## Instructionsfor completing the Fuel Material AnalysisInformation

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony,beryllium, cadmium, chromium,cobalt, lead, manganese, nickel, and selenium.This spreadsheet is intended to be used for one boiler of one facilitybut is designed to allow multiple (up to 4) fuel analyses at that specificboiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets.Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Pleasename each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls(example:8100_Unit_2_Fuels_Testing.xls).

Pleaserefer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Informationworksheet. 2. Please enter the test date on the Boiler Informationworksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet.If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet.For example:"ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet(orange tab). If the units

measurethat you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choosethe units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 compositesamples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of

measure.

## Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony,beryllium, cadmium, chromium,cobalt, lead, manganese, nickel, and selenium.This spreadsheet is intended to be used for one boiler of one facilitybut is designed to allow multiple (up to 4) fuel analyses at that specificboiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Informationworksheet.

down in the fuel column of the Boiler Information worksheet.If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet.For example:"ASTM D5865

-
5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet(orange tab). If the unitsof

measurethat you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choosethe units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 compositesamples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA Facility Code Facility Name Boiler ID Fuel Type 1 Fuel Type 2 Fuel Type 3 Other Fuel Description 3148 Martins Creek 4 No.6 Fuel Oil (residual or bunker C)

### EIA Facility Code Facility Name Boiler ID Basis Analyte Analysis Method for each Analyte (example: A

STM D5865-04)


## 3148Martins Creek 4As Received Heat of Combustion 

## ASTM D240 3148Martins Creek 4As Received Water by Distillation 

## ASTM D95 3148Martins Creek 4As Received Metals 

## EPA 3040A 6010B 3148Martins Creek 4As Received Anions 

## EPA 5050 9056 3148Martins Creek 4As Received Mercury 

## EPA 245.1 3148Martins Creek 4As Received Carbon, Hydrogen, Nitrogen 

## ASTM D5291 3148Martins Creek 4As Received Oxygen 

## ASTM D5291_MOD 3148Martins Creek 4As Received Sulfur 

## ASTM D4294EIA Facility Code Facility Name Boiler ID HAPs Test Group
3148 Martins Creek 4Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) % Ash

(as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Ash (Dry Basis) 2010-PHIL-002077-020 7/20/2010 7/20/2010 18291 Btu/lb n/a n/a 0.633 152327 Btu/gallon n/a 2010-PHIL-002077-024 7/21/2010 7/21/2010 18310 Btu/lb n/a n/a 0.631 152815 Btu/gallon n/a 2010-PHIL-002077-028 7/22/2010 7/22/2010 18168 Btu/lb n/a n/a 0.633 151303 Btu/gallon n/a Fuel Testing Results% Sulfur (Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) n/a 42.6 ppm < 0.2 μg/g 2.3 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 17.0 n/a 35.1 ppm < 0.2 μg/g 3.08 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 17.7 n/a 25.5 ppm < 0.2 μg/g 4.72 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 17.6Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Nickel Units Selenium

(Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen μg/g 1.84 μg/g < 17.4 ppm 0.853 μg/g μg/g < 1.16 μg/g < 17.4 ppm 1.01 μg/g μg/g < 1.16 μg/g < 17.4 ppm 0.618 μg/g Proximate Analyses, % by wt Ultimate Analyses, % by wtEIA Facility Code Facility Name Boiler ID HAPs Test Group
3148 Martins Creek 4Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) % Ash

(as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Ash (Dry Basis) 2010-PHIL-002077-020 7/20/2010 7/20/2010 18291 Btu/lb n/a n/a 0.633 152327 Btu/gallon n/a 2010-PHIL-002077-024 7/21/2010 7/21/2010 18310 Btu/lb n/a n/a 0.631 152815 Btu/gallon n/a 2010-PHIL-002077-028 7/22/2010 7/22/2010 18168 Btu/lb n/a n/a 0.633 151303 Btu/gallon n/a Fuel Testing Results% Sulfur (Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) n/a 42.6 ppm < 0.2 μg/g 2.3 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 17.0 n/a 35.1 ppm < 0.2 μg/g 3.08 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 17.7 n/a 25.5 ppm < 0.2 μg/g 4.72 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 17.6Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Nickel Units Selenium

(Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen μg/g 1.84 μg/g < 17.4 ppm 0.853 μg/g μg/g < 1.16 μg/g < 17.4 ppm 1.01 μg/g μg/g < 1.16 μg/g < 17.4 ppm 0.618 μg/g Proximate Analyses, % by wt Ultimate Analyses, % by wtEIA Facility Code Facility Name Boiler ID HAPs Test Group
3148 Martins Creek 4Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) % Ash

(as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Ash (Dry Basis) 2010-PHIL-002077-020 7/20/2010 7/20/2010 18291 Btu/lb n/a n/a 0.633 152327 Btu/gallon n/a 2010-PHIL-002077-024 7/21/2010 7/21/2010 18310 Btu/lb n/a n/a 0.631 152815 Btu/gallon n/a 2010-PHIL-002077-028 7/22/2010 7/22/2010 18168 Btu/lb n/a n/a 0.633 151303 Btu/gallon n/a Fuel Testing Results% Sulfur (Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) n/a 42.6 ppm < 0.2 μg/g 2.3 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 17.0 n/a 35.1 ppm < 0.2 μg/g 3.08 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 17.7 n/a 25.5 ppm < 0.2 μg/g 4.72 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 17.6Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Nickel Units Selenium

(Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen μg/g 1.84 μg/g < 17.4 ppm 0.853 μg/g μg/g < 1.16 μg/g < 17.4 ppm 1.01 μg/g μg/g < 1.16 μg/g < 17.4 ppm 0.618 μg/g Proximate Analyses, % by wt Ultimate Analyses, % by wtEIA Facility Code Facility Name Boiler ID HAPs Test Group
3148 Martins Creek 4Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) % Ash

(as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Ash (Dry Basis) 2010-PHIL-002077-020 7/20/2010 7/20/2010 18291 Btu/lb n/a n/a 0.633 152327 Btu/gallon n/a 2010-PHIL-002077-024 7/21/2010 7/21/2010 18310 Btu/lb n/a n/a 0.631 152815 Btu/gallon n/a 2010-PHIL-002077-028 7/22/2010 7/22/2010 18168 Btu/lb n/a n/a 0.633 151303 Btu/gallon n/a Fuel Testing Results% Sulfur (Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) n/a 42.6 ppm < 0.2 μg/g 2.3 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 17.0 n/a 35.1 ppm < 0.2 μg/g 3.08 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 17.7 n/a 25.5 ppm < 0.2 μg/g 4.72 μg/g < 1.12 μg/g < 0.485 μg/g < 0.372 μg/g < 0.280 μg/g < 1.66 μg/g < 0.624 μg/g 17.6Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Nickel Units Selenium

(Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen μg/g 1.84 μg/g < 17.4 ppm 0.853 μg/g μg/g < 1.16 μg/g < 17.4 ppm 1.01 μg/g μg/g < 1.16 μg/g < 17.4 ppm 0.618 μg/g Proximate Analyses, % by wt Ultimate Analyses, % by wt