### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

3152 Sunbury

Generation 4 

### bituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte



### 3152 Sunbury Generation 4 As Received Higher Heating Value 

### 3152 Sunbury Generation 4 As Received % Moisture 

### 3152 Sunbury Generation 4 As Received % Ash 

### 3152 Sunbury Generation 4 As Received % Sulfur 

### 3152 Sunbury Generation 4 Dry basis Higher Heating Value 

### 3152 Sunbury Generation 4 Dry basis % Ash 

### 3152 Sunbury Generation 4 Dry basis % Sulfur 

### 3152 Sunbury Generation 4 Dry basis Antim ony 

### 3152 Sunbury Generation 4 Dry basis Arsenic 

### 3152 Sunbury Generation 4 Dry basis Bery llium 

### 3152 Sunbury Generation 4 Dry basis Cadmium 

### 3152 Sunbury Generation 4 Dry basis Chlorine 

### 3152 Sunbury Generation 4 Dry basis Chromium 

### 3152 Sunbury Generation 4 Dry basis Cobalt 

### 3152 Sunbury Generation 4 Dry basis Fluorine 

### 3152 Sunbury Generation 4 Dry basis Lead 

### 3152 Sunbury Generation 4 Dry basis Manganese 

### 3152 Sunbury Generation 4 Dry basis Mercury 

### 3152 Sunbury Generation 4 Dry basis Nickel 

### 3152 Sunbury Generation 4 Dry basis SeleniumAn alysis M ethod for each A nalyte

(example: ASTM D5865-04) 

### ASTM D5865 ASTM D3302 ASTM D3174 ASTM D4239 Method B ASTM D5865 ASTM D3174 ASTM D4239 Method B ASTM D6357 ASTM D6357 ASTM D6357 ASTM D6357 ASTM D6721 ASTM D6357 ASTM D6357 ASTM D3761 ASTM D6357 ASTM D6357 ASTM D6722 ASTM D6357 SW-846-7740EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 3152 Sunbury Generation 4 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### Sample - 018 8/10/2010 8/10/2010 12463 Btu/lb Sample - 021 8/11/2010 8/11/2010 12384 Btu/lb Sample - 024 8/12/2010 8/12/2010 12248 Btu/lb Fuel Testing Results

### Mercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 7.63 9.73 1.79 13493 Btu/lb 10.54 1.94 6.35 11.03 2.01 13223 Btu/lb 11.78 2.15 7.32 11.44 1.86 13215 Btu/lb 12.35 2.01Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis) 

### 900 ppm 0.15 μg/g [<1.00] μg/g 8 μg/g 1.1 700 ppm 0.18 μg/g [<1.00] μg/g 11 μg/g 1.2 700 ppm 0.18 μg/g [<1.00] μg/g 10 μg/g 1.2Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### μg/g [<0.2] μg/g 19 μg/g 6 μg/g 33 μg/g μg/g [<0.2] μg/g 19 μg/g 7 μg/g 28 μg/g μg/g [<0.2] μg/g 21 μg/g 7 μg/g 32 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 11 μg/g 4 μg/g 74 ppm 4 μg/g 11 μg/g 4 μg/g 73 ppm 4 μg/g 12 μg/g 3 μg/g 79 ppm 4 μg/g Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 

### 33.73 10.54 55.73 79.07 4.77 1.45 1.94 34.00 11.78 54.22 76.49 4.59 1.43 2.15 33.50 12.35 54.15 76.27 4.59 1.44 2.01 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen



### 2.23 3.56 3.34EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 3152 Sunbury Generation 4 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 

### Sample - 027 8/13/2010 8/13/2010 12076 Btu/lb Sample - 030 8/13/2010 8/13/2010 12188 Btu/lb Sample - 033 8/13/2010 8/13/2010 12285 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 6.95 13.07 1.73 12978 Btu/lb 14.05 1.85 7.38 12.34 1.99 13159 Btu/lb 13.33 2.15 7.17 12.10 1.81 13234 Btu/lb 13.03 1.95Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis) 

### 760 ppm 720 ppm 690 ppmBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 

### 68.8 ppm 66.5 ppm 73.9 ppmNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur



### 33.09 14.05 52.86 74.48 4.46 1.40 1.85 33.05 13.33 53.62 75.75 4.55 1.41 2.15 33.41 13.03 53.56 76.61 4.62 1.43 1.95 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 

### 3.76 2.81 2.36EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 3152 Sunbury Generation 4 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### Sample - 027 8/13/2010 8/13/2010 12076 Btu/lb Sample - 030 8/13/2010 8/13/2010 12188 Btu/lb Sample - 033 8/13/2010 8/13/2010 12285 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 6.95 13.07 1.73 12978 Btu/lb 14.05 1.85 7.38 12.34 1.99 13159 Btu/lb 13.33 2.15 7.17 12.10 1.81 13234 Btu/lb 13.03 1.95Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis) 

### 760 ppm 720 ppm 690 ppmBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 68.8 ppm 66.5 ppm 73.9 ppm Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 33.09 14.05 52.86 74.48 4.46 1.40 1.85 3.76 33.05 13.33 53.62 75.75 4.55 1.41 2.15 2.81 33.41 13.03 53.56 76.61 4.62 1.43 1.95 2.36 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 3152 Sunbury Generation 4 Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wt