### Name:

Title: Company: Sign Date: Name: Title: Company: Sign Date: Permitted Facility Representative / Date Testing Company Representative / Date Final Test Report for

/ / Based on information and belief formed after reasonable inquiry, I certify that the statements and information in this test report are true, accurate, and complete. I have reviewed all testing details and results in this test report and hereby certify that the test report is authentic and accurate.

Monday, March 07, 2011 Page 1 of 18

### Facility Information:

PREPA Aguirre Power Station Enter physical Address

Enter physical city Contact:Person to contact for more detail Phone:Of above person Fax: Of above person Email:Of above person Testing Company: Name of primary testing organization US postal address of above

US postal address of abov Contact:Field test leader Phone:Of above person Fax: Of above person Email:Of above person

Air Permit Number: Enter your facilities ORIS Number here Permitted Source ID/Name: Enter the Boiler ID of the tested boiler (left) SJ8 Permitted Maximum Process Rate: N/A Max. Normal Operation Process Rate: N/A Target Process Test Rate N/A

Description of the source (including control equipment). Please see the attachments for source or process flow diagram: This description should describe the process and associated controls to differentiate this facility from, or document similarity with others of same SCC. Industry/SCC/NAIS221112

Sampling Location Information:

Test Parameter Information: AFS #:Enter ARS ID FRS #:Enter FRS ID

SCC / Description10100404 External Combustion Boilers - Electric Generation - Residual Oil - Grade 6 Oil: Tangential Firing

The following state and federal regulations that apply to the proposed testing:

Location Round

Duct Diam. Distance from upstream dist. Distance from

downstream dist. Number of

Traverse Ports Equiv. Diam Min.Travers Points Rect. Duct Length /Width Stack Exit 0 0 0 0 0 0 0 0

Target Parameter Test Method Number of

Test RunsTest Run

DurationSample

Points Comments Location% H2O Method 1 - 4 3 180 0 Stack Exit Carbon Monoxide Method 10 3 120 0 Stack Exit Formaldehyde Method 0011 3 120 0 Stack Exit 2,3,7,8-TCDD Method 23 3 480 0 Stack Exit 1,2,3,7,8-PeCDD Method 23 3 480 0 Stack Exit 1,2,3,4,7,8-HxCDD Method 23 3 480 0 Stack Exit 1,2,3,6,7,8-HxCDD Method 23 3 480 0 Stack Exit



### Monday, March 07, 2011 Page 2 of 181,2,3,7,8,9-HxCDD Method 23 3 480 0

Stack Exit 1,2,3,4,6,7,8-HpCDD Method 23 3 480 0 Stack Exit OCDD Method 23 3 480 0 Stack Exit 2,3,7,8-TCDF Method 23 3 480 0 Stack Exit 1,2,3,7,8-PeCDF Method 23 3 480 0 Stack Exit 2,3,4,7,8-PeCDF Method 23 3 480 0 Stack Exit 1,2,3,4,7,8-HxCDF Method 23 3 480 0 Stack Exit 1,2,3,6,7,8-HxCDF Method 23 3 480 0 Stack Exit 2,3,4,6,7,8-HxCDF Method 23 3 480 0 Stack Exit 1,2,3,7,8,9-HxCDF Method 23 3 480 0 Stack Exit 1,2,3,4,6,7,8-HpCDF Method 23 3 480 0 Stack Exit 1,2,3,4,7,8,9-HpCDF Method 23 3 480 0 Stack Exit OCDF Method 23 3 480 0 Stack Exit Other TCDD Method 23 0 Stack Exit Other PeCDD Method 23 0 Stack Exit Other HxCDD Method 23 0 Stack Exit Other HpCDD Method 23 0 Stack Exit Other TCDF Method 23 0 Stack Exit Other PeCDF Method 23 0 Stack Exit Other HxCDF Method 23 0 Stack Exit Other HpCDF Method 23 0 Stack Exit Total Dioxins Method 23 3 480 0 Stack Exit Total Furans Method 23 3 480 0 Stack Exit 3,3',4,4'-TCB (PCB77) Method 23 3 480 0 Stack Exit 3,4,4',5-TCB (PCB81) Method 23 3 480 0 Stack Exit 2,3,3',4,4'-PeCB (PCB105) Method 23 3 480 0 Stack Exit 2,3,4,4',5-PeCB (PCB114) Method 23 3 480 0 Stack Exit 2,3',4,4',5-PeCB (PCB118) Method 23 3 480 0 Stack Exit 2',3,4,4',5-PeCB (PCB123) Method 23 3 480 0 Stack Exit 3,3',4,4',5-PeCB (PCB126) Method 23 3 480 0 Stack Exit 2,3,3',4,4',5/2,3,3',4,4',5'-

HxCB (PCBs156/157) Method 23 3 480 0 Stack Exit

2,3',4,4',5,5'-HxCB (PCB167)Method 23 3 480 0 Stack Exit 3,3',4,4',5,5'-HxCB (PCB169)Method 23 3 480 0 Stack Exit 2,3,3',4,4',5,5'-HpCB

(PCB189) Method 23 3 480 0 Stack Exit

Total PCBs Method 23 3 480 0 Stack Exit Total TEQ Method 23 3 480 0 Stack Exit Total organic compounds

(TOC) as Propane Method 25A 3 120 0 Stack Exit
Hydrogen Chloride Method 26 3 180 0 Stack Exit Hydrogen Fluoride Method 26 3 180 0 Stack Exit Hydrogen Chloride Method 26A 3 180 0 Stack Exit Hydrogen Fluoride Method 26A 3 180 0 Stack Exit Inorganic (Aqueous)

Condensible Part. OTM - 27/28 3 240 0 Use only for dry stacks. Delete Method 5/OTM28 tests. Stack Exit

Filterable PM2.5 OTM - 27/28 3 240 0 Use only for dry stacks. Delete Method 5/OTM28 tests. Stack Exit

Organic Condensible

Particulate OTM - 27/28 3 240 0 Use only for dry stacks. Delete Method 5/OTM28 tests. Stack Exit



### Monday, March 07, 2011 Page 3 of 18

### The following describes any modifications and/or deviations to the applicable test

methods. If alternative methods were requested, see the attachments for documentation of request AND approval, including dates. In this section, identify the promulgation date of any specified test method that you use for determining the procedures followed. This field is also used to document any modifications that are necessary to conduct the emissions test if they are outside the requirements of the cited method. If this modification was approved verbally by a regulatory agency, the name and date of approval should be included. Written formal approval should be attached to this file using the "Attach File" button. Test procedures that are different from those published in the Federal Register should be attached using the "Attach File" button.

Total PM2.5 OTM - 27/28 3 240 0 Use only for dry stacks. Delete Method 5/OTM28 tests. Stack Exit

Total Particulate OTM - 27/28 3 240 0 Use only for dry stacks. Delete Method 5/OTM28 tests. Stack Exit

Filterable Particulate OTM - 27/28 3 240 0 Use only for dry stacks. Delete Method 5/OTM28 tests. Stack Exit

Arsenic Method 29 3 240 0 Stack Exit Nickel Method 29 3 240 0 Stack Exit Selenium Method 29 3 240 0 Stack Exit Lead Method 29 3 240 0 Stack Exit Chromium Method 29 3 240 0 Stack Exit Cadmium Method 29 3 240 0 Stack Exit Manganese Method 29 3 240 0 Stack Exit Beryllium Method 29 3 240 0 Stack Exit Filterable Particulate Method 29 3 240 0 Stack Exit Antimony Method 29 3 240 0 Stack Exit Co2 Method 3A CO2 3 120 0 Stack Exit Co2 Method 3A CO2 3 240 0 Stack Exit O2 Method 3A O2 3 240 0 Stack Exit O2 Method 3A O2 3 480 0 Stack Exit Co2 Method 3A CO2 3 480 0 Stack Exit O2 Method 3A O2 3 120 0 Stack Exit Inorganic (Aqueous)

Condensible Part. Method 5/OTM-28 3 240 0 Use only for wet stacks. Delete OTM27/OTM28 test. Stack Exit

Organic Condensible

Particulate Method 5/OTM-28 3 240 0 Use only for wet stacks. Delete OTM27/OTM28 test. Stack Exit

Total Particulate Method 5/OTM-28 3 240 0 Use only for wet stacks. Delete OTM27/OTM28 test. Stack Exit

Filterable Particulate Method 5 3 240 0 Stack Exit Filterable Particulate Method 5/OTM-28 3 240 0 Use only for wet stacks. Delete OTM27/OTM28 test. Stack Exit

Sulfur Dioxide Method 6C 3 180 0 Stack Exit Nitrogen oxides (NOx) Method 7E 3 180 0 Stack Exit



### Monday, March 07, 2011 Page 4 of 18

### Sampling / Stack Data Results Summary



### LocationStack Exit - Method 23 Average Run Number 1 2 3
Test Date 12/13/201012/14/2010 12/15/2010 Run Start Time 8:45:00 AM 9:45:00 AM8:45:00 AM

Run Finish Time 5:15:00 PM6:15:00 PM5:15:00 PM Net Run Time, minutes 480 480 480 Dry Gas Meter Volume Sampled, dscf 239.226 234.030 239.226 237.494 Moisture Content of Stack Gas, % 10.45 9.94 10.45 10.280 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Carbon Dioxide, % 10.3 10.3 10.3 10.300 Oxygen, % 8.1 8.1 8.1 8.100 Average Stack Gas Temperature, °F 262.29 262.83 262.29 262.470 Dry Volumetric Flow Rate, dry scfm 0.0 0.0 0.0 0.000 Actual Wet Volumetric Flue Gas Flow Rate, acfm 0.0 0.0 0.0 0.000 Percent Isokinetic of Sampling Rate, % 103.3 102.2 103.3 102.933 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000
Fw 10320 10320 10320 10,320.000
Fc 1420 1420 1420 1,420.000



### Monday, March 07, 2011 Page 5 of 18

### LocationStack Exit - Method 29 Average

Run Number 1 2 3
Test Date 12/16/201012/16/2010 2/17/2010 Run Start Time 8:20:00 AM2:08:00 PM8:45:00 AM Run Finish Time 12:50:00 PM6:38:00 PM1:15:00 PM Net Run Time, minutes 240 240 240 Dry Gas Meter Volume Sampled, dscf 121.854 116.797 118.955 119.202 Moisture Content of Stack Gas, % 10.54 10.57 10.36 10.490 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Carbon Dioxide, % 10.3 10.6 10.5 10.467 Oxygen, % 8.1 7.7 7.8 7.867 Average Stack Gas Temperature, °F 261.54 261.00 261.08 261.207 Dry Volumetric Flow Rate, dry scfm 0.0 0.0 0.0 0.000 Actual Wet Volumetric Flue Gas Flow Rate, acfm 0.0 0.0 0.0 0.000 Percent Isokinetic of Sampling Rate, % 102.8 102.7 103.2 102.900 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000
Fw 10320 10320 10320 10,320.000
Fc 1420 1420 1420 1,420.000



### LocationStack Exit - OTM - 27/28 Average Run Number 1 2 3
Test Date 12/15/201012/16/2010 12/16/2010 Run Start Time 12:00:00 AM Run Finish Time 11:29:00 PM Net Run Time, minutes 120 Dry Gas Meter Volume Sampled, dscf Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Carbon Dioxide, % 10.2 10.200 Oxygen, % 8.1 8.100 Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % F-Factor, dscfm/MMBtu @ %O2 9190 0 0 3,063.333
Fw 10320 0 0 3,440.000
Fc 1420 0 0 473.333



### Monday, March 07, 2011 Page 6 of 18

### Emissions Summary



### Location: Stack Exit - Method 23 Compound: 1,2,3,4,6,7,8-HpCDD Average RunNumber 1 2 3 Mass_mg 0.0000000071 0.0000000043 0.0000000066 0.000 lb/mmBtuO2 9.82E-13 6.08E-13 9.13E-13 0.000 ng/dscm 1.05E-03 6.49E-04 9.74E-04 0.001 ng/dscm@7%O2 1.14E-03 7.05E-04 1.06E-03 0.001 

### Compound: 1,2,3,4,6,7,8-HpCDF Average RunNumber 1 2 3 Mass_mg 0.0000000078 0.0000000028 0.0000000059 0.000 lb/mmBtuO2 1.08E-12 3.96E-13 8.16E-13 0.000 ng/dscm 1.15E-03 4.23E-04 8.71E-04 0.001 ng/dscm@7%O2 1.25E-03 4.59E-04 9.46E-04 0.001 

### Compound: 1,2,3,4,7,8,9-HpCDF Average RunNumber 1 2 3 Mass_mg 0.0000000029 0.0000000024 0.0000000036 0.000 lb/mmBtuO2 4.01E-13 3.39E-13 4.98E-13 0.000 ng/dscm 4.28E-04 3.62E-04 5.32E-04 0.000 ng/dscm@7%O2 4.65E-04 3.93E-04 5.78E-04 0.000 

### Compound: 1,2,3,4,7,8-HxCDD Average RunNumber 1 2 3 Mass_mg 0.0000000033 0.0000000025 0.0000000031 0.000 lb/mmBtuO2 4.56E-13 3.53E-13 4.29E-13 0.000 ng/dscm 4.87E-04 3.77E-04 4.58E-04 0.000 ng/dscm@7%O2 5.29E-04 4.09E-04 4.97E-04 0.000 

### Compound: 1,2,3,4,7,8-HxCDF Average RunNumber 1 2 3 Mass_mg 0.0000000043 0.0000000031 0.0000000035 0.000 lb/mmBtuO2 5.95E-13 4.38E-13 4.84E-13 0.000 ng/dscm 6.35E-04 4.68E-04 5.17E-04 0.001 ng/dscm@7%O2 6.90E-04 5.08E-04 5.61E-04 0.001 

### Compound: 1,2,3,6,7,8-HxCDD Average RunNumber 1 2 3 Mass_mg 0.0000000032 0.0000000024 0.0000000031 0.000 lb/mmBtuO2 4.43E-13 3.39E-13 4.29E-13 0.000 ng/dscm 4.72E-04 3.62E-04 4.58E-04 0.000 ng/dscm@7%O2 5.13E-04 3.93E-04 4.97E-04 0.000 

### Compound: 1,2,3,6,7,8-HxCDF Average



### Monday, March 07, 2011 Page 7 of 18RunNumber 1 2 3 Mass_mg 0.0000000067 0.0000000027 0.0000000042 0.000 lb/mmBtuO2 9.27E-13 3.82E-13 5.81E-13 0.000 ng/dscm 9.89E-04 4.07E-04 6.20E-04 0.001 ng/dscm@7%O2 1.07E-03 4.42E-04 6.73E-04 0.001 

### Compound: 1,2,3,7,8,9-HxCDD Average RunNumber 1 2 3 Mass_mg 0.0000000035 0.0000000027 0.0000000034 0.000 lb/mmBtuO2 4.84E-13 3.82E-13 4.70E-13 0.000 ng/dscm 5.17E-04 4.07E-04 5.02E-04 0.000 ng/dscm@7%O2 5.61E-04 4.42E-04 5.45E-04 0.001 

### Compound: 1,2,3,7,8,9-HxCDF Average RunNumber 1 2 3 Mass_mg 0.0000000042 0.0000000036 0.0000000035 0.000 lb/mmBtuO2 5.81E-13 5.09E-13 4.84E-13 0.000 ng/dscm 6.20E-04 5.43E-04 5.17E-04 0.001 ng/dscm@7%O2 6.73E-04 5.90E-04 5.61E-04 0.001 

### Compound: 1,2,3,7,8-PeCDD Average RunNumber 1 2 3 Mass_mg 0.0000000032 0.0000000019 0.0000000032 0.000 lb/mmBtuO2 4.43E-13 2.69E-13 4.43E-13 0.000 ng/dscm 4.72E-04 2.87E-04 4.72E-04 0.000 ng/dscm@7%O2 5.13E-04 3.12E-04 5.13E-04 0.000 

### Compound: 1,2,3,7,8-PeCDF Average RunNumber 1 2 3 Mass_mg 0.0000000053 0.0000000028 0.0000000028 0.000 lb/mmBtuO2 7.33E-13 3.96E-13 3.87E-13 0.000 ng/dscm 7.83E-04 4.23E-04 4.13E-04 0.001 ng/dscm@7%O2 8.50E-04 4.59E-04 4.48E-04 0.001 

### Compound:2,3,3',4,4',5,5'-HpCB (PCB189) Average RunNumber 1 2 3 Mass_mg 0.0000000068 0.0000000098 0.000000007 0.000 lb/mmBtuO2 9.40E-13 1.39E-12 9.68E-13 0.000 ng/dscm 1.00E-03 1.48E-03 1.03E-03 0.001 ng/dscm@7%O2 1.09E-03 1.61E-03 1.12E-03 0.001 

### Compound:2,3,3',4,4',5/2,3,3',4,4',5'-HxCB (PC Average RunNumber 1 2 3 Mass_mg 0.0000000554 0.0000000535 0.0000000533 0.000 lb/mmBtuO2 7.66E-12 7.56E-12 7.37E-12 0.000 ng/dscm 8.18E-03 8.07E-03 7.87E-03 0.008 ng/dscm@7%O2 8.88E-03 8.76E-03 8.55E-03 0.009



### Monday, March 07, 2011 Page 8 of 18

### Compound:2,3,3',4,4'-PeCB (PCB105) Average RunNumber 1 2 3 Mass_mg 0.000000163 0.000000121 0.000000118 0.000 lb/mmBtuO2 2.25E-11 1.71E-11 1.63E-11 0.000 ng/dscm 2.41E-02 1.83E-02 1.74E-02 0.020 ng/dscm@7%O2 2.62E-02 1.99E-02 1.89E-02 0.022 

### Compound:2,3',4,4',5,5'-HxCB (PCB167) Average RunNumber 1 2 3 Mass_mg 0.0000000261 0.0000000211 0.000000008 0.000 lb/mmBtuO2 3.61E-12 2.98E-12 1.11E-12 0.000 ng/dscm 3.85E-03 3.18E-03 1.18E-03 0.003 ng/dscm@7%O2 4.18E-03 3.45E-03 1.28E-03 0.003 

### Compound:2,3,4,4',5-PeCB (PCB114) Average RunNumber 1 2 3 Mass_mg 0.0000000079 0.0000000077 0.0000000078 0.000 lb/mmBtuO2 1.09E-12 1.09E-12 1.08E-12 0.000 ng/dscm 1.17E-03 1.16E-03 1.15E-03 0.001 ng/dscm@7%O2 1.27E-03 1.26E-03 1.25E-03 0.001 

### Compound:2,3',4,4',5-PeCB (PCB118) Average RunNumber 1 2 3 Mass_mg 0.000000433 0.000000325 0.000000282 0.000 lb/mmBtuO2 5.99E-11 4.59E-11 3.90E-11 0.000 ng/dscm 6.39E-02 4.90E-02 4.16E-02 0.052 ng/dscm@7%O2 6.94E-02 5.32E-02 4.52E-02 0.056 

### Compound:2',3,4,4',5-PeCB (PCB123) Average RunNumber 1 2 3 Mass_mg 0.0000000077 0.000000008 0.000000008 0.000 lb/mmBtuO2 1.06E-12 1.13E-12 1.11E-12 0.000 ng/dscm 1.14E-03 1.21E-03 1.18E-03 0.001 ng/dscm@7%O2 1.24E-03 1.31E-03 1.28E-03 0.001 

### Compound:2,3,4,6,7,8-HxCDF Average RunNumber 1 2 3 Mass_mg 0.0000000073 0.0000000025 0.0000000024 0.000 lb/mmBtuO2 1.01E-12 3.53E-13 3.32E-13 0.000 ng/dscm 1.08E-03 3.77E-04 3.54E-04 0.001 ng/dscm@7%O2 1.17E-03 4.09E-04 3.84E-04 0.001 

### Compound:2,3,4,7,8-PeCDF Average RunNumber 1 2 3 Mass_mg 0.0000000108 0.0000000058 0.000000007 0.000 lb/mmBtuO2 1.49E-12 8.20E-13 9.68E-13 0.000



### Monday, March 07, 2011 Page 9 of 18ng/dscm 1.59E-03 8.75E-04 1.03E-03 0.001 ng/dscm@7%O2 1.73E-03 9.50E-04 1.12E-03 0.001 

### Compound:2,3,7,8-TCDD Average RunNumber 1 2 3 Mass_mg 0.0000000022 0.0000000017 0.0000000022 0.000 lb/mmBtuO2 3.04E-13 2.40E-13 3.04E-13 0.000 ng/dscm 3.25E-04 2.57E-04 3.25E-04 0.000 ng/dscm@7%O2 3.53E-04 2.79E-04 3.53E-04 0.000 

### Compound:2,3,7,8-TCDF Average RunNumber 1 2 3 Mass_mg 0.0000000029 0.0000000016 0.0000000017 0.000 lb/mmBtuO2 4.01E-13 2.26E-13 2.35E-13 0.000 ng/dscm 4.28E-04 2.41E-04 2.51E-04 0.000 ng/dscm@7%O2 4.65E-04 2.62E-04 2.73E-04 0.000 

### Compound:3,3',4,4',5,5'-HxCB (PCB169) Average RunNumber 1 2 3 Mass_mg 0.0000000071 0.0000000111 0.0000000087 0.000 lb/mmBtuO2 9.82E-13 1.57E-12 1.20E-12 0.000 ng/dscm 1.05E-03 1.68E-03 1.28E-03 0.001 ng/dscm@7%O2 1.14E-03 1.82E-03 1.39E-03 0.001 

### Compound:3,3',4,4',5-PeCB (PCB126) Average RunNumber 1 2 3 Mass_mg 0.0000000083 0.0000000093 0.0000000083 0.000 lb/mmBtuO2 1.15E-12 1.31E-12 1.15E-12 0.000 ng/dscm 1.23E-03 1.40E-03 1.23E-03 0.001 ng/dscm@7%O2 1.34E-03 1.52E-03 1.34E-03 0.001 

### Compound:3,3',4,4'-TCB (PCB77) Average RunNumber 1 2 3 Mass_mg 0.0000000991 0.0000000657 0.0000000412 0.000 lb/mmBtuO2 1.37E-11 9.29E-12 5.70E-12 0.000 ng/dscm 1.46E-02 9.92E-03 6.08E-03 0.010 ng/dscm@7%O2 1.59E-02 1.08E-02 6.60E-03 0.011 

### Compound:3,4,4',5-TCB (PCB81) Average RunNumber 1 2 3 Mass_mg 0.0000000073 0.000000011 0.0000000083 0.000 lb/mmBtuO2 1.01E-12 1.55E-12 1.15E-12 0.000 ng/dscm 1.08E-03 1.66E-03 1.23E-03 0.001 ng/dscm@7%O2 1.17E-03 1.80E-03 1.34E-03 0.001 

### Compound:OCDD Average RunNumber 1 2 3


### Monday, March 07, 2011 Page 10 of 18Mass_mg 0.0000000149 0.0000000041 0.0000000122 0.000 lb/mmBtuO2 2.06E-12 5.80E-13 1.69E-12 0.000 ng/dscm 2.20E-03 6.19E-04 1.80E-03 0.002 ng/dscm@7%O2 2.39E-03 6.72E-04 1.95E-03 0.002 

### Compound:OCDF Average RunNumber 1 2 3 Mass_mg 0.0000000089 0.0000000033 0.0000000039 0.000 lb/mmBtuO2 1.23E-12 4.66E-13 5.39E-13 0.000 ng/dscm 1.31E-03 4.98E-04 5.76E-04 0.001 ng/dscm@7%O2 1.42E-03 5.41E-04 6.26E-04 0.001 

### Compound:Other HpCDD Average RunNumber 1 2 3 Mass_mg 0.0000000076 0.0000000039 0.0000000066 0.000 lb/mmBtuO2 1.05E-12 5.51E-13 9.13E-13 0.000 ng/dscm 1.12E-03 5.89E-04 9.74E-04 0.001 ng/dscm@7%O2 1.22E-03 6.40E-04 1.06E-03 0.001 

### Compound:Other HpCDF Average RunNumber 1 2 3 Mass_mg 0 0 0 0.000 lb/mmBtuO2 0.00E+00 0.00E+00 0.00E+00 0.000 ng/dscm 0.00E+00 0.00E+00 0.00E+00 0.000 ng/dscm@7%O2 0.00E+00 0.00E+00 0.00E+00 0.000 

### Compound:Other HxCDD Average RunNumber 1 2 3 Mass_mg 0.0000000065 0 0.0000000081 0.000 lb/mmBtuO2 8.99E-13 0.00E+00 1.12E-12 0.000 ng/dscm 9.60E-04 0.00E+00 1.20E-03 0.001 ng/dscm@7%O2 1.04E-03 0.00E+00 1.30E-03 0.001 

### Compound:Other HxCDF Average RunNumber 1 2 3 Mass_mg 0.000000009 0.0000000047 0.0000000066 0.000 lb/mmBtuO2 1.24E-12 6.64E-13 9.13E-13 0.000 ng/dscm 1.33E-03 7.09E-04 9.74E-04 0.001 ng/dscm@7%O2 1.44E-03 7.70E-04 1.06E-03 0.001 

### Compound:Other PeCDD Average RunNumber 1 2 3 Mass_mg 0 0 0 0.000 lb/mmBtuO2 0.00E+00 0.00E+00 0.00E+00 0.000 ng/dscm 0.00E+00 0.00E+00 0.00E+00 0.000 ng/dscm@7%O2 0.00E+00 0.00E+00 0.00E+00 0.000



### Monday, March 07, 2011 Page 11 of 18

### Compound:Other PeCDF Average RunNumber 1 2 3 Mass_mg 0.0000000291 0.0000000052 0.000000019 0.000 lb/mmBtuO2 4.02E-12 7.35E-13 2.63E-12 0.000 ng/dscm 4.30E-03 7.85E-04 2.81E-03 0.003 ng/dscm@7%O2 4.67E-03 8.52E-04 3.05E-03 0.003 

### Compound:Other TCDD Average RunNumber 1 2 3 Mass_mg 0 0.0000000043 0.0000000069 0.000 lb/mmBtuO2 0.00E+00 6.08E-13 9.54E-13 0.000 ng/dscm 0.00E+00 6.49E-04 1.02E-03 0.001 ng/dscm@7%O2 0.00E+00 7.05E-04 1.11E-03 0.001 

### Compound:Other TCDF Average RunNumber 1 2 3 Mass_mg 0.0000000972 0.0000000257 0.0000000348 0.000 lb/mmBtuO2 1.34E-11 3.63E-12 4.81E-12 0.000 ng/dscm 1.44E-02 3.88E-03 5.14E-03 0.008 ng/dscm@7%O2 1.56E-02 4.21E-03 5.58E-03 0.008 

### Compound:Total Dioxins Average RunNumber 1 2 3 Mass_mg 0.0000000516 0.0000000277 0.0000000554 0.000 lb/mmBtuO2 7.14E-12 3.92E-12 7.66E-12 0.000 ng/dscm 7.62E-03 4.18E-03 8.18E-03 0.007 ng/dscm@7%O2 8.27E-03 4.54E-03 8.88E-03 0.007 

### Compound:Total Furans Average RunNumber 1 2 3 Mass_mg 0.0000001963 0.0000000662 0.0000000989 0.000 lb/mmBtuO2 2.71E-11 9.36E-12 1.37E-11 0.000 ng/dscm 2.90E-02 9.99E-03 1.46E-02 0.018 ng/dscm@7%O2 3.15E-02 1.08E-02 1.59E-02 0.019 

### Compound:Total PCBs Average RunNumber 1 2 3 Mass_mg 0.0000008217 0.0000006432 0.0000005506 0.000 lb/mmBtuO2 1.14E-10 9.09E-11 7.61E-11 0.000 ng/dscm 1.21E-01 9.71E-02 8.13E-02 0.100 ng/dscm@7%O2 1.31E-01 1.05E-01 8.83E-02 0.108 

### Compound:Total TEQ Average RunNumber 1 2 3 Mass_mg 0 0 0.000 lb/mmBtuO2 0.00E+00 0.00E+00 0.000



### Monday, March 07, 2011 Page 12 of 18

### Process Run Data ng/dscm #Num! ng/dscm@7%O2 #Num!



### Monday, March 07, 2011 Page 13 of 18

### Process Run Data



### Run Name Value UOM Comments Target Value 1 Heat Input 0 Million Btus 0


### 2Heat Input 0 Million Btus 0
3Heat Input 0 Million Btus 0
1 Average Heat Input 0 MMBtu/hr 0


### 2Average Heat Input 0 MMBtu/hr 0
3Average Heat Input 0 MMBtu/hr 0
1 Steam Output 01000 lb steam/hr 0


### 2Steam Output 01000 lb steam/hr 0
3 Steam Output 01000 lb steam/hr 0
1 Synfuel Firing Rate 0 0


### 2Synfuel Firing Rate 0 0
3 Synfuel Firing Rate 0 0
1 Petroleum Coke Firing Rate 0 0


### 2Petroleum Coke Firing Rate 0 0
3Petroleum Coke Firing Rate 0 0
1 Coal Gas Firing Rate 0 0


### 2Coal Gas Firing Rate 0 0
3Coal Gas Firing Rate 0 0
1 Fuel Oil Firing Rate 0 0


### 2Fuel Oil Firing Rate 0 0
3Fuel Oil Firing Rate 0 0
1 Flue Gas Flow Rate 0 dscfm 0


### 1 Pressure Drop Across FGD (if applicable) 0 in H20 0
1 FGD Scrubber Liquor pH 0 pH 0


### 1 FGD Scrubber Liquor Flow Rate 0 gal/min 0
1 Sorbent Type and Sorbent Injection Rate (if applicable) 0 lb/hr 0

1 Flue Gas Oxygen Content 0 % 0


### 1 Flue Gas Carbon Dioxide Content 0 % 0
1 Flue Gas Moisture Content 0 % 0
1 Flue Gas Sampling Point Temperature 0 Deg F 0


### 1 Flue Gas Pressure 0 atm 0
1 Standard Pressure 0 atm 0
1 Standard Temperature 0 Deg F 0



### Monday, March 07, 2011 Page 14 of 18

### APCD Run Data

Process Lab Run Data 1 Unit Gross Electrical Output 0 MW 0


### 1 Unit Net Electric Generation 0 MWh 0

Run Name Value UOM Comments Target Value 1 List all emissions control devices in order of process flow. Choose from 0 0



### 1 drop down lists. If not on list add description and provide detailed 0 0

1 desription in section 5a. 0 0

Run Name ValueUOM Comments 

### 1 See 4b Comments. 0

Monday, March 07, 2011 Page 15 of 18

### Sampling / Stack Data Results Detail



### LocationStack Exit - Method 23 Average Run Number 1 2 3 Test Date 12/13/201012/14/2010 12/15/2010 Run Start Time 8:45:00 AM9:45:00 AM8:45:00 AM Run Finish Time 5:15:00 PM6:15:00 PM5:15:00 PM Net Traversing Points 11 11 11 Net Run Time, minutes 480 480 480 Nozzle Diameter, inches 0.192 0.192 0.192 0.192 Pitot Tube Coefficient 0.84 0.84 0.84 0.840 Dry Gas Meter Calibration Factor 0.985 0.985 0.985 0.985 Barometric Pressure, inches of Mercury 29.85 29.81 29.85 29.837 Average Orifice Meter Differential, inches H2O 0.83 0.80 0.83 0.820 Dry Gas Meter Volume Sampled, cubic feet 251.146 249.036 251.146 250.443 Average Dry Gas Meter Temperature, °F 85.83 92.48 85.83 88.047 Dry Gas Meter Volume Sampled, dscf 239.226 234.030 239.226 237.494 Total Moisture Liquid collected, g 593 548.9 593 578.300 Volume of Water Vapor, standard cubic feet 27.91 25.84 27.91 27.220 Moisture Content of Stack Gas, % 10.45 9.94 10.45 10.280 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Dry Mole Fraction 0.8955 0.9006 0.8955 0.897 Carbon Dioxide, % 10.3 10.3 10.3 10.300 Oxygen, % 8.1 8.1 8.1 8.100 Carbon Monoxide & Nitrogen, % 81.6 81.6 81.6 81.600 Fuel Factor 1.24 1.24 1.24 Dry Molecular Weight, lb/lb-Mole 29.97 29.97 29.97 29.970 Wet Molecular weight, lb/lb-Mole 28.72 28.78 28.72 28.740 Flue Gas Static Pressure, inches of H2O 1 1 1 1.000 Absolute Flue Gas Pressure, inches of Mercury 29.92 29.88 29.92 29.907 Average Stack Gas Temperature, °F 262.29 262.83 262.29 262.470 Average Velocity Head, inches of H2O 0.8603882654 837010.835502055

0249410.860388265

483701 0.852
Average Stack Gas Velocity, feet/second 61.07 60.18 61.07 60.773 Stack Cross-Sectional Area, square feet 0.000 0.000 0.000 0.000 Dry Volumetric Flow Rate, dry scfm 0.0 0.0 0.0 0.000 Actual Wet Volumetric Flue Gas Flow Rate, acfm 0.0 0.0 0.0 0.000 Percent Isokinetic of Sampling Rate, % 103.3 102.2 103.3 102.933 Percent Excess Air, % 60.3 60.3 60.3 60.300 F-Factor, dscfm/MMBtu @ %O2 9190 9190 91909,190.000 Round Duct Diameter, inches 0 0 0 Rectangular Duct Width, inches 0 0 0 Rectangular Duct Length, inches 0 0 0 Fw 10320 10320 1032010,320.000 Fc 1420 1420 14201,420.000



### Monday, March 07, 2011 Page 16 of 18

### LocationStack Exit - Method 29 Average

Run Number 1 2 3 Test Date 12/16/201012/16/2010 2/17/2010 Run Start Time 8:20:00 AM2:08:00 PM8:45:00 AM Run Finish Time 12:50:00 PM6:38:00 PM1:15:00 PM Net Traversing Points 24 24 24 Net Run Time, minutes 240 240 240 Nozzle Diameter, inches 0.195 0.195 0.195 0.195 Pitot Tube Coefficient 0.84 0.84 0.84 0.840 Dry Gas Meter Calibration Factor 0.985 0.985 0.985 0.985 Barometric Pressure, inches of Mercury 30 30 30.1 30.033 Average Orifice Meter Differential, inches H2O 0.86 0.80 0.81 0.823 Dry Gas Meter Volume Sampled, cubic feet 126.933 121.949 124.638 124.507 Average Dry Gas Meter Temperature, °F 84.35 85.54 89.29 86.393 Dry Gas Meter Volume Sampled, dscf 121.854 116.797 118.955 119.202 Total Moisture Liquid collected, g 305 293.1 292.1 296.733 Volume of Water Vapor, standard cubic feet 14.36 13.80 13.75 13.970 Moisture Content of Stack Gas, % 10.54 10.57 10.36 10.490 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Dry Mole Fraction 0.8946 0.8943 0.8964 0.895 Carbon Dioxide, % 10.3 10.6 10.5 10.467 Oxygen, % 8.1 7.7 7.8 7.867 Carbon Monoxide & Nitrogen, % 81.6 81.7 81.7 81.667 Fuel Factor 1.24 1.25 1.25 Dry Molecular Weight, lb/lb-Mole 29.97 30.00 29.99 29.987 Wet Molecular weight, lb/lb-Mole 28.71 28.73 28.75 28.730 Flue Gas Static Pressure, inches of H2O 1 1 1 1.000 Absolute Flue Gas Pressure, inches of Mercury 30.07 30.07 30.17 30.103 Average Stack Gas Temperature, °F 261.54 261.00 261.08 261.207 Average Velocity Head, inches of H2O 0.8444979145 860150.776975249

7099040.792443828

307631 0.805
Average Stack Gas Velocity, feet/second 60.33 57.83 58.29 58.817 Stack Cross-Sectional Area, square feet 0.000 0.000 0.000 0.000 Dry Volumetric Flow Rate, dry scfm 0.0 0.0 0.0 0.000 Actual Wet Volumetric Flue Gas Flow Rate, acfm 0.0 0.0 0.0 0.000 Percent Isokinetic of Sampling Rate, % 102.8 102.7 103.2 102.900 Percent Excess Air, % 60.3 55.5 56.6 57.467 F-Factor, dscfm/MMBtu @ %O2 9190 9190 91909,190.000 Round Duct Diameter, inches 0 0 0 Rectangular Duct Width, inches 0 0 0 Rectangular Duct Length, inches 0 0 0 Fw 10320 10320 1032010,320.000 Fc 1420 1420 14201,420.000



### Monday, March 07, 2011 Page 17 of 18

### LocationStack Exit - OTM - 27/28 Average

Run Number 1 2 3 Test Date 12/15/201012/16/2010 12/16/2010 Run Start Time 12:00:00 AM Run Finish Time 11:29:00 PM Net Traversing Points 7 1 1 Net Run Time, minutes 120 Nozzle Diameter, inches 0.184 0.184 Pitot Tube Coefficient 0.84 0.840 Dry Gas Meter Calibration Factor 1.02 1.020 Barometric Pressure, inches of Mercury 29.8 29.800 Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet 52.432 0.000 0.000 17.477 Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g 132.8 0 0 44.267 Volume of Water Vapor, standard cubic feet 6.25 0.00 0.00 2.083 Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % 10.2 10.200 Oxygen, % 8.1 8.100 Carbon Monoxide & Nitrogen, % 81.7 81.700 Fuel Factor 1.25 Dry Molecular Weight, lb/lb-Mole 29.96 Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O 1 1.000 Absolute Flue Gas Pressure, inches of Mercury 29.87 Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O 0.8636087722 78662 0.864
Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet 0.000 0.000 0.000 0.000 Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % 60.1 F-Factor, dscfm/MMBtu @ %O2 9190 0 03,063.333 Round Duct Diameter, inches 0 0 0 Rectangular Duct Width, inches 0 0 0 Rectangular Duct Length, inches 0 0 0 Fw 10320 0 03,440.000 Fc 1420 0 0 473.333



### Monday, March 07, 2011 Page 18 of 18