Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility 

Pearl Harbor, Oahu, Hawaii 

Latitude: 21o

22’15” N 

Longitude: 157o

53’33” W 

HDOH Facility ID No. 9-102271 

HDOH Release ID No. 99051, 010011, 020028 

July 2009 

Prepared by: 

TEC Inc. 

1001 Bishop St. Suite 1400 

American Savings Bank Tower 

Honolulu, Hawaii 96813 

Prepared for: 

Commander 

Navy Region Hawaii 

Environmental Department, Code N45 

850 Ticonderoga Street, Suite 110 

Pearl Harbor, Hawaii 96860-5101 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

i 

Table of Contents 

Table of Contents ............................................................................................................................. i

Executive Summary ......................................................................................................................... 1

1.0 Introduction.......................................................................................................................... 7

1.1 Project Objective .............................................................................................................. 7

1.2 Previous Reports .............................................................................................................. 7

1.3 Background ...................................................................................................................... 8

1.3.1 Site Description ......................................................................................................... 8

1.3.2 Facility Information .................................................................................................. 8

1.3.3 UST Information ....................................................................................................... 8

1.4 Previous Environmental Investigations ............................................................................ 8

1.5 Regulatory Updates ........................................................................................................ 11

1.6 RHMW05 Installation .................................................................................................... 11

2.0 Sample Collection and Analyses ........................................................................................ 11

2.1 Monitoring Well Purging ............................................................................................... 12

2.2 Groundwater Sample Collection .................................................................................... 12

2.3 Groundwater Sample Analyses ...................................................................................... 12

3.0 Groundwater Sample Analytical Results ........................................................................... 12

3.1 May 2009 Sample Analytical Results ............................................................................ 12

3.2 Groundwater Contaminant Trend ................................................................................... 15

3.3 Results of Oil/Water Interface Measurements ............................................................... 16

3.4 Groundwater Status ........................................................................................................ 17

4.0 Summary and Conclusions ................................................................................................. 21

5.0 References .......................................................................................................................... 25

List of Tables 

Table 1 Analytical Results for Quarterly Groundwater Sampling Release Response Report ..14 

Table 2 Oil/Water Interface Measurements ..............................................................................17 

Table 3 Action Levels for Compounds of Concern ..................................................................18 

Table 4 Responses to Groundwater Monitoring Results ..........................................................18 

List of Figures 

Figure 1 TPH Trends in Groundwater, Round 15 (May 13, 2009) ............................................23 

Figure 2 PAH Trends in Groundwater, Round 15 (May 13, 2009) ............................................24 

List of Appendices 

Appendix A – Laboratory Analytical Reports 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

1 

Executive Summary 

This quarterly groundwater monitoring report presents the results of groundwater sampling 

conducted on May 13, 2009 at the United States (US) Navy Bulk Fuel Storage Facility at Red 

Hill, Oahu, Hawaii (the Facility). The sampling and reporting was conducted by TEC Inc. (TEC) 

for the Fleet and Industrial Supply Center (FISC) at Pearl Harbor, Hawaii. This report is part of 

a series of quarterly groundwater monitoring reports provided by the US Navy to the State of 

Hawaii Department of Health (HDOH) in accordance with HDOH’s release response 

requirements. Currently, there are 18 active and 2 inactive, 12.5 million gallon, field-constructed 

underground storage tanks (USTs) located at the Facility. 

Background 

In 2002, the US Navy installed a groundwater monitoring well (currently named RHMW01) into 

the basal aquifer, directly down-gradient from the Facility, within the lower access tunnel. 

Groundwater samples from this well indicated that petroleum from the Facility has migrated to 

the basal aquifer (AMEC, 2002). In 2005, the US Navy began quarterly monitoring of the 

aquifer to protect their down-gradient drinking water resource associated with the US Navy Well 

2254-01. US Navy Well 2254-01 is located approximately 3,000 feet down-gradient from the 

Facility USTs and provides approximately 24 % of the potable water to the Pearl Harbor Water 

System (PHWS). 

By September 2005, the US Navy had installed two more groundwater monitoring wells 

(RHMW02 and RHMW03) within the Facility UST system, a background groundwater 

monitoring well (RHMW04) up-gradient from the Facility adjacent to the US Navy Firing Range, 

and a groundwater monitoring well within the US Navy Well 2254-01 infiltration gallery 

(RHMW2254-01). 

All five wells were sampled twice as part of a comprehensive environmental investigation and 

risk assessment (TEC, 2006). For this investigation, groundwater samples were analyzed for 

petroleum constituents and compared against HDOH Drinking Water Environmental Action 

Levels (EALs) (HDOH, July 2005). In addition, a three-dimensional (3-D) groundwater model 

was developed to produce site-specific risk-based levels (SSRBLs) for compounds of concern. 

The results of this modeling effort indicated that Jet Propulsion (JP)–5 fuel presented the biggest 

risk to the US Navy water supply, due to its mobility and toxicity. Finally, the model 

determined that a non-aqueous plume (free product) of JP-5 would need to migrate to within 

1,100 feet of the US Navy Well 2254-01 infiltration gallery for HDOH EALs to be exceeded 

within the gallery. Based on this, free-product must be observed at RHMW01 for EALs to be 

exceeded at the US Navy Well 2254-01. 

In April 2009, another groundwater monitoring well (RHMW05) was installed down-gradient 

from the Facility, within the lower access tunnel between RHMW01 and RHMW2254-01. It 

was installed to identify the extent of contaminant migration down-gradient before it reaches the 

infiltration gallery at RHMW2254-01 (see Figure 1). 

 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

2 

During the summer and fall of 2008, HDOH updated their EALs, which resulted in significant 

changes to the action levels associated with methylnaphthalenes. The HDOH Drinking Water 

toxicity EAL for these compounds was 240 g/L. This concentration assumed that 

methylnaphthalenes were not human carcinogens. Once evidence emerged and was accepted by 

the US Environmental Protection Agency (USEPA) that methylnaphthalenes are carcinogenic to 

humans, HDOH adopted more rigorous EALs of 4.7 g/L for 1-methylnaphthalene and 24 g/L 

for 2-methylnaphthalene (HDOH, 2008). 

The HDOH Drinking Water EAL for naphthalene was also updated during this process. 

Previously, HDOH based their naphthalene EAL on USEPA Region 9 Preliminary Remediation 

Goal (USEPA PRG) of 6.2 g/L, which is associated with a non-cancer Hazard Index of 1. 

HDOH has updated their naphthalene drinking water EAL to 17 g/L, in deference to the 

California Department of Public Health’s Drinking Water Notification Levels (HDOH, 2008). 

Finally, the HDOH Drinking Water EAL for TPH-DRO was increased from 100 g/L to 210 

g/L, although the Groundwater Gross Contamination EAL for TPH-DRO remains 100 g/L. 

Groundwater Protection Plan 

In 2008, the US Navy completed the Red Hill Bulk Fuel Storage Facility Final Groundwater 

Protection Plan (TEC, 2008), which specified SSRBLs and various required actions based on the 

category status (i.e., categories 1 through 4) of each groundwater monitoring well. The main 

object of the Plan is to protect the groundwater quality of US Navy Well 2254-01, which 

provides potable water to the PHWS. This is accomplished by comparing petroleum 

concentrations in the Facility wells to established SSRBLs and taking appropriate action. A 

secondary, but important objective of the Plan is to identify leaking USTs by evaluating 

increasing concentration trends, or the presence of free product in one or more groundwater 

monitoring wells. This quarterly report compares observed water quality to these established 

categories and associated actions. 

Current Results 

On May 13, 2009, five groundwater samples (i.e., RHMW01, RHMW02, RHMW03, RHMW05 

and RHMW2254-01), along with the required quality control samples (duplicate, matrix spike, 

spike duplicate, and trip blank) were collected for analysis. Samples were analyzed for Total 

Petroleum Hydrocarbons (TPH) quantified as Diesel-Range Organics (DRO) and Gasoline 

Range Organics (GRO), Volatile Organic Compounds (VOCs), Polynuclear Aromatic 

Hydrocarbons (PAHs), and dissolved lead. 

TPH-DRO

TPH-DRO was detected at 373 micrograms per liter (μg/L) in RHMW01, 1,810 μg/L (i.e., the 

average of normal and duplicate samples) in RHMW02, and at 200 μg/L in RHMW05 (i.e., the 

recently installed monitoring well). TPH-DRO was not detected above the laboratory method 

detection limit (MDL) at RHMW03 and RHMW2254-01. The HDOH Drinking Water EAL and 

SSRBL for TPH-DRO are 210 μg/L and 4,500 μg/L, respectively. 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

3 

TPH-GRO

For TPH-GRO the HDOH Drinking Water EAL is 100 μg/L. In samples RHMW01, RHMW02, 

RHMW02D (i.e., the duplicate sample collected), RHMW03, RHMW05, and RHMW2254-01 

estimated values (i.e., values below the laboratory reporting limit, but above the MDL) were 

observed at the following respective levels: 16.6 μg/L, 39.1 μg/L, 36.7 μg/L, 14.8 μg/L, 13.2 

μg/L, and 19.1 μg/L. The estimated value of 19.1 μg/L of TPH-GRO detected in RHMW2254-

01, is below the HDOH Drinking Water EAL of 100 μg/L and was just above the estimated 

value observed in the previous sampling round (i.e., 14 μg/L). 

Other Parameters above HDOH Drinking Water EALs

At RHMW02, average concentrations between the normal and duplicate samples were 

determined to be above the HDOH Drinking Water EAL for 1-methylnaphthalene (i.e., analyzed 

to be 21.25 μg/L vs. the HDOH Drinking Water EAL of 4.7 μg/L). 

Other Results

It is noteworthy that 2-methylnaphthalene was detected in RHMW2254-01 at the estimated 

concentration of 0.018 μg/L during the May 2009 sampling event which is significantly below 

the HDOH Drinking Water EAL of 24 μg/L. 

Trend Analysis 

RHMW01

At RHMW01, concentrations of TPH-DRO have been greater than the HDOH Drinking Water 

EAL since September 2005, but less than 25 percent of the SSRBL of 4,500 g/L. In May 2009, 

TPH-DRO was lower in concentration (i.e., 373 g/L) than in February 2009 (i.e., 387 g/L) and 

October 2008 (i.e., 459 g/L). Prior to a peak observed in October 2008, TPH-DRO 

concentrations had decreased for three consecutive sampling rounds. 

RHMW02

At RHMW02, concentrations of TPH-DRO have been greater than the HDOH Drinking Water 

EAL since September 2005 and greater than 50 percent of the SSRBL (estimated solubility limit 

of 4,500 g/L) over that same period. In May 2009 however, the average TPH-DRO 

concentration (i.e., average of normal and duplicate samples of 1,810 g/L) was below 50 

percent of the SSRBL for the first time since September 2005. The average TPH-DRO 

concentration from the February 2009 sampling event was 2,840 g/L, and the October 2008 

average TPH-DRO concentration of 5,420 g/L was above the SSRBL. 

The average of three parameters (i.e., naphthalene, 1-methylnaphthalene, and 2-

methylnaphthalene) have been at or exceeding the EALs since September 2005. In October 

2008, the average of these parameters decreased in concentrations following increasing trends 

over three previous rounds (since January 2008). During the May 2009 sampling event, the 

average of all three parameters continued the decreasing trend. Only the 1-methylnaphthalene 

average (i.e., 21.25 g/L) was observed above the HDOH Drinking Water EAL (i.e., 4.7 g/L). 

There are no SSRBLs established for these parameters. 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

4 

RHMW03

At RHMW03, concentrations of TPH-DRO have fluctuated around the HDOH Drinking Water 

EAL since September 2005 and have been significantly lower than corresponding values 

observed at RHMW01 and RHMW02. During the May 2009 sampling event, TPH-DRO was 

not detected above the MDL, continuing a decreasing trend that has existed since October 2008. 

Prior to a peak observed in October 2008 of 244 g/L, TPH-DRO had been increasing in 

concentration since April 2008. 

Current Groundwater Status 

Based on the monitoring event that occurred in May 2009, no free product was observed at 

RHMW01, RHMW02, or RHMW03. 

RHMW05

Based upon the May 2009 sampling event, the first for this newly installed well, RHMW05 

avoids being placed in Category 1 status. This is because although the TPH-DRO estimated 

concentration of 200 g/L is above the MDL, but below the HDOH Drinking Water EAL of 210 

g/L, no contamination trend (i.e., two or more consecutive sampling rounds) has yet to be 

observed. 

Category 1 Status Locations

US Navy Well 2254-01(measured at RHMW2254-01) 

Following the May 2009 sampling event, the US Navy Well 2254-01 is now in a provisional 

Category 1 status because over the course of the past two sampling events (i.e., February and 

May 2009) TPH-GRO has been detected above the MDL, but below the HDOH Drinking Water 

EAL of 100 g/L with relatively stable concentrations (i.e., an estimated value of 14 g/L in 

February and 19.1 g/L in May). 

The laboratory Practical Quantification Limit (PQL) or Reporting Limit (RL) for TPH-GRO is 

100 ug/l. The RHMW2254-01 May 2009 sample result was assigned an estimated “J” value of 

19.1 ug/l; which is five times below the laboratory PQL or RL. However, the associated 

laboratory method blank also gave an estimated “J” value of 14.9 ug/l. The pattern observed in 

the RHMW2254-01 sample chromatogram matches the pattern in the laboratory method blank. 

Based on evaluation of these data, it appears that the MDL for the TPH-GRO of 10 ug/l may be 

set too low. Standard laboratory procedures would typically set the MDL at approximately 1/3 

of the PQL or 30 ug/l and not at 10 ug/l or 3 times lower than that level. 

The TPH-GRO method measures the area of peaks over an integration range. Thus, any slight 

changes in the baseline could be counted as TPH-GRO. This is different than methods that 

target a single peak (e.g., benzene) where the baseline is much easier to define. Consequently, 

any changes in the condition of the instrument may produce slight baseline changes giving an 

indication that TPH-GRO is present. Since the residual TPH-GRO response over the integration 

range for RHMW2254-01 and the associated method blank both gave estimated positive values, 

the estimated value of 19.1 ug/l for RHMW2254-01 may represent a “false positive”. Due to this 

uncertainty, a provisional Category 1 status has been assigned to the US Navy Well 2254-01. 

This provisional status will be reevaluated following the next quarterly sampling event. 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

5 

Category 1 status for the US Navy Well 2254-01 requires: 

1. Quarterly reports to be sent to HDOH; 

2. Notification of the FISC chain of command within 1 day; 

3. Reevaluate Tier 3 Risk Assessment and groundwater model results and develop a course 

of action proposal for HDOH; and 

4. As appropriate, prepare for alternative water source. 

RHMW03 

Based upon the May 2009 sampling event, RHMW03 remains in Category 1 status, because over 

the course of the past two sampling events (i.e., February and May 2009) TPH-GRO has been 

detected above the MDL, but was below the HDOH Drinking Water EAL of 100 g/L with 

relatively stable concentrations (i.e., an estimated value of 16.1 g/L in February and 14.8 g/L 

in May). 

Category 1 response for RHMW03 requires: 

1. Quarterly reports to be sent to HDOH. 

Category 2 Status Locations

RHMW01 

The May 2009 sampling event results in RHMW01 remaining in Category 2 status, since the 

TPH-DRO concentration of 373 g/L is greater than the HDOH Drinking Water EAL (210 g/L), 

but less than half the SSRBL of 4,500 g/L (estimated solubility limit of JP-5). 

RHMW02 

The May 2009 sampling event results in RHMW02 being downgraded from Category 3 to 

Category 2 status since TPH-DRO [1,620 g/L and 2,000 g/L (duplicate)] is greater than the 

HDOH Drinking Water EAL (210 g/L), but is less than one half the established SSRBL value 

of 4,500 g/L (estimated solubility limit of JP-5). 

Category 2 for RHMW01 and RHMW02 requires: 

1. Quarterly reports to be sent to HDOH; and 

2. Initiation of a leak determination program to identify if tanks are leaking. 

Category 3 or 4 Status Locations

There is no Category 3 or 4 status location. 

Conclusions and Recommendations 

There is no indication of an immediate threat of disruption to drinking water resources of the US 

Navy Well 2254-01 as a result in the May 2009 data, but the US Navy Well 2254-01 has been 

given a provisional Category 1 status for the first time since quarterly sampling has been 

conducted by TEC. Provisional Category 1 status has been assigned to the US Navy Well 2254-

01 because over the course of the past two sampling events, (i.e., February and May 2009) TPHGRO was reported at trace concentrations above the MDL, but was below the HDOH Drinking 

Water EAL of 100 g/L with relatively stable concentrations (i.e., an estimated value of 14 g/L 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

6 

in February and 19.1 g/L in May). However, it is noteworthy that the associated laboratory 

method blank also reported an estimated trace concentration of TPH-GRO (i.e., 14.9 g/L) 

presenting some analytical uncertainty. This new provisional Category 1 status for US Navy 

Well 2254-01 requires that certain actions be taken (e.g., reevaluation of risks and the 

groundwater model). These actions are currently in the process of being implemented. 

Subsequent sampling events will determine if the trace concentrations of TPH-GRO detected in 

the last two sampling events represent a long-term trend. Given the May 2009 sampling data 

relative to the US Navy Well 2254-01, the status of this well be closely monitored and evaluated 

during subsequent planned sampling events. 

With the exception of the US Navy Well 2254-01, May 2009 concentrations for the other 

monitoring wells have improved as compared to the results from the February 2009 sampling 

event. In fact, the May 2009 event has resulted in RHMW02 being downgraded from Category 3 

to Category 2 status. 

Quarterly groundwater sampling for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead 

will continue at the Facility until such time that data indicates that a different monitoring plan is 

warranted. It is recommended that future quarterly analytical results be closely monitored at 

RHMW2254-01 to monitor and evaluate for the presence of trace quantities of TPH-GRO. 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

7 

1.0 Introduction

This report presents the results of the 15th groundwater sampling event, conducted in May 2009 

at the Red Hill Fuel Storage Facility, Oahu, Hawaii (hereafter referred to as “the Facility”). The 

Facility consists of 18 active and 2 inactive underground storage tanks (USTs) operated by the 

Fleet and Industrial Supply Center (FISC), Pearl Harbor. The groundwater sampling and 

analysis event is part of a groundwater monitoring program for the UST site in response to past 

UST releases, previous environmental investigations, and recommendations from the State of 

Hawaii Department of Health (HDOH). 

1.1 Project Objective 

This groundwater sampling project was performed to evaluate the presence of chemicals of 

potential concern in groundwater underlying the Facility. The project was conducted to ensure 

the Navy remains in compliance with HDOH UST release response requirements as described in 

Hawaii Administrative Rules (HAR) 11-281 Subchapter 7, Release Response Action. The 

groundwater sampling program followed the procedures described in Red Hill Bulk Fuel Storage 

Facility Groundwater Protection Plan [TEC Inc. (TEC), 2008], also referred to as “the Plan”. 

This groundwater sampling event was conducted by TEC under United States (US) Navy 

Contract Number N47408-04-D-8514, Task Order No. 54. 

1.2 Previous Reports 

The following groundwater monitoring reports were previously submitted to the HDOH: 

1. Groundwater Sampling Report, First Quarter 2005 (submitted April 2005); 

2. Groundwater Sampling Report, Second Quarter 2005 (submitted August 2005); 

3. Groundwater Sampling Report, Third Quarter 2005 (submitted November 2005); 

4. Groundwater Sampling Report, Fourth Quarter 2005 (submitted February 2006); 

5. Groundwater Monitoring Results, July 2006 (submitted September 2006); 

6. Groundwater Monitoring Results, December 2006 (submitted January 2007); 

7. Groundwater Monitoring Results, March 2007 (submitted May 2007); 

8. Groundwater Monitoring Results, June 2007 (submitted August 2007); 

9. Groundwater Monitoring Results, September 2007 (submitted October 2007); 

10. Groundwater Monitoring Results, January 2008 (submitted March 2008); 

11. Groundwater Monitoring Results, April 2008 (submitted May 2008); 

12. Groundwater Monitoring Results, July 2008 (submitted October 2008); 

13. Groundwater Monitoring Results, October and December 2008 (submitted February 

2009); and 

14. Groundwater Monitoring Results, February 2009 (submitted May 2009) 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

8 

1.3 Background 

The following sections provide a description of the site and information on the Facility and USTs. 

1.3.1 Site Description 

The Facility is located in Halawa Heights on Oahu, Hawaii. Land adjacent to the north of the 

Facility is occupied by Halawa Correctional Facility and private businesses. Land to the south 

and west of the Facility includes the Coast Guard Reservation. Moanalua Valley is located east 

of the Facility (Dawson, 2006). 

The Navy Public Works Department operates a potable water infiltration tunnel approximately 

1,550 feet hydraulically down-gradient from the Facility (Dawson, 2006). The US Navy Well 

2254-01 is located approximately 3,000 feet down-gradient (west) of the Facility and provides 

approximately 24% of the potable water to the Pearl Harbor Water System, which serves 

approximately 52,200 military consumers (TEC, 2008). 

1.3.2 Facility Information 

The Facility consists of 18 active and 2 inactive USTs operated by Navy FISC Pearl Harbor. 

Each UST has a capacity of 12.5 million gallons. The Facility is located approximately 100 feet 

above the basal aquifer (Dawson, 2006). 

1.3.3 UST Information 

The USTs were constructed in the early 1940s. The tanks were constructed of steel and currently 

contain Jet Propulsion (JP)–5 fuel and F-76 (diesel marine fuel). Previously, several tanks stored 

Navy Special Fuel Oil, Navy Distillate, aviation gasoline, and motor gasoline. Each tank 

measures approximately 245 feet in height and 100 feet in diameter. The upper domes of the 

tanks lie at depths varying between approximately 100 feet and 200 feet below the existing 

ground surface (TEC, 2006). 

1.4 Previous Environmental Investigations 

1998 to 2001: From 1998 to 2001, the Navy conducted an investigation at the Facility to assess 

potential releases from the fuel storage USTs and piping systems. In February 2001, the Navy 

installed a one-inch diameter RHMW01 (previously known as MW-V1D) to monitor for 

contamination of the basal aquifer underlying the Facility. The well was installed and completed 

at approximately 100 feet below grade within the lower access tunnel. At the time of well 

completion, depth to water in RHMW01 was measured at 86 feet below grade (Dawson, 2006). 

In February 2001, groundwater samples collected from RHMW01 contained total petroleum 

hydrocarbons (TPH) concentrations ranging from 883 micrograms per liter (g/L) to 1,050 g/L 

and total lead ranging from 10.4 g/L to 15 g/L. The maximum total lead concentration in the 

samples was equal to the primary drinking water standard of 15 g/L for lead and exceeded the 

HDOH Tier 1 groundwater action level of 5.6 g/L (Dawson, 2006). 

2005 – Groundwater Sampling: The Navy began quarterly groundwater sampling at existing 

monitoring wells in 2005. Dawson Group, Inc. collected groundwater samples from RHMW01 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

9 

and the Red Hill Navy Pump Station (US Navy Well 2254-01) in February, June, September, and 

December 2005. 

Samples collected in February and June 2005 were not filtered in the field prior to analysis for 

lead. Analytical results for samples collected from RHMW01 indicated concentrations of total 

lead were above the HDOH Tier 1 action level of 5.6 g/L. The results were not considered 

appropriate for risk assessment since the sample had not been filtered. In addition, lead was not 

a component of fuels from the tanks near RHMW01. Lead may have been part of the Facility 

construction material (TEC, 2007). 

Samples were filtered in September and December 2005, and dissolved lead concentrations were 

below the HDOH Tier 1 action level. Concentrations of all other contaminants of potential 

concern were below HDOH Tier 1 action levels. 

2005 – Site Investigation: As part of a site investigation, TEC installed three groundwater 

monitoring wells at the Facility between June and September 2005. Well RHMW02 was 

installed in the lower access tunnel near Tanks 5 and 6. Well RHMW03 was installed in the 

lower access tunnel near Tanks 13 and 14. Well RHMW04 was installed hydraulically 

upgradient of the USTs to provide geochemistry for water moving through the basal aquifer 

beneath the Facility. Wells RHMW02 and RHMW03 were completed to depths of 

approximately 125 feet below the tunnel floor, and well RHMW04 was completed to a depth of 

approximately 300 feet below ground surface outside the tunnel. Groundwater samples were 

collected from the three newly installed wells and two existing wells (RHMW01 and US Navy 

Well 2254-01) in September 2005. 

Naphthalene and trichloroethylene were detected in samples collected from RHMW02 at 

concentrations greater than the HDOH Tier 1 action levels. Lead was detected in the sample 

collected from RHMW01 at a concentration greater than the HDOH Tier 1 action level; 

however, the sample was not filtered in the field prior to analysis. Analytical results for filtered 

samples obtained by Dawson during the same period indicated concentrations of dissolved lead 

were below the HDOH Tier 1 action level. 

2006 – Site Investigation: Dedicated sampling pumps were installed in five wells (RHMW01, 

RHMW02, RHMW03, RHMW04, and US Navy Well 2254-01). TEC collected groundwater 

samples from the wells in July 2006. The groundwater samples were analyzed for petroleum 

constituents. Naphthalene was detected in samples collected from RHMW02 at concentrations 

above the HDOH Tier 1 action level. 

In September 2005, with concurrence from the HDOH, the Navy decided to use the newer 

HDOH Environmental Action Levels (EALs) for the Red Hill Site Investigation and Risk 

Assessment project. The EALs are current and provide action levels for more chemicals, and are 

much more useful for conducting screening risk assessments. Since the HDOH (HDOH May 

2005) Policy Letter stated that the two sets of action levels should not be mixed, the Tier 1 

screening levels presented in HAR Section 11-281-78 would no longer be used to evaluate 

environmental impact at the Facility. 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

10 

2006 – Groundwater Sampling: Groundwater samples were collected in December 2006. 

Analytical results indicated the following: 

 No chemicals were detected in groundwater from US Navy Well 2254-01 or RHMW03; 

 TPH as diesel range organics (TPH-DRO) was detected in groundwater above the HDOH 

Drinking Water EALs in RHMW01; and 

 TPH as gasoline range organics (TPH-GRO), TPH-DRO, and naphthalene were detected 

in groundwater above the HDOH Drinking Water EALs in RHMW02. 

2007 – Groundwater Sampling: Groundwater samples were collected in March, June, and 

September 2007. Analytical results indicated the following: 

 No chemicals were detected above HDOH Drinking Water EALs at US Navy Well 

2254-01; 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW01 during all three 

sampling events; 

 TPH-GRO exceeded HDOH Drinking Water EALs at RHMW02 in March; 

 TPH-DRO and naphthalene exceeded HDOH Drinking Water EALs at RHMW02 during 

all three sampling events; 

 1-methylnaphthalene and 2-methylnaphthalene exceeded the HDOH Groundwater Gross 

Contamination EAL at RHMW02 during all three sampling events; and 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW03 in June. 

2008 – Groundwater Sampling: Groundwater samples were collected in January, April, July, 

and October 2008. Analytical results indicated the following: 

 No chemicals were detected above HDOH Drinking Water EALs at US Navy Well 

2254-01; 

 Trace detections of 1-methylnaphthalene and naphthalene prompted a resample event in 

December at US Navy Well 2254-01, no chemicals were detected above the MDL; 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW01 during all four sampling 

events; 

 TPH-GRO did not exceed HDOH Drinking Water EALs at RHMW02; 

 TPH-DRO, naphthalene, 1-methylnaphthalene, and 2-methylnaphthalene exceeded 

HDOH Drinking Water EALs at RHMW02; and 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW03 during all four sampling 

events. 

2009 – Groundwater Sampling: Groundwater samples were collected in February 2009. 

Analytical results indicated the following: 

 No chemicals were detected above HDOH Drinking Water EALs at US Navy Well 

2254-01; 

 Trace TPH-GRO at US Navy Well 2254-01 was reported just above the laboratory MDL 

and significantly below the laboratory reporting limit and HDOH EAL; 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW01; 

 TPH-GRO did not exceed HDOH Drinking Water EALs at RHMW02; 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

11 

 TPH-DRO, naphthalene, 1-methylnaphthalene, and 2-methylnaphthalene exceeded 

HDOH Drinking Water EALs at RHMW02; and 

 TPH-DRO exceeded HDOH Drinking Water EALs at RHMW03. 

1.5 Regulatory Updates 

During the summer and fall of 2008, HDOH updated their EALs, which resulted in significant 

changes to the action levels associated with methylnaphthalenes. The drinking water toxicity 

EAL for these compounds was 240 g/L. This concentration presumed that methylnaphthalenes 

were non-carcinogenic. Evidence that they are human carcinogens has now been accepted by the 

US Environmental Protection Agency (USEPA). As a result, HDOH adopted more rigorous 

EALs of 4.7 g/L for 1-methylnaphthalene and 24 g/L for 2-methylnaphthalene, corresponding 

to a residential tap water scenario, and a 1 in a million cancer risk (HDOH, 2008). 

The drinking water EAL for naphthalene has also been updated during this process. Previously, 

HDOH based their naphthalene EAL on USEPA Region 9 Preliminary Remediation Goal 

(USEPA PRG) of 6.2 g/L, which is associated with a non-cancer Hazard Index of 1. HDOH 

has updated their naphthalene drinking water EAL to 17 g/L, in deference to the California 

Department of Public Health’s Drinking Water Notification Levels, a Hazard Index of 2.7 

(HDOH, 2008). 

Finally, the HDOH Drinking Water EAL for TPH-DRO was increased from 100 g/L to 210 

g/L, although the HDOH Groundwater Gross Contamination EAL for TPH-DRO remains 100 

g/L. 

1.6 RHMW05 Installation 

In April 2009, a new groundwater monitoring well, RHMW05, was installed by TEC under US 

Navy Contract Number N47408-04-D-8514, Task Order No. 54. RHMW05 is located downgradient from the Facility, within the lower access tunnel between RHMW01 and RHMW2254-

01(located at the US Navy Well 2254-01). It was installed to identify the extent of contaminant 

migration down-gradient prior to contaminants reaching the infiltration gallery at the US Navy 

Well 2254-01. 

2.0 Sample Collection and Analyses 

Field activities relating to groundwater sample collection were conducted on May 13, 2009. 

Groundwater samples were collected from four monitoring wells located inside the Facility 

lower access tunnel and one monitoring well located at the Red Hill Navy Pump Station. 

Sampling and analysis were conducted according to Red Hill Bulk Fuel Storage Facility 

Groundwater Protection Plan (TEC, 2009). A total of eight samples were collected as follows: 

 one environmental sample from RHMW2254-01 (i.e., located at the US Navy Well 

2254-01), RHMW01, RHMW02, RHMW03, and RHMW05; 

 one duplicate sample from RHMW02 (sampled as RHMWA01 and reported as 

RHMW02D); and 

 one matrix spike and matrix spike duplicate from RHMW2254-01. 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

12 

2.1 Monitoring Well Purging 

Following monitoring well installation, well development of RHMW05 was conducted on April 

27, 2009. During this process, more than ten well volumes of groundwater (i.e. 25 gallons total) 

were purged and intermittent mechanical surging was conducted using a stainless steel bailer. 

On May 6, 2009, nine additional gallons were purged from RHMW05 using a dedicated bailer. 

Prior to sampling on May 13, nine gallons more were purged from RHMW05 to allow for the 

collection of a representative groundwater sample. Field parameters were measured at regular 

intervals to ensure parameter stabilization during development and sampling activities. 

All monitoring wells were purged prior to sampling. Well purging was considered complete 

when no less than three successive water quality parameter measurements had stabilized within 

approximately 10 percent. Field parameters were measured at regular intervals during well 

purging and included pH, temperature, specific conductivity, dissolved oxygen, and turbidity. 

Purge water was collected and disposed in the Facility oil/water separator system. 

2.2 Groundwater Sample Collection 

Each monitoring well was sampled immediately following purging. All wells were sampled 

directly from their dedicated bladder pump system, except for RHMW05. RHMW05 was 

sampled using a dedicated bailer. Samples were placed into sampling containers with 

appropriate preservatives [i.e., hydrochloric acid (HCl) for volatile organic analysis, nitric acid 

(HNO3) for dissolved lead]. Dissolved lead samples were filtered in the field and placed in 

preserved bottles. Sample containers were labeled with the date, sample identification number, 

type of analysis, and sampler’s name. The containers were placed on ice in sample coolers and 

transported under chain-of-custody procedures to the certified laboratory for analysis. 

2.3 Groundwater Sample Analyses 

Groundwater samples were analyzed by SGS Environmental Service, Inc. in Anchorage, Alaska 

for TPH-DRO and TPH-GRO by EPA Method 8015B, VOCs by EPA Method 8260B, 

polynuclear aromatic hydrocarbons (PAHs) by EPA Method 8270C SIM, and dissolved lead by 

EPA Method 6020. 

3.0 Groundwater Sample Analytical Results 

This section provides a summary of analytical results for groundwater samples collected from 

four monitoring wells located in the lower access tunnel of the Facility and one monitoring well 

located at the Red Hill Navy Pump Station. Duplicate sample results from monitoring wells 

RHMW02 are reported in this document as RHMW02D. A summary of groundwater analytical 

results is included in Table 1. Complete analytical laboratory reports are provided in Appendix 

A. 

3.1 May 2009 Sample Analytical Results 

All groundwater samples were analyzed for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved 

lead. The trip blank sample (i.e., a blank sample provided by the lab and transported with the 

sample bottles to detect the potential incursion of contaminants from outside sources) was 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

13 

analyzed for TPH-GRO and VOCs. The results for each groundwater monitoring well are 

discussed below. 

RHMW01

TPH-DRO at 373 μg/L exceeded the HDOH Drinking Water EAL of 210 μg/L. Trace 

concentrations of TPH-GRO, fluorene, naphthalene, and acenaphthalene were detected below 

HDOH EALs (Table 1). All other constituents were not detected. 

RHMW02

Six petroleum constituents were detected at RHMW02: TPH-DRO, TPH-GRO, 1-

methylnaphthalene, 2-methylnaphthalene, naphthalene, and phenanthrene. TPH-DRO was 

detected at RHMW02 in the normal and duplicate samples, at 1,620 μg/L and 2,000 μg/L, 

respectively. This result exceeded the HDOH EAL of 210 μg/L, but not the site-specific risk 

based level (SSRBL) of 4,500 μg/L. TPH-GRO was detected at a concentration below the 

HDOH Drinking Water EAL of 100 μg/L with an average estimated concentration of 37.9 μg/L 

(i.e., an average of the normal and duplicate sample). 

Naphthalene was analyzed by USEPA Method 8270C SIM and USEPA Method 8260B. Only 

USEPA Method 8270C SIM detected naphthalene above the MDL, at an average concentration 

of 1.125 μg/L from the normal and duplicate sample, but below the HDOH Drinking Water EAL 

of 17 μg/L. In addition, 1-methylnaphthalene and 2-methylnapthalene were detected by USEPA 

Method 8270C SIM in the normal and duplicate samples. The average result for 1-

methylnaphthalene was 21.25 μg/L, greater than the HDOH Drinking Water EAL of 4.7 μg/L. 

The average result for 2-methylnaphthalene was 0.1215 μg/L, significantly less than the HDOH 

Drinking Water EAL of 24 μg/L and the HDOH Groundwater Gross Contamination EAL of 10 

g/L. The only other petroleum constituent detected was phenanthrene found at estimated 

concentrations significantly below HDOH Drinking Water EALs (Table 1). 
Page 1 of 1

Table 1. Analytical Results for Quarterly Groundwater Monitoring Release Response Report (May 13, 2009)

Red Hill Fuel Storage Facility, Pearl Harbor, Hawaii

Result Q MDL RL Result Q MDL RL Result Q MDL RL Result Q MDL RL Result Q MDL RL Result Q MDL RL

TPH as DIESEL RANGE ORGANICS 210 100 373 F 169 449 1620 167 444 2000 160 426 ND U 161 430 200 F 161 430 ND U 169 449

TPH as GASOLINE RANGE ORGANICS 100 100 16.6 F 10 100 39.1 F 10 100 36.7 F 10 100 14.8 F 10 100 13.2 F 10 100 19.1 F 10 100

1-METHYLNAPHTHALENE 4.7 10 ND U 0.015 0.05 17.9 0.15 0.5 24.6 0.155 0.515 ND U 0.0152 0.0505 ND U 0.0158 0.0526 ND U 0.0156 0.0521

2-METHYLNAPHTHALENE 24 10 ND U 0.015 0.05 0.136 0.015 0.05 0.107 0.0155 0.0515 ND U 0.0152 0.0505 ND U 0.0158 0.0526 0.018 F 0.0156 0.0521

ACENAPHTHENE 370 20 0.0243 F 0.015 0.05 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.0152 0.0505 ND U 0.0158 0.0526 ND U 0.0156 0.0521

ACENAPHTHYLENE 240 2000 ND U 0.015 0.05 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.0152 0.0505 ND U 0.0158 0.0526 ND U 0.0156 0.0521

ANTHRACENE 1800 22 ND U 0.015 0.05 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.0152 0.0505 ND U 0.0158 0.0526 ND U 0.0156 0.0521

BENZO(a)ANTHRACENE 0.092 4.7 ND U 0.015 0.05 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.0152 0.0505 ND U 0.0158 0.0526 ND U 0.0156 0.0521

BENZO(a)PYRENE 0.2 0.81 ND U 0.015 0.05 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.0152 0.0505 ND U 0.0158 0.0526 ND U 0.0156 0.0521

BENZO(b)FLUORANTHENE 0.092 0.75 ND U 0.015 0.05 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.0152 0.0505 ND U 0.0158 0.0526 ND U 0.0156 0.0521

BENZO(g,h,i)PERYLENE 1500 0.13 ND U 0.015 0.05 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.0152 0.0505 ND U 0.0158 0.0526 ND U 0.0156 0.0521

BENZO(k)FLUORANTHENE 0.92 0.4 ND U 0.015 0.05 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.0152 0.0505 ND U 0.0158 0.0526 ND U 0.0156 0.0521

CHRYSENE 9.2 1 ND U 0.015 0.05 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.0152 0.0505 ND U 0.0158 0.0526 ND U 0.0156 0.0521

DIBENZ(a,h)ANTHRACENE 0.0092 0.52 ND U 0.015 0.05 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.0152 0.0505 ND U 0.0158 0.0526 ND U 0.0156 0.0521

FLUORANTHENE 1500 130 ND U 0.015 0.05 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.0152 0.0505 ND U 0.0158 0.0526 ND U 0.0156 0.0521

FLUORENE 240 950 0.0246 F 0.015 0.05 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.0152 0.0505 ND U 0.0158 0.0526 ND U 0.0156 0.0521

INDENO(1,2,3-c,d)PYRENE 0.092 0.095 ND U 0.015 0.05 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.0152 0.0505 ND U 0.0158 0.0526 ND U 0.0156 0.0521

NAPHTHALENE 17 21 0.182 0.031 0.1 1.17 0.031 0.1 1.08 0.032 0.103 ND U 0.0313 0.101 ND U 0.0326 0.105 ND U 0.0323 0.104

PHENANTHRENE 240 410 ND U 0.015 0.05 0.0162 F 0.015 0.05 0.0171 F 0.0155 0.0515 ND U 0.0152 0.0505 ND U 0.0158 0.0526 ND U 0.0156 0.0521

PYRENE 180 68 ND U 0.015 0.05 ND U 0.015 0.05 ND U 0.0155 0.0515 ND U 0.0152 0.0505 ND U 0.0158 0.0526 ND U 0.0156 0.0521

1,1,1,2-TETRACHLOROETHANE 0.52 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5

1,1,1-TRICHLOROETHANE 200 970 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

1,1,2,2-TETRACHLOROETHANE 0.067 500 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5

1,1,2-TRICHLOROETHANE 5 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

1,1-DICHLOROETHANE 2.4 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

1,2,3-TRICHLOROPROPANE (TCP) 0.6 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

1,2,4-TRICHLOROBENZENE 70 3000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

1,2-DIBROMO-3-CHLOROPROPANE (DBCP) 0.04 10 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2

1,2-DIBROMOETHANE (EDB) 0.0065 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

1,2-DICHLOROBENZENE 600 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

1,2-DICHLOROETHANE 0.15 700 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5

1,2-DICHLOROPROPANE 5 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

1,3-DICHLOROBENZENE 180 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

1,3-DICHLOROPROPENE 0.43 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5

1,4-DICHLOROBENZENE 75 5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5

ACETONE 22000 20000 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 10.4 3.1 10 ND U 3.1 10

BENZENE 5 170 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4

BROMODICHLOROMETHANE 0.22 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5

BROMOFORM 100 510 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

BROMOMETHANE 8.7 50000 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3

CARBON TETRACHLORIDE 5 520 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

CHLOROBENZENE 100 50 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5

CHLOROETHANE 8600 16 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

CHLOROFORM 70 2400 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1

CHLOROMETHANE 1.8 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

cis-1,2-DICHLOROETHYLENE 70 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

DIBROMOCHLOROMETHANE 0.16 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5

ETHYLBENZENE 700 30 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

HEXACHLOROBUTADIENE 0.86 6 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

M,P-XYLENE (SUM OF ISOMERS) 10000 20 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2

METHYL ETHYL KETONE (2-BUTANONE) 7100 8400 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10

METHYL ISOBUTYL KETONE (4-METHYL-2-PENTANONE) 2000 1300 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10

METHYLENE CHLORIDE 4.8 9100 ND U 1 5 ND U 1 5 ND U 1 5 ND U 1 5 ND U 1 5 ND U 1 5

NAPHTHALENE 17 21 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2

STYRENE 100 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

TETRACHLOROETHYLENE(PCE) 5 170 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

TOLUENE 1000 40 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

trans-1,2-DICHLOROETHENE 100 260 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

TRICHLOROETHYLENE (TCE) 5 310 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

VINYL CHLORIDE 2 3400 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

6020 LEAD 15 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1

PAHs - Polynuclear aromatic hydrocarbons MDL - Method detection limit

VOCs - Volatile organic compounds RL - Reporting limit

UG/L - Micrograms per Liter TPH - Total petroleum hydrocarbons 

Q - Data qualifier ND - Indicates that the compound was not detected above the stated method detection limit

U - Indicates that the compound was analyzed for but not detected at or above the stated limit NA - not analyzed

F - Indicates that the compound was identified but the concentration was above the MDL and below the RL

- Result exceeds one or both HDOH EALs

1

2

Method

HDOH Drinking Water 

EALs1

for Human Toxicity 

UG/L

HDOH Groundwater 

Gross Contamination 

EALs2

UG/L

Final Drinking Water Action Levels for Human Toxicity, Table D-3a, Screening for Environmental Concerns at Sites with 

Contaminated Soil and Groundwater, HDOH, 2009

Groundwater Gross Contamination Action Levels, Table G-1, Screening for Environmental Concerns at Sites with 

Contaminated Soil and Groundwater, HDOH, 2009

8015B (Petroleum)

8270C SIM 

(PAHs)

8260B 

(VOCs)

UG/L

RHMW03

UG/L

May 13, 2009 May 13, 2009 May 13, 2009 May 13, 2009 May 13, 2009 May 13, 2009 Chemical

RHMW01

UG/L

RHMW05

UG/L

RHMW2254

UG/L

RHMW02

UG/L

RHMW02D

200
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

15 

RHMW03

One constituent was detected at RHMW03: TPH-GRO (Table 1). TPH-GRO was detected at an 

estimated 14.8 μg/L, significantly below the HDOH Drinking Water EALs of 100 μg/L. All 

other constituents were not detected above the MDL at RHMW03. 

RHMW05

TPH-DRO was detected at a concentration of 200 μg/L. This concentration is just below the 

HDOH Drinking Water EAL of 210 μg/L, but greater than the HDOH Groundwater Gross 

Contamination EAL of 100 μg/L. Trace concentrations of TPH-GRO and acetone (a common 

laboratory solvent) were detected below HDOH EALs (Table 1). All other constituents were not 

detected. 

US Navy Well 2254-01

TPH-GRO and 2-methylnaphthalene were reported just above the MDL at estimated 

concentrations of 19.1 μg/L and 0.018 μg/L, respectively. The HDOH Drinking Water EALs for 

TPH-GRO and 2-methylnaphthalene are 100 μg/L and 24 μg/L, respectively. 

3.2 Groundwater Contaminant Trend 

Groundwater samples have been collected and analyzed by TEC since September 2005. Figure 1 

shows TPH trends in groundwater at the Facility. Figure 2 shows PAH trends in groundwater at 

the Facility. In these figures, open icons (without data) represent locations where the compounds 

being analyzed were not detected. 

RHMW01

TPH-GRO has only previously been detected in April 2008 and February 2009 at estimated 

values below the HDOH Drinking Water EAL of 100 μg/L. In May 2009, TPH-GRO was 

detected at an estimated value of 16.6 μg/L. TPH-DRO has been detected above the HDOH 

Drinking Water EAL during all groundwater sampling events. The concentration of TPH-DRO 

observed in May 2009 (i.e., 373 μg/L) shows a decreasing trend over the last three consecutive 

sampling events, after an increase in October 2008 (i.e., 459 μg/L). Prior to the October 2008 

sampling event, TPH-DRO concentrations had decreased for three consecutive sampling rounds. 

RHMW02

TPH-GRO was detected in all but one of the sampling rounds since September 2005, and 

exceeded the HDOH Drinking Water EAL of 100 μg/L three times during 2006 and 2007. The 

maximum concentration detected has been 148 μg/L. TPH-GRO shows a decreasing trend with 

the lowest concentration since September 2005 detected in May 2009 (i.e., the average of normal 

and duplicate samples of 37.9 μg/L). 

The concentration of TPH-DRO was relatively stable at RHMW02 until July 2008, ranging from 

2,250 to 2,995 μg/L. However, during the July and October 2008 sampling events, these average 

concentrations increased (i.e., average between the normal and duplicate samples). Specifically, 

the July 2008 average concentration was 4,055 μg/L and the October 2008 average concentration 

was 5,420 μg/L. Both of these values were significantly above the HDOH Drinking Water EAL 

of 210 μg/L, with the October 2008 average also exceeding the SSRBL of 4,500 μg/L. TPH-
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

16 

DRO at RHMW02 has shown a decreasing trend since October 2008. The average concentration 

of TPH-DRO observed during the May 2009 sampling event (i.e., 1,810 μg/L) was below 50 

percent of the SSRBL for the first time since September 2005. The decrease in the May 2009 

sampling event downgraded RHMW02 to a Category 2 status from the previous Category 3 

status that followed the February 2009 sampling event. 

1-Methylnaphthalene at RHMW02 remains above the HDOH Drinking Water EAL (i.e., 4.7 

μg/L). However, naphthalene has decreased below the HDOH Drinking Water EAL (i.e., 17 

μg/L). In general, PAH concentrations have been decreasing after a slightly increasing trend 

through July 2008. 

RHMW03

TPH-GRO had never been detected prior to February 2009. In May 2009 there was a slight 

decrease from the February 2009 sampling event. TPH-GRO decreased from estimated values of 

16.1 μg/L in February 2009 to 14.8 μg/L in May 2009, both estimated values significantly below 

the HDOH Drinking Water EAL of 100 μg/L. 

TPH-DRO had shown a slightly increasing trend that peaked at 244 μg/L during the October 

2008 sampling event. During the May 2009 sampling event TPH-DRO was not detected above 

the MDL, following a decreasing trend since October 2008. In the past, the concentrations of 

TPH-DRO have remained relatively stable, near the DOH Drinking Water EAL of 210 μg/L. 

Concentrations of petroleum-related compounds at RHMW03 have normally been lower than 

those detected at RHMW01 or RHMWO2. 

RHMW05

Based upon the May 2009 sampling event, the first event for this newly installed well, TPHDRO was detected at an estimated concentration of 200 g/L, which is below the HDOH 

Drinking Water EAL of 210 g/L. However, since this is the first sampling event for RHMW05, 

no contamination trend (i.e., two or more consecutive sampling rounds) has yet to be observed. 

US Navy Well 2254-01

The US Navy Well 2254-01 has been given a provisional Category 1 status for the first time 

since quarterly sampling has been conducted by TEC. Category 1 status has been assigned to the 

US Navy Well 2254-01 because over the course of the past two sampling events, (i.e., February 

and May 2009) TPH-GRO has been reported at trace concentrations above the MDL, but was 

below the HDOH Drinking Water EAL of 100 g/L with relatively stable concentrations (i.e., an 

estimated value of 14 g/L in February and 19.1 g/L in May). However, it is noteworthy that 

the associated laboratory method blank also contained estimated trace concentrations of TPHGRO. 

3.3 Results of Oil/Water Interface Measurements 

The presence and thickness of light-non aqueous phased liquids (LNAPL), otherwise known as 

free product, released from the USTs were measured during this sampling event using a 300 foot 

Heron Oil/Water Interface Meter. The static water levels were measured to a precision of ± 0.01 

feet and fuel thickness was measured to a precision of ± 0.01 feet with this equipment. 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

17 

In January 2008, fuel was measured in monitoring wells RHMW01 and RHMW02 at a thickness 

of < 0.01 ft, but has not been observed in other monitoring wells. 

Measurements to determine the presence and thickness of fuel were conducted at RHMW01, 

RHMW02, and RHMW03 prior to the May 2009 sampling round. At the end of May a 

subsequent round of oil/water interface measurements was conducted. No free product was 

observed in any of these wells during either of the May 2009 events (see Table 2). 

Table 2. Oil/Water Interface Measurements 

        

Date 

RHMW01 RHMW02 RHMW03 

SWL 

(ft) 

LNAPL 

(ft) 

SWL 

(ft) 

LNAPL 

(ft) 

SWL 

(ft) 

LNAPL 

(ft) 

 January 2008 17.74 < 0.01 18.78 < 0.01 NT NT 

 July 2008 19.04 0.00 18.91 0.00 18.86 0.00 

October 2008 18.61 0.00 18.56 0.00 18.82 0.00 

November 2008 18.50 0.00 18.45 0.00 18.51 0.00 

January 2009 19.28 0.00 19.22 0.00 19.27 0.00 

February 2009 NT NT 18.66 0.00 18.75 0.00 

March 2009 18.59 0.00 18.57 0.00 18.67 0.00 

May 2009* 18.69 0.00 18.64 0.00 18.72 0.00 

May 2009 18.91 0.00 18.86 0.00 18.90 0.00 

 

SWL Static water level, elevation above mean sea level 

LNAPL Light Non-Aqueous Phased Liquid, fuel product on groundwater 

ft Feet 

NT Not Taken 

* The measurements scheduled for April 2009 were conducted on May 6, 2009 

due to RHMW05 drilling activities 

3.4 Groundwater Status 

Constituents of concern are defined as petroleum-related chemicals that have been observed in 

the groundwater samples above the HDOH EALs. In accordance with the Red Hill Bulk Fuel 

Storage Facility Final Groundwater Protection Plan (TEC, 2008), Table 3 defines the 

constituents of concern in groundwater at the Facility and the SSRBLs and updated EALs for 

each (HDOH 2008). 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

18 

Table 3. Action Levels for Constituents of Concern 

Chemical EAL (μg/L) SSRBL (μg/L) 

Petroleum Mixtures 

TPH-DRO 210 4,500 

TPH-GRO 100 4,500 

Semi-Volatile Compounds 

1-Methylnaphthalene 4.7 NA 

2-Methylnaphthalene 24 NA 

Naphthalene 17 NA 

NA – Not applicable or not determined 

SSRBLs are applicable at RHMW01, RHMW02, RHMW03, and RHMW05 

EALs are applicable at US Navy Well 2254-01 

In addition, the Plan defines four results categories of groundwater status for the Facility, based 

on concentrations of constituents of concern in RHMW01, RHMW02, RHMW03 and the US 

Navy Well 2254-01, and requires specific responses when these categories are observed during 

quarterly groundwater sampling. Table 4 describes each of the four results categories and 

identifies response actions to be taken in accordance with the Plan. 

 Table 4. Results Categories and Response Actions to Changes in Groundwater Status 

Results Category RHMW02 

RHMW03 or 

RHMW05* 

RHMW01 US Navy Pumping 

Well 2254-01 

Results Category 1: Result above 

detection limit but below drinking 

water EAL and trend for all 

compounds stable or decreasing 

A A A,D,M,E 

Results Category 2: Trend for any 

compound increasing or drinking 

water EAL exceeded 

A, B A, B A,B,C,D,E,F,G,K, 

L,O 

Results Category 3: Result 

Between 1/10X SSRBL and 

SSRBL for benzene, or between 

1/2X SSRBL and SSRBL for TPH 

A,B,G,H,I,J A,B,E,G,H,I,J A,B,C,D,E,F,G,I,J,

K,L,O 

Results Category 4: Result 

Exceeding any SSRBL or 

petroleum product observed 

A,C,D,E,F,I,J, 

K,M,N 

A,C,D,E,F,I, 

J,K,M,N,O 

A,C,D,E,F,G,I,J,K,

L,O 

*RHMW05 was installed in April 2009 and has been subsequently been added to this Table. 

Specific Responses: 

A. Send quarterly reports to HDOH 

B. Begin program to determine the source of leak 

C. Notify HDOH verbally within 1 day and follow with written notification in 30 days 

D. Notify FISC Chain of Command within 1 day 

E. Send Type 1 Report (see box below) to HDOH 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

19 

F. Send Type 2 Report (see box below) to HDOH 

G. Increase monitoring frequency to once per month (if concentrations increasing) 

H. Notify HDOH verbally within 7 days and follow with written notification in 30 days 

I. Remove sampling pumps, measure product in pertinent wells with interface probe, re-install 

pumps if product is not detected. 

J. Immediately determine leaking tank 

K. Collect samples from nearby Halawa Deep Monitoring Well (2253-03) and OWDF MW01 

L. Provide alternative water source at 2254-01 

M. Prepare for alternative water source at US Navy Well 2254-01 

N. Re-measure for product every month with reports to HDOH 

O. Install additional monitoring well downgradient 

Report Types 

HDOH Type 1 Report 

 Re-evaluate Tier 3 Risk Assessment/groundwater model results 

 Proposal to HDOH on a course of action 

HDOH Type 2 Report 

 Proposal for groundwater treatment 

Free Product Measurements

In response to the previous Category 3 status at RHMW02, free product measurements were 

collected in October 2008, November 2008, January 2009, February 2009, March 2009, and May 

2009 at Red Hill tunnel monitoring wells (Table 2). To date, there is no evidence of fuel on 

groundwater at any of these wells based upon these measurements. These free product 

measurements are planned to continue on a monthly basis. 

RHMW05

Based upon the May 2009 sampling event, the first event for this newly installed well, RHMW05 

avoids being placed in Category 1 status. This is because although the TPH-DRO estimated 

concentration of 200 g/L is above the MDL, but below the HDOH Drinking Water EAL of 210 

g/L, no contamination trend (i.e., two or more consecutive sampling rounds) has yet to be 

observed. 

Category 1 Status Locations

US Navy Well 2254-01(measured at RHMW2254-01) 

Following the May 2009 sampling event, the US Navy Well 2254-01 is now in a provisional 

Category 1 status because over the course of the past two sampling events (i.e., February and 

May 2009) TPH-GRO has been detected above the MDL, but below the HDOH Drinking Water 

EAL of 100 g/L with relatively stable concentrations (i.e., an estimated value of 14 g/L in 

February and 19.1 g/L in May). 

The laboratory Practical Quantification Limit (PQL) or Reporting Limit (RL) for TPH-GRO is 

100 ug/l. The RHMW2254-01 May 2009 sample result was assigned an estimated “J” value of 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

20 

19.1 ug/l; which is five times below the laboratory PQL or RL. However, the associated 

laboratory method blank also gave an estimated “J” value of 14.9 ug/l. The pattern observed in 

the RHMW2254-01 sample chromatogram matches the pattern in the laboratory method blank. 

Based on evaluation of these data, it appears that the MDL for the TPH-GRO of 10 ug/l may be 

set too low. Standard laboratory procedures would typically set the MDL at approximately 1/3 

of the PQL or 30 ug/l and not at 10 ug/l or 3 times lower than that level. 

The TPH-GRO method measures the area of peaks over an integration range. Thus, any slight 

changes in the baseline could be counted as TPH-GRO. This is different than methods that 

target a single peak (e.g., benzene) where the baseline is much easier to define. Consequently, 

any changes in the condition of the instrument may produce slight baseline changes giving an 

indication that TPH-GRO is present. Since the residual TPH-GRO response over the integration 

range for RHMW2254-01 and the associated method blank both gave estimated positive values, 

the estimated value of 19.1 ug/l for RHMW2254-01 may represent a “false positive”. Due to this 

uncertainty, a provisional Category 1 status has been assigned to the US Navy Well 2254-01. 

This provisional status will be reevaluated following the next quarterly sampling event. 

Category 1 status for the US Navy Well 2254-01 requires: 

1. Quarterly reports to be sent to HDOH; 

2. Notification of the FISC chain of command within 1 day; 

3. Reevaluate Tier 3 Risk Assessment and groundwater model results and develop a course 

of action proposal for HDOH; and 

4. As appropriate, prepare for alternative water source. 

RHMW03 

Based upon the May 2009 sampling event, RHMW03 remains in Category 1 status, because over 

the course of the past two sampling events (i.e., February and May 2009) TPH-GRO has been 

detected above the MDL, but was below the HDOH Drinking Water EAL of 100 g/L with 

relatively stable concentrations (i.e., an estimated value of 16.1 g/L in February and 14.8 g/L 

in May). 

Category 1 response for RHMW03 requires: 

1. Quarterly reports to be sent to HDOH. 

Category 2 Status Locations

RHMW01 

Results from the May 2009 sampling event indicate that RHMW01 remains in Category 2 status, 

since the TPH-DRO concentration of 373 g/L has been relatively stable and is greater than the 

HDOH Drinking Water EAL (210 g/L), but less than half the SSRBL of 4,500 g/L (estimated 

solubility limit of JP-5). 

RHMW02 

Results from the May 2009 sampling event indicate that RHMW02 is now downgraded from 

Category 3 to Category 2 status since TPH-DRO [1,620 g/L and 2,000 g/L (duplicate)] is 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

21 

greater than the HDOH Drinking Water EAL (210 g/L), but is less than one half the established 

SSRBL value of 4,500 g/L (estimated solubility limit of JP-5). 

Category 2 for RHMW01 and RHMW02 requires: 

3. Quarterly reports to be sent to HDOH; and 

4. Initiation of a leak determination program to identify if tanks are leaking. 

Category 3 or 4 Status Locations

There is no Category 3 or 4 status location. 

4.0 Summary and Conclusions 

Summary

At RHMW02, the concentration of TPH-DRO exceeded the Drinking Water EAL of 210 g/L 

and was less than one half of the established SSRBL value of 4,500 g/L, which places 

RHMW02 in a Category 2 status. This represents a downgrade from Category 3 status, which 

was prompted by the February 2009 sampling results. Although TPH-GRO was again detected 

at RHMW2254-01, it was also detected in laboratory method blank sample. The estimated TPHGRO concentration at RHMW2254-01 (i.e., 19.1 g/L) was significantly below the HDOH 

Drinking Water EAL of 100 μg/L and just above the MDL of 10 μg/L. 

Conclusions/Recommendations

 Oil/water interface measurements were collected in October 2008, November 2008, 

January 2009, February 2009, March 2009, and May 2009 from Red Hill tunnel 

monitoring wells and no free product was measured (Table 2). 

 The concentration of TPH-DRO measured at RHMW01 in May 2009 (373 g/L) 

exceeded HDOH EALs, but was less than one half of the SSRBL. RHMW01 is downgradient from RHMW02 and between RHMW02 and the US Navy Well 2254-01, an 

important drinking water source for the PHWS.

 The concentration of TPH-DRO measured at the new monitoring well, RHMW05, in 

May 2009 (200 g/L) was less than the HDOH Drinking Water EAL. RHMW05 is 

located between RHMW01 and the US Navy Well 2254-01. 

 The US Navy Well 2254-01 is not imminently threatened at this time; however, 

conditions should be monitored closely to determine whether or not the estimated value 

at RHMW2254-01 of 19.1 g/L of TPH-GRO from the May 2009 sampling event 

represents an analytical trend. 

 The following activities will be implemented to continue to monitor and/or clarify the 

groundwater contamination situation at the Facility: 

1. Re-evaluate risk assessment and groundwater model (TEC, 2007) to ensure both 

are valid and protective of human health and the environment under the existing 

conditions; 

2. Continue monthly free product measurements at RHMW01, RHMW02, and 

RHMW03, and include RHMW05 in future measurements and provide monthly 

letter reports of the results; 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

22 

3. Collect samples from nearby Halawa Deep Monitoring Well (2253-03), OWDF 

MW01, and RHMW04; 

4. Conduct Massachusetts Department of Environmental Protection (MADEP) 

extractable petroleum hydrocarbon and volatile petroleum hydrocarbon analysis 

to better characterize the dissolved fuel plume; 

5. Prepare for alternative water source at US Navy Well 2254-01, as necessary. 

6. Continue quarterly groundwater sampling for TPH-DRO, TPH-GRO, VOCs, 

PAHs, and lead until such time that new data indicates that a different monitoring 

program is warranted. The quarterly collection and analysis of groundwater 

samples will continue to monitor the quality of the groundwater located beneath 

the Facility. Groundwater monitoring reports will be submitted to the HDOH 

upon receipt and evaluation of laboratory analytical results. 

7. Closely monitor RHMW2254-01 to assess whether the detection of estimated 

trace quantities (i.e., 14 g/L) of TPH-GRO from the February 2009 sampling 

event and 19.1 g/L during the May 2009 event represent an analytical trend. In 

addition, due to the possibility of a “false positive” result reported for 

RHMW2254-01(see Section 3.4 discussion), the MDL for future analysis of TPHGRO will be increased to 30 g/L. 
Figure 1

TPH Trends in Groundwater

Round 15 (May 13, 2009)

Red Hill Fuel Storage Facility

Oahu, Hawaii

The HDOH toxicity EALs were updated in Fall, 2008. •TPH-DRO Residential Tap Water EAL is 210 ug/L; and •TPH-GRO Residential Tap Water EAL is 100 ug/L;

(HDOH, 2008).
Figure 2

PAH Trends in Groundwater

Round 15 (May 13, 2009)

Red Hill Fuel Storage Facility

Oahu, Hawaii

The HDOH toxicity EALs were updated in Fall, 2008. 

• Naphthalene Residential Tap Water EAL is 17 ug/L;

• 1-methylnaphthalene Residential Tap Water EAL is 4.7 ug/L; and

• 2- methylnaphthalene Residential Tap Water EAL is 24 ug/L

(HDOH, 2008).
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility July 2009 

 ____________________________________________________________________________________________ 

25 

5.0 References 

AMEC. Red Hill Bulk Fuel Storage Facility Investigation Report, Prepared for NAVFAC 

Pacific, August 2002. 

Dawson Group, Inc. Fourth Quarter 2005 Groundwater Sampling Report, Red Hill Fuel 

Storage Facility, Hawaii. February 2006. 

Hawaii Administrative Rules, Title 11, Chapter 281, Subchapter 7. 

HDOH. Screening for Environmental Concerns at Sites with Contaminated Soil and 

Groundwater, Summary Lookup Tables. March 2009. 

HDOH. Use of May 2005 Environmental Action Levels (“EALs”) at Leaking Underground 

Storage Tank Sites. Memo. July 2005. 

HDOH. Evaluation of Environmental Hazards at Sites with Contaminated Soil and 

Groundwater. Summer 2008 (updated October 2008). 

The Environmental Company, Inc. and AMEC. Red Hill Bulk Fuel Storage Facility Work Plan, 

Pearl Harbor, Hawaii. June 2005. 

TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final – Addendum Planning Documents, Pearl 

Harbor, Hawaii. May 2006. 

TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final Technical Report, Pearl Harbor, Hawaii. 

August 2007. 

TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final Groundwater Protection Plan, Pearl 

Harbor, Hawaii. January 2008. 
Appendix A 

Laboratory Analytical Reports 
SGS Work Order:

Contents:

Cover Page

Case Narrative

Final Report Pages

Quality Control Summary Forms

Chain of Custody/Sample Receipt Forms

Project:

Client:

SGS North America Inc.

 Alaska Division

Level II Laboratory Data Report

Released by: 

Note:

Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the 

SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference.

Red Hills BFSF

The Environmental Company, Inc. (TEC)

1092054

1 of 101
Case Narrative

THEENVC The Environmental Company, Inc. (TEC)

1092054 Red Hills BFSF

Customer:

Project:

NPDL WO:

SGS North America Inc.

Refer to the sample receipt form for information on sample condition.

1092054005 PS RHMW02-WG15

8015C - DRO - The pattern is consistent with a weathered middle distillate.

1092054006 PS RHMWA01-WG15

8015C - DRO - The pattern is consistent with a weathered middle distillate.

1092054008 PS RHMW05-WG15

8270D SIM - Sample extracted and analyzed outside of hold time due to laboratory error.

1092054002 BMS RHMW2254-WG15 MS

8270D SIM - Surrogate recovery for terphenyl-d14 is outside of QC criteria (biased low). Sample was re-extracted 

and analyzed outside of the hold time. The results did confirm with passing QC. The original results are reported 

here.

896080 LCS VXX/19405]

8260B - LCS/LCSD RPD for several analytes do not meet QC criteria (biased high). Refer to MS/MSD RPD for 

precision.

896081 LCSD VXX/19405

8260B - LCS/LCSD RPD for several analytes do not meet QC criteria (biased high). Refer to MS/MSD RPD for 

precision.

896084 CCV VMS/10497]

8260B - ICV recovery for dichlorodifluoromethane, chloromethane and vinyl chloride does not meet QC criteria 

(biased high). These analytes were not detected above the PQL in the associated samples.

2 of 101
Report of Manual Integrations Print Date: 6/8/2009 11:50 am

Laboratory ID Client Sample ID Analytical Batch Method Analyte Reason

1092054005 RHMW02-WG15 XMS4898 8270D SIMS Naphthalene SP

Manual Integration Reason Code Descriptions

Code Description

O Original Chromatogram

M Modified Chromatogram

SS Skimmed surrogate

BLG Closed baseline gap

RP Reassign peak name

PIR Pattern integration required

IT Included tail

SP Split peak

RSP Removed split peak

FPS Forced peak start/stop

BLC Baseline correction

PNF Peak not found by software

All DRO/RRO analysis are integrated per SOP.

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2343 f (907 ) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)

3 of 101
Laboratory Analytical Report

Project:

Client:

Workorder No.:

The Environmental Company, Inc. (TEC)

1092054

Certification:

I certify that this data package is in compliance with the terms and conditions of the contract, 

both technically and for completeness, other than the conditions noted on the sample data 

sheet(s) and/or the case narrative. This certification applies only to the tested parameters and 

the specific sample(s) received at the laboratory.

1001 Bishop Street Ste 1400

ASB Tower

Honolulu, HI 96813

Attn: Jeff Hart

T: (808)528-1445 F:(808)528-0768

jshart@tecinc.com

Tamara Rentz

tamara.rentz@sgs.com

Project Manager

Red Hills BFSF

If you have any questions regarding this report, or if we can be of further assistance, please 

contact your SGS Project Manager.

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2343 f (907 ) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup

4 of 101
Enclosed are the analytical results associated with this workorder.

As required by the state of Alaska and the USEPA, a formal Quality Assurance/Quality Control Program is maintained by SGS. A copy of 

our Quality Assurance Plan (QAP), which outlines this program is available at your request.

The Laboratory certification numbers are AK971-05 (DW), UTS-005 (CS) and AK00971 (Micro) for ADEC and AK100001 for NELAP (RCRA 

methods: 1020A, 1311, 6010B, 7470A, 7471A, 9040B, 9045C, 9056, 9060, 8015B, 8021B, 8081A/8082, 8260B, 8270C).

Except as specifically noted, all statements and data in this report are in conformance to the provisions set forth by the SGS QAP, the 

National Environmental Laboratory Accreditation Program and, when applicable, other regulatory authorities.

If you have any questions regarding this report or if we can be of any assistance, please contact your SGS Project Manager at 

907-562-2343. All work is being provided under SGS general terms and conditions (http://www.sgs.com/terms_and_conditions.htm) 

The following descriptors may be found on your report which will serve to further qualify the data.

MDL Method Detection Limit

PQL Practical Quantitation Limit (reporting limit).

CL Control Limit

U Indicates the analyte was analyzed for but not detected.

F Indicates value that is greater than or equal to the MDL.

J The quantitation is an estimation.

ND Indicates the analyte is not detected

B Indicates the analyte is found in a blank associated with the sample.

* The analyte has exceeded allowable regulatory or control limits.

D The analyte concentration is the result of dilution.

GT Greater Than

LT Less Than

Q QC parameter out of acceptance range.

M A matrix effect was present.

E The analyte result is above the calibrated range.

R Rejected

DF Analytical Dilution Factor

JL The analyte was positively identified, but the quantitation is a low estimation.

<Surr> Surrogate QC spiked standard

<Surr/IS> Surrogate / Internal Standard QC spiked standard

QC Quality Control

QA Quality Assurance

MB Method Blank

LCS (D) Laboratory Control Sample (Duplicate)

MS(D) Matrix Spike (Duplicate)

BMS(D) Site Specific Matrix Spike (Duplicate)

RPD Relative Percent Difference

ICV Initial Calibration Verification

CCV Continuous Calibration Verification

MSA Method of Standard Addition

Notes: Soil samples are reported on a dry weight basis unless otherwise specified

Print Date: 6/8/2009

Notes: All DRO/RRO analyses are integrated per SOP.

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2343 f (907 ) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup

5 of 101
SAMPLE SUMMARY

Client Name: The Environmental Company, Inc. (TEC)

Project Name: Red Hills BFSF

Workorder No.: 1092054

Analytical Methods

Method Description Analytical Method

8270 PAH SIM Semi-Vol GC/MS Liq/Liq ext. 8270D SIMS

AFCEE 3.1 8260 (W) SW8260B

Dissolved Metals by ICP-MS SW6020

DRO by 8015B (W) SW8015C

GRO (W) SW8015C

Print Date: 6/8/2009 11:50 am

Sample ID Cross Reference

Lab Sample ID Client Sample ID

1092054001 RHMW2254-WG15

1092054002 RHMW2254-WG15 MS

1092054003 RHMW2254-WG15 MSD

1092054004 RHMW03-WG15

1092054005 RHMW02-WG15

1092054006 RHMWA01-WG15

1092054007 RHMW01-WG15

1092054008 RHMW05-WG15

1092054009 TB01-WG15

S G S N orth A m erica Inc . A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2343 f (907 ) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)

6 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW2254-WG15

SGS Ref. #: 1092054001 Collection Date/Time: 05/13/09 09:10

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5916 MXX21701

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5916

Analytical Method: SW6020

Analysis Date/Time: 05/25/09 01:50

Prep Batch: MXX21701

Prep Method: SW3010A

Prep Date/Time: 05/22/09 17:30 Container ID:1092054001-G

Dilution Factor: 5 Analyst: NRB

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

7 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW2254-WG15

SGS Ref. #: 1092054001 Collection Date/Time: 05/13/09 09:10

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics 19.1 J 100 10.0 ug/L 1 VFC9431 VXX19416

4-Bromofluorobenzene <surr> 103 50-150 % 1 VFC9431 VXX19416

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9431

Analytical Method: SW8015C

Analysis Date/Time: 05/26/09 17:18

Prep Batch: VXX19416

Prep Method: SW5030B

Prep Date/Time: 05/26/09 09:17 Container ID:1092054001-B

Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

8 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW2254-WG15

SGS Ref. #: 1092054001 Collection Date/Time: 05/13/09 09:10

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics ND 0.449 0.169 mg/L 1 XFC8556 XXX20835

5a Androstane <surr> 86.1 50-150 % 1 XFC8556 XXX20835

Batch Information

Initial Prep Wt./Vol.: 890 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8556

Analytical Method: SW8015C

Analysis Date/Time: 06/03/09 07:16

Prep Batch: XXX20835

Prep Method: SW3520C

Prep Date/Time: 05/20/09 09:00 Container ID:1092054001-J

Dilution Factor: 1 Analyst: KDC

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

9 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW2254-WG15

SGS Ref. #: 1092054001 Collection Date/Time: 05/13/09 09:10

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10497 VXX19405

Toluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10497 VXX19405

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Styrene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Acetone ND 10.0 3.10 ug/L 1 VMS10497 VXX19405

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10497 VXX19405

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10497 VXX19405

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10497 VXX19405

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

Chloroform ND 1.00 0.300 ug/L 1 VMS10497 VXX19405

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Chloromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Bromomethane ND 3.00 0.940 ug/L 1 VMS10497 VXX19405

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

10 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW2254-WG15

SGS Ref. #: 1092054001 Collection Date/Time: 05/13/09 09:10

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10497 VXX19405

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10497 VXX19405

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10497 VXX19405

Naphthalene ND 2.00 0.620 ug/L 1 VMS10497 VXX19405

o-Xylene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Bromoform ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10501 VXX19411

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2-Dichloroethane-D4 <surr> 115 73-120 % 1 VMS10497 VXX19405

Toluene-d8 <surr> 98.8 80-120 % 1 VMS10497 VXX19405

4-Bromofluorobenzene <surr> 101 76-120 % 1 VMS10497 VXX19405

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

11 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW2254-WG15

SGS Ref. #: 1092054001 Collection Date/Time: 05/13/09 09:10

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10497

Analytical Method: SW8260B

Analysis Date/Time: 05/20/09 18:22

Prep Batch: VXX19405

Prep Method: SW5030B

Prep Date/Time: 05/20/09 11:43 Container ID:1092054001-D

Dilution Factor: 1 Analyst: DSH

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10501

Analytical Method: SW8260B

Analysis Date/Time: 05/24/09 23:20

Prep Batch: VXX19411

Prep Method: SW5030B

Prep Date/Time: 05/24/09 17:14 Container ID:1092054001-E

Dilution Factor: 1 Analyst: DSH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

12 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW2254-WG15

SGS Ref. #: 1092054001 Collection Date/Time: 05/13/09 09:10

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0521 0.0156 ug/L 1 XMS4898 XXX20829

Acenaphthene ND 0.0521 0.0156 ug/L 1 XMS4898 XXX20829

Fluorene ND 0.0521 0.0156 ug/L 1 XMS4898 XXX20829

Phenanthrene ND 0.0521 0.0156 ug/L 1 XMS4898 XXX20829

Anthracene ND 0.0521 0.0156 ug/L 1 XMS4898 XXX20829

Fluoranthene ND 0.0521 0.0156 ug/L 1 XMS4898 XXX20829

Pyrene ND 0.0521 0.0156 ug/L 1 XMS4898 XXX20829

Benzo(a)Anthracene ND 0.0521 0.0156 ug/L 1 XMS4898 XXX20829

Chrysene ND 0.0521 0.0156 ug/L 1 XMS4898 XXX20829

Benzo[b]Fluoranthene ND 0.0521 0.0156 ug/L 1 XMS4898 XXX20829

Benzo[k]fluoranthene ND 0.0521 0.0156 ug/L 1 XMS4898 XXX20829

Benzo[a]pyrene ND 0.0521 0.0156 ug/L 1 XMS4898 XXX20829

Indeno[1,2,3-c,d] pyrene ND 0.0521 0.0156 ug/L 1 XMS4898 XXX20829

Dibenzo[a,h]anthracene ND 0.0521 0.0156 ug/L 1 XMS4898 XXX20829

Benzo[g,h,i]perylene ND 0.0521 0.0156 ug/L 1 XMS4898 XXX20829

Naphthalene ND 0.104 0.0323 ug/L 1 XMS4898 XXX20829

1-Methylnaphthalene ND 0.0521 0.0156 ug/L 1 XMS4898 XXX20829

2-Methylnaphthalene 0.0180 J 0.0521 0.0156 ug/L 1 XMS4898 XXX20829

Terphenyl-d14 <surr> 94.1 50-135 % 1 XMS4898 XXX20829

Batch Information

Initial Prep Wt./Vol.: 960 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4898

Analytical Method: 8270D SIMS

Analysis Date/Time: 05/22/09 17:37

Prep Batch: XXX20829

Prep Method: SW3520C

Prep Date/Time: 05/19/09 09:45 Container ID:1092054001-H

Dilution Factor: 1 Analyst: JDH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

13 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW03-WG15

SGS Ref. #: 1092054004 Collection Date/Time: 05/13/09 11:00

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5916 MXX21701

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5916

Analytical Method: SW6020

Analysis Date/Time: 05/25/09 02:15

Prep Batch: MXX21701

Prep Method: SW3010A

Prep Date/Time: 05/22/09 17:30 Container ID:1092054004-G

Dilution Factor: 5 Analyst: NRB

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

14 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW03-WG15

SGS Ref. #: 1092054004 Collection Date/Time: 05/13/09 11:00

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics 14.8 J 100 10.0 ug/L 1 VFC9431 VXX19416

4-Bromofluorobenzene <surr> 100 50-150 % 1 VFC9431 VXX19416

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9431

Analytical Method: SW8015C

Analysis Date/Time: 05/26/09 17:36

Prep Batch: VXX19416

Prep Method: SW5030B

Prep Date/Time: 05/26/09 09:17 Container ID:1092054004-B

Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

15 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW03-WG15

SGS Ref. #: 1092054004 Collection Date/Time: 05/13/09 11:00

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics ND 0.430 0.161 mg/L 1 XFC8556 XXX20835

5a Androstane <surr> 84.5 50-150 % 1 XFC8556 XXX20835

Batch Information

Initial Prep Wt./Vol.: 930 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8556

Analytical Method: SW8015C

Analysis Date/Time: 06/03/09 07:53

Prep Batch: XXX20835

Prep Method: SW3520C

Prep Date/Time: 05/20/09 09:00 Container ID:1092054004-J

Dilution Factor: 1 Analyst: KDC

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

16 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW03-WG15

SGS Ref. #: 1092054004 Collection Date/Time: 05/13/09 11:00

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10497 VXX19405

Toluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10497 VXX19405

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Styrene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Acetone ND 10.0 3.10 ug/L 1 VMS10497 VXX19405

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10497 VXX19405

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10497 VXX19405

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10497 VXX19405

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

Chloroform ND 1.00 0.300 ug/L 1 VMS10497 VXX19405

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Chloromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Bromomethane ND 3.00 0.940 ug/L 1 VMS10497 VXX19405

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

17 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW03-WG15

SGS Ref. #: 1092054004 Collection Date/Time: 05/13/09 11:00

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10497 VXX19405

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10497 VXX19405

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10497 VXX19405

Naphthalene ND 2.00 0.620 ug/L 1 VMS10497 VXX19405

o-Xylene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Bromoform ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10501 VXX19411

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2-Dichloroethane-D4 <surr> 111 73-120 % 1 VMS10497 VXX19405

Toluene-d8 <surr> 98.1 80-120 % 1 VMS10497 VXX19405

4-Bromofluorobenzene <surr> 99 76-120 % 1 VMS10497 VXX19405

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

18 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW03-WG15

SGS Ref. #: 1092054004 Collection Date/Time: 05/13/09 11:00

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10497

Analytical Method: SW8260B

Analysis Date/Time: 05/20/09 18:56

Prep Batch: VXX19405

Prep Method: SW5030B

Prep Date/Time: 05/20/09 11:43 Container ID:1092054004-D

Dilution Factor: 1 Analyst: DSH

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10501

Analytical Method: SW8260B

Analysis Date/Time: 05/24/09 23:54

Prep Batch: VXX19411

Prep Method: SW5030B

Prep Date/Time: 05/24/09 17:14 Container ID:1092054004-E

Dilution Factor: 1 Analyst: DSH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

19 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW03-WG15

SGS Ref. #: 1092054004 Collection Date/Time: 05/13/09 11:00

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0505 0.0152 ug/L 1 XMS4898 XXX20829

Acenaphthene ND 0.0505 0.0152 ug/L 1 XMS4898 XXX20829

Fluorene ND 0.0505 0.0152 ug/L 1 XMS4898 XXX20829

Phenanthrene ND 0.0505 0.0152 ug/L 1 XMS4898 XXX20829

Anthracene ND 0.0505 0.0152 ug/L 1 XMS4898 XXX20829

Fluoranthene ND 0.0505 0.0152 ug/L 1 XMS4898 XXX20829

Pyrene ND 0.0505 0.0152 ug/L 1 XMS4898 XXX20829

Benzo(a)Anthracene ND 0.0505 0.0152 ug/L 1 XMS4898 XXX20829

Chrysene ND 0.0505 0.0152 ug/L 1 XMS4898 XXX20829

Benzo[b]Fluoranthene ND 0.0505 0.0152 ug/L 1 XMS4898 XXX20829

Benzo[k]fluoranthene ND 0.0505 0.0152 ug/L 1 XMS4898 XXX20829

Benzo[a]pyrene ND 0.0505 0.0152 ug/L 1 XMS4898 XXX20829

Indeno[1,2,3-c,d] pyrene ND 0.0505 0.0152 ug/L 1 XMS4898 XXX20829

Dibenzo[a,h]anthracene ND 0.0505 0.0152 ug/L 1 XMS4898 XXX20829

Benzo[g,h,i]perylene ND 0.0505 0.0152 ug/L 1 XMS4898 XXX20829

Naphthalene ND 0.101 0.0313 ug/L 1 XMS4898 XXX20829

1-Methylnaphthalene ND 0.0505 0.0152 ug/L 1 XMS4898 XXX20829

2-Methylnaphthalene ND 0.0505 0.0152 ug/L 1 XMS4898 XXX20829

Terphenyl-d14 <surr> 91 50-135 % 1 XMS4898 XXX20829

Batch Information

Initial Prep Wt./Vol.: 990 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4898

Analytical Method: 8270D SIMS

Analysis Date/Time: 05/22/09 19:15

Prep Batch: XXX20829

Prep Method: SW3520C

Prep Date/Time: 05/19/09 09:45 Container ID:1092054004-H

Dilution Factor: 1 Analyst: JDH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

20 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW02-WG15

SGS Ref. #: 1092054005 Collection Date/Time: 05/13/09 12:50

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5916 MXX21701

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5916

Analytical Method: SW6020

Analysis Date/Time: 05/25/09 02:17

Prep Batch: MXX21701

Prep Method: SW3010A

Prep Date/Time: 05/22/09 17:30 Container ID:1092054005-G

Dilution Factor: 5 Analyst: NRB

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

21 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW02-WG15

SGS Ref. #: 1092054005 Collection Date/Time: 05/13/09 12:50

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics 39.1 J 100 10.0 ug/L 1 VFC9431 VXX19416

4-Bromofluorobenzene <surr> 124 50-150 % 1 VFC9431 VXX19416

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9431

Analytical Method: SW8015C

Analysis Date/Time: 05/26/09 19:10

Prep Batch: VXX19416

Prep Method: SW5030B

Prep Date/Time: 05/26/09 09:17 Container ID:1092054005-B

Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

22 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW02-WG15

SGS Ref. #: 1092054005 Collection Date/Time: 05/13/09 12:50

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 1.62 0.444 0.167 mg/L 1 XFC8556 XXX20835

5a Androstane <surr> 85.1 50-150 % 1 XFC8556 XXX20835

Batch Information

Initial Prep Wt./Vol.: 900 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8556

Analytical Method: SW8015C

Analysis Date/Time: 06/03/09 08:21

Prep Batch: XXX20835

Prep Method: SW3520C

Prep Date/Time: 05/20/09 09:00 Container ID:1092054005-J

Dilution Factor: 1 Analyst: KDC

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

23 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW02-WG15

SGS Ref. #: 1092054005 Collection Date/Time: 05/13/09 12:50

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10497 VXX19405

Toluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

n-Butylbenzene 2.19 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10497 VXX19405

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

n-Propylbenzene 2.24 1.00 0.310 ug/L 1 VMS10497 VXX19405

Styrene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Acetone ND 10.0 3.10 ug/L 1 VMS10497 VXX19405

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10497 VXX19405

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10497 VXX19405

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10497 VXX19405

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

Chloroform ND 1.00 0.300 ug/L 1 VMS10497 VXX19405

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Chloromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Bromomethane ND 3.00 0.940 ug/L 1 VMS10497 VXX19405

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

24 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW02-WG15

SGS Ref. #: 1092054005 Collection Date/Time: 05/13/09 12:50

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

sec-Butylbenzene 6.26 1.00 0.310 ug/L 1 VMS10497 VXX19405

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10497 VXX19405

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10497 VXX19405

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10497 VXX19405

Naphthalene ND 2.00 0.620 ug/L 1 VMS10497 VXX19405

o-Xylene 0.310 J 1.00 0.310 ug/L 1 VMS10497 VXX19405

Bromoform ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

tert-Butylbenzene 1.05 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10501 VXX19411

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Isopropylbenzene (Cumene) 5.08 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2-Dichloroethane-D4 <surr> 113 73-120 % 1 VMS10497 VXX19405

Toluene-d8 <surr> 96.8 80-120 % 1 VMS10497 VXX19405

4-Bromofluorobenzene <surr> 103 76-120 % 1 VMS10497 VXX19405

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

25 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW02-WG15

SGS Ref. #: 1092054005 Collection Date/Time: 05/13/09 12:50

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10497

Analytical Method: SW8260B

Analysis Date/Time: 05/20/09 19:30

Prep Batch: VXX19405

Prep Method: SW5030B

Prep Date/Time: 05/20/09 11:43 Container ID:1092054005-D

Dilution Factor: 1 Analyst: DSH

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10501

Analytical Method: SW8260B

Analysis Date/Time: 05/25/09 00:28

Prep Batch: VXX19411

Prep Method: SW5030B

Prep Date/Time: 05/24/09 17:14 Container ID:1092054005-E

Dilution Factor: 1 Analyst: DSH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

26 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW02-WG15

SGS Ref. #: 1092054005 Collection Date/Time: 05/13/09 12:50

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Acenaphthene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Fluorene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Phenanthrene 0.0162 J 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Anthracene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Fluoranthene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Pyrene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Benzo(a)Anthracene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Chrysene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Benzo[b]Fluoranthene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Benzo[k]fluoranthene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Benzo[a]pyrene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Indeno[1,2,3-c,d] pyrene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Dibenzo[a,h]anthracene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Benzo[g,h,i]perylene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Naphthalene 1.17 0.100 0.0310 ug/L 1 XMS4898 XXX20829

1-Methylnaphthalene 17.9 0.500 0.150 ug/L 10 XMS4901 XXX20829

2-Methylnaphthalene 0.136 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Terphenyl-d14 <surr> 86.5 50-135 % 1 XMS4898 XXX20829

Batch Information

Initial Prep Wt./Vol.: 1000 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4898

Analytical Method: 8270D SIMS

Analysis Date/Time: 05/22/09 19:48

Prep Batch: XXX20829

Prep Method: SW3520C

Prep Date/Time: 05/19/09 09:45 Container ID:1092054005-H

Dilution Factor: 1 Analyst: JDH

Initial Prep Wt./Vol.: 1000 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4901

Analytical Method: 8270D SIMS

Analysis Date/Time: 05/23/09 14:32

Prep Batch: XXX20829

Prep Method: SW3520C

Prep Date/Time: 05/19/09 09:45 Container ID:1092054005-H

Dilution Factor: 10 Analyst: JDH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

27 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMWA01-WG15

SGS Ref. #: 1092054006 Collection Date/Time: 05/13/09 12:05

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5916 MXX21701

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5916

Analytical Method: SW6020

Analysis Date/Time: 05/25/09 02:19

Prep Batch: MXX21701

Prep Method: SW3010A

Prep Date/Time: 05/22/09 17:30 Container ID:1092054006-G

Dilution Factor: 5 Analyst: NRB

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

28 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMWA01-WG15

SGS Ref. #: 1092054006 Collection Date/Time: 05/13/09 12:05

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics 36.7 J 100 10.0 ug/L 1 VFC9431 VXX19416

4-Bromofluorobenzene <surr> 121 50-150 % 1 VFC9431 VXX19416

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9431

Analytical Method: SW8015C

Analysis Date/Time: 05/26/09 19:29

Prep Batch: VXX19416

Prep Method: SW5030B

Prep Date/Time: 05/26/09 09:17 Container ID:1092054006-B

Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

29 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMWA01-WG15

SGS Ref. #: 1092054006 Collection Date/Time: 05/13/09 12:05

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 2.00 0.426 0.160 mg/L 1 XFC8556 XXX20835

5a Androstane <surr> 96.2 50-150 % 1 XFC8556 XXX20835

Batch Information

Initial Prep Wt./Vol.: 940 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8556

Analytical Method: SW8015C

Analysis Date/Time: 06/03/09 08:31

Prep Batch: XXX20835

Prep Method: SW3520C

Prep Date/Time: 05/20/09 09:00 Container ID:1092054006-J

Dilution Factor: 1 Analyst: KDC

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

30 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMWA01-WG15

SGS Ref. #: 1092054006 Collection Date/Time: 05/13/09 12:05

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10497 VXX19405

Toluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

n-Butylbenzene 2.06 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10497 VXX19405

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

n-Propylbenzene 2.16 1.00 0.310 ug/L 1 VMS10497 VXX19405

Styrene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Acetone ND 10.0 3.10 ug/L 1 VMS10497 VXX19405

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10497 VXX19405

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10497 VXX19405

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10497 VXX19405

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

Chloroform ND 1.00 0.300 ug/L 1 VMS10497 VXX19405

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Chloromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Bromomethane ND 3.00 0.940 ug/L 1 VMS10497 VXX19405

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

31 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMWA01-WG15

SGS Ref. #: 1092054006 Collection Date/Time: 05/13/09 12:05

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

sec-Butylbenzene 5.84 1.00 0.310 ug/L 1 VMS10497 VXX19405

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10497 VXX19405

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10497 VXX19405

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10497 VXX19405

Naphthalene ND 2.00 0.620 ug/L 1 VMS10497 VXX19405

o-Xylene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Bromoform ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

tert-Butylbenzene 0.970 J 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10501 VXX19411

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Isopropylbenzene (Cumene) 4.86 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2-Dichloroethane-D4 <surr> 115 73-120 % 1 VMS10497 VXX19405

Toluene-d8 <surr> 97.9 80-120 % 1 VMS10497 VXX19405

4-Bromofluorobenzene <surr> 103 76-120 % 1 VMS10497 VXX19405

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

32 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMWA01-WG15

SGS Ref. #: 1092054006 Collection Date/Time: 05/13/09 12:05

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10497

Analytical Method: SW8260B

Analysis Date/Time: 05/20/09 20:04

Prep Batch: VXX19405

Prep Method: SW5030B

Prep Date/Time: 05/20/09 11:43 Container ID:1092054006-D

Dilution Factor: 1 Analyst: DSH

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10501

Analytical Method: SW8260B

Analysis Date/Time: 05/25/09 01:02

Prep Batch: VXX19411

Prep Method: SW5030B

Prep Date/Time: 05/24/09 17:14 Container ID:1092054006-E

Dilution Factor: 1 Analyst: DSH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

33 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMWA01-WG15

SGS Ref. #: 1092054006 Collection Date/Time: 05/13/09 12:05

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0515 0.0155 ug/L 1 XMS4898 XXX20829

Acenaphthene ND 0.0515 0.0155 ug/L 1 XMS4898 XXX20829

Fluorene ND 0.0515 0.0155 ug/L 1 XMS4898 XXX20829

Phenanthrene 0.0171 J 0.0515 0.0155 ug/L 1 XMS4898 XXX20829

Anthracene ND 0.0515 0.0155 ug/L 1 XMS4898 XXX20829

Fluoranthene ND 0.0515 0.0155 ug/L 1 XMS4898 XXX20829

Pyrene ND 0.0515 0.0155 ug/L 1 XMS4898 XXX20829

Benzo(a)Anthracene ND 0.0515 0.0155 ug/L 1 XMS4898 XXX20829

Chrysene ND 0.0515 0.0155 ug/L 1 XMS4898 XXX20829

Benzo[b]Fluoranthene ND 0.0515 0.0155 ug/L 1 XMS4898 XXX20829

Benzo[k]fluoranthene ND 0.0515 0.0155 ug/L 1 XMS4898 XXX20829

Benzo[a]pyrene ND 0.0515 0.0155 ug/L 1 XMS4898 XXX20829

Indeno[1,2,3-c,d] pyrene ND 0.0515 0.0155 ug/L 1 XMS4898 XXX20829

Dibenzo[a,h]anthracene ND 0.0515 0.0155 ug/L 1 XMS4898 XXX20829

Benzo[g,h,i]perylene ND 0.0515 0.0155 ug/L 1 XMS4898 XXX20829

Naphthalene 1.08 0.103 0.0320 ug/L 1 XMS4898 XXX20829

1-Methylnaphthalene 24.6 0.515 0.155 ug/L 10 XMS4901 XXX20829

2-Methylnaphthalene 0.107 0.0515 0.0155 ug/L 1 XMS4898 XXX20829

Terphenyl-d14 <surr> 86.4 50-135 % 1 XMS4898 XXX20829

Batch Information

Initial Prep Wt./Vol.: 970 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4898

Analytical Method: 8270D SIMS

Analysis Date/Time: 05/22/09 20:20

Prep Batch: XXX20829

Prep Method: SW3520C

Prep Date/Time: 05/19/09 09:45 Container ID:1092054006-H

Dilution Factor: 1 Analyst: JDH

Initial Prep Wt./Vol.: 970 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4901

Analytical Method: 8270D SIMS

Analysis Date/Time: 05/23/09 15:05

Prep Batch: XXX20829

Prep Method: SW3520C

Prep Date/Time: 05/19/09 09:45 Container ID:1092054006-H

Dilution Factor: 10 Analyst: JDH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

34 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW01-WG15

SGS Ref. #: 1092054007 Collection Date/Time: 05/13/09 15:05

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5916 MXX21701

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5916

Analytical Method: SW6020

Analysis Date/Time: 05/25/09 02:21

Prep Batch: MXX21701

Prep Method: SW3010A

Prep Date/Time: 05/22/09 17:30 Container ID:1092054007-G

Dilution Factor: 5 Analyst: NRB

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

35 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW01-WG15

SGS Ref. #: 1092054007 Collection Date/Time: 05/13/09 15:05

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics 16.6 J 100 10.0 ug/L 1 VFC9431 VXX19416

4-Bromofluorobenzene <surr> 106 50-150 % 1 VFC9431 VXX19416

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9431

Analytical Method: SW8015C

Analysis Date/Time: 05/26/09 19:48

Prep Batch: VXX19416

Prep Method: SW5030B

Prep Date/Time: 05/26/09 09:17 Container ID:1092054007-B

Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

36 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW01-WG15

SGS Ref. #: 1092054007 Collection Date/Time: 05/13/09 15:05

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 0.373 J 0.449 0.169 mg/L 1 XFC8556 XXX20835

5a Androstane <surr> 99 50-150 % 1 XFC8556 XXX20835

Batch Information

Initial Prep Wt./Vol.: 890 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8556

Analytical Method: SW8015C

Analysis Date/Time: 06/03/09 08:40

Prep Batch: XXX20835

Prep Method: SW3520C

Prep Date/Time: 05/20/09 09:00 Container ID:1092054007-J

Dilution Factor: 1 Analyst: KDC

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

37 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW01-WG15

SGS Ref. #: 1092054007 Collection Date/Time: 05/13/09 15:05

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10497 VXX19405

Toluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10497 VXX19405

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Styrene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Acetone ND 10.0 3.10 ug/L 1 VMS10497 VXX19405

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10497 VXX19405

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10497 VXX19405

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10497 VXX19405

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

Chloroform ND 1.00 0.300 ug/L 1 VMS10497 VXX19405

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Chloromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Bromomethane ND 3.00 0.940 ug/L 1 VMS10497 VXX19405

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

38 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW01-WG15

SGS Ref. #: 1092054007 Collection Date/Time: 05/13/09 15:05

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10497 VXX19405

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10497 VXX19405

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10497 VXX19405

Naphthalene ND 2.00 0.620 ug/L 1 VMS10497 VXX19405

o-Xylene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Bromoform ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10501 VXX19411

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2-Dichloroethane-D4 <surr> 115 73-120 % 1 VMS10497 VXX19405

Toluene-d8 <surr> 99 80-120 % 1 VMS10497 VXX19405

4-Bromofluorobenzene <surr> 99.2 76-120 % 1 VMS10497 VXX19405

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

39 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW01-WG15

SGS Ref. #: 1092054007 Collection Date/Time: 05/13/09 15:05

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10497

Analytical Method: SW8260B

Analysis Date/Time: 05/20/09 20:38

Prep Batch: VXX19405

Prep Method: SW5030B

Prep Date/Time: 05/20/09 11:43 Container ID:1092054007-D

Dilution Factor: 1 Analyst: DSH

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10501

Analytical Method: SW8260B

Analysis Date/Time: 05/25/09 01:36

Prep Batch: VXX19411

Prep Method: SW5030B

Prep Date/Time: 05/24/09 17:14 Container ID:1092054007-E

Dilution Factor: 1 Analyst: DSH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

40 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW01-WG15

SGS Ref. #: 1092054007 Collection Date/Time: 05/13/09 15:05

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Acenaphthene 0.0243 J 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Fluorene 0.0246 J 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Phenanthrene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Anthracene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Fluoranthene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Pyrene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Benzo(a)Anthracene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Chrysene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Benzo[b]Fluoranthene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Benzo[k]fluoranthene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Benzo[a]pyrene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Indeno[1,2,3-c,d] pyrene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Dibenzo[a,h]anthracene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Benzo[g,h,i]perylene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Naphthalene 0.182 0.100 0.0310 ug/L 1 XMS4898 XXX20829

1-Methylnaphthalene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

2-Methylnaphthalene ND 0.0500 0.0150 ug/L 1 XMS4898 XXX20829

Terphenyl-d14 <surr> 72.1 50-135 % 1 XMS4898 XXX20829

Batch Information

Initial Prep Wt./Vol.: 1000 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4898

Analytical Method: 8270D SIMS

Analysis Date/Time: 05/22/09 20:53

Prep Batch: XXX20829

Prep Method: SW3520C

Prep Date/Time: 05/19/09 09:45 Container ID:1092054007-H

Dilution Factor: 1 Analyst: JDH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

41 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW05-WG15

SGS Ref. #: 1092054008 Collection Date/Time: 05/13/09 07:40

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5916 MXX21701

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5916

Analytical Method: SW6020

Analysis Date/Time: 05/25/09 02:23

Prep Batch: MXX21701

Prep Method: SW3010A

Prep Date/Time: 05/22/09 17:30 Container ID:1092054008-G

Dilution Factor: 5 Analyst: NRB

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

42 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW05-WG15

SGS Ref. #: 1092054008 Collection Date/Time: 05/13/09 07:40

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics 13.2 J 100 10.0 ug/L 1 VFC9431 VXX19416

4-Bromofluorobenzene <surr> 105 50-150 % 1 VFC9431 VXX19416

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9431

Analytical Method: SW8015C

Analysis Date/Time: 05/26/09 20:06

Prep Batch: VXX19416

Prep Method: SW5030B

Prep Date/Time: 05/26/09 09:17 Container ID:1092054008-B

Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

43 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW05-WG15

SGS Ref. #: 1092054008 Collection Date/Time: 05/13/09 07:40

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 0.200 J 0.430 0.161 mg/L 1 XFC8556 XXX20835

5a Androstane <surr> 86.1 50-150 % 1 XFC8556 XXX20835

Batch Information

Initial Prep Wt./Vol.: 930 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8556

Analytical Method: SW8015C

Analysis Date/Time: 06/03/09 08:49

Prep Batch: XXX20835

Prep Method: SW3520C

Prep Date/Time: 05/20/09 09:00 Container ID:1092054008-J

Dilution Factor: 1 Analyst: KDC

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

44 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW05-WG15

SGS Ref. #: 1092054008 Collection Date/Time: 05/13/09 07:40

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10497 VXX19405

Toluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10497 VXX19405

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Styrene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Acetone 10.4 10.0 3.10 ug/L 1 VMS10497 VXX19405

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10497 VXX19405

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10497 VXX19405

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10497 VXX19405

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

Chloroform ND 1.00 0.300 ug/L 1 VMS10497 VXX19405

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Chloromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Bromomethane ND 3.00 0.940 ug/L 1 VMS10497 VXX19405

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

45 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW05-WG15

SGS Ref. #: 1092054008 Collection Date/Time: 05/13/09 07:40

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10497 VXX19405

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10497 VXX19405

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10497 VXX19405

Naphthalene ND 2.00 0.620 ug/L 1 VMS10497 VXX19405

o-Xylene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Bromoform ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10501 VXX19411

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2-Dichloroethane-D4 <surr> 109 73-120 % 1 VMS10497 VXX19405

Toluene-d8 <surr> 99.1 80-120 % 1 VMS10497 VXX19405

4-Bromofluorobenzene <surr> 102 76-120 % 1 VMS10497 VXX19405

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

46 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW05-WG15

SGS Ref. #: 1092054008 Collection Date/Time: 05/13/09 07:40

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10497

Analytical Method: SW8260B

Analysis Date/Time: 05/20/09 21:12

Prep Batch: VXX19405

Prep Method: SW5030B

Prep Date/Time: 05/20/09 11:43 Container ID:1092054008-D

Dilution Factor: 1 Analyst: DSH

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10501

Analytical Method: SW8260B

Analysis Date/Time: 05/25/09 02:10

Prep Batch: VXX19411

Prep Method: SW5030B

Prep Date/Time: 05/24/09 17:14 Container ID:1092054008-E

Dilution Factor: 1 Analyst: DSH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

47 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: RHMW05-WG15

SGS Ref. #: 1092054008 Collection Date/Time: 05/13/09 07:40

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0526 0.0158 ug/L 1 XMS4906 XXX20855

Acenaphthene ND 0.0526 0.0158 ug/L 1 XMS4906 XXX20855

Fluorene ND 0.0526 0.0158 ug/L 1 XMS4906 XXX20855

Phenanthrene ND 0.0526 0.0158 ug/L 1 XMS4906 XXX20855

Anthracene ND 0.0526 0.0158 ug/L 1 XMS4906 XXX20855

Fluoranthene ND 0.0526 0.0158 ug/L 1 XMS4906 XXX20855

Pyrene ND 0.0526 0.0158 ug/L 1 XMS4906 XXX20855

Benzo(a)Anthracene ND 0.0526 0.0158 ug/L 1 XMS4906 XXX20855

Chrysene ND 0.0526 0.0158 ug/L 1 XMS4906 XXX20855

Benzo[b]Fluoranthene ND 0.0526 0.0158 ug/L 1 XMS4906 XXX20855

Benzo[k]fluoranthene ND 0.0526 0.0158 ug/L 1 XMS4906 XXX20855

Benzo[a]pyrene ND 0.0526 0.0158 ug/L 1 XMS4906 XXX20855

Indeno[1,2,3-c,d] pyrene ND 0.0526 0.0158 ug/L 1 XMS4906 XXX20855

Dibenzo[a,h]anthracene ND 0.0526 0.0158 ug/L 1 XMS4906 XXX20855

Benzo[g,h,i]perylene ND 0.0526 0.0158 ug/L 1 XMS4906 XXX20855

Naphthalene ND 0.105 0.0326 ug/L 1 XMS4906 XXX20855

1-Methylnaphthalene ND 0.0526 0.0158 ug/L 1 XMS4906 XXX20855

2-Methylnaphthalene ND 0.0526 0.0158 ug/L 1 XMS4906 XXX20855

Terphenyl-d14 <surr> 73.3 50-135 % 1 XMS4906 XXX20855

Batch Information

Initial Prep Wt./Vol.: 950 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4906

Analytical Method: 8270D SIMS

Analysis Date/Time: 05/28/09 09:12

Prep Batch: XXX20855

Prep Method: SW3520C

Prep Date/Time: 05/26/09 10:30 Container ID:1092054008-I

Dilution Factor: 1 Analyst: JDH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

48 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: TB01-WG15

SGS Ref. #: 1092054009 Collection Date/Time: 05/13/09 08:05

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics 11.5 J 100 10.0 ug/L 1 VFC9438 VXX19432

4-Bromofluorobenzene <surr> 102 50-150 % 1 VFC9438 VXX19432

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9438

Analytical Method: SW8015C

Analysis Date/Time: 05/21/09 20:51

Prep Batch: VXX19432

Prep Method: SW5030B

Prep Date/Time: 05/21/09 07:15 Container ID:1092054009-A

Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

49 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: TB01-WG15

SGS Ref. #: 1092054009 Collection Date/Time: 05/13/09 08:05

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10497 VXX19405

Toluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10497 VXX19405

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Styrene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Acetone ND 10.0 3.10 ug/L 1 VMS10497 VXX19405

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10497 VXX19405

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10497 VXX19405

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10497 VXX19405

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

Chloroform ND 1.00 0.300 ug/L 1 VMS10497 VXX19405

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Chloromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Bromomethane ND 3.00 0.940 ug/L 1 VMS10497 VXX19405

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

50 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: TB01-WG15

SGS Ref. #: 1092054009 Collection Date/Time: 05/13/09 08:05

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10497 VXX19405

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10497 VXX19405

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10497 VXX19405

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10497 VXX19405

Naphthalene ND 2.00 0.620 ug/L 1 VMS10497 VXX19405

o-Xylene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Bromoform ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10501 VXX19411

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10497 VXX19405

1,2-Dichloroethane-D4 <surr> 111 73-120 % 1 VMS10497 VXX19405

Toluene-d8 <surr> 96.6 80-120 % 1 VMS10497 VXX19405

4-Bromofluorobenzene <surr> 98 76-120 % 1 VMS10497 VXX19405

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

51 of 101
The Environmental Company, Inc. (TEC) Print Date: 6/8/2009 11:50 am

Client Sample ID: TB01-WG15

SGS Ref. #: 1092054009 Collection Date/Time: 05/13/09 08:05

Project ID: Red Hills BFSF Receipt Date/Time: 05/15/09 11:20

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10497

Analytical Method: SW8260B

Analysis Date/Time: 05/20/09 17:48

Prep Batch: VXX19405

Prep Method: SW5030B

Prep Date/Time: 05/20/09 11:43 Container ID:1092054009-B

Dilution Factor: 1 Analyst: DSH

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10501

Analytical Method: SW8260B

Analysis Date/Time: 05/24/09 22:47

Prep Batch: VXX19411

Prep Method: SW5030B

Prep Date/Time: 05/24/09 17:14 Container ID:1092054009-C

Dilution Factor: 1 Analyst: DSH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

52 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

895548 Method Blank

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

XXX20829

SW3520C

05/19/2009

QC results affect the following production samples:

1092054001, 1092054004, 1092054005, 1092054006, 1092054007

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Polynuclear Aromatics GC/MS

Acenaphthylene ND 0.0500 0.0150 ug/L 05/22/09

Acenaphthene ND 0.0500 0.0150 ug/L 05/22/09

Fluorene ND 0.0500 0.0150 ug/L 05/22/09

Phenanthrene ND 0.0500 0.0150 ug/L 05/22/09

Anthracene ND 0.0500 0.0150 ug/L 05/22/09

Fluoranthene ND 0.0500 0.0150 ug/L 05/22/09

Pyrene ND 0.0500 0.0150 ug/L 05/22/09

Benzo(a)Anthracene ND 0.0500 0.0150 ug/L 05/22/09

Chrysene ND 0.0500 0.0150 ug/L 05/22/09

Benzo[b]Fluoranthene ND 0.0500 0.0150 ug/L 05/22/09

Benzo[k]fluoranthene ND 0.0500 0.0150 ug/L 05/22/09

Benzo[a]pyrene ND 0.0500 0.0150 ug/L 05/22/09

Indeno[1,2,3-c,d] pyrene ND 0.0500 0.0150 ug/L 05/22/09

Dibenzo[a,h]anthracene ND 0.0500 0.0150 ug/L 05/22/09

Benzo[g,h,i]perylene ND 0.0500 0.0150 ug/L 05/22/09

Naphthalene ND 0.100 0.0310 ug/L 05/22/09

1-Methylnaphthalene ND 0.0500 0.0150 ug/L 05/22/09

2-Methylnaphthalene ND 0.0500 0.0150 ug/L 05/22/09

Surrogates 

Terphenyl-d14 <surr> 96 50-135 % 05/22/09

Instrument

Method

Batch XMS4898

8270D SIMS

HP 6890/5973 MS SVOA

53 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

895711 Method Blank

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

XXX20835

SW3520C

05/20/2009

QC results affect the following production samples:

1092054001, 1092054004, 1092054005, 1092054006, 1092054007, 1092054008

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Semivolatile Organic Fuels Department

Diesel Range Organics ND 0.400 0.150 mg/L 06/03/09

Surrogates 

5a Androstane <surr> 84 60-120 % 06/03/09

Instrument

Method

Batch XFC8556

SW8015C

HP 6890 Series II FID SV D R

54 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896079 Method Blank

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

VXX19405

SW5030B

05/20/2009

QC results affect the following production samples:

1092054001, 1092054004, 1092054005, 1092054006, 1092054007, 1092054008, 1092054009

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

55 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896079 Method Blank

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

VXX19405

SW5030B

05/20/2009

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

Benzene ND 0.400 0.120 ug/L 05/20/09

Toluene ND 1.00 0.310 ug/L 05/20/09

Ethylbenzene ND 1.00 0.310 ug/L 05/20/09

n-Butylbenzene ND 1.00 0.310 ug/L 05/20/09

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 05/20/09

1,2-Dichloroethane ND 0.500 0.150 ug/L 05/20/09

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 05/20/09

4-Chlorotoluene ND 1.00 0.310 ug/L 05/20/09

Chlorobenzene ND 0.500 0.150 ug/L 05/20/09

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 05/20/09

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 05/20/09

4-Isopropyltoluene ND 1.00 0.310 ug/L 05/20/09

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 05/20/09

n-Propylbenzene ND 1.00 0.310 ug/L 05/20/09

Styrene ND 1.00 0.310 ug/L 05/20/09

Dibromomethane ND 1.00 0.310 ug/L 05/20/09

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 05/20/09

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 05/20/09

Acetone ND 10.0 3.10 ug/L 05/20/09

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 05/20/09

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 05/20/09

Methyl-t-butyl ether ND 5.00 1.50 ug/L 05/20/09

Tetrachloroethene ND 1.00 0.310 ug/L 05/20/09

Dibromochloromethane ND 0.500 0.150 ug/L 05/20/09

1,3-Dichloropropane ND 0.400 0.120 ug/L 05/20/09

1,2-Dibromoethane ND 1.00 0.310 ug/L 05/20/09

Carbon tetrachloride ND 1.00 0.310 ug/L 05/20/09

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 05/20/09

Chloroform ND 1.00 0.300 ug/L 05/20/09

Bromobenzene ND 1.00 0.310 ug/L 05/20/09

Chloromethane ND 1.00 0.310 ug/L 05/20/09

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 05/20/09

Bromomethane ND 3.00 0.940 ug/L 05/20/09

Bromochloromethane ND 1.00 0.310 ug/L 05/20/09

Vinyl chloride ND 1.00 0.310 ug/L 05/20/09

Dichlorodifluoromethane ND 1.00 0.310 ug/L 05/20/09

Chloroethane ND 1.00 0.310 ug/L 05/20/09

sec-Butylbenzene ND 1.00 0.310 ug/L 05/20/09

Bromodichloromethane ND 0.500 0.150 ug/L 05/20/09

56 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896079 Method Blank

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

VXX19405

SW5030B

05/20/2009

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

1,1-Dichloroethene ND 1.00 0.310 ug/L 05/20/09

2-Butanone (MEK) ND 10.0 3.10 ug/L 05/20/09

Methylene chloride ND 5.00 1.00 ug/L 05/20/09

Trichlorofluoromethane ND 1.00 0.310 ug/L 05/20/09

P & M -Xylene ND 2.00 0.620 ug/L 05/20/09

Naphthalene ND 2.00 0.620 ug/L 05/20/09

o-Xylene ND 1.00 0.310 ug/L 05/20/09

Bromoform ND 1.00 0.310 ug/L 05/20/09

1-Chlorohexane ND 1.00 0.310 ug/L 05/20/09

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 05/20/09

tert-Butylbenzene ND 1.00 0.310 ug/L 05/20/09

1,1-Dichloroethane ND 1.00 0.310 ug/L 05/20/09

2-Chlorotoluene ND 1.00 0.310 ug/L 05/20/09

Trichloroethene ND 1.00 0.310 ug/L 05/20/09

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 05/20/09

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 05/20/09

2,2-Dichloropropane ND 1.00 0.310 ug/L 05/20/09

Hexachlorobutadiene ND 1.00 0.310 ug/L 05/20/09

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 05/20/09

1,2-Dichloropropane ND 1.00 0.310 ug/L 05/20/09

1,1-Dichloropropene ND 1.00 0.310 ug/L 05/20/09

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 05/20/09

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 05/20/09

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 05/20/09

Surrogates 

1,2-Dichloroethane-D4 <surr> 112 73-120 % 05/20/09

Toluene-d8 <surr> 96.5 80-120 % 05/20/09

4-Bromofluorobenzene <surr> 99.4 76-120 % 05/20/09

Instrument

Method

Batch VMS10497

SW8260B

HP 5890 Series II MS3 VNA

57 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896435 Method Blank

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

MXX21701

SW3010A

05/22/2009

QC results affect the following production samples:

1092054001, 1092054004, 1092054005, 1092054006, 1092054007, 1092054008

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Metals by ICP/MS

Lead ND 1.00 0.310 ug/L 05/25/09

Instrument

Method

Batch MMS5916

SW6020

Perkin Elmer Sciex ICP-MS P3

58 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896525 Method Blank

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

VXX19411

SW5030B

05/24/2009

QC results affect the following production samples:

1092054001, 1092054004, 1092054005, 1092054006, 1092054007, 1092054008, 1092054009

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 05/24/09

Surrogates 

1,2-Dichloroethane-D4 <surr> 110 73-120 % 05/24/09

Toluene-d8 <surr> 99.7 80-120 % 05/24/09

4-Bromofluorobenzene <surr> 99.5 76-120 % 05/24/09

Instrument

Method

Batch VMS10501

SW8260B

HP 5890 Series II MS3 VNA

59 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896553 Method Blank

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

XXX20855

SW3520C

05/26/2009

QC results affect the following production samples:

1092054008

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Polynuclear Aromatics GC/MS

Acenaphthylene ND 0.0500 0.0150 ug/L 05/28/09

Acenaphthene ND 0.0500 0.0150 ug/L 05/28/09

Fluorene ND 0.0500 0.0150 ug/L 05/28/09

Phenanthrene ND 0.0500 0.0150 ug/L 05/28/09

Anthracene ND 0.0500 0.0150 ug/L 05/28/09

Fluoranthene ND 0.0500 0.0150 ug/L 05/28/09

Pyrene ND 0.0500 0.0150 ug/L 05/28/09

Benzo(a)Anthracene ND 0.0500 0.0150 ug/L 05/28/09

Chrysene ND 0.0500 0.0150 ug/L 05/28/09

Benzo[b]Fluoranthene ND 0.0500 0.0150 ug/L 05/28/09

Benzo[k]fluoranthene ND 0.0500 0.0150 ug/L 05/28/09

Benzo[a]pyrene ND 0.0500 0.0150 ug/L 05/28/09

Indeno[1,2,3-c,d] pyrene ND 0.0500 0.0150 ug/L 05/28/09

Dibenzo[a,h]anthracene ND 0.0500 0.0150 ug/L 05/28/09

Benzo[g,h,i]perylene ND 0.0500 0.0150 ug/L 05/28/09

Naphthalene ND 0.100 0.0310 ug/L 05/28/09

1-Methylnaphthalene ND 0.0500 0.0150 ug/L 05/28/09

2-Methylnaphthalene ND 0.0500 0.0150 ug/L 05/28/09

Surrogates 

Terphenyl-d14 <surr> 85.2 50-135 % 05/28/09

Instrument

Method

Batch XMS4906

8270D SIMS

HP 6890/5973 MS SVOA

60 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896687 Method Blank

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

VXX19416

SW5030B

05/26/2009

QC results affect the following production samples:

1092054001, 1092054004, 1092054005, 1092054006, 1092054007, 1092054008

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Fuels Department

Gasoline Range Organics 14.9 J 100 10.0 ug/L 05/26/09

Surrogates 

4-Bromofluorobenzene <surr> 102 50-150 % 05/26/09

Instrument

Method

Batch VFC9431

SW8015C

HP 5890 Series II PID+HECD VBA

61 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896796 Method Blank

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

XXX20862

SW3520C

05/27/2009

QC results affect the following production samples:

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Polynuclear Aromatics GC/MS

Acenaphthylene ND 0.0500 0.0150 ug/L 05/28/09

Acenaphthene ND 0.0500 0.0150 ug/L 05/28/09

Fluorene ND 0.0500 0.0150 ug/L 05/28/09

Phenanthrene ND 0.0500 0.0150 ug/L 05/28/09

Anthracene ND 0.0500 0.0150 ug/L 05/28/09

Fluoranthene ND 0.0500 0.0150 ug/L 05/28/09

Pyrene ND 0.0500 0.0150 ug/L 05/28/09

Benzo(a)Anthracene ND 0.0500 0.0150 ug/L 05/28/09

Chrysene ND 0.0500 0.0150 ug/L 05/28/09

Benzo[b]Fluoranthene ND 0.0500 0.0150 ug/L 05/28/09

Benzo[k]fluoranthene ND 0.0500 0.0150 ug/L 05/28/09

Benzo[a]pyrene ND 0.0500 0.0150 ug/L 05/28/09

Indeno[1,2,3-c,d] pyrene ND 0.0500 0.0150 ug/L 05/28/09

Dibenzo[a,h]anthracene ND 0.0500 0.0150 ug/L 05/28/09

Benzo[g,h,i]perylene ND 0.0500 0.0150 ug/L 05/28/09

Naphthalene ND 0.100 0.0310 ug/L 05/28/09

1-Methylnaphthalene ND 0.0500 0.0150 ug/L 05/28/09

2-Methylnaphthalene ND 0.0500 0.0150 ug/L 05/28/09

Surrogates 

Terphenyl-d14 <surr> 84.4 50-135 % 05/28/09

Instrument

Method

Batch XMS4906

8270D SIMS

HP 6890/5973 MS SVOA

62 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

897585 Method Blank

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

VXX19432

SW5030B

05/21/2009

QC results affect the following production samples:

1092054009

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Fuels Department

Gasoline Range Organics 14.5 J 100 10.0 ug/L 05/21/09

Surrogates 

4-Bromofluorobenzene <surr> 102 50-150 % 05/21/09

Instrument

Method

Batch VFC9438

SW8015C

HP 5890 Series II PID+HECD VBA

63 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

895549 Lab Control Sample

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

XXX20829

SW3520C

05/19/2009

QC results affect the following production samples:

1092054001, 1092054004, 1092054005, 1092054006, 1092054007

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Acenaphthylene LCS 0.394 79 ( 50-105 ) 0.5 ug/L 05/22/2009

Acenaphthene LCS 0.387 77 ( 45-110 ) 0.5 ug/L 05/22/2009

Fluorene LCS 0.404 81 ( 50-110 ) 0.5 ug/L 05/22/2009

Phenanthrene LCS 0.400 80 ( 50-115 ) 0.5 ug/L 05/22/2009

Anthracene LCS 0.408 82 ( 55-110 ) 0.5 ug/L 05/22/2009

Fluoranthene LCS 0.483 97 ( 55-125 ) 0.5 ug/L 05/22/2009

Pyrene LCS 0.466 93 ( 50-130 ) 0.5 ug/L 05/22/2009

Benzo(a)Anthracene LCS 0.465 93 ( 55-120 ) 0.5 ug/L 05/22/2009

Chrysene LCS 0.451 90 ( 55-120 ) 0.5 ug/L 05/22/2009

Benzo[b]Fluoranthene LCS 0.454 91 ( 46-130 ) 0.5 ug/L 05/22/2009

Benzo[k]fluoranthene LCS 0.448 90 ( 60-125 ) 0.5 ug/L 05/22/2009

Benzo[a]pyrene LCS 0.464 93 ( 55-120 ) 0.5 ug/L 05/22/2009

Indeno[1,2,3-c,d] pyrene LCS 0.455 91 ( 45-125 ) 0.5 ug/L 05/22/2009

Dibenzo[a,h]anthracene LCS 0.468 94 ( 41-140 ) 0.5 ug/L 05/22/2009

Benzo[g,h,i]perylene LCS 0.439 88 ( 46-125 ) 0.5 ug/L 05/22/2009

Naphthalene LCS 0.367 73 ( 42-100 ) 0.5 ug/L 05/22/2009

1-Methylnaphthalene LCS 0.391 78 ( 46-115 ) 0.5 ug/L 05/22/2009

2-Methylnaphthalene LCS 0.358 72 ( 45-105 ) 0.5 ug/L 05/22/2009

Surrogates 

Terphenyl-d14 <surr> LCS 97 ( 50-135 ) 05/22/2009

64 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

895549 Lab Control Sample

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

XXX20829

SW3520C

05/19/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Batch

Method

Instrument

XMS4898

8270D SIMS

HP 6890/5973 MS SVOA

65 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

895713 Lab Control Sample

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

XXX20835

SW3520C

05/20/2009

QC results affect the following production samples:

1092054001, 1092054004, 1092054005, 1092054006, 1092054007, 1092054008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Semivolatile Organic Fuels Department

Diesel Range Organics LCS 4.35 87 ( 75-125 ) 5 mg/L 06/03/2009

Surrogates 

5a Androstane <surr> LCS 97 ( 60-120 ) 06/03/2009

Batch

Method

Instrument

XFC8556

SW8015C

HP 6890 Series II FID SV D R

66 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896080 Lab Control Sample

896081 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

VXX19405

SW5030B

05/20/2009

QC results affect the following production samples:

1092054001, 1092054004, 1092054005, 1092054006, 1092054007, 1092054008, 1092054009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

67 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896080 Lab Control Sample

896081 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

VXX19405

SW5030B

05/20/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Benzene LCS 29.9 100 ( 80-120 ) 30 ug/L 05/20/2009

LCSD 26.8 89 11 (< 20 ) 30 ug/L 05/20/2009

Toluene LCS 31.0 103 ( 77-120 ) 30 ug/L 05/20/2009

LCSD 27.9 93 11 (< 20 ) 30 ug/L 05/20/2009

Ethylbenzene LCS 31.6 105 ( 80-120 ) 30 ug/L 05/20/2009

LCSD 29.3 98 7 (< 20 ) 30 ug/L 05/20/2009

n-Butylbenzene LCS 32.0 107 ( 80-124 ) 30 ug/L 05/20/2009

LCSD 30.0 100 6 (< 20 ) 30 ug/L 05/20/2009

1,4-Dichlorobenzene LCS 32.2 107 ( 80-120 ) 30 ug/L 05/20/2009

LCSD 30.3 101 6 (< 20 ) 30 ug/L 05/20/2009

1,2-Dichloroethane LCS 33.5 112 ( 80-129 ) 30 ug/L 05/20/2009

LCSD 27.9 93 18 (< 20 ) 30 ug/L 05/20/2009

1,3,5-Trimethylbenzene LCS 31.6 105 ( 80-128 ) 30 ug/L 05/20/2009

LCSD 29.3 98 7 (< 20 ) 30 ug/L 05/20/2009

4-Chlorotoluene LCS 32.5 108 ( 79-128 ) 30 ug/L 05/20/2009

LCSD 29.8 99 9 (< 20 ) 30 ug/L 05/20/2009

Chlorobenzene LCS 31.6 105 ( 80-120 ) 30 ug/L 05/20/2009

LCSD 29.0 97 9 (< 20 ) 30 ug/L 05/20/2009

4-Methyl-2-pentanone (MIBK) LCS 99.5 111 ( 69-134 ) 90 ug/L 05/20/2009

LCSD 99.5 111 0 (< 20 ) 90 ug/L 05/20/2009

cis-1,2-Dichloroethene LCS 33.8 113 ( 80-125 ) 30 ug/L 05/20/2009

LCSD 29.9 100 12 (< 20 ) 30 ug/L 05/20/2009

4-Isopropyltoluene LCS 32.4 108 ( 80-125 ) 30 ug/L 05/20/2009

LCSD 30.2 101 7 (< 20 ) 30 ug/L 05/20/2009

cis-1,3-Dichloropropene LCS 30.2 101 ( 80-120 ) 30 ug/L 05/20/2009

LCSD 25.0 83 19 (< 20 ) 30 ug/L 05/20/2009

n-Propylbenzene LCS 32.2 107 ( 80-129 ) 30 ug/L 05/20/2009

LCSD 29.6 99 8 (< 20 ) 30 ug/L 05/20/2009

68 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896080 Lab Control Sample

896081 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

VXX19405

SW5030B

05/20/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Styrene LCS 32.6 109 ( 80-120 ) 30 ug/L 05/20/2009

LCSD 30.7 102 6 (< 20 ) 30 ug/L 05/20/2009

Dibromomethane LCS 32.2 107 ( 80-120 ) 30 ug/L 05/20/2009

LCSD 28.3 94 13 (< 20 ) 30 ug/L 05/20/2009

trans-1,3-Dichloropropene LCS 33.5 112 ( 80-124 ) 30 ug/L 05/20/2009

LCSD 27.9 93 18 (< 20 ) 30 ug/L 05/20/2009

1,2,4-Trichlorobenzene LCS 32.2 107 ( 80-120 ) 30 ug/L 05/20/2009

LCSD 31.6 105 2 (< 20 ) 30 ug/L 05/20/2009

Acetone LCS 95.1 106 ( 50-135 ) 90 ug/L 05/20/2009

LCSD 90.9 101 5 (< 20 ) 90 ug/L 05/20/2009

1,1,2,2-Tetrachloroethane LCS 31.6 105 ( 76-123 ) 30 ug/L 05/20/2009

LCSD 29.5 98 7 (< 20 ) 30 ug/L 05/20/2009

1,2-Dibromo-3-chloropropane LCS 33.6 112 ( 73-130 ) 30 ug/L 05/20/2009

LCSD 32.7 109 3 (< 20 ) 30 ug/L 05/20/2009

Methyl-t-butyl ether LCS 51.5 115 ( 80-120 ) 45 ug/L 05/20/2009

LCSD 42.4 94 20 (< 20 ) 45 ug/L 05/20/2009

Tetrachloroethene LCS 32.5 108 ( 79-122 ) 30 ug/L 05/20/2009

LCSD 28.4 95 14 (< 20 ) 30 ug/L 05/20/2009

Dibromochloromethane LCS 34.9 116 ( 80-120 ) 30 ug/L 05/20/2009

LCSD 28.5 95 20 * (< 20 ) 30 ug/L 05/20/2009

1,3-Dichloropropane LCS 33.3 111 ( 80-121 ) 30 ug/L 05/20/2009

LCSD 27.9 93 18 (< 20 ) 30 ug/L 05/20/2009

1,2-Dibromoethane LCS 31.7 106 ( 80-120 ) 30 ug/L 05/20/2009

LCSD 27.3 91 15 (< 20 ) 30 ug/L 05/20/2009

Carbon tetrachloride LCS 32.6 109 ( 80-126 ) 30 ug/L 05/20/2009

LCSD 25.2 84 25 * (< 20 ) 30 ug/L 05/20/2009

1,1,1,2-Tetrachloroethane LCS 34.1 114 ( 80-120 ) 30 ug/L 05/20/2009

69 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896080 Lab Control Sample

896081 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

VXX19405

SW5030B

05/20/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

LCSD 29.0 97 16 (< 20 ) 30 ug/L 05/20/2009

Chloroform LCS 31.5 105 ( 80-124 ) 30 ug/L 05/20/2009

LCSD 27.3 91 14 (< 20 ) 30 ug/L 05/20/2009

Bromobenzene LCS 31.2 104 ( 80-120 ) 30 ug/L 05/20/2009

LCSD 29.4 98 6 (< 20 ) 30 ug/L 05/20/2009

Chloromethane LCS 27.4 91 ( 67-125 ) 30 ug/L 05/20/2009

LCSD 26.9 90 2 (< 20 ) 30 ug/L 05/20/2009

1,2,3-Trichloropropane LCS 29.9 100 ( 80-120 ) 30 ug/L 05/20/2009

LCSD 28.7 96 4 (< 20 ) 30 ug/L 05/20/2009

Bromomethane LCS 29.4 98 ( 30-140 ) 30 ug/L 05/20/2009

LCSD 30.5 102 4 (< 20 ) 30 ug/L 05/20/2009

Bromochloromethane LCS 32.5 108 ( 77-129 ) 30 ug/L 05/20/2009

LCSD 30.9 103 5 (< 20 ) 30 ug/L 05/20/2009

Vinyl chloride LCS 31.2 104 ( 72-145 ) 30 ug/L 05/20/2009

LCSD 30.8 103 1 (< 20 ) 30 ug/L 05/20/2009

Dichlorodifluoromethane LCS 32.3 108 ( 62-153 ) 30 ug/L 05/20/2009

LCSD 30.3 101 6 (< 20 ) 30 ug/L 05/20/2009

Chloroethane LCS 34.6 115 ( 67-133 ) 30 ug/L 05/20/2009

LCSD 29.8 99 15 (< 20 ) 30 ug/L 05/20/2009

sec-Butylbenzene LCS 31.6 105 ( 80-120 ) 30 ug/L 05/20/2009

LCSD 29.3 98 7 (< 20 ) 30 ug/L 05/20/2009

Bromodichloromethane LCS 32.6 109 ( 80-120 ) 30 ug/L 05/20/2009

LCSD 25.4 85 25 * (< 20 ) 30 ug/L 05/20/2009

1,1-Dichloroethene LCS 32.7 109 ( 76-130 ) 30 ug/L 05/20/2009

LCSD 29.6 99 10 (< 20 ) 30 ug/L 05/20/2009

2-Butanone (MEK) LCS 98.7 110 ( 66-136 ) 90 ug/L 05/20/2009

LCSD 87.1 97 13 (< 20 ) 90 ug/L 05/20/2009

70 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896080 Lab Control Sample

896081 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

VXX19405

SW5030B

05/20/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Methylene chloride LCS 32.1 107 ( 63-131 ) 30 ug/L 05/20/2009

LCSD 31.3 104 3 (< 20 ) 30 ug/L 05/20/2009

Trichlorofluoromethane LCS 34.3 114 ( 68-145 ) 30 ug/L 05/20/2009

LCSD 31.3 104 9 (< 20 ) 30 ug/L 05/20/2009

P & M -Xylene LCS 63.7 106 ( 80-120 ) 60 ug/L 05/20/2009

LCSD 58.2 97 9 (< 20 ) 60 ug/L 05/20/2009

Naphthalene LCS 29.4 98 ( 75-120 ) 30 ug/L 05/20/2009

LCSD 29.7 99 1 (< 20 ) 30 ug/L 05/20/2009

o-Xylene LCS 32.5 108 ( 80-120 ) 30 ug/L 05/20/2009

LCSD 30.5 102 6 (< 20 ) 30 ug/L 05/20/2009

Bromoform LCS 29.9 100 ( 80-120 ) 30 ug/L 05/20/2009

LCSD 27.0 90 10 (< 20 ) 30 ug/L 05/20/2009

1-Chlorohexane LCS 50.2 111 ( 70-125 ) 45 ug/L 05/20/2009

LCSD 45.0 100 11 (< 20 ) 45 ug/L 05/20/2009

1,2,4-Trimethylbenzene LCS 32.0 107 ( 80-125 ) 30 ug/L 05/20/2009

LCSD 29.8 99 7 (< 20 ) 30 ug/L 05/20/2009

tert-Butylbenzene LCS 33.0 110 ( 80-122 ) 30 ug/L 05/20/2009

LCSD 30.7 102 7 (< 20 ) 30 ug/L 05/20/2009

1,1-Dichloroethane LCS 34.8 116 ( 80-120 ) 30 ug/L 05/20/2009

LCSD 32.0 107 8 (< 20 ) 30 ug/L 05/20/2009

2-Chlorotoluene LCS 31.0 103 ( 80-125 ) 30 ug/L 05/20/2009

LCSD 31.7 106 2 (< 20 ) 30 ug/L 05/20/2009

Trichloroethene LCS 32.3 108 ( 80-125 ) 30 ug/L 05/20/2009

LCSD 27.3 91 17 (< 20 ) 30 ug/L 05/20/2009

trans-1,2-Dichloroethene LCS 32.2 107 ( 79-132 ) 30 ug/L 05/20/2009

LCSD 27.2 91 17 (< 20 ) 30 ug/L 05/20/2009

1,2-Dichlorobenzene LCS 31.3 104 ( 80-120 ) 30 ug/L 05/20/2009

LCSD 30.0 100 4 (< 20 ) 30 ug/L 05/20/2009

71 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896080 Lab Control Sample

896081 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

VXX19405

SW5030B

05/20/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

2,2-Dichloropropane LCS 35.6 119 ( 80-132 ) 30 ug/L 05/20/2009

LCSD 27.6 92 25 * (< 20 ) 30 ug/L 05/20/2009

Hexachlorobutadiene LCS 33.0 110 ( 77-125 ) 30 ug/L 05/20/2009

LCSD 31.3 104 5 (< 20 ) 30 ug/L 05/20/2009

Isopropylbenzene (Cumene) LCS 33.3 111 ( 80-121 ) 30 ug/L 05/20/2009

LCSD 30.7 102 8 (< 20 ) 30 ug/L 05/20/2009

1,2-Dichloropropane LCS 33.1 110 ( 80-121 ) 30 ug/L 05/20/2009

LCSD 28.2 94 16 (< 20 ) 30 ug/L 05/20/2009

1,1-Dichloropropene LCS 31.4 105 ( 80-122 ) 30 ug/L 05/20/2009

LCSD 26.0 87 19 (< 20 ) 30 ug/L 05/20/2009

1,1,2-Trichloroethane LCS 31.9 106 ( 77-120 ) 30 ug/L 05/20/2009

LCSD 26.4 88 19 (< 20 ) 30 ug/L 05/20/2009

1,3-Dichlorobenzene LCS 32.0 107 ( 80-120 ) 30 ug/L 05/20/2009

LCSD 30.0 100 7 (< 20 ) 30 ug/L 05/20/2009

1,2,3-Trichlorobenzene LCS 32.4 108 ( 77-120 ) 30 ug/L 05/20/2009

LCSD 31.3 104 3 (< 20 ) 30 ug/L 05/20/2009

Surrogates 

1,2-Dichloroethane-D4 <surr> LCS 107 ( 73-120 ) 05/20/2009

LCSD 93 14 05/20/2009

Toluene-d8 <surr> LCS 99 ( 80-120 ) 05/20/2009

LCSD 96 3 05/20/2009

4-Bromofluorobenzene <surr> LCS 99 ( 76-120 ) 05/20/2009

LCSD 99 0 05/20/2009

Batch

Method

Instrument

VMS10497

SW8260B

HP 5890 Series II MS3 VNA

72 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896436 Lab Control Sample

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

MXX21701

SW3010A

05/22/2009

QC results affect the following production samples:

1092054001, 1092054004, 1092054005, 1092054006, 1092054007, 1092054008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Metals by ICP/MS

Lead LCS 907 91 ( 80-120 ) 1000 ug/L 05/25/2009

Batch

Method

Instrument

MMS5916

SW6020

Perkin Elmer Sciex ICP-MS P3

73 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896526 Lab Control Sample

896527 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

VXX19411

SW5030B

05/24/2009

QC results affect the following production samples:

1092054001, 1092054004, 1092054005, 1092054006, 1092054007, 1092054008, 1092054009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

1,1,1-Trichloroethane LCS 35.0 117 ( 80-122 ) 30 ug/L 05/24/2009

LCSD 33.4 111 5 (< 20 ) 30 ug/L 05/24/2009

Surrogates 

1,2-Dichloroethane-D4 <surr> LCS 102 ( 73-120 ) 05/24/2009

LCSD 103 1 05/24/2009

Toluene-d8 <surr> LCS 100 ( 80-120 ) 05/24/2009

LCSD 100 0 05/24/2009

4-Bromofluorobenzene <surr> LCS 99 ( 76-120 ) 05/24/2009

LCSD 99 0 05/24/2009

Batch

Method

Instrument

VMS10501

SW8260B

HP 5890 Series II MS3 VNA

74 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896554 Lab Control Sample

896555 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

XXX20855

SW3520C

05/26/2009

QC results affect the following production samples:

1092054008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

75 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896554 Lab Control Sample

896555 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

XXX20855

SW3520C

05/26/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Acenaphthylene LCS 0.348 70 ( 50-105 ) 0.5 ug/L 05/28/2009

LCSD 0.340 68 2 (< 30 ) 0.5 ug/L 05/28/2009

Acenaphthene LCS 0.360 72 ( 45-110 ) 0.5 ug/L 05/28/2009

LCSD 0.350 70 3 (< 30 ) 0.5 ug/L 05/28/2009

Fluorene LCS 0.382 76 ( 50-110 ) 0.5 ug/L 05/28/2009

LCSD 0.376 75 2 (< 30 ) 0.5 ug/L 05/28/2009

Phenanthrene LCS 0.364 73 ( 50-115 ) 0.5 ug/L 05/28/2009

LCSD 0.364 73 0 (< 30 ) 0.5 ug/L 05/28/2009

Anthracene LCS 0.413 83 ( 55-110 ) 0.5 ug/L 05/28/2009

LCSD 0.408 82 1 (< 30 ) 0.5 ug/L 05/28/2009

Fluoranthene LCS 0.452 90 ( 55-125 ) 0.5 ug/L 05/28/2009

LCSD 0.439 88 3 (< 30 ) 0.5 ug/L 05/28/2009

Pyrene LCS 0.435 87 ( 50-130 ) 0.5 ug/L 05/28/2009

LCSD 0.422 84 3 (< 30 ) 0.5 ug/L 05/28/2009

Benzo(a)Anthracene LCS 0.452 90 ( 55-120 ) 0.5 ug/L 05/28/2009

LCSD 0.437 87 3 (< 30 ) 0.5 ug/L 05/28/2009

Chrysene LCS 0.466 93 ( 55-120 ) 0.5 ug/L 05/28/2009

LCSD 0.455 91 2 (< 30 ) 0.5 ug/L 05/28/2009

Benzo[b]Fluoranthene LCS 0.421 84 ( 46-130 ) 0.5 ug/L 05/28/2009

LCSD 0.416 83 1 (< 30 ) 0.5 ug/L 05/28/2009

Benzo[k]fluoranthene LCS 0.511 102 ( 60-125 ) 0.5 ug/L 05/28/2009

LCSD 0.485 97 5 (< 30 ) 0.5 ug/L 05/28/2009

Benzo[a]pyrene LCS 0.479 96 ( 55-120 ) 0.5 ug/L 05/28/2009

LCSD 0.461 92 4 (< 30 ) 0.5 ug/L 05/28/2009

Indeno[1,2,3-c,d] pyrene LCS 0.471 94 ( 45-125 ) 0.5 ug/L 05/28/2009

LCSD 0.452 90 4 (< 30 ) 0.5 ug/L 05/28/2009

Dibenzo[a,h]anthracene LCS 0.475 95 ( 41-140 ) 0.5 ug/L 05/28/2009

LCSD 0.457 91 4 (< 30 ) 0.5 ug/L 05/28/2009

76 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896554 Lab Control Sample

896555 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

XXX20855

SW3520C

05/26/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Benzo[g,h,i]perylene LCS 0.464 93 ( 46-125 ) 0.5 ug/L 05/28/2009

LCSD 0.438 88 6 (< 30 ) 0.5 ug/L 05/28/2009

Naphthalene LCS 0.328 66 ( 42-100 ) 0.5 ug/L 05/28/2009

LCSD 0.324 65 2 (< 30 ) 0.5 ug/L 05/28/2009

1-Methylnaphthalene LCS 0.326 65 ( 46-115 ) 0.5 ug/L 05/28/2009

LCSD 0.316 63 3 (< 30 ) 0.5 ug/L 05/28/2009

2-Methylnaphthalene LCS 0.264 53 ( 45-105 ) 0.5 ug/L 05/28/2009

LCSD 0.263 53 0 (< 30 ) 0.5 ug/L 05/28/2009

Surrogates 

Terphenyl-d14 <surr> LCS 77 ( 50-135 ) 05/28/2009

LCSD 79 3 05/28/2009

Batch

Method

Instrument

XMS4906

8270D SIMS

HP 6890/5973 MS SVOA

77 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896689 Lab Control Sample

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

VXX19416

SW5030B

05/26/2009

QC results affect the following production samples:

1092054001, 1092054004, 1092054005, 1092054006, 1092054007, 1092054008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Fuels Department

Gasoline Range Organics LCS 215 108 ( 79-108 ) 200 ug/L 05/26/2009

Surrogates 

4-Bromofluorobenzene <surr> LCS 102 ( 50-150 ) 05/26/2009

Batch

Method

Instrument

VFC9431

SW8015C

HP 5890 Series II PID+HECD VBA

78 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896797 Lab Control Sample

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

XXX20862

SW3520C

05/27/2009

QC results affect the following production samples:

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

79 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896797 Lab Control Sample

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

XXX20862

SW3520C

05/27/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Acenaphthylene LCS 0.316 63 ( 50-105 ) 0.5 ug/L 05/28/2009

Acenaphthene LCS 0.327 65 ( 45-110 ) 0.5 ug/L 05/28/2009

Fluorene LCS 0.349 70 ( 50-110 ) 0.5 ug/L 05/28/2009

Phenanthrene LCS 0.350 70 ( 50-115 ) 0.5 ug/L 05/28/2009

Anthracene LCS 0.390 78 ( 55-110 ) 0.5 ug/L 05/28/2009

Fluoranthene LCS 0.416 83 ( 55-125 ) 0.5 ug/L 05/28/2009

Pyrene LCS 0.406 81 ( 50-130 ) 0.5 ug/L 05/28/2009

Benzo(a)Anthracene LCS 0.419 84 ( 55-120 ) 0.5 ug/L 05/28/2009

Chrysene LCS 0.442 88 ( 55-120 ) 0.5 ug/L 05/28/2009

Benzo[b]Fluoranthene LCS 0.389 78 ( 46-130 ) 0.5 ug/L 05/28/2009

Benzo[k]fluoranthene LCS 0.440 88 ( 60-125 ) 0.5 ug/L 05/28/2009

Benzo[a]pyrene LCS 0.443 89 ( 55-120 ) 0.5 ug/L 05/28/2009

Indeno[1,2,3-c,d] pyrene LCS 0.421 84 ( 45-125 ) 0.5 ug/L 05/28/2009

Dibenzo[a,h]anthracene LCS 0.417 83 ( 41-140 ) 0.5 ug/L 05/28/2009

Benzo[g,h,i]perylene LCS 0.407 81 ( 46-125 ) 0.5 ug/L 05/28/2009

Naphthalene LCS 0.314 63 ( 42-100 ) 0.5 ug/L 05/28/2009

1-Methylnaphthalene LCS 0.301 60 ( 46-115 ) 0.5 ug/L 05/28/2009

2-Methylnaphthalene LCS 0.244 49 ( 45-105 ) 0.5 ug/L 05/28/2009

Surrogates 

Terphenyl-d14 <surr> LCS 84 ( 50-135 ) 05/28/2009

80 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

896797 Lab Control Sample

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

XXX20862

SW3520C

05/27/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Batch

Method

Instrument

XMS4906

8270D SIMS

HP 6890/5973 MS SVOA

81 of 101
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Prep

897586 Lab Control Sample

897587 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

Red Hills BFSF

Water (Surface, Eff., Ground)

VXX19432

SW5030B

05/21/2009

QC results affect the following production samples:

1092054009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Fuels Department

Gasoline Range Organics LCS 203 101 ( 79-108 ) 200 ug/L 05/21/2009

LCSD 199 99 2 (< 20 ) 200 ug/L 05/22/2009

Surrogates 

4-Bromofluorobenzene <surr> LCS 103 ( 50-150 ) 05/21/2009

LCSD 109 5 05/22/2009

Batch

Method

Instrument

VFC9438

SW8015C

HP 5890 Series II PID+HECD VBA

82 of 101
Matrix

SGS Ref.# Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Original

Prep

1092054002 Billable Matrix Spike

1092054003 Billable Matrix Spike Dup.

1092054001

Water (Surface, Eff., Ground)

MXX21701

3010 H20 Digest for Metals ICP-MS

05/22/2009

QC results affect the following production samples:

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Dissolved Metals by ICP/MS

Lead BMS ND 977 98 ( 80-120 ) 1000 ug/L 05/25/2009

BMSD 991 99 1 (< 15 ) 1000 ug/L 05/25/2009

Batch

Method

Instrument

MMS5916

SW6020

Perkin Elmer Sciex ICP-MS P3

Volatile Fuels Department

Gasoline Range Organics BMS 19.1 J 485 103 ( 79-108 ) 450 ug/L 05/26/2009

BMSD 464 99 4 (< 20 ) 450 ug/L 05/26/2009

Surrogates 

4-Bromofluorobenzene <surr> BMS 54.5 109 ( 50-150 ) 05/26/2009

BMSD 54.3 109 0 05/26/2009

Batch

Method

Instrument

VFC9431

SW8015C

HP 5890 Series II PID+HECD VBA

Semivolatile Organic Fuels Department

Diesel Range Organics BMS ND 5.11 90 ( 75-125 ) 5.68 mg/L 06/03/2009

BMSD 4.95 88 3 (< 30 ) 5.62 mg/L 06/03/2009

Surrogates 

5a Androstane <surr> BMS .112 98 ( 50-150 ) 06/03/2009

BMSD 0.111 99 0 06/03/2009

Batch

Method

Instrument

XFC8556

SW8015C

HP 6890 Series II FID SV D R

Volatile Gas Chromatography/Mass Spectroscopy

83 of 101
Matrix

SGS Ref.# Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Original

Prep

1092054002 Billable Matrix Spike

1092054003 Billable Matrix Spike Dup.

1092054001

Water (Surface, Eff., Ground)

VXX19405

Volatiles Extraction AFCEE 3.1 8260 (

05/20/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

Benzene BMS ND 28 93 ( 80-120 ) 30.0 ug/L 05/20/2009

BMSD 28.6 95 2 (< 20 ) 30.0 ug/L 05/20/2009

Toluene BMS ND 28.2 94 ( 77-120 ) 30.0 ug/L 05/20/2009

BMSD 29.2 97 4 (< 20 ) 30.0 ug/L 05/20/2009

Ethylbenzene BMS ND 29.7 99 ( 80-120 ) 30.0 ug/L 05/20/2009

BMSD 30.1 100 1 (< 20 ) 30.0 ug/L 05/20/2009

n-Butylbenzene BMS ND 30.6 102 ( 80-124 ) 30.0 ug/L 05/20/2009

BMSD 31.5 105 3 (< 20 ) 30.0 ug/L 05/20/2009

1,4-Dichlorobenzene BMS ND 30.3 101 ( 80-120 ) 30.0 ug/L 05/20/2009

BMSD 31.8 106 5 (< 20 ) 30.0 ug/L 05/20/2009

1,2-Dichloroethane BMS ND 29.2 97 ( 80-129 ) 30.0 ug/L 05/20/2009

BMSD 27.7 93 5 (< 20 ) 30.0 ug/L 05/20/2009

1,3,5-Trimethylbenzene BMS ND 29.9 100 ( 80-128 ) 30.0 ug/L 05/20/2009

BMSD 30.4 101 2 (< 20 ) 30.0 ug/L 05/20/2009

4-Chlorotoluene BMS ND 30.5 102 ( 79-128 ) 30.0 ug/L 05/20/2009

BMSD 31.3 104 3 (< 20 ) 30.0 ug/L 05/20/2009

Chlorobenzene BMS ND 29.3 98 ( 80-120 ) 30.0 ug/L 05/20/2009

BMSD 30.3 101 3 (< 20 ) 30.0 ug/L 05/20/2009

4-Methyl-2-pentanone (MIBK) BMS ND 93.5 104 ( 69-134 ) 90.0 ug/L 05/20/2009

BMSD 97.0 108 4 (< 20 ) 90.0 ug/L 05/20/2009

cis-1,2-Dichloroethene BMS ND 30.6 102 ( 80-125 ) 30.0 ug/L 05/20/2009

BMSD 30.4 101 1 (< 20 ) 30.0 ug/L 05/20/2009

4-Isopropyltoluene BMS ND 30.7 102 ( 80-125 ) 30.0 ug/L 05/20/2009

BMSD 32.0 107 4 (< 20 ) 30.0 ug/L 05/20/2009

cis-1,3-Dichloropropene BMS ND 27.9 93 ( 80-120 ) 30.0 ug/L 05/20/2009

BMSD 28.1 94 1 (< 20 ) 30.0 ug/L 05/20/2009

n-Propylbenzene BMS ND 30.3 101 ( 80-129 ) 30.0 ug/L 05/20/2009

BMSD 30.9 103 2 (< 20 ) 30.0 ug/L 05/20/2009

Styrene BMS ND 30.3 101 ( 80-120 ) 30.0 ug/L 05/20/2009

BMSD 30.4 101 0 (< 20 ) 30.0 ug/L 05/20/2009

Dibromomethane BMS ND 28.3 94 ( 80-120 ) 30.0 ug/L 05/20/2009

BMSD 28.1 94 0 (< 20 ) 30.0 ug/L 05/20/2009

trans-1,3-Dichloropropene BMS ND 29.8 99 ( 80-124 ) 30.0 ug/L 05/20/2009

BMSD 29.6 99 1 (< 20 ) 30.0 ug/L 05/20/2009

1,2,4-Trichlorobenzene BMS ND 31.1 104 ( 80-120 ) 30.0 ug/L 05/20/2009

BMSD 32.5 108 5 (< 20 ) 30.0 ug/L 05/20/2009

Acetone BMS ND 86.3 96 ( 50-135 ) 90.0 ug/L 05/20/2009

BMSD 89.4 99 3 (< 20 ) 90.0 ug/L 05/20/2009

1,1,2,2-Tetrachloroethane BMS ND 29.7 99 ( 76-123 ) 30.0 ug/L 05/20/2009

BMSD 30.3 101 2 (< 20 ) 30.0 ug/L 05/20/2009

84 of 101
Matrix

SGS Ref.# Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Original

Prep

1092054002 Billable Matrix Spike

1092054003 Billable Matrix Spike Dup.

1092054001

Water (Surface, Eff., Ground)

VXX19405

Volatiles Extraction AFCEE 3.1 8260 (

05/20/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

1,2-Dibromo-3-chloropropane BMS ND 31.1 104 ( 73-130 ) 30.0 ug/L 05/20/2009

BMSD 32.4 108 4 (< 20 ) 30.0 ug/L 05/20/2009

Methyl-t-butyl ether BMS ND 44.9 100 ( 80-120 ) 45.0 ug/L 05/20/2009

BMSD 45.6 101 2 (< 20 ) 45.0 ug/L 05/20/2009

Tetrachloroethene BMS ND 29.9 100 ( 79-122 ) 30.0 ug/L 05/20/2009

BMSD 30.8 103 3 (< 20 ) 30.0 ug/L 05/20/2009

Dibromochloromethane BMS ND 31 103 ( 80-120 ) 30.0 ug/L 05/20/2009

BMSD 31.4 105 1 (< 20 ) 30.0 ug/L 05/20/2009

1,3-Dichloropropane BMS ND 29.6 99 ( 80-121 ) 30.0 ug/L 05/20/2009

BMSD 29.7 99 0 (< 20 ) 30.0 ug/L 05/20/2009

1,2-Dibromoethane BMS ND 28.5 95 ( 80-120 ) 30.0 ug/L 05/20/2009

BMSD 29.0 97 2 (< 20 ) 30.0 ug/L 05/20/2009

Carbon tetrachloride BMS ND 28.6 95 ( 80-126 ) 30.0 ug/L 05/20/2009

BMSD 27.7 92 3 (< 20 ) 30.0 ug/L 05/20/2009

1,1,1,2-Tetrachloroethane BMS ND 30.9 103 ( 80-120 ) 30.0 ug/L 05/20/2009

BMSD 31.7 106 2 (< 20 ) 30.0 ug/L 05/20/2009

Chloroform BMS ND 27.6 92 ( 80-124 ) 30.0 ug/L 05/20/2009

BMSD 27.9 93 1 (< 20 ) 30.0 ug/L 05/20/2009

Bromobenzene BMS ND 29.7 99 ( 80-120 ) 30.0 ug/L 05/20/2009

BMSD 31.1 104 5 (< 20 ) 30.0 ug/L 05/20/2009

Chloromethane BMS ND 26.4 88 ( 67-125 ) 30.0 ug/L 05/20/2009

BMSD 26.1 87 1 (< 20 ) 30.0 ug/L 05/20/2009

1,2,3-Trichloropropane BMS ND 28.2 94 ( 80-120 ) 30.0 ug/L 05/20/2009

BMSD 29.6 99 5 (< 20 ) 30.0 ug/L 05/20/2009

Bromomethane BMS ND 31.6 105 ( 30-140 ) 30.0 ug/L 05/20/2009

BMSD 31.9 106 1 (< 20 ) 30.0 ug/L 05/20/2009

Bromochloromethane BMS ND 30.7 102 ( 77-129 ) 30.0 ug/L 05/20/2009

BMSD 31.7 106 3 (< 20 ) 30.0 ug/L 05/20/2009

Vinyl chloride BMS ND 30.7 102 ( 72-145 ) 30.0 ug/L 05/20/2009

BMSD 30.0 100 3 (< 20 ) 30.0 ug/L 05/20/2009

Dichlorodifluoromethane BMS ND 29.1 97 ( 62-153 ) 30.0 ug/L 05/20/2009

BMSD 29.3 98 1 (< 20 ) 30.0 ug/L 05/20/2009

Chloroethane BMS ND 29.9 100 ( 67-133 ) 30.0 ug/L 05/20/2009

BMSD 31.3 104 4 (< 20 ) 30.0 ug/L 05/20/2009

sec-Butylbenzene BMS ND 30.2 101 ( 80-120 ) 30.0 ug/L 05/20/2009

BMSD 31.0 103 3 (< 20 ) 30.0 ug/L 05/20/2009

Bromodichloromethane BMS ND 28.2 94 ( 80-120 ) 30.0 ug/L 05/20/2009

BMSD 27.7 92 2 (< 20 ) 30.0 ug/L 05/20/2009

1,1-Dichloroethene BMS ND 30.7 102 ( 76-130 ) 30.0 ug/L 05/20/2009

BMSD 31.0 103 1 (< 20 ) 30.0 ug/L 05/20/2009

85 of 101
Matrix

SGS Ref.# Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Original

Prep

1092054002 Billable Matrix Spike

1092054003 Billable Matrix Spike Dup.

1092054001

Water (Surface, Eff., Ground)

VXX19405

Volatiles Extraction AFCEE 3.1 8260 (

05/20/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

2-Butanone (MEK) BMS ND 90 100 ( 66-136 ) 90.0 ug/L 05/20/2009

BMSD 86.6 96 4 (< 20 ) 90.0 ug/L 05/20/2009

Methylene chloride BMS ND 30.3 101 ( 63-131 ) 30.0 ug/L 05/20/2009

BMSD 31.4 105 3 (< 20 ) 30.0 ug/L 05/20/2009

Trichlorofluoromethane BMS ND 31.6 105 ( 68-145 ) 30.0 ug/L 05/20/2009

BMSD 30.7 102 3 (< 20 ) 30.0 ug/L 05/20/2009

P & M -Xylene BMS ND 59.2 99 ( 80-120 ) 60.0 ug/L 05/20/2009

BMSD 60.5 101 2 (< 20 ) 60.0 ug/L 05/20/2009

Naphthalene BMS ND 28.7 96 ( 75-120 ) 30.0 ug/L 05/20/2009

BMSD 30.0 100 5 (< 20 ) 30.0 ug/L 05/20/2009

o-Xylene BMS ND 30.4 101 ( 80-120 ) 30.0 ug/L 05/20/2009

BMSD 31.1 104 2 (< 20 ) 30.0 ug/L 05/20/2009

Bromoform BMS ND 27.7 92 ( 80-120 ) 30.0 ug/L 05/20/2009

BMSD 28.1 94 2 (< 20 ) 30.0 ug/L 05/20/2009

1-Chlorohexane BMS ND 46.5 103 ( 70-125 ) 45.0 ug/L 05/20/2009

BMSD 47.0 104 1 (< 20 ) 45.0 ug/L 05/20/2009

1,2,4-Trimethylbenzene BMS ND 30 100 ( 80-125 ) 30.0 ug/L 05/20/2009

BMSD 31.0 103 3 (< 20 ) 30.0 ug/L 05/20/2009

tert-Butylbenzene BMS ND 31.6 105 ( 80-122 ) 30.0 ug/L 05/20/2009

BMSD 31.3 104 1 (< 20 ) 30.0 ug/L 05/20/2009

1,1,1-Trichloroethane BMS ND 34.5 115 ( 80-122 ) 30.0 ug/L 05/24/2009

BMSD 32.7 109 6 (< 20 ) 30.0 ug/L 05/24/2009

1,1-Dichloroethane BMS ND 32.4 108 ( 80-120 ) 30.0 ug/L 05/20/2009

BMSD 32.4 108 0 (< 20 ) 30.0 ug/L 05/20/2009

2-Chlorotoluene BMS ND 28.8 96 ( 80-125 ) 30.0 ug/L 05/20/2009

BMSD 30.0 100 4 (< 20 ) 30.0 ug/L 05/20/2009

Trichloroethene BMS ND 30.2 101 ( 80-125 ) 30.0 ug/L 05/20/2009

BMSD 29.9 100 1 (< 20 ) 30.0 ug/L 05/20/2009

trans-1,2-Dichloroethene BMS ND 28.4 95 ( 79-132 ) 30.0 ug/L 05/20/2009

BMSD 28.1 94 1 (< 20 ) 30.0 ug/L 05/20/2009

1,2-Dichlorobenzene BMS ND 29.5 98 ( 80-120 ) 30.0 ug/L 05/20/2009

BMSD 31.1 104 5 (< 20 ) 30.0 ug/L 05/20/2009

2,2-Dichloropropane BMS ND 31.6 105 ( 80-132 ) 30.0 ug/L 05/20/2009

BMSD 30.9 103 2 (< 20 ) 30.0 ug/L 05/20/2009

Hexachlorobutadiene BMS ND 32.2 107 ( 77-125 ) 30.0 ug/L 05/20/2009

BMSD 33.5 112 4 (< 20 ) 30.0 ug/L 05/20/2009

Isopropylbenzene (Cumene) BMS ND 31.2 104 ( 80-121 ) 30.0 ug/L 05/20/2009

BMSD 31.9 106 2 (< 20 ) 30.0 ug/L 05/20/2009

1,2-Dichloropropane BMS ND 30.5 102 ( 80-121 ) 30.0 ug/L 05/20/2009

BMSD 30.8 103 1 (< 20 ) 30.0 ug/L 05/20/2009

86 of 101
Matrix

SGS Ref.# Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Original

Prep

1092054002 Billable Matrix Spike

1092054003 Billable Matrix Spike Dup.

1092054001

Water (Surface, Eff., Ground)

VXX19405

Volatiles Extraction AFCEE 3.1 8260 (

05/20/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

1,1-Dichloropropene BMS ND 29.1 97 ( 80-122 ) 30.0 ug/L 05/20/2009

BMSD 28.5 95 2 (< 20 ) 30.0 ug/L 05/20/2009

1,1,2-Trichloroethane BMS ND 28.3 94 ( 77-120 ) 30.0 ug/L 05/20/2009

BMSD 28.7 96 1 (< 20 ) 30.0 ug/L 05/20/2009

1,3-Dichlorobenzene BMS ND 30 100 ( 80-120 ) 30.0 ug/L 05/20/2009

BMSD 31.3 104 4 (< 20 ) 30.0 ug/L 05/20/2009

1,2,3-Trichlorobenzene BMS ND 30.3 101 ( 77-120 ) 30.0 ug/L 05/20/2009

BMSD 31.9 106 5 (< 20 ) 30.0 ug/L 05/20/2009

Surrogates 

1,2-Dichloroethane-D4 <surr> BMS 28.3 94 ( 73-120 ) 05/20/2009

BMSD 28.0 93 1 05/20/2009

Toluene-d8 <surr> BMS 29 97 ( 80-120 ) 05/20/2009

BMSD 29.2 97 1 05/20/2009

4-Bromofluorobenzene <surr> BMS 29.7 99 ( 76-120 ) 05/20/2009

BMSD 29.8 99 0 05/20/2009

Batch

Method

Instrument

VMS10497

SW8260B

HP 5890 Series II MS3 VNA

Polynuclear Aromatics GC/MS

87 of 101
Matrix

SGS Ref.# Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Original

Prep

1092054002 Billable Matrix Spike

1092054003 Billable Matrix Spike Dup.

1092054001

Water (Surface, Eff., Ground)

XXX20829

3520 Liquid/Liquid Ext for 8270 SIM

05/19/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Polynuclear Aromatics GC/MS

Acenaphthylene BMS ND .375 73 ( 50-105 ) 0.510 ug/L 05/22/2009

BMSD 0.357 70 5 (< 30 ) 0.510 ug/L 05/22/2009

Acenaphthene BMS ND .374 73 ( 45-110 ) 0.510 ug/L 05/22/2009

BMSD 0.351 69 6 (< 30 ) 0.510 ug/L 05/22/2009

Fluorene BMS ND .385 76 ( 50-110 ) 0.510 ug/L 05/22/2009

BMSD 0.366 72 5 (< 30 ) 0.510 ug/L 05/22/2009

Phenanthrene BMS ND .393 77 ( 50-115 ) 0.510 ug/L 05/22/2009

BMSD 0.358 70 9 (< 30 ) 0.510 ug/L 05/22/2009

Anthracene BMS ND .387 76 ( 55-110 ) 0.510 ug/L 05/22/2009

BMSD 0.370 73 4 (< 30 ) 0.510 ug/L 05/22/2009

Fluoranthene BMS ND .473 93 ( 55-125 ) 0.510 ug/L 05/22/2009

BMSD 0.460 90 3 (< 30 ) 0.510 ug/L 05/22/2009

Pyrene BMS ND .454 89 ( 50-130 ) 0.510 ug/L 05/22/2009

BMSD 0.437 86 4 (< 30 ) 0.510 ug/L 05/22/2009

Benzo(a)Anthracene BMS ND .454 89 ( 55-120 ) 0.510 ug/L 05/22/2009

BMSD 0.456 89 0 (< 30 ) 0.510 ug/L 05/22/2009

Chrysene BMS ND .454 89 ( 55-120 ) 0.510 ug/L 05/22/2009

BMSD 0.448 88 2 (< 30 ) 0.510 ug/L 05/22/2009

Benzo[b]Fluoranthene BMS ND .441 87 ( 46-130 ) 0.510 ug/L 05/22/2009

BMSD 0.462 91 5 (< 30 ) 0.510 ug/L 05/22/2009

Benzo[k]fluoranthene BMS ND .447 88 ( 60-125 ) 0.510 ug/L 05/22/2009

BMSD 0.431 84 4 (< 30 ) 0.510 ug/L 05/22/2009

Benzo[a]pyrene BMS ND .443 87 ( 55-120 ) 0.510 ug/L 05/22/2009

BMSD 0.447 88 1 (< 30 ) 0.510 ug/L 05/22/2009

Indeno[1,2,3-c,d] pyrene BMS ND .45 88 ( 45-125 ) 0.510 ug/L 05/22/2009

BMSD 0.447 88 1 (< 30 ) 0.510 ug/L 05/22/2009

Dibenzo[a,h]anthracene BMS ND .458 90 ( 41-140 ) 0.510 ug/L 05/22/2009

BMSD 0.456 89 0 (< 30 ) 0.510 ug/L 05/22/2009

Benzo[g,h,i]perylene BMS ND .431 85 ( 46-125 ) 0.510 ug/L 05/22/2009

BMSD 0.435 85 1 (< 30 ) 0.510 ug/L 05/22/2009

Naphthalene BMS ND .35 69 ( 42-100 ) 0.510 ug/L 05/22/2009

BMSD 0.342 67 2 (< 30 ) 0.510 ug/L 05/22/2009

1-Methylnaphthalene BMS ND .374 73 ( 46-115 ) 0.510 ug/L 05/22/2009

BMSD 0.334 65 11 (< 30 ) 0.510 ug/L 05/22/2009

2-Methylnaphthalene BMS 0.0180 J .336 62 ( 45-105 ) 0.510 ug/L 05/22/2009

BMSD 0.328 61 2 (< 30 ) 0.510 ug/L 05/22/2009

Surrogates 

Terphenyl-d14 <surr> BMS .211 41* ( 50-135 ) 05/22/2009

BMSD 0.428 84 68 05/22/2009

88 of 101
Matrix

SGS Ref.# Printed Date/Time 06/08/2009 11:50

Batch

Method

Date

Original

Prep

1092054002 Billable Matrix Spike

1092054003 Billable Matrix Spike Dup.

1092054001

Water (Surface, Eff., Ground)

XXX20829

3520 Liquid/Liquid Ext for 8270 SIM

05/19/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Polynuclear Aromatics GC/MS

Batch

Method

Instrument

XMS4898

8270D SIMS

HP 6890/5973 MS SVOA

89 of 101
90 of 101
91 of 101
92 of 101
93 of 101
94 of 101
95 of 101
96 of 101
97 of 101
98 of 101
99 of 101
100 of 101
101 of 101