Instructions for completing the Fuel Material AnalysisInformation

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concernare: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium.This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets.Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Pleasename each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Pleaserefer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet. If you choose "other",please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

-04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of

measure.EIA

Facility Code Facility Name Boiler ID Fuel Type 1

6761 Rawhide 101 subbituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis Analyte

6761 Rawhide 101 As Received Higher Heating Value 6761 Rawhide 101 As Received % Moisture 6761 Rawhide 101 As Received % Ash 6761 Rawhide 101 As Received % Sulfur 6761 Rawhide 101 Dry basis Higher Heating Value 6761 Rawhide 101 Dry basis % Ash 6761 Rawhide 101 Dry basis % Sulfur 6761 Rawhide 101 Dry basis Antimony 6761 Rawhide 101 Dry basis Arsenic 6761 Rawhide 101 Dry basis Beryllium 6761 Rawhide 101 Dry basis Cadmium 6761 Rawhide 101 Dry basis Chlorine 6761 Rawhide 101 Dry basis Chromium 6761 Rawhide 101 Dry basis Cobalt 6761 Rawhide 101 Dry basis Fluorine 6761 Rawhide 101 Dry basis Lead 6761 Rawhide 101 Dry basis Manganese 6761 Rawhide 101 Dry basis Mercury 6761 Rawhide 101 Dry basis Nickel 6761 Rawhide 101 Dry basis SeleniumAnalysis Method for each Analyte

(example: ASTM D5865-04) ASTM D 5865 ASTM D 3302 ASTM D 3174/5142 ASTM D 4239 ASTM D 5865 ASTM D 3174/5142 ASTM D 4239 ASTM D 6357 ASTM D 6357 ASTM D 6357 ASTM D 6357 ASTM D 6721 ASTM D 6357 ASTM D 6357 ASTM D 6357 ASTM D 6357 ASTM D 6357 ASTM D 6722 ASTM D 6357 SW7740EIA Facility Code Facility

Name Boiler ID HAPs Test Group 6761 Rawhide 101 Mercury and non-mercury

metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) % A sh (as received) % Sulfur (as received) Run 1, Sample 1 5/4/2010 5/4/2010 8824.00 Btu/lb 25.81 5.82 0.22 Run 1, Sample 2 5/4/2010 5/4/2010 8864.00 Btu/lb 26.02 5.44 0.21 Run 1, Sample 3 5/4/2010 5/4/2010 8839.00 Btu/lb 26.28 5.32 0.22 Run 1, Sample 4 5/4/2010 5/4/2010 8762.00 Btu/lb 26.1 5.83 0.21 Run 1, Sample 5 5/4/2010 5/4/2010 8872.00 Btu/lb 26.26 5.11 0.22 Run 2, Sample 1 5/5/2010 5/5/2010 8877.00 Btu/lb 26.17 4.99 0.24 Run 2, Sample 2 5/5/2010 5/5/2010 8897.00 Btu/lb 26.14 4.86 0.23 Run 2, Sample 3 5/5/2010 5/5/2010 8883.00 Btu/lb 26.15 5 0.23 Run 2, Sample 4 5/5/2010 5/5/2010 8856.00 Btu/lb 26.36 5.06 0.21 Run 3, Sample 1 5/6/2010 5/6/2010 8790.00 Btu/lb 26.43 5.67 0.2 Run 3, Sample 2 5/6/2010 5/6/2010 8840.00 Btu/lb 26.41 5.32 0.21 Run 3, Sample 3 5/6/2010 5/6/2010 8852.00 Btu/lb 26.35 5.3 0.22 Run 3, Sample 4 5/6/2010 5/6/2010 8844.00 Btu/lb 26.36 5.37 0.2 Fuel Testing ResultsHigher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony (Dry Basis) Antimony

Units 11894 Btu/lb 0 7.85 0.3[<10] μg/g 0.07 μg/g [<1] μg/g 11982 Btu/lb 0 7.35 0.29[<10] μg/g 0.13 μg/g [<1] μg/g 11989Btu/lb 0 7.22 0.29[<10] μg/g 0.06 μg/g [<1] μg/g 11856 Btu/lb 0 7.89 0.28[<10] μg/g 0.06 μg/g [<1] μg/g 12031 Btu/lb 0 6.93 0.3[<10] μg/g 0.06 μg/g [<1] μg/g 12024 Btu/lb 0 6.76 0.32 12 μg/g 0.06 μg/g [<1] μg/g 12045Btu/lb 0 6.58 0.32 [<10] μg/g 0.07 μg/g [<1] μg/g 12029Btu/lb 0 6.77 0.31 [<10] μg/g 0.07 μg/g [<1] μg/g 12026 Btu/lb 0 6.87 0.29[<10] μg/g 0.1 μg/g [<1] μg/g 11948Btu/lb 0 7.71 0.28[<10] μg/g 0.06 μg/g [<1] μg/g 12012 Btu/lb 0 7.23 0.28[<10] μg/g 0.06 μg/g [<1] μg/g 12020 Btu/lb 0 7.2 0.29[<10] μg/g 0.05 μg/g [<1] μg/g 12010 Btu/lb 0 7.29 0.28[<10] μg/g 0.1 μg/g [<1] μg/gArsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units [<1] μg/g 0.3 μg/g [<0.2] μg/g 5 μg/g 3 μg/g 4 μg/g [<1] μg/g 0.4 μg/g [<0.2] μg/g 5 μg/g 3 μg/g 4 μg/g [<1] μg/g 0.4 μg/g [<0.2] μg/g 5 μg/g 3 μg/g 5 μg/g [<1] μg/g 0.4 μg/g [<0.2] μg/g 5 μg/g 3 μg/g 5 μg/g [<1] μg/g 0.3 μg/g [<0.2] μg/g 5 μg/g 3 μg/g 5 μg/g [<1] μg/g 0.3 μg/g [<0.2] μg/g 5 μg/g 2 μg/g 5 μg/g [<1] μg/g 0.3 μg/g [<0.2] μg/g 5 μg/g 2 μg/g 5 μg/g [<1] μg/g 0.3 μg/g [<0.2] μg/g 5 μg/g 2 μg/g 4 μg/g [<1] μg/g 0.3 μg/g [<0.2] μg/g 5 μg/g 3 μg/g 4 μg/g

1 μg/g 0.4 μg/g [<0.2] μg/g 6 μg/g 3 μg/g 4 μg/g [<1] μg/g 0.4 μg/g [<0.2] μg/g 5 μg/g 3 μg/g 4 μg/g [<1] μg/g 0.4 μg/g [<0.2] μg/g 5 μg/g 3 μg/g 4 μg/g [<1] μg/g 0.3 μg/g [<0.2] μg/g 5 μg/g 3 μg/g 4 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units 5 μg/g [<1] μg/g 55 μg/g 2 μg/g 5 μg/g [<1] μg/g 49 μg/g 2 μg/g 5 μg/g [<1] μg/g 51 μg/g 2 μg/g 5 μg/g [<1] μg/g 45 μg/g 2 μg/g 5 μg/g [<1] μg/g 58 μg/g 2 μg/g 5 μg/g [<1] μg/g 47 μg/g 2 μg/g 5 μg/g [<1] μg/g 35 μg/g 2 μg/g 5 μg/g [<1] μg/g 43 μg/g 2 μg/g 5 μg/g [<1] μg/g 47 μg/g 2 μg/g 5 μg/g [<1] μg/g 55 μg/g 2 μg/g 5 μg/g [<1] μg/g 53 μg/g 2 μg/g 5 μg/g [<1] μg/g 53 μg/g 2 μg/g 5 μg/g [<1] μg/g 53 μg/g 2 μg/gEIA Facility Code Facility

Name Boiler ID HAPs Test Group 6761 Rawhide 101 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Run 1, Sample 1 5/5/2010 5/5/2010 8877.00 Btu/lb Run 1, Sample 2 5/5/2010 5/5/2010 8897.00 Btu/lb Run 1, Sample 3 5/5/2010 5/5/2010 8883.00 Btu/lb Run 2, Sample 1 5/5/2010 5/5/2010 8883.00 Btu/lb Run 2, Sample 2 5/5/2010 5/5/2010 8856.00 Btu/lb Run 3, Sample 1 5/6/2010 5/6/2010 8790.00 Btu/lb Run 3, Sample 2 5/6/2010 5/6/2010 8840.00 Btu/lb Run 3, Sample 3 5/6/2010 5/6/2010 8852.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) 26.17 4.99 0.24 12024 Btu/lb 0 6.76 26.14 4.86 0.23 12045Btu/lb 0 6.58 26.15 5 0.23 12029Btu/lb 0 6.77 26.15 5 0.23 12029Btu/lb 0 6.77 26.36 5.06 0.21 12026 Btu/lb 0 6.87 26.43 5.67 0.2 11948Btu/lb 0 7.71 26.41 5.32 0.21 12012 Btu/lb 0 7.23 26.35 5.3 0.22 12020 Btu/lb 0 7.2% Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony (Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic Units 0.32 12 μg/g 0.06 μg/g [<1] μg/g [<1] μg/g 0.32 [<10] μg/g 0.07 μg/g [<1] μg/g [<1] μg/g 0.31 [<10] μg/g 0.07 μg/g [<1] μg/g [<1] μg/g 0.31 [<10] μg/g 0.07 μg/g [<1] μg/g [<1] μg/g 0.29[<10] μg/g 0.1 μg/g [<1] μg/g [<1] μg/g 0.28[<10] μg/g 0.06 μg/g [<1] μg/g 1 μg/g 0.28[<10] μg/g 0.06 μg/g [<1] μg/g [<1] μg/g 0.29[<10] μg/g 0.05 μg/g [<1] μg/g [<1] μg/gBeryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) 0.3 μg/g [<0.2] μg/g 5 μg/g 2 μg/g 5 0.3 μg/g [<0.2] μg/g 5 μg/g 2 μg/g 5 0.3 μg/g [<0.2] μg/g 5 μg/g 2 μg/g 4 0.3 μg/g [<0.2] μg/g 5 μg/g 2 μg/g 4 0.3 μg/g [<0.2] μg/g 5 μg/g 3 μg/g 4 0.4 μg/g [<0.2] μg/g 6 μg/g 3 μg/g 4 0.4 μg/g [<0.2] μg/g 5 μg/g 3 μg/g 4 0.4 μg/g [<0.2] μg/g 5 μg/g 3 μg/g 4Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units μg/g 5 μg/g [<1] μg/g 47 μg/g 2 μg/g μg/g 5 μg/g [<1] μg/g 35 μg/g 2 μg/g μg/g 5 μg/g [<1] μg/g 43 μg/g 2 μg/g μg/g 5 μg/g [<1] μg/g 43 μg/g 2 μg/g μg/g 5 μg/g [<1] μg/g 47 μg/g 2 μg/g μg/g 5 μg/g [<1] μg/g 55 μg/g 2 μg/g μg/g 5 μg/g [<1] μg/g 53 μg/g 2 μg/g μg/g 5 μg/g [<1] μg/g 53 μg/g 2 μg/gEIA Facility Code Facility

Name Boiler ID HAPs Test Group 6761 Rawhide 101 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Run 1, Sample 1 5/7/2010 5/7/2010 8839.00 Btu/lb Run 1, Sample 2 5/7/2010 5/7/2010 8854.00 Btu/lb Run 1, Sample 3 5/7/2010 5/7/2010 8841.00 Btu/lb Run 2, Sample 1 5/7/2010 5/7/2010 8809.00 Btu/lb Run 2, Sample 2 5/7/2010 5/7/2010 8821.00 Btu/lb Run 2, Sample 3 5/7/2010 5/7/2010 8833.00 Btu/lb Run 3, Sample 1 5/7/2010 5/7/2010 8778.00 Btu/lb Run 3, Sample 2 5/7/2010 5/7/2010 8826.00 Btu/lb Run 3, Sample 3 5/7/2010 5/7/2010 8779.00 Btu/lb Fuel Testing ResultsNon-dioxin/furan organic HAPs

% Moisture (as received) % A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) 26.39 5.4 0.2 12008Btu/lb 0 7.34 26.13 5.59 0.21 11986 Btu/lb 0 7.57 26.39 5.43 0.21 12011 Btu/lb 0 7.38 26.39 5.49 0.21 11967 Btu/lb 0 7.46 26.4 5.51 0.2 11985Btu/lb 0 7.48 26.23 5.67 0.2 11975Btu/lb 0 7.68 26.12 6.1 0.21 11882 Btu/lb 0 8.25 26.06 5.81 0.2 11937 Btu/lb 0 7.86 26.07 6.01 0.22 11875Btu/lb 0 8.13% Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony (Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic Units 0.27 0.28 0.29 0.29 0.28 0.28 0.28 0.27 0.3Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis)Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsEIA Facility Code Facility

Name Boiler ID HAPs Test Group 6761 Rawhide 101

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis)% Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony (Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic UnitsBeryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis)Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bituminous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to theorangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm μg/g