P2694 - TEQ

Project ID: P-10124 

Sample Summary

Part 1 Method 23

Analyte 0_8209_

MB001

Plant 4 

Inlet-R1

Plant 4 

Inlet-R2

Plant 4 

Inlet-R3

Plant 4 

OutletR1

Plant 4 

OutletR2

Plant 4 

OutletR3

Plant 4 

OvenR1

Plant 4 

OvenR2

Plant 4 

OvenR13Blank

pg pg pg pg pg pg pg pg pg pg pg

2,3,7,8-TCDD (5.83) (3.27) (2.18) (3.37) (4) (3.66) (3.73) (3.05) (3.86) (4.82) (2.85)

1,2,3,7,8-PeCDD (5.77) (3.65) 3.34 (4.24) (4.05) (3.23) (4.12) (2.86) (4.57) (5.13) (2.53)

1,2,3,4,7,8-HxCDD (5.56) (2.67) (2.2) (3.44) (3.74) (3.41) (3.92) (2.45) (2.92) (3.87) (2.56)

1,2,3,6,7,8-HxCDD (5.59) (2.57) (2.32) (3.14) (3.64) (3.36) (3.55) [3.43] (3.12) (3.61) (2.42)

1,2,3,7,8,9-HxCDD (6.35) (2.76) (2.5) (3.9) (4.32) (3.79) (4.12) [4.47] (3.14) (3.98) (2.81)

1,2,3,4,6,7,8-HpCDD (7.09) [29.3] 13.6 [9.52] (5.42) (4.97) (3.8) 41.2 [13.9] 6.53 (2.64)

OCDD (9.71) 148 63.2 42.4 [19.7] 17.3 (7.51) 284 77.2 [28.4] (4.01)

2,3,7,8-TCDF (3.59) 9 [7.53] 4.56 (2.83) (2.11) (2.36) (2.3) (2.29) (3.09) (1.54)

1,2,3,7,8-PeCDF (3.39) 11.3 20.2 7.73 (2.19) (2.25) (2.37) (1.42) (1.9) (2.6) (1.58)

2,3,4,7,8-PeCDF (3.23) 9.67 10.5 [6.36] (2.23) (2.15) (2.05) (1.31) (1.69) (2.32) (1.44)

1,2,3,4,7,8-HxCDF (3.6) 9.72 13.8 9.07 (2.26) (2.24) (2.39) (1.54) (1.51) (2.37) (1.46)

1,2,3,6,7,8-HxCDF (3.18) 10.4 [10.7] [7.78] (2.18) (1.98) (2.15) (1.41) (1.34) (2.39) (1.33)

2,3,4,6,7,8-HxCDF (3.38) [11.9] 9.45 [6.39] (2.32) (2.2) (2.29) (1.43) (1.56) (2.46) (1.35)

1,2,3,7,8,9-HxCDF (4.65) (2.68) (1.97) (2.92) (3.03) (3.2) (2.94) (1.99) (1.92) (3.23) (1.84)

1,2,3,4,6,7,8-HpCDF (3.28) 29.4 23.1 21.5 [1.52] [1.71] 5.97 5.03 (2.36) (2.38) (1.59)

1,2,3,4,7,8,9-HpCDF (4.34) (3.14) [2.36] (2.96) (4.23) (3.06) (3.18) (3.15) (3.12) (3.43) (2.21)

OCDF (8.04) 14.1 11.2 19 (5.81) (3.95) [7.79] (22) (3.56) (5.9) (3.18)

ITEF TEQ (ND=0; EMPC=0) 0.00 8.77 10.7 2.03 0.00 0.0173 0.0597 0.746 0.0772 0.0653 0.00

ITEF TEQ (ND=0; EMPC=EMPC) 0.00 10.3 12.6 6.72 0.0349 0.0344 0.0675 1.54 0.216 0.0937 0.00

ITEF TEQ (ND=DL/2; EMPC=0) 7.13 12.0 12.4 6.18 4.91 4.41 4.75 4.18 4.56 5.69 3.26

ITEF TEQ (ND=DL/2; EMPC=EMPC) 7.13 13.3 14.1 10.2 4.93 4.42 4.76 4.72 4.68 5.71 3.26

ITEF TEQ (ND=DL; EMPC=EMPC) 14.3 16.4 15.6 13.6 9.82 8.81 9.45 7.90 9.14 11.3 6.52

Checkcode 823-702 901-690 058-218 555-716 246-880 601-566 072-909 607-417 315-975 781-663 624-408

Lab ID MB1_8209_DF_SDS P2694_8209_001 P2694_8209_002 P2694_8209_003 P2694_8209_004 P2694_8209_005 P2694_8209_006 P2694_8209_007 P2694_8209_008 P2694_8209_009 P2694_8209_010

( ) = DL

[ ] = EMPC
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pg

WHO-2005-TEQ

Project ID: P-10124

P2694

ND=0; EMPC=0

ND=0; EMPC=EMPC

ND=DL/2; EMPC=0

ND=DL/2; EMPC=EMPC

ND=DL; EMPC=EMPC
 P2694 - WHO-2005-TEQ

Project ID: P-10124 

Sample Summary

Part 1 Method 23

Analyte 0_8209_

MB001

Plant 4 

Inlet-R1

Plant 4 

Inlet-R2

Plant 4 

Inlet-R3

Plant 4 

OutletR1

Plant 4 

OutletR2

Plant 4 

OutletR3

Plant 4 

OvenR1

Plant 4 

OvenR2

Plant 4 

OvenR13Blank

pg pg pg pg pg pg pg pg pg pg pg

2,3,7,8-TCDD (5.83) (3.27) (2.18) (3.37) (4) (3.66) (3.73) (3.05) (3.86) (4.82) (2.85)

1,2,3,7,8-PeCDD (5.77) (3.65) 3.34 (4.24) (4.05) (3.23) (4.12) (2.86) (4.57) (5.13) (2.53)

1,2,3,4,7,8-HxCDD (5.56) (2.67) (2.2) (3.44) (3.74) (3.41) (3.92) (2.45) (2.92) (3.87) (2.56)

1,2,3,6,7,8-HxCDD (5.59) (2.57) (2.32) (3.14) (3.64) (3.36) (3.55) [3.43] (3.12) (3.61) (2.42)

1,2,3,7,8,9-HxCDD (6.35) (2.76) (2.5) (3.9) (4.32) (3.79) (4.12) [4.47] (3.14) (3.98) (2.81)

1,2,3,4,6,7,8-HpCDD (7.09) [29.3] 13.6 [9.52] (5.42) (4.97) (3.8) 41.2 [13.9] 6.53 (2.64)

OCDD (9.71) 148 63.2 42.4 [19.7] 17.3 (7.51) 284 77.2 [28.4] (4.01)

2,3,7,8-TCDF (3.59) 9 [7.53] 4.56 (2.83) (2.11) (2.36) (2.3) (2.29) (3.09) (1.54)

1,2,3,7,8-PeCDF (3.39) 11.3 20.2 7.73 (2.19) (2.25) (2.37) (1.42) (1.9) (2.6) (1.58)

2,3,4,7,8-PeCDF (3.23) 9.67 10.5 [6.36] (2.23) (2.15) (2.05) (1.31) (1.69) (2.32) (1.44)

1,2,3,4,7,8-HxCDF (3.6) 9.72 13.8 9.07 (2.26) (2.24) (2.39) (1.54) (1.51) (2.37) (1.46)

1,2,3,6,7,8-HxCDF (3.18) 10.4 [10.7] [7.78] (2.18) (1.98) (2.15) (1.41) (1.34) (2.39) (1.33)

2,3,4,6,7,8-HxCDF (3.38) [11.9] 9.45 [6.39] (2.32) (2.2) (2.29) (1.43) (1.56) (2.46) (1.35)

1,2,3,7,8,9-HxCDF (4.65) (2.68) (1.97) (2.92) (3.03) (3.2) (2.94) (1.99) (1.92) (3.23) (1.84)

1,2,3,4,6,7,8-HpCDF (3.28) 29.4 23.1 21.5 [1.52] [1.71] 5.97 5.03 (2.36) (2.38) (1.59)

1,2,3,4,7,8,9-HpCDF (4.34) (3.14) [2.36] (2.96) (4.23) (3.06) (3.18) (3.15) (3.12) (3.43) (2.21)

OCDF (8.04) 14.1 11.2 19 (5.81) (3.95) [7.79] (22) (3.56) (5.9) (3.18)

WHO-2005 TEQ (ND=0; EMPC=0) 0.00 6.5 9.83 1.83 0.00 0.00518 0.0597 0.548 0.0232 0.0653 0.00

WHO-2005 TEQ (ND=0; EMPC=EMPC) 0.00 7.98 11.7 5.25 0.0211 0.0223 0.062 1.34 0.162 0.0738 0.00

WHO-2005 TEQ (ND=DL/2; EMPC=0) 8.2 10.6 11.5 6.84 5.67 4.97 5.55 4.55 5.45 6.71 3.73

WHO-2005 TEQ (ND=DL/2; EMPC=EMPC) 8.2 12.0 13.2 9.74 5.68 4.98 5.55 5.08 5.58 6.71 3.73

WHO-2005 TEQ (ND=DL; EMPC=EMPC) 16.4 16.0 14.7 14.2 11.3 9.93 11.0 8.83 11.0 13.4 7.46

Checkcode 823-702 901-690 058-218 555-716 246-880 601-566 072-909 607-417 315-975 781-663 624-408

Lab ID MB1_8209_DF_SDS P2694_8209_001 P2694_8209_002 P2694_8209_003 P2694_8209_004 P2694_8209_005 P2694_8209_006 P2694_8209_007 P2694_8209_008 P2694_8209_009 P2694_8209_010

( ) = DL

[ ] = EMPC
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Totals

Project ID: P-10124

P2694

Total PCDD/Fs (ND=0; EMPC=0)

Total PCDD/Fs (ND=0; EMPC=EMPC)

Total PCDD/Fs (2378-X ND=DL; EMPC=EMPC)
 P2694 - Totals

Project ID: P-10124 

Sample Summary

Part 2 Method 23

Analyte 0_8209_

MB001

Plant 4 

Inlet-R1

Plant 4 

Inlet-R2

Plant 4 

Inlet-R3

Plant 4 

OutletR1

Plant 4 

OutletR2

Plant 4 

OutletR3

Plant 4 

OvenR1

Plant 4 

OvenR2

Plant 4 

OvenR13Blank

pg pg pg pg pg pg pg pg pg pg pg

Totals

TCDDs 0 35.5 15.2 11.1 0 5.97 6.79 7.69 40.7 0 0

PeCDDs 0 18.1 58.2 23.8 0 0 0 33 68.9 0 0

HxCDDs 0 26.2 31.3 11.7 0 0 0 44.3 95.2 0 0

HpCDDs 0 0 30.1 11.3 7.75 0 0 97.9 0 15.5 0

OCDD 0 148 63.2 42.4 19.7 17.3 0 284 77.2 28.4 0

TCDFs 0 84.7 76.7 21.9 0 0 0 22.5 28.8 0 0

PeCDFs 0 78.7 105 25.7 0 0 0 0 0 0 0

HxCDFs 0 57.4 63.9 24.4 0 0 0 0 0 0 0

HpCDFs 0 37.4 23.1 26.4 0 0 5.97 5.03 0 0 0

OCDF 0 14.1 11.2 19 0 0 7.79 0 0 0 0

Total PCDD/Fs (ND=0; EMPC=0) 0.00 500 478 218 7.75 23.2 12.8 494 311 15.5 0.00

Total PCDD/Fs (ND=0; EMPC=EMPC) 0.00 710 575 325 29.0 25.0 20.5 576 408 63.6 0.00

Total PCDD/Fs (2378-X ND=DL; EMPC=EMPC) 86.6 731 586 349 81.2 70.5 71.0 621 447 115 37.4

Total 2378s (ND=0; EMPC=0) 0.00 242 168 104 0.00 17.3 5.97 330 77.2 6.53 0.00

Total 2378s (ND=0.5; EMPC=0) 43.3 256 177 121 31.6 41.1 34.2 355 98.3 36.4 18.7

Total 2378s (ND=1; EMPC=0) 86.6 269 185 138 63.1 64.9 62.4 380 119 66.2 37.4

Total 2378s (ND=0; EMPC=1) 0.00 283 189 134 21.2 19.0 13.8 338 91.1 35.0 0.00

Total 2378s (ND=0.5; EMPC=1) 43.3 294 195 146 47.3 41.8 39.0 360 110 60.8 18.7

Total 2378s (ND=1; EMPC=1) 86.6 304 200 158 73.5 64.5 64.2 383 130 86.5 37.4

Checkcode 823-702 901-690 058-218 555-716 246-880 601-566 072-909 607-417 315-975 781-663 624-408

Lab ID MB1_8209_DF_SDS P2694_8209_001 P2694_8209_002 P2694_8209_003 P2694_8209_004 P2694_8209_005 P2694_8209_006 P2694_8209_007 P2694_8209_008 P2694_8209_009 P2694_8209_010

( ) = DL

[ ] = EMPC
 P2694 - Others

Project ID: P-10124 

Sample Summary

Part 3 Method 23

Analyte 0_8209_

MB001

Plant 4 

Inlet-R1

Plant 4 

Inlet-R2

Plant 4 

Inlet-R3

Plant 4 

OutletR1

Plant 4 

OutletR2

Plant 4 

OutletR3

Plant 4 

OvenR1

Plant 4 

OvenR2

Plant 4 

OvenR13Blank

pg pg pg pg pg pg pg pg pg pg pg

Other PCDD/Fs (ND=0, EMPC=0)

Other TCDD 0 35.5 15.2 11.1 0 5.97 6.79 7.69 40.7 0 0

Other PeCDD 0 18.1 54.9 23.8 0 0 0 33 68.9 0 0

Other HxCDD 0 26.2 31.3 11.7 0 0 0 44.3 95.2 0 0

Other HpCDD 0 0 16.5 11.3 7.75 0 0 56.7 0 8.95 0

Other TCDF 0 75.7 76.7 17.4 0 0 0 22.5 28.8 0 0

Other PeCDF 0 57.8 74 18 0 0 0 0 0 0 0

Other HxCDF 0 37.2 37.5 15.3 0 0 0 0 0 0 0

Other HpCDF 0 7.98 0 4.94 0 0 0 0 0 0 0

Other PCDD/Fs (ND=0, EMPC=EMPC)

Other TCDD 0 35.5 27.3 15.1 0 5.97 6.79 41.1 54.1 7.1 0

Other PeCDD 0 36.4 60.6 23.8 0 0 0 45.3 82.4 0 0

Other HxCDD 0 36.9 41.6 25.3 0 0 0 64.8 95.2 7.97 0

Other HpCDD 0 37.4 16.5 11.3 7.75 0 0 56.7 43.5 8.95 0

Other TCDF 0 142 94.2 47.1 0 0 0 26.4 42.1 4.59 0

Other PeCDF 0 84.5 80.5 33.3 0 0 0 0 0 0 0

Other HxCDF 0 39.5 52.2 24.7 0 0 0 4.09 0 0 0

Other HpCDF 0 14.6 10.2 9.78 0 0 0 0 0 0 0

Checkcode 823-702 901-690 058-218 555-716 246-880 601-566 072-909 607-417 315-975 781-663 624-408

Lab ID MB1_8209_DF_SDS P2694_8209_001 P2694_8209_002 P2694_8209_003 P2694_8209_004 P2694_8209_005 P2694_8209_006 P2694_8209_007 P2694_8209_008 P2694_8209_009 P2694_8209_010

( ) = DL

[ ] = EMPC
 P2694 - TEQ overview

Project ID: P-10124 

TEQ Summary

Part 4

( ) = DL

[ ] = EMPC
Method Specification Limits: Tetra-Hexa ES: 40-130%, Hepta-Octa ES: 25-130% (F = fail)

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Mean Recoveries of Extraction Standards (N=11)

Project ID: P-10124

P2694 Mean Std. Dev.
Method Specification Limits: Tetra-Octa SS: 70-130% (F = fail)

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% Rec.

Mean Recoveries of Sampling Standards (N=11)

Project ID: P-10124

P2694 Mean Std. Dev.
0_8209_MB001 85.9 82.4 91.7 94.3 93.1 86.3 84.8 86.1 84.3 82.6 89.2

Plant 4 Inlet-R1 77.8 75.8 82.1 83.1 82.3 78.2 72.9 77.2 73.3 74.4 76.9

Plant 4 Inlet-R2 85.2 84.7 87.4 89 89.4 85.7 81.6 86 82.8 84.3 84.7

Plant 4 Inlet-R3 76.4 76.3 80.4 79.4 78 83.1 78.3 72.5 71.9 73.1 79.9

Plant 4 Outlet-R1 80.5 84.5 85.1 85.3 84.3 79.7 81.6 80.7 77.6 78.3 82.8

Plant 4 Outlet-R2 83.1 84.4 82.4 81.5 81.9 79.4 76.3 81 79.2 79.6 78.7

Plant 4 Outlet-R3 89.6 89 81.7 82.6 84.4 80.6 76.2 87.5 85.3 88.3 79.4

Plant 4 Oven-R1 82.4 80.9 73.6 77.5 74.1 69.7 4.68 85.8 78.6 78.9 70.7

Plant 4 Oven-R2 84.7 87.2 85.7 83.7 85.7 83.2 77.8 83.5 81.2 84.3 80.9

Plant 4 Oven-R13 82.8 84.4 86.6 88.1 89.1 85.1 81.9 83.4 81.2 83.5 84.4

Blank 81.5 86.4 84.4 88.3 85.9 85.9 80.1 81.7 78.9 82.7 83.6

Average 83 83 84 85 84 82 72 82 79 81 81

SD 4 4 5 5 5 5 23 4 4 5 5

Min 76.4 75.8 73.6 77.5 74.1 69.7 4.68 72.5 71.9 73.1 70.7

Max 89.6 89 91.7 94.3 93.1 86.3 84.8 87.5 85.3 88.3 89.2

Within M23 QC TRUE TRUE TRUE TRUE TRUE TRUE FALSE TRUE TRUE TRUE TRUE

13CHxCDD13CHxCDD13CHpCDD

Sample Number 13CTCDD

13CPeCDD13CHxCDD

Extraction Standard Percent Recoveries, %

13CPeCDF13CPeCDF13COCDD13CTCDF13CHxCDF
89.7 90.7 87.3 86.3 86.4 81.6 0_8209_MB001 91.4 98.2 95.7 96.7 96.1

78.5 80 77.2 76.2 73.3 73.7 Plant 4 Inlet-R1 95.7 100 98.9 96.8 99.4

86.8 85.9 83.3 80.9 83 80.5 Plant 4 Inlet-R2 96 98.6 99 95.6 102

80.3 79.3 78.9 77 80 74.5 Plant 4 Inlet-R3 101 102 103 99.7 108

82.6 82.6 80.1 82 77.3 77.1 Plant 4 Outlet-R1 99.3 102 100 99 96.5

79.5 78.1 76.4 78.6 72.4 74.4 Plant 4 Outlet-R2 99.1 102 102 96.9 94.8

80.9 79.3 78.4 77.6 76.3 72.3 Plant 4 Outlet-R3 92 103 101 94.6 99.5

72.4 73.2 72.1 52.9 68 11.9 Plant 4 Oven-R1 96.4 94.1 97.2 97 127

83.4 83.9 80.9 81.1 80.6 74.8 Plant 4 Oven-R2 95.2 95 99.7 96.8 98.3

86.2 85.8 84 83.7 82.1 78.6 Plant 4 Oven-R13 96.2 100 103 99.2 99.4

84.6 85.4 80 82.8 79.8 79.2 Blank 102 102 105 101 103

82 82 80 78 78 71 Average 97 100 100 98 102

5 5 4 9 5 20 SD 3 3 3 2 9

72.4 73.2 72.1 52.9 68 11.9 Min 91.4 94.1 95.7 94.6 94.8

89.7 90.7 87.3 86.3 86.4 81.6 Max 102 103 105 101 127

TRUE TRUE TRUE TRUE TRUE FALSE Min within M23 QC TRUE TRUE TRUE TRUE TRUE

13CHpCDF13COCDF13CHxCDF13CHxCDF13CHxCDF13CHpCDF

Sample Number

CS/SS Percent Recoveries, %

37ClTCDD13CPeCDD13CHxCDF13CHpCDF13CPeCDF
 P2694 Page 1 of 6
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 P2694 Page 6 of 6
 P2694 - DLs

Project ID: P-10124 

Sample Summary

Part 5 (DLs) Method 23

Analyte 0_8209_

MB001

Plant 4 

Inlet-R1

Plant 4 

Inlet-R2

Plant 4 

Inlet-R3

Plant 4 

OutletR1

Plant 4 

OutletR2

Plant 4 

OutletR3

Plant 4 

OvenR1

Plant 4 

OvenR2

Plant 4 

OvenR13Blank

pg pg pg pg pg pg pg pg pg pg pg

2,3,7,8-TCDD 5.83 3.27 2.18 3.37 4 3.66 3.73 3.05 3.86 4.82 2.85

1,2,3,7,8-PeCDD 5.77 3.65 2.54 4.24 4.05 3.23 4.12 2.86 4.57 5.13 2.53

1,2,3,4,7,8-HxCDD 5.56 2.67 2.2 3.44 3.74 3.41 3.92 2.45 2.92 3.87 2.56

1,2,3,6,7,8-HxCDD 5.59 2.57 2.32 3.14 3.64 3.36 3.55 2.55 3.12 3.61 2.42

1,2,3,7,8,9-HxCDD 6.35 2.76 2.5 3.9 4.32 3.79 4.12 2.53 3.14 3.98 2.81

1,2,3,4,6,7,8-HpCDD 7.09 4.61 2.57 3.5 5.42 4.97 3.8 3.24 3.33 3.57 2.64

OCDD 9.71 6.83 4.5 5.49 8.29 5.59 7.51 62 6 8.14 4.01

2,3,7,8-TCDF 3.59 1.95 1.71 2.52 2.83 2.11 2.36 2.3 2.29 3.09 1.54

1,2,3,7,8-PeCDF 3.39 2.01 1.82 2.23 2.19 2.25 2.37 1.42 1.9 2.6 1.58

2,3,4,7,8-PeCDF 3.23 1.75 1.75 2.02 2.23 2.15 2.05 1.31 1.69 2.32 1.44

1,2,3,4,7,8-HxCDF 3.6 2.14 1.6 2.14 2.26 2.24 2.39 1.54 1.51 2.37 1.46

1,2,3,6,7,8-HxCDF 3.18 1.95 1.49 1.93 2.18 1.98 2.15 1.41 1.34 2.39 1.33

2,3,4,6,7,8-HxCDF 3.38 2.06 1.61 2.04 2.32 2.2 2.29 1.43 1.56 2.46 1.35

1,2,3,7,8,9-HxCDF 4.65 2.68 1.97 2.92 3.03 3.2 2.94 1.99 1.92 3.23 1.84

1,2,3,4,6,7,8-HpCDF 3.28 2.46 1.5 2.08 2.62 2.09 2.35 3.37 2.36 2.38 1.59

1,2,3,4,7,8,9-HpCDF 4.34 3.14 2.07 2.96 4.23 3.06 3.18 3.15 3.12 3.43 2.21

OCDF 8.04 5.1 2.69 4.8 5.81 3.95 5.92 22 3.56 5.9 3.18

Total TCDD 5.83 3.27 2.18 3.37 4 3.66 3.73 3.05 3.86 4.82 2.85

Total PeCDD 5.77 3.65 2.54 4.24 4.05 3.23 4.12 2.86 4.57 5.13 2.53

Total HxCDD 5.82 2.66 2.34 3.48 3.89 3.51 3.85 2.5 3.05 3.81 2.59

Total HpCDD 7.09 4.61 2.57 3.5 5.42 4.97 3.8 3.24 3.33 3.57 2.64

Total TCDF 3.59 1.95 1.71 2.52 2.83 2.11 2.36 2.3 2.29 3.09 1.54

Total PeCDF 3.31 1.87 1.78 2.12 2.21 2.2 2.21 1.36 1.79 2.45 1.51

Total HxCDF 3.66 2.19 1.65 2.23 2.42 2.37 2.42 1.58 1.57 2.59 1.48

Total HpCDF 3.75 2.76 1.76 2.48 3.32 2.5 2.72 3.26 2.7 2.84 1.87

Checkcode 823-702 901-690 058-218 555-716 246-880 601-566 072-909 607-417 315-975 781-663 624-408

Lab ID MB1_8209_DF_SDS P2694_8209_001 P2694_8209_002 P2694_8209_003 P2694_8209_004 P2694_8209_005 P2694_8209_006 P2694_8209_007 P2694_8209_008 P2694_8209_009 P2694_8209_010