### Instructionsfor filling the Emission Test Template

This Information Collection Request (ICR) spreadsheet is intended to collect information about emission data from fossil fuel burning power plants and which test methods were used to do so for cases where the test methods are not currently supported by the Electronic Reporting Tool (ERT). This spreadsheet should only be used if the method is not in the ERT or if you do not have access to a lab which performs methods that are in the ERT. Constituents of concern are: Carbon Monoxide,Formaldehyde, Methane, Speciated Volatile Hazardous Air Pollutants (HAPs), Speciated Semi HAPs, Sulfur Dioxide, Oxygen, Carbon Dioxide, Hydrogen Cyanide, Nitrogen Oxides, Total DissolvedSolids (TDS), and Total Suspended Solids (TSS). You must complete3 separate sampling events for each of the requested constituents. spreadsheet is intended to be used for one boiler of one facility.Data for multiple boilers should be handled by using separate copies of this spreadsheet.Fields shaded in yellow are required. All cells that are shaded in light green are populated using drop

-down lists. You do not need to populate cells shaded in gray, as they are automaticallypopulated fromthe Boiler Information worksheet.Please Do Not modify the structure of this spreadsheet by adding or subtracting

rows,columns, cells.Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_EmisTestMethods.xls(example:8100_Unit_2_EmisTestMethods.xls).

Pleaserefer to the following steps when using these spreadsheets.

Boiler InformationWorksheet

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Informationworksheet. 2. Please enter the control device configuration.

EmissionData Worksheets

The emission data worksheetsare provided for each constituent or constituent family required for this analysis. On each spreadsheet,you must enter boiler operating informationduring sampling, fuel input information, and emissiontest results. There are generally 1 to 3 emissiontest results records to be entered depending on the constituent or constituent family.For example, CO only requires 1 record with 3 sample events, while Mercury requires that you enter both Hg Hg+2

### , or if the Ontario

-Hydro Method was used, you would need to enter Hg0

### , HgP, and Hg VolatileOrganic HAP and Speciated Semi

-VolatileOrganic HAP worksheetsallow you to use a drop Constituentfield to define as many records as needed to record each HAP that you have results for. General instructions followfor these worksheets:

Boiler Operation Information

1. Please determine which units of measure (acfm or dscfm) were used for Exhaust Flow Rate and which units of measure (deg C or deg F) were used for Exhaust Temperature. Fill these units of measure into the Units of Measure field. 2. Please provide the values of all requested parametersfor each of the 3 sample testing periods in the Sample 1, Sample 2,and Sample 3 fields

. 3. Please provide any other supporting informationor commentsin the Other Supporting Informationfield.

Fuel Information

1. Pleaseenter what types of fuel are being used in your boiler using the drop

-downs in the Fuel Type Selection field. You may enter up to 4 fuel types. Then, enter the input rate of each fuel in the Sample 1, Sample 2, and Sample 3 fields. If you are not burning one or more of the fuel types entered in one or more samples, then enter an input rate of zero.

### If you are not burning one or more of the fuel types entered in one or more samples, then enter an input rate of zero. 2. Please enter the unit of measure using the drop down provided. 3. Please enter the test method used to determine the fuel input rate. 4. Please provide any other information that you feel may be important in the Other Supporting Information field.

EmissionData

1. Some constituents ask for the emission rate results of each of the 3 samples in two different units of measure, while othersdo not. If emission rate results are requested in two different units of measure (ex. lb/MMBtu (Pounds per million BTU) and ppmvd @ 7% O2

### (parts per million by volumedry basis at 7 percent oxygen)), you are required to provide both. 2. Please provide the test method used. This may or may not match the example given in the Test Method Used field. Pleaseensure that the name includes the owning organization of the test method(ex. U.S. EPA Method 0010). 3.Please provide any other information that you feel may be important in the Other Supporting Information field. 4. If data sheets and QA/QC documentationtables are provided for the test method you are entering data for please also enter these data.1 

### This Information Collection Request (ICR) spreadsheet is intended to collect information about emission data from fossil fuel burning power plants and which test methods were used to do so for cases where the test methods are not currently supported by the Electronic Reporting Tool (ERT). This spreadsheet should only be used if the method is not in the ERT or if you do not have access to a lab which performs methods that are in the ERT. Constituents of concern are: Carbon Monoxide,Formaldehyde, Methane, Speciated Volatile Hazardous Air Pollutants (HAPs), Speciated Semi

-VolatileOrganic HAPs, Sulfur Dioxide, Oxygen, Carbon Dioxide, Hydrogen Cyanide, Nitrogen Oxides, Total DissolvedSolids (TDS), and Total Suspended Solids (TSS). You must complete3 separate sampling events for each of the requested constituents.This spreadsheet is intended to be used for one boiler of one facility.Data for multiple boilers should be handled by using Fields shaded in yellow are required. All cells that are shaded in light green are down lists. You do not need to populate cells shaded in gray, as they are automaticallypopulated

Please Do Not modify the structure of this spreadsheet by adding or subtracting Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_EmisTestMethods.xls(example:8100_Unit_2_EmisTestMethods.xls).

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Informationworksheet.

The emission data worksheetsare provided for each constituent or constituent family required for this analysis. On each spreadsheet,you must enter boiler operating informationduring sampling, fuel input information, and emissiontest results. There are generally 1 to 3 emissiontest results records to be entered depending on the constituent or constituent family.For example, CO only requires 1 record with 3 sample events, while Mercury requires that you enter both Hg0

### and , HgP, and Hg+2

### . However,both the Speciated VolatileOrganic HAP worksheetsallow you to use a drop

-down provided in the Constituentfield to define as many records as needed to record each HAP that you have results for. General instructions

1. Please determine which units of measure (acfm or dscfm) were used for Exhaust Flow Rate and which units of measure (deg C or deg F) were used for Exhaust Temperature. Fill these units of measure into the Units of Measure field. 2. Please provide the values of all requested parametersfor each of the 3 sample testing periods in the Sample 1, Sample

3. Please provide any other supporting informationor commentsin the Other Supporting Informationfield.

downs in the Fuel Type Selection field. You may enter up to 4 fuel types. Then, enter the input rate of each fuel in the Sample 1, Sample 2, and Sample 3 fields. If you are not burning one or more of the fuel types entered in one or more samples, then enter an input rate of zero.

### If you are not burning one or more of the fuel types entered in one or more samples, then enter an input rate of zero.

4. Please provide any other information that you feel may be important in the Other Supporting Information field.

1. Some constituents ask for the emission rate results of each of the 3 samples in two different units of measure, while othersdo not. If emission rate results are requested in two different units of measure (ex. lb/MMBtu (Pounds per million (parts per million by volumedry basis at 7 percent oxygen)), you are required to provide both. 2. Please provide the test method used. This may or may not match the example given in the Test Method Used field. Pleaseensure that the name includes the owning organization of the test method(ex. U.S. EPA Method 0010). Please provide any other information that you feel may be important in the Other Supporting Information field. 4. If data sheets and QA/QC documentationtables are provided for the test method you are entering data for please alsoEIA

Facility Code Facility Name Boiler ID

1943Hoot Lake (ORIS 1943) 2Control Device Configuraton

Listed (by

boiler) in the Configuration Order Section of the Facility Unit Configurations Section of the Electronic ICRListed (by boiler) in the Configuration Order Section of the Facility Unit Configurations Section of the Electronic ICREIA

Facility Code Facility Name Boiler ID 1943Hoot Lake (ORIS 1943) 2

Parameter Sample 1 Sample 2 Sample 3 Date of Testing 5/27/2010 5/27/2010 5/27/2010 SteamOutput (1000 lb/hr) 0.4074 0.4069 0.4069 Total Heat Input (MMBtu/hr) 645.4 643.8 651.9 Basis (Wet/Dry) Wet Wet Wet Exhaust Steam % Moisture Exhaust Flow Rate (acfm or dscfm) 166,336.7 165,801.7 166,750.6 Exhaust Temperature (deg C or deg F) 363 371 371

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate

Sample 2 Fuel Input Rate

Sample 3 subbituminous 0.0292 0.0291 0.0292

Emission Test Results Methane Emission Rate Sample 1 (lb/MMBtu) Methane

Emission Rate Sample 1 (ppmvd @ 7% O2) Methane

Emission Rate Sample 2 (lb/MMBtu) 4.294E-05 0.070 4.233E-05

Instrument - Thermo 55C

Zero Gas (Nitrogen) = 0ppm Mid Level Cal. Gas (Propane) = 24.95ppm High Level Cal. Gas (Methane) = 42.02ppm

Date Time Zero Gas 5/26/2010 9:49 to 10:03 0.00 5/26/2010 10:52 to 11:56 0.06 5/26/2010 17:07 to 17:42 -0.18 5/26/2010 17:55 to 18:13 -0.18 5/26/2010 21:36 to 21:42 0.01 5/27/2010 7:48 to 7:52

– 5/27/2010 8:09 to 9:21 0.00 5/27/2010 8:24 to 8:54 0.07 5/27/2010 10:18 to 10:32 0.08 5/27/2010 11:47 to 11:59 0.08 Calibration Data*5/27/2010 13:28 to 13:37 0.07 5/27/2010 14:58 to 15:09 0.10 5/27/2010 16:20 to 16:28 0.08 5/27/2010 17:50 to 18:02

– *See ERT for Additional Calibration Data for Thermo 55C instrument (EPA Method 25A)Unit of Measure Other Supporting Information

1000 lb/hr From Plant DCS MMBtu/hr From CEMS N/A % Do Not Measure scfm From CEMS - Note EU Changed deg F From Plant DAHS

Unit of Measure Fuel Flow

Measurement Method Other Supporting

Information ktons/hr Other Note EU changed, fuel flow calculated off of feeder speed

Methane Emission Rate Sample 2 (ppmvd @ 7% O2) Methane

Emission Rate Sample 3 (lb/MMBtu) Methane

Emission Rate Sample 3 (ppmvd @ 7% O2) Test Method Used

(ex. U.S. EPA Method 18) 0.069 1.472E-05 0.024 U.S. EPA Method 18

Recovery Recovery Mid Level Gas % High Level % 25.30 101.40

– – 24.95 100.00 41.89 99.69 24.83 99.52 42.06 100.10 24.30 97.39 40.91 97.36 24.75 99.20 42.01 99.98 31.60 126.65 42.01 99.98 24.73 99.12 41.82 99.52 24.38 97.72 40.77 97.03 23.87 95.67 40.74 96.95 23.46 94.03 40.95 97.45 Calibration Data*24.85 99.60 41.58 98.95

24.76 99.24 42.09 100.17 24.83 99.52 42.03 100.02 24.91 99.84 42.30 100.67Note EU changed, fuel flow calculated off of feeder speed

Other Supporting Information

O2 = 6.9%, 124, 125, and 122 points/sample Fd = 9820 ft3/106@ 0% O2 CH4 Molecular Weight =16.04 Measured CH4 = 0.0706, 0.0694, and 0.0246 Sampling Data and Calibration logbook located in A-4 of Test Report AppendixDate/Time CH4, ppm Date/Time CH4, ppm Date/Time CH4, ppm

5/27/2010 9:13 0.20 5/27/2010 12:22 0.22 5/27/2010 15:18 0.00 5/27/2010 9:14 0.22 5/27/2010 12:23 0.20 5/27/2010 15:19 0.00 5/27/2010 9:15 0.22 5/27/2010 12:24 0.22 5/27/2010 15:20 0.00 5/27/2010 9:16 0.20 5/27/2010 12:25 0.22 5/27/2010 15:21 0.00 5/27/2010 9:17 0.20 5/27/2010 12:26 0.02 5/27/2010 15:22 0.02 5/27/2010 9:18 0.20 5/27/2010 12:27 0.02 5/27/2010 15:23 0.00 5/27/2010 9:19 0.20 5/27/2010 12:28 0.22 5/27/2010 15:24 0.00 5/27/2010 9:20 0.22 5/27/2010 12:29 0.20 5/27/2010 15:25 0.02

5/27/2010 9:21 0.20 5/27/2010 12:30 0.00 5/27/2010 15:26 0.20 5/27/2010 9:22 0.20 5/27/2010 12:31 0.02 5/27/2010 15:27 0.22 5/27/2010 9:23 0.22 5/27/2010 12:32 0.00 5/27/2010 15:28 0.02 5/27/2010 9:24 0.02 5/27/2010 12:33 0.02 5/27/2010 15:29 0.02 5/27/2010 9:25 0.02 5/27/2010 12:34 0.02 5/27/2010 15:30 0.00 5/27/2010 9:26 0.20 5/27/2010 12:35 0.02 5/27/2010 15:31 0.02

5/27/2010 9:27 0.22 5/27/2010 12:36 0.00 5/27/2010 15:32 0.00 5/27/2010 9:28 0.02 5/27/2010 12:37 0.00 5/27/2010 15:33 0.00 5/27/2010 9:29 0.00 5/27/2010 12:38 0.00 5/27/2010 15:34 0.22 5/27/2010 9:30 0.20 5/27/2010 12:39 0.00 5/27/2010 15:35 0.22 5/27/2010 9:31 0.22 5/27/2010 12:40 0.00 5/27/2010 15:36 0.20 5/27/2010 9:32 0.20 5/27/2010 12:41 0.00 5/27/2010 15:37 0.00 5/27/2010 9:33 0.22 5/27/2010 12:42 0.02 5/27/2010 15:38 0.02 5/27/2010 9:34 0.20 5/27/2010 12:43 0.02 5/27/2010 15:39 0.00 5/27/2010 9:35 0.02 5/27/2010 12:44 0.02 5/27/2010 15:40 0.00 5/27/2010 9:36 0.02 5/27/2010 12:45 0.00 5/27/2010 15:41 0.02 5/27/2010 9:37 0.22 5/27/2010 12:46 0.00 5/27/2010 15:42 0.02 5/27/2010 9:38 0.20 5/27/2010 12:47 0.02 5/27/2010 15:43 0.00 5/27/2010 9:39 -0.20 5/27/2010 12:48 0.00 5/27/2010 15:44 0.02 5/27/2010 9:40 -0.18 5/27/2010 12:49 0.02 5/27/2010 15:45 0.02 5/27/2010 9:41 0.00 5/27/2010 12:50 0.02 5/27/2010 15:46 0.02 5/27/2010 9:42 0.00 5/27/2010 12:51 0.00 5/27/2010 15:47 0.00 5/27/2010 9:43 0.22 5/27/2010 12:52 0.20 5/27/2010 15:48 0.00 5/27/2010 9:44 0.20 5/27/2010 12:53 0.20 5/27/2010 15:49 0.00 5/27/2010 9:45 0.22 5/27/2010 12:54 0.22 5/27/2010 15:50 0.02 5/27/2010 9:46 0.02 5/27/2010 12:55 0.22 5/27/2010 15:51 0.00 5/27/2010 9:47 0.00 5/27/2010 12:56 0.20 5/27/2010 15:52 0.02 5/27/2010 9:48 0.60 5/27/2010 12:57 0.20 5/27/2010 15:53 0.00 5/27/2010 9:49 0.62 5/27/2010 12:58 0.22 5/27/2010 15:54 0.02 5/27/2010 9:50 0.20 5/27/2010 12:59 0.00 5/27/2010 15:55 0.02 5/27/2010 9:51 0.22 5/27/2010 13:00 0.00 5/27/2010 15:56 0.00

Run #1 Run #2 Run #3 

## METHANE RUN RESULTS - EPA METHOD 185/27/2010 9:52 0.00 5/27/2010 13:01 0.02 5/27/2010 15:57 0.00

5/27/2010 9:53 0.00 5/27/2010 13:02 0.02 5/27/2010 15:58 0.00 5/27/2010 9:54 0.00 5/27/2010 13:03 0.00 5/27/2010 15:59 0.00 5/27/2010 9:55 0.00 5/27/2010 13:04 0.00 5/27/2010 16:00 0.02 5/27/2010 9:56 0.02 5/27/2010 13:05 0.02 5/27/2010 16:01 0.00 5/27/2010 9:57 0.00 5/27/2010 13:06 0.02 5/27/2010 16:02 0.02 5/27/2010 9:58 0.00 5/27/2010 13:07 0.00 5/27/2010 16:03 0.02 5/27/2010 9:59 0.20 5/27/2010 13:08 0.00 5/27/2010 16:04 0.00 5/27/2010 10:00 0.20 5/27/2010 13:09 0.00 5/27/2010 16:05 0.02 5/27/2010 10:01 0.02 5/27/2010 13:10 0.22 5/27/2010 16:06 0.02 5/27/2010 10:02 0.00 5/27/2010 13:11 0.22 5/27/2010 16:07 0.00 5/27/2010 10:03 0.02 5/27/2010 13:12 0.02 5/27/2010 16:08 0.00 5/27/2010 10:04 0.02 5/27/2010 13:13 0.00 5/27/2010 16:09 0.02 5/27/2010 10:05 0.00 5/27/2010 13:14 0.02 5/27/2010 16:10 0.00 5/27/2010 10:06 0.00 5/27/2010 13:15 0.02 5/27/2010 16:11 0.02 5/27/2010 10:07 0.00 5/27/2010 13:16 0.22 5/27/2010 16:12 0.00 5/27/2010 10:08 0.00 5/27/2010 13:17 0.20 5/27/2010 16:13 0.00 5/27/2010 10:09 0.00 5/27/2010 13:18 0.00 5/27/2010 16:14 0.00 5/27/2010 10:10 0.20 5/27/2010 13:19 0.00 5/27/2010 16:15 0.00 5/27/2010 10:11 0.20 5/27/2010 13:20 0.02 5/27/2010 16:16 0.22 5/27/2010 10:12 0.02 5/27/2010 13:21 0.22 5/27/2010 16:17 0.20 5/27/2010 10:13 0.00 5/27/2010 13:22 0.22 5/27/2010 16:18 0.02 5/27/2010 10:14 0.02 5/27/2010 13:23 0.00 5/27/2010 16:48 0.02 5/27/2010 10:15 0.00 5/27/2010 13:24 0.02 5/27/2010 16:49 0.00 5/27/2010 10:45 0.02 5/27/2010 13:25 0.00 5/27/2010 16:50 0.00 5/27/2010 10:46 0.00 5/27/2010 13:57 0.02 5/27/2010 16:51 0.02 5/27/2010 10:47 0.02 5/27/2010 13:58 0.00 5/27/2010 16:52 0.00 5/27/2010 10:48 0.00 5/27/2010 13:59 0.00 5/27/2010 16:53 0.00 5/27/2010 10:49 0.02 5/27/2010 14:00 0.20 5/27/2010 16:54 0.02 5/27/2010 10:50 0.02 5/27/2010 14:01 0.22 5/27/2010 16:55 0.00 5/27/2010 10:51 0.00 5/27/2010 14:02 0.20 5/27/2010 16:56 0.02 5/27/2010 10:52 0.00 5/27/2010 14:03 0.20 5/27/2010 16:57 0.02 5/27/2010 10:53 0.00 5/27/2010 14:04 0.00 5/27/2010 16:58 0.22 5/27/2010 10:54 0.00 5/27/2010 14:05 0.02 5/27/2010 16:59 0.22 5/27/2010 10:55 0.02 5/27/2010 14:06 0.00 5/27/2010 17:00 0.02 5/27/2010 10:56 0.02 5/27/2010 14:07 0.00 5/27/2010 17:01 0.00 5/27/2010 10:57 0.00 5/27/2010 14:08 0.02 5/27/2010 17:02 0.00 5/27/2010 10:58 0.00 5/27/2010 14:09 0.02 5/27/2010 17:03 0.02 5/27/2010 10:59 0.02 5/27/2010 14:10 0.00 5/27/2010 17:04 0.00 5/27/2010 11:00 0.20 5/27/2010 14:11 0.00 5/27/2010 17:05 0.02 5/27/2010 11:01 0.22 5/27/2010 14:12 0.02 5/27/2010 17:06 0.02 5/27/2010 11:02 0.00 5/27/2010 14:13 0.02 5/27/2010 17:07 0.02 5/27/2010 11:03 0.00 5/27/2010 14:14 0.02 5/27/2010 17:08 0.00 5/27/2010 11:04 0.02 5/27/2010 14:15 0.20 5/27/2010 17:09 0.02 5/27/2010 11:05 0.02 5/27/2010 14:16 0.20 5/27/2010 17:10 0.02 5/27/2010 11:06 0.00 5/27/2010 14:17 0.22 5/27/2010 17:11 0.00 5/27/2010 11:07 0.02 5/27/2010 14:18 0.02 5/27/2010 17:12 0.00 5/27/2010 11:08 0.02 5/27/2010 14:19 0.02 5/27/2010 17:13 0.00 5/27/2010 11:09 0.20 5/27/2010 14:20 0.20 5/27/2010 17:14 0.02 5/27/2010 11:10 0.22 5/27/2010 14:21 0.22 5/27/2010 17:15 0.00 5/27/2010 11:11 0.00 5/27/2010 14:22 0.00 5/27/2010 17:16 0.00 5/27/2010 11:12 0.02 5/27/2010 14:23 0.02 5/27/2010 17:17 0.02 5/27/2010 11:13 0.22 5/27/2010 14:24 0.00 5/27/2010 17:18 0.02 5/27/2010 11:14 0.20 5/27/2010 14:25 0.00 5/27/2010 17:19 0.02 5/27/2010 11:15 0.22 5/27/2010 14:26 0.00 5/27/2010 17:20 0.005/27/2010 11:16 0.02 5/27/2010 14:27 0.02 5/27/2010 17:21 0.00

5/27/2010 11:17 0.00 5/27/2010 14:28 0.02 5/27/2010 17:22 0.02 5/27/2010 11:18 0.02 5/27/2010 14:29 0.02 5/27/2010 17:23 0.02 5/27/2010 11:19 0.02 5/27/2010 14:30 0.02 5/27/2010 17:24 0.00 5/27/2010 11:20 0.02 5/27/2010 14:31 0.22 5/27/2010 17:25 0.00 5/27/2010 11:21 0.00 5/27/2010 14:32 0.22 5/27/2010 17:26 0.00 5/27/2010 11:22 0.02 5/27/2010 14:33 0.02 5/27/2010 17:27 0.02 5/27/2010 11:23 0.00 5/27/2010 14:34 0.02 5/27/2010 17:28 0.02 5/27/2010 11:24 -0.18 5/27/2010 14:35 0.00 5/27/2010 17:29 0.02 5/27/2010 11:25 -0.18 5/27/2010 14:36 0.02 5/27/2010 17:30 0.00 5/27/2010 11:26 0.02 5/27/2010 14:37 0.00 5/27/2010 17:31 0.02 5/27/2010 11:27 0.00 5/27/2010 14:38 0.00 5/27/2010 17:32 0.02 5/27/2010 11:28 0.02 5/27/2010 14:39 0.02 5/27/2010 17:33 0.00 5/27/2010 11:29 0.00 5/27/2010 14:40 0.02 5/27/2010 17:34 0.02 5/27/2010 11:30 0.00 5/27/2010 14:41 0.00 5/27/2010 17:35 0.00 5/27/2010 11:31 0.02 5/27/2010 14:42 0.02 5/27/2010 17:36 0.02 5/27/2010 11:32 0.02 5/27/2010 14:43 0.00 5/27/2010 17:37 0.00 5/27/2010 11:33 0.00 5/27/2010 14:44 0.22 5/27/2010 17:38 0.00 5/27/2010 11:34 0.00 5/27/2010 14:45 0.22 5/27/2010 17:39 0.02 5/27/2010 11:35 0.00 5/27/2010 14:46 0.22 5/27/2010 17:40 0.02 5/27/2010 11:36 0.00 5/27/2010 14:47 0.22 5/27/2010 17:41 0.00 5/27/2010 11:37 0.02 5/27/2010 14:48 0.20 5/27/2010 17:42 0.00 5/27/2010 11:38 0.00 5/27/2010 14:49 0.22 5/27/2010 17:43 0.02 5/27/2010 11:39 0.02 5/27/2010 14:50 0.20 5/27/2010 17:44 0.00 5/27/2010 11:40 0.00 5/27/2010 14:51 0.00 5/27/2010 17:45 0.00 5/27/2010 11:41 0.02 5/27/2010 14:52 0.00 5/27/2010 17:46 0.02 5/27/2010 11:42 0.02 5/27/2010 14:53 0.02 5/27/2010 17:47 0.02 5/27/2010 11:43 0.00 5/27/2010 14:54 0.00 5/27/2010 17:48 0.02 5/27/2010 11:44 0.02 5/27/2010 14:55 0.00 5/27/2010 11:45 0.02 5/27/2010 14:56 0.00 5/27/2010 14:57 0.00

Average 0.071 Average 0.069 Average 0.025 No Points in Avg 124 No Points in Avg 125 No Points in Avg 122 Min/Pt 1 Min/Pt 1 Min/Pt 1EIA

Facility Code Facility Name Boiler ID 1943Hoot Lake (ORIS 1943) 2

Parameter Sample 1 Sample 2 Date of Testing 5/20/2010 5/20/2010 SteamOutput (1000 lb/hr) 0.4063 0.4039 Total Heat Input (MMBtu/hr) 684.5 680.7 Basis (Wet/Dry) Wet Wet Exhaust Steam % Moisture Exhaust Flow Rate (acfm or dscfm) 168,946.5 170,638.2 Exhaust Temperature (deg C or deg F) 349 349

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2 subbituminous 0.0261 0.0262

Compound (use drop down to define for as many

rows as needed) Volatile Organic HAP Emission Rate Sample

1 (lb/MMBtu) Volatile Organic HAP

Emission Rate Sample

1 (ppmvd @ 7% O2) Acetone 2.203E-04 0.0975 Benzene 7.902E-06 0.0028 Bromodichloromethane 8.269E-06 0.0013 Bromoform 1.223E-05 0.0013 Bromomethane 1.387E-05 0.0038 Carbon disulfide 2.047E-05 0.0070 Carbon tetrachloride 1.242E-05 0.0021 Chlorobenzene 8.322E-06 0.0019 Chloroethane 8.573E-06 0.0035 Chloroform 8.269E-06 0.0018 Chloromethane 1.744E-05 0.0090 cis-1,3-Dichloropropene 8.269E-06 0.0019 Dibromomethane 8.322E-06 0.0012 Dichlorodifluoromethane 1.664E-05 0.0036 Ethylbenzene 1.228E-05 0.0030 Iodomethane 1.247E-05 0.0023 m-Xylene 1.242E-05 0.0031 2-Hexanone 2.681E-05 0.0070 2-Butanone (MEK) 3.355E-05 0.0121 Methylene chloride 1.664E-05 0.0051 o-Xylene 1.242E-05 0.0031 Styrene 8.322E-06 0.0021 Toluene 1.474E-05 0.0042 trans-1,3-Dichloropropene 4.372E-06 0.0010 Trichlorofluoromethane 9.114E-06 0.0017 Vinyl chloride 1.223E-05 0.0051 Speciated Volatile Organic HAP Emission Data1,1,1,2-Tetrachloroethane 8.322E-06 0.0013

1,1,2,2-Tetrachloroethane 1.308E-05 0.0020 1,1,1-Trichloroethane 1.228E-05 0.0024 1,1,2-Trichloroethane 1.242E-05 0.0024 1,1-Dichloroethane 8.269E-06 0.0022 1,2-Dichloroethane 4.319E-06 0.0011 1,2,3-Trichloropropane 1.247E-05 0.0022 1,3-Dichlorobenzene 1.638E-05 0.0029 1,4-Dichlorobenzene 1.638E-05 0.0029 1,2-Dichlorobenzene 1.638E-05 0.0029 1,2-Dichloropropane 8.322E-06 0.0019 Chlorodibromomethane 8.256E-06 0.0010 1,2-Dibromoethane 8.322E-06 0.0012 4-Methyl-2-pentanone (MIBK) 1.876E-05 0.0049 Tetrachloroethene 1.638E-05 0.0026 Trichloroethene 8.322E-06 0.0017 1,1-Dichloroethene 8.586E-06 0.0023 trans-1,2-Dichloroethene 8.586E-06 0.0023 cis-1,2 Dichloroethene 8.586E-06 0.0023

Grey are those results below detection limists (The detection limits for each analyte are provided in the attached spreadsheet for EPA Method 0031) Method Detection Limits are calculated by using the standard deviation from a minimum of 8 replicate low level spikes. Each analytes standard deviation is multiplied by the appropriate Student T value to determine the statistically derived reporting limit.Sample 3 Unit of Measure Other Supporting Information 5/21/2010 0.40271000 lb/hr From Plant DCS 695.4MMBtu/hr From CEMS Wet N/A

% Do Not Measure 171,809.7scfm From CEMS - Note EU Changed 341deg F From Plant DAHS

Fuel Input Rate Sample 3 Unit of Measure Fuel Flow Measurement Method Other Supporting

Information 0.0272ktons/hr Other Note EU changed, fuel flow calculated off of feeder speed

Volatile Organic HAP Emission Rate Sample 2 (lb/MMBtu) Volatile Organic

HAP Emission Rate Sample 2 (ppmvd @ 7% O2) Volatile Organic HAP Emission Rate Sample 3 (lb/MMBtu) Volatile Organic

HAP Emission Rate Sample 3 (ppmvd @ 7% O2) 1.728E-04 0.0774 1.743E-04 0.0781 1.352E-05 0.0048 1.691E-05 0.0060 1.553E-05 0.0025 2.036E-05 0.0032 2.064E-05 0.0021 2.540E-05 0.0026 2.324E-05 0.0064 3.301E-05 0.0091 3.218E-05 0.0110 3.805E-05 0.0130 2.196E-05 0.0037 2.797E-05 0.0047 1.558E-05 0.0036 2.041E-05 0.0047 1.456E-05 0.0059 1.814E-05 0.0073 1.553E-05 0.0034 2.036E-05 0.0044 3.933E-05 0.0203 5.393E-05 0.0279 1.425E-05 0.0033 3.553E-05 0.0084 1.430E-05 0.0021 1.814E-05 0.0027 2.860E-05 0.0062 2.036E-05 0.0044 2.069E-05 0.0051 1.784E-05 0.0044 2.201E-05 0.0040 1.784E-05 0.0033 2.196E-05 0.0054 1.789E-05 0.0044 5.108E-05 0.0133 2.066E-05 0.0054 5.746E-05 0.0208 3.579E-05 0.0129 2.860E-05 0.0088 2.545E-05 0.0078 2.196E-05 0.0054 1.789E-05 0.0044 1.558E-05 0.0039 2.802E-05 0.0070 2.078E-05 0.0059 2.802E-05 0.0079 9.245E-06 0.0022 2.797E-05 0.0066 1.507E-05 0.0029 6.804E-05 0.0129 2.064E-05 0.0086 7.308E-05 0.03051.430E-05 0.0022 3.553E-05 0.0055

2.145E-05 0.0033 3.780E-05 0.0059 2.069E-05 0.0040 3.553E-05 0.0069 2.196E-05 0.0043 3.579E-05 0.0070 1.553E-05 0.0041 1.285E-05 0.0034 9.194E-06 0.0024 2.797E-05 0.0074 2.201E-05 0.0039 2.041E-05 0.0036 2.835E-05 0.0050 3.301E-05 0.0059 2.835E-05 0.0050 1.814E-05 0.0032 2.835E-05 0.0050 2.545E-05 0.0045 1.558E-05 0.0036 1.290E-05 0.0030 1.425E-05 0.0018 2.041E-05 0.0026 1.430E-05 0.0020 2.041E-05 0.0028 3.065E-05 0.0080 2.540E-05 0.0066 2.707E-05 0.0043 2.621E-05 0.0041 1.558E-05 0.0031 1.865E-05 0.0037 1.583E-05 0.0043 2.797E-05 0.0075 1.456E-05 0.0039 1.789E-05 0.0048 1.456E-05 0.0039 2.545E-05 0.0068

Grey are those results below detection limists (The detection limits for each analyte are provided in the attached spreadsheet for EPA Method 0031) Method Detection Limits are calculated by using the standard deviation from a minimum of 8 replicate low level spikes. Each analytes standard deviation is multiplied by the appropriate Student T value to determine the statistically derived reporting limit.Note EU changed, fuel flow calculated off of feeder speed

Test Method Used U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260BU.S. EPA Method 0031 with SW-846 Method 8260B

U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260B U.S. EPA Method 0031 with SW-846 Method 8260BOther Supporting Information*

DLL, DLL, DLL (Method is not valid for Acetone) DLL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, DDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL DLL, DLL, DLL (Method is not valid for Chloromethane) BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL (Method is not valid for 2-Butanone) BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL DLL, DLL, BDL BDL, BDL, BDL DLL, BDL, BDL BDL, BDL, BDLBDL, BDL, BDL

BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL Sampling and Lab Data as well as QA/QC results are provided in A-10 of the Appendix of the test report. Calculations are provided in Tab M031 SVOC-Calculations of this spreadsheet5/20/10 m3/g-mole @ Fd Water Cond. 13:17 Volatile Organics Units MW 20 C ft3/10 Btu Sample Vol, l Trap 1 Acetone (2-Propanone) ug 58.08 0.02404 9820 0.04 0.1 Benzene ug 78.11 0.02404 9280 0.04 0.0 Bromodichloromethane ug 163.8 0.02404 9820 0.04 0.0 Bromoform ug 252.73 0.02404 9820 0.04 0.0 Bromomethane ug 94.94 0.02404 9820 0.04 0.0 Carbon Disulfide ug 76.139 0.02404 9820 0.04 0.0 Carbon Tetrachloride ug 153.82 0.02404 9820 0.04 0.0 Chlorobenzene ug 112.56 0.02404 9820 0.04 0.0 Chloroethane ug 64.51 0.02404 9820 0.04 0.0 Chloroform ug 119.38 0.02404 9820 0.04 0.0 Chloromethane ug 50.49 0.02404 9820 0.04 0.1 cis-1,3-Dichloropropene ug 110.97 0.02404 9820 0.04 0.0 Dibromomethane ug 173.83 0.02404 9820 0.04 0.0 Dichlorodifluoromethane (FREON 12) ug 120.91 0.02404 9820 0.04 0.0 Ethylbenzene ug 106.167 0.02404 9820 0.04 0.0 Iodomethane ug 141.94 0.02404 9820 0.04 0.0 m / p-Xylene ug 106.16 0.02404 9820 0.04 0.0 Methyl Butyl Ketone (2-Hexanone) ug 100.16 0.02404 9820 0.04 0.0 Methyl Ethyl Ketone (2-Butanone) ug 72.11 0.02404 9820 0.04 0.0 Methylene Chloride(Dichloromethane) ug 84.93 0.02404 9820 0.04 0.0 o-Xylene ug 106.16 0.02404 9820 0.04 0.0 Styrene ug 104.15 0.02404 9820 0.04 0.0 Toluene ug 92.14 0.02404 9820 0.04 0.1 trans-1,3-Dichloropropene ug 110.97 0.02404 9820 0.04 0.0 Trichlorofluoromethane (FREON 11) ug 137.37 0.02404 9820 0.04 0.0 Vinyl Chloride ug 62.498 0.02404 9820 0.04 0.0 1,1,1,2-Tetrachloroethane ug 167.85 0.02404 9820 0.04 0.0 1,1,2,2-Tetrachloroethane ug 167.85 0.02404 9820 0.04 0.0 1,1,1-Trichloroethane ug 133.4 0.02404 9820 0.04 0.0 1,1,2-Trichloroethane ug 133.4 0.02404 9820 0.04 0.0 1,1-Dichloroethane ug 98.96 0.02404 9820 0.04 0.0 1,2-Dichloroethane ug 98.96 0.02404 9820 0.04 0.0 1,2,3-Trichloropropane ug 147.43 0.02404 9820 0.04 0.0 1,3-Dichlorobenzene ug 147.01 0.02404 9820 0.04 0.0 1,4-Dichlorobenzene ug 147.0014 0.02404 9820 0.04 0.0 1,2-Dichlorobenzene ug 147.01 0.02404 9820 0.04 0.0 1,2-Dichloropropane ug 112.99 0.02404 9820 0.04 0.0 Dibromochloromethane (chlorodibromethane) ug 208.28 0.02404 9820 0.04 0.0 Ethylene Dibromide (1,2-Dibromoethane) ug 187.86 0.02404 9820 0.04 0.0 Methyl Isobutyl Ketone (MIBK) ug 100.2 0.02404 9820 0.04 0.0 Tetrachloroethylene (Tetrachloroethene) ug 165.8 0.02404 9820 0.04 0.0 Trichloroethylene (Trichloroethene) ug 131.39 0.02404 9820 0.04 0.0 1,1-Dichloroethylene (1,1-Dichloroethene) ug 96.94 0.02404 9820 0.04 0.0 trans-1,2-Dichloroethylene (trans-1,2 Dichlorethene) ug 96.95 0.02404 9820 0.04 0.0 cis-1,2-Dichloroethylene (cis-1,2 Dichlorethene) ug 96.95 0.02404 9820 0.04 0.0 

# EPA Method 0031 Calculations5/20/10 5/20/10 5/20/10 5/20/10

13:56 14:37 15:23 13:17 μg/dNm3 ppmvd ppmvd Trap 2 Trap 3 Trap 4 Condensor 1 2 3 4 O2 actual O2actual O2 7% O2 0.9 0.9 0.9 340 17.675 17.462 17.520 17.628 7.1 233.90 0.0968 0.0989 0.2 0.2 0.2 0.5 17.675 17.462 17.520 17.628 7.1 9.01 0.0028 0.0028 0.2 0.2 0.2 0.4 17.675 17.462 17.520 17.628 7.1 8.91 0.0013 0.0013 0.3 0.3 0.3 0.4 17.675 17.462 17.520 17.628 7.1 13.17 0.0013 0.0013 0.3 0.3 0.3 3.0 17.675 17.462 17.520 17.628 7.1 14.94 0.0038 0.0038 0.5 0.5 0.5 0.5 17.675 17.462 17.520 17.628 7.1 22.05 0.0070 0.0070 0.3 0.3 0.3 0.5 17.675 17.462 17.520 17.628 7.1 13.37 0.0021 0.0021 0.2 0.2 0.2 0.5 17.675 17.462 17.520 17.628 7.1 8.96 0.0019 0.0019 0.2 0.2 0.2 1.0 17.675 17.462 17.520 17.628 7.1 9.23 0.0034 0.0035 0.2 0.2 0.2 0.4 17.675 17.462 17.520 17.628 7.1 8.91 0.0018 0.0018 0.4 0.4 0.3 2.0 17.675 17.462 17.520 17.628 7.1 18.78 0.0089 0.0090 0.2 0.2 0.2 0.4 17.675 17.462 17.520 17.628 7.1 8.91 0.0019 0.0019 0.2 0.2 0.2 0.5 17.675 17.462 17.520 17.628 7.1 8.96 0.0012 0.0012 0.4 0.4 0.4 1.0 17.675 17.462 17.520 17.628 7.1 17.93 0.0036 0.0036 0.3 0.3 0.3 0.5 17.675 17.462 17.520 17.628 7.1 13.23 0.0030 0.0030 0.3 0.3 0.3 0.6 17.675 17.462 17.520 17.628 7.1 13.43 0.0023 0.0023 0.3 0.3 0.3 0.5 17.675 17.462 17.520 17.628 7.1 13.37 0.0030 0.0031 0.6 0.6 0.6 5.0 17.675 17.462 17.520 17.628 7.1 28.88 0.0069 0.0070 0.7 0.7 0.7 10.0 17.675 17.462 17.520 17.628 7.1 36.14 0.0120 0.0121 0.4 0.4 0.4 1.0 17.675 17.462 17.520 17.628 7.1 17.93 0.0051 0.0051 0.3 0.3 0.3 0.5 17.675 17.462 17.520 17.628 7.1 13.37 0.0030 0.0031 0.2 0.2 0.2 0.5 17.675 17.462 17.520 17.628 7.1 8.96 0.0021 0.0021 0.3 0.3 0.3 3.9 17.675 17.462 17.520 17.628 7.1 15.88 0.0041 0.0042 0.1 0.1 0.1 0.6 17.675 17.462 17.520 17.628 7.1 4.71 0.0010 0.0010 0.2 0.2 0.2 2.0 17.675 17.462 17.520 17.628 7.1 9.82 0.0017 0.0017 0.3 0.3 0.3 0.4 17.675 17.462 17.520 17.628 7.1 13.17 0.0051 0.0051 0.2 0.2 0.2 0.5 17.675 17.462 17.520 17.628 7.1 8.96 0.0013 0.0013 0.3 0.3 0.3 2.0 17.675 17.462 17.520 17.628 7.1 14.09 0.0020 0.0020 0.3 0.3 0.3 0.5 17.675 17.462 17.520 17.628 7.1 13.23 0.0024 0.0024 0.3 0.3 0.3 0.5 17.675 17.462 17.520 17.628 7.1 13.37 0.0024 0.0024 0.2 0.2 0.2 0.4 17.675 17.462 17.520 17.628 7.1 8.91 0.0022 0.0022 0.1 0.1 0.1 0.5 17.675 17.462 17.520 17.628 7.1 4.65 0.0011 0.0011 0.3 0.3 0.3 0.6 17.675 17.462 17.520 17.628 7.1 13.43 0.0022 0.0022 0.4 0.4 0.4 0.5 17.675 17.462 17.520 17.628 7.1 17.64 0.0029 0.0029 0.4 0.4 0.4 0.5 17.675 17.462 17.520 17.628 7.1 17.64 0.0029 0.0029 0.4 0.4 0.4 0.5 17.675 17.462 17.520 17.628 7.1 17.64 0.0029 0.0029 0.2 0.2 0.2 0.5 17.675 17.462 17.520 17.628 7.1 8.96 0.0019 0.0019 0.2 0.2 0.2 0.4 17.675 17.462 17.520 17.628 7.1 8.89 0.0010 0.0010 0.2 0.2 0.2 0.5 17.675 17.462 17.520 17.628 7.1 8.96 0.0011 0.0012 0.4 0.4 0.4 5.0 17.675 17.462 17.520 17.628 7.1 20.20 0.0048 0.0049 0.4 0.4 0.4 0.5 17.675 17.462 17.520 17.628 7.1 17.64 0.0026 0.0026 0.2 0.2 0.2 0.5 17.675 17.462 17.520 17.628 7.1 8.96 0.0016 0.0017 0.2 0.2 0.2 1.0 17.675 17.462 17.520 17.628 7.1 9.25 0.0023 0.0023 0.2 0.2 0.2 1.0 17.675 17.462 17.520 17.628 7.1 9.25 0.0023 0.0023 0.2 0.2 0.2 1.0 17.675 17.462 17.520 17.628 7.1 9.25 0.0023 0.0023 Flue Gas Sample Volume, l 

# RUN #1

Concentration5/20/10 5/20/10 5/20/10 5/20/10 5/20/10

ppmvd 16:55 17:39 18:21 19:04 16:55 0% O2 lb/MMBtu Flag Trap 1 Trap 2 Trap 3 Trap 4 Condensor 1 2 3 0.1488 2.203E-04 DLL 0.9 0.9 0.9 2.0 220 18.111 17.989 18.319 0.0042 7.902E-06 DLL 0.2 0.2 0.2 0.5 0.5 18.111 17.989 18.319 0.0020 8.269E-06 BDL 0.2 0.2 0.2 0.6 0.4 18.111 17.989 18.319 0.0019 1.223E-05 BDL 0.3 0.3 0.3 0.7 0.4 18.111 17.989 18.319 0.0057 1.387E-05 BDL 0.3 0.3 0.3 0.8 3.0 18.111 17.989 18.319 0.0105 2.047E-05 BDL 0.5 0.5 0.5 1.0 0.5 18.111 17.989 18.319 0.0032 1.242E-05 BDL 0.3 0.3 0.3 0.8 0.5 18.111 17.989 18.319 0.0029 8.322E-06 BDL 0.2 0.2 0.2 0.6 0.5 18.111 17.989 18.319 0.0052 8.573E-06 BDL 0.2 0.2 0.2 0.5 1.0 18.111 17.989 18.319 0.0027 8.269E-06 BDL 0.2 0.2 0.2 0.6 0.4 18.111 17.989 18.319 0.0135 1.744E-05 DLL 0.4 0.3 0.6 1.7 2.0 18.111 17.989 18.319 0.0029 8.269E-06 BDL 0.2 0.2 0.2 0.5 0.4 18.111 17.989 18.319 0.0019 8.322E-06 BDL 0.2 0.2 0.2 0.5 0.5 18.111 17.989 18.319 0.0054 1.664E-05 BDL 0.4 0.4 0.4 1.0 1.0 18.111 17.989 18.319 0.0045 1.228E-05 BDL 0.3 0.3 0.3 0.7 0.5 18.111 17.989 18.319 0.0034 1.247E-05 BDL 0.3 0.3 0.3 0.8 0.6 18.111 17.989 18.319 0.0046 1.242E-05 BDL 0.3 0.3 0.3 0.8 0.5 18.111 17.989 18.319 0.0105 2.681E-05 BDL 0.6 0.6 0.6 2.0 5.0 18.111 17.989 18.319 0.0182 3.355E-05 BDL 0.7 0.7 0.7 2.0 10.0 18.111 17.989 18.319 0.0077 1.664E-05 BDL 0.4 0.4 0.4 1.0 1.0 18.111 17.989 18.319 0.0046 1.242E-05 BDL 0.3 0.3 0.3 0.8 0.5 18.111 17.989 18.319 0.0031 8.322E-06 BDL 0.2 0.2 0.2 0.6 0.5 18.111 17.989 18.319 0.0063 1.474E-05 DLL 0.3 0.3 0.3 0.7 0.7 18.111 17.989 18.319 0.0015 4.372E-06 BDL 0.1 0.1 0.1 0.4 0.6 18.111 17.989 18.319 0.0026 9.114E-06 DLL 0.2 0.2 0.2 0.5 2.0 18.111 17.989 18.319 0.0077 1.223E-05 BDL 0.3 0.3 0.3 0.7 0.4 18.111 17.989 18.319 0.0019 8.322E-06 BDL 0.2 0.2 0.2 0.5 0.5 18.111 17.989 18.319 0.0031 1.308E-05 BDL 0.3 0.3 0.3 0.7 2.0 18.111 17.989 18.319 0.0036 1.228E-05 BDL 0.3 0.3 0.3 0.7 0.5 18.111 17.989 18.319 0.0036 1.242E-05 BDL 0.3 0.3 0.3 0.8 0.5 18.111 17.989 18.319 0.0033 8.269E-06 BDL 0.2 0.2 0.2 0.6 0.4 18.111 17.989 18.319 0.0017 4.319E-06 BDL 0.1 0.1 0.1 0.4 0.5 18.111 17.989 18.319 0.0033 1.247E-05 BDL 0.3 0.3 0.3 0.8 0.6 18.111 17.989 18.319 0.0044 1.638E-05 BDL 0.4 0.4 0.4 1.0 0.5 18.111 17.989 18.319 0.0044 1.638E-05 BDL 0.4 0.4 0.4 1.0 0.5 18.111 17.989 18.319 0.0044 1.638E-05 BDL 0.4 0.4 0.4 1.0 0.5 18.111 17.989 18.319 0.0029 8.322E-06 BDL 0.2 0.2 0.2 0.6 0.5 18.111 17.989 18.319 0.0016 8.256E-06 BDL 0.2 0.2 0.2 0.5 0.4 18.111 17.989 18.319 0.0017 8.322E-06 BDL 0.2 0.2 0.2 0.5 0.5 18.111 17.989 18.319 0.0073 1.876E-05 BDL 0.4 0.4 0.4 1.0 5.0 18.111 17.989 18.319 0.0039 1.638E-05 BDL 0.4 0.4 0.4 0.9 0.5 18.111 17.989 18.319 0.0025 8.322E-06 BDL 0.2 0.2 0.2 0.6 0.5 18.111 17.989 18.319 0.0035 8.586E-06 BDL 0.2 0.2 0.2 0.6 1.0 18.111 17.989 18.319 0.0035 8.586E-06 BDL 0.2 0.2 0.2 0.5 1.0 18.111 17.989 18.319 0.0035 8.586E-06 BDL 0.2 0.2 0.2 0.5 1.0 18.111 17.989 18.319 Flue Gas Sample Volume, l 

# RUN #2

Concentration5/21/10 5/21/10 5/21/10

O2 μg/dNm3 ppmvd ppmvdppmvd 9:00 9:41 10:21 4 % actual O2actual O2 7% O2 0% O2lb/MMBtu Flag Trap 1 Trap 2 Trap 3 18.2877.1 185.68 0.0769 0.0774 0.1167 1.728E-04 DLL 0.9 0.9 2.0 18.2877.1 15.40 0.0047 0.0048 0.0072 1.352E-05 BDL 0.2 0.2 0.5 18.2877.1 16.72 0.0025 0.0025 0.0037 1.553E-05 DLL 0.2 0.2 0.6 18.2877.1 22.23 0.0021 0.0021 0.0032 2.064E-05 BDL 0.3 0.3 0.7 18.2877.1 25.03 0.0063 0.0064 0.0096 2.324E-05 BDL 0.5 0.4 0.8 18.2877.1 34.66 0.0109 0.0110 0.0166 3.218E-05 BDL 0.5 0.5 1.0 18.2877.1 23.66 0.0037 0.0037 0.0056 2.196E-05 BDL 0.3 0.3 0.8 18.2877.1 16.78 0.0036 0.0036 0.0054 1.558E-05 BDL 0.2 0.2 0.6 18.2877.1 15.68 0.0058 0.0059 0.0088 1.456E-05 BDL 0.2 0.2 0.5 18.2877.1 16.72 0.0034 0.0034 0.0051 1.553E-05 BDL 0.2 0.2 0.6 18.2877.1 42.36 0.0202 0.0203 0.0305 3.933E-05 DLL 1.3 0.8 1.1 18.2877.1 15.35 0.0033 0.0033 0.0050 1.425E-05 BDL 0.4 0.4 1.0 18.2877.1 15.40 0.0021 0.0021 0.0032 1.430E-05 BDL 0.2 0.2 0.5 18.2877.1 30.81 0.0061 0.0062 0.0093 2.860E-05 BDL 0.2 0.2 0.6 18.2877.1 22.28 0.0050 0.0051 0.0076 2.069E-05 BDL 0.2 0.2 0.5 18.2877.1 23.71 0.0040 0.0040 0.0061 2.201E-05 BDL 0.2 0.2 0.5 18.2877.1 23.66 0.0054 0.0054 0.0081 2.196E-05 BDL 0.2 0.2 0.5 18.2877.1 55.02 0.0132 0.0133 0.0200 5.108E-05 BDL 0.2 0.2 0.6 18.2877.1 61.89 0.0206 0.0208 0.0312 5.746E-05 BDL 0.4 0.4 1.0 18.2877.1 30.81 0.0087 0.0088 0.0132 2.860E-05 BDL 0.3 0.3 0.7 18.2877.1 23.66 0.0054 0.0054 0.0081 2.196E-05 BDL 0.2 0.2 0.5 18.2877.1 16.78 0.0039 0.0039 0.0059 1.558E-05 BDL 0.3 0.3 0.8 18.2877.1 22.38 0.0058 0.0059 0.0088 2.078E-05 DLL 0.3 0.3 0.8 18.2877.1 9.96 0.0022 0.0022 0.0033 9.245E-06 BDL 0.3 0.3 0.8 18.2877.1 16.23 0.0028 0.0029 0.0043 1.507E-05 BDL 0.6 0.6 2.0 18.2877.1 22.23 0.0085 0.0086 0.0129 2.064E-05 BDL 0.7 0.7 2.0 18.2877.1 15.40 0.0022 0.0022 0.0033 1.430E-05 BDL 0.4 0.4 1.0 18.2877.1 23.11 0.0033 0.0033 0.0050 2.145E-05 BDL 0.4 0.4 1.0 18.2877.1 22.28 0.0040 0.0040 0.0061 2.069E-05 BDL 0.4 0.4 1.0 18.2877.1 23.66 0.0043 0.0043 0.0065 2.196E-05 BDL 0.4 0.4 1.0 18.2877.1 16.72 0.0041 0.0041 0.0062 1.553E-05 BDL 0.1 0.1 0.4 18.2877.1 9.90 0.0024 0.0024 0.0036 9.194E-06 BDL 0.3 0.3 0.8 18.2877.1 23.71 0.0039 0.0039 0.0059 2.201E-05 BDL 0.2 0.2 0.6 18.2877.1 30.53 0.0050 0.0050 0.0076 2.835E-05 BDL 0.4 0.4 0.9 18.2877.1 30.53 0.0050 0.0050 0.0076 2.835E-05 BDL 0.2 0.2 0.5 18.2877.1 30.53 0.0050 0.0050 0.0076 2.835E-05 BDL 0.3 0.3 0.7 18.2877.1 16.78 0.0036 0.0036 0.0054 1.558E-05 BDL 0.1 0.1 0.4 18.2877.1 15.35 0.0018 0.0018 0.0027 1.425E-05 BDL 0.2 0.2 0.6 18.2877.1 15.40 0.0020 0.0020 0.0030 1.430E-05 BDL 0.2 0.2 0.6 18.2877.1 33.01 0.0079 0.0080 0.0120 3.065E-05 BDL 0.3 0.3 0.7 18.2877.1 29.16 0.0042 0.0043 0.0064 2.707E-05 BDL 0.3 0.3 0.7 18.2877.1 16.78 0.0031 0.0031 0.0046 1.558E-05 BDL 0.2 0.2 0.5 18.2877.1 17.05 0.0042 0.0043 0.0064 1.583E-05 BDL 0.3 0.3 0.8 18.2877.1 15.68 0.0039 0.0039 0.0059 1.456E-05 BDL 0.2 0.2 0.5 18.2877.1 15.68 0.0039 0.0039 0.0059 1.456E-05 BDL 0.3 0.3 0.7 Flue Gas Sample Volume, l 

# RUN #2

Concentration5/21/10 5/21/10

11:02 9:00 μg/dNm3 ppmvd ppmvdppmvd Trap 4 Condensor 1 2 3 4 O2 actual O2actual O2 7% O2 0% O2lb/MMBtu 2.0 200 18.688 18.497 18.388 18.6417.2 185.95 0.0770 0.0781 0.1177 1.743E-04 0.5 0.5 18.688 18.497 18.388 18.6417.2 19.13 0.0059 0.0060 0.0090 1.691E-05 0.6 0.4 18.688 18.497 18.388 18.6417.2 21.77 0.0032 0.0032 0.0049 2.036E-05 0.7 0.4 18.688 18.497 18.388 18.6417.2 27.16 0.0026 0.0026 0.0039 2.540E-05 0.8 3.0 18.688 18.497 18.388 18.6417.2 35.30 0.0089 0.0091 0.0136 3.301E-05 1.0 0.5 18.688 18.497 18.388 18.6417.2 40.69 0.0128 0.0130 0.0196 3.805E-05 0.8 0.5 18.688 18.497 18.388 18.6417.2 29.91 0.0047 0.0047 0.0071 2.797E-05 0.6 0.5 18.688 18.497 18.388 18.6417.2 21.83 0.0047 0.0047 0.0071 2.041E-05 0.5 1.0 18.688 18.497 18.388 18.6417.2 19.40 0.0072 0.0073 0.0110 1.814E-05 0.6 0.4 18.688 18.497 18.388 18.6417.2 21.77 0.0044 0.0044 0.0067 2.036E-05 1.0 2.0 18.688 18.497 18.388 18.6417.2 57.67 0.0275 0.0279 0.0419 5.393E-05 1.0 0.5 18.688 18.497 18.388 18.6417.2 38.00 0.0082 0.0084 0.0126 3.553E-05 0.5 1.0 18.688 18.497 18.388 18.6417.2 19.40 0.0027 0.0027 0.0041 1.814E-05 0.6 0.4 18.688 18.497 18.388 18.6417.2 21.77 0.0043 0.0044 0.0066 2.036E-05 0.5 0.4 18.688 18.497 18.388 18.6417.2 19.08 0.0043 0.0044 0.0066 1.784E-05 0.5 0.4 18.688 18.497 18.388 18.6417.2 19.08 0.0032 0.0033 0.0049 1.784E-05 0.5 0.5 18.688 18.497 18.388 18.6417.2 19.13 0.0043 0.0044 0.0066 1.789E-05 0.6 1.0 18.688 18.497 18.388 18.6417.2 22.10 0.0053 0.0054 0.0081 2.066E-05 1.0 1.0 18.688 18.497 18.388 18.6417.2 38.27 0.0128 0.0129 0.0195 3.579E-05 0.7 0.5 18.688 18.497 18.388 18.6417.2 27.22 0.0077 0.0078 0.0118 2.545E-05 0.5 0.5 18.688 18.497 18.388 18.6417.2 19.13 0.0043 0.0044 0.0066 1.789E-05 0.8 0.6 18.688 18.497 18.388 18.6417.2 29.97 0.0069 0.0070 0.0106 2.802E-05 0.8 0.6 18.688 18.497 18.388 18.6417.2 29.97 0.0078 0.0079 0.0119 2.802E-05 0.8 0.5 18.688 18.497 18.388 18.6417.2 29.91 0.0065 0.0066 0.0099 2.797E-05 2.0 5.0 18.688 18.497 18.388 18.6417.2 72.76 0.0127 0.0129 0.0194 6.804E-05 2.0 10.0 18.688 18.497 18.388 18.6417.2 78.15 0.0301 0.0305 0.0459 7.308E-05 1.0 0.5 18.688 18.497 18.388 18.6417.2 38.00 0.0054 0.0055 0.0083 3.553E-05 1.0 5.0 18.688 18.497 18.388 18.6417.2 40.42 0.0058 0.0059 0.0088 3.780E-05 1.0 0.5 18.688 18.497 18.388 18.6417.2 38.00 0.0068 0.0069 0.0104 3.553E-05 1.0 1.0 18.688 18.497 18.388 18.6417.2 38.27 0.0069 0.0070 0.0105 3.579E-05 0.4 0.5 18.688 18.497 18.388 18.6417.2 13.74 0.0033 0.0034 0.0051 1.285E-05 0.8 0.5 18.688 18.497 18.388 18.6417.2 29.91 0.0073 0.0074 0.0111 2.797E-05 0.6 0.5 18.688 18.497 18.388 18.6417.2 21.83 0.0036 0.0036 0.0054 2.041E-05 0.9 0.5 18.688 18.497 18.388 18.6417.2 35.30 0.0058 0.0059 0.0088 3.301E-05 0.5 1.0 18.688 18.497 18.388 18.6417.2 19.40 0.0032 0.0032 0.0048 1.814E-05 0.7 0.5 18.688 18.497 18.388 18.6417.2 27.22 0.0045 0.0045 0.0068 2.545E-05 0.4 0.6 18.688 18.497 18.388 18.6417.2 13.80 0.0029 0.0030 0.0045 1.290E-05 0.6 0.5 18.688 18.497 18.388 18.6417.2 21.83 0.0025 0.0026 0.0038 2.041E-05 0.6 0.5 18.688 18.497 18.388 18.6417.2 21.83 0.0028 0.0028 0.0043 2.041E-05 0.7 0.4 18.688 18.497 18.388 18.6417.2 27.16 0.0065 0.0066 0.0099 2.540E-05 0.7 2.0 18.688 18.497 18.388 18.6417.2 28.03 0.0041 0.0041 0.0062 2.621E-05 0.5 2.0 18.688 18.497 18.388 18.6417.2 19.94 0.0036 0.0037 0.0056 1.865E-05 0.8 0.5 18.688 18.497 18.388 18.6417.2 29.91 0.0074 0.0075 0.0113 2.797E-05 0.5 0.5 18.688 18.497 18.388 18.6417.2 19.13 0.0047 0.0048 0.0072 1.789E-05 0.7 0.5 18.688 18.497 18.388 18.6417.2 27.22 0.0067 0.0068 0.0103 2.545E-05 Flue Gas Sample Volume, l 

# RUN #3

ConcentrationFlag Comments

DLL Method not valid for Acetone BDL BDL BDL DLL BDL BDL BDL BDL BDL DLL Method not valid for Chlormethane BDL BDL BDL BDL BDL BDL BDL BDL Method not valid for 2-Butonone BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDLEIA

Facility Code Facility Name Boiler ID 1943Hoot Lake (ORIS 1943) 2

Parameter Sample 1 Sample 2 Date of Testing 5/20/2010 5/21/2010 SteamOutput (1000 lb/hr) 0.4038 0.4023 Total Heat Input (MMBtu/hr) 675.2 692.1 Basis (Wet/Dry) Wet Wet Exhaust Steam % Moisture Exhaust Flow Rate (acfm or dscfm) 170,883.7 171,558.0 Exhaust Temperature (deg C or deg F) 350 350

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate Sample 2 subbituminous 0.0262 0.027

Compound (use drop down to define for as many rows as needed) Semi-Volatile Organic HAP Emission Rate Sample 1 (lb/MMBtu) Semi-Volatile Organic HAP Emission Rate Sample 1 (ppmvd @ 7% O2) Acenaphthene 5.955E-08 1.007E-05 Acenaphthylene 5.627E-08 1.020E-05 Aniline 7.940E-06 2.223E-03 Anthracene 5.955E-08 8.713E-06 Tetralin 1.191E-07 1.206E-05 Coronene 2.382E-07 3.235E-05 Benzo(e)pyrene 1.191E-07 1.405E-05 Perylene 2.382E-07 2.128E-05 Benzo(a)fluorene 2.382E-07 2.128E-05 Benzo(b)fluorene 1.191E-07 9.515E-06 Benzo(k)fluoranthene 5.955E-08 6.155E-06 Benzo(g,h,i)perylene 3.970E-07 3.747E-05 Benzo(a)pyrene 5.955E-08 6.155E-06 Benzyl alcohol 2.382E-06 5.744E-04 9,10-Dimethylanthracene 2.382E-07 2.136E-05 o-Terphenyl 1.191E-07 1.068E-05 Carbazole 7.940E-06 7.120E-04 Bis(2-chloroethoxy)methane 1.588E-06 2.393E-04 Bis(2-chloroethyl) ether 1.985E-06 3.620E-04 Bis(2-chloroisopropyl) ether 1.985E-06 3.026E-04 Bis(2-ethylhexyl) phthalate 3.176E-06 2.121E-04 4-Bromophenyl phenyl ether 7.940E-07 8.312E-05 1-Methylnaphthalene 1.191E-07 8.898E-06 Quinoline 2.382E-07 2.067E-05 m-Terphenyl 1.191E-07 1.544E-05 Biphenyl 1.191E-07 1.404E-05 p-Terphenyl 1.191E-07 9.059E-06 4-Chloroaniline 7.940E-06 1.623E-03 Speciated Semi Volatile Organic HAP Emission Data4-Chloro-3-methylphenol 1.985E-06 3.631E-04

1-Chloronaphthalene 2.382E-06 3.820E-04 2-Chloronaphthalene 1.191E-07 1.910E-05 2-Chlorophenol 3.176E-06 6.443E-04 4-Chlorophenyl phenyl ether 1.191E-06 1.518E-04 Chrysene 5.955E-08 6.803E-06 Dibenz(a,h)anthracene 5.955E-08 5.579E-06 Dibenzofuran 7.940E-06 1.231E-03 Dibenzo(a,e)pyrene 2.382E-07 2.054E-05 Di-n-butyl phthalate 1.191E-06 1.116E-04 1,2-Dichlorobenzene 2.382E-06 4.226E-04 1,3-Dichlorobenzene 2.382E-06 4.226E-04 1,4-Dichlorobenzene 2.382E-06 4.226E-04 3,3'-Dichlorobenzidine 3.176E-06 3.272E-04 2,4-Dichlorophenol 1.588E-06 2.541E-04 Diethyl phthalate 1.191E-06 1.398E-04 7,12-Dimethylbenzo(a)-anthracene 2.382E-07 2.423E-05 2,4-Dimethylphenol 2.382E-06 5.085E-04 Dimethyl phthalate 1.191E-06 1.600E-04 4,6-Dinitro-2-methylphenol 3.970E-06 5.225E-04 2,4-Dinitrophenol 3.970E-06 5.623E-04 2,4-Dinitrotoluene 7.940E-07 1.137E-04 2,6-Dinitrotoluene 1.191E-06 1.705E-04 Di-n-octyl phthalate 1.191E-06 7.953E-05 Fluoranthene 5.955E-08 7.678E-06 Fluorene 5.955E-08 9.343E-06 Hexachlorobenzene 2.382E-06 2.181E-04 Hexachlorobutadiene 2.382E-06 2.382E-04 Hexachlorocyclopentadiene 2.382E-06 2.277E-04 Hexachloroethane 2.382E-06 2.624E-04 Indeno(1,2,3-cd)pyrene 5.955E-08 5.620E-06 Isophorone 3.970E-06 7.491E-04 3-Methylcholanthrene 2.382E-07 2.315E-05 2-Methylnaphthalene 5.955E-08 1.092E-05 2-Methylphenol 3.573E-06 8.616E-04 3-Methylphenol 3.970E-06 9.574E-04 Naphthalene 1.393E-07 2.827E-05 2-Nitroaniline 7.940E-06 1.499E-03 3-Nitroaniline 7.940E-06 1.499E-03 4-Nitroaniline 7.940E-06 1.499E-03 Nitrobenzene 2.382E-06 5.046E-04 2-Nitrophenol 1.985E-06 3.721E-04 4-Nitrophenol 3.970E-06 7.442E-04 N-Nitrosodimethylamine 1.191E-05 4.193E-03 N-Nitrosodiphenylamine 2.382E-06 3.134E-04 N-Nitrosodi-n-propylamine 2.382E-06 4.771E-04 Pentachlorophenol 3.573E-06 3.498E-04 Phenanthrene 5.955E-08 8.713E-06 Phenol 1.985E-06 5.501E-04 Pyrene 5.955E-08 7.678E-06 1,2,4-Trichlorobenzene 2.382E-06 3.423E-04 2,4,5-Trichlorophenol 2.382E-06 3.146E-04 2,4,6-Trichlorophenol 1.985E-06 2.622E-04 Benzo(b)fluoranthene 5.955E-08 6.155E-06 2-Methylanthracene 1.191E-07 8.607E-06Benzidine 2.382E-05 3.372E-03

Benzoic acid 5.836E-05 1.246E-02 Benz(a)anthracene 5.955E-08 6.803E-06 1-Methylphenanthrene 1.191E-07 1.068E-05 Butyl benzyl phthalate 7.940E-07 6.629E-05Sample 3 Unit of Measure Other Supporting Information 5/26/2010 0.40941000 lb/hr From Plant DCS

686.5MMBtu/hr From CEMS Wet N/A % Do Not Measure 166,342.3scfm From CEMS - Note EU Changed 355deg F From Plant DAHS

Fuel Input Rate Sample 3 Unit of Measure Fuel Flow Measurement Method 0.285ktons/hr Other

Semi-Volatile Organic HAP Emission Rate Sample 2 (lb/MMBtu) Semi-Volatile Organic HAP Emission Rate Sample 2 (ppmvd @ 7% O2) Semi-Volatile Organic HAP Emission Rate Sample 3 (lb/MMBtu) 8.749E-07 1.480E-04 5.955E-08 8.268E-07 1.499E-04 5.627E-08 8.749E-06 2.450E-03 7.940E-06 4.375E-07 6.401E-05 5.955E-08 1.312E-07 1.329E-05 1.191E-07 2.625E-07 3.565E-05 2.382E-07 1.312E-07 1.549E-05 1.191E-07 2.625E-07 2.344E-05 2.382E-07 2.625E-07 2.344E-05 2.382E-07 1.312E-07 1.049E-05 1.191E-07 8.749E-07 9.043E-05 5.955E-08 4.375E-07 4.129E-05 3.970E-07 8.749E-07 9.043E-05 5.955E-08 2.625E-06 6.330E-04 2.382E-06 2.625E-07 2.354E-05 2.382E-07 1.312E-07 1.177E-05 1.191E-07 8.749E-06 7.846E-04 7.940E-06 1.750E-06 2.637E-04 1.588E-06 2.187E-06 3.989E-04 1.985E-06 2.187E-06 3.335E-04 1.985E-06 3.500E-06 2.337E-04 3.176E-06 8.749E-07 9.160E-05 7.940E-07 3.937E-06 2.942E-04 1.191E-07 2.625E-07 2.277E-05 2.382E-07 1.312E-07 1.701E-05 1.191E-07 2.625E-06 3.094E-04 1.191E-07 1.312E-07 9.983E-06 1.191E-07 8.749E-06 1.789E-03 7.940E-062.187E-06 4.001E-04 1.985E-06

2.625E-06 4.209E-04 2.382E-06 1.312E-06 2.105E-04 1.191E-07 3.500E-06 7.099E-04 3.176E-06 1.312E-06 1.672E-04 1.191E-06 4.375E-07 4.997E-05 5.955E-08 4.375E-07 4.099E-05 5.955E-08 8.749E-06 1.357E-03 7.940E-06 2.625E-07 2.264E-05 2.382E-07 1.312E-06 1.230E-04 1.191E-06 2.625E-06 4.657E-04 2.382E-06 2.625E-06 4.657E-04 2.382E-06 2.625E-06 4.657E-04 2.382E-06 3.500E-06 3.606E-04 3.176E-06 1.750E-06 2.800E-04 1.588E-06 1.312E-06 1.540E-04 1.191E-06 2.625E-07 2.670E-05 2.382E-07 2.625E-06 5.604E-04 2.382E-06 1.312E-06 1.763E-04 1.191E-06 4.375E-06 5.758E-04 3.970E-06 4.375E-06 6.197E-04 3.970E-06 8.749E-07 1.253E-04 7.940E-07 1.312E-06 1.879E-04 1.191E-06 1.312E-06 8.763E-05 1.191E-06 4.375E-07 5.641E-05 3.970E-07 4.375E-07 6.864E-05 5.955E-08 2.625E-06 2.404E-04 2.382E-06 2.625E-06 2.625E-04 2.382E-06 2.625E-06 2.510E-04 2.382E-06 2.625E-06 2.891E-04 2.382E-06 8.749E-07 8.257E-05 5.955E-08 4.375E-06 8.255E-04 3.970E-06 2.625E-07 2.551E-05 2.382E-07 2.187E-06 4.012E-04 5.955E-08 3.937E-06 9.495E-04 3.573E-06 4.375E-06 1.055E-03 3.970E-06 8.749E-07 1.780E-04 1.191E-07 8.749E-06 1.652E-03 7.940E-06 8.749E-06 1.652E-03 7.940E-06 8.749E-06 1.652E-03 7.940E-06 2.625E-06 5.560E-04 2.382E-06 2.187E-06 4.101E-04 1.985E-06 4.375E-06 8.201E-04 3.970E-06 1.312E-05 4.620E-03 1.191E-05 2.625E-06 3.453E-04 2.382E-06 2.625E-06 5.258E-04 2.382E-06 3.937E-06 3.855E-04 3.573E-06 4.375E-07 6.401E-05 5.955E-08 2.187E-06 6.061E-04 1.985E-06 8.749E-07 1.128E-04 7.940E-07 2.625E-06 3.773E-04 2.382E-06 2.625E-06 3.467E-04 2.382E-06 2.187E-06 2.889E-04 1.985E-06 4.375E-07 4.522E-05 5.955E-08 1.312E-07 9.484E-06 1.191E-072.625E-05 3.715E-03 2.382E-05

7.130E-05 1.523E-02 3.970E-06 4.375E-07 4.997E-05 5.955E-08 1.312E-07 1.177E-05 1.191E-07 8.749E-07 7.305E-05 7.940E-07From CEMS - Note EU Changed

Other Supporting Information Note EU changed, fuel flow calculated off of feeder speed

Semi-Volatile Organic HAP Emission Rate Sample 3 (ppmvd @ 7% O2) Test Method Used 1.007E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 1.020E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 2.223E-03 U.S. EPA Method 0010 with SW-846 Method 8270D 8.713E-06 U.S. EPA Method 0010 with SW-846 Method 8270D 1.206E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 3.235E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 1.405E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 2.128E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 2.128E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 9.515E-06 U.S. EPA Method 0010 with SW-846 Method 8270D 6.155E-06 U.S. EPA Method 0010 with SW-846 Method 8270D 3.747E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 6.155E-06 U.S. EPA Method 0010 with SW-846 Method 8270D 5.744E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 2.136E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 1.068E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 7.120E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 2.393E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 3.620E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 3.026E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 2.121E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 8.312E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 8.898E-06 U.S. EPA Method 0010 with SW-846 Method 8270D 2.067E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 1.544E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 1.404E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 9.059E-06 U.S. EPA Method 0010 with SW-846 Method 8270D 1.623E-03 U.S. EPA Method 0010 with SW-846 Method 8270D3.631E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 3.820E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 1.910E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 6.443E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 1.518E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 6.803E-06 U.S. EPA Method 0010 with SW-846 Method 8270D 5.579E-06 U.S. EPA Method 0010 with SW-846 Method 8270D 1.231E-03 U.S. EPA Method 0010 with SW-846 Method 8270D 2.054E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 1.116E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 4.226E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 4.226E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 4.226E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 3.272E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 2.541E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 1.398E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 2.423E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 5.085E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 1.600E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 5.225E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 5.623E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 1.137E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 1.705E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 7.953E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 5.119E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 9.343E-06 U.S. EPA Method 0010 with SW-846 Method 8270D 2.181E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 2.382E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 2.277E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 2.624E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 5.620E-06 U.S. EPA Method 0010 with SW-846 Method 8270D 7.491E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 2.315E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 1.092E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 8.616E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 9.574E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 2.423E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 1.499E-03 U.S. EPA Method 0010 with SW-846 Method 8270D 1.499E-03 U.S. EPA Method 0010 with SW-846 Method 8270D 1.499E-03 U.S. EPA Method 0010 with SW-846 Method 8270D 5.046E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 3.721E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 7.442E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 4.193E-03 U.S. EPA Method 0010 with SW-846 Method 8270D 3.134E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 4.771E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 3.498E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 8.713E-06 U.S. EPA Method 0010 with SW-846 Method 8270D 5.501E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 1.024E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 3.423E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 3.146E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 2.622E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 6.155E-06 U.S. EPA Method 0010 with SW-846 Method 8270D 8.607E-06 U.S. EPA Method 0010 with SW-846 Method 8270D3.372E-03 U.S. EPA Method 0010 with SW-846 Method 8270D

8.478E-04 U.S. EPA Method 0010 with SW-846 Method 8270D 6.803E-06 U.S. EPA Method 0010 with SW-846 Method 8270D 1.068E-05 U.S. EPA Method 0010 with SW-846 Method 8270D 6.629E-05 U.S. EPA Method 0010 with SW-846 Method 8270DOther Supporting Information

BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDLBDL, BDL, BDL

BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDl, BDL, Includes both 3 and 4 Methylphenol ADL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDLBDL, BDL, BDL

ADL, ADL, BDL. It was unexpected to see results ADL for Runs 1 and 2. Benzoic acid can be produced commercially by oxidation of toluene with an oxygen containing gas, so perhaps this interaction occurred here? BDL, BDL, BDL BDL, BDL, BDL BDL, BDL, BDL Sampling and Lab Data as well as QA/QC results are provided in A-9 of the Appendix of the test report. Calculations are provided in Tab M010 SSVOC-Calculations of this spreadsheet5/20/10 Sample m3/g-mole @ Fd 18:22 Vol. Semi Volatile Organics Units MW 20 C ft3/106Btu Trap dscf O2 Acenaphthene μg 154.21 0.02404 9820 0.15 83.19 7.1 Acenaphthylene μg 152.19 0.02404 9280 0.15 83.19 7.1 Aniline μg 93.13 0.02404 9820 20 83.19 7.1 Anthracene μg 178.23 0.02404 9820 0.15 83.19 7.1 Tetralin μg 257.54 0.02404 9820 0.3 83.19 7.1 Coronene μg 192.00 0.02404 9820 0.6 83.19 7.1 Benzo(e)pyrene μg 221.00 0.02404 9820 0.3 83.19 7.1 Perylene μg 291.98 0.02404 9820 0.6 83.19 7.1 Benzo(a)fluorene μg 291.98 0.02404 9820 0.6 83.19 7.1 Benzo(b)fluorene μg 326.43 0.02404 9820 0.3 83.19 7.1 Benzo(k)fluoranthene μg 252.31 0.02404 9820 0.15 83.19 7.1 Benzo(g,h,i)perylene μg 276.33 0.02404 9820 1 83.19 7.1 Benzo(a)pyrene μg 252.31 0.02404 9820 0.15 83.19 7.1 Benzyl alcohol μg 108.14 0.02404 9820 6 83.19 7.1 9,10-Dimethylanthracene μg 290.83 0.02404 9820 0.6 83.19 7.1 o-Terphenyl μg 290.83 0.02404 9820 0.3 83.19 7.1 Carbazole μg 290.83 0.02404 9820 20 83.19 7.1 Bis(2-chloroethoxy)methane μg 173.04 0.02404 9820 4 83.19 7.1 Bis(2-chloroethyl) ether μg 143.01 0.02404 9820 5 83.19 7.1 Bis(2-chloroisopropyl) ether μg 171.06 0.02404 9820 5 83.19 7.1 Bis(2-ethylhexyl) phthalate μg 390.56 0.02404 9820 8 83.19 7.1 4-Bromophenyl phenyl ether μg 249.10 0.02404 9820 2 83.19 7.1 1-Methylnaphthalene μg 349.06 0.02404 9820 0.3 83.19 7.1 Quinoline μg 300.59 0.02404 9820 0.6 83.19 7.1 m-Terphenyl μg 201.22 0.02404 9820 0.3 83.19 7.1 Biphenyl μg 221.25 0.02404 9820 0.3 83.19 7.1 p-Terphenyl μg 342.86 0.02404 9820 0.3 83.19 7.1 4-Chloroaniline μg 127.57 0.02404 9820 20 83.19 7.1 4-Chloro-3-methylphenol μg 142.58 0.02404 9820 5 83.19 7.1 1-Chloronaphthalene μg 162.62 0.02404 9820 6 83.19 7.1 2-Chloronaphthalene μg 162.62 0.02404 9820 0.3 83.19 7.1 2-Chlorophenol μg 128.56 0.02404 9820 8 83.19 7.1 4-Chlorophenyl phenyl ether μg 204.65 0.02404 9820 3 83.19 7.1 Chrysene μg 228.29 0.02404 9820 0.15 83.19 7.1 Dibenz(a,h)anthracene μg 278.35 0.02404 9820 0.15 83.19 7.1 Dibenzofuran μg 168.19 0.02404 9820 20 83.19 7.1 Dibenzo(a,e)pyrene μg 302.37 0.02404 9820 0.6 83.19 7.1 Di-n-butyl phthalate μg 278.34 0.02404 9820 3 83.19 7.1 1,2-Dichlorobenzene μg 147.00 0.02404 9820 6 83.19 7.1 1,3-Dichlorobenzene μg 147.00 0.02404 9820 6 83.19 7.1 1,4-Dichlorobenzene μg 147.00 0.02404 9820 6 83.19 7.1 3,3'-Dichlorobenzidine μg 253.13 0.02404 9820 8 83.19 7.1 2,4-Dichlorophenol μg 163.00 0.02404 9820 4 83.19 7.1 Diethyl phthalate μg 222.24 0.02404 9820 3 83.19 7.1 7,12-Dimethylbenz(a)-anthracene μg 256.34 0.02404 9820 0.6 83.19 7.1 2,4-Dimethylphenol μg 122.16 0.02404 9820 6 83.19 7.1 Dimethyl phthalate μg 194.18 0.02404 9820 3 83.19 7.1 4,6-Dinitro-2-methylphenol μg 198.13 0.02404 9820 10 83.19 7.1 2,4-Dinitrophenol μg 184.11 0.02404 9820 10 83.19 7.1 2,4-Dinitrotoluene μg 182.13 0.02404 9820 2 83.19 7.1 

# EPA Method 0010 Calculations2,6-Dinitrotoluene μg 182.13 0.02404 9820 3 83.19 7.1

Di-n-octyl phthalate μg 390.56 0.02404 9820 3 83.19 7.1 Fluoranthene μg 202.25 0.02404 9820 0.15 83.19 7.1 Fluorene μg 166.22 0.02404 9820 0.15 83.19 7.1 Hexachlorobenzene μg 284.78 0.02404 9820 6 83.19 7.1 Hexachlorobutadiene μg 260.76 0.02404 9820 6 83.19 7.1 Hexachlorocyclopentadiene μg 272.77 0.02404 9820 6 83.19 7.1 Hexachloroethane μg 236.74 0.02404 9820 6 83.19 7.1 Indeno(1,2,3-cd)pyrene μg 276.33 0.02404 9820 0.15 83.19 7.1 Isophorone μg 138.21 0.02404 9820 10 83.19 7.1 3-Methylcholanthrene μg 268.35 0.02404 9820 0.6 83.19 7.1 2-Methylnaphthalene μg 142.20 0.02404 9820 0.15 83.19 7.1 2-Methylphenol μg 108.14 0.02404 9820 9 83.19 7.1 3-Methylphenol μg 108.14 0.02404 9820 10 83.19 7.1 Naphthalene μg 128.17 0.02404 9820 0.35 83.19 7.1 2-Nitroaniline μg 138.12 0.02404 9820 20 83.19 7.1 3-Nitroaniline μg 138.12 0.02404 9820 20 83.19 7.1 4-Nitroaniline μg 138.12 0.02404 9820 20 83.19 7.1 Nitrobenzene μg 123.11 0.02404 9820 6 83.19 7.1 2-Nitrophenol μg 139.11 0.02404 9820 5 83.19 7.1 4-Nitrophenol μg 139.11 0.02404 9820 10 83.19 7.1 N-Nitrosodimethylamine μg 74.08 0.02404 9820 30 83.19 7.1 N-Nitrosodiphenylamine μg 198.22 0.02404 9820 6 83.19 7.1 N-Nitrosodi-n-propylamine μg 130.19 0.02404 9820 6 83.19 7.1 Pentachlorophenol μg 266.34 0.02404 9820 9 83.19 7.1 Phenanthrene μg 178.23 0.02404 9820 0.15 83.19 7.1 Phenol μg 94.11 0.02404 9820 5 83.19 7.1 Pyrene μg 202.25 0.02404 9820 0.15 83.19 7.1 1,2,4-Trichlorobenzene μg 181.45 0.02404 9820 6 83.19 7.1 2,4,5-Trichlorophenol μg 197.45 0.02404 9820 6 83.19 7.1 2,4,6-Trichlorophenol μg 197.45 0.02404 9820 5 83.19 7.1 Benzo(b)fluoranthene μg 252.31 0.02404 9820 0.15 83.19 7.1 2-Methylanthracene μg 360.87 0.02404 9820 0.3 83.19 7.1 Benzidine μg 184.24 0.02404 9820 60 83.19 7.1 Benzoic acid μg 122.12 0.02404 9820 147 83.19 7.1 Benzo(a)anthracene μg 228.29 0.02404 9820 0.15 83.19 7.1 1-Methylphenanthrene μg 290.83 0.02404 9820 0.3 83.19 7.1 Butyl benzyl phthalate μg 312.36 0.02404 9820 2 83.19 7.15/21/10 Sample

μg/dNm3 ppmvd ppmvd ppmvd 13:58 Vol. μg/dNm3 actual O2 actual O2 7% O2 0% O2 lb/MMBtu Flag Trap dscf O2 actual O2 0.0637 9.927E-06 1.007E-05 1.514E-05 5.95463E-08 BDL 2 77.17 7.4 0.9153 0.0637 1.006E-05 1.020E-05 1.534E-05 5.62719E-08 BDL 2 77.17 7.4 0.9153 8.4902 2.192E-03 2.223E-03 3.343E-03 7.93951E-06 BDL 20 77.17 7.4 9.1525 0.0637 8.589E-06 8.713E-06 1.310E-05 5.95463E-08 BDL 1 77.17 7.4 0.4576 0.1274 1.189E-05 1.206E-05 1.813E-05 1.19093E-07 BDL 0.3 77.17 7.4 0.1373 0.2547 3.189E-05 3.235E-05 4.865E-05 2.38185E-07 BDL 0.6 77.17 7.4 0.2746 0.1274 1.385E-05 1.405E-05 2.113E-05 1.19093E-07 BDL 0.3 77.17 7.4 0.1373 0.2547 2.097E-05 2.128E-05 3.199E-05 2.38185E-07 BDL 0.6 77.17 7.4 0.2746 0.2547 2.097E-05 2.128E-05 3.199E-05 2.38185E-07 BDL 0.6 77.17 7.4 0.2746 0.1274 9.379E-06 9.515E-06 1.431E-05 1.19093E-07 BDL 0.3 77.17 7.4 0.1373 0.0637 6.067E-06 6.155E-06 9.255E-06 5.95463E-08 BDL 2 77.17 7.4 0.9153 0.4245 3.693E-05 3.747E-05 5.633E-05 3.96975E-07 BDL 1 77.17 7.4 0.4576 0.0637 6.067E-06 6.155E-06 9.255E-06 5.95463E-08 BDL 2 77.17 7.4 0.9153 2.5471 5.662E-04 5.744E-04 8.637E-04 2.38185E-06 BDL 6 77.17 7.4 2.7458 0.2547 2.105E-05 2.136E-05 3.212E-05 2.38185E-07 BDL 0.6 77.17 7.4 0.2746 0.1274 1.053E-05 1.068E-05 1.606E-05 1.19093E-07 BDL 0.3 77.17 7.4 0.1373 8.4902 7.018E-04 7.120E-04 1.071E-03 7.93951E-06 BDL 20 77.17 7.4 9.1525 1.6980 2.359E-04 2.393E-04 3.598E-04 1.5879E-06 BDL 4 77.17 7.4 1.8305 2.1226 3.568E-04 3.620E-04 5.443E-04 1.98488E-06 BDL 5 77.17 7.4 2.2881 2.1226 2.983E-04 3.026E-04 4.550E-04 1.98488E-06 BDL 5 77.17 7.4 2.2881 3.3961 2.090E-04 2.121E-04 3.189E-04 3.1758E-06 BDL 8 77.17 7.4 3.6610 0.8490 8.194E-05 8.312E-05 1.250E-04 7.93951E-07 BDL 2 77.17 7.4 0.9153 0.1274 8.771E-06 8.898E-06 1.338E-05 1.19093E-07 BDL 9 77.17 7.4 4.1186 0.2547 2.037E-05 2.067E-05 3.107E-05 2.38185E-07 BDL 0.6 77.17 7.4 0.2746 0.1274 1.522E-05 1.544E-05 2.321E-05 1.19093E-07 BDL 0.3 77.17 7.4 0.1373 0.1274 1.384E-05 1.404E-05 2.111E-05 1.19093E-07 BDL 6 77.17 7.4 2.7458 0.1274 8.929E-06 9.059E-06 1.362E-05 1.19093E-07 BDL 0.3 77.17 7.4 0.1373 8.4902 1.600E-03 1.623E-03 2.441E-03 7.93951E-06 BDL 20 77.17 7.4 9.1525 2.1226 3.579E-04 3.631E-04 5.459E-04 1.98488E-06 BDL 5 77.17 7.4 2.2881 2.5471 3.765E-04 3.820E-04 5.744E-04 2.38185E-06 BDL 6 77.17 7.4 2.7458 0.1274 1.883E-05 1.910E-05 2.872E-05 1.19093E-07 BDL 3 77.17 7.4 1.3729 3.3961 6.350E-04 6.443E-04 9.687E-04 3.1758E-06 BDL 8 77.17 7.4 3.6610 1.2735 1.496E-04 1.518E-04 2.282E-04 1.19093E-06 BDL 3 77.17 7.4 1.3729 0.0637 6.705E-06 6.803E-06 1.023E-05 5.95463E-08 BDL 1 77.17 7.4 0.4576 0.0637 5.499E-06 5.579E-06 8.389E-06 5.95463E-08 BDL 1 77.17 7.4 0.4576 8.4902 1.214E-03 1.231E-03 1.851E-03 7.93951E-06 BDL 20 77.17 7.4 9.1525 0.2547 2.025E-05 2.054E-05 3.089E-05 2.38185E-07 BDL 0.6 77.17 7.4 0.2746 1.2735 1.100E-04 1.116E-04 1.678E-04 1.19093E-06 BDL 3 77.17 7.4 1.3729 2.5471 4.165E-04 4.226E-04 6.354E-04 2.38185E-06 BDL 6 77.17 7.4 2.7458 2.5471 4.165E-04 4.226E-04 6.354E-04 2.38185E-06 BDL 6 77.17 7.4 2.7458 2.5471 4.165E-04 4.226E-04 6.354E-04 2.38185E-06 BDL 6 77.17 7.4 2.7458 3.3961 3.225E-04 3.272E-04 4.920E-04 3.1758E-06 BDL 8 77.17 7.4 3.6610 1.6980 2.504E-04 2.541E-04 3.820E-04 1.5879E-06 BDL 4 77.17 7.4 1.8305 1.2735 1.378E-04 1.398E-04 2.101E-04 1.19093E-06 BDL 3 77.17 7.4 1.3729 0.2547 2.389E-05 2.423E-05 3.644E-05 2.38185E-07 BDL 0.6 77.17 7.4 0.2746 2.5471 5.012E-04 5.085E-04 7.646E-04 2.38185E-06 BDL 6 77.17 7.4 2.7458 1.2735 1.577E-04 1.600E-04 2.405E-04 1.19093E-06 BDL 3 77.17 7.4 1.3729 4.2451 5.151E-04 5.225E-04 7.857E-04 3.96975E-06 BDL 10 77.17 7.4 4.5763 4.2451 5.543E-04 5.623E-04 8.455E-04 3.96975E-06 BDL 10 77.17 7.4 4.5763 0.8490 1.121E-04 1.137E-04 1.709E-04 7.93951E-07 BDL 2 77.17 7.4 0.9153

Concentration 

## Run #11.2735 1.681E-04 1.705E-04 2.564E-04 1.19093E-06 BDL 3 77.17 7.4 1.3729

1.2735 7.839E-05 7.953E-05 1.196E-04 1.19093E-06 BDL 3 77.17 7.4 1.3729 0.0637 7.569E-06 7.678E-06 1.155E-05 5.95463E-08 BDL 1 77.17 7.4 0.4576 0.0637 9.209E-06 9.343E-06 1.405E-05 5.95463E-08 BDL 1 77.17 7.4 0.4576 2.5471 2.150E-04 2.181E-04 3.280E-04 2.38185E-06 BDL 6 77.17 7.4 2.7458 2.5471 2.348E-04 2.382E-04 3.582E-04 2.38185E-06 BDL 6 77.17 7.4 2.7458 2.5471 2.245E-04 2.277E-04 3.424E-04 2.38185E-06 BDL 6 77.17 7.4 2.7458 2.5471 2.586E-04 2.624E-04 3.945E-04 2.38185E-06 BDL 6 77.17 7.4 2.7458 0.0637 5.540E-06 5.620E-06 8.450E-06 5.95463E-08 BDL 2 77.17 7.4 0.9153 4.2451 7.384E-04 7.491E-04 1.126E-03 3.96975E-06 BDL 10 77.17 7.4 4.5763 0.2547 2.282E-05 2.315E-05 3.481E-05 2.38185E-07 BDL 0.6 77.17 7.4 0.2746 0.0637 1.077E-05 1.092E-05 1.642E-05 5.95463E-08 BDL 5 77.17 7.4 2.2881 3.8206 8.493E-04 8.616E-04 1.296E-03 3.57278E-06 BDL 9 77.17 7.4 4.1186 4.2451 9.437E-04 9.574E-04 1.440E-03 3.96975E-06 BDL 10 77.17 7.4 4.5763 0.1486 2.787E-05 2.827E-05 4.261E-05 1.393E-07 ADL 2 77.17 7.4 0.9153 8.4902 1.478E-03 1.499E-03 2.254E-03 7.93951E-06 BDL 20 77.17 7.4 9.1525 8.4902 1.478E-03 1.499E-03 2.254E-03 7.93951E-06 BDL 20 77.17 7.4 9.1525 8.4902 1.478E-03 1.499E-03 2.254E-03 7.93951E-06 BDL 20 77.17 7.4 9.1525 2.5471 4.974E-04 5.046E-04 7.587E-04 2.38185E-06 BDL 6 77.17 7.4 2.7458 2.1226 3.668E-04 3.721E-04 5.595E-04 1.98488E-06 BDL 5 77.17 7.4 2.2881 4.2451 7.336E-04 7.442E-04 1.119E-03 3.96975E-06 BDL 10 77.17 7.4 4.5763 12.7353 4.133E-03 4.193E-03 6.304E-03 1.19093E-05 BDL 30 77.17 7.4 13.7288 2.5471 3.089E-04 3.134E-04 4.712E-04 2.38185E-06 BDL 6 77.17 7.4 2.7458 2.5471 4.703E-04 4.771E-04 7.174E-04 2.38185E-06 BDL 6 77.17 7.4 2.7458 3.8206 3.448E-04 3.498E-04 5.260E-04 3.57278E-06 BDL 9 77.17 7.4 4.1186 0.0637 8.589E-06 8.713E-06 1.310E-05 5.95463E-08 BDL 1 77.17 7.4 0.4576 2.1226 5.422E-04 5.501E-04 8.271E-04 1.98488E-06 BDL 5 77.17 7.4 2.2881 0.0637 7.569E-06 7.678E-06 1.155E-05 5.95463E-08 BDL 2 77.17 7.4 0.9153 2.5471 3.375E-04 3.423E-04 5.148E-04 2.38185E-06 BDL 6 77.17 7.4 2.7458 2.5471 3.101E-04 3.146E-04 4.730E-04 2.38185E-06 BDL 6 77.17 7.4 2.7458 2.1226 2.584E-04 2.622E-04 3.942E-04 1.98488E-06 BDL 5 77.17 7.4 2.2881 0.0637 6.067E-06 6.155E-06 9.255E-06 5.95463E-08 BDL 1 77.17 7.4 0.4576 0.1274 8.484E-06 8.607E-06 1.294E-05 1.19093E-07 BDL 0.3 77.17 7.4 0.1373 25.4706 3.323E-03 3.372E-03 5.070E-03 2.38185E-05 BDL 60 77.17 7.4 27.4576 62.4030 1.228E-02 1.246E-02 1.874E-02 5.836E-05 ADL 163 77.17 7.4 74.5930 0.0637 6.705E-06 6.803E-06 1.023E-05 5.95463E-08 BDL 1 77.17 7.4 0.4576 0.1274 1.053E-05 1.068E-05 1.606E-05 1.19093E-07 BDL 0.3 77.17 7.4 0.1373 0.8490 6.534E-05 6.629E-05 9.967E-05 7.93951E-07 BDL 2 77.17 7.4 0.91535/26/10 Sample

ppmvd ppmvd ppmvd 15:36 Vol. μg/dNm3 ppmvd ppmvd actual O2 7% O2 0% O2 lb/MMBtu Flag Trap dscf O2 actual O2 actual O2 7% O2 1.427E-04 1.480E-04 2.225E-04 8.749E-07 BDL 0.15 83.19 7.1 0.06 9.92662E-06 1.007E-05 1.446E-04 1.499E-04 2.254E-04 8.268E-07 BDL 0.15 83.19 7.1 0.06 1.00584E-05 1.020E-05 2.363E-03 2.450E-03 3.684E-03 8.749E-06 BDL 20 83.19 7.1 8.49 0.002191608 2.223E-03 6.173E-05 6.401E-05 9.625E-05 4.375E-07 BDL 0.15 83.19 7.1 0.06 8.58881E-06 8.713E-06 1.282E-05 1.329E-05 1.998E-05 1.312E-07 BDL 0.3 83.19 7.1 0.13 1.18877E-05 1.206E-05 3.438E-05 3.565E-05 5.361E-05 2.625E-07 BDL 0.6 83.19 7.1 0.25 3.18913E-05 3.235E-05 1.493E-05 1.549E-05 2.329E-05 1.312E-07 BDL 0.3 83.19 7.1 0.13 1.38532E-05 1.405E-05 2.261E-05 2.344E-05 3.525E-05 2.625E-07 BDL 0.6 83.19 7.1 0.25 2.09711E-05 2.128E-05 2.261E-05 2.344E-05 3.525E-05 2.625E-07 BDL 0.6 83.19 7.1 0.25 2.09711E-05 2.128E-05 1.011E-05 1.049E-05 1.577E-05 1.312E-07 BDL 0.3 83.19 7.1 0.13 9.37894E-06 9.515E-06 8.720E-05 9.043E-05 1.360E-04 8.749E-07 BDL 0.15 83.19 7.1 0.06 6.06707E-06 6.155E-06 3.981E-05 4.129E-05 6.208E-05 4.375E-07 BDL 1 83.19 7.1 0.42 3.69313E-05 3.747E-05 8.720E-05 9.043E-05 1.360E-04 8.749E-07 BDL 0.15 83.19 7.1 0.06 6.06707E-06 6.155E-06 6.104E-04 6.330E-04 9.518E-04 2.625E-06 BDL 6 83.19 7.1 2.55 0.000566223 5.744E-04 2.270E-05 2.354E-05 3.539E-05 2.625E-07 BDL 0.6 83.19 7.1 0.25 2.1054E-05 2.136E-05 1.135E-05 1.177E-05 1.770E-05 1.312E-07 BDL 0.3 83.19 7.1 0.13 1.0527E-05 1.068E-05 7.565E-04 7.846E-04 1.180E-03 8.749E-06 BDL 20 83.19 7.1 8.49 0.0007018 7.120E-04 2.543E-04 2.637E-04 3.965E-04 1.75E-06 BDL 4 83.19 7.1 1.70 0.000235904 2.393E-04 3.846E-04 3.989E-04 5.998E-04 2.187E-06 BDL 5 83.19 7.1 2.12 0.000356801 3.620E-04 3.216E-04 3.335E-04 5.014E-04 2.187E-06 BDL 5 83.19 7.1 2.12 0.000298294 3.026E-04 2.253E-04 2.337E-04 3.514E-04 3.5E-06 BDL 8 83.19 7.1 3.40 0.000209038 2.121E-04 8.833E-05 9.160E-05 1.377E-04 8.749E-07 BDL 2 83.19 7.1 0.85 8.19368E-05 8.312E-05 2.837E-04 2.942E-04 4.423E-04 3.937E-06 BDL 0.3 83.19 7.1 0.13 8.77089E-06 8.898E-06 2.196E-05 2.277E-05 3.424E-05 2.625E-07 BDL 0.6 83.19 7.1 0.25 2.03704E-05 2.067E-05 1.640E-05 1.701E-05 2.558E-05 1.312E-07 BDL 0.3 83.19 7.1 0.13 1.5215E-05 1.544E-05 2.983E-04 3.094E-04 4.652E-04 2.625E-06 BDL 0.3 83.19 7.1 0.13 1.38376E-05 1.404E-05 9.626E-06 9.983E-06 1.501E-05 1.312E-07 BDL 0.3 83.19 7.1 0.13 8.9295E-06 9.059E-06 1.725E-03 1.789E-03 2.689E-03 8.749E-06 BDL 20 83.19 7.1 8.49 0.001599941 1.623E-03 3.858E-04 4.001E-04 6.016E-04 2.187E-06 BDL 5 83.19 7.1 2.12 0.000357877 3.631E-04 4.059E-04 4.209E-04 6.329E-04 2.625E-06 BDL 6 83.19 7.1 2.55 0.00037653 3.820E-04 2.030E-04 2.105E-04 3.165E-04 1.312E-06 BDL 0.3 83.19 7.1 0.13 1.88265E-05 1.910E-05 6.846E-04 7.099E-04 1.067E-03 3.5E-06 BDL 8 83.19 7.1 3.40 0.000635048 6.443E-04 1.613E-04 1.672E-04 2.515E-04 1.312E-06 BDL 3 83.19 7.1 1.27 0.0001496 1.518E-04 4.819E-05 4.997E-05 7.514E-05 4.375E-07 BDL 0.15 83.19 7.1 0.06 6.70543E-06 6.803E-06 3.952E-05 4.099E-05 6.163E-05 4.375E-07 BDL 0.15 83.19 7.1 0.06 5.49949E-06 5.579E-06 1.308E-03 1.357E-03 2.040E-03 8.749E-06 BDL 20 83.19 7.1 8.49 0.001213535 1.231E-03 2.183E-05 2.264E-05 3.404E-05 2.625E-07 BDL 0.6 83.19 7.1 0.25 2.02505E-05 2.054E-05 1.186E-04 1.230E-04 1.849E-04 1.312E-06 BDL 3 83.19 7.1 1.27 0.000109994 1.116E-04 4.490E-04 4.657E-04 7.002E-04 2.625E-06 BDL 6 83.19 7.1 2.55 0.00041654 4.226E-04 4.490E-04 4.657E-04 7.002E-04 2.625E-06 BDL 6 83.19 7.1 2.55 0.00041654 4.226E-04 4.490E-04 4.657E-04 7.002E-04 2.625E-06 BDL 6 83.19 7.1 2.55 0.00041654 4.226E-04 3.477E-04 3.606E-04 5.421E-04 3.5E-06 BDL 8 83.19 7.1 3.40 0.000322529 3.272E-04 2.700E-04 2.800E-04 4.210E-04 1.75E-06 BDL 4 83.19 7.1 1.70 0.000250435 2.541E-04 1.485E-04 1.540E-04 2.316E-04 1.312E-06 BDL 3 83.19 7.1 1.27 0.00013776 1.398E-04 2.575E-05 2.670E-05 4.015E-05 2.625E-07 BDL 0.6 83.19 7.1 0.25 2.38868E-05 2.423E-05 5.403E-04 5.604E-04 8.425E-04 2.625E-06 BDL 6 83.19 7.1 2.55 0.000501239 5.085E-04 1.700E-04 1.763E-04 2.650E-04 1.312E-06 BDL 3 83.19 7.1 1.27 0.000157666 1.600E-04 5.553E-04 5.758E-04 8.658E-04 4.375E-06 BDL 10 83.19 7.1 4.25 5.151E-04 5.225E-04 5.975E-04 6.197E-04 9.317E-04 4.375E-06 BDL 10 83.19 7.1 4.25 5.543E-04 5.623E-04 1.208E-04 1.253E-04 1.884E-04 8.749E-07 BDL 2 83.19 7.1 0.85 1.121E-04 1.137E-04 

## Run #2

Concentration 

## Run #3

Concentration1.812E-04 1.879E-04 2.826E-04 1.312E-06 BDL 3 83.19 7.1 1.27 1.681E-04 1.705E-04

8.450E-05 8.763E-05 1.318E-04 1.312E-06 BDL 3 83.19 7.1 1.27 7.839E-05 7.953E-05 5.439E-05 5.641E-05 8.482E-05 4.375E-07 BDL 1 83.19 7.1 0.42 5.046E-05 5.119E-05 6.619E-05 6.864E-05 1.032E-04 4.375E-07 BDL 0.15 83.19 7.1 0.06 9.209E-06 9.343E-06 2.318E-04 2.404E-04 3.614E-04 2.625E-06 BDL 6 83.19 7.1 2.55 2.150E-04 2.181E-04 2.531E-04 2.625E-04 3.947E-04 2.625E-06 BDL 6 83.19 7.1 2.55 2.348E-04 2.382E-04 2.420E-04 2.510E-04 3.773E-04 2.625E-06 BDL 6 83.19 7.1 2.55 2.245E-04 2.277E-04 2.788E-04 2.891E-04 4.348E-04 2.625E-06 BDL 6 83.19 7.1 2.55 2.586E-04 2.624E-04 7.962E-05 8.257E-05 1.242E-04 8.749E-07 BDL 0.15 83.19 7.1 0.06 5.540E-06 5.620E-06 7.960E-04 8.255E-04 1.241E-03 4.375E-06 BDL 10 83.19 7.1 4.25 7.384E-04 7.491E-04 2.460E-05 2.551E-05 3.835E-05 2.625E-07 BDL 0.6 83.19 7.1 0.25 2.282E-05 2.315E-05 3.868E-04 4.012E-04 6.032E-04 2.187E-06 BDL 0.15 83.19 7.1 0.06 1.077E-05 1.092E-05 9.156E-04 9.495E-04 1.428E-03 3.937E-06 BDL 9 83.19 7.1 3.82 8.493E-04 8.616E-04 1.017E-03 1.055E-03 1.586E-03 4.375E-06 BDL 10 83.19 7.1 4.25 9.437E-04 9.574E-04 1.717E-04 1.780E-04 2.677E-04 8.749E-07 BDL 0.3 83.19 7.1 0.13 2.389E-05 2.423E-05 1.593E-03 1.652E-03 2.484E-03 8.749E-06 BDL 20 83.19 7.1 8.49 1.478E-03 1.499E-03 1.593E-03 1.652E-03 2.484E-03 8.749E-06 BDL 20 83.19 7.1 8.49 1.478E-03 1.499E-03 1.593E-03 1.652E-03 2.484E-03 8.749E-06 BDL 20 83.19 7.1 8.49 1.478E-03 1.499E-03 5.362E-04 5.560E-04 8.360E-04 2.625E-06 BDL 6 83.19 7.1 2.55 4.974E-04 5.046E-04 3.954E-04 4.101E-04 6.166E-04 2.187E-06 BDL 5 83.19 7.1 2.12 3.668E-04 3.721E-04 7.908E-04 8.201E-04 1.233E-03 4.375E-06 BDL 10 83.19 7.1 4.25 7.336E-04 7.442E-04 4.455E-03 4.620E-03 6.947E-03 1.312E-05 BDL 30 83.19 7.1 12.74 4.133E-03 4.193E-03 3.330E-04 3.453E-04 5.192E-04 2.625E-06 BDL 6 83.19 7.1 2.55 3.089E-04 3.134E-04 5.070E-04 5.258E-04 7.906E-04 2.625E-06 BDL 6 83.19 7.1 2.55 4.703E-04 4.771E-04 3.718E-04 3.855E-04 5.797E-04 3.937E-06 BDL 9 83.19 7.1 3.82 3.448E-04 3.498E-04 6.173E-05 6.401E-05 9.625E-05 4.375E-07 BDL 0.15 83.19 7.1 0.06 8.589E-06 8.713E-06 5.845E-04 6.061E-04 9.114E-04 2.187E-06 BDL 5 83.19 7.1 2.12 5.422E-04 5.501E-04 1.088E-04 1.128E-04 1.696E-04 8.749E-07 BDL 2 83.19 7.1 0.85 1.009E-04 1.024E-04 3.638E-04 3.773E-04 5.672E-04 2.625E-06 BDL 6 83.19 7.1 2.55 3.375E-04 3.423E-04 3.343E-04 3.467E-04 5.213E-04 2.625E-06 BDL 6 83.19 7.1 2.55 3.101E-04 3.146E-04 2.786E-04 2.889E-04 4.344E-04 2.187E-06 BDL 5 83.19 7.1 2.12 2.584E-04 2.622E-04 4.360E-05 4.522E-05 6.799E-05 4.375E-07 BDL 0.15 83.19 7.1 0.06 6.067E-06 6.155E-06 9.146E-06 9.484E-06 1.426E-05 1.312E-07 BDL 0.3 83.19 7.1 0.13 8.484E-06 8.607E-06 3.583E-03 3.715E-03 5.586E-03 2.625E-05 BDL 60 83.19 7.1 25.47 3.323E-03 3.372E-03 1.468E-02 1.523E-02 2.290E-02 7.130E-05 ADL 10 83.19 7.1 4.25 8.357E-04 8.478E-04 4.819E-05 4.997E-05 7.514E-05 4.375E-07 BDL 0.15 83.19 7.1 0.06 6.705E-06 6.803E-06 1.135E-05 1.177E-05 1.770E-05 1.312E-07 BDL 0.3 83.19 7.1 0.13 1.053E-05 1.068E-05 7.044E-05 7.305E-05 1.098E-04 8.749E-07 BDL 2 83.19 7.1 0.85 6.534E-05 6.629E-05ppmvd

0% O2 lb/MMBtu Flag 1.514E-05 5.95463E-08 BDL 1.534E-05 5.62719E-08 BDL 3.343E-03 7.93951E-06 BDL 1.310E-05 5.95463E-08 BDL 1.813E-05 1.19093E-07 BDL 4.865E-05 2.38185E-07 BDL 2.113E-05 1.19093E-07 BDL 3.199E-05 2.38185E-07 BDL 3.199E-05 2.38185E-07 BDL 1.431E-05 1.19093E-07 BDL 9.255E-06 5.95463E-08 BDL 5.633E-05 3.96975E-07 BDL 9.255E-06 5.95463E-08 BDL 8.637E-04 2.38185E-06 BDL 3.212E-05 2.38185E-07 BDL 1.606E-05 1.19093E-07 BDL 1.071E-03 7.93951E-06 BDL 3.598E-04 1.5879E-06 BDL 5.443E-04 1.98488E-06 BDL 4.550E-04 1.98488E-06 BDL 3.189E-04 3.1758E-06 BDL 1.250E-04 7.93951E-07 BDL 1.338E-05 1.19093E-07 BDL 3.107E-05 2.38185E-07 BDL 2.321E-05 1.19093E-07 BDL 2.111E-05 1.19093E-07 BDL 1.362E-05 1.19093E-07 BDL 2.441E-03 7.93951E-06 BDL 5.459E-04 1.98488E-06 BDL 5.744E-04 2.38185E-06 BDL 2.872E-05 1.19093E-07 BDL 9.687E-04 3.1758E-06 BDL 2.282E-04 1.19093E-06 BDL 1.023E-05 5.95463E-08 BDL 8.389E-06 5.95463E-08 BDL 1.851E-03 7.93951E-06 BDL 3.089E-05 2.38185E-07 BDL 1.678E-04 1.19093E-06 BDL 6.354E-04 2.38185E-06 BDL 6.354E-04 2.38185E-06 BDL 6.354E-04 2.38185E-06 BDL 4.920E-04 3.1758E-06 BDL 3.820E-04 1.5879E-06 BDL 2.101E-04 1.19093E-06 BDL 3.644E-05 2.38185E-07 BDL 7.646E-04 2.38185E-06 BDL 2.405E-04 1.19093E-06 BDL 7.857E-04 3.96975E-06 BDL 8.455E-04 3.96975E-06 BDL 1.709E-04 7.93951E-07 BDL Concentration2.564E-04 1.19093E-06 BDL

1.196E-04 1.19093E-06 BDL 7.697E-05 3.96975E-07 BDL 1.405E-05 5.95463E-08 BDL 3.280E-04 2.38185E-06 BDL 3.582E-04 2.38185E-06 BDL 3.424E-04 2.38185E-06 BDL 3.945E-04 2.38185E-06 BDL 8.450E-06 5.95463E-08 BDL 1.126E-03 3.96975E-06 BDL 3.481E-05 2.38185E-07 BDL 1.642E-05 5.95463E-08 BDL 1.296E-03 3.57278E-06 BDL 1.440E-03 3.96975E-06 BDL 3.644E-05 1.19093E-07 BDL 2.254E-03 7.93951E-06 BDL 2.254E-03 7.93951E-06 BDL 2.254E-03 7.93951E-06 BDL 7.587E-04 2.38185E-06 BDL 5.595E-04 1.98488E-06 BDL 1.119E-03 3.96975E-06 BDL 6.304E-03 1.19093E-05 BDL 4.712E-04 2.38185E-06 BDL 7.174E-04 2.38185E-06 BDL 5.260E-04 3.57278E-06 BDL 1.310E-05 5.95463E-08 BDL 8.271E-04 1.98488E-06 BDL 1.539E-04 7.93951E-07 BDL 5.148E-04 2.38185E-06 BDL 4.730E-04 2.38185E-06 BDL 3.942E-04 1.98488E-06 BDL 9.255E-06 5.95463E-08 BDL 1.294E-05 1.19093E-07 BDL 5.070E-03 2.38185E-05 BDL 1.275E-03 3.96975E-06 BDL 1.023E-05 5.95463E-08 BDL 1.606E-05 1.19093E-07 BDL 9.967E-05 7.93951E-07 BDLEIA

Facility Code Facility Name Boiler ID 1943Hoot Lake (ORIS 1943) 2

Parameter Sample 1 Sample 2 Sample 3 Date of Testing 5/18/2010 5/18/2010 5/18/2010 SteamOutput (1000 lb/hr) 0.4031 0.405 0.3998 Total Heat Input (MMBtu/hr) 698 677.3 641.4 Basis (Wet/Dry) Wet Wet Wet Exhaust Steam % Moisture Exhaust Flow Rate (acfm or dscfm) 167,019.4 168,864.1 161,240.0 Exhaust Temperature (deg C or deg F) 349 356 340

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate

Sample 2 Fuel Input Rate

Sample 3 subbituminous 0.0272 0.0272 0.0266

Emission Test Results Hydrogen Cyanide Emission Rate Sample 1 (lb/MMBtu) Hydrogen Cyanide

Emission Rate Sample 2 (lb/MMBtu) Hydrogen Cyanide

Emission Rate Sample 3 (lb/MMBtu)

5.97E-04 6.87E-04 7.17E-04

Grey are those results below detection limistsUnit of Measure Other Supporting Information

1000 lb/hr From Plant DCS MMBtu/hr From CEMS N/A % Do Not Measure scfm From CEMS - Note EU Changed deg F From Plant DAHS

Unit of Measure Fuel Flow Measurement Method ktons/hr Other

Test Method Used (ex. U.S. EPA

Conditional Test Method 033) Other Supporting Information

U.S. EPA Conditional Test Method 033 (CTM-033) As shown in lab data the values (<700 μg) were BDL for all three runs. Sampling and lab data as well as the QA/QC results are provided in A-11 of the Appendix of the test reportPlant Location

Date Start

Q DN Cp

Other Supporting Information Y Note EU changed, fuel flow calculated off of feeder speed PBr DH Vm tm Vmstd

Vlc

Vwstd % H2O % H2Osat Mfd %CO2 %O2 % CO+ N2 Fo Md Ms Pg Ps ts DPavg

vs As Qsd Qaw %I % EA Fd

Copyright by Walter SmithHoot Lake U2 Address Fergus Falls, MN Job # HL-U2-STK-HCN ESP OUT DCT PersonnelDW Average M033-1 M-033-2 M-033-3 Test Date 5/18/10 5/18/10 5/19/10 Run Start Time 9:13 21:25 8:23 Run Finish Time 11:22 23:15 11:12 Net Traversing Points 30 30 30 Net Run Time, minutes 60 60 60 60 Nozzle Dianeter, inches 0.245 0.225 0.225 0.232 Pitot Tube Coeficient 0.84 0.84 0.84 0.84

Dry Gas Meter Calibration Factor 1.000 1.000 1.000 1.000 Barometric Pressure, inches of Mercury 28.88 28.86 28.91 28.88 Average orifice meter Differential, inches H2O 1.22 0.97 0.95 1.05 Dry Gas Meter Volume Sampled, cubic feet 40.412 34.856 34.078 36.449 Average Dry

Gas Meter Temperature, °F 74 73 73 73 Dry Gas Meter Volume Sampled, dscf 38.717 33.396 32.689 34.934

Total Moisture Liquid collected, ml

Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % 9.6 9.6 9.6 9.6 Moisture Saturation at Stack Gas Temperature, % 100 100 100 100 Dry Mole Fraction 0.904 0.904 0.904 0.904 Carbon Dioxide, % 11.8 11.8 11.5 11.7 Oxygen, % 7.2 7.1 7.4 7.2 Carbon Monoxide & Nitrogen, % 81 81.1 81.1 81.1 Fuel Factor 1.16 1.17 1.17 1.17 Dry Molecular Weight, lb/lb-Mole 30.176 30.172 30.136 30.161 Wet Molecular weight, lb/lb-Mole 29.007 29.003 28.971 28.994 Flue Gas Static Pressure, inches of H2O -7.3 -7.1 -7.3 -7.2 Absolute Flue Gas Pressure, inches of Mercury 28.34 28.34 28.37 28.35 Average Stack Gas Temperature, °F 353 359 350 354 Average Velocity

Head, inches of H2O 0.669 0.756 0.730 0.719 Average Stack Gas Velocity, feet/second 58.415 62.348 60.908 60.557 Stack Crossectional Area, square feet 78.0 78.0 78.0 78.0 Dry Volumetric Flow Rate, dry scfm 152,108 161,030 159,295 157,478 Actual Wet Volumetric Flue Gas Flow Rate, acfm 273,384 291,790 285,050 283,408 Percent Isokinetic of Sampling Rate, % 101.1 97.6 96.6 98.4 Percent Excess Air, % 50.7 49.6 52.8 51.0 F-Factor, dscfm/MMBtu @ )%O2 9820 9820 9820 9820

Copyright by Walter Smith Run Number



## Summary

of Sampling Data for OTM-0033 (HCN)EIA

Facility Code Facility Name Boiler ID

1943Hoot Lake (ORIS 1943) 2

Parameter Sample 1 Sample 2 Sample 3 Date of Testing SteamOutput (1000 lb/hr) Total Heat Input (MMBtu/hr) Basis (Wet/Dry) Exhaust Steam % Moisture Exhaust Flow Rate (acfm or dscfm) Exhaust Temperature (deg C or deg F)

Fuel Type Selection Fuel Input Rate Sample 1 Fuel Input Rate

Sample 2 Fuel Input Rate Sample 3

subbituminous

Emission Test Results Constituent Consitutent Emission Rate Sample 1 (%) Consitutent Emission

Rate Sample 2 (%)

O2 7.0 6.9 CO2 11.7 11.8

Date: 5-17-10 Run CO2 1 15.6 2 15.5 3 15.5 4 15.7 5 15.6 6 15.5 7 15.6 Average 15.57 Cal gas 16.05 Diff, % 0.49 QQ/QC PASS



### Calibration QA/QC Check See Dates in Table to the RightUnit of Measure Other Supporting Information

1000 lb/hr MMBtu/hr N/A %

Unit of Measure Fuel Flow Measurement Method Other Supporting Information

Consitutent Emission Rate Sample 3 (%) Test Method Used

(ex. U.S. EPA

Method 3B) Other Supporting

Information

7.0U.S. EPA Method 3B The calibration log book and complete results

11.9U.S. EPA Method 3B are provided in A-1 of the test report Appendix

O2

– (Valve Error) 4.8 4.8 4.8

– (Valve Error) 4.8 4.8 4.80 4.499 0.301 PASS 

### Calibration QA/QC Check

### Meter Pump Vm

Date Start time End time MethodBox # ID ID pre leak Vms Vme

Sample 1 Tests 5/17 11:13 22:51 23-1 12 6738 105117419 

### 559.301559.410 894.034 5/18 9:13 11:22 33-1 11 6737 1-0108105471 466.697466.748 507.160 5/19 15:24 23:01 27/28-1 11 

### 6737 1-0108105471 576.443576.487 716.772 5/24 9:31 13:57 29-1 11 

### 6737 1-0108105471 126.911127.072 266.587 5/24 12:45 16:28 26-1 12 6738 105117419 

### 790.901790.992 888.310 5/24 16:16 18:44 0011-1 11 

### 6737 1-0108105471 266.735266.768 338.814 Sample 2 Tests 5/18 11:14 22:06 23-2 12 6738 105117419 

### 894.138894.3141215.359

5/18 21:25 23:15 33-2 11 

### 6737 1-0108105471507.221507.362 542.218 5/20 10:32 16:48 27/28-2 11 

### 6737 1-0108105471 754.456754.610 892.190 5/25 8:22 10:53 0011-2 11 

### 6737 1-0108105471338.876338.934407.812 5/25 11:47 16:22 29-2 11 

### 6737 1-0108105471 407.866407.947 538.374 5/25 14:10 17:19 26-2 12 6738 105117419 

### 22.142 22.238 119.462 Sample 3 Tests

5/19 8:24 11:12 33-3 11 

### 6737 1-0108105471542.269542.318 576.396

5/19 11:14 23:54 23-3 12 6738 105117419 

### 215.498215.624 531.989

5/21 9:51 16:41 27/28-3 11 

### 6737 1-0108105471939.601939.7461076.500

5/25 9:35 11:51 0011-3 12 6738 105117419 

### 957.548957.6001022.090 5/26 10:11 14:40 29-3 11 

### 6737 1-0108105471541.245541.404 670.431 5/26 12:45 16:22 26-3 12 6738 105117419 

### 215.933216.034 311.525 

## SUMMARY OF ORSA

T DA TA

### Vm Dn Pitot Probe Probe TC Tedlar O2O2O2



### post leak Dn ID ID ID STK ID Pb Ps Cm ΔH@H2O Bag ID 1 2 3

894.1380.254 245L7-A-PTT-13 7-A 7-A-STK 28.97 -7.1 1.03 

### 1.59 9.3 HL-23-1 7.27.27.3 

### 507.2210.245 245L7-B-PTT-17 7-B 7-B-STK 28.88 -7.3 1.01 1.48 9.6 HL-33-17.27.1 7.2 

### 716.9320.172 4 

### 7-B-PTT-17 7-B 7-B-STK 28.91 -7.2 

### 1.01 1.48 9.7 HL-27-1 7.37.47.2 

### 266.7350.225225D

### 7-B-PTT-17 7-B 7-B-STK 28.62 -7.5 

### 1.01 1.48 10.8HL-29-16.36.46.5 

### 888.4040.219 219J7-A-PTT-13 7-A 7-A-STK 28.62 -6.9 1.03 

### 1.59 11.0HL-26-16.96.86.9 

### 338.8640.225225D

### 7-B-PTT-17 7-B 7-B-STK 28.62 -7.4 

### 1.01 1.48 10.3HL-11-1 7.27.1 7.1



### 1215.4750.221 221R7-A-PTT-13 7-A 7-A-STK 28.91 -7.5 1.03 

### 1.59 9.6 HL-23-27.1 7.1 7.2



### 542.2690.225225D

### 7-B-PTT-17 7-B 7-B-STK 28.86 -7.1 

### 1.01 1.48 9.6 HL-33-27.27.1 7.1 

### 892.3460.172 4 

### 7-B-PTT-17 7-B 7-B-STK 28.85 -7.5 

### 1.01 1.48 9.3 HL-27-27.1 7.27.1 

### 407.8660.225225D

### 7-B-PTT-17 7-B 7-B-STK 28.71 -7.2 

### 1.01 1.48 9.7 HL-11-27.07.1 7.0 

### 538.5320.215215S

### 7-B-PTT-17 7-B 7-B-STK 28.79 -7.2 

### 1.01 1.48 10.0HL-29-26.26.36.2 

### 119.5640.219 219J7-A-PTT-13 7-A 7-A-STK 28.76 -7.3 1.03 

### 1.59 10.1 HL-26-26.97.06.8



### 576.4430.225225D

### 7-B-PTT-17 7-B 7-B-STK 28.91 -7.3 

### 1.01 1.48 9.4 HL-33-37.47.47.5



### 532.1140.217217H7-A-PTT-13 7-A 7-A-STK 28.91 -7.3 1.03 

### 1.59 9.4 HL-23-37.27.47.2



### 1076.6470.172 4 

### 7-B-PTT-17 7-B 7-B-STK 28.74 -7.1 

### 1.01 1.48 10.0HL-27-37.37.27.1



### 1022.1430.219 219J7-A-PTT-13 7-A 7-A-STK 28.74 -7.4 1.03 

### 1.59 10.1 HL-11-36.97.06.9 

### 670.5860.215215S

### 7-B-PTT-17 7-B 7-B-STK 28.79 -7.5 

### 1.01 1.48 10.1 HL-29-36.36.26.4 

### 311.6490.219 219J7-A-PTT-13 7-A 7-A-STK 28.81 -7.4 1.03 

### 1.59 10.2HL-26-36.97.07.0 

## SUMMARY OF ORSA

T DA TA

### O2 CO2CO2CO2

### CO2

Avg. 1 2 3 Avg

7.2 11.6 11.5 11.5

### 11.5 7.2 11.8 11.8 11.7

### 11.8 7.3 11.6 11.6 11.5

### 11.6 6.4 11.7 11.8 11.8

### 11.8 6.9 11.7 11.8 11.8

### 11.8 7.1 11.5 11.5 11.6

### 11.5

7.1 11.6 11.7 11.5

### 11.6

7.1 11.8 11.8 11.8

### 11.8

7.1 11.5 11.4 11.4

### 11.4 7.0 11.6 11.4 11.5

### 11.5 6.2 12.3 12.2 12.4

### 12.3 6.9 12.4 12.1 12.4

### 12.3

7.4 11.6 11.4 11.5

### 11.5

7.3 11.6 11.5 11.8

### 11.6

7.2 11.3 11.6 11.6

### 11.5

6.9 12.1 12.1 12.1

### 12.1 6.3 12.3 12.6 12.3

### 12.4 7.0 12.4 12.2 12.3

### 12.3Fuel

anthracite bituminous subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) synfuel petroleum coke other

Relative to Control Device Upstream Downstream

Fuel Input Units of Measure MMBtu/hr standard cubic feet per minute (scfm) gallon/minute ktons/hr lb/hour ton/day

Exhaust Flow Rate Units of Measure acfm scfm dscfm

Exhaust Temperature Units of Measure deg C deg F

Test Method Used for Fuel Input Rate F-Factor gas fuel meter boiler efficiency

calculation Other

CO Test Method U.S. EPA Method 10A U.S. EPA Method 10B

Formaldehyde Test Method U.S. EPA Method 320CH4 Test Method

U.S. EPA Method 18 U.S. EPA Method 320

SO2 Test Method U.S. EPA Method 6

Hg Test Method U.S. EPA Method 30B

Speciated Volatile Organic HAP Method U.S. EPA Method 0031 with SW-846 Method 8260B

Speciated Semi-Volatile Organic HAP Method U.S. EPA Method 0010 with SW-846 Method 8270D

HCN Test Method U.S. EPA Conditional Test Method 033 (CTM-033)

O2/CO2 Test Method U.S. EPA Method 3B

NOX Test Method U.S. EPA Method 7 U.S. EPA Method 7A U.S. EPA Method 7B U.S. EPA Method 7C U.S. EPA Method 7D

TDS/TSS Test Method Standard Test Method for Filterable and Nonfilterable Matter in Water ASTM D5907 Standard Methods of the Examination of Water and Wastewater Method 2540B

Control Configuration 

### Listed (by boiler) in Question 16 (page 17) of the questionnaire Listed (by boiler) in the Configuration Order Section of the Facility Unit Configurations Section of the Electronic ICR

Hg Ontario Hydro Test Method ASTM Method D6784Constituent CAS Acetone 67-64-1 Acetonitrile 75-05-8 Acrolein (Propenal) 107-02-8 Acrylonitrile 107-13-1 Allyl alcohol 107-18-6 Allyl chloride 107-05-1 Benzene 71-43-2 Benzyl chloride 100-44-7 Bis(2-chloroethyl)sulfide 505-60-2 Bromoacetone 598-31-2 Bromochloromethane 74-97-5 Bromodichloromethane 75-27-4 4-Bromofluorobenzene (surr) 460-00-4 Bromoform 75-25-2 Bromomethane 74-83-9 n-Butanol 71-36-3 2-Butanone (MEK) 78-93-3 t-Butyl alcohol 75-65-0 Carbon disulfide 75-15-0 Carbon tetrachloride 56-23-5 Chloral hydrate 302-17-0 Chlorobenzene 108-90-7 Chlorobenzene-d (IS) Chlorodibromomethane 124-48-1 Chloroethane 75-00-3 2-Chloroethanol 107-07-3 2-Chloroethyl vinyl ether 110-75-8 Chloroform 67-66-3 Chloromethane 74-87-3 Chloroprene 126-99-8 3-Chloropropionitrile 542-76-7 Crotonaldehyde 4170-30-3 1,2-Dibromo-3-chloropropane 96-12-8 1,2-Dibromoethane 106-93-4 Dibromomethane 74-95-3 1,2-Dichlorobenzene 95-50-1 1,3-Dichlorobenzene 541-73-1 1,4-Dichlorobenzene 106-46-7 1,4-Dichlorobenzene-d (IS) cis-1,4-Dichloro-2-butene 1476-11-5 trans-1,4-Dichloro-2-butene 110-57-6 Dichlorodifluoromethane 75-71-8 1,1-Dichloroethane 75-34-3 1,2-Dichloroethane 107-06-2 1,2-Dichloroethane-d (surr) 1,1-Dichloroethene 75-35-4 trans-1,2-Dichloroethene 156-60-5 1,2-Dichloropropane 78-87-5 cis-1,2 Dichloroethene 156-59-2 cis-1,3-Dichloropropene 10061-01-5 trans-1,3-Dichloropropene 10061-02-6 Speciated Volatile Organic HAPs1,2,3,4-Diepoxybutane 1464-53-5 Diethyl ether 60-29-7 1,4-Difluorobenzene (IS) 540-36-3 1,4-Dioxane 123-91-1 Epichlorohydrin 106-89-8 Ethanol 64-17-5 Ethyl acetate 141-78-6 Ethylbenzene 100-41-4 Ethylene oxide 75-21-8 Ethyl methacrylate 97-63-2 Fluorobenzene (IS) 462-06-6 Hexachlorobutadiene 87-68-3 Hexachloroethane 67-72-1 2-Hexanone 591-78-6 2-Hydroxypropionitrile 78-97-7 Iodomethane 74-88-4 Isobutyl alcohol 78-83-1 Isopropylbenzene 98-82-8 Malononitrile 109-77-3 Methacrylonitrile 126-98-7 Methanol 67-56-1 Methylene chloride 75-09-2 Methyl methacrylate 80-62-6 4-Methyl-2-pentanone (MIBK) 108-10-1 Naphthalene 91-20-3 Nitrobenzene 98-95-3 2-Nitropropane 79-46-9 N-Nitroso-di-n-butylamine 924-16-3 Paraldehyde 123-63-7 Pentachloroethane 76-01-7 2-Pentanone 107-87-9 2-Picoline 109-06-8 1-Propanol 71-23-8 2-Propanol 67-63-0 Propargyl alcohol 107-19-7 $-Propiolactone 57-57-8 Propionitrile (ethyl cyanide) 107-12-0 n-Propylamine 107-10-8 Pyridine 110-86-1 Styrene 100-42-5 1,1,1,2-Tetrachloroethane 630-20-6 1,1,2,2-Tetrachloroethane 79-34-5 Tetrachloroethene 127-18-4 Toluene 108-88-3 

### Listed (by boiler) in the Configuration Order Section of the Facility Unit Configurations Section of the Electronic ICR Toluene-d (surr) 2037-26-5 o-Toluidine 95-53-4 1,2,4-Trichlorobenzene 120-82-1 1,1,1-Trichloroethane 71-55-6 1,1,2-Trichloroethane 79-00-5 Trichloroethene 79-01-6 Trichlorofluoromethane 75-69-4 1,2,3-Trichloropropane 96-18-4 Vinyl acetate 108-05-4Vinyl chloride 75-01-4 o-Xylene 95-47-6 m-Xylene 108-38-3 p-Xylene 106-42-3Speciated Semi-volatile Organic HAPs

Constituent CAS Acenaphthene 83-32-9 Acenaphthylene 208-96-8 Acetophenone 98-86-2 2-Acetylaminofluorene 53-96-3 1-Acetyl-2-thiourea 591-08-2 Aldrin 309-00-2 2-Aminoanthraquinone 117-79-3 Aminoazobenzene 60-09-3 4-Aminobiphenyl 92-67-1 3-Amino-9-ethylcarbazole 132-32-1 Anilazine 101-05-3 Aniline 62-53-3 o-Anisidine 90-04-0 Anthracene 120-12-7 Aramite 140-57-8 Tetralin 119-64-2 Coronene 191-07-1 Benzo(e)pyrene 192-97-2 Perylene 198-55-0 Benzo(a)fluorene 238-84-6 Benzo(b)fluorene 243-17-4 2-Methylanthracene 613-12-7 Azinphos-methyl 86-50-0 Barban 101-27-9 Benzidine 92-87-5 Benzoic acid 65-85-0 Benz(a)anthracene 56-55-3 Benzo(b)fluoranthene 205-99-2 Benzo(k)fluoranthene 207-08-9 Benzo(g,h,i)perylene 191-24-2 Benzo(a)pyrene 50-32-8 p-Benzoquinone 106-51-4 Benzyl alcohol 100-51-6 9,10-Dimethylanthracene 781-43-1 1-Methylphenanthrene 832-69-9 o-Terphenyl 84-15-1 Carbazole 86-74-8 Bis(2-chloroethoxy)methane 111-91-1 Bis(2-chloroethyl) ether 111-44-4 Bis(2-chloroisopropyl) ether 39638-32-9 Bis(2-ethylhexyl) phthalate 117-81-7 4-Bromophenyl phenyl ether 101-55-3 Bromoxynil 1689-84-5 Butyl benzyl phthalate 85-68-7 1-Methylnaphthalene 90-12-0 Quinoline 91-22-5 m-Terphenyl 92-06-8 Biphenyl 92-52-4 p-Terphenyl 92-94-4 Chlordane (NOS) 57-74-9 Chlorfenvinphos 470-90-64-Chloroaniline 106-47-8

Chlorobenzilate 510-15-6 5-Chloro-2-methylaniline 95-79-4 4-Chloro-3-methylphenol 59-50-7 3-(Chloromethyl)pyridine hydrochloride 6959-48-4 1-Chloronaphthalene 90-13-1 2-Chloronaphthalene 91-58-7 2-Chlorophenol 95-57-8 4-Chloro-1,2-phenylenediamine 95-83-0 4-Chloro-1,3-phenylenediamine 5131-60-2 4-Chlorophenyl phenyl ether 7005-72-3 Chrysene 218-01-9 Coumaphos 56-72-4 p-Cresidine 120-71-8 Crotoxyphos 7700-17-6 2-Cyclohexyl-4,6-dinitro-phenol 131-89-5 4,4'-DDD 72-54-8 4,4'-DDE 72-55-9 4,4'-DDT 50-29-3 Demeton-O 298-03-3 Demeton-S 126-75-0 Diallate (cis or trans) 2303-16-4 2,4-Diaminotoluene 95-80-7 Dibenz(a,j)acridine 224-42-0 Dibenz(a,h)anthracene 53-70-3 Dibenzofuran 132-64-9 Dibenzo(a,e)pyrene 192-65-4 1,2-Dibromo-3-chloropropane 96-12-8 Di-n-butyl phthalate 84-74-2 Dichlone 117-80-6 1,2-Dichlorobenzene 95-50-1 1,3-Dichlorobenzene 541-73-1 1,4-Dichlorobenzene 106-46-7 3,3'-Dichlorobenzidine 91-94-1 2,4-Dichlorophenol 120-83-2 2,6-Dichlorophenol 87-65-0 Dichlorovos 62-73-7 Dicrotophos 141-66-2 Dieldrin 60-57-1 Diethyl phthalate 84-66-2 Diethylstilbestrol 56-53-1 Diethyl sulfate 64-67-5 Dimethoate 60-51-5 3,3'-Dimethoxybenzidine 119-90-4 Dimethylaminoazobenzene 60-11-7 7,12-Dimethylbenzo(a)-anthracene 57-97-6 3,3'-Dimethylbenzidine 119-93-7 α,α-Dimethylphenethylamine 122-09-8 2,4-Dimethylphenol 105-67-9 Dimethyl phthalate 131-11-3 1,2-Dinitrobenzene 528-29-0 1,3-Dinitrobenzene 99-65-0 1,4-Dinitrobenzene 100-25-44,6-Dinitro-2-methylphenol 534-52-1

2,4-Dinitrophenol 51-28-5 2,4-Dinitrotoluene 121-14-2 2,6-Dinitrotoluene 606-20-2 Dinocap 39300-45-3 Dinoseb 88-85-7 Diphenylamine 122-39-4 5,5-Diphenylhydantoin 57-41-0 1,2-Diphenylhydrazine 122-66-7 Di-n-octyl phthalate 117-84-0 Disulfoton 298-04-4 Endosulfan I 959-98-8 Endosulfan II 33213-65-9 Endosulfan sulfate 1031-07-8 Endrin 72-20-8 Endrin aldehyde 7421-93-4 Endrin ketone 53494-70-5 X X ND X X 53494-70-5 EPN 2104-64-5 Ethion 563-12-2 Ethyl carbamate 51-79-6 Ethyl methanesulfonate 62-50-0 Famphur 52-85-7 Fensulfothion 115-90-2 Fenthion 55-38-9 Fluchloralin 33245-39-5 Fluoranthene 206-44-0 Fluorene 86-73-7 2-Fluorobiphenyl (surr) 321-60-8 2-Fluorophenol (surr) 367-12-4 Heptachlor 76-44-8 Heptachlor epoxide 1024-57-3 Hexachlorobenzene 118-74-1 Hexachlorobutadiene 87-68-3 Hexachlorocyclopentadiene 77-47-4 Hexachloroethane 67-72-1 Hexachlorophene 70-30-4 Hexachloropropene 1888-71-7 Hexamethylphosphoramide 680-31-9 Hydroquinone 123-31-9 Indeno(1,2,3-cd)pyrene 193-39-5 Isodrin 465-73-6 Isophorone 78-59-1 Isosafrole 120-58-1 Kepone 143-50-0 Leptophos 21609-90-5 Malathion 121-75-5 Maleic anhydride 108-31-6 Mestranol 72-33-3 Methapyrilene 91-80-5 Methoxychlor 72-43-5 3-Methylcholanthrene 56-49-5 4,4'-Methylenebis (2-chloroaniline) 101-14-4 4,4'-Methylenebis(N,N-dimethylaniline) 101-61-1 1-Methylphenanthrene 832-69-9 2-Methylnaphthalene 91-57-62-Methylanthracene 613-12-7

2-Methylphenol 95-48-7 3-Methylphenol 108-39-4 4-Methylphenol 106-44-5 Mevinphos 7786-34-7 Mexacarbate 315-18-4 Mirex 2385-85-5 Monocrotophos 6923-22-4 Naled 300-76-5 Naphthalene 91-20-3 1,4-Naphthoquinone 130-15-4 1-Naphthylamine 134-32-7 2-Naphthylamine 91-59-8 Nicotine 54-11-5 5-Nitroacenaphthene 602-87-9 2-Nitroaniline 88-74-4 3-Nitroaniline 99-09-2 4-Nitroaniline 100-01-6 5-Nitro-o-anisidine 99-59-2 Nitrobenzene 98-95-3 4-Nitrobiphenyl 92-93-3 Nitrofen 1836-75-5 2-Nitrophenol 88-75-5 4-Nitrophenol 100-02-7 5-Nitro-o-toluidine 99-55-8 Nitroquinoline-1-oxide 56-57-5 N-Nitrosodi-n-butylamine 924-16-3 N-Nitrosodiethylamine 55-18-5 N-Nitrosodimethylamine 62-75-9 N-Nitrosodiphenylamine 86-30-6 N-Nitrosodi-n-propylamine 621-64-7 N-Nitrosomethylethylamine 10595-95-6 N-Nitrosomorpholine 59-89-2 N-Nitrosopiperidine 100-75-4 N-Nitrosopyrrolidine 930-55-2 Octamethyl pyrophosphoramide 152-16-9 4,4'-Oxydianiline 101-80-4 Parathion 56-38-2 Pentachlorobenzene 608-93-5 Pentachloronitrobenzene 82-68-8 Pentachlorophenol 87-86-5 Phenacetin 62-44-2 Phenanthrene 85-01-8 Phenobarbital 50-06-6 Phenol 108-95-2 1,4-Phenylenediamine 106-50-3 Phorate 298-02-2 Phosalone 2310-17-0 Phosmet 732-11-6 Phosphamidon 13171-21-6 Phthalic anhydride 85-44-9 2-Picoline (2-Methylpyridine) 109-06-8 Piperonyl sulfoxide 120-62-7 Pronamide 23950-58-5 Propylthiouracil 51-52-5Pyrene 129-00-0

Resorcinol 108-46-3 Safrole 94-59-7 Strychnine 57-24-9 Sulfallate 95-06-7 Terbufos 13071-79-9 1,2,4,5-Tetrachlorobenzene 95-94-3 2,3,4,6-Tetrachlorophenol 58-90-2 Tetrachlorvinphos 961-11-5 Tetraethyl dithiopyrophosphate 3689-24-5 Tetraethyl pyrophosphate 107-49-3 Thionazine 297-97-2 Thiophenol (Benzenethiol) 108-98-5 Toluene diisocyanate 584-84-9 o-Toluidine 95-53-4 Toxaphene 8001-35-2 1,2,4-Trichlorobenzene 120-82-1 2,4,5-Trichlorophenol 95-95-4 2,4,6-Trichlorophenol 88-06-2 Trifluralin 1582-09-8 2,4,5-Trimethylaniline 137-17-7 Trimethyl phosphate 512-56-1 1,3,5-Trinitrobenzene 99-35-4 Tris(2,3-dibromopropyl) phosphate 126-72-7 Tri-p-tolyl phosphate 78-32-0 O,O,O-Triethyl phosphorothioate 126-68-1