Instructionsfor completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls(example:8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet.If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example:"ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of

measure.Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet.If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example:"ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

2837 Eastlake 3 subbituminousFuel Type 2 Fuel Type 3 Other Fuel Description

bituminousEIA

Facility Code Facility Name Boiler ID Basis Analyte

2837 Eastlake 3 As Received Higher Heating Value 2837 Eastlake 3 As Received % Moisture 2837 Eastlake 3 As Received % Ash 2837 Eastlake 3 As Received % Sulfur 2837 Eastlake 3 Dry basis Higher Heating Value 2837 Eastlake 3 Dry basis % Ash 2837 Eastlake 3 Dry basis % Sulfur 2837 Eastlake 3 Dry basis Antimony 2837 Eastlake 3 Dry basis Arsenic 2837 Eastlake 3 Dry basis Beryllium 2837 Eastlake 3 Dry basis Cadmium 2837 Eastlake 3 Dry basis Chlorine 2837 Eastlake 3 Dry basis Chromium 2837 Eastlake 3 Dry basis Cobalt 2837 Eastlake 3 Dry basis Fluorine 2837 Eastlake 3 Dry basis Lead 2837 Eastlake 3 Dry basis Manganese 2837 Eastlake 3 Dry basis Mercury 2837 Eastlake 3 Dry basis Nickel 2837 Eastlake 3 Dry basis SeleniumAnalysis Method for each Analyte

(example: ASTM D5865-04) ASTM D5865-07 ASTM D5142-09 ASTM D5142-09 ASTM D4239-08 ASTM D5865-07 ASTM D5142-09 ASTM D4239-08 ASTM D6357-04A SW-846 3050B/6020 ASTM D6357-04A ASTM D6357-04A SW-846 5050/9076 ASTM D6357-04A ASTM D6357-04A SW-846 5050/9076 ASTM D6357-04A ASTM D6357-04A ASTM D6414-01A ASTM D6357-04A SW-846 3050B/6020EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 2837 Eastlake 3 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units AA26746 6/4/2010 8/26/2010 10793 BTU/lb AA26747 6/4/2010 8/26/2010 11701 BTU/lb AA26748 6/4/2010 8/26/2010 11644 BTU/lb AA26749 6/4/2010 8/26/2010 11800 BTU/lb AA30303 7/20/2010 8/26/2010 10262 BTU/lb AA30304 7/20/2010 8/26/2010 11163 BTU/lb AA30305 7/20/2010 8/26/2010 10981 BTU/lb Fuel Testing ResultsMercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 7.13 7.25 1.3 12648 BTU/lb 8.5 1.52 5.91 7.61 1.42 13422 BTU/lb 8.73 1.63 6.98 7.4 1.45 13381 BTU/lb 8.51 1.67 7.04 7.4 1.42 13549 BTU/lb 8.5 1.63 9.55 6.8 1.01 12902 BTU/lb 8.55 1.27 9.12 7.11 1.44 13343 BTU/lb 8.49 1.72 10.2 6.93 1.31 13157 BTU/lb 8.31 1.57Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 662 mg/kg 0.215 mg/kg <1 mg/kg 7.5 mg/kg <1 744 mg/kg 0.188 mg/kg <1 mg/kg 7.4 mg/kg <1 747 mg/kg 0.197 mg/kg <1 mg/kg 10 mg/kg <1 757 mg/kg 0.173 mg/kg <1 mg/kg 7.2 mg/kg <1 424 mg/kg 0.178 mg/kg <1 mg/kg 4.2 mg/kg <1 668 mg/kg 0.193 mg/kg <1 mg/kg 6.2 mg/kg <1 599 mg/kg 0.069 mg/kg <1 mg/kg 5.1 mg/kg <1Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units mg/kg <1 mg/kg 3.67 mg/kg 3.08 mg/kg 8.07 mg/kg mg/kg <1 mg/kg 3.99 mg/kg 3.31 mg/kg 11 mg/kg mg/kg <1 mg/kg 3.84 mg/kg 2.72 mg/kg 8.21 mg/kg mg/kg <1 mg/kg 1.71 mg/kg 2.75 mg/kg 9.88 mg/kg mg/kg <1 mg/kg 3.3 mg/kg 2.57 mg/kg 10.4 mg/kg mg/kg <1 mg/kg 3.99 mg/kg 3.22 mg/kg 12.9 mg/kg mg/kg <1 mg/kg 4.07 mg/kg 3 mg/kg 13.2 mg/kgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 4.51 mg/kg <2.1 mg/kg 66.9 mg/kg 2 mg/kg 14.7 4.58 mg/kg <2.2 mg/kg 68 mg/kg 2.08 mg/kg 12.8 5.29 mg/kg <2.1 mg/kg 70.7 mg/kg 2.22 mg/kg 13 4.51 mg/kg <2.1 mg/kg 63.8 mg/kg 2.02 mg/kg 12.9 3.42 mg/kg <2.2 mg/kg 53.7 mg/kg 1.55 mg/kg 20.5 4.11 mg/kg <2.1 mg/kg 60.6 mg/kg 2.01 mg/kg 16.3 3.52 mg/kg <2.1 mg/kg 54.6 mg/kg 1.83 mg/kg 16.5 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 38.97 8.5 52.57 74.23 6.08 1.3 1.52 37.89 8.73 53.42 74.57 6.01 1.34 1.63 38.56 8.51 52.91 74.61 5.75 1.34 1.67 37.94 8.5 53.58 75.03 5.8 1.37 1.63 40.88 8.55 50.6 73.46 6.61 1.27 1.27 39.34 8.49 52.14 73.86 5.99 1.31 1.72 40.25 8.31 51.43 74.13 5.91 1.32 1.57 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen

17.21 15.64 15.02 14.41 22.55 17.25 16.35EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 2837 Eastlake 3 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units AA26750 6/4/2010 8/12/2010 11760 BTU/lb AA26751 6/4/2010 8/12/2010 11569 BTU/lb AA26752 6/4/2010 8/12/2010 11556 BTU/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 6.71 7.29 1.41 13616 BTU/lb 8.44 1.63 7.92 7.19 1.27 13673 BTU/lb 8.5 1.5 7.67 7.15 1.31 13493 BTU/lb 8.34 1.53Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 694 mg/kg 0 0 0 0 0 0 0 605 mg/kg 0 0 0 0 0 0 0 651 mg/kg 0 0 0 0 0 0 0Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 0 0 0 0 0 0 0 1.04 mg/kg 0 0 0 0 0 0 0 1.04 mg/kg 0 0 0 0 0 0 0 1.04 mg/kgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 0 0 0 0 66 mg/kg 0 0 0 0 0 0 63.9 mg/kg 0 0 0 0 0 0 64.4 mg/kg 0 0Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

13.6 38.26 8.44 53.36 74.85 5.92 1.34 1.63 15.4 39.06 8.5 52.45 74.33 5.97 1.31 1.5 14.4 38.91 8.34 52.72 75.04 5.97 1.34 1.53 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 15.84 17.22 15.59EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 2837 Eastlake 3 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units AA26748 6/4/2010 8/26/2010 11644 BTU/lb AA26749 6/4/2010 8/26/2010 11800 BTU/lb AA26750 6/4/2010 8/12/2010 11760 BTU/lb AA26751 6/4/2010 8/12/2010 11569 BTU/lb AA26752 6/4/2010 8/12/2010 11556 BTU/lb AA28209 6/22/2010 8/12/2010 10838 BTU/lb AA28210 6/22/2010 8/12/2010 11167 BTU/lb AA28211 6/22/2010 8/12/2010 11381 BTU/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 6.98 7.4 1.45 13381 BTU/lb 8.51 1.67 7.04 7.4 1.42 13549 BTU/lb 8.5 1.63 6.71 7.29 1.41 13616 BTU/lb 8.44 1.63 7.92 7.19 1.27 13673 BTU/lb 8.5 1.5 7.67 7.15 1.31 13493 BTU/lb 8.34 1.53 8.77 6.4 1.01 13058 BTU/lb 7.7 1.22 8.49 7.28 1.08 13210 BTU/lb 8.62 1.28 8.19 6.49 1.19 13404 BTU/lb 7.64 1.41Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 747 mg/kg 0.197 mg/kg <1 mg/kg 10 mg/kg <1 757 mg/kg 0.173 mg/kg <1 mg/kg 7.2 mg/kg <1 694 mg/kg 0 0 0 0 0 0 0 605 mg/kg 0 0 0 0 0 0 0 651 mg/kg 0 0 0 0 0 0 0 649 mg/kg 0 0 0 0 0 0 0 693 mg/kg 0 0 0 0 0 0 0 714 mg/kg 0 0 0 0 0 0 0Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units mg/kg <1 mg/kg 3.84 mg/kg 2.72 mg/kg 8.21 mg/kg mg/kg <1 mg/kg 1.71 mg/kg 2.75 mg/kg 9.88 mg/kg 0 0 0 0 0 0 0 1.04 mg/kg 0 0 0 0 0 0 0 1.04 mg/kg 0 0 0 0 0 0 0 1.04 mg/kg 0 0 0 0 0 0 0 1.04 mg/kg 0 0 0 0 0 0 0 1.04 mg/kg 0 0 0 0 0 0 0 1.04 mg/kgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 5.29 mg/kg <2.1 mg/kg 70.7 mg/kg 2.22 mg/kg 13 4.51 mg/kg <2.1 mg/kg 63.8 mg/kg 2.02 mg/kg 12.9 0 0 0 0 66 mg/kg 0 0 13.6 0 0 0 0 63.9 mg/kg 0 0 15.4 0 0 0 0 64.4 mg/kg 0 0 14.4 0 0 0 0 59.3 mg/kg 0 0 17 0 0 0 0 59.1 mg/kg 0 0 15.5 0 0 0 0 57.4 mg/kg 0 0 15.1 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 38.56 8.51 52.91 74.61 5.75 1.34 1.67 15.02 37.94 8.5 53.58 75.03 5.8 1.37 1.63 14.41 38.26 8.44 53.36 74.85 5.92 1.34 1.63 15.84 39.06 8.5 52.45 74.33 5.97 1.31 1.5 17.22 38.91 8.34 52.72 75.04 5.97 1.34 1.53 15.59 39.99 7.7 52.32 74.63 6.25 1.3 1.22 18.81 38.2 8.62 53.15 75.56 6.03 1.37 1.28 15.39 38.07 7.64 54.28 76.02 5.98 1.38 1.41 15.7 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 2837 Eastlake 3

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bituminous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm