VES 003135.pdf 
VEOLIA ES TECHNICAL SOLUTIONS, L.L.C. RESPONSES TO THE UNITED STATES 

ENVIRONMENTAL PROTECI'ION AGENCY'S REQUl!ST TO PROVIDE 

INFORMATION PURSUANT TO THE CLEAN AIRACI' DATED JANUARY 29, 2009 

Exhibit J Continued ( 1 ) 

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Spike Concentration Calculations: 

[Chloride concentration in hexachloroethane: ChCCCI3] . 

. Percent chlorine in compound - 89.85% 

Pulity- 99.93% 

(0.9993) x (89.85) = 89.8% Chlorine 

[Lead COn<:enllation in lead nitiate: Pb(NO,h] 

Percent lead in compound - 62.,56% 

Purity- 99.2% 

(0:992) X (62.56) = 62.1% Lead 

. [an'omium cOncentration in chromic acid: Cr03 (Batch CH0 E00~3)] 

Percent chromium in compound- 52.00"/o 

Chromic acid content- 458.0 gil 

Specific gravity- 1.310 glml 

(458.0 g/1) X (ml/1.310 g) X (0.001 1/inl) = 34.96% Cr03 

(0.3496) x (52.00) = 18.18% Chromium 

· · [Mercury concentration in mercuric nillate] 

Determined by analysis of test run samples. 

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MmTALSANDCBLO~SPllffiSPROTOCOL 

INCINERATOR TESTING 

VEOUAES 

SAUGET,IL 

Iable of Contents 

Quality Control 

Spike Preparation Procedures 

Spike Feeding Procedures 

Attachments . 

• Specification Shec!s 

• Laboratory Analysis 

• Calibration Records 

• Feed Calculations· 

• Recoxdkeeping Documents 

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VES 003171 
• , Qaality Control 

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Qvenicals for Spiks 

The following_ spikes have been selected for incinerator testing: 

Mercwy (II) rutri.to hydrate (bigb volatility metal) 

Lead nitrate (medium volalility metal) 

Chromic ~d (low volatility me131)' 

Hexacbloroethane (chlorine) 

These chemicals were purchased from suppliers and specificaliqn sheets with any applicable 

.lot ex batch numbers provided for each item. Tbese spcc:ification sheeCs aro included in tho 

attaclunents of this report. 

The Mercury (IJ) ni.trate ~ will be put into solution with dO-ionized water and sligblly 

acidified with a small amount of concentrated nitric acid 1o bdp pcevent anY precipil2ti.on of 

solids.~ amounts of this solution will be (ed during incinerator testing within 

plastic vials placed with tho solid feed charges. Because the targeted mercwy feed rate is · 

sigllificantly greater 'for the testing of No.4 Incineralor, two differeni concentrations of 

Mercury nitrate solution batches will be prepared for use as spikes in the incinerator feeds. 

Tho Lead nitrate will be put inlo re-olosable plastic baS$ in pre-determined'amounts and fed · 

to the incinerators during testing by placing !hem with the solid feed charges. · · 

The Chromic acid bas a conce.otcation of 35% and will be fed to the incinerators at a predetermined rate via metering pumps on an electronic' scale device. 

The Hexachloroedlane will be put into ro-closable plastic bags in pre-determined amoUDls 

and fed 1o thO incinerators during testing by placmg them with the solid feed ~ges. 

Because the targeted chlorine feod rate is greater for the testing of No. 4lnciMzlilor, a greater 

quantity of Hexachloroethane wiD be placed in the spike bags 1o be used when testing this . 

incinernlor. 

Certification of Spike Measuring EQuioment 

The concentration of the prepared Mercwy nitrate solution will be determined by an 

independent laboratory using an ICP atomic emission spectrometer. The analytical procedure 

is Method 7470A for cold vapor atomic absorption .The results of this analysis are i11cluded 

in the attachment of this report. 

The weighing devices used for measuring out the Lead nitrate spike bags and 

Hexachloroethane spike bags are electronic scales with digital readout and oontrol panels. 

They have been calt'bratod prior to use by a professional scale services oompany. Eacb scale 

panel bears a sticker indi~ the ca!J'bration dale and a report on the calibmtiod is included 

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in the attaclm!ems of this' report. In addition, tho procedures fix preparing these spike ba~ 

require the _scales 1o be zeroed on a: consistent basis during use. 

The device used for feeding G:bromic acid combines a holding tank, metering pumps and an . 

electronic scale with a digital ,readout and i:putrol panel It has been calibrated prior lo use by 

a professional seale services company. The scale paoel bears a sticker indicating the 

calibrntion date and a report on tlio calibration is included in the attachments .of this report. 

Spike PreparaUoo. Procedures 

The procedures written below 1te the steps taken by personnel when measuring out and 

clocumentiog the spilces used for incinerator testing. 

Mercury NiJrate Spike Solution J>nomptjnn Procedure 

1. Obtain M=ry ni1l:ale solution and plastic vials. 

2. Rinse. the repipet dispeoser aod transfer container used for mtastuing Mercury 

nitrate solution fint with do-ionized water, then twice with a portion of the 

solutioa. 

3. Transfer desired amount of the selected Mercnry nilrate solution from the storage 

vessel lo the transfer container. Tbe concentration of the solution is dependent on 

which incinerator the spike vials are being prepared for. 

No.2 and No. 3 lqcinerator- 710 ppm solution 

No. 4 Incinerator- 1.05 %solution 1, 1.04% solution 2, 1.1 r. solution 3 

4. Position equipment within a laboratory hood. 

S. Number eadl vial needed with a permanent marlc.er starting at number "I". 

6. Using the pip~pump, transfa' the specified amount ofMereury nib:ate solution 

inlo the vial. The amount of solution. transfern:d to the vial is depeodeo.t on which 

incinerator the spike vials are being prepared for. · 

No.2 and No. 31Dcinerator- 14 ml per vial 

No. 41Dcinerator- 23 ml pa: vial solutions I and 2, 22 m1 per v ial solution 3 

7. Document the vial nwnber and volume on the spike vial sheet. 

8. Securely seal the vial and carefully place it i.olo a plastic sloragc buckel 

9. Repeat steps for number of spike vials needed. 

VES 003173 
.. 

J 

) 

10. . ~ oomplek, closo the ~ $fotlge buckets and place in designated :area. All 

peuoimd involved in prcpariug the vials iJiust have their lWl!CS written On the 

spike vial sheet. 

Lead Ni!r:llte Sllike l{ag Preparation e<lure 

I. 

2: 

3. 

' 

4. 

s. 

6. 

7. 

Obtain Lead nitratc ;,;w m.aterial and ro-cloSab1e plastic bags. 

Position elcolronic scales u;_ the selected area and ~ the scales before. u,se. 

"Put on required PPE before exposure to the Lead.nitrate. l>ersoDDel directly handling 

Lead nitrate need full-face resp.irator with OV/AG cartridges, Tyvdi: suit, and nitn1e 

gloves tap~ at wrist. · · 

Numl>e£ each plastic bag needed with a pennanmt Dl8lk.er starting at "1". 

Open a bag of raw material and use· seoop or equivalent device to place between 2.5 

. and 2.7 poUDds ofl.;ead nitrate into the numbered plastic bag. 

. . Document 'the bag number and weight on the spike bag sbecL 

Secure1y seal !he bag and carefully place it into a p lastic storage drw:n: 

. 8. Repeat steps for number of spike bags needed. Re-zero tire scale at leaSt once every 100 bags. . . . . 

9. When complete, close and seal the plastic storage drums and place in the 

designated area. All personnel involved in preparing the bags must have their 

name$ writ1m on the spike bag sheeL · 

Hexachloroe!h.ane Spike BAA Preparation Procedure 

l . Obtain Hexachloroetbane raw material and re-cl~le plastic bags. 

2. Position electronic scales in the selected area and .zero the scales before use. 

3. Put on ii:quirod. PPB before exposure to the Hexachloroethane. Personnel directly · 

bandli,ng HexachlOroethane need full-face respirator with OV/AG cartridges, Tyvek 

suit, and nitrile gloves tap~ nt wrisL 

4. Number each plastic bag needed with a peananent marke£ starting at "1" . 

. S. Open a bag ofraw lll8lerial and use scoop or equivalent deviee to place specified 

amount ofHex.achloroeibane into the numbered plastic bag. The amount of maiCriat 

placed in the bag is depcodent on which incinerator Ike bags are being prepared ·cor and 

the Chlorine contn"bution. of the was1e feeds on the respective iJ)eiuerator. 

VES 003174 
) 

.r 

6. 

7. 

No. 2 and No. 3 lncincntor- 5. 7-5.9 pounds or 6.3.- 6.5 pounds per bag 

No.4 Incinerator - 6.8 - 7.0 pounds per bag 

Document the bag nwnbe£ and weight on tbe spiXe bag sbcet 

Secucely seal the bag and carefully place it into a plastic storage drum. 

8. Repeat slqlS for number of spike bags needed. Re-zero the scale at least once every I 00 

bag$. . 

9. Wbcn complete, close and seal the plastic storage drums and place in the 

designated area. All peuonnel in~Jved in prc:parin& the bags must have tbeir 

names writ~QJ. on the spike bag sheet. 

Spik.e Feedinc I'TGceda.res 

The procedures written below are the steps taken by peuonnel when feeding spikes used for 

inci.nentor testing. 

Feeding Proced\Ue for Mercury. Lead and Chlorine 'Spikes 

l. Position the Mercury nitrate spike vials, Lead nillale spike bags and Hexachloroethane 

spike bags near the loading point oo the solid charge feed conveyor. 

2. Place one spike container of each chemical into each charge. Because the mercury and 

cblorine feed rates a~e depeodeot oo the incinerator, the correct spike vial and correct 

Hexachloroethane spike bag must be fed to the respective incinerator. 

No.2 and No. 3 ln<:inentcm - 14 ml vial, 5.8 pounds or 6A pounds bag 

No. 4lncinerator-22 ml or 23 ml vial, 6.9 p(>unds bag 

3. Document the waste charge number, vial number 8.o.d bag numbers on the charge 

sheet. All personnel involved in feeding tbc charges must have tbeir names 

written on the charge sheet. 

F~.ffljng Procedures for Cbromjum Spjkc 

I. Place the feeding device and selected drums of Cbromic acid near the injection point on 

the incinerator. 

2. Activate the power panel for the feeding device and zero the electronic scales. 

3. Put on tbe Personnel Protective Equipment recommended by the MSDS for Cbromic 

Acid and lnln.sfer the desired amowit of material to the holding tank on the feeding 

. device. 

VES 003175 
4. 

5. 

). 

·, 

i 

' At~ desigoated.lime, start them~ pumps and select pump sett;Dgs that deliver the targeted feed rate . . 

Document scale readings and lime at selected intervals on the Chromic acid feed 

chart In verify that the desired feed rate is being achieved during the incinerator 

testing period. All personnel involved in feeding the Chromic acid must have their 

names written on the feed chart 

/ 

VES 003176 
·-"---o-i--''- - -••ou ·-•-•• .. ''''''''" •·•• • 

8512t't2008 11:21 · · ·31438983n 

l '.• •• 

. . . . iJIZ1{%K1 u:u ri:i. l i .. m tu• . ·. . .. 

. . 

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--

·. ·. · . . . . . .. . . 

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·. 

. . 

~ 

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i ; • ;j. 

: ~ .- t ••• 

. .. 

~ .• 

PAlE· 82/84 

VES 003177 
.. ll1 :tUIO<iK FUJX a;:W . . ' . " . ·.· . ··.·t . • ' . .. . ... . 

; . 

Rat. No. SG1326Bl?-Q8 . . . ·. 

··. . : · 

... 

. . . .. .... .• . ,:-. . . ' . ·. . . . ~ -·. .. ...... . ·.: ..... -~ .: .... : : .. · . 

. · .. .. ... ····. '· . :··· . 

. .. 

. . ; .. 

·. {c~~i .c~;.~~·!Ji,l.f~·. PRQDUC1' 

I'ORM 

COLOR 

900R 

: . HEXACliLOROETHANE . . . . . . . ·. . 

: .. :wHr:rE. C~vSTALUIE POWDER . ,: (l'Ri$:-f OVII)NGW,~ · : : 

. i Sr.JOW-Wii~E· > .. . . . . . 

. . ; : . . .. ~ . ' ~ ' ; 

. •• .. (<l PURITY·(%· BY GLC) .~ · .119.9a% . 

1sa oc 

0.016o/.: 

. . . 

~ M ·' EI,.llNG PQIHT 

f))· .MOISTURE (% WT .1 

141 ASH{% WT.) . .. 0.076% . · . . 

Ill ffi!IE CliLORINE 

(&f WA "feR SOLUBLE : . : . ·0.002%. CHt.ORlDE (% ~.ct) ' : . ·. . . 

. .. . . ' 

171 GRADING 

. •., 

·18 +150 Meilh.BSS · 

.. ·. : · . 

. - · :....... .. -.-· 

Post-U" Fax No$ : .. '7671 1"-., ;/??.inti:.:.. .. ·1/1 

Y.'J.e - S:· '· 

~ _ILc.c>l•<>.. ... '!'- Jl. 1;1J., P(u;,. <:. ..o . 

-· ........ • .... 27(-Dit~'t · -· .. 

..· 

•. -

. .. 

VES 003178 
............................ .., · PAGE 63/8-\ _ ... --· ---- -· ··--

,

1 Technical Information · ·. . . 

·51ieei No.: cHROMIC ACID Uquid (35%) 

Revtrion ~T-217 

lt.ADS 10 No.: 7566 j 7 

.. 

·,CHROMIC AClD '• . 

, liquid_ (35%) 

) . 

INTROOU,CTION 

CHROMIC ACID Uquicl .(35._41-is a hl!II>-Pwity productl'o'atl siJitad for use in ch~~m pta&n!J and-anocfiziniJ . 

appllcatlQns.lt ·can also be used in the ,_~of ~ate conversion compounds lor %inc and cadinlum, 

btjghtdlpsforcopper, brass, aluminum. arid magnesium, for producing certairitypes of pigments, as.anOlddant 

in organlo syndMJ$eS In lhe pharmac:eoticol indlls1ry, and as a catalyst in oe<1aln pelfofeurn ref1nin9 pmcos~. 

SPECIFICA TIOHS 

Chromic Add crO, -

Sulfate (SO.) -

Chto<ide (CI) • 

tnsoluble Materials -

Sodium (Na) -

Scec!tk;atio!l 

57.3 oz/gal (430 g/Q Min. 

~ .. 

: ... 

~ 

. 60 oz/gal (450 gfll 

0.07% 

0.002% 

0.002% 

0.023% . . 

Rmived Ti•t M1y. 21. 2008 5:21PM No. 2359 . 

.· 

,. 

VES 003179 
.. , 

) 

-' 

ra'! ATOIECH . ....... 

lii\RCROS CHBMICALS DIC 

4330 GBRAIDINB AVB 

SAIIIT LOOIS NJ ~3115 

Atotech 1JSA IDe. 

Quality COiltzol 

1 ?SO Ovexvie• <hive 

Rod< IU.U, SC 29731-~009 .. 

QC Lalf Telt (803) 811-3575 Pax• (S03) 817-3606 

C11RCMr Servi~• (80o) ?52·MU (1111 OO..toeen ODly) 

Ddt 

~: 

-.... TQi: 

-0... : 

-OI'dtrNo: 

Dt"-Y No: . 

o.a.-.Ho: 

Qoot.Onlot No: 

08/i?/2008 

2280oti-6oss-•-ooo ~ cnmctc ACm ·ICIIl 

ciloelionu 

Ot/O'i/2'010 

soo2ons2s 

51)06059~67 

020051042 . 

rhis io to certify· that tbe ~roduet ideotithd baa tsstl!<S Ulk1<lr' .;.,.,..,,_,tled 

labozatocy eooclitiODS and fOUJ:Id . to .eet our apeeific:atioua and quality aaoruR=e 

st~~ · · · · 

I~ Date: 08/07/2008 

Characteristio Looler Liait 

Appearance 

Color 

Specitic Gravity 20 deg c 1 . 285 

concent: Chrootic acid U9.3 

IIpper Limit 

1 . 315 

C71.5 

value 

clear liquid 

Red 

1-2~2 

. 639.9 

G{HL 

GIL . 

:· r&.is is a controlled co.rpu.ter p~intout valid Yit.Jlout a signature. 

Quality Control Laboratory 

Lal>oratocy Mauagar 

l1lf1S STATIMEHT PAIHTS OH A COA RlR A lilG<.AAA SH~Ptro<T~ 

. ' 

'· 

VES 003180 
) 

A TO TECH 

HARCROS CHBMICJILS DIC 

4330 GBRALDINB AVB 

SAXNT LOUIS MO 63115 

Atoteeh USA Inc. 

Quality Control 

1750 overview drive /)31./ 

Rock Bill, SC 29731-20GO 

.QC Lab Tel, (803 ) 817- 3575 - Fax, (803) 817-3606 

Customer Service< (80Q) 752 - 8•6• (US Oust~ only) 

o·a.te 

AAiele-No: 

r.cat.ial: . 

a.""': 

~nOaw: 

Atotoeh OtCiot No: 

Oetivefy No: 

Cusi.U.t.Ho: 

Ont.~det No: 

05/23/2008 

2200041- 0055-.4 - 0QO 

LXQDXD CHROMIC ACXD ( Cll) 

CH08C028<l2 

03/19/2010 

50020.60087 

5006093116 

020050339 

. 'Ibh is to cert.ity that the product identifi~ has been tested under controlled 

laboratory conditions' and found to meet o ur SI("'Cifications and quality· assuran~e 

standards. 

Inspection Date: 03/19/2008 

) Characteristic . Lower Lindt Upp&r Limit Value Unit 

Appear an.ce 

Color 

specific Gravity 20 deg c 

Content: Chromic acid 

1.285 1.315 

419.3 471.5 

· Clear liquid 

·Red 

1. 310 

460.0 

This is a control1ed computer pt-intout valid wlthout a signature . 

Quality Control Laboratory 

Laboratory Manager 

G/ML 

G/L 

VES 003181 
·. ., 

' 

ATO'FECH ' .At otoch USA InC. 

Qu&l.i ty contra 1 

~ 750 OvexvieV drive 

Rock Hill; sc 29731-2000 

QC Lab Tel: (803) 8 17 - 3 575 Fax: (803) 817- 3606 

CUotoaer service: (800) 752 - 84 64 (US CU.toaere Only) 

RARCR.OS CHSMICAJ.S INC 

4330 GSRAwiNB AVE 

·SAINT LOUXS NO 63115 

,_ ~-- ' '. ' 

it--"1 T£1:_:?\~1(1•1- ~(. ;:.:..:~?(;H;i - , . ·" _.•..:-. ··"-'fh~"''::">:...~ ~' ~ .t...,. . ' . 

O.tc 06/03/2008 

Attf : 22000U- 0055-4-000 

M•teriel:. LXQUXD CKROMXC ACXD 

IIATCH: 0108800643 

e.p;.aoton O.tc : 05/27/2010 

Atoted\ Orrde!' tlo: 50020600 87 Dol,..,. No: 5 006093728 

CI.4\..Nat.No: 

Cuot.O.S.W No: 0 20050339 

(CHI 

'n>J.e i..s to cexti.fy l:hat the p roduct i4eo tifted bas .been te,.te<i under COilt:rolle<l 

labor,.tory ConclitiollB 'and found to -ot our specifico.ti.ons alld quaUty aasux;mce 

at.nd.ards. 

lnspeetlon Dote: 05/ 27/20 08 ' 

)Characteristic 

. Lowar Lillit tlppor &.i.h: Val ue 

Appe..ro.nce Clear l:lqui4 

COlor Red 

Specific Gravity 20 deg c 1.285 1. 31.5 l. 31.0 

content: Chromic acid U9 .3 471.5 458. 0 

'l'hia is a controlled cocoputer printout v'alid without a signature. 

Q\'•lity control ~oratory 

Laboratory Mana r 

(THIS STAlOMENT PAINTS ON A COA FOR A REGVI.AR SHIPMENT! 

llnit 

G/ML 

G/L 

,, 

r. 

. f 

VES 003182 
..• · 

: .. , 

PDC Lab.orirt;,ries. 'lri.e. c·. 3278 ti Hlgh...qi?. f-1~ MO~:. . . . , . 

(314)432-0SSO • (800)3:J:l.FAS1<;!278l• FAX(314l4.32-4S'/7 : ·~ : . . '. . .. · . .. .. ·. " ·: 

. .. 

Veolla·Env~~tal SetVioes 

#7 M9bile Av~ · · 

, · Sai'!iet: lL. eZ!o1· 

Ant;' ::.w; Trey Formby 

.·. 

. . . .. ( 

p;amp1e No:. ta0180.17·1. 

~10: 8801MN Sile: 

•Coloct Oli\li · 0810flll8 ·oo:01 ·· 

·. i.oeaior: ·_( ... ____ _j 

£PA 24S.1 

Metc:.>Jry • 

. . 

: 

: Quatlller ,.,;.,.~· b&t~ 'AnalYst 

.. . . 

AQCBEQITATJONS. 

· . 

. . .... 

·:· .. : .WI>!; 

: 

~C~1!qn for V¥astewa~. ~ aod sOikt wastes FK!Ids oi T~ Uvougt) ll.EPAI...ab Ko. 1002'53.· . 0 o o 0 ' , 0 + 0 o ' H o o • .. 0 0 ' o ' 

.. . . . 

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. ·.·· 

VES 003183 
PDC Laboiatories. hie. ---.... 

. . - 3278 N. lllghwar fJ • Flodc ~ I(() 60033 ;.: I ~ 

-:-'J . ( ....__ <314) 432-0550 • CJI00)333-FAST Cl27ln ~ PIJ. (314). <l32-t9'l1 

......,..., 

fPA24S.1 . 

......... 

Saugol. u. 62201 

A!ln : Mr. Troy Formby 

r;::~ =~~:.· _· =;~:L- P"'*""Ier" sw-- S~P14660108R2.0 

) 1vhNc 

·-

Cadmll.m 

Dale ReceM!d : QM)5I08 17:00 

Report Dale : 08107108 CUslomer. : 205130 . 

P.O. Number :1'2008-2 

F:dlly : 

Calect Dale 081051111 00:01 

lOcator: 

- -·------,c'"'o~oo"" '"' · D;IW> ,....,.-o_S/0 ___ 5101 oo;oi ·• ·-···----"1 

$<!: ---- - ---- . --· l..ocollol': - . --- --· - - -; 

Quallfiet Resutt Anal}'$ ~ Dote Analyst 

08I06IOD 11 :00 JS 

... _ oeiD6/08 .~, ... W!'S < 0.2~, *lG/08 1$!$9 WI'S 

2.4 mgtkg _...,5:51 WPS 

u mQII<g 08IOI5IOa 1 S:5i WPS 

~ 0810Ml&1- WPS 

·-· <:JMliM)8 18;20 WPS 

~-,• .,No-:""o"aoa=eo=78-3=-=- ·-·-··- .... - _;:·· ·--- --------;COIIe<t ;-:,--,~,.c--,-:- 810 5108 =-oo~:=-,---- --; 

I CIIOnl tD: 2aszro TF- )-c-o t.vJ>j:_~·~:.. , :!.sTL~ ______ __ __:L:::oca=tor:::.:. : _ ____ . J 

~Cf' 

sW....o- s.m...-lion 

SW..,..150108 R2A ........ IJety1IO.m 

CodnOum 

C>wLood 

SW-U& 7470ARt..G 

-a.oy 

< 

tt.sult 

_•.s 0-2_ mo'I<U 

·-·-

..,_ 

···-

1,4 mgJl 

*-

Analyols D"'• Analyst 

~11:00 JS 

ClMl6lll1l ..... WPS 

oeiD6/08 ..... WPS 

D&tD6101!11 5:02 WI'S 

0&'0111011 t$:02 WPS 

0810S10St6~ WPS 

oOio6roe 16-'20 WPS 

,_ 1 ot2 -· 

' ' ' ••, • f, 'I • ., '• • ••• • • • •• <I& •' ". • " •• • l -. . .·.· .,.,.,_ ........ · ... . , • .... ,-, ... •<'"'•' • , .~·", V'! •" !:' /1, 

' f. 

VES 003184 
PDC Laboratories. Inc. .3218 N. l!!Qb...,Y67· -M063033 

· (314)~ (800)333-f.AST~· AX(314)432-4S1'7 · 

Saugat. IL 82201 

Attn : Mr. Trey Formbv 

~te Received :0Ml6108 09:00 

Rq>ott 0.. : 08/CJ7/08 

~# 205131) 

P.O. Number :Pzoo6-2 

. FaciliCy : 

-·· ···· ·· ···-··Qji~ OIIIOM1810:01 . f- No: 08!'118'1 1 .. , 

1 cr""'tiO : 08oeo&l -'-\1-h \ ~ Sile: STL · -·-- ·· ·..!:L:::oca=!Dr:..::.... ---~--__j Ponmetw Analyst 

EPAUS-t 

~ -, 

) 

' ' · . 

. ·. · 

·. 

-. 

·<i> - P3ge 1 of 1 

,"("'.·.· .. .. . ..................... \ ....... ... . ... . ... ....... · ' . . .... •' .. ·. . . ... ,, . . . . ... ... 

VES 003185 
- PDC Labonrtorles. Inc. 

:rm H.~Qgto..., C7 •!'Iori_., Nci ll3033 

(3t0'43%-05SO •IIIQ m-FAST r.mtll• P.U(3lO 433-4571 .. 

."- ..... . - . . - ·~,.: :_!C 

.. 

vecr.a Envirorimental s.imoes 

Ill l.loC>I1e Avenue 

Saugei,.IL G2201 

Date.Receiwd :08/11/0a 13:13 

Report Dale.: 08/12108 

E#.sl9me.:• : 205130 

P.O. Number' : . 

Fa<:llly : . Alln : Mr. Trey Fonnby 

~""'ole No: 010&1191-f C..ect~1e oat10Jil8 D<t!111 I 

~l Chm:: 1oa~o~----~------~~=:~:~STL ----------------~L=Na::m<~~'- --------~----------~! Quall1fer 1\Mult Anolysls.Oata 

~1t;SS 

. E No: Oto&at81 ~ . ; . ·- ·- . . 011/1(11011 00:01 

,· Q;ent_!P: !!:!!.~.: ______ _· _ __ : sn: ____________ - - .!-~ : -· -- ·-----------

. · PlnQieter Quallftor Resvtt AnalY$)$ Oaf~! 

· .. · EPA14S.1 

Analyst 

... _ 

1.G4" WPS . 

,..,,_._,..be _ _ ........ 1\.1._ ... _ -ctotictabolaiC<y. . .. . 

J 

*- oil 

. . . . .. · .... _ .. , .. .. .~ ... . ... . . \,• ......... .. ~ ~ .. ·. . . . "~ •;. ·. :· . .. •':-

'. 

~ 

i: 

i. 

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~ 

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VES 003186 
. ' 

PDC I.abomtorioS:~ 

- .... ·~ 

.; ~ ' ,--

3278 N.ll!gb'"'T 101 • flor!apt M0631m 

• ell{)~ • (I!CQ:J33.1'ASf 132181 · i'llx!'l{) m..rm 0 

.. : ' - . ' ( ' ' :- . 

Labotato<y Results 

Veolla EnWonmenlal SErvices 

lfT~AvellOO 

Saugol. IL 62201 

Allll : Mr. Trey Formby 

r

""""" No: 08oall398-1 

0"- 10 : 0821080 . Sfto : BATCH 3 

"2/DI·f-I>·Z>.. Ouolifiet 

EPA.24S.t 

-· 

.f'--

. EPA:zA$.1 

-

~No:D8018398-0 

~ 10 : D8Z108G 

EPAl4S.t 

~ 

.:. ~-·· ·· r·:· ·· ·· .~: ·\, 

QualUier 

Site : BATCH • 

Ouoolifier 

····.·· ... .... ··:.···· 

~ t "' 

Re.sult 

1.1 % 

Ruult 

u v. 

~· 

1. 1"' 

*--

Date Rec<!iv&d :08/22108 Oil"()() 

RePort Qato :08/22108 

Custornerlt :20§130 

P.Q:·.N\JIIIIKl!:.;P2008-2 

FaQiily : 

Cdlect Dote 0812111)8 0.:01 

LocolO<·: 

Analysis Date 

08Q2.(1813:00 

C<>I«<Dale 08121101 oe:01 

LocolO< : 

Analysis o.<e 

Ofti'2:1ANl 13.:00 

I 

\WS 

I 

Anoly$1 

' )M'S 

,AnJ.,yst 

MPS 

Page 

•••• •:<. , •.• • ••• ••• ........ • • • •• ' • ·, ( •• - ... • • 

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VES 003187 
. .. . ~·· .. . . .... · .. ·' 

'· 

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... 

... . .. . . · . . . · . .. · . .. 

:: ~~C&. :.;; Out· -.PJ t~Uo1'Trt f-'=CJ'Al~ . 

'sc.fe ln~lon it.j,;,rt ... 

c.no-. ONYX ENVIRONiiieNTAL (88) . 

17 MOBil:E AVENuE . ·. 

,. . . 

.·. . . ... . ·· . 

SAI:IGEr, lL 62201 .. 

.. .... ! •· 

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•·. • • I.Oc:Oiioo· • · ·• Plat11 

: .= ·M!'G, .. otJ<!.: .· '· 32018' . 

· S.... ""* Bei]Ch · 

· .. 21io lb$' 

. ·.; . . :::::. n~~3.ClCf)l4 · 

. . · OM~· ,,:.!.· . ···· . . I ' ~ ' 

'. · .. .· 

.. ' 

CO~I' l ' 

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· .. . , ·.' • , . 

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VES 003196 
'. . : 

"'""- CHROMIC ACID SPIKE FEEp .-Target Ra,te: )<.X pounds/llour 

) lncineralor No. . . Test Run __ _ 

Date--'- ,__--

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VES 003197 
: . •.: · . . . .:.· .. 

·. .·· . .. ·. :_': :". ~- . .. : .... :;. :: : . . .... , SOUD FEED CHARGElf-TargefRaie: 40 ~0\)r 

•···} lndneralor No. · Tes! ~un -- . .. 

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.. .. · 

\ 

VES 003198 
( 

0 

. 

. 

. 

Appendix B 

' 

Reference Method Field Data and Calculations 

ENSR. 

' ; > 

i . 

. :. : . 

. . 

! 

VES 003199