### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

10671 AES Shady

Point Units 1 & Unit 2 

### bituminousFuel Type 2 Fuel Type 3 Other Fuel Description



### subbituminousEIA

Facility Code Facility Name Boiler ID Basis An alyte



### 10671 AES Shady Point Units 1 & Unit 2 As Received Higher Heating Value 

### 10671 AES Shady Point Units 1 & Unit 2 As Received % Moisture 

### 10671 AES Shady Point Units 1 & Unit 2 As Received % Ash 

### 10671 AES Shady Point Units 1 & Unit 2 As Received % Sulfur 

### 10671 AES Shady Point Units 1 & Unit 2 Dry basis Higher Heating Value 

### 10671 AES Shady Point Units 1 & Unit 2 Dry basis % Ash 

### 10671 AES Shady Point Units 1 & Unit 2 Dry basis % Sulfur 

### 10671 AES Shady Point Units 1 & Unit 2 Dry basis Antim ony 

### 10671 AES Shady Point Units 1 & Unit 2 Dry basis Arsenic 

### 10671 AES Shady Point Units 1 & Unit 2 Dry basis Bery llium 

### 10671 AES Shady Point Units 1 & Unit 2 Dry basis Cadmium 

### 10671 AES Shady Point Units 1 & Unit 2 Dry basis Chlorine 

### 10671 AES Shady Point Units 1 & Unit 2 Dry basis Chromium 

### 10671 AES Shady Point Units 1 & Unit 2 Dry basis Cobalt 

### 10671 AES Shady Point Units 1 & Unit 2 Dry basis Fluorine 

### 10671 AES Shady Point Units 1 & Unit 2 Dry basis Lead 

### 10671 AES Shady Point Units 1 & Unit 2 Dry basis Manganese 

### 10671 AES Shady Point Units 1 & Unit 2 Dry basis Mercury 

### 10671 AES Shady Point Units 1 & Unit 2 Dry basis Nickel 

### 10671 AES Shady Point Units 1 & Unit 2 Dry basis SeleniumAn alysis M ethod for each A nalyte

(example: ASTM D5865-04) 

### D4809 160.3 MOD D482 D1552 D5865 D3174 D4239 6020 6020 6020 6020 9056 6020 6020 9056 6020 6020 7471A 6020 6020EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 10671 AES Shady Point Units 1 & Unit 2 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units PM-001 

### 6/6/2010 6/6/2010 9169 Btu/lb PM-002 6/7/2010 6/7/2010 9041 Btu/lb PM-003 6/8/2010 6/8/2010 8797 Btu/lb HG-010 6/5/2010 6/5/2010 8814 Btu/lb HG-011 6/5/2010 6/5/2010 9189 Btu/lb HG-012 6/5/2010 6/5/2010 9191 Btu/lb Fuel Testing Results

### Mercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 21.9 13.3 0.886 11740 Btu/lb 1.135 23.3 11.72 0.929 11787 Btu/lb 1.211 25.8 10.51 0.778 11856 Btu/lb 1.049 23.2 13.38 0.850 11477 Btu/lb 1.107 20.7 13.84 0.944 11588 Btu/lb 1.19 19.8 14.32 0.965 11460 Btu/lb 1.203Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 0.308 mg/Kg ND mg/Kg 5.8 mg/Kg 0.52 0.256 mg/Kg ND mg/Kg 5.3 mg/Kg ND 0.22 mg/Kg ND mg/Kg 7.8 mg/Kg ND 105 ppm 0.301 mg/Kg ND mg/Kg 2.5 mg/Kg 0.61 101 ppm 0.213 mg/Kg ND mg/Kg 3.9 mg/Kg 0.6 105 ppm 0.452 mg/Kg ND mg/Kg 5.4 mg/Kg NDBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### mg/Kg ND mg/Kg 7.9 mg/Kg 6.1 mg/Kg 59 mg/Kg mg/Kg ND mg/Kg 8.2 mg/Kg 8 mg/Kg 78 mg/Kg mg/Kg ND mg/Kg 7.8 mg/Kg 2.9 mg/Kg 37 mg/Kg mg/Kg ND mg/Kg 7.4 mg/Kg 3.3 mg/Kg 59 mg/Kg mg/Kg ND mg/Kg 9.5 mg/Kg 4.6 mg/Kg 102 mg/Kg mg/Kg ND mg/Kg 9.2 mg/Kg 6.3 mg/Kg 126 mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 16 mg/Kg 5.2 mg/Kg 5.6 mg/Kg 21.9 14 mg/Kg ND mg/Kg 5.2 mg/Kg 23.3 8.5 mg/Kg ND mg/Kg 3.3 mg/Kg 25.8 8.9 mg/Kg ND mg/Kg 4.3 mg/Kg 23.2 12 mg/Kg ND mg/Kg 4.9 mg/Kg 20.7 17 mg/Kg ND mg/Kg 6.1 mg/Kg 19.8 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 

### 30.28 17.03 52.6 68.26 4.2 1.48 1.315 32.04 15.28 52.69 69.11 3.96 1.65 1.211 32.5 14.17 53.33 72.16 3.99 1.76 1.049 31.05 17.43 51.51 65.4 4.23 1.23 1.107 30.4 17.45 52.15 67.31 4.37 1.28 1.19 30.12 17.86 52.02 64.73 3.99 0.62 1.203 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen



### 8.39 7.61 8.69 9.18 10.84 7.04EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 10671 AES Shady Point Units 1 & Unit 2 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 

### AG-004 6/6/2010 6/6/2010 9300 Btu/lb AG-005 6/7/2010 6/7/2010 9214 Btu/lb AG-006 6/8/2010 6/8/2010 9154 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 20.2 13.5 0.925 11654 Btu/lb 1.159 21.4 12.04 0.913 11723 Btu/lb 1.162 22.2 11.58 0.806 11766 Btu/lb 1.036Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 108 ppm 99 ppm 90 ppmBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 

### 70 ppm 74 ppm 68 ppmNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur



### 20.2 30.57 16.92 52.51 68.85 4.23 1.58 1.159 21.4 31.19 15.32 53.48 70.62 3.98 1.8 1.162 22.2 33.22 14.89 51.89 69.71 3.95 1.38 1.036 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 

### 7.33 6.23 5.63EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 10671 AES Shady Point Units 1 & Unit 2 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### ORG-007 6/3/2010 6/3/2010 9408 Btu/lb ORG-008 6/4/2010 6/4/2010 9699 Btu/lb ORG-009 6/4/2010 6/4/2010 9327 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 19.1 14.45 1.006 11629 Btu/lb 1.244 18.1 13.49 1.112 11842 Btu/lb 1.358 21.6 12.58 1.024 11897 Btu/lb 1.306Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 94 ppm 104 ppm 92 ppmBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture

### 19.1 18.1 21.6 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 31.73 17.86 50.4 65.74 4.53 1.18 1.244 8.48 30.75 16.48 52.78 69.47 4.17 1.36 1.358 8.33 31.66 16.05 52.3 68.04 4.38 1.25 1.306 10.22 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 10671 AES Shady Point Units 1 & Unit 2

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm