toluene-d8 (Surr) 89 75 - 122

4-Bromofluorobenzene (Surr) 81 70 - 122

Dibromofluoromethane 81 75 - 120

Lab Sample ID: LCSD 500-173973/7 Client Sample ID: Lab Control Sample Dup

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173973

Acetone 50.0 55.07 ug/Kg 110 50 - 138 14 30

Analyte

LCSD LCSD

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits RPD Limit

RPD

2-Butanone (MEK) 50.0 44.82 ug/Kg 90 58 - 133 4 30

1,2-Dichloroethane-d4 (Surr) 70 - 134

Surrogate

88

LCSD LCSD

%Recovery Qualifier Limits

Toluene-d8 (Surr) 93 75 - 122

4-Bromofluorobenzene (Surr) 87 70 - 122

Dibromofluoromethane 91 75 - 120

Lab Sample ID: MB 500-173987/7 Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173987

RL MDL

Acetone <5.00 5.00 1.29 ug/L 12/27/12 14:10 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

2-Butanone (MEK) <5.00 5.00 1.47 ug/L 12/27/12 14:10 1

1,2-Dichloroethane-d4 (Surr) 98 75 - 125 12/27/12 14:10 1

MB MB

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)

Lab Sample ID: MB 500-173987/7 Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173987

Toluene-d8 (Surr) 103 75 - 120 12/27/12 14:10 1

MB MB

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

4-Bromofluorobenzene (Surr) 97 75 - 120 12/27/12 14:10 1

Dibromofluoromethane 97 75 - 120 12/27/12 14:10 1

Lab Sample ID: LCS 500-173987/4 Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173987

Acetone 50.0 53.44 ug/L 107 46 - 153

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

2-Butanone (MEK) 50.0 46.97 ug/L 94 54 - 138

1,2-Dichloroethane-d4 (Surr) 75 - 125

Surrogate

92

LCS LCS

%Recovery Qualifier Limits

Toluene-d8 (Surr) 96 75 - 120

4-Bromofluorobenzene (Surr) 96 75 - 120

Dibromofluoromethane 94 75 - 120

Lab Sample ID: MB 500-174064/6 Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174064

RL MDL

Acetone <5.00 5.00 1.30 ug/Kg 12/28/12 10:45 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

2-Butanone (MEK) <5.00 5.00 1.47 ug/Kg 12/28/12 10:45 1

1,2-Dichloroethane-d4 (Surr) 101 75 - 125 12/28/12 10:45 1

MB MB

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 101 75 - 120 12/28/12 10:45 1

4-Bromofluorobenzene (Surr) 98 75 - 120 12/28/12 10:45 1

Dibromofluoromethane 96 75 - 120 12/28/12 10:45 1

Lab Sample ID: LCS 500-174064/4 Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174064

Acetone 50.0 50.53 ug/Kg 101 46 - 153

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

2-Butanone (MEK) 50.0 43.61 ug/Kg 87 54 - 138

1,2-Dichloroethane-d4 (Surr) 75 - 125

Surrogate

95

LCS LCS

%Recovery Qualifier Limits

Toluene-d8 (Surr) 97 75 - 120

4-Bromofluorobenzene (Surr) 97 75 - 120

Dibromofluoromethane 100 75 - 120

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 6010B - Metals (ICP)

Lab Sample ID: MB 500-173848/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173964 Prep Batch: 173848

RL MDL

Barium <1.00 1.00 0.119 mg/Kg 12/24/12 15:00 12/26/12 21:54 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper <1.00 1.00 0.271 mg/Kg 12/24/12 15:00 12/26/12 21:54 1

Chromium <1.00 1.00 0.167 mg/Kg 12/24/12 15:00 12/26/12 21:54 1

Nickel <1.00 1.00 0.219 mg/Kg 12/24/12 15:00 12/26/12 21:54 1

Lead 0.1770 J 0.500 0.172 mg/Kg 12/24/12 15:00 12/26/12 21:54 1

Vanadium <0.500 0.500 0.0759 mg/Kg 12/24/12 15:00 12/26/12 21:54 1

Zinc <2.00 2.00 0.686 mg/Kg 12/24/12 15:00 12/26/12 21:54 1

Lab Sample ID: LCS 500-173848/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173964 Prep Batch: 173848

Barium 200 200.1 mg/Kg 100 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Copper 25.0 25.74 mg/Kg 103 80 - 120

Chromium 20.0 20.94 mg/Kg 105 80 - 120

Nickel 50.0 51.09 mg/Kg 102 80 - 120

Lead 10.0 10.73 mg/Kg 107 80 - 120

Vanadium 50.0 51.21 mg/Kg 102 80 - 120

Zinc 50.0 53.63 mg/Kg 107 80 - 120

Lab Sample ID: MB 500-173849/1-A Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173963 Prep Batch: 173849

RL MDL

Barium <0.0100 0.0100 0.000440 mg/L 12/24/12 14:30 12/26/12 16:35 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper <0.0100 0.0100 0.00106 mg/L 12/24/12 14:30 12/26/12 16:35 1

Chromium <0.0100 0.0100 0.000960 mg/L 12/24/12 14:30 12/26/12 16:35 1

Nickel <0.0100 0.0100 0.00190 mg/L 12/24/12 14:30 12/26/12 16:35 1

Lead <0.00500 0.00500 0.00158 mg/L 12/24/12 14:30 12/26/12 16:35 1

Vanadium <0.00500 0.00500 0.000620 mg/L 12/24/12 14:30 12/26/12 16:35 1

Zinc <0.0200 0.0200 0.00472 mg/L 12/24/12 14:30 12/26/12 16:35 1

Lab Sample ID: LCS 500-173849/2-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173963 Prep Batch: 173849

Barium 2.00 1.902 mg/L 95 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Copper 0.250 0.2317 mg/L 93 80 - 120

Chromium 0.200 0.1856 mg/L 93 80 - 120

Nickel 0.500 0.4572 mg/L 91 80 - 120

Lead 0.100 0.09439 mg/L 94 80 - 120

Vanadium 0.500 0.4686 mg/L 94 80 - 120

Zinc 0.500 0.4470 mg/L 89 80 - 120

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 6010B - Metals (ICP) (Continued)

Lab Sample ID: LCS 500-173872/3-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173964 Prep Batch: 173872

Barium 2.00 1.928 mg/L 96 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Copper 0.250 0.2512 mg/L 100 80 - 120

Chromium 0.200 0.2016 mg/L 101 80 - 120

Nickel 0.500 0.4930 mg/L 99 80 - 120

Lead 0.100 0.1042 mg/L 104 80 - 120

Vanadium 0.500 0.4994 mg/L 100 80 - 120

Zinc 0.500 0.5058 mg/L 101 80 - 120

Lab Sample ID: LB 500-173836/1-B LB Client Sample ID: Method Blank

Matrix: Solid Prep Type: TCLP

Analysis Batch: 173964 Prep Batch: 173872

RL MDL

Barium <0.500 0.500 0.0100 mg/L 12/26/12 07:50 12/26/12 17:12 1

LB LB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper <0.0250 0.0250 0.0100 mg/L 12/26/12 07:50 12/26/12 17:12 1

Chromium <0.0250 0.0250 0.0100 mg/L 12/26/12 07:50 12/26/12 17:12 1

Nickel <0.0250 0.0250 0.0100 mg/L 12/26/12 07:50 12/26/12 17:12 1

Lead <0.0500 0.0500 0.00500 mg/L 12/26/12 07:50 12/26/12 17:12 1

Vanadium <0.0250 0.0250 0.00500 mg/L 12/26/12 07:50 12/26/12 17:12 1

Zinc <0.100 0.100 0.0200 mg/L 12/26/12 07:50 12/26/12 17:12 1

Lab Sample ID: LB2 500-173838/1-B LB2 Client Sample ID: Method Blank

Matrix: Solid Prep Type: TCLP

Analysis Batch: 173964 Prep Batch: 173872

RL MDL

Barium <0.500 0.500 0.0100 mg/L 12/26/12 07:50 12/26/12 17:18 1

LB2 LB2

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper <0.0250 0.0250 0.0100 mg/L 12/26/12 07:50 12/26/12 17:18 1

Chromium <0.0250 0.0250 0.0100 mg/L 12/26/12 07:50 12/26/12 17:18 1

Nickel <0.0250 0.0250 0.0100 mg/L 12/26/12 07:50 12/26/12 17:18 1

Lead <0.0500 0.0500 0.00500 mg/L 12/26/12 07:50 12/26/12 17:18 1

Vanadium <0.0250 0.0250 0.00500 mg/L 12/26/12 07:50 12/26/12 17:18 1

Zinc <0.100 0.100 0.0200 mg/L 12/26/12 07:50 12/26/12 17:18 1

Method: 7470A - Mercury (CVAA)

Lab Sample ID: MB 500-173908/7-A Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173997 Prep Batch: 173908

RL MDL

Mercury <0.000200 0.000200 0.0000710 mg/L 12/26/12 13:00 12/27/12 08:41 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173908/8-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173997 Prep Batch: 173908

Mercury 0.00200 0.002121 mg/L 106 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 7470A - Mercury (CVAA) (Continued)

Lab Sample ID: MB 500-173909/7-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173997 Prep Batch: 173909

RL MDL

Mercury 0.00003040 J 0.000200 0.0000200 mg/L 12/26/12 13:00 12/27/12 09:28 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173909/8-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173997 Prep Batch: 173909

Mercury 0.00200 0.002139 mg/L 107 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: LB 500-173836/1-C LB Client Sample ID: Method Blank

Matrix: Solid Prep Type: TCLP

Analysis Batch: 173997 Prep Batch: 173909

RL MDL

Mercury 0.00003420 J 0.000200 0.0000200 mg/L 12/26/12 13:00 12/27/12 09:49 1

LB LB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LB2 500-173838/1-C LB2 Client Sample ID: Method Blank

Matrix: Solid Prep Type: TCLP

Analysis Batch: 173997 Prep Batch: 173909

RL MDL

Mercury 0.00003260 J 0.000200 0.0000200 mg/L 12/26/12 13:00 12/27/12 09:51 1

LB2 LB2

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: 500-53491-2 MS Client Sample ID: FC D COMPOSITE 6

Matrix: Solid Prep Type: TCLP

Analysis Batch: 173997 Prep Batch: 173909

Mercury <0.000200 0.00100 0.0007703 mg/L 77 50 - 150

Analyte

MS MS

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Lab Sample ID: 500-53491-2 DU Client Sample ID: FC D COMPOSITE 6

Matrix: Solid Prep Type: TCLP

Analysis Batch: 173997 Prep Batch: 173909

Mercury <0.000200 0.00004470 J mg/L NC 20

Analyte

DU DU

Result Qualifier Unit D

Sample

Result

Sample

Qualifier RPD Limit

RPD

Method: 7471A - Mercury (CVAA)

Lab Sample ID: MB 500-173881/7-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173984 Prep Batch: 173881

RL MDL

Mercury <0.0167 0.0167 0.00637 mg/Kg 12/26/12 14:00 12/27/12 08:17 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 7471A - Mercury (CVAA) (Continued)

Lab Sample ID: LCS 500-173881/8-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173984 Prep Batch: 173881

Mercury 0.167 0.1600 mg/Kg 96 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Method: 1664A - HEM and SGT-HEM

Lab Sample ID: MB 500-174563/1-A Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 174564 Prep Batch: 174563

RL MDL

HEM (Oil & Grease) <5.00 5.00 1.45 mg/L 01/08/13 05:35 01/08/13 11:00 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-174563/2-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 174564 Prep Batch: 174563

HEM (Oil & Grease) 40.0 32.00 mg/L 80 78 - 114

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Method: 7196A - Chromium, Hexavalent

Lab Sample ID: MB 500-173790/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174027 Prep Batch: 173790

RL MDL

Chromium, hexavalent <1.00 1.00 0.389 mg/Kg 12/22/12 12:00 12/27/12 12:41 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173790/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174027 Prep Batch: 173790

Chromium, hexavalent 10.0 9.188 mg/Kg 92 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: LCS 500-173790/3-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174027 Prep Batch: 173790

Chromium, hexavalent 676 669.0 mg/Kg 99 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: MB 500-173793/3 Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173793

RL MDL

Chromium, hexavalent <0.0100 0.0100 0.00325 mg/L 12/22/12 14:11 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 7196A - Chromium, Hexavalent (Continued)

Lab Sample ID: LCS 500-173793/4 Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173793

Chromium, hexavalent 0.250 0.2575 mg/L 103 85 - 115

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: 500-53491-5 MS Client Sample ID: FC EB 6

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173793

Chromium, hexavalent <0.0100 H 0.250 0.2660 mg/L 106 85 - 115

Analyte

MS MS

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Lab Sample ID: 500-53491-5 MSD Client Sample ID: FC EB 6

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173793

Chromium, hexavalent <0.0100 H 0.250 0.2541 mg/L 102 85 - 115 5 20

Analyte

MSD MSD

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits RPD Limit

RPD

Method: 9014 - Cyanide

Lab Sample ID: MB 500-173980/1-A Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 174042 Prep Batch: 173980

RL MDL

Cyanide, Total <0.0100 0.0100 0.00331 mg/L 12/27/12 09:50 12/27/12 14:40 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173980/2-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 174042 Prep Batch: 173980

Cyanide, Total 0.100 0.1066 mg/L 107 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: MB 500-174096/12-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174173 Prep Batch: 174096

RL MDL

Cyanide, Total <0.500 0.500 0.165 mg/Kg 12/28/12 11:20 12/28/12 15:30 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-174096/13-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174173 Prep Batch: 174096

Cyanide, Total 5.00 5.325 mg/Kg 107 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 9014 - Cyanide (Continued)

Lab Sample ID: 500-53491-2 MS Client Sample ID: FC D COMPOSITE 6

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174173 Prep Batch: 174096

Cyanide, Total 1.29 J 7.50 7.442 mg/Kg ☼ 82 75 - 125

Analyte

MS MS

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Lab Sample ID: 500-53491-2 MSD Client Sample ID: FC D COMPOSITE 6

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174173 Prep Batch: 174096

Cyanide, Total 1.29 J 7.44 8.170 mg/Kg ☼ 92 75 - 125 9 20

Analyte

MSD MSD

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits RPD Limit

RPD

Method: 9034 - Sulfide, Reactive

Lab Sample ID: MB 500-173844/1-A Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173845 Prep Batch: 173844

RL MDL

Sulfide, Reactive <1.00 1.00 1.00 mg/L 12/24/12 08:00 12/24/12 13:19 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173844/2-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173845 Prep Batch: 173844

Sulfide, Reactive 3.60 3.767 mg/L 105 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: MB 500-174101/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174145 Prep Batch: 174101

RL MDL

Sulfide, Reactive <50.0 50.0 3.90 mg/Kg 12/28/12 11:35 12/28/12 12:55 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-174101/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174145 Prep Batch: 174101

Sulfide, Reactive 180 169.4 mg/Kg 94 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Method: 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric)

Lab Sample ID: MB 500-173846/1 Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173846

RL MDL

Sulfide <1.00 1.00 0.230 mg/L 12/24/12 13:19 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric) (Continued)

Lab Sample ID: LCS 500-173846/2 Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173846

Sulfide 3.60 3.760 mg/L 104 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: MB 500-174100/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174144 Prep Batch: 174100

RL MDL

Sulfide <25.0 25.0 4.00 mg/Kg 12/28/12 12:20 12/28/12 14:35 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-174100/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174144 Prep Batch: 174100

Sulfide 180 173.0 mg/Kg 96 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Method: 9071B - HEM and SGT-HEM

Lab Sample ID: MB 500-174369/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174372 Prep Batch: 174369

RL MDL

HEM (Oil & Grease) <500 500 222 mg/Kg 01/04/13 05:35 01/04/13 09:45 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-174369/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174372 Prep Batch: 174369

HEM (Oil & Grease) 4000 4050 mg/Kg 101 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: 500-53491-1 MS Client Sample ID: FC COMPOSITE 6

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174372 Prep Batch: 174369

HEM (Oil & Grease) 16600 14800 39400 F mg/Kg ☼ 154 75 - 125

Analyte

MS MS

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Lab Sample ID: 500-53491-1 MSD Client Sample ID: FC COMPOSITE 6

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 174372 Prep Batch: 174369

HEM (Oil & Grease) 16600 14800 40340 F mg/Kg ☼ 160 75 - 125 2 20

Analyte

MSD MSD

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits RPD Limit

RPD

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Lab Chronicle

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC COMPOSITE 6 Lab Sample ID: 500-53491-1

Date Collected: 12/19/12 14:30 Matrix: Solid

Date Received: 12/22/12 11:30

Leach 1311 173838 12/24/12 11:50 DB TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

TCLP

TCLP Prep 3010A 173872 12/26/12 07:50 LAH TAL CHI

TCLP Analysis 6010B 1 173964 12/26/12 18:41 PJ TAL CHI

Total/NA Prep 3050B 173848 12/24/12 15:00 RL TAL CHI

Total/NA Analysis 6010B 1 173964 12/26/12 23:57 PJ TAL CHI

Total/NA Prep 7471A 173881 12/26/12 14:00 BJB TAL CHI

Total/NA Analysis 7471A 1 173984 12/27/12 08:55 BJB TAL CHI

TCLP Prep 7470A 173909 12/26/12 13:00 BJB TAL CHI

TCLP Analysis 7470A 1 173997 12/27/12 09:57 BJB TAL CHI

Total/NA Analysis Moisture 1 173788 12/22/12 13:24 CMV TAL CHI

Total/NA Analysis 9045C 1 173936 CLM TAL CHI

12/26/12 14:25

12/26/12 14:27

(Start)

(End)

Total/NA Analysis SM 2540G 1 173970 12/27/12 07:30 CMV TAL CHI

Total/NA Prep 3060A 173790 12/22/12 12:00 APW TAL CHI

Total/NA Analysis 7196A 1 174027 APW TAL CHI

12/27/12 12:51

12/27/12 12:51

(Start)

(End)

Total/NA Prep 9030B 174100 12/28/12 12:20 CLM TAL CHI

Total/NA Analysis 9034 1 174144 12/28/12 14:43 CLM TAL CHI

Total/NA Prep 7.3.4 174101 12/28/12 11:57 CLM TAL CHI

Total/NA Analysis 9034 1 174145 12/28/12 12:58 CLM TAL CHI

Total/NA Prep 9010B 174096 12/28/12 11:20 EAT TAL CHI

Total/NA Analysis 9014 1 174173 EAT TAL CHI

12/28/12 15:31

12/28/12 15:31

(Start)

(End)

Total/NA Analysis 1010 1 174336 APW TAL CHI

01/02/13 09:30

01/02/13 10:52

(Start)

(End)

Total/NA Prep 9071B 174369 01/04/13 05:35 MTB TAL CHI

Total/NA Analysis 9071B 1 174372 01/04/13 10:13 MTB TAL CHI

Client Sample ID: FC D COMPOSITE 6 Lab Sample ID: 500-53491-2

Date Collected: 12/19/12 14:40 Matrix: Solid

Date Received: 12/22/12 11:30

Leach 1311 173836 12/24/12 11:50 DB TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

TCLP

TCLP Prep 3010A 173872 12/26/12 07:50 LAH TAL CHI

TCLP Analysis 6010B 1 173964 12/26/12 18:47 PJ TAL CHI

Total/NA Prep 3050B 173848 12/24/12 15:00 RL TAL CHI

Total/NA Analysis 6010B 1 173964 12/27/12 00:03 PJ TAL CHI

Total/NA Prep 7471A 173881 12/26/12 14:00 BJB TAL CHI

Total/NA Analysis 7471A 1 173984 12/27/12 09:04 BJB TAL CHI

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Lab Chronicle

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC D COMPOSITE 6 Lab Sample ID: 500-53491-2

Date Collected: 12/19/12 14:40 Matrix: Solid

Date Received: 12/22/12 11:30

Prep 7470A 173909 12/26/12 13:00 BJB TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

TCLP

TCLP Analysis 7470A 1 173997 12/27/12 09:58 BJB TAL CHI

Total/NA Analysis Moisture 1 173788 12/22/12 13:24 CMV TAL CHI

Total/NA Analysis 9045C 1 173936 CLM TAL CHI

12/26/12 14:27

12/26/12 14:30

(Start)

(End)

Total/NA Analysis SM 2540G 1 173970 12/27/12 07:30 CMV TAL CHI

Total/NA Prep 3060A 173790 12/22/12 12:00 APW TAL CHI

Total/NA Analysis 7196A 1 174027 APW TAL CHI

12/27/12 12:53

12/27/12 12:53

(Start)

(End)

Total/NA Prep 9030B 174100 12/28/12 12:20 CLM TAL CHI

Total/NA Analysis 9034 1 174144 12/28/12 14:44 CLM TAL CHI

Total/NA Prep 7.3.4 174101 12/28/12 12:01 CLM TAL CHI

Total/NA Analysis 9034 1 174145 12/28/12 12:59 CLM TAL CHI

Total/NA Prep 9010B 174096 12/28/12 11:20 EAT TAL CHI

Total/NA Analysis 9014 1 174173 EAT TAL CHI

12/28/12 15:31

12/28/12 15:32

(Start)

(End)

Total/NA Analysis 1010 1 174336 APW TAL CHI

01/02/13 10:52

01/02/13 12:14

(Start)

(End)

Total/NA Prep 9071B 174369 01/04/13 05:35 MTB TAL CHI

Total/NA Analysis 9071B 1 174372 01/04/13 10:56 MTB TAL CHI

Client Sample ID: FC DISCRETE 6 Lab Sample ID: 500-53491-3

Date Collected: 12/19/12 14:20 Matrix: Solid

Date Received: 12/22/12 11:30 Percent Solids: 25.9

Analysis 8260B 1 173973 12/27/12 13:36 DJD TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Total/NA Prep 5030B DL 173990 12/27/12 10:28 WRE TAL CHI

Total/NA Analysis 8260B DL 50 174064 12/28/12 11:08 BDA TAL CHI

Total/NA Analysis Moisture 1 174071 12/28/12 10:09 CMV TAL CHI

Client Sample ID: FC D DISCRETE 6 Lab Sample ID: 500-53491-4

Date Collected: 12/19/12 14:45 Matrix: Solid

Date Received: 12/22/12 11:30 Percent Solids: 27.6

Analysis 8260B 1 173973 12/27/12 13:59 DJD TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Total/NA Prep 5030B DL 173990 12/27/12 10:28 WRE TAL CHI

Total/NA Analysis 8260B DL 50 174064 12/28/12 11:31 BDA TAL CHI

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Lab Chronicle

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC D DISCRETE 6 Lab Sample ID: 500-53491-4

Date Collected: 12/19/12 14:45 Matrix: Solid

Date Received: 12/22/12 11:30

Analysis Moisture 1 174071 12/28/12 10:09 CMV TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Client Sample ID: FC EB 6 Lab Sample ID: 500-53491-5

Date Collected: 12/19/12 14:10 Matrix: Water

Date Received: 12/22/12 11:30

Analysis 8260B 1 173987 12/27/12 15:54 LM TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Total/NA Prep 3010A 173849 12/24/12 14:30 RL TAL CHI

Total/NA Analysis 6010B 1 173963 12/26/12 17:03 PJ TAL CHI

Total/NA Prep 7470A 173908 12/26/12 13:00 BJB TAL CHI

Total/NA Analysis 7470A 1 173997 12/27/12 09:26 BJB TAL CHI

Total/NA Analysis 7196A 1 173793 APW TAL CHI

12/22/12 14:12

12/22/12 14:13

(Start)

(End)

Total/NA Prep 7.3.4 173844 12/24/12 08:45 CLB TAL CHI

Total/NA Analysis 9034 1 173845 12/24/12 13:51 CLB TAL CHI

Total/NA Analysis 9034 1 173846 CLB TAL CHI

12/24/12 14:00

12/24/12 14:02

(Start)

(End)

Total/NA Prep 9010B 173980 12/27/12 09:50 EAT TAL CHI

Total/NA Analysis 9014 1 174042 EAT TAL CHI

12/27/12 14:45

12/27/12 14:45

(Start)

(End)

Total/NA Prep 1664A 174563 01/08/13 06:01 MTB TAL CHI

Total/NA Analysis 1664A 1 174564 01/08/13 11:08 MTB TAL CHI

Client Sample ID: TRIP BLANK Lab Sample ID: 500-53491-6

Date Collected: 12/19/12 00:00 Matrix: Water

Date Received: 12/22/12 11:30

Analysis 8260B 1 173987 12/27/12 15:28 LM TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Laboratory References:

TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200

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Certification Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53491-1

Project/Site: John Deere Des Moines Works (JDDMW)

Laboratory: TestAmerica Chicago

All certifications held by this laboratory are listed. Not all certifications are applicable to this report.

Authority Program EPA Region Certification ID Expiration Date

Alabama State Program 4 40461 04-30-13

California NELAP 9 01132CA 04-30-13

Georgia State Program 4 N/A 04-30-13

Georgia State Program 4 939 04-30-13

Hawaii State Program 9 N/A 04-30-13

Illinois NELAP 5 100201 04-30-13

Indiana State Program 5 C-IL-02 04-30-13

Iowa State Program 7 82 05-01-14

Kansas NELAP 7 E-10161 10-31-13

Kentucky State Program 4 90023 12-31-12

Kentucky (UST) State Program 4 66 04-11-13

Louisiana NELAP 6 30720 06-30-13

Massachusetts State Program 1 M-IL035 06-30-13

Mississippi State Program 4 N/A 04-30-13

North Carolina DENR State Program 4 291 12-31-13

North Dakota State Program 8 R-194 04-30-13

Oklahoma State Program 6 8908 08-31-13

South Carolina State Program 4 77001 04-30-13

Texas NELAP 6 T104704252-09-TX 02-28-13

USDA Federal P330-12-00038 02-06-15

Virginia NELAP 3 460142 06-14-13

Wisconsin State Program 5 999580010 08-31-13

Wyoming State Program 8 8TMS-Q 04-30-13

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Login Sample Receipt Checklist

Client: Project Integration, Inc Job Number: 500-53491-1

Login Number: 53491

Question Answer Comment

Creator: Lunt, Jeff T

List Source: TestAmerica Chicago

List Number: 1

Radioactivity wasn't checked or is </= background as measured by a survey True

meter.

The cooler's custody seal, if present, is intact. True

Sample custody seals, if present, are intact. True

The cooler or samples do not appear to have been compromised or True

tampered with.

Samples were received on ice. True 1.3

Cooler Temperature is acceptable. True

Cooler Temperature is recorded. True

COC is present. True

COC is filled out in ink and legible. True

COC is filled out with all pertinent information. True

Is the Field Sampler's name present on COC? True

There are no discrepancies between the containers received and the COC. True

Samples are received within Holding Time. False

Sample containers have legible labels. True

Containers are not broken or leaking. True

Sample collection date/times are provided. True

Appropriate sample containers are used. True

Sample bottles are completely filled. True

Sample Preservation Verified. True

There is sufficient vol. for all requested analyses, incl. any requested True

MS/MSDs

Containers requiring zero headspace have no headspace or bubble is True

<6mm (1/4").

Multiphasic samples are not present. True

Samples do not require splitting or compositing. True

Residual Chlorine Checked. N/A

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