## Instructions **for completing the Fuel Material Analysis Information** 

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. **be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific**  **boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested.**  **Data for multiple boilers should be handled by using separate spreadsheets.** Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.
1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". **Instructions for completing the Fuel Material Analysis**  **Information**
This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. **be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific**  **boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested.**  **Data for multiple boilers should be handled by using separate spreadsheets.** Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.
1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

## Information
This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. **This spreadsheet is intended to be used for one boiler of one facility**  **but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th**  **is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested.**  Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- **Information**
This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. **This spreadsheet is intended to be used for one boiler of one facility**  **but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th**  **is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested.**  Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units of

### EIA

**Facility Code Facility Name**  **Boiler ID Fuel Type 1** 

7446811 Cleco Power, LLC EQT 38 

## petroleum coke

### Fuel Type 2 **Fuel Type 3 Other Fuel Description** 

### EIA

**Facility Code Facility Name**  **Boiler ID Basis**  **An alyte**  

## 7446811 Cleco Power, LLC EQT 38 As Received Higher Heating Value 

## 7446811 Cleco Power, LLC EQT 38 As Received % Moisture 

## 7446811 Cleco Power, LLC EQT 38 As Received % Ash 

## 7446811 Cleco Power, LLC EQT 38 As Received % Sulfur 

## 7446811 Cleco Power, LLC EQT 38 Dry basis Higher Heating Value 

## 7446811 Cleco Power, LLC EQT 38 Dry basis % Ash 

## 7446811 Cleco Power, LLC EQT 38 Dry basis % Sulfur 

## 7446811 Cleco Power, LLC EQT 38 Dry basis Antim ony 

## 7446811 Cleco Power, LLC EQT 38 Dry basis Arsenic 

## 7446811 Cleco Power, LLC EQT 38 Dry basis Bery llium 

## 7446811 Cleco Power, LLC EQT 38 Dry basis Cadmium 

## 7446811 Cleco Power, LLC EQT 38 Dry basis Chlorine 

## 7446811 Cleco Power, LLC EQT 38 Dry basis Chromium 

## 7446811 Cleco Power, LLC EQT 38 Dry basis Cobalt 

## 7446811 Cleco Power, LLC EQT 38 Dry basis Fluorine 

## 7446811 Cleco Power, LLC EQT 38 Dry basis Lead 

## 7446811 Cleco Power, LLC EQT 38 Dry basis Manganese 

## 7446811 Cleco Power, LLC EQT 38 Dry basis Mercury 

## 7446811 Cleco Power, LLC EQT 38 Dry basis Nickel 

## 7446811 Cleco Power, LLC EQT 38 Dry basis Selenium

### An **alysis M ethod for each A**  **nalyte**

**(example: A STM D5865-04)** 



## ASTM D 3302 ASTM D 4422 ASTM D 4239 ASTM D 5865 ASTM D 4422 ASTM D 4239 ASTM D 5600 ASTM D 3684/6357 ASTM D 3683 mod/ICP ASTM D 3683 mod/ICP ASRM D 6721 ASTM D 3683 mod/ICP ASTM D 3683 mod/ICP ASTM D 3761 mod. ASTM D 3683 mod/ICP ASTM D 3683 mod/ICP ASTM D 6722 ASTM D 3683 mod/ICP ASTM D 3684/6357**EIA**

**Facility Code**  **Facility**

**Name Boiler ID**  

### HA **Ps Test Group** 

## 7446811 Cleco Power, LLC EQT 38

**Sample Number (minimum of 3**  **composite samples)**  **Test Start Date**

**(MM/DD/YYYY) Test Stop Date** 

**(MM/DD/YYYY) Higher Heating Value**  **(HHV) (as received)**  **HHV Units** 

## 2/15/2011 2/15/2011 13314.00 Btu/lb **Fuel Testing Results % Moisture** 

**(as received)**  **% A**

**sh (as**  **received) % Sulfur** 

**(as received)**  **Higher**

**Heating Value (HHV)**  **(Dry Basis)**  **HHV Units % A**  **sh (Dry**  **Basis) % Sulfur** 

**(Dry Basis)**  

## 5.01 7.77 4.83 14017 Btu/lb 8.18 5.08**Chlorine**

**(Dry Basis)**  **Chlorine**

**Units Mercury** 

**(Dry Basis)**  **Mercury**

**Units An**  **timony**

**(Dry Basis)**  **An timony** 

**Units Ar** **senic (Dry**

**Basis) Ar** **senic**

**Units Bery**  **llium**

**(Dry Basis)**  

## 57 μg/g <0.02 μg/g <1 μg/g 1 μg/g <1**Bery llium** 

**Units Cadmium** 

**(Dry Basis)**  **Cadmium**

**Units Chromium** 

**(Dry Basis)**  **Chromium**

**Units Lead (Dry** 

**Basis) Lead Units**  **Manganese (Dry**  **Basis) Manganese** 

**Units** 

## μg/g <1 μg/g 18 μg/g <2 μg/g 4 μg/g**Nickel (Dry**

**Basis) Nickel Units**  **Selenium (Dry**  **Basis) Selenium** 

**Units Fluorine** 

**(Dry Basis)**  **Fluorine**

**Units Cobalt (Dry** 

**Basis) Cobalt Units**  **Total Moisture** 

## 281 μg/g <1 μg/g <20 μg/g 1 μg/g 5.01 **Proximate A naly** 

**ses, % by**

**wt**

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

**Volatiles As**  **h Fixed Carbon**  **Carbon Hy** **drogen Nitrogen**  **Total Sulfur**



## 8.18 5.08 3.4 1.6 5.08 **Proximate A naly** 

**ses, % by**

**wt Ultimate A**  **naly ses, % by** 

**wt Oxy** **gen**



## 0.64**EIA**

**Facility Code**  **Facility**

**Name Boiler ID**  

### HA **Ps Test Group** 

## 7446811 Cleco Power, LLC EQT 38

**Sample Number (minimum of 3**  **composite samples)**  **Test Start Date**

**(MM/DD/YYYY) Test Stop Date** 

**(MM/DD/YYYY) Higher Heating** 

**Value (HHV) (as received)**  **HHV Units** 

## 2/15/2011 2/15/2011 13602.00 Btu/lb **Fuel Testing Results % Moisture** 

**(as received)**  **% A**

**sh (as**  **received) % Sulfur** 

**(as received)**  **Higher**

**Heating Value (HHV)**  **(Dry Basis)**  **HHV Units % A**  **sh (Dry**  **Basis) % Sulfur** 

**(Dry Basis)**  

## 5.14 5.39 4.95 14339 Btu/lb 5.68 5.22**Chlorine**

**(Dry Basis)**  **Chlorine**

**Units Mercury** 

**(Dry Basis)**  **Mercury**

**Units An**  **timony**

**(Dry Basis)**  **An timony** 

**Units Ar** **senic (Dry**

**Basis) Ar** **senic**

**Units Bery**  **llium**

**(Dry Basis)**  

## 55 μg/g <0.02 μg/g <1 μg/g 1 μg/g <1**Bery llium** 

**Units Cadmium** 

**(Dry Basis)**  **Cadmium**

**Units Chromium** 

**(Dry Basis)**  **Chromium**

**Units Lead (Dry** 

**Basis) Lead Units**  **Manganese (Dry**  **Basis) Manganese** 

**Units** 

## μg/g <1 μg/g 14 μg/g <2 μg/g 3 μg/g**Nickel (Dry**

**Basis) Nickel Units**  **Selenium (Dry**  **Basis) Selenium** 

**Units Fluorine** 

**(Dry Basis)**  **Fluorine**

**Units Cobalt (Dry** 

**Basis) Cobalt Units**  

## 292 μg/g <1 μg/g <20 μg/g 2 μg/g

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

**Total Moisture Volatiles**  **As h**  **Fixed Carbon Carbon**  **Hy drogen**  **Nitrogen Total Sulfur** 



## 5.14 5.68 82.88 3.39 1.6 5.22 **Proximate A naly** 

**ses, % by**

**wt Ultimate A**  **naly ses, % by** 

**wt**

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

**Oxy gen**  

## 1.23**EIA**

**Facility Code**  **Facility**

**Name Boiler ID**  

### HA **Ps Test Group** 

## 7446811 Cleco Power, LLC EQT 38

**Sample Number (minimum of 3**  **composite samples)**  **Test Start Date**

**(MM/DD/YYYY) Test Stop Date**  **(MM/DD/YYYY) Higher**  **Heating Value (HHV)**  **(as received)**  **HHV Units** 

### Fuel Testing Results**% Moisture**

**(as received)**  **% A**

**sh (as**  **received) % Sulfur** 

**(as received)**  **Higher**

**Heating Value (HHV)**  **(Dry Basis)**  **HHV Units % A**  **sh (Dry**  **Basis) % Sulfur** 

**(Dry Basis)** **Chlorine**

**(Dry Basis)**  **Chlorine**

**Units Mercury** 

**(Dry Basis)**  **Mercury**

**Units An**  **timony**

**(Dry Basis)**  **An timony** 

**Units Ar** **senic (Dry**

**Basis) Ar** **senic**

**Units Bery**  **llium**

**(Dry Basis)** **Bery llium** 

**Units Cadmium** 

**(Dry Basis)**  **Cadmium**

**Units Chromium** 

**(Dry Basis)**  **Chromium**

**Units Lead (Dry** 

**Basis) Lead Units**  **Manganese (Dry**  **Basis) Manganese** 

**Units Nickel (Dry** 

**Basis) Nickel Units**  **Selenium (Dry**  **Basis) Selenium** 

**Units Fluorine** 

**(Dry Basis)**  **Fluorine**

**Units Cobalt (Dry** 

**Basis) Cobalt Units**  **Total Moisture Proximate A**  **naly**

**ses, % by**

**wt**

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

**Volatiles As**  **h Fixed Carbon**  **Carbon Hy** **drogen Nitrogen**  **Total Sulfur Oxy** **gen Proximate A**  **naly**

**ses, % by**

**wt Ultimate A**  **naly ses, % by** 

**wt EIA** 

**Facility Code**  **Facility**

**Name Boiler ID**  

### HA **Ps Test Group** 

## 7446811 Cleco Power, LLC EQT 38

**Sample Number (minimum of 3**  **composite samples)**  **Test Start Date**

**(MM/DD/YYYY) Test Stop Date** 

**(MM/DD/YYYY) Higher Heating**  **Value (HHV) (as received)**  **HHV Units** 

### Fuel Testing Results**% Moisture**

**(as received)**  **% A**

**sh (as**  **received) % Sulfur** 

**(as received)**  **Higher**

**Heating Value (HHV)**  **(Dry Basis)**  **HHV Units % A**  **sh (Dry**  **Basis) % Sulfur** 

**(Dry Basis)** **Chlorine**

**(Dry Basis)**  **Chlorine**

**Units Mercury** 

**(Dry Basis)**  **Mercury**

**Units An**  **timony**

**(Dry Basis)**  **An timony** 

**Units Ar** **senic (Dry**

**Basis) Ar** **senic**

**Units Bery**  **llium**

**(Dry Basis)** **Bery llium** 

**Units Cadmium** 

**(Dry Basis)**  **Cadmium**

**Units Chromium** 

**(Dry Basis)**  **Chromium**

**Units Lead (Dry** 

**Basis) Lead Units**  **Manganese (Dry**  **Basis) Manganese** 

**Units Nickel (Dry** 

**Basis) Nickel Units**  **Selenium (Dry**  **Basis) Selenium** 

**Units Fluorine** 

**(Dry Basis)**  **Fluorine**

**Units Cobalt (Dry** 

**Basis) Cobalt Units**  **Total Moisture Proximate A**  **naly ses, % by** 

**wt**

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

**Volatiles As**  **h Fixed Carbon**  **Carbon Hy** **drogen Nitrogen**  **Total Sulfur Oxy** **gen Proximate A**  **naly**

**ses, % by**

**wt Ultimate A**  **naly ses, % by** 

**wt**

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

**Fuel Units of Measure - HHV**  anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) **Units of Measure - Metals** sy nfuel mg /g petroleum coke μg/g other mg /Kg

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the **orange** hightlighted cell, if necessary

.

**Units of Measure - Cl, Fl** % ppm μg/g