# MEMORANDUM

TO: Jim Eddinger, U.S. Environmental Protection Agency, OAQPS

FROM: Eastern Research Group, Inc.

DATE: May 2012

SUBJECT: Revised (May 2012) Analysis of Minimum Detection Levels from Industrial,

Commercial, and Institutional Boilers and Process Heaters National Emission

Standards for Hazardous Air Pollutants

‐ Major Source

1.0 INTRODUCTION

The purpose of this memorandum is to discuss the methodology used to compute a

value equal to three times the representative method detection limit (3x RDL) and how these

3x RDL values were used to establish emission standards for boilers and process heaters at

major sources of hazardous air pollutants (HAP). This memorandum focuses only on the

changes to the 3x RDL analyses that were conducted for the December 23, 2011 proposed

reconsideration of the rule (76 FR 80598). The methods used to develop 3x RDL values for the

proposed rule are provided in another memorandum. 1 

# For this revised analysis, 3x RDL values

were estimated for mercury (Hg), hydrogen chloride (HCl), filterable particulate matter (PM),

and the sum of eight metallic hazardous air pollutants (TSM8).

This memorandum is organized as follows:

1.0 Introduction

2.0 3x RDL for Mercury, Hydrogen Chloride, and Filterable Particulate Matter

3.0 3x RDL for Metallic HAP

4.0 3x RDL for Carbon Monoxide

5.0 References

Appendix A: Calculation of 3x RDL for Mercury

# Appendix B: Calculation of 3x RDL for Hydrogen Chloride

Appendix C: Calculation of 3x RDL for Filterable Particulate Matter

Appendix D: Calculation of 3x RDL for Metallic HAP

# 2.0 3x RDL FOR MERCURY, HYDROGEN CHLORIDE, AND FILTERABLE PARTICULATE MATTER

The 3x RDL analyses conducted for mercury (Hg), hydrogen chloride (HCl), and filterable

particulate matter (PM) were conducted using the same methodology used in the previous

analysis. 1 

# However, since the list of top performers for each pollutant changed, the resultant 3x

RDL values for each pollutant also changed slightly in some cases. Summaries of the 3x RDL

calculation for Hg, HCl, and PM are provided in Appendices A, B, and C, respectively.

3.0 3x RDL FOR METALLIC HAP

The methodology used to calculate the 3x RDL values for the sum of eight metallic

hazardous air pollutants (HAP) (TSM8) has changed since the previous analysis. An RDL was

developed by EPA for each of the eight individual metals that comprise TSM8 (arsenic,

beryllium, cadmium, chromium, lead, manganese, nickel, and selenium). 2 

# This analysis

developed a separate RDL for each metal based on the laboratory instrument used to analyze

the Method 29 samples. One set of RDL values was generated for the use of inductively

coupled plasma/atomic emission spectrometry (ICP/AES) or atomic absorption (AA), whereas

an alternative set of RDL values was developed for the use of inductively coupled plasma/mass

spectrometry (ICP/MS) or graphite furnace atomic absorption (GFAA). This is similar to how

separate RDL values were generated for methods 26 and 26A for HCl.

EPA conducted a review of top performer test reports for consistency in TSM8

reporting. The results of this test report review are provided in another memorandum. 3 

# The

reported sample catch, in micrograms ( μ g), was extracted for each test run by EPA, along with

other test

‐ specific parameters such as sample time, sample volume, and stack oxygen

concentration. This review also included identifying what laboratory analysis was used to

analyze the method 29 samples for each metal. Some laboratories used a mixture of laboratory

instruments to analyze all eight metals. For example, one laboratory tended to use ICP/MS to

analyze samples for cadmium (Cd) and ICP/AES for the remaining seven metals.

The actual reported sample volume for each metal was calculated using the reported

sample catch and sample volume, as shown in Equation 1 below.

# ܥ ௘௠௧௔௟ 

# ൌ ௠ ೘೐೟ೌ೗



# ௏ ೞ೟೏ 

# (Equation 1)

Where:

C

metal 

# = Concentration, micrograms per cubic meter at dry standard conditions ( μ g/dscm)

m metal 

# = Reported sample catch for the metal, μ g

V

std 

# = Reported sample volume, cubic meter at dry standard conditions (dscm)



# The actual concentration for the metal was compared to the corresponding RDL

concentration for the respective laboratory instrument used and for the respective sampling

time developed by EPA. 2 

# If the reported concentration was less than the RDL concentration

developed by EPA, the reported concentration was corrected upwards to the RDL

concentration. This comparison was done for all eight metals for each top performer test run,

where test report data were available. After the comparison was done for all eight metals,

each of the eight values was summed in order to get the TSM8 3x RDL value for the test run.

The 3x RDL value for each subcategory was based on the minimum TSM8 3x RDL test

run value calculated using the aforementioned steps. The 3x RDL concentrations were

converted to emission rates, in units of pounds per million British thermal unit of heat input

(lb/MMBtu), using Equation 2 below.

ܧ ଷ௫ ோ஽௅ 

# ൌ ܥ ଷ௫ ோ஽௅ 

# ቀ ଵ

ଷହ.ଷଵହ 

# ቁ ቀ ଵ

ସହଷ,ହଽ଴,଴଴଴ 

# ቁ ሺ ܨ ஽ 

# ሻ ቀ ଶ଴.ଽସ଺

ଶ଴.ଽସ଺ିை మ 

# ቁ (Equation 2)

Where:

E

3x RDL 

# = TSM8 3x RDL emission rate, lb/MMBtu

C

3x RDL 

# = TSM8 3x RDL concentration, μ g/dscm

35.315 = Conversion factor, cubic meters to cubic feet

453,590,000 = Conversion factor, micrograms to pounds

F

D 

# = Fuel

‐ specific factor from Method 19, cubic foot at dry standard conditions per MMBtu (dscf/MMBtu)

20.946 = Approximate amount of oxygen in ambient air, percentage (%)

O 2 

# = Average oxygen concentration from test report review for the subcategory, %



# 4.0 3x RDL FOR CARBON MONOXIDE

The methods used to calculate 3x RDL values for carbon monoxide (CO) are provided in

another memorandum. 4 

# This additional memorandum provides the actual 3x RDL values that

were used to compare to the 99% UPL calculated for the regulated subcategories. The CO 3x

RDL only applies where the calculated 99% UPL, when rounded to the nearest whole number, is

# less than 5 parts per million (ppm). Only one subcategory for new sources (units designed to

burn light liquid fuels) qualified for the 3x RDL for CO.

# 5.0 REFERENCES

1. Eastern Research Group, Inc. Analysis of Dioxin/Furan Data and Minimum Detection

Levels from Industrial, Commercial, and Institutional Boilers and Process Heaters

National Emission Standards for Hazardous Air Pollutants

– Major Source. November

2011.

2. Westlin, Peter, U.S. EPA SPPD, MTG, & Ray Merrill, U.S. EPA AQAD, MTG. Data and

Procedure for Handling Below Detection Level Data in Analyzing Various Pollutant

Emissions Databases for MACT and RTR Emissions Limits. December, 2011.

3. Eastern Research Group, Inc. Revised (May 2012) Summary of Test Report Data Review

from Best Performing Units at Industrial, Commercial, and Institutional Boilers and

Process Heaters National Emission Standards for Hazardous Air Pollutants

‐ Major

Source. May 2012.

4. Westlin, Peter. U.S. EPA OAQPS/SPPD. Measurement Detection Capabilities for EPA for

Instrumental Test Methods. April 10, 2012.

# Appendix A

Calculation of 3x RDL for Mercury

### Appendix A-1: Sample Times and Oxygen Percentages Used to Estimate Hg 3x RDL

Facility ID Combusor ID Fuel Category Test ID Sample

Volume (dscf) Sample

Volume

(dscm) Sample

Time (min) Sample

Time (hrs) Stack Oxygen

Concentration

(%) Use in

New

Source 3x

RDL?

AKDoyonUtilities_AK #4 Solid Sample #1 60.192 1.70 60 1.00 7

AKDoyonUtilities_AK #4 Solid Sample #2 61.418 1.74 60 1.00 6.67

AKDoyonUtilities_AK #4 Solid Sample #3 59.13 1.67 60 1.00 6

GAGPSRMRiincon EU 002 Solid Sample #1 60.459 1.71 120 2.00

GAGPSRMRiincon EU 002 Solid Sample #2 50.327 1.43 120 2.00

GAGPSRMRiincon EU 002 Solid Sample #1 52.468 1.49 120 2.00

GAGPSRMRiincon EU 002 Solid Sample #2 52.281 1.48 120 2.00

IDAmalgamatedSugarCoTwinFalls SB-1 Solid Sample #1 78.341 2.22 120 2.00 6.9

IDAmalgamatedSugarCoTwinFalls SB-1 Solid Sample #2 80.205 2.27 120 2.00 6.9

IDAmalgamatedSugarCoTwinFalls SB-1 Solid Sample #3 77.571 2.20 120 2.00 6

MITBSimonPowerPlant Unit 1 Solid Sample #1 78.628 2.23 120 2.00

MITBSimonPowerPlant Unit 1 Solid Sample #2 76.747 2.17 120 2.00

MITBSimonPowerPlant Unit 1 Solid Sample #3 74.277 2.10 120 2.00

ALIPCourtland No. 3 Combination Boier / 11CU301 Solid Sample #1 127 3.60 240 4.00

ALIPCourtland No. 3 Combination Boier / 11CU301 Solid Sample #2 125 3.54 240 4.00

ALIPCourtland No. 3 Combination Boier / 11CU301 Solid Sample #3 119 3.37 240 4.00

GASPNewsprint PB2 Solid Sample #1 163 4.62 240 4.00

GASPNewsprint PB2 Solid Sample #2 139 3.94 240 4.00

GASPNewsprint PB2 Solid Sample #3 139 3.94 240 4.00

IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #1 165.27 4.68 240 4.00 7

IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #2 169.796 4.81 240 4.00 6.8

IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #3 166.058 4.70 240 4.00 6.9

IAMonsantoMuscatine Boiler #8 (EP-195) Solid 8.3

IAMonsantoMuscatine Boiler #8 (EP-195) Solid 8.1

IAMonsantoMuscatine Boiler #8 (EP-195) Solid 8.3

IAMonsantoMuscatine Boiler #8 (EP-195) Solid 9.3

IAMonsantoMuscatine Boiler #8 (EP-195) Solid 9

IAMonsantoMuscatine Boiler #8 (EP-195) Solid 9

IAMonsantoMuscatine Boiler #8 (EP-195) Solid 8.3

IAMonsantoMuscatine Boiler #8 (EP-195) Solid 7.9

IAMonsantoMuscatine Boiler #8 (EP-195) Solid 8.3

IARoquetteAmerica Circulating Fluidized Bed Boiler (121) Solid Sample #1 150.658 4.27 192 3.20

IARoquetteAmerica Circulating Fluidized Bed Boiler (121) Solid Sample #2 151.674 4.29 192 3.20

IARoquetteAmerica Circulating Fluidized Bed Boiler (121) Solid Sample #3 148.593 4.21 192 3.20

ILPolyOne B1 Solid Sample #1 172.203 4.88 240 4.00 8.4

ILPolyOne B1 Solid Sample #2 164.574 4.66 240 4.00 8.1

ILPolyOne B1 Solid Sample #3 165.647 4.69 240 4.00 8.3

MITBSimonPowerPlant Unit 1 Solid Sample #1 178.791 5.06 240 4.00

MITBSimonPowerPlant Unit 1 Solid Sample #2 198.23 5.61 240 4.00

MITBSimonPowerPlant Unit 1 Solid Sample #3 196.014 5.55 240 4.00

NCDomtar 65-25-0310 (No. 2 Hog Fuel Boiler) Solid Sample #1 161.884 4.58 240 4.00

NCDomtar 65-25-0310 (No. 2 Hog Fuel Boiler) Solid Sample #2 166.996 4.73 240 4.00

NCDomtar 65-25-0310 (No. 2 Hog Fuel Boiler) Solid Sample #3 157.615 4.46 240 4.00

NCTysonHarmony TYS-ES-21 Solid Sample #1 77.941 2.21 120 2.00

NCTysonHarmony TYS-ES-21 Solid Sample #2 74.864 2.12 120 2.00

NCTysonHarmony TYS-ES-21 Solid Sample #3 82.735 2.34 120 2.00

NJVinelandMuniElectric-HowardDown Unit 9 Liquid Sample #1 147.289 4.17 240 4.00 4.76

NJVinelandMuniElectric-HowardDown Unit 9 Liquid Sample #2 149.988 4.25 240 4.00 4.95

NJVinelandMuniElectric-HowardDown Unit 9 Liquid Sample #3 147.912 4.19 240 4.00 5.01

PABoeingRidleyPark 033 Liquid Sample #1 150.708 4.27 240 4.00 5.4

PABoeingRidleyPark 033 Liquid Sample #2 139.304 3.94 240 4.00 5.5

PABoeingRidleyPark 033 Liquid Sample #3 132.854 3.76 240 4.00 6.8

SCBowaterCoatedPaper Combination Boiler No. 2 Solid Sample #3 177.254 5.02 240 4.00

SCBowaterCoatedPaper Combination Boiler No. 2 Solid Sample #1 52.934 1.50 96 1.60

SCBowaterCoatedPaper Combination Boiler No. 2 Solid Sample #2 53.144 1.50 96 1.60

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #1 41.8825 1.19 60 1.00

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #2 40.4945 1.15 60 1.00

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #3 38.888 1.10 60 1.00

TNNissanSmyrna Boiler 2 Solid Sample #1 40.79 1.16 60 1.00

TNNissanSmyrna Boiler 2 Solid Sample #2 44.133 1.25 60 1.00

TNNissanSmyrna Boiler 2 Solid Sample #3 42.609 1.21 60 1.00

TNNissanSmyrna Boiler 3 Solid Sample #1 43.078 1.22 60 1.00

TNNissanSmyrna Boiler 3 Solid Sample #2 44.819 1.27 60 1.00

TNNissanSmyrna Boiler 3 Solid Sample #3 43.161 1.22 60 1.00

VADukeEnergyNarrows Boiler #2 Solid Sample #1 42.371 1.20 60 1.00 14.1

VADukeEnergyNarrows Boiler #2 Solid Sample #2 32.941 0.93 60 1.00 12.53

VADukeEnergyNarrows Boiler #2 Solid Sample #3 41.279 1.17 60 1.00 13.03

VADukeEnergyNarrows Boiler #7 Solid Sample #1 46.005 1.30 60 1.00

VADukeEnergyNarrows Boiler #7 Solid Sample #2 37.101 1.05 60 1.00

VADukeEnergyNarrows Boiler #7 Solid Sample #3 47.861 1.36 60 1.00

VAUniversityofVirginia 7103-1-01R Solid Sample #1 176.38 4.99 240 4.00

VAUniversityofVirginia 7103-1-01R Solid Sample #2 169.546 4.80 240 4.00

VAUniversityofVirginia 7103-1-01R Solid Sample #3 177.945 5.04 240 4.00

GATempleInlandRome WF Solid Sample #1 141.451 4.01 240 4.00

GATempleInlandRome WF Solid Sample #2 148.796 4.21 240 4.00

GATempleInlandRome WF Solid Sample #3 153.993 4.36 240 4.00

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #1 218.31 6.18 240 4.00 5.58

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #2 214.84 6.08 240 4.00 5.56

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #3 217.37 6.16 240 4.00 5.66

Page 1 of 3

### Appendix A-1: Sample Times and Oxygen Percentages Used to Estimate Hg 3x RDL

Facility ID Combusor ID Fuel Category Test ID Sample

Volume (dscf) Sample

Volume

(dscm) Sample

Time (min) Sample

Time (hrs) Stack Oxygen

Concentration

(%) Use in

New

Source 3x

RDL?

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid 6.9

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid 7.9

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid 7.9

MNGPDuluth EU33 Boiler #3 Liquid Sample #1 15.87 0.45 180 3.00 4

MNGPDuluth EU33 Boiler #3 Liquid Sample #2 148.38 4.20 180 3.00 4.2

MNGPDuluth EU33 Boiler #3 Liquid Sample #3 144.35 4.09 180 3.00 4.6

SCCogenSouth B001 - Main Boiler Solid Sample #1 91.6 2.59 120 2.00

SCCogenSouth B001 - Main Boiler Solid Sample #2 93.38 2.64 120 2.00

SCCogenSouth B001 - Main Boiler Solid Sample #3 87.44 2.48 120 2.00

SCCogenSouth B001 - Main Boiler Solid Sample #1 76.74 2.17 120 2.00

SCCogenSouth B001 - Main Boiler Solid Sample #2 78.3 2.22 120 2.00

SCCogenSouth B001 - Main Boiler Solid Sample #3 76.47 2.17 120 2.00

SCCogenSouth B001 - Main Boiler Solid Sample #1 108.73 3.08 120 2.00

SCCogenSouth B001 - Main Boiler Solid Sample #2 107.32 3.04 120 2.00

SCCogenSouth B001 - Main Boiler Solid Sample #3 106.37 3.01 120 2.00

SCCogenSouth B001 - Main Boiler Solid Sample #1 155.04 4.39 240 4.00

SCCogenSouth B001 - Main Boiler Solid Sample #2 154.94 4.39 240 4.00

SCCogenSouth B001 - Main Boiler Solid Sample #3 158.45 4.49 240 4.00

WVMountainStateCarbonFollansbee S1 Process Gas Sample #1 163.271 4.62 240 4.00 4.5 YES

WVMountainStateCarbonFollansbee S1 Process Gas Sample #2 124.385 3.52 240 4.00 4.7 YES

WVMountainStateCarbonFollansbee S1 Process Gas Sample #3 143.477 4.06 240 4.00 4.8 YES

NCDomtar 65-25-0310 (No. 2 Hog Fuel Boiler) Solid Sample #1 74.893 2.12 120 2.00

NCDomtar 65-25-0310 (No. 2 Hog Fuel Boiler) Solid Sample #2 78.324 2.22 120 2.00

NCDomtar 65-25-0310 (No. 2 Hog Fuel Boiler) Solid Sample #3 77.557 2.20 120 2.00

TNCargillMemphis Stoker Boiler 8001 Solid Sample #1 169.383 4.80 240 4.00 10.84

TNCargillMemphis Stoker Boiler 8001 Solid Sample #2 172.476 4.88 240 4.00 10.31

TNCargillMemphis Stoker Boiler 8001 Solid Sample #3 158.663 4.49 240 4.00 10.25

TNCargillMemphis Stoker Boiler 8001 Solid 12.4

TNCargillMemphis Stoker Boiler 8001 Solid 12.2

TNCargillMemphis Stoker Boiler 8001 Solid 11.9

VADukeEnergyNarrows Boiler #1 Solid Sample #1 37.837 1.07 60 1.00

VADukeEnergyNarrows Boiler #1 Solid Sample #3 38.994 1.10 60 1.00

VADukeEnergyNarrows Boiler #1 Solid Sample #4 38.585 1.09 60 1.00

VADukeEnergyNarrows Boiler #1 Solid Sample #1 54.38 1.54 60 1.00

VADukeEnergyNarrows Boiler #1 Solid Sample #2 51.201 1.45 60 1.00

VADukeEnergyNarrows Boiler #1 Solid Sample #3 55.212 1.56 60 1.00

VADukeEnergyNarrows Boiler #7 Solid Sample #1 59.38 1.68 60 1.00

VADukeEnergyNarrows Boiler #7 Solid Sample #2 41.135 1.16 60 1.00

VADukeEnergyNarrows Boiler #7 Solid Sample #3 43.425 1.23 60 1.00

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Liquid Sample #1 166.745 4.72 4.3 YES

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Liquid Sample #2 167.281 4.74 4.3 YES

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Liquid Sample #3 168.63 4.78 5.3 YES

ARPotlatchForestWarren Wellons Boiler 40065 Solid Sample #1 208.754 5.91

ARPotlatchForestWarren Wellons Boiler 40065 Solid Sample #2 220.995 6.26

ARPotlatchForestWarren Wellons Boiler 40065 Solid Sample #3 217.503 6.16

CACovantaDelano Unit 1 Solid Sample #1 100.827 2.86

CACovantaDelano Unit 1 Solid Sample #2 102.364 2.90

CACovantaDelano Unit 1 Solid Sample #3 101.458 2.87

CTElectric Boat EMU 17 Liquid Sample #1 153.219 4.34

CTElectric Boat EMU 17 Liquid Sample #2 153.208 4.34

CTElectric Boat EMU 17 Liquid Sample #3 151.403 4.29

FLCFRC252 Boiler #3 (McBurney) Solid Sample #1 49.908 1.41

FLCFRC252 Boiler #3 (McBurney) Solid Sample #2 45.423 1.29

FLCFRC252 Boiler #3 (McBurney) Solid Sample #3 44.795 1.27

FLRayonierPerformance PB06 Solid Sample #1 80.598 2.28

FLRayonierPerformance PB06 Solid Sample #2 77.547 2.20

FLRayonierPerformance PB06 Solid Sample #3 67.32 1.91

FLRayonierPerformance PB06 Solid Sample #1 78.359 2.22

FLRayonierPerformance PB06 Solid Sample #2 77.714 2.20

FLRayonierPerformance PB06 Solid Sample #3 76.063 2.15

FLRayonierPerformance PB06 Solid Sample #1 76.412 2.16

FLRayonierPerformance PB06 Solid Sample #2 70.516 2.00

FLRayonierPerformance PB06 Solid Sample #3 72.781 2.06

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #1

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #2

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #3

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #1

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #2

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #3

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #1 176.217 4.99

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #2 171.561 4.86

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #3 172.454 4.88

GAInternationalPaperAugustaMills PB3A Solid Sample #1 62.864 1.78

GAInternationalPaperAugustaMills PB3A Solid Sample #2 70.654 2.00

GAInternationalPaperAugustaMills PB3A Solid Sample #3 68.063 1.93

HIPuuneneSugarMill Boiler 1 Solid Sample #1 98.787 2.80

HIPuuneneSugarMill Boiler 1 Solid Sample #2 95.978 2.72

HIPuuneneSugarMill Boiler 1 Solid Sample #3 118.402 3.35

HIPuuneneSugarMill Boiler 2 Solid Sample #1 98.787 2.80

Page 2 of 3

### Appendix A-1: Sample Times and Oxygen Percentages Used to Estimate Hg 3x RDL

Facility ID Combusor ID Fuel Category Test ID Sample

Volume (dscf) Sample

Volume

(dscm) Sample

Time (min) Sample

Time (hrs) Stack Oxygen

Concentration

(%) Use in

New

Source 3x

RDL?

HIPuuneneSugarMill Boiler 2 Solid Sample #2 95.978 2.72

HIPuuneneSugarMill Boiler 2 Solid Sample #3 118.402 3.35

ILCornProductsInt B10 Solid Sample #1 69.38 1.96

ILCornProductsInt B10 Solid Sample #2 70.43 1.99

ILCornProductsInt B10 Solid Sample #3 70.11 1.99

ILCornProductsInt B10 Solid Sample #1 74.8 2.12

ILCornProductsInt B10 Solid Sample #2 72.48 2.05

ILCornProductsInt B10 Solid Sample #3 73.06 2.07

ILPolyOne B1 Solid Sample #1 85.115 2.41

ILPolyOne B1 Solid Sample #2 83.675 2.37

ILPolyOne B1 Solid Sample #3 87.072 2.47

INTateLyleSagamore 31B1 Solid Sample #1 161.58 4.58

INTateLyleSagamore 31B1 Solid Sample #2 139.34 3.95

INTateLyleSagamore 31B1 Solid Sample #3 133.63 3.78

KYNewPage-Wickliffe B09 Solid Sample #1 84.796 2.40

KYNewPage-Wickliffe B09 Solid Sample #2 91.306 2.59

KYNewPage-Wickliffe B09 Solid Sample #3 97.028 2.75

KYNewPage-Wickliffe B09 Solid Sample #1 94.26 2.67

KYNewPage-Wickliffe B09 Solid Sample #2 86.917 2.46

KYNewPage-Wickliffe B09 Solid Sample #3 91.778 2.60

MEBoralexStratton Boiler #1 Solid Sample #1 168.8 4.78

MEBoralexStratton Boiler #1 Solid Sample #2 169.22 4.79

MEBoralexStratton Boiler #1 Solid Sample #3 168.75 4.78

MSGPNewAugusta AA-015 Power Boiler Solid Sample #1 68.96 1.95

MSGPNewAugusta AA-015 Power Boiler Solid Sample #2 55.59 1.57

MSGPNewAugusta AA-015 Power Boiler Solid Sample #3 61.31 1.74

MSGPNewAugusta AA-015 Power Boiler Solid Sample #1 139.834 3.96

MSGPNewAugusta AA-015 Power Boiler Solid Sample #2 136.646 3.87

MSGPNewAugusta AA-015 Power Boiler Solid Sample #3 127.831 3.62

MSGPNewAugusta AA-015 Power Boiler Solid Sample #1 137.153 3.88

MSGPNewAugusta AA-015 Power Boiler Solid Sample #2 169.443 4.80

MSGPNewAugusta AA-015 Power Boiler Solid Sample #3 126.858 3.59

NDCargillWestFargo Foster Wheeler Boiler (EU43) Solid Sample #1 126.485 3.58

NDCargillWestFargo Foster Wheeler Boiler (EU43) Solid Sample #2 134.933 3.82

NDCargillWestFargo Foster Wheeler Boiler (EU43) Solid Sample #3 138.135 3.91

NYBlackRiverGen E00001, E00002, E00003 Solid Sample #1 93.621 2.65 4.8 YES

NYBlackRiverGen E00001, E00002, E00003 Solid Sample #2 77.728 2.20 4.7 YES

NYBlackRiverGen E00001, E00002, E00003 Solid Sample #3 88.341 2.50 4.9 YES

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid 1N 44.229 1.25

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid 2N 44.634 1.26

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid 3N 41.309 1.17

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid 1S 32.963 0.93

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid 2S 31.301 0.89

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid 3S 45.924 1.30

TNCargillMemphis Stoker Boiler 8001 Solid Sample #1 169.383 4.80

TNCargillMemphis Stoker Boiler 8001 Solid Sample #2

TNCargillMemphis Stoker Boiler 8001 Solid Sample #3

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Liquid Sample #1 169.188 4.79

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Liquid Sample #2 170.974 4.84

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Liquid Sample #3 171.329 4.85

Page 3 of 3**Table A-2a: Summary of Hg 3x RDL for Existing Sources Fuel Category Average Sample Time (hrs)** **3x RDL (μg/dscm)** **F d** **Factor for Subcategory** **(dscf/MMBtu) Average Stack Oxygen** **Concentration (%) 3x RDL** **(lb/MMBtu)**Solid37.10E-019,7808.30**7.18E-07**Liquid46.20E-019,1904.90**4.64E-07**Process Gas46.20E-018,7104.70**4.35E-07 Table A-2b: Summary of Hg 3x RDL for New Sources** **Fuel Category Average Sample Time (hrs) 3x RDL** **(μg/dscm) F** **d Factor for** **Subcategory (dscf/MMBtu)** **Average Stack Oxygen Concentration (%)** **3x RDL (lb/MMBtu)** Solid21.00E+009,7804.80**7.92E-07**Liquid56.20E-019,1904.60**4.56E-07**Process Gas46.20E-018,7104.70**4.35E-07**Page 1 of 1

# Appendix B

Calculation of 3x RDL for Hydrogen Chloride**Appendix B-1: Sample Times and Oxygen Percentages Used to Estimate HCl 3x RDL**

**Facility ID Combusor ID Fuel Category Test ID Test Date Test** 

**Method Sample** 

**Time**

**(min) Sample** 

**Time (hrs) Stack Oxygen** 

**Concentration**

**(%) 3x RDL** 

**(μg/dscm) F**  **d Factor** 

**(dscf/MMBtu) 3x RDL** 

**(lb/MMBtu) Use in** 

**New**

**Source 3x**

**RDL?**

ALBoiseWhitePaperJackson 102-0001-Z013 Solid 1 8/5/2009 26A 120 2.00 9.00E+01 9,780

ALBoiseWhitePaperJackson 102-0001-Z013 Solid 2 8/5/2009 26A 120 2.00 9.00E+01 9,780

ALBoiseWhitePaperJackson 102-0001-Z013 Solid 3 8/5/2009 26A 120 2.00 9.00E+01 9,780

ALIPCourtland No. 3 Combination Boier / 11Cu301 Solid Sample #1 7/7/2009 26A 120 2.00 9.00E+01 9,780

ALIPCourtland No. 3 Combination Boier / 11Cu301 Solid Sample #2 7/7/2009 26A 120 2.00 9.00E+01 9,780

ALIPCourtland No. 3 Combination Boier / 11Cu301 Solid Sample #3 7/8/2009 26A 120 2.00 9.00E+01 9,780

ARAnthonyForestProducts SN-12 Solid Sample #1 9/1/2009 26 120 2.00 1.25E+02 9,780

ARAnthonyForestProducts SN-12 Solid Sample #2 9/1/2009 26 120 2.00 1.25E+02 9,780

ARAnthonyForestProducts SN-12 Solid Sample #3 9/2/2009 26 120 2.00 1.25E+02 9,780

ARPotlatchForestWarren Wellons Boiler Solid Sample #1 8/8/2006 26A 60 1.00 16 1.80E+02 9,780 4.65E-04 YES

ARPotlatchForestWarren Wellons Boiler Solid Sample #2 8/8/2006 26A 60 1.00 15.5 1.80E+02 9,780 4.23E-04 YES

ARPotlatchForestWarren Wellons Boiler Solid Sample #3 9/8/2006 26A 60 1.00 16 1.80E+02 9,780 4.65E-04 YES

ARPotlatchForestWarren Wellons Boiler Solid 1 9/8/2009 26A 60 1.00 4.22 1.80E+02 9,780 1.38E-04 YES

ARPotlatchForestWarren Wellons Boiler Solid 2 9/8/2009 26A 60 1.00 4.9 1.80E+02 9,780 1.43E-04 YES

ARPotlatchForestWarren Wellons Boiler Solid 3 9/8/2009 26A 60 1.00 4.39 1.80E+02 9,780 1.39E-04 YES

AZCatalystPaperSnowflake Power Boiler #2 Coal Solid Sample #1 3/24/2006 26A 60 1.00 1.80E+02 9,780

AZCatalystPaperSnowflake Power Boiler #2 Coal Solid Sample #2 3/24/2006 26A 60 1.00 1.80E+02 9,780

AZCatalystPaperSnowflake Power Boiler #2 Coal Solid Sample #3 3/24/2006 26A 60 1.00 1.80E+02 9,780

FLSugarCaneGrowersCoop Boiler No. 8 Solid Sample #1 12/16/2002 9,780

FLSugarCaneGrowersCoop Boiler No. 8 Solid Sample #2 12/16/2002 9,780

FLSugarCaneGrowersCoop Boiler No. 8 Solid Sample #3 12/16/2002 9,780

FLSugarCaneGrowersCoop Boiler No. 8 Solid Sample #1 1/19/2005 9,780

FLSugarCaneGrowersCoop Boiler No. 8 Solid Sample #2 1/19/2005 9,780

FLSugarCaneGrowersCoop Boiler No. 8 Solid Sample #3 1/19/2005 9,780

FLUSSugarCorp Boiler No. 4 Solid Sample #1 12/10/2002 9,780

FLUSSugarCorp Boiler No. 4 Solid Sample #2 12/10/2002 9,780

FLUSSugarCorp Boiler No. 4 Solid Sample #3 12/10/2002 9,780

FLUSSugarCorp Boiler No. 4 Solid Sample #1 12/1/2006 26A 60 1.00 1.80E+02 9,780

FLUSSugarCorp Boiler No. 4 Solid Sample #1 12/1/2006 9,780

FLUSSugarCorp Boiler No. 4 Solid Sample #2 12/1/2006 26A 60 1.00 1.80E+02 9,780

FLUSSugarCorp Boiler No. 4 Solid Sample #2 12/1/2006 9,780

FLUSSugarCorp Boiler No. 4 Solid Sample #3 12/1/2006 26A 60 1.00 1.80E+02 9,780

FLUSSugarCorp Boiler No. 4 Solid Sample #3 12/1/2006 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #1 12/31/2002 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #2 12/31/2002 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #3 12/31/2002 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #1 1/2/2003 26A 60 1.00 1.80E+02 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #2 1/2/2003 26A 60 1.00 1.80E+02 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #3 1/2/2003 26A 60 1.00 1.80E+02 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #1 1/25/2007 26A 60 1.00 1.80E+02 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #2 1/25/2007 26A 60 1.00 1.80E+02 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #3 1/25/2007 26A 50 0.83 1.80E+02 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #1 5/15/2007 26A 60 1.00 1.80E+02 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #2 5/15/2007 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #3 5/16/2007 9,780

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #1 8/13/2009 26 240 4.00 6.25E+01 9,780

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #2 8/13/2009 26 240 4.00 6.25E+01 9,780

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #3 8/14/2009 26 240 4.00 6.25E+01 9,780

GARayonierJesupMill PB01 Solid Sample #1 5/11/2004 9,780

GARayonierJesupMill PB01 Solid Sample #2 5/11/2004 9,780

GARayonierJesupMill PB01 Solid Sample #3 5/12/2004 9,780

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #1 8/24/2009 FTIR 240 4.00 9,780

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #2 8/24/2009 FTIR 240 4.00 9,780

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #3 8/25/2009 FTIR 240 4.00 9,780

IARoquetteAmerica Circulating Fluidized Bed Boiler (121) Solid 1 6/2/2009 26A 120 2.00 9.00E+01 9,780

IARoquetteAmerica Circulating Fluidized Bed Boiler (121) Solid 2 6/2/2009 26A 120 2.00 9.00E+01 9,780

IARoquetteAmerica Circulating Fluidized Bed Boiler (121) Solid 3 6/3/2009 26A 120 2.00 9.00E+01 9,780

IDMoyieSprings Lumber420 HFB1 Solid Sample #1 9/12/2003 9,780

IDMoyieSprings Lumber420 HFB1 Solid Sample #2 9/12/2003 9,780

IDMoyieSprings Lumber420 HFB1 Solid Sample #3 9/12/2003 9,780

IDPotlatch PB-1 CE Solid Sample #1 7/28/2009 26 60 1.00 13.2 2.50E+02 9,780 4.13E-04

IDPotlatch PB-1 CE Solid Sample #2 7/28/2009 26 60 1.00 13.8 2.50E+02 9,780 4.47E-04

IDPotlatch PB-1 CE Solid Sample #3 7/28/2009 26 60 1.00 13 2.50E+02 9,780 4.02E-04

IDTASCOPaul Babcock and Wilcox (B&W) Boiler Solid Sample #1 6/1/2006 26A 64 1.07 1.80E+02 9,780

IDTASCOPaul Erie City Boiler Solid Sample #1 6/20/2006 26A 64 1.07 1.80E+02 9,780

IDTASCOPaul Erie City Boiler Solid Sample #2 6/20/2006 26A 64 1.07 1.80E+02 9,780

IDTASCOPaul Erie City Boiler Solid Sample #3 6/21/2006 26A 64 1.07 1.80E+02 9,780

INAlcoaWarrick Unit #3 Solid M26A-1 8/17/2009 9,780

INAlcoaWarrick Unit #3 Solid M26A-2 8/17/2009 9,780

INAlcoaWarrick Unit #3 Solid M26A-3 8/17/2009 9,780

LAGPPortHudson EQT0109 - No. 6 CFB Boiler Solid Sample #1 8/14/2007 26A 60 1.00 1.80E+02 9,780

LAGPPortHudson EQT0109 - No. 6 CFB Boiler Solid Sample #2 8/14/2007 26A 60 1.00 1.80E+02 9,780

LAGPPortHudson EQT0109 - No. 6 CFB Boiler Solid Sample #3 8/14/2007 26A 60 1.00 1.80E+02 9,780

MEBoralexStratton Boiler #1 Solid Sample #1 10/21/2009 26A 60 1.00 6.3 1.80E+02 9,780 1.57E-04

MEBoralexStratton Boiler #1 Solid Sample #2 10/21/2009 26A 60 1.00 5.9 1.80E+02 9,780 1.53E-04

MEBoralexStratton Boiler #1 Solid Sample #3 10/21/2009 26A 60 1.00 5.9 1.80E+02 9,780 1.53E-04

MICityofEscanaba EUBOILER#1 Solid Sample #1 10/27/2004 26A 60 1.00 1.80E+02 9,780

MICityofEscanaba EUBOILER#1 Solid Sample #2 10/27/2004 26A 60 1.00 1.80E+02 9,780

MICityofEscanaba EUBOILER#1 Solid Sample #3 10/27/2004 26A 60 1.00 1.80E+02 9,780

MSBowaterSouth Bark Boiler Solid Sample #1 1/23/2007 9,780

MSBowaterSouth Bark Boiler Solid Sample #2 1/23/2007 9,780

MSBowaterSouth Bark Boiler Solid Sample #3 1/23/2007 9,780

MSGPNewAugusta AA-015 Power Boiler Solid Sample #1 7/12/2006 9,780

MSGPNewAugusta AA-015 Power Boiler Solid Sample #2 7/12/2006 9,780

MSGPNewAugusta AA-015 Power Boiler Solid Sample #3 7/12/2006 9,780

MSGPNewAugusta AA-015 Power Boiler Solid Sample #1 9/22/2010 9,780

MSGPNewAugusta AA-015 Power Boiler Solid Sample #2 9/23/2010 9,780

MSGPNewAugusta AA-015 Power Boiler Solid Sample #3 9/23/2010 9,780

MSGPNewAugusta AA-015 Power Boiler Solid Sample #1 9/28/2010 9,780

MSGPNewAugusta AA-015 Power Boiler Solid Sample #2 9/29/2010 9,780

MSGPNewAugusta AA-015 Power Boiler Solid Sample #3 9/30/2010 9,780

MSHankinsLumber Boiler #1 (AA-001) Solid Sample #2 1/10/2005 9,780

MSHoodWaynesboro AA-001 (Wood-Fired Boiler) Solid Sample #1 10/14/2003 26A 60 1.00 1.80E+02 9,780

MSHoodWaynesboro AA-001 (Wood-Fired Boiler) Solid Sample #2 10/14/2003 26A 60 1.00 1.80E+02 9,780

MSHoodWaynesboro AA-001 (Wood-Fired Boiler) Solid Sample #3 10/14/2003 26A 60 1.00 1.80E+02 9,780

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #1 8/6/2009 26A 120 2.00 8.06 9.00E+01 9,780 8.93E-05

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #2 8/6/2009 26A 120 2.00 7.25 9.00E+01 9,780 8.40E-05

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #3 8/6/2009 26A 120 2.00 7.63 9.00E+01 9,780 8.64E-05

NCGPRoxboro ES-1 Wood fired Boiler Solid Sample #1 7/14/2004 26A 60 1.00 1.80E+02 9,780

NCGPRoxboro ES-1 Wood fired Boiler Solid Sample #2 7/14/2004 26A 120 2.00 9.00E+01 9,780

Page 1 of 3**Appendix B-1: Sample Times and Oxygen Percentages Used to Estimate HCl 3x RDL**

**Facility ID Combusor ID Fuel Category Test ID Test Date Test** 

**Method Sample** 

**Time**

**(min) Sample** 

**Time (hrs) Stack Oxygen** 

**Concentration**

**(%) 3x RDL** 

**(μg/dscm) F**  **d Factor** 

**(dscf/MMBtu) 3x RDL** 

**(lb/MMBtu) Use in** 

**New**

**Source 3x**

**RDL?**

NCGPRoxboro ES-1 Wood fired Boiler Solid Sample #3 7/14/2004 26A 120 2.00 9.00E+01 9,780

NCLPRoaringRiver Boiler #2 Solid Sample #1 10/13/2004 9,780

NCLPRoaringRiver Boiler #2 Solid Sample #2 10/14/2004 9,780

NCLPRoaringRiver Boiler #2 Solid Sample #3 10/14/2004 9,780

NDCargillWestFargo Foster Wheeler Boiler (EU43) Solid 1 8/25/2009 26A 120 2.00 9.00E+01 9,780

NDCargillWestFargo Foster Wheeler Boiler (EU43) Solid 2 8/25/2009 26A 120 2.00 9.00E+01 9,780

NDCargillWestFargo Foster Wheeler Boiler (EU43) Solid 3 8/25/2009 26A 120 2.00 9.00E+01 9,780

NDMinnDakFarmers Babcock and Wilcox Boiler #5 Solid Sample #1 10/26/2006 26A 60 1.00 1.80E+02 9,780

NDMinnDakFarmers Babcock and Wilcox Boiler #5 Solid Sample #2 10/26/2006 26A 60 1.00 1.80E+02 9,780

NDMinnDakFarmers Babcock and Wilcox Boiler #5 Solid Sample #3 10/26/2006 26A 60 1.00 1.80E+02 9,780

ORRoseburgCoquille Boiler 1 Solid Sample #1 10/14/2004 26A 60 1.00 1.80E+02 9,780

ORRoseburgCoquille Boiler 1 Solid Sample #1 10/14/2004 26A 60 1.00 1.80E+02 9,780

ORRoseburgCoquille Boiler 1 Solid Sample #1 10/14/2004 26A 60 1.00 1.80E+02 9,780

ORRoseburgCoquille Boiler 1 Solid Sample #2 10/14/2004 26A 60 1.00 1.80E+02 9,780

ORRoseburgCoquille Boiler 1 Solid Sample #2 10/14/2004 26A 60 1.00 1.80E+02 9,780

ORRoseburgCoquille Boiler 1 Solid Sample #2 10/14/2004 26A 60 1.00 1.80E+02 9,780

ORRoseburgRiddle2 Boiler #2 Solid Sample #1 10/11/2004 26A 60 1.00 1.80E+02 9,780

ORRoseburgRiddle2 Boiler #2 Solid Sample #2 10/11/2004 26A 60 1.00 1.80E+02 9,780

ORRoseburgRiddle2 Boiler #2 Solid Sample #3 10/11/2004 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #81 Coal Boiler Solid Sample #3 7/17/2007 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #81 Coal Boiler Solid Sample #1 7/18/2007 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #81 Coal Boiler Solid Sample #2 7/18/2007 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #81 Coal Boiler Solid 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #81 Coal Boiler Solid 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #81 Coal Boiler Solid 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #82 Coal Boiler Solid Sample #3 7/17/2007 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #82 Coal Boiler Solid Sample #1 7/18/2007 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #82 Coal Boiler Solid Sample #2 7/18/2007 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #82 Coal Boiler Solid 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #82 Coal Boiler Solid 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #82 Coal Boiler Solid 26A 60 1.00 1.80E+02 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #1 11/25/2003 26A 60 1.00 1.80E+02 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #2 11/25/2003 26A 60 1.00 1.80E+02 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #3 11/25/2003 26A 60 1.00 1.80E+02 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #1 11/3/2005 26A 60 1.00 1.80E+02 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #2 11/3/2005 26A 60 1.00 1.80E+02 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #3 11/3/2005 26A 60 1.00 1.80E+02 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #1 11/7/2007 26A 60 1.00 1.80E+02 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #2 11/7/2007 26A 60 1.00 1.80E+02 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #3 11/7/2007 26A 60 1.00 1.80E+02 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #1 8/18/2009 26A 240 4.00 4.50E+01 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #2 8/18/2009 26A 240 4.00 4.50E+01 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #3 8/19/2009 26A 240 4.00 4.50E+01 9,780

SCMarlboroPaper Hogged Fuel Boiler Solid Sample #1 7/14/2009 26A 180 3.00 9.74 6.00E+01 9,780 6.85E-05

SCMarlboroPaper Hogged Fuel Boiler Solid Sample #2 7/14/2009 26A 180 3.00 9.38 6.00E+01 9,780 6.63E-05

SCMarlboroPaper Hogged Fuel Boiler Solid Sample #3 7/14/2009 26A 180 3.00 9.11 6.00E+01 9,780 6.48E-05

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #1 10/6/2005 9,780

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #2 10/6/2005 9,780

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #3 10/6/2005 9,780

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #1 10/7/2005 9,780

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #2 10/7/2005 9,780

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #3 10/7/2005 9,780

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #1 8/4/2009 26A 120 2.00 9.00E+01 9,780

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #2 8/4/2009 26A 120 2.00 9.00E+01 9,780

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #3 8/5/2009 26A 120 2.00 9.00E+01 9,780

TNEastman_NO_CBIDATA Boiler 30 Solid Sample #1 8/26/2009 26A 120 2.00 9.00E+01 9,780

TNEastman_NO_CBIDATA Boiler 30 Solid Sample #2 8/27/2009 26A 120 2.00 9.00E+01 9,780

TNEastman_NO_CBIDATA Boiler 30 Solid Sample #3 8/27/2009 26A 120 2.00 9.00E+01 9,780

TXDibollTemple-Inland PB-44 Solid Sample #1 6/29/2007 26A 60 1.00 1.80E+02 9,780

TXDibollTemple-Inland PB-44 Solid Sample #2 6/29/2007 26A 60 1.00 1.80E+02 9,780

TXDibollTemple-Inland PB-44 Solid Sample #3 6/29/2007 26A 60 1.00 1.80E+02 9,780

VASmurfitStoneWestpt PB08 Solid Sample #1 11/8/2004 9,780

VASmurfitStoneWestpt PB08 Solid Sample #2 11/8/2004 26A 60 1.00 1.80E+02 9,780

VASmurfitStoneWestpt PB08 Solid Sample #3 11/8/2004 26A 60 1.00 1.80E+02 9,780

VASmurfitStoneWestpt PB08 Solid Sample #1 9/26/2009 26A 120 2.00 9.00E+01 9,780

VASmurfitStoneWestpt PB08 Solid Sample #2 9/26/2009 26A 120 2.00 9.00E+01 9,780

VASmurfitStoneWestpt PB08 Solid Sample #3 9/26/2009 26A 120 2.00 9.00E+01 9,780

VAUniversityofVirginia 7103-1-01R Solid M26A-1 9/15/2009 26A 120 2.00 9.00E+01 9,780

VAUniversityofVirginia 7103-1-01R Solid M26A-2 9/16/2009 26A 120 2.00 9.00E+01 9,780

VAUniversityofVirginia 7103-1-01R Solid M26A-3 9/17/2009 26A 120 2.00 9.00E+01 9,780

WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #1 6/22/2006 26 60 1.00 2.50E+02 9,780

WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #2 6/22/2006 26 60 1.00 2.50E+02 9,780

WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #3 6/22/2006 26 60 1.00 2.50E+02 9,780

WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #1 8/14/2009 26 60 1.00 2.50E+02 9,780

WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #2 8/14/2009 26 60 1.00 2.50E+02 9,780

WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #3 8/14/2009 26 60 1.00 2.50E+02 9,780

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Solid Sample #1 8/11/2009 26 240 4.00 7 6.25E+01 9,780 5.73E-05

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Solid Sample #2 8/11/2009 26 240 4.00 7 6.25E+01 9,780 5.73E-05

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Solid Sample #3 8/12/2009 26 240 4.00 7 6.25E+01 9,780 5.73E-05

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #1 10/27/1992 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #2 10/27/1992 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #3 10/27/1992 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #1 8/10/2004 26A 60 1.00 6 1.80E+02 9,780 1.54E-04

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #2 8/10/2004 26A 60 1.00 6 1.80E+02 9,780 1.54E-04

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #3 8/11/2004 26A 60 1.00 6 1.80E+02 9,780 1.54E-04

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #1 7/19/2005 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #2 7/19/2005 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #3 7/19/2005 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #1 8/21/2006 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #2 8/21/2006 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #3 8/21/2006 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid 26A 60 1.00 1.80E+02 9,780

WINewPageBiron B24 Solid Sample #1 9/12/2007 26A 60 1.00 1.80E+02 9,780

WINewPageBiron B24 Solid Sample #2 9/12/2007 26A 60 1.00 1.80E+02 9,780

WINewPageBiron B24 Solid Sample #3 9/12/2007 26A 60 1.00 1.80E+02 9,780

Page 2 of 3**Appendix B-1: Sample Times and Oxygen Percentages Used to Estimate HCl 3x RDL**

**Facility ID Combusor ID Fuel Category Test ID Test Date Test** 

**Method Sample** 

**Time**

**(min) Sample** 

**Time (hrs) Stack Oxygen** 

**Concentration**

**(%) 3x RDL** 

**(μg/dscm) F**  **d Factor** 

**(dscf/MMBtu) 3x RDL** 

**(lb/MMBtu) Use in** 

**New**

**Source 3x**

**RDL?**

WINewPageBiron B24 Solid 1 8/25/2009 26A 120 2.00 9.00E+01 9,780

WINewPageBiron B24 Solid 2 9/22/2009 26A 120 2.00 9.00E+01 9,780

WINewPageBiron B24 Solid 3 9/22/2009 26A 120 2.00 9.00E+01 9,780

WINewPage-WisconsinRapids Power Boiler 1 - B21 Solid Sample #1 12/14/2005 26A 60 1.00 1.80E+02 9,780

WINewPage-WisconsinRapids Power Boiler 1 - B21 Solid Sample #2 12/15/2005 26A 60 1.00 1.80E+02 9,780

WINewPage-WisconsinRapids Power Boiler 1 - B21 Solid Sample #3 12/15/2005 26A 60 1.00 1.80E+02 9,780

CTElectric Boat EMU 17 Liquid 1 8/17/2009 9,190

CTElectric Boat EMU 17 Liquid 2 8/17/2009 9,190

CTElectric Boat EMU 17 Liquid 3 8/17/2009 9,190

PABoeingRidleyPark 033 Liquid Sample #1 9/22/2009 9,190

PABoeingRidleyPark 033 Liquid Sample #2 9/23/2009 9,190

PABoeingRidleyPark 033 Liquid Sample #3 9/24/2009 9,190

SCMilliken-Dewey D30 Liquid Sample #1 8/13/2009 26A 120 2.00 3.83 9.00E+01 9,190 6.32E-05

SCMilliken-Dewey D30 Liquid Sample #2 8/13/2009 26A 120 2.00 4.02 9.00E+01 9,190 6.39E-05

SCMilliken-Dewey D30 Liquid Sample #3 8/13/2009 26A 120 2.00 3.96 9.00E+01 9,190 6.37E-05

TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #1 8/31/2006 26A 60 1.00 10 1.80E+02 9,190 1.98E-04 YES

TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #2 8/31/2006 26A 60 1.00 9.9 1.80E+02 9,190 1.96E-04 YES

TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #3 8/31/2006 26A 60 1.00 9.9 1.80E+02 9,190 1.96E-04 YES

TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #1 7/29/2009 26A 60 1.00 7.4 1.80E+02 9,190 1.60E-04 YES

TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #2 7/30/2009 26A 60 1.00 6.4 1.80E+02 9,190 1.49E-04 YES

TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #3 7/30/2009 26A 60 1.00 6.8 1.80E+02 9,190 1.53E-04 YES

WVMountainStateCarbonFollansbee S1 Process Gas Sample #1 10/22/2009 26A 120 2.00 4.5 9.00E+01 8,710 6.23E-05 YES

WVMountainStateCarbonFollansbee S1 Process Gas Sample #2 10/22/2009 26A 120 2.00 4.7 9.00E+01 8,710 6.31E-05 YES

WVMountainStateCarbonFollansbee S1 Process Gas Sample #3 10/23/2009 26A 120 2.00 4.8 9.00E+01 8,710 6.35E-05 YES

CTElectric Boat EMU 17 Liquid 8/17/2009 26A 60 1.00 4.63 1.80E+02 9,190 1.33E-04

CTElectric Boat EMU 17 Liquid 8/17/2009 26A 60 1.00 4.67 1.80E+02 9,190 1.33E-04

CTElectric Boat EMU 17 Liquid 8/17/2009 26A 60 1.00 4.68 1.80E+02 9,190 1.33E-04

FLSugarCaneGrowersCoop Boiler No. 8 Solid 1/19/2005 26A 60 1.00 7.93 1.80E+02 9,780 1.77E-04

FLSugarCaneGrowersCoop Boiler No. 8 Solid 1/19/2005 26A 60 1.00 7.38 1.80E+02 9,780 1.70E-04

FLSugarCaneGrowersCoop Boiler No. 8 Solid 1/19/2005 26A 60 1.00 7.32 1.80E+02 9,780 1.69E-04

FLSugarCaneGrowersCoop Boiler No. 8 Solid 12/16/2002 26A 60 1.00 8.6 1.80E+02 9,780 1.86E-04

FLSugarCaneGrowersCoop Boiler No. 8 Solid 12/16/2002 26A 60 1.00 7.85 1.80E+02 9,780 1.76E-04

FLSugarCaneGrowersCoop Boiler No. 8 Solid 12/16/2002 26A 60 1.00 8.85 1.80E+02 9,780 1.90E-04

FLUSSugarCorp Boiler No. 7 Solid 12/31/2002 26A 60 1.00 8.48 1.80E+02 9,780 1.85E-04

FLUSSugarCorp Boiler No. 7 Solid 37623 26A 60 1.00 1.80E+02 9,780

FLUSSugarCorp Boiler No. 7 Solid 37623 26A 60 1.00 1.80E+02 9,780

IDMoyieSprings Lumber420 HFB1 Solid 9/12/2003 26A 72 1.20 1.80E+02 9,780

IDMoyieSprings Lumber420 HFB1 Solid 9/12/2003 26A 72 1.20 1.80E+02 9,780

IDMoyieSprings Lumber420 HFB1 Solid 9/12/2003 26A 72 1.20 1.80E+02 9,780

INAlcoaWarrick Unit #3 Solid 8/17/2009 26A 120 2.00 5.4 9.00E+01 9,780 7.40E-05

INAlcoaWarrick Unit #3 Solid 8/17/2009 26A 120 2.00 5.49 9.00E+01 9,780 7.45E-05

INAlcoaWarrick Unit #3 Solid 8/17/2009 26A 120 2.00 5.55 9.00E+01 9,780 7.48E-05

MEFPLEnergyWyman Unit #5 Liquid 10/5/2009 26A 9,190

MEFPLEnergyWyman Unit #5 Liquid 10/5/2009 26A 9,190

MEFPLEnergyWyman Unit #5 Liquid 10/5/2009 26A 9,190

MIConsumerEnergyCo-Campbell EUAUXBLR12 Liquid 9/1/2009 320 153 2.55 9,190

MIConsumerEnergyCo-Campbell EUAUXBLR12 Liquid 9/1/2009 320 149 2.48 9,190

MIConsumerEnergyCo-Campbell EUAUXBLR12 Liquid 9/1/2009 320 124 2.07 9,190

MIConsumerEnergyCo-Campbell EUAUXBLR12 Liquid 9/1/2009 320 124 2.07 9,190

MNGPDuluth EU33 Boiler #3 Liquid 8/6/2009 26A 120 2.00 9.00E+01 9,190

MNGPDuluth EU33 Boiler #3 Liquid 8/6/2009 26A 120 2.00 9.00E+01 9,190

MNGPDuluth EU33 Boiler #3 Liquid 8/6/2009 26A 120 2.00 9.00E+01 9,190

MSGPNewAugusta AA-015 Power Boiler Solid 7/12/2006 26 60 1.00 2.50E+02 9,780

MSGPNewAugusta AA-015 Power Boiler Solid 7/12/2006 26 60 1.00 2.50E+02 9,780

MSGPNewAugusta AA-015 Power Boiler Solid 7/12/2006 26 60 1.00 2.50E+02 9,780

MSGPNewAugusta AA-015 Power Boiler Solid 9/22/2010 26 240 4.00 9,780

MSGPNewAugusta AA-015 Power Boiler Solid 9/22/2010 26 240 4.00 9,780

MSGPNewAugusta AA-015 Power Boiler Solid 9/22/2010 26 240 4.00 9,780

MSGPNewAugusta AA-015 Power Boiler Solid 40449 26 240 4.00 9,780

MSGPNewAugusta AA-015 Power Boiler Solid 40449 26 240 4.00 9,780

MSGPNewAugusta AA-015 Power Boiler Solid 40449 26 240 4.00 9,780

NCLPRoaringRiver Boiler #2 Solid 10/13/2004 26A 64 1.07 1.80E+02 9,780

NCLPRoaringRiver Boiler #2 Solid 10/13/2004 26A 64 1.07 1.80E+02 9,780

NCLPRoaringRiver Boiler #2 Solid 10/13/2004 26A 64 1.07 1.80E+02 9,780

PABoeingRidleyPark 033 Liquid 9/22/2009 26A 120 2.00 9.00E+01 9,190

PABoeingRidleyPark 033 Liquid 9/22/2009 26A 120 2.00 9.00E+01 9,190

PABoeingRidleyPark 033 Liquid 9/22/2009 26A 120 2.00 9.00E+01 9,190

SCDAKAmericas P8F Liquid 7/15/2009 26A 120 2.00 3.6 9.00E+01 9,190 6.24E-05

SCDAKAmericas P8F Liquid 7/15/2009 26A 120 2.00 3.5 9.00E+01 9,190 6.20E-05

SCDAKAmericas P8F Liquid 40010 26A 120 2.00 3.6 9.00E+01 9,190 6.24E-05

TNBowaterNewsprint BFB North Solid 40092 26A 60 1.00 5.6 1.80E+02 9,780 1.50E-04

TNBowaterNewsprint BFB North Solid 40092 26A 60 1.00 5.4 1.80E+02 9,780 1.48E-04

TNBowaterNewsprint BFB North Solid 40092 26A 60 1.00 5.8 1.80E+02 9,780 1.52E-04

TNBowaterNewsprint BFB South Solid 40092 26A 60 1.00 1.80E+02 9,780

TNBowaterNewsprint BFB South Solid 40092 26A 60 1.00 1.80E+02 9,780

TNBowaterNewsprint BFB South Solid 40092 26A 60 1.00 1.80E+02 9,780

WINewPageBiron B24 - boiler 5 Solid 9/22/2009 26A 140 2.33 7.1 9.00E+01 9,780 8.31E-05

WINewPageBiron B24 - boiler 5 Solid 9/22/2009 26A 140 2.33 7.1 9.00E+01 9,780 8.31E-05

WINewPageBiron B24 - boiler 5 Solid 9/22/2009 26A 140 2.33 9.7 9.00E+01 9,780 1.02E-04

Page 3 of 3**Table B-2a: Summary of HCl 3x RDL for Existing Sources Fuel Category** **Average Sample Volume (dscm) or Sample Time (hrs)** **3x RDL (μg/dscm)** **F d** **Factor for Subcategory** **(dscf/MMBtu) Average Stack Oxygen** **Concentration (%) 3x RDL** **(lb/MMBtu)**Solid28.07E+001489780.00**1.65E-04**Liquid25.79E+001299190.00**1.22E-04**Process Gas24.67E+00908710.00**6.30E-05 Table B-2b: Summary of HCl 3x RDL for New Sources** **Fuel Category Average Sample Volume (dscm)** **or Sample Time (hrs) 3x RDL** **(μg/dscm) F** **d Factor for** **Subcategory (dscf/MMBtu)** **Average Stack Oxygen Concentration (%)** **3x RDL (lb/MMBtu)** Solid11.02E+011809780.00**2.96E-04**Liquid18.40E+001809190.00**1.75E-04**Process Gas24.67E+00908710.00**6.30E-05**Page 1 of 1

# Appendix C

Calculation of 3x RDL for Filterable Particulate Matter

### Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

**Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date Sample** 

**Time**

**(min) Sample** 

**Time (hrs) Stack Oxygen** 

**Concentration**

**(%) Use in** 

**New**

**Source 3x**

**RDL?**

ALIPCourtland No. 3 Combination Boier / 11Cu301 Biomass FB Sample #1 7/7/2009

ALIPCourtland No. 3 Combination Boier / 11Cu301 Biomass FB Sample #2 7/7/2009

ALIPCourtland No. 3 Combination Boier / 11Cu301 Biomass FB Sample #3 7/8/2009

ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner Sample #1 8/8/2006 60 1.00 16

ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner Sample #2 8/8/2006 60 1.00 15.5

ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner Sample #3 8/8/2006 60 1.00 16

ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner 1 9/9/2009 240 4.00 4.22

ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner 2 9/9/2009 240 4.00 4.9

ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner 3 9/10/2009 240 4.00 4.39

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #1 8/7/1997 120 2.00 6.7 YES

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #2 8/7/1997 120 2.00 6.4 YES

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #3 8/7/1997 120 2.00 6.4 YES

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #1 12/5/2002 60 1.00 8.07 YES

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #2 12/5/2002 60 1.00 7.84 YES

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #3 12/5/2002 60 1.00 7.84 YES

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #1 7/22/2009 240 4.00 9.18 YES

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #2 7/23/2009 240 4.00 9.23 YES

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #3 7/23/2009 240 4.00 9.33 YES

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 1/20/1998

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 1/20/1998

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 1/20/1998

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 11/24/1998

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 11/24/1998

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 11/24/1998

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 11/22/1999

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 11/22/1999

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 11/22/1999

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #4 11/22/1999

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 12/1/1999

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 12/1/1999

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 12/1/1999

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 1/18/2001

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 1/18/2001

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 1/18/2001

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 11/20/2001

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 11/20/2001

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 11/20/2001

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 12/2/2002

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 12/2/2002

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 12/2/2002

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 1/13/2004

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 1/13/2004

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 1/13/2004

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 1/21/2005

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 1/21/2005

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 1/21/2005

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 1/18/2006

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 1/18/2006

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 1/18/2006

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 12/7/2006

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 12/7/2006

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 12/7/2006

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 12/19/2007

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 12/19/2007

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 12/19/2007

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 1/13/2009

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 1/13/2009

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 1/13/2009

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 12/22/2009

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 12/22/2009

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 12/22/2009

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 12/7/2010

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 12/7/2010

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 12/7/2010

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 2/8/1999

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 2/8/1999

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 2/8/1999

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 12/17/1999

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 12/17/1999

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 12/17/1999

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 1/31/2000

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 1/31/2000

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 1/31/2000

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 1/5/2001

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 1/5/2001

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 1/6/2001

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 1/9/2002

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 1/9/2002

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 1/9/2002

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 11/15/2002

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 11/15/2002

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 11/15/2002

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 12/30/2003

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 12/30/2003

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 12/30/2003

Page 1 of 12

### Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

**Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date Sample** 

**Time**

**(min) Sample** 

**Time (hrs) Stack Oxygen** 

**Concentration**

**(%) Use in** 

**New**

**Source 3x**

**RDL?**

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 2/4/2005

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 2/4/2005

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 2/4/2005

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 1/5/2006

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 1/5/2006

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 1/5/2006

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 1/25/2007

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 1/25/2007

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 1/25/2007

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 1/24/2008

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 1/24/2008

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 1/24/2008

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 12/4/2008

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 12/4/2008

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 12/4/2008

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 11/20/2009

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 11/20/2009

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 11/20/2009

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 11/4/2010

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 11/4/2010

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 11/4/2010

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 3/24/2005

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 3/24/2005

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 3/24/2005

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 3/26/2005

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 3/26/2005

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 3/26/2005

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 1/10/2006

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 1/10/2006

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 1/10/2006

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 6/2/2006 60 1.00 7.58

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 6/2/2006 60 1.00 7.99

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 6/2/2006 60 1.00 9.22

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #4 6/2/2006 60 1.00 9.84

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #5 6/2/2006 60 1.00 9.1

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 8/22/2006 64 1.07 10.36

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 8/22/2006 64 1.07 10.43

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 8/22/2006 64 1.07 10.3

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 39083 60 1.00 6.52

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 39083 60 1.00 6.96

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #4 39083 60 1.00 6.53

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 1/5/2007 60 1.00 7.73

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 1/5/2007 60 1.00 7.65

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 1/5/2007 60 1.00 7.25

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 11/30/2007

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 11/30/2007

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 11/30/2007

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 12/11/2008

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 12/11/2008

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 12/11/2008

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #4 12/11/2008

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 12/2/2009 60 1.00 6.4

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 12/2/2009 60 1.00 7

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 12/3/2009 60 1.00 5.6

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 11/30/2010

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 11/30/2010

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 11/30/2010

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #4 12/2/2010

GATempleInlandRome WF Biomass FB 1 7/27/2009

GATempleInlandRome WF Biomass FB 2 7/28/2009

GATempleInlandRome WF Biomass FB 3 7/28/2009

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #1 4/18/1994

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #2 4/18/1994

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 4/18/1994

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #1 5/22/1995

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #2 5/22/1995

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 5/22/1995

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #1 9/11/1997

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #2 9/11/1997

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 9/11/1997

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #1 7/12/2000

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #2 7/12/2000

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 7/12/2000

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #1 9/25/2003

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #2 9/25/2003

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 9/25/2003

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #1 10/07/2004

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #2 10/07/2004

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 10/07/2004

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #1 4/11/2005

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #2 4/11/2005

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 4/11/2005

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #1 4/12/2005

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #2 4/12/2005

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 4/12/2005

Page 2 of 12

### Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

**Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date Sample** 

**Time**

**(min) Sample** 

**Time (hrs) Stack Oxygen** 

**Concentration**

**(%) Use in** 

**New**

**Source 3x**

**RDL?**

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #4 4/12/2005

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #5 4/12/2005

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #6 4/13/2005

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #7 4/13/2005

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #8 4/13/2005

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #1 7/16/2007

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #2 7/17/2007

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 7/17/2007

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #1 8/23/2010

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #2 8/23/2010

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 8/23/2010

IDPotlatch PB-1 CE Biomass Fuel Cell Sample #1 4/30/2008

IDPotlatch PB-1 CE Biomass Fuel Cell Sample #2 4/30/2008

IDPotlatch PB-1 CE Biomass Fuel Cell Sample #3 4/30/2008

IDPotlatch PB-1 CE Biomass Fuel Cell Sample #1 7/28/2009 240 4.00 13.2

IDPotlatch PB-1 CE Biomass Fuel Cell Sample #2 7/28/2009 240 4.00 13.8

IDPotlatch PB-1 CE Biomass Fuel Cell Sample #3 7/29/2009 240 4.00 13

MNWeyerhaeuserIronton EU 001 - 4 Cell Furnace Biomass Fuel Cell Sample #1 12/20/2006

MNWeyerhaeuserIronton EU 001 - 4 Cell Furnace Biomass Fuel Cell Sample #2 12/20/2006

MNWeyerhaeuserIronton EU 001 - 4 Cell Furnace Biomass Fuel Cell Sample #3 12/20/2006

MSNorbordMS Wellons No. 1 Biomass Fuel Cell Sample #1 8/1/2007

MSNorbordMS Wellons No. 1 Biomass Fuel Cell Sample #2 8/1/2007

MSNorbordMS Wellons No. 1 Biomass Fuel Cell Sample #3 8/1/2007

MSNorbordMS Wellons No. 2 Biomass Fuel Cell Sample #1 8/1/2007

MSNorbordMS Wellons No. 2 Biomass Fuel Cell Sample #2 8/1/2007

MSNorbordMS Wellons No. 2 Biomass Fuel Cell Sample #3 8/1/2007

MSNorbordMS Wellons No. 3 Biomass Fuel Cell Sample #1 8/1/2007

MSNorbordMS Wellons No. 3 Biomass Fuel Cell Sample #2 8/1/2007

MSNorbordMS Wellons No. 3 Biomass Fuel Cell Sample #3 8/1/2007

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #1 2/26/1993

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #2 2/26/1993

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #3 2/26/1993

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #1 8/23/1999

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #2 8/23/1999

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #3 8/23/1999

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #1 7/11/2003

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #2 7/11/2003

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #3 7/11/2003

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #1 6/28/2005

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #2 6/28/2005

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #3 6/28/2005

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #1 2/22/2006

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #2 2/22/2006

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #3 2/22/2006

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #1 8/31/2007

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #2 8/31/2007

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #3 8/31/2007

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #1 8/5/2009 180 3.00 8.06

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #2 8/5/2009 180 3.00 7.25

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #3 8/5/2009 180 3.00 7.63

OHSauderWoodArchbold B009 Biomass Suspension Burner Sample #1 6/18/2008 60 1.00 9.7 YES

OHSauderWoodArchbold B009 Biomass Suspension Burner Sample #2 6/18/2008 60 1.00 9.48 YES

OHSauderWoodArchbold B009 Biomass Suspension Burner Sample #3 6/18/2008 60 1.00 9.43 YES

ORGeorgiaPacificWaunaMill EU35 - Fluidized Bed Boiler Biomass FB Sample #1 3/22/2006

ORGeorgiaPacificWaunaMill EU35 - Fluidized Bed Boiler Biomass FB Sample #2 3/22/2006

ORGeorgiaPacificWaunaMill EU35 - Fluidized Bed Boiler Biomass FB Sample #3 3/22/2006

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB Sample #1 10/6/2005

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB Sample #2 10/6/2005

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB Sample #3 10/6/2005

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB Sample #1 10/7/2005

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB Sample #2 10/7/2005

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB Sample #3 10/7/2005

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 1 8/4/2009

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 2 8/4/2009

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 3 8/5/2009

TXRGVSG Boiler No. 6 Biomass Suspension/Grate Sample #1 1/13/2009

TXRGVSG Boiler No. 6 Biomass Suspension/Grate Sample #2 1/13/2009

TXRGVSG Boiler No. 6 Biomass Suspension/Grate Sample #3 1/13/2009

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #1 9/18/1996 120 2.00 10.7 YES

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #2 9/18/1996 120 2.00 10.6 YES

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #3 9/18/1996 120 2.00 9.4 YES

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #1 11/10/2004 60 1.00 9.5 YES

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #2 11/10/2004 60 1.00 9.3 YES

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #3 11/10/2004 60 1.00 8.7 YES

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #1 8/11/2009 240 4.00 7 YES

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #2 8/11/2009 240 4.00 7 YES

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #3 8/12/2009 240 4.00 7 YES

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Biomass FB Sample #1 9/19/2007 60 1.00

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Biomass FB Sample #2 9/19/2007 60 1.00

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Biomass FB Sample #3 9/19/2007 60 1.00

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Biomass FB Sample #1 8/20/2009 240 4.00 7

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Biomass FB Sample #2 8/20/2009 240 4.00 7

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Biomass FB Sample #3 8/21/2009 240 4.00 7

WVGPMtHopeOSB 5600 - Wellons Energy System Biomass Dutch Oven/Pile Burner Sample #1 7/11/2006

WVGPMtHopeOSB 5600 - Wellons Energy System Biomass Dutch Oven/Pile Burner Sample #2 7/11/2006

Page 3 of 12

### Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

**Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date Sample** 

**Time**

**(min) Sample** 

**Time (hrs) Stack Oxygen** 

**Concentration**

**(%) Use in** 

**New**

**Source 3x**

**RDL?**

WVGPMtHopeOSB 5600 - Wellons Energy System Biomass Dutch Oven/Pile Burner Sample #3 7/11/2006

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 12/12/2007

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 12/12/2007

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 12/12/2007

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 12/12/2007

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 12/12/2007

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 12/12/2007

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 12/12/2007

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 12/12/2007

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 12/12/2007

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 7/11/2008

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 7/11/2008

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 7/11/2008

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 7/11/2008

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 7/11/2008

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 7/11/2008

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 7/11/2008

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 7/11/2008

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 7/11/2008

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/24/2009

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/24/2009

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/24/2009

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/14/2011

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/14/2011

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/14/2011

ARLeolaLumberMill SN-01A Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/14/2006

ARLeolaLumberMill SN-01A Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/14/2006

ARLeolaLumberMill SN-01A Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/14/2006

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #1 8/11/1997 60 1.00 9

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #2 8/11/1997 60 1.00 9

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #3 8/11/1997 60 1.00 9

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #1 11/21/1998

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #2 11/21/1998

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #3 11/21/1998

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #1 12/10/1999

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #2 12/10/1999

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #3 12/10/1999

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #1 11/9/2000

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #2 11/9/2000

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #3 11/9/2000

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #1 12/5/2001

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #2 12/5/2001

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #3 12/5/2001

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #1 12/4/2002

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #2 12/4/2002

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #3 12/4/2002

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #1 12/4/2003

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #2 12/4/2003

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #3 12/4/2003

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #1 9/29/2004

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #2 9/29/2004

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #3 9/29/2004

CASierraPacificLincoln McBurney Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 3/5/2008

CASierraPacificLincoln McBurney Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 3/5/2008

CASierraPacificLincoln McBurney Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 3/5/2008

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 37773 120 2.00 9.78 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 37773 120 2.00 9.55 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 37773 120 2.00 7.91 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 10/14/2004 60 1.00 8.82 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 10/14/2004 60 1.00 8.76 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 10/14/2004 60 1.00 9.06 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/15/2006 60 1.00 7.75 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/15/2006 60 1.00 8.13 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/15/2006 60 1.00 8.46 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/16/2006

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/16/2006

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/16/2006

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 9/18/2007 60 1.00 7.35 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 9/18/2007

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 9/18/2007 60 1.00 6.6 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 9/18/2007

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 9/18/2007 60 1.00 7.51 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 9/18/2007

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 9/19/2007

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 9/19/2007

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 9/19/2007

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 1 8/11/2009

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 2 8/12/2009

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 3 8/12/2009

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 8/27/2009 240 4.00 8.88 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 8/27/2009

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 8/27/2009 240 4.00 8.21 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 8/27/2009

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 8/27/2009 240 4.00 7.21 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 8/27/2009

Page 4 of 12

### Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

**Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date Sample** 

**Time**

**(min) Sample** 

**Time (hrs) Stack Oxygen** 

**Concentration**

**(%) Use in** 

**New**

**Source 3x**

**RDL?**

GATempleInlandRome PB4 Wet Biomass Stoker/SlopedGrate/Other Sample #1 2/27/2008

GATempleInlandRome PB4 Wet Biomass Stoker/SlopedGrate/Other Sample #2 2/27/2008

GATempleInlandRome PB4 Wet Biomass Stoker/SlopedGrate/Other Sample #3 2/27/2008

IDPotlatch PB-2 Riley Wet Biomass Stoker/SlopedGrate/Other Sample #1 5/1/2008

IDPotlatch PB-2 Riley Wet Biomass Stoker/SlopedGrate/Other Sample #2 5/1/2008

IDPotlatch PB-2 Riley Wet Biomass Stoker/SlopedGrate/Other Sample #3 5/1/2008

IDRileyCreekLumber HFB1 Wet Biomass Stoker/SlopedGrate/Other Sample #1 4/24/2003 60 1.00 8

IDRileyCreekLumber HFB1 Wet Biomass Stoker/SlopedGrate/Other Sample #2 4/24/2003 60 1.00 8

IDRileyCreekLumber HFB1 Wet Biomass Stoker/SlopedGrate/Other Sample #3 4/24/2003 60 1.00 8

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other Sample #1 5/31/2002

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other Sample #2 5/31/2002

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other Sample #3 5/31/2002

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other Sample #1 5/29/2007

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other Sample #2 5/29/2007

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other Sample #3 5/29/2007

MEBoralexStratton Boiler #1 Wet Biomass Stoker/SlopedGrate/Other Sample #1 10/21/2009 55.6 0.93 6.3

MEBoralexStratton Boiler #1 Wet Biomass Stoker/SlopedGrate/Other Sample #2 10/21/2009 61.3 1.02 5.9

MEBoralexStratton Boiler #1 Wet Biomass Stoker/SlopedGrate/Other Sample #3 10/21/2009 63.5 1.06 5.9

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 7/12/2006

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 7/12/2006

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 7/12/2006

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 9/22/2010

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 9/23/2010

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 9/23/2010

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 9/28/2010

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 9/29/2010

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 9/30/2010

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 8/19/1993 90 1.50 7.1

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 8/19/1993 90 1.50 7.1

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 8/19/1993 90 1.50 7.5

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 8/16/1995 120 2.00 8.3

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 8/16/1995 120 2.00 7.1

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 8/16/1995 120 2.00 6.3

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 8/13/1997 125 2.08 3.6

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 8/13/1997 125 2.08 3.3

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 8/13/1997 125 2.08 3.1

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/16/1999 125 2.08 6.5

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/16/1999 125 2.08 6.3

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/16/1999 125 2.08 6.1

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/5/2003 125 2.08 8.7

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/5/2003 125 2.08 8.3

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/5/2003 125 2.08 8.4

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 1/4/2007

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 1/4/2007

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 1/4/2007

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 7/14/2009 180 3.00 9.74

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 7/14/2009 180 3.00 9.38

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 7/14/2009 180 3.00 9.11

WIDomtar2814 B11, S11 Wet Biomass Stoker/SlopedGrate/Other Sample #1 8/29/2007 60 1.00 7

WIDomtar2814 B11, S11 Wet Biomass Stoker/SlopedGrate/Other Sample #2 8/29/2007 60 1.00 7

WIDomtar2814 B11, S11 Wet Biomass Stoker/SlopedGrate/Other Sample #3 8/29/2007 60 1.00 7

WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other Sample #1 3/24/2005 120 2.00 7.8 YES

WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other Sample #2 3/24/2005 120 2.00 8.1 YES

WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other Sample #3 3/24/2005 120 2.00 8.4 YES

WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other Sample #4 3/24/2005 120 2.00 7.3 YES

AKDoyonUtilities_AK 4 Coal Stoker/SlopedGrate/Other Sample #1 8/17/2005 60 1.00 7

AKDoyonUtilities_AK 4 Coal Stoker/SlopedGrate/Other Sample #2 8/17/2005 60 1.00 6.67

AKDoyonUtilities_AK 4 Coal Stoker/SlopedGrate/Other Sample #3 8/17/2005 60 1.00 6.6

AKDoyonUtilities_AK 7 Coal Stoker/SlopedGrate/Other Sample #1 8/16/2005 60 1.00 7.6

AKDoyonUtilities_AK 7 Coal Stoker/SlopedGrate/Other Sample #2 8/16/2005 60 1.00 7.93

AKDoyonUtilities_AK 7 Coal Stoker/SlopedGrate/Other Sample #3 8/16/2005 60 1.00 8

FLSmurfit-Stone 7PB Coal PC Sample #1 7/11/2007 60 1.00 7.05

FLSmurfit-Stone 7PB Coal PC Sample #2 7/11/2007 60 1.00 7.29

FLSmurfit-Stone 7PB Coal PC Sample #3 7/11/2007 60 1.00 7.41

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #1 6/3/2008 100 1.67 6.9

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #2 6/3/2008 100 1.67 7.9

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #3 6/3/2008 100 1.67 7.9

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #1 8/26/2009 240 4.00 5.58

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #2 8/26/2009 240 4.00 5.56

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #3 8/27/2009 240 4.00 5.66

IAIAStateUnivPowerPlant B1 Coal FB Sample #1 3/26/2008 62.5 1.04 4.3

IAIAStateUnivPowerPlant B1 Coal FB Sample #2 3/26/2008 62.5 1.04 3.9

IAIAStateUnivPowerPlant B1 Coal FB Sample #3 3/26/2008 62.5 1.04 4.4

IAIAStateUnivPowerPlant B2 Coal FB Sample #1 3/27/2008 62.5 1.04 4

IAIAStateUnivPowerPlant B2 Coal FB Sample #2 3/27/2008 62.5 1.04 3.9

IAIAStateUnivPowerPlant B2 Coal FB Sample #3 3/27/2008 62.5 1.04 3.7

IAUofNorthernIowa Boiler #3 Coal PC 4 10/6/2009

IAUofNorthernIowa Boiler #3 Coal PC 5 10/6/2009

IAUofNorthernIowa Boiler #3 Coal PC 6 10/7/2009

IDAmalgamatedSugarCoTwinFalls S-B1 Coal Stoker/SlopedGrate/Other Sample #1 9/26/2006 120 2.00 6.9

IDAmalgamatedSugarCoTwinFalls S-B1 Coal Stoker/SlopedGrate/Other Sample #2 9/26/2006 120 2.00 6.9

IDAmalgamatedSugarCoTwinFalls S-B1 Coal Stoker/SlopedGrate/Other Sample #3 9/26/2006 120 2.00 6

ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other Sample #1 8/22/2007

ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other Sample #2 8/22/2007

ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other Sample #3 8/22/2007

Page 5 of 12

### Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

**Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date Sample** 

**Time**

**(min) Sample** 

**Time (hrs) Stack Oxygen** 

**Concentration**

**(%) Use in** 

**New**

**Source 3x**

**RDL?**

ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other OTM28-1 8/4/2009

ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other OTM28-2 8/5/2009

ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other OTM28-3 8/5/2009

ILRockIslandArsenal NBN 12602 (Boiler #1) Coal Stoker/SlopedGrate/Other Sample #1 3/13/2007

ILRockIslandArsenal NBN 12602 (Boiler #1) Coal Stoker/SlopedGrate/Other Sample #2 3/13/2007

ILRockIslandArsenal NBN 12602 (Boiler #1) Coal Stoker/SlopedGrate/Other Sample #3 3/13/2007

INNotreDame B-4 Coal Stoker/SlopedGrate/Other Sample #1 8/26/2009

INNotreDame B-4 Coal Stoker/SlopedGrate/Other Sample #2 8/26/2009

INNotreDame B-4 Coal Stoker/SlopedGrate/Other Sample #3 8/27/2009

INSABICInnovativePlastics 01-001 BW1 Boiler Coal PC Sample #1 4/7/2005 121 2.02 7

INSABICInnovativePlastics 01-001 BW1 Boiler Coal PC Sample #2 4/7/2005 121 2.02 7

INSABICInnovativePlastics 01-001 BW1 Boiler Coal PC Sample #3 4/7/2005 121 2.02 7

INSABICInnovativePlastics 01-001 BW1 Boiler Coal PC Sample #1 6/28/2006

INSABICInnovativePlastics 01-001 BW1 Boiler Coal PC Sample #2 6/28/2006

INSABICInnovativePlastics 01-001 BW1 Boiler Coal PC Sample #3 6/28/2006

INSABICInnovativePlastics 01-001 BW2 Boiler Coal PC Sample #1 4/7/2005 123 2.05 7

INSABICInnovativePlastics 01-001 BW2 Boiler Coal PC Sample #2 4/7/2005 123 2.05 7

INSABICInnovativePlastics 01-001 BW2 Boiler Coal PC Sample #3 4/7/2005 123 2.05 7

INSABICInnovativePlastics 01-001 BW2 Boiler Coal PC Sample #1 6/28/2006 125 2.08

INSABICInnovativePlastics 01-001 BW2 Boiler Coal PC Sample #2 6/28/2006 125 2.08

INSABICInnovativePlastics 01-001 BW2 Boiler Coal PC Sample #3 6/28/2006 125 2.08

MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #1 10/31/2005 60 1.00 11.5

MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #2 10/31/2005 60 1.00 11.5

MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #3 10/31/2005 60 1.00 11.5

MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #1 11/2/2005

MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #2 11/2/2005

MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #3 11/2/2005

MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #1 11/3/2005

MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #2 11/3/2005

MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #3 11/3/2005

NCEPCORRoxboro 1-A Coal Stoker/SlopedGrate/Other Sample #1 6/16/2008

NCEPCORRoxboro 1-A Coal Stoker/SlopedGrate/Other Sample #2 6/16/2008

NCEPCORRoxboro 1-A Coal Stoker/SlopedGrate/Other Sample #3 6/16/2008

NCEPCORRoxboro 1-B Coal Stoker/SlopedGrate/Other Sample #1 6/16/2008

NCEPCORRoxboro 1-B Coal Stoker/SlopedGrate/Other Sample #2 6/16/2008

NCEPCORRoxboro 1-B Coal Stoker/SlopedGrate/Other Sample #3 6/16/2008

NCEPCORRoxboro 1-C Coal Stoker/SlopedGrate/Other Sample #1 6/16/2008

NCEPCORRoxboro 1-C Coal Stoker/SlopedGrate/Other Sample #2 6/16/2008

NCEPCORRoxboro 1-C Coal Stoker/SlopedGrate/Other Sample #3 6/16/2008

NCHanesDyeWinstonSalem ES B01 Coal Stoker/SlopedGrate/Other Sample #1 3/21/2007

NCHanesDyeWinstonSalem ES B01 Coal Stoker/SlopedGrate/Other Sample #2 3/21/2007

NCHanesDyeWinstonSalem ES B01 Coal Stoker/SlopedGrate/Other Sample #3 3/21/2007

NCHanesDyeWinstonSalem ES B02 Coal Stoker/SlopedGrate/Other Sample #1 3/21/2007

NCHanesDyeWinstonSalem ES B02 Coal Stoker/SlopedGrate/Other Sample #2 3/21/2007

NCHanesDyeWinstonSalem ES B02 Coal Stoker/SlopedGrate/Other Sample #3 3/21/2007

OHMortonSaltRittman B003 - Coal-Fired Boiler #1 Coal Stoker/SlopedGrate/Other Sample #1 8/21/2007

OHMortonSaltRittman B003 - Coal-Fired Boiler #1 Coal Stoker/SlopedGrate/Other Sample #2 8/21/2007

OHMortonSaltRittman B003 - Coal-Fired Boiler #1 Coal Stoker/SlopedGrate/Other Sample #3 8/21/2007

OHSmartPapersHoldingsLLC B010 Coal PC Sample #1 8/11/2005 120 2.00 7.9

OHSmartPapersHoldingsLLC B010 Coal PC Sample #2 8/11/2005 120 2.00 7.8

OHSmartPapersHoldingsLLC B010 Coal PC Sample #3 8/11/2005 120 2.00 7.8

OHSmartPapersHoldingsLLC B020 Coal Stoker/SlopedGrate/Other Sample #1 9/22/2005

OHSmartPapersHoldingsLLC B020 Coal Stoker/SlopedGrate/Other Sample #2 9/22/2005

OHSmartPapersHoldingsLLC B020 Coal Stoker/SlopedGrate/Other Sample #3 9/22/2005

OHUofCincinnati B108 Coal Stoker/SlopedGrate/Other Sample #3 4/27/2005

OHUofCincinnati B108 Coal Stoker/SlopedGrate/Other Sample #1 4/26/2006

OHUofCincinnati B108 Coal Stoker/SlopedGrate/Other Sample #2 4/26/2006

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #1 10/24/2000 60 1.00 6

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #2 10/24/2000 60 1.00 6.1

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #3 10/24/2000 60 1.00 5.9

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #1 10/9/2002 60 1.00 6.1

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #2 10/9/2002 60 1.00 3.1

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #3 10/9/2002 60 1.00 5.8

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #1 10/19/2004 60 1.00 5.6

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #2 10/19/2004 60 1.00 5.9

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #3 10/19/2004 60 1.00 5.4

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #1 10/25/2006 60 1.00 3.2

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #2 10/25/2006 60 1.00 3.6

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #3 10/25/2006 60 1.00 3.8

TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other Sample #1 7/17/2007 60 1.00 12.4

TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other Sample #2 7/17/2007 60 1.00 12.2

TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other Sample #3 7/17/2007 60 1.00 11.9

TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other 1 8/5/2009 240 4.00 10.84

TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other 3 8/6/2009 240 4.00 10.25

TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other 2 11/6/2009 240 4.00 10.31

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #1 8/20/1996 64 1.07

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #2 8/20/1996 64 1.07

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #3 8/20/1996 64 1.07

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #1 8/8/2000 64 1.07 7

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #2 8/8/2000 64 1.07 7

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #3 8/8/2000 64 1.07 7

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #2 6/29/2004 60 1.00 7

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #3 6/29/2004 60 1.00 7

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #1 11/9/2004 120 2.00

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #2 11/9/2004 120 2.00

Page 6 of 12

### Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

**Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date Sample** 

**Time**

**(min) Sample** 

**Time (hrs) Stack Oxygen** 

**Concentration**

**(%) Use in** 

**New**

**Source 3x**

**RDL?**

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #1 11/10/2004 120 2.00

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #2 11/10/2004 120 2.00

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #3 11/10/2004 120 2.00

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #3 11/11/2004 120 2.00

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #1 7/24/2008 60 1.00 7

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #2 7/24/2008 60 1.00 7

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #3 7/24/2008 60 1.00 7

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #1 7/12/1993 64 1.07 7

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #2 7/12/1993 64 1.07 7

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #3 7/12/1993 64 1.07 7

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #1 9/30/1997 64 1.07 7

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #2 9/30/1997 64 1.07 7

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #3 9/30/1997 64 1.07 7

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #1 8/14/2001 60 1.00 7

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #2 8/14/2001 60 1.00 7

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #3 8/14/2001 60 1.00 7

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #1 6/21/2005

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #2 6/21/2005

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #3 6/21/2005

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #1 7/12/1993 64 1.07 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #2 7/12/1993 64 1.07 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #3 7/12/1993 64 1.07 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #1 9/25/1997 64 1.07 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #2 9/25/1997 64 1.07 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #3 9/25/1997 64 1.07 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #1 8/28/2001 60 1.00 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #2 8/28/2001 60 1.00 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #3 8/28/2001 60 1.00 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #1 3/9/2005 120 2.00

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #2 3/9/2005 120 2.00

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #3 3/9/2005 120 2.00

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #1 3/10/2005 120 2.00

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #2 3/10/2005 120 2.00

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #3 3/10/2005 120 2.00

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #1 5/17/2005 60 1.00 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #2 5/17/2005 60 1.00 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #3 5/17/2005 60 1.00 7

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #1 7/29/1994

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #2 7/29/1994

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #3 7/29/1994

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #1 7/7/1998

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #2 7/7/1998

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #3 7/7/1998

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #1 6/6/2002

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #2 6/6/2002

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #3 6/6/2002

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #1 8/22/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #2 8/22/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #3 8/22/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #1 11/8/1994 75 1.25 7

TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #2 11/8/1994 75 1.25 7

TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #3 11/8/1994 75 1.25 7

TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #1 9/19/2002 60 1.00 7

TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #2 9/19/2002 60 1.00 7

TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #3 9/19/2002 60 1.00 7

TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #1 9/19/2006 60 1.00 7

TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #2 9/19/2006 60 1.00 7

TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #3 9/19/2006 60 1.00 7

TNEastman_NO_CBIDATA Boiler 30 Coal PC 1 8/26/2009

TNEastman_NO_CBIDATA Boiler 30 Coal PC 2 8/27/2009

TNEastman_NO_CBIDATA Boiler 30 Coal PC 3 8/27/2009

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #1 8/4/1994 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #2 8/4/1994 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #3 8/4/1994 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #1 12/14/1994 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #2 12/15/1994 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #3 12/15/1994 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #1 9/29/1998 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #2 9/29/1998 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #3 9/29/1998 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #1 7/25/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #2 7/25/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #3 7/25/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #1 8/14/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #2 8/14/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #3 8/14/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #1 12/6/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #2 12/6/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #3 12/6/2006 125 2.08 7

VADukeEnergyNarrows Boiler #2 Coal PC Sample #1 10/12/2004

VADukeEnergyNarrows Boiler #2 Coal PC Sample #1 10/12/2004

VADukeEnergyNarrows Boiler #2 Coal PC Sample #2 10/12/2004

VADukeEnergyNarrows Boiler #2 Coal PC Sample #2 10/12/2004

VADukeEnergyNarrows Boiler #2 Coal PC Sample #3 10/12/2004

VADukeEnergyNarrows Boiler #2 Coal PC Sample #3 10/12/2004

Page 7 of 12

### Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

**Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date Sample** 

**Time**

**(min) Sample** 

**Time (hrs) Stack Oxygen** 

**Concentration**

**(%) Use in** 

**New**

**Source 3x**

**RDL?**

VADukeEnergyNarrows Boiler #3 Coal PC Sample #1 4/14/2004

VADukeEnergyNarrows Boiler #3 Coal PC Sample #2 4/14/2004

VADukeEnergyNarrows Boiler #3 Coal PC Sample #3 4/14/2004

VADukeEnergyNarrows Boiler #3 Coal PC Sample #1 10/14/2004

VADukeEnergyNarrows Boiler #3 Coal PC Sample #2 10/14/2004

VADukeEnergyNarrows Boiler #3 Coal PC Sample #3 10/14/2004

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #1 2/3/2004

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #2 2/3/2004

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #3 2/3/2004

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #1 5/24/2005

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #2 5/24/2005

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #3 5/24/2005

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #1 7/13/2006

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #2 7/13/2006

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #3 7/13/2006

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #1 5/1/2007 120 2.00

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #2 5/1/2007 120 2.00

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #3 5/1/2007 120 2.00

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #1 9/9/2008

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #2 9/9/2008

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #3 9/9/2008

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #1 3/30/2009

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #2 3/30/2009

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #3 3/30/2009

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #1 4/8/2009

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #2 4/8/2009

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #3 4/8/2009

VAUniversityofVirginia 7103-1-05 Coal Stoker/SlopedGrate/Other Sample #1 4/4/2008 60 1.00 6.8

VAUniversityofVirginia 7103-1-05 Coal Stoker/SlopedGrate/Other Sample #2 4/4/2008 60 1.00 7.5

VAUniversityofVirginia 7103-1-05 Coal Stoker/SlopedGrate/Other Sample #3 4/4/2008 60 1.00 8.5

VAUniversityofVirginia 7103-1-01R Coal Stoker/SlopedGrate/Other Sample #1 12/6/2007 60 1.00 7.07

VAUniversityofVirginia 7103-1-01R Coal Stoker/SlopedGrate/Other Sample #2 12/6/2007 60 1.00 7.09

VAUniversityofVirginia 7103-1-01R Coal Stoker/SlopedGrate/Other Sample #3 12/6/2007 60 1.00 6.98

VAUniversityofVirginia 7103-1-01R Coal Stoker/SlopedGrate/Other M027-1 9/17/2009 240 4.00

VAUniversityofVirginia 7103-1-01R Coal Stoker/SlopedGrate/Other M027-2 9/17/2009 240 4.00

VAUniversityofVirginia 7103-1-01R Coal Stoker/SlopedGrate/Other M027-3 9/18/2009 240 4.00

VAUniversityofVirginia 7103-1-02R Coal Stoker/SlopedGrate/Other Sample #1 1/16/2007 60 1.00 6.64

VAUniversityofVirginia 7103-1-02R Coal Stoker/SlopedGrate/Other Sample #2 1/16/2007 60 1.00 6.96

VAUniversityofVirginia 7103-1-02R Coal Stoker/SlopedGrate/Other Sample #3 1/16/2007 60 1.00 6.74

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 10/27/1992 120 2.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 10/27/1992 120 2.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 10/27/1992 120 2.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 9/24/1994 120 2.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 9/24/1994 120 2.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 9/24/1994 120 2.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 7/28/1998 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 7/28/1998 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 7/28/1998 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 11/9/1999

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 11/9/1999

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 11/9/1999

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 2/2/2000 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 2/2/2000 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 2/2/2000 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 7/19/2000 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 7/19/2000 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 7/19/2000 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 8/29/2000 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 8/29/2000 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 8/29/2000 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 8/28/2002 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 8/28/2002 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 8/28/2002 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 8/10/2004 60 1.00 6

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 8/10/2004 60 1.00 6

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 8/10/2004 60 1.00 6

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 9/21/2007

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 9/21/2007

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 9/21/2007

WINewPageBiron B24 Coal Stoker/SlopedGrate/Other Sample #1 9/12/2007 60 1.00

WINewPageBiron B24 Coal Stoker/SlopedGrate/Other Sample #2 9/12/2007 60 1.00

WINewPageBiron B24 Coal Stoker/SlopedGrate/Other Sample #3 9/12/2007 60 1.00

WINewPageBiron B24 Coal Stoker/SlopedGrate/Other 1 9/22/2009 240 4.00

WINewPageBiron B24 Coal Stoker/SlopedGrate/Other 2 9/22/2009 240 4.00

WINewPageBiron B24 Coal Stoker/SlopedGrate/Other 3 9/23/2009 240 4.00

WIThilmanyPapersNicoletMill B23 Coal Stoker/SlopedGrate/Other Sample #1 2/22/2006 60 1.00

WIThilmanyPapersNicoletMill B23 Coal Stoker/SlopedGrate/Other Sample #2 2/22/2006 60 1.00

WIThilmanyPapersNicoletMill B23 Coal Stoker/SlopedGrate/Other Sample #3 2/22/2006 60 1.00

WIThilmanyPapersNicoletMill B24 Coal Stoker/SlopedGrate/Other Sample #1 2/22/2006 60 1.00

WIThilmanyPapersNicoletMill B24 Coal Stoker/SlopedGrate/Other Sample #2 2/22/2006 60 1.00

WIThilmanyPapersNicoletMill B24 Coal Stoker/SlopedGrate/Other Sample #3 2/22/2006 60 1.00

WIWausau # 5 Power Boiler (B24) Coal Stoker/SlopedGrate/Other Sample #1 7/24/2007 60 1.00

WIWausau # 5 Power Boiler (B24) Coal Stoker/SlopedGrate/Other Sample #2 7/24/2007 60 1.00

WIWausau # 5 Power Boiler (B24) Coal Stoker/SlopedGrate/Other Sample #3 7/24/2007 60 1.00

MNGPDuluth EU33 Boiler #3 Heavy Liquid N/A 1 9/10/2009

Page 8 of 12

### Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

**Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date Sample** 

**Time**

**(min) Sample** 

**Time (hrs) Stack Oxygen** 

**Concentration**

**(%) Use in** 

**New**

**Source 3x**

**RDL?**

MNGPDuluth EU33 Boiler #3 Heavy Liquid N/A 2 9/10/2009

MNGPDuluth EU33 Boiler #3 Heavy Liquid N/A 3 9/10/2009

NYConEd59thStStationNewYork Boiler 118 Heavy Liquid N/A M5-1 8/19/2009

NYConEd59thStStationNewYork Boiler 118 Heavy Liquid N/A M5-2 8/19/2009

NYConEd59thStStationNewYork Boiler 118 Heavy Liquid N/A M5-3 8/19/2009

PABoeingRidleyPark 033 Heavy Liquid N/A M29-1 9/22/2009

PABoeingRidleyPark 033 Heavy Liquid N/A M29-2 9/23/2009

PABoeingRidleyPark 033 Heavy Liquid N/A M29-3 9/24/2009

SCMilliken-Dewey D30 Heavy Liquid N/A Sample #1 8/12/2009 180 3.00 3.83

SCMilliken-Dewey D30 Heavy Liquid N/A Sample #2 8/12/2009 180 3.00 4.02

SCMilliken-Dewey D30 Heavy Liquid N/A Sample #3 8/12/2009 180 3.00 3.96

ALBP-Decatur24 AB-8301 Light Liquid N/A Sample #1 1/24/2001

ALBP-Decatur24 AB-8301 Light Liquid N/A Sample #2 1/24/2001

ALBP-Decatur24 AB-8301 Light Liquid N/A Sample #3 1/24/2001

SCGPChemRussellville FO Boiler Light Liquid N/A Sample #1 8/26/2009 120 2.00 8.06

SCGPChemRussellville FO Boiler Light Liquid N/A Sample #2 8/26/2009 120 2.00 7.26

SCGPChemRussellville FO Boiler Light Liquid N/A Sample #3 8/26/2009 120 2.00 7.31

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Light Liquid N/A 1 11/17/2009 216 3.60 YES

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Light Liquid N/A 2 11/17/2009 216 3.60 YES

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Light Liquid N/A 3 11/18/2009 216 3.60 YES

HITesoro SG1102 Non-Continental Liquid N/A Sample #1 10/9/2010 60 1.00 4.89 YES

HITesoro SG1102 Non-Continental Liquid N/A Sample #2 10/9/2010 60 1.00 5.19 YES

HITesoro SG1102 Non-Continental Liquid N/A Sample #3 10/9/2010 60 1.00 5.29 YES

HITesoro SG1102 Non-Continental Liquid N/A Sample #1 12/13/2010 192 3.20 6.3 YES

HITesoro SG1102 Non-Continental Liquid N/A Sample #2 12/13/2010 192 3.20 6.42 YES

HITesoro SG1102 Non-Continental Liquid N/A Sample #3 12/13/2010 192 3.20 6.77 YES

WVMountainStateCarbonFollansbee S1 Process Gas N/A Sample #1 10/19/2009 240 4.00 4.5 YES

WVMountainStateCarbonFollansbee S1 Process Gas N/A Sample #2 10/19/2009 240 4.00 4.7 YES

WVMountainStateCarbonFollansbee S1 Process Gas N/A Sample #3 10/20/2009 240 4.00 4.8 YES

ALBP-Decatur24 AB-8301 Light Liquid N/A 1 1/24/2001 120 2.00 4

ALBP-Decatur24 AB-8301 Light Liquid N/A 2 1/24/2001 120 4.4

ALBP-Decatur24 AB-8301 Light Liquid N/A 3 1/24/2001 120 4.2

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 1 12/12/2007 60 10.7

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 12/12/2007 60 9.9

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 12/12/2007 60 10

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 1 12/12/2007 60 9.8

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 12/12/2007 60 9.6

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 12/12/2007 60 9.8

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 1 6/14/2011 60 7.31

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 6/14/2011 60 8.02

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 6/14/2011 60 6.78

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 1 6/14/2011 60 7.44

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 6/14/2011 60 7.77

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 6/14/2011 60 7.67

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 1 6/24/2009 60 5.9

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 6/24/2009 60 7.1

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 6/24/2009 60 9.2

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 1 6/24/2009 60 6.1

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 6/24/2009 60 7.5

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 6/24/2009 60 9

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 1 7/11/2008 60 6.9

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 7/11/2008 60 6.3

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 7/11/2008 60 5.8

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 1 7/11/2008 60 6.4

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 7/11/2008 60 5.9

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 7/11/2008 60 6.1

ALIPCourtland No. 3 Combination Boier / 11Cu301 Biomass FB 1 7/7/2009 240 11.3

ALIPCourtland No. 3 Combination Boier / 11Cu301 Biomass FB 2 7/7/2009 240 11.4

ALIPCourtland No. 3 Combination Boier / 11Cu301 Biomass FB 3 7/7/2009 240 11.5

ARLeolaLumberMill SN-01A Wet Biomass Stoker/SlopedGrate/Other 1 6/14/2006 120 9.8

ARLeolaLumberMill SN-01A Wet Biomass Stoker/SlopedGrate/Other 2 6/14/2006 120 10.2

ARLeolaLumberMill SN-01A Wet Biomass Stoker/SlopedGrate/Other 3 6/14/2006 120 10

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 1 12/4/2002 60 11.51

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 2 12/4/2002 60 11.68

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 3 12/4/2002 60 11.56

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 1 12/4/2003 60 10.74

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 2 12/4/2003 60 10.65

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 3 12/4/2003 60 10.35

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 1 8/11/1997 60 9

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 2 8/11/1997 60 9

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 3 8/11/1997 60 9

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 1 9/29/2004 60 9.6

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 2 9/29/2004 60 10.17

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 3 9/29/2004 60 9.94

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner 1 8/7/1997 120 6.7 YES

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner 2 8/7/1997 120 6.4 YES

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner 3 8/7/1997 120 6.4 YES

CASierraPacificLincoln McBurney Boiler Wet Biomass Stoker/SlopedGrate/Other 1 3/11/2008 ? 3.277

CASierraPacificLincoln McBurney Boiler Wet Biomass Stoker/SlopedGrate/Other 2 3/11/2008 ? 3.71

CASierraPacificLincoln McBurney Boiler Wet Biomass Stoker/SlopedGrate/Other 3 3/11/2008 ? 2.42

CASierraPacificLincoln McBurney Boiler Wet Biomass Stoker/SlopedGrate/Other 1 3/5/2008 ? 2.208

CASierraPacificLincoln McBurney Boiler Wet Biomass Stoker/SlopedGrate/Other 2 3/5/2008 ? 3.085

CASierraPacificLincoln McBurney Boiler Wet Biomass Stoker/SlopedGrate/Other 3 3/5/2008 ? 2.565

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate 1 1/18/2001 60 10.74

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate 2 1/18/2001 60 11.05

Page 9 of 12

### Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

**Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date Sample** 

**Time**

**(min) Sample** 

**Time (hrs) Stack Oxygen** 

**Concentration**

**(%) Use in** 

**New**

**Source 3x**

**RDL?**

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate 3 1/18/2001 60 10.76

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 12/30/2003 60 6.36

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 2 12/30/2003 60 6.99

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 3 12/30/2003 60 6.58

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 1/24/2008 60 7.18

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 2 1/24/2008 60 6.77

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 3 1/24/2008 60 6.84

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 1/25/2007 60 10.56

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 2 1/25/2007 60 9.78

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 3 1/25/2007 60 10.71

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 1/31/2000 60 6.14

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 3 1/31/2000 60 5.98

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 4 1/31/2000 60 5.78

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 1/5/2001 60 9.08

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 2 1/5/2001 60 8.98

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 4 1/5/2001 60 8.98

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 1/5/2006 60 9.78

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 2 1/5/2006 60 8.8

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 3 1/5/2006 60 8.76

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 1/9/2002 60 6.67

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 2 1/9/2002 60 6.43

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 3 1/9/2002 60 6.41

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 11/15/2002 60 6.56

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 2 11/15/2002 60 7.65

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 3 11/15/2002 60 7.96

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 12/17/1999 60 3.6

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 2 12/17/1999 60 4.8

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 3 12/17/1999 60 4.9

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 2/4/2005 60 10.72

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 2 2/4/2005 60 10.8

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 3 2/4/2005 60 11.28

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 2/8/1999 60 6.4

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 2 2/8/1999 60 7.5

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 3 2/8/1999 60 7.5

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate 1 1/10/2006 ? ?

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate 2 1/10/2006 ? ?

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate 3 1/10/2006 ? ?

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate 1 11/29/2007 ? ?

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate 2 11/29/2007 ? ?

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate 3 11/29/2007 ? ?

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 1 8/27/2009 60 7.01 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 2 8/27/2009 60 7.92 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 3 8/27/2009 60 7.58 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 4 8/27/2009 60 6.93 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 5 8/27/2009 60 6.73 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 6 8/27/2009 60 8.24 YES

GATempleInlandRome WF Biomass FB 1 7/27/2009 204 5.1 YES

GATempleInlandRome WF Biomass FB 2 7/27/2009 204 5 YES

GATempleInlandRome WF Biomass FB 3 7/27/2009 204 5.2 YES

HITesoro SG1102 Non-Continental Liquid N/A 1 60 4.89 YES

HITesoro SG1102 Non-Continental Liquid N/A 2 60 5.19 YES

HITesoro SG1102 Non-Continental Liquid N/A 3 60 5.29 YES

HITesoro SG1102 Non-Continental Liquid N/A 1 64 6.9 YES

HITesoro SG1102 Non-Continental Liquid N/A 2 64 7 YES

HITesoro SG1102 Non-Continental Liquid N/A 3 64 6.9 YES

IAUofIowa EP7 Boiler 11 Coal FB 1 2/15/2006 60 4.7

IAUofIowa EP7 Boiler 11 Coal FB 2 2/15/2006 60 4.4

IAUofIowa EP7 Boiler 11 Coal FB 3 2/15/2006 60 4.4

IAUofIowa EP7 Boiler 11 Coal FB 1 2/22/2006 60 7.2

IAUofIowa EP7 Boiler 11 Coal FB 2 2/22/2006 60 7.2

IAUofIowa EP7 Boiler 11 Coal FB 3 2/22/2006 60 7.2

IAUofIowa EP7 Boiler 11 Coal FB 2 8/4/2009 240 5

IAUofIowa EP7 Boiler 11 Coal FB 3 8/4/2009 240 4.7

IAUofIowa EP7 Boiler 11 Coal FB 4 8/4/2009 240 4.8

IDPotlatch PB-1 CE Biomass Fuel Cell 1 4/30/2008 60 11.79

IDPotlatch PB-1 CE Biomass Fuel Cell 2 4/30/2008 60 11.65

IDPotlatch PB-1 CE Biomass Fuel Cell 3 4/30/2008 60 11.53

IDPotlatch PB-2 Riley Wet Biomass Stoker/SlopedGrate/Other 1 5/1/2008 60 8.78

IDPotlatch PB-2 Riley Wet Biomass Stoker/SlopedGrate/Other 2 5/1/2008 60 9.08

IDPotlatch PB-2 Riley Wet Biomass Stoker/SlopedGrate/Other 3 5/1/2008 60 7.82

ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other 1 8/4/2009 240 9.985

ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other 2 8/4/2009 240 10.16

ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other 3 8/4/2009 240 10.179

ILPolyOne B1 Coal Stoker/SlopedGrate/Other 1 11/14/2006 120 7.3

ILPolyOne B1 Coal Stoker/SlopedGrate/Other 2 11/14/2006 120 7.6

ILPolyOne B1 Coal Stoker/SlopedGrate/Other 3 11/14/2006 120 7.7

ILRockIslandArsenal NBN 12602 (Boiler #1) Coal Stoker/SlopedGrate/Other 1 3/13/2007 60 9.7

ILRockIslandArsenal NBN 12602 (Boiler #1) Coal Stoker/SlopedGrate/Other 2 3/13/2007 60 8.3

ILRockIslandArsenal NBN 12602 (Boiler #1) Coal Stoker/SlopedGrate/Other 3 3/13/2007 60 8

INNotreDame B-4 Coal Stoker/SlopedGrate/Other 1 240 5.7

INNotreDame B-4 Coal Stoker/SlopedGrate/Other 2 240 5.6

INNotreDame B-4 Coal Stoker/SlopedGrate/Other 3 240 5.6

MENewPage-Rumford Cogen#6 Wet Biomass Stoker/SlopedGrate/Other 1 9/6/2007 60 10

MENewPage-Rumford Cogen#6 Wet Biomass Stoker/SlopedGrate/Other 2 9/6/2007 60 10

MENewPage-Rumford Cogen#6 Wet Biomass Stoker/SlopedGrate/Other 3 9/6/2007 60 10

Page 10 of 12

### Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

**Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date Sample** 

**Time**

**(min) Sample** 

**Time (hrs) Stack Oxygen** 

**Concentration**

**(%) Use in** 

**New**

**Source 3x**

**RDL?**

MENewPage-Rumford Cogen#7 Wet Biomass Stoker/SlopedGrate/Other 1 9/6/2007 60 10

MENewPage-Rumford Cogen#7 Wet Biomass Stoker/SlopedGrate/Other 2 9/6/2007 60 10

MENewPage-Rumford Cogen#7 Wet Biomass Stoker/SlopedGrate/Other 3 9/6/2007 60 10

MESDWarren #21 Boiler Wet Biomass Stoker/SlopedGrate/Other 1 11/10/2006 60 5.4

MESDWarren #21 Boiler Wet Biomass Stoker/SlopedGrate/Other 2 11/10/2006 60 5.2

MESDWarren #21 Boiler Wet Biomass Stoker/SlopedGrate/Other 3 11/10/2006 60 5.6

MNGPDuluth EU33 Boiler #3 Heavy Liquid N/A 1 9/10/2009 180 16.6 YES

MNGPDuluth EU33 Boiler #3 Heavy Liquid N/A 2 9/10/2009 180 16.3 YES

MNGPDuluth EU33 Boiler #3 Heavy Liquid N/A 3 9/10/2009 180 16 YES

MNWeyerhaeuserIronton EU 001 - 4 Cell Furnace Biomass Fuel Cell 1 12/20/2006 60 12.6

MNWeyerhaeuserIronton EU 001 - 4 Cell Furnace Biomass Fuel Cell 2 12/20/2006 60 12.5

MNWeyerhaeuserIronton EU 001 - 4 Cell Furnace Biomass Fuel Cell 3 12/20/2006 60 12.4

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 1 7/12/2006 90 10.2

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 7/12/2006 90 11.2

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 7/12/2006 90 12

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 9/22/2010 240 8.8

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 9/22/2010 240 8.3

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 4 9/22/2010 240 7.8

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 1 9/28/2010 240 12.4

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 9/28/2010 240 12.3

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 9/28/2010 240 10.7

MSNorbordMS Wellons No. 1 Biomass Fuel Cell 1 8/1/2007 60 14.21

MSNorbordMS Wellons No. 1 Biomass Fuel Cell 2 8/1/2007 60 14.56

MSNorbordMS Wellons No. 1 Biomass Fuel Cell 3 8/1/2007 60 14.12

MSNorbordMS Wellons No. 2 Biomass Fuel Cell 1 8/1/2007 60 14.21

MSNorbordMS Wellons No. 2 Biomass Fuel Cell 2 8/1/2007 60 14.56

MSNorbordMS Wellons No. 2 Biomass Fuel Cell 3 8/1/2007 60 14.12

MSNorbordMS Wellons No. 3 Biomass Fuel Cell 1 8/1/2007 60 14.21

MSNorbordMS Wellons No. 3 Biomass Fuel Cell 2 8/1/2007 60 14.56

MSNorbordMS Wellons No. 3 Biomass Fuel Cell 3 8/1/2007 60 14.12

NYConEd59thStStationNewYork Boiler 118 Heavy Liquid N/A 1 250 7.6

NYConEd59thStStationNewYork Boiler 118 Heavy Liquid N/A 2 250 7.4

NYConEd59thStStationNewYork Boiler 118 Heavy Liquid N/A 3 250 7.4

OHSauderWoodArchbold B009 Biomass Suspension Burner 1 60 9.45

OHSauderWoodArchbold B009 Biomass Suspension Burner 2 60 9.45

OHSauderWoodArchbold B009 Biomass Suspension Burner 3 60 9.79

OHSmartPapersHoldingsLLC B020 Coal Stoker/SlopedGrate/Other 1 9/22/2005 120 9.1

OHSmartPapersHoldingsLLC B020 Coal Stoker/SlopedGrate/Other 2 9/22/2005 120 9.4

OHSmartPapersHoldingsLLC B020 Coal Stoker/SlopedGrate/Other 3 9/22/2005 120 8.9

ORGeorgiaPacificWaunaMill EU35 - Fluidized Bed Boiler Biomass FB 1 3/22/2006 120 8.24

ORGeorgiaPacificWaunaMill EU35 - Fluidized Bed Boiler Biomass FB 2 3/22/2006 120 8.22

ORGeorgiaPacificWaunaMill EU35 - Fluidized Bed Boiler Biomass FB 3 3/22/2006 120 8.22

PABoeingRidleyPark 033 Heavy Liquid N/A 1 9/22/2009 240 5.4

PABoeingRidleyPark 033 Heavy Liquid N/A 2 9/22/2009 240 5.5

PABoeingRidleyPark 033 Heavy Liquid N/A 3 9/22/2009 240 6.8

SCCogenSouth B002 - Auxiliary Boiler #1 Heavy Liquid N/A 1 11/14/2006 120 4

SCCogenSouth B002 - Auxiliary Boiler #1 Heavy Liquid N/A 2 11/14/2006 120 1.5

SCCogenSouth B002 - Auxiliary Boiler #1 Heavy Liquid N/A 3 11/14/2006 120 4.5

SCCogenSouth B002 - Auxiliary Boiler #1 Heavy Liquid N/A 1 11/30/2004 60 5.4

SCCogenSouth B002 - Auxiliary Boiler #1 Heavy Liquid N/A 2 11/30/2004 60 5.4

SCCogenSouth B002 - Auxiliary Boiler #1 Heavy Liquid N/A 3 11/30/2004 60 5.4

SCCogenSouth B003 - Auxiliary Boiler #2 Heavy Liquid N/A 1 11/14/2006 120 4

SCCogenSouth B003 - Auxiliary Boiler #2 Heavy Liquid N/A 2 11/14/2006 120 1.5

SCCogenSouth B003 - Auxiliary Boiler #2 Heavy Liquid N/A 3 11/14/2006 120 4.5

SCCogenSouth B003 - Auxiliary Boiler #2 Heavy Liquid N/A 1 11/30/2004 60 5.4

SCCogenSouth B003 - Auxiliary Boiler #2 Heavy Liquid N/A 2 11/30/2004 60 5.4

SCCogenSouth B003 - Auxiliary Boiler #2 Heavy Liquid N/A 3 11/30/2004 60 5.4

SCCogenSouth B004 - Auxiliary Boiler #3 Heavy Liquid N/A 1 11/14/2006 120 4

SCCogenSouth B004 - Auxiliary Boiler #3 Heavy Liquid N/A 2 11/14/2006 120 1.5

SCCogenSouth B004 - Auxiliary Boiler #3 Heavy Liquid N/A 3 11/14/2006 120 4.5

SCCogenSouth B004 - Auxiliary Boiler #3 Heavy Liquid N/A 1 11/30/2004 60 5.4

SCCogenSouth B004 - Auxiliary Boiler #3 Heavy Liquid N/A 2 11/30/2004 60 5.4

SCCogenSouth B004 - Auxiliary Boiler #3 Heavy Liquid N/A 3 11/30/2004 60 5.4

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other 1 1/26/2005 120 5.37

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other 2 1/26/2005 120 6.56

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other 3 1/26/2005 120 6.89

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other 1 1/4/2007 120 8.5

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other 2 1/4/2007 120 8.45

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other 3 1/4/2007 120 7.8

SCMitsubishiPolyesterFilm Dowtherm Heater 4 (4FPDDOWHSA) Heavy Liquid N/A 1 7/23/2009 125 8

SCMitsubishiPolyesterFilm Dowtherm Heater 4 (4FPDDOWHSA) Heavy Liquid N/A 2 7/23/2009 125 8

SCMitsubishiPolyesterFilm Dowtherm Heater 4 (4FPDDOWHSA) Heavy Liquid N/A 3 7/23/2009 125 8

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 1 10/6/2005 120 5.6

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 2 10/6/2005 120 5.5

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 3 10/6/2005 120 5.7

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 1 120 4.75

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 2 120 5.1

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 3 120 5.2

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 1 8/4/2009 208 6.6

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 2 8/4/2009 208 7

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 3 8/4/2009 208 6.8

TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other 1 11/6/2009 ? ?

TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other 2 11/6/2009 ? ?

TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other 3 11/6/2009 ? ?

TXRGVSG Boiler No. 6 Biomass Suspension/Grate 2 1/13/2009 120 6.6 YES

Page 11 of 12

### Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

**Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date Sample** 

**Time**

**(min) Sample** 

**Time (hrs) Stack Oxygen** 

**Concentration**

**(%) Use in** 

**New**

**Source 3x**

**RDL?**

TXRGVSG Boiler No. 6 Biomass Suspension/Grate 3 1/13/2009 120 7 YES

TXRGVSG Boiler No. 6 Biomass Suspension/Grate 4 1/13/2009 120 6.8 YES

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB 1 9/21/2007 60 9.4

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB 2 9/21/2007 60 9.4

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB 3 9/21/2007 60 9.8

WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other 1 3/24/2005 120 7.8

WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other 2 3/24/2005 120 8.1

WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other 3 3/24/2005 120 8.4

WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other 4 3/24/2005 120 7.3

WVGPMtHopeOSB 5600 - Wellons Energy System Biomass Dutch Oven/Pile Burner 1 7/11/2006 120 16.26

WVGPMtHopeOSB 5600 - Wellons Energy System Biomass Dutch Oven/Pile Burner 2 7/11/2006 120 17.1

WVGPMtHopeOSB 5600 - Wellons Energy System Biomass Dutch Oven/Pile Burner 3 7/11/2006 120 17.26

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other 1 7/13/2010 60 10.01

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other 2 7/13/2010 60 9.74

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other 4 7/13/2010 60 10.2

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other 1 5/5/2010 50 8.8

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other 2 5/5/2010 50 9.05

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other 3 5/5/2010 50 9.25

OKGPMuskogeeMill B-2 Coal PC 1 9/27/2010 240 8.1

OKGPMuskogeeMill B-2 Coal PC 2 9/28/2010 240 9.8

OKGPMuskogeeMill B-2 Coal PC 3 9/28/2010 240 9.4

OKGPMuskogeeMill B-2 Coal PC 1 10/1/2010 240 8.1

OKGPMuskogeeMill B-2 Coal PC 2 10/1/2010 240 8.1

OKGPMuskogeeMill B-2 Coal PC 3 10/2/2010 240 7.8

OKGPMuskogeeMill B-3 Coal PC 1 9/29/2010 240 7.2

OKGPMuskogeeMill B-3 Coal PC 2 9/29/2010 240 7

OKGPMuskogeeMill B-3 Coal PC 3 9/30/2010 240 7.2

OKGPMuskogeeMill B-4 Coal PC 1 10/5/2010 240 6.5

OKGPMuskogeeMill B-4 Coal PC 2 10/5/2010 240 6.3

OKGPMuskogeeMill B-4 Coal PC 3 10/6/2010 240 6.5

HITesoro SG1102 Non-Continental Liquid N/A 1 1/26/2012 60 4.21 YES

HITesoro SG1102 Non-Continental Liquid N/A 2 1/26/2012 60 4.24 YES

HITesoro SG1102 Non-Continental Liquid N/A 3 1/26/2012 60 4.27 YES

HITesoro H101B Non-Continental Liquid N/A 1 1/25/2012 60 6.53

HITesoro H101B Non-Continental Liquid N/A 2 1/25/2012 60 6.62

HITesoro H101B Non-Continental Liquid N/A 3 1/25/2012 60 6.75

Page 12 of 12**Table C-2a: Summary of PM 3x RDL for Existing Sources Fuel Category Combustor Design Average Sample Time (hrs)** **3x RDL (μg/dscm)** **F d** **Factor for Subcategory** **(dscf/MMBtu) Average Stack Oxygen** **Concentration (%) 3x RDL** **(lb/MMBtu)**Coal N/A23.00E+039,7807.11**2.77E-03**Dutch Oven/Pile Burner23.00E+039,4209.22**3.15E-03**FB32.00E+039,4207.02**1.77E-03**Fuel Cell23.00E+039,42013.40**4.90E-03**Suspension Burner16.00E+039,2409.55**6.36E-03**Suspension/Grate16.00E+039,4207.90**5.67E-03**Wet Biomass Stoker/Other16.00E+039,4208.05**5.73E-03**Dry Biomass Stoker/Other23.00E+039,2407.90**2.78E-03**Heavy Liquid N/A23.00E+039,1906.16**2.44E-03**Light Liquid N/A32.00E+039,1905.87**1.59E-03**Non-Continental Liquid N/A1 6.00E+03 9,190 5.76**4.75E-03**Process Gas N/A41.50E+038,7104.67**1.05E-03 Table C-2b: Summary of PM 3x RDL for New Sources** **Fuel Category Combustor Design Average Sample Time (hrs) 3x RDL** **(μg/dscm) F** **d Factor for** **Subcategory (dscf/MMBtu)** **Average Stack Oxygen Concentration (%)** **3x RDL (lb/MMBtu)** Coal N/A41.50E+039,7807.11**1.39E-03**Dutch Oven/Pile Burner23.00E+039,4208.80**3.04E-03**FB32.00E+039,4205.10**1.55E-03**Fuel Cell23.00E+039,4207.89**2.83E-03**Suspension Burner16.00E+039,2409.54**6.36E-03**Suspension/Grate23.00E+039,4206.80**2.61E-03**Wet Biomass Stoker/Other23.00E+039,4208.27**2.92E-03**Dry Biomass Stoker/Other23.00E+039,2407.90**2.78E-03**Heavy Liquid N/A32.00E+039,19016.30**5.17E-03**Light Liquid N/A41.50E+039,1904.63**1.10E-03**Non-Continental Liquid N/A2 3.00E+03 9,190 5.29**2.30E-03**Process Gas N/A41.50E+038,7104.67**1.05E-03**BiomassBiomassPage 1 of 1

# Appendix D

Calculation of 3x RDL for Metallic HAP**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FuelCategoryCombustorDesignBasis of NewSource Floor?FacilityID UnitIDRunNumberTest DateSampleTime(min)SampleTime (hr)Coal N/A No AKDoyonUtilities_AK 4 Sample #1 8/17/2005 60 1Coal N/A No AKDoyonUtilities_AK 4 Sample #2 8/17/2005 60 1Coal N/A No AKDoyonUtilities_AK 4 Sample #3 8/17/2005 60 1Coal N/A No AKDoyonUtilities_AK 7 Sample #1 8/16/2005 60 1Coal N/A No AKDoyonUtilities_AK 7 Sample #2 8/16/2005 60 1Coal N/A No AKDoyonUtilities_AK 7 Sample #3 8/16/2005 60 1Biomass FB No ALIPCourtlandNo. 3 Combination Boier / 11Cu301Sample #1 7/7/2009 240 4Biomass FB No ALIPCourtlandNo. 3 Combination Boier / 11Cu301Sample #2 7/7/2009 240 4Biomass FB No ALIPCourtlandNo. 3 Combination Boier / 11Cu301Sample #3 7/8/2009 240 4Biomass Fuel Cell No ARAnthonyForestProducts SN-12 1 9/1/2009 216 4Biomass Fuel Cell No ARAnthonyForestProducts SN-12 2 9/1/2009 216 4Biomass Fuel Cell No ARAnthonyForestProducts SN-12 3 9/2/2009 216 4Wet BiomassStoker/SlopedGrate/OtherNo ARLeolaLumberMill SN-01A Sample #1 6/14/2006 120 2Wet BiomassStoker/SlopedGrate/OtherNo ARLeolaLumberMill SN-01A Sample #2 6/14/2006 120 2Wet BiomassStoker/SlopedGrate/OtherNo ARLeolaLumberMill SN-01A Sample #3 6/14/2006 120 2Wet BiomassStoker/SlopedGrate/OtherNo ARLeolaLumberMill SN-01B Sample #1 6/14/2006 120 2Wet BiomassStoker/SlopedGrate/OtherNo ARLeolaLumberMill SN-01B Sample #2 6/14/2006 120 2Wet BiomassStoker/SlopedGrate/OtherNo ARLeolaLumberMill SN-01B Sample #3 6/14/2006 120 2BiomassDutch Oven/Pile BurnerNo ARPotlatchForestWarren Wellons Boiler 1 9/9/2009 240 4BiomassDutch Oven/Pile BurnerNo ARPotlatchForestWarren Wellons Boiler 2 9/9/2009 240 4BiomassDutch Oven/Pile BurnerNo ARPotlatchForestWarren Wellons Boiler 3 9/9/2009 240 4BiomassSuspension/GrateNo FLSugarCaneGrowersCoop Boiler No. 8 Sample #1 1/19/2005 65 1BiomassSuspension/GrateNo FLSugarCaneGrowersCoop Boiler No. 8 Sample #2 1/19/2005 65 1BiomassSuspension/GrateNo FLSugarCaneGrowersCoop Boiler No. 8 Sample #3 1/19/2005 62 1Wet BiomassStoker/SlopedGrate/OtherNo GAGPMadisonPly800 Wood Waste Boiler1 8/11/2009 240 4Wet BiomassStoker/SlopedGrate/OtherNo GAGPMadisonPly800 Wood Waste Boiler2 8/12/2009 240 4**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FuelCategoryCombustorDesignBasis of NewSource Floor?FacilityID UnitIDRunNumberTest DateSampleTime(min)SampleTime (hr)Wet BiomassStoker/SlopedGrate/OtherNo GAGPMadisonPly800 Wood Waste Boiler3 8/12/2009 240 4Biomass FB No GATempleInlandRome WF 1 7/27/2009 204 3Biomass FB No GATempleInlandRome WF 2 7/28/2009 204 3Biomass FB No GATempleInlandRome WF 3 7/28/2009 204 3BiomassSuspension/GrateYes HIPuuneneSugarMill Boiler 1 Sample #1 5/28/2006 ?BiomassSuspension/GrateYes HIPuuneneSugarMill Boiler 1 Sample #2 5/29/2006 ?BiomassSuspension/GrateYes HIPuuneneSugarMill Boiler 1 Sample #3 5/30/2006 ?BiomassSuspension/GrateYes HIPuuneneSugarMill Boiler 1 Sample #1 7/25/2007BiomassSuspension/GrateYes HIPuuneneSugarMill Boiler 1 Sample #2 7/25/2007BiomassSuspension/GrateYes HIPuuneneSugarMill Boiler 1 Sample #3 7/25/2007BiomassSuspension/GrateYes HIPuuneneSugarMill Boiler 2 Sample #1 5/28/2006 ?BiomassSuspension/GrateYes HIPuuneneSugarMill Boiler 2 Sample #2 5/29/2006 ?BiomassSuspension/GrateYes HIPuuneneSugarMill Boiler 2 Sample #3 5/30/2006 ?BiomassSuspension/GrateYes HIPuuneneSugarMill Boiler 2 Sample #1 7/25/2007BiomassSuspension/GrateYes HIPuuneneSugarMill Boiler 2 Sample #2 7/25/2007BiomassSuspension/GrateYes HIPuuneneSugarMill Boiler 2 Sample #3 7/25/2007BiomassSuspension/GrateNo HIPuuneneSugarMill Boiler 3 Sample #1 5/23/2006BiomassSuspension/GrateNo HIPuuneneSugarMill Boiler 3 Sample #2 5/24/2006BiomassSuspension/GrateNo HIPuuneneSugarMill Boiler 3 Sample #3 5/25/2006BiomassSuspension/GrateNo HIPuuneneSugarMill Boiler 3 Sample #1 7/16/2007BiomassSuspension/GrateNo HIPuuneneSugarMill Boiler 3 Sample #2 7/17/2007BiomassSuspension/GrateNo HIPuuneneSugarMill Boiler 3 Sample #3 7/17/2007Coal N/A No IARoquetteAmericaCirculating Fluidized Bed Boiler (121)1 6/3/2009 192 3Coal N/A No IARoquetteAmericaCirculating Fluidized Bed Boiler (121)2 6/3/2009 192 3Coal N/A No IARoquetteAmericaCirculating Fluidized Bed Boiler (121)3 6/4/2009 192 3Coal N/A No IAUofNorthernIowa Boiler #3 4 10/6/2009 240 4**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FuelCategoryCombustorDesignBasis of NewSource Floor?FacilityID UnitIDRunNumberTest DateSampleTime(min)SampleTime (hr)Coal N/A No IAUofNorthernIowa Boiler #3 5 10/6/2009 240 4Coal N/A No IAUofNorthernIowa Boiler #3 6 10/7/2009 240 4Coal N/A NoIDAmalgamatedSugarCoTwinFallsS-B1 Sample #1 9/26/2006 120 2Coal N/A NoIDAmalgamatedSugarCoTwinFallsS-B1 Sample #2 9/26/2006 120 2Coal N/A NoIDAmalgamatedSugarCoTwinFallsS-B1 Sample #3 9/26/2006 120 2Biomass Fuel Cell Yes IDPotlatch PB-1 CE Sample #1 7/20/2006Biomass Fuel Cell Yes IDPotlatch PB-1 CE Sample #2 7/20/2006Biomass Fuel Cell Yes IDPotlatch PB-1 CE Sample #3 7/20/2006Biomass Fuel Cell Yes IDPotlatch PB-1 CE M29-R1 7/28/2009 240 4Biomass Fuel Cell Yes IDPotlatch PB-1 CE M29-R2 7/28/2009 240 4Biomass Fuel Cell Yes IDPotlatch PB-1 CE M29-R3 7/29/2009 240 4Wet BiomassStoker/SlopedGrate/OtherYes IDPotlatch PB-2 Riley Sample #1 7/27/2006Wet BiomassStoker/SlopedGrate/OtherYes IDPotlatch PB-2 Riley Sample #2 7/27/2006Wet BiomassStoker/SlopedGrate/OtherYes IDPotlatch PB-2 Riley Sample #3 7/27/2006Coal N/A No IDTASCONampaBabcock and Wilcox (B&W) #1Sample #1 12/4/2006 120 2Coal N/A No IDTASCONampaBabcock and Wilcox (B&W) #1Sample #2 12/4/2006 120 2Coal N/A No IDTASCONampaBabcock and Wilcox (B&W) #1Sample #3 12/4/2006 120 2Coal N/A No IDTASCONampaBabcock and Wilcox (B&W) #2Sample #1 12/4/2006 120 2Coal N/A No IDTASCONampaBabcock and Wilcox (B&W) #2Sample #2 12/4/2006 120 2Coal N/A No IDTASCONampaBabcock and Wilcox (B&W) #2Sample #3 12/4/2006 120 2Coal N/A Yes ILPolyOne B1 Sample #1 11/14/2006 120 2Coal N/A Yes ILPolyOne B1 Sample #2 11/14/2006Coal N/A Yes ILPolyOne B1 Sample #3 11/14/2006Coal N/A Yes ILPolyOne B1 1 9/9/2009 240 4Coal N/A Yes ILPolyOne B1 2 9/9/2009 240 4Coal N/A Yes ILPolyOne B1 3 9/10/2009 240 4**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FuelCategoryCombustorDesignBasis of NewSource Floor?FacilityID UnitIDRunNumberTest DateSampleTime(min)SampleTime (hr)Coal N/A No INSABICInnovativePlastics 01-001 BW1 Boiler Sample #1 6/28/2006 120 2Coal N/A No INSABICInnovativePlastics 01-001 BW1 Boiler Sample #2 6/28/2006 120 2Coal N/A No INSABICInnovativePlastics 01-001 BW1 Boiler Sample #3 6/28/2006 120 2Coal N/A No INSABICInnovativePlastics 01-001 BW2 Boiler Sample #1 6/28/2006 120 2Coal N/A No INSABICInnovativePlastics 01-001 BW2 Boiler Sample #2 6/28/2006 120 2Coal N/A No INSABICInnovativePlastics 01-001 BW2 Boiler Sample #3 6/28/2006 120 2Coal N/A No INTateLyleSagamore 31B1 M29-1 9/1/2009 240 4Coal N/A No INTateLyleSagamore 31B1 M29-2 9/2/2009 240 4Coal N/A No INTateLyleSagamore 31B1 M29-3 9/3/2009 240 4Coal N/A No MNHibbing Unit 1A Sample #1 9/21/2004 64 1Coal N/A No MNHibbing Unit 1A Sample #2 9/21/2004 65 1Coal N/A No MNHibbing Unit 1A Sample #3 9/21/2004 66 1Coal N/A No MNHibbing Unit 2A Sample #1 9/22/2004 67 1Coal N/A No MNHibbing Unit 2A Sample #2 9/22/2004 66 1Coal N/A No MNHibbing Unit 2A Sample #3 9/22/2004 66 1Wet BiomassStoker/SlopedGrate/OtherNo MSGPNewAugusta AA-015 Power Boiler Sample #1 7/12/2006 90 2Wet BiomassStoker/SlopedGrate/OtherNo MSGPNewAugusta AA-015 Power Boiler Sample #2 7/12/2006 90 2Wet BiomassStoker/SlopedGrate/OtherNo MSGPNewAugusta AA-015 Power Boiler Sample #3 7/12/2006 90 2BiomassDutch Oven/Pile BurnerNo MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #1 8/5/2009 180 3BiomassDutch Oven/Pile BurnerNo MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #2 8/5/2009 180 3BiomassDutch Oven/Pile BurnerNo MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #3 8/5/2009 180 3Biomass FB Yes NDCargillWestFargoFoster Wheeler Boiler (EU43)1 8/26/2009 240 4Biomass FB Yes NDCargillWestFargoFoster Wheeler Boiler (EU43)2 8/26/2009 240 4Biomass FB Yes NDCargillWestFargoFoster Wheeler Boiler (EU43)3 8/27/2009 240 4Coal N/A No OKGPMuskogeeMill B-4 Sample #1 4/16/2003 120 2Coal N/A No OKGPMuskogeeMill B-4 Sample #2 4/16/2003 120 2**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FuelCategoryCombustorDesignBasis of NewSource Floor?FacilityID UnitIDRunNumberTest DateSampleTime(min)SampleTime (hr)Coal N/A No OKGPMuskogeeMill B-4 Sample #3 4/16/2003 120 2Wet BiomassStoker/SlopedGrate/OtherNo SCMarlboroPaper Hogged Fuel Boiler Sample #1 7/14/2009 180 3Wet BiomassStoker/SlopedGrate/OtherNo SCMarlboroPaper Hogged Fuel Boiler Sample #2 7/14/2009 180 3Wet BiomassStoker/SlopedGrate/OtherNo SCMarlboroPaper Hogged Fuel Boiler Sample #3 7/14/2009 180 3Biomass FB No TNBowaterNewsprintBubbling Fluidized Bed BoilerSample #1 10/6/2005 60 1Biomass FB No TNBowaterNewsprintBubbling Fluidized Bed BoilerSample #2 10/6/2005 60 1Biomass FB No TNBowaterNewsprintBubbling Fluidized Bed BoilerSample #3 10/6/2005 60 1Biomass FB No TNBowaterNewsprintBubbling Fluidized Bed Boiler1 8/4/2009 208 3Biomass FB No TNBowaterNewsprintBubbling Fluidized Bed Boiler2 8/4/2009 208 3Biomass FB No TNBowaterNewsprintBubbling Fluidized Bed Boiler3 8/5/2009 208 3Coal N/A No TNEastman_NO_CBIDATA Boiler 30 1 8/26/2009 225 4Coal N/A No TNEastman_NO_CBIDATA Boiler 30 2 8/27/2009 225 4Coal N/A No TNEastman_NO_CBIDATA Boiler 30 3 8/27/2009 225 4BiomassSuspension BurnerNo TXDibollTemple-Inland PB-44 Sample #1 6/29/2007 120 2BiomassSuspension BurnerNo TXDibollTemple-Inland PB-44 Sample #2 6/29/2007 120 2BiomassDutch Oven/Pile BurnerNoVAGeorgiaPacificBrooknealGladys5600 Sample #1 7/6/2006 60 1BiomassDutch Oven/Pile BurnerNoVAGeorgiaPacificBrooknealGladys5600 Sample #2 7/6/2006 60 1BiomassDutch Oven/Pile BurnerNoVAGeorgiaPacificBrooknealGladys5600 Sample #3 7/6/2006 60 1Coal N/A No VAUniversityofVirginia 7103-1-01R M29-1 9/17/2009 240 4Coal N/A No VAUniversityofVirginia 7103-1-01R M29-2 9/17/2009 240 4Coal N/A No VAUniversityofVirginia 7103-1-01R M29-3 9/18/2009 240 4Coal N/A No VAVirginiaPolytechnic Boiler 11 Sample #1 2/27/2007 120 2Coal N/A No VAVirginiaPolytechnic Boiler 11 Sample #1Coal N/A No VAVirginiaPolytechnic Boiler 11 Sample #2Coal N/A No VAVirginiaPolytechnic Boiler 7 Sample #3 2/28/2007 120 2Coal N/A No VAVirginiaPolytechnic Boiler 7 Sample #1**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FuelCategoryCombustorDesignBasis of NewSource Floor?FacilityID UnitIDRunNumberTest DateSampleTime(min)SampleTime (hr)Coal N/A No VAVirginiaPolytechnic Boiler 7 Sample #1BiomassDutch Oven/Pile BurnerYes WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #1 8/11/2009 ?BiomassDutch Oven/Pile BurnerYes WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #2 8/11/2009 ?BiomassDutch Oven/Pile BurnerYes WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #3 8/12/2009 ?Biomass FB No WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #1 7/21/2005 60 1Biomass FB No WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #2 7/21/2005 60 1Biomass FB No WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #3 7/22/2005 60 1Biomass FB No WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #1 8/20/2009 240 4Biomass FB No WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #2 8/20/2009 240 4Biomass FB No WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #3 8/21/2009 240 4Coal N/A No WINewPageBiron B24 Sample #1 9/12/2007 120 2Coal N/A No WINewPageBiron B24 Sample #2 9/12/2007 120 2Coal N/A No WINewPageBiron B24 Sample #3 9/12/2007 120 2Coal N/A No WINewPageBiron B24 1 9/22/2009 240 4Coal N/A No WINewPageBiron B24 2 9/22/2009 240 4Coal N/A No WINewPageBiron B24 3 9/23/2009 240 4Coal N/A No WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #1 9/18/2003 60 1Coal N/A No WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #2 9/18/2003 60 1Coal N/A No WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #3 9/18/2003 60 1Process Gas N/A YesWVMountainStateCarbonFollansbeeS1 Sample #1 10/19/2009 240 4Process Gas N/A YesWVMountainStateCarbonFollansbeeS1 Sample #2 10/19/2009 240 4Process Gas N/A YesWVMountainStateCarbonFollansbeeS1 Sample #3 10/20/2009 240 4Coal N/A No WVPPGMartinsville R011-Boiler 3 1 7/22/2009 243.75 4Coal N/A No WVPPGMartinsville R011-Boiler 3 2 7/23/2009 243.75 4Coal N/A No WVPPGMartinsville R011-Boiler 3 3 7/23/2009 243.75 4Heavy LiquidN/ASCMilliken-DeweyD30Sample #18/12/20091803**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FuelCategoryCombustorDesignBasis of NewSource Floor?FacilityID UnitIDRunNumberTest DateSampleTime(min)SampleTime (hr)Heavy LiquidN/ASCMilliken-DeweyD30Sample #28/12/20091803Heavy LiquidN/ASCMilliken-DeweyD30Sample #38/12/20091803Heavy LiquidN/AYesMNGPDuluthEU33 Boiler #319/10/20091803Heavy LiquidN/AYesMNGPDuluthEU33 Boiler #329/10/20091803Heavy LiquidN/AYesMNGPDuluthEU33 Boiler #339/10/20091803Light LiquidN/AYesTNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86111/17/20092164Light LiquidN/AYesTNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86211/17/20092164Light LiquidN/AYesTNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86311/18/20092164**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateAKDoyonUtilities_AK 4 Sample #1 8/17/2005AKDoyonUtilities_AK 4 Sample #2 8/17/2005AKDoyonUtilities_AK 4 Sample #3 8/17/2005AKDoyonUtilities_AK 7 Sample #1 8/16/2005AKDoyonUtilities_AK 7 Sample #2 8/16/2005AKDoyonUtilities_AK 7 Sample #3 8/16/2005ALIPCourtlandNo. 3 Combination Boier / 11Cu301Sample #1 7/7/2009ALIPCourtlandNo. 3 Combination Boier / 11Cu301Sample #2 7/7/2009ALIPCourtlandNo. 3 Combination Boier / 11Cu301Sample #3 7/8/2009ARAnthonyForestProducts SN-12 1 9/1/2009ARAnthonyForestProducts SN-12 2 9/1/2009ARAnthonyForestProducts SN-12 3 9/2/2009ARLeolaLumberMill SN-01A Sample #1 6/14/2006ARLeolaLumberMill SN-01A Sample #2 6/14/2006ARLeolaLumberMill SN-01A Sample #3 6/14/2006ARLeolaLumberMill SN-01B Sample #1 6/14/2006ARLeolaLumberMill SN-01B Sample #2 6/14/2006ARLeolaLumberMill SN-01B Sample #3 6/14/2006ARPotlatchForestWarren Wellons Boiler 1 9/9/2009ARPotlatchForestWarren Wellons Boiler 2 9/9/2009ARPotlatchForestWarren Wellons Boiler 3 9/9/2009FLSugarCaneGrowersCoop Boiler No. 8 Sample #1 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #2 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #3 1/19/2005GAGPMadisonPly800 Wood Waste Boiler1 8/11/2009GAGPMadisonPly800 Wood Waste Boiler2 8/12/2009SampleVolume(dscf)SampleVolume(dscm)SampleO2 (%)As Catch(μg)As LabAnalysisBe Catch(μg)61.671 1.746312 7 1.8 ICP/MS 0.461.448 1.739997 6.7 2.1 ICP/MS 0.459.464 1.683817 6.6 1.9 ICP/MS 0.461.025 1.728019 7.6 1.4 ICP/MS 0.457.17 1.618859 7.9 1.6 ICP/MS 0.455.76 1.578932 8 1.5 ICP/MS 0.4133.522 3.780886 11.3 0.015 ICP/MS 0.015131.979 3.737194 11.4 0 ICP/MS 0.2015126.265 3.575393 11.5 0.012 ICP/MS 0.062150.232 4.254056 8.5 4.06 ICP/MS 0.55148.205 4.196659 8 4.56 ICP/MS 0.55143.731 4.06997 7.8 4.06 ICP/MS 0.5586.482 2.448874 9.8 2.2 ICP/MS 0.1184.128 2.382217 10.2 2.2 ICP/MS 0.1684.546 2.394054 10 2.2 ICP/MS 0.1589.483 2.533852 11.9 2.2 ICP/MS 0.1193.536 2.64862 12 2.2 ICP/MS 0.1590.405 2.55996 11.6 2.2 ICP/MS 0.15208.754 5.911199 4.22 7.59 ICP/MS 0.119220.995 6.257822 4.9 0.46 ICP/MS 0.0275217.503 6.158941 4.39 0.23 ICP/MS 0.03139.778 1.126377 7.93 ?35.816 1.014187 7.38 ?36.457 1.032338 7.32 ?156.922 4.443494 8.88 1.389 ICP/MS 0.05154.062 4.362509 8.21 1.8975 ICP/MS 0.0665**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateGAGPMadisonPly800 Wood Waste Boiler3 8/12/2009GATempleInlandRome WF 1 7/27/2009GATempleInlandRome WF 2 7/28/2009GATempleInlandRome WF 3 7/28/2009HIPuuneneSugarMill Boiler 1 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 1 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 1 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 1 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 2 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 2 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 2 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 3 Sample #1 5/23/2006HIPuuneneSugarMill Boiler 3 Sample #2 5/24/2006HIPuuneneSugarMill Boiler 3 Sample #3 5/25/2006HIPuuneneSugarMill Boiler 3 Sample #1 7/16/2007HIPuuneneSugarMill Boiler 3 Sample #2 7/17/2007HIPuuneneSugarMill Boiler 3 Sample #3 7/17/2007IARoquetteAmericaCirculating Fluidized Bed Boiler (121)1 6/3/2009IARoquetteAmericaCirculating Fluidized Bed Boiler (121)2 6/3/2009IARoquetteAmericaCirculating Fluidized Bed Boiler (121)3 6/4/2009IAUofNorthernIowa Boiler #3 4 10/6/2009SampleVolume(dscf)SampleVolume(dscm)SampleO2 (%)As Catch(μg)As LabAnalysisBe Catch(μg)159.888 4.527481 7.21 1.343 ICP/MS 0.059150.483 4.261164 5.1 12.3 ICP/MS 0.25157.17 4.450517 5 5.88 ICP/MS 0.25163.398 4.626872 5.2 10.06 ICP/MS 0.2596.787 2.797 10.06 16 ICP/AES 0.4895.978 2.718 9.84 16 ICP/AES 0.31118.402 3.353 10.27 30 ICP/AES 0.8696.787 2.797 10.06 16 ICP/AES 0.4895.978 2.718 9.84 16 ICP/AES 0.31118.402 3.353 10.27 30 ICP/AES 0.86150.658 4.266119 5.8 1.24 ICP/AES 0.32151.674 4.294889 6.1 1.27 ICP/AES 0.35148.593 4.207645 5.6 1.33 ICP/AES 0.32164.415 4.65567 5.8 3.37 ? 0.12**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateIAUofNorthernIowa Boiler #3 5 10/6/2009IAUofNorthernIowa Boiler #3 6 10/7/2009IDAmalgamatedSugarCoTwinFallsS-B1 Sample #1 9/26/2006IDAmalgamatedSugarCoTwinFallsS-B1 Sample #2 9/26/2006IDAmalgamatedSugarCoTwinFallsS-B1 Sample #3 9/26/2006IDPotlatch PB-1 CE Sample #1 7/20/2006IDPotlatch PB-1 CE Sample #2 7/20/2006IDPotlatch PB-1 CE Sample #3 7/20/2006IDPotlatch PB-1 CE M29-R1 7/28/2009IDPotlatch PB-1 CE M29-R2 7/28/2009IDPotlatch PB-1 CE M29-R3 7/29/2009IDPotlatch PB-2 Riley Sample #1 7/27/2006IDPotlatch PB-2 Riley Sample #2 7/27/2006IDPotlatch PB-2 Riley Sample #3 7/27/2006IDTASCONampaBabcock and Wilcox (B&W) #1Sample #1 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #1Sample #2 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #1Sample #3 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #2Sample #1 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #2Sample #2 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #2Sample #3 12/4/2006ILPolyOne B1 Sample #1 11/14/2006ILPolyOne B1 Sample #2 11/14/2006ILPolyOne B1 Sample #3 11/14/2006ILPolyOne B1 1 9/9/2009ILPolyOne B1 2 9/9/2009ILPolyOne B1 3 9/10/2009SampleVolume(dscf)SampleVolume(dscm)SampleO2 (%)As Catch(μg)As LabAnalysisBe Catch(μg)165.331 4.681608 5.3 2.83 ? 0.51166.356 4.710633 6 2.26 ? 0.7178.341 2.218349 6.9 5.1 ICP/AES 0.2580.205 2.271131 6.9 5.2 ICP/AES 0.2677.571 2.196545 6 5.2 ICP/AES 0.26159.52 4.517061 13.2 0.9 ICP/MS 0.04170.7 4.83364 13.8 0.7 ICP/MS 0.022161.05 4.560385 13 0.99 ICP/MS 0.02289.928 2.546453 7.4 0.53 GFAA 0.3294.073 2.663826 6.9 0.65 GFAA 0.2794.027 2.662523 6.9 0.47 GFAA 1.1889.928 2.546453 7.4 0.53 GFAA 0.3294.073 2.663826 6.9 0.65 GFAA 0.2794.027 2.662523 6.9 0.47 GFAA 0.2383.69 2.369815 7.5 3 ICP/MS 0.753 0.753.1 0.75172.203 4.8762 8.4 2.8 ICP/MS 0.7164.574 4.660173 8.09 2.8 ICP/MS 0.7165.647 4.690556 8.27 2.8 ICP/MS 0.78**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateINSABICInnovativePlastics 01-001 BW1 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #3 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #3 6/28/2006INTateLyleSagamore 31B1 M29-1 9/1/2009INTateLyleSagamore 31B1 M29-2 9/2/2009INTateLyleSagamore 31B1 M29-3 9/3/2009MNHibbing Unit 1A Sample #1 9/21/2004MNHibbing Unit 1A Sample #2 9/21/2004MNHibbing Unit 1A Sample #3 9/21/2004MNHibbing Unit 2A Sample #1 9/22/2004MNHibbing Unit 2A Sample #2 9/22/2004MNHibbing Unit 2A Sample #3 9/22/2004MSGPNewAugusta AA-015 Power Boiler Sample #1 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #2 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #3 7/12/2006MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #1 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #2 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #3 8/5/2009NDCargillWestFargoFoster Wheeler Boiler (EU43)1 8/26/2009NDCargillWestFargoFoster Wheeler Boiler (EU43)2 8/26/2009NDCargillWestFargoFoster Wheeler Boiler (EU43)3 8/27/2009OKGPMuskogeeMill B-4 Sample #1 4/16/2003OKGPMuskogeeMill B-4 Sample #2 4/16/2003SampleVolume(dscf)SampleVolume(dscm)SampleO2 (%)As Catch(μg)As LabAnalysisBe Catch(μg)91.73 2.59748 8 11.2 GFAA 0.989.671 2.539176 8 10 GFAA 0.6486.571 2.451395 8 10 GFAA 0.5591.73 2.59748 8 11.2 GFAA 0.989.671 2.539176 8 10 GFAA 0.6486.571 2.451395 8 10 GFAA 0.55161.58 4.575393 5.57 5.33 ICP/MS 3.365139.34 3.945632 5.26 4.42 ICP/MS 2.955133.63 3.783944 5.97 2.986 ICP/MS 1.75538.31 1.084808 6.5 2 ICP/AES 0.539.3 1.112842 7.21 2 ICP/AES 0.540.92 1.158714 6.84 2 ICP/AES 0.535.81 1.014017 6.46 2 ICP/AES 0.537.43 1.05989 6.82 2 ICP/AES 0.537.97 1.075181 7.01 2 ICP/AES 0.568.96 1.952711 10.2 1.96 ICP/MS 0.3555.59 1.574119 11.2 1.4 ICP/MS 0.3561.31 1.736089 12 1.42 ICP/MS 0.35174.983 4.95492 8.06 0.812 ICP/MS 0.1180.328 5.106272 7.25 1.066 ICP/MS 0.1178.997 5.068583 7.63 0.575 ICP/MS 0.1126.485 3.581623 12.68 0.37 ICP/AES 0.32134.933 3.820841 12.68 0.58 ICP/AES 0.32138.135 3.911511 12.79 0.38 ICP/AES 0.3287.1 2.466374 7.5 1.2 ICP/MS 0.1685.634 2.424862 6.5 0.77 ICP/MS 0.21**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateOKGPMuskogeeMill B-4 Sample #3 4/16/2003SCMarlboroPaper Hogged Fuel Boiler Sample #1 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #2 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #3 7/14/2009TNBowaterNewsprintBubbling Fluidized Bed BoilerSample #1 10/6/2005TNBowaterNewsprintBubbling Fluidized Bed BoilerSample #2 10/6/2005TNBowaterNewsprintBubbling Fluidized Bed BoilerSample #3 10/6/2005TNBowaterNewsprintBubbling Fluidized Bed Boiler1 8/4/2009TNBowaterNewsprintBubbling Fluidized Bed Boiler2 8/4/2009TNBowaterNewsprintBubbling Fluidized Bed Boiler3 8/5/2009TNEastman_NO_CBIDATA Boiler 30 1 8/26/2009TNEastman_NO_CBIDATA Boiler 30 2 8/27/2009TNEastman_NO_CBIDATA Boiler 30 3 8/27/2009TXDibollTemple-Inland PB-44 Sample #1 6/29/2007TXDibollTemple-Inland PB-44 Sample #2 6/29/2007VAGeorgiaPacificBrooknealGladys5600 Sample #1 7/6/2006VAGeorgiaPacificBrooknealGladys5600 Sample #2 7/6/2006VAGeorgiaPacificBrooknealGladys5600 Sample #3 7/6/2006VAUniversityofVirginia 7103-1-01R M29-1 9/17/2009VAUniversityofVirginia 7103-1-01R M29-2 9/17/2009VAUniversityofVirginia 7103-1-01R M29-3 9/18/2009VAVirginiaPolytechnic Boiler 11 Sample #1 2/27/2007VAVirginiaPolytechnic Boiler 11 Sample #1VAVirginiaPolytechnic Boiler 11 Sample #2VAVirginiaPolytechnic Boiler 7 Sample #3 2/28/2007VAVirginiaPolytechnic Boiler 7 Sample #1SampleVolume(dscf)SampleVolume(dscm)SampleO2 (%)As Catch(μg)As LabAnalysisBe Catch(μg)80.062 2.267082 6 0.71 ICP/MS 0.12142.32 4.030016 9.74 0.633 ICP/MS 0.05135.96 3.849922 9.38 0.69 ICP/MS 0.05146.64 4.152343 9.11 0.6 ICP/MS 0.0585.293 2.415206 5.6 4.5 ICP/MS 0.282.303 2.330539 5.5 2.8 ICP/MS 0.278.77 2.230497 5.7 3 ICP/MS 0.5163.647 4.633923 6.6 16.56 ICP/MS 1.05152.054 4.305649 7 15.21 ICP/MS 1.05159.337 4.511879 6.8 8.16 ICP/MS 1.05162.383 4.598131 6.3 7.64 ICP/MS 0.75163.694 4.635254 6.3 4.12 ICP/MS 0.7165.392 4.683336 6.3 4.13 ICP/MS 0.761.4876 1.741119 12.1 0.085 ICP/MS 0.0561.4138 1.739029 12.10.122ICP/MS 0.0547 1.330879 15.27 0.2 ICP/MS 0.0547.22 1.337109 15.55 0.2 ICP/MS 0.0547.68 1.350135 15.07 0.2 ICP/MS 0.05176.38 4.994478 7.06 0.747 ICP/MS 0.05169.546 4.800963 7.14 1.539 ICP/MS 0.05172.911 4.896248 7.07 0.213 ICP/MS 0.0586.64567 2.453509 5.436667 7 GFAA 0.54.4 0.344.3 0.3482.27867 2.32985 5.436667 3.7 GFAA 0.2213.8 0.59**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateVAVirginiaPolytechnic Boiler 7 Sample #1WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #1 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #2 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #3 8/12/2009WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #1 7/21/2005WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #2 7/21/2005WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #3 7/22/2005WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #1 8/20/2009WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #2 8/20/2009WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #3 8/21/2009WINewPageBiron B24 Sample #1 9/12/2007WINewPageBiron B24 Sample #2 9/12/2007WINewPageBiron B24 Sample #3 9/12/2007WINewPageBiron B24 1 9/22/2009WINewPageBiron B24 2 9/22/2009WINewPageBiron B24 3 9/23/2009WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #1 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #2 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #3 9/18/2003WVMountainStateCarbonFollansbeeS1 Sample #1 10/19/2009WVMountainStateCarbonFollansbeeS1 Sample #2 10/19/2009WVMountainStateCarbonFollansbeeS1 Sample #3 10/20/2009WVPPGMartinsville R011-Boiler 3 1 7/22/2009WVPPGMartinsville R011-Boiler 3 2 7/23/2009WVPPGMartinsville R011-Boiler 3 3 7/23/2009SCMilliken-DeweyD30Sample #18/12/2009SampleVolume(dscf)SampleVolume(dscm)SampleO2 (%)As Catch(μg)As LabAnalysisBe Catch(μg)3.1 0.17154.1 4.363585 11.85 0.65 ? 0.32162.62 4.604842 11.21 0.64 ? 0.32161.92 4.585021 10.22 0.64 ? 0.3240.974 1.160244 11.7 0.5 ICP/MS 0.0543.734 1.238397 12 6.77 ICP/MS 0.0545.025 1.274954 12 0.5 ICP/MS 0.05155.597 4.405975 8.1 0.279 ICP/MS 0.05155.139 4.393006 8.8 0.212 ICP/MS 0.05147.746 4.183661 7.8 0.236 ICP/MS 0.05125.571 3.555741 7 6.99 ICP/MS 0.75114.102 3.230978 7 6.69 ICP/MS 0.75112.147 3.175619 7 5.09 ICP/MS 0.75167.363 4.739148 7.7 3.9 ICP/MS 0.7148.569 4.206966 6.9 4.75 ICP/MS 0.7150.007 4.247685 7.2 4.52 ICP/MS 0.755.11 1.560527 8.8 2.24 ? 0.1653.27 1.508424 8.8 2.37 ? 0.1654.06 1.530794 8.6 2.08 ? 0.16163.271 4.623276 4.5 21 ICP/MS 0.45124.385 3.522158 4.7 26.2 ICP/MS 0.45143.477 4.062778 4.8 21.6 ICP/MS 0.45139.67 3.954977 7.8 14.95 GFAA 0.28169.97 4.812969 8.6 10.18 GFAA 0.31130.74 3.70211 8.03 12.45 GFAA 0.28155.074.3910523.835.28ICP/MS0.05**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateSCMilliken-DeweyD30Sample #28/12/2009SCMilliken-DeweyD30Sample #38/12/2009MNGPDuluthEU33 Boiler #319/10/2009MNGPDuluthEU33 Boiler #329/10/2009MNGPDuluthEU33 Boiler #339/10/2009TNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86111/17/2009TNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86211/17/2009TNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86311/18/2009SampleVolume(dscf)SampleVolume(dscm)SampleO2 (%)As Catch(μg)As LabAnalysisBe Catch(μg)136.43.8623814.022.654ICP/MS0.05140.573.9804623.961.8ICP/MS0.05152.874.32875516.61.34ICP/MS0.18148.384.20161416.271.81ICP/MS0.18144.354.087498161.43ICP/MS0.18166.7454.7216484.30.1ICP/MS0.25167.2814.7368264.31.44ICP/MS0.25168.634.7750255.31ICP/MS0.25**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateAKDoyonUtilities_AK 4 Sample #1 8/17/2005AKDoyonUtilities_AK 4 Sample #2 8/17/2005AKDoyonUtilities_AK 4 Sample #3 8/17/2005AKDoyonUtilities_AK 7 Sample #1 8/16/2005AKDoyonUtilities_AK 7 Sample #2 8/16/2005AKDoyonUtilities_AK 7 Sample #3 8/16/2005ALIPCourtlandNo. 3 Combination Boier / 11Cu301Sample #1 7/7/2009ALIPCourtlandNo. 3 Combination Boier / 11Cu301Sample #2 7/7/2009ALIPCourtlandNo. 3 Combination Boier / 11Cu301Sample #3 7/8/2009ARAnthonyForestProducts SN-12 1 9/1/2009ARAnthonyForestProducts SN-12 2 9/1/2009ARAnthonyForestProducts SN-12 3 9/2/2009ARLeolaLumberMill SN-01A Sample #1 6/14/2006ARLeolaLumberMill SN-01A Sample #2 6/14/2006ARLeolaLumberMill SN-01A Sample #3 6/14/2006ARLeolaLumberMill SN-01B Sample #1 6/14/2006ARLeolaLumberMill SN-01B Sample #2 6/14/2006ARLeolaLumberMill SN-01B Sample #3 6/14/2006ARPotlatchForestWarren Wellons Boiler 1 9/9/2009ARPotlatchForestWarren Wellons Boiler 2 9/9/2009ARPotlatchForestWarren Wellons Boiler 3 9/9/2009FLSugarCaneGrowersCoop Boiler No. 8 Sample #1 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #2 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #3 1/19/2005GAGPMadisonPly800 Wood Waste Boiler1 8/11/2009GAGPMadisonPly800 Wood Waste Boiler2 8/12/2009Be LabAnalysisCd Catch(μg)Cd LabAnalysisCr Catch(μg)Cr LabAnalysisPb Catch(μg)ICP/MS 0.79 ICP/MS 1.2 ICP/MS 3.2ICP/MS 0.9 ICP/MS 1.8 ICP/MS 5ICP/MS 0.6 ICP/MS 1.5 ICP/MS 3.8ICP/MS 0.6 ICP/MS 3.3 ICP/MS 2.3ICP/MS 1.2 ICP/MS 3.3 ICP/MS 11.9ICP/MS 0.6 ICP/MS 2.2 ICP/MS 3.5ICP/MS 1.946 ICP/MS 0.415 ICP/MS 0.535ICP/MS 0.0175 ICP/MS 0.06 ICP/MS 0.65ICP/MS 0.289 ICP/MS 0.17 ICP/MS 0.42ICP/MS 26.46 ICP/MS 17.41 ICP/MS 38.24ICP/MS 36.21 ICP/MS 20.4 ICP/MS 35.85ICP/MS 35.41 ICP/MS 19.31 ICP/MS 37.59ICP/MS 2.15 ICP/MS 1.2 ICP/MS 1.31ICP/MS 3.18 ICP/MS 2.8 ICP/MS 1.68ICP/MS 1.24 ICP/MS 2.3 ICP/MS 0.92ICP/MS 6.9 ICP/MS 1.3 ICP/MS 2.36ICP/MS 0.97 ICP/MS 1.4 ICP/MS 1.9ICP/MS 1.22 ICP/MS 2.6 ICP/MS 1.91ICP/MS 9.04 ICP/MS 19.893 ICP/MS 38.364ICP/MS 0.605 ICP/MS 4.087 ICP/MS 4.761ICP/MS 0.55 ICP/MS 4.546 ICP/MS 2.258? ? ?? ? ?? ? ?ICP/MS 2.829 ICP/MS 36.369 ICP/MS 6.591ICP/MS 2.92 ICP/MS 35.522 ICP/MS 1.367**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateGAGPMadisonPly800 Wood Waste Boiler3 8/12/2009GATempleInlandRome WF 1 7/27/2009GATempleInlandRome WF 2 7/28/2009GATempleInlandRome WF 3 7/28/2009HIPuuneneSugarMill Boiler 1 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 1 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 1 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 1 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 2 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 2 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 2 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 3 Sample #1 5/23/2006HIPuuneneSugarMill Boiler 3 Sample #2 5/24/2006HIPuuneneSugarMill Boiler 3 Sample #3 5/25/2006HIPuuneneSugarMill Boiler 3 Sample #1 7/16/2007HIPuuneneSugarMill Boiler 3 Sample #2 7/17/2007HIPuuneneSugarMill Boiler 3 Sample #3 7/17/2007IARoquetteAmericaCirculating Fluidized Bed Boiler (121)1 6/3/2009IARoquetteAmericaCirculating Fluidized Bed Boiler (121)2 6/3/2009IARoquetteAmericaCirculating Fluidized Bed Boiler (121)3 6/4/2009IAUofNorthernIowa Boiler #3 4 10/6/2009Be LabAnalysisCd Catch(μg)Cd LabAnalysisCr Catch(μg)Cr LabAnalysisPb Catch(μg)ICP/MS 1.048 ICP/MS 46.022 ICP/MS 1.063ICP/MS 0.62 ICP/MS 12.58 ICP/MS 17.93ICP/MS 0.538 ICP/MS 13.29 ICP/MS 12.11ICP/MS 0.54 ICP/MS 11.28 ICP/MS 10.85ICP/AES 2.4 ICP/MS 27 ICP/AES 21ICP/AES 2.7 ICP/MS 21 ICP/AES 23ICP/AES 5.9 ICP/MS 43 ICP/AES 47ICP/AES 2.4 ICP/MS 27 ICP/AES 21ICP/AES 2.7 ICP/MS 21 ICP/AES 23ICP/AES 5.9 ICP/MS 43 ICP/AES 47ICP/AES 4.1 ICP/AES 8.2 ICP/AES 6.6ICP/AES 7.3 ICP/AES 5.7 ICP/AES 4.6ICP/AES 1.34 ICP/AES 3.96 ICP/AES 10.3? 0.45 ? 12.72 ? 4.33**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateIAUofNorthernIowa Boiler #3 5 10/6/2009IAUofNorthernIowa Boiler #3 6 10/7/2009IDAmalgamatedSugarCoTwinFallsS-B1 Sample #1 9/26/2006IDAmalgamatedSugarCoTwinFallsS-B1 Sample #2 9/26/2006IDAmalgamatedSugarCoTwinFallsS-B1 Sample #3 9/26/2006IDPotlatch PB-1 CE Sample #1 7/20/2006IDPotlatch PB-1 CE Sample #2 7/20/2006IDPotlatch PB-1 CE Sample #3 7/20/2006IDPotlatch PB-1 CE M29-R1 7/28/2009IDPotlatch PB-1 CE M29-R2 7/28/2009IDPotlatch PB-1 CE M29-R3 7/29/2009IDPotlatch PB-2 Riley Sample #1 7/27/2006IDPotlatch PB-2 Riley Sample #2 7/27/2006IDPotlatch PB-2 Riley Sample #3 7/27/2006IDTASCONampaBabcock and Wilcox (B&W) #1Sample #1 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #1Sample #2 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #1Sample #3 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #2Sample #1 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #2Sample #2 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #2Sample #3 12/4/2006ILPolyOne B1 Sample #1 11/14/2006ILPolyOne B1 Sample #2 11/14/2006ILPolyOne B1 Sample #3 11/14/2006ILPolyOne B1 1 9/9/2009ILPolyOne B1 2 9/9/2009ILPolyOne B1 3 9/10/2009Be LabAnalysisCd Catch(μg)Cd LabAnalysisCr Catch(μg)Cr LabAnalysisPb Catch(μg)? 0.36 ? 22.26 ? 4.77? 0.48 ? 9.51 ? 4.62ICP/AES 0.25 ICP/AES 149.7 ICP/AES 5.1ICP/AES 0.31 ICP/AES 2.6 ICP/AES 5.2ICP/AES 0.29 ICP/AES 0.52 ICP/AES 5.2ICP/MS 0.3 ICP/MS 1.3 ICP/MS 1.56ICP/MS 0.65 ICP/MS 1.3 ICP/MS 4.1ICP/MS 0.13 ICP/MS 3.4 ICP/MS 1.58ICP/AES 7.26 ICP/AES 2.16 ICP/AES 5.9ICP/AES 0.61 ICP/AES 1.65 ICP/AES 4ICP/AES 1.18 ICP/AES 0.87 ICP/AES 3.34ICP/AES 7.26 ICP/AES 2.16 ICP/AES 5.9ICP/AES 0.61 ICP/AES 1.65 ICP/AES 4ICP/AES 1.18 ICP/AES 0.87 ICP/AES 3.34ICP/MS 0.75 ICP/MS 2.25 ICP/MS 3.20.75 2.68 3.20.75 2.25 2.6ICP/MS 0.72 ICP/MS 4.24 ICP/MS 4.44ICP/MS 0.7 ICP/MS 4.52 ICP/MS 3.71ICP/MS 0.7 ICP/MS 4.84 ICP/MS 3.75**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateINSABICInnovativePlastics 01-001 BW1 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #3 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #3 6/28/2006INTateLyleSagamore 31B1 M29-1 9/1/2009INTateLyleSagamore 31B1 M29-2 9/2/2009INTateLyleSagamore 31B1 M29-3 9/3/2009MNHibbing Unit 1A Sample #1 9/21/2004MNHibbing Unit 1A Sample #2 9/21/2004MNHibbing Unit 1A Sample #3 9/21/2004MNHibbing Unit 2A Sample #1 9/22/2004MNHibbing Unit 2A Sample #2 9/22/2004MNHibbing Unit 2A Sample #3 9/22/2004MSGPNewAugusta AA-015 Power Boiler Sample #1 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #2 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #3 7/12/2006MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #1 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #2 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #3 8/5/2009NDCargillWestFargoFoster Wheeler Boiler (EU43)1 8/26/2009NDCargillWestFargoFoster Wheeler Boiler (EU43)2 8/26/2009NDCargillWestFargoFoster Wheeler Boiler (EU43)3 8/27/2009OKGPMuskogeeMill B-4 Sample #1 4/16/2003OKGPMuskogeeMill B-4 Sample #2 4/16/2003Be LabAnalysisCd Catch(μg)Cd LabAnalysisCr Catch(μg)Cr LabAnalysisPb Catch(μg)ICP/AES 3.23 ICP/AES 16.4 ICP/AES 10ICP/AES 3.19 ICP/AES 13.01 ICP/AES 8.1ICP/AES 2.86 ICP/AES 15.8 ICP/AES 6ICP/AES 3.23 ICP/AES 16.4 ICP/AES 10ICP/AES 3.19 ICP/AES 13.01 ICP/AES 8.1ICP/AES 2.86 ICP/AES 15.8 ICP/AES 6ICP/MS 1.731 ICP/MS 29.79 ICP/MS 11.64ICP/MS 1.544 ICP/MS 28.33 ICP/MS 10.378ICP/MS 0.94 ICP/MS 13.59 ICP/MS 6.574ICP/AES 0.2 ICP/AES 5.3 ICP/AES 2ICP/AES 0.2 ICP/AES 2 ICP/AES 2ICP/AES 0.2 ICP/AES 2.1 ICP/AES 2ICP/AES 0.2 ICP/AES 6.2 ICP/AES 2.7ICP/AES 0.71 ICP/AES 4.3 ICP/AES 4ICP/AES 0.41 ICP/AES 2.6 ICP/AES 3.8ICP/MS 0.392 ICP/MS 2.75 ICP/MS 4.45ICP/MS 0.212 ICP/MS 0.79 ICP/MS 1.24ICP/MS 0.152 ICP/MS 1.43 ICP/MS 1.22ICP/MS 1.009 ICP/MS 8.14 ICP/MS 10.924ICP/MS 1.25 ICP/MS 6.63 ICP/MS 10.381ICP/MS 1.05 ICP/MS 5 ICP/MS 7.291ICP/AES 2.9 ICP/AES 2.74 ICP/AES 4.02ICP/AES 4.93 ICP/AES 1.8 ICP/AES 3.9ICP/AES 4.4 ICP/AES 1.82 ICP/AES 2.17ICP/MS 0.31 ICP/MS 71 ICP/MS 3.3ICP/MS 2 ICP/MS 20 ICP/MS 2.6**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateOKGPMuskogeeMill B-4 Sample #3 4/16/2003SCMarlboroPaper Hogged Fuel Boiler Sample #1 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #2 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #3 7/14/2009TNBowaterNewsprintBubbling Fluidized Bed BoilerSample #1 10/6/2005TNBowaterNewsprintBubbling Fluidized Bed BoilerSample #2 10/6/2005TNBowaterNewsprintBubbling Fluidized Bed BoilerSample #3 10/6/2005TNBowaterNewsprintBubbling Fluidized Bed Boiler1 8/4/2009TNBowaterNewsprintBubbling Fluidized Bed Boiler2 8/4/2009TNBowaterNewsprintBubbling Fluidized Bed Boiler3 8/5/2009TNEastman_NO_CBIDATA Boiler 30 1 8/26/2009TNEastman_NO_CBIDATA Boiler 30 2 8/27/2009TNEastman_NO_CBIDATA Boiler 30 3 8/27/2009TXDibollTemple-Inland PB-44 Sample #1 6/29/2007TXDibollTemple-Inland PB-44 Sample #2 6/29/2007VAGeorgiaPacificBrooknealGladys5600 Sample #1 7/6/2006VAGeorgiaPacificBrooknealGladys5600 Sample #2 7/6/2006VAGeorgiaPacificBrooknealGladys5600 Sample #3 7/6/2006VAUniversityofVirginia 7103-1-01R M29-1 9/17/2009VAUniversityofVirginia 7103-1-01R M29-2 9/17/2009VAUniversityofVirginia 7103-1-01R M29-3 9/18/2009VAVirginiaPolytechnic Boiler 11 Sample #1 2/27/2007VAVirginiaPolytechnic Boiler 11 Sample #1VAVirginiaPolytechnic Boiler 11 Sample #2VAVirginiaPolytechnic Boiler 7 Sample #3 2/28/2007VAVirginiaPolytechnic Boiler 7 Sample #1Be LabAnalysisCd Catch(μg)Cd LabAnalysisCr Catch(μg)Cr LabAnalysisPb Catch(μg)ICP/MS 0.1 ICP/MS 120 ICP/MS 2.3ICP/MS 0.414 ICP/MS 0.566 ICP/MS 5.409ICP/MS 0.433 ICP/MS 3.517 ICP/MS 4.491ICP/MS 0.26 ICP/MS 1.643 ICP/MS 1.797ICP/MS 1.3 ICP/MS 25.8 ICP/MS 6.8ICP/MS 1.2 ICP/MS 24.7 ICP/MS 6.7ICP/MS 0.8 ICP/MS 20 ICP/MS 5ICP/MS 2.553 ICP/MS 22.504 ICP/MS 43.81ICP/MS 2.601 ICP/MS 22.527 ICP/MS 40.69ICP/MS 1.45 ICP/MS 13.9155 ICP/MS 24.19ICP/MS 0.77 ICP/MS 8.85 ICP/MS 5.11ICP/MS 0.65 ICP/MS 7.385 ICP/MS 5.48ICP/MS 1.09 ICP/MS 4.99 ICP/MS 3.12ICP/MS 0.218 ICP/MS 0.22 ICP/MS 2.27ICP/MS 0.196 ICP/MS 0.77 ICP/MS 1.33ICP/MS 1.01 ICP/MS 1.4 ICP/MS 1.21ICP/MS 0.39 ICP/MS 1.02 ICP/MS 2.24ICP/MS 0.44 ICP/MS 1.33 ICP/MS 1.37ICP/MS 0.465 ICP/MS 14.389 ICP/MS 3.314ICP/MS 0.489 ICP/MS 4.781 ICP/MS 3.793ICP/MS 0.325 ICP/MS 4.752 ICP/MS 1.009GFAA 3.08 GFAA 5.355 GFAA 30.040.26 2.67 25.0250.28 2.95 19.295GFAA 4.55 GFAA 2.86 GFAA 12.746.41 4.765 15.275**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateVAVirginiaPolytechnic Boiler 7 Sample #1WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #1 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #2 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #3 8/12/2009WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #1 7/21/2005WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #2 7/21/2005WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #3 7/22/2005WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #1 8/20/2009WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #2 8/20/2009WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #3 8/21/2009WINewPageBiron B24 Sample #1 9/12/2007WINewPageBiron B24 Sample #2 9/12/2007WINewPageBiron B24 Sample #3 9/12/2007WINewPageBiron B24 1 9/22/2009WINewPageBiron B24 2 9/22/2009WINewPageBiron B24 3 9/23/2009WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #1 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #2 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #3 9/18/2003WVMountainStateCarbonFollansbeeS1 Sample #1 10/19/2009WVMountainStateCarbonFollansbeeS1 Sample #2 10/19/2009WVMountainStateCarbonFollansbeeS1 Sample #3 10/20/2009WVPPGMartinsville R011-Boiler 3 1 7/22/2009WVPPGMartinsville R011-Boiler 3 2 7/23/2009WVPPGMartinsville R011-Boiler 3 3 7/23/2009SCMilliken-DeweyD30Sample #18/12/2009Be LabAnalysisCd Catch(μg)Cd LabAnalysisCr Catch(μg)Cr LabAnalysisPb Catch(μg)0.73 2.065 7.89? 0.32 ? 3.9 ? 0.86? 0.69 ? 1.5 ? 0.76? 0.32 ? 1.7 ? 0.57ICP/MS 2.8 ICP/MS 18.2 ICP/MS 2.82ICP/MS 1.76 ICP/MS 14.4 ICP/MS 2.92ICP/MS 1.7 ICP/MS 8.89 ICP/MS 1.68ICP/MS 1.796 ICP/MS 9.15 ICP/MS 3.175ICP/MS 1.66 ICP/MS 4.922 ICP/MS 3.865ICP/MS 1.721 ICP/MS 6.45 ICP/MS 3.58ICP/MS 2.44 ICP/MS 4.5 ICP/MS 15.82ICP/MS 1.48 ICP/MS 1.9 ICP/MS 13.22ICP/MS 2.03 ICP/MS 0.66 ICP/MS 11.17ICP/MS 0.7 ICP/MS 1.7 ICP/MS 3.81ICP/MS 0.7 ICP/MS 2.21 ICP/MS 4.45ICP/MS 0.7 ICP/MS 2.03 ICP/MS 4.76? 0.45 ? 3.66 ? 6.94? 0.43 ? 4.14 ? 6.15? 0.36 ? 3.88 ? 5.03ICP/MS 434.13 ICP/MS 39.09 ICP/MS 10.99ICP/MS 35.8915 ICP/MS 38.8 ICP/MS 8.9ICP/MS 43.365 ICP/MS 49.28 ICP/MS 9.66GFAA 0.3265 GFAA 7.42 ICP/AES 3.36GFAA 0.0665 GFAA 9.34 ICP/AES 3.76GFAA 0.0955 GFAA 6.22 ICP/AES 2.66ICP/MS0.234ICP/MS1.989ICP/MS1.941**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateSCMilliken-DeweyD30Sample #28/12/2009SCMilliken-DeweyD30Sample #38/12/2009MNGPDuluthEU33 Boiler #319/10/2009MNGPDuluthEU33 Boiler #329/10/2009MNGPDuluthEU33 Boiler #339/10/2009TNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86111/17/2009TNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86211/17/2009TNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86311/18/2009Be LabAnalysisCd Catch(μg)Cd LabAnalysisCr Catch(μg)Cr LabAnalysisPb Catch(μg)ICP/MS0.221ICP/MS1.95ICP/MS1.32ICP/MS0.255ICP/MS1.735ICP/MS1.243ICP/MS0.43ICP/MS3.98ICP/MS3.44ICP/MS0.22ICP/MS3.81ICP/MS2.34ICP/MS0.26ICP/MS3.61ICP/MS2.11ICP/MS0.25ICP/MS5.73ICP/MS27.54ICP/MS0.278ICP/MS5.79ICP/MS99.62ICP/MS0.25ICP/MS5.26ICP/MS32.03**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateAKDoyonUtilities_AK 4 Sample #1 8/17/2005AKDoyonUtilities_AK 4 Sample #2 8/17/2005AKDoyonUtilities_AK 4 Sample #3 8/17/2005AKDoyonUtilities_AK 7 Sample #1 8/16/2005AKDoyonUtilities_AK 7 Sample #2 8/16/2005AKDoyonUtilities_AK 7 Sample #3 8/16/2005ALIPCourtlandNo. 3 Combination Boier / 11Cu301Sample #1 7/7/2009ALIPCourtlandNo. 3 Combination Boier / 11Cu301Sample #2 7/7/2009ALIPCourtlandNo. 3 Combination Boier / 11Cu301Sample #3 7/8/2009ARAnthonyForestProducts SN-12 1 9/1/2009ARAnthonyForestProducts SN-12 2 9/1/2009ARAnthonyForestProducts SN-12 3 9/2/2009ARLeolaLumberMill SN-01A Sample #1 6/14/2006ARLeolaLumberMill SN-01A Sample #2 6/14/2006ARLeolaLumberMill SN-01A Sample #3 6/14/2006ARLeolaLumberMill SN-01B Sample #1 6/14/2006ARLeolaLumberMill SN-01B Sample #2 6/14/2006ARLeolaLumberMill SN-01B Sample #3 6/14/2006ARPotlatchForestWarren Wellons Boiler 1 9/9/2009ARPotlatchForestWarren Wellons Boiler 2 9/9/2009ARPotlatchForestWarren Wellons Boiler 3 9/9/2009FLSugarCaneGrowersCoop Boiler No. 8 Sample #1 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #2 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #3 1/19/2005GAGPMadisonPly800 Wood Waste Boiler1 8/11/2009GAGPMadisonPly800 Wood Waste Boiler2 8/12/2009Pb LabAnalysisMn Catch(μg)Mn LabAnalysisNi Catch(μg)Ni LabAnalysisSe Catch(μg)ICP/MS 3 ICP/MS 2.3 ICP/MS 5ICP/MS 3.5 ICP/MS 3.7 ICP/MS 4ICP/MS 2.6 ICP/MS 2.7 ICP/MS 4ICP/MS 47.5 ICP/MS 5.55 ICP/MS 4ICP/MS 40 ICP/MS 3.6 ICP/MS 4ICP/MS 92 ICP/MS 2.3 ICP/MS 4ICP/MS 3.31 ICP/MS 0.92 ICP/MS 0.4065ICP/MS 4.21 ICP/MS 0.19 ICP/MS 3.082ICP/MS 2.07 ICP/MS 0.4 ICP/MS 3.142ICP/MS 11359.12 ICP/MS 25.62 ICP/MS 5.5ICP/MS 13896.81 ICP/MS 31.27 ICP/MS 7.24ICP/MS 12899.31 ICP/MS 28 ICP/MS 5.5ICP/MS 15.5 ICP/MS 3 ICP/MS 5.5ICP/MS 18.7 ICP/MS 3.7 ICP/MS 5.5ICP/MS 11.41 ICP/MS 2.5 ICP/MS 5.5ICP/MS 50.21 ICP/MS 3.8 ICP/MS 5.5ICP/MS 46.51 ICP/MS 1.3 ICP/MS 5.5ICP/MS 47.51 ICP/MS 5.5 ICP/MS 5.5ICP/MS 2075.173 ICP/MS 10.685 ICP/MS 0.2ICP/MS 199.453 ICP/MS 1.795 ICP/MS 0.2ICP/MS 78.353 ICP/MS 1.395 ICP/MS 0.2? ? ? 6.3? ? ? 6.3? ? ? 1.6ICP/MS 18.46 ICP/MS 46.041 ICP/MS 7.52ICP/MS 23.95 ICP/MS 88.355 ICP/MS 6.235**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateGAGPMadisonPly800 Wood Waste Boiler3 8/12/2009GATempleInlandRome WF 1 7/27/2009GATempleInlandRome WF 2 7/28/2009GATempleInlandRome WF 3 7/28/2009HIPuuneneSugarMill Boiler 1 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 1 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 1 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 1 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 2 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 2 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 2 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 3 Sample #1 5/23/2006HIPuuneneSugarMill Boiler 3 Sample #2 5/24/2006HIPuuneneSugarMill Boiler 3 Sample #3 5/25/2006HIPuuneneSugarMill Boiler 3 Sample #1 7/16/2007HIPuuneneSugarMill Boiler 3 Sample #2 7/17/2007HIPuuneneSugarMill Boiler 3 Sample #3 7/17/2007IARoquetteAmericaCirculating Fluidized Bed Boiler (121)1 6/3/2009IARoquetteAmericaCirculating Fluidized Bed Boiler (121)2 6/3/2009IARoquetteAmericaCirculating Fluidized Bed Boiler (121)3 6/4/2009IAUofNorthernIowa Boiler #3 4 10/6/2009Pb LabAnalysisMn Catch(μg)Mn LabAnalysisNi Catch(μg)Ni LabAnalysisSe Catch(μg)ICP/MS 34.42 ICP/MS 75.48 ICP/MS 4.847ICP/MS 366.77 ICP/MS 8.95 ICP/MS 2.5ICP/MS 429.9 ICP/MS 8.95 ICP/MS 2.5ICP/MS 358.18 ICP/MS 9.25 ICP/MS 2.5ICP/AES 370 ICP/AES 22 ICP/AES 0.28ICP/AES 180 ICP/AES 8.4 ICP/AES 0.28ICP/AES 880 ICP/AES 75 ICP/AES 0.28ICP/AES 370 ICP/AES 22 ICP/AES 0.28ICP/AES 180 ICP/AES 8.4 ICP/AES 0.28ICP/AES 880 ICP/AES 75 ICP/AES 0.28ICP/AES 15.2 ICP/AES 17 ICP/AES 6.73ICP/AES 13.6 ICP/AES 15.8 ICP/AES 6.43ICP/AES 9.1 ICP/AES 14.8 ICP/AES 6.63? 59.9 ? 10.79 ? 29.69**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateIAUofNorthernIowa Boiler #3 5 10/6/2009IAUofNorthernIowa Boiler #3 6 10/7/2009IDAmalgamatedSugarCoTwinFallsS-B1 Sample #1 9/26/2006IDAmalgamatedSugarCoTwinFallsS-B1 Sample #2 9/26/2006IDAmalgamatedSugarCoTwinFallsS-B1 Sample #3 9/26/2006IDPotlatch PB-1 CE Sample #1 7/20/2006IDPotlatch PB-1 CE Sample #2 7/20/2006IDPotlatch PB-1 CE Sample #3 7/20/2006IDPotlatch PB-1 CE M29-R1 7/28/2009IDPotlatch PB-1 CE M29-R2 7/28/2009IDPotlatch PB-1 CE M29-R3 7/29/2009IDPotlatch PB-2 Riley Sample #1 7/27/2006IDPotlatch PB-2 Riley Sample #2 7/27/2006IDPotlatch PB-2 Riley Sample #3 7/27/2006IDTASCONampaBabcock and Wilcox (B&W) #1Sample #1 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #1Sample #2 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #1Sample #3 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #2Sample #1 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #2Sample #2 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #2Sample #3 12/4/2006ILPolyOne B1 Sample #1 11/14/2006ILPolyOne B1 Sample #2 11/14/2006ILPolyOne B1 Sample #3 11/14/2006ILPolyOne B1 1 9/9/2009ILPolyOne B1 2 9/9/2009ILPolyOne B1 3 9/10/2009Pb LabAnalysisMn Catch(μg)Mn LabAnalysisNi Catch(μg)Ni LabAnalysisSe Catch(μg)? 53.8 ? 20.87 ? 55.95? 69.2 ? 16.47 ? 49.91ICP/AES 64.95 ICP/AES 94.7 ICP/AES 5.1ICP/AES 52.47 ICP/AES 41.7 ICP/AES 5.2ICP/AES 83.5 ICP/AES 16.7 ICP/AES 7.2ICP/MS 16.88 ICP/MS 2 ICP/MS 25.3ICP/MS 19.53 ICP/MS 0.9 ICP/MS 16.5ICP/MS 17.82 ICP/MS 1.3 ICP/MS 7.9GFAA 10.6 ICP/AES 15.4 ICP/AES 29.1GFAA 11.9 ICP/AES 18.3 ICP/AES 54.2GFAA 8.8 ICP/AES 17.5 ICP/AES 20.9GFAA 10.6 ICP/AES 15.4 ICP/AES 29.1GFAA 11.9 ICP/AES 18.3 ICP/AES 54.2GFAA 8.8 ICP/AES 17.5 ICP/AES 20.9ICP/MS 12.2 ICP/MS 4.3 ICP/MS 7.527.4 4.8 7.56 4.4 7.5ICP/MS 9.6 ICP/MS 5.7 ICP/MS 7ICP/MS 10.5 ICP/MS 5.4 ICP/MS 7ICP/MS 11.5 ICP/MS 5.5 ICP/MS 7**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateINSABICInnovativePlastics 01-001 BW1 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #3 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #3 6/28/2006INTateLyleSagamore 31B1 M29-1 9/1/2009INTateLyleSagamore 31B1 M29-2 9/2/2009INTateLyleSagamore 31B1 M29-3 9/3/2009MNHibbing Unit 1A Sample #1 9/21/2004MNHibbing Unit 1A Sample #2 9/21/2004MNHibbing Unit 1A Sample #3 9/21/2004MNHibbing Unit 2A Sample #1 9/22/2004MNHibbing Unit 2A Sample #2 9/22/2004MNHibbing Unit 2A Sample #3 9/22/2004MSGPNewAugusta AA-015 Power Boiler Sample #1 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #2 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #3 7/12/2006MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #1 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #2 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #3 8/5/2009NDCargillWestFargoFoster Wheeler Boiler (EU43)1 8/26/2009NDCargillWestFargoFoster Wheeler Boiler (EU43)2 8/26/2009NDCargillWestFargoFoster Wheeler Boiler (EU43)3 8/27/2009OKGPMuskogeeMill B-4 Sample #1 4/16/2003OKGPMuskogeeMill B-4 Sample #2 4/16/2003Pb LabAnalysisMn Catch(μg)Mn LabAnalysisNi Catch(μg)Ni LabAnalysisSe Catch(μg)ICP/AES 11.9 ICP/AES 20.4 ICP/AES 86ICP/AES 6 ICP/AES 15.4 ICP/AES 78ICP/AES 10 ICP/AES 16.7 ICP/AES 63ICP/AES 11.9 ICP/AES 20.4 ICP/AES 86ICP/AES 6 ICP/AES 15.4 ICP/AES 78ICP/AES 10 ICP/AES 16.7 ICP/AES 63ICP/MS 45.75 ICP/MS 77.28 ICP/MS 65.01ICP/MS 43.62 ICP/MS 85.63 ICP/MS 55.46ICP/MS 24.11 ICP/MS 36.4 ICP/MS 37.72ICP/AES 4 ICP/AES 4.8 ICP/AES 5.5ICP/AES 3.9 ICP/AES 2.6 ICP/AES 5ICP/AES 3.8 ICP/AES 1.5 ICP/AES 5.8ICP/AES 5.7 ICP/AES 6.3 ICP/AES 5.5ICP/AES 6.3 ICP/AES 3.2 ICP/AES 6.8ICP/AES 8.9 ICP/AES 4.4 ICP/AES 5.8ICP/MS 82.805 ICP/MS 2.405 ICP/MS 3.5ICP/MS 13.675 ICP/MS 0.825 ICP/MS 3.5ICP/MS 16.07 ICP/MS 1.035 ICP/MS 3.5ICP/MS 234.1725 ICP/MS 4.118 ICP/MS 1.097ICP/MS 355.35 ICP/MS 3.098 ICP/MS 1.584ICP/MS 144.1825 ICP/MS 0.648 ICP/MS 0.7ICP/AES 12.47 ICP/AES 1.21 ICP/AES 7.43ICP/AES 17.85 ICP/AES 1.53 ICP/AES 12.33ICP/AES 10.98 ICP/AES 2.73 ICP/AES 8.83ICP/MS 15 ICP/MS 29 ICP/MS 1.1ICP/MS 12 ICP/MS 15 ICP/MS 1**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateOKGPMuskogeeMill B-4 Sample #3 4/16/2003SCMarlboroPaper Hogged Fuel Boiler Sample #1 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #2 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #3 7/14/2009TNBowaterNewsprintBubbling Fluidized Bed BoilerSample #1 10/6/2005TNBowaterNewsprintBubbling Fluidized Bed BoilerSample #2 10/6/2005TNBowaterNewsprintBubbling Fluidized Bed BoilerSample #3 10/6/2005TNBowaterNewsprintBubbling Fluidized Bed Boiler1 8/4/2009TNBowaterNewsprintBubbling Fluidized Bed Boiler2 8/4/2009TNBowaterNewsprintBubbling Fluidized Bed Boiler3 8/5/2009TNEastman_NO_CBIDATA Boiler 30 1 8/26/2009TNEastman_NO_CBIDATA Boiler 30 2 8/27/2009TNEastman_NO_CBIDATA Boiler 30 3 8/27/2009TXDibollTemple-Inland PB-44 Sample #1 6/29/2007TXDibollTemple-Inland PB-44 Sample #2 6/29/2007VAGeorgiaPacificBrooknealGladys5600 Sample #1 7/6/2006VAGeorgiaPacificBrooknealGladys5600 Sample #2 7/6/2006VAGeorgiaPacificBrooknealGladys5600 Sample #3 7/6/2006VAUniversityofVirginia 7103-1-01R M29-1 9/17/2009VAUniversityofVirginia 7103-1-01R M29-2 9/17/2009VAUniversityofVirginia 7103-1-01R M29-3 9/18/2009VAVirginiaPolytechnic Boiler 11 Sample #1 2/27/2007VAVirginiaPolytechnic Boiler 11 Sample #1VAVirginiaPolytechnic Boiler 11 Sample #2VAVirginiaPolytechnic Boiler 7 Sample #3 2/28/2007VAVirginiaPolytechnic Boiler 7 Sample #1Pb LabAnalysisMn Catch(μg)Mn LabAnalysisNi Catch(μg)Ni LabAnalysisSe Catch(μg)ICP/MS 20 ICP/MS 31 ICP/MS 1ICP/MS 7.727 ICP/MS 3.387 ICP/MS 5.72ICP/MS 10.748 ICP/MS 5.447 ICP/MS 8.04ICP/MS 9.568 ICP/MS -0.133 ICP/MS 1.179ICP/MS 153 ICP/MS 19.2 ICP/MS 22ICP/MS 201 ICP/MS 13.9 ICP/MS 2ICP/MS 130 ICP/MS 10 ICP/MS 5ICP/MS 2522.5 ICP/MS 25.51 ICP/MS 10.5ICP/MS 2641.88 ICP/MS 27.65 ICP/MS 11.51ICP/MS 1482.1 ICP/MS 10.39 ICP/MS 10.5ICP/MS 12.27 ICP/MS 8.72 ICP/MS 7.3ICP/MS 11.97 ICP/MS 7.82 ICP/MS 7ICP/MS 6.97 ICP/MS 5.22 ICP/MS 7ICP/MS 77.71 ICP/MS 0.97 ICP/MS 0.2ICP/MS 437 ICP/MS 2.56 ICP/MS 0.2ICP/MS 96.9 ICP/MS 0.6 ICP/MS 0.82ICP/MS 47.88 ICP/MS 0.71 ICP/MS 0.2ICP/MS 115.9 ICP/MS 0.18 ICP/MS 0.25ICP/MS 37.824 ICP/MS 5.072 ICP/MS 4.31ICP/MS 30.264 ICP/MS 11.623 ICP/MS 4.456ICP/MS 19.264 ICP/MS 21.802 ICP/MS 1.3GFAA 48.14 GFAA 10.74 GFAA 10.665.335 6.735 16.211.89 6.04 7.8GFAA 26.385 GFAA 4.63 GFAA 5.426.14 7.935 6.9**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateVAVirginiaPolytechnic Boiler 7 Sample #1WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #1 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #2 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #3 8/12/2009WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #1 7/21/2005WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #2 7/21/2005WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #3 7/22/2005WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #1 8/20/2009WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #2 8/20/2009WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #3 8/21/2009WINewPageBiron B24 Sample #1 9/12/2007WINewPageBiron B24 Sample #2 9/12/2007WINewPageBiron B24 Sample #3 9/12/2007WINewPageBiron B24 1 9/22/2009WINewPageBiron B24 2 9/22/2009WINewPageBiron B24 3 9/23/2009WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #1 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #2 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #3 9/18/2003WVMountainStateCarbonFollansbeeS1 Sample #1 10/19/2009WVMountainStateCarbonFollansbeeS1 Sample #2 10/19/2009WVMountainStateCarbonFollansbeeS1 Sample #3 10/20/2009WVPPGMartinsville R011-Boiler 3 1 7/22/2009WVPPGMartinsville R011-Boiler 3 2 7/23/2009WVPPGMartinsville R011-Boiler 3 3 7/23/2009SCMilliken-DeweyD30Sample #18/12/2009Pb LabAnalysisMn Catch(μg)Mn LabAnalysisNi Catch(μg)Ni LabAnalysisSe Catch(μg)17.77 4.23 5? 65.2 ? 4.1 ? 1.6? 45.2 ? 1.3 ? 1.1? 30.7 ? 2.1 ? 1.3ICP/MS 7.43 ICP/MS 10.6 ICP/MS 0.909ICP/MS 11.7 ICP/MS 14.8 ICP/MS 0.5ICP/MS 46.1 ICP/MS 7.17 ICP/MS 0.981ICP/MS 12.23 ICP/MS 6.56 ICP/MS 1.28ICP/MS 6.01 ICP/MS 4.61 ICP/MS 0.404ICP/MS 28.42 ICP/MS 3.99 ICP/MS 0.2ICP/MS 5.63 ICP/MS 6.46 ICP/MS 23.1ICP/MS 84.43 ICP/MS 5.26 ICP/MS 29.9ICP/MS 96.43 ICP/MS 4.16 ICP/MS 22.6ICP/MS 36.7 ICP/MS 4.19 ICP/MS 30.3ICP/MS 9.2 ICP/MS 3.69 ICP/MS 29.3ICP/MS 9.5 ICP/MS 3.69 ICP/MS 21.5? 35.14 ? 3.14 ? 0.34? 31.2 ? 3.18 ? 0.34? 29.81 ? 2.77 ? 0.34ICP/MS 28.15 ICP/MS 46.47 ICP/MS 29.9ICP/MS 60.7 ICP/MS 22.67 ICP/MS 24.6ICP/MS 25.69 ICP/MS 23.67 ICP/MS 24.3GFAA 9.999 ICP/AES 9.528 ICP/AES 54.15GFAA 15.885 ICP/AES 14.486 ICP/AES 87.4GFAA 12.07 ICP/AES 8.777 ICP/AES 172.2ICP/MS6.4ICP/MS2.545ICP/MS0.282**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateSCMilliken-DeweyD30Sample #28/12/2009SCMilliken-DeweyD30Sample #38/12/2009MNGPDuluthEU33 Boiler #319/10/2009MNGPDuluthEU33 Boiler #329/10/2009MNGPDuluthEU33 Boiler #339/10/2009TNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86111/17/2009TNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86211/17/2009TNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86311/18/2009Pb LabAnalysisMn Catch(μg)Mn LabAnalysisNi Catch(μg)Ni LabAnalysisSe Catch(μg)ICP/MS4.81ICP/MS1.959ICP/MS0.54ICP/MS3.94ICP/MS2.499ICP/MS0.255ICP/MS27.71ICP/MS22.61ICP/MS0.54ICP/MS30.42ICP/MS27.09ICP/MS0.54ICP/MS12.59ICP/MS12.36ICP/MS0.54ICP/MS12.97ICP/MS5.77ICP/MS2.61ICP/MS6.25ICP/MS6.41ICP/MS2.5ICP/MS18.2ICP/MS5.8ICP/MS2.5**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateAKDoyonUtilities_AK 4 Sample #1 8/17/2005AKDoyonUtilities_AK 4 Sample #2 8/17/2005AKDoyonUtilities_AK 4 Sample #3 8/17/2005AKDoyonUtilities_AK 7 Sample #1 8/16/2005AKDoyonUtilities_AK 7 Sample #2 8/16/2005AKDoyonUtilities_AK 7 Sample #3 8/16/2005ALIPCourtlandNo. 3 Combination Boier / 11Cu301Sample #1 7/7/2009ALIPCourtlandNo. 3 Combination Boier / 11Cu301Sample #2 7/7/2009ALIPCourtlandNo. 3 Combination Boier / 11Cu301Sample #3 7/8/2009ARAnthonyForestProducts SN-12 1 9/1/2009ARAnthonyForestProducts SN-12 2 9/1/2009ARAnthonyForestProducts SN-12 3 9/2/2009ARLeolaLumberMill SN-01A Sample #1 6/14/2006ARLeolaLumberMill SN-01A Sample #2 6/14/2006ARLeolaLumberMill SN-01A Sample #3 6/14/2006ARLeolaLumberMill SN-01B Sample #1 6/14/2006ARLeolaLumberMill SN-01B Sample #2 6/14/2006ARLeolaLumberMill SN-01B Sample #3 6/14/2006ARPotlatchForestWarren Wellons Boiler 1 9/9/2009ARPotlatchForestWarren Wellons Boiler 2 9/9/2009ARPotlatchForestWarren Wellons Boiler 3 9/9/2009FLSugarCaneGrowersCoop Boiler No. 8 Sample #1 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #2 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #3 1/19/2005GAGPMadisonPly800 Wood Waste Boiler1 8/11/2009GAGPMadisonPly800 Wood Waste Boiler2 8/12/2009Se LabAnalysisAs 3x RDLConcentration(μg/dscm)Be 3x RDLConcentration(μg/dscm)Cd 3x RDLConcentration(μg/dscm)ICP/MS 1.2 0.24 0.452381995ICP/MS 1.206898516 0.24 0.517242221ICP/MS 1.2 0.24 0.356333244ICP/MS 1.2 0.24 0.347218353ICP/MS 1.2 0.247087633 0.7412629ICP/MS 1.2 0.253335725 0.380003587ICP/MS 0.3 0.06 0.514694133ICP/MS 0.3 0.06 0.023ICP/MS 0.3 0.06 0.080830278ICP/MS 0.954383221 0.129288367 6.219945817ICP/MS 1.086578725 0.131056645 8.628292905ICP/MS 0.997550285 0.135136122 8.700309258ICP/MS 0.898371916 0.12 0.877954372ICP/MS 0.923509414 0.12 1.334890881ICP/MS 0.918943534 0.12 0.517949992ICP/MS 0.86824313 0.12 2.72312618ICP/MS 0.830621365 0.12 0.366228511ICP/MS 0.859388308 0.12 0.47656988ICP/MS 1.28400342 0.06 1.529300516ICP/MS 0.3 0.06 0.096678997ICP/MS 0.3 0.06 0.089301067???ICP/MS 0.312591829 0.06 0.636661112ICP/MS 0.434956138 0.06 0.669339617**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateGAGPMadisonPly800 Wood Waste Boiler3 8/12/2009GATempleInlandRome WF 1 7/27/2009GATempleInlandRome WF 2 7/28/2009GATempleInlandRome WF 3 7/28/2009HIPuuneneSugarMill Boiler 1 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 1 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 1 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 1 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 2 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 2 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 2 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 3 Sample #1 5/23/2006HIPuuneneSugarMill Boiler 3 Sample #2 5/24/2006HIPuuneneSugarMill Boiler 3 Sample #3 5/25/2006HIPuuneneSugarMill Boiler 3 Sample #1 7/16/2007HIPuuneneSugarMill Boiler 3 Sample #2 7/17/2007HIPuuneneSugarMill Boiler 3 Sample #3 7/17/2007IARoquetteAmericaCirculating Fluidized Bed Boiler (121)1 6/3/2009IARoquetteAmericaCirculating Fluidized Bed Boiler (121)2 6/3/2009IARoquetteAmericaCirculating Fluidized Bed Boiler (121)3 6/4/2009IAUofNorthernIowa Boiler #3 4 10/6/2009Se LabAnalysisAs 3x RDLConcentration(μg/dscm)Be 3x RDLConcentration(μg/dscm)Cd 3x RDLConcentration(μg/dscm)ICP/MS 0.3 0.06 0.231475283ICP/MS 2.886535356 0.08 0.145500156ICP/MS 1.321194885 0.08 0.120884838ICP/MS 2.174254887 0.08 0.116709507ICP/AES #N/A #N/A #N/AICP/AES #N/A #N/A #N/AICP/AES #N/A #N/A #N/AICP/AES #N/A #N/A #N/AICP/AES #N/A #N/A #N/AICP/AES #N/A #N/A #N/AICP/AES 19 0.11 1.5ICP/AES 19 0.11 1.69969474ICP/AES 19 0.11 1.5? #VALUE! #VALUE! #VALUE!**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateIAUofNorthernIowa Boiler #3 5 10/6/2009IAUofNorthernIowa Boiler #3 6 10/7/2009IDAmalgamatedSugarCoTwinFallsS-B1 Sample #1 9/26/2006IDAmalgamatedSugarCoTwinFallsS-B1 Sample #2 9/26/2006IDAmalgamatedSugarCoTwinFallsS-B1 Sample #3 9/26/2006IDPotlatch PB-1 CE Sample #1 7/20/2006IDPotlatch PB-1 CE Sample #2 7/20/2006IDPotlatch PB-1 CE Sample #3 7/20/2006IDPotlatch PB-1 CE M29-R1 7/28/2009IDPotlatch PB-1 CE M29-R2 7/28/2009IDPotlatch PB-1 CE M29-R3 7/29/2009IDPotlatch PB-2 Riley Sample #1 7/27/2006IDPotlatch PB-2 Riley Sample #2 7/27/2006IDPotlatch PB-2 Riley Sample #3 7/27/2006IDTASCONampaBabcock and Wilcox (B&W) #1Sample #1 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #1Sample #2 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #1Sample #3 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #2Sample #1 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #2Sample #2 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #2Sample #3 12/4/2006ILPolyOne B1 Sample #1 11/14/2006ILPolyOne B1 Sample #2 11/14/2006ILPolyOne B1 Sample #3 11/14/2006ILPolyOne B1 1 9/9/2009ILPolyOne B1 2 9/9/2009ILPolyOne B1 3 9/10/2009Se LabAnalysisAs 3x RDLConcentration(μg/dscm)Be 3x RDLConcentration(μg/dscm)Cd 3x RDLConcentration(μg/dscm)? #VALUE! #VALUE! #VALUE!? #VALUE! #VALUE! #VALUE!ICP/AES 29 0.17 2.3ICP/AES 29 0.17 2.3ICP/AES 29 0.17 2.3ICP/MS 0.3 0.06 0.06641487ICP/MS 0.3 0.06 0.134474224ICP/MS 0.3 0.06 0.028506364GFAA 0.6 0.17 2.851024153GFAA 0.6 0.17 2.3GFAA 0.6 0.443188659 2.3GFAA 0.6 0.17 2.851024153GFAA 0.6 0.17 2.3GFAA 0.6 0.17 2.3ICP/MS 1.265921854 0.316480464 0.316480464#DIV/0! #DIV/0! #DIV/0!#DIV/0! #DIV/0! #DIV/0!ICP/MS 0.574217638 0.14355441 0.147655964ICP/MS 0.600836098 0.150209025 0.150209025ICP/MS 0.596944104 0.166291572 0.149236026**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateINSABICInnovativePlastics 01-001 BW1 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #3 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #3 6/28/2006INTateLyleSagamore 31B1 M29-1 9/1/2009INTateLyleSagamore 31B1 M29-2 9/2/2009INTateLyleSagamore 31B1 M29-3 9/3/2009MNHibbing Unit 1A Sample #1 9/21/2004MNHibbing Unit 1A Sample #2 9/21/2004MNHibbing Unit 1A Sample #3 9/21/2004MNHibbing Unit 2A Sample #1 9/22/2004MNHibbing Unit 2A Sample #2 9/22/2004MNHibbing Unit 2A Sample #3 9/22/2004MSGPNewAugusta AA-015 Power Boiler Sample #1 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #2 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #3 7/12/2006MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #1 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #2 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #3 8/5/2009NDCargillWestFargoFoster Wheeler Boiler (EU43)1 8/26/2009NDCargillWestFargoFoster Wheeler Boiler (EU43)2 8/26/2009NDCargillWestFargoFoster Wheeler Boiler (EU43)3 8/27/2009OKGPMuskogeeMill B-4 Sample #1 4/16/2003OKGPMuskogeeMill B-4 Sample #2 4/16/2003Se LabAnalysisAs 3x RDLConcentration(μg/dscm)Be 3x RDLConcentration(μg/dscm)Cd 3x RDLConcentration(μg/dscm)GFAA 4.311871798 0.346489698 2.3GFAA 3.93828551 0.252050273 2.3GFAA 4.079310624 0.224362084 2.3GFAA 4.311871798 0.346489698 2.3GFAA 3.93828551 0.252050273 2.3GFAA 4.079310624 0.224362084 2.3ICP/MS 1.164927281 0.735455966 0.378328166ICP/MS 1.120226066 0.748929417 0.391318789ICP/MS 0.789123625 0.463801729 0.24841802ICP/AES 57 0.460910989 4.5ICP/AES 57 0.449300254 4.5ICP/AES 57 0.431512708 4.5ICP/AES 57 0.493088523 4.5ICP/AES 57 0.471747262 4.5ICP/AES 57 0.465038188 4.5ICP/MS 1.003732599 0.179237964 0.20074652ICP/MS 0.88938658 0.222346645 0.134678539ICP/MS 0.817930191 0.201602512 0.087553091ICP/MS 0.4 0.08 0.203635982ICP/MS 0.4 0.08 0.244796981ICP/MS 0.4 0.08 0.2071585ICP/AES 14 0.089344982 1.1ICP/AES 14 0.083751195 1.290291849ICP/AES 14 0.083 1.124885076ICP/MS 0.6 0.12 0.125690586ICP/MS 0.6 0.12 0.824789219**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateOKGPMuskogeeMill B-4 Sample #3 4/16/2003SCMarlboroPaper Hogged Fuel Boiler Sample #1 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #2 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #3 7/14/2009TNBowaterNewsprintBubbling Fluidized Bed BoilerSample #1 10/6/2005TNBowaterNewsprintBubbling Fluidized Bed BoilerSample #2 10/6/2005TNBowaterNewsprintBubbling Fluidized Bed BoilerSample #3 10/6/2005TNBowaterNewsprintBubbling Fluidized Bed Boiler1 8/4/2009TNBowaterNewsprintBubbling Fluidized Bed Boiler2 8/4/2009TNBowaterNewsprintBubbling Fluidized Bed Boiler3 8/5/2009TNEastman_NO_CBIDATA Boiler 30 1 8/26/2009TNEastman_NO_CBIDATA Boiler 30 2 8/27/2009TNEastman_NO_CBIDATA Boiler 30 3 8/27/2009TXDibollTemple-Inland PB-44 Sample #1 6/29/2007TXDibollTemple-Inland PB-44 Sample #2 6/29/2007VAGeorgiaPacificBrooknealGladys5600 Sample #1 7/6/2006VAGeorgiaPacificBrooknealGladys5600 Sample #2 7/6/2006VAGeorgiaPacificBrooknealGladys5600 Sample #3 7/6/2006VAUniversityofVirginia 7103-1-01R M29-1 9/17/2009VAUniversityofVirginia 7103-1-01R M29-2 9/17/2009VAUniversityofVirginia 7103-1-01R M29-3 9/18/2009VAVirginiaPolytechnic Boiler 11 Sample #1 2/27/2007VAVirginiaPolytechnic Boiler 11 Sample #1VAVirginiaPolytechnic Boiler 11 Sample #2VAVirginiaPolytechnic Boiler 7 Sample #3 2/28/2007VAVirginiaPolytechnic Boiler 7 Sample #1Se LabAnalysisAs 3x RDLConcentration(μg/dscm)Be 3x RDLConcentration(μg/dscm)Cd 3x RDLConcentration(μg/dscm)ICP/MS 0.6 0.12 0.045ICP/MS 0.4 0.08 0.102729132ICP/MS 0.4 0.08 0.112469807ICP/MS 0.4 0.08 0.062615248ICP/MS 1.863195104 0.24 0.538256363ICP/MS 1.201438587 0.24 0.514902251ICP/MS 1.344991748 0.24 0.358664466ICP/MS 3.573645713 0.226589855 0.550937047ICP/MS 3.532568364 0.243865666 0.604090093ICP/MS 1.808559217 0.232719017 0.321373881ICP/MS 1.66154462 0.163109747 0.16745934ICP/MS 0.888840153 0.151016531 0.140229636ICP/MS 0.881850089 0.149466117 0.232740096ICP/MS 0.6 0.12 0.125206871ICP/MS 0.6 0.12 0.11270659ICP/MS 1.2 0.24 0.758896809ICP/MS 1.2 0.24 0.291674079ICP/MS 1.2 0.24 0.325893456ICP/MS 0.3 0.06 0.093102818ICP/MS 0.320560703 0.06 0.10185457ICP/MS 0.3 0.06 0.066377356GFAA 2.853056702 0.203789764 1.255344949#DIV/0! #DIV/0! #DIV/0!#DIV/0! #DIV/0! #DIV/0!GFAA 1.588084801 0.12 1.952915093#DIV/0! #DIV/0! #DIV/0!**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateVAVirginiaPolytechnic Boiler 7 Sample #1WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #1 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #2 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #3 8/12/2009WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #1 7/21/2005WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #2 7/21/2005WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #3 7/22/2005WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #1 8/20/2009WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #2 8/20/2009WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #3 8/21/2009WINewPageBiron B24 Sample #1 9/12/2007WINewPageBiron B24 Sample #2 9/12/2007WINewPageBiron B24 Sample #3 9/12/2007WINewPageBiron B24 1 9/22/2009WINewPageBiron B24 2 9/22/2009WINewPageBiron B24 3 9/23/2009WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #1 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #2 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #3 9/18/2003WVMountainStateCarbonFollansbeeS1 Sample #1 10/19/2009WVMountainStateCarbonFollansbeeS1 Sample #2 10/19/2009WVMountainStateCarbonFollansbeeS1 Sample #3 10/20/2009WVPPGMartinsville R011-Boiler 3 1 7/22/2009WVPPGMartinsville R011-Boiler 3 2 7/23/2009WVPPGMartinsville R011-Boiler 3 3 7/23/2009SCMilliken-DeweyD30Sample #18/12/2009Se LabAnalysisAs 3x RDLConcentration(μg/dscm)Be 3x RDLConcentration(μg/dscm)Cd 3x RDLConcentration(μg/dscm)#DIV/0! #DIV/0! #DIV/0!? #VALUE! #VALUE! #VALUE!? #VALUE! #VALUE! #VALUE!? #VALUE! #VALUE! #VALUE!ICP/MS 1.2 0.24 2.413286474ICP/MS 5.466743266 0.24 1.42119175ICP/MS 1.2 0.24 1.333381455ICP/MS 0.3 0.06 0.407628296ICP/MS 0.3 0.06 0.377873391ICP/MS 0.3 0.06 0.411362169ICP/MS 1.965834866 0.210926488 0.686214174ICP/MS 2.07058027 0.232127833 0.45806559ICP/MS 1.602836902 0.236174396 0.639245365ICP/MS 0.822932787 0.147705885 0.147705885ICP/MS 1.129079754 0.166390701 0.166390701ICP/MS 1.064109008 0.164795643 0.164795643? #VALUE! #VALUE! #VALUE!? #VALUE! #VALUE! #VALUE!? #VALUE! #VALUE! #VALUE!ICP/MS 4.542233465 0.097333574 93.90094352ICP/MS 7.43862202 0.127762592 10.19020238ICP/MS 5.316559449 0.110761655 10.6737315GFAA 3.780047612 0.070796878 0.082554217GFAA 2.11511855 0.064409308 0.023GFAA 3.362947453 0.075632553 0.025796103ICP/MS 1.202445347 0.08 0.053290192**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateSCMilliken-DeweyD30Sample #28/12/2009SCMilliken-DeweyD30Sample #38/12/2009MNGPDuluthEU33 Boiler #319/10/2009MNGPDuluthEU33 Boiler #329/10/2009MNGPDuluthEU33 Boiler #339/10/2009TNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86111/17/2009TNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86211/17/2009TNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86311/18/2009Se LabAnalysisAs 3x RDLConcentration(μg/dscm)Be 3x RDLConcentration(μg/dscm)Cd 3x RDLConcentration(μg/dscm)ICP/MS 0.687140836 0.08 0.057218585ICP/MS 0.452208864 0.08 0.064062922ICP/MS 0.4 0.08 0.09933571ICP/MS 0.430786831 0.08 0.05236083ICP/MS 0.4 0.08 0.06360859ICP/MS 0.3 0.06 0.052947615ICP/MS 0.304001052 0.06 0.058689092ICP/MS 0.3 0.06 0.052355749**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateAKDoyonUtilities_AK 4 Sample #1 8/17/2005AKDoyonUtilities_AK 4 Sample #2 8/17/2005AKDoyonUtilities_AK 4 Sample #3 8/17/2005AKDoyonUtilities_AK 7 Sample #1 8/16/2005AKDoyonUtilities_AK 7 Sample #2 8/16/2005AKDoyonUtilities_AK 7 Sample #3 8/16/2005ALIPCourtlandNo. 3 Combination Boier / 11Cu301Sample #1 7/7/2009ALIPCourtlandNo. 3 Combination Boier / 11Cu301Sample #2 7/7/2009ALIPCourtlandNo. 3 Combination Boier / 11Cu301Sample #3 7/8/2009ARAnthonyForestProducts SN-12 1 9/1/2009ARAnthonyForestProducts SN-12 2 9/1/2009ARAnthonyForestProducts SN-12 3 9/2/2009ARLeolaLumberMill SN-01A Sample #1 6/14/2006ARLeolaLumberMill SN-01A Sample #2 6/14/2006ARLeolaLumberMill SN-01A Sample #3 6/14/2006ARLeolaLumberMill SN-01B Sample #1 6/14/2006ARLeolaLumberMill SN-01B Sample #2 6/14/2006ARLeolaLumberMill SN-01B Sample #3 6/14/2006ARPotlatchForestWarren Wellons Boiler 1 9/9/2009ARPotlatchForestWarren Wellons Boiler 2 9/9/2009ARPotlatchForestWarren Wellons Boiler 3 9/9/2009FLSugarCaneGrowersCoop Boiler No. 8 Sample #1 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #2 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #3 1/19/2005GAGPMadisonPly800 Wood Waste Boiler1 8/11/2009GAGPMadisonPly800 Wood Waste Boiler2 8/12/2009Cr 3x RDLConcentration(μg/dscm)Pb 3x RDLConcentration(μg/dscm)Mn 3x RDLConcentration(μg/dscm)Ni 3x RDLConcentration(μg/dscm)0.9 1.832433397 1.717906309 161.034484442 2.873567895 2.011497526 160.9 2.25677721 1.544110722 161.909700942 1.331003687 27.48811962 162.038472975 7.350857093 24.70876334 161.393346485 2.21668759 58.26721664 160.23 0.23 0.875456105 4.10.23 0.23 1.126513688 4.10.23 0.23 0.578957352 4.14.0925645 8.989067575 2670.185598 6.022487224.861010087 8.542510374 3311.398706 7.4511659534.744506404 9.235939707 3169.38679 6.8796571370.490021045 0.534939641 6.329438496 8.11.175375618 0.705225371 7.849830021 8.10.960713694 0.45 4.765975327 8.10.513052759 0.931388085 19.81567616 8.10.528577232 0.717354815 17.56009077 8.11.015640728 0.746105304 18.55888115 8.13.365306988 6.490053652 351.0578695 4.10.653102582 0.760807778 31.8725885 4.10.738113911 0.366621472 12.72183002 4.18.184774824 1.483292113 4.154388167 10.361440178.14256228 0.3133518 5.489960211 20.25325405**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateGAGPMadisonPly800 Wood Waste Boiler3 8/12/2009GATempleInlandRome WF 1 7/27/2009GATempleInlandRome WF 2 7/28/2009GATempleInlandRome WF 3 7/28/2009HIPuuneneSugarMill Boiler 1 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 1 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 1 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 1 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 2 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 2 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 2 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 3 Sample #1 5/23/2006HIPuuneneSugarMill Boiler 3 Sample #2 5/24/2006HIPuuneneSugarMill Boiler 3 Sample #3 5/25/2006HIPuuneneSugarMill Boiler 3 Sample #1 7/16/2007HIPuuneneSugarMill Boiler 3 Sample #2 7/17/2007HIPuuneneSugarMill Boiler 3 Sample #3 7/17/2007IARoquetteAmericaCirculating Fluidized Bed Boiler (121)1 6/3/2009IARoquetteAmericaCirculating Fluidized Bed Boiler (121)2 6/3/2009IARoquetteAmericaCirculating Fluidized Bed Boiler (121)3 6/4/2009IAUofNorthernIowa Boiler #3 4 10/6/2009Cr 3x RDLConcentration(μg/dscm)Pb 3x RDLConcentration(μg/dscm)Mn 3x RDLConcentration(μg/dscm)Ni 3x RDLConcentration(μg/dscm)10.16503384 0.234788383 7.602461098 16.671521312.952245104 4.207770645 86.07272948 5.42.986170071 2.721032322 96.59552395 5.42.437931921 2.344996573 77.41298364 5.4#N/A #N/A #N/A #N/A#N/A #N/A #N/A #N/A#N/A #N/A #N/A #N/A#N/A #N/A #N/A #N/A#N/A #N/A #N/A #N/A#N/A #N/A #N/A #N/A2.5 15 3.562957161 5.42.5 15 3.166554584 5.42.5 15 2.162729738 5.4#VALUE! #VALUE! #VALUE! #VALUE!**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateIAUofNorthernIowa Boiler #3 5 10/6/2009IAUofNorthernIowa Boiler #3 6 10/7/2009IDAmalgamatedSugarCoTwinFallsS-B1 Sample #1 9/26/2006IDAmalgamatedSugarCoTwinFallsS-B1 Sample #2 9/26/2006IDAmalgamatedSugarCoTwinFallsS-B1 Sample #3 9/26/2006IDPotlatch PB-1 CE Sample #1 7/20/2006IDPotlatch PB-1 CE Sample #2 7/20/2006IDPotlatch PB-1 CE Sample #3 7/20/2006IDPotlatch PB-1 CE M29-R1 7/28/2009IDPotlatch PB-1 CE M29-R2 7/28/2009IDPotlatch PB-1 CE M29-R3 7/29/2009IDPotlatch PB-2 Riley Sample #1 7/27/2006IDPotlatch PB-2 Riley Sample #2 7/27/2006IDPotlatch PB-2 Riley Sample #3 7/27/2006IDTASCONampaBabcock and Wilcox (B&W) #1Sample #1 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #1Sample #2 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #1Sample #3 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #2Sample #1 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #2Sample #2 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #2Sample #3 12/4/2006ILPolyOne B1 Sample #1 11/14/2006ILPolyOne B1 Sample #2 11/14/2006ILPolyOne B1 Sample #3 11/14/2006ILPolyOne B1 1 9/9/2009ILPolyOne B1 2 9/9/2009ILPolyOne B1 3 9/10/2009Cr 3x RDLConcentration(μg/dscm)Pb 3x RDLConcentration(μg/dscm)Mn 3x RDLConcentration(μg/dscm)Ni 3x RDLConcentration(μg/dscm)#VALUE! #VALUE! #VALUE! #VALUE!#VALUE! #VALUE! #VALUE! #VALUE!67.48261447 23 29.27852912 42.689402743.8 23 23.10302413 18.360893963.8 23 38.01423857 8.10.287797768 0.345357322 3.73694333 4.10.268948448 0.848222027 4.040433216 4.10.745551071 0.346461968 3.907564731 4.13.8 2.316948003 4.162652344 8.13.8 1.501599821 4.467259469 8.13.8 1.254449254 3.305135759 8.13.8 2.316948003 4.162652344 8.13.8 1.501599821 4.467259469 8.13.8 1.254449254 3.305135759 8.10.949441391 1.350316645 5.148082208 8.1#DIV/0! #DIV/0! #DIV/0! #DIV/0!#DIV/0! #DIV/0! #DIV/0! #DIV/0!0.869529567 0.910545112 1.968746189 4.10.96992113 0.79610783 2.253135368 4.11.031860523 0.799478711 2.451734713 4.1**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateINSABICInnovativePlastics 01-001 BW1 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #3 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #3 6/28/2006INTateLyleSagamore 31B1 M29-1 9/1/2009INTateLyleSagamore 31B1 M29-2 9/2/2009INTateLyleSagamore 31B1 M29-3 9/3/2009MNHibbing Unit 1A Sample #1 9/21/2004MNHibbing Unit 1A Sample #2 9/21/2004MNHibbing Unit 1A Sample #3 9/21/2004MNHibbing Unit 2A Sample #1 9/22/2004MNHibbing Unit 2A Sample #2 9/22/2004MNHibbing Unit 2A Sample #3 9/22/2004MSGPNewAugusta AA-015 Power Boiler Sample #1 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #2 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #3 7/12/2006MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #1 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #2 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #3 8/5/2009NDCargillWestFargoFoster Wheeler Boiler (EU43)1 8/26/2009NDCargillWestFargoFoster Wheeler Boiler (EU43)2 8/26/2009NDCargillWestFargoFoster Wheeler Boiler (EU43)3 8/27/2009OKGPMuskogeeMill B-4 Sample #1 4/16/2003OKGPMuskogeeMill B-4 Sample #2 4/16/2003Cr 3x RDLConcentration(μg/dscm)Pb 3x RDLConcentration(μg/dscm)Mn 3x RDLConcentration(μg/dscm)Ni 3x RDLConcentration(μg/dscm)6.313812275 23 4.581363785 8.15.123709449 23 2.362971306 8.16.445310785 23 4.079310624 8.16.313812275 23 4.581363785 8.15.123709449 23 2.362971306 8.16.445310785 23 4.079310624 8.16.510916264 2.544043817 9.999141292 16.890352777.180091503 2.630250251 11.05526267 21.702479193.591490309 1.737340492 6.371657936 9.6195914097.5 45 3.687287914 167.5 45 3.504541985 167.5 45 3.279496579 167.5 45 5.621209159 167.5 45 5.944015496 167.5 45 8.277679747 161.408298289 2.278882686 42.40514175 8.10.501868142 0.7877424 8.687401061 8.10.823690263 0.702728756 9.256435329 8.11.642811587 2.204677369 47.26060153 5.41.298403188 2.032989968 69.59088577 5.40.986469047 1.438469164 28.44631467 5.41.9 11 3.481662252 4.11.9 11 4.671746348 4.11.9 11 2.807099577 4.128.78719862 1.337996556 6.081802526 11.758151558.247892192 1.072225985 4.948735315 8.1**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateOKGPMuskogeeMill B-4 Sample #3 4/16/2003SCMarlboroPaper Hogged Fuel Boiler Sample #1 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #2 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #3 7/14/2009TNBowaterNewsprintBubbling Fluidized Bed BoilerSample #1 10/6/2005TNBowaterNewsprintBubbling Fluidized Bed BoilerSample #2 10/6/2005TNBowaterNewsprintBubbling Fluidized Bed BoilerSample #3 10/6/2005TNBowaterNewsprintBubbling Fluidized Bed Boiler1 8/4/2009TNBowaterNewsprintBubbling Fluidized Bed Boiler2 8/4/2009TNBowaterNewsprintBubbling Fluidized Bed Boiler3 8/5/2009TNEastman_NO_CBIDATA Boiler 30 1 8/26/2009TNEastman_NO_CBIDATA Boiler 30 2 8/27/2009TNEastman_NO_CBIDATA Boiler 30 3 8/27/2009TXDibollTemple-Inland PB-44 Sample #1 6/29/2007TXDibollTemple-Inland PB-44 Sample #2 6/29/2007VAGeorgiaPacificBrooknealGladys5600 Sample #1 7/6/2006VAGeorgiaPacificBrooknealGladys5600 Sample #2 7/6/2006VAGeorgiaPacificBrooknealGladys5600 Sample #3 7/6/2006VAUniversityofVirginia 7103-1-01R M29-1 9/17/2009VAUniversityofVirginia 7103-1-01R M29-2 9/17/2009VAUniversityofVirginia 7103-1-01R M29-3 9/18/2009VAVirginiaPolytechnic Boiler 11 Sample #1 2/27/2007VAVirginiaPolytechnic Boiler 11 Sample #1VAVirginiaPolytechnic Boiler 11 Sample #2VAVirginiaPolytechnic Boiler 7 Sample #3 2/28/2007VAVirginiaPolytechnic Boiler 7 Sample #1Cr 3x RDLConcentration(μg/dscm)Pb 3x RDLConcentration(μg/dscm)Mn 3x RDLConcentration(μg/dscm)Ni 3x RDLConcentration(μg/dscm)52.9314781 1.014519997 8.821913017 13.673965180.3 1.342178436 1.917362317 5.40.913524971 1.166517101 2.791744778 5.40.395680203 0.432767696 2.304241135 5.410.6823186 2.815494824 63.34863353 1610.59840468 2.874870904 86.24612712 168.966611654 2.241652914 58.28297575 164.856360092 9.45419195 544.3551516 5.5050544775.231963677 9.450375196 613.5845963 6.4217958753.084191886 5.361402876 328.4884333 5.41.924695011 1.111321074 2.668475456 4.11.5932244 1.182243699 2.582382677 4.11.06547989 0.666191835 1.488255478 4.10.45 1.30375962 44.6322291 8.10.45 0.76479472 251.2896938 8.11.05193617 0.909173404 72.80901064 160.9 1.675256247 35.80860229 160.985087039 1.014713716 85.84329908 162.880981602 0.66353277 7.573163397 4.10.995841925 0.790049868 6.303735623 4.10.970539063 0.23 3.934441187 4.4527972772.182588377 12.24368905 19.62087852 8.1#DIV/0! #DIV/0! #DIV/0! #DIV/0!#DIV/0! #DIV/0! #DIV/0! #DIV/0!1.22754663 5.468162262 11.32476148 8.1#DIV/0! #DIV/0! #DIV/0! #DIV/0!**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateVAVirginiaPolytechnic Boiler 7 Sample #1WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #1 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #2 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #3 8/12/2009WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #1 7/21/2005WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #2 7/21/2005WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #3 7/22/2005WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #1 8/20/2009WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #2 8/20/2009WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #3 8/21/2009WINewPageBiron B24 Sample #1 9/12/2007WINewPageBiron B24 Sample #2 9/12/2007WINewPageBiron B24 Sample #3 9/12/2007WINewPageBiron B24 1 9/22/2009WINewPageBiron B24 2 9/22/2009WINewPageBiron B24 3 9/23/2009WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #1 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #2 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #3 9/18/2003WVMountainStateCarbonFollansbeeS1 Sample #1 10/19/2009WVMountainStateCarbonFollansbeeS1 Sample #2 10/19/2009WVMountainStateCarbonFollansbeeS1 Sample #3 10/20/2009WVPPGMartinsville R011-Boiler 3 1 7/22/2009WVPPGMartinsville R011-Boiler 3 2 7/23/2009WVPPGMartinsville R011-Boiler 3 3 7/23/2009SCMilliken-DeweyD30Sample #18/12/2009Cr 3x RDLConcentration(μg/dscm)Pb 3x RDLConcentration(μg/dscm)Mn 3x RDLConcentration(μg/dscm)Ni 3x RDLConcentration(μg/dscm)#DIV/0! #DIV/0! #DIV/0! #DIV/0!#VALUE! #VALUE! #VALUE! #VALUE!#VALUE! #VALUE! #VALUE! #VALUE!#VALUE! #VALUE! #VALUE! #VALUE!15.68636208 2.430524235 6.403828037 1611.6279325 2.357886313 9.447695157 166.972800666 1.317694614 36.15816768 162.076725451 0.720612383 2.775776204 4.11.120417368 0.879807624 1.368083783 4.11.541711789 0.855709799 6.793092876 4.11.265558927 4.449142716 1.583354835 8.10.588057177 4.091639936 26.13140392 8.10.45 3.517424006 30.36572936 8.10.358714292 0.80394203 7.744008532 4.10.525319212 1.057769454 2.186849208 4.10.477907364 1.120610372 2.236512296 4.1#VALUE! #VALUE! #VALUE! #VALUE!#VALUE! #VALUE! #VALUE! #VALUE!#VALUE! #VALUE! #VALUE! #VALUE!8.455043149 2.37710218 6.088755811 10.0513137711.0159746 2.526860152 17.23375407 6.43639546612.12963193 2.377683531 6.323259826 5.8260630621.9 0.84956254 2.528207095 4.11.940590104 0.781222569 3.300457581 4.11.9 0.718509255 3.260303274 4.10.452966628 0.442035307 1.457509512 5.4**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateSCMilliken-DeweyD30Sample #28/12/2009SCMilliken-DeweyD30Sample #38/12/2009MNGPDuluthEU33 Boiler #319/10/2009MNGPDuluthEU33 Boiler #329/10/2009MNGPDuluthEU33 Boiler #339/10/2009TNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86111/17/2009TNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86211/17/2009TNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86311/18/2009Cr 3x RDLConcentration(μg/dscm)Pb 3x RDLConcentration(μg/dscm)Mn 3x RDLConcentration(μg/dscm)Ni 3x RDLConcentration(μg/dscm)0.504869868 0.341758065 1.245345674 5.40.435879099 0.312275343 0.989834958 5.40.919432851 0.794685681 6.401377968 5.40.906794379 0.556928831 7.240074808 6.447522240.883180811 0.516208175 3.080123658 5.41.213559327 5.832709227 2.746922247 4.11.222337564 21.03096168 1.319449011 4.11.101564965 6.707818597 3.811498547 4.1**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateAKDoyonUtilities_AK 4 Sample #1 8/17/2005AKDoyonUtilities_AK 4 Sample #2 8/17/2005AKDoyonUtilities_AK 4 Sample #3 8/17/2005AKDoyonUtilities_AK 7 Sample #1 8/16/2005AKDoyonUtilities_AK 7 Sample #2 8/16/2005AKDoyonUtilities_AK 7 Sample #3 8/16/2005ALIPCourtlandNo. 3 Combination Boier / 11Cu301Sample #1 7/7/2009ALIPCourtlandNo. 3 Combination Boier / 11Cu301Sample #2 7/7/2009ALIPCourtlandNo. 3 Combination Boier / 11Cu301Sample #3 7/8/2009ARAnthonyForestProducts SN-12 1 9/1/2009ARAnthonyForestProducts SN-12 2 9/1/2009ARAnthonyForestProducts SN-12 3 9/2/2009ARLeolaLumberMill SN-01A Sample #1 6/14/2006ARLeolaLumberMill SN-01A Sample #2 6/14/2006ARLeolaLumberMill SN-01A Sample #3 6/14/2006ARLeolaLumberMill SN-01B Sample #1 6/14/2006ARLeolaLumberMill SN-01B Sample #2 6/14/2006ARLeolaLumberMill SN-01B Sample #3 6/14/2006ARPotlatchForestWarren Wellons Boiler 1 9/9/2009ARPotlatchForestWarren Wellons Boiler 2 9/9/2009ARPotlatchForestWarren Wellons Boiler 3 9/9/2009FLSugarCaneGrowersCoop Boiler No. 8 Sample #1 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #2 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #3 1/19/2005GAGPMadisonPly800 Wood Waste Boiler1 8/11/2009GAGPMadisonPly800 Wood Waste Boiler2 8/12/2009Se 3x RDLConcentration(μg/dscm)Total Metals,adjusting for 3xRDLConcentration atindividual metals(μg/dscm)2.863177182 25.205898882.4 26.28369062.4 24.897221182.4 50.916042612.470876334 54.757320272.533357245 82.243947270.6 6.9101502370.824682942 6.894196630.87878454 6.458572171.292883673 2697.8862191.725182011 3343.8245021.351361223 3201.431252.245929789 19.596655262.308773536 22.517604842.297358834 18.130941382.170607825 35.242094142.076553413 30.29942612.14847077 32.025056140.6 368.48653410.6 38.443177850.6 18.97586647#VALUE!#VALUE!#VALUE!1.69236181 26.885510031.429223462 36.79264755**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateGAGPMadisonPly800 Wood Waste Boiler3 8/12/2009GATempleInlandRome WF 1 7/27/2009GATempleInlandRome WF 2 7/28/2009GATempleInlandRome WF 3 7/28/2009HIPuuneneSugarMill Boiler 1 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 1 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 1 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 1 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 2 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 2 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 2 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 3 Sample #1 5/23/2006HIPuuneneSugarMill Boiler 3 Sample #2 5/24/2006HIPuuneneSugarMill Boiler 3 Sample #3 5/25/2006HIPuuneneSugarMill Boiler 3 Sample #1 7/16/2007HIPuuneneSugarMill Boiler 3 Sample #2 7/17/2007HIPuuneneSugarMill Boiler 3 Sample #3 7/17/2007IARoquetteAmericaCirculating Fluidized Bed Boiler (121)1 6/3/2009IARoquetteAmericaCirculating Fluidized Bed Boiler (121)2 6/3/2009IARoquetteAmericaCirculating Fluidized Bed Boiler (121)3 6/4/2009IAUofNorthernIowa Boiler #3 4 10/6/2009Se 3x RDLConcentration(μg/dscm)Total Metals,adjusting for 3xRDLConcentration atindividual metals(μg/dscm)1.070573182 36.33585310.8 102.54478070.8 110.02480610.8 90.76687652#N/A#N/A#N/A#N/A#N/A#N/A27 74.0729571627 73.8762493227 72.67272974#VALUE!**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateIAUofNorthernIowa Boiler #3 5 10/6/2009IAUofNorthernIowa Boiler #3 6 10/7/2009IDAmalgamatedSugarCoTwinFallsS-B1 Sample #1 9/26/2006IDAmalgamatedSugarCoTwinFallsS-B1 Sample #2 9/26/2006IDAmalgamatedSugarCoTwinFallsS-B1 Sample #3 9/26/2006IDPotlatch PB-1 CE Sample #1 7/20/2006IDPotlatch PB-1 CE Sample #2 7/20/2006IDPotlatch PB-1 CE Sample #3 7/20/2006IDPotlatch PB-1 CE M29-R1 7/28/2009IDPotlatch PB-1 CE M29-R2 7/28/2009IDPotlatch PB-1 CE M29-R3 7/29/2009IDPotlatch PB-2 Riley Sample #1 7/27/2006IDPotlatch PB-2 Riley Sample #2 7/27/2006IDPotlatch PB-2 Riley Sample #3 7/27/2006IDTASCONampaBabcock and Wilcox (B&W) #1Sample #1 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #1Sample #2 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #1Sample #3 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #2Sample #1 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #2Sample #2 12/4/2006IDTASCONampaBabcock and Wilcox (B&W) #2Sample #3 12/4/2006ILPolyOne B1 Sample #1 11/14/2006ILPolyOne B1 Sample #2 11/14/2006ILPolyOne B1 Sample #3 11/14/2006ILPolyOne B1 1 9/9/2009ILPolyOne B1 2 9/9/2009ILPolyOne B1 3 9/10/2009Se 3x RDLConcentration(μg/dscm)Total Metals,adjusting for 3xRDLConcentration atindividual metals(μg/dscm)#VALUE!#VALUE!41 234.920546341 140.733918141 145.38423865.600987337 14.497500633.41357645 13.165654361.732309842 11.2203939811.42765879 33.4282832920.34667758 41.285536877.849697427 27.652471111.42765879 33.4282832920.34667758 41.285536877.849697427 27.379282443.164804636 20.61152766#DIV/0!#DIV/0!1.435544096 10.149792981.502090245 10.522508721.49236026 10.78790591**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateINSABICInnovativePlastics 01-001 BW1 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #3 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #3 6/28/2006INTateLyleSagamore 31B1 M29-1 9/1/2009INTateLyleSagamore 31B1 M29-2 9/2/2009INTateLyleSagamore 31B1 M29-3 9/3/2009MNHibbing Unit 1A Sample #1 9/21/2004MNHibbing Unit 1A Sample #2 9/21/2004MNHibbing Unit 1A Sample #3 9/21/2004MNHibbing Unit 2A Sample #1 9/22/2004MNHibbing Unit 2A Sample #2 9/22/2004MNHibbing Unit 2A Sample #3 9/22/2004MSGPNewAugusta AA-015 Power Boiler Sample #1 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #2 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #3 7/12/2006MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #1 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #2 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #3 8/5/2009NDCargillWestFargoFoster Wheeler Boiler (EU43)1 8/26/2009NDCargillWestFargoFoster Wheeler Boiler (EU43)2 8/26/2009NDCargillWestFargoFoster Wheeler Boiler (EU43)3 8/27/2009OKGPMuskogeeMill B-4 Sample #1 4/16/2003OKGPMuskogeeMill B-4 Sample #2 4/16/2003Se 3x RDLConcentration(μg/dscm)Total Metals,adjusting for 3xRDLConcentration atindividual metals(μg/dscm)33.10901559 82.0625531530.71862698 75.7956435225.69965693 73.9279510533.10901559 82.0625531530.71862698 75.7956435225.69965693 73.9279510514.20861586 52.4317814114.05604923 58.884607119.968433735 32.7898572681 215.148198981 214.953842281 214.711009381 217.114297781 217.415762881 219.74271791.79237964 57.368419452.223466451 21.546889822.016025118 22.005965260.8 57.991726470.8 79.847075910.8 37.7584113820 55.6710072320 57.0457893920 55.014984651.2 50.010839841.2 25.11364271**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateOKGPMuskogeeMill B-4 Sample #3 4/16/2003SCMarlboroPaper Hogged Fuel Boiler Sample #1 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #2 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #3 7/14/2009TNBowaterNewsprintBubbling Fluidized Bed BoilerSample #1 10/6/2005TNBowaterNewsprintBubbling Fluidized Bed BoilerSample #2 10/6/2005TNBowaterNewsprintBubbling Fluidized Bed BoilerSample #3 10/6/2005TNBowaterNewsprintBubbling Fluidized Bed Boiler1 8/4/2009TNBowaterNewsprintBubbling Fluidized Bed Boiler2 8/4/2009TNBowaterNewsprintBubbling Fluidized Bed Boiler3 8/5/2009TNEastman_NO_CBIDATA Boiler 30 1 8/26/2009TNEastman_NO_CBIDATA Boiler 30 2 8/27/2009TNEastman_NO_CBIDATA Boiler 30 3 8/27/2009TXDibollTemple-Inland PB-44 Sample #1 6/29/2007TXDibollTemple-Inland PB-44 Sample #2 6/29/2007VAGeorgiaPacificBrooknealGladys5600 Sample #1 7/6/2006VAGeorgiaPacificBrooknealGladys5600 Sample #2 7/6/2006VAGeorgiaPacificBrooknealGladys5600 Sample #3 7/6/2006VAUniversityofVirginia 7103-1-01R M29-1 9/17/2009VAUniversityofVirginia 7103-1-01R M29-2 9/17/2009VAUniversityofVirginia 7103-1-01R M29-3 9/18/2009VAVirginiaPolytechnic Boiler 11 Sample #1 2/27/2007VAVirginiaPolytechnic Boiler 11 Sample #1VAVirginiaPolytechnic Boiler 11 Sample #2VAVirginiaPolytechnic Boiler 7 Sample #3 2/28/2007VAVirginiaPolytechnic Boiler 7 Sample #1Se 3x RDLConcentration(μg/dscm)Total Metals,adjusting for 3xRDLConcentration atindividual metals(μg/dscm)1.2 78.40687631.419349354 10.961619242.088353928 12.952610580.8 9.8753042839.108953841 104.59685232.4 120.07574352.4 89.834896532.26589855 570.78782932.673232207 641.74248732.327190169 347.02387041.587601535 13.384206781.510165308 12.14810241.494661169 10.078644671.2 56.531195591.2 262.63719522.4 95.369017022.4 58.515532612.4 108.00899330.862952999 16.533733590.928147169 13.600189860.6 10.614154884.320343006 50.77969037#DIV/0!#DIV/0!2.317745386 32.09921565#DIV/0!**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateVAVirginiaPolytechnic Boiler 7 Sample #1WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #1 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #2 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #3 8/12/2009WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #1 7/21/2005WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #2 7/21/2005WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #3 7/22/2005WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #1 8/20/2009WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #2 8/20/2009WIGPGreenBay2818B10 - Wastepaper Sludge-Fired Boiler 10Sample #3 8/21/2009WINewPageBiron B24 Sample #1 9/12/2007WINewPageBiron B24 Sample #2 9/12/2007WINewPageBiron B24 Sample #3 9/12/2007WINewPageBiron B24 1 9/22/2009WINewPageBiron B24 2 9/22/2009WINewPageBiron B24 3 9/23/2009WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #1 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #2 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #3 9/18/2003WVMountainStateCarbonFollansbeeS1 Sample #1 10/19/2009WVMountainStateCarbonFollansbeeS1 Sample #2 10/19/2009WVMountainStateCarbonFollansbeeS1 Sample #3 10/20/2009WVPPGMartinsville R011-Boiler 3 1 7/22/2009WVPPGMartinsville R011-Boiler 3 2 7/23/2009WVPPGMartinsville R011-Boiler 3 3 7/23/2009SCMilliken-DeweyD30Sample #18/12/2009Se 3x RDLConcentration(μg/dscm)Total Metals,adjusting for 3xRDLConcentration atindividual metals(μg/dscm)#DIV/0!#VALUE!#VALUE!#VALUE!2.4 46.774000832.4 48.961448992.4 65.622044420.6 11.040742330.6 8.8061821660.6 14.661876636.496535824 24.757567839.254162942 50.926037677.116721803 52.028131836.393554728 20.518564146.964639326 16.296438365.06158046 14.39031079#VALUE!#VALUE!#VALUE!6.467275266 131.98000076.984355027 61.95392635.98112938 48.7388203313.69161058 27.0027789318.15926928 30.4840673946.51402019 59.957208830.8 9.888246985**Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL**FacilityID UnitIDRunNumberTest DateSCMilliken-DeweyD30Sample #28/12/2009SCMilliken-DeweyD30Sample #38/12/2009MNGPDuluthEU33 Boiler #319/10/2009MNGPDuluthEU33 Boiler #329/10/2009MNGPDuluthEU33 Boiler #339/10/2009TNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86111/17/2009TNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86211/17/2009TNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86311/18/2009Se 3x RDLConcentration(μg/dscm)Total Metals,adjusting for 3xRDLConcentration atindividual metals(μg/dscm)0.8 9.1163330280.8 8.5342611870.8 14.894832210.8 16.514467920.8 11.223121230.6 14.906138410.6 28.695438390.6 16.73323786**Table D-2a: Summary of TSM8 3x RDL for Existing Sources Fuel Category Combustor Design** **Average Sample Time (hrs)** **Average Stack O2 (%)** **Concentration (μg/dscm)** **Fd Factor (dscf/MMBtu)** **Emission Rate (lb/MMBtu)** Coal/Fossil Solid N/A 2 7.03 1.01E+01 9,780**9.26E-06**Dutch Oven/Pile Burner 3 9.64 1.90E+01 9,420**2.07E-05**FB 3 8.82 6.46E+00 9,420**6.56E-06**Fuel Cell 4 10.72 1.12E+01 9,420**1.35E-05**Suspension Burner 2 12.1 5.65E+01 9,240**7.72E-05**Suspension/GrateWet Biomass Stoker/SlopedGrate/Other 3 10.1 9.88E+00 9,420**1.12E-05**Dry Biomass Stoker/SlopedGrate/OtherProcess Gas N/A 4 4.67 4.87E+01 8,710**3.41E-05**Heavy Liquid N/A 3 10.11 8.53E+00 9,190**9.46E-06**Light Liquid N/A 4 4.63 1.49E+01 9,190**1.10E-05**Non-ContinentalLiquidN/A**Table D-2b: Summary of TSM8 3x RDL for New Sources Fuel Category Combustor Design** **Average Sample Time (hrs)** **Average Stack O2 (%)** **Concentration (μg/dscm)** **Fd Factor (dscf/MMBtu)** **Emission Rate (lb/MMBtu)** Coal/Fossil Solid N/A 4 8.07 1.01E+01 9,780**1.01E-05**Dutch Oven/Pile BurnerFB 4 12.72 5.50E+01 9,420**8.24E-05**Fuel Cell 4 13.33 1.12E+01 9,420**1.81E-05**Suspension BurnerSuspension/GrateWet Biomass Stoker/SlopedGrate/OtherDry Biomass Stoker/SlopedGrate/OtherProcess Gas N/A 4 4.67 4.87E+01 8,710**3.41E-05**Heavy Liquid N/A 3 16.29 1.12E+01 9,190**2.90E-05**Light Liquid N/A 4 4.63 1.49E+01 9,190**1.10E-05**Non-ContinentalLiquidN/ABiomass/Bio-BasedSolidN/A - No test reports for top performers in this subcategory.N/A - Unable to calculate 3x RDL based on data in available test reports.N/A - No test reports for top performers in this subcategory.Biomass/Bio-BasedSolidN/A - Unable to calculate 3x RDL based on data in available test reports.N/A - No test reports for top performers in this subcategory.N/A - No test reports for top performers in this subcategory.N/A - Unable to calculate 3x RDL based on data in available test reports.N/A - Unable to calculate 3x RDL based on data in available test reports.N/A - Unable to calculate 3x RDL based on data in available test reports.