I **~** C abot Oil & Gas Corporation North Region Mr. Steve Socash Residual Waste Program Manager Bureau of Waste Management Pennsylvania Department of Environmental Protection P.O. Box 8472 14th Floor **Harrisb~g,** P A 1 71 01 March 18, 2010 AEC.E!VED . ·, MAR 3 0 2010 01';/'""1"'

· ., **~** •. f ... .; ...... f \,....-. **~.~: ·~-**  **,~-** ,..l.il - --
., • oil .,
. • 1., & **~lt:S:OUAL ~VAS'fE**  Re: Submittal of Cabot Oil & Gas Corporation's 2009 Form 26R- Chemical Analysis of Residual Waste Annual Report by the Generator Dear Mr. Socash: Please fmd attached Cabot Oil & Gas Corporation's submittal of Form 26R- "Chemical Analysis of Residual Waste Annual Report by the Generator" for the 2009 calendar year. We trust this submittal will satisfy the requirements of your Division. Should you have any questions, please do not hesitate to . contact me at 412-249-3854 or via e-mail at John

. Smelko@cabotog.com. Sincerely, John J. Smelko Environmental and Regulatory Compliance Manager- North Region Enclosures: 2009 Form 26R with Attachments cc:/ Mr. Jeff Mulligan- Johnstown Regional Sewage POTW Mr. Mark Dublisky- PSC Environmental Services, LLC Mr. Shawn Barrett

- Clean Harbors Environmental Services, Inc. Mr. Norm Zellers- Sunbury Generation, LP Ms. Karen Zug -US Environmental Inc. File Five Penn Center West, Suite 401, Pittsburgh, Pennsylvania 15276-0120

• 412 249-3850 An Equal Opportunity Employer

**~** <:::) <:::) ]:» -o :::0 I N :po X - .. 0 \J) (/\ 0 c 4 ::c :i:o I'Tl' **(/\~** --i"'' ::'0 ,..,., C) 0 - . ,. . ::--2540-PM-BWM0347 612005 **-~~~~~!~.!!~** COMMONWEALTH OF PENNSYLVANIA DEPARTMENT OF ENVIRONMENTAL PROTECTION BUREAU OF WASTE MANAGEMENT FORM 26R CHEMICAL ANALYSIS OF RESIDUAL WASTE ANNUAL REPORT BY THE GENERATOR

This form must be fully an accurately completed. All required information must be typed or legibly printed in the spaces provided. If additional space Is necessary, Identify each attached sheet as Form 26R, reference the item number and identify the date prepared. The date on attached sheets needs to match the date noted below. General 287.54 Date Prepared/Revised 03/18/10 Company Mailing Address Une 2 c.

- 1 - Generator ID#2540-PM-BWM0347 612005 a. A detailed description the waste, as specified in the instructions, is attached

. b.
.. **,.''""'~T•c** of manufacturing and/or pollution control processes producing

· the waste, as specified In the instructions, is attached. c.

are a confidentiality claim, as described in the instructions, is attached. b. Facility Name c. Address Line 1 Address Line 1 Address City State ZIP Municipality Faclllty Title Phone
County Cambria jeffmulligan@pennswoods.net d. of waste shipped to processing or disposal facility In the previous year. 7,281,120

D cu yd 1:8] gal D lb 0 ton (check one) a. Solid waste permit n b. Facility Name Address Line 1 Address Line 1 Address City State ZIP Municipality c. Facility Contact Name Title Phone 610-731-7200 MDublisky@pscnow.com pped to processing or disposal facility in the previous year. D cu yd 1:8] gal D lb D ton (check one) b.

D ton (check one) -2-

·No2540-PM-BWM0347 6/2005 I certify, under penalty of law, that

I have personally examined and am familiar with the information submitted In this Annual Report and all attached documents and that based upon .my inquiry of those individuals immediately responsible for obtaining the Information,

I verify that the submitted information Is true, accurate and complete to the best of my knowledge.

I understand that the submission of false information herein is made subject to the penalties of 18 Pa. C.S. §4904, relating to unsworn falsification to authorities, which Include fine and imprisonment. Check the following, if applicable

:- - 0

I certify the information required In Section 8-A, General Properties was supplied to the Department for the year __ and has not changed. Form Submitted:

0 Form 26R 0 Other (specify) Date Submitted: O

I certify the information required In Section 8-8, Chemical Analysis was supplied to the Department for the year __ and has not changed. Form Submitted:

0 Form26R 0 Other (specify) Date Submitted: O

I certify the information required in Section 8-C, Process Description and Schematic, was supplied to the Department for the year __ and has not changed. Form Submitted:

0 Form 26R 0 Other (specify) Date Submitted: Name of Responsible Official

Title Date 03/18/1 0 - 3 -ANALYTICAL

& ENVIRONMENTAL LABORATORIES. INC. Randy Spencer Cabot Oil & Gas Corporation 5 Penn Center West Suite 1500 Pittsburgh, PA 15276 March 12. 2010 **Oat~** S13mpied: Time Sampled: bate Received

: Matrix

: Sampled by : PIT/ TANK COMPOSITE. WASTE WATER DIMOCK, PA OPERA 'TIONAL AREA PARAMETER RESULT pH 8.75 Nitrite as N <2

. 50 Nitrate asN

< 10
. 0 MBAS <4.00 BOD6 648 Chloride 21800 Sulfate <2500 Specific Conductance 47840 Hardness 6353 Alkalinity 3110 TSS 60650 IDS 23200 Acidity
<5

. 0 Toluene

0 . 011 Benzene <0.005 Ethylene Glycol

< 10
. 0 Phenols 0.084 TKN

84

. 8 AmmoniaasN

56

. 5 COD 46326 011& Grease
12
. 5 Bromide

71

. 7 UNITS METHOD pH units SM20 4500 H+ B mgiL SM20 4500 N02 B mgll SM 20 4500 N0 3 D mg/L SM 20 5540C mgll SM205210
B mg/L ASTM 0512-89(99)C mg/L ASTM 0516-90,02 uS/em EPA 120

. 1 mg/L **$~23408** mg/L SM:!o2320
B mg/l SM 20 2540 0 mgll SMzo2540C mg/L SM 20 2310 B mg/L EPA624 mg/L EPA624 mgJL EPA8015M mgJL EPA420.4 mg/L SM 20 451ID-NOI'R C rng/L SM20 4500 NH3 D mg/L SM 20 52200 mgJL EPA 1664A mg/L EPA300.0 DICKSON CITY INDUSTRIAL PARK 824 ENTERPRISE STRUT Joe R . Mussan. 111 Laboratory Director DICKSON CITY, PA **18519-151~** PHONE: (570) 489-8984 FAXJ (570) 488-8985 02-Mar-10 __ composite 02-Mar-10 WasteWater LM/SRWR ANALYZED 02-Mar-10 04-Mar-10 04-Mar-10 04-Mar-10 03-Mar-10 12-Mar-10 12-Mar-10 02-Mar-10 12-Mar-10 10-Mar-10 08-Mar-10 08-Mar-10 10-Mar-10 05-Mar

- 10 05-Mar-10 08-Mar-10 10-Mar-10 11-Mar-10 12-Mar-10 11-Mar-10 05 - Mar-10 09-Mar-10o.UANTU4f ANALYTICAL

& ENVIRONMENTAL LABORATORIES, INC. March 12, 2010 Randy
**.§ ~Emcer** 

Date Sampled

: Cabot Oil & Gas Corporation 5 Penn Center West Suite401

Time Sampled

: Date Received

: Matrix

:

02-Mar-10 composite 02-Mar-10 WasteWater LM/SRWR Pittsburgh, PA 15276 PARAMETER Aluminum, total Arssnic

. total B$rium. total **~lyflium,** total Boron, total Cadmium. total Chromium, Ill Cqbalt. total Copper, tlltal Iron, total Iron, DiSSOlved Lfl.ad, total Manganese, total Magnesll!m

, total Mercury. total Molybdenum

, total Nickel, total PQ.tassium Selenium, total Silver, total strontium, total Zinc, total Lithium. total Sodium, total Calcium, total Sampled by : PIT/ TANK COMPOSITE WASTE WATER DIMOCK, PA OPERATIONAL AREA RESULT UNITS METHOD 686 mgll EPA200.7 1.1 mg/L EPA200.7 31.7 mgll EPA200

. 7 <0

. 050 mgll t:;PA200

. 7 4.2 mg/L EPA200.7 < 0.050 mgll EPA200,7 2.2 mgll EPA200.7 0 . 75 mgll EPA200

. 7 4.2 mgll EPA2ob

. 7 1390 mg/L EPA200

. 7 < 1.0 mgll EPA200.7 3.6 mgll EPA200.7 28.8 mgiL EPA200.7 318 mg/L EPA200.7 0.0079 mgll EPA245

. 1 1. 5 mg/L EPA200.7 3 . 2 mgll EPA200.7 327 mgll EPA200.7 <0.25 mgll EPA200

. 7 0.093 mgll EPA200.7 268 mg/L EPA200

. 7 17
. 1 mgll EPA200

. 7 45

. 1 mg/L EPA200.7 12000 mg/L EPA200.7 2020 mgll EPA200.7 ANALVZED 05-Mar-10 05-Mar-10 05-Mar-10 05-Mar-10 05-Mar-10 05-Mat-10 05-Mar-10 05-Mar-10 05-Mar-10 05-Mar-10 09-Mar-10 05-Mar-10 05-Mar-10 05-Mar-10 05-Mar-10 05-Mar-10 05-Mar-10 05-Mar-10 05-Mar-10 05-Mar-10 05-Mar-10 05-Mar-10 05-Mar-10 05-Mar-10 05-Mar-10 DICKSON CITY INDUSTRIAL PARK 824 ENTERPRISE STREET Laboratory Director DICKSON CITY, PA 1851.1513 PHONE: (570) 489-8964 FAX: (570) 489-8985o,UANTU4f ANALYTICAL
& ENVIRONMENTAL LABORATORIES, INC. March 16, 2010 Randy Spencer Cabot Oil & Gas Corporation 5 Penn Center West
Date Sampled: 02-Mar-10 Time Sampled

: composite Date Received: 02-Mar-10 Suite 401
Matrix

: Waste Water Pittsburgh, PA 15276 Sampled by: LM/ SRWR PARAMETER Gross Alpha Gross 86ta Radium-226 Radium-228 PIT/ TANK COMPOSITE WASTE WATER DIMOCK, PA OPERATIONAL AREA RESULT UNCERTAINTY (MDA) UNITS METHOD -30.984
:!. 108 (200) pCi/L EPA900.0M 15.7
:!. 109 (188) pCi/L EPA900.0M 55.7
:!. 11
. 2 (0
. 818) pCi/L EPA903

. 1 5.59
:!. 1.35 (1.14) pCi/L EPA904.0 MDA Minimum Detectable Activity PARAMETER Thorium Uranium RESULT UNITS 0.0773 mg/L 164.8 ug/L DICKSON CITY INDUSTRIAL PARK 824 ENTERPRISI! STREET DICKSON CITY, PA 111519-1513 METHOD EPA200.8 EPA200

. 8 :£9m Laboratory Director PHONI!: (570) 489-8964 FAXr (570) 489-8985 ANALVZED 04-Mar-10 04-Mar-10 09-Mar-10 15-Mar-10 ANALVZED 04-Mar-10 04-Mar-10Test America TH E Uil\OER lN ENVIRONMENTAL "tES **TIN(~** \ldrdo 10.2010

3 : 17;39PM <\un: Quantum AlE Labs. Inc . 824 Enterprise Sttect Dicl\sim City, - f>A 18519 Vi;.;ld Nagy

W<ork Order: NTC02-14 **Prol~ct** Nome· Ethylene Glywl **Pt~~iet1·** Nbr
:

l none
l Pi()Nbr: **Dat~ Rcc~ivcd:**  OJI(J3i!V SAMPLE !J)J,Nl

' !FJCA TION 015-030210

!.All Nl. M.R£R NT( '0.24·!- 0 I COl

. l.f.CIIO:\ IH.Tt. AlliD **l'I ~U**  il3HJ2!Hl Otl;(JI .-\n e.x.-cuted

. copy ofdle chain orcu>t<'ll)·. the **l)l'(lJC~!** ij!talit> < ' ontr<.>l dala, **width~ !~ample**  receipt form Qr.: abo ind\!<lcd ll.i an lldtkndum too **hi~** '"port. **lf~ou hn~**  any **question~** re!Qting t<ltbJs **41l~local** r<'Jll>n. plea.-,., ,;.;mtact )'PUr l.abomtory Po'*'' **Mar.~gtr** ill 1-8ll0-765-09SO. Any (\pinions. **if"'l"~~~ed.** are outside

. the scope uflhc
l . ah<>r•tory'' atetcditariou. Thi$ m4tcttal

· ;s Intended

. onl) for the usc of **th~** iudlvidual(s) or entit; to wh(\1!1 it is addressed. and ma) contain lnfonnati<lfl llmt " privileged and

· i::ilnfidc:ntiat If you ru-e nor the intended recopicnt l)r doe **~'1llploy~** or agent **re~pol~\ibl~** 1\lr dcliveril'i this material lQ rto< !ntendO:d rotiplent, you ru-e hereb y notified that nn) disscminaroon. di.wibutiQn, or cOjlying of this material i.s Sllictly probibln.>d If you **hav~ r~..:dvcd**  **thi~** material

. in ermr
.• pk11sC- noufy us immcdintely at 61 5-726.() 177 **l'cnp~-yl•·oma (;~ifiClllron**  Number: 68-00585 T h< Chaiu(•l wCuswdy,
2 **page~.** are included ;ond arc an integr:,l part of this tep.>n r hc<e results rclal\! only to the it<'n'

' 1•"''"'!

. , hi ' <¢p<.>rt shtdl nvt he rcrt<'lluced **~xcept** in full>mt! **~>i:h** perm;,,;,,. o1rhe l"boratory. ;\ 11 wlid' results an: reportc:J in we-t "eight u111t: 's sp<dtically **>~cd.** I stimatcd **un~.unty** is a•11ilahl< tlpun reque -s t ' ) **h~> r~'P"rl**  hn> bt:ot **e)ectwnicull~**

**<o n<**  Rq"'rt Approved By:

l'uge

I ol 8Test America THE lf:A0£1'1 IN OIV!I'lONMENTAl TESTING (l n:nt Quu:ltum A.:'E Labs. lu..: **82~** Enl<lprist

· Str«'l l'hck

; mCity

, J>A **18~19** "\till \'icJ..I'Nftt') Resulr Work Order Project Ntlfnt: **I~Ojcd** NumMr: R!'<.'CJVCd MJAL YllCAL

. ltEPORT Unill; MDL MR1. Sample lD : NTC0244-01 (015-030110

• Waten Sampled: 03102fl0 UO;OI (jlycol$ by El' A Method 8(ll 5 (modified} Elhykm

· Gly<ol **Sr~,.,. _**  :-Bu,•oxwthtmol

t -16-12996) 1.4; **91~**
l.O() 10.0 NTC0l44 Erhylcm

.. ( J iycol lnmu:J (13l!l.311 ti OHI() Oilution .Fuclfrr Analysis Oaleffime Mclhod Olill&IO **11!<~9 SW~46S0i5B**  I)Jli)JSIJU 1/1:59 Sli'M6 81il511 BolCh IOCW3l lf>I."QVJ/ **l'ag~** 2 ull\Test America i H F. LEA O E:R IN £NVIRONM€NlAl. TE:STING '1ocot (.Jl• .. num NE 1 obs . 1..: **~24 l:ntt:rpris~**  Strt::d l)icl.•on
**~y** PA 18519 **.'\nt!tr~**
fslanl V'?th.c Glycols by EPA Metll.od 801.5 (modifitd) 10C0931·BLK1 f;dlyle1)e **Gly~:ot**

• I.(;() S,'1"f"t'(.J#Ctt

• · : ·fSliiO.\f</h.l#()i 9\l% Wod.Ordl.!r. NTC0244 **Pt~Jc:..1. ~Nn.i**  Ethylene **Gl y~J**  Prt,jt>\.t **t~mher** tnunc] P""O.lECT QlJ"UTY CO?Iil ROt

. . DATA lllnk **tJuit~**

(: .C BAA:h .tng l J. }(!(.."!)«<ll **:0( (1<1).1**  03/()Jfl Q 08
: 00 L•h !-<umber **l0C()9)~** .fill..K.l l!i(

. 09J I·ULIU

.. **.\mip .t..**  **~l}.ll,:** 'Tune \ll-Oit

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E NTAL fltSTINC Cli<'lll Quantum N E l.AI>I

. In< , **~24 Eni<IJ!ris~**  S!n:<t Dickson Ci1y
. PA **l~>l'i** Attn ViddNa.gy J\JmlyW Glyrob by .EPA Mer hod 80l5 (modif!Cd) **10C09~1•.8$1** Ertrylme GJyi.'CI **l'rog:J~** J..81./,hX)>rlikJU vl ._....,..,Vol
: 1i) . O **0** Wc'fl< Order Pmjl"(.t NNn .. • · **pro_~(":t** Number **l~cet·n cd**  I'ROJEC:T QI J .. \U'f-\cCON:ntOl

. llXU LCS

NT<' 0 24·1 Ethylene **Gl ~**  (nunc] {)3.'03il0 08 . ()(1 **'\n~ly.te'd** V..al

0 **ma;:~; ~"'**  R!!e **4~** "! mg"L 43 7
9J'!t T"f"' AM! yJ' ...:d **iUpg~** Borti! t; Date ·n u·w 71. 12! **lt>C~JI**

0 .;1:1)& 10 j! 17 **129** l(l('JO;I

0 } U8.10 lip Page 4 t:>f 3Test America Clknt f.)u3Juum Nr l.:rlx;., "'' 824 Emerpn<e SW<1 ()JcksvnOty, PA 18Sl9 Attn Vi.;.l<i Nagy **Glyco~** by U'A M.dhod 8015 (modified) 10C0931-MS1 W<nk{ltdcr ...-IP.IC<..tNt'J W ! **Pr~jc!c1 'Num~r**  **R~'CI\"i!d.** J'ROJf:<l' Qli AI.rfY ('O"'TROL DA T.'\ Matrix St•ike Omt? .16.1 l'iTCOH4 **f;th~lcm: Gl~:.:ol**  '""""' HY03:10 **08~~!0** ltl(DIIll llll:<ml Sut:Tpi!' 'i.p·•e.J NrCt•ll"-41 Arui\lt::tf Dalc·r,r:-:Test America THI! l€AOER IN tNViRONMEN1Al. "'li!Sfti'IG CUt"nt (luu.n1mn **J\;l~** lltb \. hu. **~14 En~rJ'fi"se**  Strrcl **Dit:~5CJnCI!y** F•A **IS~** It; Am• V1cki Nom Gly<Ois by EPA Methud 8015 (m<>dlfted) **10C0931~MSD1 Eib)'ff'tt~**  01)'¢1 Slt!'r<Jgqlr

; **}•lhJk,.A}~IIWIH.I'!**

.:.l.6 **·~** Wr_,rktlrdcr PwJecr NnmL' l'r•>jc.:cl Nnmbt.'f· Rccci\'td. 'if(02H FlhjJcne (.,ty\:

: ol [none] VHtliiOO&·O(i PROJECr QtJ.\LITV COii:TROI ... DATA **'~<btri~** Spik• Dup **~•kc** Tqcl t ' rnts Lc.'l.. "-,. Re.: **Ra.n~c** RPO
t im!t 'SUQ Si 11 '- -U · t.W $0 _ t,; **~ -ll\-1~9**  1t:Jttl931 IOC(i"131 **~:;mpJ.) lr.;rh~tcd**  **~('0119-<ii :-fi\;PI~Ii** 
M 0...'1
; C - 1 **~d~S u.~**  **~** n l)f.vflTest America T HE UAD E H ftJ !:NVIRONMI:NTAL TESTIN G C lh. • _ n l **Qu ~mtum**  :\. 1.- L ;t b , lu<. 8:!4 **rnw m~**  ,S trt:-et **Oid,,'¢1l<.i~C-.** PA 13:'1\1 , o\mt V!Cid N'<tg} Mell> <>ti SW!\46 81Ji>B **M~trix** W-ater WorkOrd<r

· Pmjrct **No:n~** Pr\"",to.: <: l Numbct **RI!:~CIYt'd** CER'IlFJCATIO:"i SUMMARY Nda:
.: NTC 0 !44 Elhrtnw: 0lv«>

l lnnm:} ((\1(13

; 10 OS 00 X

i ' •; uTestArnerica (;lK>tl1 (.lUMU!Ilt

: \:-1: **l.t!~ lfi.C**  .!-i1:4 £merprJ'5(' Street Di1.:k:..Tm·Cit). PA ISS I•.' 1,\-,)Jk(lfdL'f

. l>ro .. **~~..'t** Namt Pw,:ect Numl'oct **Rt'CC:I~""Ctl NTCI12~4**  **Fthyl~n¢ Ol~eol**  fnoncj !lYOJiiO 08
· 00 OAT,;\ QI.\J,UU

: RS A -.o UHii\J liONS .J Ano.lyrc **!ktc~ted ur~**  levd ks.> t.h•n the Rcptllting l.imit tRL land **grett~r** th.m or cqun! l<> the Mclhvd fktcclion

l. tmtt I MDL). Com:cntrJIIUfiS \\tthln thi$ range tln! C',)1in)all

.. >d . i\'D N<rt **d.:r.:ct~d** at the **r~pt1ning** limtl formetMd dete..1:ion limit ir **hom')** METHOD MOIHFICA TIO"' NOTtSLAB 10: 39-00401 LAB ID: 08-00380 SEND DATA TO: NAME: COMPANY: ADDRESS: PHONE: FAX: 015-030210 Joe Mussari Quantum La!:} 824 Enterprise Street Dickson City; PA HJ519 (570) 481).6994 (5 70) 489-6965 RECEiVED FOR LAB BY: DLM2 SAMfilE: 01$.03021() SAIAPL£0 BY· Client. SAMPLE: 01 $.030.210 SAMPLED BY. Client REMARKS: Benchmark Analytics, Inc. Eastern Division 2566 Pennsylvania Ave. Sayre. PA 18840 Phone: (570}888cQ169 Fax: (57m 888-0717 TEST REPORT WO#: PAGE

· PO#: PWSID# Work Order: 10030546 10030546 1 of 1 DATE: 03/0312010 17
: .05 Pagel of I Result 71.7-mgJL B!!ilil.! 0.1le.4 ntg/L ub ID: 100J0546,.001A Composite EPA300.0 Sample Tome: 03/o212010 0:00 !4tJbgsl EPA420.4 An!!MIS S!art J\!1a!'M End **~e** 2.50 03109110 9:55 03/DQI10 HOP.CV Analvs!s Stari Anatt§ia ED!! **~** 0.1l25 03110/1011:14 03/10/10 RHN-SA The at>ove test procedures meet all tml requirements of NELAC ar.C relale only to **~hess** samples. • CV"' Benchmar1\ Arlalytics,lnc

. Celll!!K Valley, PA ; SA = BeriChmark Anatylics; me , Sayle, PA z Due 1<> mat11x tllas, spike l'l!(lQYefY **wa:~ ou~i<)e**  ae<:eplanre nmHs MANAGER /1 ""'· **~~:~** - **·---~------~-----·--······--**
DATE: J!fi)I]()J()LAB 10: 39-0.0401 LAB ID: 0 8 -00380 SEND DAT.t>. TO ; NAME: COMPANY; ADDRESS: PHONE

: FAX: Joe Mus.sari OO<Jntum-L.ao 824 Enterpr

i se Street Didtson City, PA 18519 {570)489-6964 {570) 489-6965 General Pricing RECEIVED FOR LAB BY: OMB SAMPLE

: 015.030210 SAMPLED BY : Client ml Thori u m Uran•Um **U~;aniim** REMARKS Benchmark Analytics, Inc. 4777 Saucon Creek Road Genter Valley

, PA 18034 Work Order: 10030350 Phone

· (610) 974-8100 Fax
: (610) 974-8104 TEST REPORT WO#: PAGE

· PO#: PWSID# 10030350 1 of 1 DATE

: 0310312010 8:40
I'age I ofl **~** 0 . 0773fT91., 164

: 81lgll 110.4 pCf/L Lab it> : 1003035Q-001A Gral) Sample Tlll1&

: 03/0212010 0:00 0 lCO .Mdl2d. EPA200

. 8 . EPA200

. 8 EPA2008

Bl!9.. l.l!!:!ii

. Anatylp!$ Start O::V03110 9:15 30 03/03110
9 · t5 **~109:15** Alla!vsisEnd **~** 03/04110 JRA.CV 03104110 JRA.CV 03104/10 JRA·O/ Tile abo v e t est procedures meet aH the requirements c! NE L A C ;md relate only to lhes& samples. • CV **~** Be'lChmari< Anelyti(:s

. · rnc. Center Va!le y , PA ; SA = Benchmark Analytic$, ll'IC. Sa)'!'$

, PA Q 0_,., !C mattix effects. not all quali:y Ccllitrn! param•lers mel a<:cep!ance crltelia MANA G ER - ---

· -- - - ___ **~~**

.. .. ........ ---· --·

· -·- - - DATE

: Ji 8 ! 2 (! / 0March

1 6 . 2010 Mr. Joe Mus.sari Quantum Analytical & Environmental 824 Enterprise Street Dickson City, PA 18519 RE : -proj(Jct: RAD AND METALS Pace Project No

. : 3023711 Dear Mr. Mussari:

**P~~<oo** Anollfllc>l S.Mc4s. In<. H;16 Ro....,..,.., Roaa- Suites 2.J,4 o-tli5bUI'g, PA 15001 (724;!)5Q.56((1 Enclosed are ttte al'lalytical results for sample(s) received by tne laboratory on March 03, 2010. The results relate orily to the samples included in this report

. ResultS reported herein conform to the most current NELAC standards. where applicable. unless otherwise narrated in the body of _ the report. Cooler **t~pe~e** 7.4 • C upon receipt Ice was present. lf you have any questions concerning this report. please feel1ree to contact me . Sincerely, Rachel Christner rachel.christner@pacelabs.com Project Manager REPORT OF LABORATORY ANALYSIS r, **:i~** r;,:po rt f,.tMii r<U t brf n'!J'Irt>d!.ICO<J, CX'C'Opl ..-: iuit **;,t::l !~U~**  i•;e **~mnnn** <'Cfi sel'lt of Poce **Ana~** SetVJe:es ir.c - nelac
'•,Q"J / .. FiceAnalytica( ......
. p.s:tnb!

. ...., RAO AND METAlS 3023"f11 CERTIFICATIONS **PJ~nnsylvanla** Certification IDs ·r;;38 Roseytowr. Read Solros 2.3&4 Gmensburg, PA 15601 Massachusetts Ce:tilir.at!Qn #: M-PA1457 Ma,YI;!nd Certifiro1:on #. 308 Wyomltlg Cenillcatlon #: 8H .. 'IS-Q \"'t..<e;eonsii"'JPAOEP <AirttncaSOn Wes! Virginia Corti/ication !1: 143 \'J3shlng:oo Certmcatlon #: .C1941 VIrginia Certffi<Oation #: 00112 Vrrgin l:;tandiPADEP Cortlfu:ation IJtahiNElAC C.etiificollon #:ANTE Texas!NELAC CmMeation #: T1047041li6-09 TX Tennessee Ceftffication #: TN2867 **Sou~r** Dakota Ceriifleation Puerto Rieo Cefllfics1ion 1#: PAIJ1457 **Pennsylvania!NElAC ~**  #: ®$5-282 OregoniNElAC C$t!illt:alion #:. PA200002 North Carolina Certlf\cation #:- 42706 New YorkliiiElAC Certification#: 10888 New M&x!G6 Certlflcallon

·
· Ne-"' Jersey!NELAC

. teru11caiion #: PA 051 New **Ham~hireiNElAC** CertlflcaliOn #; 2976 Nevada **Certifi~**

.
.. Montllna Certification#. Cort **~82** MissOuri Certifrcalion
#
' . 235· **Mid1J9an.'PADEP~~_!!~ ~--·**  **~-lain&** CertificatiOn II. PA0091 Loulslatta<NELAC **Certi~eation**

# • LA080002 Loui•iana!NElAC CertifiCa('On
# : 4085 ' Kantircky **Certific:~tion** #: 00133 Kansa$.'NELAC **Cetlifica~on** #: E-10358 Iowa e&nl!lcation ·#: 391 lndianaiPAOEP (:ertifor.ation liUnolsiPAOEP Cortiflcatkln IdahO Certificlation HawaliiPADEP Certificahon Gi.amiPADEP Certiflcallon Ge<ifgia eerufi<:&tm 11.'968 Florida!NELAC Certif!C<Ition #: E67663 Delaware. Certification Ccnnecti.;ut t!'ftincal!on II: PH 0694 Colorado Certlffcation Califon'lia/NELAC C'..erl!llcation
#: 04n2CA Ari<ansas Cei'lific:ation ArilDna Certlf>G<Jiion

. #: AZ0734 Alabe<l);l Certification ·it 41590 REPORT OF LABORATORY ANALYSIS **i':.1~X\rt ~!1flli'JCI!**  bte **~toduc~ M**  **.·:~~~H ~:**  Ju:; ""' tl " t:J •• ' **;:e** wrl!i t> !'! **t~ll** c.f **P.x.e At**  **a~ -:1!**  S r. .. **·Ac;tl~**

l n.:: .: netac

' . .

.
Pocv AnQJytical ServkQs, Inc :0:38 Rosft,..lt:i'Ari' Roao SW.$ .:.3,4f ,;_,.b<Jrg. 1'4 '1561)1 t r2.!J65C-'50oo Page 2of 1 4Project. RAD AND MEiALS Par.e Project No.: 3ll23711 Sarrople: 015.030210 Pa!e!:mete-rs 200.7 **r~elats,** Total Alurninum Arsenic Barium Beryl hum **Bo<Of~** Cadmium Calcium Chrorr-ium Cobali Copper Iron lBad LithJum **Magne~ium** Mangpncse Molybdenum Nidc:&l **Potasa~** Selenium SilVer Sodlum Strontium ZlllG 200.7 **Met~ls,** DISsolvor,! •rcn, Oi$sotved 245,2 Mercury ANALYTICAL RESULTS
l'llu Analytic<>l S.NI,_, In<:. -:638 **R~:.OW'I"'** ftond
• **S~s.** ;Z.3..4 Gmensbc.lt'9

. PA **1~601 U~4;8!10-i?BQG**  Lab 10: 3023711001 Collect ad · o:l!o2t10 oo oo Received 03103/10

1: 0 ' 30 MalriX Wa:ter Results Ullits ReiJQrt Limit DF .PYepaoeo Analytical Method: EPA200 7 Pri<paoalion Method. EPA200.7 686 mgiL

2 . 5 10 03104!10 1N5 1.1 mg!L 025 10 o31o4fm 11 : 45 31
. 7 mg/L 05\J 10 03!04110 11 : 45 NO mgll

0 . 050 10 03104110 11 : 45 4 . 2 mgtL
2,5 10 03.104110 11:45 NO mgtl

0 . 050 10 03i04ito 11:45 2020 mg)L 50.0 10 03104i1{) 11;45 2.2 rngll

0 . 25 10 .03/04!10 **11:.~5** 0.75 mg/L 0:25 10 _031()4!1 0 11·.4 5 4.2 mgiL 0.25 10 03104/1011:45 1390 rn!J>ll
25 10 03i04i10 11:45 3.8 mgll 010 10 03104110 11:45 4$.1 ln9IL

2 . 5 10 03,1{)4110 11:45 318 1)1gil

10
. (1 1!> o.3t04i10 11:45 28.8 mgil

0 . 25 10 031{)4110 11:45 1.5 mgtL

1 . 0 10 03194110 11;45 3.2 l'ngll.

0 . 50 10 03/04110 11:45 327 mgtL 25.0 10 03itW10 1"1:45 NO mgll 025 10 03/04110 11 : 45 O.oiJ3 m!iJL

0 . 050 fO 03104110 11:45 12000 mgtL

50
. 0 10 03104110 11 ; 45 268 mgJL

**~5** 10 03104110 11:45 17.1 mgiL 0.50 io "03104!10 11:45 Analytical Method: EPA20!>.7 Preparation Melhoo· EPA200.7 NO 111g1l.
1.0 tO 03105!10 14:24 Analytical Method: EPA245.2 Prep<lrotion Mathod: EPA 245.2 0.0079 mgll 0.00050 03104110 12:07 REPOR T OJ= LABdRATORY ANALYSIS lnrs re pen s hall not t)e t l:!Of lJCJ Urt.>e v oc r e p : • rl .-.: J t ' I CM: tt.e w nrtan c;:onsent of PlJ:::::e. **~** l '" t
' I'(, • ) '!" t)f **~'lr!t** trv:- ,; f1eJac

· Aouty:eC CAS No Qua! 03105110

' 14
: 02 7429--90·5 03105110 14
: 02 7440-38·2 03 1 05'10

' 14

' 02 7440-39-3 0 . 3105/10 14 : 02 7440-41;7 03105110 H
: 02 744().42-8 03 .l ii5110 14 : 02 7440-43-il 03105110 14:02 7440.70·2 0:1!05110 14 : 02 7440.47-3 03/05110 14
: 02 7440.46-4 03105110

. 14:02 '1440·5().8 o3lo5i10 14:02 7439-89--6 O:ir'OS/10 1-4:02 74.19-92·1 03!05!!0 14 : 02 7439-93·2 03i05i10 14 : 02 74:19,.95-4 031051-10 14
: 02 7439-96'-6 OJ/051!0 14:Q2 7439-lliH 03/05110 14:02 7440-02,{) 03105!10 1-4 : 0?. 7440-01J,.7 Oato51'10 14 : 02 7782-4g,.2 031{)511 0 14
: 02 7440-'22-4 03105110 14:02 744().23·5 031{)511 0 14M '1440-24-6 031{)511 0 14:02 **'144~** 03/09110 10
: 49 **7439-~** 03105110 10.04 **7~39-97-6** Pag<> 3 **ol1~**PrOject RAD AND METALS Pace'Proje<:t No. **~0237,1** QC Battll. MPRPi3439 ac·earch Method: EPA 200.7 AsSoCiated **L~b** Sam!Jles

. 3023711()01 **MET~IOO** B!.ANK. 145791 Associated Lab S:Jmp!as· 3023711001 QUALITY CONTROL DATA Analysis Method. Anaty

. sis 08SC':tiption Matrix: Wete: EP.._20!J.f 200 7 **Me!~!s,** Total **.P~** AM'Yt'ca.I

· Servfc.es. Inc. **''h:5:"~8 Ras«t~**  **~d Sot:~s-**  2.3.4 **i.:~ret\~turg,** F·t, -:; 5&1 1 **~7'24}esa-sgec** Parnrncter Resun Limit Ana!y.zed 03<05110 12:06' 03!()5110 12:08 Ol'()5110 12:00 03.105110 12:00 O:J/05!10 12:06 03105!10 12:00 03105!10 12:06 03/j);i!W 12:06 03'05!1 0 12:06 \}3.105110 12:06 03105!10 :2:00 01105!10 12:06 03105!10 12:06 03!05111) 12:06 03/il(\.11 0 12:06 03/05!'1 0 12:00 03i05i!G 12:00 03!0!>'
I 0 12:06 O:li05i1 0 12:06 03!05!10 12:06 03!05110 12:06 Q3i05! H) 12:06 03!05'1 0 12:06 Quallflers -------------- **-~--·-----** ----- ------ .f\ium.inum mQIL
NO IW50 .Arsenic
mgll

.
NO

0 . 0050 Batiun1 msJL
NO 0.010 86rylllun1 mgil
NO

0 . 0010 BOron mgil
NO o.oso Cadmium mgiL
NO 0.0010 Calcium
mgil.
NO 1.0 Chrornium mg/L
NO 0,0050 Co!Jslt mg/L
NO ().0050 Coppet mg!L
NO o.oo5iJ Iron mgiL
NO 0.050 Lead mg/L
NO 0.0020 lilhil!rn n>giL
NO o.oso M.91Jnesium
mg/1.
NO 0.20 **~nese** mg/L
NO 0.0050 Molybdenum '"9'L
No

0 . 020 Nickel mg;J..
NO 0.010 Po[asSi\Jm mg'L
I'IP 050 Selenium mgll
NO 1Hi050 Silver
rngiL

.
NO 0.0010 Sodium "'9IL
NO

1 . 0 Strontium mg!L
NO 0.0050 Zinc <ngiL
NO 0:010 LABORATORY CONTROL SAMPLE· 145192 Spike LCS lCS Parameter Units C!lnc. **~suit** %Re< ---·------ --·-- ·---------- -------- ---------· Aluminum Arsenic Barium !leryHium Beron Cadmiurn CaiOurn Chromium Cobail C"..opper Iron Lettd Uthil!m Magnesium mg!L mgil mgil m,>il. **!if:.~:'!** ntgil mg ! l. mgil

. rn<;ii
. **!"I",~J;l na~F.L**  mg :1 m<J!\.. mg :l

() . 5 .5 . 5 5 .5 5 . 5 .5 .5 5 .5 . 6 5 4Jj fJ? Q50 **~00** 0.50 101 0.50 1(>() 0.51 102 0.50

1 00 4.8 9:7 0.49 **S~)** 0.4(! 98 0.50 <C:1 4.9 **~e** 0.50 t'J9 1) . 49 **~H** 49 9f! o/oRee Lim•tl; -------· 8()-120 80-120 60-120 60-120 8(1-120 00.120 60-120 80-120 60-120 i!C-120 80-120 80·12(1 80-120 60-120 Dale

. 03!1612010 01
· 09 PM REPORT OF LABORATORY ANALYSIS ·rrns. roOOtt sM!f not bt'f **M.'PfOdt~ t?~**  **~·~L·'** = r•, :!. **-t~ilhoor** me written **am~** ot Pal:e **AMt)'t~~l S·J~·,.**  **«.:.** It :. Quallllet$ Page 4 of 14QUALITY CONTROL DATA Proj,,eo RAD ANO MElALS Pace PtOJEK.1 No . 3023711 **-------·--~------------------------~--** L•\BORATORY CONTHOL SAMPLE: 145?92 .Spike Parameter

**Con~** LCS Resuh LCS %Rec ·--

· -·------------- --------

· -- ---- ----- -- - - - **~v.fanganes€'.** Molybdem;m NickG! **PV1assu.,~"i1** Selenium Silver Sodium Sr . ronti!.ltn Z1nc mgil mgil **IT'iJ'~** nlg:l.

. rny;'L mg!L mg/L mgil rny!l MATRIX SPIKE & MATRIX SPIKE DUPliCATE. 145'794 Par..,.,ter

lAS 3023666007 Spike

. Units Res"lt Cone. .5 5 . 5 ;; .5 . 25 5 .5 .5 MSD. Splka Coro. 1).50 0 . . 52 0.50 4"'1 0.51 0.25 4.5 0.50 0.48 145795 MS 'Resul! w o !04 1(1() 101 101 91 100 97 MSO Resuh Pwca **~k.ot1 Servi~flS.**  (It(:. t636 F«):\ftVL"'NWn.RoO;d

· Su!le!!- 2,:J.4 Greensbti<\1 <'A 15601 ( 7;/<1/850· 5f>OO lllnilll OuaftfietS · --- ---- ·- 80-120 80-120 SG-120 8().120 80.120 80-120 80-120 eo-120 8()..120 MSO %Rec % R&!: lomi\$ RPO .AJumioom Arsenic Barium ---- m<Ji;:-- **-~**
- . **-~** ---5 ---- s.2 ·--- s.2 -- 103 -----:;(i3 -75:m --:5 ---- Beryllium Boron Cadmium Cak:iuf!l Chroroium Cobalt C'.cpper Iron Lead Uthium Magnesium Molybdeoum N1dt:al Potassium Selenium Silver Sodium **S:ronr.h.~m** Zinc mg;L NO ,5 .5 0 . 52
0 . 52 103 103 i5-125
2 mgiL 20.5 .'5 .5 0.52 0.52 100 100 75-125

3 rflgiL mgil mgiL mg!L mgil mglt. mg!L rng;l. IT!'J.'l I"'J'L "'i}'l

. mg:l. mq;L mg.t. uglL NO 6M c'l)iL NO 113000 ugll No NO SOugil 5e50 ug;l. NO NO 13400 ugil 101 **UQI~** 21 8 ugil NO 27100 uglL ND ND :rs....-.ao tl{ji1. 355 :.rg/L 11 a ug/L

' 5 : .5 .5 5 :.$ :5 · .5 5 .5 . 5 . 5 .5 .5 .5 5 .!> .25 5 5 5 .5. .5 .5 5 .5 .5 .5 5 .5 .5 5 .5 .s .5 5 . 5 .25 5 5 5 0 51 0 59 0 . 49 118 o.so 0.49 **0.~2** 105 0.50 0 . 58 **18~** O . tiO 0.55 0.50 0.51 059 0.49 118 v.so 0..49 0.52 10.5 0.50 0.58 18:\ 0.60 0 **~iS** 05{; 33 1 0 . 5:1 <)26 REPORT OF LABORATORY ANALYSIS **fr~;s** (eP\)1\ st.all t\01 be **rermx ~** 

t :,- • • ? ; :;' • .... t>'>O" .Jttt,e **T.t ~nconse**  **to! ~·**  **1-:** ..... **,~~ !~"'..:**  / rletac
· 102 106 97 103 ll!l 98 103 97 100 113 98 99 105 99 !'19 104 104 164 99 95 102. 75-125
.1 106 75-125 .3 97 '75-125 104 75-125 02 . 99 75-'125 .01 99 75-125 .2 104 75-125

. 6 96 75-125 09 100 75-125 113 75-125 91 75-125 100 75-125
2 l06 75-125
5 98 75-125 121 75-125 104 75-12!'> 09 104 75-125
5 179 75-125
4 M1 99 75-125 95 75-1?.5 ,.)6**~eAnalytical WMoW)>:Di!**  **ccm**

Pace- Astalytical SeMc.tn\, frtc. **1~$8 R~eytow~~:**  Road
- Sutes '2.3 **~** Gr;>ensbu:g. **;:>~,** ., ;ee 1 **(72<~50 5600**  QUALITY CONTROL DATA Prtlj<>CI RAD A.'IC METAlS Pace Project No
. **~023"11"!** MAmiXSP!KE SAMPLE: 145797

MS %Rec MS Resun Parameter Units

% Rec Limils Qualifte<o 3()23737002 Result Spike **Con ~**  -,.,-lu-,-n-.n-v.-,.,-- ·------ -/lllll- . L----- ----s7allgt

.. ·- ----;; **--~** ---102 ---.-75--12-5 -- - ---- Atseilic mgll

NO

5

0 . 5 i 102 75-125 Batium mgll.. 43.3ug,1.

. 5 0.54 100 75·125 Slu' 7 10um rngll

NO

. 5 0.50 101

· rs-125 eoron /l1llfL 80.7ugJL

5

0 . 60 105 75 - l25 C . ?dmium mgTL
ND .5 0.48
!l6 75-125 **--~~um** mg!L

1 31000 ugll.

5 134 72 75-125 Ml Chromium mgll

NO .5

0 49 97 75-125 Collar. mgll

NO
.5 0.49 97 7$-125 **~r** mg_Tl
52 tiJl l l .S O.S2 Hl2 7>i25 lmn "'')il 503 ug/L

5 5:4 97 75-m; Lead rngli.

NO

5 **0.~** 98 75-125 Lithium "''JIL
N(l .5 0.5"7 111 75-125 · Magnesfum mg/L 12300 ug!l

5 17:0 96 75-12!1 **~-** mgli.

16 . 1 UIJ'1.

. 5

0 51 98 75-125 Moly-num n'!JII.

NO
.5 0.5) 1'04 75-125 Nlcl<el lll!)IL

.
NO
.5 OA9 97 75-125 ' Potas&lum mg/1.. 3970 ugll

5 10.0 1:21 75-125 Si>leniurn rngll

NO

5 0.51 103 75-i25 Si1Yer R'(l!l.

Nb

. 25

0 . 26 104 75-125 ' S¢)um mgiL 110000 ug!l

5 i25 199 7S-

. i25 . $trootium mg/l 339 ug/L .5 0.83 98 7S:.i25 · z;ni: rngll
174 ogll
.5 U.64 94 75-12:; **,_~_,_-.,-,----**

**--· ---~-----**  SAMPLE OUPLIC.ATE

·. 145793 3023668007 Oup Parameter Unit$ R$Sult Result RPO .,AAnninum **~'l** . Ai'SMJc mgll Batitlm rng/l **~ium** mgil Boi'on cngll (;a(lmium 17J9!L . CalciiJm mgJL CII<Omiom mg!L Cob<lll "'9'1. Cilpper mgil. Iron mwt. Load mg.1. Lithium

mg i l MagneSIUm mg!l Manganese
"19'1. Mol'fb!lenum ffilj•\. Nicl<el m;)'i. POiassium

"19

' 1. Sele!Wm nl<j'1. **Si~~er** mgil. Dale 0-1!tiiJ2l)llJ

!l 1 : 09PM ------- NO NO NO "''0 20

. 5 UQI\.

0 . 02() NO NO il2 6 UQ11. 0.054 NO ND 113000ugil 113 NO NO NO ND 5.0 ugil tLOOSJ 5650 ug!L 5.5 NO ND NO NO ,3400 ugll

**~J. S**  101 ug;l.

(l H1 2 1 . 1;\ugil. 0(•21 NO

. 0078-J 271Co0 ug / L 2? G NO
N O NO ND REPOftf'OF LABORATORY ANALYSIS **~** ieporf *-all "lCrt !K! **p; od.x--i**  **;(l~ ):.:**  **n'** h **h~** w.10lout **dle ~-n**  **oonscnt** o f **Pao; ~**  **,~{!1\ l;.::r**  **~~! ,i;**  **i~** Qualifiers ------- 2 :z 2 3 6 3 . 09QUALITY CONTROL DATA ProJect RADAND METALS Pace Protec

l No 3023711 ·---------

- -----------··- --- SAMPLE DUP U CA'T!: '4579.1 **Par~meter Un~s**  Result Resull RPD --·- --- -- --·- ------ ---------

· ·----- ----·-- **-~--** Sodium Srronbum Zirr SI'.MPLE DUPI.ICATE

. Pararneler Aluminum Atsen.c Barium Beryllium Elo<on Cadmium yalcrurn Chromium Cobalt Copper Iron Lead Ulhiom Magnesium r.bng:mese Molybdenum Nh:;l<el Pottrsslom Selenium Silver Sodium Strontium Zinc HS;'9G mg/L mg/L mg/L Units 175000 ug/L 175

3 355 ugil

0 . 36

. 003 11 8 ug!L

. 0093,1 3023737002 Dup Result Resuil RPO ------- ----·-··--- mg!L mgll. mgiL mg/L •1'9-'L "'911. mg/l mg!L mgil mgll rng/L '"II'L mgiL rn!JI\. mg:'L mlliL mgi1. mgll mgiL. mgiL mgiL mg/l mgll 57.6uQ11.. 0056 NO NO 43.3ug/L 0Cl:f3 ND NO 601 ug/L 0.08\ NO NO 131000\1¢. 130 ND NO NO ND 5.2 ugll 00056 503 vgil 050 NO ND NO NO 12300 llg/L 122 16.1 ug/L ()016 NO 012J NO NO 3970ugll 39 NO NO NO NO l19000ugll 118 339 ugll

0 . 3-l 17-4 ugll

0 17 REPORT OF LABORATORY ANALYSIS TM **rope~** snaa t'.ot be **ropt· tJ.~,.;.**  **,;c.** c-(<:! ::- J. ! ' i 'l ""ilf';Oi'.lf **t~** wr ftf er. CO!l!:-tOI of P'3Ce **4.!-~.;."!;;t:~.l. ~i:r**  **.i!r ~**  ;""nelac,

- 4 .9 . 2 .9 6 .3 .9 3 2 1 .8 .7 Qualiflj){S Ouautiers Pac.o **A.t~tiCJ**

I SeMe-n, tru:. **1~ ~~tovm**  At;ad- SU1!es **~.;~,<4 l~i'~h4.if'Q.**  PA 1560i **(7'24}851,)·~·00**Pro1ect RAOANO **~EIALS P~**  Projoct No . 3023711 OCBatd1· QC Batch Melhoo **MPRPI34~3** EPA2W.7 lls.•ocial<lO Lab Samples: ;)023711001 METHOD BLANK. 146405 Associatea Lab Samples: 30:.!3711001 QUALITY CONTROL DATA **An~lys:is** Methcd

. · Analysis o,osoip!iOt> Matrix· VV?.tt1r **B!a~.l<** Repcrtll\g EP.\200 7 200.7 Metals, DiSSOlVed Paee Analytical Sorvk;..es, lnc. **l~38 ~~1own**  Hoad- **S~t~** 1.3:,4 Grvun&httn;, PA 111!>0 1 Parameter Unas Result lur<t Al)alyzed Qualifidrs ·----· ----------- --·---·_..:.. **~- ;;.**  **---·-** ----·-

**~** 1101\ Dissolved nlg/L
ND 0.050 Ol/08110 20:24 LABORATORY CONTROl. SAMPLE·

. 146406
%Rec Parametat Dni.ts
f_imil£ !.CS Result LCS '!'.Rile Qualifiers ·---- ----- ---- ---·-··-·

· --- - - ·---·----- **~-·** --- --·
.. -- Iron. Dissolve<! mgll MATRIX SPIKE & MATRIX SPiKE DUPLICATE: l-46406 Parameter

MS 3023791001 Spike Units Resort Cone. 5 4.6 14C-..109 MSD **Spi~e** MS Cone

. Result 92 80-120 MSD MS MSD

0 /o Rae Result %Rec %R&'- Umils RPD Qual ·----

- **~ ~**  --- -----; ---4-6 ·---u ---9-2 ---8-9-75-125------- Iron. Di<>Golved MATRIX SPIKE SAMPLE. Parameter lrM
, Dissbived SAMPLE OUPUGATE. H6407 Paramelllr !ron, Ois.solved SAMPLE. DUPUCI\T::: 1;l6410 146411 3023821007 Spike MS MS %Rec \Jnits Result Cone. Reoulf. %Rec limib> ------- mg/L 104 ug!L

5 4.5 88 75-

· 1;>;\ 3023791001 Dup Ulllts Resuli Resutl RPO auarmers mgil
NO 3023621007 [iup Res edt RPD Qualllle,; ------·-----· -·-·-·-·--··--·-··-·· ,._,_, ___ ---- mgil 1().1 ug i L REPORT OF LABORATOR
Y ANALYSIS Ttlt S r epott S l"-alt **~1** l ot' **~~~ w**  . **.u~**
, ... • • · ttrl **~r~ ..a~**  wihlut lhi **·mt CC**  **o;a ft**  <!l ¥.:.b'U

· "'',:.t.:¥' **~r.·~ i..tr5**  f r':(. nela c

.5 Qualll'l<!ts Pdljo a or 14**~Analytical" >nnJ~lb**  **.rom** Projott· Paca ProJect No RAD AND METALS 30237'1"i QUALITY CONTROL DATA _Q_C_Ba-tr.-.h-----:-M=ER=:P:-:-:11-:::72:-;:6------- Analysis Method: EPA2451 245.2 Me;cury 0.C Batch Method· EPA245

. 2 **Analysi~** De$<""Jiplion: A=ciated **L~b** Samples. 30'.23711001 METHOD BLANK 145815

t .. iat ri .x: Wate_r AssDG!aled Lab Samples. 3023711001 Bl<lnk R&ptlrting Unilll Result tim!! Anal)>l!ed Quai.ifiers Paco Aniltyttc.al **Svrvk.e._~.** Jnr. . 1QS8. **Roseyto~:~l** A:oao

. . **S.~t~s-2.3,JI Gffl!i:;'\6~11"),**  PA ."!'S€!'Y1 F:« )ll5a,seoo ------- ------ 1)19/L Parameter
**Sp1~e** Cone. NO 0.00020 03/05!10 09·54 LCS Result LCS %Rec %Rec limits Qyalifterli ---------------------- --------- Mercury MATRIX SPIKE S.'IMPLE: Parameter mgiL **14~818** Units .001 :)02370 1(JO 1 Result 0.00090 Spike Cono. 96 MS. Re$ult 85-116 MS %Rec 'o/c; **Re(.**

· limits Qualiliers --------------------------,- ------ ·----------- NO .0025 0.0025 102 Mercury mg/L --------------------- SAMPLE !JUPUGATE H5817 Pammeler Dat6. **OJ!1~:'2Gi0** 01 09 PM Units

3023701001 Rewlt Dup R-rlt RPD Quatifiars ----------------- NO NO REPORT OF LABORATORY ANAl.YSIS **n;~!: ~ec<..\11**  sni,l! **~1~** t-.:; (C;lfl:"·:1ut:oa. fUtc:t't'pl if\ t!.rl! **~!r:o;.l,** ttl!:! \'->lfn!: ti **lf~se:;:** '-'t 1-"'a;;:e A.""lafY!:tr..(jl **&:,r-;11_-:;~** hi( 75-125 **"'a~9of** 14Pru;er.L Pace **Pr.Jjet.~t** No .. RAD AND MElALS 30;!3? 11 ANALYTICAL RESULTS
Pilr.:D Analytical $ervkn

. fPC. **H~31J Ro~><M1~**  **~ ~S,JltM**  2,l.4 Gree•'ISbUrg,_ f>A 1560t **il~** 18!10-5800 Sample: 015-030210 W.'S·
Lab 10: 3023711001 SMID: COIIIlc:ted: 03t1l2f10 oo·oo **Re~-eived.** 03103!10 10:30 Ma!ri.: wa:"' Sample Typa. Parnmaters **Gms~A!pha** Gross Beta Radium-226 Ra<flum-228 MdhOd Act± **un~** tMDC) Untl& EPJ\900

. 0m -30.984 :1: 108 !200t !iC&It EPA90il.Om 15.7:1:109 f188) pC•'L EPA903

. 1 55.7:1:11.2 (0.818) ;b!L EPA SIJ4.0 5.59 t 1.35 (1.14t pCill REPORT OF LABORATORY ANALYStS • !1 =-.. **rt 1~**  **~** J)<.J **~~cr'ua**

.. •o . **C"J :c:e~**  tn !u il ... **~··v** !: !'!r - _. .... **n** Cll t" .S !i'tl!
· of **P~** Ar.; t'it:ca
l **Se-rvi<" ~.**  in!: Analyzet1 GAS No. Oual 03i04i,O 16:41 12587-46-l 03il)4t!O 16:41 12587-47-2 03iO!li10 12·SJ 13982·63-3 03!15110 09·37 15262·2Q>.i Page
1 0ot 1 4Project. P:ace P:ojet'1. Nc **QCBa c~**  RADAND METAL$ 3023711 RADC!4446 .QUALITY CONTROL DATA **Anal~s** Melhod: EPAOOO.Om CIC Batr.h **Met~od·** EPA 900 !lm Analysis Description 900

. 0 **Gr~s** AlphaiBc;a Associated Lab Samples: 30237111)(!"1 METHOD BLANK: 14!;€56 Marnx. **Wat~r A.~SOCiated**  l.eb Samples. 3023711001 Gross t,!plla Gross 8ela **Par~metef** Act± Unc (MOC) ·0.474 ± 0.386 (i .69) o.5oO ± o:;n iUSJ pCf/L pCl

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. o Radium 228 Units Analy>.JJd -------- Radium-228

0 358 **~** 0 298 (0 592) pCiil. 0311 si10 09:36 Date 03' 16!2010 01:09PM REPORT OF LABORATORY ANALYSIS l! ts :l."'1Y.::-t **s~ ll**  not be .,.prodi:ce-1. o:1l<Wpt

' ' ' : ...:1. **~"· :"!'**  **If** T l'l r. **wr~ll.en** cor.&Ylt of Pace **I''\J\3~i,.'!i~l Soi!~**  **v!c~ ':,**  l n.; **!h~t\**

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· Setviats, fnc. ;f!S3 R""'r"""" RQao- **.S<Jnesz.~.~ 9~~rg.**  PA 1560l **7:21!!-~·~0** Quaiifters Page 13 ol14Pace **Anilrytk~l** Servtce3, Inc. 1$38 RQ3e)'1own **Ro~** • **S~Kt&l** l.3.4 **(;q.~l'lSbf.:r.j.** P,.\ 15BHi QUALIFIERS ProJect RAO AND METALS Pace Project No. **30~3711** DEFINtTIONS Of- **Di!<~llon** Factor, 1f repartsd. repr8sems the factor **appi~Vd** 1<1 the repottoo data due to cilm•?.•• ;;, sample preparation, Ullutlon of the sample aliQuot; orn!<>isture <:orMnl. NO • Not Detected at or above MjusleO reportinQ fimi

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. LC."i(D)- Labomt<>ry Control Sample (Ouplicallll MStD)- Matrix Spike (Dupllc;!ie) DUP • Sample 0\!pli<:ale RPD • Relative Pertam Difference NC • Not Catwlable. Pace Analytical.is NELAP aCCIBdlle<l_. Contact your Pace PM for the cvrrenl **~st** of acaediled analyles. U • lndk.a

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· ()Q PM REPORT OF lABORATORY ANALYSIS ':' r l:f, **'~PO ~!**  ).h\Jit net 00 rop«ll:h)(:.(!.d

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Page 14 .lt 14cabot Oil and Gas Standard Well Water Testing Techniques The following sampling techniques shall be followed for obtaining grab sample for testing of the following items. Brine Water, Pit Water, Drilling Mud Frac Water, Production Water. 1. Wear disposable gloves to collect samples and discard gloves between the samples at different locations. 2. Complete
a sample label and affix it to a clean container. The containers should be glass or plastic with tight fitting sealed lids. A niinimum of one half gallon of material should be obtained for testing. 3. Samples must be collected directly into the sample container. It is not acceptable to collect the sample water for some testing parameters and then pour into a different sample container. 4. Chose a proper and safe sampling location. Pour or drip container into sample material for the listed waters above. Seal jar and properly clean outside of container. Make sure that there is no leaking of materials from container or lid. 5. Chain of custody form provides written record of custody of the time samples are collected until they have been delivered to the lab. The form is furnished by the laboratory chosen to conduct the analyses. The lab will maintain and sign off on the custody record during their custody of the samples. 6. After collection of any of these samples, they are to be delivered to or picked up by the laboratory conducting the testing as soon as possible.Jason Clark Drilling Fluid

' "' Chemicals are added to water (creating drilling fluid),

· mixed and pumped down drill pipe and carry formation cuttings up the outside of drill pipe. Formation cuttings and drilling fluid are separated at surface. Rowback Watel"'- Propant and water are mixed at surface, pumped at high pressures into formation. A portion of the fluid flows back after the frac job (creating flowback water). Jason Clark Drilling Manager cabot Oil and Gas Corp. **CMfice:3~720-5932** Mobile: **~545-6858** jason.clark@cabotog.com

1Form 26R Date: 03/18/10 Section C. Management of Residual Waste (b. -d.)- Additional Facilities Clean Harbors Environmental Services, Inc. 3 Sutton Place Edison, NJ 08817 Municipality: Edison Township Facility Contact: Shawn Barrett Phone: 908-413-3809 County: Middlesex E-mail Address: barretts@cleanharbors.com Volume of waste shipped for disposal in 2009- 10,000 gallons Sunbury Generation, LP 2384 North Old Trail Road P.O. Box517 Shamokin Dam, PA 17876 Municipality

: Shamokin Dam Facility Contact: Norm Zellers Phone: 570-884-1250 County: Snyder E-mail Address: Norm.Zellers@sunburvgen.com Volume of waste shipped for disposal in 2009- 1,285,490 gallons U S Environmental Inc (Williamsport) 409 Boot Road Downingtown, PA 19335 Municipality: Downingtown Facility Contact: Karen Zug Phone: 61Q-518-5800 E-mail Address: KZug@usenv.com County: Chester Volume of waste shipped for disposal in 2009- 3,829,800 gallons

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a NELAP recognized uccrrditing authority. Customers an l!rged to ve-rify lhl' labontory's current accreditation **~tanding.** www.dc:p.slalq>a.us
l"l't' llalc: 12.'221106

1 )Pennsytvanra Oe.partrnent of Env • ro n rrenta• Protect!on Laboratory Scope of Accretlittllioft Page 2 of 27 Attachment to Certifitate of **A~cnditotion** 0116, eJ<piratiqn d•le Oe<:emwr 31 , 2010. This li•th•g of ><<rtl11t«< 3nnlylu should w ustd only whtn **ossocl~led** with a vnlid rerlifirplt or accr.cd

. italion. State l,aboniory JD: 35-03470 IWA Lab Code: PA01354 _ Quantum **Analyti~l** & Environmetltal **Lahoratorie~** Inc. 1124 Enterprbe Street Dic:kson City, PA .1851_9_-1_5_9_3 ___ _ _ **~-----** ProKram Drinking Water Method Analyt.- l o P A 524.2 **,2·Dichlor~¢nc (o-Ui..:h!!»~ben7<'tl<ii**  HPA 524.2 **,2-l;.ichl~rodhonc** EPA 524.2

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Issue **IJat~;** 12!2112009Pennsylvan1a Department of Enwonmental Prote

. ct•on Laboratory Scope of Accreditation Page 3 Qf27 Attachment to Certificate pf Accreditatic;m ()(1(1, upintlon lUte **Dec:embe~·** 31, 2010. Th

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. sting of attrtdittd analytes sbould bt used only when associated wiU1 11 valid certificate

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• . Slate l.aboralory 10: JS-03470 EPA lAb Code: I'A01354 (570) 489-6964 Quantum Analytical & **EnYironm~ntal Laboralorie.~**  Inc. 824 EnierpM Street Dickson City, PA 18519-15!13 l'rogratn Drinking Water Method EPA 524.2 EPA 524

. 1 EPA 324.2 f,P.-'l 5241 EPA 524.l EPA 324.2 SM2121)B SM 215011 &".121)0 El SM 23409 SM 2540C SM 2550 B SMJII21l SM3113B SM3113ll SMJII3 D SM311lll SM 1500-Cr ll (10ifl.ed.) SM 3500-Mf:ll (Will f:d.) SM 4500·1:-c SM 4500-NO:l-
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. STATE PA PA PA PA PA l'l\ PA l'A P,\ PA I' A PA P ,\ PA PA PA PA PA P A PA P.'l PA PA Pi\ I' A I' A PA PA PA PA 10/19!'1001 1011912007 IO!l9il007 10119t.200J 10!19/10(17 10/19i100? **10119/~001** 10119/1007 IOII'J/l007 lfllf9J21)01 **4191200~** IWI9!10Q7 lor.w.!.009 10119/2007 Hl i 191l001 1011912007 10/19/1007 5!181200'1 10/1912007 lll/19/2007 1011912001 1011'112007 Hl/1'112001 I0/19r.2007 Ulii'IJ200 7 1011912007 **IVI/21~** 1011912007 12/1121l04 1011912007 The Penosylvaui!l Departmeat or Environmental Protection Laboratory Accreditation Program is a NELAP rttogn.ized aeereditmlauthority. Customer> are urged to verify the laboratory's current ac<:reditation standing. www.dep.state.pa.us
Issue Date
: 12122

. '2004Penrn;;ylvama Department t>f E nv;rotltl>ental Protect•on Laboratory Scope of Accreditation Page 4 of 27 **Alm~bmcnt** 1o **C~rtiflute** or **A~credillltioo** 006, expiration date l)er••nber Jl, 2010. Tbis listing of accredited a_nulytcs should he U$td only when assi;dated w.i(b o valid **tertif~eate** of accreditation. Slllte Laboratory ID: 3$-03470 EPA IA1b C!lde: Quantum Analytical & Environnu.•nbtl Laboratorks lnr. 824 Enterprise Street Diek.1on City, PA J85J9-1"593 Program Non--Potable Water Mttb!ld Analyte

· PAOI354 Ai:ec·editation Type Al.iM **D117~9JA** FIL"ri<k ---·-·---sr::..rc
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: proceduce tSI'U') STi\l"lo EI'A 160.1 Rcsiduo, filterable ('rDS) STATE liPA 160.2 Residue, ll<>!lfihtrable (fSS) STATic U'A 1603 RtstdllO, **to~al·** S'JAfE EPA 1.60.4 **Rtsi~.** volacile **~TAn:·** f.I'A 160.5 Residuo,scctleabk STA'Hi EPA 1664

. Rev A **Nc>n-pl!~** material S'f,\JT EPA 166-1 Rev A Qilondgc._ STATF EPA lbliHtevA
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STAll' EPA 100.7 Calcium
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STAIT EPA200.7
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- ' current acc,-editation standing, '11--ww.dep.s(ate.pa.us
**ls~ue** l>ale: 12;'221200'.1Pennsytvama Department of E:nv1ronmentai Protechon Laboratory Scope of Aureditatio11 Page 5 of 27 Attachment 10 Certllkate l)f Attredltation 006, upiratlon <holt l>cL"ember :JI, 2010. This listing of **a<-.:r~diled** analytes shoold be ll$"d only wh"n ass01:iated with a valid **~ertilkatr** of **nt~rcditatlon** Stnte· Liaboratuty ID: Jf'-0347{} EPA Lab (:ode: Quantum Analytieal &. f:uvlronmentallaboramries
Inc. 824 **Eoterprlse·str~t** Dickson City, PA 185

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b a N£LAP recogni:ud a«redltiDg authority. Customrrs are urged to veriJY the **laboratory'~** rurrent **act rNitation**  standiog. www.dep.state.pa.us
Issue Oatc: 12f22j100

' 1Pennsylvanta Department of **~>vtr onn"ental**  Protechon Laboratory Scope of Accreditation Page 6 of 27 Atf!ldJIQtnt to Certlnra!t of Anrrdltalion 006, upiratlon dAI• Ot«mbtr Jl. ZOIO. This listing of s«redited anal.)1ts should ho u.>red only 'vtleo ""ociated with a vtdid **c~rtilkate** of **3<cr~dlt~tiou.** F.PA l,nb Code: **I'A013~.J** (S70) 489-69(14 Quantum Analytical & Environmeutnl Laboratorks Inc. 82-' I<:nterprise Slreet Dickson City, PA **18519~1593** l'rogr3m Non-Potable wa;cr--

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Issue Dale: l2 i 2Zn!l!l•lPennsylllama Department or Envtronmental Protection Laboratory Scope of Accreditation Page

1 ot27 AUachmeot to **Certirlcat~** of A«redltarion 006, **e~piration** dnk **~c~mb«r** ;)I, :toto
, This li1ting of ;accrtdittcl analyt•s thould be uacd only when associattd wi!h a vafld certlfic:llle of arcrtdiiation. State Laboratory lD: 35-03470 t:PA Lab **Cod~:** Quantum Analytical & Envlronmenllll Ln®rl!lories **lu~.** 814 Enterprise Street Dickson Cily, PA **1851~1.,_5_9_3** __________ ----·· Pro&raro Non-Potable Water Method

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'i' I' A 10il9110(17 PA 11)!19/21))7 I' A 10il9l!007 i'A I0/1'#l(ifo7 The Penosylvania Department of Environmental Protec:tlon Laboratory Accreditation Program is a NELAP r«ognizcu accrediting aulhority. Customen are urged to verify **th~** laboratory's .:urnmt aecredllation standing. www.dep.state.pa.us
!<sue narc
: 12l2l!2tUI'lPennsylvania Department of Eov•ror1mental Protect

, on Laboratory Scope of Accreditatiolt Page 8 bf 27 AUachmenl to **Certifi~ate** of **Acct~ditation** 006, **e~piration** date U..rein ber 3 t, 2010. Tbk listing C>f llttrtdittd **anal~** Its should be used only **~'hen** associated with a vtlld tnlifkatt of attreditati;)l)

. State Laboratory ID: 35-03470 Quantum Analytical & Environmenlnl Labonllories Inc. 824 Enterprise Street I'AQI354 (570} 4119-6964 Dickson City, PA 18519-1593 Program NoU:Potiiitt.,.Water

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! 21KI1 The Penmylvania Department of Envlronmentllll.,rotection Lllbor11tory ,\ccrwilation Program

· 1s a NEL.-\1' rccogniud accrediting authority. Customers are urged to verify the **labon~lory's** currenlac:creditailon standing. **www.dep ~latr**  **pa.u~** Issue Date: 12fl?
i 2H\I"Pennsylvanta Department of Env1ronmental Protection LaboratorySc()pe of Accreditation Page 9 of 27 Attachment to Certificate o( Accreditlltion 006, uplratlon date **Oe~erubu** 31,2010. This listing ofll«redited **•nalyt~J** should b.e used only when ass<ltiated with n valid ctrtifiute
**of •(crtdit~lion.**  State Lal!or!lf.vrY ID: 35-03470 EPA Lab C11de: PA01354 (570) 489-6964 Quantum Analytical & **t:nviroum~ntal** Laboratories Inc. 824 Enterprise Street ffickson City, PA 18519-1593 "i>rovam .Ncui·Potable Water Method

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. Program l' a Nf:LAP rrcogniud acerediting autllority. Customers an urged to verify the labomlory's current llt:c!'Wilalion **~tanding.** www.dep.stale.pa.us
Issue note: **1"2 lli200<~** Pennsyl\larna Department of Envtronrrental Protechon Laboratory Scope of Accreditation Page

. 10 of 27 **Atta~hm~ut** tl! Certifkate of **,\tcndl~tion** 0116, uplrallon dale Decembn

. 31, 2011l. rhlllutlng of orrredited **•maly~~** should be
. used only when RSsoeiated wilh A valid **c~rtilkate** of nrc...,dltation. Statt **l.o~boratory** Ill: 35-03470 Efi\ Lab Code: PAOJ35.4 Quantum Analytical & F-nvirnnmenlal Laboratories Inc. S::Z<I"Entifrprise street Dkkson City, PA **-'8~5 1-:9-:-:-l:-S-,-9,_3**  ______

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bsut IJaie-: 12i22 f 2009Penll$yt'lanta Department of En·monrnental Protection Laboratory Scope of At."Creditatioll Page 16 or 27 Attatbmeo.Ho Certificate of AccrKitRiion 006, e.r.pirado11 date **Dec:~mber** 31, 1010. Tbi.'ll;.cint of attnditw IUIDiytes should b4! u5ed only **wii~A au~~eiated**  with a vlllld **rcrtilit~tle** of Slctrt<lit111iul"!. EPA l.ab Code: PA01354 **(~70)** 489-6964 Quantum Analytical & Environmental Laboratorres Inc. 824 Enterprise **Stre~t** Dickson City, PA 1"1'"1593 Provam Non-Potable Water Method Analyte Atttedltation

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) !;TAlE PJ\ 10!19/:!007 EPA 8270 Mlln STATE 1011912007 EP/\ 81.70 Potathooo, <dtyl **(l:thyll-hi<>•~** Pmmflion) s·L..,Tio Pi\ l0/1912097 The Pennsylvania DepartJDept or **iovi~IIIJU~ntal** Protection Laboratory A.ttredUatlon Program is a NELAP retognlzed **ac~rediting** authority. Customers are urged to verify the laboratory's 1:11rrrnt accreditation standing. www.dep.stale.pa.JP
**ls.•u~** l>••te: 1212212009Pennsylvania Department of **Env~ronmental** Protect1on Laboratory Scope of Accreditation Page

· **1~** of 27 . ... ttacbment to Certificate of AccreditatiOII 006, explratlo11 d»te ltectmber 31, l!lJO. This listing of liCtrt!diled AMI)'tt• **~ould** be used only Wbtn IISSodated with 1> v•lid corlillrA(e of **~ccrodllatlnn** State Laboratory ID: 35-03470 EPA
l , abCode: Quan!_um AnalyUral & Envlronmcf!lal Lnbornlories Inc. 824 Enterprise **Str~t** . Dfcksolt City. PA l81119--l593 Progralll Non-Potable Water Method Analyte PA01354 (S70) **48~·6964 Areredit~tion**  'fypt Primary Ef'rrdin

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' l)t'\ 10/1912007 The Pennsylva.Dia Departll)ent of Envinmmental Protection Laboratory A.c"redftalion Program is a NELAP rrcogoized **a~tredldng auth~;~rlty,**  Cust.,mers arr urged lo verify the laboratory's (Urrenta«reditalion **~tAnding.** www.dtp.slate.pa.us
hmr **J)al~:** 12122/21HI9PennsyiVanta Department ot l;nvtronrrentat Proteclton Laboratory Scope of Accreditation Page 17 of 27 Atht.,bment to Certificate or Acueditatlou 006, espintion date Dffn1ber 31, 1010. Tbi3 fitting of accrodited analyta sllould be tued only when **O!~Sj~inted** "·ith a vAlid ceriUlcate <!hccnditalion. State Laboratory ID: 35-03470 f.PA
l . ab Code: Quantutn Analytical & Environmencal Laboratories

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' s eurrent accreditation standing. www

. dep.state.JIIl.Ui
Issue Dllle: ll/2212009PennsyiVal'lla Department of f:nvtronrnental Protectron Laboratory Scope of Ac.•creditation Page 18 of 27 Attachment to Certirlcate or Accrt<lilation 006, expiration **dat~** Dtctmber

3 · 1, 2010. This littint of actrwit"tl analytu •hould be used only whtll •ssociatt<l with a **"~lid** certificate of actrrdil:ilion. Stille Laboratory ID; 35-03470 EPA Lob Codr: Quantum Analytical & ii:nvironrne,•lal LabnratQrics Inc. 824 Enterprue Street Dickson Cily, PA **18519-159~** Program Solid and Chemknl M11terials Method Analyte PAD1354 A<creditl!fion Type l!PA 1010 -lgnitabi"i"ii;-· ---------··-·--·-

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**ls~uc** Uatr: .12/2212009Pennsytvan•a Department of E:nv1ronmentat Protect•on Laboratory Scope of Accreditation Page

· 19 af:27 Attachment to **Certlfk~te** or **A~rrrdillttioo** 006, expintioo date DMember
J I, 2010. lbis listing uf accredited **analyt~** should br used only when U&odated witb a **v:~lid** certilirnlt of accreditation. State liaboratory ID: J>OJ470 EPA t...b Codt: Quantum Analytical & Environmental Laboratories Jne. 8l4 Entei'pm Strut Dickson City, PA 18519--1593 ·Program Solid and Cbemltal Materials t•A013S4 {570} 489-6964 ----"--·---·· M.,thlld Analyie **Accr~italiilll** l;ype Prht\Qry EII'Mtln Datf -1,-;:::1':-:
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b 11 NELAP recogniud ateteditlag authority. Customers are urged to verify the laboratory's currrnt accredltallon standing. www.dep.state.pa.us

**h~ut** llatc: 12122/2009Pennsylvania Department of Enwo'lmentat Protection Laboratc>ry Scope of Accteditation Page 20 of 27 AttachmeJII to **C~rtifKate** ot Accrcditaiion 006, u.pb·atlon d.ale Dttemm 31, 2010. This **llrtin~** of aecrediltd **4\llalyt~** should be ustd on!y wbeo **auod~ttd** J>ith a nlid ctrtiliutt or orcrediration, State Laboratory 10: 35-03479 EPA1.ab Code: PA01354 _ Quantum Analytical & Environmtntal

. Laboratorlcs.lnc. 824 Enterprise Street Diek.Soil CiCy, PA 18519-1593 T'rogram SOlid and **ChemieaH~'lalerials** Method 'iiii.Ai26o ___ _ EPA 826!1 EPAH260 EPA 81611 iii'A&260 EI'AllWI ilPA 8260 IOJ'A 8;!60 llPA 11261! f.l'AS26Q tPA&i(;iJ EPA&260 EPA 8260 I'.PA &26G i! . i'A826o I!PA 8260 iiPA ili6o !-'l'A82611. lsPA.$260 l,'Pi\8260 EPA &260 . EPAtl60 EPA82(.0, F.PAS260 **t:PA~** El't\ SUO EPA 8260 **1~.\** 8260 EPA&260 £l.PA 8260 f:PA&260 F.PA 8260 EPA8260 l'PA !260 EPA 8260 EPA8260 Allalyte **-------.s~::r,:;m.u;yib<ntt.....-·-** 13-D.:hlori>-l-pnlpM"' 1 , 3-l>ichlorobcnttne \m-Dichl0!'011cnlen<) l,.l-Dii:hiOroprop'lnt 1,1-i>ichloro.,.,nzcnc **(J>.Dichloro!wt~zco1C) 1.4-0io~**  {1,4-0ltth.Jiltncru:idc:) I .(ldoolbulanc 1-Chl(J<QIICxone I.J'ropanol {n-Pmpanol) 2 , 2-Dicbloiopropanc l-8U1>1101W (MCtb)l **ethyl~-** MHK
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I' A 10il9!1001 :>rATE PA 10/19!2001 **~TATE** Pi\ IOil'll2001 The Penmylvanla Department **ofEn~ironmental P~tectio11**  Laboratory Accreditalion Program is a JI(ELAP rccogni7.ed **a~:ereditlng** authority. Customers are urged to verify the **laboratory'~ currentaecr~ditatlon**  standing. www,!)ep.5hlle.llli.US
Issue

. Onle: 1212212009Pennsytvanta Department of f:nwo n mental Protec:t•on Laboratory Scope of Accreditation Page 21 of 27 Attllchmotto Certificate of Atcreditlltion 006, eaplration datto Otceonber 31, 2111ll. Tllis listing ofol'no=dited Allalytes ahould be used only wbl!n fllllbcllittd with a valid cntifknte of accreditation. State Laboratory ID: 35-0.3470 !i:Pt\ l..ab Code: Quantum A11aly*al & Environmental Lttboratories Inc. 824 **Enterpr~** Street Dickson City, PA 18519-1593 -P;:(;arlll!l Solid and Cheml<:al Materials Method EPA 826!1 EPA826Q F.PA &260 I!PA8260 EI'A 826{) I;PA 8260 EPA 8260 EPA 8260 l'l'A 8260 EPA 8260 (;PI\ R260 EPA8260 EI'A!liiO F.PA

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I' A P:\ PA I' A I' A . rA PA PA I' A PA I' A PA . ""' I'A Pt\ I' A P · A PI\ I' A PA PA PA PA I'A Pt\ PA PA PA PA PA rA · pi\ PA PA PA 101191200? l(l/19tl001 10t'i9ho07 IQI19/Z007 10ij9n()!l1 Hl!J9i200i l!l/1912007 !Oil il/1007 ltl/19!2007 1 . 01194007 11)119/2007 lllli9!1007 11)11912007 iOII'h2007 **1~1:91.!007** 10119:'2007 10111112007 10119!1007 10tl9iZ007 lO/I\112007 l<i/191.!007 1011912007 I 0/1912007 lili!Ciii007 111119!1001 10119/2007 11111Wl007 10!1912007 101!9;2007 10119!1007 10!19:2007 l0il9!2007 10!19i2007 10119/2007 10119/2007 The Penosylnula Department ofEnvironmenhll Protec:tfou Laboratory Accreditation Program b a NF;LAP ruognizrd actredldng aatbority. Customers arc urg.al to verily the laboratory's c11rrent accreditation tlauding. www.dcp.slate.pa.u!
IMue U:ue: 12/22!ZOO'lPennsytvanta Department of Envrro n n-ental Protect•on Laboratory Scope of Accreditation Page 22 of 27 Attachment to Ctrtlfi<ate of Accreditation 006, upiralion dot• U«ember :n, 2010.

· nus listing o( accrwite<l **aa•lyi~** should be oscil only w'hen 11ssoeisted -.itb M v•lid eerlificate of atrre<lltnllon. State Loboral4r)' ID: 35-0-3470 Quantum Anulytkal & Rnvironm\!ntal Labor;ltories Inc. 824 •;nterprise Street Dickson City, PA 18519--1593 PAOU54 - Program Solbl and Chemi\:11l Materials---- ·- -
· -

· --

· - - ----------

- - Method **An>~lytl! Ac~rcditation**  Type **fl>,\8i6il'"-·----------i elrO.:ii'i.;;:~(l>{**  **i:rei<iii¢iO<ihyi<DC)**

-

· ·· · -·---·-Sf.-\

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f I) Sl'ATF !!PA&l611
Viilyt aett>lc
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Vinyl ciilorido (t111nroedtcne)

S ' l l ll'E EPA&2611 Xyknes. wtol S'IAU: !.'PAS160

**~is-** I ,2 ·Dich!Qroc:lhcnc
STAl E I;I'AS160 ciS·1,3-Dichlo«ipropcne S'II\TE EPA 82iiO cis-1.4--l.'la:f1le<<P2-b<lll1nc STAll' EPA 8260 n•Ruiyl alcubol (n.Bui>nii!

, 1-Uutar:tOI) Sl,\T E !>PAS160

n - Outylb<:wae STATE! l!l'A 82611 n·PwpylllTJiine

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<>· Tulu1dine {2-Toluidirre

. 2·Mdhyl•uili"")

s · J,\H
: EPA 8260 s«-Butylbt.oune 'iTA!'!' I'.PA8260 ""'-Butyl nlcolool (2 · Mclhyl·21'mpnaol) <:IATf

: EPA 8260 **1\'n-no,Y~** ST-\JF EPA S1611 trans-J,2-Dicblorucitbci1< **~L'\TE** EPA 8260 ......... 1 ,3-f)icllloroproJ"'IIC

ST Ar F EPA 8260 iiuns-1,4·Dichlon>-2·butole
Sl'AT E F.I'A826o.tl:Ue.ndcd DlbiumodiJolroinetlw••

ST,\1 E EI'A8270 1,2,-I.S-T **e~ra<:tilorobeftlenc**

HA TE EPA&270 1.2-0iuit.-obaueoe ('1.2 - 0NB) SfAl'l

: F..PA 8270 1,2-Diphenylh)draz.lt>t

l>lA T L EPA &270 **I,J.~·irini!ro~**

(I , .U·fNU) STAl F EPA8270 IJ·Dinllrnbtnzent

( I,H>NB) Sl'AIE l ! PA 8210 1.4-IJin\tr®enupe

t 1.4-DNII) STAlE li.PAS210

1.4 -NIIphthoquincnc STATE f:PA8270 1.4-l'lu:nylenediamlile STATE EPA 8170 l·Acctyl·2-thinurco STATE l : I'A 8270

**I·~** 'hfllflmllphthah:m: '<TATE I!PA8270 I·Naphlltyiamine (•lplla-Napbthybnm•CJ SIATio liP A &270

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I 0119t'2007 f>A !0Mi2007 PA Hlil9!2007 I' A 10/J%lll07 PA 101t•)f!007 PA t0il9!'2007 PA Wll'1tl001 PA 1011"12007 PA I!WI911007 PA 10!19/1001 PA 1011912001 I' A 10/191!007 PA 10/191200
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' 1111111!1007 I' A I0!19!l001 I' A J0iJ9t'2iJ07 I' A 10i1W200'1 I' A ll)ll9!2flfi7 I' A IU/1911007 p,, **1011~12001** The Pennsylvania Department of
. • :nvironmental Protection l..aboratory Afcteditailon Program Is a NELAP r«ognized accrediting authority. Customers are urged to verify lbt: **laborahlry'~** current **al~reditation** standing. www.dep

. state.pa.us **ls~uc** l>atc: 1212212009Pennsytvanta Oepar1ment of Env1ronrrental Prolactton Laboratory Scope of AccreditatiOJt Page 23 of27 Attachment to Certl(ICII!e of Acrredltation 006, up i ratiiJII d11tt ln<embrr 31,.2610. Thi.•listing of ltt'('

. retlitrd •nnlytu shQUid be usrd only **wlt~n anociat~**  with " valid **ctrlili<~~te** or ntneclilaiion. State Laboratory JD: 3S-o;J470 EPA Lab Code

: J>AOJ354 (570) 4!19-6%4 Quantum Analytical & Environmental **Laboral~>ries** Inc. 824 En.lerprise Stree

· r

- l>ieks.on CUy, PA

. 18519-1593 Program -Solid and Cbemkal Materials 1\'fetbod Analyte A«rrclitl!tion l")•pe Primar y t : rfcctive Date El'A 82 ? 0 **------- 2A.~·Tri**  **h!orop!1cool**

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STA I'E PA tli l l'l-'!!))7 F.PA827U

2.4 - Dim<thylphcnol
STAT J; PA 10119 1 1007 lf.I'A8270 2,4-Dinitn.>phcnol

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I' A 1011912007 EPA 8270 **2,6-l)ic;fllnfor~K>l** STAn; PA 1(1!19/1007 f:PA 8270 l.I>-Diilitrotol111:11e (7,6-DNf) S'I.'\TE l'A 1011<1.'2007 FJ'A8270 **~-.-\c¢ylllllli~-**
STAll

; l'A 1()119

! 10!17 liPA8270 2·Ami110111111uajuinoue S'fJ\Tii

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2 - Methyl-4,6-<li.JiiUQ!lbencil STI\Tli PA

1 \)i iU/200'1 (4.6-0inicn>-2-<11t111Yfpltmol)

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1 0' 1? 1 100! Jo::PI\ 11170 !-Nl!ph\hylamim: (l)cla-'Nophthtlamiu<) SlATF.

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StA T E PA IWI9!2007 EI'A$l70 2-Nitrop!l<m\ll. SlATf,

I' A 1011'1•'2007 llPA8270

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I' A trJI9

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l ()i iQ · 200 i EI'A8270 J-Methyloftri\an!h!<IJ!' SI'A!'E

I' A W!l9!l0{}7 l.ll'A 8270 J·M<il>ylpl)enol **{!li'C:Ie!ll~)** STMF PI\ Hl: f0 'l 007 EPA 8270 J-Nilroonili""

· ST/\11' PA 11) 1 !9 • 21)() ) EPA8270

4,4 '-. r..1ell!)'lcnebia(.khl""""'ilin<) Sl'ATf. PI\ **007** H•A8270 **~.4'-Mc\hykodliS{N** N-dimtlhylaniline) STi\TE f>A

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I **,3'-phell}'lenediamit~t** STATE PA lt}!lU!J.OO'J EPA8170 4·Ch1Qfo>-J-mclhylph<mol S'fATI:

' PA **1!1'19!;!~17** EPA8270 4·1..'111oroanilinc s·r.ur; **I~A 10il~>i2007**  llPI\8270 4·('hloroplomyl

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<I · M<:IhylpheDOI (p.('R$01) STAlli FA Jll!l9:l(J!)j The Pennsylvania l>eparlment or Eavlronmentai

· ProteeCioa Laboratory Accrooltatlon .Pmgrilm b a NELAP r«ogniud aecrediliog authOTity. Customers are urged to verify tbe laboratory's current a«:ndllatlon standing. **www.dep.stalc.pa.u~**
**lssu~** ()lite 12!22 f 2f!i)<JPennsytvama **D~partment** of Enwonrrenlal Protect•on Laboratory Scope of Accreditation Page 24 or27 AUatlltllfllt to Certirtute of **Accr~i tfttlop**  00(;, nplntion date ll<e<mbn 31, 1010. Tblt listing of **actt~itod** analyt•• should be used only when Assodatod with R valid certHic2te ofDccnditation

. Stnte l..almmtory ID: .35--63470 F:l'A Lllb Code: I'A01354 (570) 489-6964 Quantum **.4,11alyti_~;al** & Environmental **l..allori!fQ.rj~** Inc. 824 Enterprise Street ..,:J>.::..ic::.:k.s=:

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STAll

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I' A 1011'1!2007 EPAS270 llcf:nilline
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I' I\ 10!1912007 EPAS21Q lli:nro(a)py"'nc STATE PA 1011912007 EI 1 All270 **lkn1,0(b1f}~**
STAT!':

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!>TAl f. PA IIJ/19!1007 llPA 827() Ocnzoic add. S:TATf. PA 10/19 1 2007 F..PA 8270 lkneyt lllcobQI STATE p,\ 10/l<r-100 7 EPA&270
Butyl btnzyl **phlbola~t:** (lknl}l **u~ ·l**  vh t holafc
) STATE

I' A 10!19!20117 EPA S271l Carbazole
!HAT F. PA lfliiW2007 EPA 82i0 Ou:yscnc **{lktrlo(ajphcnonlh~nc)** STATE PA Hlfl9!l007 EPA 817!1 Ut-n-bulyl phlballfte STArt PA IQ /1 '1!2007 EPA tl70 Ol·noQctyl phlhalolc STATE

.. ,, **l!l!l9/1l~l7** EI'AII270 **(>ibc&[a,i~** STATi: PA 10/1912007 F.PAS2.70 Oibemofa,ejpytenC STATE PA 10!19!1011'! FJ'A 8270 Dibcli7Al{'ll,h.lon!llrao<D< **~'TATE** p,,

l 0 fJUl2007 EPA 827!1 lld>ent.olilr111 STArE l'A 101J9jl007 EPAS171} IJiclhyl phlhaJale

· stAT!! PA hJ/

! 9:'2007 l'P , \ &270 **Di<!hyli<~lf*** STATE PA Hl/i911007 EPAS170 IJiclhylslitbeslrol STATE Pi\ Jll!l9:2!)1

) 7 EPA 11270 **l>ihyd~·tr~k** STAH< PA 1011912007 The Pennsylvania Department of Environmental Protedlon Laboratory Accre(Jitatlon Program Is a NELI\P rtcogni7.ed accrediting authority. Customers are urged to nrify the laborntory's current uc:rtditlition 'fllnding. **www.dtp.,latc.pa.u**
hsue Date
: 12112 / 2009PennsylvaniaDepartmentofProtectionLaboratoryScopeofAccreditationPage25of2'1Attachmentt1lCertincateofAccreditation00<1,aplralklo31,2UUl.Thisn.tinganalytushouldbeusedonlywht'nassoeiatedwith11validcortifKaleofStateLaboratoryJD:35-03470QuantumAnalytical&EnvlronqientalLaboratoriesIa•··814EnterpriseStreelDicksonCity,PA18Sl9-"1593ProgramSolidandChemicalMaterialsMdbod.E.I'A8270HPA82'/0EPA8270EPA8270llPAii270EPA8270EPA8270EPA8210EPA8270m•AS270F.PA8270El'Aimo11I'A827ilEPA8270EPA8270I!PA8270El'/\8270lii>A8270El'i\8'21(1EPA82708270F.PA8270EPA8'110EPAF.PA82701:.1'1\8270EPA8270El'/\11'170EPA8270fJ>i\8270El'A8270EPA8170El'A8270f.l'A8270I!P/\8270AnRlyte·nitncii;Yirl."ihal:uc(4-Dimelhylumin<>al.obcnlCIIC)DiphenyhunincE!hylcarbamtl(e(UrtthW1t)f.tbylrnclhancsulfun•wFluuf1lrll})encfioorcnell•><adllorub<nzen•flexnehlorocyclopentadicneHcxacltk>nliJNI'CTICfll"'roquinoru:lnlknu(lsopll<mmcMalercanhydrideMesttOJ!tltMttllllpyrikntMtlh)'lmctlrBt"'sutronateN-Nitm:..,di·n'1"opylatnmcN-Nilt<>Sodiethylarninc:N-Nitros<•dunc1hylam""'N·NiiJosodipheny\amineN-Nitr<>S<liJIL'Ih)i<'lhylamiru:N-Nitr<noplperidineN-Niln»opyrroliJincNicotineNitroquinolinc-1-<Jltide.PcnlacblotonitJoben:u:ro:tPCNB)l'cnt..:hk•roph.:rwl(PCP)Phenai:CtinPhenanthrenePhcnobarbi&alPhenolPAOI354(570)489-6964PrlmoryDnteSTAiii"·-------PA_____io/iiifi007'-·S'IATEPAlil!J9!2ll071\1:\'l'i!$'1'1\TI'Sft\TF.STAff.SfATES!Arf:stAtliSTA'rt:STAl'FSTATr·STNW.8fA111STAfFS'!Al'loS1J\TI:!STI\Tf:SIAfl:sr,wtSTATi'.S'IATESTMF!\lATESTATESTATESTATEST/\1'1;STATESTATEHAT!:Sl"Al'ESTAll:STATESTi\Tt:I'APAI'AI'APAl'APAPAPAI'AI'AI'APAI'APAI'APAPAPAPAp,\VAPAI'APA-PAPi\J',\PAPAPA"''I'AIOIIW2ml7IIJ/JI),'2f,07\01191200710/tWZ0071011W2007h)l!<)!2007lili19i20U7I<I!IWZ!IQ'!l1Ji1W21JQ7IOIIW!007H)fl9!2007IO.t91200?I0/Itlf2007IO!I'i!l.r.m10;19:.!0(}7Wtft:if2U07H!!l9,2tlf}7lO/)>J'/"lOH?!WI9.'!00i11)!10/2001lfl!l9-'l007!Oii<J,!O{)'Ifd(l9/200110!1911001II)!)9!]flO']ThePennsylvaniaDepartmentofEnvironmentalProtectionLaboratoryAc¢redllatlonProgram1$aNEL.APr«<gnizedacereditiogauthority.Cu5tomersareurgedtoverifytbelaburatory'srun·eutaccreditationilandlng.www.dcp.state.pa.usIssueJ)at<':12.'22:200'1Pennsy"'arua Department of f:.nwonmenlal **Prot~ctton** Laboratory Scope of Accreditation Page 26 of 2-7 Attachment to Certificate of **Attr~ditatloa** 000. expiratiof! date **lluemb~r** 31,21116. This **lt~Hng** of **n~crrdlt~d** analyt•• should be und only when **as1ociat~** with a valid rulificnt" of **a~creditation.** State Laboratory 10: 35-03470
EP i\ l.ab Code

: I'A01354 (570) 489-696<1 Quantum Analytical & **Environm~ntlll** La.ooratories Inc. 824 :ti:nrerprise Stree

. l l)ick.son City, PA 185l9-l593 . Program sOlid ancrchemicafMateriats Mdhod Anelyte **c~~itntion** Type **l~rllll~ry** t:n'tctivt Datt EPA 8210 ry,.,,. ---------

- STA fii - --- ·- -;p-;\ --- --i071912cl01 EI'A 32711 ReforoinoJ
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· Sufruic
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I' A

I 0!19!2001 Hl>A 8270 ·Thioplu:nol tBerm:,.,Unol) S'fAIIl

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I' A !Oi!9!2007 EPA8270 bil{2-Chlorois6propy1) ether 'STilT£ PA 10!19!1001 EP,\ 8270 bi$(2-EthYtlmyl) plllhalat<: {OI!fiP) **STAT!~**

I' A 10/1912007 lii'A8270 l>i<:ldorovos

: (I>OVP. Oidllom>.,) STATE PA 10!19!2007 F.!' A 8270 Oinoscb (2 · tc<-DUI)'I-4

, 6-diniuopheool. DNill') STAt!:

I' A 10fl912c)07 EPA 1270 Anihwnc SlATE l'A 10119120117 F.I'A 8210 Co(llatOi

STA

: m
I' A 10119!2007 l i PAII270 Chlorohen'zi16te STATE }'A 101l9!200i EPA 8210 lsodrin S'i'Al'E

I) A 10119!:!007 EPA8270 K\!llCJtiG l>'TAl:E l'A lli/19i200i EPA 8210 Mirex STAlE

. p,, 10!1912007 EP,\ 8270 Tri!lutalin **!T~ellAAl** STA'fll !'A l01!9'200i J:PA 8270 l.'l,•l-Tricb!OfDbewt:riC lHA'H; PI\ 10/1912007 **~:rAsno 1,2-l>i•'ld<I~(Q**  **I>i<:hl""~nc:)** 5rATE

I' A IIJ11912007 fJ>A 8270 **1.3-0ichloro)lr:lurene.{m-Diclolomb<n t~ll'!l**  !itir{E

1 1 1\ 10il911(107 EPA 8211l **4-Dlchk•~** (p-l>icllk'fllbenll!"") STAT!; PA 1<1 1 1912007 EP/\8210 2-Piooline **(2-~XIhylpyridine)** STATE

. PA 1(1!19/1((17 EPA 82i0 HeQclllombutl!dicnc

( I.J

· HtJ<ar:htM > htrtadituc) STATE

1' - \ Wl9i'l001 l'.l'A8!10 **~lc:otadllurodhanc** STATE
M lb'f9 / 2007 EP/\8270 N-Ni!r.....,di-n-')lurylaminc

. STATio PA IQ!I0/2007 El'A 8270 Nophthaknc SlATE I'A 1!1!19121107 EPA 82'10 Nitrobenzene SlWI'E P,\ 10119!2c)07 EI'A 3270 Pyridine SJ'i\TE

I' A !IJrJW.lOOi EPA H270 **~Toluidine** (2¥Toluidinc 2·MctiJ)

· Iunlh!lt") STATE )';\ **l~:i1'si2()()1** EPA '1038 Sulfore STAlli PA 10<19/1007 EPA 91160
Total o<i!anic carbon

i fiX

' ) STATE Jlf\ !l)!l912ll07 EPA 9070

Oil and grease STATE PA **~/2008** f! . PA 9071 **Ollqndl!lt~** STAll: PA **~5!.!008** The Pennsylvania Department of Environmental Protec:tloo **IAiborntor~** Accreditallon P.rograll) is a NI\LAP rtcognized acrrtdiling autllorily, Custolllt'rs are urged to vrriry lhe laboratory's current **ac;cred~stion** 'landing

, www.dep.stale.pa.us
lsw.- Oatr. 12 i 12i2009Laboratory Scope of Accretlitation Page 27 of 27 Attachmenllo Certificate or A<.-neditation 006, expiration dale **Det~mbcr**

J - 1,20111. Thisli5fing of **attr~dited ~n~lyte~**  "bould be lf!.,d only when AS50tboted witb a **vt~lid** certificate **ohc~reditatlon.** SlAte Laboratory ID: JS-03410 EPA Lub Code: Quantum Analytic:al & Environmeutal l.aboratorif.1 tile. 824 **E11lerpr~e** Street Dkkson City, PA 18519-1593 PA013S4 (570) 489-6964 ProgTam Solid and Chemical Materla""7ls---------------

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# COM· MONWEALTIIOFPENNSYLVANIA 

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Issue Onie: 05!27/2009

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Issue Date: 0212612010

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