VEOLI A E S TECHNICA L SOLUTIONS , L.L.C . RESPONSE S T O TH E UNITE D STATE S ENVIRONMENTA L PROTECTIO N AGENCY' S REQUES TT O PROVID E INFORMATIO N PURSUAN TT O TH E CLEA N AI R AC TDATE D JANUAR Y29 , 200 9



### Exhibit s C - G

# c

VE S 00229 1

# Evaluatio n of Metals , Particulat e Matte r

an d PCDD/PCD F Emission s fo rFixe d Heart h Incinerato rUni t 3 Jun e 200 6

ENS R Corporatio n Septembe r 200

6 Documen t No. : 10002-01 7

### Prepare d for : Veoli a E S Technica l Solution s Sauget , Illinoi s



# Evaluatio n o

f Metals , Particulat e Matte r an d PCDD/PCD F Emission s fo rFixe d Heart h Incinerato rUni t 3 Jun e 200 6

Prepare d By : Jeffre

y T . Gorman , Projec

t Manage r

Reviewe d By : Crai g R . Doolittle.rE , Manager, Ai r Measurement s

ENS R Corporation September 200

6 Document No. : 10002-01 7

## ENS R



# Content s 1. 6 Introductio n . 1 

## " 1 

## 1. 1 Progra m Summar

y •1- 1 2. 0 incinerato rProces s Descriptio n .. . . 2- 1 2. 1 Proces

s Overvie w2- 1 22. Wast e Fee d System s [4 0 CF R §63.1207(f)(1)(i«)(D)(E ) and (f)(1)(ii)(C) ] 2-

1 2. 3 Manufacturer

, Mak e and Mode l o

fth e Incinerato

r [4 0 CF R §63.1207(f)(1)(iii)(A)j* 2- 1 2. 4 Ai rPollutio

n Control Equipmen

t [4 0 CF R §63.1207(f)(1)(iii)(Q) ] 2- 2 2.4. 1 Lim

e Syste m 2- 2 2.4.2 Spra

y Dr y Absorber2- 3 2.4.3 Fabri c Filte

r2- 3 2.4.4 Induce

d Draf t Fa n an d Stack

- 2- 3 3.0 Summar

y o fResults . . ... . . • 3- 1 

## 3.1 Introduction.... . 3- 1 3. 2 Stack Emission Result

s fo rPCDDs/PCDFs 3- t 3.3 Stack

Emission Result

s for Targe

t Metal s an d Particulat

e Matte r 3-

1 3.4 Metal s Sampl e Contamination 3- 2 4. 0 Samplin g an d Analytica l Procedures 4- 1 4. 1 Sampling Procedure s 4- 1 4.1. 1 Velocity

, Moistur e and Fixe

d Gas Determination

s 4- 1 4.1.2 PCDD/PCD F Samplin g • •4- 1 4.1.3 Metals and Particulat e Sampling 4- 1 4.2 Analytical Procedure s 4- 1 4.2. 1 PCDD/PCD F Analyse s 4- 1 4.2.2 Melal s Analyse

s •4- 2 4. 3 Proces

s Operating Conditions 4- 2 5.0 Qualit

y Assurance.. . . ..... . 5- 1 5.1 Introductio

n 5- 1 5.1. 1 Pre-Sampling Activitie s 5- 1 5.1. 2 Equipmen

t Calibration , 5- 1 5.1. 3 Glasswar

e Preparation 5- 2

CADocumenlsardSetling^««xx*i»ar*ljoca l I September200 6 Setdr^sXTemporai

y Interne t Rles\0LK7O0ny

x200 6 Tes t Reportdoc



## VE S 00230 1

## ENS R



# List o fAppendice

s Appendi xA Facilit

y Operatin g Dat

a Appendi xB Referenc

e Metho d Rei d Dat

a and Calculations Appendi xC Referenc

e Metho d Calibrations, Verifications, and Certification s Appendi xD Stack

Configuration , Sampling Por t and Travers

e Poin t Location s Appendi xE Laborator

y Dat a 

# List o fTables Tabl e 3- 1 PCD D /

PCD F Emission Result

s - TE Q Basi s 3- 3 Tabl e 3- 2 Emission Result

s forLV M Metal

s - Ma y200 6 3- 4 Tabl e 3- 3 Emission Result

s forLV M Metals - June 200 6 -3- 5 Tabl e 3- 4 Emission Result

s forSV M Metals and Mercur y 3- 6 Tabl e 3- 5 Summar

y o fTarge t Metals 3- 7 Tabl e 3- 6 Emission Result

s forParticulat

e Matte r - Ma y 200 6 3- 8 Tabl e 3- 7 Emission Result

s forParticulat

e Matter-Jun e 200

6 3- 9

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x200 6 Tes t Repoitdoc



## VE S

## ENS R



# 1. 0 Introductio n
1. 1 Progra m Summary ENS R wa s retaine d b yVeoli a E S Technica l Solutions (Veolia) , formerl y Ony xEnvironmenta

l Service s t o conduc t stack ga s emission sampling during the week s o fMa y8,2006 an

d June 19 , 2006 . Th e sampling wa

s performe

d o n th e Fixe d Heart h Hazardous Wast

e Incinerato

r Uni t 3 a t thei r facilit y i n Sauge

t Illinois. Th e purpos

e o fthi s Performanc

e Tes t wa s t o evaluat e the performanc

e o f th e incinerato

r relativ e t o th e emission

s standard

s forexisting incinerator

s found i n 4

0 CF R Par

t 63 , Subpar t EE E (th e HW C MAC Tregulations). T

o this end , th

e specifi c objective

s o fthis Perfonnanc

e Tes t wer e t o demonstrat

e emissions o

fth e followin g pollutants :

•Mercur

y •Lo wVolatile Metals (arsenic, beryllium , an d chromium ) •Semi-volatil

e Metal s (lea d an d cadmium

)
•Dioxin

s an d Furans •Particulat

e Matte r Th e Performanc

e Tes t include d feedin g certai n type

s o fwaste s and material

s int o th e incinerator

, sampling and analyzing thes e feedstreams, monitorin g certai n proces

s parameter

s whil e concurrentl

y conducting emission

s testing . Th e result

s fro m this testing indicat

e tha t emissions forthe abov

e pollutant

s me t the emission standard s forth e HW C MAC Tregulations. A summar y o fth e tes t result s can b e found i n Section 3 o fthis report

.

C:\Oocumenl s and Settina^^woodvorcALoca J SettngsNTemporai

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## 1- 1 September200 6

## ENS R



# 2. 0 Incinerator Process Descriptio n -
2. 1 Proces s Overview Veoli a operate

s 2 Fixe d Heart h Dual Chambere

d Incinerator

s (Unit s 2 and 3 ) and on e rotar y kil n (Uni t 4 ) a t th e Sauge t I L facility

. Th e tw o fixe d heart h unit s ar e rate d a t 1 6 millio

n Btu/h reach . Incineratio

n Uni t No . 3 i s a mirro

r imag e o fUni t No . 2 . Bot

h o fthes e unit s hav e thei r ow

n wast e handlin g systems as describe d i n th e sections tha

t follow . Th e onl y differenc

e being Uni

t No . 2 i s equippe d wit h fou r(4 ) baghous

e modules, whil

e Uni t No . 3 is equippe

d wit h thre e (3 ) baghous

e modules. Uni

t 4 is rate d a t 5 0 millio n Btu/h rand i s equippe

d wit h it s ow n tan k far m system , dru m storage, bul k

solids storag

e and fee d systems . 2. 2 Wast e Fee d System s [4 0 CF R §63.1207(f)(1)(»i)(DKE ) an d (f)(1)(H)(C) ] Fixe d heart h incinerato

r no . 3 is designe

d t o receiv e containers, aqueous liqui d wastes ; organic liquid waste

s fe d through air-atomizing nozzles , specialt y liquid feed s and direc

t injec t liquid s fe d throug h th

e aqueous ororganic liqui d fee d systems . Thi s uni

t can receiv

e an y combinatio

n o f waste s - liquid , semi-solid , o

rsolid - wit

h a hea t valu e o fu p t o 1 6 millio

n Btu/hr . Eac h o fth e fixe d heart h incinerator

s ar e supporte

d b y storage/blend tank

s locate d i n Tan k

Far m #1 . Rate s o ffee d ar e controlle

d a t eac h incinerator

. Segregate

d liquid waste

s ar e store d unti l utilize

d i n th e wast e blending facilities . A

t tha t time, liquid

s ar e delivere d t o the blendin

g tank s wher e th e dail y liqui d fee d t o the incinerato

r is formulated , tested , and release d t o the incinerator

. Blending o

f store d liquid waste

s to achiev

e optimum heating valu

e an d viscosit y forincineratio

n take s plac e i n Tank s 2,4, 6 & 8 . Sixadditional tank s (10,20,30,40,5 0 & 60 ) ar e use d t o segregat

e differen t wast e stream type

s for . blending o

fliquid fee

d t o th e incinerator

. Severa l criteria ar

e importan

t i n designing a blend fro

m available waste

s tha t hav e been segregate

d principall

y b yphysical and chemical properties. Thes e includ e compatibility

, prope rrang e o fheating value, and permi t restriction s regarding elemental compositio n (base d on emission Hmitations) . I n complianc

e wit h th e Benzene NESHAP , al l tank s ar e vente d to individua

l carbon adsorption canister s forremova

l o forganic s befor e vapori s discharge

d t o th e atmosphere

. Eac h carbon adsorbercanisteri s essentiall y equivalen

t t o a 5 5 gallon containe

ro rgreater

, i fnecessary. Al l tank

s ar e equippe

d wit h conservation vents , i n addition t o th e carbon canisteradsorber . Al l tank s ar e grounded , and flam

e arrestor s ar e installe d betwee n th e carbon adsorber

s and th e tanks . 2. 3 Manufacturer , Mak e an d Mode l ofth e Incinerato r [40 CF R §63.1207(f)( 1 )(iii)(A)] Incinerato r uni t no . 3 feature

s a two-stag

e combustio

n process . Ignitio

n o fwast e materia l take s plac e i n th e primar y (lower ) combustio

n chamber

. A secondar

y (upper ) combustio

n chambe

rserve s a s an "after-burner" forproces s gases . Ignitio

n o fth e wast e take s plac e a t temperature

s i n exces

s o f1,60 0 degree s F . Th e secondar

y combustio

n chambe

rmaintain

s a minimum temperatur e o f 1,80 0 degree s F . Thes

e temperature

s ar e presente

d in curren

t operating conditions. Th e Serie

s 2 incinerato

r ha s a total o

ftw o burners, on

e bumer , a Nort h America

n burner , rate d a t 12. 0 million Btu/hr. , i s use

d i n th e lowe r chambe rt o maintai n temperatures. I t wil l bu m onl

y natura l ga s orNo . 2 fue l oil . A second bume ris mounte

d i n th e uppe rchamber ; i

t to o wil l b e use d t o suppl y additional hea

t and wil l b

e fuele d wit h natura l ga s or# 2 fuel oil . Thi s burne

r is a Nort

h America

n

C:\Document

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x200 6 Tes t Report.do c 

## 2- 1 Septembe r 200 6

## ENS R Burner , rate d a t 6. 0 million Btu/hr

. Liquid o rgaseous waste

s ar e injecte d throug h separat

e feed nozzle s a s describe

d i n section 2.2 , above. Th e primar

y an d secondar

y chamber

s hav e an external diamete

r o f9 feet, and ar

e 17. 5 fee t long . Th e interio

r wall s o fbot h chamber

s ar e line d wit h approximatel

y 1 0 inche

s o fbrick refractor y an d insulatio n backing , making the interna l operating diamete

r approximatel

y 72" . Th e cross^sectional are a o fth e chamber

s i s thu s 40.3 squar

e feet. Combustio

n ai ri s controlle

d separatel

y i n th e uppe r and lowe r chambers. Followin g ignitio n o fth e wast e materia l unde rcontrolle d o rstarved-ai r condition

s i n th e lowe r chamber , off-gase s trave l through a refractory-line d flue ga s passage int

o the uppe

rchamber

, whic h act s a s an afterburner

. Turbulenc

e is achieve

d b y th e tangential introductio

n o fai ran d additional fue l i n th e uppe rchamber

. Ga s temperature

s ar e normall y maintaine

d a t 1,800-2,20

0 degree s F i n th e uppe rchambe rand 1500-190

0 degree s F i n th e lowe r chamber

, pursuan t to curren

t Illinoi s EP A permi t operating conditions. Leaving th

e uppe rchamber

, th e ho t ga s strea m travels throug h 2

8 fee t o frefractory-line

d stac k sections befor

e reaching the star

t o fth e ga s scrubbin

g system . Th e combine

d volum e o fth e uppe r and lowe r chambers, the flue ga

s passag e and th e ho t crossoversectio n i s approximatel y 1,56 7 cubic feet. Th e total retentio n tim e o fcombustio

n gase s within th

e system i s approximatel y 5 seconds . Th e incinerato

r i s rate d a t 1 6 millio n Btu/hr. , wit

h a desig n uni

t hea t releas e o f approximatel

y 10,00 0 Bt u percubic foo

t Maximum ga

s volum e whe n firing a hea

t releas e o f1 6 millio n Btu/hr . is abou t 15,00 0 acf m a t 40 0 degree s F . 2. 4 Ai rPollutio n Contro l Equipmen t [4 0 CF R §63.1207(f)( 1 )(iii)(G)] Th e ai rpollutio

n control syste

m consist s o fa spra y drye r absorbe ran d fabric filter baghouse. Th e ai rpollutio

n contro l system neutralize

s acidi c compound

s and remove

s particulat

e fro m th e exhaus t gas . Tw o subsystems, the spra

y drye r absorbe rand th e fabric filter

, carr y ou t the chemical neutralizatio

n an d particulat

e remova l functions, respectively

. A thir d subsystem , th

e lim e system , is use d t o prepar e an d provid

e lim e slurr y t o th e spra y drye r absorberfor us

e i n the chemical neutralizatio

n process . Th e induce

d draf t fa n an d stack provid e th e mechanical energ

y require d t o transpor t th e flu e ga s throug h th

e interconnectin

g ductwork

, t o it s eventual discharg

e poin t t o atmosphere

. 2.4. 1 Lim e Syste m Th e lim e syste m prepare

s lim e slurr y forus e i n th e chemical neutralization proces s i n sufficien

t suppl y and concentratio

n t o maintai n continuou

s flu e ga s treatmen

t i n the spra

y drye r absorber

. The syste m ha s been designe

d forbatc h mixin g t o provid e this service . Hydrate d lim e is store d i n a storag

e bi n abov

e th e lim e preparatio

n area . The storag

e bi n i s sized t

o hol d enoug h hydrate

d lim e t o maintai n several day

s o fsyste m operation atth e maximum combustio

n rat e o fth e incinerator

. Lim e i s discharge

d through the conica l storag e bi n bottom . Th e flo wofth e materia

l fro m th e bi n is aide

d b ya vibrating live bottom, " o rbi n activator

. A variable spee d rotar y feeder i s use

d t o mete r th e hydrate d lim e i n th e proportion

s require d forbatch mixin

g lim e slurry . The lim e i s mixe d wit h wate r i n a tan k

beneat h th e lim e storag e bin . Th e rotar

y feeder spee d and th e rat e tha t wate r is adde d t o th e lim e slurr y tan k ar e variable s

o tha t the desire

d 20 % lim e solids concentratio

n can b e achieve d i n th e tank . Th e variable feed adjustment s allo wwate r and lim e t o b e adde d t o th e lim e slurr y tan k a t a rat e tha t wil l allo wa batch mod

e o fmixing . A n agitato r i s provide

d i n the slurr

y tan k t o mi xth e wate r an d lim e and t o maintai n th

e suspensio n o

f

C:\Document

s and SetlingsVwoodwanftLoca l Set6ngs\Temporar

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x200 6 Tes t Repondo c 

## 2- 2 Septembe r 200 6

## ENS R lim e solids . Th e mixe

d lim e slurr y i s pumpe

d a t a continuou

s rat e o fflo wthroug h a recirculatio

n loo p t o the atomizer

. 2.4.2 Spra

y Dr y Absorbe r Slurr y flowt o th e spra y drye r absorberi s metere

d b y a flo wcontrol valv

e t o obtai n th

e prope rfee d concentration t

o th e spra y drye r absorberatomizer

. Automati

c (o r manual ) adjustmen

t t o th e flo wi s mad e as a functio

n o fth e outpu t fro m a hydrochloric aci d (HCI ) analyzer i n th

e gas duc

t downstrea

m o fth e Fabri c filter

. Th e amoun

t o fslurr y metere d i s proportiona

l t o the amoun

t o fHC I monitored . Th e slurr y passe s throug h a stationar

y swirl-typ

e liquid distributo

r int o th e atomize

r whee l wher e induce d centrifuga

l forc e fro m th e rapidl y spinning whee

l discharge

s th e slurr y throug h th

e whee l nozzle s a t hig h velocity

. Th e desig n o

fth e atomize

r wheel , it

s rat e o fspin , an d the discharg

e velocit y o fth e slurry , creat e a cloud o

ffinel y divide d droplet s around th

e peripher

y o fth e atomize

r wheel . A feedback

signa l fro

m the atomize

r powe r transmitte

r provide s verification tha

t wate r flo wto th e atomize

r increase s o rdecrease

s i n proportio

n t o th e spra y drye r absorbe routle t temperature

. Flue gas enter

s fro m th e botto m o fthe spra

y drye r absorberthroug h a vertical , centrall y locate d disperser. Th e disperse

rdirect s th e flue ga s through the zone fille

d b y th e atomize

d slurr y cloud wher e th e flue ga s an d slurr

y mix , an d mos

t o fth e absorptio

n occurs . The spra y drye r absorbe rfeature s a two-poin

t produc t discharge. A portio

n o fthe drie d spen t chemicals and ash settl

e t o th e botto m o fth e chamber

. Thi s material i s discharge d a t th e bas e o f th e powde r discharg

e cone . I t then passe

s throug h a lump breake r whic h reduce s larg e agglomeration

s o fmateria l t o a manageabl

e size . Finally, i

t is discharge

d throug h a rotar

y valv e to th e conveying system . The remainde r ofth e spen

t chemicals i s carrie

d fro m the modul

e entraine

d i n th e flu e gas . 2.4.3 Fabri c Filte r Ga s exhauste

d fro m the spra

y drye r absorberis distribute

d b y manifol d duct s t o thre e fabric filte

r module s a t Uni t 3 . Withi n each filter module , th e ga s i s passe

d throug h Teflon-coate

d fiberglas

s clot h bags . Th e ga

s passe s fro m th e outsid e t o the insid

e o fth e filterbags . Particulate, entraine d i n th e gas stream , is mechanicall y deposite

d on th e outsid e o fthe filter bag

s as th e ga s passe s throug h th

e cloth . Th e fabri c filte

r cleaning mechanis

m utilize s jet s o fai r t o clean the filter bags . Periodically , th e cleanin g sequenc

e wil l b e initiated . Th e sequenc e i s eithe r starte d a t th e end o fa time d cycle , o r whe n th e differentia

l pressur e acros s th e filte r reache s a predetermine

d setpoin t o fapproximatel

y 7.0" w.c . Th e controlle

rthe n sequence

s t o eac h ro

wo ffilte r bag s i n each module, releasing a burs t o fai r opposit

e t o th e directio n o fga s flow . Th e quickl

y release d burs t o fai r dislodge

s dus t cak e o n th e exterio r o feach ba g a s i t travels fro

m th e to p t o th e botto m o fthe bags . Release

d fro m th e bag , th e dus t cak e fall s b y gravit y int o th e hoppe ra t th e botto m o fth e module . The dus t cleane d fro m th e filte r bags i s remove

d a t th e bas e o fth e hoppe rthroug h a rotar

y valv e fo r discharg e t o th e conveying system . Treate d b y th e spra y drye r absorberand filtere

d b y th e fabri c filter , the cleane

d flue ga s exit s th e fabric filter module

s t o an outle

t manifol d for exhaust

. 2.4.4 Induce

d Draf t Fa n an d Stac k The induce

d draf t fa n and stack

ar e locate d downstrea

m o fth e fabric filter

. Combustio

n gase s ar e draw n through th

e syste m b y a 7 5 hp induce

d draf t (ID ) fan , rate

d a t 15,00 0 acf m a t 400 ° F saturated , and 22" wate r colum n pressure . The induce d draf t fan provide

s th e mechanis

m for

C:\Document

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x20O B Tes t Reportdoc 

## 2- 3 Septembe r 200 6

## ENS R transporting th

e incinerato

r flu e ga s throug h the spra

y drye r absorber, Fabri c filter, and al l interconnecting ducts. The velocit y o fth e ga s withi n th

e ducting an d treatmen

t device s i s regulate

d b y the dampe

rassociate

d wit h th e fan . Treate

d gasse s exhauste

d fro m the induce

d draf t fa n to th e atmospher

e through a 90-ft

. high stack

. Th e stack

diamete r for Uni t 3 i s 39 inche

s I.D . Th e stack

i s equippe d wit h instrumen

t sampling port

s and a samplin

g platfor m fo r emissions testing . Appendi xD provide s details o

n th e desig n and sample por t location s and configuration

s for Uni t 3 .

C:\Docunent

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6 Tes t Remtdo c 

## 2- 4 Septembe r 200 6

# 3.0 Summar y o fResult s ENS R

3. 1 Introductio n Thi s section summarize

s th e tes t progra m results. Appendi

xB present

s copie s o fENSR' s fiel d dat

a an d calculations. Emission dat a i s summarize

d i n this section and fee d an d proces

s operating dat

a ar e include d i n Appendi

xA . 3. 2 Stac k

Emissio n Result s fo rPCDDs/PCDF s Metho d 0023 A require d separat e analysi s o

fth e front-hal

fand back-hal

fsample trai n fractions . Progra m sample

s wer e submitte

d t o Att a Analytical Laboratorie

s i n E l Dorado Hills , CA foral l analysi s o

fal l targe t parameters. A summar y o fthe PCDD/PCD F emission result s on a TE Q basi s forUni t 3 ar e include d i n Tabl e 3-1 .
•Th e PCDD/PCD F emissions forUni t 3 (averag

e emissions fo rrun

s 1, 2 and 3 wer

e 0.02 4 ng/m 3

## @ 7

% O2 ) ar e belo wthe HW

C MAC Temission standar

d o f0.2 ng/m 3

## @ 7

% Oz . 3. 3 Stac k

Emissio n Result s fo rTarget Metal s an d Particulat e Matte r A summar

y o fth e metal s an d particulat

e matte r emissions forUni

t 3 is include

d i n Table

s 3- 2 throug h 3-7 . Table

s 3- 2 and 3- 3 provid e a detaile

d summar

y o fthe Lo wVolatile Metals (LVM) emissions fro

m th e Ma y 200 6 and June 200

6 testing . A detaile

d summar

y o fmetals emissions categorize

d b ySemi-volatil

e Metals (SVM) an

d mercur y i s provide

d i n Tabl e 3-4 . Table 3-

5 provide s a summar

y o fal l si xtarge t metals. Table

s 3- 6 an d 3- 7 summariz

e th e particulat

e matte r emissions fro m th e Ma y 200 6 an d Jun e 200 6 testing .

. Th e LV M metal

s emission

s forUni t 3 fro m th e Ma y 200 6 testing (averag

e emissions fo rrun

s 1, 2 an d 3 wer

e 24 9 pg/m 3

## @ 7

% 0 2 

## fo r LVMs

) wer e highe rtha n th e HW C MAC Temission standard

s o f9 7 ug/m 3 

## ;

. Th e LVM metal

s emissions forUni

t 3 fro m the June 200

6 testing (averag

e emissions forrun

s 1 , 2 and 3 wer

e 7.6 1 ug/m 3

## @ 7

% O 2

## fo rLVMs

) wer e lowe r tha n the HW C MAC Temission standard s o f9 7 ug/m 3 

## ;

. Th e SV M and mercur y emissions forUni

t 3 (averag

e for run s 1, 2 and 3 wer

e 16. 6 pg/m 3

## @ 7

% 0 2 

## fo r SVM s and 61.5 pg/m 3

## @ 7%0 2 

## fo r mercury ) wer e belo wth e HW C MAC Temission standard s o fand 24 0 pg/m 3

## (correcte

d t o 7 % Oa ) and 13 0 pg/m 3

## @ 7

% 0 2 

## forSVM s an d mercur y respectively;

. Th e particulat

e matte r emissions forUni

t 3 fro m th e Ma y 200 6 testing (averag

e emissions for run s 1, 2 and 3 wer

e 6.3 9 mg/m 3

## @ 7

% 0 2 

## ) i s belo

wth e HWC MAC

Temission standar

d o f3 4 mg/m 3

## @ 7

% 0 2 

## ;

. Th e particulat

e matte r emissions forUni

t 3 fro m the June 200

6 testing (averag

e emissions for run s 1, 2 an d 3 wer e 2.6 6 mg/m 3

## @ 7

% 0 2 

## ) i s belo

wth e HWC MAC

Temission standar

d o f3 4 mg/m 3

## @ 7

% 0 2 

## .

C:\Document

s and Settings^oodvrardiLoca l Settings\.Temporar

y Inteme t Rtes\OUC7C\Oyx2006 Tes t Reoort-do

c 

## 3- 1 Septembe r 200 6

## ENS R
3. 4 Metal s Sampl e Contaminatio n During th e Ma y200 6 testing , hig h arseni c levels , whic h wer e inconsisten

t among the thre

e runs , wer e detecte d i n sampl

e result s fro m th e Metho d 2 9 train . A detaile

d revie wwa s conducte

d b ybot h ENS R and Veoli a personne l t o assess possible cause s and/orsource

s o fcros s contamination . Thi s revie wincluded :

•Sampl

e trai n clean-u p and preparatio n procedure

s •Sample por

t access an d preparatio

n forsampling •Sampling anomalie

s (i.e. , observation

s o ffilter , sampl e trai n an d procedures

) •Lab contaminatio

n o rincorrec t result s (duplicat

e sample s wer e analyze

d a t a separat

e laboratory

) •Operating o

requipmen

t issue s tha t coul d hav

e cause d non-representativ

e particulat

e matte r containing hig h arsenic t o b e collecte d i n th e sampl e trai n I t wa s conclude

d tha t ther e wa s crossrcontaminatio

n o fth e sampl e trai n during sampling tha t wa s mos t likel y cause d b ydislodgemen

t and re-entrainmen

t in th e flue ga s o fscal e tha

t ha d buil t u p o n th e insid e o fth e stack sampl e por t ove rtime, causin g a non-representativ e result. Also , during thi s revie wi t wa s determine

d tha t th e numbe ro ftravers e point s forth e port s use d forth e dioxi n an d furan sampling wa

s incorrec t base d on Metho

d 1 criteria, althoug h result s wer e wel l withi n th

e MAC Temission standards. A s a result , Uni t 3 wa s re-teste d i n June t

o furthe r evaluat e lo wvolatil e meta l and dioxi n and furan emissions performance

. Port s wer e cleane d priort o testing and th

e correc t numbe ro ftravers e point s wa s use d forth e selecte

d sampling locations . Dioxi n and furan result s wer e agai n wel l withi n th e emission standard . Lo

wvolatil e meta l result s wer e als o wel l within th

e emission standard .

C:\Oocument

s an d Settngs^woadoaroMocal SeWix}s\Ternporar

y Inteme t Files\OLK7aOny

x200 6 Tes t Reportdoc 

## 3- 2 September 200 6

## ENS R Tabl e 3- 1 PCD D /

PCD F Emissio n Results - TE Q Basi s

Ru n No . 

## Run 1 Ru n 2 Ru n 3 Dat e 19-JW1-0 6 20-JUT1-O 6 2i-jun-o 6 Star t Tim e 

## 14:4 0 09:3

0 09:3

0 StooTim e 

## 17:5 9 13:0

5 11:4

3 Units Sample Volume dsc f 128.36

3 129.71 0 126.37 9 Sample Volume m 3 

## 3.6 3 3.6

7 3.5

8 Moistur e Conten t %v/

v 44.4 47. 7 45. 6 0 2 

## Concentration %vyv(div ) 

## 10.0 0 8.2

0 9.6

0 C0 2

## Concentration %wMdrv ) 

## 7.4 0 7.6

0 7.4

0 Isokinetic s % 9 9 10

4 10

0 Stack Flowrat e dscf

m 5,44

1 5,21 2 5,28 0 PCDD/PCD F p g ng/m 3 

## p

g ng/m 3 

## p

g ng/m 3 

## Parameter

s TEF ' TE Q TE Q TE Q 2,3,7,8-TCD D 1.0 0 0.0

0 0.0E+0

0 3.4 4 

## 9.4E-0

4 0.0 0 

## O.OE+0

0 1,2,3,7,8-PeCD D 0.5 0 17.0 2.3E-0

3 17.6 2.4E-0

3 16. 7 2.3E-0

3 1,2,3,4,7,8-HxCD D 0.1 0 19. 1 5.3E-0 4 16.8 4.6E-0

4 14.6 4. 1 E-0

4 1,2,3,6,7,8-HxCD D 0.1 0 46. 1 1.3E-0 3 34. 7 9.4E-0

4 35.7 1.0E-0

3 1,2,3,7,8,9-HxCD D 0.1 0 37.0 1.0E-0 3 27. 1 7.4E-0

4 26.3 7.3E-0

4 1,2,3,4,6,7,8-HpCD D 0.0 1 19

0 5.2E-0

4 17 5 4.8E-04 156.0 4.4E-0 4 OCD D 0.00 1 24

7 6.8E-0

5 ! 17 5 4.8E-0

5 15 1 4.2E-05 2,3,7,8-TCD F 0.1 0 3 0 8.1 E-0

4 32. 8 8.9E-0

4 31.8 8.9E-0

4 1,2,3,7,8-PeCD F 0.0 5 3

6 4.9E-0

4 4 1 5.6E-0

4 4 1 5.7E-0

4 2,3,4,7,8-PeCD F 0.5 0 6

5 9.0E-0

3 7 0 9.6E-0

3 7 6 1.1E-0

2 1,2,3,4,7,8-HxCD F 0.1 0 3 6 9.9E-0

4 3 3 9.0E-0

4 3 8 1.1E-0

3 1,2,3,6,7,8-HxCD F 0.1 0 3 2 8.8E-0

4 3 2 8.6E-0

4 3 4 9.4E-0

4 2,3,4,6,7,8-HxCD F 0.1 0 4 4 1.2E-0

3 4 2 1.1E-0

3 4 5 1.3E-0

3 1,2,3,7,8,9-HxCD F 0.1 0 1 0 2.8E-0 4 1 2 3.2E-0

4 1 1 3. 1 E-0

4 1,2,3,4,6,7,8-HpCD F 0.0 1 7

8 2. 1 E-0

4 6 7 1.8E-0

4 7 1 2.0E-0

4 1,2,3,4,7,8,9-HpCD F 0.0 1 8 2.2E-0

5 5 1.4E-0

5 7 2.0E-0

5 OCD F 0.00 1 

# I 2

0 5.6E-0 6 1 5 4.0E-06 1 3 3.7E-0 6 Tota l TEQ s (ng/m 3



## ) s 

## 0.02 0 0.02

0 0.021 | Tota l TEQ s (ng/m 3

## @ 7 % 0 2 

## ) zz 

## 0.02 5 0.02

2 I 0.02

6 % o fStandard " 

## = 12 % 11 % j 13 % j

aU.S.EP A (1989

) Toxi c Equivalenc

y Facto r
6PCDD/PCD F Standar

d = 0.20 ng/dsc m @ 7

% O 2

C:\Document

s and SetSr^wood*ard\Loca ! 3- 3 September 200 6 SettngsYTemporar

y interne t FSe£JDLK7COny

x200 6 Tes t Reoortjdo

c



## VE S 0023 1

### Tabl e 3- 2 Emissio n Results lo rLV M Metal s - Ma y200 6
Ru n No . Ru n 1 Ru n 2 Ru n 3 Dat e 10-May-0 6 1O-May-0 6 11-May-0 6 

### Star t Time Unit s 10:0

8 15:0

0 115 5 Sto p Time 12:5 1 17:1 6 13:3 9 AVG S Sampling Parameter

s - Barometric Pressur

e in . H g 29.1 0 29.0 2 29.0

5 29.0

6 Volume Metere

d do

t 81.24

8 83.54

6 76.761 80.51 8 Sample Volum

e dsc

f 79.59

8 84.05

6 76.26

9 79.97

4 Moistur e %v/ v 43. 0 43. 6 44. 6 43. 7 0 2 

### a t Stac k %dry 12.4 0 9.4

0 10.0

0 10.6

0 Avg . Stac k

Temp . ° F 38 1 37

1 37

1 37

5 Stac k Flowrat e dscfm 5,57 6 5,69

1 5,08

8 5,451 I Isokinetic

s % 10 9 10

1 10

2 10

4 Arseni c (As

) — LV M Quantit y Collecte

d M

9 8.5

0 24

8 94

5 40

1 Stac k Cone . @ 7%0 2 

### ug/m 3 

### 6.1 4 12 6 55

7 23

0 Stac k Emission Rat

e Ib/h r 7.88E-0 5 2.22E-0

3 8.34E-0

3 3.55E-0

3 g/se c 9.92E-0

6 2.80E-0

4 1.05E-0

3 4.47E-0

4 BervUiu m (Bel - - LV M Quantit y Collecte

d M

S 0.1 0 0.1 0 0.1 0 0.1 0 Stac k Cone . @ 7

% 0 2 

### ug/m 3 

### 0.0 7 0.0

5 0.0

6 0.0

6 Stac k Emissio n Rat

e Ib/h r 9.27E-0 7 8.96E-0

7 8.82E-0

7 9.02E-0

7 g/sec 1.17E-0

7 1.13E-0

7 1.11E-0

7 0.0

0 Tota l Chromiu m TO ) - LV M Quantit y Collecte

d M

9 16.7 28. 0 54. 8 33.2 I Stac k

Cone . @ 7

% 0 2 

### pg/m 3 

### 12. 1 14. 2 32. 3 19. 5 | Stac k

Emissio n Rat

e lb/h r 1.55E-0 4 2.51 E-0

4 4.83E-0

4 2.96E-0

4 

# I g/sec 1.95E-0 5 3.16E-0

5 6.09E-0

5 0.0

0

C:\Docurnent

s an d Setfings\jwoodwardMjOCa l SetSngsVremporai

y Interne t RleslOUCZOOny

x200 6 Tes t Repottdo c 

### 3- 4

## ENS R Tabl e 3- 3 Emissio n Results fo rLV M Metal s - Jun e 200 8 Ru n No . Ru n 1 Ru n 2 Ru n 3 Dat e 19-Jun-0 6 2<KJun-0 6 21>Jun-0 6 

## Star t Tim e Unit

s 15:1 2 10:0 6 10:0

6 1 Sto p Tim e 17:2 9 12:2

9 12:4

4 AVG S Samplin g Parameter s — 

## Barometri c Pressur

e in . Hg 29.5

5 29.5

5 29.5

0 29.5

3 Volum e Metere d de

f 78.24

4 82.90

2 81.74

5 80.96

4 Sample Volum

e dsc

f 72.24

7 76.48

2 75.57

3 74.76

8 Moistur e %v/

v 46. 7 47. 8 45. 5 46. 7 O z

## a t Stack %dr y 10.0

0 8.2

0 9.6

0 9.2

7 Avg . Stack

Temp . ° F 38 6 38

8 38

6 38

7 Stac k Flowrat e dscf

m 4,73

0 4,91 5 5,11 4 4,92 0 I Isokinetic

s % 

## 10 4 10

6 10

1 10

4 1 Arseni c (As ) — 

## LV M Quantit y Collecte

d pg 5.5 3 3.6

9 5.2

0 4.81 Stack Cone . @ 7

% O z 

## pg/m 3 

## 3.4 4 1.8

6 2.9

8 2.7

6 Stack Emission Rat

e Ib/h r 4.79E-0 5 3.14E-0

5 4.65E-0

5 4.19E-0

5 g/sec 6.03E-0

6 3.95E-0

6 0.0

0 0.0

0 Berylliu m (Be)

— 

## LV M Quantit y Collecte

d p

g 0.0

0 0.087

0 0.0

0 0.029

0 Stack Cone . @ 7

% 0 2 

## pg/m 3 

## 0.0 0 0.043

9 0.0

0 0.014

6 Stac k Emission Rat

e Ib/h r 0.00E+0 0 7.39E-0

7 0.00E+0

0 2.46E-0

7 g/se c 0.00E+0

0 9.32E-0

8 O.OOE+O

O 3.11E-0

8 Tota l Chromiu m (Cr ) - 

## LV M Quantit y Collecte

d p

g 9.9

1 3.8

5 11.2 8.3 0 Stac k Cone . @ 7

% 0 2 

## pg/m 3 

## 6.1 7 1.9 4 6.4

0 4.8

4 Stac k Emission Rat

e Ib/hr 8.58E-0

5 3.27E-0

5 9.98E-0

5 7.28E-0

5 g/se c 1.08E-0

5 4.12E-0

6 1.26E-0

5 9.17E-0

6

C:\Document

5 and Setbngs\jwoodwartfLocal SettngsWemporai

y Inteme t FitesSOlK7CV3rry

x200 6 Tes t Reportdo c 

## 3- 5 Septembe r 200 6

## ENS R Tabl e 3- 4 Emissio n Result

s fo rSV M Metal s an d Mercur y Ru n No . Ru n 1 Ru n 2 Ru n 3 Dat e 10-May-o s 10-May-0 6 11-May-0 6 

## Star t Tim e Unit

s 10:0

8 15:0

0 11:2

5 Sto p Tim e 12:5 1 17:1 6 13:3 9 AVG S SamDiin e Parameter s — 

## Barometric Pressur

e in . 

## H g 29.1 0 29.0 2 29.0

5 29.0

6 Volum e Metere d de

f 81.24

8 83.54

6 76.761 80.51 8 Sample Volum

e dsc

f 79.59

8 84.05

6 76.26

9 79.97

4 Moisture ' %v/ v 43. 0 43.6 44. 6 43. 7 0 2 

## a t Stac k %dr y 12.4

0 9.4

0 10.0

0 10.6

0 Avg . Stack

Temp . ° F 38 1 37

1 37

1 37

5 Stac k Flowrat e dscf

m 5,57

6 5,69

1 5,08

8 5,451 Isokinetic s % 

## 10 9 10

1 10

2 10

4
Cadmiu m (Cd)

- 

## SV M Quantit y Collecte

d ug 0.3

4 1.0

4 2.4

2 1.2

7 Stac k Cone . @ 7

% 0 2 

## pg/m 3 

## 0.2

5 0.5

3 1.4

3 0.7

3 Stac k Emissio n Rat

e Ib/hr 3.15E-0

6 9.3 1 E-0 6 2.14E-0

5 1.13E-0

5 I g/sec 3.97E-0 7 1.17E-0

6 2.69E-0

6 0.0

0 1 Lead(Pb) » 

## SV M J Quantit

y Collecte

d M

9 21. 2 19. 6 37. 9 26. 2 j Stac k

Cone . @ 7

% 0 2 

## pg/m 3 

## 15.3 9.9 22. 3 15. 9 Stac k Emissio n Rat

e Ib/hr 1.96E-0

4 1.76E-0

4 3.34E-0

4 2.35E-0

4 g/se c 2.47E-0

5 2.2 1 E-0 5 4.21 E-0

5 2.97E-0

5 Mercur y (Ha

) - 

## V M Quantit y Collecte

d pg 97. 3 12 1 89.4 .10 3 Stack Cone . @ 7

% 0 2 

## pg/m 3 

## 70. 3 61.5 52. 7 61. 5 Stack Emissio n Rat

e Ib/hr 9.0

1 E-0 4 1.09E-0

3 7.88E-0

4 9.25E-0

4 g/se c 1.14E-0

4 1.37E-0

4 9.93E-0

5 1.17E-0

4

C.ADocumerf

c and Setb'ng^\jwoodward\Loca l SetbngsVremporai

y Interne t RIes\OLK7CV0nyx200

6 Tes t Reportdoc 

## 3- 6 September200 6

### ENS R Tabl e 3- 5 Summar

y of Targe

t Metal s Lo wVolatil e Metal s Emission s - micrograms/m 3



### Ma y 200 6 Test Metal s As Be C r Tota l LV M Run 1 6.1 4 0.0 7 12.0 5 18. 3 Ru n 2 12 6 0.0 5 14.2 14 0 Ru n 3 55 7 0.0 6 32. 3 589 Averag e

23 0 0.0 6 19.5 24 9 Jun e 200

6 Test Metal s As Be C r Tota l LV M Ru n 1 3.4 0.0 0 6.1 7 9.6 1 Ru n 2

1. 9 0.0 4 1.9 4 3.8 5 Ru n 3 2.9 8 0.0 0 6.4 0 9.3 8 Averag e

2.8 0.0 1 4.8 4 7.6 1 LVM Regulator

y Standar

d = 9 7 micrograms/m3 

### Semi-Volatil e I

V eta l E m ssion s - micrograms/m 3


### Metal s P b C d Tota l SV M Run 1 15.3 0.2 5 15.6 Ru n 2

9.9 0.5 3 10. 5 Ru n 3 22. 3 1.4 3 23. 8 Averag e

15.9 0.7 3 16.6 SV M Regulator

y Standar

d = 24 0 micrograms/m 3 

### Mercur y Emission s - micr o 

## zramsfm3 

### Metal s 

# 1 H a Run l 70.3 Ru n 2

61.5 Ru n 3

52.7 Averag e

61. 5 1 Mercur y Regulator

y Standar

d = 13 0 micrograms/m3

C:\Document

s and Settings*jwoodwar<flUca I 3- 7 September 200 6 SetfingsXTentporai

y Interne t Rtes\QLK7O0ny

x200 6 Tes t Reportdoc


## VE S

## ENS R Tabl e 3- 6 Emissio n Results fo rParticulat e Matter - Ma

y 200 6 Ru n No . Ru n 1 Ru n 2 Ru n 3 Dat e 10-May-os 10-May-0 6 11-May-0 6 

### Star t Time Unit s 10:0

8 15:0

0 11:2

5 Sto p Time 12:5 1 17:1 6 13:3 9 AVG S SamDlin a Parameter

s — Barometric Pressur

e in . H g 29.1 0 29.0 2 29.0

5 29.0

6 Volum e Metere d de l 81.99 1 84.12 8 81.69

9 82.60

6 Volum e o fGas Collecte

d dsc f 79.526 83.46 2 80.40

2 81.13

0 Moistur e %v/ v 44. 4 44.8 44. 1 44.4 0 2 

### a t Stac k %dry 12.5 0 9.4

0 10.0

0 10.6

3 CO 2 a t Stac k %dry 6.4 0 6.8

0 7.0

0 6.7

3 Avg . Stack

Temp . ° F 37 6 36

6 36

4 36

9 Stac k Flowrat e dscfm 5,46 8 5,48

3 5,28

7 5,41 3 Isokinetic s % 

### 10 9 10

0 10

0 10

3 Particulat

e Emissio n Result s - 8 Fron t Hal fRins e 9 0.0031 0.006 6 0.005

8 0.005

2 Particulat e Filter 9 0.003 0 0.008

1 0.007

1 0.0061 Tota l Particulat

e m g 6.1 0 14. 7 12.9 11.2 P M Loadin g @ 7

% O a 

### mg/dsc m 4.4 6 7.5

1 7.21 6.3 9 Grai n Loadin g gr/dsc f 0.001 2 0.002 7 0.002

5 0.0021 Grai n Loadin g @ 7

% 0 2 

### .gr/dsc f 0.001 9 0.003 3 0.0031 0.002 8

aParticulat

e Matte r Standar d = 3 4 mg/dsc m @ 7

% O z

C:\Document

s and SetSrtgs^woodwardMjoca ! SeffitigsWernporai

y Inteme t RlesNrXK7C\Qny

x200 6 Tes t Report-do c 

## 3- 8 Septembe r200 6

## ENS R Tabl e 3- 7 Emissio n Result

s fo r Particulat

e Matter - Jun e 200

6 Ru n No . Ru n 1 Ru n 2 Ru n 3 Dat e IWun-0 6 2O-Jun-0 6 21-Jun-0 6 

## Star t Time Unit s 15:1 2 10:0 6 10:0

6 Stop Time 17:2 9 12:2

9 12:4

4 AVG S Samolin e Parameter s - 

## Barometric Pressur

e in.H g 29.5 5 29.5

5 29.5

0 29.53 Volum e Metere d dc

f 78.24

4 82.90

2 81.74

5 80.96

4 Volum e o fGas Collecte

d dsc

f 72.24

7 76.48

2 75.57

3 74.76

8 Moistur e %vA / 

## 46. 7 47. 8 45.5 46. 7 O 2 a t Stac k %dr y 10.0

0 8.2

0 9.6

0 9.2

7 C0 2

## a t Stac k %dr y 7.4

0 7.6

0 7.4

0 7.4

7 Avg . Stac k

Temp . ° F 38 6 38

8 38

6 38

7 Stac k Flowrat e dscf m 4,73

0 4,91 5 5,11 4 4,920 Isokinetic s % 10 4 10

6 10

1 10

4 Particulat e Emissio n Result s - 

## Front Hal fRins e Q 

## 0.004 0 0.002

8 0.001 7 0. 0 Particulat e Filter g 0.002 2 0.001 7 0.001 6 0. 0 Tota l Particulat

e m

g 6.2

0 4.4

6 3.2

5 4.6

4 J P M Loadin g @7%0 2 

## mg/dscm 3.8 6 2.2

5 1.8

7 2.6

6 1 Grai n Loadin g gr/dsc f 0.001 3 0.00O90 

## 0.0006 6 0.001 0 I Grai n Loadin g @7%0 2 

## gr/dsc f 0.001 7 0.001 0 0.000 8 0.001 2

* Particulat e Matte r Standar d = 3 4 mg/dsc m @ 7 % Q z

C:\Document

s an d SeMngs\fwoodwafdlLoca l SetfingsVTemporai

y Inteme l ResCLKTOOnyx2006Te a Reportdo c 

## 3- 9 September 200 6

# 4.0 Samplin g an d Analytica l Procedure s ENS R

4. 1 Samplin g Procedure s Severa l differen

t sampling an d monitorin g technique

s wer e use d t o provid e th e require d dat a t o mee t the goals o

fthis tes t program . Thre

e (3 ) run s eac h wer

e conducte

d on Uni t 3 fo rEP A Metho

d 0023A , EPA Metho

d 29 , an d EP A Metho

d 5 . Th e sampling activitje s describe

d belo wwer e conducte d durin g al l runs. Al l fiel d activitie s wer e documente

d i n accordanc

e wit h EP A accepte

d procedure

s and copie

s o fal l fiel d note

s and dat a sheet s ar e include d i n Appendi

xB o fthi s repor t 4.1. 1 Velocity , Moistur e an d Fixed Ga s Determination s Gas strea

m velocit y an d temperatur

e wer e determine

d i n conjunctio

n wit h eac h manua

l sampling method . A typ

e "S " pito t tub e connecte

d t o an incline

d wate r manomete

r wa s use d t o determin

e velocit y hea d o fth e flue ga s a t eac h duc

t travers e poin t a s specifie d i n EPA Referenc

e Metho d 2 . Th e temperatur

e profil e o fth e flu e ga s a t eac h duc

t travers e poin t wa s obtaine d b y taking reading

s wit h a thermocoupl

e an d pyromete

r concurren

t wit h the velocit

y hea d measurements. Moistur e conten t wa s determine

d a s specifie d i n EP A Metho

d 4 . Velocit

y and temperatur

e measuremen

t profile s wer e establishe

d prio rt o testing t

o ai d i n sampl

e trai n set-up . Sample

s fo rth e determinatio

n o fth e fixe d ga s compositio

n wer e collecte

d using th

e integrate

d ba g techniqu

e detaile d i n EPA Referenc e Metho d 3 . 4.1.2 PCDD/PCD F Samplin g Sampling fo

rdioxin s and furans wa

s complete

d i n accordanc

e wit h EP A Metho

d 23 A (4 0 CF R 60 , Appendi xA) . Eac h sampling ru n wa s 19 2 minute s i n duratio

n covering 1 6 sampling point s a t 1 2 minute s pe rpoint . 4.1. 3 Metal s an d Particulat e Samplin g Th e EP A Multipl

e Metals Trai n (EPA Metho d 29,4 0 CF R 6

0 Appendi

xA ) wa s utilize d durin g the testing progra

m forth e collection ofth e followin g metals : arsenic , beryllium , cadmium , chromium , lead , an d mercury

. Prio rt o metal s analyse

s th e tare d filter an d fron t hal facetone rinse wer

e analyze d gravimetricall

y forparticulat

e matte r i n accordanc

e wit h EP A R M 5 . Eac h run wa s 12 0 minute s i n duratio

n covering 1 6 sampling point s a t 7. 5 minute s perpoint

. 4. 2 Analytica l Procedure s 4.2. 1 PCDD/PCD F Analyse s PCDD/PCD F analyse

s wer e performe

d b yAlt a Analytical Laboratory

, Inc . i n E l Dorad

o Hills , CA . Sample fraction

s wer e extracted , concentrate d an d analyze

d b y EP A Metho

d 829 0 (High Resolution Ga

s Chromatograph /

Hig h Resolutio

n Mas s Spectrophotomete

r(HRGC/HRMS)) . Th e trai n fraction

s recovere

d foranalysi s o

fPCDDs/PCDFs includ

e th e fron t hal frinse , th e particulat

e filter , th e bac k hal frins e and the XA D resi n trap. Th e analytical result s forth e fron t hal fan d back hal ffraction s wer e analyze

d an d reporte

d separately

.

C:\Document

s an d Setings\woodvrar<?Loca l SetSngs\Tempotar

y Inteme t Files\OLK7CNOny

x200 6 Tes t ReporLdo

c 

## 4- 1 Septembe r 200 6

## ENS R 4.2.2 Metal s Analyses Metals analyse

s for th e wast e fee d sample s wer e complete

d usin g tw

o separat e procedures. Rrs t sample s wer e prepare

d and analyze

d forarsenic , beryllium , cadmium , chromium , and lea d as specifie d i n EP A Metho

d 602 0 (ICP-MS) , SW846,3" 1 

## Edition . Mercur y wa s analyze d vi a metho

d 7471A . Metals analyse

s wer e performe

d b y Maxxa m Analytical Inc

. o fBurlington , Ontari

o (Canada) . 4. 3 Proces s Operatin g Condition s Throughou

t th e fiel d program , detaile

d proces s informatio

n wa s collecte d continuousl

y b y th e facility' s proces s control computer

s an d dat a acquisition syste

m (DAS) . Proces

s dat a including minimum , maximum and averag e value s forke y proces s variable s recorde d during eac h tes

t condition . In general , target-operating condition s specifie d wer e achieved .

C:\Documenr

s an d Set6ngs\jwoodwai*LocaI SetfingsvTemporar

y Inteme t F9esVOLK7C\Ony

x200 6 Tes t Reportdoc 

## 4- 2 Septembe r 200 6

## ENS R



# 5. 0 Qualit

y Assurance
5. 1 Introductio n Thi s section present

s the result

s o fal l QA/Q C measure

s implemente

d during th

e fiel d sampling progra m an d al l phase

s o fsubsequen

t analysis . Dat

a generate

d forth e progra m ar e judge d t o b e vali d as overal l accurac

y an d precision result

s ar e consisten

t wit h general objectives. Analytical QA/Q C dat

a ar e presente

d t o suppor t al l sample result

s use d fordetermining complianc e wit h performanc

e criteria o remission standards . Throughou t th e overal l program , al l sampling wa s performe d using sampling protocols describe d herei n and approve

d b y USEP A and th

e Illinoi s Environmenta

l Protection Agency

. 5.1. 1 Pre-Samplin g Activities Pre-sampling activitie

s include d equipmen

t calibration , sample media preparation , cleanin g o f sampl e trai n glassware, preparation o fcomputer-generate

d sample labels and othe r miscellaneous tasks . Eac h o

fthes e activitie s ar e describe

d o rreference

d i n the followin

g subsections . Othe

r presampling activitie

s include d such detail s a

s tea m meetings, equipmen

t packing and shipment

, equipmen

t setup , and finalization o fal l details leadin g up t

o th e coordinate

d initiatio n o fthe samplin g program . 5.1. 2 Equipment Calibratio n A mos t importan

t aspec t o fpre-sampling preparation s wa s th e inspection and calibration o fal l equipmen

t use d forth e fiel d effort

. Equipmen

t wa s inspecte

d fo rprope

roperatio n and durabilit

y prio rt o calibration . Calibration o fequipmen

t wa s conducte

d i n accordanc

e wit h the procedure

s outline d i n th e EPA documen

t entitle d "Qualit y Assuranc

e Handboo

k forAi rPollutio

n Measuremen

t Systems ; Volum

e III—Stationar

y Sourc e Specifi c Methods " (EPA-600/4-77-027b) . Equipmen t calibration wa

s performe

d i n accordanc

e wit h EP A guideline

s and/or manufacturer'

s recommendations

. Copie s o fthese s calibrations ar

e presente

d i n Appendi

xC . Example

s o ffiel d equipmen

t use d and typical calibration requirement s follows :

•PROB E NOZZLE

S (Q A Handboo

k Section 3.4.2 , pg . 19

) - measurement

s o fth e nozzle I D (t

o the neares

t 0.00 1 -in. ) alon g thre

e differen t diameter

s wit h a micrometer

. Differenc

e betwee n th e hig h and lo

wvalue s shoul d no

t excee d 0.00 4 in . Post-tes

t check s - inspec t for damage . •PITO TTUBE S (Q A Handboo

k Section 3.1.2 , pp . 1-13

) - measure

d forappropriat

e spacin g an d dimension

s o rcalibrat e i n a win

d tunnel . Rejection criteria given on th e calibration shee

t Post-tes t check s - inspec

t for damage . •THERMOCOUPLE

S (Q A Handbook

Section 3.4.2 , pp. 15-18 ) - verif y agains t a mercury-in-glas

s thermomete

r a t tw o o rmor e point s including the anticipate d measuremen

t range. Acceptanc

e limit s - impinge

r±2°F ; DG M ±5.4°F ; stack ±1. 5 percen

t o fstack temperature. •DR YGA S METER S (Q A Handbook

Section 3.4.2 , pp . 1-12) - calibrat e agains t a we t tes t meter . Acceptanc

e criteria - pretes

t Y i = Y±0.2 ; pos

t tes t Y= ±0.0

5 Yi . •FIEL D BAROMETER

S (Q A Handbook

Section 3.4.2 , pp . 18-19 ) - compar

e agains t a mercury

in-glas s baromete

r o rus e Airpor t Station B P an d correc

t forelevation . Acceptanc e criteria - ±0.0 2 in . Hg ; post-tes

t check s - same .

C:\Document

s an d SeOingsVwoodwanHLoca l Settings\Temporar

y Interne t ReslOLK7C\Ony

x200 6 Tes t Reportdo c 

## 5- 1 September 200 6

## ENS R

5.1.3 Glasswar

e Preparatio n Sample trai n glasswar

e and sampl

e container

s require d specialize

d pre-cleanin g t

o avoid contaminatio

n o fth e sample fro

m th e collection containe

r ordevices . Cleaning/storag e procedure

s for sample trai n glasswar e ar e summarize

d below . Not e tha t al l bottl e cap s ar e fitte d wit h Teflon liners , whic

h wer e cleane d i n th e same manne

r as th e bottle s themselves . Sample container s use d fo r wast e fee d stream s ar e purchase

d pre-cleane

d and seale

d t o specifie d EP A protocols.

•EP A

## METHO

D 001 0 / 0023 A GLASSWAR

E AN D CONTAINER

S (PCDDS/PCDFS ) 

## - washe d wit h soa p an d water

, rinsed thre

e time s wit h deionize

d (Dl ) water , bake d a t 400° C fo

r 2-hours, rinsed thre

e times wit

h pesticid

e grad e methylen

e chloride, rinse

d thre e times wit

h pesticid

e grad e toluen e and ai rdry

.
•EP AMETHO

D 5729/006

0 GLASSWAR

E AN D CONTAINER

S (METAL S AN D PARTICULAT

E MATTER

)

- washe d wit h soap an

d water , rinse d wit h ho t tap wate

r an d rinsed thre

e times wit

h reagen t water . The glasswar

e wa s soake d i n a 10 % nitri c acid solution fora minimum o f4-hours , . rinsed thre

e time s wit h reagen t water , rinse d a final tim

e wit h aceton e and air-dried . Al l glasswar e opening

s wher e contaminatio

n ca n occur

ar e covere d wit h Parafil m unti l th

e sampling trai n wa

s assemble

d prio r t o sampling . 5.1.3. 1 Sampl e Medi a Preparatio n Al l reagent

s wer e checke d i n accordanc

e wit h ENSR' s existing Q C Progra m t o minimiz

e th e probabilit y o fusing contaminate

d solvents . Thi s include d th e us e o fth e prope rgrad e reagents/solvent

s as specifie

d i n th e tes t method , selection o

freagent s fro m the sam

e lo t an d collection and analysis o fth e appropriat

e blanks . Sampling media wa s procure d and prepare

d i n accordanc

e wit h th e appropriat

e tes t method s a s describe

d below:

•XA D resi n use

d i n th e Metho d 0023 A trai n wa

s purchase

d ne wand packe

d i n speciall

y designe d sorben t traps. Al l glas

s cleanin g and sorben

t packing procedure

s followe d th e protocol s specifie d i n EP A Metho

d 0023A.
•Quart z filter s use d i n th e Metho d 5 / 29 / 006 0 sampling trai n wer

e supplie d b y Maxxa m Analytics , Inc. wh

o pre-screen filter

s fo rmetal s content .

C:\Document

s an d SettirxjsVwoooVarALocal SetSngsYTemporar

y inteme t RlesJQUCTOOny

x200 6 Tes t Reportdo c 

## 5- 2 September200 6

## ENS R



# Appendi xA Facilit y Operatin g Dat

a

September200 6 S:VJOa2006\Onyx\PeribrmanceTest\BeportV ^ Tes t Reportdo

c


## VE S 0023 2

### Uni t # 3 Run# l Date : 05/10/0

6 Tes t Time : 09:4

7 to 13:5 1 Ru n Length : 19

9 minutes PP M PP M PP M PP M Wast e Type Btu/l b %Chlorine %As h Mercur y Lead Cadmiu m Arseni c PC C Hig h Bt

u 682 0 0.

5 0.3 0.1 3 2.5 1 5 PC C Lo wBtu 50 0 0.

5 0.3

3 0.0

5 2.5 1 5 {Chlorin e Spike ) 50

0 85.

5 0. 1 0.1 3 2.5 1 

### 5 PC C S p Fd r 50 0 0.5 0. 1 0.0 5 2.5 1 5 (Chromiu m Spike

) 50

0 0.

5 23. 4 0.1 3 2.5 1 

### 1. 3 PC C Soli d Charge

s 50

0 0.5 81. 8 0.2 1 20. 1 1 & 6 (Lea d Spike ) 50 0 0.

5 66. 4 0.1 3 63000 0 20

8 6 (Chlorine Spike

) 50

0 63. 5 96. 3 0.1 3 2.5 1 

### 5 (Mercur y Spike ) 50

0 0.5 0. 1 60 0 2.5 1 

### 5
Total s

### Average Therma l Chlorine As h Mercur y Lea d P M PP M Feedrat e Loading Loadin g Loadin g Loadin g Loadin g Iliu m Chromiu m (Mvr) (MMBtu/hr; (Ib/hr ) (Ib/hr

) (Ib/hr

) (Ib/hr

) 0. 1 2.5 98 2 6.7

0 4.91 2.9

5 0.00012

8 0.0

0 0.1 2.5 171 5 0.8 6 8.5

8 5.6

6 0.00008

6 0.0

0 0.1 2.5 11 7 0.0 6 100.0

4 0.1 2 0.00001 5 0.0 0 0. 1 2.5 45 8 0.2

3 2.29 0.4

6 0.00002

3 0.0

0 0.1 18000

0 25

1 0.1 3 1.2

6 58.7

3 Q.00003

3 0.0

0 0.2 9 26. 1 61 9 0.3 1 3.1 0 506.3

4 0.00013

0 0.01 0. 1 2.5 9 2 0.0

5 0.4

6 61.0

9 0.00001 2 57.9

6 0.1 2.5 13 8 0.0

7 87.6

3 132.8

9 0.00001 8 0.0

0 0.1 2.5 1.3 5 0.0

0 0.0

1 0.0

0 0.00081 0 0.0

0
437 3 8.3

9 208.2

6 7685 4 0.0012

5 57.9

8

### Cadmiu m Arseni c Berylliu m Chromiu m Loadin g Loading Loading Loading (Ib/hr ) (lb/hr

) (Ib/hr

) (Ib/hr

) 0.0 0 0.0

0 0.0

0 0.0

0 0.0 0 0.0

1 0.0

0 0.0

0 0.0 0 0.0

0 0.0

0 0.0

0 0.0 0 0.0

0 0.0

0 0.0

0 0.0 0 0.0

0 0.0

0 

### 45.1 8 0.0 0 0.0

1 0.0

0 0.0

2 0.0 2 0.0

0 0.0

0 0.0

0 0.0 0 0.0

0 0.0

0 0.0

0 0.0 0 0.0

0 

### o.o

o 0.0

0
0.0 2 0.0

2 0.0

0 45.2

0

### Uni t # 3 Ru n # 2 Date : 05/10/0

6 Tes t Time : 14:5 1 t o 18:1 7 Ru n Length : 20

6 minutes PP M PP M PP M PP M Wast e Typ e Btu/l b %Chlorine %As h Mercur y Lead Cadmiu m Arseni c PC C Hig h Btu 672 0 0.5

6 0.2

8 0.1 3 2. 5 1 5 PC C Lo wBt u 50 0 0.

5 0.3

2 0.0

5 2. 5 1 5 (Chlorine Spike

) 50

0 85.

5 0.1 0.1 3 2. 5
" 1 

### 5 PC C S p Fd r 50 0 0.

5 0. 1 0.0

5 2.5 1 5 (Chromiu m Spike

) 50

0 0.

5 23. 4 0.1 3 2. 5 1 

### 2. 6 PC C Soli d Charges 50 0 0.5 8

2 0.1 9 19. 6 1 9. 5 (Lea d Spike ) 50 0 0.

5 66.4 0.1 3 63000 0 22

1 1.

6 (Chlorine Spike

) 50

0 63.5 96.3 0.1 3 2.5 1 5 (Mercur y Spike ) 50

0 0.

5 0.1 60

0 2. 5 1 

### 5
Total s

### PP M PP M Berylliu m Chromiu m Averag e Therma l Chlorine As h Mercur y Lead Feedrat e Loading Loadin g Loadin g Loadin g Loadin g (Ib/hr ) (MMBtu/hr

) (fo/hr ) (Ib/hr

) (Ib/hr

) (lb/hr

) 0.1 2. 5 99 2 6.6

7 5.5

6 2.7

8 0.00012

9 0.0

0 0.1 2.5 168 1 0.8

4 8.4

1 5.3

8 0.00008

4 0.0

0 0.1 2.5 10 0 0.0

5 85.5

0 0.1 0 0.00001 3 0.0 0 0.1 2.5 461 0.2 3 2.31 0.4

6 0.00002

3 0.0

0 0.1 18000

0 25

5 0.1 3 1.2

8 59.6

7 0.00003

3 0.0

0 0.4 3 28. 1 71 9 0.3 6 3.6

0 589.5

8 0.00013

7 .0.0 1 0. 1 2.5 10 8 0.0

5 0.5

4 71.71 0.00001 4 68.0 4 0.1 2.5 16 1 0.0

8 102.2

4 155.0

4 0.00002 1 0.0

0 0. 1 2.5 1.5 8 0.0

0 0.0

1 0.0

0 0.00094

8 0.0

0
447 9 8.4

1 209.4

2 884.7

2 0.0014

0 68.0

6



## VE S

### Cadmiu m Arseni c Berylliu m Chromiu m Loadin g Loadin g Loadin g Loadin g (lb/hr ) (Ib/hr

) (IWhr

) (Ib/hr

)
0.0 0 0.0 0 0.0 0 0.0 0
0.0 0 0.0 1 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0
0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 45.9 0
0.0 0 0.0 1 0.0 0 0.0 2 0.0 2 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 o.o o 0.0 0 0.0 0 0.0 0

0.0 3 0.0 2 0.0 0 45.9 3

### Unit # 3 Ru n # 3 Date : 05/11/0

6 Test Time : 11:2

5 t o 14:4

8 Ru n Length : 20

3 minutes PP M PP M PP M PP M Wast e Typ e Btu/l b %Chlorin e %As h Mercur y Lead Cadmiu m Arseni c PC C Hig h Bt

u 763 0 0.6

6 0.2

8 0.1 3 2.5 1 5 PC C Lo wBt u 50 0 0.5 0.31 0.0 5 2.5 1 5 (Chlorine Spike

) 50

0 85. 5 0. 1 0.1 3 2.5 1 

### 5 PC C S p Fd r 50 0 0.5 0. 1 0.0 5 2.5 1 5 (Chromiu m Spike

) 50

0 0. 5 23. 4 0.1 3 2. 5 1 

### 2 PC C Soli d Charge

s 50

0 0. 5 82. 6 0.3 5 36. 8 1 11 5 (Lea d Spike ) 50 0 0.5 66. 4 0.1 3 63000 0 28

3 9. 1 (Chlorine Spike

) 50

0 63.'

5 96. 3 0.1 3 15 0 1 5 (Mercur y Spike ) 50

0 0.5 0.1 60 0 2.5 1 

### 5
Total s

### Average Therma l Chlorine As h Mercur y Lea d
3 

### M PP M Feedrat e Loadin g Loadin g Loading Loadin g Loading Bu m Chromiu m (IWhr ) (MMBtu/hr

] (Ib/hr ) (Ib/hr

) (Ib/hr

) (Ib/hr

) 0. 1 2.5 100 0 7.6

3 6.6

0 2.8

0 0.00013

0 0.0

0 0. 1 2.5 1931 0.9 7 9.6

6 5.9

9 0.00009

7 0.0

0 0. 1 2.5 9 2 0.0

5 78.6

6 0.0

9 0.00001 2 0.0

0 0. 1 2.5 44 8 0.2

2 2.2

4 0.4

5 0.00002

2 0.0

0 0.1 - 18000

0 24

5 0.1 2 1.2

3 57.3

3 0.00003

2 0.0

0 0. 9 26.3 723 0.3 6 3.6

2 597.2

0 0.00025

3 0.0

3 0. 1 1.

3 10

6 0.0

5 0.5

3 70.3

8 0.00001 4 66.7

8 0. 1 2.5 15 8 0.0

8 100.3

3 1152.1 5 0.00002 1 0.0 2 0. 1 2. 5 1.5 5 0.0

0 0.0

1 0.0

0 0.00093

0 0.0

0
470 5 9.4B 202.8

6 886.3

9 0.0015 1 66.8

4

### Cadmiu m Arseni c Berylliu m Chromiu m Loadin g Loadin g Loading Loading (lb/hr ) (Ib/hr

) (Ib/hr

) (IWhr

) 0.0 0 0.0

1 0.0

0 0.0

0 0.0 0 0.0

1 0.0

0 0.0

0 0.0 0 0.0

0 0.0

0 0.0

0 0.0 0 0.0

0 0.0

0 0.0

0 0.0 0 0.0

0 0.0

0 44.1 0 0.0 0 0.0

1 0.0

0 0.0

2 0.0 3 0.0

0 0.0

0 0.0

0 0.0 0 0.0

0 0.0

0 0.0

0 0.0 0 0.0

0 0.0

0 0.0

0
0.0 3 0.0

3 0.0

0 44.1 3

### Uni t # 3 Run# 1 Date : 06/19/0

6 Tes t Time : 14:4

0 t o 18:0

5 Ru n Length : 20

5 minute

s PP M PP M PP M PP M Wast e Typ e Btu/l b %Chlorine %As h Mercur y Lead Cadmiu m Arseni c PC C Hig h Btu 993 0 3. 2 1. 5 0.41 3 18. 8 1.9 8 2. 5 PC C Lo wBtu 50 0 0. 5 0. 2 0.0202 15 7 0.0372 0.27 2 (Chlorine Spike

) 317 0 85. 5 0. 1 0.01 1 0. 1 0.0 2 02. PC C S p Fd r 50 0 0. 5 0. 1 0.0003 5 1.3 8 0.005 2 12. 1 (Chromiu m Spike

) 50 0 0. 5 25. 9 0.00 2 80 0 97 0 88 0 PC C Soli d Charges ea o 0. 6 70. 6 0.02 5 12.9 3 0.3 0 6.7 3 (Lea d Spike ) 50 0 0. 5 65. 6 0.0 2 63000 0 2 7 2 5 (Chlorine Spike

) 50 0 63. 5 97. 4 0.0 2 170 5 2 5 (Mercur y Spike ) 50 0 0. 5 0. 1 64 6 0. 1 0.02 0. 2
Total s

### Average Therma l Chlorine As h Mercur y Lead
J 

### P M PP M Feedrat e Loadin g Loadin g Loadin g Loadin g Loadin g /Iliu m Chromiu m (Ib/hr ) (MMBtu/hr

) (Ib/hr

) (Ib/hr

) (Ib/hr

) (Ib/hr

) 0.1 13.

3 111 0 11.0 2 35.5

2 16.6

5 0.00045

8 0.0

2 0.001 0.46

2 189

6 0.9

5 9.4

8 3.7

9 0.000038 0.0

0 0.0 5 0.0

4 9

5 0.3

0 81.2

3 0.1 0 0.000001 0.0 0 0.0 1 0.0121 56 9 05 8 2.8

5 0.5

7 0.00000

0 0.0

0 96 0 18000

0 251 0.1 3 1.2 6 65.0 1 0.000001 05 0 0.3 7 157.8

1 79

8 0.7

0 4.7

1 563.7

4 0.00002

0 0.0

1 4. 8 2 11 9 0.0 6 0.6

0 78.0

6 0.00000

2 74.9

7 2.5 2 17 9 0.0

9 113.6

7 174.3

5 0.00000

4 0.0

3 0.0 5 0.0

4 1.7

5 0.0

0 0.0

1 0.0

0 0.001131 0.0

0
501 9 13.5

3 249.3

0 902.2

7 0.0016

6 75.2

4



## VE S

### Cadmiu m Arseni c Berylliu m Chromiu m Loadin g Loadin g Loadin g Loadin g (lb/hr ) (Ib/hr

) (lb/hr

) (IWhr

) 0.0 0 0.0

0 0.0

0 0.0

1 0.0 0 0.0

0 0.0

0 0.0

0 0.0 0 0.0

0 0.0

0 0.0

0 0.0 0 0.0

1 0.0

0 0.0

0 0.2 4 0.2

2 0.2

4 45.1 8 0.0 0 0.0

1 0.0

0 0.1 3 0.0 0 0.0

0 0.0

0 0.0

0 0.0 0 0.0

0 0.0

0 0.0

0 0.0 0 0.0

0 0.0

0 0.0

0
0.2 5 0.2

4 0.2

4 45.3

2

### Uni t # 3 Ru n # 2 Date : 06/20/0

6 Tes t Time : 09:3

0 to 13:0

5 Ru n Length : 21 5 minutes PP M PP M PP M PP M Wast e Typ e Btu/l b %Chlorine %As h Mercur y Lea

d Cadmiu m Arseni c PC C Hig h Bt

u 900 0 2. 3 4. 9 0.41 3 4 0.3 5 2.5 PC C Lo wBt u (Chlorine Spike

) 50

0 317 0 0.5 85.5 0.2

0. 1 0.0019

2 0.01 4 0.0

4 0. 1 0.003

4 0.0 2 0.25

3 0. 2 PC C S p Fd r (Chromiu m Spike

) 50

0 50 0 0.

5 0.5 0. 1

25. 9 0.000

2 0.00 2 0.091 4 10 0 0.00

2 2 0 0.18

6 20 0 PC C Soli d Charge

s (Lea d Spike ) (Chlorine Spike

) (Mercur y Spike ) 82

4 50 0 50 0 50 0 0.6 0.5 63.5 0. 5 69. 9 65. 6 97.4 0. 1 0.03

8 0.0 2 0.0 2 64 6 16.4

5 63000 0 4 2 0. 1 0.3

7 3 2 5 0.0 2 6.2

5 2 5 2 5 0.2
Total s

### Average Therma l Chlorin e As h Mercur y Lea

d PP M PP M Feedrat e Loadin g Loadin g Loadin g Loadin g Loadin g Berylliu m Chromiu m (Ib/hr ) (MMBtu/hr

) (IWhr

) (Ib/hr

) (IWhr

) (Ib/hr

) 0. 1 1 3 112 6 10.1 3 25.9

0 55.1 7 0.00046

5 0.0

0 0.001 0.057

9 195

9 0.9

8 9.8

0 3.9

2 0.00000

4 0.0

0 0.0 5 0.04

6 10

2 0.3

2 87.21 0.1 0 0.000001 0.0 0 0.001 0.011 6 54 3 0.2

7 2.7

2 0.5

4 0.00000

0 0.0

0 50 18000

0 25

0 0.1 3 1.2

5 64.7

5 0.000001 0.0

3 0.31 11.8

8 80

5 0.6

6 4.9

6 563.01 0.00003

0 0.0

1 7. 8 2 11 7 0.0 6 0.5

9 76.7

5 0.00000

2 737 1 2. 5 2 17 6 ' 0.0

9 111.7

6 171.4

2 0.00000

4 0.0

1 0.0 5 0.0

4 1.7

2 0.0

0 0.0

1 0.0

0 0.00111 1 0.0

0
508 0 12.6

4 244.1 8 935.6

7 0.0016

2 73.7

6

### Cadmiu m Arseni c Berylliu m Chromiu m Loadin g Loadin g Loading Loadin g (Ib/hr ) (Ib/hr

) (Ib/hr

) (Ib/hr

) 0.0 0 0.0

0 0.0

0 0.0

1 0.0 0 0.0

0 0.0

0 0.0

0 0.0 0 0.0

0 0.0

0 0.0

0 0.0 0 0.0

0 0.0

0 0.0

0 0.01 . 0.0

5 0.0

1 45.0

0 0.0 0 0.0

1 0.0

0 0.0

1 0.0 0 0.0

0 0.0

0 0.0

0 0.0 0 0.0

0 0.0

0 0.0

0 0.0 0 0.0

0 0.0

0 0.0

0
0.0 1 0.0

7 0.0

1 45.0

2

### Uni t # 3 Ru n # 3 Date : 06/21/0

6 Test Time : 09:3

0 to 13:1 9 Ru n Length : 22

9 minute

s PP M PP M PP M PP M Wast e Typ e Btu/l b %Chlorine %As h Mercur y Lead Cadmiu m Arseni c PC C Hig h Btu 1022 0 3. 1 0.4 0.67 9 3.8

5 0.8

3 6.7

7 PC C Lo wBtu 50 0 0.5 0. 2 0.0018 4 0.0

4 0.005

4 0.25

7 (Chlorin e Spike ) 317

0 85.5 0. 1 0.004 5 0. 1 0.0

2 0.2 PC C S p Fd r 50 0 0.5 0. 1 0.000 2 0.043

2 0.00

2 0.070

9 (Chromiu m Spike

) 50

0 0. 5 25. 9 0.00 2 10

0 2

0 200 PC C Soli d Charge

s 79

3 0.5 70. 8 0.15 7 18.4

6 0.4

4 5.7

6 (Lea d Spike ) 50 0 0. 5 65. 6 0.0 2 63000

0 4

2 25 (Chlorin e Spike ) 50

0 63. 5 97. 4 0.0 2 1 8 5 25 (Mercur y Spike ) 50

0 0. 5 0. 1 64 6 0. 1 0.0

2 02.
Total s

### Average Therma l Chlorine As h Mercur y Lead PP M PP M Feedrat e Loadin g Loadin g Loadin g Loadin g Loading Berylliu m Chromiu m (Ib/hr ) (MMBtu/hr

) (Ib/hr

) (lb/hr

) (Ib/hr

) (Ib/hr

) 0. 1 5.7

4 107

9 11.0

3 33.4

5 4.3

2 0.00073

3 0.0

0 0.00 1 0.058

6 203

9 1.0

2 10.2

0 4.0

8 0.00000

4 0.0

0 0.0 5 0.0

4 9

6 0.3

0 62.0

8 0.1 0 0.00000

0 0.0

0 0.00 1 0.040

8 54

7 05 7 2.7

3 0.5

5 0.00000

0 0.0

0 50 18000

0 24

9 0.1 2 1.2

5 64.4

9 0.00000

0 0.0

2 0.3 5 12.4

7 81 5 0:6 5 4.31 577.2

9 0.00012

8 0.0

2 8. 1 2 11 9 0.0 6 0.6

0 78.0

6 0.000002 74.9

7 2. 5 2 17 8 0.0

9 113.0

3 173.3

7 0.000004 0.0

0 0.0 5 0.0

4 1.7

4 0.0

0 0.0

1 0.0

0 0.00112

4 0.0

0
512 4 13.5

5 247.6

5 902.2

5 0.0020

0 75.0

2



## VE S

### Cadmiu m Arseni c Berylliu m Chromiu m Loadin g Loadin g Loadin g Loadin g (Ib/hr ) (lb/hr

) (Ib/hr

) (Ib/hr

) 0.0 0 0.0

1 0.0

0 0.0

1 0.0 0 0.0

0 0.0

0 0.0

0 0.0 0 0.0

0 0.0

0 0.0

0 0.0 0 0.0

0 0.0

0 0.0

0 0.0 0 0.0

5 0.0

1 44.8

2 0.0 0 0.0

0 0.0

0 0.0

1 0.0 0 0.0

0 0.0

0 0.0

0 0.0 0 0.0

0 0.0

0 0.0

0 0.0 0 0.0

0 0.0

0 0.0

0
0.0 1 0.0

7 0.0

1 44.8

4

### Uni t 3 Operating.Parameter s June , 200 6

Ru n 

### 1 Ru n 

### 2 Ru n 

### 3 Averag e Baghous e Inle

t Temp . (De g F

) (Ave . o ftes t ru n ave.'s

) 42 0 42

1 42 1 42 0
PC C Temp . (Deg F

) (Ave . o ftes t ru n ave.'s

) 173 5 172

5 1741 173 4
SC C Temp . (Deg F

) (Ave . o ftes t ru n ave.'s

) 184 5 185

0 1851 184 9
Stackflo w(ACFM ) (Ave . o fmax . HRA' s o feac h tes

t run) 1488

8 1534

9 1526

7 1516

8 Pumpabl e Wast

e Fee d (Lb/hr

) (Ave . o fmax . HRA' s o

feac h tes

t run ) (Includes

average spiked

liquids flows) 414

7
346 

### 416

1
352 

### 417

2
345 

### 416

0
n a 

### Tota l Wast

e Fee d (Lb/hr

) (Ave . o fmax. HRA' s o

t eac h tes

t run) (Includes

average

spiked liquids

flows) 527

3
346 

### 536

7 35 2 

### 5391

345 

### 534

4
n a 

### Mercur y Fee d (Lb/hr

) (Ave . o ftes t ru n ave.'s

) 0.001 7 0.001 6 0.0020 0.001 8
As h Fee d (Lb/hr

) (Ave . o ftes t ru n ave.'s

) 90 2 93

6 90

2 91 3
LV M Fee d (Lb/hr

) (Ave. o ftes t ru n ave.'s

) 4 6 4

5 4

5 4

5
SV M Fee d (Lb/hr

) (Ave . o ftes t ru n ave.'s

) 75 ' 7 4 7

5 7

5
Chlorin e Feed (Lb/hr

) 24 9 24

4 24

8 24

7 (Ave. o ftes t ru n ave.'s

)



## VE S

### Uni t 3 Operatin g Parameter s May , 200 6

Ru n 

### 1
42 0
171 3
184 5
1487 3
371 8 368 471 7
368 0.001 3
76 8
4 5
5 8
20 8 

### Ru n 

### 2

42 0
171 5
184 5
1542 8
368 3
35 5 486 2 355 0.001 4
885
4 6
6 8
20 9 

### Ru n 3

42 0
171 2
184 6
1446 8
380 0
337 479 3
337 0.001 5
88 6
4 4
6 7
20 3 

### Averag e

42 0
171 3
1845
1492 3
373 4
n a 479 1
n a 0.001 4
846
4 5
6 4
20 7

## ENS R



# Appendi xB Referenc e Metho d Fiel d Dat

a an d Calculation s

September200 6 S*_JO^00aOny^ ^ Tes t Repor t Jo e 

## VE S 002 3

### M a y 200 6 Tes t



## VE S 0023 '

### Particulat e Matte r Dat a

VE S 0023 '

### Veoli a E S Technica l Solution s Fixed Heart

h Incinerator #

3 Metho d 5 Samplin g Parameter s 1 Ru n No . Ru n 1 Ru n 2 Ru n 3
AVG S Dat e 10-May-06 10-May0 6 11-May-0 6 AVG S Star t Tim e Unit s 10:0

8 15:0

0 11:2

5 AVG S Sto p Tim e 12:5 1 17:1 6 13:3 9 Nozzl e Diamete

r inche s 0.41 2 0.44 0 0.44

0 0.43

1 Barometric Pressur

e in . H g 29.1 0 29.0 2 29.0

5 29.0

6 Ne t Sampling Tim

e min . 120.0 120.0 120.0 120. 0 Volum e Metere d dc f 81.99

1 84.12

8 81.69

9 82.60

6 Avg . DG M Temp . ° F 85.9 72. 5 77. 1 78.5 Av g Delt a H inH z O 1.5 7 1.7

3 1.5

6 1.6

2 Av g Delt a H in.H g 0.115 8 0.127

4 0.114

6 0.119

3 DG M Calibration Facto r 

# - 1.027 0 1.027

0 1.O27

0 1.027

0 Ga s Sampl e Volum e dscf 79.52 6 83.46 2 80.40

2 81.13 0 Tota l Water Collecte

d m L 1344. 7 1438.

7 1343.

8 1375.

7 Volum e o fWater Vapo r sc f 63.40

3 67.83

5 63.36

0 64.86

6 1 Moistur

e (measured

) %v/

v 44.4 44. 8 44. 1 44. 4 Moistur e ( @ saturation

) %v/

v 102.

8 103.0 103.0 102. 9 Dr y Mol e Fraction . 100-%

M



# - 0.556 4 0.551 6 0.559 3 0.555

8 C0 2a t Stack %dt y 6.4

0 6.8

0 7.0

0 6.7

3 0 2 a t Stack %dr y 12.5

0 9.4

0 10.0

0 10.6

3 C O + N 2 %dr y 81.1 0 83.8 0 83.0

0 82.6

3 Dr y Molecula

r Weigh t Ib/lb-mol e 29.5 2 29.4

6 29.5

2 29.5

0 We t Molecular Weigh

t Ib/ltwnol e 24.4 1 24.3

2 24.4

4 24.3 9 Exces s Ai r a t Stack % 140.3 73.9 83. 9 99.4 Stack Diamete r inche s 39. 0 39.0 39. 0 39.0 Stack Are a sq . in . 1194.6 1194.6 1194. 6 1194.6 Static Pressur

e i n H z O 0.2 2 0.2

2 0.0

7 0.1 7 Stack Pressur e in.H g 29.1 2 29.0 4 29.0

6 29.0

7 Avg . Stac k

Temp . " F 376.4 366 5 364.3 369.0 I Avg . Sqroo

t o fDelt a P 

# - 0.412 5 0.414

5 6.394

6 0.407

2 SD E Averag

e 

# - . 11.93 1 11.91 5 11.33 0 11.72

5 Pito t Coefficien

t 

# - 0.8 4 0.8

4 0.8

4 0.8

4 Stac k Gas Velocit

y afp

m 1,92

8 1,93

2 1,83

2 1,89

7 Stack Flowrat e we t acfm 15,99

8 16,02

7 15,19

8 15,74

1 Stack Flowrat e we t scfm 9,82

7 9,94

0 9.45

3 9,74

0 Stac k Fiowrat e dscf m 5,46 8 5,48

3 5,28

7 5,41 3 isokinetics % 10 9 10 0 10 0 10 3 Meter Bo xNo . 

### _ 8061 0 8061 0 8061 0 — Delt a H @ inHji O 1.80 3 1.80

3 1.80

3 

# - • Fiel d Q A Yq c 

# - 1.046 5 1.059

1 1.037

5 1.047

7 [Deviation

] Pre- Y % 1.90 % 3.13

% 1.02

% 2.02

%

### Metho d 5 Samplin g Parameters Run l r 

### Ran 2 Ru n 3 P T Delt

a P SOR T DG M DG M Delt a H STAC K j Delt a P SOR T DG M DQ M Deli a H STAC K Delt a P SOR T DG M DQ M Delt a H STAC K Deli a P I N OU T TEM P Deli a P I N OU T TEM P Delt a P I N OU T TEM P a1 

### 0.1 5 0.387

3 7 0 7 0 1.3

8 34

6 0.1 8 0.424

3 7 6 7 5 1.9 0 37 0 0.1 3 0.360

6 7 0 6 9 1.3 0 35 0 a 2 

### 0.2 0 0.447

2 7 7 7 2 1.8

1 37

8 0.2

0 0.447

2 7 5 7 4 1.9 9 37 0 0.1 6 0.400

0 7 4 6 9 1.5 8 36 4 B 3 

### 0.2 0 0.447

2 8 2 7 4 1.8

1 37

8 0.2 1 0.458

3 7 6 7 3 2.0 9 36 8 0.1 7 0.412

3 7 7 7 0 1.6 8 36 9 a 4 

### 0.2 1 0.458

3 8 5 7 5 1.8

9 38

8 0.2

0 0.447

2 7 7 7 2 1.9 9 36 6 0.1 9 0.435

9 8 0 7 1 1.8 8 36 9 a S 

### 0.2 0 0.447

2 8 6 8 0 1.8

2 39

0 0.1 9 0.435

9 7 5 7 1 1.9 0 36 3 0.1 7 0.412

3 8 1 7 2 1.7 0 36 8 a 6 

### 0.1 8 0.424

3 9 0 8 2 1.6

6 37

4 0.1 9 0.435

9 7 1 6 9 1.9 0 36 4 0.1 6 0.400

0 8 2 7 3 1.6 0 36 2 a7 

### 0.1 5 0.387

3 9 2 8 2 1.3

8 37

5 0.1 5 0.387

3 7 6 6 9 1.5 0 36 2 0.1 6 0.400

0 8 3 7 4 1.6 0 36 4 a « 

### 0.1 1 0.331 7 9 3 8 3 1.0

2 37

4 0.1 1 0.331 7 7 6 6 9 1.1 0 36

3 0.1 4 0.374

2 8 3 7 5 1.4 0 36 5 b 1 

### 0.1 6 0.400

0 8 6 8 4 1.4

8 37

4 0.1 2 0.346

4 6 9 6 8 1.2 0 36 5 0.1 5 0.387

3 7 5 7 4 1.5 0 36 3 b 2 

### 0.1 8 0.424

3 9 3 8 5 1.6

7 37

7 0.1 6 0.400

0 7 4 6 8 1.6 0 36 5 0.1 7 0.412

3 8 0 7 5 1.7 0 36 6 b 3 

### 0.1 8 0.424

3 9 4 8 6 1.6

7 37

8 0.1 8 0.424

3 7 5 6 8 1.8 0 36 5 0.1 7 0.412

3 8 3 7 5 1.7 0 36 6 b 4 

### 0.1 6 0.400

0 9 6 8 8 1.4

8 37

9 0.1 8 0.424

3 7 6 6 9 1.8 0 36 6 0.1 7 0.412

3 8 4 7 6 1.7 0 36 5 b S 

### 0.1 8 0.424

3 9 6 8 8 1.6

6 37

9 0.1 8 0.424

3 7 5 6 8 1.8 0 36 4 0.1 6 0.400

0 8 4 7 6 1.6 0 36 5 b 6 

### 0.1 9 0.435

9 9 6 8 8 1.7

5 37

8 0.2

0 0.447

2 7 6 6 8 1.9 8 37 2 0.1 5 0.387

3 8 5 7 7 1.5 0 36 8 b 7 

### 0.1 5 0.387

3 9 7 9 0 1.3

9 37

8 0.1 8 0.424

3 7 7 6 8 1.7 8 37 2 0.1 3 0.360

6 8 2 7 7 1.3 0 36 4 b 8 

### 0.1 4 0.374

2 9 8 9 1 1.3

2 37

7 0.1 4 0.374

2 7 8 6 8 1.4 0 36 4 0.1 2 0.346

4 8 4 7 7 1.20 ' 36

1 ^•^lil: ! i-i l iii i ?:;;;; ! 1 '>• '• ' 

### AV G 0.1 7 0.412

5 85.9 -• : : • 

### 1.5 7 37

6 0.1 7 0.414

5 72. 5 1.7

3 36 6 0.1 6 0.394

6 77 A 1.5

6 36 4

< m co 

### o o r o o o -r > r n

# EN S MtCO M EP A ISOKINETI C SAMPUN G •FIEL D DAT A SHEE T
SAMPLIN G TRAIN : M5 / Paniculat e PLANT : ONY XEnvironmenta l DATE : 

### O5-.0-<?f e TES TLOCATION : Uni t # 3 Fixe d Heart h RU N NUMBER : R l Stac k Diamete r •Inches : 39 " OPERATOR : STAR TTIME : STO P TIME : 

### I k .

IPQ 8 J15J . BAROMETRI C PRESSURE :

STATI C PRESSUR E (+/•) : Probe/Pilo t Number : .Pilo t Coefflcient : Filte r Bo xNo. : .Mete r Bo xNumber : .Orific e Coefficien t fY) : Delt a M@ : Nozzl e Size : XA O Thermocoupl e ID : Impinge r Outle

t 10 : _22
_ INITIA L VAC . MI D VAC . FINA L VAC . ' LEA KCHECKS :

) V In . CF M

CF M ' CF M ' In . In . 

### •00

6

•0P 3 OM 

# ma [MJf l 

## L&2J L INIT . PITO T

" FINA L PITO T ORSA TInitial : 

### 3 1' FILTE R DATA '

* *?T<- 3 0R8A TFinal : 

### 10 0 10 0

Fina l Vol . 

### 51 1

1 0



### I T T ORSA TDAT A



### ffr V Ttftil i

FO R MOISTUR E CALC : INE TGAIN : |^<j* j .'

1 ml . SAMP1 6 • vpoitfr,; . ;OM»P . tu n . . oRir w . .QAS.M«TS R i.i*-'-**it:.i'>.iJr'

. u-iu V TEMPERATUR E RE#,OINQS,* F SAMP1 6 • vpoitfr,; . ;OM»P . tu n . . oRir w . .QAS.M«TS R i.i*-'-**it:.i'>.iJr'

. u-iu V .'••;:$TAC K*:,.'

• ; , PROBE?.'. : .V.:.«h' : 

### •.. eA 

### ?, ' v&air&itt

, M 0 

### (. ^ »<6<3.»rt| r K & 

### c/ * ( 2.... - 7 5 l.ft l mo . 

### b 37& S 3 2S I ! > 

### IT |.8 \ Hlfe . 1 

### si n a n s i H

- J i 1.9 4 

### 39 . & a s i 

### l<i<i « < 

### 5 •It) \.M 426. 9 3 % 0<iU 3fc & f 116 7 fftW * 

### Si* •I S \.UL 3 W 2 HP, M l 36 8 <x > 

### 7 H9 f.3f t X1 5 a5< < 

### -XH$ s 3 

### 3 7 2 s 

### 5P, 5 

## • u 31 H 2 5 3 156 s 7 31ft W & 1 t o 

### •I t ( J1 4 a 5 3 iW S s ? 

### 2 5 4 « f (U J Pin

cAcJjf W, 5 . -tt t H5 1 . q 

### 2SV > K 

### 3 T i .1 * 1 

### -C j i5i. a ? 

### a s . S 

### sa. 5 ,t( p I.HI? 

## ^ XS I ? 3 a<fo U 

## w 5 •i e 

### U b 3-1 « 15 1 S H aft< i 

### % «f l L IT S 

# •» ! 1.1 5 37 5 a S l -^5 0 s' S .9 * 

## * / 7 |o 5 . i i 

### v i e 6 J7 « J5 I a m U 

### 1 °

\.3 3 SSVf t 31 7 Hi H A U 

## n i 13.1 )

nmu m MM.m . -.MI.. . •••i l . « l l »|,r J | llULl | j | , j < m w o o r o 0 0 4 ^

# ENSFC ! AECO M £' . -', 3
EP A ISOKINETI C SAMPLIN Q - FIEL D DAT A 8HEE T
SAMPLIN G TRAIN : PLANT : DATE : 5/10/2006 TES TLOCATION : RU N NUMBER : R 2 Stac k Diamete r •Inches : OPERATOR : START TIMfc : STO P TIME : M 5 BAROMETRI C PRESSURE : Ony xSTATI C PRESSUR E (•>-) :

Probe/Wtot Number : Unit # 3 Prin t Coefficient ;

Filte r Bo xNo, : 39 Mete r Bo xNumber : Orific e Coefficien t <V) : J . Gorma n Delt a H@ : I SO Q Nozzl e Size : n td ? XADThermocoupl e 10 : .2142 - INITIA L VAC . MI D VAC . FINA L VAC. ' LEA KCHECKS :

U In . CF M

In . In . 0.00 3 CF M CFM " 0.84 8081 0 1.02 7 INIT . PITOT FINA L PITO T* y

## ye3"

1 7 FILTE R DAT A 1.60 3 0.44 0

_ORSA TInitial :

ORSA TFinal : 3 m Ji'ijiTAB f> '

SAMPLE;. ' CLOQK. t

;,TIM E i \ ' ii^LOCITY/ . •i * "HEA D • •JWtnP.loiw

- • " ORIFICE: . fiETERlAjt: ' .JDallaM.lnw

e •v-';6A8METE R :; - ; ; .,... ; ypui»i6-;., . : . % . TEMPERATUR E READfNGB , ¥ SAMPLE;. ' CLOQK. t

;,TIM E i \ ' ii^LOCITY/ . •i * "HEA D • •JWtnP.loiw

- • " ORIFICE: . fiETERlAjt: ' .JDallaM.lnw

e •v-';6A8METE R :; - ; ; .,... ; ypui»i6-;., . : . % . , i..ajjj5R-./, .-JJiPRpag/J- j jflPEBBO^ , :. \Xmrn; •','•> I " .iMPIHQE H --rt :

•.(jFUlKOlilU I

. »» • IETER- . • •. ../.•OUT.-i} ; 0 •1 ? I.1 H 31 0 •2*1 0 2H5 i l l l 4 7 5 « 7.

» •-3

6 •\M 37 0 as / as s 7 5 1 ? V A 3 IS

. 0 0 .3 1 H § 7% § ( ff e 1% A 4 329

0 •3

0 (•<,<

* 29 1 1 1 7, 7 A S 30.0

0 i. q I. Q S W / a w 7 5 . i i A A 37. » ;?s o ;H S LI / l 6 0 A 7 4S.0

0 l. S ) W JH S s S a<3 6 7 6 <•

$ M A S •:.« o • J As p H 6 fiS • 2 8 0 74, > 1 i+ej>r*<r f4 fori - CU V • 1 KK •l * 36 5 T<\ 5 4 M l 4, 1 ? ? ?

f a : <1. K /• b 56 s as o a l l f< / i . * V a i 75.0

0 1.9 $W 0 , b >b £ a s o 7t« < 75 « / w •3.

W < « 5-H5. 9 36 6 a C

O a«{

6 u B S 00.0

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6 7 6 ' 5 B 7 10S.O

O l.lf f 31 ^ a 5 1 SO DC S 7 7 5 u tia.e

o l Y 561 . fc> 36" ? 

# SI Ai l 7 9 '30.0 0 —r 4

1 •



# . r

* 1 :.;..' < i^aER,yoj.jC??

10 0 10 0

a s 4 f t

I D

m i ORSATDAT A

FO R MOISTUR E CALC :



# < m 

## o o r o 0 0

# ENSk i A £CO M EP A ISOKINETI C SAMPLIN G •FIEL D DAT A SHEE T
SAMPUN G TRAIN : M5 / Particulat e BAROMETRI C PRESSURE : 

## rt .O S INITIA L VAC . PLANT : ONY XEnvironmenta l STATI C PRESSUR E (•/•) : 

## .m MI D VAC . DATE : GS-ll-A k Probe/Pllo t Number : FINA L VAC . TES TLOCATION : Uni t 03 Fixe d Heart h Pitot Coefficient : 0.8 4 RU N NUMBER : RI3 Filte rBo xNo. : Stac k Diamete r•Inches : 39 " Mete rBo xNumber : acti o INIT. PITO T Orific e Coefficien t (Y) : 1.031 FINA L PITO T OPERATOR : T.ucWwu- l Deli a H @ : l.9G i STAR TTIME : 1 11 5 Nozzl e Size : W W ORSA TInitial : STO P TIME : XA D Thermocoupl e ID : ORSA TFinal : Impinge r Outlet ID : Lt-J 3 

# r CHECKS :

. In . CF M 0.6<X\

CF M CF M ' In . ' In .
FILTE R DAT A

FO R MOISTUR E CAL C NE TGAIN : \!j

^3. § ml . ,-MWfiU L 

### S B . •METER.VyL. ' OA S METE R : ! r-"votuME./- ; pFROB E 

## 2£ £
• i uo . TEMPERATUR

E REAO W 

## J l l 

## _2£

_ •BI

T ' - PUM P

(YACUU M , ftzellfogii ^ 

### JL5 . •IG

> J 5 £ J5
_ 5i?3. 5 0 5 5 5 3 

## 3 1 rAg 3



## E M m i 

## J & i a 35E T 3b f 

## a m 

## _2 L _2 i 

## _22 L 

## _13
_ T7£ T 4>o

j . o 3 5 0 

## Ji L _Li L M i 

## Jik5

_ JJl L .ii i J U L 

## i s 7 5
Tit s 

## 3 5 

## 3 1 LO 17 5 

## J l l JLS L 0 5 

## • 1 

# 1 J l l 

## 3 E 3 T "Z

5 . 1 3£L 

## a t JL5 L



## Ml, 5 JU L 3 M s 

## "13"

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## _A£ L J U - J U 33
_ 

## 33E J o s JL

V Mp.7 

## Jil L jUg
_ *5C L 

## Jil l £18 

# i t JJik . JUL JL L

< m a > 

## oj



### Metal s Dat a



## VE S 002 3

### Veoli a E S Technica l Solution s Fixed Heart h Incinerato r # 3 Metho d 006 0 (Metals

) Samplin g Parameter

s Ru n No . Ru n 1 Ru n 2 Ru n 3
AVG S I Dat e 10-May-0 6 10-May-0 6 11-May-06 AVG S I Star t Tim e Unit s 10:0 8 15:0

0 11:2

5 AVG S I Sto p Tim e 12:51 17:1 6 13:3 9 Nozzl e Diameter inche s 0.40

8 0.43 1 0.431 0.423 Barometri c Pressur

e in . H g 29.1 0 29.02 29.0 5 29.0

6 Ne t Samplin g Tim e min . 120. 0 120. 0 120. 0 120. 0 Volum e Metere

d dc f 81.24

8 83.54

6 76.76 1 80.51 8 Avg . DG M Temp . ° F 86. 8 71. 2 78. 0 78. 7 Avg Delt a H i n H 2 0 1.5 7 1.7

6 1.4

2 1.5

8 Avg Delt a H in . H g 0.115 6 0.129

2 0.1041 0.116 3 DG M Calibratio n Facto r — 1.039 0 1.033

0 1.039

0 1.039

0 Ga s Sampl e Volum e dsc f 79.598 84.05 6 76.26

9 79.97

4 Tota l Wate r Collected m L 1271. 1 1380. 4 13005 

### \3\72 Volume o

fWate r Vapo r sc f 59.93

2 65.08

6 61.30

4 62.10

8 Moistur e (measured

) % v/

v 43. 0 43. 6 44. 6 43. 7 Moistur e ( @ saturation) % v/ v 102. 8 103. 0 103. 0 102.9 Dr y Mol e Fraction , 100-%M — 0.570 5 0.563

6 0.554

4 0.562

8 C0 2a t Stac k %dry 6.4 0 6.8

0 7.0

0 6.7

3 O; , a t Stac k %dr y 12.4 0 9.4

0 

### X0.00 10.6 0 C O + Nj, %dr y 81.20 83.8 0 83.0

0 82.6

7 Dr y Molecula rWeight Ib/lb-mol e 29.52 29.4 6 29.52 29.5 0 We t Molecula rWeigh

t 1Mb-mol e 24.57 24.4 6 24.39 24.4 7 Exces s Ai ra

t Stac k % 137.2 73. 9 83. 9 98. 3 Stac k Diameter inches 39. 0 39. 0 39. 0 39. 0 Stac k Are a sq . in . 1194. 6 1194.6 1194.6 1194.6 Stati c Pressur

e inH 2 0 0.2 2 0.21 0.0 7 0.1 7 Stac k Pressur e in . H g 29.1 2 29.0 4 29.06 29.0 7 Avg . Stac k

Temp . ° F 381. 2 

### m.i 371. 4 374. 6 Avg . Sqroo

t o fDelt a P 

### _ 0.412 8 0.423

5 0.384

3 0.406

9 | SD E Average — 11.97 2 1250 9 11.08 2 11.75

4 I Pito t Coefficient — 0.8 4 0.8

4 0.8

4 0.8

4 | Stac k Gas Velocit

y afpm 1,92 9 1,97

4 1,79

4 1,89

9 

# j Stac k Flowrat e we t acfm 16,001 16,37 7 14,88

3 15,75

3 J Stac k Flowrat e we t scfm 

### 9,774 \0,097 9,17 8 9,68

3 Stac k Flowrat e dscf m 5,57 6 5,691 5,08 8 5,451 Isokinetic s % 10 9 10

1 10

2 10

4 Meter Bo xNo . 

### _ 8018 4 8018

4 8018

4 — Delt a H @ inH 2 0 1.881 0 1.881 0 1.881 0 

# - Rei d QA Yq c 

### ^.0340 1.050 0 1.031 3 1.03 8 [Deviation

} Pre- Y % 0.48 % 1.06

% 0.74

% 0.8

%Run l AVGS-METAL S 

### Metho d 006 0 (Metals

) Samplin g Parameter

s Ru n 2 AVG S - METAL S Delt a H | STAC K TEM P Ru n 3 AVG S ~ METAL S P T Delt

a P SOR T Delt a P DG M I N DG M OU T Delt

a H STAC K TEM P Delt

a P SOR T Delt a P DG M IN DG M OU T Delt a P SQR T Delt a P DG M IN DG M OU T Delt

a H
a 1 0.1 5 0.20 0.20 0.21 0,21 0,1 8 0. 1 S > 0.1 1 0.1 4 0.1 7 0.20 0.1 8 0.387

3 0.447 2 0.447 2 0.458 3 I 0,458 3 0.424 3 I 0.387 3 0,331 7 0,374 2 i 0.412 3 0,447 2 0.424 3 73 7 8 8 1 8 4 8 8 8 9 90 9 1 8 8 9 3 9 4 9 5 7

2 7 4 7 5 7 7 8 3 8 4 8 5 8 5 8 7 8 8 8 9 1.3

8 1.8 0 1.8 0 1.9 2 1.9 2 1.6 5 1.4 0 1.0 0 1.3 0 1.5 6 1.8 0 1.6 5 36

6 37 9 38 1 38 5 38 2 38 3 38 2 38 1 36 7 38 5 38 6 38 6 0.1 2 0.2 1 0.20 0.21 0.21 0.20 0.1 7 0.1 2 0.1 5 0.1 7 0.20 0.1 7 0.346

4 0,458 3 0,447 2 0.458 3 0.458 3 0.447 2 0.412 3 0.346 4 0.387 3 0.412 3 0.447 2 0.412 3 7 9 7 6 7 4 7 2 7 2 7 0 7 1 7 2 6 9 7 2 7 3 7 2 7

7 7 5 7 4 7 3 7 1 6 8 6 8 6 8 6 8 6 8 6 9 6 8 1.2

0 2.0 0 1.9 0 2.0 0 2.0 0 1.9 0 1.6 0 1.2 0 1.4 6 1.6 0 1.9 0 1.6 0 35

9 37 5 37 6 37 6 37 3 37 1 36 8 36 7 35 8 37 1 37 5 37 6 0.1 6 0.1 7 0.1 8 0.1 7 0.1 6 0.1 5 0.1 2 0.1 0 0.1 2 0.1 6 0.1 8 0.1 7 0.400

0 0.412 3 0.424 3 0.412 3 0.400 0 0.387 3 0.346 4 0.316 2 0.346 4 0.400 0 0.424 3 0.412 3 7 1 7 5 7 7 7 9 8 0 8 1 8 1 8 1 7 8 8 1 8 3 8 3 7

1 7 1 7 2 7 2 7 4 7 5 7 6 7 6 7 7 7 7 7 8 7 8 1.S

0 1.6 0 1.7 0 1.6 0 1.5 0 1.4 5 1.1 5 0.9 5 1.1 5 1.5 5 1.7 0 1.6 0

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0 0.0

0 13.7 8 0.0 0

# 1 0.0

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0 1.0

0 0.0 0

# 1 0.0

0 Aluminu m(Al ) 0.0

0 0.0

0 13.78 . . 0.0 0 0.0

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0



# - 0.0 0

# j 0.0

0 Arseni c (As ) 249.0

0 0.7 6 * 13.78 12.4 5 248.2

4 0.0

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0 1.0

0



# - 0.0 0 1 248.2

4 Bariu m(Ba ) 0.0

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0 0.0

0 1.0

0 

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0 Beryllium(Be

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0



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4 0.0

0 0.0

0 1.0

0
_ 0.0 0

# I 1.0

4 Cobal l (Co

) 0.0

0 0.0

0 13.78 . . 0,0 0 0.0

0 0.0

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0 

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0 Chromiu m(Cr ) 29.0

0 1.01 » 13.7 8 1.4 S 27.99 J 0.0 0 0.0

0 1.0

0 

## - . 0.0 0 I 27.99 Coppe r (Cu ) 0.0

0 0.0

0 13.7 8 . . 0.0 0 8 0.0

0 0.0

0 1.0

0 . . 0.0 0 0.0

0 Manganes e (Mn ) 0.0 0 0.0

0 13.7 8



# - 0.0 0 0.0

0 0,0

0 1.0

0
. 0.0 0 0.0

0 Nickel (NI ) 0.0

0 0.0

0 13.78 . . 0.0 0 0.0

0 0.0

0 1.0

0 _ 0.0 0 0.0

0 Lea d(Pb ) 22.3 0 2.70 ' 13.7 8 1.1 2 19.6 0 0.0

0 0.0

0 1.0

0 _ 0.0 0 19.6

0 Antimon y (Sb) 0.0

0 0.0

0 13.7 8 . . 0.0 0 0.0

0 0.0

0 1.0

0



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0 Seleniu m(Se ) 0.0

0 0.0

0 13.78



# - 0.0 0 0.0

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0 1.0

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0 Thallium(Tt

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0 0.0

0 13.78 0.0 0 0.0

0 0.0

0 1.0

0 0.0 0 0.0

0 Vanadiu m(V ) 0.0

0 0.0

0 13.7 8



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0 0.0

0 1.0

0 0.0 0 0.0

0 Zin c (Zn ) 0.0

0 0.0

0 13.78 

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0



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. * - valu e use dfo r blan k correctio n MERCURY : (a

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t Detecte d/ Reportabl e Detectio nLimi t * Indicate s valu e use dfo r blan k correctio n

# ENS R AECO M Multi-Metal s Blan k Correctio n



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Corrected F H + B H

" f Silve r (Ag ) 0.0

0 0.0

0 13.78 0.0 0 1 0.0

0 0.0

0 1.0

0 0.0 0 0.0

0 Aluminu m(Al ) 0.0

0 0.0

0 13.7 8 . . 0.0 0 | | 0.0

0 0.0

0 1.0

0 0.0 0 0.0

0 Arsenic (As ) 946.0

0 0.7 6 * 13.7 8 47.3 0 945.2 4 0.0

0 0.0

0 1.0

0 _ 0,0 0 945.2

4 Bariu m(Ba ) 0.0

0 0.0

0 13.7 8 

# - 0.0 0 0.0

0 0.0

0 1.0

0 

# - 0.0 0 0.0

0 Berylliu m(Be ) 0.1 0 (0.10 ) 13.78 0.0 1 0.1 0 0.0 0 0.0

0 1.0

0 

# - 0.0 0 0.1 0 Cadmiu m(Cd ) 2.7 6 0.34 * 13.7 8 0.1 4 2.4 2 0.0

0 0.0

0 1.0

0 0.0 0 2.4

2 Cobal t (Co) 0.0

0 0.0

0 13,7 8 . . 0.0 0 0.0

0 0.0

0 1.0

0 

# - 0.0 0 0.0

0 Chromiu m(Cr ) 55.80 1.01 • 13.7 8 2.79 54.79 0.0 0 0.0

0 1.0

0



# - 0.0 0 54.79 Coppe r (Cu ) 0.0

0 0,0

0 13.7 8



# - 0.0 0 0.0

0 0,0

0 1.0

0



# - 0.0 0 0.0

0 Manganes e (Mn ) 0.0 0 0,0

0 13,7 8 _ 0.0 0 0.0

0 0.0

0 1.0

0 0.0 0 0.0

0 Nicke l (Ni) 0.0

0 0.0

0 13.7 8 - . 0.0 0 0.0

0 0.0

0 1.0

0



# - 0.0 0 0.0

0 Len d(Pb ) 40.6

0 2.70 » 13.78 2.0 3 37.9

0 0.0

0 0.0

0 ' 1.0

0



# - 0.0 0 37.9

0 Antimon y (Sb ) 0.0

0 0.0

0 13.7 8 

# - 0.0 0 0.0

0 0.0

0 1.0

0



# - 0.0 0 0.0

0 Seleniu m(Se ) 0.0

0 0.0

0 13.7 8 

# - 0.0 0 0.0

0 0.0

0 1.0

0 

# - 0.0 0 0.0

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0 0.0

0 13,7 8 0.0 0 0.0

0 0.0

0 1.0

0



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0 0.0 0 0.0

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0
. 0.0

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0 0.0

0 1.0

0



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. * - volg e use dfor blan k correctio n(a

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. filte

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CLIENT : Ony x Environmenta l Service , Inc
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CLIENT : Ony x Environmenta l Service , Inc
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## M L U3
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### (DO ItS. 7 I MS Rlnt e Volume s

FO R MOISTUR E CALC :

# ENS R AECO M ORSA TANALYSI

S (EP A METHOD 3) PLANT : ONY XEnvironmenta

l Service s DATE : — LOCATION : Uni t # 3 Fixe d Heart h SAMPL E TYPE : OPERATOR : PRE-LEA KCHECK : POST-LEA KCHECK :

NOTE : Check : Liqui d leve l mus t no t fel belo wbottom o

t capitoi y tubin g h 4 minute s an d meniscu s mus

t no t change b

y mor e than 0. 2 m L » i 4 minutes . DAT A CRITERIA - CO, : Whe

n greate r tha n 4% , differenc

e betwee n reading s shal l b e 0.3 % o rless . Whe n les s tha n 4%, differenc

e betwee n reading s shal l b e 0.2 % o rless . O, : Whe

n greate r tha n o requal t o 15% , differenc e betwee n reading s shal l b e 0.2 % o rless.' Whe n les s tha n 15% , differenc

e betwee n readings sha

d b e 0.3 % o rless .

Ne t 0 2 i s actua l 0 2 minu s actua l C0 2reading.Jun e 200 6 Tes t



# )

VE S 0023 6Particulat e Matte r Dat a

### Veoli a E S Technica l Solution s Fixe d Heart h Incinerato r # 3 Method 5 Samplin g Parameter s Ru n No . Ru n 1 Ru n 2 Ru n 3
AVG S Dat e 19-Jurv0 6 20-Jun-0 6 21-Jun-0 6 

### AVG S Star t Tim e Unit s 15:1 2 10:0 6 10:0

6 AVG S Sto p Tim e 17:2 9 1£2 9 12:4 4 Nozzl e Diamete r inches 0.431 0.43 1 0.43 1 0.43 1 Barometri c Pressur

e in.H g 29.55 29.55 29.50 29.5 3 Ne t Samplin g Tim e min . 120. 0 120. 0 ^20.0 

### 120. 0 Volum e Metered dc f 78.24

4 82.90

2 81.74

5 80.964 | Avg . DG M Ternp . ° F 110. 6 111. 2 109. 0 110. 3 8 Av g Delta H inHz O 1.3 1 1.4

3 1.4

1 1.3

8 8 Av g Delta H in.H g 0.096 4 0.104

9 0.103

4 0.101 6 | DG M Calibratio n Facto r 

# - 1.007 0 1.007

0 1.007

0 

### 1.067

6 1 Ga s Sampl e Volum e dsc f 72.24 7 76.482 75.573 74.76 8 Tota l Wate r Collecte d m L 1341. 0 1487. 9 1340. 1 1389. 7 Volum e o

fWate r Vapo r sc f 6352 8 70.154 63.186 65.52 3 Moistur e (measured) %v/ v 46. 7 47. 8 45. 5 46. 7 Moistur e ( @ saturation) %v/v 101. 3 101. 3 101. 5 101. 3 Dr y Mol e Fraction , 100-% M


# - 0.5333 0.521 6 0.544 6 0.5332 C 0 2

### a t Stac k %dr y 7.4 0 7.60 7.4 0 7.47 0 2 

### a t Stac k %dr y 10.0 0 8.20 9.60 9.2 7 C O + N 2 

### %dr y 82.6 0 84.20 83.00 83.2 7 1 _JDr y MolecularJW^ight___

_ lb/1b-mol e 

### 29.58 29.54 29.57 29.5 7 | We t Molecula rWeight Ib/lb-mol e 

### 24.1 8 24.0 2 24.3 0 24.1 7 H Exces s Ai ra

t Stac k % 84. 7 58. 5 78. 0 73. 7 1 Stac k Diamete r inche s 39. 0 39. 0 39. 0 39. 0 Stac k Are a sq . in . 1194. 6 1194. 6 1194. 6 1194. 6 Stati c Pressur

e inH 2 

### 0 -0.1 5 -0.1 5 -0.1 3 -0.1 4 Stac k Pressur e in . H g 29.54 29.54 29-4 9 29.5 2 Avg . Stac k

Temp . ° F 386. 2 387. 9 385. 9 386. 6 Avg . Sqroo

t o f Delt a P — 

### 0.370 1 0.3922 0.3930 0.385 1 SD E Averag e 

# - 10.76 5 11.420 11.429 11.205 Pito t Coefficien t — 

### 0.8 4 0.8

4 0.8

4 0.8

4 Stac k Ga s Velocit

y afp m 1,73 6 1,84

7 1,84

0 1,80

8 Stac k Flowrat e we t acfm 14,39

9 15,326 15,26 2 14,996 Stac k Flowrat e we t scf m 8,87

0 9,422 9,390 9,22 8 Stac k Flowrat e dscf m 4,730 4,91 5 5,11 4 4,92 0 Isokinetic s % 10 4 10

6 10

1 10

4 Mete r Bo xNo . — 

### 8075 4 80754 80754 

# - Delta H @ inHz O 1.83 2 1.83

2 1.83

2 

# - Fiel d Q AYq c 

# - 1.006 6 ' 0.991 8 0.997 4 0.9986 [Deviation] Pre-Y % 0.04 % 1.51 % 0.95% 0.84 % S.VJO3\2006\Ony>f^erf<>mir

a TasftTes t OabUun e 2006V2n D RetesntPMjdspAT

A

### Metho d 5 Samplin g Parameter s
P T Run l Ru n 2 Ru n 3 P T Dalt

aP SOR

T Dalt aP DG

M I N OG

M OU T Deli aH STAC K

TEMP Deli aP SOR T Deli aP DG

M I N DG

M OU T Deli aH STAC K

TEM P Delt

aP SOR

T Deli aP DG

M I N DG

M OUT Deli aH STAC K

TEM P a 1 0.0 7 0.264 6 10 4 102 0.6 6 382 0.1 0 0.316 2 102 9 9 0.9 2 38 2 0.1 7 0.412 3 8 9 8 7 1.53 37 9 a 2 0.1 2 0.346 4 10 4 102 1.1 3 38 7 0.1 0 0.316 2 10 6 102 0.92 38 3 0.1 5 0.387 3 9 2 8 9 1.35 38 0 a3 0.1 9 0.435 9 109 10 4 1.7

9 38 6 0.1 6 0.400 0 108 103 1.4 7 38 6 0.1 4 0.374 2 95 9 0 1.26 37 9 B.4 0.1 9 0.435 9 11 1 10 4 1.7

9 38 7 0.1 8 0.424 3 11 1 104 1.6 6 38 9 0.1 4 0.374 2 108 10 6 1.26 38 4 a s 0.1 5 0.387 3 11 4 106 1.41 38 8 0.1 4 0.374 2 11 2 10 5 1.29 38 7 0.1 8 0.424 3 11 2 10 6 1.6 2 38 8 a B 0.1 6 0.400 0 11 5 107 1.50 38 8 0.1 5 0.387 3 11 2 106 1.3 8 38 5 0.1 8 0.424 3 11 4 . 10 7 1.6 2 38 8 a 7 0.1 2 0.346 4 11 5 106 1.1 3 38 3 0.1 8 0.424 3 11 5 107 1.6 6 38 5 0.1 2 0.346 4 11 6 10 8 1.0 8 38 7 a B 0.1 5 0.387 3 11 6 10 4 1.41 382 0.1 5 0.387 3 11 6 109 1.3 8 38 8 0.1 0 0.316 2 11 7 10 9 0.9 0 38 1 b 1 0.0 7 0.264 6 11 3 11 1 0.6 6 382 0.1 8 0.424 3 11 0 11 0 1.6 6 38 6 0.2 2 0.469 0 11 2 11 1 1.9 8 38 4 b 2 0.1 4 0.3742 11 3 11 1 1.3 2 383 0.1 8 0.424 3 11 4 11 1 1.6 6 38 8 0.1 7 0.412 3 11 2 11 1 1.53 38 8 b 3 0.1 1 0.331 7 11 5 11 1 1.0 3 38 9 0.1 8 0.424 3 11 6 11 2 1.6 6 39 0 0.1 8 0.424 3 11 6 11 2 1.6 2 38 9 6 4 0.1 3 0.360 6 11 6 11 1 1.22 39 1 0.1 6 0.400 0 11 8 11 2 1.4 7 39 1 0.1 9 0.435 9 11 8 11 3 1.7 1 39 0 b 5 0.1 4 0.374 2 11 6 11 2 1.3 2 39 0 0.1 8 0.424 3 11 9 11 3 1.6 6 39 2 0.1 8 0.424 3 12 0 11 4 1.6 2 39 0 b e 0.1 5 0.387 3 11 6 11 2 1.41 38 7 0.1 6 0.400 0 12 1 11 4 1.4 7 39 5 0.1 6 0.400 0 .12 0 11 5 1.4 4 39 2 b 7 0.1 7 0.412 3 11 7 11 2 1.60 38 8 0.1 4 0.374 2 12 1 11 4 1.29 39 2 0.1 2 0.346 4 120 11 5 1.0 8 39 1 b 8 0.1 7 0.412 3 11 7 11 2 1.60 38 6 0.1 4 0.374 2 12 2 11 5 1.29 38 7 0.1 0 0.316 2 12 0 11 5 0.9 0 38 4 • 

### ft
" ii? T 

### •y-w1.41 i
. • 38 6 AV G 0.1 4 0.370 1 I 110. 6 1.3 1 38 6 0.1 6 0.392 2 1 1 1.4 3 38 8 0.1 6 0.393 0 109. 0 - • 1.41 i
. • 38 6

### ENS R Summin g Trai n Ru nNumbe

r Cllcul Fuclllt y Legatio n .Vourt t Dat e Operato r Slac k Dl»,-In , Star t Tlui t Stop Time :.o ; 

## EP A ISOKINETIC SAMPLING - FIEL D DATA SHEET

_JUL L

MIN T 

## A L T1M B WBLIK'HV ULAP 

### P 7 Uerouietrl c Promt * Sialic )>rtilure(+/. ) Prone/Mla l Numbe r Pilo t Cocfflclut Hlltr Bo i No
. Mete r Bo x No
. OrinctCotHlclta

t 00 Dtll aH(tf , NsultSln/Nt
. XA D TbermotOMpl

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. T C ID : OWPlCi ' 

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ft? Oru t •::oi v 

### 7
. 5 1. 1 

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. 0

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ft 4 ± L 1 5 J L L 

### t • a 3 M 

## 13 . JLiL L ipi a , 9 

## dl . LL\ . r*Vrt>, r g .63 ? 

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# i

-44 - 1.3 2 I S 

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## o o N > CO

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## o o r o r o 

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## EP A ISOKINETIC SAMPLIN G - FIEL D DAT A SHEET Samplin g Trai nM3 ^ ku nNumbe

r Clleui Facilit y Locatio n Soure r \1M
_ _ Operato r J20
. 

### /

AS P'- W Ur4 i > 3 1 1 01 -J O - ftfc Barometri c Pressor * Stati c Pwtti n<•/•)

_ Probc/Plta t Numbe r Pilo t Coefflcien t _ Fille r Bo aNa
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# t\ LEA K CHECK S t n n H g INITIA LVAC
. \K MI D VAC
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. 7

FILTE RDAT A FINAI
. riTQ T Oraa t 

### •:om: - 'Y.QV.-


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. XADTttrsHcoupl

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r 5o, a : : SILIC A BEIV : 

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E Iffi D Oulle l T C ID : Lt-t l H r 5o, a Fina l P H SIAMPU ! MIN T CLONI

C TUH F ULA

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* METE R VO

L V0MIM

B TEMPERATUR E READINGS , *F < ^65 ^ i i '

' „ COMMWrt s SIAMPU ! MIN T CLONI

C TUH F ULA

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## M l 133. i ? t > — ? J 11 3 s U i , t2ft.t » 

### 3 5 a s l M R m u a i qi. 5 

### it , 1 4 1 134. 3 

# § nM« f r74<

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### p i M Y s-. . 7 »< * ).? < 

### 139. S — 

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### ENS R AECO M 

## EP A ISOKINETI

C SAMPLING - FIEL

D DATA SHEET Sumpling Trai n Hu « Nurobt

r C(i« m l-ncllll y Locatio n Suurc c Ditt e Operato r _ suc k Din
. >)u
. Star t Tin t hto p Tim e 

### ..SiVi.'ft. l Ir H

JLSL 1 tocfe Barometri c Preuur e Stati c Prentic e (+/-)
_ Probe/PHo t Numbe r Pilo t Coefficien t Filte r Bo « No
. _ _ Mete r Bo « No
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.

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. INIT
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liiiiijO i ilillilHlili^iMlliililiiilHIiiii i ifHiHflfHililHfltillllitUilSis^ liiiiijO iiiiiliiiiii i iiliiiliiiliiiiililil ; Iff ! • l| i alHsI^f^MiiitlilHillM

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### 73 a Oraa

t ; 

### ;coi. -: 

### | IA Li 

# T 1 iFUtaffirj c Ral

eMetal s Dat a

### Veoli a E S Technica l Solution s Fixed Hearth Incinerato r Unit 3 Metho d 006 0 (Metals

) Samplin g Parameter

s Ru n No . Ru n 1 Ru n 2 Ru n 3
AVG S Dat e 19-Jur>-0 6 2OJun-0 6 2WurH) 6 AVG S Star t Tim e Units 15:1 2 10:0 6 10:0

6 AVG S I Sto p Tim e 17:2 9 12-5

9 12:4

4 1 Nozzl e Diameter inche s 0.43 1 0.43 1 0.43 1 0.431 | Barometri c Pressur

e in . H g 29.55 29.5 5 29.50 29.53 j Ne t Samplin g Tim e min . 120. 0 120. 0 120. 0 120. 0 | I Volum e Metere

d dc f 78.24

4 82.90

2 81.74

5 80.96

4 Avg . DG M Temp . ° F 110. 6 111 5 109. 0 110. 3 Av g Delt a H inHg O 1.3 1 1.4

3 1.4

1 1.3

8 Av g Delt a H iri . H g 0.096 4 0.104

9 0.103

4 0.101 6 DG M Calibratio n Facto r 

# - 1.O07 0 1.007

0 1.007

0 1.007

0 Ga s Sampl e Volum e dsc f 72.24 7 76.48

2 75.57

3 74.76

8 Tota l Wate r Collected m L 1341. 0 1487.9 1340. 1 1389.7 | Volum e o

fWate r Vapo r sc f 6352 8 70.15 4 63.18

6 65.523 Moistur e (measured

) %v/

v 46. 7 47. 8 45. 5 46. 7 Moistur e ( @ saturation) %v/ v 101.3 101.3 101.5 101.3 Dr y Mol e Fraction , 100-% M — 0.533 3 0.521 6 0.544 6 0.533

2 C 0 2a t Stac k %dr y 7.4 0 7.6

0 7.4

0 7.4

7 0 2 a t Stac k %dry 10.0 0 8.20 9.6 0 95 7 C O + N 2 %dry 82.6 0 84.20 83.0 0 835 7 Dr y Molecula rWeight Ib/lb-mol e 29.58 29.5 4 29.57 29.57 We t MolecularWeight Ib/lb-mol e 24.1 8 24.0 2 24.30 24.1 7 Exces s Ai ra

t Stac k % 84. 7 58. 5 78. 0 73. 7 Stac k Diameter inches 39. 0 39. 0 39. 0 39. 0 Stac k Area sq . in . 1194.6 1194.6 1194.6 1194. 6 Stati c Pressur

e inH 2 0 -0.1 5 -0.1 5 4}.1 3 -0.1 4 Stac k Pressur e in . H g 29.5 4 29.5

4 29.4

9 29.5

2 Avg . Stac k

Temp . ° F 386. 2 387. 9 385. 9 386. 6 Avg . Sqroo

t o fDelt a P — 0.3701 0.392 2 0.393

0 0.385 1 SD E Average — 10.76 5 11.420 11.42 9 1150 5 Pito t Coefficient — 0.8 4 0.8

4 0.8

4 0.8

4 Stac k Ga s Velocit

y afp m 1,73 6 1,84

7 1,84

0 1,80

8 Stac k Flowrat e we t acfm 14,39

9 15,32

6 15,26

2 14,99

6 Stac k Flowrat e we t scf m 8,87

0 9,42

2 9,39

0 9,228 Stac k Flowrat e dscf m 4,73 0 4,91 5 5,11 4 4,920 Isokinetic s % 10 4 10

6 10

1 10

4 Mete rBo xNo . 

# - 8075 4 8075

4 8075

4 — Delta H @ inH 2 0 1.832 0 1.832

0 1.832

0 

# - I Hel d Q A Yq c — 1.006 6 0.991 8 0.997 4 0.99

9 I [Deviation] Pre-

Y % 0.04 % 1.51 % 0.95 % 0.8

%

### Run l AVGS-METAL S 

### Metho d 006 0 (Metals

) Samplin g Parameter

s Ru n 2 AVGS--METAL S 

### Run 3 AVGS-METAL S PT
a 1 Delt

a P SOR T Delt a P 0.0 7 0.264

6 DG M I N 10 4 DG M OU T 10 2 Delt

a H 0.6 6 STAC K TEM P Delt

a P 38 2 0.1 0 SQR T

Delt a P 0.316 2 DG M IN 10 2 DG M OU T 9 9 Delt

a H I 0.9 2 STAC K TEM P Dalt

a P 38 2 0.17 . SQR T

Delt a P 0.412 3 DG M I N 8 9 DG M OU T 87 Delt

a H 1.5 3 0.1 2 0.346

4 10 4 10

2 1.1 3 38

7 0.1 0 0.316

2 10 6 10

2 0.9

2 38 3 0.1 5 0.387

3 9 2 89 1.3

5 0.1 9 I 0.436

9 10 9 10

4 1.7

9 38 6 0.1 6 0.400

0 10 8 10

3 1.4

7 38 6 0.1 4 0.374

2 9 5 90 1.2

6 0.1 9 0.435

9 11 1 10

4 1.7

9 38 7 0.1 8 0.424

3 11 1 10

4 38

9 0.1 4 0.374

2 10 8 10

6 1.2

6 0.1 5 0.387

3 11 4 10

6 1.4

1 38

8 0.1 4 0.374

2 11 2 10

5 1.2

9 38 7 0.1 8 0.424

3 11 2 10

6 1.6

2

b 1 0.1 6 0.1 2 0.1 6 0.0 7 0.1 4 0.1 1 0.1 3 0.1 4 , 0.1 5 0.1 7 0.400

0 | 0.346 4 0.387 3 0.264 6 0.374 2 0.331 7 0.360 6 0.374 2 0.387 3 0.412 3 0.412 3 11 5 11 5 11 6 11 3 11 3 11 5 11 6 11 6 11 6 11 7 10

7 10 6 10 4 11 1 11 1 11 1 11 1 11 2 11 2 11 2 1.5

0 1.1 3 1.4 1 0.6 6 1.3 2 1.0 3 1.2 2 1.3 2 1.4 1 1.6 0 38

8 38 3 38 2 38 2 38 3 38 9 39 1 39 0 38 7 38 8 0.1 5 0.1 8 0.1 6 0.1 8 0.1 8 0.1 8 0.1 6 0.1 8 0.1 6 0.1 4 0.387

3 0.424 3 0.387 3 0.424 3 0.424 3 0.424 3 0.400 0 0.424 3 0.400 0 0.374 2 11 2 11 5 11 6 11 0 11 4 11 6 11 8 11 9 12 1 12 1 10

6 10 7 10 9 11 0 11 1 11 2 11 2 11 3 11 4 11 4 1.3

8 1.3 8 1.6 6 1.6 6 1.6 6 1.4 7 1.4 7 1.2 9 38 5 38 5 38 8 38 6 38 8 39 0 39 1 39 2 39 5 39 2 0.1 8 0.1 2 0.1 0 0.2 2 0.1 7 0.1 8 0.1 9 0.1 8 0.1 6 0.1 2 0.424

3 0.346 4 0.316 2 0.469 0 0.4123 0.424 3 0.435 9 0.424 3 0.400 0 0.346 4 11 4 11 6 11 7 11 2 11 2 11 6 11 8 12 0 12 0 12 0 10

7 10 8 10 9 11 1 11 1 11 2 11 3 11 4 11 5 11 5 1.6

2 1.0 8 0.9 0 1.9 8 1.5 3 1.6 2 1.7 1 1.6 2 1.4 4 1.0 8

# ENS R AECO M Multi-Metal s Blan k Correctio n
FRON T HAL F BAC K HAL F TOTA L Correcte d F H + B H K g Elemen t Sampl

e U g FidBl

k M B Defaul

t Valu e (a ) u g 5

% o f Sampl e U g Correcte

d Fron t Hal f U g Sampl

e M g Fi dBlk

u g Defaul

t Valu e U R 5 % of Sampl e M « Correcte

d Bac k Half TOTA L

Correcte d F H + B H K g Silve r (Ag) 0.0

0 0.0

0 13.7 8 0.0 0 0.0

0 0.0

0 1.0

0 0.0 0 0.0

0 Aluminu m(Al ) 0.0

0 0.0

0 13.7 8
_ 0.0 0 0.0

0 0.0

0 1.0

0 

# - 0.0 0 0.0

0 1 Arsenic (As ) 5.8 1 0.6 1 • 13.7 8 0.2 9 5.2

0 0.3 3 0.0 0 1.0

0 0.0

2 0.3 3 5.5 3 Bariu m(Ba ) 0.0

0 0.0

0 13.7 8 

# - 0.0 0 0.0

0 0.0

0 1.0

0


# - 0.0 0 0.0

0 Beryllium(Be

) 0.0

0 0.0

0 13.7 8 

# - 0.0 0 0.0

0 0.0

0 1.0

0


# - 0.0 0 0.0

0 Cadmiu m(Cd ) 0.0

0 0.0

0 13.7 8 . . . 0.0 0 0.0

0 0.0

0 1.0

0 

# - 0.0 0 I 0.0

0 Cobal t (Co) 0.0

0 0.0

0 £3.7 8 . . 0.0 0 0.0

0 0.0

0 1.0

0 

# - 0.0 0 0.0

0 Chromiu m(Cr ) 9.6

4 0.7

9 » 13.7 8 0.48 8.8 5 1.0

6 0.0

0 1.0

0 0.0

5 1.0

6 M l Coppe r (Cu ) 0.0

0 0.0

0 13.7 8 

# - 0.0 0 0.0

0 0.0

0 1.0

0 

# - 0.0 0 0.0

0 Manganes e (Mn ) 0.0 0 0.0

0 13.7 8 . . 0.0 0 0.0

0 0.0

0 1.0

0


# - 0.00 0.0 0 Nicke l (Ni ) 0.0

0 0.0

0 13.7 8 . . 0.0 0 0.0

0 0.0

0 1.0

0 

# - 0.0 0 0.0

0 Lea d(Pb) 0.0

0 0.0

0 13.7 8 - . 0.0 0 0.0

0 0.0

0 1.0

0 

# - 0.0 0 0.0

0 Antimon y (Sb ) 0.0

0 0.0

0 13.7 8 . . 0.0 0 0.0

0 0.0

0 1.0

0 0.0 0 0.0

0 Seleniu m(Se ) 0.0

0 0.0

0 13.7 8 

# - 0.0 0 0.0

0 0.0

0 1.0

0 0.0 0 0.0

0 Thallium(Tl ) 0.0

0 0,0

0 13.7 8 

## . . 0.0 0 0.0

0 0.0

0 1.0

0 0.0 0 0.0

0 Vanadiu m(V ) 0.0

0 0.0

0 13.7 8 0.0 0 0.0

0 0.0

0 1.0

0 

# - 0.0 0 0.0

0 Zinc (Zn) 0.0

0 0.0

0 13.7 8 

# - 0.0 0 0.0

0 0.0

0 1.0

0 

# - 0.0 0 0.0

0 l f FH B i s betwee

n 0 t o 13.7 8 ug us

e blank ; valu e t o correc t l f FH B > 13.78 u

g the n us e th e greate r o f 13.78 ug o r th e lesse r valu e betwee n FH B o r 5 % of FH S
. * - valu e use dfo r blan k correctio n MERCURY : (a

) - base do na3,5 4 - in
. Tille r size

Mercur y Fractio n Sampl

e PS FidBlk

M B Defaul

t Value U g 5 * of Sampl e U g Correcte

dj Amoun t H g U g FRONT HAL F 0,0 0 0.0

0 6.0

0 0.0

0 0.0

0 BAC K HAL F 0.0

0 0.0

0 6.0

0 0.0

0 0.0

0 

# I TOTA LH g 0.0 0 ' | I

f BHB i s » 0 but<

= I u g the n us e th e BH B valu

e lo correc t I f BHB is> l u

g us e ih e greate r of eithe r 1 ugor5%ofB H ( ) No t Detecte d/ Reportabl e Detectio nLimit

CLIENT : Veoli a E S Technica l Solution s PROGRAM : Fixe dHeart h Incinerato r Uni t 3 RU N NO . Rim l

l f P B i s > 0 bu t <= 6 ug the n us e th e F B valu e t o correc t ( ) No

t Detecte d/ Reportabl e Detectio nUml l I f F B i s > 6 ug us e (h e greale r o f eithe r 6 u g o r J * o f FH • Indicates valu e use dfo r blan k conectio n

# ENS R AECO M Multi-Metal s Blan k Correctio n



# < m c o 

## o o P O t o I f FB i s > 0 bu t <= 6 u g (he nus e Ih e F B valu e t o correc t I f F B i s > 6 n g us e (h e greate r of eithe r 6 ug o r 5% of F H ( ) No

t Detecte d/ Reportabl e Detectio nLimit * Indicate s valu e use dfor blan k collection FRON T HAL F BAC K HAL F TOTA L Correcte dj F H + B H M S 1 Elemen t Sampl

e M g Fi dBlk

M g Defaul

t Valu e (a ) M g 5

% of Sampl e M 8 Correcte

d Fron t Hal f M g Sampl

e M g FidBlk

M g Defaul

t Valu e M g 5 * o f Sampl e M S Correcte

d Bac k Half M g TOTA L

Correcte dj F H + B H M S 1 Silve r (Ag) 0.0

0 0.0

0 13.7 8 0,0 0 | 0.0

0 0.0

0 1.0

0 0.0 0 I 0.0

0 Aluminu m(Al ) 0.0

0 0.0

0 13.7 8 

# - 0.0 0

# 1 0.0

0 0.0

0 1.0

0 

# - 0.0 0

# j 0.0

0 I Arsenic (As ) 4.3 0 0.6 1 * 13.7 8 0.2 2 3.6

9 I 0.0

0 0.0

0 1.0

0 

# - 0.0 0 I 3.6

9 Bariu m(Ba ) 0.0

0 0.0

0 13.7 8 

# - 0.0 0 I 0.0

0 0.0

0 1.0

0 

# - 0.0 0 0.0

0 Berylliu m(Be ) 0.0

0 0.0

0 13.7 8 

### - 0.0 0 

## I 0.0

9 0.0

0 1.0

0 0.0

0 0.0

9 0.0

9 Cadmiu m(Cd ) 0.0

0 0.0

0 13.7 8 

# - 0.0 0

# 1 0.0

0 0.0

0 1.0

0


# - 0.0 0 0.0

0 Cobal t (Co ) 0.0

0 0.0

0 13.7 8 - . 0,0 0 0.0

0 0.0

0 1.0

0 

# - 0.0 0 0.0

0 Chromiu m(Cr ) 3.9 8 0.79 • 13.7 8 0.2 0 3.1 9 0.66 0.0 0 1.0

0 0.03 0.66 3.85 Coppe r (Cu) 0.0

0 0,0

0 13.7 8 0.0 0 0.0

0 0.0

0 1.0

0 

# - 0.0 0 0.0

0 Manganes e (Mn ) 0.00 0.0

0 13.7 8 0.0 0 1 0.0

0 0.0

0 1.0

0 

# - 0.0 0 0.0

0 Nicke l (Ni ) 0.0

0 0.0

0 13.7 8 

# - o.o o 1 o.o

o 0.0

0 1.0

0 

# - 0.0 0 0.0

0 Lea d(Pb ) 0.0

0 0,0

0 13.7 8 

### - 0,0 0 1 0.0

0 0.00
. 1.0 0 

# - 0.0 0 0.0

0 Antimon y (Sb) 0.0

0 0.0

0 13.7 8 0.0 0 I 0.0

0 0.0

0 1.0

0 

# - 0.0 0 1 0.0

0 Seleniu m(Se ) 0.0

0 0.0

0 13.7 8 

# - 0.0 0 I 0.0

0 0.0

0 1.0

0 

# - 0.0 0

# 0 0.0

0 Thalliu m(Tl) 0.0

0 0.0

0 13.7 8 0.0 0 - | 0.0

0 0.0

0 1.0

0 0.0 0 |
. 0.00
. Vanadiu m(V ) 0.0

0 0.0

0 13.7 8 o.o o 

# I 0.0

0 0.0

0 1.0

0 

# - 0.0 0

# I 0.0

0 Zinc (Zn ) 0.0

0 0.0

0 13.7 8 

# - 0.0 0 I 0,0

0 0.0

0 1.0

0 

# - 0.0 0

# 1 0.0

0 I f FH B i s betwee

n0 t o 13.7 8 ng us

e blank ' valu e t o correc t I f FHB > 13.78 uglhenus

e Ih e greate r of 13.78 u. g o r Ih e lesse r valu e betwee n FHB o r 5 % o f FHS
. * - valu e use dfo r blan k correctio n(a

) - base do na3.5 4 • in
. filter

siz e MERCURY : I f BH B is>Obul<=I u

g (he nus e th e BH B valu

e t o correc t l f BHB is> l M

g us e th e greate r o f eithe r 1 ugor5%o f

B H ( ) No t Detected / Reportabl e Detectio nLimit

Mercur y Fractio n Sampl

e M B Fi dBlk

M S Defaul

t Valu e M g 5

% of Sampl e M B Correcte

d Amoun t H g M 8 CLIENT : Veoli a E S Technica l Solution s PROGRA M : Fixe d Heart h Incinerato r Uni t 3 RU N NO . Ru n 2 FRONT HAL F 0.0 0 O.O

O 6.0

0 0.0

0 0.0

0 CLIENT : Veoli a E S Technica l Solution s PROGRA M : Fixe d Heart h Incinerato r Uni t 3 RU N NO . Ru n 2 BAC K HAL F 0.0

0 0.0

0 6.0

0 0.0

0 0.0

0 CLIENT : Veoli a E S Technica l Solution s PROGRA M : Fixe d Heart h Incinerato r Uni t 3 RU N NO . Ru n 2

| TOTA LH g 0.0 0 CLIENT : Veoli a E S Technica l Solution s PROGRA M : Fixe d Heart h Incinerato r Uni t 3 RU N NO . Ru n 2

# ENS R AECO M Multi-Metal s Blan k Correctio n



# < m w o o C O I f FB i s > 0 bu t <= 6 ug the n us e tb e F B valu e t o correc t I f F B i s > 6 u g us e th e greate r o f eithe r 6 ug o r 5 * o f FH ( ) No

t Detecte d/ Reportabl e Detectio nlimi t * Indicates valu

e use dfo r blan k correctio n FRON T HAL F BAC K HAL F ! TOTA L Correcte d1 F H + B H |

mJ Elemen t .Sampl

e U g Fi dBlk

U g Defaull Value (a ) U g 5% o

f Sampl e U g Correcte

d Fron t Hal f U g Sampl

e U g FidBlk

U g Defaul

t Value U g 5 * o f Sampl e u s Correcte

d Bac k Half U S ! TOTA L

Correcte d1 F H + B H |

mJ Silver (Ag) 0.0

0 0.0

0 13.7 8 0.0 0 0.0

0 0,0

0 1.0

0 0.0 0 0.0

0 Aluminu m(Al ) 0.0

0 0.0

0 13.7 8 

# - 0.0 0 0.0

0 0.0

0 1.0

0 

# - 0.0 0 0.0

0 Arsenic (As ) 5.6

0 0.6 1 » 13.7 8 0.28 4.99 0.2 1 0.0 0 1.0

0 0.0 1 0.2 1 | 5.2 0 Bariu m(Ba ) 0.0

0 0.0

0 13.7 8 _ 0.0 0 0.0

0 0.0

0 1.0

0


# - 0.0 0 0.0

0 Beryllium(Be

) 0.0

0 0.0

0 13.7 8 

### - 0.0 0 0.0

0 0.0

0 1.0

0


# - 0.0 0 0.0

0 Cadmiu m(Cd ) 0.0

0 0.0

0 13.7 8 - - 0.0 0 0.0

0 0.0

0 1.0

0 

# - 0.0 0 0.0

0 Cobal t (Co ) 0.00 0.0 0 13.7 8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

# - 0.0 0 | | 0.0

0 Chromiu m(Cr ) 11.1 0 0.79 * 13.7 8 0.5 6 10.3 1 0.8 4 0.0

0 1.0

0 0.0

4 0.8

4 11.1 5 | Coppe r (Cu ) 0.0

0 0.0

0 13.7 8 0.0 0 0.0

0 0.0

0 1.0

0 

# - 0.0 0 0.0

0 | Manganes e (Mn ) 0.0

0 0.0

0 13.7 8 0.0 0 0.0

0 0.0

0 1.0

0 

# - 0.0 0 0.0

0 I Nickel (Ni ) 0.0

0 0.0

0 13.7 8 

# - 0.0 0 0.0

0 0.0

0 1.0

0



# - 0.0 0 0.0

0 Lead(Pb ) 0.0

0 0.0

0 13.7 8 

# - 0.0 0 0.0

0 0.0

0 1.0

0 

# - 0.0 0 1 0.0

0 Antimon y (Sb ) 0.0

0 0.0

0 13.7 8 

### - 0.0 0 0.0

0 0.0

0 1.0

0 

# - 0.0 0

# 1 o.o

o Seleniu m(Se ) 0.0

0 0,0

0 13.7 8 0.0 0 0.0

0 0.0

0 1,0

0 0.0 0 

### I I 0.0 0 Thallium(Tl) 0.0

0 0.0

0 13.7 8 

## . . 0.0 0 0,0

0 0.0

0 1.0

0 

# - 0.0 0 0.0

0 Vanadiu m(V ) 0.0

0 0.0

0 13.7 8 

## . . 0.0 0 0.0

0 0.0

0 1,0

0 

## - . 0.0 0 0.0

0 Zin c (Zn ) 0.0

0 0.0

0 13.7 8
- - 0.0 0 0.0

0 0.0

0 1.0

0 

# - 0.0 0 0.0

0 I f FH B i s betwee

n 0 t o 13.7 8 u g us

e blan k valu e ( o correc t I f FH B > 13.7 8 ugthe

n us e th e greate r o f 13.7 8 u g o r th e lesse r valu e betwee n FH B o r 5 % o f FHS
. * - valu e use dfo r blan k correctio n(a

) - base do na3.54 • in
. fille r

size MERCUR Y i I f BHB i s > 0 bu t <= 1 ug tha n us e th e BH B valu

e t o correc t I f BH B i s > 1 p g us e Ih e greate r of eithe r 1 u g o r 5 % o f B H ( ) No t Detecte d/ Reportabl e Detectio nLimit

Mercur y Fractio n Sampl

e U g Fi dBlk

f g Defaul

t Value U g 5 % o

f Sampl e U g Correcte

d Amoun t H g U S CLIENT : Veoli a E S Technica l Solution s PROGRAM : Fixe d Heart h Incinerato r Uni t 3 RU N NO . Ru n 3 FRONT HAL F 0.0 0 0.0

0 6.0

0 0.0

0 0.0

0 CLIENT : Veoli a E S Technica l Solution s PROGRAM : Fixe d Heart h Incinerato r Uni t 3 RU N NO . Ru n 3 BAC K HAL F 0.0

0 0.0

0 6.0

0 0.0

0 0.0

0 CLIENT : Veoli a E S Technica l Solution s PROGRAM : Fixe d Heart h Incinerato r Uni t 3 RU N NO . Ru n 3

fi TOTA LH g 0.0 0 CLIENT : Veoli a E S Technica l Solution s PROGRAM : Fixe d Heart h Incinerato r Uni t 3 RU N NO . Ru n 3ENS R 

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## Veoli a E S Technica l Solution s Fixe d Heart h Incinerato r # 3 Method 0023

A Samplin g Parameter s Ru n No . 

### Run 1 Ru n 2 

### Ru n 3

AVG S Dat e 19-Jun-0 6 20-Jun-0

6 21-Ji«v0

6 AVG S Star t Tim e Unit s 14:40 9:3 0 9:3 0 AVG S Sto p Tim e 17:59 13:05 11:4 3 Nozzl e Diamete r inche s 0.43 5 0.43 5 0.43 5 0.43 5 Barometri c Pressur e in . H g . 29.5 5 29.5 0 29.5 0 29.5 2 Ne t Samplin g Tim e min . 192. 0 192. 0 192. 0 192. 0 Volum e Metere d dc f 135.21 5 136.33 1 133.04 6 134.86 4 Avg . DG M Temp . ° F 109. 3 107. 1 107. 9 108. 1 Av g Delt a H inH z O 1.7 1 1.74 1.67 1.71 Av g Delt a H L_.'Uj9 . 0.125 7 0.128 2 6.122 5 0.125 5 D G M Calibratio n Facto r 1.032 0 1.032 0 1.032 0 1.032 0 

### Ga s Sampl e Volum e dsc

f h f283ii 3 129.71 0 126.37 9 128.15 1 Tota l Wate r Collecte d m L 2171. 7 2509. 0 2250. 4 2310. 4 Volum e o f Wate r Vapo r sc f 102.39 6 118.29 9 106.10 6 108.93 4 Moistur e (measured ) %v/ v 44. 4 47. 7 45. 6 45. 9 Moistur e ( @ saturation ) %v/ v 101. 3 101. 5 101. 5 101. 4 Dr y Mol e Fraction , 100-% M — 0.556 3 0.523 0 0.543 6 0.541 0 C0 2 a t Stac k %dr y 7.40 7.6 0 7.4 0 7.4 7 O za t Stac k %dr y 10.0 0 8.2 0 9.6 0 9.2 7 

# I CO ' + N a %dr y 82.6 0 84.2 0 83.0 0 83.2 7 fi Dr y Moiecuia rWeigh t Ib/lb-mol e 29.5 8 29.5 4 29.5 7 29.5 7 fi We t Moiecuia rWeigh t Ib/lb-mol e 24.4 4 24.0 4 24.2 9 24.2 6 1 Exces s Ai ra t Stac k % 84. 7 58. 5 78. 0 73. 7 fi Stac k

Diamete r inche s 39. 0 39.6 " 39. 0 39. 0 fi Stac k

Are a sq . in . 1194. 6 1194. 6 1194. 6 1194. 6 R Stati c Pressur e inHa O -0.1 3 -0.1 5 -0.1 7 -0.1 5 | Stac k

Pressur e in . H g 29.5 4 29.4 9 

### 29.49 29.5 1 I Avg . Stac k

Temp . ° F 390. 4 393. 1 385. 0 389. 5 J Avg . Sqroo t o f Delt a P — 0.411 3 0.416 6 0.406 2 0.411 4 | SD E Averag e 

### -- 11.99 4 1 12.16 8 11.80 8 11.99 0 1 Pito t Coefficien t — 0.8 4 0.84 0.8 4 0.8 4 fi Stac k

Ga s Velocit y afp m 1,92 3 1,969 1,90 1 1,93 1 fi Stac k

Flowrat e we t acf m 15,95 6 16,33 8 15,77 3 16,02 2 fi Stac k

Flowrat e we t scf m 9,78 1 9,96 6 9,71 3 9,82 0 

### Stack Flowrat e dscf

m 5,44 1 5,21 2 5,28 0 5,31 1 

### isokinetic s % 9 9 104 10 0 10 1 1 Mete rBo xNo . — 8064 5 80645 8064 5 — Delt a H @ ...Jn - "9..... . 1.88 1 1.88 1 1.88 1 

# - Fiel d Q A Yq c 1.048 1.050 1.05 2 1.05 0 [Deviation ] Pre- Y % 1.6% 1.7 % 1.9% 1.7 %

# 1 S:'LJOB'a006\Ony>*PBr<ormanc e TesOTes

t OataVlun

e 200612n

d Retest<M23

A Separat

e Front , Bac k Hal f jun e 2006.xjs]DAT

A

## <

m 

# cn o o N > C O RU N 1 AVG S - - PCDDs/PCDFs 

### Metho d 0023 A Samplin g Parameter s RU N 2 AVG S » PCDDs/PCDFs RU N 3 AVG S - PCDDs/PCDF s P T O P SQR T

D P OG M

I N DG M

OU T D H STAC K TEM P D P 8QR T D P OG M

I N DQ M

OU T D H STAC K TEM P D P SQR T D P DQ M

I N OG M

OU T D H A 1 0.2 2 0.469 0 10 3 10 0 2.20 38 9 0.1 4 0.3742 94 9 3 1.4 0 367 0.1 4 0.3742 9 5 1.4 0 0.2 5 0.500

0 105 10 1 2.5 0 38 9 0.1 4 0.3742 9 5 9 3 1.4 0 38 6 0.1 1 0.331 7 9 7 9 5 1.1 0 0.25 0.500

0 11 4 10

3 8.60 38 9 0.20 0.447 2 S 6 9 4 2.0 0 38 9 0.1 5 0.387 3 

### s a 1.5 0 0.2 1 0.458 3 11 5 105 2.1 0 38 9 0.20 0.447 2 9 8 9 5 2.00 38 8 

### o.i e 0.4000 10 1 9 7 1.6 0 0.2 2 0.469 0 11 6 10 8 2.2 0 390 0.20 0,447 2 10 1 9 6 2.00 3S 0 0.1 6 0.387 3 102 9 7 1.6 0 0.2 1 0.458 3 11 7 108 2.1 0 38 9 0.20 0.447 2 105 9 7 2.00 39 0 0.1 6 0.387 3 10S 99 1.6 0 0.1 2 0.346

4 11 7 109 1.2 0 39 0 0.20 0.447 2 10 4 9 9 2.00 39 1 0.1 7 0.412 3 10 7 10

0 1.70 0.1 6 0.4000 11 6 10 8 1.6 0 38 9 0.1 6 0.387 3 106 10 0 1.50 39 2 0.1 7 0.412 3 10 7 10 1 1.70 0.2 0 0.447 2 11 6 10 9 2.00 39 0 0.1 8 0.424 3 10 8 10 1 1.8 0 39 2 0.1 4 0.3742 106 10 4 1.4

0 0.1 6 0.400

0 11 8 108 1.6 0 38 9 0.20 0.447 2 10 8 10 2 2.00 39 3 0.1 7 0.412 3 10 7 10

4 1.70 0.1 6 0.400

0 11 5 10

9 1.6

0 39 1 0,20 0.447 2 10 9 103 2.00 39 1 0.20 0.447 2 10 9 10 6 2.00 0.1 4 0.3742 11 6 10 8 1.4 0 39 1 0.2 0 0.447 2 10 9 103 2,00 38 7 0.1 S 0.367 3 11 0 103 1.6 0 0.1 3 0,360 6 11 4 10 9 1.3 0 38 3 0.1 5 0.387 3 10 9 10

4 1.50 384 0.2 0 0.447 2 11 3 10 7 2.00 0.1 6 0.387 3 11 4 10 8 1.6 0 38 3 0.1 7 0.412 3 10 8 10 4 1.70 38 5 0.20 0.447 2 11 3 10 7 2.00 0.1 3 0.360 8 11 3 108 1.3 0 367 0.1 5 0.387 3 10 8 1.6 0 384 0.2 0 0.447 2 11 4 10 7 2.00 0.1 4 0.374 2 11 2 10 5 1.4

0 38 8 0.1 5 0.387 3 11 0 10 4 1.50 39 0 0.20 0.447 2 11 6 10 8 2.00 B 1 0.1 7 0.412 3 10 8 106 1.70 39 2 0.1 6 0.387 3 10 7 10

7 1.50 384 0,1 2 0.346 4 10

9 10 8 1.2

0 0,1 7 0.412 3 107 10 6 1.70 392 0.1 4 0.3742 10 9 10

7 1.4

0 39 2 0.1 2 0.346 4 10

9 10

7 1.2

0 0.1 9 0.435 9 10 8 10 6 1.9

0 394 0.1 2 0.346 4 11 2 10 8 1.2 0 39 6 0.20 0.447 2 11 0 10 7 2.00 0.1 7 0.412 3 10 9 105 1.70 39 4 0.1 8 0.424 3 11 3 108 1.6 0 39 8 0.20 0.447 2 11 3 109 2.00 0.1 6 0.387 3 11 0 10 6 1.50 394 0.1 8 0.424 3 11 6 10 9 1.8

0 39 9 0.20 0.447 2 11 4 109 2.00 0.1 6 0,387 3 11 1 10 6 1.5 0 39 5 0.424 3 11 5 11 0 1.8 0 39 9 0.20 0.447 2 11 5 10 9 2.0 0 0.1 3 0.360 6 11 1 10 7 1.3 0 38 8 0.1 9 0.435 9 11 5 11 0 1,9 0 0.1 8 0.424 3 11 4 10 9 1.6

0 0.1 0 0.3162 11 2 10 7 1.0

0 38 3 0.1 9 0,435 9 11 6 11 0 1.9 0 40

0 0.1 8 0.424 3 11 6 11 0 1.8 0 0.1 5 0.387 3 11 2 10 7 1.50 38 8 0.1 7 0.412 3 11 S 11 2 1.70 40 1 0.1 2 0.346 4 11 5 11 0 1.2 0 0.1 6 0.400

0 11 2 10

7 1.6

0 39 0 0.1 6 0.387 3 11 6 11 1 1.50 400 0.1 4 0.3742 11 5 11 1 1.4 0 0.1 B 0.424 3 11 2 107 1.8 0 394 0.1 7 0.412 3 11 6 11 1 1.70 39 9 0.1 4 0.3742 11 5 11 2 1,4 0 0.2 0 0.447 2 11 2 10 7 2.0 0 39 3 0.1 7 0.412 3 11 6 11 2 1.70 39 8 0.1 3 0.360 6 11 6 11 1 1.3 0 0.1 7 0.412 3 11 2 10 7 1.70 39 5 0.1 8 0.424 3 11 7 11 3 1.8 0 39 9 0.1 3 0.360 6 11 5 11 1 1.3 0 0.1 7 0.412 3 11 2 10 7 0.1 8 0.424 3 11 2 10 7 1.70 1.8 0 39 5 0.20 0.447 2 11 6 11 3 2.00 39 8 0.1 7 0.412 3 11 8 11 2 39 S 0,1 8 0.424 3 11 6 11 3 1.8 0 39 8 0.2 2 0.4690 11 6 11 2 1.70 2.2 0 0.1 8 0.424 3 11 2 10 7 1.8

0 39 6 0.20 0.447 2 11 5 11 3 2.0 0 0.22 0.469 0 11 6 11 1 2,2 0



### AV Q 

## mmm 0.1 7 0.411 3 109. 3 

## 9 1



# mi 1.7

1 

### mm m 39 0 0.1 7 0.416

6 107. 1 1.7 4 39

3 0.1 7 0.406

2 107. 9 1.6 7

### ENSR|AcCO W Samplin g Trai nDlOVlV^f



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# ENS R

Appendi xC

Metho d calibrations , Verifications , an d Certification s Referenc e

S^JOBef»6\Dnyi*Per(o i Tes l Repcxtdo

c 200 6 rmanceTesftReport»nyx200 6



## VE S 0023 8

# ENS R AECO M

D R YGA S METE R CALIBRATIO N Mete r Bo xNo. : 8075

4
Chec k one Annua l Cattratio n Recalibratio n Date : 3/14/200 8 Operato r

Jame s Ruckdeschel Barometric Pressure : 28.5 5 (in Ha ) Theoretica

l Critica l Vacuum : 13.47 (InHg ) Manufacturer

: Dat a Recervea7Place

d i n service : Serial Na : AnrJetso n NUTEC H Pr e 199 0 8075 4 Pretes t Lea k Check s AJowabl a Actua

l Positiv e 0 0.0 0 (a t 5-7tn .H,P ) In. HjOpermrn . Negativ e 0 0.000 (a t 3fn.Hg) cf

m cft

n

DR YSA S METE R DAT A CRITICA L ORIFIC E DAT A
A H (InrtP) Tim

e (min ) Volum e Ter m > Critica

l Orific e Seria l # I C Orific e Cafibrarto n Actua

l Vacuum O n Ho ) Ambien

t Temperatur

e A H (InrtP) Tim

e (min ) Inros

l Fina

l Tota

l ef t Initia

l Fina

l Critica

l Orific e Seria l # I C Orific e Cafibrarto n Actua

l Vacuum O n Ho ) tntja

l Fina

l Averag

e A H (InrtP) Tim

e (min ) Inros

l Fina

l Tota

l ef t °F Critica l Orific e Seria l # Coefficien

t Actua

l Vacuum O n Ho ) " y • F 0.24 2 0 677.300 683.17 0 S.87 0 6 9 7 0 4 8 0225 1 5 6 8 6 8 6 8 0.9 1 1 6 691.800 700.15 6 8.35 6 7 4 7 4 5 2 0.427 I S 6 9 7 3 7 1 13 0 1 5 711.600 722.61 3 11.01 3 7 6 7 9 6 3 036 2 1 5 7 3 7 4 7 4 33 0 1 0 733.800 74439 0 10.79 0 8 1 8 3 7 6 0.83 1 1 5 7 2 7 3 7 3

CORRECTE D VOLUM E Dr y Ga s Mete r V m (stilt" ) Critica

l Orific e Vcr<sMf( ^ ) OR

YGA S METE R CALIBRATIO

N
' FACTOR V DR YGA S METE R CALIBRATIO

N FACTO R AH O 538 7 5.59 1 1.00 1 -O.006 1.72 7 -O.10

4 7.89 9 7.93 6 1 .00 5 0.00 1.82 9 -0.00 3 10.35 3 10^12

0 1 .00

6 0.00 1.748 -0.08 3 10.12 4 1058 1 1.01 6 0.0 1 2.02 2 0.1 9

| Avg. Y1.00 7 \ | Avg . AH O 1.83 2 | Notes : 1 ) Fo

rvali d les t rasuts, th

e Actua l Vacuu m shoul d b e 1 t o 2 iaHgg^eaierfjtian th

a Theoretic

^ 2 ) Th e Critics l Ori&c e Coefficient

. IC , mus t b e entere d i n EngBs

h units, (fl)«3-(oe

g RJ^.9((ln.Hg) > (fnin)). 3 ) Th e rniramu m numbe ro fsampl e volum e requlinsperonTicalsScubicfeet. 4 ) Fo rCastratio n Facto rY . th e rati o o l th e iBacin g o fth e caJihalio

n melwt o 5 ) 1 ^ OrrBc

e teBiraft^ Fact

w acceptabl e toleranc e o fIndividua l value s fro m th e averag e I s ±0.2 .

Bal.TCID # Fluk e RT D 213103 ! Inle t ID# : 80754-I N Outle t ID#: 80754 -OU T Ret . Sourc e Ref,° F • F A * F a An* . Ai r 6 5 6 6 - 1 6 6 1 Ho t wate r 10

6 10

6 0 104 - 2 Potentiomete r Calibration Lo w 501 = S

O Mid 45

0 ° F 45 0 High . 95

0 

## f 95 2
Notes : 1)HotWatertobeintherangeo f104-122"F. 2 ) Toleranc e allowe d fo ral l thermocoupl

e inolvidua

l readings : * 5.

4 ° F 3 ) Toleranc e allowe d fo ral l potentiomete

rindhirjua l reading s :±2* F

/ > + —
' ' V '-+46 0 »'(«r )



## VE S

# ENS R 

# AECO M

D R YGA S METE R CALIBRATIO N Mete r Bo xNo. : 80645 Chec k one ; Annua l CaBbrabo n Recalibratio n Date : 12/27/200 5 Operator : Rya n Bum s Barometri c Pressure : 293 0 P > W ) Theoretica l Critica l Vacuum : 135 2 O n Hg ) Anderso n NUTECH Pretes t Lee k Check s AaowaU e Actua

l Positiv e 0 0.0 0 (a t 5-Tin.HiP ) m.HcOt^rnin . Negativ e 0 0.00 0 (a t 3'n.Hg ) cf

m cf

m Dat e Flocave^ P lace

d in service: Seria l Na : OR YGA S METE R DAT A CRITICA L ORIFIC E DAT A
AH rnHjp ) Tim

e (nvn ) VoUne Tom 0 Critica

l Orific e Serial * K

" Orific e CaaVallo n Coelfioen t Actua

l Vacuu m (nHg) Ambien

t Ternperatuj

e AH rnHjp ) Tim

e (nvn ) Initia

l (ft 3 ) Fina

l (K 3 ) Tota l Pf) Initia

l Fina

l Critica

l Orific e Serial * K

" Orific e CaaVallo n Coelfioen t Actua

l Vacuu m (nHg) Fina l Averag

e AH rnHjp ) Tim

e (nvn ) Initia

l (ft 3 ) Fina

l (K 3 ) Tota l Pf) •p • E Critica l Orific e Serial * K

" Orific e CaaVallo n Coelfioen t Actua

l Vacuu m (nHg) 

### "e • F 0.2 6 2 0 82630 0 832.32 7 5.82 7 81 8 1 40 052 5 1 5 6 8 6 8 6 8 05 9 1 5 811.800 819.95 0 8.15 0 83 8 3 5 2 0.42 7 1 5 6 8 6 8 6 8 1.80 1 5 777.400 78820 5 10.80 5 80 8 0 6 3 0.562 1 5 6 8 6 8 6 8 4.0 0 1 0 857.400 868.22 8 10.82 8 80 8 0 7 6 033 1 1 5 6 8 6 8 6 8

CORRECTE D VOLUM E Dr y Ga s Mete r V m (staff ) Critica

l Orific e Ve r (st d tr

1 ) DR

V GA S METE R CALIBRATION FACTO R Y OR YGAS METE R CALIBRATIO

N FACTO R AH*

) 5.60 9 5.782 1.03 1 •0.00 1 1.75 0 -0.13 1 733 0 8.223 1.05 0 0.0 2 1.85 3 -0.02 8 10.45 9 10.82S 1.03 5 .03 0 134 4 0.063 1033 9 10.667 1.01 2 -0.0 2 1.977 0.1 0 | Avg . V 1.032~ 1 | Avg . AH O 1.88 1 | Notes : 1 1 Fo

rva M tes t results , BI B Actua

l Vacuu m shoul d be 1 tn2in . H g greate

r tha n th e Theoretica

l CtitMVacui m stra w 2 ) Th e Critica l Orific e Coefficient

, IC . mus t b e entere d i n Englis

h unis , (lt)»3'(deg R>Xi.5/((inJ1g)-(min)) . 3 ) Th e mriirru n numbe

r o fsampt o volum e require d po rorrfic o i s 5 cufjic foot

. 4 ) f^CaJeifa6an Facto

rY, th e rati o o fttiera 5 ) Fo rOrific e Calibratio

n Facto rAH*) , th e orific e clffeienba

) pressur e i n Inche

s o fry > tha t equate s t o 0.7 5 cf m o fai ra t 6 8 F an d 29.9 2 inche s o fHg , acceptabl e toleranc e o fIndividua l value s Iro m th e averag e i s *(X2 .
Dr y Ga s Meie r Thermocoupl

e Calibration Ref.TCID * 2131035 Inle t IO* : 80645-I N Ques

t 10* : 80645-OU T Ref . Sourc e Ref.' F " F a • F A Amb.Ai f 6 8 6 8 0 6 8 0 Ho t Wate r 11 2 11 2 0 11 1 - 1 Potentiomete r Calibration Lo w 5 0 ° F 50 Mi d 45

0 " F 44 9 Hig h 950" F 94 8

Notes : 1

> Ho i Watert

o t » i n th e range o f10 4 -122 "F . 2 ) Toleranc e aikme d to ra B Iherrtiocoupf

B Individua

l readings : ±5.

4 * F 3 ) Toleranc e allowe d fo ral l potentiomete

r individua

l readings : ±2 * F



## = r pfi Y

=•
•U» )



## VE S

# ENS R AECO M

D R YGA S METE R CALIBRATIO N Mete r Bo xNo. : 6018

4 Check-one: Annua l Calibratio n Recalibratio n Date : 1207/200 5 Operato r Rya n Bum s Barometri c Pressure : 293 0 

## On Ha) Theoretica l Critica l Vacuum : ia9 2 C<nHg ) Anderso n NUTECH Pretes t Lee k Check s Afcwabt o Actua

l Positiv e 0 0.00 (a t 5-7*1 . tfeO

) jruHsOpermin . Negativ e 0 0.00 0 (a t 3m . Hg ) cf

m d m Dat o Rece*vod/P1at

^ i n servica : Seria l No. : DR YOA S METE R DAT A CRITICA L ORIFIC E DAT A
A H IJnHrO ) Tim

e (min ) Volum

e Temp Critica l Orrfrc e Serial * I

C Orific e Calibratio n Coefficien t Actua

l Vacuu m GnHg ) Ambien

t Temperatur

e A H IJnHrO ) Tim

e (min ) Iritis

) flf) fina l

(ft 3 ) Total (ft 3 ) Ma ! Fata l Critica

l Orrfrc e Serial * I

C Orific e Calibratio n Coefficien t Actua

l Vacuu m GnHg ) Initia

l Fina

l Averag

e A H IJnHrO ) Tim

e (min ) Iritis

) flf) fina l

(ft 3 ) Total (ft 3 ) •

p ° F Critica l Orrfrc e Serial * I

C Orific e Calibratio n Coefficien t Actua

l Vacuu m GnHg ) • p • F •* 0.2 6 20 103.30 0 109.11 5 5.81 5 7 8 7 9 4 0 022 5 1 5 6 8 6 8 6 8 0.9 9 1 5 8330 0 91.38 5 8.08 5 7 5 7 6 5 2 0.427 1 5 6 8 6 8 6 8 1.80 1 5 161.70 0 172.46 8 10.76 8 8 2 8 3 6 3 036 2 1 5 6 8 6 8 6 8 4.0 0 1 0 134.00 0 144.63 1 10.63 1 8 3 8 4 7 6 0.83 1 1 5 6 8 6 8 6 8

CORRECTE D VOLUM E Dr y Ga s Critica

l DR

YGA S METE R DR YSA S METE R Mete r Orific

e CALIBRATION CALIBRATIO N Vm(stdft > ) Ve r(st d ft

5 ) FACTO R V FACTO R AH e 5 .62 3 5.78 2 1.028 -0.01 0 1.75 0
. •0.13 1 7.87 6 822 3 1.04 4 0.0 1 1.85 3 -0.02 8 10.37 5 10.82

5 1.04

3 0X 0 1.94 4 0.06 3 1028 0 10.66

7 1.03 8 0.00 1.97 7 0.1 0
\ Avg . Y1.038~ 1 | Avg . AH* ? 1.88 1 1 Notes : 1 ) Fo

rvali d tost resuKs

, tn o Actua l Vacuu m shoul d b e 1 t o 2 in . Hg graatartfta

n tri e Tneoretica

l Critica l Vacuu m show n above . 2 ) Th a Critica l Orific e Coefficient

. K, mus t b e entere d I n Englis h unis , pWldo o Hyvj.HifruHgrirmn)) . 3 ) Th e minirnur n numbe r o fsampl e voluni e require d pe rentic e i s 5 ctrbicfeeL 4 ) Fo rCaBwatio n Facto rY. th e ratt o o fth e reaolrigottraicaaWBlio

n mete r t o tf » 5 ) Fo rOrific e Caflibiatio

n Facto rAHG , th e orific e Differentia

l pressur e i n inche s o fHfi tha t equate s t o 0.7 5 cf m o fsi ra t 6 6 F an d 29.9 2 fetches o fHg . acceptabl e toleranc e o fInrXwioua l value s fro m tlie averag

e Is * OA
Dr yGa s Mete r Thermocoupl

e Calibratio n Ref . T C ID * 213103 5 Inle

t IO* : 80184

-I N Outle t ID* : 80184OU T Ref . Sourc e Ref.° F ° F A * F A Amb . Air 6 8 6 8 0 6 3 0 Ho t Wate r 11 1 11 1 0 11 1 0 PotanSomete rCafibration Lo w SO T 5 0 Mi d 45 0 ° F 45 0 Ug h 95

0 " F 95 1
Notes : 1 ) Ho

t Watert o b a i n Ih o range o t 104-12 2 °F . 2 ) Toleranc e alowe d fo ra l therrnocoupl

e individua

l readings : ±5. * *F 3 ) Tolersnc e afowe d fo r a l potentiomete

r etdividua l readings : ±2 * F 

## r° . 

## + v . w , = i7.»(y.) 7 - i -



## VE S

## ENSR I AECO M SAMPL E PROB E CALIBRATIO N DAT A FOR M TYP E "S * PITO TTUB E ASSEMBL YAN D NOZZL E

PROBED: EN S RRID42I3 !

in s Omto a CflfJOO . I0SB22S0 0 M5-4- A M M ****** rmvmvm'-a M5-4- A hi a/Ha

w •/ 315 9 273.4

8 3 4 27

4 1 2122 373. 3 21 4 37

4 0 3 '450. 0 505. 3 45 1 50

6 0.

1 MS4- A 32.5

9 273.4

6 3 4 27

4 1 212. 1 371 2 21 4 37 4 0-

3 450.0 605.

3 4S 1 sot

- 0.1 32.6 0 273.4

8 3 4 27

4 1 212.

0 373. 1 21 4 37 4 0. 3 450.0 505

5 45 1 so

s 0.1 32.5 9 273.4

8 3 4 27

4 1 212.1 371 2 21 4 37 4 0. 3 450.

0 505.

3 45 1 50

6 0.1

Leve l an d Perpendfcular Obstructio n No

a , (-10° S a,S+10" ) O j (-1Cf* S Oj,S +10") B , (-5° s B,S+5° ) 8 * (-ff s 6, 5 +S*

> 7 e z * ATanY M 0.12S" ) W= ATane(* s 0.03125' ) D , (3f16

s D, S 3/T

) A A/20 , (1.0

5 £P//D. S 1.5

) 0 4

037 5 0.92 5

dawmkilnttTUM

n o*a**te 2 .



# EM I Y>TJH

t Pfc O

2

) Iharrneeosvptotot

M MP*» 1 J Rio t tnt f a pab*t*mWi

do * >y*-

>ai r 1„ 1 l«IV. J =

' |Oat * Rooarve d an d ptaca d i n 5*mfc8 . fCurttto n o fProb e wtteftpte^towrAn : JOrVCfCCtkK

k I t cortf y th* WTyp

* S p M tOMrprot

e CU.
_ RECONDITIONE D (dtctem

)

PtNsanrw l (SlgnaS*»vOaW

) T&ar o Lftada r iSfcgniitirt/Dato

) Jcki^AssurarKMHaWoc

^ Vc*m» * Stationar y

# $omc*3p9dfo MOtods.

VE S 0023 8

## ENS R I AECO M SAMPL E PROB E CALIBRATIO N DAT A FOR M TYP E "S " PtTOTTUB E ASSEMBL YAN D NOZZL E 

### M E PROB E I h MS-4- B ENs n rrr o j?i»ic35 onwg a c n ooo . »soS20 o OrMO t C M OOO . O0CO2220 O PROB E I h MS-4- B I n A * ******* PROB E I h MS-4- B Y. 30*200

6 32-6 7 2735

2 3 4 27

4 1 212 £ 21 0 37 2 -0.3 450.

0 505.

3 44 6 50

3 -0.4 32.6 7 2735

2 3 4 27

4 i 212 £ 373. 3 21 0 37

2 -0 3 450.

0 505.

3 44 7 50

4 -0.3 32.6 7 2735

2 3 5 . 27

5 1 2122 3733 21 0 37 2 -O J 4$a o 505 J 44 7 50

4 -O J SMnaseicPneewaj

r &S&
— . 3&S 7 2735

2 3 4 27

4 1 2122 373J 3 21 0 37

2 -0.3 450.

0 505.

3 44 7 50

3 •0.4

Leve l en d Perpendicular Obstructio n Demged a , (-1Cf>

s o^ s + IO"

) O j (-10° S CfeS+10" ) 8 , (-5° * 8,S+5° ) 8 , (-5° S B, S +5" )
r e z = ATany(* s 0.125 - ) W* ATan6(* I 0L03125 T D, (3/1 6 S 0,3 ! 3/8

T A A/20 , (1.05a : PVD, ^ 1.5 )

3 ± > T»T_»a«mptA

j 

### FRSI 1

b ) PI W ai d tapeteMtfan cfc

i >3r

T »3.( r

lCoraHo n o t Prob e place

d h Mtvlea

; kkfVO C Chec k ICompletanet

s . ME W RECONDITIONE D (tircfeon.

)

Ma*ri t and« fifiplt ^ [CwWtedby : Fre d San»«o^/03-lS-aoq g Psrsonoa J (S^nMatM/OaM

) Tea m Lea^(SVyiaJijrWDa»

)



## VE S 0023 9

# ENSR AECO M SAMPL E PROB E CALIBRATIO N DAT A FOR M TYP E "S " PITO TTUB E ASSEMBL YAN D NOZZL E

• _.»K swoos . 32.1 8 27X2 5 3 3 27

4 0 211.

8 373.

0 20 9 37

1 -0.4 450.

0 505.

3 44 4 50

2 -0.7 MS-5-F 32.1 8 273J 5 3 3 27

4 0 211.

8 373.

0 20 9 37

1 •0.4 4S0.

O S0S.

3 44 3 50

1 •O S 

### """"ST — 32.1 8 273.2 5 3 3 27

4 0 211 3 373. 0 20 9 37

1 -0.4 450.

0 505.

3 44 3 50

1 OA * > •» " . ' • 32.1 8 27125 3 3 27

4 0 211.

8 373.

0 20 9 37

1 -0.

4 450.0 505.

3 44 3 50

2 .-0.

7

. ~~~ : t:: 

## - J~^V Leva ) And PoipencSeula

r Obctrucfio n Damage d a, {-10° s q, s + 10*

) 0 * (-10 * S OjS * 10"

) B , (-5° s 8, s +5*

) Bj <-5* S Bj S + S*

) T e 2 = ATanik s 0.125" ) W= ATane(*a:0.03125- ) D | (3/1 6 S D, S 3/8-

) A A/20 t (1.05 S PVD. S 15) N O N o

««tomMnfl

Tth M Calcutt

aZ .

,: oS-rr:"r

. v -i

- ^ T.V",-:*

- |y^3h'
. ^-i ' ft

r -^ f •

3+ 3 

# B H I Q 3 B

M.vdiopKB«i*iDnfli

t Y

•CondUor i a Prob e tYimptaovdhMnteo

: Oft/G O Cher t ComptMane

s _X_
_ wwtfl y tot « wTyp e 8 pI M ubtVpnt w1D*
_ Rt=CONOmOt«~ D (circl e ore ) RattoraMaras s blT^andrbrapptal^Oes^

Pereonne l {S^mknOale

) Tea m Leado r (SJgnature/O**

) U nnsitici ^ cdtetl

a i wanlsclale d EPAS0CVR-MD3BC

. Sepumberl99

4

NOTES :

# ENS

R Calibrator : Rya n Bum s Referenc e Thremomete r ID : PV M CCL0501S241 7 Date : 3/6/200 6 Las t Impinge r Thermocoupl e Calibratio n 200 6 I Thermocoupl e Referenc e Differenc e (+/ - 2° ) Thermocoupl e Referenc e Differenc e (•*£2° ) LI- 2 Ho t 21 2 21 2 0 U-2 1 Ho t 21 1 21 1 0 LI- 2 Col d 1 3 3 3 2 1 U-2 1 Col d 3 3 3 2 1 Manufacturer . Anderso n NUTEC H Manufacturer . Anderso n NUTEC H Seria l NO J Seria l No. : Date receivedWace d i n service : Pr e 199 0 Dat e receiveoVplace d i n service : Pr e 199 0
L M Ho t 21 1 21 1 

### I O U-2 2 Hot 21 3 21 2 1 L M Col d 3 3 3 3 

### I 0 U-2 2 Col d 3 5 3 3 2 Manufacture r Anderso n NUTEC H Manufacture r Seria l No. : Seria l No : Dat e received/place d i n service : Pr e 199 0 Dat e received/place d h service : Pr e 199 0
U- G Ho t 0 U-2 3 Hot 21 1 21 2 - 1 U- G Col d 0 U-2 3 Col d 3 5 3 3 2 Manufacture rAnderso n NUTEC H Manufacturer : Anderso n NUTEC H Seria l No. : Seria l No. : Dat e reeled/place d I n service : Pr e 199 0 Dat e received/place d i n service : Pr e 199 0
U- 7 Ho t 21 2 21 2 0 U-2 4 Ho t 0 U- 7 Col d 3 3 3 2 1 U-2 4 Col d 0 Manufacturer . Anderso n NUTEC H Manufacture rAnderso n NUTEC H Seria l No. : Seria l No. : Dat e received/placed i n service : Pr e 199 0 Dat e received/place d i n service : Pr e 199 0


### u- s Ho t 21 2 21 2 0 U-2 5 Ho t 21 2 21 2 0 

### u- s Col d 3 4 3 3 1 U-2 5 Col d 3 3 3 2 1 Manufacture rAnderso n NUTEC H Manufacture r Anderso n NUTEC H Seria l No. : Seria l No. : Dat e received/place d i n service : Pr e 1990 Dat e received/place d i n service : Pr e 199 0
L W Ho t 21 1 21 2 - 1 U-2 6 Ho t 21 4 21 2 2 L W Col d 3 3 3 3 0 U-2 6 Col d 3 5 3 4 1 Manufacture rAnderso n NUTEC H Manufacture r Anderso n NUTEC H Seria l No. : Seria l Na : Dat e recetvedtotace d i n service : Pr e 199 0 Dat e received/place d i n service : Pr e 199 0
U-1 0 Ho t 21 2 21 2 0 H-2 7 Ho t 21 0 21 2 - 2 U-1 0 Col d 3 2 3 2 0 H-2 7 Col d 3 4 3 3 1 Manufacture r Manufacturer . Anderso n NUTEC H Seria l No. : Seria l No. : Dat e receivedWace d i n service : Pr e 199 0 Dat e received/place d i n service : Pr e 199 0
U-1 1 Ho t 0 U-2 8 Ho t 21 2 21 2 0 U-1 1 Col d 0 U-2 8 Col d 3 3 3 3 0 Manufacture r' Anderso n NUTEC H Manufacturer : Anderso n NUTE C • 1 Seria l No. : Seria l No. : Dat e received/place d i n service : Pr e 199 0 Dat e received/place d i n service : Pr e 199 0
LI-1 2 Ho t 21 1 21 2 - 1 U-2 9 Ho t 21 2 21 2 0 LI-1 2 Col d 3

2 3

2 0 U-2 9 Col d 3 3 3 3 0 Manufacture r Anderso n NUTEC H Manufacture rAnderso n NUTEC H Seria l No. : Seria l No. : Dat e received/place d i n service : Pr e 1990 Dat e received/place d i n service : Pr e 199 0
U-1 3 Hot 21 3 21 2 1 H- 5 Hot 21 3 21 2 1 U-1 3 Col d 3

3 3

3 0 H- 5 Col d 3 4 3 3 1 Manufacture r Anderso n NUTEC H Manufacture r Anderso n NUTEC H Seria l No. : Seria l No. : Date received/place d i n service' . Pr e 1990 Dat e received/place d i n service : Pr e 199 0
LI-2 0 Ho

t 21 1 21 1 0 U-1 4 Ho t 21 1 21 1 0 LI-2 0 Col d 3

4 33 1 U-1 4 Col d 3 2 3 3 - 1 Manufacture r Anderso n NUTEC H Manufacturer . Anderso n NUTEC H Seria l No. : Seria l No. : Date received/place d i n service : Pr e 199 0 Dat e received/place d i n service : Pr e 199 0 J

### ENS R AECO M

cum x FradSMguadofc a MnmlManorMW : RufcaftTOaisioa s FitterBo xCalibritkx i Ho t B A # 1 Ho t Bo xM l Manufacture

rAndwsonriUibuH StMHai W A ^mc*todbtK*dbi«anfc

* PM109 5 tanutacajren Anderso n NUibU H MfWHc u W

A Maracatadtotar^lhaaraia

t PraWS S Calibratio n Dote : IG-ftb- K ^Bfibratto n Data : ife^aorO

S AmbJon t Ho t Anbian t Ho t m m M M TllllwWl

W M 

### « r" 7 2 9*

8 

### —a — 34

6 c4afT«np*afum 7 1 0 •mpOB**ne*flDt»«-3 J 1 Hotf i 0X«2 HotBo x#12 UawhKtura

n Anderso

n NUTEC H pa wwMtiwdfphca

d n—wfc » Pr»i«9 5 tonutactuten Ardarsc n NUTEC H SmMNoJl

W

A Jataractfcwltra^fcaan**

: PrtlW S imitatio n Date

: I 15-f*b-0

6 ^IbraUo

n Dak K 1G-Feb-«

6 1 Ambien

t Ho t Arabian t Ho t MmncaTamMtahaa

* 1 6 B 2*

8 RM4TMKaTampcim

M 7

0 Ae*jarT«<KMn*un

M | TO 2* 7 Vdut t Tafnyaralu — 7

1 24

7 2 r<nn » DAMM M (ta t ••• a •

1 •

1 Ho t BO X< S Ho t B S X61 3 Uantfacturor

: Anootjo

n NUTEC H MlniiaCaJW

: Aixter

WNUTEC H SeWNo j W

A 16-FatH S fixatio n Data: 16-F«b4 6 Ambien t He * Ambien t I Ho t Mmnc * T*rnpMfcm

a 6

9 

### •••« r W«nno i Tut p wrmma •0

7 

### j 2*

8 HctoeiTiiV—

— 6

0 A

W MualTamparau

m 6

7 I 3*

6 r«n^CMaraK*fioi.«*-2

) 0 0 TampDBannc * paL<a4-2 } 0 | 0 Hot e Ho t Bo x61 4 Manutacvw

: Anderso

n NUTEC H Msntfacfcnr

. And»r»c

n NUTEC H seNNo j W

A r^raoMwVrAc^hMfwIc

KPmlftB S Calibratio n Date : UTibratio n Date: 16-f «

•b-0 6 Um m Tampanam

i Ambien

t Ho t Ambien t Ho t Um m Tampanam

i Tl 24

4 WarancaTewipaiaiw*

* 6

6 24

7 Tampanam 7

1 ac

s Tam p DRaranc a (ta i n-*-a ) 7 0 2*

7 • T«m e OHmnc a 0DL « 0 1 Tam p DRaranc a (ta i n-*-a ) - 2 0 Ho t Bo x« S Ho t Bo x«1 5 Uanufactrer

: Anderso

n NUltC H laantfacbra

n Anderso

n NUTEC H SarWHo j W

A [^roMft>teadta**vfca : Pm199 5 Vibration Dato

e l6-F*O-0

6 Miratio n Data: 15-ftb-o e Ambien t ( Ho t MmmTMiiMraii i wcuilTcnkpfok

m tam p ORaranc * do t ••< ) Ambien

t I Ho t 6 6 | 2S

1 MmmTMiiMraii i wcuilTcnkpfok

m tam p ORaranc * do t ••< ) 6 6 2*

7 6 8 | K

2 MmmTMiiMraii i wcuilTcnkpfok

m tam p ORaranc * do t ••< ) 6 6 24

7 0 ( -

1 MmmTMiiMraii i wcuilTcnkpfok

m tam p ORaranc * do t ••< ) 2 

### 1 0 Ho t Bo x# 6 Ho t Bo x« 6 Marufactxe

n Seria l No: r^r*cihid**K»tltoa»r*jc « Anderso n NUTEC H W A Pl»199 5 Uwufacfirer . Anderso

n NUTEC H S«MN0 J W

A D«MrK«*«dfe*^ha*nrfca: Pr»199 5 Calibratio n Dea r 1SM « Calibratio n Date : 17-£eb-0

6 Mmrn>T«n9*mun

w taa^Tmp^naum Ambien t Ho t Ambian t t Ho t Mmrn>T«n9*mun

w taa^Tmp^naum 6 9 24

5 Mntc t Teavattee

a 7

1 24

T Mmrn>T«n9*mun

w taa^Tmp^naum 

### 1 | - « 5 4d^ToapiMUJM rawORwaraltoL***

) e t 34

1 Mmrn>T«n9*mun

w taa^Tmp^naum • 1 0 4d^ToapiMUJM

rawORwaraltoL***

) 2 0 Ho t Soxt T Ho t Bo x#17 ManufactUTo

n Anderso

n NUlfcC H SarUNo : N

M 0&r*c-tt*dtil*xd\j<****

PralflP

S lAanufacare n Anderso

n N O ifcO H 5afafNr> J W

A DataracahwitoMwatfataafvie*

: PralM S Calibration Dale: 1 16-Fab-0 6 Catenatio

n Dank : le-FetH K AfSuj fTtftlpanlUn

* Ambtan

t Ho t FWMM

« Tamp«ut*» Ambien

t Ho t AfSuj fTtftlpanlUn

* 7

1 24

6 FWMM

« Tamp«ut*» 6

9 M

S AfSuj fTtftlpanlUn

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n Data : 16-FatH

M Batawoc a Twywir w *<^T«rrifwam » Ambien t Ho t Ambfen t 1 Ho t Batawoc a Twywir w *<^T«rrifwam » 6 9 24

9 7 0 

### j 24

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# ENS R AECO M

XA D Thermocoupl e Calibration s - 200 6 dat e 3/13/200 6 BP : 29. 1 

### Reference Thermomete r ID# : Manufacture : Dat e place d i n Service : Calibrator : Jame s Ruckdesche l Ambien t Tem p (F) : 6 3 Fluk e Digita l RT D 213103

5 Fluk e Pre 198 0 | Ic

e Bat h Ambien t | | Thermocouple ID # Referenc

e Tem p XA D

Tem p Tem p

Differenc e ToI = +-2 F 

### Referenc e Tem p XA D

Tem p Tem p |

Differenc e j TO I = +-2F | XAD- 1 3 3 3 2 - 1 6 2 6 2 0 XAD- 2 3 3 3 3 0 6 2 6 3 1 XAD- 3 3 3 3 1 - 2 6 2 6 2 0 XAD- 4 3 1 3 1 0 6 3 6 3 0 XAD- 5 3 1 3 3 2 6 3 6 3 0 XAD- 6 3 2 3 2 0 6 3 6 3 

## o XAD- 7 3 2 3 2 0 6 4 6 4 0 XAD- 8 3 2 3 2 0 6 5 6 3 

### XAD- 9 0 

# ° XAD-1 0 3 2 3 2 0 6 6 6 4 - 2 XAD-1 1 0 0 XAD-1 2 0 

# I 0

### ENS R



# Appendi xD Stac k Configuration , Samplin g Por t an d Travers e Point Location s

Se|*ember2006 S:\_JO»2006Wny)^e!foimara ^ Tes i Report.do

c


## VE S 00239 !GROUN D LEVE L



### ENS R
ENS RCORPORATIO N 660 1 Wrkvtl U Rood E M Syroeun . M«

wYork 1305 7 AECO M 

### "FIXE D HEART H INCINERATO R UN I I 3 VEOLI A E S TECHNICA L SOLUTION S

Sound
. tlUnot

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W W reOJECTHUMGO b
_ 10002-01 7 1 O F 1



## VE S 00239 6

## TRAVERS E POIN TLOCATION

S (Particulat

e Travers

e - Circula rStack

)

FACILTY : STAC KIDENTIRCATION : STAC KDIAMETER : SAMPLIN G LOCATIONS :
MINIMU M NUMBE R O F TRAVERS E POINT S A S SPECIFIE D BYEP A METHO D 1 : Ony xEnvironmental Services Uni t 3 39 inche

s 14.9 5 diameter

s downstream 9.8 5 diameter

s upstream
1 6
NUMBE R O F TRAVERS E POINT S SAMPLED : 1 6

Traverse Poin

t Percent o

fStac k Diameter NumberFrom Insid e Wal l Distanc e i n Inche

s Fro m Inside Wall * 1 3.2 1. 2 2 10. 5 4. 1 3 19. 4 7. 6 4 32.3 12. 6 5 67.7 26. 4 6 80.6 31. 4 7 89.5 34. 9 8 96.8 37. 8

* Fo rstack

s wit h a n inside diameter (ID ) o f24 inche

s orless , n

o travers e poin t ma y b e locate d withi n 0.5 inches o

fthe inside wall . Forstack s wit h a n ID greate r ma n 24 inches , n o travers e poin t ma y b e locate d withi n 1.

0 inche s o fth e insid e wall . Anypoin

t no t meetin g the criteri a shal l b e adjusted .

# ENS R

Appendi xE Laborator

y Dat a

jo»2006\Dr^erkKmanceTe ^ TestRepoitdo c September200 6ENS R AECO M

" 574.772^34 5 f 97S.7T2,jgj g <uwv«SRsr.s*ee m CL- m

ENS RAi r

Toxic s TS PLaborator y Analytica l Repor t

Client : Jef f Gorma n ENS R 660 1 KirkvffleRoa d E . Syracuse , N Y1305 7 Clien t ID : 10002-01 7

Laborator y ID : 06-06 7 Dat e Received : 5/12/0 6

Al l wor k containe d i n thi s repor

t ha s bee n don

e i n accordanc

e with laborator

y standar d operating procedures. ENSR' s Ai r Toxics TS P Laborator

y follow s methodologie

s base d upon standar

d EPA/NIOSH/OSH A Methods . Dat a containe

d herei n shoul d b e considere

d accurat e an d complet

e t o th e bes t o fou rknowledge. Thi s repor t canno t b e duplicate

d i n par t wimou t th e written permission o fENSR .

Arthu r Carpetuto 7 Laborator

y Analys t ENS R Ai rToxics TS P Laborator y Dat e

NYSDOH /

NELA C # 1163

1

pag e 1 o f6



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.PROJEC TNARRATIV E Maxxa m Analytic s (Bnrttagto n ON ) Maxxa m Jo b ft A64446 9 Oust : ENSRIiiternatiosa l C&r t Project : 10092-017-01 7 ONY X t SAMPL E RECEIPT/ANALYSI S
a ) Sample Listin g AtVrrn m CKen t Date Dat e • Date Dat e I D Sampl e Q > Sampled Receive d Preppe d Rmt 

### Mercury IB via EPA Method

29 isms TJ3-M29-R B 06705/1 0 06705/1 2 06705/1 7 06705/1 8 L99829 U3-M29-R 1 06705/1 0 06705/1 2 06/05/1 7 06705/1 8 L99S30 U3-M29-R 2 06705/1 0 06705/1 2 06705/1 7 06705/1 8 L99S3 1 U3-M29-R 3 06705/1 0 06705/1 2 06705/1 7 06705/1 8 

### Mercury 2B via EPA Method

29 L9982 8 U3-M29-R B 06705/1 0 06705/1 2 06705/1 6 06705/1 6 L99829 TJ3-M29-R 1 06705/1 0 06705/1 2 06705/1 6 06705/1 6 L99830 TJ3-M29-R 2 067D5/1 O 06705/1 2 06/05/1 6 06705/1 6 L9983 1 U3-M29-K 3 06705/1 0 06705/1 2 06705/1 6 06705/1 6 

### Mercury 3A via EPA Method

29 L99828 U3-M29-R B 06/05/1 0 06705/1 2 06705/1 5 06705/1 6 L99829 U3-M294 U 06705/1 0 06705/1 2 06705/1 5 06705/1 6 L99830 U3-M2941 2 06/05/1 0 06705/1 2 06/05/1 5 06705/1 6 L9983 1 XJ3-M294 Q 06705/1 0 06705/1 2 06705/1 5 06705/1 6 

### Mercury 3B via EPA Method

29 L99828 U3-M294 © 06705/1 0 06705/1 2 06705/1 5 06705/1 6 L99829 U3-M294 U 06705/1 0 06705/1 2 06705/1 5 06705/1 6 L99830 U3-M29-R 2 06705/1 0 06705/1 2 06705/1 5 06705/1 6 L9983 1 TJ3-M29-R3 06705/1 0 06705/1 2 06705/1 5 06705/1 6 

### Mercury 3C via EPA Method

29 L99828 U3-M29-R B 06705/1 0 06705/1 2 06705/1 6 06705/1 8 L99829 TJ3-M29-R 1 06705/1 0 06705/1 2 06/05/1 6 06705/1 8 L9983 0 06705/1 0 06705/1 2 06705/1 6 06705/1 8 L9983 1 U3-M29-S 3 06705/1 0 06705/1 2 06705/1 6 06705/1 8 

### Metals in Air (Combined)

via EPA Method29

(ICP/MS) L99828 TJ3-M29-R B 06705/1 0 06705/1 2 06705/1 7 06705/1 9 L99829 U3-M29-R 1 06705/1 0 06705/1 2 0670571 7 06705/1 9 L9983 0 U3-M29-R 2 06705/1 0 06705/1 2 0670571 7 06/05/1 9 L9983 1 U3-M29-R 3 06705/1 0 06/05/1 2 06705/1 7 06705/1 9 Ra n Dat e i s define

d a s di e dat e o finjectio n o fthe las t calibratio n slanrlar

d (1 2 honrso

Tless ) prio r to tne sajnple

s analyze

d wnliinriatnmD ^quence . Thexd^fl^timeofau%ratio n injectio n titatdefmes di e TO Tdat e i s alwa^w ^ b ) Shippin g Problems : none encountere d
c ) Dccomentatio n Problems : none encountere d 

### J H Page l o f2I L SAMPL E PREP : N o problems encountere d O L SAMPL E ANALYSIS : Se c also comment

s withi n the appropriat

e Certificat

e o fAnalysi s a ) HoMTin^aUwithfarecorrm»en ^ b ) Instininea

t Calibration ; a U wulnncuiUru l limits c) Qualit y Control : Al l applicabl e Q C meet s contro l criteria , excep t wher e otherwis

e noted . I certif y tha t thi s dat a packag e i s i n complianc

e wit h the tenn s an d condition s o fthe contract, both ttxhm'calr y an d fo rothe r tha n the condition s detaile d above . L i addition , I certify , tha t to di e bes

t o fnrylowwledge an d belief ; tne dat a a s tepc ^ ar

e true an d acenrate

. Releas e o ftb e dat a containe

d i n fins dat

a packag e ha s been authorize

d by th e cognizant laborator

y officia l o rhis/he rdesignee, a s verified b

y thi s signature.

Mary

### J H Pag e 2 o f22 . DAT A SUMMAR Y
Certificat e o fAnalysi s -
Sampl e analyt e result Metho d blan k result LC S Result

s with ' % Recoverie

s Matri xSpik

e dat a wit h % Recoverie

s Matri xSpik

e Duplicat

e dat a wit h % Recoverie

s Surrogat e recoverie

s

# tVI 

# a 

# *2 Si 

# m . Driven by service

and Science -vvw^maxxatennaljites^coin

You rProject* : 10002-017-01 7 Site : ONY X
Attention : JeffGorma n ENS R Internationa

l 6601KkkviileR d Eas t Syracuse

, N Y US A 1305

7 Repor t Date : 2006/05/2

0
CERTIFICAT E O F ANALYSI S MAXXA M JO B # : A 64446 9 Received : 2006/05/12,12:0 0 Sampl e Matrix : Filte r # Sample s Received : 4 Analyse s Quantit y Dat e Entractc d Dat e Analyze d Laborator

y Metho d MeOo d RicfclCIMA i Mercur y I B -Ai r (Fitter*Acetone

) by CVA A$ Menu s i nAi r (Combined

) b y ICP/M S « 2006/05/1 7 2006/05/1 8 SOPIN G11 1
. 2006705/1 7 2006705/1 9 SO PIN G108/10 9 EP ACF RPT M 2 9 EPASW846-602 Q Sampl e Matrix : Impinge

r Solution # Sample s Received : 4 Analyses Quantit y Dat e Extracte d Dat e Analyze d Laborator

y Metho d Metho

d Mercur y 3 C in Af r(HC I Impinger ) b y CVA A 0 Mercur y 3 A i n Ai r(HN0

3 Rinse ) b y CVA A 6 Moon y 2 B io AjrCHN03/H20

2 nop ) b y CVA A 0 Mc«cuiy3BioAir(KMiiO4/B2S04)byCVAA $ 4 2006705/1 6 2006705/1 8 SOPIN G11 1 4 200670S/1 S 2006/05/1 6 SOPIN G11 1 4 2006705/1 6 2006705/1 6 SO PIN GII I 4 200*05/1 5 2006*5/1 6 SOPIN G11 1 EPACFRPTM2 9 EPACFRPTM-2 9 EPACFRPTM2 9 EPACFRFIM2 9 (1 ) Thi s tes

t wa s performe

d b y Maxxa m Analytic

s Burlington
YTIC S IN C

MARY-ANN E JOHNSON , B.A , BSc. Projec t Manage r MAJ/ma j end
.

Pag e I o f1 1
674 0 Campobello Road . Mississauga , Ontario Canad a L5N2L8 Tel : 905-817-570 0 Tol l free:800-563-626

8 Fax:905-817-577

7



## VE S 00240 !t >».»>

» lyric * m c Driven ta - service mid Selene wwr.m«i»n »»»»»aytte-<=» , i You rProject * 10002-017-01 7 "Site : ONY X

Attention : Jef

fGorma n ENS R Internationa

l 660lKirkvilleR d Eas t Syracuse

, N Y US A 1305

7 Repor t Date : 2006705/2

0

nranWCAJ Eo p ANALYSI S

-2 -

VaHdatedby :

Tota l cove rpages : 2

874 0 Campobell o Road . Mississauga , Ontario Canad a LS N 2L 8 Page2of1 1 Tel : 905-817-570

0 Tol l free:800-563-626 6 Fax : 905-817-677

7



## VE S 00240 6Maxxa m Job £A64446 9 Repor t Date : 2006/05/2

0 Driven by service

and Science OiS R Internationa

l Cfien t Projec t fr. 10002-017-01 7 Projec t name: ONY

X Sample r Initials : MERCUR YB YCOL O VAPOU R A A (FILTER ) Maxxa m I D L9382 8 L9982 9 L9S82 9 L9983 0 LS983 1 SampSn q Dal e 200670511 0 2006705/1 0 2006/05/1 0 2006V05i1 0 2006/05/1 0

JnH s U3-M29-R B U3-M29-R 1 U3-M2S-R 1
' Lab-Du o U3-M29-K 2 U3-M23-R 3 RD L Ct C Batc h HD L [Tota l Merctny-1 B I u

g , | tW

~ 0.27 {9.03 | 97239 5 |o.o 7

N D N D 0.1 0 W D = No

t detecte d |RD L = Reportabl e Detectio n Uml t (QC Batc h = QuaBt

y Cootro l Batc h

Pag e 3 o f1 1 674 0 Campobello Road , Mississauga, Ontari o Canad a L5N2L 8 Tel : 905-317-570 0 Td l tree:S00-563-626 e Fax:905-817-577

7



## VE S 0024 0Maxxa m Job #:A64446

9 Repor t Date : 2006V0572

0 " ' Driven

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gad Science ENS R Intamabbna

t Cfien t Projec t #: 10002-017-01 7 Projec t name: ONY

X Sample r Initials : 

## ELEMENT S B YICP/M S (FILTER ) Maxxa mI D L9982 8 L9982 9 L9982 9 L9983 0 13983 1 Samplin qDat a 2006705/1 0 2006705/1 0 200670571 0 2006705/1 0 2006705/1 0 inlt s U3-M2S-RB U3-M29-R 1 U3-M23-R 1 Lab-Ou p U3-M23-R 2 U3-M29-R 3 RD L S C Batc h MDL
Tota l Arseni c (As ) « S 0.7 6 &2 9 9.6 2 24 9 94 6 0.4O
. 97201 2 0.40 Tota l BeryBu m(Be ) U3 NO ND N D N D N D D.1 0 97201 2 0.1 0 Tota l Cadmiu m(Cd ) u g 03 4 0.6 8 0.7 1 13 8 27 6 3.1 0 97201 2 0-1 0 Tota l Chiomium(Cr) u g 1.0 1 17. 7 19, 8 29. 0 55 3 13 0 97201 2 03 0 Total'Laa d(Pb ) ug :
- 2.7 0 23. 9
. . "24. 1 22. 3 40. 6 97201 2 ND=No t detected RD L= Reportable Detectionlimi t Q C Batc h= QuaHy Contra)'Batch

Pag e 4 o f 1 1
674 0 Carnpobello Road , Mississauga , Ontario Canad a L5N2L 8 Tel : 905-817-570 0 Tol l frae:800-563-626 6 Fax : 905-817-577

7



## VE SJBrtven by service

and Science Yvww.maxacamanalyticS'Coi n ENS R Internationa

l Clien t Projec t #: 10002-017-01 7 Projec t name: ONY

X Sample r Initials : 

## MERCUR YB YCOL D VAPOU R A A (IMPINGE

R SOLUTION

)
Maxxam I D L9982 8 LB982 9 L9982 9 SarisGns

j Date 2006705/1 0 2006705/1 0 2006705/1 0

Jnit s U3-M2S-R B RD L U3-M29-R 1 U3-M29-R 1 UUU D RD L 3 C Batc h MD L
Tota l Meicury-2 B U S N D 0 3 74. 7 • 75. 4 1 3 97009 1 03 1 Tota l Mercur/-3 A u g N D 93 1 33 8 3.4 0 9.1 3 970045 0.06 Tota l Metcuy-3 8 u g 0.04 0.O 2 10. 7 10-7 0 3 97006 6 0.0 5 Tota l Meroury-3 C u g N D 3.05 8.5 5 83 8 97132 2 0.0 5 MD = No t detected F^=Reportabl e Oeted m Uni t Q C Batc h = QuaB y Contro l Batc h 

## Teti • 1t.oZ

Maxxam I D L9983 0 L9983 1 SamrJin a Dat e 2006705/1 0 2006/05/1 0

Unit s U3-M29-R 2 RD L U3-M23-R 3 RQ L 2 C Batc h HD L Tota l Mercury-2 B " 9 104 1. 7 78. 6 1 3 97009 1 03 1 Tota l Merctny-3 A u g 12 9 9.0 2 12 6 9.0 2 97004 5 0.0 5 Tota l Metcury-3 B u g 73 9 92 5 13f i 9.05 97006 6 03 5 Tota l Mercury-3 C u g 73 5 92 5 7.7 0 92 5 97132 2 03 5 RD L - Reportabl e Detectio n Limi t Q C Batc h = QuaSt

y Contro l Batc h 

## IV I st yCyisi m . Maxxa m Jo b #:A64446

9 Repor t Date : 2006/05/2

0

Pag e 5 of1 1 674 0 Campobell o Road , Mississauga, Ontario Canad a L5N2L 8 Tel : 905-817-570 0 Tel ! free:800-563-626

5 Fax:905-817-577

7



## VE S 00240 S

# IV

I axoc s m . f^^r Anjtlytlc l »*»

< Maxxa m Job # : A64446 9 Repor t Date : 2006705/2

0 Driven by service

a>ul Science ENS R Internationa

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X Sample rInitials : DaTytlcs.co m



### Tes t Summar

y
Maxxa m I D L9982 8 Collecte d 2006705/1 0 Sampl e I D U34«29-R B Shippe d Matri x Filte r Receive d 2006705/1 2 Tes t Descriptio n tnstrumentaflo n Batc h Prepare d Analyzed 1 . Artafvt t Mercur y 3 C i n Ai r(HC I Imoinqer t b vCVA A CVA A 97132 2 2006705/1 6 200S7D5/1 8 FF S Mercury . 3 A i n Ai r(HN0 3 Rinse) bvCVA A CVA A 97004 5 2006705/1 5 2006705/1 6 FF S • Mercur y 2 8 i n AHHN03/H2Q 2 Imp ) b vCV A CVA A 97009 1 2006/05/1 6 2006705/1 6 FF S Mercur y 3 B i n Air(KMrO4/rlZS04)byCV A CVA A 97006 6 2006/05/1 5 2006705/1 6 FF S Mercury I B ^Ai r(FJter+Acetcne ) b vCVA A CVA A 97239 5 2006/05/1 7 2006705/1 8 FF S Metal s i n Ai r/Combined ) b vICP/M S .- tCPI/M S 97201 2 2006/05/1 7 2006705/1 9 N R
Maxxa m I D L9982 9 Collecte d 2006705/1 0 Sampl e I D U3-M29-R 1 Shippe d Matri x Fitte r Receive d 2006705/1 2 Tes t Descriptio n Ins b lanenlatio n Batc h Prepare d Analyze d Analys t Mercur y 3 C I n Ai r(HC I Impinger ) b vCVA A CVA A 97132 2 2006705/1 6 2006705/1 8 FF S Mercur y 3 A i n Ai r(HN0 3 Rinse) b vCVA A CVA A 97004 5 200670571 5 2006705/1 6 FF S . Mercur y 2 B I n Alr(HNO3/H202lmp ) bvCV A CVA A 97009 1 2006705/1 6 2006705/1 6 •FF S Mercur y 3 B i n Ai r(KMn04/H2S04 l bvCV A CVA A 97006 6 2006/05/1 5 2003/05/1 6 FFS . •• Mercur y 1B-Al r(FBtar+Acetone ) bvCVA A CVA A 97239 5 2006705/1 7 •2006705/1 8 ,• - FF S • Metal s i n Ai r(Combined ) b vICP/M S ICP1/M S 97201 2 2006705/1 7 -2006705/1 9 N R
Maxxa m I D L99829Du p Collecte d 2006705/1 0 Sampl e I D U3-M294 M •Shippe d - Matri x Filte r Receive d 2008705/1 2 Tes t Descriptio n instrumentatio n Batc h Prepare d Analyze d Analys t Mercurv3CmAtrfHaimrtrKiertrjvCVA A CVA A 97132 2 2006705/1 6 2006705/1 8 -FF S Mercur y 3 A I n Ai r(HN0 3 Rinse) b y CVA A CVA A 97004 5 2006/05/1 5 2006705/1 6 •.FF S Mercur y 2 8 i n Air/HN03/H20 2 Imp ) b y CV A CVA A 97009 1 2006705/1 6 2006705/1 6 FF S • Mercur y 3 B i n Ai r(KMn04/H2S04 ) n vCV A CVA A 97006 6 2006/05/1 5 -2006705/1 6 " FF S Mercur y 1 B -Ai r(Riter+Acetone ) b vCVA A CVA A 97239 5 2O06705/1 7 2006705/1 8 FF S Metal s i n Ai r(Combtrted) bvtCP/M S 1CP1/M S 97201 2 200670571 7 2006705/1 9 N R
Maxxa m I D 13983 0 Collecte d 2006705/1 0 Sampl e I D U3-M2&R 2 Shippe d Matri x Fite r Receive d 2006/05/1 2 Tes t Descriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t Mercur y 3 C i n Ai r(HC I Impinger ) bvCVA A CVA A 97132 2 200670571 6 2006705/1 8 FF S Mercur y 3 A i n Ai r(HN0 3 Rinse) b vCVA A CVA A 97004 5 2006705/1 5 2006105/1 6 FF S Mercur y 2 B I n AWHN03/H20 2 fens) bvCV A CVA A 97009 1 200670571 6 2006/05/1 6 FF S Mercur y 3 B i n Ai r(KMn04/H2S04 l bvCV A CVA A 97006 6 2006/05/1 5 2006705/1 6 FF S Mercur y I B -Ai rffHter+Acetone) b vCVA A CVA A 97239 5 2006705/1 7 2006/05/1 8 •FF S Metal s h Ai r(Combined ) b y ICP/M S ICP1/M S 97201 2 2006705/1 7 2006/05/1 9 N R

t

i Pag e 6 o f1 1 j i 874

0 Camppbelt

o Road , Mississauga, Ontario Canada L5 N 2L 8 Tel : 905-817-570

0 Tpl l free;800-563-626 6 Fax : 905-817-577

7



## VE S 00241 C

# WA

# a ^? a 

# m . I Analytic * In c Maxxa m Jo b #:A64446

9 Repor t Date : 20067050

0 Dl L\Jbgp

g4j ouil

ScfCnve ENS R Internationa

l Clfcii t Project* : 10002-017-01 7 Projec t name : ONY

X Sample rInitials : Tes t Summar

y
Maxxa m I O Sampl e I D Matri x L9983 1 U3-M29-R 3 Filte r Collecte d Shippe d Receive d 2006705/1 0

2006/05/1 2 Tes t Descriptio n tns b inne r ilutlo n Batc h Prepare d Analyze d Analys t Mercur y 3 C i n Ai r(H Q ImDlrwertbvCVA A CVA A 97132 2 '2006/05/1 6 2006705/1 8 1+ 8 Mercur y 3 A m Ai r(HN0 3 RSnse l bvCVA A CVA A 970045 2006705/1 5 2006/05/1 6 FF S Mercur y 2 B I n AWHN03/H2Q2 lmp > b vCV A CVA A 97009 1 " 200670571 6 2006705/1 6 FF S Mercur y 3 B i n ArriKMn04/H2SD4 ) bvCV A CVA A 97006 6 . 2006/05/1 5 2006/05/1 6 FF S Mercur y I B -Ai rfFBter+Acetone i b vCVA A CVA A 972395 2006/05/1 7 2006705/1 8 FF S Metal s k l Ai r(Combiners ) bvJCP/M S ICP1/M S 972012 - 2006705/1 7 2006705/1 9 N R

Page7o f1 1 674 0 Campobello Road , Mississauga , Ontario Canad a L5N2L8 Tel : 905-817-570 0 Tol l free:80fr5r)3-626 6 Fa r905-817-577

7



## VE S 00241 'ENS R Internationa l Clien t Projec t ft 10002-017-04

7 Projec t narrie:C>NY

X Sample r Initials : Driven by service

and Scf ate* www.maxxauttftnslyTlcs^coi n Maxxa m Jo b £A64446 9 Repor t Date : 2006705/2

0

GENERA L COMMENT S ICPttS:Po£tfgestfcmdup& ^

• I Result s rotate onl y t o th e Item s tested.

Pag e 8 of1 1 674 0 Campobello.Road , Mississauga , Ontario Canad a LSN2L 8 Tel : 805-817-570 0 Tollfree:800-563-626

6 Fax : 905-817-577

7



## VE S 0024 1

# tVIcE l f

# ^ am . «rivw.naxxam«»nlytScxueoB » . . Driven

by service

and Science fcPJSKinternationa

l Attention : Jef

fGorma n Clien t Project s 10002-017-01 7 P.O.* : Projec t name: ONY

X Qualit y Assurance Repor

t Maxxa m Jo b Number . GA64446 9 QA/Q C • NumH t QCTvp e Paramete r Dat e Analyze d ww/mm/d d Valu e ^Recover y Units Q C Limits 97004 5 FF S MATRI XSPIK E

(I39829) ' Total Mercury-3 A ' 20067050 6 0.00 , ROL=0.1 3 102 u g 85-11 5 MATRI XSPIK E OU P 039829 ) Tota l Mercury-3 A 2006/05/1 6 0.O0 , RDL=0.1 3 105 u g 85-11 5 Spike d Blan k

. Tota l Mercury-3 A 2006/05/1 6 0.11 , RDL=0.0 1 10 6 u g 90-11 0 Spike d Blan k

OU P Tota l Mercury-3 A 2006705/1 6 0.11.RDL=O.0 1 10 7 u g 90-11 0 Metho d Blan k Tota l Mercur/-3 A 2006/05/1 6 ND . RDL=03 1 u g RP O Tota l Mercury-3 A 2006705/1 6 0 3 % 2 0 97006 6 FF S MATRI XSPIK E 85-11 S

(159829 ) Tota l Mercury-3 B 2006705/1 6 03 , RDL=0. 5 10 $ u g 85-11 S MATRI XSPIK E 85-11 5 DU P (199829

) Tota l Mercury-3 B 2006/05/1 6 03 . RDL=0 3 107 u g 85-11 5 Spike d Blan k Tota l Mercury-3 B 2006705/1 6 035 . RDL=0.0 5 11 0 u g 90-11 0 Spike d Blan k

OU P Tota l Mercury-3 B 2006705/1 6 034,RDL=0.0 5 108 u g 90-11 0 Metho d Blan k Tota l Mercury-3 B 2006705/1 6 ND . RDL=03 5 : u g RP D Tota l Mercury-3 B 2006705/1 6 0.05 % 2 0 97009 1 FF S MATRI XSPIK E

(L99829 ) Tota l Mercury-2 B 2006/05/1 6 03 . RDL=1. 6 10 0 u g 85-11 5 MATRI XSPIK E •U P (L99829

) Tota l Mercury-2 8 20067050 6 03 . RDL=1. 6 9 5 u g 85-11 5 Spike d Blan k Tota l Mercury-2 B 2006/05/1 6 0.11 , RDL=O-0 1 10 7 u g 90-11 B Spike d Blan k

DU P Tota l Mercury-2 B 2006705/1 6 0.11 , RDL=O.0 1 109 u g 90-11 0 Melho d Blan k Tota l Marcury-2 B 2008/05/1 6 ND , RDL=03 1 u g 2 0 RP D Tota l Mereurjr-2 B 2006705/1 6 0. 9 % 2 0 97132 2 FF S MATRI XSPK E 85-11 5

(L99S29 ) Tota l Mercury-3 C 2006705/1 8 034,RDL=03 5 10 8 u g 85-11 5 MATRI XSPIK E 85-115 . DU P 0-99829

) Tota l Mercury-3 C 200670571 8 0.54 , RDL=0.2 5 10 6 u g 85-115 . Spike d Blan k Tota l Mercury-3 C 2006705/1 8 0.51,RDL=O.0 5 102 ug . 90-11 0 Spike d Blan k

OU P Tota l Mercury-3 C 2006705/1 8 0.52 , RDL=0.0 5 103 ug - 90-1-1 0 Metho d Blan k Tota l Mercury-3 C 2006705/1 8 ND . RDL=03 5 u g 2 0 RP D Tota l Mercury-3 C 2006705/1 8 0. 4 % 2 0 97201 2 N_ R MATRI XSPIK E 70-13 0

(139829 ) Tota l Arseni c (As ) 2006705/1 9 493 . ROL=0.4 0 9 9 u g 70-13 0 MATRI XSPIK E 70-13 0 DU P (139829

) Tota l Arseni c (As ) 2006705/1 9 493 , ROL=0.4 0 9 9 u g 70-13 0 MATRI XSPIK E 70-13 0 (139829 ) Tota l Berylliu m (Be ) 2006705/1 9 44S,ROL=0.1 0 8 9 u g 70-13 0 MATRI XSPIK E DUP0-99S29 ) Tota l Berylu m (Be ) 2006705/1 9 453 . ROL=0.1 0 9 1 u g 70-13 0 MATRI XSPIK E 70-13 0 (L99829 ) Tota l Cadmiu m (Cd ) 2006705/1 9 263 , RDL=0.1 0 10 4 u g 70-13 0 MATRI XSPIK E DU P (139829

) Tota l Cadmiu m (Cd ) 20067050 9 263,ROL=0.1 0 105 u g 70-13 0 MATRI XSPK E 70-13 0 039829 ) Tota l Chromiu m (Cr) 2006/05/1 9 523 , RDL=O3 0 10 5 u g 70-13 0 MATRI XSPIK E DUP(L99829 ) Tota l Chromiu m (Cr) 2006/05/1 9 513 , RDL=0.3 0 10 3 u g 70-13 0 MATRI XSPIK E (L99829 ) Tota l Lea d (Pb) 2006/05/1 9 50.5 , RDL=0J2 0 10 1 u g 70-13 0 MATRI XSPK E Tota l Lea d (Pb) DUP(L99829 ) Tota l Lea d (Pb) 2006705/1 9 503 , RDL=0.2 0 10 1 u g 70-13 0 Spike d Blan k 'Tota l Arseni c (As ) 2006/05/1 9 513 , RDL=0.4 0 10 3 u g 85-11 5 Spike d Blan k

DU P Tota l Arseni c (As ) 200670571 9 513 , RDL=0.4 0 103 u g 85-11 5 Spike d Blan k Tota l Barylnj m {Be ) 2006705/1 9 473,RDL=0.1 0 9 4 u g 85-11 5 SpSce d Blan k DU P Tota l Berylliu m (Be ) 2006705/1 9 47.0,RDL=0.1 0 9 4 u g 85-11 5 Pag e 9 o f1 1 674 0 Campobelt

o Road , Mississauga . Ontario Canad a L5N2L8 Tel : 905-817-570 0 Toi l free:800-563-626 6 Fa x905-817-577

7



## VE S 0024 1

## WAsty^ylsk m Analytic * In c

QAAQ C Batc h NumInS t QCTvp e Paramete r Data Analyze d vwv/mm/d d Valu e % Recover y Unit s Q C Unit s 97201 2 N RSpike dBlan k Tota

l Caomium(Cd ) 200670571 9 253
. RDL-0.1 0 10 3 u g 85-11 5 SpSce dBlan k OU PTota l Cadmium(Cd ) 20rj8/0571 9 253
. RDL=0.1 0 10 3 u g 85-11 5 SplicedBlan

k Tota

l Chromiu m(Cr) 200670571 9 533
. RDL=0.3 0 10 6 « g 85-11 5 Spike dBlan

k DU PTota

l Chromium<Cr

) 2006705/1 9 53.5
. RDL=0.3 0 10 7 u g 85-11 5 Space dBlan k Tota

l Lead(Pb )

- 2006705/1 9 51.0
. RDL=0.2 0 10 2 u g 85-11 5
• Spice dBlan

k DU PTota

l Lead(Pb ) 2006/05/1 9 52.0
. RDL=02 0 10 * u g 85-11 5 MethodBlan

k Tota

l Arseni c (As ) 2006705/1 9 ND , RDL=0.40 u g MethodBlan

k DU PTotal Arseni c (As ) 2006705/1 9 NO , RDL=0.40 u g Metho dBlan

k Tota

l Berylu m(Be ) 2006705/1 9 ND
. RDL=0.1 0
. , u g MethodBlan

k DU PTota

l Berylu m(Be ) 2006/05/1 9 NO , RDL=0.1 0 u g Metho dBlan

k Tota

l Cadmium(Cd ) 2006)05/1 9 ND , RDL=0.1 0 u g MethodBlan

k DU PTotal Gxirnium(Cd ) 2006705/1 9 ND , ROL=0.1 0
. u g MethodBtan

k TrjtalC»iroinu»n<Cr) 2006705/1 9 NO
. RDL=03 0 u g MethodBlan

k DU PTota

l Oiromiu m(Cr

) 2006705/1 9 ND , RDC=O3 0
. u g MethodBlan

k Tota

l Lead(Pb) 2006705/1 9 ND
. RDL=0.2 0 u g MethodBlan

k DU PTota

l Lea d(Pb) 2006705/1 9 ND , RDLSO2 0 u g RP D Tota

l Arseni c (As ) 200670571 9 3 3 % 2 0 Tota l Ber/Su m(Be ) 2006705/1 9 N C % 2 0 Tota l Cadmium(Cd) 2006/05/1 9 3. 9 % 2 0 Tota l Chromlom(Cr) 2006/05/1 9 11 5 % 2 0 Tota l Lea d(Pb ) 2006705/1 9 0. 7 % 2 0 97239 5 FF S MATRI

XSPIK E (L99S29 ) Tota

l Mercury-1 B 2006705/1 8 O.30.ROL=O.0 3 9 9 u g 85-11 5 MATRI XSPIK E DU P(139829 ) Tota

l Mercury-1 B 2006/05/1 8 030
. RDL=0.0 3 100 u g 65-11 5 Spike dBlan

k ; Total Mercury-I B 2006705/1 8 031 F RDL=0.0 3 10 3 u g 90^11 0 Spike dBlan

k OUPTota

l Mercur/-1 B 200670571 8 031 , RDL=0.0 3 103 u g 90-11 Q MethodBlan

k Tota

l Mercury-1 B 2006705/1 8 ND , RDL=0.O3 u g RP D Tota

l Mercurv-I B 2006/05/1 8 N C %

. 2 0 SU 3 = No t detecte d MC=Non-calculable RP D = Relativ e Percen

t Differenc e SPIK E= Fortifie dsampl

e I

Pag e 1 0 o f1 1 674 0 CampobeH

o Road . Mississau ^ Cfltari o Canad a .LS N 2L 8 Tel : 305-817-570

0 Trtlfiw:800^63-62t » -Fax : 005-817-577 7 Drh icn £>]' service an

d Scicn

ce ENS R Internationa

l Attention : Jef

fGorma n Clien t Projec t ft 10002-017-01 7 P.O.ft Projec t name : ONY

X Qualit y Assuranc

e Repor t (Confinued) Maxxa mJo b Number : GA64446 9



## VE S 00241 4Validatio nSignatur e Pag e
Maxxa m Jo b # : A644469

Th e analytica

l dat a an d ai l Q C containe

d i n mi s repor t wer e reviewe d an d validate d b yth e following individual(s). 

# <^M\r FRAN KMO , B-Sc.,Inorganic Lab . Manage r

Maxxa m ha

s procedure

s to plac e ta guar d agains t uiiyiupaus e o fthe elecntmi e signag e an d lav e a» e rcqmra d 'ligaalories* . a

s pe r w e lio n S.10. I o f rSO/IE C 1TO25;2085(E), signin g th e reports . SC C aa d CABA L ha wapprove d a wrq^ngpra^aDddecmmicrcpmionra t

Pag e 1 1 o f1 1 674 0 Camppbello Road , Mfesissauga , Ontari o Canada . L5 N 2L 8 Tel : 905-817-570

0 Tol l free:800-563-626

6 Fax:905-817-577

7



## VE SSectio n I : Sampl e Inventor y Repor t
Dat e Received : Projec t

No. : Projec t

Name : 6722/200 6 2780 3 10002-01 7

Lab . Sampl e I D Clien t Sampl e I D Componen t D D 001 00 2 00 3 00 4 00 5 00 6 00 7 U3-M23A-XAD-R 1 U3-M23A-PF-R 1 U3-M23A-XAD-R 2 U3-M23A-PF-R 2 U3-M23A-XAD-R 3 U3-M23A-PF-R 3 U3-M23A-XAD—F B B H ACE/MeC12/TO L XA D FHACE/MeC12/TO L FILTE R B H ACE/MeCE/TO L XA D F H ACE/MeC12/TO L FILTE R B H ACE/MeC12/TO L XA D F H ACE/MeC12/TO L FILTE R BH/F H ACE/MeC12/TO L FILTE R XA D

Smpinvgnmm5.rp1

Projec t 2780 3 Projec t 2 o f46 6



## VE S 00241 6

## SECTIO N n

Projec t 2780 3 Projec t 3 o f466



## VE S 00241 7

### <

m co o o r o 4 * Metho d Blan k Matrix : MM 5 Q C Batc h No. : 812 0 La b Sample : 0-MB00 1 Sample Size : Sampl e Dat e Extracted : 22-Jun-0 6 Dat

e Analyze d DB-5 : 26-Jun-0 6 Dat

e Analyze d DB-225 : N A Analyt e Cone . (pg/Sample ) D L aEMP C b Qualifier s Labele d Standar d % R LCL-UCL d Qualifier s 2,3,7,8-TCD D N D 0 87 9 9 3 8 1,2,3,7,8-PeCD D N D 0.80 2 13C-l,2,3,7,8-PeCD D 88.8 4 0 - 13 5 1,2,3,4,7,8-HxCD D N D 1 6 9 130-1,2,3,6,7,8-HxCD D 85,3 40-13 5 1,2,3,6,7,8-HxCD D N D 1 .4 3 13C-l,2,3,4,6,7,8-HpCD D 77.3 4 0 -13 5 1,2,3,7,8,9-flxCD D N D 1.5 5 13C-0CD P w , L 59. 8 ,4 0 • < 13 5 1, 2,3,4,6,7,8-HpCD D N D 1.8 2 13C-2,3,7,8-TCD F 82. 1 40-13 5 OCD D N D 6 9 5 130-1,2,3,7,8-PeCD F h •77,9 , ; 4 0 - 135 " 2,3,7,8-TCD F N D 1.0 8 130-1,2,3,6,7,8-HxCD F 95. 9 40-13 5 1,2,3,7,8-PeCD F N D 145 13C-l,2,3,4,6,7,8-HpCD F , 79. 6 4 0 -13 5 2,3,4,7,8-PeCD F N D 1.3 3 13C-0CD F 23.2 4 0 - 13 5 H 1,2,3,4,7,8-HxCD F N D 0 58 7 P S 3701-2,3',7,8-TCD n , , 10 1 " '7Q-13 0 i ' ' 1,2,3,6,7,8-HxCD F N D 0.46 9 13C-2,3,4,7,8-PeCD F 99. 6 70 - 13 0 2,3A6.7,8-HxCD F N D 0 55 2 130-1,2,3,4,7,8-HxpD D 95,2 - 70 -130 , ' 1 ,2,3,7,8,9-HxCD F N D 0.70 7 13C-l,2,3,4,7,8-HxCD F 88. 0 70-13 0 1,2,3,4,6,7,8-HpCD F 0 38 6 130-1,2,3,4,7,8,9-HpODI F i '73, 1 

## I i 70 - 13

0 , 1,2,3,4,7,8,9-HpCD F N D 0.84 6 A S 13C-l,2,3,7,8,9-HxCD F 83.3 4 0 -13 5 DCD F N D 7 4 6 if'l ' 'r-iYellVi ; Ti>, ; ; v' ! .Ms ! Total s Toxi c Equivalen t Quotien t (TEQ ) Dat a e Tota l TCD D N D 0.87 9 TE Q (Min-Max) : 0.0038 6 - 2.8 7 Tota l PeCD O N D 0 66 9 -MS:', &h ' ^ vv S I. ^ ,TiMV,\.* M :>"/'".' - •J ' J

' '.'•f!'..'

, ..i. w Tota l HxCD D N D 1.5 5 a . Sampl e specifi c estimate d detectio n limit . Tota l HpCD D N D 1.8 2 b Estimated maximu m posstbleicortcentration.i l • Tota l TCD F N D 1.0 8 q . Metho d detectio n limit . Tota l PeCD F N D 1.3 9 d . Lowe rcontro l limi t -uppe rcontro l limit . t- : , Tota l HxCD F N D 0.56 6 e . TE Q base d o n (1989

) Internationa l Toxi c Equivalen t Factors (ITEF) , Tota l HpCD F : 0 38 6 Analyst : RA S Approve d By . Willia m J . Luksembur g 27-Jun-200

6 15:1 1 Metho d0023 A

Projec t 2780 3 Projec t 4 o f466OP R Result s Metho d0023 A
Matrix : MM 5 Q C Batc h No. : 812 0 La b Sample : 0-OPR00 1 Sampl e Size : Sampl e Date Extracted : 22-Jun-0 6 Dat

e Analyze d DB-5 : 26-Jun-0 6 Dat e Analyze d DB-225 : N A Analyt e Spik e Cone . Cone . (ng/mL ) OP R Limit s Labele d Standar d %R LCL-TJC L 2,3,7,8-TCD D 2.5 0 2 4

8 1 ,2,3,7,8-PeCD D 12. 5 12.

6 8.7

5 - 16.2 5 13C-l,2,3,7,8-PeCD D 82.3 4 0 - 13 5 1 ,2,3,4,7,8-HxCD D 1 2 5 1 2 8 8 7 5 - 1 6 2 5 13C-1.2.3. 6 7,8-HjiCp D ,^7 9 1 40-13 5 ^ 1 ,2,3,6,7,8-HxCD D 12. 5 14.

0 8.7

5 - 16.2 5 13C-1,2,3,4,6,7,8-HpCD D 77. 4 4 0 - 13 5 1,2,3,7,8,9-HxCD D 1 2 5 1 4 0 8 75-162 5 13C-OCD D , . f, 1 62, 9 

## \ ' 40 - 13 5 . , 1 ,2,3,4,6,7,8-HpCD D 12.5 12. 0 8.7

5 -16.2 5 13C-2,3,7,8-TCD F 78. 1 40 - 13 5 OCD D 25. 0 2 4 7 1 7 5-3 2 5 13C-l > 2,3,7,8-PeCDF v , r,,75. 4 40-13 5 2,3,7,8-TCD F 2.5 0 2.4

0 1.75-3.2 5 13C-l,2,3,6,7,8-HxCD F 83.5 4 0 - 13 5 1 ,2,3,7,8-PeCD F 1 2 5 1 2 5 8 7 5 - 1 6 2 5 13C-l,2,3 J 4,6,7,8-HpCD F 7 8 7 4

0 - 13 5 2,3,4,7,8-PeCD F 12. 5 11.

8 8.7

5 - 16.2 5 13C-OCD F 27. 2 40 - 13 5 1 ,2,3,4,7,8-HxCD F 1 2 5 1 2 3 8 7 5 -1 6 2 5 A S 13C-l,2,3,7,8,9-HxCP F m 90, 7 40-13 5 1 ,2,3,6,7,8-HxCD F 12. 5 13.

9 8.7

5 -16.2 5 2,3,4,6,7,8-HxCD F 1 2 5 1 3 6 8 7 5 - 1 6 2 5 1,2,3,7,8,9-HxCD F 12. 5 12.

9 8.7

5 -16.2 5 1 ,2,3,4,6,7,8-HpCD F 1 2 5 1 2 8 8 7 5 - 1 6 2 5 1 ,2,3,4,7,8,9-HpCD F 12. 5 8.9

2 8.7

5 -16.2 5 OCD F 25, 0 24.7 1 7 5-3 2 5 • H J

Analyst : RA S Approve d By : Willia m J . Luksembur g 27-Jun-200615:1 1



# < m c o § Projec t 2780 3 Projec t 5 o f466 r o

### Sample 10 : U3-M23A-XAD-R 1 Clien t Dat a Sampl e Dat a Laborator v Dat a 

### Name : ENS R Project : 10002-01 7 Dat e Collected : 19-Jun-0 6 Time Collected : Matrix : Sample Size : 

### MM 5

Sample Lab Sample : 27803-001

Q C Batc hNo. : 812 0 Dat e Analyze dDB-5 : 26-Jun-0 6 Dat

e Received : 22-Jun-0 6 Date Extracted : 22-Jun-0 6 Date s Analyze dDB-225 : 27-Jun-0 6 

### Analyt e Cone . (pg/Sample ) D L a 

### EMPC b 

### Qualifier s Labele d Standar d 

### % R LCL-UCL d 

### Qualifier s 2,3,7,8-TCD D N D 3 6 4 I S 13C-2,3,7,*8-TCD D 1,2,3,7,8-PeCD D 17. 0 J 13C-l,2,3,7,8-PeCD D 88.7 40-13 5 1,2,3,4,7,8-HxCD D 1 9 1 13C-l,2,3,6,7,8-HxCD D 89.2 -40-13 5 1,2,3,6,7,8-HxCD D 46. 1 

## s 13C-l,2,3,4,6,7,8-HpCD D 13C-OCD P 4

### „ 96. 7 4 0 -13 5 1,2,3,7,8,9-HxCD D 

### 3

7 0 13C-l,2,3,4,6,7,8-HpCD D 13C-OCD P 4

### „ ^'135 . 1,2,3,4,6,7,8-HpCD D 19 0 13C-2.3.7.8-TCD F 88.3 40-13 5 OCD D 23 6 l3C-l,2 t 

### 3,7,8-PeCDF - , 1 

## V 80 > 

### 4 0 -135 

### ; 2,3,7,8-TCD F 29. 5 13C-1,2,3,6,7,8-HxCD F 97. 0 40-13 5 1,2,3,7,8-PeCD F 

### 3

5 5 ?f ' '
. '.
. '.V' : ;;:' :' 

### 13C-l,2,3,4,6,7,8-HpCD F 92.7 

### 4 Q -13 5 2,3,4,7,8-PeCD F 65.4 13C-OCD F 83.4 40-13 5 1,2,3,4,7,8-HxCD F 3 6 0 1 

## yy^rm- E S 37Cl-2,3,7,8-TCDp r

### ' J L 

### ' • ' 8 6 1 siilisiiviiillli i 

### 1,2,3,6,7,8-HxCD F 31. 9 , J, D 13C-2,3,4,7,8-PeCD F 91. 4 70-13 0 • 2,3,4,6,7,8-HxCD F 

### 4

3 8 13C-l,2,3,4,7,8-HxCD D 7 0 - 13 0 1,2,3,7,8,9-HxCD F 10. 3 

## J 13C-l,2,3,4,7,8-HxCD F 85.9 70-13 0 1,2,3,4,6,7,8-HpCD F 7 8 1 B 13C-J,2,3,4,7,8,9'HpCD F i t 

### 1 77. 9 7P'W9 l r„ 

### 1,2,3,4,7,8,9-HpCD F 

### 8.1 0 J A S 13C-l,2,3,7,8,9-HxCD F 

### 95. 2 4 0 -13 5 OCD F 

### 2

0 4 : 

### j 

## yj: Total s Toxi c Equivalen t Quotien t (TEQ ) Dat a e 

### Tota l TCD D 118 0 TE Q (Min-Max) : 71.4-75, 0 Tota l PeCD D 86 9 :'S,v ; . *.:>.-.: V.J.** • hfivii ' 

### Tota l HxCD D 147 0 a . Sampl e specifi c eatimate

ddetectio nlimit
. 

### Tota l HpCD D 41 2 b
. Estimatedmaximu mpassible concentration ; n :-. 

### Tota l TCD F 108 0 c . Metho ddetectionlimit
. 

### Tota l PeCD F 80 0 

## 'y^isyy^'.

. d
. Lower contro l limt

f -upper control limit
. . f t'- •• '•i„--;j-!.":'--T-

i i:.r

j '-Jfe;; : :-.' : V . 4 

### Tota l HxCD F 39 1 39 5 RP e . TE Q base don(1989) Internationa

l Toxi c Equivalen

t Factors (ITEF)
. 

### Tota l HpCD F 

### 11 2 

## ^y&'^y. Analyst : RA S 

### Approve dBy : Willia m J . Luksembur g 27-Jun-200

6 15:1 1 

## o o | £Projec t 2780 3 Projec t 6 o f466Sampl e ID : TJ3-M23A-PF-R 1 

# <~$*\ Metho d0023 A Clien t Dat a S«mRl«Pst t MPW«tor v$m Name : ENS R Project : 10002-01 7 Dat e Co l lected : 19-Jun-0 6 Time Collected : Matrix : Sampl e Size : MM 5

Sample LabSampte : 27803-00 2 Q C Batc h No. : 812 0 Dat e Analyze d DB-5 : 26-JTO-0 6 Date Received :

Date Extracted : Dat e Analyze d DB-225 : 22-Jun-06

22-Jun-0 6 N A • Analyt e Cone . (pg/SampIe ) D L a EMPC b Qualifier s Labele d Standar d % R LCL-UCL d Qualifier s 2,3,7,8-TCD D 

### N

D 1.1 8 ' 91.5 ,4 0 r13 5 1,2,3,7,8-PeCD D 

### N

D 1.3 8 I3C-l,2,3,7,8-PeCD D 92. 8 4 0 -13 5 1,2,3,4,7,8-HxCD D 

### N

D 2.7 6 13C-l,2,3,6,7,8-HxCO O 89: 4 4 0 -13 5 1,2,3,6,7,8-HxCD D 

### N

D 2.3 3 13C-l,2,3,4,6,7,8-HpCD D 83. 1 40-13 5 1,2,3,7,8,9-HxQD D 

### N

D 2.5 3 13C-OCD D '86. 7 40.H35 - ' 1,2,3,4,6,7,8-HpCD D 

### N

D 2.5 2 13C-2,3,7,8-TCD F 85.3 40-13 5 OCD D 10. 8 •J 130-1,2,3,7,8-PeCD F 1 82.3 40-13 5 2,3,7,8-TCD F 

### N

D 1.2 7 13C- 1,2,3,6,7,8-HxCD F 97. 8 4 0 -13 5 1,2,3,7,8-PeCD F 

### N

D 1 5 1 13C-l,2,3,4,6,7,8-HpCD F , 80, 9 4 0 r13 5 2,3,4,7,8-PeCD F 

### N

D 1.3 8 13C-OCD F 69. 1 40-13 5 1,2,3,4,7,8-HxCD F 

### N

D 0 92 3 ES 3701-2,3,7,8-TCD p 1 94.4 , 70-13 0 1,2,3,6,7,8-HxCD F 

### N

D 0.73 7 13C-2,3,4,7,8-PeCD F 93. 9 70-13 0 2,3,4,6,7,8-HxCD F 

### N

D 0 86 8 130-1,2,3,4,7,8-HxCD D 90, 7 7 0 T13 0 1,2,3,7,8,9-HxCD F 

### N

D 1.1 1 13C-l,2,3,4,7,8-HxCD F 87.4 70-13 0 1,2,3,4,6,7,8-HpCD F 

### N

D 

# l 1.2 9 l3C-l,2,3,4,7 I 8,9-HpCD F •7? 4 7 0 - 13 Q 1,2,3,4,7,8,9-HpCD F N D 1.1 1 A S 13C-l,2,3,7,8,9-HxCD F 93. 7 40-13 5 OCD F N D 5.0 2 "". r^T " r Total s Toxi c Equivalen t Quotien t (TEQ ) Dat a c Tota l TCD D N D 1.1 8 TE Q (Min-Max) : 0.010 8 - 3.9 5 Tota l PeCD D N D 1 3 8 Tota l HxCD D N D 3.3 4 a . Sampl e specifi c estimate d detectio n limit . Tota l HpCD D 1 7 7 b . Estimated maximu m posjibte-pgncentratioti . Tota l TCD F N D 1.2 7 c . Melho d detectio n limit . Tota l PeCD F N D 144 d . Lowe r contro l Hmit .-; uppe rcontro l limit. ; . A
_ Tota l HxCD F N D 0.89 0 e . TE Q base d o n (1989

) Internationa l Toxi c Equivalen t Factor s (ITEF) . Tota l HpCD F N D 14 9 Analyst : RA S Approve d By : Willia m J . Luksembur g 27-Jun-200615:1 1 Projec t 2780 3 Projec t 7 of466Sairipleip ; U3-M23A-XAD--R 2 TB'ssy;-,* !

- t , t Metho d0023 A Clien t Dat a Samnl e Dat a Name : ENS R Project : 10002-01 7 Dat e Collected : 20-Jun-0 6 Time Collected : Matrix : Sample Size : MM 5

Sample Lab Sample : 27803-00 3 Q C Batc hNo. : 812 0 Dale Analyze dDB-5 : 27-Jun-0 6 Dat

e Received ; 22-Jun-0 6 Dat e Extracted : 22-Jun-0 6 Date s Analyze dDB-225 : 27-Jun-0 6 Analyt e Cone , (pg/Sample) D L a EMPC b Qualifier s Labele d Standar d % R LCL-UCL d Ouaiifler s 2,3,7,8-TCD D 3 4 4 I S l3C-2,3,7,8-TCD b ' 1 ' 90V 7 40-13 5 1,2,3,7,8-PeCD D 17. 6 . J l3C-l,2,3,7,8-PeCD D 96. 2 40-13 5 1,2 ,3 ,4,7,8-HxCD D 16 8 13C-l,2,3,6,7,8-HxCDt > 90_,f l 4 0 - 13 5 1,2,3,6,7,8-HxCD D 34.7 J 13C-l,2,3,4,6,7,8-HpCD D 89. 1 40 - 13 5 1,2,3,7,8,9-HxCD D 27 J • 1,2,3,4,6,7,8-HpCD D 17 5 13C-2,3,7,8-TCD F 84.8 4 0 -13 5 OCD D 17 5 40 - 135 * v 2,3,7,8-TCD F 32.8 13C-l,2,3,6,7,8-HxCD F 96. 2 40 -13 5 1,2,3,7,8-PeCD F 41 2 ISC-l ^.SAe ^.S-HpCD F 83 4 ilMlllliillllC
. 2,3,4,7,8-PeCD F 70,2 13C-OCD F 59. 8 4 0 -13 5 1,2,3,4,7,8-HxCD F 33 0 E S 37Cl-2 ,3 ,7,8-TCD D ' 1 99 , 4 - 1 70-U30 1 v' 1 1,2,3,6,7,8-HxCD F 31.7 J, D 13C-2,3,4,7,8-PeCD F 89.2 70-13 0 2,3,4,6,7,8-HxCD F 4 1 8 13CM,2 ,3 ,4,7,8-HxCD D 92 .3
. 70 - 13 0 * ' ' 1,2,3,7,8,9-HxCD F 11. 6 J 13C-l,2,3,4,7,8-HxCD F 92.3 7 0 - 13 0 1,2,3,4,6,7,8-HpCD F 6 6 8 13CM ,2 ,3 ,4,7,°>H P CD F > , 83.2 r 7 0 -P 0 1,2,3,4,7,8,9-HpCD F 5.21 j A § 13C-l,2,3,7,8,9-HxCD F 99. 2 40-13 5 OCD F 14 8 .V^ : "- ; : 

## Y'y^%y0»§^!^y0 Total s Toxi c Equivalen t Quotien t (TEQ ) Dat a e Tota l TCD D 121 0 TE Q (Min-Max) : 75. 0 - 75. 0 Tota l PeCD D S4 8 •V ' : .', :i .:''^:' : i w ' +t > ' * , 

## I Tota l HxCD D 133 0 a . Sample specifi c estimate ddetectio nlimit
. Tota l HpCD D 38 1 b
. Estimatedmaximu mpossible concontraticn
. Tota l TCD F 135 0 c . Methoddetectio nlimit
. TotalPeCDE ; >>> V • •,86 2 D .1 ; d
. Lowe r contro l limi t

- uppe r contro l limit : . « Tota l HxCD F 39 0 D e . TE Q base don(1989) Internationa

l Toxi c Equivalen

t Factors (ITEF)
. Tota l HpCD F 98. 0 ; .Vi'SOG , *::':X*f". ! Analyst : RA S Approve dBy : Willia m J . Luksembur g 27-Jun-200

6 15:1 1 Projec t 278Q 3 Projec t 8 of466

### <

m c o o o ro ro c o Sampl e ID : U3-M23A-PF-R 2
. 

### y0M0r thod6023 A Clien t Dat a Sampl e P»t a riUbowtvr y But * Name : ENS R Project : 10002-01 7 Dat e Collected : 20-Jutl-0 6 Tim e CoUected

: Matrix : Sampl e Size: MM 5

Sample La

b Sample : 27803-00 4 Q C Batc h No. : 812

0 Dat e Analyze d DB-5 : 27-Jun-0 6 Dat

e Received: Dat e Extracted: Dat e Analyze d DB-22S : 22-Jun-0

6 22-Jun-0 6 N A Analyt e Cone . (pg/Sample ) D L a EMPC b Qualifier s Labele d Standar d % R LCL-UCL d Oualifler s 2,3,7,8-TCD D N D 12 1 I S 13q-2,3,7,8-TCD D 95. 2 t4o'*m ,1 : • ' • • » • 1,2,3,7,8-PeCD D N D 3.2 6 13C-l,2,3,7,8-PeCD D 10 1 4 0 -13 5 1,2,3,4,7,8-HxCD D • N D 2 6 3 l3G-l,2,3,6,7 ,a -HxCp D < 4 0 r13 5 1,2,3,6,7,8-HxCD D N D 2.2 3 13C- 1,2,3,4,6,7,8-HpCD D 83. 0 40-13 5 1,2,3,7,8,9-HxCD D N D 2.4 1 13C-QCDT J <•

x i 88 . 2 49 *13 5 r 1,2,3,4,6,7,8-HpCD D N D 4.1 2 13C-2,3,7,8-TCD F 92. 6 40-13 5 OCD D N D 6 3 3 13C-l,2,3,7 ( 8-PeCD]r ? , ,8&9 , i 4 0 -.13 5 2,3,7,8-TCD F N D 0.951 13C-l,2,3,6,7,8-HxCD F 10 1 4 0 -13 5 1,2,3,7,8-PeCD F N D 3 4 4 1301 ,2,3,4,6,7,8-HpCD F «»4 0 - 13 5 - J i 2,3,4,7,8-PeCD F N D 3.1 4 13C-OCD F 61.5 40-13 5 1,2,3,4,7,8-HxCD F N D 0 68 4 E S 37Cl-2,3,7,8-TCDD ' '•ins 1 t O -130 1 h 1,2,3,6,7,8-HxCD F N D 0.54 6 13C-2,3,4,7,8-PeCD F 99. 4 70-13 0 2,3,4,6,7,8-HxCD F N D 064 3 13C-l,2,3, 4 7,8-HxCpD" ' i 95. 0 , 70-^13 0 , 1,2,3,7,8,9-HxCD F N D 0.82 3 13C-l,2,3,4,7,8-HxCD F 88. 7 70-13 0 1,2,3,4,6,7,8-HpCD F N D 070 5 13C.l,2,3A7,^9-HpCOF \ ,/79. 4 70*13 0 f liMlliiw?' ' 1,2,3,4,7,8,9-HpCD F N D 0.97 1 A S 13C-l,2,3,7,8,9-HxCD F 92.8 40-13 5 OCD f N D 6 3 8 :i"Af':J>v.^;^ ^ Total s Toxi c Equivalen t Quotien t (TEQ ) Dat a e Tota l TCD D N D 1.2 1 TE Q (Mln-Max) : 0-5.7 4 Tota l PeCD D N D 3 2 6 v i ••. ; .-' , kitf^iiSrir' i s S'f Tota l HxCD D N D 2.4 1 a . Sampl e specifi c estimate d detectio n limit . Tota l HpCD D N D 4 1 2 b . Estimate d maximu m possibje^fojjcentrafion

. m -\r Tota l TCD F N D 0.951 c . Metho d detectio n limit . Tota l PeCD F N D 3 2 8 d. Lowe r contro l limi t •uppe r controMimit

i >: : . i.i,i,:;i.'i^ii:<'*i.?;v:- - Tota l HxCD F N D 0.66 0 e . TE Q base d o n (19S9 ) Internationa

l Toxi c Equivalen

t Factor s (ITEF) . Tota l HpCD F N D 0 81 7 • Analyst : RA S Projec t 2780 3 Approve d By : Willia m J . Luksembur g 27-Jun-200

6 15:1 1 Projec t 9 o f46 6Sampl e ID : TJ3 -M23A-XAD-R 3 ; , Metho d0023 A Clien t P « a SumnlfPfu a Laborator y Dat a Name : ENS R Project : 10002-01 7 Dat e Collected : 21 -Jun-0 6 Time Collected : Matrix : Sample Size : MM 5

Sample La

b Sample : 27803-00 5 Q C Batc hNo. : 812 0 Dat e Analyze dDB-5 : 27-Jun-0 6 Dat

e Received : Date Extracted : Date s Analyze dDB-225 : 22-Jun-0 6 22-Jun-0 6 27-Jun-0 6 Analyt e Cone . (pg/Sample ) D L a EMPC b Qualifier s Labele d Standar d % R LCL-UCL d Ouallfier s 2,3,7,8-TCD D N D .7,,,i.^,i i;| vi: vq'ifi- 

## WIM »»8«* JI 4«| I*W,' . 1,2,3,7,8-PeCD D 16. 7

_J 13C-l,2,3,7,8-PeCD D 94. 0 40-13 5 1,2,3,4,7,8-HxCD D 1 4 6 130-1,2,3,6,7,8-HxCO D 8§* 7 I4QJ-13

5 1,2,3,6,7,8-HxCD D 35.7 J 13C-l,2,3,4,6,7,8-HpCD D 95.2 40 - 13 5 1,2,3,7,8,9-HxCD D 2 6 3 13C-QCD 0 j 95 ( ? ' 

### 40 f 13 5 f 1,2,3,4,6,7,8-HpCD D 15 6 13C-2,3,7,8-TCD F 86.6 40-13 5 OCD D 14 1 13C-l,2,3,7,8-PeCD P 8 4 3 * 4 0 -' 1^ 5 2,3,7,8-TCD F 31.8 13C-i;2,3,6,7,8-HxCD F 95. 9 4 0 -13 5 1,2,3,7,8-PeCD F 4 1 1 13C-1,2,3,4,6,7,8-HpCD F 9Q 8 40-13 5 2,3,4,7,8-PeCD F 76.2 13C-OCD F 81. 0 . 4 0 -13 5 1,2,3,4,7,8-HxCD F 3 7 8 j E S 3701-2,3,7,8-TOD D 98 2 I7 0 -13 0 \ 1,2,3,6,7,8-HxCD F 33.6 J, D 13C-2,3,4,7,8-PeCD F 97. 8 70-13 0 2,3,4,6,7,8-HxCD F 4 4 9 J 130-1,2,3,4,7,8-HxtfD D 

# m. 7()t -13 0 1,2,3,7,8,9-HxCD F 11.1 J 13C-l,2,3,4,7,8-HxCD F 90. 7 70-13 0 1,2,3,4,6,7,8-HpCD F 7 0 7 B 13C-l,2,3,4,7,8,9-«[pCD F ill ! 70^13 0 1,2,3,4,7,8,9-HpCD F 7.1 5 J A S 13C-l,2,3,7,8,9-HxCD F 91. 1 40-13 5 OCD F 1 3 2 J Total s Toxi c Equivalen t Quotien t (TEQ ) Dat a c Tota l TCD D 87 9 89 9 TE Q (Min-Max) : 74. 6 - 78. 5 Tota l PeCD D 68 6 illiil i Tota l HxCD D 111 0 a . Sampl e specifi c estimate

ddetectio nlimit
. Tota l HpCD D 33 5 b , Estimatedmaximu mpossible cflncejitration
. . ! ; . . • r 1 «:•. ! .v.:.. ,i.
. • Tota l TCD F 131 0 c . Methoddetectio nlimit
. Tota l PeCD F 94 8 D d
. Lowe r control limi t

- uppe r contro l limit
. 1 Tota l HxCD F 41 0 D e . TE Q base do n(1989 ) Internationa

l Toxi c Equivalen

t Factors (ITEF)
. Tota l HpCD F 10 2 B Analyst : RA S Approve dBy : Willia m J . Luksembur g 27-Jun-200 6 15:1 1 Projec t 2780 3 

### Projec t lQpf46 6

# <

m c o 

## o o r o Sampl e ID : TJ3-M23A-PF-R 3 ifi i
t 

### Metho d0023 A Clien t Dat a 

### Name : Project : Dat e Collected : Tim e CoUected

: ENS R 10002-01 7 21-Jun-0 6 Sampl e P»t » 

### Matrix : Sampl e Size: MM 5

Sample Analyt e Cone . (pg/Sample ) D L EMPC ° Qualifier s 2,3,7,8-TCD D N D 1,2,3,7,8-PeCD D N D 1, 2 3,4,7,8-HxCD D N D 1.2.3.6.7.8

- HxCD D N D 1.2.3.7.8.9

- HXCD D N D 1,2,3,4,6,7,8-HpCD D N D OCD D 10 1 2,3,7,8-TCD F N D 1,2,3,7,8-PeCD F N D 2,3,4,7,8-PeCD F N D 1,2,3,4,7,8-HxCD F N D 1,2,3,6,7,8-HxCD F N D 2.3.4.6.7.8- HxCD F N D 1.2.3.7.8.9

- HxCD F N D 1.2.3.4.6.7.8-HpCD F N D 1.2.3.4.7.8.9

- HpCD F N D OCD F N D 14 0 3.8 3 21 3 1.8 1 • 2.5 3 1.1 5 3 0 0 2.7 4 0 64 1 0.51 2 0 60 3 0.77 1 0 81 9 0.60 2 3 8 4 Total s Tota l TCD D TotaliPeCD D Tota l HxCD D Tota l HpCD D Tota l TCD F Tota l PeCD F * Tota l HxCD F Tota l HpCD F N D 3.3 5 : N D N D N D N D

. N D 1.4 0

, 3.8 3

1.1 5 2.8 6 0.61 8 

## I': Laborator y Dat a 

### La b Sample : Q C Batc h No. : Dat e Analyze d DB-5 : 27803-00

6 812 0 27-Jun-0 6 Dat

e Received: Dat e Extracted: Dat e Analyze d DB-225 : 22-Jun-0

6 22-Jun-0 6 N A Labele d Standar d % R LCL-UCL a

### Qualifier s 13C-l,2,3,7,8-PeCD D iaC -l,2,3,6,7,8.Hx $} P 13C-l,2,3,4,6,7,8-HpCD D 13C-OCDD, < J k 

### 13C-2,3,7,8-TCD F 13C-l,2,3,7 } 

### 8-PeCDF + 

### 13C-l,2,3,6,7,8-HxCD F l3C-l,2,3,4,6,7,?-HpCD F 13C-OCD F £ § 37Cl-2,3,7,8-XCD p , 13C-2,3,4,7,8-PeCD F 13C-1,2,3,4,7,8-HxCD D 13C-l,2,3,4,7,8-HxCD F 13C-l,2 t 

### 3,4,7,8,9-HpCR F A S 13C-l,2,3,7,8,9-HxCD F 

### WK, 88.4 i n 1 

### 93. 9 

## &3 95. 6 94. 0 89.7 84J< 99.3 85. 9 ,10 0 10 4 H ? 90. 4 9 1 3 

### 99. 0 40-13 5 4 0 r

### 13 5 ' " 3 i 

### 40-13 5 40„}3 5 40-13 5 4QV13S,.,. 1 

### 4 4 0 -13 5 40-13 5 ~ 4 0 -13 5 7 0 

### • » 13 0 7 0 -13 0 70 - 13 0 * 7 0 -13 0 7 0 * 13 0 1 

### ; 4 0 -13 5 Toxi c Equivalen t Quotien t (TEQ ) Dat a TE Q (Min-Max) : 0.010 1

c . Metho d detectio n limit . d. Lowe rcontro l limi t • e . TE Q base d o n (1989 ) Internationa

l Toxi c Equivalen

t Factor s (ITEF) , Analyst : RA S Approve d By: Willia m J . Luksembur g 27-Jun-200

6 15:1 1 Projec t 2780 3 Projec t 1 1 o f466Sampl e ID : U3-M23A-XAD—F B

- Metho dq023 A Clien t Dat a $«mpl * Pftt s Laborator y Dat a Name : ENS R Project : 10002-01 7 Date Collected : 20-Jun-0 6 Time Collected : Matrix : Sample Size : MM 5

Sample Lab Sample : 27803-00 7 Q C Batc hNo. : 8120 Dat e Analyze dDB-5 : 26-Jun-0 6 Dat

e Received : Dat e Extracted : Dat e Analyze dDB-225; 22 -Jun-0 6 22 -Jun-0 6 N A Analyt e Cone . (pg/Sample ) D L 8 EMPC b Qualifiers Labele d Standar d % R LCL-UCL d Qualifier s 2,3,7,8-TCD D N D 0.84 5 I S 13C -2 ,3 ,7 ,8-TCb D v ' ' ' i 1,2,3,7 ,8 -PeCD D N D 0.84 4 13C-l ,2 ,3 ,7 ,8-PeCD D 89
. 2 4 0 -13 5 1 ,2,3,4,7 ,8 -HxCD D N D 1 3 8 BC-l .^^S-HxSP D 4 0 -13 5 1,2,3,6,7 ,8 -HxCD D N D 1.1 6 13C-i ,2 ,3,4,6 ,7 ,8-HpCD D 80
. 2 4 0 -13 5 1 ,2,3,7,8,9-HxCD D 

## (-.N

D y - • • J-M'.% 12 6 13C-OC0 D r \ s . 

# I 84,5 40 - 135 , 1 ,2,3,4,6,7,8-HpCD D N D 1.4 2 13C -2 ,3 ,7 ,8-TCD F 85. 9 40-13 5 OCD D N D 4 2 9 130-1 ,2 ,3 ,7 ,8-PeCD E 1 

# m 40-13 5 i
. 

# t 2,3,7 ,8 -TCD F N D 0 .73 2 13C-1 ,2 ,3,6 ,7 ,8-HxCD F 96
. 2 4 0 -13 5 1,2,3,7 ,8 -PeCD F - N D 1 1 5 13C-l ,2 ,3,4,6 ,7 ,8-HpCD F 8,1,1 - 40-13 5 2,3,4,7,8-PeCD F N D 1.0 5 13C-OCD F 59. 9 40-13 5 1,2,3,4,7,8-HxCD F N D 040 1 P g 37Cl -2 ,3 ,7 ,8-TCD D 1 • 95,3 70- 13 0 

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### ro C DPROJEC TNARRATIV E Maxxa m Analytic s (Burlingto n ON ) Maxxa m Jo b #:A66217 5 Client : ENS R Internationa l Clien t Projec t 10002-017-82 0 ONY X I . SAMPL E RECEIPT/ANALYSI S
a ) Sampl e Listin g Maxxa m Clien t Dat e Date I D Sampl e I D Sampled Received Metal s i n Ai r(Bac k

Half) vi a EP A Metho d 29 M7314 6 M29-RBB H 200670672 1 200670672

2 M7314 7 M29-U3-R 1 B H 200670671 9 200670672 2 M7314 7 Di m M29-U3-R 1 B H 200670671 9 200670672 2 M7314 8 M29-U3-R2B H 200670672 0 2006/0672

2 M7314 9 M29-U3-R 3 B H 200670672 1 2006/06/2

2 Metal s i n Ai r{Fron t Half ) vi a EP A Metho d 29 M7314 2 M29-RBF H 200670672 1 2006706/2

2 M7314 3 M29-U3-R1F H 200670671 9 2006/0672 2 M7314 3 Du p M29-U3-R 1 F H 2006706/1 9 2006/0672 2 M7314 4 M29-U3-R2F H 200670672 0 2006/0672

2 M7314 5 M29-U3-R 3 F H 200670672 1 2006/0672

2 Particulate

s i n Ai r(Aceton e Rinse ) vi a EP A Metho d 5 M7314 2 M29-RBF H 200670672 1 200670672

2 M7314 3 M29-U3-R1F H 200670671 9 200670672 2 M73I4 4 M29-U3-R 2 F H 200670672 0 2006706/2

2 M7314 5 M29-U3-R3F H 200670672 1 2006706/2

2 Particulate

s i n Ai r(Filter) vi a EP A Metho d S ( M7314 2 M29-RBF H 200670672 1 2006/0672

2 M7314 3 M29-U3-R1F H 2006/06/1 9 2006706/2 2 M7314 4 M29-U3-R 2 F H 200670672 0 200670672

2 M7314 5 M29-U3-R3F H 200670672 1 2006/0672

2 Ru n Dat e i s define

d a s di e dat e o finjectio n ofth e las

t calibratio n standar

d (1 2 hour

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t ru n sequence. Therefor e th e time o fcalibratio n injectio n tha t define s th e m n dat e i s alway

s witlii n 1 2 hour

s o fth e tim e o fsampl

e injection . b ) Shippin g Problems : non e encountere

d
c ) Documentation Problems : non e encountere

d II . SAMPL E PREP : . N o problem

s encountere

d Date Date Prepped Ru n
200670672

9 200670672

9 200670672

9 200670672

9 200670672

9 200670672

9 2006706/2

9 2006/06/2

9 2006/0672

9 2006/0672

9
2006706/2

8 2006706/2

9 2006/0672

8 2006/0672

9 2006/0672

8 2006/06/2

9 2006/06/28 200670672 9 2006/0672

8 2006/06/2

9
2006/0672

7 2006/06/2

8 200670672

7 2006706/2

8 200670672

7 2006/0672

8 2006706/2

7 200670672

8
200670672

6 2006/06/2

6 200670672

6 2006/0672

6 2006/06/26 2006706/2 6 2006/06/26 200670672 6D XSAMPL E ANALYSIS : Se e als o comment

s withi n th

e appropriat

e Certificat

e o fAnalysi s a ) Ho H Times : al l withi n recommende d hol d time

s b) Instrumen

t Calibration : aU withi n contro l limit s c) Qualit y Control : Al l applicabl e Q C meet s contro l criteria , excep t wher e otherwis

e noted . I certif y tha t m b dat a packag e i s mc» ^ an d condition s o fthe contract, bot h technically an d fer other tha n th e condition s detaile d above . I n addition , I certify , ma t to th e bes t o fm y knowledg

e an d belief , th

e dat a a s reporte d ar e true an d accurate . Releas e o fthe dat

a containe

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d b y th e cognizant laborator y officia l o rhis/he rdesignee, a s verified by mi s signature.

Mary-Ann e Johnson , Projec t Manager Dat e 

# JU L 0 5 200 52 . DAT A SUMLVLfVR Y 

# Certificat e o f Analysi s -
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Attention : JeffGorma n ENS R International 6601 KirkvilleR d Eas t Syracuse, N Y US A 1305

7 Repor t Date : 2006709/1 1
CERTIFICAT E O F ANALYSI S MAXXA M JO B #: A66217 S Received : 2006/06722,13:5 0 Sampl e Matrix : Filte r # Sample s Received : 4 Dat e Dat

e Metho d Analyse s Ouantit y Extracte

d Analyze d Laborator y Method Referenc e Metal s i nAi r

(Fron t Half ) b y ICP/M S ft 4 2006/0672 8 2006/06/2

9 SO PIN G108/10

9 EP ASW846-6020 Particulates i nAi r

(Aceton e Rinse ) (MS ) 8 4 2006/06/2 7 2006/06/2 8 SO PIN G50 5 EP ACF RPT M 5 Particulates i nAi r

(Filter) 9 4 2006/06/26 2006/06/26 SO PIN G50 5 EP ACF RPT M 5 Final Volum

e o f Aceton e Prob e Rins e # 4 2006V09/I 1 2006V09/1 1 Sampl e Matrix : Impinge

r Solutio n # Sample s Received : 4 Dat e Dat

e Metho d Analyse s Quantit y Extracte

d Analyze d Laborator y Method Referenc e Metal s i nAi r

(Back Half ) b y ICP/M S % 4 2006/0672 9 2006/06/2

9 SO PIN G108/10

9 EP ASW846-3010A.6 0 (1 ) Thi s tes

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d b yMaxxa m Analytics Burlingto n

MAXXA M ANALYTIC S IN C

MARY-ANN E JOHNSON , BA , B.Sc . Projec t Manager MAJ/ma j encl .

.7 2 Pag e 1 of1 1
674 0 Campobell o Road , Mississauga , Ontari o Canad a L5 N 2L 8 Tel : 905-817-570 0 Tol l free:80O-563-626 6 Fax : 905-817-577

7



## VE S 00243 1

# M l a m Driven by service

an d Science www.marxMiimMlyttcs.coi n You r Project* : 10002-017-82 0 Site : ONY X

Attention ; Jef

fGorma n ENS R International 6601KirkvilleR d Eas t Syracuse, N Y. US A 1305

7 Repor t Date : 2006709/1 1
ryRTTFICAT R TM ? ANALYSI S

-2 -

Validatedby :

Tota l cove r pages : 2 Pag e 2 o t 1 1
r, , - r^ri* r Tel-905-817-570 0 Td l free:800-563-6266 Fax:905-817-5777 674 0 Campobell o Road , Missjssauga.Ontan o Canad a L5N2L 8 Tel . 91»-» To



## VE S 00243 2- .' Driven

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l Qien t Projec

t # : 10002-017-82

0 Projec t name : ONY

X SamplerInitials : 

## RESULT S O F ANALYSE

S O F FILTE

R
riaxxam I D M7314 2 M7314 3 M7314 4 M7314 5 Samplin q Dat e 200670672 1 2006/06/1 9 2006/06/2 0 2006/06/2 1 Unit s M29-RBF H M29-U3-R 1 F H M29-U3-B 2

F H M29-U3-R 3

F H FIO L S C Batc h MD L

• Particulate Weigh t i n Aceton e Rins e m g N D 4. 0 2. 8 1. 7 0. 5 100127 5 0. 5 Volum e m l 9 8 5 7 8 7 5 6 1 104987 0 1 Particulate Weigh t o n Filte r m g 0.6 5 1.6 5 1.5 5 0.3 0 100126 5 0.3 0 N D = No t detecte d RD L = Reportabl e Detectio n Limi t Q C Batc h = Qualit y Contro l Batc h

Pag e 3 of 1 1 674 0 Campobell o Road , Mississauga , Ontari o Canad a L5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-6266 Fax : 905-817-577 7 

# M a o ua m .

' An*lytic * in c Maxxa m Jo b #:A66217

5 Repor t Date : 2006709/1 1



## VE S 00243 3f Analytic s lo c Maxxa m Jo b # : A66217 5 Repor t Date : 2006/09/1 1 Driven by service

and Science wwwjnaxxaaianalyttcs^am ENS R Internationa

l Clien t Projec t # : 10002-017-82

0 Projec t name : ONY

X SamplerInitials : 

## ELEMENT S B YICP/M S (FILTER

)
Maxxa m I D M7314 2 M7314 3 M7314 3 M7314 4 M7314 5 Samolin q Dat e 2006/06/2 1 2006/06/1 9 . 2006/06/1 9 2006/06/2 0 2006706/2 1 Unit s M29-RBF H M29-U3-H 1 F H M29-U3-R 1

F H Lab-Ou o M29-U3-R 2

F H M29-U3-R 3

F H RD L S C Batc h HD L

Tota l Arseni c (As ) u g 0.6 1 5.8 1 6.0 1 45 7 5.6 2 3.40 100100 8 0.4 0 Tota l Berylliu m (Be ) u g N D N D N D N D N D 0.1 0 100100 8 0.1 0 Tota l Chromiu m (Cr ) u g 0.7 9 9.6 4 11.9(1 ) 3.9 8 11. 1 0.3 0 100100 8 0.3 0 N D = No t detecte d RD L = Reportabl e Detectio n Limi t S C Batc h = Qualit y Contro l Batc h [ 1 ) Pleas e refe rt o Genera l Comment s pag e fo r specifi c clarification .

Page4of1 1 674 0 Campobell o Road , Mississauga , Ontari o Canad a L5 N 2L 8 Tel : 905-817-570 0 Tol l free:800-563-6266 Fax : 905-817-577 7



## VE S 00243 4Driven by service

and Science wwwjnaxxamauuUyttcs.co m ENS R Internationa

l CHen t Projec t # : 10002-017-82

0 Projec t name : ONY

X Sampler Initials : 

## ELEMENT S B YICP/M S (IMPINGE

R SOLUTION

) MaxxamI

D M7314 6 M7314 7 M7314 7 M7314 B M7314 9 Samolin qDate 2006/06/2 1 2006/06/1 9 2006/0671 9 2006706/20 2006/06/2 1

Jnit s M29-RBB H U29-U3-R 1 B H M29-U3-R 1

B H Lab-Du n M29U3-R 2

B H M29-U3-R 3

B H RD L X

Batc h MD L
Total Arseni c (As ) u g N D 0.3 3 03 3 N D 05 1 05 0 100175 8 05 0 Total BeryMum(Be ) u g N O N D N D 0.08 7 N D 9.05 0 100175 8 0.05 0 Total Chromiu m(Cr) u s N D 1.0 6 1.02 0.6 6 0.8 4 0.1 5 100175 8 0.1 5 I N D = No t

detecte d I R D L = Reportabl e Detectio nLimi t (Q C Batc h= Qualit

y Contro l Batc h

PageSo f 1 1
674 0 Campobell o Road , Mississauga , Ontari o Canad a L5 N 2L 8 Tel : 905-817-570 0 Tol l free:80f>563-626 6 Fax : 905-817-577 7 

# M a m

''/^Analytle s In c Maxxa m Jo b #: A66217

5 Repor t Date : 2006/09/1 1



## VE S 00243 5J>riven by service

and Science www.maxj»'maxuUytlcs^com ENS R Internationa

l Clien t Projec t * : 10002-017-82

0 Projec t name : ONY

X SamplerInitials : 

### Test Summar

y

Maxxa m I D Sampl e ID ' Matri x M7314 2

M29-RBF H Fitte r Collecte d Shippe d Receive d 2006/D672 1

2006706722 Tes t Descriptio n Instrumentatio n Batc h Prepare d Analyze d Anah/s t Metal s i n Ai r(Fron t Half ) b vICP/M S ICP1/M S 100100 8 2006/06/2 8 2006/06/2 9 N R Particulate s i n Ai r(Aceton e Rinse ) (MS ) BA L 100127 5 2006706/2 7 200670672 8 IM R Particulate s i n Ai r(Filter ) BA L 100126 5 2006/06/2 6 200670672 6 VP 2 Fina l Volume o f Aceton e Prob e Rins e 104987 0 2006/09/1 1 2006/09/1 1 FM O
Maxxa m I D Sampl e I D Matri x M7314 3

M29-U3-R 1 F H Filte r Collecte d Shippe d Receive d 2006706/1 9

2006706/2 2 Tes t Descriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t Metal s i n Ai r(Fron t Half ) b vICP/M S 1CP1/M S 100100 8 2006/06/2 8 2006706/2 9 N_ R Particulate s i n Ai r(Aceton e Rinse ) (M5 ) BA L 100127 5 2006/06/2 7 2006706728 - IM R Particulate s i n Ai r(Filter ) BA L 100126 5 2006/06/2 6 2006706/2 6 VP 2 Fina l Volume of Aceton e Prob e Rins e 104987 0 2006/09/1 1 2006/09/1 1 FM O
Maxxa m I D Sampl e I D Matri x M73143Du p

M29-U3-R 1 F H Filte r Collecte d Shippe d Receive d 2006/06/1 9

2006X16/2 2 Tes t Descriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t Metal s i n Ai r(Fron t Half) b vICP/M S ICP1/M S 100100 8 2006/06/2 8 2006706/2 9 N_ R I
Maxxa m I D Sampl e I D Matri x M7314 4

M29-U3-R 2 F H filter Collecte d Shippe d Receive d 200670672 0

2006/0672 2 Tes t Descriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t Metal s i n Ai r(Fron t Half ) b vICP/M S 1CP1/M S 100100 8 2006/06/2 8 2006/0672 9 N R Particulate s i n Ai r(Aceton e Rinse ) (MS ) BA L 100127 5 2006/0672 7 2006706/2 8 IM R Particulate s i n Ai r(Filter ) BA L 100126 5 2006/0672 6 2006/0672 6 VP 2 Fina l Volum e of Aceton e Prob e Rins e 104987 0 2006/09/1 1 2006/09/1 1 FM O
Maxxa m I D Sampl e I D Matri x M7314 5

M29-U3-R3F H Filte r - Collecte d Shippe d Receive d 2006/06/2 1

2006/06/2 2 Tes t Descriptio n Instrumentatio n Batc h Prepare d Analyze d Analys t Metal s i n Ai r(Fron t Half) b vICP/M S ICP1/M S 100100 8 2006/06/2 8 2006/0672 9 N R Particulate s i n Ai r(Aceton e Rinse ) (M5 ) BA L 100127 5 2006/0672 7 2006706/2 8 IM R Particulate s i n Ai r(Rlter) BA L 100126 5 2006/0672 6 2006/0672 6 VP 2 Fina l Volum e of Aceton e Prob e Rins e 104987 0 2006/09/1 1 2006/09/1 1 FM O

Pag e 6 of 1 1 .674 0 Campobell o Road , Mississauga , Ontari o Canad a L5N2L 8 Tel : 905-817-570 0 Tol l free:800-563-6266 Fax:905-817-5777 

# Maxxam . Maxxa m Jo b #:A66217

5 Repor t Date : 2006709/1 1



## VE S 00243 6Maxxa m Jo b # : A66217 5 Repor t Dale : 2006/09/1 1 • Driven

by service

and Science www-inaxxamaiuttycicswco m ENS R international Client Projec

t # : 10002-017-82

0 Projec t name : ONY

X SamplerInitials : 

### Tes t Summar

y

Maxxa m I D M7314 6 Sampl e I D M29-R8B H Matri xImpinge r Solutio n Tes t Descriptio n IMetal s i n Ai r(Bac k

Half) b vICP/M S Instrumentatio n Batc h Collecte d 2006/06/2 1 Shippe d Receive d 2006/06/2 2 Prepare d Analyze d Analys t ICP1/M S 100175 8 2006/06/2 9 2006/06/2 9 M R
Maxxa m I D M7314 7 Sampl e I D M29-U3-R 1 B H Matri xImpinge r Solutio n Tes t Descriptio n IMetal s i n Ai r (Bac k

Hall ) b y ICP/M S Instrumentatio n Batc h Collecte d 2006/06/1 9 Shippe d Receive d 2006/06/2 2 Prepare d Analyze d Analys t 1CP1/M S 100175 8 2006706/29 . 2006706729 M R
Maxxa m I D M7314 7 Ou p Sampl e I D M29-U3-R 1 B H Matri xImpinge r Solutio n Tes t Descriptio n IMetal s i n Ai r(Bac k

Hall ) b vICP/M S Instrumentatio n Batc h Collecte d 2006/06/1 9 Shippe d Receive d 2006/08/2 2 Prepare d Analyze d Analys t ICP1/M S 100175 8 2006/06/2 9 2006706729 M R

Tes t Descriptio n Maxxa m I D M7314 8 Sampl e 1 0 M29-U3-R 2 B H Matri xImpinge r Solutio n

Instrumentatio n Batc h Collecte d 2006/06/2 0 Shippe d Receive d 2006/06/2 2 Prepare d Analyze d Analys t IMetal s i n Ai r (Bac k

Half) b vICP/M S ICP1/M S 100175 8 2006/06/2 9 2006/0672 9 M R

Maxxa m I D M7314 9 Sampl e I D M29-U3-R3B H Matri xImpinge r Solutio n Tes t Descriptio n IMetal s i n Ai r (Bac k

Hall ) bvICP/M S Instrumentatio n Batc h Collecte d 2006/06/2 1 Shippe d Receive d 2006/06/2 2 Prepare d Analyze d Analys t ICP1/M S 100175 8 2006/0672 9 2006/0672 9 M R

Pag e 7 o f 1 1 674 0 Campobell o Road , Mississauga , Ontari o Canad a L5 N 2L8 Tel : 905-817-570 0 Tol l free:800-563-6266 Fax : 905-817-577 7



## VE S 00243 7

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l Maxxa m Jo b # : A66217 5 Client Projec t # : 10002*017-82

0 Repor t Date : 2006/09/1 1 Projec t name : ONY

X SamplerInitials :

GENERA L COMMENT S
Result s relat e onl y t o th e item s tested .

Pag e 8 o f 1 1 674 0 Campobell o Road , Mississauga , Ontari o Canad a L5 N 2L 8 Tel : 905-817-570 0 Tol l 1ree:S0O-563-626 6 Fax:905-817-5777



## VE S 00243 8

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and Science A/T ^.T^"."« 1 fcNSR Internationa l www.mju.owMiyucjxo m Attention : Jef

fGorman Clien t Projec t # : 10002-O17-82

0 P.O . # : Projec t name : ONY

X 

### Qualit y Assuranc

e Repor t Maxxa m Jo b Number : GA66217 5 QA/Q C Batc h Numfcli t QCTvp e Paramete r Dat e Analyze d ww/mm/d d Valu e %Recover v Unit s QCUrnts : 100100 8 N_ R MATRI XSPIK E

(M73143 ) Tota l Arseni c (As ) 2006/06/2 9 49.5 , ROU0.4 0 9 9 u g 70-130 : MATRI XSPIK E DUP(M73143 ) Tota l Arseni c (As ) 2006/06/2 9 49.5 , ROU0.4 0 9 9 " 3 70-130: : MATRI XSPIK E (M73143 ) Tota l Berylliu m (Be ) 20OSVD6/29 48.0 , RDUO.1 0 9 6 u g 70-130 . MATRI XSPIK E DUP(M73143 ) Tota l Berylliu m (Be ) 2006706/2 9 47.0 . RDU0.1 0 9 4 u g 70-130 > ; MATRI XSPIK E (M73143 ) Tota l Chromiu m (Cr) 2006706/2 9 48.5 , RDL=0.3 0 9 7 u g 7 0 -130 ' MATRI XSPIK E DUP(M73143 ) Tota l Chromiu m (Cr) 2006/06/2 9 47.5 , RDUO.3 0 9 5 u g 70-13 0 Spike d Blan k Tota l Arseni c (As ) 2006/06/2 9 485 , RDU0.4 0 9 7 u g 85- - 11 5 . Spike d Blan k

DU P Total Arseni c (As ) 2006706/2 9 49.0 , RDU0.4 0 9 8 u g 85-11 5 • Spike d Blan k Tota l Berylliu m (Be ) 2006/06/2 9 59.5 , RDUO.1 0 119(1 ) u g 85-11 5 Spike d Blan k

DU P Tota l Berylliu m (Be ) 2006/06/2 9 58.5 , RDUO.1 0 117(1 ) u g 8S-11 5 Spike d Blan k Total Chromiu m (Cr ) 2006/06/2 9 53.0 , RDUO.3 0 10 6 u g 85.-115 > Spike d Blan k

DU P Tota l Chromiu m (Cr ) 2006706/2 9 53.0 , RDUO.3 0 10 6 u g 85-115 1 Metho d Blan k Tota l Arseni c (As ) 2006/06/2 9 ND , RDU0.4 0 u g Metho d Blan k

OU P Tota l Arseni c (As ) 2006/06/2 9 ND , RDU0.4 0 u g Metho d Blan k Tota l Berylliu m (Be ) 2006/06/2 9 ND , RDUO.1 0 u g Metho d Blan k

OU P Tota l Berylliu m (Be ) 2006/06/2 9 ND , RDUO.1 0 u g Tota l Chromiu m (Cr ) 2006/06/2 9 ND . RDUO.3 0 u g Metho d Blan k Tota l Chromiu m (Cr) 2006/06/2 9 ND , RDUO.3 0 u g RP D Tota l Arseni c (As ) 2006/06/2 9 3. 4 % 2 0

Tota l Berylliu m (Be ) 2006/06/2 9 N C % 2 0 Tota l Chromiu m (Cr ) 2006/06/2 9 21.2(1 ) % 2 0 100127 5 IM R Metho d Blan k Particulat e Weigh t i n Aceton e Rins e 2006/06/2 8 ND , ROU0. 5 m g 100175 8 N_ R MATRI XSPIK E

(M73147) Tota l Arseni c (As ) 2006/06/2 9 48.5 , RDUO.2 0 9 7 u g 7 0 -13 0 MATRI XSPIK E DU P (M73147 ) Tota l Arseni c (As ) 2006/0672 9 50.0 , RDUO.2 0 10 0 u g 70-130 ' MATRI XSPIK E (M73147 ) Total Berylliu m (Be ) 2006/0672 9 57.5 , RDU0.05 0 11 5 u g 70-130 : MATRI XSPIK E DU P (M73147) Tota l Berylliu m (Be ) 2006/06/2 9 58.5 , RDU0.05 0 11 7 u g 70-13 0 MATRI XSPIK E (M73147) Tota l Chromiu m (Cr) 2006/06/2 9 50.0 . RDU0.1 5 10 0 u g 70-13 0 MATRI XSPIK E DU P (M73147) Tota l Chromiu m (Cr ) 2006/06/2 9 51.0 , RDU0.1 5 10 2 u g 7 0 -13 0 Spike d Blan k Tota l Arseni c (As ) 2006/06/2 9 50.5 , RDUO.2 0 10 1 u g 85 - 115 5 Spike d Blan k

DU P Tota l Arseni c (As ) 2006/0672 9 50.0 , RDUO.2 0 10 0 u g 85-11 5 Spike d Blan k Tota l Berylliu m (Be ) 2006/06/2 9 58.5 , RDU0.05 0 11 7 u g 85. - 115 i Spike d Blan k

DU P Tota l Berylliu m (Be ) 2006706/2 9 58.0 , RDU0.05 0 11 6 u g 85-115. . Spike d Blan k Tota l Chromiu m (Cr) 2006/0572 9 52.0 , RDUO.1 5 10 4 u g 85-11 5 Spike d Blan k

DU P Tota l Chromiu m (Cr ) 2006/0672 9 52.0 , RDUO.1 5 10 4 u g 85-11 5 Metho d Blan k Tota l Arseni c (As ) 2006/0672 9 ND , RDUO.2 0 u g Metho d Blan k

DU P Tota l Arseni c (As ) 2006/06/2 9 ND , RDUO.2 0 u g Metho d Blan k Tota l Berylliu m (Be ) 2006/06/2 9 ND , RDU0.05 0 u g Metho d Blan k

DU P Tota l Berylliu m (Be ) 2006/0672 9 ND , RDU0.05 0 u g Metho d Blan k Tota l Chromiu m (Cr) 2006/06/2 9 ND , RDUO.1 5 u g Metho d Blan k

DU P Tota l Chromiu m (Cr) 2006/06/2 9 ND , RDU0.1 S u g RP D Tota l Arseni c (As ) 2006/06/2 9 N C % 2 0

Tota l Berylliu m (Be ) 2006/06/2 9 N C % 20 : Tota l Chromiu m (Cr) 2006/0672 9 4. 2 % 2 0 N O = No t detecte d Page 9 o f1 1 674 0 Campobell o Road , Mississauga , Ontari o Canad a L5N2L 8 Tel : 905-817-570 0 Tol l free:800-S63-6266 Fax:905-817-5777



## VE S 00243 9Ztrjyen by service

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### VE S 00244 1

# D

VE S 00244 2

## Fiur

UNITE D STATE S ENVIRONMEN TA L PROTECTIO N AGENC Y REGIO N S I N TH E MATTE R OF ; Veoli a E S Technica l Solutions , LL C 7 Mobil e Avenu e Sauget , Illinoi s 6220 1 ATTENTION S Dougla s Harris , Genera l Manage r Reques t t o Provid e Informatio n Pursuan t t o th e Clea n Ai r Ac t Th e U.S . Environmenta l Protectio n Agenc y i s requirin g Veoli a E S Technica l Solutions , LL C (Veoli a o r you ) t o submi t certai n informatio n abou t you r hazardou s wast e incinerator s a t 7 Mobil e Avenue , Sauget , Illinois . Appendi xB specifie s th e informatio n tha t yo u mus t submit . Yo u mus t sen d thi s informatio n t o u s accordin g t o th e schedul e i n Appendi xB . W e ar e issuin g thi s informatio n reques t unde r sectio n 114(a ) o fth e Clea n Ai r Ac t (Act) , 4 2 U.S.C . § 7414(a) . Sectio n 114(a ) authorize s th e Administrato r o f EP A t o requir e th e submissio n o f information . Th e Administrato r ha s delegate d thi s authorit y t o th e Directo r o f th e Ai r an d Radiatio n Division , Regio n 5 . Veoli a own s an d operate s a n emissio n source , thre e hazardou s wast e incinerator s a t 7 Mobil e Avenue , a t it s Sauget , Illinois , facility . W

e ar e requestin g thi s informatio n t o determin e whethe r you r emissio n source s ar e complyin g wit h th e Nationa l Emissio n Standard s fo r Hazardou s Ai r Pollutant s fro m Hazardou s Wast e Combustors , 4 0 CF R 63 , Subpar t EE E (hereinafter , "th e HW C MACT" ) an d t o establis h th e appropriat e operatin g paramete r limit s fo r eac h incinerator . Yo u mus t sen d al l required , informatio n to : Attn : Complianc e Tracker , AE-17 J



## VE S 00244 3M r Enforcemen t an d Complianc e Assuranc e Branc h U.S . Environmenta l Protectio n Agenc y Regio n 5 7 7 W . Jackso n Boulevard , AE-17 J Chicago , Illinoi s 6060 4 Wit h copie s t o Illinoi s Environmenta l Protectio n Agency : Ra y Pilapil , Manage r Complianc e an d Enforcemen t Sectio n Burea u o fAi r Illinoi s Environmenta l Protectio n Agenc y 102 1 Nort h Gran d Avenu e Eas t Springfield , Illinois , 6270 2 An d Michae l Reed , Uni t Manage r Clea n Ai r Ac t Permi t Progra m Burea u o fAi r Illinoi s Environmenta l Protectio n Agenc y 102 1 Nort h Gran d Avenu e Eas t Springfield , Illinoi s 6270 2 Yo u ma y conside r th e informatio n confidentia l tha t yo u submi t t o us . Yo u ma y asser t a clai m o fbusines s confidentialit y f o r an y portio n o fth e submitte d informatio n unde r 4 0 C.F.R . Par t 2 , Subpar t B . Appendi xA specifie s th e assertio n an d substantiatio n requirement s fo r busines s confidentialit y claims . Veoli a mus t submi t al l requested , informatio n unde r a n authorize d signatur e wit h th e followin g certification : I certif y unde r penalt y o fla wtha t I hav e examine d an d a m familia r wit h th e informatio n i n th e enclose d documents , includin g al l attachments . Base d o n m y inquir y o fthos e individual s wit h primar y responsibilit y fo r obtainin g th e information , I certif y tha t th e statement s an d informatio n are , t o th e best , o fm y knowledg e an d belief , tru e an d complete . I a m awar e tha t ther e ar e significan t penaltie s f o r knowingl y submittin g fals e statement s an d information , includin g th e possibilit y o ffine s o r imprisonmen t pursuan t t o sectio n 113(c)(2 ) o fth e Act , an d 1 8 U.S.C . § § 100 1 an d 1341 . W e ma y us e an y informatio n submitte d in . respons e t o thi s reques t i n a n administrative , civil , o r crimina l action .Thi s reques t i s no t subjec t t o th e Paperwor k Reductio n Act , 4 4 U.S.C . § 350 1 e t seq. , becaus e i t seek s collectio n o f informatio n fro m specifi c individual s o r entitie s a s par t \ o£ a n administrativ e actio n o xinvestigation . T o ai d i n our'electroni c recor d keepin g efforts , pleas e provid e you r respons e t o thi s reques t fo r informatio n withou t staples . Pape r clips , binde r clips , an d 3-rin g binder s ar e acceptable . Failur e t o compl y full y wit h thi s reques t fo r informatio n ma y subjec t Veoli a t o a n enforcemen t actio n unde r sectio n 11 3 o f th e Act , 4 2 U.S.C . § 7413 . Yo u shoul d direc t an y question s abou t thi s reques t fo r informatio n t o Charle s Hal l a t (312 ) 353-3443 .

Dat e Chery l L . 

### Newtotff, Actin g Directo r A i ran d Radiatio n Divisio n



### 3



### VE S 00244 5Appendi xA Confidentia l Busines s Informatio n (CBI ) Assertio n an d Substantiatio n Requirement s A . Assertio n Requirement s Yo u ma y asser t a busines s confidentialit y clai m coverin g al l o rpar t o fth e informatio n requeste d i n th e attache d letter , a s provide d i n 4 0 C.F.R . § 2.203(b) . T o mak e a confidentialit y claim , submi t th e requeste d informatio n an d indicat e tha t yo u ar e makin g a clai m o fconfidentiality . An y documen t ove r whic h yo u mak e a clai m o fconfidentialit y shoul d b e marke d b y attachin g a cove rshee t stampe d o r type d wit h a legen d t o indicat e th e inten t t o clai m confidentiality . Th e stampe d o r type d legend , o r othe r suitabl e for m o fnotice , shoul d emplo y languag e suc h a s "trad e secret " o r "proprietary " o r "compan y confidential " an d indicat e a dat e i fan y whe n th e informatio n shoul d n o longe r b e treate d a s confidential . Informatio n covere d b y suc h a clai m wil l be | disclose d b y th e EP A onl y t o th e exten t permitte d an d b y mean s o f th e procedure s se t fort h b y Sectio n 114(c ) o fth e Clea n Ai r Ac t (th e Act) , an d 4 0 C.F.R . Par t 2 . Allegedly.confidentia l portion s o fotherwis e nonconfidentia l document s shoul d b e clearl y identified . EP A wil l constru e th e failur e t o furnis h a confidentialit y clai m wit h you r respons e t o th e attache d lette r a s a waive r o ftha t claim , an d th e informatio n may b e mad e availabl e t o th e publi c withou t furthe r notic e t o you . Pleas e segregat e personnel , medica l an d simila r file s fro m you rresponse s an d includ e tha t informatio n o n separat e sheet(s ) marke d a s "Persona l Privac y Information " give n tha t disclosur e o f suc h informatio n t o th e genera l publi c ma y constitut e a n invasio n o fprivacy . B . Substantiatio n Requirement s A l l confidentialit y claim s ar e subjec t t o EP A verificatio n an d mus t b e mad e i n accordanc e wit h 4 0 C.F.R . § 2.20 8 whic h provide s i n par t tha t yo u satisfactoril y sho wtha t yo u hav e take n reasonabl e measure s t o protec t th e confidentialit y o fth e ' informatio n an d tha t yo u inten d t o continu e t o d o so ; an d tha t th e informatio n i s no t an d ha s no t bee n reasonabl y obtainabl e b y legitimat e mean s withou t you r consent . I Pursuan t t o 40 C.F.R . Par t 2 , Subpar t B , EP A ma y a t an y tim e sen d yo u a lette r askin g yo u t o substantiat e full y ybu r CB I claim . I fyo u receiv e suc h a letter , yo u mus t provid e EP A wit h a respons e withi n th e numbe r o fday s se t fort h i n th e EP A reques t letter . Failur e t o submi t you r comment s withi n tha t tim e woul d b e regarde d a s a waive r o fyou r confidentialit y clai m o r claims , an d EP A ma y releas e th e information . I fyo u receiv e suchj aletter , EP A wil l as k yo u t o specif y whic h portion s o fth e informatio n yo u conside r confidential . Yo u mus t b e specifi c b y page , paragraph , an d sentenc e whe n identifyin g th e informatio n subjec t t o you r claim . An y informatio n no t specificall y identifie d a s subjec t t o a confidentialit y clai m ma y b e disclosed , t o th e requesto r withou t furthe r notic e t o you . Fo r eac h ite m o r clas s o finformatio n tha t yo u identif y a s bein g subjec t t o CBI , yo u mus t answe r th e followin g questions , givin g a s muc h detai l a s possible ; 1 . Fo r wha t perio d o ftim e d o yo u reques t tha t th e informatio n b e maintaine d a s confidential , e.g. , unti l a certai n date , unti l th e occurrenc e o fa specifie d event , o r permanently ? I fth e occurrenc e o fa specifi c even t wil l eliminat e th e nee d fo r confidentiality , pleas e specif y tha t event . 2 . Informatio n submitte d t o EP A become s stal e ove r time . Wh y shoul d th e informatio n yo u clai m a s confidentia l b e protecte d fo r th e tim e perio d specifie d in.you r answe r t o questio n #1 ? 3 . Wha t measure s hav e yo u take n t o protec t th e informatio n claime d a s confidential ? Hav e yo u disclose d th e informatio n t o anyon e othe r tha n a governmenta l bod y o r someon e wh o i s boun d b y a n agreemen t no t t o disclos e th e informatio n further ? I fso , wh y shoul d th e informatio n stil l b e > considere d confidential ? 4 . I s th e informatio n containe d i n an y publicl y availabl e materia l suc h a s th e Internet , publicl y availabl e databases , promotiona l publications , annua l reports , o r articles ? I s ther e an y mean s b y whic h a membe r o fth e publi c coul d obtai n acces s t o th e information ? I s th e informatio n o fa kin d tha t yo u woul d customaril y no t releas e t o th e public ? 5 . Ha s an y governmenta l bod y mad e a determinatio n a s t o th e confidentialit y o fth e information ? I fso , pleas e attac h a cop y o fth e determination . 6 . Fo r eac h categor y o finformatio n claime d a s confidential , explai n wit h specificit y wh y releas e o fth e informatio n i s likel y t o caus e substantia l har m t o you r competitiv e position . Explai n th e specifi c natur e o fthos e harmfu l effects , wh y the y shoul d b e viewe d a s substantial , an d th e causa l relationshi p betwee n disclosur e an d suc h harmfu l effects . Howcoul d you r competitor s mak e us e o fthi s informatio n t o you r detriment ? 7 . D o yo u asser t tha t th e informatio n i s submitte d o n a

### voluntar y o r a mandator y

basis ? Pleas e explai nth e reaso n f o r you r assertion . I f yo u asser t tha t th e informatio ni s voluntaril y

submitte dinformation , explai nwhethe r an d wh y disclosur e o f th e informatio nwoul dten dt o lesse nth e availabilit y

t o EP A

o f simila r informatio ni nth e future . 8 . An y

othe r issu e yo u dee m relevant . Pleas e not e tha t emissio ndat a provided , unde r Sectio n11 4 o f th e Act , 4 2 U .S.C . § 7414 , i s no t entitle dt o confidentia l treatmen t unde r 4 0 C.F.R . Par t 2 . "Emissio ndata " means , wit hreferenc e t o an y sourc e o f emissio no f an y substanc e int o th e air - Informatio nnecessar y t o determin e th e identity , amount , frequency , concentration , o r othe r characteristic s (t o th e exten t relate dt o ai r quality ) o f an y emissio nwhic hha s bee nemitte db y

th e sourc e (o r o f an y pollutan t resultin g fro m an y emissio nb y

th e source) , o r an y combinatio no f th e foregoing ; Informatio nnecessar y t o determin e th e identity , amount , frequency , concentration , o r othe r characteristic s (t o th e exten t relate dt o ai r quality ) o f th e emission s which , unde r a napplicabl e standar do r limitation , th e sourc e wa s authorize dt o emi t (including , t o th e exten t necessar y fo r suc hpurposes , a descriptio no f th e manne r an d rat e o f operatio no f th e source) ; an d A genera l descriptio no f th e locatio nand/o r natur e o f th e sourc e t o th e exten t necessar y t o identif y

th e sourc e an d t o distinguis hi t fro m othe r source s (including , t o th e exten t necessar y

fo r suc hpurposes , a descriptio no f th e device ,

. installation , o r operatio nconstitutin g th e source) . 4 0 C.F.R . § 2.301(a ) (2 ) (i ) (A) , (B ) an d (C ) . Emissio ndat a includes , bu t i s no t limite dto , servic e records , statin g th e amoun t o f refrigeran t adde dt o a uni t o r reclaime d fro m a unit . I f yo u receiv e a reques t fo r a substantiatio nlette r fro m th e EPA , yo u bear.th e burde no f substantiatin g you r confidentialit y

claim . Conclusor y allegation s wil l b e give n little.o r n o weigh t i nth e determination . I nsubstantiatin g you r CB I claim(s) , yo u mus t bracke t al l tex t s o claime dan d mar k i t "CBI. " Informatio ns o designate dwil l b e disclose db y EP A onl y t o th e exten t allowe dby , an d b y mean s o f th e procedure s se t fort hin , 4 0 C.F.R . Par t 2 , Subpar t B . I f yo u fai l t o clai m th e

### informatio na s confidential , i t ma y b e made availabl e t o th e publi c withou t furthe r notic e t o you .

4



## VE S 00244 9APPENDI XB 

### Veolia . mus t submi t th e followin g informatio nregardin g Incinerato r 2 , Incinerato r 3 , an d Incinerato r 4 locate da t 7 Mobil e Avenue , Sauget , Illinoi s i naccordanc e wit hth e foregoin g reques t fo r informatio nmade pursuan t t o Sectio n114(a ) o f th e Clea nAi r Act , 4 2 U.S.C . § 7414(a) . 1 . No late r tha nJul y 15 , 2008 , Veoli a shal l conduc t a comprehensiv e performanc e tes t (CPT ) o neac hincinerato r t o demonstrat e complianc e wit hth e emissio nstandard s se t fort h i n4 0 C.F.R . § § 63.1219(a ) an d 63.1219(c ) an d t o establis h th e applicabl e operatin g paramete r limit s (OPLs ) Unde r 4 0 C.F.R . § 63.1209 . 2 . Veoli a ma

y no t reques t pursuan t t o 4 0 C.F.R . § 63.1207(c)(2 ) tha t previou s emission s tes t dat a serv e a s documentatio no f complianc e wit hth e emissio nstandard s se t fort hi n4 0 C.F.R . § § 63.1219(a ) an d 63.1219(c ) an d t o establis hth e applicabl e OPL s unde r 4 0 C.F.R . § 63.1209 . 3 . N o late r tha n4 5 day s afte r th e receip t o f thi s request , Veoli a shal l submi t t o EP A a CP T Pla ntha t include s th e informatio nspecifie da t 4 0 C.F.R . § 63.1207(f)(1) . W e hav e liste dbelo w

severa l item s tha t EP A believe s wer e missin g fro m Veolia' s CP T Pla ndate dDecembe r 29 , 2003 :
a . Pursuan t t o 4 0 C.F.R . § 63.1207(f ) (1)(i)(A) , Veoli a mus t includ e a nanalysi s o f eac hfee dstream , includin g hazardou s waste , othe r fuels , an d industria l furnac e fee dstocks , a s fired , tha t include s th e heatin g value , concentration s o f ash , lo w volatil e metal s (LVM ; arsenic , beryllium , an d chromium) , semivolatil e metal s (SVM. ; cadmiu

m an d lead) , mercury , an d tota l (organi c an dinorganic ) chlorine . b . Pursuan t t o 4 0 C.F.R . § 63.1207(f)(1)(ii)(A) , Veoli a mus t identif y

eac horgani c HA P establishe db y 4 2 U.S.C . § 7412(b)(1) , excludin g caprolacta m (CA S numbe r 105602 ) a s provide db y

§ 63.60 , tha t i s presen t i neac h hazardou s wast e fee dstream . c . Pursuan t t o 4 0 C.F.R . § 63.1207(f)(1)(ii)(B) , Veoli a mus t provide , withi nth e precisio nproduce db y analytica l procedure s o f 4 0 C.F.R. . § 63.1208(b)(8) , th e approximat e quantificatio no f th e identifie dorgani c HAP s i nth e hazardou s wast e feedstreams . d . Pursuan t t o 4 0 C.F.R . § 63.1207(f)(1)(iii)(G) , Veoli a mus t includ e a detaile dengineerin g descriptio no f th e

### design , operation , an dmaintenanc e practice s fo r an y a i r pollutio ncontro l syste m fo r eac hhazardou s wast e incinerator . e . Pursuan t t o 4 0 C.F.R . § 63.1207(f ) (1 ) (iv) , Veoli a mus t includ e a detaile ddescriptio no f samplin g an d monitorin g procedures , includin g samplin g an d monitorin g location s i nth e system , th e equipmen t t o b e used , samplin g an dmonitorin g frequency , an dplanne d analytica l procedure s fo r sampl e analysis . f . Pursuan t t o 4 0 C.F.R . § 63.120 7 (f)(1)(v) , Veoli a mus t includ e a detaile dtes t schedul e fo r eac hhazardou s wast e fo r whic hth e performanc e tes t i s planned , includin g date(s) , duration , quantit y o f hazardou s wast e t o b e burned . g . Pursuan t t o 4 0 C.F.R - § 63.1207(f)(1)(vi) , Veoli a mus t includ e a detaile dtes t protocol , including , fo r eac h hazardou s wast e identified , th e range s o f hazardou s wast e feedrat e fo r eac hfee dsystem , and , a s appropriate , th e feedrate s o f othe r fuel s an d feedstocks , an dan y othe r relevan t parameter s tha t ma y affec t th e abilit y o f th e HW

C t o mee t th e emissio n standards . h . . Pursuan t t o 4 0 C.F.R . § 63.1207(f)(1)(vii) , Veoli a mus t includ e a descriptio nof , an dplanne doperatin g condition s for , an y emissio ncontro l equipmen t tha t wil l b e used . i . Pursuan t t o 4 0 C.F.R . § 63.1207(f)(1)(xi) , i f Veoli a doe s no t continuousl y monito r regulate dconstituent s i n natura l gas , proces s ai r feedstreams , an dfeedstream s fro m vapo r recover y

system s unde r 4 0 C.F.R . § 63.1209(c)(5) , Veoli a mus t documen t th e expecte d level s o f regulate dconstituent s i nthos e feedstreams . j . Pursuan t t o 4 0 C.F.R . § 63.1207(f)(1)(xix) , Veoli a mus t documen t th e temperatur e locatio nmeasuremen t i nth e CP T plan . k . Fo r Incinerato r 4 only , pursuan t t o 4 0 C.F.R . § 63.1207(f)(1)(xx)(A) , Veoli a mus t documen t th e manufacture r specification s fo r minimu m carrie r flui d flowrat e o r pressur e drop . 1 . Fo r Incinerato r 4 only , pursuan t t o 4 0 C.F.R . § 63.1207(f)(1)(xx)(B) , Veoli a roust identif y th e ke y parameter s tha t affec t carbo nadsorption , an dth e 2



## VE S

### operatin g limit s yo uestablis hfo r thos e parameter s base do nth e carbo nuse ddurin g th e performanc e test , i f yo uelec t no t t o specif y an dus e th e bran dan dtyp e o f carbo nuse ddurin g th e CPT . m . Pursuan t t o 4 0 C.F.R . § 63.1207(f)(1)(xxv) , Veoli a mus t documen t ke y

parameter s tha t affec t adsorptio no f hydroge nchlorid e an dchlorin e ga s (HCl/Clz ) an dth e limit s yo uestablis hfo r thos e parameter s base do nth e sorben t use ddurin g th e performanc e test . n . Pursuan t t o 4 0 C.F.R . § 63.1207(f)(1)(xxvi) , fo r purpose s o f calculatin g SVM , LVM , mercury , tota l (organi c an dinorganic ) chlorine , an das hfee drat e limits , Veoli a mus t describ e ho w th e compan

y wil l handl e performanc e tes t fee dstrea m analytica l result s tha t determin e thes e constituent s ar e no t presen t a t detectabl e levels . o . Pursuan t t o 4 0 C.F.R . § § 63.1207(f)(1)(xxvii ) an d 63.1219(c)(3 ) (ii) , Veoli a mus t identif y on e o r mor e principa l organi c hazardou s constituent(s ) tha t represen t th e mos t difficul t t o destro y organi c compound s i nit s hazardou s wast e feedstreams . Veoli a mus t bas e thi s specificatio no nth e degre e o f difficult y

o f incineratio no f th e organi c constituent s i nth e hazardou s wast e an do nthei r concentratio no r mas s i nth e hazardou s wast e feed , considering ; th e result s o f hazardou s wast e analyse s o r othe r dat a an d information . Veoli a ma

y reques t EPA' s approva l t o extrapolat e th e fee d rate s o f LVMs , SVMs , o r mercury . I nsuc ha request , Veoli a mus t include :
a . A descriptio no f th e extrapolatio nmethodolog y an d rational e fo r ho

w th e approac hensure s complianc e wit h th e emissio nstandards ; b . Documentatio no f th e historica l rang e o f norma l an d maximu m (i.e. , othe r tha ndurin g complianc e testing ) metal s fee drate s fo r eac hfeedstream ;
c . Documentatio ntha t th e leve l o f spikin g recommende d durin g th e performanc e tes t wil l mas k samplin g an d analysi s imprecisio nan dinaccurac y t o th e exten t tha t th e extrapolate dfee drat e limit s adequatel y assur e complianc e wit hth e emissio nstandards ; d . Documentatio no f whethe r som e leve l o f spikin g woul db e

### appropriat e an d whethe r th e physica l for m an d specie s o f spike dmateria l i s appropriate ; an d
e . A nestimat e o f th e extrapolate dLVM , SVM , an d mercury fee drates . 5 . Veoli a ma y reques t EPA' s approva l t o us e Metho d2 3 fo r dioxins/furan s instea do f Metho d0023A . I nsuc ha request , Veoli a mus t includ e th e result s o f al l previou s dioxin/fura n (D/F ) performanc e tests . 6 . Veoli a ma y includ e a napplicatio nt o reques t alternativ e monitorin g unde r 4 0 C.F.R . § 63.1209(g)(1) . 7 . Durin g th e CPT , Veoli a mus t collec t sufficien t dat a t o establis hal l necessar y OPLs . EP A

believe s tha t th e followin g OPL s se t fort hi n4 0 C.F.R . § 63.1209(j-p ) appl y t o eac hincinerator :
a . Incinerato r # 2 63.120 9 HAP 1 

### OP L (j)(l) , (k)(2 ) DRE 2 

### , D/ F Minimu m Primar y

Combustio nChambe r Temperatur e (j)(l) , (k)(2 ) DRE , D/ F Minimu m Secondar y

Combustio n Chambe r Temperatur e (j)(2) , (k)(3) , (m)(2) , (n)(5) , (o ) (2 ) DRE , D/F , PM , 3 

### SVM/LVM , HC1/C1 2 

### Maximu m Flu e Ga s Flo w

Rat e (j)(3) , (k)(4 ) DRE , D/ F Maximum PC C Tota l Hig hBT ULiquid s Wast e Fee dRat e (j)(3) , (k ) (4 ) DRE , D/ F Maximum PC C Tota l Solid s Wast e Fee d Rat e ( j ) (3 ) , (k ) (4 ) DRE , D/ F Maximu m PC C Tota l Lo

w BT ULiquid s Wast e Fee dRat e (j){3) , (k)(4 ) DRE , D/ F Maximum PC C Tota l Specialt y Fee d Wast e Fee dRat e (j)(3) , (k ) (4 ) DRE , D/ F Maximum SC C Tota l Hig hBT ULiquid s Wast e Fee dRat e (j)(3) , (k ) (4 ) DRE , D/ F Maximum PCC , SC C Tota l Wast e Fee d Rat e (j)(3) , (k ) (4 ) DRE , D/ F Maximum PC C Pumpabl e Hig hBT U Liquid s Wast e Fee dRat e (j)(3) , (k ) (4 ) DRE , D/ F Maximum PC C Pumpabl e Solid s Wast e Fee dRat e 1 HA P = hazardou s ai r pollutant . 2 DR E = Destructio nan d Remova l Efficiency . 3 P M = Particulat e matter . 

### 4



## VE S 00245 3

### 63.120 9 HAP 1 

### OP L (j)(3) , (k) (4 ) DRE , D/ F Maximu m PCC Pumpabl e Do

w BT U Liquid s Wast e Fee dRat e (j)(3) , (k)(4 ) DRE , D/ F Maximu m PCC Pumpabl e Specialt y Fee d Wast e Fee dRat e (j)(3> , (k)(4 ) DRE , D/ F Maximu m PCC Pumpabl e Wast e Fee d Rat e (j)(3) , (k)(4 ) DRE , D/ F Maximu m SCC Pumpabl e Wast e Fee d Rat e (j)(4 ) DRE Wast e Firin g Syste m OP L fo r High . BT ULiquid s (j)(4 ) DRE Wast e Firin g Syste m OP L fo r Lo

w BT U Liquid s (k ) (1 ) , (n ) (1 ) DRE , SVM/LV M Maximu

m Fabri c Filte r Inle t Temperatur e (1)(1 ) (i ) Mercur y Maximu m Mercur y

Fee dRat e (in ) (1 ) (iv ) P M Representativ e an d reliabl e

indicato r o f P

M contro l devic e performanc e (m ) (3 ) P M Maximu m As hFee dRat e (n ) (2 ) (i ) SV M Maximu

m SV M Fee dRat e (n ) (2 ) (ii ) LV M Maximu

m Tota l LV

M Fee dRat e (n ) (2 ) (vi ) LV M Maximu

m Pumpabl e LV

M Fee dRat e (o ) (1 ) (i ) SVM/LVM , HCi/Cl 2 Maximu m HC1/C1 2 

### Fee dRat e (o ) (4 ) (i ) HCl/Cl a Spra y Dr y Adsorber : Minimu m Sorben t Fee dRat e (o ) (4 ) (ii ) HC1/C1 2 

### Spra y Dr y Adsorber : Minimu m Carrie r Flui dFlo w

Rat e O r Nozzl e Pressur e Dro p (o ) (4 ) (iii ) (A ) HC1/C1 2 

### Spra y Dr y Adsorber : Specif y an d us e th e Bran dan d Typ e o f Carbo nuse d durin g th e CP T (P ) A l l Maximu m Combustio nChambe r Pressur e b . Incinerato r # 3 63.120 9 HA P OP L (j)(l) , (k ) (2 ) DRE , D/ F Minimu m Primar y

Combustio nChambe r Temperatur e (j)(l) , (k)(2 ) DRE , D/ F Minimu m Secondary . Combustio n Chambe r Temperatur e (j)(2) , (k)(3) , (m)(2) , (n)(5) , (o ) (2 ) DRE , D/F , PM , SVM/LVM , HC1/C1 Z 

### Maximu m Flu e Ga s Flo w

Rat e (j)(3) , (k)(4 ) DRE , D/ F Maximu m PCC Tota l Hig hBT ULiquid s Wast e Fee dRat e

### 63.120 9 HA P OP L (j)(3) , <k)(4 ) DRE , D/ F Maximu m PC C Tota l Solid s Wast e Fee d Rat e (j)(3) , (k)(4 ) DRE , D/ F Maximu m PC C Tota l Lo wBT U Liquid s Wast e Fee d Rat e (j)(3) , (k)(4 ) DRE , D/ F Maximu m PC C Tota l Specialt y Fee d Wast e Fee d Rat e (j)(3) , (k)(4 ) DRE , D/ F Maximu m SC C Tota l Hig h BT U Liquid s Wast e Fee d Rat e (j)(3) , (k)(4 ) DRE , D/ F Maximu m PCC , SC C Tota l Wast e Fee d Rat e (j)(3) , (k)(4 ) DRE , D/ F Maximu m PC C Pumpabl e Hig h BT U Liquid s Wast e Fee d Rat e (j)<3) , (k ) (4 ) DRE , D/ F Maximu m PC C Pumpabl e Solid s Wast e Fee d Rat e (j)(3) , (k)(4 ) DRE , D/ F Maximu m PC C Pumpabl e Lo wBT U Liquid s Wast e Fee d Rat e (j)(3) , (k)(4 ) DRE , D/ F Maximu m PC C Pumpabl e Specialt y Fee d Wast e Fee d Rat e (j)(3) , (k)(4 ) DRE , D/ F Maximu m PC C Pumpabl e Wast e Fee d Rat e (j)(3) , (k)(4 ) DRE , D/ F Maximu m SC C Pumpabl e Wast e Fee d Rat e (j ) (4 ) DR E Wast e Firin g Syste m OP L fo r Hig h BT U Liquid s (j)(4 ) DR E Wast e Firin g Syste m OP L fo r Lo wBT U Liquid s (k)(l) , (n)(l ) DRE , SVM/LV M Maximu m Fabri c Filte r Inle t

Temperatur e (1 ) (1)(i ) Mercur y Maximu m Mercur y Fee d Rat e (m ) (1 ) (iv ) P M Representativ e an d reliabl e indicato r o f P M contro l devic e performanc e (m ) (3 ) P M Maximu m As h Fee d Rat e (n)(2)(i ) SV M Maximu m SV M Fee d Rat e (n)(2)(ii ) LV M Maximu m Tota l LV M Fee d Rat e (n ) (2 ) (vi ) LV M Maximu m Pumpabl e LV M Fee d Rat e (o ) (1)(i ) SVM/LVM , HCI /CI 2 Maximu m HCI /CI 2 Fee d Rat e (o ) (4 ) (i ) HCI /CI 2 Spra y Dr y Adsorber : Minimu m Sorben t Fee d Rat e (o)(4)(ii ) HCI /CI 2 Spra y Dr y Adsorber : Minimu m Carrie r Flui d Flo wRat e Or . Nozzl e Pressur e Dro p (o ) (4 ) (iii ) (A ) HC1/C1 2 Spra y Dr y Adsorber : Specif y an d us e t h e Bran d an d Typ e o f Carbo n use d durin g th e CP T (P ) A l l Maximu m Combustio n Chambe r Pressur e 6



## VE S 00245 5

### c . Incinerato r # 4 63.120 9 HA P OP L (j)(l) , (k)(2 ) ORE , D/ F Minimu m Primar y

Combustio nChambe r Temperatur e (j)(l) , <k)(2 ) DRE , D/ F Minimu m Secondar y

Combustio n Chambe r Temperatur e (j)(2) , (k)(3) , (ni ) (2) , (n)(5) , (o ) (2 ) DRE , D/F , PM , SVM/LVM , HC1/C1 2 

### Maximu m Flu e Ga s Flo w

Rat e (j)(3) , (k)<4 > DRE , D/ F MajdjTtu m PC C Tota l Hig hBT ULiquid s Wast e Fee dRat e (j)(3) , (k)(4 ) DRE , D/ F Maximu m PC C Tota l Solid s Wast e Fee d Rat e (j)(3) , (k)(4 ) DRE , D/ F Maximu m PC C Tota l Lo

w BT ULiquid s Wast e Fee dRat e (j)(3) , (k)(4 ) DRE , D/ F Maximu m PC C Tota l Specialt y Fee d Wast e Fee dRat e (j)<3) , (k)(4 ) DRE , D/ F Maximu m SC C Tota l Hig hBT ULiquid s Wast e Fee dRat e (j)(3) , (k)(4 ) DRE , D/ F Maximu m PCC , SC C Tota l Wast e Fee d Rat e <j)(3) , (k)(4 ) DRE , D/ F Maximu m PC C Pumpabl e Hig hBT U Liquid s Wast e Fee dRat e (j)(3) , (k)(4 ) DRE , D/ F Maximu m PC C Pumpabl e Solid s Wast e Fee dRat e . (j)(3) , (k)(4 ) DRE , D/ F Maximu m PC C Pumpabl e Lo w BT U Liquid s Wast e Fee dRat e <j)(3) , (k)(4 ) DRE , D/ F Maximu m PC C Pumpabl e Specialt y Fee d Wast e Fee dRat e {j)(3) f 

### (k)<4 ) DRE , D/ F Maximu m PC C Pumpabl e Wast e Fee d Rat e (j)(3) , (k)(4 ) DRE , D/ F Maximu m SC C Pumpabl e Wast e Fee d Rat e ( j ) (4 ) DR E Wast e Firin g Syste m OP L fo r Hig h BT ULiquid s (j)(4 ) DRE Wast e Firin g Syste m OP L fo r Lo

w BT U Liquid s (k)(l) , (n)(1 ) DRE , SVM/LV M Maximu

m Fabri c Filte r Inle t Temperatur e (k ) (6)(i ) D/ F Minimu m carbo nInjectio nRat e (k ) (6)(ii ) D/ F Minimum Carrie r Flui d(Ga s o r Liquid ) Flo w

Rat e o r Pressur e Dro p (k)(6)(iii)(A ) D/ F Bran d(i.e. , Manufacturer ) an d Typ e o f Carbo n (1)(1)(i ) Mercur y Maximu m Mercur y

Fee dRat e 7



## VE S 00245 6

### 63.120 9 HA P OP L (m ) (1 ) (iv ) P M Representativ e an d Reliabl e

Indicato r o f P

M Contro l Devic e Performanc e (m)(3 ) P M Maximu m As hFee dRat e (n ) (2 ) (i ) SV M Maximu

m SV M Fee dRat e (n ) (2 ) (ii ) LV M Maximu

m Tota l LV

M Fee dRat e (n ) (2 ) (vi ) LV M Maximu

m Pumpabl e LV

M Fee dRat e '(o ) (1 ) (i ) SVM/LVM , HCI/CI 2 

### Maximu m HC1/C1 2 

### Fee dRat e (o. ) (4 ) (i ) HCl/Cl 2 

### Spra y Dr y Adsorber : Minimu m Sorben t Fee dRat e (o ) (4)(ii ) HC1/C1 2 

### Spra y Dr y Adsorber : Minimu m Carrie r Flui dFlo w

Rat e o r Nozzl e Pressur e Dro p (o ) (4 ) (iii ) (A ) HC1/C1 2 Spra y Dr y Adsorber : Specif y an d us e th e Bran dan d Typ e o f Carbo nuse d durin g th e CP T (P ) A l l Maximu m Combustio nChambe r Pressur e Veoli a i s responsibl e fo r identifyin g an y additiona l applicabl e OPLs . 8 . I nadditio nt o th e OPL s liste dabove , pursuan t t o 4 0 C.F.R . § 63.1209(g)(2) , th e Administrato r require s Veoli a t o establis ha maximu m quenc houtle t temperatur e OP L fo r eac h incinerator . Veoli a mus t establis ha maximu m hourl y

rollin g averag e limi t a s th e averag e o f th e tes t ru naverages . 9 . Durin g th e CP T o heac hincinerator , Veoli a mus t fee dnorma l (o r higher ) level s o f chlorin e durin g th e dioxin/fura n performanc e test . 10 . Durin g th e CP T o neac hincinerator , Veoli a mus t fee dnorma l (o r higher ) level s o f as hdurin g th e LV M an d SV

M performanc e tests . 11 . Durin g th e CP T o nIncinerato r 4 , Veoli a mus t fee dnorma l (o r higher ) level s o f as hdurin g th e dioxin/fura nan d mercur y performanc e tests . 12 . Durin g th e CP T o neac hincinerator , Veoli a mus t conduc t th e PM , SVM , an d LV

M performanc e test s whe nth e P M contro l devic e undergoe s it s norma l (o r mor e frequent ) cleanin g cycle . Fo r Incinerato r 4 , Veoli a mus t als o conduc t th e dioxin/fura nan d mercur y performanc e test s whil e th e P M contro l devic e undergoe s a norma l (o r mor e frequent ) cleanin g cycle . 8

### 13 . Becaus e Veoli a mus t establis hlimit s fo r th e applicabl e operatin g parameter s specifie di n§ 63.120 9 base do n operation s durin g th e CPT , Veoli a ma y conduc t testin g unde r tw o o r mor e operatin g mode s t o provid e Operatin g flexibility . 14 . N o late r tha n3 0 day s afte r EP A approve s th e CP T an d continuou s monitorin g system-performanc e evaluatio ntes t (CM S PET ) plans , Veoli a mus t commence.th e CP T o neac h incinerator . Veoli a mus t complet e th e CP T o neac h incinerato r withi n3 0 day s o f commencement . 15 . Afte r EP A

approve s th e CP T an dCM S PE T plans , Veoli a mus t mak e the m

availabl e t o th e public, - an dissu e a notic e advisin g th e publi c wher e th e tes t plan s ar e availabl e fo r review . 16 . No late r tha n6 0 day s afte r completio no f th e CPTs , Veoli a mus t submi t t o EP A an dIllinoi s EP A a Notificatio no f Complianc e (NOC) , a s describe di n4 0 C.F.R . § § 63w7(g) , 63.9(h) , an d63.1210(d) , fo r eac hincinerato r documentin g complianc e wit hth e emissio nstandard s an dCM S requirements , an didentifyin g OPL s unde r 4 0 C.F.R . § 63.1209 . 17 . Veoli a mus t documen t an dinclud e wit hth e NO C th e result s o f an y othe r performanc e tes t runs , conducte do r attempted , befor e o r afte r th e CPT . 18 . N o late r tha n6 0 day s afte r completio no f th e CPTs , Veoli a mus t submi t a revise dPar t 7 1 permi t applicatio nt o reflect - th e OPL s determine ddurin g th e CPTs . 19 . Thes e CPT s woul dserv e a s th e CP T require dbetwee n Octobe r 14 , 2008 , th e complianc e dat e fo r th e standard s se t fort hi n4 0 C.F.R . § 63.1219(a ) an d(c. ) , an dOctobe r 14 , 2009 , th e dat e b y whic hVeoli a i s otherwis e require dt o conduc t a CP T o neac hincinerator .

9



## VE S 00245 8

### CERTIFICAT E O F MAILING

I , Lorett a Shaffer , certif y tha t I sen t a Reques t t o Provid e Informatio nPursuan t t o th e Clea nAi r Ac t b y Certifie dMail , Retur nReceip t Requested , to : Dougla s Harris , Genera l Manage r Veoli a E S Technica l Solutions , LL C 7 Mobil e Avenu e Sauget , Illinoi s 6220 1 I als o certif y

tha t I sen t a cop y o f th e Reques t t o Provid e Informatio nPursuan t t o th e Clea nAi r Ac t b y Firs t Clas s Mai l to :
Ra y Pilapil , Manage r Complianc e an dEnforcemen t Sectio nBurea uo f Ai r Illinoi s Environmenta l Protectio nAgenc y 102 1 Nort hGran dAvenu e Eas t Springfield , Illinoi s 6270 2 An d Michae l Reed , Uni t Manage r Clea nAi r Ac t Permi t Progra m Burea uo f Ai r Illinoi s Environmenta l Protectio nAgenc y 102 1 Nort hGran dAvenu e Eas t Springfield / Illinoi s 6270 2

o nth e <sy7*}

da y o f



### Certifie dMai l Receip t Number : 7/3fl / f\&6(j> Oltl 7cZJ&

### standar dbcc's : Officia l Pil e Cop y w/enclosure(s ) Sectio nReadin g Fil e w/ o enclosure(s ) Branc hReadin g Fil e w / o enclosure(s ) othe r bee's : J . Woolums , C-14 J Creatio nDate : Februar y 19 , 200 8 Filename : C : \EPAWORK\WasteCombustion\hazwaste\Sources. \ Veolia\114Letter.do c Legend : ARD:AECAB:AECAS(MN/OH) :C. hal l



## VE S 00246 0

# E

VE S 00246 1Dou g Harris/OES/ONY XT o Newton.Cheryl@epa.go v 03/21/200

8 02:2 3 P M c c Blakley.Pamela@epa.gov , Damico.Genevievfe@epa.gov, Woolums.Jane@epa.gov , Hall.Chartes@epa:gov , RamaIy.Todd@epa.gov, Blough.James@epa.gov , Grei g bc c Subjec t CP TSchedul e fo rIncinerator s 2, 3 an d 4 A s w e discusse d durin g ou rMarc h 1 3 meeting , we ar e forwardin g th e testin g schedul e fo r Incinerators 2 , 3 an d 4 . You'l l fin d attachmen t 1 bein g th e integrate d schedul e fo ral l thre e incinerators . Attachment s 2 , 3 an d 4 ar e th e individua l schedule s fo r Incinerator s 2, 4 an d 3 , respectively . Pleas e d o not hesitate t o cal l wit h an y question s o rcomments .
CP TIntegrate

d Schedul e fo r2,3,4_March , 200 8 CP TSchedul e for#2_March , 2008. d 

# m @
CP TSchedul e for#4_March , 2008. d CP TSchedul e fo r#3_March , 2008, d



## VE S 00246 2

## Integrate d Comprehensiv

e Performanc

e Testin g (CPT) Schedul

e forVeoli aIncinerator

s #2 , #3 , an d # 4

Tas k Develo p CP TPla n fo rUni t #2. Submit Uni t #

2 CP TPla n t

o Agency . Agenc y approve

s Uni t # 2 CP TPlan. 2 Begi n proces

s t o hav e the Uni t #

2 CP TPla n mad

e availabl e t

o th e publi c fo ra

t leas t 6 0 day s and issue publi c notic

e t o facility/publi c mailin g lis t pe r 4 0 CF R §63.1207(e)(2) . Uni t #2 CP T planning , scheduling , and logistics activitie s commence

d b y ENS R and Veolia . Anticipate d Duratio n Dat e T o B e Completed 1 6 0 Day s May 15,2008

May 15,2008 1 5 Day s Ma y 30,200 8

May 30,200 8

Submit CP TPla n fo rUni t #4 . Agenc y approve

s Uni t # 4 CP TPlan. 31 4 Day s Begi n proces

s t o hav e th e Uni t # 4 CP TPla n mad

e availabl e t

o th e publi c fo ra

t leas t 6 0 day s and issue publi c notic

e to facility/publi c mailin g lis t pe r4 0 CF R §63.1207(e)(2) . Uni t # 4 CP T planning , scheduling , and logistics activitie s commence

d b y ENS R and Veolia . Uni t # 2 CP TPla n availabl e t

o publi c fo ra

t leas t 6 0 6 4 Day s day s and issu

e publi c notic

e t o facility/publi c mailin g lis

t per 4 0 CF R §63.1207(eX2) . Commenc

e Uni t # 2 testing. 4 Complet e Uni t # 2 testing . 1 5 Day s Submit CP TPla n fo rUni t #3. Uni t # 4 CP TPla n availabl e t

o publi c fo ra

t leas t 6 0 6 3 Day s day s and issue publi c notic e t o facility/publi c mailin g lis

t pe r4 0 CF R §63.1207(eX2). 5 Agenc y approve

s Uni t # 3 CP TPlan. 61 5 Day s Begi n proces

s t o hav e the Uni t #

3 CP TPla n mad

e availabl e t

o th e publi c fo ra

t leas t 6 0 day s and issue publi c notic

e t o facility/publi c mailin g lis t per40CFR§63.I207(e)(2) . Unit#3CP T planning , scheduling , and logistics activitie s commence

d b y ENS R an d Veolia . Jul y 1,200 8 Jul y 15,2008 Jul y 15,2008

Augus t 1,200 8
Augus t 1,200 8 Augus t 15,2008 September15,200

8 September15,2008
September30,2008 Septembe

r 30,200 8Tas k Duratio n Anticipate d Date T o B e Complete d 1
Uni t # 2 CP TRepor

t submitte

d t o Agency. 7 Notificatio n ofComplianc e (NOC ) fo rUni t #

2 submitte d t o Agency. 7 Findin g o fComplianc

e fro m Agenc

y fo rUni t #2. 8 Commenc

e Uni t # 4 testing. 9 Uni t # 3 CP TPla n availabl e t

o publi c fo ra

t leas t 60 day s and issue publi c notic e t o facility/publi c mailin g lis

t pe r 40 CF R §63.1207(eX2). 1 0 Complet e Uni t # 4 testing . Uni t # 4 CP TRepor

t submitte

d t o Agency. 1 1 NO C fo rUni t #

4 submitte

d t o Agency . " Findin g o fComplianc

e from Agenc

y fo rUni t #4. 1 2 Commenc

e Uni t # 3 testing. 1 3 Complet e Uni t # 3 testing . Uni t #3 CP TRepor

t submitte

d t o Agency. 1 4 NO C fo rUni t #

3 submitte

d t o Agency. 1 4 Findin g o fComplianc

e from Agenc

y fo rUni t #3. 60 Day s Octobe r14,2008 9 0 Day s Novembe r13,2008
3 0 Day s Novembe r13,2008

December1,200

8 6 3 Day s December1,200 8

1 5 Day s December15 , 200 8 6 0 Day s Februar y 13,2009 9 0 Day s Marc h 13,2009 31 Day s Marc h 16,2009

Apri l 1 , 200

9 1 5 Day s Apri l 15,2009 6 1 Day s Jun e 15,2009 9 0 Day s Jul y 14,2009 3 0 Day s Augus t 14,2009

1 Opportunitie

s ma y exis t i n thi s schedule tha

t coul d result i n task

s bein g complete

d earlie r lha n th

e anticipate

d dat e o fcompletion . Conversely , throughou t this CP Tschedule tha t Veoli a i s proposing , anticipate

d completio n date

s ar e base d o n previou s actions bein g complete d o n th e give n date , j f thes

e previou s actions ar

e no t finishe d b y the liste

d du e date , i t ma

y b e necessar

y t o extend subsequen

t completio n dates .

2I f approva l o fth

e Uni t WI

CP TPla n exceeds 1 5 days , ttie May 30,2008 completio n date , and subsequen t tas k completio n dates, wil l b e revise d t o reflec t this extension ofth e schedule .

3I f approva l o fth

e Uni t # 4 CP TPla n exceeds 1 4 days , th e Jul y 15,2008 completio n date, an d subsequen

t tas k completio n dates , ma

y b e revise d t o reflec t this extension ofth e schedule . Duet o th e earl y submitta l o fthi s plan , a dela y i n Agenc

y approva l ma

y no t affec t th e schedule .

4I f a dela

y i n th e commencemen

t ofth e Uni t #

2 CP Toccur

s tha t i s beyon d th

e contro l o fVeolia , th

e Augus t 1,200 8 dat e fo rstartin g thi s testing , and subsequen t task completio n dates , wil l b e revise d t o reflec t thi s extension o fth

e schedule .5Thi s proces s wil l b e repeate d i f change

s i n th e approve

d CP TPla n fo rUni t #

4 ar e made . I f thi s proces

s i s repeated , subsequen

t tas k completio n date

s ma y be revise

d t o reflec t an extensio n o fth

e schedule .

6I f approva l ofth e Uni t # 3 CP TPla n exceed

s 1 5 days , th

e Septembe

r 30,2008 completio n date , an d subsequen

t tas k completio n dates , ma

y b e revise d t o reflec t thi s extensio n ofth e schedule . Du e t o th e early submitta l o fthi s plan , a dela y i n Agenc

y approva l ma

y no t affec t the schedule .

7I f Uni t #

2 tes t result s ar e no t obtaine d i n a timel y manne

r o rar e flawed i n som

e wa y tha t woul d dela

y th e submitta l o fme CP Trepor t and the NOC , th

e Octobe r14,2008 and th e Novembe r 13,2008 completio n dates , and subsequen

t tas k completio n dates, wil l b e revise d t o reflec t thi s extensio n o fthe schedule .

8I f the Findin g o fComplianc e fo r Uni t #

2 exceed s 3 0 days , th

e November 13,2008 completio n date , an d subsequen

t tas k completio n dates , wil l b e revise d t o reflec t thi s extension o fthe schedule .

9I f a dela

y i n th e commencemen

t ofth e Uni t #

4 CP Toccur

s tha t i s beyon d fhe contro l o fVeoli a (e.g. , th e Findin g o fComplianc e fo rUni t #

2 ha s no t been received) , th

e Decembe r 1,2008 dat e fo r startin g thi s testing , and subsequen t task completio n dates , wil l b e revise d t o reflec t thi s extensio n ofth e schedule .

1 0Thi s proces

s wil l b e repeate d i f change

s i n th e approve

d CP TPla n fo r Uni t #

3 ar e made. I f thi s proces

s

- i s repeated , subsequen t tas k completio n date

s ma y b e revise d t o reflec

t an extensio n o fthe schedule .

1 1 I f Uni t #

4 tes t result s ar e no t obtaine d i n a timel y manne

r o rar e flawed i n som

e wa y tha t woul d dela

y fhe submitta l ofth e CP Trepor t an d the NOC , th

e Februar

y 13,2009 and th

e Marc h 13,2009 completio n dates , an d subsequen

t tas k completio n dates, wil l b e revised t

o reflec t thi s extensio n o fth

e schedule .

1 2I f the Findin g o fComplianc e fo rUni t #

4 exceed s 31 days , th

e Marc h 16,2009 completio n date , and subsequen

t tas k completio n dates , wil l b e revise d to reflec

t thi s extension ofth e schedule .

1 3I f a dela

y i n th e commencemen

t o fth e Uni t # 3 CP Toccur

s tha t i s beyon d th

e contro l o fVeoli a (e.g. , the Findin g o fComplianc e fo rUni t #

4 ha s no t been received) , th

e Apri l 1,2009 dat

e fo r startin g thi s testing , an d subsequen t tas k completio n dates , wil l b e revise d t o reflec t thi s extensio n ofth

e schedule .

1 4I f Uni t #

3 tes t result s ar e no t obtaine d i n a timely manne

r or ar e flawe d i n som e wa y tha t woul d dela

y the submitta l ofth e CP Trepor t an d th e NOC , th

e Jun e 15,2009 and July 14,2009 completio n dates, an d subsequen

t task completio n date , wil l b e revise d t o reflec t thi s extension o fth

e schedule .

## VE S 00246 6

## Comprehensiv e Performanc

e Testin g (CPT) Schedul

e fo rVeoli aIncinerato

r#2

Tas k Duratio n Develo p CP TPla n fo rUni t #2 . 6 0 Day s Submit Uni t #

2 CP TPla n t

o Agency . Agenc y approve

s Uni t # 2 CP TPlan. 21 5 Days Begi n proces

s t o hav e the Uni t #

2 CP TPla n mad

e availabl e t

o th e publi c fo ra

t leas t 6 0 day s an d issu e publi c notic

e to facility/publi c mailin g lis t pe r 4 0 CF R §63.1207(e)(2) - Uni t # 2 CP T planning , scheduling , an d logistics activitie s commence

d b y ENS R and Veolia . Uni t # 2 CP TPla n availabl e t

o publi c fo ra

t leas t 6 0 6 4 Day s day s and issue publi c notic e t o facility/publi c mailin g list pe r4

0 CF R §63.1207(eX2) . Commenc

e Uni t # 2 testing. 4 Complet e Uni t # 2 testing . ' 1 5 Day s Uni t #2 CP TRepor

t submitte

d t o Agency. 760 Days Notificatio n o fComplianc e (NOC ) fo rUni t #

2 9

0 Days submitte d t o Agency. 7 Anticipate d Date T o B e Complete d 1 Ma y 15,2008 Ma y 15,2008 May 30,200 8 May 30,200 8

Augus t 1,200 8
Augus t 1,200 8 Augus t 15,2008 Octobe r14,2008 Novembe r13,2008
Findin g ofComplianc

e fro m Agenc

y fo rUni t #2. 830 Day s Novembe r13,2008

1 Opportunitie

s ma y exis t i n thi s schedule tha

t coul d result i n task

s bein g complete

d earlie r than th

e anticipate d dat e o fcompletion . Conversely , throughou t thi s CP Tschedule tha t Veoli a i s proposing , anticipate d completio n date

s ar e base d o n previou s action s bein g complete d o n the give n date. I f thes e previou s actions ar

e no t finished b

y th e liste d du e date , i t ma

y b e necessar

y t o exten d subsequen

t completio n dates.

2I f approva l o fth

e Uni t # 2 CP TPla n exceed

s 1 5 days , th

e May 30,200 8 completio n date, and subsequen t task completio n dates , wil l b e revise d t o reflec t thi s extensio n ofth e schedule .

4I f a dela

y i n th e commencemen

t o fth e Uni t # 2 CP Toccur

s tha t i s beyon d th

e contro l o fVeolia , th

e Augus t 1,200 8 dat e fo rstartin g thi s testing , and subsequen t task completio n dates , wil l b e revise d t o reflec t thi s extensio n ofth e schedule .7I f Uni t # 2 tes t result s ar e no t obtaine d i n a timely manne

ro rar e flawed i n som

e wa y tha t woul d dela

y th e submitta l ofth e CP Trepor t an d th e NOC , th

e Octobe r14,2008 and th e Novembe r13,2008 completio n dates , and subsequen

t task completio n dates, wil l b e revised t

o reflec t thi s extension ofth e schedule .

8I f the Findin g o fComplianc e fo rUni t #

2 exceed s 3 0 days , the Novembe r13,2008 completio n date, and subsequen

t tas k completio n dates , wil l b e revise d t o reflect thi s extension o fthe schedule .

## Comprehensiv e Performanc

e Testin g fCPT) Schedul

e forVeoli aIncinerato

r# 2

Tas k Duratio n Develo p CP TPla n fo r Uni t #2. 6 0 Day s Submit Uni t #

2 CP TPla n t

o Agency . Agenc y approve

s Uni t # 2 CP TPlan. 21 5 Day s Begi n proces

s t o hav e th e Uni t #2

CP TPla n mad

e availabl e t

o th e publi c fo ra

t leas t 60 day s and issue publi c notic

e t o facility/publi c mailin g lis t pe r4 0 CF R §63.1207(e)(2) . Uni t # 2 CP T planning , scheduling , and logistics activitie s commence

d by ENS R an d Veolia . Uni t # 2 CP TPla n availabl e t

o publi c fo ra

t leas t 6 0 6 4 Day s day s and issue publi c notic e t o facility/publi c mailin g lis

t pe r4 0 CF R §63.1207(e)(2) . Commenc

e Uni t #2

testing. 4 Complet e Uni t #2

testing . 1 5 Day s Uni t # 2 CP TRepor

t submitte

d t o Agency. 76 0 Day s Notificatio n o fComplianc e (NOC ) fo rUni t #

2 9

0 Day s submitte d t o Agency. 7 Anticipate d Dat e T o B e Complete d 1 May 15,2008 May 15,2008 Ma y 30,200 8 Ma y 30,200 8

Augus t 1,200 8
Augus t 1,200 8 Augus t 15,2008 Octobe r14,2008 Novembe r13,2008
Findin g o fComplianc

e from Agenc

y fo rUni t #2. 8 3

0 Day s Novembe r13,2008

1 Opportunitie

s ma y exis t i n thi s schedule tha

t coul d result i n task

s bein g complete

d earlie r than th

e anticipate

d dat e o fcompletion . Conversely j throughou

t thi s CP Tschedule tha t Veoli a i s proposing , anticipate d completio n date

s ar e base d on previous action s bein g complete d on the give n date . I f thes e previou s actions ar

e no t finishe d b y the liste

d du e date , i t ma

y b e necessar

y t o exten d subsequen

t completio n dates .

2I f approva l o fth

e Uni t #2

CP TPla n exceeds 1 5 days , th e May 30,2008 completio n date , and subsequen t task completio n dates, wil l b e revised t

o reflec t thi s extension o fth

e schedule .

4I f a dela

y i n th e commencemen

t ofth e Uni t #

2 CP Toccur

s tha t i s beyon d th

e contro l o fVeolia , th

e Augus t 1 , 200 8 dat e fo rstartin g thi s testing , an d subsequen

t task completio n dates , wil l b e revised t o reflec t this extension ofth e schedule .ff Uni t # 2 tes t result s ar e no t obtaine d i n a timel y manne

r o r ar e flawed i n som

e wa y tha t woul d dela

y th e submitta l ofth e CP Trepor t an d the NOC , the October14,2008 and the Novembe r 13,2008 completio n dates , an d subsequen

t task completio n dates, wil l b e revise d t o reflec t thi s extensio n o fthe schedule .

! I f fhe Findin g o fComplianc e fo r Uni t #

2 exceeds 30 days , th

e Novembe r 13,2008 completio n date, an d subsequen

t tas k completio n dates , wil l b e revised t

o reflec t thi s extensio n o fth

e schedule .

### Comprehensiv e Performanc

e Testin g (CPT ) Schedul e fo r Veoli a Incinerato r # 4

Tas k Duratio n Submi t CP TPla n fo rUni t #4

. Agenc y approve

s Uni t # 4 CP TPlan. 31 4 Days Begi n proces

s t o hav e the Uni t #

4 CP TPla n mad

e availabl e t

o th e publi c fo ra

t leas t 60 day s an d issue publi c notic

e to facility/publi c mailin g lis t pe r40 CF R §63.1207(e)(2) . Uni t # 4 CP T planning , scheduling , and logistics activitie s conunence

d b y ENS R and Veolia . Uni t # 4 CP TPla n availabl e t

o publi c fo ra

t leas t 60 6

3 Days day s and issue publi c notic e t o facility/publi c mailin g lis

t pe r 4 0 CF R §63.1207(eX2). 5 Commenc

e Uni t # 4 testing. 9 Complet e Uni t # 4 testing . 1 5 Days Uni t # 4 CP TRepor

t submitte

d t o Agency. " 6 0 Day s NO C fo rUni t #

4 submitte

d t o Agency. " 9 0 Day s Findin g o fComplianc

e from Agenc

y fo rUni t #4. 1 2 3

1 Day s Anticipate d

Date T o B e Complete d ' Jul y 1,200

8 Jul y 15,2008 July 15,2008

Septembe

r15,2008

December1,200

8 December 15,200

8 Februar y 13 , 200

9 Marc h 13,2009 Marc h 16,2009

1 Opportunitie

s ma y exis t i n thi s schedule tha

t coul d result i n task

s bein g complete

d earlie rman th

e anticipate

d dat e o fcompletion . Conversely , throughou t thi s CP Tschedul e tha t Veoli a i s proposing , anticipate

d completio n date

s ar e base d on previou s action s bein g complete d on the give n date . I f thes e previou s actions ar

e no t finished b

y th e listed du

e date , it ma

y b e necessar

y t o exten d subsequen

t completio n dates.

3I f approva l o fth

e Uni t # 4 CP TPla n exceed

s 1 4 days , th

e Jul y 15,2008 completio n date , and subsequen

t task completio n dates , ma

y b e revised to reflec

t thi s extensio n o fthe schedule . Du e t o th e earl y submittal o fthi s plan , a dela y i n Agenc

y approva l ma

y no t affec t the schedule .

5Thi s proces

s wil l b e repeate d i fchange

s i n th e approve

d CP TPla n fo rUni t #

4 ar e made . I f thi s proces

s i s repeated , subsequen

t tas k completio n date

s ma y b e revised t

o reflec t a n extensio n o fth

e schedule.

9I f a dela

y i n th e commencemen

t o fthe Uni t #

4 CP Toccur

s tha t is beyon d th e contro l o fVeoli a (e.g. , th e Findin g o fComplianc e fo rUni t #

2 ha s no t been received) , th

e Decembe r1,200

8 dat e fo r startin g thi s testing , and subsequen t tas k completio n dates , wil l b e revised to reflec

t thi s extensio n o fthe schedule .1 1 

### I f Uni t# 4 tes tresult s ar e no tobtaine d i n atimel y manne ro rar e flawe d i n som e wa y tha twoul d dela y th e submitta

l ofth e CP T repor tan d th e NOC , th

e Februar y 13,200 9 an d th e Marc h 13,200 9 completio

n dates , an d subsequen

ttas kcompletio

n dates , wil l b e revise d t o reflec tthi s extensio n o f th e schedule

.

1 2

### I f th e Findin g o f Complianc

e fo rUni t# 4 exceed s 3 1 days , th e Marc h 16,200 9 completio

n date , an d subsequen ttas kcompletio

n dates , wil l b e revise d t o reflectthi

s extensio n o f th e schedule

.

# F

VE S 00247 3