### Name: Bradley H. Belden

Title: Corp Manager - Occupational & Regul Company: The Belden Brick Company Sign Date: 9/29/2010 Name: Paul Jadlowiec Title: Senior Technical Consultant Company:Blue Mountain Environmental Mana Sign Date: 9/8/2010 Permitted Facility Representative / Date Testing Company Representative / Date 

## BSCP - Kiln Emission Test #2415

Final Test Report for

/ / Based on information and belief formed after reasonable inquiry, I certify that the statements and information in this test report are true, accurate, and complete. I have reviewed all testing details and results in this test report and hereby certify that the test report is authentic and accurate.

Tuesday, October 05, 2010 Page 1 of 18

### BSCP - Kiln Emission Test #2415
9/29/2010 Facility Information: The Belden Brick Company
700 Edelweiss Dr. N.E.

Sugarcreek OH44681 Contact:Bradley Belden Phone:330-456-0031 Fax: 330-456-2694 Email:bradley.belden@beldenbrick.com Testing Company: Blue Mountain Environmental Management Corpora 1191 Pittsburgh Road

Valencia PA16059 Contact:James Phillippi Phone:724-898-4500 Fax: 724-898-2908 Email:jphillippi@bluemountainusa.com

Air Permit Number: 06-79-00-0118 Permitted Source ID/Name: Kiln1 and Kiln2 P801 & P802 Permitted Maximum Process Rate: 7.77 tons/hr per kiln Max. Normal Operation Process Rate: P801 - 6.66 ton/hr, P802 - 6.2 to Target Process Test Rate P801 - 5.44 ton/hr, P802 - 6.

Description of the source (including control equipment). Please see the attachments for source or process flow diagram: Belden Brick Plant 8 produces construction grade bricks. Plant 8 has three Kilns, 1, 2, and 3. Kilns 1 and 2 were operating during this test. Kiln 3 was idle. The process begins when a clay/shale material is mined form the ground and processed through a primary crusher. This crushed raw material is transferred via conveyor to a storage building. The material is processed through a secondary crusher followed by particle sizing with a series of screens. The properly sized material is stored in a silo until it is metered into the plant. Once in the plant, the processed material is extruded into the shape of a brick and loaded onto a kiln car. The kiln car is moved first into a dryer, then into the natural gas fired kiln, where it is fired with natural gas at various temperatures depending on the desired product and the structure of the unit. After firing is completed, the brick is cooled to approximately 300 degrees Fahrenheit before being unloaded via an automatic unloading system. Industry/SCC/NAIS327121

Sampling Location Information:

Test Parameter Information: AFS #:11000741859 FRS #:110000741859

SCC / Description30500311 Industrial Processes - Mineral Products - Brick Manufacture - Curing and Firing: Gas-fired Tunnel Kilns

The following state and federal regulations that apply to the proposed testing:

Location Round

Duct Diam. Distance from upstream dist. Distance from

downstream dist. Number of

Traverse Ports Equiv. Diam Min.Travers Points Rect. Duct Length /Width Outlet of Control Device 63 201.6 160.8 2 0 24 0 0

Target Parameter Test

Method Number of

Test RunsTest Run

DurationSample

Points Comments Location2,3,7,8-TCDD Method 23 3 240 0 Outlet of Regulation Description Compound Limit Unit Section 114 of the Clean Air Act 0



### Tuesday, October 05, 2010 Page 2 of 18

### BSCP - Kiln Emission Test #2415
9/29/2010
Control Device1,2,3,7,8-PeCDDMethod 23 3 240 0 Outlet of Control Device1,2,3,4,7,8-

HxCDD Method 23 3 240 0 Outlet of Control Device1,2,3,6,7,8-

HxCDD Method 23 3 240 0 Outlet of Control Device1,2,3,7,8,9-

HxCDD Method 23 3 240 0 Outlet of Control Device1,2,3,4,6,7,8-

HpCDD Method 23 3 240 0 Outlet of Control DeviceOCDD Method 23 3 240 0 Outlet of Control Device2,3,7,8-TCDF Method 23 3 240 0 Outlet of Control Device1,2,3,7,8-PeCDFMethod 23 3 240 0 Outlet of Control Device2,3,4,7,8-PeCDFMethod 23 3 240 0 Outlet of Control Device1,2,3,4,7,8-HxCDFMethod 23 3 240 0 Outlet of Control Device1,2,3,6,7,8-HxCDFMethod 23 3 240 0 Outlet of Control Device2,3,4,6,7,8-HxCDFMethod 23 3 240 0 Outlet of Control Device1,2,3,7,8,9-HxCDFMethod 23 3 240 0 Outlet of Control Device1,2,3,4,6,7,8-

HpCDF Method 23 3 240 0 Outlet of Control Device1,2,3,4,7,8,9-

HpCDF Method 23 3 240 0 Outlet of Control DeviceOCDF Method 23 3 240 0 Outlet of Control DeviceOther TCDD Method 23 3 240 0 Outlet of Control DeviceOther PeCDD Method 23 3 240 0 Outlet of Control DeviceOther HxCDD Method 23 3 240 0 Outlet of Control DeviceOther HpCDD Method 23 3 240 0 Outlet of Control DeviceOther TCDF Method 23 3 240 0 Outlet of Control DeviceOther PeCDF Method 23 3 240 0 Outlet of Control DeviceOther HxCDF Method 23 3 240 0 Outlet of Control DeviceOther HpCDF Method 23 3 240 0 Outlet of Control DeviceTotal Dioxins Method 23 3 240 0 Outlet of Control DeviceTotal Furans Method 23 3 240 0 Outlet of Control DeviceTotal TEQ Method 23 3 240 0 Outlet of Control Device



### Tuesday, October 05, 2010 Page 3 of 18

### BSCP - Kiln Emission Test #2415
9/29/2010

The following describes any modifications and/or deviations to the applicable test methods. If alternative methods were requested, see the attachments for documentation of request AND approval, including dates.
None Chlorine Method 26A 3 60 0 Outlet of Control DeviceHydrogen FluorideMethod 26A 3 60 0 Outlet of Control DeviceHydrogen ChlorideMethod 26A 3 60 0 Outlet of Control DeviceArsenic Method 29 3 60 0 Outlet of Control DeviceNickel Method 29 3 60 0 Outlet of Control DeviceBeryllium Method 29 3 60 0 Outlet of Control DeviceChromium Method 29 3 60 0 Outlet of Control DeviceCobalt Method 29 3 60 0 Outlet of Control DeviceCadmium Method 29 3 60 0 Outlet of Control DeviceFilterable

Particulate Method 29 3 60 0 Outlet of Control DeviceAntimony Method 29 3 60 0 Outlet of Control DeviceLead Method 29 3 60 0 Outlet of Control DeviceMercury Method 29 3 60 0 Outlet of Control DeviceSelenium Method 29 3 60 0 Outlet of Control DeviceManganese Method 29 3 60 0 Outlet of Control Device



### Tuesday, October 05, 2010 Page 4 of 18

### BSCP - Kiln Emission Test #2415
9/29/2010 Sampling / Stack Data Results Summary



### LocationOutlet of Control Device - Method 23 Average Run Number 1 2 3
Test Date 7/27/20107/28/2010 7/29/2010 Run Start Time 1:46:00 PM 7:45:00 AM7:50:00 AM

Run Finish Time 5:50:00 PM 12:07:00 PM11:55:00 AM

Net Run Time, minutes 240 240 240 Dry Gas Meter Volume Sampled, dscf 163.770 177.821 174.886 172.159 Moisture Content of Stack Gas, % 7.36 7.84 7.79 7.663 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Carbon Dioxide, % 2.2 2.3 2.4 2.300 Oxygen, % 17.1 17 17.1 17.067 Average Stack Gas Temperature, °F 346.73 343.98 343.61 344.773 Dry Volumetric Flow Rate, dry scfm 30,705.9 32,473.0 30,960.8 31,379.900 Actual Wet Volumetric Flue Gas Flow Rate, acfm 51,838.3 55,202.4 52,669.6 53,236.767 Percent Isokinetic of Sampling Rate, % 98.0 100.6 103.8 100.800 F-Factor, dscfm/MMBtu @ %O2 8710 8710 8710 8,710.000
Fw 10610 10610 10610 10,610.000
Fc 1040 1040 1040 1,040.000



### Tuesday, October 05, 2010 Page 5 of 18

### BSCP - Kiln Emission Test #2415
9/29/2010
LocationOutlet of Control Device - Method 26A Average Run Number 1 2 3
Test Date 7/29/2010 7/29/2010 7/29/2010 Run Start Time 8:32:00 AM 9:55:00 AM11:11:00 AM

Run Finish Time 9:36:00 AM 10:59:00 AM12:15:00 PM

Net Run Time, minutes 60 60 60 Dry Gas Meter Volume Sampled, dscf 46.575 44.330 43.711 44.872 Moisture Content of Stack Gas, % 8.69 8.50 8.61 8.600 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Carbon Dioxide, % 2.3 2.3 2.3 2.300 Oxygen, % 16.9 16.9 17 16.933 Average Stack Gas Temperature, °F 347.00 346.56 346.84 346.800 Dry Volumetric Flow Rate, dry scfm 31,226.8 30,453.3 29,979.0 30,553.033 Actual Wet Volumetric Flue Gas Flow Rate, acfm 54,189.3 52,708.6 51,968.2 52,955.367 Percent Isokinetic of Sampling Rate, % 102.7 100.2 100.4 101.100 F-Factor, dscfm/MMBtu @ %O2 8710 8710 8710 8,710.000
Fw 10610 10610 10610 10,610.000
Fc 1040 1040 1040 1,040.000



### Tuesday, October 05, 2010 Page 6 of 18

### BSCP - Kiln Emission Test #2415
9/29/2010
LocationOutlet of Control Device - Method 29 Average Run Number 1 2 3
Test Date 7/28/2010 7/28/2010 7/28/2010 Run Start Time 8:50:00 AM 10:47:00 AM12:12:00 PM

Run Finish Time 10:28:00 AM 11:54:00 AM 1:15:00 PM

Net Run Time, minutes 60 60 60 Dry Gas Meter Volume Sampled, dscf 46.819 44.197 45.363 45.460 Moisture Content of Stack Gas, % 7.23 9.13 8.97 8.443 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Carbon Dioxide, % 2.3 2.4 2.6 2.433 Oxygen, % 17 17.1 17 17.033 Average Stack Gas Temperature, °F 345.64 345.56 346.88 346.027 Dry Volumetric Flow Rate, dry scfm 32,797.1 30,060.8 29,974.3 30,944.067 Actual Wet Volumetric Flue Gas Flow Rate, acfm 55,501.1 51,929.2 51,773.4 53,067.900 Percent Isokinetic of Sampling Rate, % 98.3 101.2 104.2 101.233 F-Factor, dscfm/MMBtu @ %O2 8710 8710 8710 8,710.000
Fw 10610 10610 10610 10,610.000
Fc 1040 1040 1040 1,040.000



### Tuesday, October 05, 2010 Page 7 of 18

### BSCP - Kiln Emission Test #2415
9/29/2010 Emissions Summary



### Location: Outlet of Control Device - Method 23 Compound: 1,2,3,4,6,7,8-HpCDD Average RunNumber 1 2 3 Mass_mg 0.0000000051 0.0000000041 0.0000000031 0.000 Eg/hr 5.74E-08 4.49E-08 3.29E-08 0.000 ng/dscm 1.10E-03 8.14E-04 6.26E-04 0.001 ng/dscm@7%O2 4.02E-03 2.90E-03 2.29E-03 0.003 

### Compound: 1,2,3,4,6,7,8-HpCDF Average RunNumber 1 2 3 Mass_mg 0.00000001 0.000000009 0.0000000082 0.000 Eg/hr 1.12E-07 9.86E-08 8.71E-08 0.000 ng/dscm 2.16E-03 1.79E-03 1.66E-03 0.002 ng/dscm@7%O2 7.90E-03 6.38E-03 6.07E-03 0.007 

### Compound: 1,2,3,4,7,8,9-HpCDF Average RunNumber 1 2 3 Mass_mg 0.000000003 0.0000000022 0.0000000017 0.000 Eg/hr 3.37E-08 2.41E-08 1.81E-08 0.000 ng/dscm 6.47E-04 4.37E-04 3.43E-04 0.000 ng/dscm@7%O2 2.37E-03 1.56E-03 1.25E-03 0.002 

### Compound: 1,2,3,4,7,8-HxCDD Average RunNumber 1 2 3 Mass_mg 0.0000000017 0.0000000018 0.0000000016 0.000 Eg/hr 1.91E-08 1.97E-08 1.70E-08 0.000 ng/dscm 3.67E-04 3.58E-04 3.23E-04 0.000 ng/dscm@7%O2 1.34E-03 1.28E-03 1.18E-03 0.001 

### Compound: 1,2,3,4,7,8-HxCDF Average RunNumber 1 2 3 Mass_mg 0.0000000041 0.0000000053 0.0000000051 0.000 Eg/hr 4.61E-08 5.81E-08 5.42E-08 0.000 ng/dscm 8.84E-04 1.05E-03 1.03E-03 0.001 ng/dscm@7%O2 3.23E-03 3.74E-03 3.77E-03 0.004 

### Compound: 1,2,3,6,7,8-HxCDD Average RunNumber 1 2 3 Mass_mg 0.0000000018 0.0000000019 0.0000000017 0.000 Eg/hr 2.02E-08 2.08E-08 1.81E-08 0.000 ng/dscm 3.88E-04 3.77E-04 3.43E-04 0.000 ng/dscm@7%O2 1.42E-03 1.34E-03 1.25E-03 0.001 

### Compound: 1,2,3,6,7,8-HxCDF Average



### Tuesday, October 05, 2010 Page 8 of 18

### BSCP - Kiln Emission Test #2415
9/29/2010
RunNumber 1 2 3 Mass_mg 0.0000000025 0.0000000026 0.0000000029 0.000 Eg/hr 2.81E-08 2.85E-08 3.08E-08 0.000 ng/dscm 5.39E-04 5.16E-04 5.86E-04 0.001 ng/dscm@7%O2 1.97E-03 1.84E-03 2.14E-03 0.002 

### Compound: 1,2,3,7,8,9-HxCDD Average RunNumber 1 2 3 Mass_mg 0.0000000017 0.0000000017 0.0000000016 0.000 Eg/hr 1.91E-08 1.86E-08 1.70E-08 0.000 ng/dscm 3.67E-04 3.38E-04 3.23E-04 0.000 ng/dscm@7%O2 1.34E-03 1.20E-03 1.18E-03 0.001 

### Compound: 1,2,3,7,8,9-HxCDF Average RunNumber 1 2 3 Mass_mg 0.0000000017 0.0000000021 0.0000000021 0.000 Eg/hr 1.91E-08 2.30E-08 2.23E-08 0.000 ng/dscm 3.67E-04 4.17E-04 4.24E-04 0.000 ng/dscm@7%O2 1.34E-03 1.49E-03 1.55E-03 0.001 

### Compound: 1,2,3,7,8-PeCDD Average RunNumber 1 2 3 Mass_mg 0.0000000027 0.0000000026 0.0000000027 0.000 Eg/hr 3.04E-08 2.85E-08 2.87E-08 0.000 ng/dscm 5.82E-04 5.16E-04 5.45E-04 0.001 ng/dscm@7%O2 2.13E-03 1.84E-03 1.99E-03 0.002 

### Compound: 1,2,3,7,8-PeCDF Average RunNumber 1 2 3 Mass_mg 0.0000000027 0.000000003 0.0000000026 0.000 Eg/hr 3.04E-08 3.29E-08 2.76E-08 0.000 ng/dscm 5.82E-04 5.96E-04 5.25E-04 0.001 ng/dscm@7%O2 2.13E-03 2.12E-03 1.92E-03 0.002 

### Compound: 2,3,4,6,7,8-HxCDF Average RunNumber 1 2 3 Mass_mg 0.0000000035 0.000000002 0.000000002 0.000 Eg/hr 3.94E-08 2.19E-08 2.12E-08 0.000 ng/dscm 7.55E-04 3.97E-04 4.04E-04 0.001 ng/dscm@7%O2 2.76E-03 1.41E-03 1.48E-03 0.002 

### Compound: 2,3,4,7,8-PeCDF Average RunNumber 1 2 3 Mass_mg 0.0000000048 0.0000000029 0.0000000054 0.000 Eg/hr 5.40E-08 3.18E-08 5.74E-08 0.000 ng/dscm 1.04E-03 5.76E-04 1.09E-03 0.001 ng/dscm@7%O2 3.80E-03 2.05E-03 3.99E-03 0.003



### Tuesday, October 05, 2010 Page 9 of 18

### BSCP - Kiln Emission Test #2415
9/29/2010 Compound: 2,3,7,8-TCDD Average RunNumber 1 2 3 Mass_mg 0.0000000023 0.0000000038 0.0000000023 0.000 Eg/hr 2.59E-08 4.16E-08 2.44E-08 0.000 ng/dscm 4.96E-04 7.55E-04 4.65E-04 0.001 ng/dscm@7%O2 1.81E-03 2.69E-03 1.70E-03 0.002 

### Compound: 2,3,7,8-TCDF Average RunNumber 1 2 3 Mass_mg 0.0000000111 0.0000000152 0.0000000131 0.000 Eg/hr 1.25E-07 1.67E-07 1.39E-07 0.000 ng/dscm 2.39E-03 3.02E-03 2.65E-03 0.003 ng/dscm@7%O2 8.74E-03 1.08E-02 9.69E-03 0.010 

### Compound: OCDD Average RunNumber 1 2 3 Mass_mg 0.0000000309 0.0000000254 0.0000000186 0.000 Eg/hr 3.48E-07 2.78E-07 1.98E-07 0.000 ng/dscm 6.66E-03 5.05E-03 3.76E-03 0.005 ng/dscm@7%O2 2.44E-02 1.80E-02 1.38E-02 0.019 

### Compound: OCDF Average RunNumber 1 2 3 Mass_mg 0.0000000201 0.0000000185 0.0000000109 0.000 Eg/hr 2.26E-07 2.03E-07 1.16E-07 0.000 ng/dscm 4.33E-03 3.67E-03 2.20E-03 0.003 ng/dscm@7%O2 1.58E-02 1.31E-02 8.05E-03 0.012 

### Compound: Other HpCDD Average RunNumber 1 2 3 Mass_mg 0 0 0.0000000025 0.000 Eg/hr 0.00E+00 0.00E+00 2.66E-08 0.000 ng/dscm 0.00E+00 0.00E+00 5.05E-04 0.000 ng/dscm@7%O2 0.00E+00 0.00E+00 1.85E-03 0.001 

### Compound: Other HpCDF Average RunNumber 1 2 3 Mass_mg 0 0 0 0.000 Eg/hr 0.00E+00 0.00E+00 0.00E+00 0.000 ng/dscm 0.00E+00 0.00E+00 0.00E+00 0.000 ng/dscm@7%O2 0.00E+00 0.00E+00 0.00E+00 0.000 

### Compound: Other HxCDD Average RunNumber 1 2 3 Mass_mg 0.0000000033 0.0000000032 0.000000004 0.000 Eg/hr 3.71E-08 3.51E-08 4.25E-08 0.000



### Tuesday, October 05, 2010 Page 10 of 18

### BSCP - Kiln Emission Test #2415
9/29/2010 ng/dscm 7.12E-04 6.36E-04 8.08E-04 0.001 ng/dscm@7%O2 2.60E-03 2.27E-03 2.96E-03 0.003 

### Compound: Other HxCDF Average RunNumber 1 2 3 Mass_mg 0.0000000074 0.0000000007 0.0000000018 0.000 Eg/hr 8.32E-08 7.67E-09 1.91E-08 0.000 ng/dscm 1.60E-03 1.39E-04 3.64E-04 0.001 ng/dscm@7%O2 5.85E-03 4.95E-04 1.33E-03 0.003 

### Compound: Other PeCDD Average RunNumber 1 2 3 Mass_mg 0.000000001 0 0.0000000014 0.000 Eg/hr 1.12E-08 0.00E+00 1.49E-08 0.000 ng/dscm 2.16E-04 0.00E+00 2.83E-04 0.000 ng/dscm@7%O2 7.90E-04 0.00E+00 1.04E-03 0.001 

### Compound: Other PeCDF Average RunNumber 1 2 3 Mass_mg 0.0000000135 0.000000006 0.0000000057 0.000 Eg/hr 1.52E-07 6.57E-08 6.05E-08 0.000 ng/dscm 2.91E-03 1.19E-03 1.15E-03 0.002 ng/dscm@7%O2 1.06E-02 4.24E-03 4.21E-03 0.006 

### Compound: Other TCDD Average RunNumber 1 2 3 Mass_mg 0.0000000018 0.000000002 0.0000000209 0.000 Eg/hr 2.02E-08 2.19E-08 2.22E-07 0.000 ng/dscm 3.88E-04 3.97E-04 4.22E-03 0.002 ng/dscm@7%O2 1.42E-03 1.41E-03 1.54E-02 0.006 

### Compound: Other TCDF Average RunNumber 1 2 3 Mass_mg 0.000000061 0.0000000318 0.000000127 0.000 Eg/hr 6.86E-07 3.48E-07 1.35E-06 0.000 ng/dscm 1.32E-02 6.32E-03 2.56E-02 0.015 ng/dscm@7%O2 4.83E-02 2.25E-02 9.36E-02 0.055 

### Compound: Total Dioxins Average RunNumber 1 2 3 Mass_mg 0.0000000383 0.0000000206 0.0000000416 0.000 Eg/hr 4.31E-07 2.26E-07 4.42E-07 0.000 ng/dscm 8.26E-03 4.09E-03 8.40E-03 0.007 ng/dscm@7%O2 3.02E-02 1.46E-02 3.07E-02 0.025 

### Compound: Total Furans Average RunNumber 1 2 3


### Tuesday, October 05, 2010 Page 11 of 18

### BSCP - Kiln Emission Test #2415
9/29/2010 Mass_mg 0.0000001378 0.0000000759 0.0000001924 0.000 Eg/hr 1.55E-06 8.32E-07 2.04E-06 0.000 ng/dscm 2.97E-02 1.51E-02 3.89E-02 0.028 ng/dscm@7%O2 1.09E-01 5.38E-02 1.42E-01 0.102 

### Compound: Total TEQ Average RunNumber 1 2 3 Mass_mg 0.00000000953 0.0000000108 0.00000000985 0.000 Eg/hr 1.07E-07 1.18E-07 1.05E-07 0.000 ng/dscm 2.06E-03 2.15E-03 1.99E-03 0.002 ng/dscm@7%O2 7.54E-03 7.66E-03 7.28E-03 0.007



### Location: Outlet of Control Device - Method 26A 

### Compound: Chlorine Average RunNumber 1 2 3 Mass_mg 3.2 3.7 3 3.300 Eg/hr 1.29E+02 1.53E+02 1.23E+02 135.000 ppm 8.23E-01 1.00E+00 8.22E-01 0.882 ppm@7%O2 2.86E+00 3.48E+00 2.93E+00 3.090 

### Compound: Hydrogen Chloride Average RunNumber 1 2 3 Mass_mg 27 24 27 26.000 Eg/hr 1.09E+03 9.89E+02 1.11E+03 1,063.000 ppm 1.35E+01 1.26E+01 1.44E+01 13.500 ppm@7%O2 4.69E+01 4.38E+01 5.13E+01 47.333 

### Compound: Hydrogen Fluoride Average RunNumber 1 2 3 Mass_mg 110 100 110 106.667 Eg/hr 4.43E+03 4.12E+03 4.53E+03 4,360.000 ppm 1.00E+02 9.58E+01 1.07E+02 100.933 ppm@7%O2 3.48E+02 3.33E+02 3.81E+02 354.000



### Location: Outlet of Control Device - Method 29 Compound: Antimony Average RunNumber 1 3 2 Mass_mg 0.0018 0.0018 0.0018 0.002 Eg/hr 7.57E-02 7.14E-02 7.35E-02 0.074 mg/dscm 1.36E-03 1.40E-03 1.44E-03 0.001 mg/dscm@7%O2 4.85E-03 4.99E-03 5.27E-03 0.005 

### Compound: Arsenic Average RunNumber 1 3 2 Mass_mg 0.00276 0.00238 0.00211 0.002 Eg/hr 1.16E-01 9.44E-02 8.61E-02 0.099 mg/dscm 2.08E-03 1.85E-03 1.69E-03 0.002


### Tuesday, October 05, 2010 Page 12 of 18

### BSCP - Kiln Emission Test #2415
9/29/2010 mg/dscm@7%O2 7.41E-03 6.59E-03 6.18E-03 0.007 

### Compound: Beryllium Average RunNumber 1 3 2 Mass_mg 0.00045 0.00045 0.00045 0.000 Eg/hr 1.89E-02 1.78E-02 1.84E-02 0.018 mg/dscm 3.39E-04 3.50E-04 3.60E-04 0.000 mg/dscm@7%O2 1.21E-03 1.25E-03 1.32E-03 0.001 

### Compound: Cadmium Average RunNumber 1 2 3 Mass_mg 0.00432 0.00423 0.00117 0.003 Eg/hr 1.82E-01 1.73E-01 4.64E-02 0.134 mg/dscm 3.26E-03 3.38E-03 9.11E-04 0.003 mg/dscm@7%O2 1.16E-02 1.24E-02 3.25E-03 0.009 

### Compound: Chromium Average RunNumber 1 3 2 Mass_mg 0.01174 0.01372 0.00912 0.012 Eg/hr 4.93E-01 5.44E-01 3.72E-01 0.470 mg/dscm 8.86E-03 1.07E-02 7.29E-03 0.009 mg/dscm@7%O2 3.16E-02 3.81E-02 2.67E-02 0.032 

### Compound: Cobalt Average RunNumber 1 3 2 Mass_mg 0.00045 0.00045 0.00045 0.000 Eg/hr 1.89E-02 1.78E-02 1.84E-02 0.018 mg/dscm 3.39E-04 3.50E-04 3.60E-04 0.000 mg/dscm@7%O2 1.21E-03 1.25E-03 1.32E-03 0.001 

### Compound:Filterable Particulate Average RunNumber 1 3 2 Mass_mg 2.76 5.16 7.26 5.060 Eg/hr 1.16E+02 2.05E+02 2.96E+02 205.667 mg/dscm 2.08E+00 4.02E+00 5.80E+00 3.967 mg/dscm@7%O2 7.41E+00 1.43E+01 2.12E+01 14.303 

### Compound:Lead Average RunNumber 1 3 2 Mass_mg 0.01309 0.00311 0.0027 0.006 Eg/hr 5.50E-01 1.23E-01 1.10E-01 0.261 mg/dscm 9.88E-03 2.42E-03 2.16E-03 0.005 mg/dscm@7%O2 3.52E-02 8.63E-03 7.90E-03 0.017 

### Compound:Manganese Average RunNumber 1 3 2 Mass_mg 0.0135 0.0101 0.0064 0.010


### Tuesday, October 05, 2010 Page 13 of 18

### BSCP - Kiln Emission Test #2415
9/29/2010

Process Run Data Eg/hr 5.67E-01 4.00E-01 2.61E-01 0.409 mg/dscm 1.02E-02 7.86E-03 5.11E-03 0.008 mg/dscm@7%O2 3.64E-02 2.80E-02 1.87E-02 0.028 

### Compound:Mercury Average RunNumber 1 3 2 Mass_mg 0.02243 0.022789 0.021235 0.022 Eg/hr 9.43E-01 9.03E-01 8.67E-01 0.904 mg/dscm 1.69E-02 1.77E-02 1.70E-02 0.017 mg/dscm@7%O2 6.02E-02 6.31E-02 6.22E-02 0.062 

### Compound:Nickel Average RunNumber 1 3 2 Mass_mg 0.0115 0.0061 0.0054 0.008 Eg/hr 4.83E-01 2.42E-01 2.20E-01 0.315 mg/dscm 8.68E-03 4.75E-03 4.32E-03 0.006 mg/dscm@7%O2 3.09E-02 1.69E-02 1.58E-02 0.021 

### Compound: Selenium Average RunNumber 1 3 2 Mass_mg 0.747 0.5582 0.466 0.590 Eg/hr 3.14E+01 2.21E+01 1.90E+01 24.167 mg/dscm 5.64E-01 4.35E-01 3.72E-01 0.457 mg/dscm@7%O2 2.01E+00 1.55E+00 1.36E+00 1.640



### Tuesday, October 05, 2010 Page 14 of 18

### BSCP - Kiln Emission Test #2415
9/29/2010 Process Run Data

APCD Run Data

Process Lab Run Data 

### Run Name Value UOM Comments Target Value 1 Brick Produced (7/27/2010) 11.6 Tons/hr 11.64


### 1 Brick Produced (7/28/2010) 11.31 Tons/hr 11.64
1 Brick Produced (7/29/2010) 10.94 Tons/hr 11.64



### Run Name Value UOM Comments Target Value 1 DRY SCRUBBER 0 lime feed 0


### 1 BAGHOUSE 0 pressure drop 0

Run Name ValueUOM Comments 1 None 0



### Tuesday, October 05, 2010 Page 15 of 18

### BSCP - Kiln Emission Test #2415
9/29/2010 Sampling / Stack Data Results Detail



### LocationOutlet of Control Device - Method 23 Average Run Number 1 2 3 Test Date 7/27/2010 7/28/2010 7/29/2010 Run Start Time 1:46:00 PM7:45:00 AM7:50:00 AM Run Finish Time 5:50:00 PM12:07:00 PM11:55:00 AM Net Traversing Points 49 49 49 Net Run Time, minutes 240 240 240 Nozzle Diameter, inches 0.3 0.3 0.3 0.300 Pitot Tube Coefficient 0.84 0.84 0.84 0.840 Dry Gas Meter Calibration Factor 1.005 1.005 1.005 1.005 Barometric Pressure, inches of Mercury 29.25 29.1 29.05 29.133 Average Orifice Meter Differential, inches H2O 1.82 1.97 1.88 1.890 Dry Gas Meter Volume Sampled, cubic feet 180.658 190.223 186.831 185.904 Average Dry Gas Meter Temperature, °F 114.87 94.84 93.02 100.910 Dry Gas Meter Volume Sampled, dscf 163.770 177.821 174.886 172.159 Total Moisture Liquid collected, g 276.4 321.5 313.8 303.900 Volume of Water Vapor, standard cubic feet 13.01 15.13 14.77 14.303 Moisture Content of Stack Gas, % 7.36 7.84 7.79 7.663 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Dry Mole Fraction 0.9264 0.9216 0.9221 0.923 Carbon Dioxide, % 2.2 2.3 2.4 2.300 Oxygen, % 17.1 17 17.1 17.067 Carbon Monoxide & Nitrogen, % 80.7 80.7 80.5 80.633 Fuel Factor 1.73 1.70 1.58 Dry Molecular Weight, lb/lb-Mole 29.04 29.05 29.07 29.053 Wet Molecular weight, lb/lb-Mole 28.23 28.18 28.21 28.207 Flue Gas Static Pressure, inches of H2O -0.28 -0.27 -0.27 -0.273 Absolute Flue Gas Pressure, inches of Mercury 29.23 29.08 29.03 29.113 Average Stack Gas Temperature, °F 346.73 343.98 343.61 344.773 Average Velocity Head, inches of H2O 0.316 0.357 0.325 0.333 Average Stack Gas Velocity, feet/second 39.91 42.50 40.55 40.987 Stack Cross-Sectional Area, square feet 21.648 21.648 21.648 21.648 Dry Volumetric Flow Rate, dry scfm 30,705.9 32,473.0 30,960.831,379.900 Actual Wet Volumetric Flue Gas Flow Rate, acfm 51,838.3 55,202.4 52,669.653,236.767 Percent Isokinetic of Sampling Rate, % 98.0 100.6 103.8 100.800 Percent Excess Air, % 406.7 394.9 411.8 404.467 F-Factor, dscfm/MMBtu @ %O2 8710 8710 87108,710.000 Round Duct Diameter, inches 63 63 63 Rectangular Duct Width, inches 0 0 0 Rectangular Duct Length, inches 0 0 0 Fw 10610 10610 1061010,610.000 Fc 1040 1040 10401,040.000



### Tuesday, October 05, 2010 Page 16 of 18

### BSCP - Kiln Emission Test #2415
9/29/2010
LocationOutlet of Control Device - Method 26A Average Run Number 1 2 3 Test Date 7/29/2010 7/29/2010 7/29/2010 Run Start Time 8:32:00 AM9:55:00 AM11:11:00 AM Run Finish Time 9:36:00 AM10:59:00 AM12:15:00 PM Net Traversing Points 25 25 25 Net Run Time, minutes 60 60 60 Nozzle Diameter, inches 0.31 0.31 0.31 0.310 Pitot Tube Coefficient 0.84 0.84 0.84 0.840 Dry Gas Meter Calibration Factor 0.997 0.997 0.997 0.997 Barometric Pressure, inches of Mercury 28.88 28.88 28.88 28.880 Average Orifice Meter Differential, inches H2O 2.22 2.10 2.03 2.117 Dry Gas Meter Volume Sampled, cubic feet 49.706 48.173 47.683 48.521 Average Dry Gas Meter Temperature, °F 85.34 95.12 97.16 92.540 Dry Gas Meter Volume Sampled, dscf 46.575 44.330 43.711 44.872 Total Moisture Liquid collected, g 94.2 87.5 87.5 89.733 Volume of Water Vapor, standard cubic feet 4.43 4.12 4.12 4.223 Moisture Content of Stack Gas, % 8.69 8.50 8.61 8.600 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Dry Mole Fraction 0.9131 0.915 0.9139 0.914 Carbon Dioxide, % 2.3 2.3 2.3 2.300 Oxygen, % 16.9 16.9 17 16.933 Carbon Monoxide & Nitrogen, % 80.8 80.8 80.7 80.767 Fuel Factor 1.74 1.74 1.70 Dry Molecular Weight, lb/lb-Mole 29.04 29.04 29.05 29.043 Wet Molecular weight, lb/lb-Mole 28.08 28.10 28.10 28.093 Flue Gas Static Pressure, inches of H2O -0.27 -0.27 -0.27 -0.270 Absolute Flue Gas Pressure, inches of Mercury 28.86 28.86 28.86 28.860 Average Stack Gas Temperature, °F 347.00 346.56 346.84 346.800 Average Velocity Head, inches of H2O 0.339 0.321 0.312 0.324 Average Stack Gas Velocity, feet/second 41.72 40.58 40.01 40.770 Stack Cross-Sectional Area, square feet 21.648 21.648 21.648 21.648 Dry Volumetric Flow Rate, dry scfm 31,226.8 30,453.3 29,979.030,553.033 Actual Wet Volumetric Flue Gas Flow Rate, acfm 54,189.3 52,708.6 51,968.252,955.367 Percent Isokinetic of Sampling Rate, % 102.7 100.2 100.4 101.100 Percent Excess Air, % 381.4 381.4 394.9 385.900 F-Factor, dscfm/MMBtu @ %O2 8710 8710 87108,710.000 Round Duct Diameter, inches 63 63 63 Rectangular Duct Width, inches 0 0 0 Rectangular Duct Length, inches 0 0 0 Fw 10610 10610 1061010,610.000 Fc 1040 1040 10401,040.000



### Tuesday, October 05, 2010 Page 17 of 18

### BSCP - Kiln Emission Test #2415
9/29/2010
LocationOutlet of Control Device - Method 29 Average Run Number 1 2 3 Test Date 7/28/2010 7/28/2010 7/28/2010 Run Start Time 8:50:00 AM10:47:00 AM12:12:00 PM Run Finish Time 10:28:00 AM11:54:00 AM 1:15:00 PM Net Traversing Points 25 25 25 Net Run Time, minutes 60 60 60 Nozzle Diameter, inches 0.31 0.31 0.31 0.310 Pitot Tube Coefficient 0.84 0.84 0.84 0.840 Dry Gas Meter Calibration Factor 0.997 0.997 0.997 0.997 Barometric Pressure, inches of Mercury 29.1 29.1 29.1 29.100 Average Orifice Meter Differential, inches H2O 2.22 2.00 1.90 2.040 Dry Gas Meter Volume Sampled, cubic feet 50.713 48.378 49.770 49.620 Average Dry Gas Meter Temperature, °F 97.68 103.26 104.42 101.787 Dry Gas Meter Volume Sampled, dscf 46.819 44.197 45.363 45.460 Total Moisture Liquid collected, g 77.6 94.3 94.9 88.933 Volume of Water Vapor, standard cubic feet 3.65 4.44 4.47 4.187 Moisture Content of Stack Gas, % 7.23 9.13 8.97 8.443 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Dry Mole Fraction 0.9277 0.9087 0.9103 0.916 Carbon Dioxide, % 2.3 2.4 2.6 2.433 Oxygen, % 17 17.1 17 17.033 Carbon Monoxide & Nitrogen, % 80.7 80.5 80.4 80.533 Fuel Factor 1.70 1.58 1.50 Dry Molecular Weight, lb/lb-Mole 29.05 29.07 29.10 29.073 Wet Molecular weight, lb/lb-Mole 28.25 28.06 28.10 28.137 Flue Gas Static Pressure, inches of H2O -0.27 -0.27 -0.27 -0.270 Absolute Flue Gas Pressure, inches of Mercury 29.08 29.08 29.08 29.080 Average Stack Gas Temperature, °F 345.64 345.56 346.88 346.027 Average Velocity Head, inches of H2O 0.361 0.314 0.312 0.329 Average Stack Gas Velocity, feet/second 42.73 39.98 39.86 40.857 Stack Cross-Sectional Area, square feet 21.648 21.648 21.648 21.648 Dry Volumetric Flow Rate, dry scfm 32,797.1 30,060.8 29,974.330,944.067 Actual Wet Volumetric Flue Gas Flow Rate, acfm 55,501.1 51,929.2 51,773.453,067.900 Percent Isokinetic of Sampling Rate, % 98.3 101.2 104.2 101.233 Percent Excess Air, % 394.9 411.8 402.3 403.000 F-Factor, dscfm/MMBtu @ %O2 8710 8710 87108,710.000 Round Duct Diameter, inches 63 63 63 Rectangular Duct Width, inches 0 0 0 Rectangular Duct Length, inches 0 0 0 Fw 10610 10610 1061010,610.000 Fc 1040 1040 10401,040.000



### Tuesday, October 05, 2010 Page 18 of 18