MEMORANDUM

TO: Jim Eddinger, U.S. Environmental Protection Agency, OAQPS

FROM: Eastern Research Group, Inc.

DATE: May 2012

SUBJECT:   Revised (May 2012) Analysis of Minimum Detection Levels from Industrial,

Commercial, and Institutional Boilers and Process Heaters National Emission

Standards for Hazardous Air Pollutants ‐ Major Source

1.0 INTRODUCTION

The purpose of this memorandum is to discuss the methodology used to compute a

value equal to three times the representative method detection limit (3x RDL) and how these

3x RDL values were used to establish emission standards for boilers and process heaters at

major sources of hazardous air pollutants (HAP).  This memorandum focuses only on the

changes to the 3x RDL analyses that were conducted for the December 23, 2011 proposed

reconsideration of the rule (76 FR 80598).  The methods used to develop 3x RDL values for the

proposed rule are provided in another memorandum.1 For this revised analysis, 3x RDL values

were estimated for mercury (Hg), hydrogen chloride (HCl), filterable particulate matter (PM),

and the sum of eight metallic hazardous air pollutants (TSM8).

This memorandum is organized as follows:

1.0 Introduction

2.0 3x RDL for Mercury, Hydrogen Chloride, and Filterable Particulate Matter

3.0 3x RDL for Metallic HAP

4.0 3x RDL for Carbon Monoxide

5.0 References

Appendix A:  Calculation of 3x RDL for Mercury
Appendix B:  Calculation of 3x RDL for Hydrogen Chloride

Appendix C:  Calculation of 3x RDL for Filterable Particulate Matter

Appendix D:  Calculation of 3x RDL for Metallic HAP

   
2.0 3x RDL FOR MERCURY, HYDROGEN CHLORIDE, AND FILTERABLE PARTICULATE MATTER

The 3x RDL analyses conducted for mercury (Hg), hydrogen chloride (HCl), and filterable

particulate matter (PM) were conducted using the same methodology used in the previous

analysis.1 However, since the list of top performers for each pollutant changed, the resultant 3x

RDL values for each pollutant also changed slightly in some cases.  Summaries of the 3x RDL

calculation for Hg, HCl, and PM are provided in Appendices A, B, and C, respectively.

3.0 3x RDL FOR METALLIC HAP

The methodology used to calculate the 3x RDL values for the sum of eight metallic

hazardous air pollutants (HAP) (TSM8) has changed since the previous analysis.  An RDL was

developed by EPA for each of the eight individual metals that comprise TSM8 (arsenic,

beryllium, cadmium, chromium, lead, manganese, nickel, and selenium).2 This analysis

developed a separate RDL for each metal based on the laboratory instrument used to analyze

the Method 29 samples.  One set of RDL values was generated for the use of inductively

coupled plasma/atomic emission spectrometry (ICP/AES) or atomic absorption (AA), whereas

an alternative set of RDL values was developed for the use of inductively coupled plasma/mass

spectrometry (ICP/MS) or graphite furnace atomic absorption (GFAA).  This is similar to how

separate RDL values were generated for methods 26 and 26A for HCl.

EPA conducted a review of top performer test reports for consistency in TSM8

reporting.  The results of this test report review are provided in another memorandum.3 The

reported sample catch, in micrograms (μg), was extracted for each test run by EPA, along with

other test‐specific parameters such as sample time, sample volume, and stack oxygen

concentration.  This review also included identifying what laboratory analysis was used to

analyze the method 29 samples for each metal.  Some laboratories used a mixture of laboratory

instruments to analyze all eight metals.  For example, one laboratory tended to use ICP/MS to

analyze samples for cadmium (Cd) and ICP/AES for the remaining seven metals.

The actual reported sample volume for each metal was calculated using the reported

sample catch and sample volume, as shown in Equation 1 below.
ܥ௘௠௧௔௟ ൌ ௠೘೐೟ೌ೗

௏ೞ೟೏

                 (Equation 1)

Where:

Cmetal = Concentration, micrograms per cubic meter at dry standard conditions (μg/dscm)

mmetal = Reported sample catch for the metal, μg

Vstd = Reported sample volume, cubic meter at dry standard conditions (dscm)

The actual concentration for the metal was compared to the corresponding RDL

concentration for the respective laboratory instrument used and for the respective sampling

time developed by EPA.2 If the reported concentration was less than the RDL concentration

developed by EPA, the reported concentration was corrected upwards to the RDL

concentration.  This comparison was done for all eight metals for each top performer test run,

where test report data were available.  After the comparison was done for all eight metals,

each of the eight values was summed in order to get the TSM8 3x RDL value for the test run.

The 3x RDL value for each subcategory was based on the minimum TSM8 3x RDL test

run value calculated using the aforementioned steps.  The 3x RDL concentrations were

converted to emission rates, in units of pounds per million British thermal unit of heat input

(lb/MMBtu), using Equation 2 below.

ܧଷ௫ ோ஽௅ ൌ ܥଷ௫ ோ஽௅ ቀ ଵ

ଷହ.ଷଵହቁ ቀ ଵସହଷ,ହଽ଴,଴଴଴ቁ ሺܨ஽ሻ ቀ ଶ଴.ଽସ଺ଶ଴.ଽସ଺ିைమ

ቁ       (Equation 2)

Where:

E3x RDL = TSM8 3x RDL emission rate, lb/MMBtu

C3x RDL = TSM8 3x RDL concentration, μg/dscm

35.315 = Conversion factor, cubic meters to cubic feet

453,590,000 = Conversion factor, micrograms to pounds

FD = Fuel‐specific factor from Method 19, cubic foot at dry standard conditions per MMBtu (dscf/MMBtu)

20.946 = Approximate amount of oxygen in ambient air, percentage (%)

O2 = Average oxygen concentration from test report review for the subcategory, %

4.0 3x RDL FOR CARBON MONOXIDE

The methods used to calculate 3x RDL values for carbon monoxide (CO) are provided in

another memorandum.4 This additional memorandum provides the actual 3x RDL values that

were used to compare to the 99% UPL calculated for the regulated subcategories.  The CO 3x

RDL only applies where the calculated 99% UPL, when rounded to the nearest whole number, is
less than 5 parts per million (ppm).  Only one subcategory for new sources (units designed to

burn light liquid fuels) qualified for the 3x RDL for CO.

   
5.0 REFERENCES

1. Eastern Research Group, Inc.  Analysis of Dioxin/Furan Data and Minimum Detection

Levels from Industrial, Commercial, and Institutional Boilers and Process Heaters

National Emission Standards for Hazardous Air Pollutants – Major Source.  November

2011.

2. Westlin, Peter, U.S. EPA SPPD, MTG, & Ray Merrill, U.S. EPA AQAD, MTG.  Data and

Procedure for Handling Below Detection Level Data in Analyzing Various Pollutant

Emissions Databases for MACT and RTR Emissions Limits.  December, 2011.

3. Eastern Research Group, Inc.  Revised (May 2012) Summary of Test Report Data Review

from Best Performing Units at Industrial, Commercial, and Institutional Boilers and

Process Heaters National Emission Standards for Hazardous Air Pollutants ‐ Major

Source.  May 2012.

4. Westlin, Peter.  U.S. EPA OAQPS/SPPD.  Measurement Detection Capabilities for EPA for

Instrumental Test Methods.  April 10, 2012.

   
Appendix A

Calculation of 3x RDL for Mercury

   
Appendix A-1: Sample Times and Oxygen Percentages Used to Estimate Hg 3x RDL

Facility ID Combusor ID Fuel Category Test ID

Sample 

Volume (dscf)

Sample 

Volume 

(dscm)

Sample 

Time (min)

Sample 

Time (hrs)

Stack Oxygen 

Concentration 

(%)

Use in 

New 

Source 3x 

RDL?

AKDoyonUtilities_AK #4 Solid Sample #1 60.192 1.70 60 1.00 7

AKDoyonUtilities_AK #4 Solid Sample #2 61.418 1.74 60 1.00 6.67

AKDoyonUtilities_AK #4 Solid Sample #3 59.13 1.67 60 1.00 6

GAGPSRMRiincon EU 002 Solid Sample #1 60.459 1.71 120 2.00

GAGPSRMRiincon EU 002 Solid Sample #2 50.327 1.43 120 2.00

GAGPSRMRiincon EU 002 Solid Sample #1 52.468 1.49 120 2.00

GAGPSRMRiincon EU 002 Solid Sample #2 52.281 1.48 120 2.00

IDAmalgamatedSugarCoTwinFalls SB-1 Solid Sample #1 78.341 2.22 120 2.00 6.9

IDAmalgamatedSugarCoTwinFalls SB-1 Solid Sample #2 80.205 2.27 120 2.00 6.9

IDAmalgamatedSugarCoTwinFalls SB-1 Solid Sample #3 77.571 2.20 120 2.00 6

MITBSimonPowerPlant Unit 1 Solid Sample #1 78.628 2.23 120 2.00

MITBSimonPowerPlant Unit 1 Solid Sample #2 76.747 2.17 120 2.00

MITBSimonPowerPlant Unit 1 Solid Sample #3 74.277 2.10 120 2.00

ALIPCourtland No. 3 Combination Boier / 11CU301 Solid Sample #1 127 3.60 240 4.00

ALIPCourtland No. 3 Combination Boier / 11CU301 Solid Sample #2 125 3.54 240 4.00

ALIPCourtland No. 3 Combination Boier / 11CU301 Solid Sample #3 119 3.37 240 4.00

GASPNewsprint PB2 Solid Sample #1 163 4.62 240 4.00

GASPNewsprint PB2 Solid Sample #2 139 3.94 240 4.00

GASPNewsprint PB2 Solid Sample #3 139 3.94 240 4.00

IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #1 165.27 4.68 240 4.00 7

IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #2 169.796 4.81 240 4.00 6.8

IAMonsantoMuscatine Boiler #8 (EP-195) Solid Sample #3 166.058 4.70 240 4.00 6.9

IAMonsantoMuscatine Boiler #8 (EP-195) Solid 8.3

IAMonsantoMuscatine Boiler #8 (EP-195) Solid 8.1

IAMonsantoMuscatine Boiler #8 (EP-195) Solid 8.3

IAMonsantoMuscatine Boiler #8 (EP-195) Solid 9.3

IAMonsantoMuscatine Boiler #8 (EP-195) Solid 9

IAMonsantoMuscatine Boiler #8 (EP-195) Solid 9

IAMonsantoMuscatine Boiler #8 (EP-195) Solid 8.3

IAMonsantoMuscatine Boiler #8 (EP-195) Solid 7.9

IAMonsantoMuscatine Boiler #8 (EP-195) Solid 8.3

IARoquetteAmerica Circulating Fluidized Bed Boiler (121) Solid Sample #1 150.658 4.27 192 3.20

IARoquetteAmerica Circulating Fluidized Bed Boiler (121) Solid Sample #2 151.674 4.29 192 3.20

IARoquetteAmerica Circulating Fluidized Bed Boiler (121) Solid Sample #3 148.593 4.21 192 3.20

ILPolyOne B1 Solid Sample #1 172.203 4.88 240 4.00 8.4

ILPolyOne B1 Solid Sample #2 164.574 4.66 240 4.00 8.1

ILPolyOne B1 Solid Sample #3 165.647 4.69 240 4.00 8.3

MITBSimonPowerPlant Unit 1 Solid Sample #1 178.791 5.06 240 4.00

MITBSimonPowerPlant Unit 1 Solid Sample #2 198.23 5.61 240 4.00

MITBSimonPowerPlant Unit 1 Solid Sample #3 196.014 5.55 240 4.00

NCDomtar 65-25-0310 (No. 2 Hog Fuel Boiler) Solid Sample #1 161.884 4.58 240 4.00

NCDomtar 65-25-0310 (No. 2 Hog Fuel Boiler) Solid Sample #2 166.996 4.73 240 4.00

NCDomtar 65-25-0310 (No. 2 Hog Fuel Boiler) Solid Sample #3 157.615 4.46 240 4.00

NCTysonHarmony TYS-ES-21 Solid Sample #1 77.941 2.21 120 2.00

NCTysonHarmony TYS-ES-21 Solid Sample #2 74.864 2.12 120 2.00

NCTysonHarmony TYS-ES-21 Solid Sample #3 82.735 2.34 120 2.00

NJVinelandMuniElectric-HowardDown Unit 9 Liquid Sample #1 147.289 4.17 240 4.00 4.76

NJVinelandMuniElectric-HowardDown Unit 9 Liquid Sample #2 149.988 4.25 240 4.00 4.95

NJVinelandMuniElectric-HowardDown Unit 9 Liquid Sample #3 147.912 4.19 240 4.00 5.01

PABoeingRidleyPark 033 Liquid Sample #1 150.708 4.27 240 4.00 5.4

PABoeingRidleyPark 033 Liquid Sample #2 139.304 3.94 240 4.00 5.5

PABoeingRidleyPark 033 Liquid Sample #3 132.854 3.76 240 4.00 6.8

SCBowaterCoatedPaper Combination Boiler No. 2 Solid Sample #3 177.254 5.02 240 4.00

SCBowaterCoatedPaper Combination Boiler No. 2 Solid Sample #1 52.934 1.50 96 1.60

SCBowaterCoatedPaper Combination Boiler No. 2 Solid Sample #2 53.144 1.50 96 1.60

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #1 41.8825 1.19 60 1.00

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #2 40.4945 1.15 60 1.00

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #3 38.888 1.10 60 1.00

TNNissanSmyrna Boiler 2 Solid Sample #1 40.79 1.16 60 1.00

TNNissanSmyrna Boiler 2 Solid Sample #2 44.133 1.25 60 1.00

TNNissanSmyrna Boiler 2 Solid Sample #3 42.609 1.21 60 1.00

TNNissanSmyrna Boiler 3 Solid Sample #1 43.078 1.22 60 1.00

TNNissanSmyrna Boiler 3 Solid Sample #2 44.819 1.27 60 1.00

TNNissanSmyrna Boiler 3 Solid Sample #3 43.161 1.22 60 1.00

VADukeEnergyNarrows Boiler #2 Solid Sample #1 42.371 1.20 60 1.00 14.1

VADukeEnergyNarrows Boiler #2 Solid Sample #2 32.941 0.93 60 1.00 12.53

VADukeEnergyNarrows Boiler #2 Solid Sample #3 41.279 1.17 60 1.00 13.03

VADukeEnergyNarrows Boiler #7 Solid Sample #1 46.005 1.30 60 1.00

VADukeEnergyNarrows Boiler #7 Solid Sample #2 37.101 1.05 60 1.00

VADukeEnergyNarrows Boiler #7 Solid Sample #3 47.861 1.36 60 1.00

VAUniversityofVirginia 7103-1-01R Solid Sample #1 176.38 4.99 240 4.00

VAUniversityofVirginia 7103-1-01R Solid Sample #2 169.546 4.80 240 4.00

VAUniversityofVirginia 7103-1-01R Solid Sample #3 177.945 5.04 240 4.00

GATempleInlandRome WF Solid Sample #1 141.451 4.01 240 4.00

GATempleInlandRome WF Solid Sample #2 148.796 4.21 240 4.00

GATempleInlandRome WF Solid Sample #3 153.993 4.36 240 4.00

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #1 218.31 6.18 240 4.00 5.58

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #2 214.84 6.08 240 4.00 5.56

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #3 217.37 6.16 240 4.00 5.66

Page 1 of 3
Appendix A-1: Sample Times and Oxygen Percentages Used to Estimate Hg 3x RDL

Facility ID Combusor ID Fuel Category Test ID

Sample 

Volume (dscf)

Sample 

Volume 

(dscm)

Sample 

Time (min)

Sample 

Time (hrs)

Stack Oxygen 

Concentration 

(%)

Use in 

New 

Source 3x 

RDL?

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid 6.9

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid 7.9

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid 7.9

MNGPDuluth EU33 Boiler #3 Liquid Sample #1 15.87 0.45 180 3.00 4

MNGPDuluth EU33 Boiler #3 Liquid Sample #2 148.38 4.20 180 3.00 4.2

MNGPDuluth EU33 Boiler #3 Liquid Sample #3 144.35 4.09 180 3.00 4.6

SCCogenSouth B001 - Main Boiler Solid Sample #1 91.6 2.59 120 2.00

SCCogenSouth B001 - Main Boiler Solid Sample #2 93.38 2.64 120 2.00

SCCogenSouth B001 - Main Boiler Solid Sample #3 87.44 2.48 120 2.00

SCCogenSouth B001 - Main Boiler Solid Sample #1 76.74 2.17 120 2.00

SCCogenSouth B001 - Main Boiler Solid Sample #2 78.3 2.22 120 2.00

SCCogenSouth B001 - Main Boiler Solid Sample #3 76.47 2.17 120 2.00

SCCogenSouth B001 - Main Boiler Solid Sample #1 108.73 3.08 120 2.00

SCCogenSouth B001 - Main Boiler Solid Sample #2 107.32 3.04 120 2.00

SCCogenSouth B001 - Main Boiler Solid Sample #3 106.37 3.01 120 2.00

SCCogenSouth B001 - Main Boiler Solid Sample #1 155.04 4.39 240 4.00

SCCogenSouth B001 - Main Boiler Solid Sample #2 154.94 4.39 240 4.00

SCCogenSouth B001 - Main Boiler Solid Sample #3 158.45 4.49 240 4.00

WVMountainStateCarbonFollansbee S1 Process Gas Sample #1 163.271 4.62 240 4.00 4.5 YES

WVMountainStateCarbonFollansbee S1 Process Gas Sample #2 124.385 3.52 240 4.00 4.7 YES

WVMountainStateCarbonFollansbee S1 Process Gas Sample #3 143.477 4.06 240 4.00 4.8 YES

NCDomtar 65-25-0310 (No. 2 Hog Fuel Boiler) Solid Sample #1 74.893 2.12 120 2.00

NCDomtar 65-25-0310 (No. 2 Hog Fuel Boiler) Solid Sample #2 78.324 2.22 120 2.00

NCDomtar 65-25-0310 (No. 2 Hog Fuel Boiler) Solid Sample #3 77.557 2.20 120 2.00

TNCargillMemphis Stoker Boiler 8001 Solid Sample #1 169.383 4.80 240 4.00 10.84

TNCargillMemphis Stoker Boiler 8001 Solid Sample #2 172.476 4.88 240 4.00 10.31

TNCargillMemphis Stoker Boiler 8001 Solid Sample #3 158.663 4.49 240 4.00 10.25

TNCargillMemphis Stoker Boiler 8001 Solid 12.4

TNCargillMemphis Stoker Boiler 8001 Solid 12.2

TNCargillMemphis Stoker Boiler 8001 Solid 11.9

VADukeEnergyNarrows Boiler #1 Solid Sample #1 37.837 1.07 60 1.00

VADukeEnergyNarrows Boiler #1 Solid Sample #3 38.994 1.10 60 1.00

VADukeEnergyNarrows Boiler #1 Solid Sample #4 38.585 1.09 60 1.00

VADukeEnergyNarrows Boiler #1 Solid Sample #1 54.38 1.54 60 1.00

VADukeEnergyNarrows Boiler #1 Solid Sample #2 51.201 1.45 60 1.00

VADukeEnergyNarrows Boiler #1 Solid Sample #3 55.212 1.56 60 1.00

VADukeEnergyNarrows Boiler #7 Solid Sample #1 59.38 1.68 60 1.00

VADukeEnergyNarrows Boiler #7 Solid Sample #2 41.135 1.16 60 1.00

VADukeEnergyNarrows Boiler #7 Solid Sample #3 43.425 1.23 60 1.00

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Liquid Sample #1 166.745 4.72 4.3 YES

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Liquid Sample #2 167.281 4.74 4.3 YES

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Liquid Sample #3 168.63 4.78 5.3 YES

ARPotlatchForestWarren Wellons Boiler 40065 Solid Sample #1 208.754 5.91

ARPotlatchForestWarren Wellons Boiler 40065 Solid Sample #2 220.995 6.26

ARPotlatchForestWarren Wellons Boiler 40065 Solid Sample #3 217.503 6.16

CACovantaDelano Unit 1 Solid Sample #1 100.827 2.86

CACovantaDelano Unit 1 Solid Sample #2 102.364 2.90

CACovantaDelano Unit 1 Solid Sample #3 101.458 2.87

CTElectric Boat EMU 17 Liquid Sample #1 153.219 4.34

CTElectric Boat EMU 17 Liquid Sample #2 153.208 4.34

CTElectric Boat EMU 17 Liquid Sample #3 151.403 4.29

FLCFRC252 Boiler #3 (McBurney) Solid Sample #1 49.908 1.41

FLCFRC252 Boiler #3 (McBurney) Solid Sample #2 45.423 1.29

FLCFRC252 Boiler #3 (McBurney) Solid Sample #3 44.795 1.27

FLRayonierPerformance PB06 Solid Sample #1 80.598 2.28

FLRayonierPerformance PB06 Solid Sample #2 77.547 2.20

FLRayonierPerformance PB06 Solid Sample #3 67.32 1.91

FLRayonierPerformance PB06 Solid Sample #1 78.359 2.22

FLRayonierPerformance PB06 Solid Sample #2 77.714 2.20

FLRayonierPerformance PB06 Solid Sample #3 76.063 2.15

FLRayonierPerformance PB06 Solid Sample #1 76.412 2.16

FLRayonierPerformance PB06 Solid Sample #2 70.516 2.00

FLRayonierPerformance PB06 Solid Sample #3 72.781 2.06

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #1

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #2

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #3

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #1

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #2

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #3

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #1 176.217 4.99

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #2 171.561 4.86

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #3 172.454 4.88

GAInternationalPaperAugustaMills PB3A Solid Sample #1 62.864 1.78

GAInternationalPaperAugustaMills PB3A Solid Sample #2 70.654 2.00

GAInternationalPaperAugustaMills PB3A Solid Sample #3 68.063 1.93

HIPuuneneSugarMill Boiler 1 Solid Sample #1 98.787 2.80

HIPuuneneSugarMill Boiler 1 Solid Sample #2 95.978 2.72

HIPuuneneSugarMill Boiler 1 Solid Sample #3 118.402 3.35

HIPuuneneSugarMill Boiler 2 Solid Sample #1 98.787 2.80

Page 2 of 3
Appendix A-1: Sample Times and Oxygen Percentages Used to Estimate Hg 3x RDL

Facility ID Combusor ID Fuel Category Test ID

Sample 

Volume (dscf)

Sample 

Volume 

(dscm)

Sample 

Time (min)

Sample 

Time (hrs)

Stack Oxygen 

Concentration 

(%)

Use in 

New 

Source 3x 

RDL?

HIPuuneneSugarMill Boiler 2 Solid Sample #2 95.978 2.72

HIPuuneneSugarMill Boiler 2 Solid Sample #3 118.402 3.35

ILCornProductsInt B10 Solid Sample #1 69.38 1.96

ILCornProductsInt B10 Solid Sample #2 70.43 1.99

ILCornProductsInt B10 Solid Sample #3 70.11 1.99

ILCornProductsInt B10 Solid Sample #1 74.8 2.12

ILCornProductsInt B10 Solid Sample #2 72.48 2.05

ILCornProductsInt B10 Solid Sample #3 73.06 2.07

ILPolyOne B1 Solid Sample #1 85.115 2.41

ILPolyOne B1 Solid Sample #2 83.675 2.37

ILPolyOne B1 Solid Sample #3 87.072 2.47

INTateLyleSagamore 31B1 Solid Sample #1 161.58 4.58

INTateLyleSagamore 31B1 Solid Sample #2 139.34 3.95

INTateLyleSagamore 31B1 Solid Sample #3 133.63 3.78

KYNewPage-Wickliffe B09 Solid Sample #1 84.796 2.40

KYNewPage-Wickliffe B09 Solid Sample #2 91.306 2.59

KYNewPage-Wickliffe B09 Solid Sample #3 97.028 2.75

KYNewPage-Wickliffe B09 Solid Sample #1 94.26 2.67

KYNewPage-Wickliffe B09 Solid Sample #2 86.917 2.46

KYNewPage-Wickliffe B09 Solid Sample #3 91.778 2.60

MEBoralexStratton Boiler #1 Solid Sample #1 168.8 4.78

MEBoralexStratton Boiler #1 Solid Sample #2 169.22 4.79

MEBoralexStratton Boiler #1 Solid Sample #3 168.75 4.78

MSGPNewAugusta AA-015 Power Boiler Solid Sample #1 68.96 1.95

MSGPNewAugusta AA-015 Power Boiler Solid Sample #2 55.59 1.57

MSGPNewAugusta AA-015 Power Boiler Solid Sample #3 61.31 1.74

MSGPNewAugusta AA-015 Power Boiler Solid Sample #1 139.834 3.96

MSGPNewAugusta AA-015 Power Boiler Solid Sample #2 136.646 3.87

MSGPNewAugusta AA-015 Power Boiler Solid Sample #3 127.831 3.62

MSGPNewAugusta AA-015 Power Boiler Solid Sample #1 137.153 3.88

MSGPNewAugusta AA-015 Power Boiler Solid Sample #2 169.443 4.80

MSGPNewAugusta AA-015 Power Boiler Solid Sample #3 126.858 3.59

NDCargillWestFargo Foster Wheeler Boiler (EU43) Solid Sample #1 126.485 3.58

NDCargillWestFargo Foster Wheeler Boiler (EU43) Solid Sample #2 134.933 3.82

NDCargillWestFargo Foster Wheeler Boiler (EU43) Solid Sample #3 138.135 3.91

NYBlackRiverGen E00001, E00002, E00003 Solid Sample #1 93.621 2.65 4.8 YES

NYBlackRiverGen E00001, E00002, E00003 Solid Sample #2 77.728 2.20 4.7 YES

NYBlackRiverGen E00001, E00002, E00003 Solid Sample #3 88.341 2.50 4.9 YES

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid 1N 44.229 1.25

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid 2N 44.634 1.26

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid 3N 41.309 1.17

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid 1S 32.963 0.93

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid 2S 31.301 0.89

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid 3S 45.924 1.30

TNCargillMemphis Stoker Boiler 8001 Solid Sample #1 169.383 4.80

TNCargillMemphis Stoker Boiler 8001 Solid Sample #2

TNCargillMemphis Stoker Boiler 8001 Solid Sample #3

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Liquid Sample #1 169.188 4.79

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Liquid Sample #2 170.974 4.84

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Liquid Sample #3 171.329 4.85

Page 3 of 3
Table A-2a: Summary of Hg 3x RDL for Existing Sources

Fuel Category Average Sample Time (hrs)

3x RDL

(μg/dscm)

Fd Factor for 

Subcategory

(dscf/MMBtu)

Average Stack Oxy

Concentration (%

Solid 3 7.10E-01 9,780 8.30 

Liquid 4 6.20E-01 9,190 4.90 

Process Gas 4 6.20E-01 8,710 4.70 

Table A-2b: Summary of Hg 3x RDL for New Sources

Fuel Category Average Sample Time (hrs)

3x RDL

(μg/dscm)

Fd Factor for 

Subcategory

(dscf/MMBtu)

Average Stack Oxy

Concentration (%

Solid 2 1.00E+00 9,780 4.80 

Liquid 5 6.20E-01 9,190 4.60 

Process Gas 4 6.20E-01 8,710 4.70 

Page 1 of 1
Appendix B

Calculation of 3x RDL for Hydrogen Chloride

   
Appendix B-1: Sample Times and Oxygen Percentages Used to Estimate HCl 3x RDL

Facility ID Combusor ID Fuel Category Test ID Test Date

Test 

Method

Sample 

Time 

(min)

Sample 

Time (hrs)

Stack Oxygen 

Concentration 

(%)

3x RDL 

(μg/dscm)

Fd Factor 

(dscf/MMBtu)

3x RDL 

(lb/MMBtu)

Use in 

New 

Source 3x 

RDL?

ALBoiseWhitePaperJackson 102-0001-Z013 Solid 1 8/5/2009 26A 120 2.00 9.00E+01 9,780

ALBoiseWhitePaperJackson 102-0001-Z013 Solid 2 8/5/2009 26A 120 2.00 9.00E+01 9,780

ALBoiseWhitePaperJackson 102-0001-Z013 Solid 3 8/5/2009 26A 120 2.00 9.00E+01 9,780

ALIPCourtland No. 3 Combination Boier / 11Cu301 Solid Sample #1 7/7/2009 26A 120 2.00 9.00E+01 9,780

ALIPCourtland No. 3 Combination Boier / 11Cu301 Solid Sample #2 7/7/2009 26A 120 2.00 9.00E+01 9,780

ALIPCourtland No. 3 Combination Boier / 11Cu301 Solid Sample #3 7/8/2009 26A 120 2.00 9.00E+01 9,780

ARAnthonyForestProducts SN-12 Solid Sample #1 9/1/2009 26 120 2.00 1.25E+02 9,780

ARAnthonyForestProducts SN-12 Solid Sample #2 9/1/2009 26 120 2.00 1.25E+02 9,780

ARAnthonyForestProducts SN-12 Solid Sample #3 9/2/2009 26 120 2.00 1.25E+02 9,780

ARPotlatchForestWarren Wellons Boiler Solid Sample #1 8/8/2006 26A 60 1.00 16 1.80E+02 9,780 4.65E-04 YES

ARPotlatchForestWarren Wellons Boiler Solid Sample #2 8/8/2006 26A 60 1.00 15.5 1.80E+02 9,780 4.23E-04 YES

ARPotlatchForestWarren Wellons Boiler Solid Sample #3 9/8/2006 26A 60 1.00 16 1.80E+02 9,780 4.65E-04 YES

ARPotlatchForestWarren Wellons Boiler Solid 1 9/8/2009 26A 60 1.00 4.22 1.80E+02 9,780 1.38E-04 YES

ARPotlatchForestWarren Wellons Boiler Solid 2 9/8/2009 26A 60 1.00 4.9 1.80E+02 9,780 1.43E-04 YES

ARPotlatchForestWarren Wellons Boiler Solid 3 9/8/2009 26A 60 1.00 4.39 1.80E+02 9,780 1.39E-04 YES

AZCatalystPaperSnowflake Power Boiler #2 Coal Solid Sample #1 3/24/2006 26A 60 1.00 1.80E+02 9,780

AZCatalystPaperSnowflake Power Boiler #2 Coal Solid Sample #2 3/24/2006 26A 60 1.00 1.80E+02 9,780

AZCatalystPaperSnowflake Power Boiler #2 Coal Solid Sample #3 3/24/2006 26A 60 1.00 1.80E+02 9,780

FLSugarCaneGrowersCoop Boiler No. 8 Solid Sample #1 12/16/2002 9,780

FLSugarCaneGrowersCoop Boiler No. 8 Solid Sample #2 12/16/2002 9,780

FLSugarCaneGrowersCoop Boiler No. 8 Solid Sample #3 12/16/2002 9,780

FLSugarCaneGrowersCoop Boiler No. 8 Solid Sample #1 1/19/2005 9,780

FLSugarCaneGrowersCoop Boiler No. 8 Solid Sample #2 1/19/2005 9,780

FLSugarCaneGrowersCoop Boiler No. 8 Solid Sample #3 1/19/2005 9,780

FLUSSugarCorp Boiler No. 4 Solid Sample #1 12/10/2002 9,780

FLUSSugarCorp Boiler No. 4 Solid Sample #2 12/10/2002 9,780

FLUSSugarCorp Boiler No. 4 Solid Sample #3 12/10/2002 9,780

FLUSSugarCorp Boiler No. 4 Solid Sample #1 12/1/2006 26A 60 1.00 1.80E+02 9,780

FLUSSugarCorp Boiler No. 4 Solid Sample #1 12/1/2006 9,780

FLUSSugarCorp Boiler No. 4 Solid Sample #2 12/1/2006 26A 60 1.00 1.80E+02 9,780

FLUSSugarCorp Boiler No. 4 Solid Sample #2 12/1/2006 9,780

FLUSSugarCorp Boiler No. 4 Solid Sample #3 12/1/2006 26A 60 1.00 1.80E+02 9,780

FLUSSugarCorp Boiler No. 4 Solid Sample #3 12/1/2006 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #1 12/31/2002 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #2 12/31/2002 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #3 12/31/2002 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #1 1/2/2003 26A 60 1.00 1.80E+02 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #2 1/2/2003 26A 60 1.00 1.80E+02 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #3 1/2/2003 26A 60 1.00 1.80E+02 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #1 1/25/2007 26A 60 1.00 1.80E+02 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #2 1/25/2007 26A 60 1.00 1.80E+02 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #3 1/25/2007 26A 50 0.83 1.80E+02 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #1 5/15/2007 26A 60 1.00 1.80E+02 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #2 5/15/2007 9,780

FLUSSugarCorp Boiler No. 7 Solid Sample #3 5/16/2007 9,780

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #1 8/13/2009 26 240 4.00 6.25E+01 9,780

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #2 8/13/2009 26 240 4.00 6.25E+01 9,780

GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #3 8/14/2009 26 240 4.00 6.25E+01 9,780

GARayonierJesupMill PB01 Solid Sample #1 5/11/2004 9,780

GARayonierJesupMill PB01 Solid Sample #2 5/11/2004 9,780

GARayonierJesupMill PB01 Solid Sample #3 5/12/2004 9,780

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #1 8/24/2009 FTIR 240 4.00 9,780

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #2 8/24/2009 FTIR 240 4.00 9,780

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #3 8/25/2009 FTIR 240 4.00 9,780

IARoquetteAmerica Circulating Fluidized Bed Boiler (121) Solid 1 6/2/2009 26A 120 2.00 9.00E+01 9,780

IARoquetteAmerica Circulating Fluidized Bed Boiler (121) Solid 2 6/2/2009 26A 120 2.00 9.00E+01 9,780

IARoquetteAmerica Circulating Fluidized Bed Boiler (121) Solid 3 6/3/2009 26A 120 2.00 9.00E+01 9,780

IDMoyieSprings Lumber420 HFB1 Solid Sample #1 9/12/2003 9,780

IDMoyieSprings Lumber420 HFB1 Solid Sample #2 9/12/2003 9,780

IDMoyieSprings Lumber420 HFB1 Solid Sample #3 9/12/2003 9,780

IDPotlatch PB-1 CE Solid Sample #1 7/28/2009 26 60 1.00 13.2 2.50E+02 9,780 4.13E-04

IDPotlatch PB-1 CE Solid Sample #2 7/28/2009 26 60 1.00 13.8 2.50E+02 9,780 4.47E-04

IDPotlatch PB-1 CE Solid Sample #3 7/28/2009 26 60 1.00 13 2.50E+02 9,780 4.02E-04

IDTASCOPaul Babcock and Wilcox (B&W) Boiler Solid Sample #1 6/1/2006 26A 64 1.07 1.80E+02 9,780

IDTASCOPaul Erie City Boiler Solid Sample #1 6/20/2006 26A 64 1.07 1.80E+02 9,780

IDTASCOPaul Erie City Boiler Solid Sample #2 6/20/2006 26A 64 1.07 1.80E+02 9,780

IDTASCOPaul Erie City Boiler Solid Sample #3 6/21/2006 26A 64 1.07 1.80E+02 9,780

INAlcoaWarrick Unit #3 Solid M26A-1 8/17/2009 9,780

INAlcoaWarrick Unit #3 Solid M26A-2 8/17/2009 9,780

INAlcoaWarrick Unit #3 Solid M26A-3 8/17/2009 9,780

LAGPPortHudson EQT0109 - No. 6 CFB Boiler Solid Sample #1 8/14/2007 26A 60 1.00 1.80E+02 9,780

LAGPPortHudson EQT0109 - No. 6 CFB Boiler Solid Sample #2 8/14/2007 26A 60 1.00 1.80E+02 9,780

LAGPPortHudson EQT0109 - No. 6 CFB Boiler Solid Sample #3 8/14/2007 26A 60 1.00 1.80E+02 9,780

MEBoralexStratton Boiler #1 Solid Sample #1 10/21/2009 26A 60 1.00 6.3 1.80E+02 9,780 1.57E-04

MEBoralexStratton Boiler #1 Solid Sample #2 10/21/2009 26A 60 1.00 5.9 1.80E+02 9,780 1.53E-04

MEBoralexStratton Boiler #1 Solid Sample #3 10/21/2009 26A 60 1.00 5.9 1.80E+02 9,780 1.53E-04

MICityofEscanaba EUBOILER#1 Solid Sample #1 10/27/2004 26A 60 1.00 1.80E+02 9,780

MICityofEscanaba EUBOILER#1 Solid Sample #2 10/27/2004 26A 60 1.00 1.80E+02 9,780

MICityofEscanaba EUBOILER#1 Solid Sample #3 10/27/2004 26A 60 1.00 1.80E+02 9,780

MSBowaterSouth Bark Boiler Solid Sample #1 1/23/2007 9,780

MSBowaterSouth Bark Boiler Solid Sample #2 1/23/2007 9,780

MSBowaterSouth Bark Boiler Solid Sample #3 1/23/2007 9,780

MSGPNewAugusta AA-015 Power Boiler Solid Sample #1 7/12/2006 9,780

MSGPNewAugusta AA-015 Power Boiler Solid Sample #2 7/12/2006 9,780

MSGPNewAugusta AA-015 Power Boiler Solid Sample #3 7/12/2006 9,780

MSGPNewAugusta AA-015 Power Boiler Solid Sample #1 9/22/2010 9,780

MSGPNewAugusta AA-015 Power Boiler Solid Sample #2 9/23/2010 9,780

MSGPNewAugusta AA-015 Power Boiler Solid Sample #3 9/23/2010 9,780

MSGPNewAugusta AA-015 Power Boiler Solid Sample #1 9/28/2010 9,780

MSGPNewAugusta AA-015 Power Boiler Solid Sample #2 9/29/2010 9,780

MSGPNewAugusta AA-015 Power Boiler Solid Sample #3 9/30/2010 9,780

MSHankinsLumber Boiler #1 (AA-001) Solid Sample #2 1/10/2005 9,780

MSHoodWaynesboro AA-001 (Wood-Fired Boiler) Solid Sample #1 10/14/2003 26A 60 1.00 1.80E+02 9,780

MSHoodWaynesboro AA-001 (Wood-Fired Boiler) Solid Sample #2 10/14/2003 26A 60 1.00 1.80E+02 9,780

MSHoodWaynesboro AA-001 (Wood-Fired Boiler) Solid Sample #3 10/14/2003 26A 60 1.00 1.80E+02 9,780

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #1 8/6/2009 26A 120 2.00 8.06 9.00E+01 9,780 8.93E-05

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #2 8/6/2009 26A 120 2.00 7.25 9.00E+01 9,780 8.40E-05

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #3 8/6/2009 26A 120 2.00 7.63 9.00E+01 9,780 8.64E-05

NCGPRoxboro ES-1 Wood fired Boiler Solid Sample #1 7/14/2004 26A 60 1.00 1.80E+02 9,780

NCGPRoxboro ES-1 Wood fired Boiler Solid Sample #2 7/14/2004 26A 120 2.00 9.00E+01 9,780

Page 1 of 3
Appendix B-1: Sample Times and Oxygen Percentages Used to Estimate HCl 3x RDL

Facility ID Combusor ID Fuel Category Test ID Test Date

Test 

Method

Sample 

Time 

(min)

Sample 

Time (hrs)

Stack Oxygen 

Concentration 

(%)

3x RDL 

(μg/dscm)

Fd Factor 

(dscf/MMBtu)

3x RDL 

(lb/MMBtu)

Use in 

New 

Source 3x 

RDL?

NCGPRoxboro ES-1 Wood fired Boiler Solid Sample #3 7/14/2004 26A 120 2.00 9.00E+01 9,780

NCLPRoaringRiver Boiler #2 Solid Sample #1 10/13/2004 9,780

NCLPRoaringRiver Boiler #2 Solid Sample #2 10/14/2004 9,780

NCLPRoaringRiver Boiler #2 Solid Sample #3 10/14/2004 9,780

NDCargillWestFargo Foster Wheeler Boiler (EU43) Solid 1 8/25/2009 26A 120 2.00 9.00E+01 9,780

NDCargillWestFargo Foster Wheeler Boiler (EU43) Solid 2 8/25/2009 26A 120 2.00 9.00E+01 9,780

NDCargillWestFargo Foster Wheeler Boiler (EU43) Solid 3 8/25/2009 26A 120 2.00 9.00E+01 9,780

NDMinnDakFarmers Babcock and Wilcox Boiler #5 Solid Sample #1 10/26/2006 26A 60 1.00 1.80E+02 9,780

NDMinnDakFarmers Babcock and Wilcox Boiler #5 Solid Sample #2 10/26/2006 26A 60 1.00 1.80E+02 9,780

NDMinnDakFarmers Babcock and Wilcox Boiler #5 Solid Sample #3 10/26/2006 26A 60 1.00 1.80E+02 9,780

ORRoseburgCoquille Boiler 1 Solid Sample #1 10/14/2004 26A 60 1.00 1.80E+02 9,780

ORRoseburgCoquille Boiler 1 Solid Sample #1 10/14/2004 26A 60 1.00 1.80E+02 9,780

ORRoseburgCoquille Boiler 1 Solid Sample #1 10/14/2004 26A 60 1.00 1.80E+02 9,780

ORRoseburgCoquille Boiler 1 Solid Sample #2 10/14/2004 26A 60 1.00 1.80E+02 9,780

ORRoseburgCoquille Boiler 1 Solid Sample #2 10/14/2004 26A 60 1.00 1.80E+02 9,780

ORRoseburgCoquille Boiler 1 Solid Sample #2 10/14/2004 26A 60 1.00 1.80E+02 9,780

ORRoseburgRiddle2 Boiler #2 Solid Sample #1 10/11/2004 26A 60 1.00 1.80E+02 9,780

ORRoseburgRiddle2 Boiler #2 Solid Sample #2 10/11/2004 26A 60 1.00 1.80E+02 9,780

ORRoseburgRiddle2 Boiler #2 Solid Sample #3 10/11/2004 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #81 Coal Boiler Solid Sample #3 7/17/2007 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #81 Coal Boiler Solid Sample #1 7/18/2007 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #81 Coal Boiler Solid Sample #2 7/18/2007 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #81 Coal Boiler Solid 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #81 Coal Boiler Solid 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #81 Coal Boiler Solid 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #82 Coal Boiler Solid Sample #3 7/17/2007 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #82 Coal Boiler Solid Sample #1 7/18/2007 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #82 Coal Boiler Solid Sample #2 7/18/2007 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #82 Coal Boiler Solid 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #82 Coal Boiler Solid 26A 60 1.00 1.80E+02 9,780

PADomtarJohnsonburg #82 Coal Boiler Solid 26A 60 1.00 1.80E+02 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #1 11/25/2003 26A 60 1.00 1.80E+02 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #2 11/25/2003 26A 60 1.00 1.80E+02 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #3 11/25/2003 26A 60 1.00 1.80E+02 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #1 11/3/2005 26A 60 1.00 1.80E+02 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #2 11/3/2005 26A 60 1.00 1.80E+02 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #3 11/3/2005 26A 60 1.00 1.80E+02 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #1 11/7/2007 26A 60 1.00 1.80E+02 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #2 11/7/2007 26A 60 1.00 1.80E+02 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #3 11/7/2007 26A 60 1.00 1.80E+02 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #1 8/18/2009 26A 240 4.00 4.50E+01 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #2 8/18/2009 26A 240 4.00 4.50E+01 9,780

SCCogenSouth B001 - Main Boiler Solid Sample #3 8/19/2009 26A 240 4.00 4.50E+01 9,780

SCMarlboroPaper Hogged Fuel Boiler Solid Sample #1 7/14/2009 26A 180 3.00 9.74 6.00E+01 9,780 6.85E-05

SCMarlboroPaper Hogged Fuel Boiler Solid Sample #2 7/14/2009 26A 180 3.00 9.38 6.00E+01 9,780 6.63E-05

SCMarlboroPaper Hogged Fuel Boiler Solid Sample #3 7/14/2009 26A 180 3.00 9.11 6.00E+01 9,780 6.48E-05

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #1 10/6/2005 9,780

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #2 10/6/2005 9,780

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #3 10/6/2005 9,780

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #1 10/7/2005 9,780

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #2 10/7/2005 9,780

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #3 10/7/2005 9,780

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #1 8/4/2009 26A 120 2.00 9.00E+01 9,780

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #2 8/4/2009 26A 120 2.00 9.00E+01 9,780

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #3 8/5/2009 26A 120 2.00 9.00E+01 9,780

TNEastman_NO_CBIDATA Boiler 30 Solid Sample #1 8/26/2009 26A 120 2.00 9.00E+01 9,780

TNEastman_NO_CBIDATA Boiler 30 Solid Sample #2 8/27/2009 26A 120 2.00 9.00E+01 9,780

TNEastman_NO_CBIDATA Boiler 30 Solid Sample #3 8/27/2009 26A 120 2.00 9.00E+01 9,780

TXDibollTemple-Inland PB-44 Solid Sample #1 6/29/2007 26A 60 1.00 1.80E+02 9,780

TXDibollTemple-Inland PB-44 Solid Sample #2 6/29/2007 26A 60 1.00 1.80E+02 9,780

TXDibollTemple-Inland PB-44 Solid Sample #3 6/29/2007 26A 60 1.00 1.80E+02 9,780

VASmurfitStoneWestpt PB08 Solid Sample #1 11/8/2004 9,780

VASmurfitStoneWestpt PB08 Solid Sample #2 11/8/2004 26A 60 1.00 1.80E+02 9,780

VASmurfitStoneWestpt PB08 Solid Sample #3 11/8/2004 26A 60 1.00 1.80E+02 9,780

VASmurfitStoneWestpt PB08 Solid Sample #1 9/26/2009 26A 120 2.00 9.00E+01 9,780

VASmurfitStoneWestpt PB08 Solid Sample #2 9/26/2009 26A 120 2.00 9.00E+01 9,780

VASmurfitStoneWestpt PB08 Solid Sample #3 9/26/2009 26A 120 2.00 9.00E+01 9,780

VAUniversityofVirginia 7103-1-01R Solid M26A-1 9/15/2009 26A 120 2.00 9.00E+01 9,780

VAUniversityofVirginia 7103-1-01R Solid M26A-2 9/16/2009 26A 120 2.00 9.00E+01 9,780

VAUniversityofVirginia 7103-1-01R Solid M26A-3 9/17/2009 26A 120 2.00 9.00E+01 9,780

WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #1 6/22/2006 26 60 1.00 2.50E+02 9,780

WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #2 6/22/2006 26 60 1.00 2.50E+02 9,780

WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #3 6/22/2006 26 60 1.00 2.50E+02 9,780

WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #1 8/14/2009 26 60 1.00 2.50E+02 9,780

WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #2 8/14/2009 26 60 1.00 2.50E+02 9,780

WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #3 8/14/2009 26 60 1.00 2.50E+02 9,780

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Solid Sample #1 8/11/2009 26 240 4.00 7 6.25E+01 9,780 5.73E-05

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Solid Sample #2 8/11/2009 26 240 4.00 7 6.25E+01 9,780 5.73E-05

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Solid Sample #3 8/12/2009 26 240 4.00 7 6.25E+01 9,780 5.73E-05

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #1 10/27/1992 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #2 10/27/1992 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #3 10/27/1992 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #1 8/10/2004 26A 60 1.00 6 1.80E+02 9,780 1.54E-04

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #2 8/10/2004 26A 60 1.00 6 1.80E+02 9,780 1.54E-04

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #3 8/11/2004 26A 60 1.00 6 1.80E+02 9,780 1.54E-04

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #1 7/19/2005 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #2 7/19/2005 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #3 7/19/2005 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #1 8/21/2006 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #2 8/21/2006 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #3 8/21/2006 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid 26A 60 1.00 1.80E+02 9,780

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid 26A 60 1.00 1.80E+02 9,780

WINewPageBiron B24 Solid Sample #1 9/12/2007 26A 60 1.00 1.80E+02 9,780

WINewPageBiron B24 Solid Sample #2 9/12/2007 26A 60 1.00 1.80E+02 9,780

WINewPageBiron B24 Solid Sample #3 9/12/2007 26A 60 1.00 1.80E+02 9,780

Page 2 of 3
Appendix B-1: Sample Times and Oxygen Percentages Used to Estimate HCl 3x RDL

Facility ID Combusor ID Fuel Category Test ID Test Date

Test 

Method

Sample 

Time 

(min)

Sample 

Time (hrs)

Stack Oxygen 

Concentration 

(%)

3x RDL 

(μg/dscm)

Fd Factor 

(dscf/MMBtu)

3x RDL 

(lb/MMBtu)

Use in 

New 

Source 3x 

RDL?

WINewPageBiron B24 Solid 1 8/25/2009 26A 120 2.00 9.00E+01 9,780

WINewPageBiron B24 Solid 2 9/22/2009 26A 120 2.00 9.00E+01 9,780

WINewPageBiron B24 Solid 3 9/22/2009 26A 120 2.00 9.00E+01 9,780

WINewPage-WisconsinRapids Power Boiler 1 - B21 Solid Sample #1 12/14/2005 26A 60 1.00 1.80E+02 9,780

WINewPage-WisconsinRapids Power Boiler 1 - B21 Solid Sample #2 12/15/2005 26A 60 1.00 1.80E+02 9,780

WINewPage-WisconsinRapids Power Boiler 1 - B21 Solid Sample #3 12/15/2005 26A 60 1.00 1.80E+02 9,780

CTElectric Boat EMU 17 Liquid 1 8/17/2009 9,190

CTElectric Boat EMU 17 Liquid 2 8/17/2009 9,190

CTElectric Boat EMU 17 Liquid 3 8/17/2009 9,190

PABoeingRidleyPark 033 Liquid Sample #1 9/22/2009 9,190

PABoeingRidleyPark 033 Liquid Sample #2 9/23/2009 9,190

PABoeingRidleyPark 033 Liquid Sample #3 9/24/2009 9,190

SCMilliken-Dewey D30 Liquid Sample #1 8/13/2009 26A 120 2.00 3.83 9.00E+01 9,190 6.32E-05

SCMilliken-Dewey D30 Liquid Sample #2 8/13/2009 26A 120 2.00 4.02 9.00E+01 9,190 6.39E-05

SCMilliken-Dewey D30 Liquid Sample #3 8/13/2009 26A 120 2.00 3.96 9.00E+01 9,190 6.37E-05

TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #1 8/31/2006 26A 60 1.00 10 1.80E+02 9,190 1.98E-04 YES

TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #2 8/31/2006 26A 60 1.00 9.9 1.80E+02 9,190 1.96E-04 YES

TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #3 8/31/2006 26A 60 1.00 9.9 1.80E+02 9,190 1.96E-04 YES

TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #1 7/29/2009 26A 60 1.00 7.4 1.80E+02 9,190 1.60E-04 YES

TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #2 7/30/2009 26A 60 1.00 6.4 1.80E+02 9,190 1.49E-04 YES

TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #3 7/30/2009 26A 60 1.00 6.8 1.80E+02 9,190 1.53E-04 YES

WVMountainStateCarbonFollansbee S1 Process Gas Sample #1 10/22/2009 26A 120 2.00 4.5 9.00E+01 8,710 6.23E-05 YES

WVMountainStateCarbonFollansbee S1 Process Gas Sample #2 10/22/2009 26A 120 2.00 4.7 9.00E+01 8,710 6.31E-05 YES

WVMountainStateCarbonFollansbee S1 Process Gas Sample #3 10/23/2009 26A 120 2.00 4.8 9.00E+01 8,710 6.35E-05 YES

CTElectric Boat EMU 17 Liquid 8/17/2009 26A 60 1.00 4.63 1.80E+02 9,190 1.33E-04

CTElectric Boat EMU 17 Liquid 8/17/2009 26A 60 1.00 4.67 1.80E+02 9,190 1.33E-04

CTElectric Boat EMU 17 Liquid 8/17/2009 26A 60 1.00 4.68 1.80E+02 9,190 1.33E-04

FLSugarCaneGrowersCoop Boiler No. 8 Solid 1/19/2005 26A 60 1.00 7.93 1.80E+02 9,780 1.77E-04

FLSugarCaneGrowersCoop Boiler No. 8 Solid 1/19/2005 26A 60 1.00 7.38 1.80E+02 9,780 1.70E-04

FLSugarCaneGrowersCoop Boiler No. 8 Solid 1/19/2005 26A 60 1.00 7.32 1.80E+02 9,780 1.69E-04

FLSugarCaneGrowersCoop Boiler No. 8 Solid 12/16/2002 26A 60 1.00 8.6 1.80E+02 9,780 1.86E-04

FLSugarCaneGrowersCoop Boiler No. 8 Solid 12/16/2002 26A 60 1.00 7.85 1.80E+02 9,780 1.76E-04

FLSugarCaneGrowersCoop Boiler No. 8 Solid 12/16/2002 26A 60 1.00 8.85 1.80E+02 9,780 1.90E-04

FLUSSugarCorp Boiler No. 7 Solid 12/31/2002 26A 60 1.00 8.48 1.80E+02 9,780 1.85E-04

FLUSSugarCorp Boiler No. 7 Solid 37623 26A 60 1.00 1.80E+02 9,780

FLUSSugarCorp Boiler No. 7 Solid 37623 26A 60 1.00 1.80E+02 9,780

IDMoyieSprings Lumber420 HFB1 Solid 9/12/2003 26A 72 1.20 1.80E+02 9,780

IDMoyieSprings Lumber420 HFB1 Solid 9/12/2003 26A 72 1.20 1.80E+02 9,780

IDMoyieSprings Lumber420 HFB1 Solid 9/12/2003 26A 72 1.20 1.80E+02 9,780

INAlcoaWarrick Unit #3 Solid 8/17/2009 26A 120 2.00 5.4 9.00E+01 9,780 7.40E-05

INAlcoaWarrick Unit #3 Solid 8/17/2009 26A 120 2.00 5.49 9.00E+01 9,780 7.45E-05

INAlcoaWarrick Unit #3 Solid 8/17/2009 26A 120 2.00 5.55 9.00E+01 9,780 7.48E-05

MEFPLEnergyWyman Unit #5 Liquid 10/5/2009 26A 9,190

MEFPLEnergyWyman Unit #5 Liquid 10/5/2009 26A 9,190

MEFPLEnergyWyman Unit #5 Liquid 10/5/2009 26A 9,190

MIConsumerEnergyCo-Campbell EUAUXBLR12 Liquid 9/1/2009 320 153 2.55 9,190

MIConsumerEnergyCo-Campbell EUAUXBLR12 Liquid 9/1/2009 320 149 2.48 9,190

MIConsumerEnergyCo-Campbell EUAUXBLR12 Liquid 9/1/2009 320 124 2.07 9,190

MIConsumerEnergyCo-Campbell EUAUXBLR12 Liquid 9/1/2009 320 124 2.07 9,190

MNGPDuluth EU33 Boiler #3 Liquid 8/6/2009 26A 120 2.00 9.00E+01 9,190

MNGPDuluth EU33 Boiler #3 Liquid 8/6/2009 26A 120 2.00 9.00E+01 9,190

MNGPDuluth EU33 Boiler #3 Liquid 8/6/2009 26A 120 2.00 9.00E+01 9,190

MSGPNewAugusta AA-015 Power Boiler Solid 7/12/2006 26 60 1.00 2.50E+02 9,780

MSGPNewAugusta AA-015 Power Boiler Solid 7/12/2006 26 60 1.00 2.50E+02 9,780

MSGPNewAugusta AA-015 Power Boiler Solid 7/12/2006 26 60 1.00 2.50E+02 9,780

MSGPNewAugusta AA-015 Power Boiler Solid 9/22/2010 26 240 4.00 9,780

MSGPNewAugusta AA-015 Power Boiler Solid 9/22/2010 26 240 4.00 9,780

MSGPNewAugusta AA-015 Power Boiler Solid 9/22/2010 26 240 4.00 9,780

MSGPNewAugusta AA-015 Power Boiler Solid 40449 26 240 4.00 9,780

MSGPNewAugusta AA-015 Power Boiler Solid 40449 26 240 4.00 9,780

MSGPNewAugusta AA-015 Power Boiler Solid 40449 26 240 4.00 9,780

NCLPRoaringRiver Boiler #2 Solid 10/13/2004 26A 64 1.07 1.80E+02 9,780

NCLPRoaringRiver Boiler #2 Solid 10/13/2004 26A 64 1.07 1.80E+02 9,780

NCLPRoaringRiver Boiler #2 Solid 10/13/2004 26A 64 1.07 1.80E+02 9,780

PABoeingRidleyPark 033 Liquid 9/22/2009 26A 120 2.00 9.00E+01 9,190

PABoeingRidleyPark 033 Liquid 9/22/2009 26A 120 2.00 9.00E+01 9,190

PABoeingRidleyPark 033 Liquid 9/22/2009 26A 120 2.00 9.00E+01 9,190

SCDAKAmericas P8F Liquid 7/15/2009 26A 120 2.00 3.6 9.00E+01 9,190 6.24E-05

SCDAKAmericas P8F Liquid 7/15/2009 26A 120 2.00 3.5 9.00E+01 9,190 6.20E-05

SCDAKAmericas P8F Liquid 40010 26A 120 2.00 3.6 9.00E+01 9,190 6.24E-05

TNBowaterNewsprint BFB North Solid 40092 26A 60 1.00 5.6 1.80E+02 9,780 1.50E-04

TNBowaterNewsprint BFB North Solid 40092 26A 60 1.00 5.4 1.80E+02 9,780 1.48E-04

TNBowaterNewsprint BFB North Solid 40092 26A 60 1.00 5.8 1.80E+02 9,780 1.52E-04

TNBowaterNewsprint BFB South Solid 40092 26A 60 1.00 1.80E+02 9,780

TNBowaterNewsprint BFB South Solid 40092 26A 60 1.00 1.80E+02 9,780

TNBowaterNewsprint BFB South Solid 40092 26A 60 1.00 1.80E+02 9,780

WINewPageBiron B24 - boiler 5 Solid 9/22/2009 26A 140 2.33 7.1 9.00E+01 9,780 8.31E-05

WINewPageBiron B24 - boiler 5 Solid 9/22/2009 26A 140 2.33 7.1 9.00E+01 9,780 8.31E-05

WINewPageBiron B24 - boiler 5 Solid 9/22/2009 26A 140 2.33 9.7 9.00E+01 9,780 1.02E-04

Page 3 of 3
Table B-2a: Summary of HCl 3x RDL for Existing Sources

Fuel Category

Average Sample Volume (dscm)

 or Sample Time (hrs)

3x RDL

(μg/dscm)

Fd Factor for 

Subcategory

(dscf/MMBtu)

Average Stack Oxy

Concentration (%

Solid 2 8.07E+00 148 9780.00 

Liquid 2 5.79E+00 129 9190.00 

Process Gas 2 4.67E+00 90 8710.00 

Table B-2b: Summary of HCl 3x RDL for New Sources

Fuel Category

Average Sample Volume (dscm)

 or Sample Time (hrs)

3x RDL

(μg/dscm)

Fd Factor for 

Subcategory

(dscf/MMBtu)

Average Stack Oxy

Concentration (%

Solid 1 1.02E+01 180 9780.00 

Liquid 1 8.40E+00 180 9190.00 

Process Gas 2 4.67E+00 90 8710.00 

Page 1 of 1
Appendix C

Calculation of 3x RDL for Filterable Particulate Matter

   
Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date

Sample 

Time 

(min)

Sample 

Time (hrs)

Stack Oxygen 

Concentration 

(%)

Use in 

New 

Source 3x 

RDL?

ALIPCourtland No. 3 Combination Boier / 11Cu301 Biomass FB Sample #1 7/7/2009

ALIPCourtland No. 3 Combination Boier / 11Cu301 Biomass FB Sample #2 7/7/2009

ALIPCourtland No. 3 Combination Boier / 11Cu301 Biomass FB Sample #3 7/8/2009

ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner Sample #1 8/8/2006 60 1.00 16

ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner Sample #2 8/8/2006 60 1.00 15.5

ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner Sample #3 8/8/2006 60 1.00 16

ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner 1 9/9/2009 240 4.00 4.22

ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner 2 9/9/2009 240 4.00 4.9

ARPotlatchForestWarren Wellons Boiler Biomass Dutch Oven/Pile Burner 3 9/10/2009 240 4.00 4.39

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #1 8/7/1997 120 2.00 6.7 YES

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #2 8/7/1997 120 2.00 6.4 YES

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #3 8/7/1997 120 2.00 6.4 YES

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #1 12/5/2002 60 1.00 8.07 YES

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #2 12/5/2002 60 1.00 7.84 YES

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #3 12/5/2002 60 1.00 7.84 YES

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #1 7/22/2009 240 4.00 9.18 YES

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #2 7/23/2009 240 4.00 9.23 YES

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner Sample #3 7/23/2009 240 4.00 9.33 YES

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 1/20/1998

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 1/20/1998

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 1/20/1998

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 11/24/1998

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 11/24/1998

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 11/24/1998

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 11/22/1999

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 11/22/1999

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 11/22/1999

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #4 11/22/1999

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 12/1/1999

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 12/1/1999

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 12/1/1999

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 1/18/2001

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 1/18/2001

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 1/18/2001

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 11/20/2001

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 11/20/2001

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 11/20/2001

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 12/2/2002

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 12/2/2002

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 12/2/2002

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 1/13/2004

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 1/13/2004

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 1/13/2004

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 1/21/2005

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 1/21/2005

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 1/21/2005

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 1/18/2006

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 1/18/2006

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 1/18/2006

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 12/7/2006

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 12/7/2006

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 12/7/2006

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 12/19/2007

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 12/19/2007

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 12/19/2007

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 1/13/2009

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 1/13/2009

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 1/13/2009

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 12/22/2009

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 12/22/2009

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 12/22/2009

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #1 12/7/2010

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #2 12/7/2010

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate Sample #3 12/7/2010

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 2/8/1999

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 2/8/1999

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 2/8/1999

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 12/17/1999

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 12/17/1999

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 12/17/1999

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 1/31/2000

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 1/31/2000

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 1/31/2000

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 1/5/2001

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 1/5/2001

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 1/6/2001

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 1/9/2002

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 1/9/2002

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 1/9/2002

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 11/15/2002

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 11/15/2002

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 11/15/2002

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 12/30/2003

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 12/30/2003

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 12/30/2003

Page 1 of 12
Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date

Sample 

Time 

(min)

Sample 

Time (hrs)

Stack Oxygen 

Concentration 

(%)

Use in 

New 

Source 3x 

RDL?

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 2/4/2005

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 2/4/2005

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 2/4/2005

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 1/5/2006

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 1/5/2006

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 1/5/2006

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 1/25/2007

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 1/25/2007

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 1/25/2007

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 1/24/2008

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 1/24/2008

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 1/24/2008

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 12/4/2008

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 12/4/2008

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 12/4/2008

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 11/20/2009

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 11/20/2009

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 11/20/2009

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #1 11/4/2010

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #2 11/4/2010

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate Sample #3 11/4/2010

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 3/24/2005

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 3/24/2005

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 3/24/2005

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 3/26/2005

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 3/26/2005

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 3/26/2005

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 1/10/2006

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 1/10/2006

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 1/10/2006

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 6/2/2006 60 1.00 7.58

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 6/2/2006 60 1.00 7.99

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 6/2/2006 60 1.00 9.22

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #4 6/2/2006 60 1.00 9.84

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #5 6/2/2006 60 1.00 9.1

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 8/22/2006 64 1.07 10.36

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 8/22/2006 64 1.07 10.43

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 8/22/2006 64 1.07 10.3

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 39083 60 1.00 6.52

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 39083 60 1.00 6.96

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #4 39083 60 1.00 6.53

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 1/5/2007 60 1.00 7.73

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 1/5/2007 60 1.00 7.65

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 1/5/2007 60 1.00 7.25

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 11/30/2007

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 11/30/2007

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 11/30/2007

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 12/11/2008

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 12/11/2008

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 12/11/2008

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #4 12/11/2008

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 12/2/2009 60 1.00 6.4

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 12/2/2009 60 1.00 7

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 12/3/2009 60 1.00 5.6

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #1 11/30/2010

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #2 11/30/2010

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #3 11/30/2010

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate Sample #4 12/2/2010

GATempleInlandRome WF Biomass FB 1 7/27/2009

GATempleInlandRome WF Biomass FB 2 7/28/2009

GATempleInlandRome WF Biomass FB 3 7/28/2009

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #1 4/18/1994

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #2 4/18/1994

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 4/18/1994

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #1 5/22/1995

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #2 5/22/1995

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 5/22/1995

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #1 9/11/1997

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #2 9/11/1997

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 9/11/1997

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #1 7/12/2000

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #2 7/12/2000

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 7/12/2000

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #1 9/25/2003

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #2 9/25/2003

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 9/25/2003

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #1 10/07/2004

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #2 10/07/2004

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 10/07/2004

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #1 4/11/2005

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #2 4/11/2005

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 4/11/2005

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #1 4/12/2005

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #2 4/12/2005

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 4/12/2005

Page 2 of 12
Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date

Sample 

Time 

(min)

Sample 

Time (hrs)

Stack Oxygen 

Concentration 

(%)

Use in 

New 

Source 3x 

RDL?

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #4 4/12/2005

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #5 4/12/2005

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #6 4/13/2005

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #7 4/13/2005

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #8 4/13/2005

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #1 7/16/2007

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #2 7/17/2007

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 7/17/2007

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #1 8/23/2010

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #2 8/23/2010

HIPuuneneSugarMill Boiler 3 Biomass Suspension/Grate Sample #3 8/23/2010

IDPotlatch PB-1 CE Biomass Fuel Cell Sample #1 4/30/2008

IDPotlatch PB-1 CE Biomass Fuel Cell Sample #2 4/30/2008

IDPotlatch PB-1 CE Biomass Fuel Cell Sample #3 4/30/2008

IDPotlatch PB-1 CE Biomass Fuel Cell Sample #1 7/28/2009 240 4.00 13.2

IDPotlatch PB-1 CE Biomass Fuel Cell Sample #2 7/28/2009 240 4.00 13.8

IDPotlatch PB-1 CE Biomass Fuel Cell Sample #3 7/29/2009 240 4.00 13

MNWeyerhaeuserIronton EU 001 - 4 Cell Furnace Biomass Fuel Cell Sample #1 12/20/2006

MNWeyerhaeuserIronton EU 001 - 4 Cell Furnace Biomass Fuel Cell Sample #2 12/20/2006

MNWeyerhaeuserIronton EU 001 - 4 Cell Furnace Biomass Fuel Cell Sample #3 12/20/2006

MSNorbordMS Wellons No. 1 Biomass Fuel Cell Sample #1 8/1/2007

MSNorbordMS Wellons No. 1 Biomass Fuel Cell Sample #2 8/1/2007

MSNorbordMS Wellons No. 1 Biomass Fuel Cell Sample #3 8/1/2007

MSNorbordMS Wellons No. 2 Biomass Fuel Cell Sample #1 8/1/2007

MSNorbordMS Wellons No. 2 Biomass Fuel Cell Sample #2 8/1/2007

MSNorbordMS Wellons No. 2 Biomass Fuel Cell Sample #3 8/1/2007

MSNorbordMS Wellons No. 3 Biomass Fuel Cell Sample #1 8/1/2007

MSNorbordMS Wellons No. 3 Biomass Fuel Cell Sample #2 8/1/2007

MSNorbordMS Wellons No. 3 Biomass Fuel Cell Sample #3 8/1/2007

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #1 2/26/1993

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #2 2/26/1993

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #3 2/26/1993

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #1 8/23/1999

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #2 8/23/1999

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #3 8/23/1999

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #1 7/11/2003

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #2 7/11/2003

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #3 7/11/2003

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #1 6/28/2005

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #2 6/28/2005

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #3 6/28/2005

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #1 2/22/2006

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #2 2/22/2006

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #3 2/22/2006

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #1 8/31/2007

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #2 8/31/2007

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #3 8/31/2007

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #1 8/5/2009 180 3.00 8.06

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #2 8/5/2009 180 3.00 7.25

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Biomass Dutch Oven/Pile Burner Sample #3 8/5/2009 180 3.00 7.63

OHSauderWoodArchbold B009 Biomass Suspension Burner Sample #1 6/18/2008 60 1.00 9.7 YES

OHSauderWoodArchbold B009 Biomass Suspension Burner Sample #2 6/18/2008 60 1.00 9.48 YES

OHSauderWoodArchbold B009 Biomass Suspension Burner Sample #3 6/18/2008 60 1.00 9.43 YES

ORGeorgiaPacificWaunaMill EU35 - Fluidized Bed Boiler Biomass FB Sample #1 3/22/2006

ORGeorgiaPacificWaunaMill EU35 - Fluidized Bed Boiler Biomass FB Sample #2 3/22/2006

ORGeorgiaPacificWaunaMill EU35 - Fluidized Bed Boiler Biomass FB Sample #3 3/22/2006

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB Sample #1 10/6/2005

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB Sample #2 10/6/2005

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB Sample #3 10/6/2005

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB Sample #1 10/7/2005

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB Sample #2 10/7/2005

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB Sample #3 10/7/2005

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 1 8/4/2009

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 2 8/4/2009

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 3 8/5/2009

TXRGVSG Boiler No. 6 Biomass Suspension/Grate Sample #1 1/13/2009

TXRGVSG Boiler No. 6 Biomass Suspension/Grate Sample #2 1/13/2009

TXRGVSG Boiler No. 6 Biomass Suspension/Grate Sample #3 1/13/2009

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #1 9/18/1996 120 2.00 10.7 YES

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #2 9/18/1996 120 2.00 10.6 YES

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #3 9/18/1996 120 2.00 9.4 YES

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #1 11/10/2004 60 1.00 9.5 YES

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #2 11/10/2004 60 1.00 9.3 YES

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #3 11/10/2004 60 1.00 8.7 YES

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #1 8/11/2009 240 4.00 7 YES

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #2 8/11/2009 240 4.00 7 YES

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Biomass Dutch Oven/Pile Burner Sample #3 8/12/2009 240 4.00 7 YES

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Biomass FB Sample #1 9/19/2007 60 1.00

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Biomass FB Sample #2 9/19/2007 60 1.00

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Biomass FB Sample #3 9/19/2007 60 1.00

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Biomass FB Sample #1 8/20/2009 240 4.00 7

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Biomass FB Sample #2 8/20/2009 240 4.00 7

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Biomass FB Sample #3 8/21/2009 240 4.00 7

WVGPMtHopeOSB 5600 - Wellons Energy System Biomass Dutch Oven/Pile Burner Sample #1 7/11/2006

WVGPMtHopeOSB 5600 - Wellons Energy System Biomass Dutch Oven/Pile Burner Sample #2 7/11/2006

Page 3 of 12
Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date

Sample 

Time 

(min)

Sample 

Time (hrs)

Stack Oxygen 

Concentration 

(%)

Use in 

New 

Source 3x 

RDL?

WVGPMtHopeOSB 5600 - Wellons Energy System Biomass Dutch Oven/Pile Burner Sample #3 7/11/2006

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 12/12/2007

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 12/12/2007

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 12/12/2007

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 12/12/2007

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 12/12/2007

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 12/12/2007

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 12/12/2007

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 12/12/2007

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 12/12/2007

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 7/11/2008

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 7/11/2008

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 7/11/2008

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 7/11/2008

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 7/11/2008

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 7/11/2008

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 7/11/2008

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 7/11/2008

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 7/11/2008

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/24/2009

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/24/2009

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/24/2009

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/14/2011

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/14/2011

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/14/2011

ARLeolaLumberMill SN-01A Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/14/2006

ARLeolaLumberMill SN-01A Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/14/2006

ARLeolaLumberMill SN-01A Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/14/2006

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #1 8/11/1997 60 1.00 9

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #2 8/11/1997 60 1.00 9

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #3 8/11/1997 60 1.00 9

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #1 11/21/1998

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #2 11/21/1998

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #3 11/21/1998

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #1 12/10/1999

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #2 12/10/1999

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #3 12/10/1999

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #1 11/9/2000

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #2 11/9/2000

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #3 11/9/2000

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #1 12/5/2001

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #2 12/5/2001

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #3 12/5/2001

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #1 12/4/2002

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #2 12/4/2002

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #3 12/4/2002

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #1 12/4/2003

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #2 12/4/2003

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #3 12/4/2003

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #1 9/29/2004

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #2 9/29/2004

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other Sample #3 9/29/2004

CASierraPacificLincoln McBurney Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 3/5/2008

CASierraPacificLincoln McBurney Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 3/5/2008

CASierraPacificLincoln McBurney Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 3/5/2008

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 37773 120 2.00 9.78 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 37773 120 2.00 9.55 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 37773 120 2.00 7.91 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 10/14/2004 60 1.00 8.82 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 10/14/2004 60 1.00 8.76 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 10/14/2004 60 1.00 9.06 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/15/2006 60 1.00 7.75 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/15/2006 60 1.00 8.13 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/15/2006 60 1.00 8.46 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/16/2006

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/16/2006

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/16/2006

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 9/18/2007 60 1.00 7.35 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 9/18/2007

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 9/18/2007 60 1.00 6.6 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 9/18/2007

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 9/18/2007 60 1.00 7.51 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 9/18/2007

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 9/19/2007

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 9/19/2007

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 9/19/2007

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 1 8/11/2009

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 2 8/12/2009

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 3 8/12/2009

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 8/27/2009 240 4.00 8.88 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 8/27/2009

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 8/27/2009 240 4.00 8.21 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 8/27/2009

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 8/27/2009 240 4.00 7.21 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 8/27/2009

Page 4 of 12
Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date

Sample 

Time 

(min)

Sample 

Time (hrs)

Stack Oxygen 

Concentration 

(%)

Use in 

New 

Source 3x 

RDL?

GATempleInlandRome PB4 Wet Biomass Stoker/SlopedGrate/Other Sample #1 2/27/2008

GATempleInlandRome PB4 Wet Biomass Stoker/SlopedGrate/Other Sample #2 2/27/2008

GATempleInlandRome PB4 Wet Biomass Stoker/SlopedGrate/Other Sample #3 2/27/2008

IDPotlatch PB-2 Riley Wet Biomass Stoker/SlopedGrate/Other Sample #1 5/1/2008

IDPotlatch PB-2 Riley Wet Biomass Stoker/SlopedGrate/Other Sample #2 5/1/2008

IDPotlatch PB-2 Riley Wet Biomass Stoker/SlopedGrate/Other Sample #3 5/1/2008

IDRileyCreekLumber HFB1 Wet Biomass Stoker/SlopedGrate/Other Sample #1 4/24/2003 60 1.00 8

IDRileyCreekLumber HFB1 Wet Biomass Stoker/SlopedGrate/Other Sample #2 4/24/2003 60 1.00 8

IDRileyCreekLumber HFB1 Wet Biomass Stoker/SlopedGrate/Other Sample #3 4/24/2003 60 1.00 8

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other Sample #1 5/31/2002

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other Sample #2 5/31/2002

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other Sample #3 5/31/2002

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other Sample #1 5/29/2007

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other Sample #2 5/29/2007

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other Sample #3 5/29/2007

MEBoralexStratton Boiler #1 Wet Biomass Stoker/SlopedGrate/Other Sample #1 10/21/2009 55.6 0.93 6.3

MEBoralexStratton Boiler #1 Wet Biomass Stoker/SlopedGrate/Other Sample #2 10/21/2009 61.3 1.02 5.9

MEBoralexStratton Boiler #1 Wet Biomass Stoker/SlopedGrate/Other Sample #3 10/21/2009 63.5 1.06 5.9

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 7/12/2006

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 7/12/2006

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 7/12/2006

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 9/22/2010

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 9/23/2010

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 9/23/2010

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 9/28/2010

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 9/29/2010

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 9/30/2010

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 8/19/1993 90 1.50 7.1

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 8/19/1993 90 1.50 7.1

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 8/19/1993 90 1.50 7.5

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 8/16/1995 120 2.00 8.3

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 8/16/1995 120 2.00 7.1

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 8/16/1995 120 2.00 6.3

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 8/13/1997 125 2.08 3.6

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 8/13/1997 125 2.08 3.3

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 8/13/1997 125 2.08 3.1

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/16/1999 125 2.08 6.5

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/16/1999 125 2.08 6.3

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/16/1999 125 2.08 6.1

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 6/5/2003 125 2.08 8.7

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 6/5/2003 125 2.08 8.3

SCInternationalPaperEastover No. 2 Power Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 6/5/2003 125 2.08 8.4

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 1/4/2007

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 1/4/2007

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 1/4/2007

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #1 7/14/2009 180 3.00 9.74

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #2 7/14/2009 180 3.00 9.38

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other Sample #3 7/14/2009 180 3.00 9.11

WIDomtar2814 B11, S11 Wet Biomass Stoker/SlopedGrate/Other Sample #1 8/29/2007 60 1.00 7

WIDomtar2814 B11, S11 Wet Biomass Stoker/SlopedGrate/Other Sample #2 8/29/2007 60 1.00 7

WIDomtar2814 B11, S11 Wet Biomass Stoker/SlopedGrate/Other Sample #3 8/29/2007 60 1.00 7

WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other Sample #1 3/24/2005 120 2.00 7.8 YES

WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other Sample #2 3/24/2005 120 2.00 8.1 YES

WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other Sample #3 3/24/2005 120 2.00 8.4 YES

WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other Sample #4 3/24/2005 120 2.00 7.3 YES

AKDoyonUtilities_AK 4 Coal Stoker/SlopedGrate/Other Sample #1 8/17/2005 60 1.00 7

AKDoyonUtilities_AK 4 Coal Stoker/SlopedGrate/Other Sample #2 8/17/2005 60 1.00 6.67

AKDoyonUtilities_AK 4 Coal Stoker/SlopedGrate/Other Sample #3 8/17/2005 60 1.00 6.6

AKDoyonUtilities_AK 7 Coal Stoker/SlopedGrate/Other Sample #1 8/16/2005 60 1.00 7.6

AKDoyonUtilities_AK 7 Coal Stoker/SlopedGrate/Other Sample #2 8/16/2005 60 1.00 7.93

AKDoyonUtilities_AK 7 Coal Stoker/SlopedGrate/Other Sample #3 8/16/2005 60 1.00 8

FLSmurfit-Stone 7PB Coal PC Sample #1 7/11/2007 60 1.00 7.05

FLSmurfit-Stone 7PB Coal PC Sample #2 7/11/2007 60 1.00 7.29

FLSmurfit-Stone 7PB Coal PC Sample #3 7/11/2007 60 1.00 7.41

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #1 6/3/2008 100 1.67 6.9

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #2 6/3/2008 100 1.67 7.9

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #3 6/3/2008 100 1.67 7.9

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #1 8/26/2009 240 4.00 5.58

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #2 8/26/2009 240 4.00 5.56

IAArchersDanielsMidlandDesMoines Asea Boiler #1 Coal FB Sample #3 8/27/2009 240 4.00 5.66

IAIAStateUnivPowerPlant B1 Coal FB Sample #1 3/26/2008 62.5 1.04 4.3

IAIAStateUnivPowerPlant B1 Coal FB Sample #2 3/26/2008 62.5 1.04 3.9

IAIAStateUnivPowerPlant B1 Coal FB Sample #3 3/26/2008 62.5 1.04 4.4

IAIAStateUnivPowerPlant B2 Coal FB Sample #1 3/27/2008 62.5 1.04 4

IAIAStateUnivPowerPlant B2 Coal FB Sample #2 3/27/2008 62.5 1.04 3.9

IAIAStateUnivPowerPlant B2 Coal FB Sample #3 3/27/2008 62.5 1.04 3.7

IAUofNorthernIowa Boiler #3 Coal PC 4 10/6/2009

IAUofNorthernIowa Boiler #3 Coal PC 5 10/6/2009

IAUofNorthernIowa Boiler #3 Coal PC 6 10/7/2009

IDAmalgamatedSugarCoTwinFalls S-B1 Coal Stoker/SlopedGrate/Other Sample #1 9/26/2006 120 2.00 6.9

IDAmalgamatedSugarCoTwinFalls S-B1 Coal Stoker/SlopedGrate/Other Sample #2 9/26/2006 120 2.00 6.9

IDAmalgamatedSugarCoTwinFalls S-B1 Coal Stoker/SlopedGrate/Other Sample #3 9/26/2006 120 2.00 6

ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other Sample #1 8/22/2007

ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other Sample #2 8/22/2007

ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other Sample #3 8/22/2007

Page 5 of 12
Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date

Sample 

Time 

(min)

Sample 

Time (hrs)

Stack Oxygen 

Concentration 

(%)

Use in 

New 

Source 3x 

RDL?

ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other OTM28-1 8/4/2009

ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other OTM28-2 8/5/2009

ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other OTM28-3 8/5/2009

ILRockIslandArsenal NBN 12602 (Boiler #1) Coal Stoker/SlopedGrate/Other Sample #1 3/13/2007

ILRockIslandArsenal NBN 12602 (Boiler #1) Coal Stoker/SlopedGrate/Other Sample #2 3/13/2007

ILRockIslandArsenal NBN 12602 (Boiler #1) Coal Stoker/SlopedGrate/Other Sample #3 3/13/2007

INNotreDame B-4 Coal Stoker/SlopedGrate/Other Sample #1 8/26/2009

INNotreDame B-4 Coal Stoker/SlopedGrate/Other Sample #2 8/26/2009

INNotreDame B-4 Coal Stoker/SlopedGrate/Other Sample #3 8/27/2009

INSABICInnovativePlastics 01-001 BW1 Boiler Coal PC Sample #1 4/7/2005 121 2.02 7

INSABICInnovativePlastics 01-001 BW1 Boiler Coal PC Sample #2 4/7/2005 121 2.02 7

INSABICInnovativePlastics 01-001 BW1 Boiler Coal PC Sample #3 4/7/2005 121 2.02 7

INSABICInnovativePlastics 01-001 BW1 Boiler Coal PC Sample #1 6/28/2006

INSABICInnovativePlastics 01-001 BW1 Boiler Coal PC Sample #2 6/28/2006

INSABICInnovativePlastics 01-001 BW1 Boiler Coal PC Sample #3 6/28/2006

INSABICInnovativePlastics 01-001 BW2 Boiler Coal PC Sample #1 4/7/2005 123 2.05 7

INSABICInnovativePlastics 01-001 BW2 Boiler Coal PC Sample #2 4/7/2005 123 2.05 7

INSABICInnovativePlastics 01-001 BW2 Boiler Coal PC Sample #3 4/7/2005 123 2.05 7

INSABICInnovativePlastics 01-001 BW2 Boiler Coal PC Sample #1 6/28/2006 125 2.08

INSABICInnovativePlastics 01-001 BW2 Boiler Coal PC Sample #2 6/28/2006 125 2.08

INSABICInnovativePlastics 01-001 BW2 Boiler Coal PC Sample #3 6/28/2006 125 2.08

MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #1 10/31/2005 60 1.00 11.5

MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #2 10/31/2005 60 1.00 11.5

MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #3 10/31/2005 60 1.00 11.5

MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #1 11/2/2005

MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #2 11/2/2005

MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #3 11/2/2005

MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #1 11/3/2005

MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #2 11/3/2005

MNAmericanCrystalCrookston Boiler 1 Coal Stoker/SlopedGrate/Other Sample #3 11/3/2005

NCEPCORRoxboro 1-A Coal Stoker/SlopedGrate/Other Sample #1 6/16/2008

NCEPCORRoxboro 1-A Coal Stoker/SlopedGrate/Other Sample #2 6/16/2008

NCEPCORRoxboro 1-A Coal Stoker/SlopedGrate/Other Sample #3 6/16/2008

NCEPCORRoxboro 1-B Coal Stoker/SlopedGrate/Other Sample #1 6/16/2008

NCEPCORRoxboro 1-B Coal Stoker/SlopedGrate/Other Sample #2 6/16/2008

NCEPCORRoxboro 1-B Coal Stoker/SlopedGrate/Other Sample #3 6/16/2008

NCEPCORRoxboro 1-C Coal Stoker/SlopedGrate/Other Sample #1 6/16/2008

NCEPCORRoxboro 1-C Coal Stoker/SlopedGrate/Other Sample #2 6/16/2008

NCEPCORRoxboro 1-C Coal Stoker/SlopedGrate/Other Sample #3 6/16/2008

NCHanesDyeWinstonSalem ES B01 Coal Stoker/SlopedGrate/Other Sample #1 3/21/2007

NCHanesDyeWinstonSalem ES B01 Coal Stoker/SlopedGrate/Other Sample #2 3/21/2007

NCHanesDyeWinstonSalem ES B01 Coal Stoker/SlopedGrate/Other Sample #3 3/21/2007

NCHanesDyeWinstonSalem ES B02 Coal Stoker/SlopedGrate/Other Sample #1 3/21/2007

NCHanesDyeWinstonSalem ES B02 Coal Stoker/SlopedGrate/Other Sample #2 3/21/2007

NCHanesDyeWinstonSalem ES B02 Coal Stoker/SlopedGrate/Other Sample #3 3/21/2007

OHMortonSaltRittman B003 - Coal-Fired Boiler #1 Coal Stoker/SlopedGrate/Other Sample #1 8/21/2007

OHMortonSaltRittman B003 - Coal-Fired Boiler #1 Coal Stoker/SlopedGrate/Other Sample #2 8/21/2007

OHMortonSaltRittman B003 - Coal-Fired Boiler #1 Coal Stoker/SlopedGrate/Other Sample #3 8/21/2007

OHSmartPapersHoldingsLLC B010 Coal PC Sample #1 8/11/2005 120 2.00 7.9

OHSmartPapersHoldingsLLC B010 Coal PC Sample #2 8/11/2005 120 2.00 7.8

OHSmartPapersHoldingsLLC B010 Coal PC Sample #3 8/11/2005 120 2.00 7.8

OHSmartPapersHoldingsLLC B020 Coal Stoker/SlopedGrate/Other Sample #1 9/22/2005

OHSmartPapersHoldingsLLC B020 Coal Stoker/SlopedGrate/Other Sample #2 9/22/2005

OHSmartPapersHoldingsLLC B020 Coal Stoker/SlopedGrate/Other Sample #3 9/22/2005

OHUofCincinnati B108 Coal Stoker/SlopedGrate/Other Sample #3 4/27/2005

OHUofCincinnati B108 Coal Stoker/SlopedGrate/Other Sample #1 4/26/2006

OHUofCincinnati B108 Coal Stoker/SlopedGrate/Other Sample #2 4/26/2006

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #1 10/24/2000 60 1.00 6

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #2 10/24/2000 60 1.00 6.1

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #3 10/24/2000 60 1.00 5.9

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #1 10/9/2002 60 1.00 6.1

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #2 10/9/2002 60 1.00 3.1

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #3 10/9/2002 60 1.00 5.8

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #1 10/19/2004 60 1.00 5.6

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #2 10/19/2004 60 1.00 5.9

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #3 10/19/2004 60 1.00 5.4

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #1 10/25/2006 60 1.00 3.2

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #2 10/25/2006 60 1.00 3.6

SCInternationalPaperEastover No. 1 Power Boiler Coal Stoker/SlopedGrate/Other Sample #3 10/25/2006 60 1.00 3.8

TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other Sample #1 7/17/2007 60 1.00 12.4

TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other Sample #2 7/17/2007 60 1.00 12.2

TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other Sample #3 7/17/2007 60 1.00 11.9

TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other 1 8/5/2009 240 4.00 10.84

TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other 3 8/6/2009 240 4.00 10.25

TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other 2 11/6/2009 240 4.00 10.31

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #1 8/20/1996 64 1.07

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #2 8/20/1996 64 1.07

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #3 8/20/1996 64 1.07

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #1 8/8/2000 64 1.07 7

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #2 8/8/2000 64 1.07 7

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #3 8/8/2000 64 1.07 7

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #2 6/29/2004 60 1.00 7

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #3 6/29/2004 60 1.00 7

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #1 11/9/2004 120 2.00

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #2 11/9/2004 120 2.00

Page 6 of 12
Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date

Sample 

Time 

(min)

Sample 

Time (hrs)

Stack Oxygen 

Concentration 

(%)

Use in 

New 

Source 3x 

RDL?

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #1 11/10/2004 120 2.00

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #2 11/10/2004 120 2.00

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #3 11/10/2004 120 2.00

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #3 11/11/2004 120 2.00

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #1 7/24/2008 60 1.00 7

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #2 7/24/2008 60 1.00 7

TNEastman_NO_CBIDATA Boiler 25 Coal PC Sample #3 7/24/2008 60 1.00 7

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #1 7/12/1993 64 1.07 7

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #2 7/12/1993 64 1.07 7

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #3 7/12/1993 64 1.07 7

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #1 9/30/1997 64 1.07 7

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #2 9/30/1997 64 1.07 7

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #3 9/30/1997 64 1.07 7

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #1 8/14/2001 60 1.00 7

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #2 8/14/2001 60 1.00 7

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #3 8/14/2001 60 1.00 7

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #1 6/21/2005

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #2 6/21/2005

TNEastman_NO_CBIDATA Boiler 26 Coal PC Sample #3 6/21/2005

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #1 7/12/1993 64 1.07 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #2 7/12/1993 64 1.07 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #3 7/12/1993 64 1.07 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #1 9/25/1997 64 1.07 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #2 9/25/1997 64 1.07 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #3 9/25/1997 64 1.07 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #1 8/28/2001 60 1.00 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #2 8/28/2001 60 1.00 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #3 8/28/2001 60 1.00 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #1 3/9/2005 120 2.00

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #2 3/9/2005 120 2.00

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #3 3/9/2005 120 2.00

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #1 3/10/2005 120 2.00

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #2 3/10/2005 120 2.00

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #3 3/10/2005 120 2.00

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #1 5/17/2005 60 1.00 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #2 5/17/2005 60 1.00 7

TNEastman_NO_CBIDATA Boiler 27 Coal PC Sample #3 5/17/2005 60 1.00 7

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #1 7/29/1994

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #2 7/29/1994

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #3 7/29/1994

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #1 7/7/1998

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #2 7/7/1998

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #3 7/7/1998

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #1 6/6/2002

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #2 6/6/2002

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #3 6/6/2002

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #1 8/22/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #2 8/22/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 28 Coal PC Sample #3 8/22/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #1 11/8/1994 75 1.25 7

TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #2 11/8/1994 75 1.25 7

TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #3 11/8/1994 75 1.25 7

TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #1 9/19/2002 60 1.00 7

TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #2 9/19/2002 60 1.00 7

TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #3 9/19/2002 60 1.00 7

TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #1 9/19/2006 60 1.00 7

TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #2 9/19/2006 60 1.00 7

TNEastman_NO_CBIDATA Boiler 30 Coal PC Sample #3 9/19/2006 60 1.00 7

TNEastman_NO_CBIDATA Boiler 30 Coal PC 1 8/26/2009

TNEastman_NO_CBIDATA Boiler 30 Coal PC 2 8/27/2009

TNEastman_NO_CBIDATA Boiler 30 Coal PC 3 8/27/2009

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #1 8/4/1994 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #2 8/4/1994 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #3 8/4/1994 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #1 12/14/1994 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #2 12/15/1994 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #3 12/15/1994 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #1 9/29/1998 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #2 9/29/1998 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #3 9/29/1998 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #1 7/25/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #2 7/25/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #3 7/25/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #1 8/14/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #2 8/14/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #3 8/14/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #1 12/6/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #2 12/6/2006 125 2.08 7

TNEastman_NO_CBIDATA Boiler 31 Coal PC Sample #3 12/6/2006 125 2.08 7

VADukeEnergyNarrows Boiler #2 Coal PC Sample #1 10/12/2004

VADukeEnergyNarrows Boiler #2 Coal PC Sample #1 10/12/2004

VADukeEnergyNarrows Boiler #2 Coal PC Sample #2 10/12/2004

VADukeEnergyNarrows Boiler #2 Coal PC Sample #2 10/12/2004

VADukeEnergyNarrows Boiler #2 Coal PC Sample #3 10/12/2004

VADukeEnergyNarrows Boiler #2 Coal PC Sample #3 10/12/2004

Page 7 of 12
Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date

Sample 

Time 

(min)

Sample 

Time (hrs)

Stack Oxygen 

Concentration 

(%)

Use in 

New 

Source 3x 

RDL?

VADukeEnergyNarrows Boiler #3 Coal PC Sample #1 4/14/2004

VADukeEnergyNarrows Boiler #3 Coal PC Sample #2 4/14/2004

VADukeEnergyNarrows Boiler #3 Coal PC Sample #3 4/14/2004

VADukeEnergyNarrows Boiler #3 Coal PC Sample #1 10/14/2004

VADukeEnergyNarrows Boiler #3 Coal PC Sample #2 10/14/2004

VADukeEnergyNarrows Boiler #3 Coal PC Sample #3 10/14/2004

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #1 2/3/2004

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #2 2/3/2004

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #3 2/3/2004

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #1 5/24/2005

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #2 5/24/2005

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #3 5/24/2005

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #1 7/13/2006

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #2 7/13/2006

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #3 7/13/2006

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #1 5/1/2007 120 2.00

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #2 5/1/2007 120 2.00

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #3 5/1/2007 120 2.00

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #1 9/9/2008

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #2 9/9/2008

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #3 9/9/2008

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #1 3/30/2009

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #2 3/30/2009

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #3 3/30/2009

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #1 4/8/2009

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #2 4/8/2009

VAGPBigIsland2703 PWR04 - No. 4 Power Boiler Coal PC Sample #3 4/8/2009

VAUniversityofVirginia 7103-1-05 Coal Stoker/SlopedGrate/Other Sample #1 4/4/2008 60 1.00 6.8

VAUniversityofVirginia 7103-1-05 Coal Stoker/SlopedGrate/Other Sample #2 4/4/2008 60 1.00 7.5

VAUniversityofVirginia 7103-1-05 Coal Stoker/SlopedGrate/Other Sample #3 4/4/2008 60 1.00 8.5

VAUniversityofVirginia 7103-1-01R Coal Stoker/SlopedGrate/Other Sample #1 12/6/2007 60 1.00 7.07

VAUniversityofVirginia 7103-1-01R Coal Stoker/SlopedGrate/Other Sample #2 12/6/2007 60 1.00 7.09

VAUniversityofVirginia 7103-1-01R Coal Stoker/SlopedGrate/Other Sample #3 12/6/2007 60 1.00 6.98

VAUniversityofVirginia 7103-1-01R Coal Stoker/SlopedGrate/Other M027-1 9/17/2009 240 4.00

VAUniversityofVirginia 7103-1-01R Coal Stoker/SlopedGrate/Other M027-2 9/17/2009 240 4.00

VAUniversityofVirginia 7103-1-01R Coal Stoker/SlopedGrate/Other M027-3 9/18/2009 240 4.00

VAUniversityofVirginia 7103-1-02R Coal Stoker/SlopedGrate/Other Sample #1 1/16/2007 60 1.00 6.64

VAUniversityofVirginia 7103-1-02R Coal Stoker/SlopedGrate/Other Sample #2 1/16/2007 60 1.00 6.96

VAUniversityofVirginia 7103-1-02R Coal Stoker/SlopedGrate/Other Sample #3 1/16/2007 60 1.00 6.74

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 10/27/1992 120 2.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 10/27/1992 120 2.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 10/27/1992 120 2.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 9/24/1994 120 2.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 9/24/1994 120 2.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 9/24/1994 120 2.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 7/28/1998 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 7/28/1998 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 7/28/1998 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 11/9/1999

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 11/9/1999

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 11/9/1999

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 2/2/2000 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 2/2/2000 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 2/2/2000 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 7/19/2000 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 7/19/2000 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 7/19/2000 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 8/29/2000 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 8/29/2000 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 8/29/2000 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 8/28/2002 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 8/28/2002 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 8/28/2002 60 1.00

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 8/10/2004 60 1.00 6

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 8/10/2004 60 1.00 6

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 8/10/2004 60 1.00 6

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #1 9/21/2007

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #2 9/21/2007

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB Sample #3 9/21/2007

WINewPageBiron B24 Coal Stoker/SlopedGrate/Other Sample #1 9/12/2007 60 1.00

WINewPageBiron B24 Coal Stoker/SlopedGrate/Other Sample #2 9/12/2007 60 1.00

WINewPageBiron B24 Coal Stoker/SlopedGrate/Other Sample #3 9/12/2007 60 1.00

WINewPageBiron B24 Coal Stoker/SlopedGrate/Other 1 9/22/2009 240 4.00

WINewPageBiron B24 Coal Stoker/SlopedGrate/Other 2 9/22/2009 240 4.00

WINewPageBiron B24 Coal Stoker/SlopedGrate/Other 3 9/23/2009 240 4.00

WIThilmanyPapersNicoletMill B23 Coal Stoker/SlopedGrate/Other Sample #1 2/22/2006 60 1.00

WIThilmanyPapersNicoletMill B23 Coal Stoker/SlopedGrate/Other Sample #2 2/22/2006 60 1.00

WIThilmanyPapersNicoletMill B23 Coal Stoker/SlopedGrate/Other Sample #3 2/22/2006 60 1.00

WIThilmanyPapersNicoletMill B24 Coal Stoker/SlopedGrate/Other Sample #1 2/22/2006 60 1.00

WIThilmanyPapersNicoletMill B24 Coal Stoker/SlopedGrate/Other Sample #2 2/22/2006 60 1.00

WIThilmanyPapersNicoletMill B24 Coal Stoker/SlopedGrate/Other Sample #3 2/22/2006 60 1.00

WIWausau # 5 Power Boiler (B24) Coal Stoker/SlopedGrate/Other Sample #1 7/24/2007 60 1.00

WIWausau # 5 Power Boiler (B24) Coal Stoker/SlopedGrate/Other Sample #2 7/24/2007 60 1.00

WIWausau # 5 Power Boiler (B24) Coal Stoker/SlopedGrate/Other Sample #3 7/24/2007 60 1.00

MNGPDuluth EU33 Boiler #3 Heavy Liquid N/A 1 9/10/2009

Page 8 of 12
Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date

Sample 

Time 

(min)

Sample 

Time (hrs)

Stack Oxygen 

Concentration 

(%)

Use in 

New 

Source 3x 

RDL?

MNGPDuluth EU33 Boiler #3 Heavy Liquid N/A 2 9/10/2009

MNGPDuluth EU33 Boiler #3 Heavy Liquid N/A 3 9/10/2009

NYConEd59thStStationNewYork Boiler 118 Heavy Liquid N/A M5-1 8/19/2009

NYConEd59thStStationNewYork Boiler 118 Heavy Liquid N/A M5-2 8/19/2009

NYConEd59thStStationNewYork Boiler 118 Heavy Liquid N/A M5-3 8/19/2009

PABoeingRidleyPark 033 Heavy Liquid N/A M29-1 9/22/2009

PABoeingRidleyPark 033 Heavy Liquid N/A M29-2 9/23/2009

PABoeingRidleyPark 033 Heavy Liquid N/A M29-3 9/24/2009

SCMilliken-Dewey D30 Heavy Liquid N/A Sample #1 8/12/2009 180 3.00 3.83

SCMilliken-Dewey D30 Heavy Liquid N/A Sample #2 8/12/2009 180 3.00 4.02

SCMilliken-Dewey D30 Heavy Liquid N/A Sample #3 8/12/2009 180 3.00 3.96

ALBP-Decatur24 AB-8301 Light Liquid N/A Sample #1 1/24/2001

ALBP-Decatur24 AB-8301 Light Liquid N/A Sample #2 1/24/2001

ALBP-Decatur24 AB-8301 Light Liquid N/A Sample #3 1/24/2001

SCGPChemRussellville FO Boiler Light Liquid N/A Sample #1 8/26/2009 120 2.00 8.06

SCGPChemRussellville FO Boiler Light Liquid N/A Sample #2 8/26/2009 120 2.00 7.26

SCGPChemRussellville FO Boiler Light Liquid N/A Sample #3 8/26/2009 120 2.00 7.31

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Light Liquid N/A 1 11/17/2009 216 3.60 YES

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Light Liquid N/A 2 11/17/2009 216 3.60 YES

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 Light Liquid N/A 3 11/18/2009 216 3.60 YES

HITesoro SG1102 Non-Continental Liquid N/A Sample #1 10/9/2010 60 1.00 4.89 YES

HITesoro SG1102 Non-Continental Liquid N/A Sample #2 10/9/2010 60 1.00 5.19 YES

HITesoro SG1102 Non-Continental Liquid N/A Sample #3 10/9/2010 60 1.00 5.29 YES

HITesoro SG1102 Non-Continental Liquid N/A Sample #1 12/13/2010 192 3.20 6.3 YES

HITesoro SG1102 Non-Continental Liquid N/A Sample #2 12/13/2010 192 3.20 6.42 YES

HITesoro SG1102 Non-Continental Liquid N/A Sample #3 12/13/2010 192 3.20 6.77 YES

WVMountainStateCarbonFollansbee S1 Process Gas N/A Sample #1 10/19/2009 240 4.00 4.5 YES

WVMountainStateCarbonFollansbee S1 Process Gas N/A Sample #2 10/19/2009 240 4.00 4.7 YES

WVMountainStateCarbonFollansbee S1 Process Gas N/A Sample #3 10/20/2009 240 4.00 4.8 YES

ALBP-Decatur24 AB-8301 Light Liquid N/A 1 1/24/2001 120 2.00 4

ALBP-Decatur24 AB-8301 Light Liquid N/A 2 1/24/2001 120 4.4

ALBP-Decatur24 AB-8301 Light Liquid N/A 3 1/24/2001 120 4.2

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 1 12/12/2007 60 10.7

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 12/12/2007 60 9.9

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 12/12/2007 60 10

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 1 12/12/2007 60 9.8

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 12/12/2007 60 9.6

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 12/12/2007 60 9.8

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 1 6/14/2011 60 7.31

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 6/14/2011 60 8.02

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 6/14/2011 60 6.78

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 1 6/14/2011 60 7.44

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 6/14/2011 60 7.77

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 6/14/2011 60 7.67

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 1 6/24/2009 60 5.9

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 6/24/2009 60 7.1

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 6/24/2009 60 9.2

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 1 6/24/2009 60 6.1

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 6/24/2009 60 7.5

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 6/24/2009 60 9

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 1 7/11/2008 60 6.9

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 7/11/2008 60 6.3

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 7/11/2008 60 5.8

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 1 7/11/2008 60 6.4

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 7/11/2008 60 5.9

ALGPBrewtonMill BR-PSG0-S026 No. 3 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 7/11/2008 60 6.1

ALIPCourtland No. 3 Combination Boier / 11Cu301 Biomass FB 1 7/7/2009 240 11.3

ALIPCourtland No. 3 Combination Boier / 11Cu301 Biomass FB 2 7/7/2009 240 11.4

ALIPCourtland No. 3 Combination Boier / 11Cu301 Biomass FB 3 7/7/2009 240 11.5

ARLeolaLumberMill SN-01A Wet Biomass Stoker/SlopedGrate/Other 1 6/14/2006 120 9.8

ARLeolaLumberMill SN-01A Wet Biomass Stoker/SlopedGrate/Other 2 6/14/2006 120 10.2

ARLeolaLumberMill SN-01A Wet Biomass Stoker/SlopedGrate/Other 3 6/14/2006 120 10

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 1 12/4/2002 60 11.51

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 2 12/4/2002 60 11.68

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 3 12/4/2002 60 11.56

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 1 12/4/2003 60 10.74

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 2 12/4/2003 60 10.65

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 3 12/4/2003 60 10.35

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 1 8/11/1997 60 9

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 2 8/11/1997 60 9

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 3 8/11/1997 60 9

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 1 9/29/2004 60 9.6

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 2 9/29/2004 60 10.17

ARWeyerhaeuserDierksMill SN-32 Wet Biomass Stoker/SlopedGrate/Other 3 9/29/2004 60 9.94

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner 1 8/7/1997 120 6.7 YES

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner 2 8/7/1997 120 6.4 YES

ARWeyerhaeuserDierksMill SN-45 Biomass Dutch Oven/Pile Burner 3 8/7/1997 120 6.4 YES

CASierraPacificLincoln McBurney Boiler Wet Biomass Stoker/SlopedGrate/Other 1 3/11/2008 ? 3.277

CASierraPacificLincoln McBurney Boiler Wet Biomass Stoker/SlopedGrate/Other 2 3/11/2008 ? 3.71

CASierraPacificLincoln McBurney Boiler Wet Biomass Stoker/SlopedGrate/Other 3 3/11/2008 ? 2.42

CASierraPacificLincoln McBurney Boiler Wet Biomass Stoker/SlopedGrate/Other 1 3/5/2008 ? 2.208

CASierraPacificLincoln McBurney Boiler Wet Biomass Stoker/SlopedGrate/Other 2 3/5/2008 ? 3.085

CASierraPacificLincoln McBurney Boiler Wet Biomass Stoker/SlopedGrate/Other 3 3/5/2008 ? 2.565

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate 1 1/18/2001 60 10.74

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate 2 1/18/2001 60 11.05

Page 9 of 12
Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date

Sample 

Time 

(min)

Sample 

Time (hrs)

Stack Oxygen 

Concentration 

(%)

Use in 

New 

Source 3x 

RDL?

FLSugarCaneGrowersCoop Boiler No. 3 Biomass Suspension/Grate 3 1/18/2001 60 10.76

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 12/30/2003 60 6.36

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 2 12/30/2003 60 6.99

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 3 12/30/2003 60 6.58

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 1/24/2008 60 7.18

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 2 1/24/2008 60 6.77

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 3 1/24/2008 60 6.84

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 1/25/2007 60 10.56

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 2 1/25/2007 60 9.78

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 3 1/25/2007 60 10.71

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 1/31/2000 60 6.14

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 3 1/31/2000 60 5.98

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 4 1/31/2000 60 5.78

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 1/5/2001 60 9.08

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 2 1/5/2001 60 8.98

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 4 1/5/2001 60 8.98

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 1/5/2006 60 9.78

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 2 1/5/2006 60 8.8

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 3 1/5/2006 60 8.76

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 1/9/2002 60 6.67

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 2 1/9/2002 60 6.43

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 3 1/9/2002 60 6.41

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 11/15/2002 60 6.56

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 2 11/15/2002 60 7.65

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 3 11/15/2002 60 7.96

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 12/17/1999 60 3.6

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 2 12/17/1999 60 4.8

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 3 12/17/1999 60 4.9

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 2/4/2005 60 10.72

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 2 2/4/2005 60 10.8

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 3 2/4/2005 60 11.28

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 1 2/8/1999 60 6.4

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 2 2/8/1999 60 7.5

FLUSSugarCorp Boiler No. 7 Biomass Suspension/Grate 3 2/8/1999 60 7.5

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate 1 1/10/2006 ? ?

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate 2 1/10/2006 ? ?

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate 3 1/10/2006 ? ?

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate 1 11/29/2007 ? ?

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate 2 11/29/2007 ? ?

FLUSSugarCorp Boiler No. 8 Biomass Suspension/Grate 3 11/29/2007 ? ?

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 1 8/27/2009 60 7.01 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 2 8/27/2009 60 7.92 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 3 8/27/2009 60 7.58 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 4 8/27/2009 60 6.93 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 5 8/27/2009 60 6.73 YES

GAGPMadisonPly 800 Wood Waste Boiler Wet Biomass Stoker/SlopedGrate/Other 6 8/27/2009 60 8.24 YES

GATempleInlandRome WF Biomass FB 1 7/27/2009 204 5.1 YES

GATempleInlandRome WF Biomass FB 2 7/27/2009 204 5 YES

GATempleInlandRome WF Biomass FB 3 7/27/2009 204 5.2 YES

HITesoro SG1102 Non-Continental Liquid N/A 1 60 4.89 YES

HITesoro SG1102 Non-Continental Liquid N/A 2 60 5.19 YES

HITesoro SG1102 Non-Continental Liquid N/A 3 60 5.29 YES

HITesoro SG1102 Non-Continental Liquid N/A 1 64 6.9 YES

HITesoro SG1102 Non-Continental Liquid N/A 2 64 7 YES

HITesoro SG1102 Non-Continental Liquid N/A 3 64 6.9 YES

IAUofIowa EP7 Boiler 11 Coal FB 1 2/15/2006 60 4.7

IAUofIowa EP7 Boiler 11 Coal FB 2 2/15/2006 60 4.4

IAUofIowa EP7 Boiler 11 Coal FB 3 2/15/2006 60 4.4

IAUofIowa EP7 Boiler 11 Coal FB 1 2/22/2006 60 7.2

IAUofIowa EP7 Boiler 11 Coal FB 2 2/22/2006 60 7.2

IAUofIowa EP7 Boiler 11 Coal FB 3 2/22/2006 60 7.2

IAUofIowa EP7 Boiler 11 Coal FB 2 8/4/2009 240 5

IAUofIowa EP7 Boiler 11 Coal FB 3 8/4/2009 240 4.7

IAUofIowa EP7 Boiler 11 Coal FB 4 8/4/2009 240 4.8

IDPotlatch PB-1 CE Biomass Fuel Cell 1 4/30/2008 60 11.79

IDPotlatch PB-1 CE Biomass Fuel Cell 2 4/30/2008 60 11.65

IDPotlatch PB-1 CE Biomass Fuel Cell 3 4/30/2008 60 11.53

IDPotlatch PB-2 Riley Wet Biomass Stoker/SlopedGrate/Other 1 5/1/2008 60 8.78

IDPotlatch PB-2 Riley Wet Biomass Stoker/SlopedGrate/Other 2 5/1/2008 60 9.08

IDPotlatch PB-2 Riley Wet Biomass Stoker/SlopedGrate/Other 3 5/1/2008 60 7.82

ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other 1 8/4/2009 240 9.985

ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other 2 8/4/2009 240 10.16

ILAbbottAbbottPark Unit 5AP Coal Stoker/SlopedGrate/Other 3 8/4/2009 240 10.179

ILPolyOne B1 Coal Stoker/SlopedGrate/Other 1 11/14/2006 120 7.3

ILPolyOne B1 Coal Stoker/SlopedGrate/Other 2 11/14/2006 120 7.6

ILPolyOne B1 Coal Stoker/SlopedGrate/Other 3 11/14/2006 120 7.7

ILRockIslandArsenal NBN 12602 (Boiler #1) Coal Stoker/SlopedGrate/Other 1 3/13/2007 60 9.7

ILRockIslandArsenal NBN 12602 (Boiler #1) Coal Stoker/SlopedGrate/Other 2 3/13/2007 60 8.3

ILRockIslandArsenal NBN 12602 (Boiler #1) Coal Stoker/SlopedGrate/Other 3 3/13/2007 60 8

INNotreDame B-4 Coal Stoker/SlopedGrate/Other 1 240 5.7

INNotreDame B-4 Coal Stoker/SlopedGrate/Other 2 240 5.6

INNotreDame B-4 Coal Stoker/SlopedGrate/Other 3 240 5.6

MENewPage-Rumford Cogen#6 Wet Biomass Stoker/SlopedGrate/Other 1 9/6/2007 60 10

MENewPage-Rumford Cogen#6 Wet Biomass Stoker/SlopedGrate/Other 2 9/6/2007 60 10

MENewPage-Rumford Cogen#6 Wet Biomass Stoker/SlopedGrate/Other 3 9/6/2007 60 10

Page 10 of 12
Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date

Sample 

Time 

(min)

Sample 

Time (hrs)

Stack Oxygen 

Concentration 

(%)

Use in 

New 

Source 3x 

RDL?

MENewPage-Rumford Cogen#7 Wet Biomass Stoker/SlopedGrate/Other 1 9/6/2007 60 10

MENewPage-Rumford Cogen#7 Wet Biomass Stoker/SlopedGrate/Other 2 9/6/2007 60 10

MENewPage-Rumford Cogen#7 Wet Biomass Stoker/SlopedGrate/Other 3 9/6/2007 60 10

MESDWarren #21 Boiler Wet Biomass Stoker/SlopedGrate/Other 1 11/10/2006 60 5.4

MESDWarren #21 Boiler Wet Biomass Stoker/SlopedGrate/Other 2 11/10/2006 60 5.2

MESDWarren #21 Boiler Wet Biomass Stoker/SlopedGrate/Other 3 11/10/2006 60 5.6

MNGPDuluth EU33 Boiler #3 Heavy Liquid N/A 1 9/10/2009 180 16.6 YES

MNGPDuluth EU33 Boiler #3 Heavy Liquid N/A 2 9/10/2009 180 16.3 YES

MNGPDuluth EU33 Boiler #3 Heavy Liquid N/A 3 9/10/2009 180 16 YES

MNWeyerhaeuserIronton EU 001 - 4 Cell Furnace Biomass Fuel Cell 1 12/20/2006 60 12.6

MNWeyerhaeuserIronton EU 001 - 4 Cell Furnace Biomass Fuel Cell 2 12/20/2006 60 12.5

MNWeyerhaeuserIronton EU 001 - 4 Cell Furnace Biomass Fuel Cell 3 12/20/2006 60 12.4

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 1 7/12/2006 90 10.2

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 7/12/2006 90 11.2

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 7/12/2006 90 12

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 9/22/2010 240 8.8

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 9/22/2010 240 8.3

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 4 9/22/2010 240 7.8

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 1 9/28/2010 240 12.4

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 2 9/28/2010 240 12.3

MSGPNewAugusta AA-015 Power Boiler Wet Biomass Stoker/SlopedGrate/Other 3 9/28/2010 240 10.7

MSNorbordMS Wellons No. 1 Biomass Fuel Cell 1 8/1/2007 60 14.21

MSNorbordMS Wellons No. 1 Biomass Fuel Cell 2 8/1/2007 60 14.56

MSNorbordMS Wellons No. 1 Biomass Fuel Cell 3 8/1/2007 60 14.12

MSNorbordMS Wellons No. 2 Biomass Fuel Cell 1 8/1/2007 60 14.21

MSNorbordMS Wellons No. 2 Biomass Fuel Cell 2 8/1/2007 60 14.56

MSNorbordMS Wellons No. 2 Biomass Fuel Cell 3 8/1/2007 60 14.12

MSNorbordMS Wellons No. 3 Biomass Fuel Cell 1 8/1/2007 60 14.21

MSNorbordMS Wellons No. 3 Biomass Fuel Cell 2 8/1/2007 60 14.56

MSNorbordMS Wellons No. 3 Biomass Fuel Cell 3 8/1/2007 60 14.12

NYConEd59thStStationNewYork Boiler 118 Heavy Liquid N/A 1 250 7.6

NYConEd59thStStationNewYork Boiler 118 Heavy Liquid N/A 2 250 7.4

NYConEd59thStStationNewYork Boiler 118 Heavy Liquid N/A 3 250 7.4

OHSauderWoodArchbold B009 Biomass Suspension Burner 1 60 9.45

OHSauderWoodArchbold B009 Biomass Suspension Burner 2 60 9.45

OHSauderWoodArchbold B009 Biomass Suspension Burner 3 60 9.79

OHSmartPapersHoldingsLLC B020 Coal Stoker/SlopedGrate/Other 1 9/22/2005 120 9.1

OHSmartPapersHoldingsLLC B020 Coal Stoker/SlopedGrate/Other 2 9/22/2005 120 9.4

OHSmartPapersHoldingsLLC B020 Coal Stoker/SlopedGrate/Other 3 9/22/2005 120 8.9

ORGeorgiaPacificWaunaMill EU35 - Fluidized Bed Boiler Biomass FB 1 3/22/2006 120 8.24

ORGeorgiaPacificWaunaMill EU35 - Fluidized Bed Boiler Biomass FB 2 3/22/2006 120 8.22

ORGeorgiaPacificWaunaMill EU35 - Fluidized Bed Boiler Biomass FB 3 3/22/2006 120 8.22

PABoeingRidleyPark 033 Heavy Liquid N/A 1 9/22/2009 240 5.4

PABoeingRidleyPark 033 Heavy Liquid N/A 2 9/22/2009 240 5.5

PABoeingRidleyPark 033 Heavy Liquid N/A 3 9/22/2009 240 6.8

SCCogenSouth B002 - Auxiliary Boiler #1 Heavy Liquid N/A 1 11/14/2006 120 4

SCCogenSouth B002 - Auxiliary Boiler #1 Heavy Liquid N/A 2 11/14/2006 120 1.5

SCCogenSouth B002 - Auxiliary Boiler #1 Heavy Liquid N/A 3 11/14/2006 120 4.5

SCCogenSouth B002 - Auxiliary Boiler #1 Heavy Liquid N/A 1 11/30/2004 60 5.4

SCCogenSouth B002 - Auxiliary Boiler #1 Heavy Liquid N/A 2 11/30/2004 60 5.4

SCCogenSouth B002 - Auxiliary Boiler #1 Heavy Liquid N/A 3 11/30/2004 60 5.4

SCCogenSouth B003 - Auxiliary Boiler #2 Heavy Liquid N/A 1 11/14/2006 120 4

SCCogenSouth B003 - Auxiliary Boiler #2 Heavy Liquid N/A 2 11/14/2006 120 1.5

SCCogenSouth B003 - Auxiliary Boiler #2 Heavy Liquid N/A 3 11/14/2006 120 4.5

SCCogenSouth B003 - Auxiliary Boiler #2 Heavy Liquid N/A 1 11/30/2004 60 5.4

SCCogenSouth B003 - Auxiliary Boiler #2 Heavy Liquid N/A 2 11/30/2004 60 5.4

SCCogenSouth B003 - Auxiliary Boiler #2 Heavy Liquid N/A 3 11/30/2004 60 5.4

SCCogenSouth B004 - Auxiliary Boiler #3 Heavy Liquid N/A 1 11/14/2006 120 4

SCCogenSouth B004 - Auxiliary Boiler #3 Heavy Liquid N/A 2 11/14/2006 120 1.5

SCCogenSouth B004 - Auxiliary Boiler #3 Heavy Liquid N/A 3 11/14/2006 120 4.5

SCCogenSouth B004 - Auxiliary Boiler #3 Heavy Liquid N/A 1 11/30/2004 60 5.4

SCCogenSouth B004 - Auxiliary Boiler #3 Heavy Liquid N/A 2 11/30/2004 60 5.4

SCCogenSouth B004 - Auxiliary Boiler #3 Heavy Liquid N/A 3 11/30/2004 60 5.4

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other 1 1/26/2005 120 5.37

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other 2 1/26/2005 120 6.56

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other 3 1/26/2005 120 6.89

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other 1 1/4/2007 120 8.5

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other 2 1/4/2007 120 8.45

SCMarlboroPaper Hogged Fuel Boiler Wet Biomass Stoker/SlopedGrate/Other 3 1/4/2007 120 7.8

SCMitsubishiPolyesterFilm Dowtherm Heater 4 (4FPDDOWHSA) Heavy Liquid N/A 1 7/23/2009 125 8

SCMitsubishiPolyesterFilm Dowtherm Heater 4 (4FPDDOWHSA) Heavy Liquid N/A 2 7/23/2009 125 8

SCMitsubishiPolyesterFilm Dowtherm Heater 4 (4FPDDOWHSA) Heavy Liquid N/A 3 7/23/2009 125 8

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 1 10/6/2005 120 5.6

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 2 10/6/2005 120 5.5

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 3 10/6/2005 120 5.7

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 1 120 4.75

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 2 120 5.1

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 3 120 5.2

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 1 8/4/2009 208 6.6

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 2 8/4/2009 208 7

TNBowaterNewsprint Bubbling Fluidized Bed Boiler Biomass FB 3 8/4/2009 208 6.8

TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other 1 11/6/2009 ? ?

TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other 2 11/6/2009 ? ?

TNCargillMemphis Stoker Boiler 8001 Coal Stoker/SlopedGrate/Other 3 11/6/2009 ? ?

TXRGVSG Boiler No. 6 Biomass Suspension/Grate 2 1/13/2009 120 6.6 YES

Page 11 of 12
Appendix C-1: Sample Times and Oxygen Percentages Used to Estimate PM 3x RDL

Facility ID Combusor ID Fuel Category Combustor Design Test ID Test Date

Sample 

Time 

(min)

Sample 

Time (hrs)

Stack Oxygen 

Concentration 

(%)

Use in 

New 

Source 3x 

RDL?

TXRGVSG Boiler No. 6 Biomass Suspension/Grate 3 1/13/2009 120 7 YES

TXRGVSG Boiler No. 6 Biomass Suspension/Grate 4 1/13/2009 120 6.8 YES

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB 1 9/21/2007 60 9.4

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB 2 9/21/2007 60 9.4

WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Coal FB 3 9/21/2007 60 9.8

WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other 1 3/24/2005 120 7.8

WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other 2 3/24/2005 120 8.1

WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other 3 3/24/2005 120 8.4

WVAmericanWoodmark B2 Dry Biomass Stoker/SlopedGrate/Other 4 3/24/2005 120 7.3

WVGPMtHopeOSB 5600 - Wellons Energy System Biomass Dutch Oven/Pile Burner 1 7/11/2006 120 16.26

WVGPMtHopeOSB 5600 - Wellons Energy System Biomass Dutch Oven/Pile Burner 2 7/11/2006 120 17.1

WVGPMtHopeOSB 5600 - Wellons Energy System Biomass Dutch Oven/Pile Burner 3 7/11/2006 120 17.26

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other 1 7/13/2010 60 10.01

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other 2 7/13/2010 60 9.74

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other 4 7/13/2010 60 10.2

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other 1 5/5/2010 50 8.8

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other 2 5/5/2010 50 9.05

LAWeyerhaeuserDodson ES-017 WFB Wet Biomass Stoker/SlopedGrate/Other 3 5/5/2010 50 9.25

OKGPMuskogeeMill B-2 Coal PC 1 9/27/2010 240 8.1

OKGPMuskogeeMill B-2 Coal PC 2 9/28/2010 240 9.8

OKGPMuskogeeMill B-2 Coal PC 3 9/28/2010 240 9.4

OKGPMuskogeeMill B-2 Coal PC 1 10/1/2010 240 8.1

OKGPMuskogeeMill B-2 Coal PC 2 10/1/2010 240 8.1

OKGPMuskogeeMill B-2 Coal PC 3 10/2/2010 240 7.8

OKGPMuskogeeMill B-3 Coal PC 1 9/29/2010 240 7.2

OKGPMuskogeeMill B-3 Coal PC 2 9/29/2010 240 7

OKGPMuskogeeMill B-3 Coal PC 3 9/30/2010 240 7.2

OKGPMuskogeeMill B-4 Coal PC 1 10/5/2010 240 6.5

OKGPMuskogeeMill B-4 Coal PC 2 10/5/2010 240 6.3

OKGPMuskogeeMill B-4 Coal PC 3 10/6/2010 240 6.5

HITesoro SG1102 Non-Continental Liquid N/A 1 1/26/2012 60 4.21 YES

HITesoro SG1102 Non-Continental Liquid N/A 2 1/26/2012 60 4.24 YES

HITesoro SG1102 Non-Continental Liquid N/A 3 1/26/2012 60 4.27 YES

HITesoro H101B Non-Continental Liquid N/A 1 1/25/2012 60 6.53

HITesoro H101B Non-Continental Liquid N/A 2 1/25/2012 60 6.62

HITesoro H101B Non-Continental Liquid N/A 3 1/25/2012 60 6.75

Page 12 of 12
Table C-2a: Summary of PM 3x RDL for Existing Sources

Fuel Category Combustor Design Average Sample Time (hrs)

3x RDL

(μg/dscm)

Fd Factor for 

Subcategory

(dscf/MMBtu)

Average Stack 

Concentratio

Coal N/A 2 3.00E+03 9,780 7.11 

Dutch Oven/Pile Burner 2 3.00E+03 9,420 9.22 

FB 3 2.00E+03 9,420 7.02 

Fuel Cell 2 3.00E+03 9,420 13.40 

Suspension Burner 1 6.00E+03 9,240 9.55 

Suspension/Grate 1 6.00E+03 9,420 7.90 

Wet Biomass Stoker/Other 1 6.00E+03 9,420 8.05 

Dry Biomass Stoker/Other 2 3.00E+03 9,240 7.90 

Heavy Liquid N/A 2 3.00E+03 9,190 6.16 

Light Liquid N/A 3 2.00E+03 9,190 5.87 

Non-Continental Liquid N/A 1 6.00E+03 9,190 5.76 

Process Gas N/A 4 1.50E+03 8,710 4.67 

Table C-2b: Summary of PM 3x RDL for New Sources

Fuel Category Combustor Design Average Sample Time (hrs)

3x RDL

(μg/dscm)

Fd Factor for 

Subcategory

(dscf/MMBtu)

Average Stack 

Concentratio

Coal N/A 4 1.50E+03 9,780 7.11 

Dutch Oven/Pile Burner 2 3.00E+03 9,420 8.80 

FB 3 2.00E+03 9,420 5.10 

Fuel Cell 2 3.00E+03 9,420 7.89 

Suspension Burner 1 6.00E+03 9,240 9.54 

Suspension/Grate 2 3.00E+03 9,420 6.80 

Wet Biomass Stoker/Other 2 3.00E+03 9,420 8.27 

Dry Biomass Stoker/Other 2 3.00E+03 9,240 7.90 

Heavy Liquid N/A 3 2.00E+03 9,190 16.30 

Light Liquid N/A 4 1.50E+03 9,190 4.63 

Non-Continental Liquid N/A 2 3.00E+03 9,190 5.29 

Process Gas N/A 4 1.50E+03 8,710 4.67 

BiomassBiomass

Page 1 of 1
Appendix D

Calculation of 3x RDL for Metallic HAP
Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL

Fuel 

Category

Combustor 

Design

Basis of New 

Source Floor? FacilityID UnitID Run Number Test Date S

Coal N/A No AKDoyonUtilities_AK 4 Sample #1 8/17/2005 Coal N/A No AKDoyonUtilities_AK 4 Sample #2 8/17/2005 Coal N/A No AKDoyonUtilities_AK 4 Sample #3 8/17/2005 Coal N/A No AKDoyonUtilities_AK 7 Sample #1 8/16/2005 Coal N/A No AKDoyonUtilities_AK 7 Sample #2 8/16/2005 Coal N/A No AKDoyonUtilities_AK 7 Sample #3 8/16/2005 

Biomass FB No ALIPCourtland No. 3 Combination Boier / 11Cu301 Sample #1 7/7/2009 

Biomass FB No ALIPCourtland No. 3 Combination Boier / 11Cu301 Sample #2 7/7/2009 Biomass FB No ALIPCourtland No. 3 Combination Boier / 11Cu301 Sample #3 7/8/2009 Biomass Fuel Cell No ARAnthonyForestProducts SN-12 1 9/1/2009 Biomass Fuel Cell No ARAnthonyForestProducts SN-12 2 9/1/2009 Biomass Fuel Cell No ARAnthonyForestProducts SN-12 3 9/2/2009 

Wet Biomass Stoker/SlopedGrate/OtherNo ARLeolaLumberMill SN-01A Sample #1 6/14/2006 

Wet Biomass Stoker/SlopedGrate/OtherNo ARLeolaLumberMill SN-01A Sample #2 6/14/2006 Wet Biomass Stoker/SlopedGrate/OtherNo ARLeolaLumberMill SN-01A Sample #3 6/14/2006 Wet Biomass Stoker/SlopedGrate/OtherNo ARLeolaLumberMill SN-01B Sample #1 6/14/2006 Wet Biomass Stoker/SlopedGrate/OtherNo ARLeolaLumberMill SN-01B Sample #2 6/14/2006 Wet Biomass Stoker/SlopedGrate/OtherNo ARLeolaLumberMill SN-01B Sample #3 6/14/2006 

BiomassDutch Oven/Pile Burner No ARPotlatchForestWarren Wellons Boiler 1 9/9/2009 BiomassDutch Oven/Pile Burner No ARPotlatchForestWarren Wellons Boiler 2 9/9/2009 BiomassDutch Oven/Pile Burner No ARPotlatchForestWarren Wellons Boiler 3 9/9/2009 Biomass Suspension/Grate No FLSugarCaneGrowersCoop Boiler No. 8 Sample #1 1/19/2005 Biomass Suspension/Grate No FLSugarCaneGrowersCoop Boiler No. 8 Sample #2 1/19/2005 Biomass Suspension/Grate No FLSugarCaneGrowersCoop Boiler No. 8 Sample #3 1/19/2005 

Wet Biomass Stoker/SlopedGrate/OtherNo GAGPMadisonPly 800 Wood Waste Boiler 1 8/11/2009 

Wet Biomass Stoker/SlopedGrate/OtherNo GAGPMadisonPly 800 Wood Waste Boiler 2 8/12/2009 
Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL

Fuel 

Category

Combustor 

Design

Basis of New 

Source Floor? FacilityID UnitID Run Number Test Date S

Wet Biomass Stoker/SlopedGrate/OtherNo GAGPMadisonPly 800 Wood Waste Boiler 3 8/12/2009 

Biomass FB No GATempleInlandRome WF 1 7/27/2009 Biomass FB No GATempleInlandRome WF 2 7/28/2009 Biomass FB No GATempleInlandRome WF 3 7/28/2009 Biomass Suspension/Grate Yes HIPuuneneSugarMill Boiler 1 Sample #1 5/28/2006 

Biomass Suspension/Grate Yes HIPuuneneSugarMill Boiler 1 Sample #2 5/29/2006 Biomass Suspension/Grate Yes HIPuuneneSugarMill Boiler 1 Sample #3 5/30/2006 Biomass Suspension/Grate Yes HIPuuneneSugarMill Boiler 1 Sample #1 7/25/2007Biomass Suspension/Grate Yes HIPuuneneSugarMill Boiler 1 Sample #2 7/25/2007Biomass Suspension/Grate Yes HIPuuneneSugarMill Boiler 1 Sample #3 7/25/2007Biomass Suspension/Grate Yes HIPuuneneSugarMill Boiler 2 Sample #1 5/28/2006 Biomass Suspension/Grate Yes HIPuuneneSugarMill Boiler 2 Sample #2 5/29/2006 Biomass Suspension/Grate Yes HIPuuneneSugarMill Boiler 2 Sample #3 5/30/2006 Biomass Suspension/Grate Yes HIPuuneneSugarMill Boiler 2 Sample #1 7/25/2007Biomass Suspension/Grate Yes HIPuuneneSugarMill Boiler 2 Sample #2 7/25/2007Biomass Suspension/Grate Yes HIPuuneneSugarMill Boiler 2 Sample #3 7/25/2007Biomass Suspension/Grate No HIPuuneneSugarMill Boiler 3 Sample #1 5/23/2006Biomass Suspension/Grate No HIPuuneneSugarMill Boiler 3 Sample #2 5/24/2006Biomass Suspension/Grate No HIPuuneneSugarMill Boiler 3 Sample #3 5/25/2006Biomass Suspension/Grate No HIPuuneneSugarMill Boiler 3 Sample #1 7/16/2007Biomass Suspension/Grate No HIPuuneneSugarMill Boiler 3 Sample #2 7/17/2007Biomass Suspension/Grate No HIPuuneneSugarMill Boiler 3 Sample #3 7/17/2007

Coal N/A No IARoquetteAmericaCirculating Fluidized Bed Boiler (121)1 6/3/2009 

Coal N/A No IARoquetteAmericaCirculating Fluidized Bed Boiler (121)2 6/3/2009 Coal N/A No IARoquetteAmericaCirculating Fluidized Bed Boiler (121)3 6/4/2009 Coal N/A No IAUofNorthernIowa Boiler #3 4 10/6/2009 
Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL

Fuel 

Category

Combustor 

Design

Basis of New 

Source Floor? FacilityID UnitID Run Number Test Date S

Coal N/A No IAUofNorthernIowa Boiler #3 5 10/6/2009 Coal N/A No IAUofNorthernIowa Boiler #3 6 10/7/2009 Coal N/A No IDAmalgamatedSugarCoTwinFalls S-B1 Sample #1 9/26/2006 

Coal N/A No IDAmalgamatedSugarCoTwinFalls S-B1 Sample #2 9/26/2006 Coal N/A No IDAmalgamatedSugarCoTwinFalls S-B1 Sample #3 9/26/2006 

Biomass Fuel Cell Yes IDPotlatch PB-1 CE Sample #1 7/20/2006Biomass Fuel Cell Yes IDPotlatch PB-1 CE Sample #2 7/20/2006Biomass Fuel Cell Yes IDPotlatch PB-1 CE Sample #3 7/20/2006Biomass Fuel Cell Yes IDPotlatch PB-1 CE M29-R1 7/28/2009 Biomass Fuel Cell Yes IDPotlatch PB-1 CE M29-R2 7/28/2009 Biomass Fuel Cell Yes IDPotlatch PB-1 CE M29-R3 7/29/2009 

Wet Biomass Stoker/SlopedGrate/OtherYes IDPotlatch PB-2 Riley Sample #1 7/27/2006

Wet Biomass Stoker/SlopedGrate/OtherYes IDPotlatch PB-2 Riley Sample #2 7/27/2006Wet Biomass Stoker/SlopedGrate/OtherYes IDPotlatch PB-2 Riley Sample #3 7/27/2006

Coal N/A No IDTASCONampa Babcock and Wilcox (B&W) #1Sample #1 12/4/2006 

Coal N/A No IDTASCONampa Babcock and Wilcox (B&W) #1Sample #2 12/4/2006 Coal N/A No IDTASCONampa Babcock and Wilcox (B&W) #1Sample #3 12/4/2006 Coal N/A No IDTASCONampa Babcock and Wilcox (B&W) #2Sample #1 12/4/2006 Coal N/A No IDTASCONampa Babcock and Wilcox (B&W) #2Sample #2 12/4/2006 Coal N/A No IDTASCONampa Babcock and Wilcox (B&W) #2Sample #3 12/4/2006 Coal N/A Yes ILPolyOne B1 Sample #1 11/14/2006 Coal N/A Yes ILPolyOne B1 Sample #2 11/14/2006Coal N/A Yes ILPolyOne B1 Sample #3 11/14/2006Coal N/A Yes ILPolyOne B1 1 9/9/2009 Coal N/A Yes ILPolyOne B1 2 9/9/2009 Coal N/A Yes ILPolyOne B1 3 9/10/2009 
Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL

Fuel 

Category

Combustor 

Design

Basis of New 

Source Floor? FacilityID UnitID Run Number Test Date S

Coal N/A No INSABICInnovativePlastics 01-001 BW1 Boiler Sample #1 6/28/2006 Coal N/A No INSABICInnovativePlastics 01-001 BW1 Boiler Sample #2 6/28/2006 Coal N/A No INSABICInnovativePlastics 01-001 BW1 Boiler Sample #3 6/28/2006 Coal N/A No INSABICInnovativePlastics 01-001 BW2 Boiler Sample #1 6/28/2006 Coal N/A No INSABICInnovativePlastics 01-001 BW2 Boiler Sample #2 6/28/2006 Coal N/A No INSABICInnovativePlastics 01-001 BW2 Boiler Sample #3 6/28/2006 Coal N/A No INTateLyleSagamore 31B1 M29-1 9/1/2009 Coal N/A No INTateLyleSagamore 31B1 M29-2 9/2/2009 Coal N/A No INTateLyleSagamore 31B1 M29-3 9/3/2009 Coal N/A No MNHibbing Unit 1A Sample #1 9/21/2004 Coal N/A No MNHibbing Unit 1A Sample #2 9/21/2004 Coal N/A No MNHibbing Unit 1A Sample #3 9/21/2004 Coal N/A No MNHibbing Unit 2A Sample #1 9/22/2004 Coal N/A No MNHibbing Unit 2A Sample #2 9/22/2004 Coal N/A No MNHibbing Unit 2A Sample #3 9/22/2004 

Wet Biomass Stoker/SlopedGrate/OtherNo MSGPNewAugusta AA-015 Power Boiler Sample #1 7/12/2006 

Wet Biomass Stoker/SlopedGrate/OtherNo MSGPNewAugusta AA-015 Power Boiler Sample #2 7/12/2006 Wet Biomass Stoker/SlopedGrate/OtherNo MSGPNewAugusta AA-015 Power Boiler Sample #3 7/12/2006 

BiomassDutch Oven/Pile Burner No MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #1 8/5/2009 BiomassDutch Oven/Pile Burner No MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #2 8/5/2009 BiomassDutch Oven/Pile Burner No MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #3 8/5/2009 Biomass FB Yes NDCargillWestFargo Foster Wheeler Boiler (EU43) 1 8/26/2009 

Biomass FB Yes NDCargillWestFargo Foster Wheeler Boiler (EU43) 2 8/26/2009 Biomass FB Yes NDCargillWestFargo Foster Wheeler Boiler (EU43) 3 8/27/2009 

Coal N/A No OKGPMuskogeeMill B-4 Sample #1 4/16/2003 Coal N/A No OKGPMuskogeeMill B-4 Sample #2 4/16/2003 
Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL

Fuel 

Category

Combustor 

Design

Basis of New 

Source Floor? FacilityID UnitID Run Number Test Date S

Coal N/A No OKGPMuskogeeMill B-4 Sample #3 4/16/2003 

Wet Biomass Stoker/SlopedGrate/OtherNo SCMarlboroPaper Hogged Fuel Boiler Sample #1 7/14/2009 

Wet Biomass Stoker/SlopedGrate/OtherNo SCMarlboroPaper Hogged Fuel Boiler Sample #2 7/14/2009 Wet Biomass Stoker/SlopedGrate/OtherNo SCMarlboroPaper Hogged Fuel Boiler Sample #3 7/14/2009 

Biomass FB No TNBowaterNewsprint Bubbling Fluidized Bed BoilerSample #1 10/6/2005 

Biomass FB No TNBowaterNewsprint Bubbling Fluidized Bed BoilerSample #2 10/6/2005 Biomass FB No TNBowaterNewsprint Bubbling Fluidized Bed BoilerSample #3 10/6/2005 Biomass FB No TNBowaterNewsprint Bubbling Fluidized Bed Boiler 1 8/4/2009 Biomass FB No TNBowaterNewsprint Bubbling Fluidized Bed Boiler 2 8/4/2009 Biomass FB No TNBowaterNewsprint Bubbling Fluidized Bed Boiler 3 8/5/2009 

Coal N/A No TNEastman_NO_CBIDATA Boiler 30 1 8/26/2009 Coal N/A No TNEastman_NO_CBIDATA Boiler 30 2 8/27/2009 Coal N/A No TNEastman_NO_CBIDATA Boiler 30 3 8/27/2009 

Biomass Suspension Burner No TXDibollTemple-Inland PB-44 Sample #1 6/29/2007 

Biomass Suspension Burner No TXDibollTemple-Inland PB-44 Sample #2 6/29/2007 BiomassDutch Oven/Pile Burner No VAGeorgiaPacificBrooknealGladys 5600 Sample #1 7/6/2006 

BiomassDutch Oven/Pile Burner No VAGeorgiaPacificBrooknealGladys 5600 Sample #2 7/6/2006 BiomassDutch Oven/Pile Burner No VAGeorgiaPacificBrooknealGladys 5600 Sample #3 7/6/2006 

Coal N/A No VAUniversityofVirginia 7103-1-01R M29-1 9/17/2009 Coal N/A No VAUniversityofVirginia 7103-1-01R M29-2 9/17/2009 Coal N/A No VAUniversityofVirginia 7103-1-01R M29-3 9/18/2009 Coal N/A No VAVirginiaPolytechnic Boiler 11 Sample #1 2/27/2007 Coal N/A No VAVirginiaPolytechnic Boiler 11 Sample #1Coal N/A No VAVirginiaPolytechnic Boiler 11 Sample #2Coal N/A No VAVirginiaPolytechnic Boiler 7 Sample #3 2/28/2007 Coal N/A No VAVirginiaPolytechnic Boiler 7 Sample #1
Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL

Fuel 

Category

Combustor 

Design

Basis of New 

Source Floor? FacilityID UnitID Run Number Test Date S

Coal N/A No VAVirginiaPolytechnic Boiler 7 Sample #1

BiomassDutch Oven/Pile Burner Yes WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #1 8/11/2009 

BiomassDutch Oven/Pile Burner Yes WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #2 8/11/2009 BiomassDutch Oven/Pile Burner Yes WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #3 8/12/2009 Biomass FB No WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #1 7/21/2005 

Biomass FB No WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #2 7/21/2005 Biomass FB No WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #3 7/22/2005 Biomass FB No WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #1 8/20/2009 Biomass FB No WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #2 8/20/2009 Biomass FB No WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #3 8/21/2009 

Coal N/A No WINewPageBiron B24 Sample #1 9/12/2007 Coal N/A No WINewPageBiron B24 Sample #2 9/12/2007 Coal N/A No WINewPageBiron B24 Sample #3 9/12/2007 Coal N/A No WINewPageBiron B24 1 9/22/2009 Coal N/A No WINewPageBiron B24 2 9/22/2009 Coal N/A No WINewPageBiron B24 3 9/23/2009 Coal N/A No WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #1 9/18/2003 Coal N/A No WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #2 9/18/2003 Coal N/A No WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #3 9/18/2003 

Process Gas N/A Yes WVMountainStateCarbonFollansbee S1 Sample #1 10/19/2009 

Process Gas N/A Yes WVMountainStateCarbonFollansbee S1 Sample #2 10/19/2009 Process Gas N/A Yes WVMountainStateCarbonFollansbee S1 Sample #3 10/20/2009 

Coal N/A No WVPPGMartinsville R011-Boiler 3 1 7/22/2009 Coal N/A No WVPPGMartinsville R011-Boiler 3 2 7/23/2009 Coal N/A No WVPPGMartinsville R011-Boiler 3 3 7/23/2009 

Heavy Liquid N/A SCMilliken-Dewey D30 Sample #1 8/12/2009 
Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate TSM8 3x RDL

Fuel 

Category

Combustor 

Design

Basis of New 

Source Floor? FacilityID UnitID Run Number Test Date S

Heavy Liquid N/A SCMilliken-Dewey D30 Sample #2 8/12/2009 Heavy Liquid N/A SCMilliken-Dewey D30 Sample #3 8/12/2009 Heavy Liquid N/A Yes MNGPDuluth EU33 Boiler #3 1 9/10/2009 Heavy Liquid N/A Yes MNGPDuluth EU33 Boiler #3 2 9/10/2009 Heavy Liquid N/A Yes MNGPDuluth EU33 Boiler #3 3 9/10/2009 

Light Liquid N/A Yes TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 1 11/17/2009 Light Liquid N/A Yes TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 2 11/17/2009 Light Liquid N/A Yes TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 3 11/18/2009 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

AKDoyonUtilities_AK 4 Sample #1 8/17/2005AKDoyonUtilities_AK 4 Sample #2 8/17/2005AKDoyonUtilities_AK 4 Sample #3 8/17/2005AKDoyonUtilities_AK 7 Sample #1 8/16/2005AKDoyonUtilities_AK 7 Sample #2 8/16/2005AKDoyonUtilities_AK 7 Sample #3 8/16/2005

ALIPCourtland No. 3 Combination Boier / 11Cu301 Sample #1 7/7/2009

ALIPCourtland No. 3 Combination Boier / 11Cu301 Sample #2 7/7/2009ALIPCourtland No. 3 Combination Boier / 11Cu301 Sample #3 7/8/2009

ARAnthonyForestProducts SN-12 1 9/1/2009ARAnthonyForestProducts SN-12 2 9/1/2009ARAnthonyForestProducts SN-12 3 9/2/2009

ARLeolaLumberMill SN-01A Sample #1 6/14/2006ARLeolaLumberMill SN-01A Sample #2 6/14/2006ARLeolaLumberMill SN-01A Sample #3 6/14/2006ARLeolaLumberMill SN-01B Sample #1 6/14/2006ARLeolaLumberMill SN-01B Sample #2 6/14/2006ARLeolaLumberMill SN-01B Sample #3 6/14/2006

ARPotlatchForestWarren Wellons Boiler 1 9/9/2009ARPotlatchForestWarren Wellons Boiler 2 9/9/2009ARPotlatchForestWarren Wellons Boiler 3 9/9/2009

FLSugarCaneGrowersCoop Boiler No. 8 Sample #1 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #2 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #3 1/19/2005

GAGPMadisonPly 800 Wood Waste Boiler 1 8/11/2009

GAGPMadisonPly 800 Wood Waste Boiler 2 8/12/2009

Sample 

Volume 

(dscf)

Sample 

Volume 

(dscm)

Sample 

O2 (%)

As Catch 

(μg)

61.671 1.746312 7 1.8 61.448 1.739997 6.7 2.1 59.464 1.683817 6.6 1.9 61.025 1.728019 7.6 1.4 

57.17 1.618859 7.9 1.6 55.76 1.578932 8 1.5 

133.522 3.780886 11.3 0.015 131.979 3.737194 11.4 0 126.265 3.575393 11.5 0.012 150.232 4.254056 8.5 4.06 148.205 4.196659 8 4.56 143.731 4.06997 7.8 4.06 

86.482 2.448874 9.8 2.2 84.128 2.382217 10.2 2.2 84.546 2.394054 10 2.2 89.483 2.533852 11.9 2.2 93.536 2.64862 12 2.2 90.405 2.55996 11.6 2.2 

208.754 5.911199 4.22 7.59 220.995 6.257822 4.9 0.46 217.503 6.158941 4.39 0.23 

39.778 1.126377 7.93 35.816 1.014187 7.38 36.457 1.032338 7.32 

156.922 4.443494 8.88 1.389 154.062 4.362509 8.21 1.8975 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

GAGPMadisonPly 800 Wood Waste Boiler 3 8/12/2009

GATempleInlandRome WF 1 7/27/2009GATempleInlandRome WF 2 7/28/2009GATempleInlandRome WF 3 7/28/2009

HIPuuneneSugarMill Boiler 1 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 1 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 1 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 1 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 2 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 2 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 2 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 3 Sample #1 5/23/2006HIPuuneneSugarMill Boiler 3 Sample #2 5/24/2006HIPuuneneSugarMill Boiler 3 Sample #3 5/25/2006HIPuuneneSugarMill Boiler 3 Sample #1 7/16/2007HIPuuneneSugarMill Boiler 3 Sample #2 7/17/2007HIPuuneneSugarMill Boiler 3 Sample #3 7/17/2007

IARoquetteAmericaCirculating Fluidized Bed Boiler (121)1 6/3/2009

IARoquetteAmericaCirculating Fluidized Bed Boiler (121)2 6/3/2009IARoquetteAmericaCirculating Fluidized Bed Boiler (121)3 6/4/2009

IAUofNorthernIowa Boiler #3 4 10/6/2009

Sample 

Volume 

(dscf)

Sample 

Volume 

(dscm)

Sample 

O2 (%)

As Catch 

(μg)

159.888 4.527481 7.21 1.343 150.483 4.261164 5.1 12.3 

157.17 4.450517 5 5.88 

163.398 4.626872 5.2 10.06 

96.787 2.797 10.06 16 95.978 2.718 9.84 16 

118.402 3.353 10.27 30 

96.787 2.797 10.06 16 95.978 2.718 9.84 16 

118.402 3.353 10.27 30 150.658 4.266119 5.8 1.24 151.674 4.294889 6.1 1.27 148.593 4.207645 5.6 1.33 164.415 4.65567 5.8 3.37 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

IAUofNorthernIowa Boiler #3 5 10/6/2009IAUofNorthernIowa Boiler #3 6 10/7/2009

IDAmalgamatedSugarCoTwinFalls S-B1 Sample #1 9/26/2006IDAmalgamatedSugarCoTwinFalls S-B1 Sample #2 9/26/2006IDAmalgamatedSugarCoTwinFalls S-B1 Sample #3 9/26/2006

IDPotlatch PB-1 CE Sample #1 7/20/2006IDPotlatch PB-1 CE Sample #2 7/20/2006IDPotlatch PB-1 CE Sample #3 7/20/2006IDPotlatch PB-1 CE M29-R1 7/28/2009IDPotlatch PB-1 CE M29-R2 7/28/2009IDPotlatch PB-1 CE M29-R3 7/29/2009IDPotlatch PB-2 Riley Sample #1 7/27/2006IDPotlatch PB-2 Riley Sample #2 7/27/2006IDPotlatch PB-2 Riley Sample #3 7/27/2006

IDTASCONampa Babcock and Wilcox (B&W) #1Sample #1 12/4/2006

IDTASCONampa Babcock and Wilcox (B&W) #1Sample #2 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #1Sample #3 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #2Sample #1 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #2Sample #2 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #2Sample #3 12/4/2006

ILPolyOne B1 Sample #1 11/14/2006ILPolyOne B1 Sample #2 11/14/2006ILPolyOne B1 Sample #3 11/14/2006ILPolyOne B1 1 9/9/2009ILPolyOne B1 2 9/9/2009ILPolyOne B1 3 9/10/2009

Sample 

Volume 

(dscf)

Sample 

Volume 

(dscm)

Sample 

O2 (%)

As Catch 

(μg)

165.331 4.681608 5.3 2.83 166.356 4.710633 6 2.26 

78.341 2.218349 6.9 5.1 80.205 2.271131 6.9 5.2 77.571 2.196545 6 5.2 159.52 4.517061 13.2 0.9 

170.7 4.83364 13.8 0.7 

161.05 4.560385 13 0.99 89.928 2.546453 7.4 0.53 94.073 2.663826 6.9 0.65 94.027 2.662523 6.9 0.47 89.928 2.546453 7.4 0.53 94.073 2.663826 6.9 0.65 94.027 2.662523 6.9 0.47 

83.69 2.369815 7.5 3 

3 

3.1 

172.203 4.8762 8.4 2.8 164.574 4.660173 8.09 2.8 165.647 4.690556 8.27 2.8 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

INSABICInnovativePlastics 01-001 BW1 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #3 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #3 6/28/2006

INTateLyleSagamore 31B1 M29-1 9/1/2009INTateLyleSagamore 31B1 M29-2 9/2/2009INTateLyleSagamore 31B1 M29-3 9/3/2009

MNHibbing Unit 1A Sample #1 9/21/2004MNHibbing Unit 1A Sample #2 9/21/2004MNHibbing Unit 1A Sample #3 9/21/2004MNHibbing Unit 2A Sample #1 9/22/2004MNHibbing Unit 2A Sample #2 9/22/2004MNHibbing Unit 2A Sample #3 9/22/2004

MSGPNewAugusta AA-015 Power Boiler Sample #1 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #2 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #3 7/12/2006

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #1 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #2 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #3 8/5/2009

NDCargillWestFargo Foster Wheeler Boiler (EU43) 1 8/26/2009

NDCargillWestFargo Foster Wheeler Boiler (EU43) 2 8/26/2009NDCargillWestFargo Foster Wheeler Boiler (EU43) 3 8/27/2009

OKGPMuskogeeMill B-4 Sample #1 4/16/2003OKGPMuskogeeMill B-4 Sample #2 4/16/2003

Sample 

Volume 

(dscf)

Sample 

Volume 

(dscm)

Sample 

O2 (%)

As Catch 

(μg)

91.73 2.59748 8 11.2 

89.671 2.539176 8 10 86.571 2.451395 8 10 

91.73 2.59748 8 11.2 

89.671 2.539176 8 10 86.571 2.451395 8 10 161.58 4.575393 5.57 5.33 139.34 3.945632 5.26 4.42 133.63 3.783944 5.97 2.986 

38.31 1.084808 6.5 2 

39.3 1.112842 7.21 2 

40.92 1.158714 6.84 2 35.81 1.014017 6.46 2 37.43 1.05989 6.82 2 37.97 1.075181 7.01 2 68.96 1.952711 10.2 1.96 55.59 1.574119 11.2 1.4 61.31 1.736089 12 1.42 

174.983 4.95492 8.06 0.812 180.328 5.106272 7.25 1.066 178.997 5.068583 7.63 0.575 126.485 3.581623 12.68 0.37 134.933 3.820841 12.68 0.58 138.135 3.911511 12.79 0.38 

87.1 2.466374 7.5 1.2 

85.634 2.424862 6.5 0.77 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

OKGPMuskogeeMill B-4 Sample #3 4/16/2003

SCMarlboroPaper Hogged Fuel Boiler Sample #1 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #2 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #3 7/14/2009

TNBowaterNewsprint Bubbling Fluidized Bed BoilerSample #1 10/6/2005TNBowaterNewsprint Bubbling Fluidized Bed BoilerSample #2 10/6/2005TNBowaterNewsprint Bubbling Fluidized Bed BoilerSample #3 10/6/2005TNBowaterNewsprint Bubbling Fluidized Bed Boiler 1 8/4/2009

TNBowaterNewsprint Bubbling Fluidized Bed Boiler 2 8/4/2009TNBowaterNewsprint Bubbling Fluidized Bed Boiler 3 8/5/2009

TNEastman_NO_CBIDATA Boiler 30 1 8/26/2009TNEastman_NO_CBIDATA Boiler 30 2 8/27/2009TNEastman_NO_CBIDATA Boiler 30 3 8/27/2009

TXDibollTemple-Inland PB-44 Sample #1 6/29/2007TXDibollTemple-Inland PB-44 Sample #2 6/29/2007

VAGeorgiaPacificBrooknealGladys 5600 Sample #1 7/6/2006VAGeorgiaPacificBrooknealGladys 5600 Sample #2 7/6/2006VAGeorgiaPacificBrooknealGladys 5600 Sample #3 7/6/2006

VAUniversityofVirginia 7103-1-01R M29-1 9/17/2009VAUniversityofVirginia 7103-1-01R M29-2 9/17/2009VAUniversityofVirginia 7103-1-01R M29-3 9/18/2009

VAVirginiaPolytechnic Boiler 11 Sample #1 2/27/2007VAVirginiaPolytechnic Boiler 11 Sample #1VAVirginiaPolytechnic Boiler 11 Sample #2VAVirginiaPolytechnic Boiler 7 Sample #3 2/28/2007VAVirginiaPolytechnic Boiler 7 Sample #1

Sample 

Volume 

(dscf)

Sample 

Volume 

(dscm)

Sample 

O2 (%)

As Catch 

(μg)

80.062 2.267082 6 0.71 142.32 4.030016 9.74 0.633 135.96 3.849922 9.38 0.69 146.64 4.152343 9.11 0.6 85.293 2.415206 5.6 4.5 82.303 2.330539 5.5 2.8 

78.77 2.230497 5.7 3 

163.647 4.633923 6.6 16.56 152.054 4.305649 7 15.21 159.337 4.511879 6.8 8.16 162.383 4.598131 6.3 7.64 163.694 4.635254 6.3 4.12 165.392 4.683336 6.3 4.13 61.4876 1.741119 12.1 0.085 61.4138 1.739029 12.1 0.122 

47 1.330879 15.27 0.2 

47.22 1.337109 15.55 0.2 47.68 1.350135 15.07 0.2 

176.38 4.994478 7.06 0.747 

169.546 4.800963 7.14 1.539 172.911 4.896248 7.07 0.213 

86.64567 2.453509 5.436667 7 

4.4 4.3 

82.27867 2.32985 5.436667 3.7 

13.8 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

VAVirginiaPolytechnic Boiler 7 Sample #1

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #1 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #2 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #3 8/12/2009

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #1 7/21/2005

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #2 7/21/2005WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #3 7/22/2005WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #1 8/20/2009WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #2 8/20/2009WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #3 8/21/2009

WINewPageBiron B24 Sample #1 9/12/2007WINewPageBiron B24 Sample #2 9/12/2007WINewPageBiron B24 Sample #3 9/12/2007WINewPageBiron B24 1 9/22/2009WINewPageBiron B24 2 9/22/2009WINewPageBiron B24 3 9/23/2009

WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #1 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #2 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #3 9/18/2003

WVMountainStateCarbonFollansbee S1 Sample #1 10/19/2009WVMountainStateCarbonFollansbee S1 Sample #2 10/19/2009WVMountainStateCarbonFollansbee S1 Sample #3 10/20/2009

WVPPGMartinsville R011-Boiler 3 1 7/22/2009WVPPGMartinsville R011-Boiler 3 2 7/23/2009WVPPGMartinsville R011-Boiler 3 3 7/23/2009

SCMilliken-Dewey D30 Sample #1 8/12/2009

Sample 

Volume 

(dscf)

Sample 

Volume 

(dscm)

Sample 

O2 (%)

As Catch 

(μg)

3.1 

154.1 4.363585 11.85 0.65 

162.62 4.604842 11.21 0.64 161.92 4.585021 10.22 0.64 40.974 1.160244 11.7 0.5 43.734 1.238397 12 6.77 45.025 1.274954 12 0.5 

155.597 4.405975 8.1 0.279 155.139 4.393006 8.8 0.212 147.746 4.183661 7.8 0.236 125.571 3.555741 7 6.99 114.102 3.230978 7 6.69 112.147 3.175619 7 5.09 167.363 4.739148 7.7 3.9 148.569 4.206966 6.9 4.75 150.007 4.247685 7.2 4.52 

55.11 1.560527 8.8 2.24 53.27 1.508424 8.8 2.37 54.06 1.530794 8.6 2.08 

163.271 4.623276 4.5 21 124.385 3.522158 4.7 26.2 143.477 4.062778 4.8 21.6 

139.67 3.954977 7.8 14.95 169.97 4.812969 8.6 10.18 130.74 3.70211 8.03 12.45 155.07 4.391052 3.83 5.28 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

SCMilliken-Dewey D30 Sample #2 8/12/2009SCMilliken-Dewey D30 Sample #3 8/12/2009

MNGPDuluth EU33 Boiler #3 1 9/10/2009MNGPDuluth EU33 Boiler #3 2 9/10/2009MNGPDuluth EU33 Boiler #3 3 9/10/2009

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 1 11/17/2009TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 2 11/17/2009TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 3 11/18/2009

Sample 

Volume 

(dscf)

Sample 

Volume 

(dscm)

Sample 

O2 (%)

As Catch 

(μg)

136.4 3.862381 4.02 2.654 

140.57 3.980462 3.96 1.8 152.87 4.328755 16.6 1.34 148.38 4.201614 16.27 1.81 144.35 4.087498 16 1.43 

166.745 4.721648 4.3 0.1 167.281 4.736826 4.3 1.44 

168.63 4.775025 5.3 1 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

AKDoyonUtilities_AK 4 Sample #1 8/17/2005AKDoyonUtilities_AK 4 Sample #2 8/17/2005AKDoyonUtilities_AK 4 Sample #3 8/17/2005AKDoyonUtilities_AK 7 Sample #1 8/16/2005AKDoyonUtilities_AK 7 Sample #2 8/16/2005AKDoyonUtilities_AK 7 Sample #3 8/16/2005

ALIPCourtland No. 3 Combination Boier / 11Cu301 Sample #1 7/7/2009

ALIPCourtland No. 3 Combination Boier / 11Cu301 Sample #2 7/7/2009ALIPCourtland No. 3 Combination Boier / 11Cu301 Sample #3 7/8/2009

ARAnthonyForestProducts SN-12 1 9/1/2009ARAnthonyForestProducts SN-12 2 9/1/2009ARAnthonyForestProducts SN-12 3 9/2/2009

ARLeolaLumberMill SN-01A Sample #1 6/14/2006ARLeolaLumberMill SN-01A Sample #2 6/14/2006ARLeolaLumberMill SN-01A Sample #3 6/14/2006ARLeolaLumberMill SN-01B Sample #1 6/14/2006ARLeolaLumberMill SN-01B Sample #2 6/14/2006ARLeolaLumberMill SN-01B Sample #3 6/14/2006

ARPotlatchForestWarren Wellons Boiler 1 9/9/2009ARPotlatchForestWarren Wellons Boiler 2 9/9/2009ARPotlatchForestWarren Wellons Boiler 3 9/9/2009

FLSugarCaneGrowersCoop Boiler No. 8 Sample #1 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #2 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #3 1/19/2005

GAGPMadisonPly 800 Wood Waste Boiler 1 8/11/2009

GAGPMadisonPly 800 Wood Waste Boiler 2 8/12/2009

Be Lab 

Analysis

Cd Catch 

(μg)

Cd Lab 

Analysis

Cr Catch 

(μg)

ICP/MS 0.79 ICP/MS 1.2 ICP/MS 0.9 ICP/MS 1.8 ICP/MS 0.6 ICP/MS 1.5 ICP/MS 0.6 ICP/MS 3.3 ICP/MS 1.2 ICP/MS 3.3 ICP/MS 0.6 ICP/MS 2.2 ICP/MS 1.946 ICP/MS 0.415 ICP/MS 0.0175 ICP/MS 0.06 ICP/MS 0.289 ICP/MS 0.17 ICP/MS 26.46 ICP/MS 17.41 ICP/MS 36.21 ICP/MS 20.4 ICP/MS 35.41 ICP/MS 19.31 ICP/MS 2.15 ICP/MS 1.2 ICP/MS 3.18 ICP/MS 2.8 ICP/MS 1.24 ICP/MS 2.3 ICP/MS 6.9 ICP/MS 1.3 ICP/MS 0.97 ICP/MS 1.4 ICP/MS 1.22 ICP/MS 2.6 ICP/MS 9.04 ICP/MS 19.893 ICP/MS 0.605 ICP/MS 4.087 ICP/MS 0.55 ICP/MS 4.546 

? ? ? ? ? ? 

ICP/MS 2.829 ICP/MS 36.369 ICP/MS 2.92 ICP/MS 35.522 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

GAGPMadisonPly 800 Wood Waste Boiler 3 8/12/2009

GATempleInlandRome WF 1 7/27/2009GATempleInlandRome WF 2 7/28/2009GATempleInlandRome WF 3 7/28/2009

HIPuuneneSugarMill Boiler 1 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 1 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 1 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 1 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 2 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 2 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 2 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 3 Sample #1 5/23/2006HIPuuneneSugarMill Boiler 3 Sample #2 5/24/2006HIPuuneneSugarMill Boiler 3 Sample #3 5/25/2006HIPuuneneSugarMill Boiler 3 Sample #1 7/16/2007HIPuuneneSugarMill Boiler 3 Sample #2 7/17/2007HIPuuneneSugarMill Boiler 3 Sample #3 7/17/2007

IARoquetteAmericaCirculating Fluidized Bed Boiler (121)1 6/3/2009

IARoquetteAmericaCirculating Fluidized Bed Boiler (121)2 6/3/2009IARoquetteAmericaCirculating Fluidized Bed Boiler (121)3 6/4/2009

IAUofNorthernIowa Boiler #3 4 10/6/2009

Be Lab 

Analysis

Cd Catch 

(μg)

Cd Lab 

Analysis

Cr Catch 

(μg)

ICP/MS 1.048 ICP/MS 46.022 ICP/MS 0.62 ICP/MS 12.58 ICP/MS 0.538 ICP/MS 13.29 ICP/MS 0.54 ICP/MS 11.28 

ICP/AES 2.4 ICP/MS 27 ICP/AES 2.7 ICP/MS 21 ICP/AES 5.9 ICP/MS 43 ICP/AES 2.4 ICP/MS 27 ICP/AES 2.7 ICP/MS 21 ICP/AES 5.9 ICP/MS 43 ICP/AES 4.1 ICP/AES 8.2 ICP/AES 7.3 ICP/AES 5.7 ICP/AES 1.34 ICP/AES 3.96 

? 0.45 ? 12.72 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

IAUofNorthernIowa Boiler #3 5 10/6/2009IAUofNorthernIowa Boiler #3 6 10/7/2009

IDAmalgamatedSugarCoTwinFalls S-B1 Sample #1 9/26/2006IDAmalgamatedSugarCoTwinFalls S-B1 Sample #2 9/26/2006IDAmalgamatedSugarCoTwinFalls S-B1 Sample #3 9/26/2006

IDPotlatch PB-1 CE Sample #1 7/20/2006IDPotlatch PB-1 CE Sample #2 7/20/2006IDPotlatch PB-1 CE Sample #3 7/20/2006IDPotlatch PB-1 CE M29-R1 7/28/2009IDPotlatch PB-1 CE M29-R2 7/28/2009IDPotlatch PB-1 CE M29-R3 7/29/2009IDPotlatch PB-2 Riley Sample #1 7/27/2006IDPotlatch PB-2 Riley Sample #2 7/27/2006IDPotlatch PB-2 Riley Sample #3 7/27/2006

IDTASCONampa Babcock and Wilcox (B&W) #1Sample #1 12/4/2006

IDTASCONampa Babcock and Wilcox (B&W) #1Sample #2 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #1Sample #3 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #2Sample #1 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #2Sample #2 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #2Sample #3 12/4/2006

ILPolyOne B1 Sample #1 11/14/2006ILPolyOne B1 Sample #2 11/14/2006ILPolyOne B1 Sample #3 11/14/2006ILPolyOne B1 1 9/9/2009ILPolyOne B1 2 9/9/2009ILPolyOne B1 3 9/10/2009

Be Lab 

Analysis

Cd Catch 

(μg)

Cd Lab 

Analysis

Cr Catch 

(μg)

? 0.36 ? 22.26 ? 0.48 ? 9.51 

ICP/AES 0.25 ICP/AES 149.7 ICP/AES 0.31 ICP/AES 2.6 ICP/AES 0.29 ICP/AES 0.52 

ICP/MS 0.3 ICP/MS 1.3 ICP/MS 0.65 ICP/MS 1.3 ICP/MS 0.13 ICP/MS 3.4 

ICP/AES 7.26 ICP/AES 2.16 ICP/AES 0.61 ICP/AES 1.65 ICP/AES 1.18 ICP/AES 0.87 ICP/AES 7.26 ICP/AES 2.16 ICP/AES 0.61 ICP/AES 1.65 ICP/AES 1.18 ICP/AES 0.87 

ICP/MS 0.75 ICP/MS 2.25 

0.75 2.68 0.75 2.25 

ICP/MS 0.72 ICP/MS 4.24 ICP/MS 0.7 ICP/MS 4.52 ICP/MS 0.7 ICP/MS 4.84 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

INSABICInnovativePlastics 01-001 BW1 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #3 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #3 6/28/2006

INTateLyleSagamore 31B1 M29-1 9/1/2009INTateLyleSagamore 31B1 M29-2 9/2/2009INTateLyleSagamore 31B1 M29-3 9/3/2009

MNHibbing Unit 1A Sample #1 9/21/2004MNHibbing Unit 1A Sample #2 9/21/2004MNHibbing Unit 1A Sample #3 9/21/2004MNHibbing Unit 2A Sample #1 9/22/2004MNHibbing Unit 2A Sample #2 9/22/2004MNHibbing Unit 2A Sample #3 9/22/2004

MSGPNewAugusta AA-015 Power Boiler Sample #1 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #2 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #3 7/12/2006

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #1 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #2 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #3 8/5/2009

NDCargillWestFargo Foster Wheeler Boiler (EU43) 1 8/26/2009

NDCargillWestFargo Foster Wheeler Boiler (EU43) 2 8/26/2009NDCargillWestFargo Foster Wheeler Boiler (EU43) 3 8/27/2009

OKGPMuskogeeMill B-4 Sample #1 4/16/2003OKGPMuskogeeMill B-4 Sample #2 4/16/2003

Be Lab 

Analysis

Cd Catch 

(μg)

Cd Lab 

Analysis

Cr Catch 

(μg)

ICP/AES 3.23 ICP/AES 16.4 ICP/AES 3.19 ICP/AES 13.01 ICP/AES 2.86 ICP/AES 15.8 ICP/AES 3.23 ICP/AES 16.4 ICP/AES 3.19 ICP/AES 13.01 ICP/AES 2.86 ICP/AES 15.8 

ICP/MS 1.731 ICP/MS 29.79 ICP/MS 1.544 ICP/MS 28.33 ICP/MS 0.94 ICP/MS 13.59 

ICP/AES 0.2 ICP/AES 5.3 ICP/AES 0.2 ICP/AES 2 ICP/AES 0.2 ICP/AES 2.1 ICP/AES 0.2 ICP/AES 6.2 ICP/AES 0.71 ICP/AES 4.3 ICP/AES 0.41 ICP/AES 2.6 

ICP/MS 0.392 ICP/MS 2.75 ICP/MS 0.212 ICP/MS 0.79 ICP/MS 0.152 ICP/MS 1.43 ICP/MS 1.009 ICP/MS 8.14 ICP/MS 1.25 ICP/MS 6.63 ICP/MS 1.05 ICP/MS 5 

ICP/AES 2.9 ICP/AES 2.74 ICP/AES 4.93 ICP/AES 1.8 ICP/AES 4.4 ICP/AES 1.82 

ICP/MS 0.31 ICP/MS 71 ICP/MS 2 ICP/MS 20 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

OKGPMuskogeeMill B-4 Sample #3 4/16/2003

SCMarlboroPaper Hogged Fuel Boiler Sample #1 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #2 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #3 7/14/2009

TNBowaterNewsprint Bubbling Fluidized Bed BoilerSample #1 10/6/2005TNBowaterNewsprint Bubbling Fluidized Bed BoilerSample #2 10/6/2005TNBowaterNewsprint Bubbling Fluidized Bed BoilerSample #3 10/6/2005TNBowaterNewsprint Bubbling Fluidized Bed Boiler 1 8/4/2009

TNBowaterNewsprint Bubbling Fluidized Bed Boiler 2 8/4/2009TNBowaterNewsprint Bubbling Fluidized Bed Boiler 3 8/5/2009

TNEastman_NO_CBIDATA Boiler 30 1 8/26/2009TNEastman_NO_CBIDATA Boiler 30 2 8/27/2009TNEastman_NO_CBIDATA Boiler 30 3 8/27/2009

TXDibollTemple-Inland PB-44 Sample #1 6/29/2007TXDibollTemple-Inland PB-44 Sample #2 6/29/2007

VAGeorgiaPacificBrooknealGladys 5600 Sample #1 7/6/2006VAGeorgiaPacificBrooknealGladys 5600 Sample #2 7/6/2006VAGeorgiaPacificBrooknealGladys 5600 Sample #3 7/6/2006

VAUniversityofVirginia 7103-1-01R M29-1 9/17/2009VAUniversityofVirginia 7103-1-01R M29-2 9/17/2009VAUniversityofVirginia 7103-1-01R M29-3 9/18/2009

VAVirginiaPolytechnic Boiler 11 Sample #1 2/27/2007VAVirginiaPolytechnic Boiler 11 Sample #1VAVirginiaPolytechnic Boiler 11 Sample #2VAVirginiaPolytechnic Boiler 7 Sample #3 2/28/2007VAVirginiaPolytechnic Boiler 7 Sample #1

Be Lab 

Analysis

Cd Catch 

(μg)

Cd Lab 

Analysis

Cr Catch 

(μg)

ICP/MS 0.1 ICP/MS 120 ICP/MS 0.414 ICP/MS 0.566 ICP/MS 0.433 ICP/MS 3.517 ICP/MS 0.26 ICP/MS 1.643 ICP/MS 1.3 ICP/MS 25.8 ICP/MS 1.2 ICP/MS 24.7 ICP/MS 0.8 ICP/MS 20 ICP/MS 2.553 ICP/MS 22.504 ICP/MS 2.601 ICP/MS 22.527 ICP/MS 1.45 ICP/MS 13.9155 ICP/MS 0.77 ICP/MS 8.85 ICP/MS 0.65 ICP/MS 7.385 ICP/MS 1.09 ICP/MS 4.99 ICP/MS 0.218 ICP/MS 0.22 ICP/MS 0.196 ICP/MS 0.77 ICP/MS 1.01 ICP/MS 1.4 ICP/MS 0.39 ICP/MS 1.02 ICP/MS 0.44 ICP/MS 1.33 ICP/MS 0.465 ICP/MS 14.389 ICP/MS 0.489 ICP/MS 4.781 ICP/MS 0.325 ICP/MS 4.752 

GFAA 3.08 GFAA 5.355 

0.26 2.67 0.28 2.95 

GFAA 4.55 GFAA 2.86 

6.41 4.765 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

VAVirginiaPolytechnic Boiler 7 Sample #1

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #1 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #2 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #3 8/12/2009

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #1 7/21/2005

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #2 7/21/2005WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #3 7/22/2005WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #1 8/20/2009WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #2 8/20/2009WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #3 8/21/2009

WINewPageBiron B24 Sample #1 9/12/2007WINewPageBiron B24 Sample #2 9/12/2007WINewPageBiron B24 Sample #3 9/12/2007WINewPageBiron B24 1 9/22/2009WINewPageBiron B24 2 9/22/2009WINewPageBiron B24 3 9/23/2009

WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #1 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #2 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #3 9/18/2003

WVMountainStateCarbonFollansbee S1 Sample #1 10/19/2009WVMountainStateCarbonFollansbee S1 Sample #2 10/19/2009WVMountainStateCarbonFollansbee S1 Sample #3 10/20/2009

WVPPGMartinsville R011-Boiler 3 1 7/22/2009WVPPGMartinsville R011-Boiler 3 2 7/23/2009WVPPGMartinsville R011-Boiler 3 3 7/23/2009

SCMilliken-Dewey D30 Sample #1 8/12/2009

Be Lab 

Analysis

Cd Catch 

(μg)

Cd Lab 

Analysis

Cr Catch 

(μg)

0.73 2.065 

? 0.32 ? 3.9 ? 0.69 ? 1.5 ? 0.32 ? 1.7 

ICP/MS 2.8 ICP/MS 18.2 ICP/MS 1.76 ICP/MS 14.4 ICP/MS 1.7 ICP/MS 8.89 ICP/MS 1.796 ICP/MS 9.15 ICP/MS 1.66 ICP/MS 4.922 ICP/MS 1.721 ICP/MS 6.45 ICP/MS 2.44 ICP/MS 4.5 ICP/MS 1.48 ICP/MS 1.9 ICP/MS 2.03 ICP/MS 0.66 ICP/MS 0.7 ICP/MS 1.7 ICP/MS 0.7 ICP/MS 2.21 ICP/MS 0.7 ICP/MS 2.03 

? 0.45 ? 3.66 ? 0.43 ? 4.14 ? 0.36 ? 3.88 

ICP/MS 434.13 ICP/MS 39.09 ICP/MS 35.8915 ICP/MS 38.8 ICP/MS 43.365 ICP/MS 49.28 

GFAA 0.3265 GFAA 7.42 GFAA 0.0665 GFAA 9.34 GFAA 0.0955 GFAA 6.22 

ICP/MS 0.234 ICP/MS 1.989 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

SCMilliken-Dewey D30 Sample #2 8/12/2009SCMilliken-Dewey D30 Sample #3 8/12/2009

MNGPDuluth EU33 Boiler #3 1 9/10/2009MNGPDuluth EU33 Boiler #3 2 9/10/2009MNGPDuluth EU33 Boiler #3 3 9/10/2009

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 1 11/17/2009TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 2 11/17/2009TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 3 11/18/2009

Be Lab 

Analysis

Cd Catch 

(μg)

Cd Lab 

Analysis

Cr Catch 

(μg)

ICP/MS 0.221 ICP/MS 1.95 ICP/MS 0.255 ICP/MS 1.735 ICP/MS 0.43 ICP/MS 3.98 ICP/MS 0.22 ICP/MS 3.81 ICP/MS 0.26 ICP/MS 3.61 ICP/MS 0.25 ICP/MS 5.73 ICP/MS 0.278 ICP/MS 5.79 ICP/MS 0.25 ICP/MS 5.26 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

AKDoyonUtilities_AK 4 Sample #1 8/17/2005AKDoyonUtilities_AK 4 Sample #2 8/17/2005AKDoyonUtilities_AK 4 Sample #3 8/17/2005AKDoyonUtilities_AK 7 Sample #1 8/16/2005AKDoyonUtilities_AK 7 Sample #2 8/16/2005AKDoyonUtilities_AK 7 Sample #3 8/16/2005

ALIPCourtland No. 3 Combination Boier / 11Cu301 Sample #1 7/7/2009

ALIPCourtland No. 3 Combination Boier / 11Cu301 Sample #2 7/7/2009ALIPCourtland No. 3 Combination Boier / 11Cu301 Sample #3 7/8/2009

ARAnthonyForestProducts SN-12 1 9/1/2009ARAnthonyForestProducts SN-12 2 9/1/2009ARAnthonyForestProducts SN-12 3 9/2/2009

ARLeolaLumberMill SN-01A Sample #1 6/14/2006ARLeolaLumberMill SN-01A Sample #2 6/14/2006ARLeolaLumberMill SN-01A Sample #3 6/14/2006ARLeolaLumberMill SN-01B Sample #1 6/14/2006ARLeolaLumberMill SN-01B Sample #2 6/14/2006ARLeolaLumberMill SN-01B Sample #3 6/14/2006

ARPotlatchForestWarren Wellons Boiler 1 9/9/2009ARPotlatchForestWarren Wellons Boiler 2 9/9/2009ARPotlatchForestWarren Wellons Boiler 3 9/9/2009

FLSugarCaneGrowersCoop Boiler No. 8 Sample #1 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #2 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #3 1/19/2005

GAGPMadisonPly 800 Wood Waste Boiler 1 8/11/2009

GAGPMadisonPly 800 Wood Waste Boiler 2 8/12/2009

Pb Lab 

Analysis

Mn Catch 

(μg)

Mn Lab 

Analysis

Ni Catch 

(μg)

ICP/MS 3 ICP/MS 2.3 ICP/MS 3.5 ICP/MS 3.7 ICP/MS 2.6 ICP/MS 2.7 ICP/MS 47.5 ICP/MS 5.55 ICP/MS 40 ICP/MS 3.6 ICP/MS 92 ICP/MS 2.3 ICP/MS 3.31 ICP/MS 0.92 ICP/MS 4.21 ICP/MS 0.19 ICP/MS 2.07 ICP/MS 0.4 ICP/MS 11359.12 ICP/MS 25.62 ICP/MS 13896.81 ICP/MS 31.27 ICP/MS 12899.31 ICP/MS 28 ICP/MS 15.5 ICP/MS 3 ICP/MS 18.7 ICP/MS 3.7 ICP/MS 11.41 ICP/MS 2.5 ICP/MS 50.21 ICP/MS 3.8 ICP/MS 46.51 ICP/MS 1.3 ICP/MS 47.51 ICP/MS 5.5 ICP/MS 2075.173 ICP/MS 10.685 ICP/MS 199.453 ICP/MS 1.795 ICP/MS 78.353 ICP/MS 1.395 

? ? ? ? ? ? 

ICP/MS 18.46 ICP/MS 46.041 ICP/MS 23.95 ICP/MS 88.355 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

GAGPMadisonPly 800 Wood Waste Boiler 3 8/12/2009

GATempleInlandRome WF 1 7/27/2009GATempleInlandRome WF 2 7/28/2009GATempleInlandRome WF 3 7/28/2009

HIPuuneneSugarMill Boiler 1 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 1 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 1 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 1 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 2 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 2 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 2 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 3 Sample #1 5/23/2006HIPuuneneSugarMill Boiler 3 Sample #2 5/24/2006HIPuuneneSugarMill Boiler 3 Sample #3 5/25/2006HIPuuneneSugarMill Boiler 3 Sample #1 7/16/2007HIPuuneneSugarMill Boiler 3 Sample #2 7/17/2007HIPuuneneSugarMill Boiler 3 Sample #3 7/17/2007

IARoquetteAmericaCirculating Fluidized Bed Boiler (121)1 6/3/2009

IARoquetteAmericaCirculating Fluidized Bed Boiler (121)2 6/3/2009IARoquetteAmericaCirculating Fluidized Bed Boiler (121)3 6/4/2009

IAUofNorthernIowa Boiler #3 4 10/6/2009

Pb Lab 

Analysis

Mn Catch 

(μg)

Mn Lab 

Analysis

Ni Catch 

(μg)

ICP/MS 34.42 ICP/MS 75.48 ICP/MS 366.77 ICP/MS 8.95 ICP/MS 429.9 ICP/MS 8.95 ICP/MS 358.18 ICP/MS 9.25 

ICP/AES 370 ICP/AES 22 ICP/AES 180 ICP/AES 8.4 ICP/AES 880 ICP/AES 75 ICP/AES 370 ICP/AES 22 ICP/AES 180 ICP/AES 8.4 ICP/AES 880 ICP/AES 75 ICP/AES 15.2 ICP/AES 17 ICP/AES 13.6 ICP/AES 15.8 ICP/AES 9.1 ICP/AES 14.8 

? 59.9 ? 10.79 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

IAUofNorthernIowa Boiler #3 5 10/6/2009IAUofNorthernIowa Boiler #3 6 10/7/2009

IDAmalgamatedSugarCoTwinFalls S-B1 Sample #1 9/26/2006IDAmalgamatedSugarCoTwinFalls S-B1 Sample #2 9/26/2006IDAmalgamatedSugarCoTwinFalls S-B1 Sample #3 9/26/2006

IDPotlatch PB-1 CE Sample #1 7/20/2006IDPotlatch PB-1 CE Sample #2 7/20/2006IDPotlatch PB-1 CE Sample #3 7/20/2006IDPotlatch PB-1 CE M29-R1 7/28/2009IDPotlatch PB-1 CE M29-R2 7/28/2009IDPotlatch PB-1 CE M29-R3 7/29/2009IDPotlatch PB-2 Riley Sample #1 7/27/2006IDPotlatch PB-2 Riley Sample #2 7/27/2006IDPotlatch PB-2 Riley Sample #3 7/27/2006

IDTASCONampa Babcock and Wilcox (B&W) #1Sample #1 12/4/2006

IDTASCONampa Babcock and Wilcox (B&W) #1Sample #2 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #1Sample #3 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #2Sample #1 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #2Sample #2 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #2Sample #3 12/4/2006

ILPolyOne B1 Sample #1 11/14/2006ILPolyOne B1 Sample #2 11/14/2006ILPolyOne B1 Sample #3 11/14/2006ILPolyOne B1 1 9/9/2009ILPolyOne B1 2 9/9/2009ILPolyOne B1 3 9/10/2009

Pb Lab 

Analysis

Mn Catch 

(μg)

Mn Lab 

Analysis

Ni Catch 

(μg)

? 53.8 ? 20.87 ? 69.2 ? 16.47 

ICP/AES 64.95 ICP/AES 94.7 ICP/AES 52.47 ICP/AES 41.7 ICP/AES 83.5 ICP/AES 16.7 

ICP/MS 16.88 ICP/MS 2 ICP/MS 19.53 ICP/MS 0.9 ICP/MS 17.82 ICP/MS 1.3 

GFAA 10.6 ICP/AES 15.4 GFAA 11.9 ICP/AES 18.3 GFAA 8.8 ICP/AES 17.5 GFAA 10.6 ICP/AES 15.4 GFAA 11.9 ICP/AES 18.3 GFAA 8.8 ICP/AES 17.5 

ICP/MS 12.2 ICP/MS 4.3 

27.4 4.8 

6 4.4 

ICP/MS 9.6 ICP/MS 5.7 ICP/MS 10.5 ICP/MS 5.4 ICP/MS 11.5 ICP/MS 5.5 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

INSABICInnovativePlastics 01-001 BW1 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #3 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #3 6/28/2006

INTateLyleSagamore 31B1 M29-1 9/1/2009INTateLyleSagamore 31B1 M29-2 9/2/2009INTateLyleSagamore 31B1 M29-3 9/3/2009

MNHibbing Unit 1A Sample #1 9/21/2004MNHibbing Unit 1A Sample #2 9/21/2004MNHibbing Unit 1A Sample #3 9/21/2004MNHibbing Unit 2A Sample #1 9/22/2004MNHibbing Unit 2A Sample #2 9/22/2004MNHibbing Unit 2A Sample #3 9/22/2004

MSGPNewAugusta AA-015 Power Boiler Sample #1 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #2 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #3 7/12/2006

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #1 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #2 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #3 8/5/2009

NDCargillWestFargo Foster Wheeler Boiler (EU43) 1 8/26/2009

NDCargillWestFargo Foster Wheeler Boiler (EU43) 2 8/26/2009NDCargillWestFargo Foster Wheeler Boiler (EU43) 3 8/27/2009

OKGPMuskogeeMill B-4 Sample #1 4/16/2003OKGPMuskogeeMill B-4 Sample #2 4/16/2003

Pb Lab 

Analysis

Mn Catch 

(μg)

Mn Lab 

Analysis

Ni Catch 

(μg)

ICP/AES 11.9 ICP/AES 20.4 ICP/AES 6 ICP/AES 15.4 ICP/AES 10 ICP/AES 16.7 ICP/AES 11.9 ICP/AES 20.4 ICP/AES 6 ICP/AES 15.4 ICP/AES 10 ICP/AES 16.7 

ICP/MS 45.75 ICP/MS 77.28 ICP/MS 43.62 ICP/MS 85.63 ICP/MS 24.11 ICP/MS 36.4 

ICP/AES 4 ICP/AES 4.8 ICP/AES 3.9 ICP/AES 2.6 ICP/AES 3.8 ICP/AES 1.5 ICP/AES 5.7 ICP/AES 6.3 ICP/AES 6.3 ICP/AES 3.2 ICP/AES 8.9 ICP/AES 4.4 

ICP/MS 82.805 ICP/MS 2.405 ICP/MS 13.675 ICP/MS 0.825 ICP/MS 16.07 ICP/MS 1.035 ICP/MS 234.1725 ICP/MS 4.118 ICP/MS 355.35 ICP/MS 3.098 ICP/MS 144.1825 ICP/MS 0.648 

ICP/AES 12.47 ICP/AES 1.21 ICP/AES 17.85 ICP/AES 1.53 ICP/AES 10.98 ICP/AES 2.73 

ICP/MS 15 ICP/MS 29 ICP/MS 12 ICP/MS 15 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

OKGPMuskogeeMill B-4 Sample #3 4/16/2003

SCMarlboroPaper Hogged Fuel Boiler Sample #1 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #2 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #3 7/14/2009

TNBowaterNewsprint Bubbling Fluidized Bed BoilerSample #1 10/6/2005TNBowaterNewsprint Bubbling Fluidized Bed BoilerSample #2 10/6/2005TNBowaterNewsprint Bubbling Fluidized Bed BoilerSample #3 10/6/2005TNBowaterNewsprint Bubbling Fluidized Bed Boiler 1 8/4/2009

TNBowaterNewsprint Bubbling Fluidized Bed Boiler 2 8/4/2009TNBowaterNewsprint Bubbling Fluidized Bed Boiler 3 8/5/2009

TNEastman_NO_CBIDATA Boiler 30 1 8/26/2009TNEastman_NO_CBIDATA Boiler 30 2 8/27/2009TNEastman_NO_CBIDATA Boiler 30 3 8/27/2009

TXDibollTemple-Inland PB-44 Sample #1 6/29/2007TXDibollTemple-Inland PB-44 Sample #2 6/29/2007

VAGeorgiaPacificBrooknealGladys 5600 Sample #1 7/6/2006VAGeorgiaPacificBrooknealGladys 5600 Sample #2 7/6/2006VAGeorgiaPacificBrooknealGladys 5600 Sample #3 7/6/2006

VAUniversityofVirginia 7103-1-01R M29-1 9/17/2009VAUniversityofVirginia 7103-1-01R M29-2 9/17/2009VAUniversityofVirginia 7103-1-01R M29-3 9/18/2009

VAVirginiaPolytechnic Boiler 11 Sample #1 2/27/2007VAVirginiaPolytechnic Boiler 11 Sample #1VAVirginiaPolytechnic Boiler 11 Sample #2VAVirginiaPolytechnic Boiler 7 Sample #3 2/28/2007VAVirginiaPolytechnic Boiler 7 Sample #1

Pb Lab 

Analysis

Mn Catch 

(μg)

Mn Lab 

Analysis

Ni Catch 

(μg)

ICP/MS 20 ICP/MS 31 ICP/MS 7.727 ICP/MS 3.387 ICP/MS 10.748 ICP/MS 5.447 ICP/MS 9.568 ICP/MS -0.133 ICP/MS 153 ICP/MS 19.2 ICP/MS 201 ICP/MS 13.9 ICP/MS 130 ICP/MS 10 ICP/MS 2522.5 ICP/MS 25.51 ICP/MS 2641.88 ICP/MS 27.65 ICP/MS 1482.1 ICP/MS 10.39 ICP/MS 12.27 ICP/MS 8.72 ICP/MS 11.97 ICP/MS 7.82 ICP/MS 6.97 ICP/MS 5.22 ICP/MS 77.71 ICP/MS 0.97 ICP/MS 437 ICP/MS 2.56 ICP/MS 96.9 ICP/MS 0.6 ICP/MS 47.88 ICP/MS 0.71 ICP/MS 115.9 ICP/MS 0.18 ICP/MS 37.824 ICP/MS 5.072 ICP/MS 30.264 ICP/MS 11.623 ICP/MS 19.264 ICP/MS 21.802 

GFAA 48.14 GFAA 10.74 

65.335 6.735 

11.89 6.04 

GFAA 26.385 GFAA 4.63 

26.14 7.935 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

VAVirginiaPolytechnic Boiler 7 Sample #1

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #1 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #2 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #3 8/12/2009

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #1 7/21/2005

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #2 7/21/2005WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #3 7/22/2005WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #1 8/20/2009WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #2 8/20/2009WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #3 8/21/2009

WINewPageBiron B24 Sample #1 9/12/2007WINewPageBiron B24 Sample #2 9/12/2007WINewPageBiron B24 Sample #3 9/12/2007WINewPageBiron B24 1 9/22/2009WINewPageBiron B24 2 9/22/2009WINewPageBiron B24 3 9/23/2009

WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #1 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #2 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #3 9/18/2003

WVMountainStateCarbonFollansbee S1 Sample #1 10/19/2009WVMountainStateCarbonFollansbee S1 Sample #2 10/19/2009WVMountainStateCarbonFollansbee S1 Sample #3 10/20/2009

WVPPGMartinsville R011-Boiler 3 1 7/22/2009WVPPGMartinsville R011-Boiler 3 2 7/23/2009WVPPGMartinsville R011-Boiler 3 3 7/23/2009

SCMilliken-Dewey D30 Sample #1 8/12/2009

Pb Lab 

Analysis

Mn Catch 

(μg)

Mn Lab 

Analysis

Ni Catch 

(μg)

17.77 4.23 

? 65.2 ? 4.1 ? 45.2 ? 1.3 ? 30.7 ? 2.1 

ICP/MS 7.43 ICP/MS 10.6 ICP/MS 11.7 ICP/MS 14.8 ICP/MS 46.1 ICP/MS 7.17 ICP/MS 12.23 ICP/MS 6.56 ICP/MS 6.01 ICP/MS 4.61 ICP/MS 28.42 ICP/MS 3.99 ICP/MS 5.63 ICP/MS 6.46 ICP/MS 84.43 ICP/MS 5.26 ICP/MS 96.43 ICP/MS 4.16 ICP/MS 36.7 ICP/MS 4.19 ICP/MS 9.2 ICP/MS 3.69 ICP/MS 9.5 ICP/MS 3.69 

? 35.14 ? 3.14 ? 31.2 ? 3.18 ? 29.81 ? 2.77 

ICP/MS 28.15 ICP/MS 46.47 ICP/MS 60.7 ICP/MS 22.67 ICP/MS 25.69 ICP/MS 23.67 

GFAA 9.999 ICP/AES 9.528 GFAA 15.885 ICP/AES 14.486 GFAA 12.07 ICP/AES 8.777 

ICP/MS 6.4 ICP/MS 2.545 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

SCMilliken-Dewey D30 Sample #2 8/12/2009SCMilliken-Dewey D30 Sample #3 8/12/2009

MNGPDuluth EU33 Boiler #3 1 9/10/2009MNGPDuluth EU33 Boiler #3 2 9/10/2009MNGPDuluth EU33 Boiler #3 3 9/10/2009

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 1 11/17/2009TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 2 11/17/2009TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 3 11/18/2009

Pb Lab 

Analysis

Mn Catch 

(μg)

Mn Lab 

Analysis

Ni Catch 

(μg)

ICP/MS 4.81 ICP/MS 1.959 ICP/MS 3.94 ICP/MS 2.499 ICP/MS 27.71 ICP/MS 22.61 ICP/MS 30.42 ICP/MS 27.09 ICP/MS 12.59 ICP/MS 12.36 ICP/MS 12.97 ICP/MS 5.77 ICP/MS 6.25 ICP/MS 6.41 ICP/MS 18.2 ICP/MS 5.8 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

AKDoyonUtilities_AK 4 Sample #1 8/17/2005AKDoyonUtilities_AK 4 Sample #2 8/17/2005AKDoyonUtilities_AK 4 Sample #3 8/17/2005AKDoyonUtilities_AK 7 Sample #1 8/16/2005AKDoyonUtilities_AK 7 Sample #2 8/16/2005AKDoyonUtilities_AK 7 Sample #3 8/16/2005

ALIPCourtland No. 3 Combination Boier / 11Cu301 Sample #1 7/7/2009

ALIPCourtland No. 3 Combination Boier / 11Cu301 Sample #2 7/7/2009ALIPCourtland No. 3 Combination Boier / 11Cu301 Sample #3 7/8/2009

ARAnthonyForestProducts SN-12 1 9/1/2009ARAnthonyForestProducts SN-12 2 9/1/2009ARAnthonyForestProducts SN-12 3 9/2/2009

ARLeolaLumberMill SN-01A Sample #1 6/14/2006ARLeolaLumberMill SN-01A Sample #2 6/14/2006ARLeolaLumberMill SN-01A Sample #3 6/14/2006ARLeolaLumberMill SN-01B Sample #1 6/14/2006ARLeolaLumberMill SN-01B Sample #2 6/14/2006ARLeolaLumberMill SN-01B Sample #3 6/14/2006

ARPotlatchForestWarren Wellons Boiler 1 9/9/2009ARPotlatchForestWarren Wellons Boiler 2 9/9/2009ARPotlatchForestWarren Wellons Boiler 3 9/9/2009

FLSugarCaneGrowersCoop Boiler No. 8 Sample #1 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #2 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #3 1/19/2005

GAGPMadisonPly 800 Wood Waste Boiler 1 8/11/2009

GAGPMadisonPly 800 Wood Waste Boiler 2 8/12/2009

Se Lab 

Analysis

As 3x RDL 

Concentration 

(μg/dscm)

Be 3x RDL 

Concentration 

(μg/dscm)

ICP/MS 1.2 0.24 ICP/MS 1.206898516 0.24 ICP/MS 1.2 0.24 ICP/MS 1.2 0.24 ICP/MS 1.2 0.247087633 ICP/MS 1.2 0.253335725 ICP/MS 0.3 0.06 ICP/MS 0.3 0.06 ICP/MS 0.3 0.06 ICP/MS 0.954383221 0.129288367 ICP/MS 1.086578725 0.131056645 ICP/MS 0.997550285 0.135136122 ICP/MS 0.898371916 0.12 ICP/MS 0.923509414 0.12 ICP/MS 0.918943534 0.12 ICP/MS 0.86824313 0.12 ICP/MS 0.830621365 0.12 ICP/MS 0.859388308 0.12 ICP/MS 1.28400342 0.06 ICP/MS 0.3 0.06 ICP/MS 0.3 0.06 

???

ICP/MS 0.312591829 0.06 ICP/MS 0.434956138 0.06 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

GAGPMadisonPly 800 Wood Waste Boiler 3 8/12/2009

GATempleInlandRome WF 1 7/27/2009GATempleInlandRome WF 2 7/28/2009GATempleInlandRome WF 3 7/28/2009

HIPuuneneSugarMill Boiler 1 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 1 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 1 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 1 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 2 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 2 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 2 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 3 Sample #1 5/23/2006HIPuuneneSugarMill Boiler 3 Sample #2 5/24/2006HIPuuneneSugarMill Boiler 3 Sample #3 5/25/2006HIPuuneneSugarMill Boiler 3 Sample #1 7/16/2007HIPuuneneSugarMill Boiler 3 Sample #2 7/17/2007HIPuuneneSugarMill Boiler 3 Sample #3 7/17/2007

IARoquetteAmericaCirculating Fluidized Bed Boiler (121)1 6/3/2009

IARoquetteAmericaCirculating Fluidized Bed Boiler (121)2 6/3/2009IARoquetteAmericaCirculating Fluidized Bed Boiler (121)3 6/4/2009

IAUofNorthernIowa Boiler #3 4 10/6/2009

Se Lab 

Analysis

As 3x RDL 

Concentration 

(μg/dscm)

Be 3x RDL 

Concentration 

(μg/dscm)

ICP/MS 0.3 0.06 ICP/MS 2.886535356 0.08 ICP/MS 1.321194885 0.08 ICP/MS 2.174254887 0.08 

ICP/AES #N/A #N/A ICP/AES #N/A #N/A ICP/AES #N/A #N/A ICP/AES #N/A #N/A ICP/AES #N/A #N/A ICP/AES #N/A #N/A ICP/AES 19 0.11 ICP/AES 19 0.11 ICP/AES 19 0.11 

? #VALUE! #VALUE! 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

IAUofNorthernIowa Boiler #3 5 10/6/2009IAUofNorthernIowa Boiler #3 6 10/7/2009

IDAmalgamatedSugarCoTwinFalls S-B1 Sample #1 9/26/2006IDAmalgamatedSugarCoTwinFalls S-B1 Sample #2 9/26/2006IDAmalgamatedSugarCoTwinFalls S-B1 Sample #3 9/26/2006

IDPotlatch PB-1 CE Sample #1 7/20/2006IDPotlatch PB-1 CE Sample #2 7/20/2006IDPotlatch PB-1 CE Sample #3 7/20/2006IDPotlatch PB-1 CE M29-R1 7/28/2009IDPotlatch PB-1 CE M29-R2 7/28/2009IDPotlatch PB-1 CE M29-R3 7/29/2009IDPotlatch PB-2 Riley Sample #1 7/27/2006IDPotlatch PB-2 Riley Sample #2 7/27/2006IDPotlatch PB-2 Riley Sample #3 7/27/2006

IDTASCONampa Babcock and Wilcox (B&W) #1Sample #1 12/4/2006

IDTASCONampa Babcock and Wilcox (B&W) #1Sample #2 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #1Sample #3 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #2Sample #1 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #2Sample #2 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #2Sample #3 12/4/2006

ILPolyOne B1 Sample #1 11/14/2006ILPolyOne B1 Sample #2 11/14/2006ILPolyOne B1 Sample #3 11/14/2006ILPolyOne B1 1 9/9/2009ILPolyOne B1 2 9/9/2009ILPolyOne B1 3 9/10/2009

Se Lab 

Analysis

As 3x RDL 

Concentration 

(μg/dscm)

Be 3x RDL 

Concentration 

(μg/dscm)

? #VALUE! #VALUE! ? #VALUE! #VALUE! 

ICP/AES 29 0.17 ICP/AES 29 0.17 ICP/AES 29 0.17 

ICP/MS 0.3 0.06 ICP/MS 0.3 0.06 ICP/MS 0.3 0.06 

GFAA 0.6 0.17 GFAA 0.6 0.17 GFAA 0.6 0.443188659 GFAA 0.6 0.17 GFAA 0.6 0.17 GFAA 0.6 0.17 

ICP/MS 1.265921854 0.316480464 

#DIV/0! #DIV/0! #DIV/0! #DIV/0! 

ICP/MS 0.574217638 0.14355441 ICP/MS 0.600836098 0.150209025 ICP/MS 0.596944104 0.166291572 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

INSABICInnovativePlastics 01-001 BW1 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #3 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #3 6/28/2006

INTateLyleSagamore 31B1 M29-1 9/1/2009INTateLyleSagamore 31B1 M29-2 9/2/2009INTateLyleSagamore 31B1 M29-3 9/3/2009

MNHibbing Unit 1A Sample #1 9/21/2004MNHibbing Unit 1A Sample #2 9/21/2004MNHibbing Unit 1A Sample #3 9/21/2004MNHibbing Unit 2A Sample #1 9/22/2004MNHibbing Unit 2A Sample #2 9/22/2004MNHibbing Unit 2A Sample #3 9/22/2004

MSGPNewAugusta AA-015 Power Boiler Sample #1 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #2 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #3 7/12/2006

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #1 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #2 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #3 8/5/2009

NDCargillWestFargo Foster Wheeler Boiler (EU43) 1 8/26/2009

NDCargillWestFargo Foster Wheeler Boiler (EU43) 2 8/26/2009NDCargillWestFargo Foster Wheeler Boiler (EU43) 3 8/27/2009

OKGPMuskogeeMill B-4 Sample #1 4/16/2003OKGPMuskogeeMill B-4 Sample #2 4/16/2003

Se Lab 

Analysis

As 3x RDL 

Concentration 

(μg/dscm)

Be 3x RDL 

Concentration 

(μg/dscm)

GFAA 4.311871798 0.346489698 GFAA 3.93828551 0.252050273 GFAA 4.079310624 0.224362084 GFAA 4.311871798 0.346489698 GFAA 3.93828551 0.252050273 GFAA 4.079310624 0.224362084 

ICP/MS 1.164927281 0.735455966 ICP/MS 1.120226066 0.748929417 ICP/MS 0.789123625 0.463801729 

ICP/AES 57 0.460910989 ICP/AES 57 0.449300254 ICP/AES 57 0.431512708 ICP/AES 57 0.493088523 ICP/AES 57 0.471747262 ICP/AES 57 0.465038188 

ICP/MS 1.003732599 0.179237964 ICP/MS 0.88938658 0.222346645 ICP/MS 0.817930191 0.201602512 ICP/MS 0.4 0.08 ICP/MS 0.4 0.08 ICP/MS 0.4 0.08 

ICP/AES 14 0.089344982 ICP/AES 14 0.083751195 ICP/AES 14 0.083 

ICP/MS 0.6 0.12 ICP/MS 0.6 0.12 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

OKGPMuskogeeMill B-4 Sample #3 4/16/2003

SCMarlboroPaper Hogged Fuel Boiler Sample #1 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #2 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #3 7/14/2009

TNBowaterNewsprint Bubbling Fluidized Bed BoilerSample #1 10/6/2005TNBowaterNewsprint Bubbling Fluidized Bed BoilerSample #2 10/6/2005TNBowaterNewsprint Bubbling Fluidized Bed BoilerSample #3 10/6/2005TNBowaterNewsprint Bubbling Fluidized Bed Boiler 1 8/4/2009

TNBowaterNewsprint Bubbling Fluidized Bed Boiler 2 8/4/2009TNBowaterNewsprint Bubbling Fluidized Bed Boiler 3 8/5/2009

TNEastman_NO_CBIDATA Boiler 30 1 8/26/2009TNEastman_NO_CBIDATA Boiler 30 2 8/27/2009TNEastman_NO_CBIDATA Boiler 30 3 8/27/2009

TXDibollTemple-Inland PB-44 Sample #1 6/29/2007TXDibollTemple-Inland PB-44 Sample #2 6/29/2007

VAGeorgiaPacificBrooknealGladys 5600 Sample #1 7/6/2006VAGeorgiaPacificBrooknealGladys 5600 Sample #2 7/6/2006VAGeorgiaPacificBrooknealGladys 5600 Sample #3 7/6/2006

VAUniversityofVirginia 7103-1-01R M29-1 9/17/2009VAUniversityofVirginia 7103-1-01R M29-2 9/17/2009VAUniversityofVirginia 7103-1-01R M29-3 9/18/2009

VAVirginiaPolytechnic Boiler 11 Sample #1 2/27/2007VAVirginiaPolytechnic Boiler 11 Sample #1VAVirginiaPolytechnic Boiler 11 Sample #2VAVirginiaPolytechnic Boiler 7 Sample #3 2/28/2007VAVirginiaPolytechnic Boiler 7 Sample #1

Se Lab 

Analysis

As 3x RDL 

Concentration 

(μg/dscm)

Be 3x RDL 

Concentration 

(μg/dscm)

ICP/MS 0.6 0.12 ICP/MS 0.4 0.08 ICP/MS 0.4 0.08 ICP/MS 0.4 0.08 ICP/MS 1.863195104 0.24 ICP/MS 1.201438587 0.24 ICP/MS 1.344991748 0.24 ICP/MS 3.573645713 0.226589855 ICP/MS 3.532568364 0.243865666 ICP/MS 1.808559217 0.232719017 ICP/MS 1.66154462 0.163109747 ICP/MS 0.888840153 0.151016531 ICP/MS 0.881850089 0.149466117 ICP/MS 0.6 0.12 ICP/MS 0.6 0.12 ICP/MS 1.2 0.24 ICP/MS 1.2 0.24 ICP/MS 1.2 0.24 ICP/MS 0.3 0.06 ICP/MS 0.320560703 0.06 ICP/MS 0.3 0.06 

GFAA 2.853056702 0.203789764 

#DIV/0! #DIV/0! #DIV/0! #DIV/0! 

GFAA 1.588084801 0.12 

#DIV/0! #DIV/0! 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

VAVirginiaPolytechnic Boiler 7 Sample #1

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #1 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #2 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #3 8/12/2009

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #1 7/21/2005

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #2 7/21/2005WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #3 7/22/2005WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #1 8/20/2009WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #2 8/20/2009WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #3 8/21/2009

WINewPageBiron B24 Sample #1 9/12/2007WINewPageBiron B24 Sample #2 9/12/2007WINewPageBiron B24 Sample #3 9/12/2007WINewPageBiron B24 1 9/22/2009WINewPageBiron B24 2 9/22/2009WINewPageBiron B24 3 9/23/2009

WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #1 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #2 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #3 9/18/2003

WVMountainStateCarbonFollansbee S1 Sample #1 10/19/2009WVMountainStateCarbonFollansbee S1 Sample #2 10/19/2009WVMountainStateCarbonFollansbee S1 Sample #3 10/20/2009

WVPPGMartinsville R011-Boiler 3 1 7/22/2009WVPPGMartinsville R011-Boiler 3 2 7/23/2009WVPPGMartinsville R011-Boiler 3 3 7/23/2009

SCMilliken-Dewey D30 Sample #1 8/12/2009

Se Lab 

Analysis

As 3x RDL 

Concentration 

(μg/dscm)

Be 3x RDL 

Concentration 

(μg/dscm)

#DIV/0! #DIV/0! 

? #VALUE! #VALUE! ? #VALUE! #VALUE! ? #VALUE! #VALUE! 

ICP/MS 1.2 0.24 ICP/MS 5.466743266 0.24 ICP/MS 1.2 0.24 ICP/MS 0.3 0.06 ICP/MS 0.3 0.06 ICP/MS 0.3 0.06 ICP/MS 1.965834866 0.210926488 ICP/MS 2.07058027 0.232127833 ICP/MS 1.602836902 0.236174396 ICP/MS 0.822932787 0.147705885 ICP/MS 1.129079754 0.166390701 ICP/MS 1.064109008 0.164795643 

? #VALUE! #VALUE! ? #VALUE! #VALUE! ? #VALUE! #VALUE! 

ICP/MS 4.542233465 0.097333574 ICP/MS 7.43862202 0.127762592 ICP/MS 5.316559449 0.110761655 

GFAA 3.780047612 0.070796878 GFAA 2.11511855 0.064409308 GFAA 3.362947453 0.075632553 

ICP/MS 1.202445347 0.08 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

SCMilliken-Dewey D30 Sample #2 8/12/2009SCMilliken-Dewey D30 Sample #3 8/12/2009

MNGPDuluth EU33 Boiler #3 1 9/10/2009MNGPDuluth EU33 Boiler #3 2 9/10/2009MNGPDuluth EU33 Boiler #3 3 9/10/2009

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 1 11/17/2009TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 2 11/17/2009TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 3 11/18/2009

Se Lab 

Analysis

As 3x RDL 

Concentration 

(μg/dscm)

Be 3x RDL 

Concentration 

(μg/dscm)

ICP/MS 0.687140836 0.08 ICP/MS 0.452208864 0.08 ICP/MS 0.4 0.08 ICP/MS 0.430786831 0.08 ICP/MS 0.4 0.08 ICP/MS 0.3 0.06 ICP/MS 0.304001052 0.06 ICP/MS 0.3 0.06 
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

AKDoyonUtilities_AK 4 Sample #1 8/17/2005AKDoyonUtilities_AK 4 Sample #2 8/17/2005AKDoyonUtilities_AK 4 Sample #3 8/17/2005AKDoyonUtilities_AK 7 Sample #1 8/16/2005AKDoyonUtilities_AK 7 Sample #2 8/16/2005AKDoyonUtilities_AK 7 Sample #3 8/16/2005

ALIPCourtland No. 3 Combination Boier / 11Cu301 Sample #1 7/7/2009

ALIPCourtland No. 3 Combination Boier / 11Cu301 Sample #2 7/7/2009ALIPCourtland No. 3 Combination Boier / 11Cu301 Sample #3 7/8/2009

ARAnthonyForestProducts SN-12 1 9/1/2009ARAnthonyForestProducts SN-12 2 9/1/2009ARAnthonyForestProducts SN-12 3 9/2/2009

ARLeolaLumberMill SN-01A Sample #1 6/14/2006ARLeolaLumberMill SN-01A Sample #2 6/14/2006ARLeolaLumberMill SN-01A Sample #3 6/14/2006ARLeolaLumberMill SN-01B Sample #1 6/14/2006ARLeolaLumberMill SN-01B Sample #2 6/14/2006ARLeolaLumberMill SN-01B Sample #3 6/14/2006

ARPotlatchForestWarren Wellons Boiler 1 9/9/2009ARPotlatchForestWarren Wellons Boiler 2 9/9/2009ARPotlatchForestWarren Wellons Boiler 3 9/9/2009

FLSugarCaneGrowersCoop Boiler No. 8 Sample #1 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #2 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #3 1/19/2005

GAGPMadisonPly 800 Wood Waste Boiler 1 8/11/2009

GAGPMadisonPly 800 Wood Waste Boiler 2 8/12/2009

Cr 3x RDL 

Concentration 

(μg/dscm)

Pb 3x RDL 

Concentration 

(μg/dscm)

Mn 3

Concen

(μg/d

0.9 1.832433397 1.7179

1.034484442 2.873567895 2.0114

0.9 2.25677721 1.5441

1.909700942 1.331003687 27.4882.038472975 7.350857093 24.7081.393346485 2.21668759 58.267

0.23 0.23 0.87540.23 0.23 1.12650.23 0.23 0.5789

4.0925645 8.989067575 2670.1

4.861010087 8.542510374 3311.34.744506404 9.235939707 3169.0.490021045 0.534939641 6.32941.175375618 0.705225371 7.84980.960713694 0.45 4.76590.513052759 0.931388085 19.8150.528577232 0.717354815 17.5601.015640728 0.746105304 18.5583.365306988 6.490053652 351.050.653102582 0.760807778 31.870.738113911 0.366621472 12.7218.184774824 1.483292113 4.1543

8.14256228 0.3133518 5.4899
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

GAGPMadisonPly 800 Wood Waste Boiler 3 8/12/2009

GATempleInlandRome WF 1 7/27/2009GATempleInlandRome WF 2 7/28/2009GATempleInlandRome WF 3 7/28/2009

HIPuuneneSugarMill Boiler 1 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 1 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 1 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 1 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 2 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 2 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 2 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 3 Sample #1 5/23/2006HIPuuneneSugarMill Boiler 3 Sample #2 5/24/2006HIPuuneneSugarMill Boiler 3 Sample #3 5/25/2006HIPuuneneSugarMill Boiler 3 Sample #1 7/16/2007HIPuuneneSugarMill Boiler 3 Sample #2 7/17/2007HIPuuneneSugarMill Boiler 3 Sample #3 7/17/2007

IARoquetteAmericaCirculating Fluidized Bed Boiler (121)1 6/3/2009

IARoquetteAmericaCirculating Fluidized Bed Boiler (121)2 6/3/2009IARoquetteAmericaCirculating Fluidized Bed Boiler (121)3 6/4/2009

IAUofNorthernIowa Boiler #3 4 10/6/2009

Cr 3x RDL 

Concentration 

(μg/dscm)

Pb 3x RDL 

Concentration 

(μg/dscm)

Mn 3

Concen

(μg/d

10.16503384 0.234788383 7.60242.952245104 4.207770645 86.0722.986170071 2.721032322 96.5952.437931921 2.344996573 77.412

#N/A #N/A #N#N/A #N/A #N#N/A #N/A #N#N/A #N/A #N#N/A #N/A #N#N/A #N/A #N

2.5 15 3.56292.5 15 3.16652.5 15 2.1627

#VALUE! #VALUE! #VA
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

IAUofNorthernIowa Boiler #3 5 10/6/2009IAUofNorthernIowa Boiler #3 6 10/7/2009

IDAmalgamatedSugarCoTwinFalls S-B1 Sample #1 9/26/2006IDAmalgamatedSugarCoTwinFalls S-B1 Sample #2 9/26/2006IDAmalgamatedSugarCoTwinFalls S-B1 Sample #3 9/26/2006

IDPotlatch PB-1 CE Sample #1 7/20/2006IDPotlatch PB-1 CE Sample #2 7/20/2006IDPotlatch PB-1 CE Sample #3 7/20/2006IDPotlatch PB-1 CE M29-R1 7/28/2009IDPotlatch PB-1 CE M29-R2 7/28/2009IDPotlatch PB-1 CE M29-R3 7/29/2009IDPotlatch PB-2 Riley Sample #1 7/27/2006IDPotlatch PB-2 Riley Sample #2 7/27/2006IDPotlatch PB-2 Riley Sample #3 7/27/2006

IDTASCONampa Babcock and Wilcox (B&W) #1Sample #1 12/4/2006

IDTASCONampa Babcock and Wilcox (B&W) #1Sample #2 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #1Sample #3 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #2Sample #1 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #2Sample #2 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #2Sample #3 12/4/2006

ILPolyOne B1 Sample #1 11/14/2006ILPolyOne B1 Sample #2 11/14/2006ILPolyOne B1 Sample #3 11/14/2006ILPolyOne B1 1 9/9/2009ILPolyOne B1 2 9/9/2009ILPolyOne B1 3 9/10/2009

Cr 3x RDL 

Concentration 

(μg/dscm)

Pb 3x RDL 

Concentration 

(μg/dscm)

Mn 3

Concen

(μg/d

#VALUE! #VALUE! #VA#VALUE! #VALUE! #VA

67.48261447 23 29.278

3.8 23 23.1033.8 23 38.014

0.287797768 0.345357322 3.7360.268948448 0.848222027 4.04040.745551071 0.346461968 3.9075

3.8 2.316948003 4.16263.8 1.501599821 4.46723.8 1.254449254 3.30513.8 2.316948003 4.16263.8 1.501599821 4.46723.8 1.254449254 3.3051

0.949441391 1.350316645 5.1480

#DIV/0! #DIV/0! #DI#DIV/0! #DIV/0! #DI

0.869529567 0.910545112 1.9687

0.96992113 0.79610783 2.2531

1.031860523 0.799478711 2.4517
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

INSABICInnovativePlastics 01-001 BW1 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #3 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #3 6/28/2006

INTateLyleSagamore 31B1 M29-1 9/1/2009INTateLyleSagamore 31B1 M29-2 9/2/2009INTateLyleSagamore 31B1 M29-3 9/3/2009

MNHibbing Unit 1A Sample #1 9/21/2004MNHibbing Unit 1A Sample #2 9/21/2004MNHibbing Unit 1A Sample #3 9/21/2004MNHibbing Unit 2A Sample #1 9/22/2004MNHibbing Unit 2A Sample #2 9/22/2004MNHibbing Unit 2A Sample #3 9/22/2004

MSGPNewAugusta AA-015 Power Boiler Sample #1 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #2 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #3 7/12/2006

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #1 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #2 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #3 8/5/2009

NDCargillWestFargo Foster Wheeler Boiler (EU43) 1 8/26/2009

NDCargillWestFargo Foster Wheeler Boiler (EU43) 2 8/26/2009NDCargillWestFargo Foster Wheeler Boiler (EU43) 3 8/27/2009

OKGPMuskogeeMill B-4 Sample #1 4/16/2003OKGPMuskogeeMill B-4 Sample #2 4/16/2003

Cr 3x RDL 

Concentration 

(μg/dscm)

Pb 3x RDL 

Concentration 

(μg/dscm)

Mn 3

Concen

(μg/d

6.313812275 23 4.58135.123709449 23 2.36296.445310785 23 4.07936.313812275 23 4.58135.123709449 23 2.36296.445310785 23 4.07936.510916264 2.544043817 9.99917.180091503 2.630250251 11.0553.591490309 1.737340492 6.3716

7.5 45 3.68727.5 45 3.50457.5 45 3.27947.5 45 5.62127.5 45 5.94407.5 45 8.2776

1.408298289 2.278882686 42.4050.501868142 0.7877424 8.68740.823690263 0.702728756 9.25641.642811587 2.204677369 47.2601.298403188 2.032989968 69.5900.986469047 1.438469164 28.446

1.9 11 3.48161.9 11 4.67171.9 11 2.8070

28.78719862 1.337996556 6.08188.247892192 1.072225985 4.9487
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

OKGPMuskogeeMill B-4 Sample #3 4/16/2003

SCMarlboroPaper Hogged Fuel Boiler Sample #1 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #2 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #3 7/14/2009

TNBowaterNewsprint Bubbling Fluidized Bed BoilerSample #1 10/6/2005TNBowaterNewsprint Bubbling Fluidized Bed BoilerSample #2 10/6/2005TNBowaterNewsprint Bubbling Fluidized Bed BoilerSample #3 10/6/2005TNBowaterNewsprint Bubbling Fluidized Bed Boiler 1 8/4/2009

TNBowaterNewsprint Bubbling Fluidized Bed Boiler 2 8/4/2009TNBowaterNewsprint Bubbling Fluidized Bed Boiler 3 8/5/2009

TNEastman_NO_CBIDATA Boiler 30 1 8/26/2009TNEastman_NO_CBIDATA Boiler 30 2 8/27/2009TNEastman_NO_CBIDATA Boiler 30 3 8/27/2009

TXDibollTemple-Inland PB-44 Sample #1 6/29/2007TXDibollTemple-Inland PB-44 Sample #2 6/29/2007

VAGeorgiaPacificBrooknealGladys 5600 Sample #1 7/6/2006VAGeorgiaPacificBrooknealGladys 5600 Sample #2 7/6/2006VAGeorgiaPacificBrooknealGladys 5600 Sample #3 7/6/2006

VAUniversityofVirginia 7103-1-01R M29-1 9/17/2009VAUniversityofVirginia 7103-1-01R M29-2 9/17/2009VAUniversityofVirginia 7103-1-01R M29-3 9/18/2009

VAVirginiaPolytechnic Boiler 11 Sample #1 2/27/2007VAVirginiaPolytechnic Boiler 11 Sample #1VAVirginiaPolytechnic Boiler 11 Sample #2VAVirginiaPolytechnic Boiler 7 Sample #3 2/28/2007VAVirginiaPolytechnic Boiler 7 Sample #1

Cr 3x RDL 

Concentration 

(μg/dscm)

Pb 3x RDL 

Concentration 

(μg/dscm)

Mn 3

Concen

(μg/d

52.9314781 1.014519997 8.8219

0.3 1.342178436 1.9173

0.913524971 1.166517101 2.79170.395680203 0.432767696 2.3042

10.6823186 2.815494824 63.348

10.59840468 2.874870904 86.2468.966611654 2.241652914 58.2824.856360092 9.45419195 544.355.231963677 9.450375196 613.583.084191886 5.361402876 328.481.924695011 1.111321074 2.6684

1.5932244 1.182243699 2.5823

1.06547989 0.666191835 1.4882

0.45 1.30375962 44.630.45 0.76479472 251.28

1.05193617 0.909173404 72.809

0.9 1.675256247 35.808

0.985087039 1.014713716 85.8432.880981602 0.66353277 7.57310.995841925 0.790049868 6.30370.970539063 0.23 3.93442.182588377 12.24368905 19.620

#DIV/0! #DIV/0! #DI#DIV/0! #DIV/0! #DI

1.22754663 5.468162262 11.324

#DIV/0! #DIV/0! #DI
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

VAVirginiaPolytechnic Boiler 7 Sample #1

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #1 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #2 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #3 8/12/2009

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #1 7/21/2005

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #2 7/21/2005WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #3 7/22/2005WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #1 8/20/2009WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #2 8/20/2009WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #3 8/21/2009

WINewPageBiron B24 Sample #1 9/12/2007WINewPageBiron B24 Sample #2 9/12/2007WINewPageBiron B24 Sample #3 9/12/2007WINewPageBiron B24 1 9/22/2009WINewPageBiron B24 2 9/22/2009WINewPageBiron B24 3 9/23/2009

WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #1 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #2 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #3 9/18/2003

WVMountainStateCarbonFollansbee S1 Sample #1 10/19/2009WVMountainStateCarbonFollansbee S1 Sample #2 10/19/2009WVMountainStateCarbonFollansbee S1 Sample #3 10/20/2009

WVPPGMartinsville R011-Boiler 3 1 7/22/2009WVPPGMartinsville R011-Boiler 3 2 7/23/2009WVPPGMartinsville R011-Boiler 3 3 7/23/2009

SCMilliken-Dewey D30 Sample #1 8/12/2009

Cr 3x RDL 

Concentration 

(μg/dscm)

Pb 3x RDL 

Concentration 

(μg/dscm)

Mn 3

Concen

(μg/d

#DIV/0! #DIV/0! #DI

#VALUE! #VALUE! #VA#VALUE! #VALUE! #VA#VALUE! #VALUE! #VA

15.68636208 2.430524235 6.4038

11.6279325 2.357886313 9.4476

6.972800666 1.317694614 36.1582.076725451 0.720612383 2.77571.120417368 0.879807624 1.36801.541711789 0.855709799 6.79301.265558927 4.449142716 1.58330.588057177 4.091639936 26.131

0.45 3.517424006 30.365

0.358714292 0.80394203 7.74400.525319212 1.057769454 2.18680.477907364 1.120610372 2.2365

#VALUE! #VALUE! #VA#VALUE! #VALUE! #VA#VALUE! #VALUE! #VA

8.455043149 2.37710218 6.0887

11.0159746 2.526860152 17.233

12.12963193 2.377683531 6.3232

1.9 0.84956254 2.5282

1.940590104 0.781222569 3.3004

1.9 0.718509255 3.2603

0.452966628 0.442035307 1.4575
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

SCMilliken-Dewey D30 Sample #2 8/12/2009SCMilliken-Dewey D30 Sample #3 8/12/2009

MNGPDuluth EU33 Boiler #3 1 9/10/2009MNGPDuluth EU33 Boiler #3 2 9/10/2009MNGPDuluth EU33 Boiler #3 3 9/10/2009

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 1 11/17/2009TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 2 11/17/2009TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 3 11/18/2009

Cr 3x RDL 

Concentration 

(μg/dscm)

Pb 3x RDL 

Concentration 

(μg/dscm)

Mn 3

Concen

(μg/d

0.504869868 0.341758065 1.24530.435879099 0.312275343 0.98980.919432851 0.794685681 6.40130.906794379 0.556928831 7.24000.883180811 0.516208175 3.08011.213559327 5.832709227 2.74691.222337564 21.03096168 1.31941.101564965 6.707818597 3.8114
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

AKDoyonUtilities_AK 4 Sample #1 8/17/2005AKDoyonUtilities_AK 4 Sample #2 8/17/2005AKDoyonUtilities_AK 4 Sample #3 8/17/2005AKDoyonUtilities_AK 7 Sample #1 8/16/2005AKDoyonUtilities_AK 7 Sample #2 8/16/2005AKDoyonUtilities_AK 7 Sample #3 8/16/2005

ALIPCourtland No. 3 Combination Boier / 11Cu301 Sample #1 7/7/2009

ALIPCourtland No. 3 Combination Boier / 11Cu301 Sample #2 7/7/2009ALIPCourtland No. 3 Combination Boier / 11Cu301 Sample #3 7/8/2009

ARAnthonyForestProducts SN-12 1 9/1/2009ARAnthonyForestProducts SN-12 2 9/1/2009ARAnthonyForestProducts SN-12 3 9/2/2009

ARLeolaLumberMill SN-01A Sample #1 6/14/2006ARLeolaLumberMill SN-01A Sample #2 6/14/2006ARLeolaLumberMill SN-01A Sample #3 6/14/2006ARLeolaLumberMill SN-01B Sample #1 6/14/2006ARLeolaLumberMill SN-01B Sample #2 6/14/2006ARLeolaLumberMill SN-01B Sample #3 6/14/2006

ARPotlatchForestWarren Wellons Boiler 1 9/9/2009ARPotlatchForestWarren Wellons Boiler 2 9/9/2009ARPotlatchForestWarren Wellons Boiler 3 9/9/2009

FLSugarCaneGrowersCoop Boiler No. 8 Sample #1 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #2 1/19/2005FLSugarCaneGrowersCoop Boiler No. 8 Sample #3 1/19/2005

GAGPMadisonPly 800 Wood Waste Boiler 1 8/11/2009

GAGPMadisonPly 800 Wood Waste Boiler 2 8/12/2009

Se 3x RDL 

Concentration 

(μg/dscm)

Total Metals, 

adjusting for 3x 

RDL 

Concentration at 

individual metals 

(μg/dscm) 

2.863177182 25.20589888

2.4 26.28369062.4 24.897221182.4 50.91604261

2.470876334 54.757320272.533357245 82.24394727

0.6 6.910150237

0.824682942 6.89419663

0.87878454 6.45857217

1.292883673 2697.8862191.725182011 3343.8245021.351361223 3201.431252.245929789 19.596655262.308773536 22.517604842.297358834 18.130941382.170607825 35.242094142.076553413 30.2994261

2.14847077 32.02505614

0.6 368.48653410.6 38.443177850.6 18.97586647

#VALUE!#VALUE!#VALUE!

1.69236181 26.88551003

1.429223462 36.79264755
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

GAGPMadisonPly 800 Wood Waste Boiler 3 8/12/2009

GATempleInlandRome WF 1 7/27/2009GATempleInlandRome WF 2 7/28/2009GATempleInlandRome WF 3 7/28/2009

HIPuuneneSugarMill Boiler 1 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 1 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 1 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 1 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 1 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #1 5/28/2006HIPuuneneSugarMill Boiler 2 Sample #2 5/29/2006HIPuuneneSugarMill Boiler 2 Sample #3 5/30/2006HIPuuneneSugarMill Boiler 2 Sample #1 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #2 7/25/2007HIPuuneneSugarMill Boiler 2 Sample #3 7/25/2007HIPuuneneSugarMill Boiler 3 Sample #1 5/23/2006HIPuuneneSugarMill Boiler 3 Sample #2 5/24/2006HIPuuneneSugarMill Boiler 3 Sample #3 5/25/2006HIPuuneneSugarMill Boiler 3 Sample #1 7/16/2007HIPuuneneSugarMill Boiler 3 Sample #2 7/17/2007HIPuuneneSugarMill Boiler 3 Sample #3 7/17/2007

IARoquetteAmericaCirculating Fluidized Bed Boiler (121)1 6/3/2009

IARoquetteAmericaCirculating Fluidized Bed Boiler (121)2 6/3/2009IARoquetteAmericaCirculating Fluidized Bed Boiler (121)3 6/4/2009

IAUofNorthernIowa Boiler #3 4 10/6/2009

Se 3x RDL 

Concentration 

(μg/dscm)

Total Metals, 

adjusting for 3x 

RDL 

Concentration at 

individual metals 

(μg/dscm) 

1.070573182 36.3358531

0.8 102.54478070.8 110.02480610.8 90.76687652

#N/A#N/A#N/A#N/A#N/A#N/A

27 74.0729571627 73.8762493227 72.67272974

#VALUE!
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

IAUofNorthernIowa Boiler #3 5 10/6/2009IAUofNorthernIowa Boiler #3 6 10/7/2009

IDAmalgamatedSugarCoTwinFalls S-B1 Sample #1 9/26/2006IDAmalgamatedSugarCoTwinFalls S-B1 Sample #2 9/26/2006IDAmalgamatedSugarCoTwinFalls S-B1 Sample #3 9/26/2006

IDPotlatch PB-1 CE Sample #1 7/20/2006IDPotlatch PB-1 CE Sample #2 7/20/2006IDPotlatch PB-1 CE Sample #3 7/20/2006IDPotlatch PB-1 CE M29-R1 7/28/2009IDPotlatch PB-1 CE M29-R2 7/28/2009IDPotlatch PB-1 CE M29-R3 7/29/2009IDPotlatch PB-2 Riley Sample #1 7/27/2006IDPotlatch PB-2 Riley Sample #2 7/27/2006IDPotlatch PB-2 Riley Sample #3 7/27/2006

IDTASCONampa Babcock and Wilcox (B&W) #1Sample #1 12/4/2006

IDTASCONampa Babcock and Wilcox (B&W) #1Sample #2 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #1Sample #3 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #2Sample #1 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #2Sample #2 12/4/2006IDTASCONampa Babcock and Wilcox (B&W) #2Sample #3 12/4/2006

ILPolyOne B1 Sample #1 11/14/2006ILPolyOne B1 Sample #2 11/14/2006ILPolyOne B1 Sample #3 11/14/2006ILPolyOne B1 1 9/9/2009ILPolyOne B1 2 9/9/2009ILPolyOne B1 3 9/10/2009

Se 3x RDL 

Concentration 

(μg/dscm)

Total Metals, 

adjusting for 3x 

RDL 

Concentration at 

individual metals 

(μg/dscm) 

#VALUE!#VALUE!

41 234.920546341 140.733918141 145.3842386

5.600987337 14.49750063

3.41357645 13.16565436

1.732309842 11.2203939811.42765879 33.4282832920.34667758 41.285536877.849697427 27.652471111.42765879 33.4282832920.34667758 41.285536877.849697427 27.379282443.164804636 20.61152766

#DIV/0!#DIV/0!

1.435544096 10.149792981.502090245 10.52250872

1.49236026 10.78790591
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

INSABICInnovativePlastics 01-001 BW1 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW1 Boiler Sample #3 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #1 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #2 6/28/2006INSABICInnovativePlastics 01-001 BW2 Boiler Sample #3 6/28/2006

INTateLyleSagamore 31B1 M29-1 9/1/2009INTateLyleSagamore 31B1 M29-2 9/2/2009INTateLyleSagamore 31B1 M29-3 9/3/2009

MNHibbing Unit 1A Sample #1 9/21/2004MNHibbing Unit 1A Sample #2 9/21/2004MNHibbing Unit 1A Sample #3 9/21/2004MNHibbing Unit 2A Sample #1 9/22/2004MNHibbing Unit 2A Sample #2 9/22/2004MNHibbing Unit 2A Sample #3 9/22/2004

MSGPNewAugusta AA-015 Power Boiler Sample #1 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #2 7/12/2006MSGPNewAugusta AA-015 Power Boiler Sample #3 7/12/2006

MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #1 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #2 8/5/2009MSWeyerhaeuserBruce AA-002 No. 2 Boiler Sample #3 8/5/2009

NDCargillWestFargo Foster Wheeler Boiler (EU43) 1 8/26/2009

NDCargillWestFargo Foster Wheeler Boiler (EU43) 2 8/26/2009NDCargillWestFargo Foster Wheeler Boiler (EU43) 3 8/27/2009

OKGPMuskogeeMill B-4 Sample #1 4/16/2003OKGPMuskogeeMill B-4 Sample #2 4/16/2003

Se 3x RDL 

Concentration 

(μg/dscm)

Total Metals, 

adjusting for 3x 

RDL 

Concentration at 

individual metals 

(μg/dscm) 

33.10901559 82.0625531530.71862698 75.7956435225.69965693 73.9279510533.10901559 82.0625531530.71862698 75.7956435225.69965693 73.9279510514.20861586 52.4317814114.05604923 58.884607119.968433735 32.78985726

81 215.148198981 214.953842281 214.711009381 217.114297781 217.415762881 219.7427179

1.79237964 57.36841945

2.223466451 21.546889822.016025118 22.00596526

0.8 57.991726470.8 79.847075910.8 37.75841138

20 55.6710072320 57.0457893920 55.01498465

1.2 50.010839841.2 25.11364271
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

OKGPMuskogeeMill B-4 Sample #3 4/16/2003

SCMarlboroPaper Hogged Fuel Boiler Sample #1 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #2 7/14/2009SCMarlboroPaper Hogged Fuel Boiler Sample #3 7/14/2009

TNBowaterNewsprint Bubbling Fluidized Bed BoilerSample #1 10/6/2005TNBowaterNewsprint Bubbling Fluidized Bed BoilerSample #2 10/6/2005TNBowaterNewsprint Bubbling Fluidized Bed BoilerSample #3 10/6/2005TNBowaterNewsprint Bubbling Fluidized Bed Boiler 1 8/4/2009

TNBowaterNewsprint Bubbling Fluidized Bed Boiler 2 8/4/2009TNBowaterNewsprint Bubbling Fluidized Bed Boiler 3 8/5/2009

TNEastman_NO_CBIDATA Boiler 30 1 8/26/2009TNEastman_NO_CBIDATA Boiler 30 2 8/27/2009TNEastman_NO_CBIDATA Boiler 30 3 8/27/2009

TXDibollTemple-Inland PB-44 Sample #1 6/29/2007TXDibollTemple-Inland PB-44 Sample #2 6/29/2007

VAGeorgiaPacificBrooknealGladys 5600 Sample #1 7/6/2006VAGeorgiaPacificBrooknealGladys 5600 Sample #2 7/6/2006VAGeorgiaPacificBrooknealGladys 5600 Sample #3 7/6/2006

VAUniversityofVirginia 7103-1-01R M29-1 9/17/2009VAUniversityofVirginia 7103-1-01R M29-2 9/17/2009VAUniversityofVirginia 7103-1-01R M29-3 9/18/2009

VAVirginiaPolytechnic Boiler 11 Sample #1 2/27/2007VAVirginiaPolytechnic Boiler 11 Sample #1VAVirginiaPolytechnic Boiler 11 Sample #2VAVirginiaPolytechnic Boiler 7 Sample #3 2/28/2007VAVirginiaPolytechnic Boiler 7 Sample #1

Se 3x RDL 

Concentration 

(μg/dscm)

Total Metals, 

adjusting for 3x 

RDL 

Concentration at 

individual metals 

(μg/dscm) 

1.2 78.4068763

1.419349354 10.961619242.088353928 12.95261058

0.8 9.875304283

9.108953841 104.5968523

2.4 120.07574352.4 89.83489653

2.26589855 570.7878293

2.673232207 641.74248732.327190169 347.02387041.587601535 13.384206781.510165308 12.14810241.494661169 10.07864467

1.2 56.531195591.2 262.63719522.4 95.369017022.4 58.515532612.4 108.0089933

0.862952999 16.533733590.928147169 13.60018986

0.6 10.61415488

4.320343006 50.77969037

#DIV/0!#DIV/0!

2.317745386 32.09921565

#DIV/0!
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

VAVirginiaPolytechnic Boiler 7 Sample #1

WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #1 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #2 8/11/2009WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Sample #3 8/12/2009

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #1 7/21/2005

WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #2 7/21/2005WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #3 7/22/2005WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #1 8/20/2009WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #2 8/20/2009WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 Sample #3 8/21/2009

WINewPageBiron B24 Sample #1 9/12/2007WINewPageBiron B24 Sample #2 9/12/2007WINewPageBiron B24 Sample #3 9/12/2007WINewPageBiron B24 1 9/22/2009WINewPageBiron B24 2 9/22/2009WINewPageBiron B24 3 9/23/2009

WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #1 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #2 9/18/2003WINewPage-WisconsinRapids Power Boiler 2 - B20 Sample #3 9/18/2003

WVMountainStateCarbonFollansbee S1 Sample #1 10/19/2009WVMountainStateCarbonFollansbee S1 Sample #2 10/19/2009WVMountainStateCarbonFollansbee S1 Sample #3 10/20/2009

WVPPGMartinsville R011-Boiler 3 1 7/22/2009WVPPGMartinsville R011-Boiler 3 2 7/23/2009WVPPGMartinsville R011-Boiler 3 3 7/23/2009

SCMilliken-Dewey D30 Sample #1 8/12/2009

Se 3x RDL 

Concentration 

(μg/dscm)

Total Metals, 

adjusting for 3x 

RDL 

Concentration at 

individual metals 

(μg/dscm) 

#DIV/0!

#VALUE!#VALUE!#VALUE!

2.4 46.774000832.4 48.961448992.4 65.622044420.6 11.040742330.6 8.8061821660.6 14.66187663

6.496535824 24.757567839.254162942 50.926037677.116721803 52.028131836.393554728 20.518564146.964639326 16.29643836

5.06158046 14.39031079

#VALUE!#VALUE!#VALUE!

6.467275266 131.98000076.984355027 61.9539263

5.98112938 48.73882033

13.69161058 27.0027789318.15926928 30.4840673946.51402019 59.95720883

0.8 9.888246985
es and Oxygen Percentages Used to Estimate TSM8 3x RDL

FacilityID UnitID Run Number Test Date

SCMilliken-Dewey D30 Sample #2 8/12/2009SCMilliken-Dewey D30 Sample #3 8/12/2009

MNGPDuluth EU33 Boiler #3 1 9/10/2009MNGPDuluth EU33 Boiler #3 2 9/10/2009MNGPDuluth EU33 Boiler #3 3 9/10/2009

TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 1 11/17/2009TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 2 11/17/2009TNMilanArmyAmmunitionPlant D88L-1, Source #27-0010-86 3 11/18/2009

Se 3x RDL 

Concentration 

(μg/dscm)

Total Metals, 

adjusting for 3x 

RDL 

Concentration at 

individual metals 

(μg/dscm) 

0.8 9.1163330280.8 8.5342611870.8 14.894832210.8 16.514467920.8 11.223121230.6 14.906138410.6 28.695438390.6 16.73323786
Table D-2a: Summary of TSM8 3x RDL for Existing Sources

Fuel Category Combustor Design Average Sample Time (hrs) Average Stack O2 (%) Concentration (μg/dscm) Fd Fact

(dscf/MM

Coal/Fossil Solid N/A 2 7.03 1.01E+01 9,780 

Dutch Oven/Pile Burner 3 9.64 1.90E+01 9,420 

FB 3 8.82 6.46E+00 9,420 

Fuel Cell 4 10.72 1.12E+01 9,420 

Suspension Burner 2 12.1 5.65E+01 9,240 

Suspension/Grate

Wet Biomass Stoker/SlopedGrate/Other 3 10.1 9.88E+00 9,420 

Dry Biomass Stoker/SlopedGrate/Other

Process Gas N/A 4 4.67 4.87E+01 8,710 

Heavy Liquid N/A 3 10.11 8.53E+00 9,190 

Light Liquid N/A 4 4.63 1.49E+01 9,190 

Non-Continental 

Liquid N/A

Table D-2b: Summary of TSM8 3x RDL for New Sources

Fuel Category Combustor Design Average Sample Time (hrs) Average Stack O2 (%) Concentration (μg/dscm) Fd Fact

(dscf/MM

Coal/Fossil Solid N/A 4 8.07 1.01E+01 9,780 

Dutch Oven/Pile Burner

FB 4 12.72 5.50E+01 9,420 

Fuel Cell 4 13.33 1.12E+01 9,420 

Suspension Burner

Suspension/Grate

Wet Biomass Stoker/SlopedGrate/Other

Dry Biomass Stoker/SlopedGrate/Other

Process Gas N/A 4 4.67 4.87E+01 8,710 

Heavy Liquid N/A 3 16.29 1.12E+01 9,190 

Light Liquid N/A 4 4.63 1.49E+01 9,190 

Non-Continental 

Liquid N/A

Biomass/Bio-Based 

Solid

N/A - No test reports for top performers in this subca

N/A - Unable to calculate 3x RDL based on data in availabl

N/A - No test reports for top performers in this subca

Biomass/Bio-Based 

Solid

N/A - Unable to calculate 3x RDL based on data in availabl

N/A - No test reports for top performers in this subcaN/A - No test reports for top performers in this subca

N/A - Unable to calculate 3x RDL based on data in availablN/A - Unable to calculate 3x RDL based on data in availablN/A - Unable to calculate 3x RDL based on data in availabl