BIWEEKL YUNI T# 4 (CM S Tas k IC4032 ) PAG E 1 O F 3 WAST E FEE D CUT ; OFF

_ PAS S FAI L

1 - TSHH-30 5 KIL N HIG H HIG H S 2 TSHH-31 7 SC C HIG H HIG H ^ 3 PAHH-30 0 KIL N HIG H PRESSUR E / \C 4 PAHH-32 4 SC C HIG H PRESSUR E ^ 6 TAHH-40 4 TEMPERIN G CHAMBE R HIG H TEM P f 7 VIOLATIO N OPACIT YHIG H INSTANTATEOU S 8 PROCES S MONITO R FAILE D ./ ^ 9 WAST E FEE D MONITO R FAILE D y/ ^ 1 2 VIOLATIO N STAC KFLO WHIG H 1 MI N S 1 3 VIOLATIO N ZAC-31 6 (TRV ) OPE N S 1 4 VIOLATIO N ZAC-02 6 SURG E VEN TOPE N ^ 1 5 UA-55 7 ANALYZE R FAI L HC LX ^

- o UA-55 8 ANALYZE R FAI L C O , 1 7 UA-56 0 ANALYZE R FAI L 0 2 S 1 8 UA-56 2 ANALYZE R FAI L H C ^ 1 9 PDAL-56 3 LO WDELT AP
. (I D FA N FAILURE ) ^/ ^ 2 0 WFD-OF F CARBO N INJECTIO N SYSTE M FAILE D ^/ ^ 2 1 PSL-10O/PSL-20 0 SC C COMB
. AI R FA N FAILE D sf 2 3 PSL-20 9 X-1 4 PRIMAR YFUE LLO WPRES S (ONL YAPPLICABL E FO R # 2 FUE LOIL ) \ f 2 5 STAC KFLO WHIG H INSTANTANEOU S ^ 3 5 " VIOLATIO N SC C TEMP
. LO W1 MI N AVERAG E / 3 6 VIOLATIO N KIL N TEMP
. LO W1 MI N AVERAG E ^ 3 7 WFD-OF F HC LHIG H 1 MI N AVERAG E ^ 3 8 WFD-OF F OPACIT YHIG H 1 MI N AVERAG E ^ 3 9 WFD-OF F C O HIG H 1 MI N AVERAG E WFD-OF F H C (THC ) HIG H 1 MI N AVERAG E f j S 4 1 WFD-OF F BAGHOUS E DELT AP HIG H 1 MI N AVERAG E
. c ;



### VES01899 9BIWEEKL YUNI T# 4 (CM S Tas k IC4032 ) PAG E 2 O F 3
' ST E FEE D CUT-OF F PAS S FAI L

y

y _ 4 2 WFD-OF F SD AOUTLE THIG H TEMP
. 1 MI N AVERAG E 4 3 WFD-OF F OXYGE N (02 ) LO W1 MI N AVERAG E 4 4 VIOLATIO N HC L HIG H 1 HOU R AVERAG E 4 5 VIOLATIO N C O HIG H 1 HOU R AVERAG E 4 6 VIOLATIO N SC C TEMP
. LO W1 HOU R AVERAG E 4 7 WFD-OF F KIL N TEMP
. LO W1 BHF F AVERAG E y 4 8 VIOLATIO N OPACIT YHIG H 48 0 SEC/HOU R S 4 9 WFD-OF F BAGHOUS E DELT AP LO W1 MI N AVERAG E y ^ 5 2 Ba g Lea k

Detectio n Syste m (Tribo ) y ^ 6 5 Pumpabl e 1 Hou rRollin g Tota l OP L 6 6 Non-Pumpabl e 1 Hou rRollin g Tota l OP L °q Tota l Wast e 1 Hou rRollin g Tota l OP L 6 8 BT U 1 Hour.Tota i OP L y 6 9 C L1 2 Hou rRollin g Tota l OP L y ^ 7 0 Lo wViolatil e 1 2 Hou rRollin g Tota l OP L y ^ 7 1 Sem i Violatil e 1 2 Hou rRollin g Tota l OP L 7 2 Mercur y1 2 Hou rRollin g Tota l OP L 7 3 As h 1 2 Hou rRollin g Tota l OP L 7 4 PC C Temperatur e 1 Hou rRollin g Averag e Lo wOP L 7 5 SC C Temperatur e 1 Hou rRollin g Averag e Lo wOP L 7 6 SD AOutle t Temperatur e 1 Hou rRollin g Averag e Hig h OP L 7 7 Baghous e Differentia l Pressur e 1 Minut e Averag e Lo wOP L 7 8 Baghous e Differentia l Pressur e 1 Minut e Averag e Hig h OP L 7 9 Stac k

HC L Correcte d 1 Hou rRollin g Averag e Hig h OP L 8 0 Stac k

C O Correcte d 1 Hou rRollin g Averag e Hig h OP L M Stac k

Flo w1 Hou rRollin g Averag e Hig h OP L 8 2 Hr t Cl/Hr a Lim e Flo w1 Minut e Averag e OP L



### VESO1900 0PAG E 3 O F 3

5 0 WAST E FEE D CUT-OF F TES TB YOPERATO R UNI T# 4 OPERATO R T O CLOS E MANUA LHAN D VALV E A TLIQUI D INJECTO R BEFOR E FLE XLIM E & AI R LIN E T O SCREENE D FEEDE R XV-01 3 SLID E GATE
. UNI TM OPERATO R T O VERIF YCUT-OF F B YPRESSIN G EAC H STAR TBUTTON
. (THE N INITIA L & SIG N SHEET ) SHREDDE D SCREENE D MAI N CONVEYO R AU XCONVEYO R X -11 _3_
_ x -1 2 CT? " x -2 2 "yy 2 ^ VERIF YATOMIZIN G AI R ALAR M B YMANUALL YSHUTTIN G AI R T O PRESSUR E SWITCH . (NOZZE L MUS TB E OPE N FO R ALAR M T O FUNCTION )

x " 1 0X -1 1 77 ^ X -1 2 

### ^jy - X-22

VT ^

8 3 Lim e Slurr

y Density Lo w1 Hou rRollin g Averag e Shoutdow n 4 LO G CHECK S I N OPERATION S BOO K 8 5 RO D OU TKIL N PRESSUR E LIN E (PT-300 )
COMMENTS :

CHECKE D BY : Date : j/./T-Q ^ Time : 2 ' SO A M
APPROVE D BY : Place : Contro l Roo m BIWEEKLY_ 4 9/10/0 7 H K



### VES01900 1" BivVEEKL YUNI T# 4 (CM S Tas k IC4032 ) PAG E 1 O F 3
' "AST E FEE D CUT-OF F [ PAS S _.fAI L

1 TSHH-30 5 KIL N HIG H HIG H ^ 2 TSHH-31 7 SC C HIG H HIG H X 3 PAHH-30 0 KIL N HIG H PRESSUR E X * 4 PAHH-32 4 SC C HIG H PRESSUR E / 6 TAHH-40 4 TEMPERIN G CHAMBE R HIG H TEM P X 7 VIOLATIO N OPACIT YHIG H INSTANTATEOU S S~ 8 PROCES S MONITO R FAILE D ^ 9 WAST E FEE D MONITO R FAILE D ^ 1 2 VIOLATIO N STAC KFLO WHIG H 1 MI N 1 3 VIOLATIO N ZAC-31 6 (TRV ) OPE N X 1 4 VIOLATIO N ZAC-02 6 SURG E VEN TOPE N S 1 5 UA-55 7 ANALYZE R FAI L HC LX 1 6 UA-55 8 ANALYZE R FAI L C O , X 1 7 UA-56 0 ANALYZE R FAI L 0 2 1 8 UA-56 2 ANALYZE R FAI L H C 1 9 PDAL-56 3 LO WDELT AP
. (I D FA N FAILURE ) / "

- 2 0 WFD-OF F CARBO N INJECTIO N SYSTE M FAILE D 2 1 PSL-1O0/PSL-20 0 SC C COMB
. AI R FA N FAILE D * S 2 3 PSL-20 9 X-1 4 PRIMAR YFUE LLO WPRESS
. (ONL YAPPLICABL E FO R # 2 FUE LOIL ) ^ 2 5 STAC KFLO WHIG H INSTANTANEOU S ^ 3 5 VIOLATIO N SC C TEMP
. LO W1 MI N AVERAG E X ^ X " 3 6 VIOLATIO N KIL N TEMP
. LO W1 MI N AVERAG E 3 7 WFD-OF F HC L HIG H 1 MI N AVERAG E ^ 3 8 WFDOF F OPACIT YHIG H 1 MI N AVERAG E ^ 3 9 WFD-OF F C O HIG H 1 MI N AVERAG E ^ .'4 0 WFD-OF F H C (THC ) HIG H 1 MI N AVERAG E X ^ 4 1 WFD-OF F BAGHOUS E DELT AP HIG H 1 MI N AVERAG E S


### VES01900 2BIWEEKL YUNI T# 4 (CM S Tas k IC4032 ) PAG E 2 O F 3 • ' ' ^ST E FEEDCUT-OF F PAS S FAI_L
_

4 2 WFD-OF F SD AOUTLE THIG H TEMP
. 1 MI N AVERAG E 4 3 WFD-OF F OXYGE N (02 ) LO W1 MI N AVERAG E

4 8 VIOLATIO N OPACIT YHIG H 48 0 SEC/HOU R 4 9 WFD-OF F BAGHOUS E DELT AP LO W1 MI N AVERAG E 5 2 Ba g Lea k

Detectio n Syste m (Tribo ) 6 5 Pumpabl e 1 Hou rRollin g Tota l OP L 6 6 Non-Pumpabl e 1 Hou rRollin g Tota l OP L 6 7 Tota l Wast e 1 Hou rRollin g Tota l OP L 6 8 BT U 1 Hou rTota l OP L 6 9 C L 1 2 Hou rRollin g Tota l OP L 7 0 Lo wVTolatil e 1 2 Hou rRollin g Tota l OP L 7 1 Sem i Violatil e 1 2 Hou rRollin g Tota l OP L 7 2 Mercur y1 2 Hou rRollin g Tota l OP L 7 3 As h 1 2 Hou rRollin g Tota l OP L 7 4 PC C Temperatur e 1 Hou rRollin g Averag e Lo wOP L 7 5 SC C Temperatur e 1 Hou rRollin g Averag e Lo wOP L 4 4 VIOLATIO N HC L HIG H 1 HOU R AVERAG E X 7 4 5 VIOLATIO N C O HIG H 1 HOU R AVERAG E / ~ 4 6 VIOLATIO N SC C TEMP
. LO W1 HOU R AVERAG E / ~ k\0<A1LX 4 7 WFD-OF F KIL N TEMP
. LO WHMtt * AVERAG E ' 

# X



# r 7 6 SD AOutle t Temperatur e 1 Hou rRollin g Averag e Hig h OP L f 7 7 Baghous e Differentia l Pressur e 1 Minut e Averag e Lo wOP L 7 8 Baghous e Differentia l Pressur e 1 Minut e Averag e Hig h OP L 7 9 Stac k

HC L Correcte d 1 Hou rRollin g Averag e Hig h OP L 8 0 Stac k

C O Correcte d 1 Hou rRollin g Averag e Hig h OP L 3 1 Stac k

Flo w1 Hou rRollin g Averag e Hig h OP L 8 2 Hr t Cl/Hr a Lim e Flo w1 Minut e Averag e OP L



### VES01900 3BIWEEKL YUNI T# 4

\ST E FEE D CUT-OF F CHECKSHEE T PAG E 3 O F 3

5 0 WAST E FEE D CUT-OF F TES TB YOPERATO R UNI T# 4 OPERATO R T O CLOS E MANUA LHAN D VALV E A TLIQUI D INJECTO R BEFOR E FLE XLIM E & AI R LIN E T O SCREENE D FEEDE R XV-01 3 SLID E GATE
. UNI Tm OPERATO R T O VERIF YCUT-OF F B YPRESSIN G EAC H STAR TBUTTON
. (THE N INITIA L & SIG N SHEET ) SHREDDED
_ X-1 0 _SCREENED
_ X -1 1 MAI N CONVEYO R X-1 2 A U XCONVEYO R X -2 2 VERIF YATOMIZIN G AI R ALAR M B YMANUALL YSHUTTIN G AI R T O PRESSUR E SWITCH . (NOZZE L MUS TB E OPE N FO R ALAR M T O FUNCTION ) X-1 0 X -1 1 X -1 2 X -2 2 ALS O CHEC KOPE I CHECKE D BY : O F RA M COOLIN G WATE R LOWiFLO WALAR M (MSG * >278 )

8 3 Lim e Slurry Densit y Lo w1 Hou r Rollin g Averag e

, JA LO G CHECK S I N OPERATION S BOOK . 8 5 RO D OU TKIL N PRESSUR E LIN E (PT-300 ) Shoutdow n

COMMENTS :

CHECKE D BY : 

### APPROVED BY : Date:lo^-VD° l Time : I < (a^Vm -
Place : Contro l Roo m
BIWEEKLY_ 4 9/10/0 7 H K



### VES01900 4ABSOLUT E CALIBRATIO N AUDI T(ACA ) DAT A SHEE T

Uni t # 4Seria l #

Paramete r NIS TTraceabl e Calibratio n Standard s

> 0 2 25 % G a s Concentratio n

« * CO-lo wrang e 200pp m 

### Lo w(Zero ) 0 

# + 0. 5
r CO-hig h rang e 3000pp m 

### Mi d 8.9 3 

# ± 0. 5
r HC I 1000pp m 

### Hig h 1 5 

# + 0. 5 

### Ru n Numbe r Concentratio

n Differenc e Referenc e Analyze

r Lo

w Mi

d High 1-Lo w 0 0. 1 -0.1 — — 

### 2-Mid 8.9

3 8.9

8 — 

### -0.0 5 — 

### 3-Hig h 1 5 15. 3

—' — 

### -0.3 4-Lo w 0 0. 1 -0.1 — — 

### 5-Mi d 8.9

3 9

— . 

### -0.0 7 

# _ 6-High 1 5 15. 2 x — — 

### -0.2 7rL0 W 

### 0

. 0.

1 -0.1

. . —. —. 

### 8-Mi d 8.9

3 8.

9 — 

### 0.0 3 — 

### 9-Hig h 1 5 15. 2 — — 

### -0.2 Mea n Differenc

e = -0.1 0 -0.0 3 -0.2

3 Calibratio n Erro r= -0.40

% -0.12

% -0.93

% Calibratio n Erro r= Mea n Difference/Spa n Valu

e * 10 0

E/ITec h 

### Titl e 9/22/200 9 

### Dat e

VES01900 5ABSOLUT E CALIBRATIO N AUDI T(ACA ) DAT A SHEE T

Unit # 4Seria l #

Paramete r NIS TTraceabl e Calibratio n Standard s 

### r 0 2 25 % G a s Concentratio n CO-lo wrang e 200pp m 

### Lo w(Zero ) 0 

# ± 10

r CO-hig h rang e 3000pp m 

### Mi d 68.

9 

# ± 10

rHC I 1000pp m 

### Hig h 15

4 

# ± 1 0 Run Numbe

r Concentratio

n Differenc e Referenc e Analyze

r Lo

w Mi

d Hig

h 1-Lo w 0 -0. 2 0.

2 — — 

### 2^Mi d 68.

9 66.

7 — 

### 2. 2 — 

### 3-High 15

4 152.

6 — —. 

### 1. 4 4-Lo w 0 -0. 4 0.

4 — — 

### 5-Mi d 68.

9 66.

8 — 

### 2. 1 

# _ 6-High 15

4 154.

5 — — 

### -0.5 7-Low . 0 -0.1 0. 1 — — 

### 8-Mi d 68.

9 6

7 — 

### 1. 9 — 

### 9-High 15

4 153.

4 — — 

### 0. 6 Mea n Differenc

e = 0.2

3 2.0

7 0.5

0 Calibratio n Erro r= 0.12

% 1.03

% 0.25

% Calibratio n Erro r= Mea n Differenc

e / Spa n Valu e * 10 0

E / l Tec h 

### Titl e 9/22/200 9 

### Dat e

VES01900 6ABSOLUT E CALIBRATIO N AUDI T(ACA ) DAT A SHEE T

Unit # 4Seria l #

Paramete r NIS TTraceabl e Calibratio n Standard s 

### r 0 2 25 % G a s Concentratio n
r CO-lo wrang e 200pp m 

### Lo w(Zero ) 0 

# ± 15 0 CO-hig h rang e 3000pp m 

### Mi d 1079. 1 

# ± 15 0
r HC I 1000pp m 

### Hig h 228 9 

# ± 15 0 

### Ru n Numbe

r Concentratio

n Differenc e Referenc e Analyze

r Lo

w Mi

d Hig

h 1-Low . 0 -0. 2 0.

2 — — 

### 2-Mi d . 1079.

1 1086.

5 — 

### -7. 4 — 

### 3-High 228

9 228

7 — — 

### 2 4-Lo w 0 -0. 4 0.

4 — — 

### 5-Mi d 1079.

1 1077.

6 — 

### 1. 5 — 

### 6-High 228

9 2317.4

. — — 

### -28. 4 7-Lo w 0 -0.1 0. 1 — — 

### 8-Mi d 1079.1 1077. 7 — 

### 1. 4 — 

### 9-Hig h 228

9 2301.

9 — — 

### -12. 9 Mea n Difference

= 0.2 3 -1.50' -13.1 0 Calibratio n Erro r= 0.01 % -0.05

% -0.44

% Calibratio n Erro r= Mea n Differenc

e / Spa n Valu e * 10 0

E / l Tec h Titl e 9/22/200 9 Dat e



### VES01900 7ABSOLUT E CALIBRATIO N AUDI T(ACA ) DAT A SHEE T

Uni t # 4Seria l #

Paramete r 

### r 0 2 25 %
r CO-lo wrang e 200pp m
rCO-hig h rang e 3000pp m ffHC I 1000pp m NIS TTraceabl e Calibratio n Standard s Paramete r 

### r 0 2 25 %
r CO-lo wrang e 200pp m
rCO-hig h rang e 3000pp m ffHC I 1000pp m G a s Concentratio n Paramete r 

### r 0 2 25 %
r CO-lo wrang e 200pp m
rCO-hig h rang e 3000pp m ffHC I 1000pp m 

### Lo w(Zero ) 0 

# ± 5 0 Paramete r 

### r 0 2 25 %
r CO-lo wrang e 200pp m
rCO-hig h rang e 3000pp m ffHC I 1000pp m 

### Mi d 31 8 

# + 5 0 Paramete r 

### r 0 2 25 %
r CO-lo wrang e 200pp m
rCO-hig h rang e 3000pp m ffHC I 1000pp m 

### Hig h 70

7 

# + 5 0 Run Numbe

r Concentratio

n Differenc e Referenc e Analyze

r Lo

w Mi

d • Hig

h 1-Lo w 0 -0. 3 0.

3 — — 

### 2-Mi d 31 8 284. 9 — 

### 33.1 — 

### 3-High 70

7 713.1 — — 

### -6.1 4-Lo w 0 0 0 — — 

### 5-Mi d 31 8 306. 2 — 

### 11. 8 

# _ 6-High 70

7 707.

1 ' — — 

### -0.1 7-Lo w 0 0. 6 -0.

6 — — 

### 8-Mi d 31 8 314. 2 — 

### 3. 8 — 

### 9-High 707 . 708. 6 — — 

### -1. 6 Mea n Differenc

e = Calibratio n Erro r= -0.1 0 16.2

3 -2.6

0 Mea n Differenc

e = Calibratio n Erro r= -0.01 % 1.62

% -0.26

% Calibratio n Erro r= Mea n Differenc

e / Spa n Valu e * 10 0

E/ITec h 

### Titl e 9/22/200 9 

### Dat e

VES01900 8Tabl e 1 Summar y o fRelativ e Accurac yTes t Audi t Result s

Veoli a E S Technica l Solution s

Sauget , Illinoi s Jun e 22,2 3 an d 24,200 9 CEM S Paramete r Unit s Measure d R A Criteri a Pass/Fai l 

### Uni t 2 C O pp m @ 7 % 0 2 

### 0.00

4 ppm a 

### 5 a 

### ' b 

### Pas s Uni t 2 0 2 

### , dr

y %o 2 

### 0.09% a 

### 1.

0 a 

### - c 

### Pas

s Uni t 2
0 2 

### , we

t %o 2 

### 0.13% a 

### 1.

0 a 

### ' ° Pas

s Uni t 3 C O pp m @ 7 % 0 2 

### 0.06

3 ppm a 

### Pas s Uni t 3 0 2 

### , dr

y %o 2 

### 0.02% a 

### 1.

0 a 

### ' c 

### Pas

s Uni t 3 0 2 

### , we

t %0 2 

### 0.31% a 

### 1.0 a,c 

### Pas s Uni t 4 C O pp m @ 7 % 0 2 

### 1.14

6 ppm " 5



### a. b Pas

s t 4 0 2 

### , dr

y %o 2 

### 0.15% a 

### 1.0 a 

### 'c 

### Pas

s Uni t 4 0 2 

### , we

t %o 2

### , 0.46% a 

### 1.

0 a 

### ' c 

### Pas

s

a

### Percen t o femissio n standar d o rabsolut e averag e differenc

e (pp m or%) . b 

### PS4B . C 

### PS3 .

INCINERATO R CEM S RAT A 5 JUL Y7,200 9 VEOLI A E S CE C Projec t 090-86 1

### VES01900 9Incinerato r Dat a Poin t

Carbo n Injectio n Flo w Lim e Slurr yDensit y Stac k Opacit y Stac k C O RCR A S D AOutle t Tem p Baghous e Dif fPres s Lo w Baghous e Dif fPres s Hig h Stac k TH C X1 1 Weigh t X 2 2 Weigh t X 1 2 Weigh t X 1 0 Weigh t Stac k HC L RCR A Veoli a Environmenta l Service s Sauge t Illinoi s Create d Perio d Star

t Perio d E n 1/1/201 0 6:00 A M 1/1/201 0 6:00 A M 1/1/201 0 6:00 A M Pag e 5 of 7 

### 4 IMi n IMi n IMi n I H r Rol l 1 H r Rol l 1 H r Rol l I H r Rol l 1 H r Rol l I H r Rol l 1 2 H r 1 2 H r 1 2 H r 1 H r To t 1 H r To t 1 H r To t A V G AV G AV G War n Shu t OP L To t To t Shu t To t OP L Rol l To t Rol l To t Rol l To t War n War n Shu t OP L War n Warn Shu t Shu t OP L OP L

65.0000 0 8.00000 0 10.0000

0 450.000 0 500.000

0 440.000 0 500.000

0 3.00000 0 2.00000

0 9.00000 0 10.0000

0 8.00000 0 10.0000

0 . 6.60000 0 6.30000

0 6.20000

0 65.5000 0 65.4000

0 65.2000

0

30.0000 0 40.0000

0 100.000

0 429.000 0 431.000

0 434.000

0

. 900.000

0 950.000

0 1008.00

0

400.000 0 500.000

0 15.0000 0 32.0000

0 35.0000

0 . 1550.00 0 1650.00

0 1700.00

0

. 850.000

0 950.000

0 1 000.00

0

. 1000.00

0 1050.00

0 1100.00

0

. 1600.00

0 1650.00

0 1700.00

0



### VES01901 0Veoli a Environmenta l Service s Sauge t Illinoi s 4.00000 0 3.00000

0 30.0000 0 33.5000

0 37.2000

0 Stac k 0 2 RCR A HCLtoLim e Shredde d Weigh t Temperin g Chambe rTem p soo.ooo o 1200.00 0 P C C Tem p 1300.00 0 1240.00

0 S C C Tem p 1850 .00 0 1825.00

0 Stac k C O Correcte d Stac k HC L Correcte d Stac k 0 2 Correcte d Stac k Flo w L o wBT U Liqui d Weigh t Hig h BT U Liqui d Weigh t Liqui d Weigh t Containerize d Weigh t Solid s Weigh t Weigh t 450.000 0 500.000

0 100.000 0 150.000

0 4.00000 0 38000.0 0 1570.00 0 1515.00

0 1507.00

0 1905.00 0 1890.00

0 1886.00

0 30.0000 0 75.0000

0 100.000

0 25.0000 0 32.0000

0

37000.0 0 37600.0

0 38086.0

0

. 2800.00

0 3050.00

0 3256.00

0

. 1500.00

0

. 10000.0

0

. 12500.0

0 13000.0

0 13796.0

0 Create d

Perio d Star

t Perio d E n 1/1/201 0 6:00 A M 1/1/201 0 6:00 A M 1/1/201 0 6:00 A M Pag e 6 of 7

13000.0 0 145O0.0

0 15000.0

0

1600.00 0 165O.00

0 1700.00

0 1000.00 0 1050.00

0 1100.00

0

2500.00 0 2750.00

0 3000.00

0 13000.0 0 140O0.0

0 15000.0

0



### VES01901 1I

B T U Chlorin e Mercur y As h L o wVolatil e Sem i Volatil e Veoli a Environmenta l Service s Sauge t Illinoi s

. 235.000

0 252.000

0

. 0.02100

0 0.02600

0

. 8000.00

0 8777.00

0

. 43.0000

0 47.0000

0

. 60.0000

0 64.0000

0 Create d Perio d Star

t Perio d E n 1/1/201 0 6:00 A M 1/1/201 0 6:00 A M 1/1/201 0 6:00 A M

Pag e 7 of 7

. 4800000

0 490OD00

0 5000000

0

. 2800.00

0 2900.00

0 3024.00

0 400.000

0 450.0000 500.000 0

. 0.25000

0 0.27500

0 0.31200

0

. 90000.0

0 100000.0 105324.0

. 500.000

0 540.000

0 564.000

0

. 700.000

0 740.000

0 768.000

0



### VES01901 2Facilit y Oxyge n Dat a



### VES01901 3

### December , 200 9 Averag e Oxyge n Concentration s fo r Unit s 2 , 3 , an d 4

Uni t 4 Dat e Metho d 5/2 6 We t 0 2 Dr y 0 2 (% ) (%

) Metho d 0023 A

We t 0 2 Dry 0 2 (% ) (%

) 12/8/200 9 5. 6 10. 3 4. 8 9. 1 12/9/200 9 5. 8 10. 4 5. 1 9. 3 12/10/200 9 5. 1 9. 3 4. 3 8. 2

Dat e Metho d

We t 0 2 (% ) 5/2 6 Dr y 0 2 (% ) Metho d 0023 A

We t 0 2 Dr y 0 2 (% ) (%

) 12/1/200 9 5. 7 9. 5 4. 0 7. 3 12/2/200 9 4. 5 7. 8 4. 1 7. 3 12/3/200 9 6. 2 10. 4 5. 6 9. 5

Dat e Metho d 5/2 6

We t 0 2 Dr y 0 2 (% ) (%

) Metho d 0023 A

We t 0 2 Dry 0 2 (% ) (%

) 12/16/200 9 8. 6 12. 7 7. 7 12. 6 12/17/200 9 7. 9 12. 5 8. 0 12. 4 12/18/200 9 7. 3 12. 6 6. 9 12. 3C D



### VES01901 5

# AECOM

Appendi xB J Referenc e Metho d Fiel d Dat a an d Calculation s j



### VES01901 6Metho d 5/26 A



### VES01901 7Particulat e Result s Summar y Uni t 4 Veoli a E S Technica l Solution s

Sauget , I L Averag e

0.0016 B 0.0028 2 0.0012 0 Tes t Results : Ru n 1 Ru n 2 Ru n 3 Particulat

e Emissio n Concentration : grains/dscf grains/dsc

f@ 7 % 0 2 grains/dscf®

15 % 0 2 0.0013 8 0.0023 4 0.0009 9 0.0011 8 0.0019 S 0.0008 3 0.0024 6 0.0041 5 0.0017 6

Where ;
pj^s$^^ ^



### VES01901 8Result s Summar y Uni t 4 Veoli a E S Technica l Solution s

Sauget , I L Ru n 1 Ru n 2 Ru n 3 Average Parameter : Molecular (Total

mg)'mg/dscm', (ppm@ (Ib/hr)

(Total

mgymg/dscm;

(ppm%

(Ib/hr)

(Total

mgy.mg/dsom)

(ppm@

(IM")

(mg/dscm;

(ppm®

(Ib/hr) Weight 7%02) 7%02) 7%02) 7%02) HC I | 36.4 6 | I 34.6 I 26. 0 29. 1 1.8 3 I 43. 1 [ 33. 1 36.2 2.3 2 I 3. 6 I 3.0 3.3 0.2 0 20. 7 22. 8 1.4 5 CL2 | 70. 9 I | 0.4 8 I 0.4 5 0.1 6 0.00

B I 0.4

7 I 0.4 4 0.1 5 O.0

1 I 0.4

8 I 0.4 3 0.1 5 0.01 0.4 4 0.1 5 0.0 1 Tota l 29.2 36. 3 3.6 23. 0

Where :

m6«?a* = rMBqcWat fHWWtiwrdr) ! sfwaarsfcubi cmelsi- = (msftscf^S ! (3 S St4-^icfe«/eu|*ns<star ) UlJrnK S @ 7%02 - OSrt

s pSrrtifc n « 7%6xtfgej^(<mfl/(l5cm'2, 4 0 4 litsra/mQl!/ftKil > »*n*((ZO,9-7)/(20.9.a?%) )



### VES01901 9Calculation s Summar y Uni t 4 Veoli a E S Technica l Solution s

Sauget , I L
Vw(std) , sc f= Vm(std) , dsc f= Bws = Md = Ms = Vs , ft/se c= Qs , acf m = Qs(std) , dscfr n = Isokineti cSamplin g Rate , % Ru n 1 26.124 47.00 4 0.35 7 29.4 2 25.34 61. 8 46,60 3 18,84 5 101.7 Ru n 2

26.081 45.92 1 0.36 2 29.4 4 25.30 62. 1 46,84 7 18,64 6 100.4 Ru n 3

23.91 6 43.01 6 0.35 7 29.3 8 25.3 2 59.2 44,65 3 17,70 4 99.0 Averaq e

25.37 4 45.31 4 0.35 9 29.41 25.3 2 61. 1 46,03 4 18,39 8 100.4

Where : Vw£std > volum e o f wate rvapo ri n gas , standar d condition s * 0M7G7V\c Vm(sld ) *Vol
. o f^a s sampled , Standar d cOridrttori s = 1 7 64 7 xV m xgamm a xTP b + (dH/136)j/Tm<R ) B\fe!!i^aiir& ^ M d molecula rweigh t O fstac k gas , dr ybasf e =

> (0.4 4 x%C02)

+ (0.3 2 x%02 ) + [02 B X(%N2 + %CQ) ] M s = • molecula rweigh t of

stac k gas , we t basi s * [M d x(1-Bws) ] + • (18> Q xBws ) V s * staci s ga s velocit y= 85.4 9 XC p x(avg
. S q Ri dP ) x]5q,R t (Ts(R»/(M s xPS) J Qs(std ) * > stac k ga s flqwrate rstandar d condition s = Q s x(1-Bws ) x<528/(Ts<R)>x(Ps/2 9 92 )



### VES01902 0Tes t Dat a Summar y Uni t 4 Veoli a E S Technica l Solution s

Sauget , I L

12/16/0 9 11:3 8 12:4 1 6 0 0.30 7 0.8 4 0.99 1 1.80 1 Paramete rRu n 1 Ru n Dat e Star t Tim e Sto p Tim e Duratio n o fRun , Minute s A>ve
. Nozzl e Diameter , inche s Pito t Calibratio n Factor , C F Mete rGamm a Mete rDelt a H , inche s o fH2 0 Stac k Diameter , inche s Rectangula rWidth , inche s Rectangula rLength , inche s Stac k Area , sq.ft
. Barometri cPressure , inche s o fH g Stati cPressure , inche s o fH2 0 Dr yGa s Mete rSampl e Volume
. (VM)ft 3

Initia l Fina l Differenc e 43.84 2 4 8

12.5 7 30. 2 -0.4 7
580.37 8 624.2 2 Ru n 2 12/17/0 9 9:4 6 10:4 8 6 0 0.30 7 0.8 4 0.99 1 1.80 1 4 8

12.5 7 3 0 -0.5 1
755.41 4 799.16 4 43.7 5 Ru n 3 12/18/0 9 9:5 0 10:5 2 6 0 0.307 0.8 4 0.99 1 1.80 1 4 8

12.5 7 29.6 5 -0.3 4
930.62 5 972.95 7 42.33 2 Avve
. Stac k

Temperature , Ts(F ) A>ve
. Mete rTemperature , Tm(F ) A,ve
. Ru n Delt a H , inche s ofH2 0 /\ve
. Squar e Roo t o fDelt a P 386. 2 34. 8 1.8 5 0.818 1 387. 3 42. 1 1.8 3 0.818 4 387. 4 52. 4 1.6 5 0.775 8 Moistur e Dat a Volum e o fwate rcollected , mi s Silic a Gel , gram s Tota l Collected , mi s 54 6
55 5 54 4 10. 1 554. 1 49 9 9. 1 508. 1 ORSA TDat a

%0 2 %C0 2 %C O 12. 7 5. 7 12. 5 5. 9 12. 6 5. 5



### VES01902 1Fiel d Data Summar y Uni t 4 Veoli a E S Technica l Solution s

Sauget , I L Travens e Pain t Star t Temp(F) Delta

P Delta W TmtF) SQRT

Delta P Stack

TempfF) Delta

P Delt a

H TmlF) SQRT

Delta P StacH

TempfF) Delt a

P Delt a W TmlF) sou r

Delta P Star t Temp(F) Delta

P Delta W In out SQRT

Delta P Stack

TempfF) Delta

P Delt a

H In

out SQRT

Delta P StacH

TempfF) Delt a

P Delt a W in out sou r

Delta P 38 2 072 2.0

0 2 7 2 8 0.848

5 38

7 0.7 0 1.9

0 33 3

6 0.B36

7 \ - 38

3 0.7 2 2.0 0 3 9 3 9 0.84B 5 386 0.6

8 1.9 0 2 6 3 4 0.824

6 38

7 0.7 0 1.9

0 34 4

0 0.836

7 ; l | : 3B

0 0.6 6 1.9 0 3 9 4 5 0.824 8 38 8 0.6 7 1.8 S 2 9 3 6 0.818

5 39

1 0.7 4 2.0

0 3 5 4 3 0.860

2 ; ! 38

9 0.6 5 1.6 0 4 0 4 9 0.806 2 387 0.7

0 1.9 0 29 3

7 0.836

7 38

4 0.7 4 2.0

0 3 6 4

5 0.B60

2 I : 38

8 0.6 3 1.7 0 4 2 , 5 3 0.793 7 38 6 0.6 6 1.8 0 3 0 3 9 0.B24

6 3B

4 0.6 4 1.7

5 3 6 4

6 0.800

0 : • 

### i 38

8 0.6 0 1.6 5 4 4 5 6 0.7746 38 4 0.5 7 1.6 0 3 1 4 0 0.755

0 38

4 0.5 3 1.4

5 3 7 4 7 0.728

0 :• • 38

5 0.4 9 1.3 5 4 6 5 9 0.7000 38 4 0.7 3 2.0 0 3 1 3 9 0.864

4 38

5 0.6 4 1.7

5 3 8 4 7 o.soo o :• • 38

6 0.6 3 1.7 0 4 9 6 0 0.793 7 38 5 0.6 6 1.9 0 3 2 4 0 0.824

6 38

6 0.7 2 2.0

0 3 6 4 8 0.B4B

5 : i 38

B 0.6 3 1.7 0 5 1 6 2 0.793 7 390 0.7

3 2.0 0 3 3 4 2 0.854

4 38

8 0.7 4 2.0

0 4 0 5 1 0.860

2 ; i 38

7 0.6 0 1.6 5 5 2 6 4 0.774 6 39 0 073 2.0

0 3 4 4 2 0.854

4 39

2 0.7 4 2.0

0 40 5

1 0.860

2 i : 36

9 0.6 0 1.6 5 5 4 6 6 0.774 6 389 0.6

4 1.6 0 3 4 4 2 0.800

0 39

0 0.7 0 1.9

0 41 5

3 0.836

7 : i 38

8 0.5 7 1.5 5 5 5 6 7 0.755 0 383 0.S 2 1.4 0 3 5 4 4 0.721 1 36 9 0.4 3 1.3

0 4 2 5 3 0.692

8 \ \ i i 36

8 0.4 5 1.2 0 5 7 6 9 0.670 8

-

366. 2 0.67 1.8 5 3 1 3 9 0.818 1 387. 3 0.67 1.83 38 4 7 0.8184 387. 4 0.6 0 1.6 5 47 5 7 0.775 8 M 2 3 4 5 6 8 1 2 3 4 5 6

Averag e Laborator

y Result s FuelF-factor.dscf/MMBt u File rI D Fron t Hal fResidues : Filte rwt , g Aceton e rinse volume , ml Aceton e wt, g F H Total , g Bac k Hal fResidues : BH . Total. g Aceton e Blan k

Residues : Aceton e blan k

volume , m

l Aceton e Blan k weigh t g Aceton e weight gain. g Aseton B Blan k

concentratio n .001 % o fAceton e Blan k

Weight Weioht o

fResidu e i n Aceton e Wash , g Corrected Aceton e Blan k Value , g (F.H . Total+B.H . Total-Blank) : Ru n 1 1 I T161 5 I f j

I 0.001 5 I I 0.001 5 ~ l 3 C 3 0.Q02 6 I I 0,0021 1 Ru n 3 T181 8 I

0.004 2 I ~-iT~ l 0.002 8 I

1 155.469 6 I I 155.469

6 '

I 0.000 1 0.000

3 I 19

8 I I 155.4696 1 I 0.000 3 I

0.000 1 I I 0.000 1 0.00007 4 I C a = MalVaP a

W a = CaVawP a

Total , g



### VES01902 2

### Dr yGa s Mete r Calibratio n Dat a Summar

y Uni t 4 Veoli a E S Technica l Solution s

Sauget , I L Paramete r Ru n I D Ru n Dat e Mete rBo xI D Duratio n o fRun , Minute s Mete rGamm a Delt a H@ , inche s o fH2 0 Barometri cPressure , inche s o fH g Sampl e Volume , dc f(Vm ) Ave
. Mete rTemperature , F (Tin ) DryMolecula rWeigh t (Md ) Ave
. Delt a H , inche s o fH2 0 Ave
. SQR TDelt a H , inche s o fH2 0 Yq a (calculate d calibratio n factor ) % Differenc e 12/16/200 9 00 2 6 0 0.99 1 1.801 30. 2 43.84 2 34.8 3 29.4 2 1.8 5 1.3 6 0.9S 3 0. 2 12/17/200 9

00 2 60 0.99 1 1.80 1 3 0 43.75 0 42.0 8 29.2 8 1.8 3 1.3 5 1.00 1 1. 0 12/18/200 9

00 2 6 0 0.99 1 1.80 1 29.6 5 42.33 2 52.3 8 29.3 8 1.6 5 1.2 8 0.99 8 0. 7 Averag e

0. 6 Yq a = (tes t durationA/m ) x(SQRT(0.0319*TmR)/(Delt a H @ x(Pba r+ Ave
. Delt a H/13.6) ) x(SQRT(29/Md) ) xAve.(SQR TDelt a % Differenc e = (Yq a - Mete rGamma)/Mete rGamm a Thre e ru n Averag e % Differenc e mus t b e < = 5 %



### VES01902 3

## EP A ISOKINETI C SAMPLIN G - FIEL D DAT A SHEE T Samplin g Trai n M 5 Ru n Numbe r Clien t 

# ± Veoli a E S Technica l Solution s Facilit y Locatio n Sourc e Dat e Operato r Stac k Dia , - in . Star t Tim e Sto p Tim e Sauget

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e ID : tap Outle t T C ID : 

## 3a. 2, LEA KCHECK S i n "H g INITIA L VAC . /JiFINA L VAC . CFM€?,0O>-j p

CF M CF M



## - y + . ' 7 * / FINA

L PITO T* / * H FILTE RDATA

i vp IN T r i K r \ n o I 

## sffillliLi I HU

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## 2.7$- G 4 M H A k TEMPERATUR E READINGS , ° F 

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## VES01902 4

## AECOM EP A ISOKINETI C SAMPLIN G - FIEL D DAT A SHEE T Samplin g Train Ru n Numbe r Clien t Barometri c Pressur e 

## $DJB> Veoli a E S Technica l Solution s Facilit y Locatio n Sourc e Dat e Operato r Stac k Dia . - in. Star t Tim e Sto p Tim e Sauget

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V . Pito t Coefficien t . Q .ff Filte rBo xNo . Q^> e \ Mete r Bo xNo . LEA KCHECK S i n "H g INITIA L VAC . /QL. MI D VAC . -- ~ - FINA L VAC . /O CF

M 

## O CF M CF M O 

## .<sa INIT . PITO T 

## JBL Orific e Coefficien t (Y ) <Q f Delt a H @ /

~/HO I Nozzl e Size/No . Q.SOl FINA L PITO T FILTE RDAT A 

### iQ. t/f /O ¥8 *A D Thermocoupl

e ID: M<7Td~2 Mil l IMPlNGIl t V0 1 > , I JNH V "30 " 

# 1W

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## 160 (Co. ? * 3 RINS E

V 7 

## ur 1 Orsa

t 1 | C02. .

, 02 

## V' 1

Fina l Purg e Rat e fl / AI Pc P O N h , I T



## mfflMrl W o i n r H \

i vF K •ft i 1 TEMPERATUR E READINGS , ° F PUM P \AC Ii i M ill . H p COMMENT S I Pc P O N h , I T



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i vF K •ft i 1 i \

i i Hi n O W N (U K\<l l Mllll l 1 1 1 MPINGER I 1 \SM I III I PUM P \AC Ii i M ill . H p COMMENT S I Pc P O N h , I T



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## VES01902 5

### AECOM EP A ISOKINETI C SAMPLIN G - FIEL D DAT A SHEE T IM I IM.I l < Mi l 1 1 Orsa t Samplin g Trai n /' V//TO / Barometri c Pressur e oi 7. j f ©—' LEA

KCHECK S i n "H g IM I IIN\ I ,RINSE s ;coi?' - Ru n Numbe rZ ' Stati c Pressur e <+/- ) -~0 ,'3 T INITIA

L V VI1 D VAC . FINA L W INIT . PIT O n

. CF M 

### V n . CF M n . CF M S O 

### f.r Clien t Veoli

a E S Technica l Solution s Probe/Pito t Numbe r.£jftt£V tff

c INITIA

L V VI1 D VAC . FINA L W INIT . PIT O n

. CF M 

### V n . CF M n . CF M 

### m 

### f.r Facilit y Locutio n Sauget

, IL Pito t Coctficien t Filte rBo xNo . Mete r Bo xNo . INITIA L V VI1 D VAC . FINA L W INIT . PIT O ^C . n

. CF M 

### V n . CF M n . CF M ff,0 0 2

- 

### /Od Sourc e /Mf/T

*t V Pito t Coctficien t Filte rBo xNo . Mete r Bo xNo . INITIA L V VI1 D VAC . FINA L W INIT . PIT O T FINA

L PITO T DAT A + 

# / > &fTf Da, e /3-/*-7d<l« y Pito t Coctficien t Filte rBo xNo . Mete r Bo xNo . INITIA L V VI1 D VAC . FINA L W INIT . PIT O T FINA

L PITO T DAT A + 

# / > /CO Operato r Stac k Dta . - i n Star t Tim e Sto p Tim e 

### tiUUtobLf

-t - tv>*«oL&f Orific e Coefficien

t 0 Delt a H @ Nozzl e Size/No . XA D Thermocoupl

e Im p Outle t T C ID; 0 £ > <& / INITIA L V VI1 D VAC . FINA L W INIT . PIT O FILTE R

FINA L PITO T DAT A 

### pa Operato r Stac k Dta . - i n Star t Tim e Sto p Tim e Orific e Coefficien

t 0 Delt a H @ Nozzl e Size/No . XA D Thermocoupl

e Im p Outle t T C ID; MiMli m | IXK I. &JfC* Operato r Stac k Dta . - i n Star t Tim e Sto p Tim e Orific e Coefficien

t 0 Delt a H @ Nozzl e Size/No . XA D Thermocoupl

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### 0***1 Operato r Stac k Dta . - i n Star t Tim e Sto p Tim e Orific e Coefficien

t 0 Delt a H @ Nozzl e Size/No . XA D Thermocoupl

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### I ' m SHK 'At .I L Fina l Pur g eRat e Operato r Stac k Dta . - i n Star t Tim e Sto p Tim e Orific e Coefficien

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e Im p Outle t T C ID; 3P1 J 1 Fina l P H h . L A MI B | | TEMPERATUR E READING S F | 1 1 % > n COMMENT S h . 0 1 T N RV M

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-



### VES01902 6

### AECO M



# UNI Tf SAMPL E TRAI N MOISTUR E RECOVER YDAT A SHEE T Referenc e Metho d / Samplin g Trai n : Recovere d b y: N

J \fo (Ho^fi-iS Recovere d by : 

### .^J7/ V \ AVUrtCtfJ ' Recovere d by : <dii * t^lWlJ " RunNo
. 

# U'-f'r U Date : |>-lltl<> f Ru n No
. U 4 —I t X - Dat e : Ru n No
. U«f-jV 3 Date :

l
. •" '—" T X A D Modul e No. : M | X A D Modul e No. : | 0 1 ft X A D Modul e No. : P
. Filte rNo. : <^\%& 0' t H>3>3 Filte rNo. : 

# *T

7 f f/ ? 

### <9,^flf Filte rNo. : "T/ rf 0 - W I m pinge rNo
. an d Volum e I m pinge rNo
. an d Volum e I m pinge rNo
. an d Volum e N o
. Initia l

(mL ) Fina l

(mL ) Rins e

(mL ) No
. Initia l (mL ) Fina l

(mL ) Rins e

(mL ) No
. Initia l (mL ) Fina l

(mL ) Rins e

(mL )
1 1 f 1 

### Sv
2 / o o 2 | o o 2 jOT J
3 /ot > 3 | 0 0 

# \ 

# \ 0 

### |T >0 1
4 0 i g o 4 0 4 0 5 /OT ) 

### 1 0 0 

### I 5 I O O J O © 5 /oe > 

# /tr o

6 1 0 0 6 l o o r 6 t o o 4 3
7 7 7 DIFF : DIFF : 7 DIFF : Total s M S o Total s 

### *f£o Total s

initia l

. (9 ) Fina l

'(B ) Initia l (g ) Fina l

(g ) Initia l (g ) Fina l

(g ) initia l

. (9 ) Fina l

'(B ) DIF F : Initia l (g ) Fina l

(g ) D l F Initia l (g ) Fina l

(g ) DIFF : Silic a G e l Silic a Ge l 

### /«. / Silic a Ge l 

### 9. 7 Fina l Ne t Moistur e Gain : 

### 55 5 Fina l Ne t Moistur e Gain : Fina l Ne t Moistur e Gain : CADocument s an d Seitings\mllos\Desktop\(MoistiJre Recovery.xls] A



### VES01902 7Metho d 0023 A



### VES01902 8

### PCD D Veoli i ! PCD F Emi j Metho d ( Ru n No
. 

### i

E S Technica l £ ssio n Result s - 1 )023 A Samplin g

1 (Olution s 

### "E Q Basi s - Fron t Parameter s 2 

### Hal f
3 Dat e Start Tim e Sto p Tim e 16-Dec-0 9 13:5 4 16:5 9 17-Dec-0 9 12:3 0 15:3 5 18-Dec-0 9 11:4 5 14:5 0 Unit s Sampl e Volum e dsc f 137.45 5 131.66 7 131.71 7 Sampl e Volum e m 3 3.8 9 3.7 3 3.7 3 Moisture Conten t % v/ v 35. 6 36. 4 36. 0 0 2 Concentratio n % v/ v(dry) 12.6 0 12.4 0 12.3 0 C 0 2Concentratio n % v/ v(dry) 5.6 6 4.8 7 5.5 4 Isokinetic s % 10 0 101 9 9 Stac k Flowrate dscf m 18,60 1 17,66 5 18,00 2 PCDD/PCD F Parameter s T E F (a ) p g ng/m 3

TE Q P

9 ng/m 3

TE Q pg ng/m 3 T E Q 2 ,3 ,7 ,8-TCD D 1.0 0 0.3 3 8.3E-0 5 0.5 7 1.5E-0 4 0.3 8 1.0E-0 4 1,2 ,3 ,7 ,8-PeCD D 0.5 0 14. 1 1.8E-0 3 12. 9 1.7E-0 3 17. 7 2.4E-0 3 1,2 ,3,4 ,7 ,8-HxCD D 0.1 0 22. 3 5.7E-0 4 20. 5 5.5E-0 4 27. 0 7.2E-0 4 1,2 ,3,6 ,7 ,8-HxCD D 0.1 0 64. 5 1.7E-0 3 62. 5 1.7E-0 3 84. 3 2.3E-0 3 1,2 ,3 ,7 ,8 ,9 -HxCD D 0.1 0 37. 2 9.6E-0 4 28. 6 7.7E-0 4 41. 3 1.1E-0 3 1,2 ,3,4,6 ,7 ,8-HpCD D 0.0 1 36 4 9.4E-0 4 35 2 , 9.4E-0 4 51 5 1.4E-0 3 OCD D 0.00 1 .263 6.8E-0 5 27 6 7.4E-0 5 37 7 1.0E-0 4 2 ,3 ,7 ,8-TCD F 0.1 0 3.6 6 9.4E-0 5 3.6 6 9.8E-0 5 4.8 5 1.3E-0 4 1,2 ,3 ,7 ,8-PeCD F 0.0 5 6.4 7 8.3E-0 5 6.5 7 8.8E-0 5 9.7 8 1.3E-0 4 2 ,3,4 ,7 ,8-PeCD F 0.5 0 30. 1 3.9E-0 3 26. 4 3.5E-0 3 45. 3 6.1E-0 3 1,2 ,3,4 ,7 ,8-HxCD F 0.1 0 17. 8 4.6E-0 4 17. 9 4.8E-0 4 28. 4 7.6E-0 4 1,2 ,3,6 ,7 ,8-HxCD F 0.1 0 24. 4 6.3E-0 4 24. 0 

### I 6.4E-0 4 36, 3 9.7E-0 4 2 ,3,4,6,7,8-HxCD F 0.1 0 64. 4 1.7E-0 3 61. 0 1.6E-0 3 99. 1 2.7E-0 3 1,2 ,3 ,7 ,8 ,9 -HxCD F 0.1 0 10. 9 2.8E-0 4 10. 4 2.8E-0 4 15. 8 4.2E-0 4 1,2 ,3,4,6,7,8-HpCD F 0.0 1 90. 0 2.3E-0 4 91. 6 2.5E-0 4 13 7 3.7E-0 4 1,2 ,3,4 ,7 ,8 ,9 -HpCD F 0.0 1 20. 9 5.4E-0 5 21. 4 5.7E-0 5 33. 5 9.0E-O 5 OCD F 0.00 1 44. 7 1. 1 E-0 5 i o rn o 47. 0 1.3E-0 5 68. 1 1.8E-0 5 o n cn o X\J l^Lu JLJCfV£

S ^Ug/U l ) — TOTA LTEQ s (ng/m 3@ 7 % 0 2 ) 1 .oc-u z 2.2E-0 2 2.1E-0 2 3.2E-0 2 TOTA LTEQ s (g/s ) 1.2E-1 0 1.1E-1 0 1.7E-1 0 (a ) U.S.EP A(1989 ) Toxi cEquivalenc yFacto r

S:\_JOB\2009WeoliaVres t DataUJni t 4\[unit4_M0023A_0. 4 slandard.xlslTEQS-F H



### VES01902 9

### Veoli a PCD D / PCD F Emi s Metho d 0 E S Technica l S

.sio n Result s - 1 023 A Samplin g olution s

E Q Basi s - Bac k

Hal f Parameter s Ru n No . 1 2 3 Dat e 16-Dec-0 9 17-Dec-09 18-Dec-0 9 Star t Tim e 13:5 4 12:3 0 11:4 5 Sto p Tim e 1 Init c 16:5 9 15:3 5 14:5 0 Sampl e Volum e unit s dsc f 137.45 5 131.66 7 131.71 7 Sampl e Volum e m 5 3.8 9 3.7 3 3.7 3 Moisture Conten t % v/ v 35. 6 36. 4 36. 0 0 2 Concentratio n % v/ v(dry ) 12.6 0 12.4 0 12.3 0 C 0 2Concentratio n % v/ v(dry ) 5.6 6 4.8 7 5.5 4 Isokinetic s 

### % 100 10 1 9 9 Stac k Flowrat e dscf m 18,60 1 17,66 5 18,00 2 PCDD/PCD F Parameter s TE F (a ) p g 'rig/m 3

TE Q p g ng/m 3 TE Q p g ng/m 3 T E Q 2 ,3,7,8-TCD D 1.00 18. 5 4.8E-0 3 24. 0 6.4E-0 3 I 20. 3 5.4E-0 3 1,2 ,3 ,7 ,8-PeCD D 0.5 0 27 5 3.5E-0 2 32 7 4.4E-0 2 29 3 3.9E-0 2 1,2 ,3,4 ,7 ,8-HxCD D 6.1 0 29 8 7.7E-0 3 26 6 7.1E-0 3 25 9 6.9E-0 3 1,2 ,3,6 ,7 ,8-HxCD D 6.1 0 85 9 2.2E-0 2 79 1 2.1E-0 2 81 7 2.2E-0 2 1,2 ,3 ,7 ,8,9-HxCD D 0.1 0 34 1 [ 8.8E-03 25 6 6.9E-0 3 347 9.3E-0 3 1 ,2,3,4,6,7,8-HpCD D 0.0 1 2,58 0 6.6E-0 3 2,09 0 5.6E-0 3 2,38 0 6.4E-0 3 OCD D 0.00 1 98 5 2.5E-0 4 71 1 1.9E-0 4 81 2 2.2E-0 4 2 ,3,7,8-TCD F 0.1 0 86. 5 2.2E-0 3 83. 8 2.2E-0 3 85. 5 2.3E-0 3 1,2 ,3 ,7 ,8-PeCD F 0.0 5 12 6 1.6E-0 3 11 2 1.5E-0 3 141 1.9E-0 3 2 ,3,4 ,7 ,8-PeCD F 0.5 0 57 8 7.4E-0 2 48 4 6.5E-0 2 64 7 8.7E-0 2 1,2 ,3,4 ,7 ,8-HxCD F 0.1 0 264 6.8E-0 3 22 4 6.0E-0 3 26 3 7.1E-0 3 1,2 ,3,6 ,7 ,8-HxCD F 0.1 0 34 3 8.8E-0 3 26 8 7.2E-0 3 34 3 9.2E-0 3 2 ,3,4,6 ,7 ,8-HxCD F 0.1 0 79 6 2.0E-0 2 55 4 1.5E-0 2 74 9 2.0E-0 2 1,2 ,3 ,7 ,8,9-HxCD F 0.1 0 8 6 2.2E-0 3 45. 9 1.2E-0 3 70. 8 1.9B0 3 1 ,2,3,4,6,7,8-HpCD F 0.0 1 86 7 2.2E-0 3 63 8 1.7E-0 3 87 0 2.3E-0 3 1,2 ,3,4 ,7 ,8,9-HpCD F 0.0 1 11 1 2.9E-0 4 57. 5 1.5E-0 4 96. 6 2.6E-0 4 OCD F 0.00 1 16 5 4.2E-0 5 85. 9 2.3E-0 5 135 3.6E-0 5 TOTA L TEQ s (ng/m 3 ) = T O T A T TI H O C Cna/m 3fil 1 0/ . n 1 = 0.20 4 0 3d 1 0.19 1 O ^1 1 0.22 1 0 35 6 TOTA L TEQ s (g/s ) 1.8E-0 9 Uat ) 1 1 1.6E-0 9 1.9E-0 9 (a ) U.S.EP A(1989 ) Toxi cEquivalenc yFacto r

S:t_JOBE009Weolia\Tes l DataUJni t 4\[uniM_M0023A_O..< ! standard.xIsJTEQS-F H



### VES01903 0

### Veoli a E S Technica l Solution s Rotary Kil n Incinerato r # 4 Metho d 0023 A Samplin g Parameter s Ru n No . 1 16-Dec-0 9 13:5 4 16:5 9 2

17-Dec-0 9 12:3 0 15:35 3

18-Dec-0 9 11:4 5 14:5 0 AVG S Dat e 1 16-Dec-0 9 13:5 4 16:5 9 2

17-Dec-0 9 12:3 0 15:35 3

18-Dec-0 9 11:4 5 14:5 0 AVG S Start Tim e j Unit s 1 16-Dec-0 9 13:5 4 16:5 9 2

17-Dec-0 9 12:3 0 15:35 3

18-Dec-0 9 11:4 5 14:5 0 AVG S Sto p Tim e 1 16-Dec-0 9 13:5 4 16:5 9 2

17-Dec-0 9 12:3 0 15:35 3

18-Dec-0 9 11:4 5 14:5 0 AVG S Nozzl e Diamete r inche s 0.30 7 30.2 0 180. 0 130.65 7 0.30 7

30.0 0 180. 0 128.873 0.30 7

29.6 5 180. 0 131.25 3 0.30 7 Barometri c Pressur e in . H g 0.30 7 30.2 0 180. 0 130.65 7 0.30 7

30.0 0 180. 0 128.873 0.30 7

29.6 5 180. 0 131.25 3 29.9 5 Ne t Samplin g Tim e min . 0.30 7 30.2 0 180. 0 130.65 7 0.30 7

30.0 0 180. 0 128.873 0.30 7

29.6 5 180. 0 131.25 3 180. 0 Volum e Metere d dc f 0.30 7 30.2 0 180. 0 130.65 7 0.30 7

30.0 0 180. 0 128.873 0.30 7

29.6 5 180. 0 131.25 3 130.26 1 Avg . DG M Temp . ° F 44. 2 55. 6 58. 9 52. 9 Av g Delt a H i n H 2 0 1.80 1.69 1.75 1.75 Av g Delt a H in . H g 0.132 5 0.124 5 0.128 5 0.128 5 DG M Calibratio n Facto r — 0.991 0 0.991 0 0.991 0 0.991 0 Ga s Sampl e Volum e dsc f 137.45 5 131.66 7 131.71 7 133.61 3 Tota l Wate r Collecte d ml " 1613. 0 1595. 1 1569. 5 1592. 5 Volum e ofWate r Vapo r sc f 76.05 3 75.20 9 74.00 2 75.08 8 Moistur e (measured ) % v/ v 35. 6 36. 4 36. 0 36. 0 Moistur e ( @ saturation ) %v/ v 99. 2 99. 9 101. 0 

### loo. o Dry Mol e Fraction , 100-% M 

# - 0.643 8 0.636 5 0.640 3 0.640 2 C O za t Stac k %dr y 5.6 6 12.6 0 4.8 7

12.40 5.5 4

12.3 0 5.3 6 0 2 at Stac k %dr y 5.6 6 12.6 0 4.8 7

12.40 5.5 4

12.3 0 12.4 3 C O + N 2 %dr y 81.7 4 i 82.7 3 82.1 6 82.2 1 Dry Molecula rWeigh t lb/fb-mol e 29.4 1 ' 29.2 8 f29.3 8 29.3 5 We t Molecula rWeigh t Ib/lb-mol e 25.35 25.1 8 I 25.2 9 .25.2 7 Exces s Ai ra

t Stac k % 140. 3 131. 3 131. 0 134. 2 Stac k Diamete r inche s 48. 0 48. 0 48. 0 48. 0 i Stac k

Are a sq . in . 1809. 6 1809. 6 1809. 6 1809. 6 Stati c Pressur e i n H 2 0 -0.4 8 -0.5 0 -0.4 6 -0.4 8 Stac k Pressur e in . H g 30.1 6 29.9 6 29.6 2 29.9 1 i Avg . Stac k

Temp . ° F 389. 4 389. 2 391. 8 390. 1 r Avg . Sqroo t o fDelt a P — 0.807 7 0.775 9 0.793 4 0.792 3 I SD E Averag e — 23.54 0 22.60 9 23.15 6 23.10 2 Pitot Coefficien t 

# - 0.8 4 0.8 4 6.8 4 0.8 4 Stac k Ga s Velocity afp m 3,66 9 3,54 7 3,64 6 j 3,62 1 Stac k Flowrate wet acf m 46,10 1 44,57 6 45,82 2 45,50 0 Stac k Flowrate we t scf m 28,89 2 27,75 6 28,11 7 28,25 5 Stac k Flowrat e dscf m j 

### i"8V6"6" l 17,66 5 18,00 2 18,08 9 Isokinetic s % 1 10 0 10 1 9 9 10 0 Mete rBo xNo . — 2 1.801 0 2

1.801 0 2

1.801 0 — Delt a H @ 1 in . H g 2 1.801 0 2

1.801 0 2

1.801 0 ~ Fiel d Q A Yg c — 0.99 7 0.99 6 1.00 1 0.99 8 [Deviation ] Pre- Y % 0.6 % 0.5 % 1.0% 0.7 % S:\_JO8\2009Weolia\Tes t DataUJni t 4\[unit4_MQ023A_0. 4 slandard.xls]DAT A



### VES01903 1Metho d 0023 A Samplin g Parameter s P T R U N 1AVGS - - PCDDs / PCDF s R U N 2 AVG S - PCDDs/PCDF s R U N 3 AVG S - PCDDs/PCDF s P T D P SQR T

D P DG M

I N DG M

OU T D H STAC K

TEM P D P SQR T D P DG M

I N DG M

OU T D H STAC K

TEM P D P SQR T D P DG M

I N DG M

OU T D H STAC K

TEM P a 1 0.7 0 0.836 7 4 0 4 2 1.90 39 2 0.64 0.800 0 4 9 5 2 1.7 5 38 9 0.6 3 0.793 7 6 7 6 7 1.7 5 39 2 1 0.6 S 0.824 6 4 0 4 5 1.9 0 38 8 0.6 4 0.800 0 5 0 5 6 1.7 5 38 7 0.6 0 0.774 6 6 6 6 9 1.6 5 39 2 a 2 0.6 5 0.806 2 4 1 4 7 1.8 0 38 8 0.6 6 0.812 4 5 1 5 7 1.8 0 38 9 0.6 3 0.793 7 6 5 6 8 1.7 5 39 5 2 0.6 8 0.824 6 4 1 4 7 1.90 39 0 0.6 6 0.812 4 5 1 5 7 1.8 0 39 0 0.6 3 0.793 7 64 6 6 1.7 5 39 3 a 3 0.7 2 0.848 5 4 1 4 7 2.0 0 39 0 0.6 4 0.800 D 5 1 5 7 1.7 5
. 39 2 0.6 5 0.806 2 6 2 6 5 1.8 0 39 3 3 0.6 8 0.824 6 4 1 4 7 1.90 38 9 0.6 2 0.7874 5 1 5 7 1.70 39 1 0.6 8 0.624 6 6 1 6 3 1.9 0 39 4 a 4 0.7 3 0.8544 4 2 4 7 2.0 0 38 9 0.6 4 0.800 0 5 1 57 1.7 5 39 1 0.6 5 0.806 2 5 9 6 3 1.8 0 39 3 4 0.7 0 0.836 7 4 2 4 7 1.90 39 0 0.7 0 0.836 7 5 2 5 7 1.90 39 1 0.6 5 0.806 2 5 8 6 2 1.8 0 39 3 a S 0.6 7 0.818 5 4 3 4 8 1.8 5 39 1 0.6 0 0.774 6 5 2 5 7 1.65 38 9 0.6 0 0.774 6 5 7 6 1 1.6 5 39 2 5 0.6 5 0.806 2 4 3 4 8 1.8 0 39 0 0.6 5 0.806 2 5 2 5 8 1.8 0 38 9 0.6 5 0.806 2 5 6 5 9 1.8 0 39 1 a 6 0.5 7 0.755 0 4 2 4 8 1.55 38 7 0.5 0 0.707 1 5 3 5 8 1.4 0 38 5 0.4 5 0.670 8 5 5 5 9 1.2 5 39 0 6 0.5 5 0.741 6 4 2 4 8 1.50 38 7 0.5 0 0.707 1 5 3 5 9 1.40 38 3 0.4 5 0.670 8 5 4 5 8 1.2 5 39 0 b 1 0.7 0 0.836 7 4 2 4 7 1.9 0 38 6 0.6 2 0.7874 5 4 5 7 1.7 0 39 0 0.6 5 0.806 2 5 3 5 7 1.8 0 39 0 1 0.7 0 0.836 7 4 2 4 7 1.90 39 1 0.6 8 0.824 6 5 3 58 1,90 39 0 0.6 8 0.824 6 5 3 5 9 1.9 0 38 8 b 2 0.6 8 0.824 6 4 2 4 8 1.90 38 9 0.6 5 0.806 2 5 3 5 9 1.80 38 7 0.6 8 0.824 6 5 3 5 9 1.9 0 38 9 2 0.7 2 0.848 5 4 2 4 8 2.0 0 38 7 0.6 8 0.824 6 5 4 5 9 1.90 39 0 0.74 0.860 2 5 3 5 9 2.0 0 39 2 b 3 0.6 8 0.824 6 4 2 4 7 1.90 39 1 0.6 8 0.824 6 5 3 5 9 1.90 38 7 0.7 2 0.848 5 5 3 5 9 2.0 0 39 2 3 0.6 7 0.818 5 4 2 4 7 1.8 5 39 0 0.6 5 0.806 2 5 4 6 0 1.8 0 39 1 0.7 0 0.836 7 5 2 5 9 1.9 0 39 3 b 4 0.6 5 0.806 2 4 2 4 7 1.8 0 39 0 0.6 5 0.806 2 5 4 6 0 1.8 0 39 1 0.6 8 0.824 6 5 2 5 9 1.9 0 39 2 4 0.6 5 0.806 2 4 1 4 7 1.8 0 39 2 0.6 8 0.824 6 5 4 6 1 1.9 0 39 2 0.6 8 0.824 6 5 3 6 0 1.9 0 39 2 b S 0.6 0 0.774 6 4 1 4 6 1.6 5 39 2 0.6 0 0.774 6 5 4 6 2 1.6 5 39 0 0.6 3 0.793 7 5 3 6 0 1.7 5 39 2 5 0.6 0 0.774 6 4 1 4 7 1.6 5 39 0 0.4 0 0.632 5 5 5 6 3 1.6 5 39 0 0.6 3 0.793 7 5 3 6 0 1.7 5 39 2 b 6 0.5 3 0.728 0 4 1 4 7 1.4 5 38 8 0.4 0 0.632 5 5 5 6 3 1.1 0 38 9 0.5 5 0.741 6 5 3 5 9 1.5 0 39 2 6 0.5 3 0.728 0 4 1 4 7 1.4 5 38 8 0.4 0 0.632 5 5 6 6 3 1.1 0 38 8 0.5 5 0.741 6 5 4 6 0 1.5 0 39 0
A V G 0.6 5 0.807 7 44. 2 1.8 0 38 9 0.6 1 0.775 9 55. 6 1.6 9 38 9 0.6 3 0.793 4 58. 9 1.7 5 39 2



### VES01903 2

### AECOM Samplin g Train fY[ 

## EP A ISOKINETI C SAMPLIN G - FIEL D DAT A SHEE T
Ru n Numbe r Clien t Veoli

a E S Technica l Solution s Facilit y Locatio n Sourc e U>t e Operato r Stac k Dia . - in. SUr t Tim e Slo p Tim e Sauget

, IL . ( I N r t # 4 : 

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### VES01903 3\
AECO M 

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a E S Technica

l Solution s Facilit y Locatio n Sourc e __ _ Dat e Operato r Stac k Dia . - in. Siar t Tim e Sto p Tim e Sauget

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t Q. Filte r Bo xNo . Mete r Bo xNo . Orific e Coefficien

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VES01903 4

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r Client Barometri c Pressur e Stati c Pressur

e (+/- ) Veoli a E S Technica l Solutions Facilit y Locatio n Sourc e Dat e Operato r___

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### VES01903 5

# AECOM

SAMPL E TRAI N MOISTUR E RECOVER YDAT A SHEE T Heferenc e Metho d /

Samplin g Trai n : Ih 2 $ J s Recovere d by : of fto /Hdjt ^l i Recovere d by : ^fift v'fH'tffli- / Recovere d b y: 

### (ft Av 0 Ru n No
. Utf - " ( Da t e : |^/|fc (» f Ru n No
. U^'P " Date. : (>//?/ a f Ru n No
. Date : ^^/" ? XA. D Modul e No. : 

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## rVv~cjW« ( <sf Filte rNo. : Filte rNo. : tV e-C l eewwJ L fi- F I m pinge rNo
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# (g ) lliillillPll s Initial
.



# (g ) Fina l 

# (g ) I Initia l 

# (g ) Fina l 

# (g ) DIFF : ' N Initia l



# (g ) Fina l 

# (g ) DIF F lliillillPll s Initial
.



# (g ) Fina l 

# (g ) DIFF : a G e l Silic a G e l Silic a Ge l 

### 3 f U ? Fina l Ne t Moistur e Gain : Fina l Ne t Moistur e Gain : Fina l Ne t Moistur e Gain : C:\Document s an d Seltings\milos\Desktop\[Moisture Recovery.xls] A

•US C Do^bl t col l 

### t*>nk**i *Jrf falls' 

# 'l^ktsp+fify ~ fvUrWH* - 01* 3 S" S 7

-{^vr X 

### VES01903 6

# Metho d 25 A

VES01903 7

### AVERAGE D CE M DAT A Jo b Number : 

### 60133216 Star t Time : 

### 14:07:00 R u n ID : R1B Star t Date : 12/16/09 Dat e Tim e ~ TH C 12/16/200 9 14:09:0 0 0.5 6 12/16/200 9 14:11:0 0 0. 5 12/16/200 9 14:13:0 0 0.5 6 12/16/200 9 14:15:0 0 0.4 7 12/16/200 9 14:17:0 0 0.4 8 12/16/200 9 14:19:0 0 0.4 2 12/16/200 9 14:21:0 0 0.3 9 12/16/200 9 14:23:0 0 0.4 2 12/16/200 9 14:25:0 0 0.4 6 12/16/200 9 14:27:0 0 0.4 4 12/16/200 9 14:29:0 0 0. 4 12/16/200 9 14:31:0 0 0.3 1 12/16/200 9 14:33:0 0 0.4 2 12/16/200 9 14:35:0 0 0.3 2 12/16/200 9 14:37:00
. 0.3 7 12/16/200 9 14:39:0 0 0.2 4 12/16/200 9 14:41:0 0 0.1 9 12/16/200 9 14:43:0 0 0.2 4 12/16/200 9 14:45:0 0 0.2 4 12/16/200 9 14:47:0 0 0.2 9 12/16/200 9 14:49:0 0 0.2 8 12/16/200 9 14:51:0 0 0.3 1 12/16/2009
. 14:53:0 0 0.2 9 12/16/200 9 14:55:0 0 0.3 4 12/16/200 9 14:57:0 0 0.4 3 12/16/200 9 14:59:0 0 0. 6 12/16/200 9 15:01:0 0 0.6 3 12/16/200 9 15:03:0 0 0.7 3 12/16/200 9 15:05:0 0 0.7 5 12/16/200 9 15:07:0 0 0.7 2 Averag e Value : 0.4 3 Correcte d Average : .5 2


### VES01903 8

### AVERAGE D CE M DAT A Jo bNumber : 

### 60133216 Star t Time : 

### 12:51:00 R u n ID : R2B Star t Date : 12/17/09 Dat e Tim e T H C 12/17/200 9 12:53:0 0 0.3 5 12/17/200 9 12:55:0 0 0.4 3 12/17/200 9 12:57:0 0 0.4 9 12/17/200 9 12:59:0 0 0.4 5 12/17/200 9 13:01:0 0 0.4 5 12/17/200 9 13:03:0 0 0.5 2 12/17/200 9 13:05:0 0 0.5 4 12/17/200 9 13:07:0 0 0.5 7 12/17/200 9 13:09:0 0 0. 6 12/17/200 9 13:11:0 0 0.5 7 12/17/200 9 13:13:0 0 0.5 2 12/17/200 9 13:15:0 0 0.4 3 12/17/200 9 13:17:0 0 0.5 2 12/17/200 9 13:19:0 0 ! 0.5 2 12/17/200 9 13:21:0 0 j 0.5 1 12/17/200 9 13:23:0 0 ' 0.5 3 12/17/200 9 13:25:0 0 0.4 7 12/17/200 9 13:27:0 0 0.5 1 12/17/200 9 13:29:0 0 0.5 2 12/17/200 9 13:31:0 0 0.5 1 12/17/200 9 13:33:0 0 0.4 5 12/17/200 9 13:35:0 0 0.5 1 12/17/200 9 13:37:0 0 0.5 7 12/17/200 9 13:39:0 0 0.5 1 12/17/200 9 13:41:0 0 0.5 1 12/17/200 9 13:43:0 0 0.5 1 12/17/200 9 13:45:0 0 0.5 3 12/17/200 9 13:47:0 0 0.4 9 12/17/200 9 13:49:0 0 0.4 9 12/17/200 9 13:51:0 0 0. 5 Averag e Value : 0. 5 Correcte d Average : .5 5


### VES01903 9j /



### AVERAGE D CE M DAT A Jo b Number : 

### 60133216 Star t Time : 

### 11:45:00 R u n ID : R3B Star t Date : 12/18/09
Dat e Tim e T H C 12/18/200 9 11:47:0 0 0.1 4 12/18/200 9 11:49:0 0 0.0 6 12/18/200 9 11:51:0 0 0.1 2 12/18/200 9 11:53:0 0 0.1 3 12/18/200 9 11:55:0 0 0.1 6 12/18/200 9 11:57:0 0 0.1 5 12/18/200 9 11:59:0 0 0.1 3 12/18/200 9 12:01:0 0 0.1 6 12/18/200 9 12:03:0 0 0.1 8 12/18/200 9 12:05:0 0 0.1 7 12/18/200 9 12:07:0 0 0.1 7 12/18/200 9 12:09:0 0 0.1 5 12/18/200 9 12:11:0 0 0.1 5 12/18/200 9 12:13:0 0 0.1 2 12/18/200 9 12:15:0 0 0.1 5 12/18/200 9 12:17:0 0 j 0.1 4 12/18/200 9 12:19:0 0 0.1 1 12/18/200 9 12:21:0 0 0.0 4 12/18/200 9 12:23:0 0 0.1 5 12/18/200 9 12:25:0 0 0.1 7 12/18/200 9 12:27:0 0 0.1 9 12/18/200 9 12:29:0 0 0.2 1 12/18/200 9 12:31:0 0 0.1 8 12/18/200 9 12:33:0 0 0.1 2 12/18/200 9 12:35:0 0 0.1 9 12/18/200 9 12:37:0 0 0.0 9 12/18/200 9 12:39:0 0 0.1 4 12/18/200 9 12:41.0 0 0.1 2 12/18/200 9 12:43:0 0 0.1 4 12/18/200 9 12:45:0 0 0.1 8 Averag e Value : 0.1 4 Correcte d Average : . .2 4


### VES01904 0

### o

VES01904 1

# AECOM

Appendix C Referenc e Metho d Calibrations , Verifications , an d Certification s ^

(... )



### VES01904 2

# AECOM

Calibrator : MikeO'tool e Referenc e Thermometer: SYR-CAL- 1 | Filte rBo xCalibratio n Ho t Bo x#

5 Ho t Bo x#8 D Manufacturer : Anderso n NUTEC H Seria l No. : N/ A Dat e received/olace

d i n servi c Pr

e 199 5 Manufacturer : Anderso n NUTEC H

Seria l No. : N/ A Dat e received/place

d i n servi o Pr

e 199 5 Calibratio n Date : 8-Jan-0 9 Calibratio n Date : 8-Jan-0 9 Referenc e Temperature

s Actua l Temperature

s Tem p Differenc

e (tol . = +-2

) Ambien t Ho t Referenc e Temperature

s Actual Temperature

s Tem p Differenc

e (tol . = +-2

) Ambien t Ho t Referenc e Temperature

s Actua l Temperature

s Tem p Differenc

e (tol . = +-2

) 6

7 25

0 Referenc

e Temperature

s Actual Temperature

s Tem p Differenc

e (tol . = +-2

) 6

9 25

0 Referenc e Temperature

s Actua l Temperature

s Tem p Differenc

e (tol . = +-2

) 6

6 24

9 Referenc

e Temperature

s Actual Temperature

s Tem p Differenc

e (tol . = +-2

) 6

9 24

9 Referenc e Temperature

s Actua l Temperature

s Tem p Differenc

e (tol . = +-2

) 1 1 Referenc e Temperature

s Actual Temperature

s Tem p Differenc

e (tol . = +-2

) 0 1 Ho t B < JX # 6 Ho t Bo x# 9 Manufacturer : Anderso n NUTEC H Seria l No. : N/ A Dat e received/place

d i n servi c Pr

e 199 5 Manufacturer : Anderso n NUTEC H

Seria l No. : N/ A Dat e received/place

d i n servi o Pr

e 199 5 Calibratio n Date : 8-Jan-0 9 Calibratio n Date : 8-Jan-0 9 Referenc e Temperature

s Actua l Temperature

s Tem p Differenc

e (tol . = +-2

) Ambien t Ho t Referenc e Temperature

s Actual Temperature

s Tem p Differenc

e (tol . = +-2

) Ambien t Ho t Referenc e Temperature

s Actua l Temperature

s Tem p Differenc

e (tol . = +-2

) 6

9 25

0 Referenc

e Temperature

s Actual Temperature

s Tem p Differenc

e (tol . = +-2

) 6

8 25

1 Referenc e Temperature

s Actua l Temperature

s Tem p Differenc

e (tol . = +-2

) 6

9 25

0 Referenc

e Temperature

s Actual Temperature

s Tem p Differenc

e (tol . = +-2

) 6

8 25

0 Referenc e Temperature

s Actua l Temperature

s Tem p Differenc

e (tol . = +-2

) 0 0 Referenc e Temperature

s Actual Temperature

s Tem p Differenc

e (tol . = +-2

) 0 1 Ho t Bo x#

7 Ho t Bo x#1 0 Manufacturer : Anderso n NUTEC H Seria l No. : N/ A Dat e received/place

d i n servi c Pr

e 199 5 Manufacturer : Anderso n NUTEC H

Seria l No. : N/ A Dat e received/place

d i n servi o Pr

e 199 5 Calibratio n Date : 8-Jan-0 9 Calibratio n Date : 8-Jan-0 9 Referenc e Temperature

s Actua l Temperature

s Tem p Differenc

e (tol . = +-2

) Ambien t Ho t Referenc e Temperature

s Actual Temperature

s Tem p Differenc

e (tol . = +-2

) Ambien t Ho t Referenc e Temperature

s Actua l Temperature

s Tem p Differenc

e (tol . = +-2

) 6

8 25

0 Referenc

e Temperature

s Actual Temperature

s Tem p Differenc

e (tol . = +-2

) 7

1 25

0 Referenc e Temperature

s Actua l Temperature

s Tem p Differenc

e (tol . = +-2

) 6

9 24

9 Referenc

e Temperature

s Actual Temperature

s Tem p Differenc

e (tol . = +-2

) 7

1 25

0 Referenc e Temperature

s Actua l Temperature

s Tem p Differenc

e (tol . = +-2

) -

1 1 Referenc e Temperature

s Actual Temperature

s Tem p Differenc

e (tol . = +-2

) 0 0 Ho t Be )X #7 A Ho t Bo x#1 1 Manufacturer : Anderso n NUTEC H Seria l No. : N/ A Dat R rHCBived/Dlace d i n servi c Pr e 199 5 Manufacturer : Anderso n NUTEC H

Seria l No. : N/ A Dat e received/place

d i n servi o Pr

e 199 5 Calibratio n Date : 8-Jan-0 9 Calibratio n Date : 7-Jan-0 9 Referenc e Temperature

s Actua l Temperature

s Tem p Differenc

e (tol . = +-2

) Ambien t Ho t Referenc e Temperature

s Actual Temperature

s Tem p Differenc

e (tol . = +-2

) Ambien t Ho t Referenc e Temperature

s Actua l Temperature

s Tem p Differenc

e (tol . = +-2

) 6

9 25

0 Referenc

e Temperature

s Actual Temperature

s Tem p Differenc

e (tol . = +-2

) 7

0 25

1 Referenc e Temperature

s Actua l Temperature

s Tem p Differenc

e (tol . = +-2

) 6

9 24

9 Referenc

e Temperature

s Actual Temperature

s Tem p Differenc

e (tol . = +-2

) 6

9 25

0 Referenc e Temperature

s Actua l Temperature

s Tem p Differenc

e (tol . = +-2

) 0 1 Referenc e Temperature

s Actual Temperature

s Tem p Differenc

e (tol . = +-2

) 1 1 Ho t E o x#

8 Manufacturer : Anderso n NUTEC H Seria l No. : N/ A Dat e received/oiace

d i n servi c Pr

e 199 5 Calibratio n Date : 8-Jan-0 9 Referenc e Temperature

s Actua l Temperature

s Tem p Differenc

e (tol . = +-2

) Ambien t Ho t Referenc e Temperature

s Actua l Temperature

s Tem p Differenc

e (tol . = +-2

) 6

9 25

0 Referenc e Temperature

s Actua l Temperature

s Tem p Differenc

e (tol . = +-2

) 6

9 24

8 Referenc e Temperature

s Actua l Temperature

s Tem p Differenc

e (tol . = +-2

) 0 2 Checke d amp h connector , t-coupl e an d plug s Q C checke

d b yS Milo 2/9/0

9



### VES01904 3

### AICO M DR YGA S METE R CALIBRATIO N Mete rBo xNo. : Chec k one : Annua l Calibratio n Recalibratio n Date : 7/10/200 9 Operator : S . Mil o Barometri c Pressure : 29.6 1 (i n Hg ) Theoretica l Critica l Vacuum : 14.0 6 (i n Hg ) Manufacturer: Environmental Suppl y Dat e Received/Place

d i n service : 200 2 Seria l No. ; 2 Pretes t Lea k Check s Allowabl e Actua l Positiv e 0 i 0.0 0 (a t 5-7ln.H : 0 ) In. Hj O pe rmin . Negativ e 0 0.00 0 Ca t 3 In. Hg

) cf

m cf

m

DR YGA S METE R DAT A CRITICA L ORIFIC E DAT A Volume * Tern P Critica l K'Orific e Actual Ambien t Temperatur

e Tim e Initia

l Final Total Initia l Fina l Orific e Callbratio

r Vacuu m Initia l Final Averaq e (i n H 2 0 ) (min

) <ft J ) (te i (ft 1) ° F * F Seria l # Coefficien t fln-Hg) " F • F " F 0.2 9 2 0 0.05 O 6.37 8 6.32 8 7 1 7 3 4 0 0.24 0 2 4 7 0 7 1 7 1 0.6 4 1 5 6.40 2 13.32 5 6.92 3 72 7 6 4 8 0.35 0 22. 5 72 7 2 72 1.1 5 1 5 13.39 6 22.53 3 9.13 7 7 5 7 7 5 5 0.46 0 2 1 7 3 72 ' 7 3 1.9 0 1 0 22.57 7 30.45 1 7.87 4 7 7 7 9 6 3 0.59 4 1 9 7 3 72 7 3 3.7 0 1 0 30.50 7 41.27 1 10.76 4 7 8 3 2 7 3 0.80 9 1 6 7 3 7 4 7 4

CORRECTE D VOLUM E Dr y Gas Meter V m (st d ft

3 ) Critica l Orific e Ve r(st d ft" ) DR

YGAS METE R CALIBRATIO N FACTO R Y DRYGA S METE R CALIBRATIO

N FACTO R AH @ 6.25 9 . 6.21 2 0.99 3 0.00 1 1.69 1 -0.11 1 6.33 1 6.77 9 0.99 2 0.0 0 1.76 2 -0.03 9 8.98 9 8.91 9 0.99 2 0.0 0 1.83 0 0.02 8 7.73 2 7.66 8 0.99 2 0.0 0 1.81 8 0.0 2 10.58 2 10.44 6 0.98 7 0.0 0 1.90 7 0.1 1

1 ) Forvali d tes

t rasults , th

e Actual Vacuu m shoul

d b e 1 t o 2 in . H g greaterthan th e Theoretica l Critica l Vacuu m show n above . 2 ) Th e Critica l Orific

e Coefficient , K, mus

t b e entere d i n Englis h units, (ft) A 3*(de g R)

A 0.5/(fln.Hgnrr.iri)) . 3 ) Th e minimu m numbe

ro fsample volum

e require d pe rorific

e i s 5 cubi c feet 4 ) Fo rCalibratio n Facto rY , the rati o o fthe reading o

fthe calibration meter t

o th e dr y gas meter

, acceptabl

e toleranc

e o findividual value

s fro m th e averag e i s ±0.0 2 5 ) ForOrific

e Calibratio n Facto rAH@ , th e orific e differential pressur

e i n inche

s o fH 2 0 lha t equate s t o 0.7 5 cfm o fai ra t 6 3 F an d 29.9 2 inche s o fHg , acceptable toleranc

e o findividual value

s fro m th e average f

s ±0.2 .
Dr y Ga s Meter Thennocoupl e calibratio n Ref. T C ID

# RE F -SY R -TC

2 Inle t ID* : 002-I N OutletlD * 002-OU T Rer . Sourc e Ref, T • F °F A Amb . Ai r 6 5 6 6 - 1 6 6 1 Ho t Water 11 8 11 8 0 11 7 - 1 Notes : 1 ) Ho

t Wate r t o b e i n the r a igeof1Q4 - 2

2 °F . 2 ) Toleranc

e allowe d foral l thermocoupl

e individual readings : ±5. 4 ° F 3 ) Toleranc

e allowe d fo ral l potentiomete

rindividual readings : ±2 ° F Potentiomete rCalibratio n Lo w 10

0 " F 9 9 Mi d 40

0 " F 40 0 Hig h 90

0 ° F 89 9

k„t,*i=> ? - s , K)— — ^+46 0 

### tl(llJ)

VES01904 4

### AZCOM Calibrator : Date : Steve n Mil o

12/16/200

8 Referenc e Thremomete rID : CL-100 0
Last Imolrmer Thermocoupl e Calibratio n 200 7 Thermocoupl e Referenc e Difference (+/-2° ) Thermocoupl e Referenc e Differenc e (+/-2° ) LI- 1 Ho t 21 0 21 2 - 2 LI-1 8 Ho t 21 0 21 2 - 2 LI- 1 Col d 3

2 3

3 -

1 LI-1 8 Col d 3 2 3

2 0 Manufacturer: Anderson NUTEC H Manufacturer: Anderso n NUTEC H Seria l No. : Seria l No. : Dat e received/place

d i n service : Pr

e 199 0 T-coupl e 200

6 Dat e received/place

d i n service : Pr

e 199 0

, LI- 3 Ho t 21 1 21 3 -2 LI-2 0 Ho t 21 1 21 2 -1 LI- 3 Col d 3

2 3

2 0 LI-2 0 Col d 3

2 3

2 0 Manufacturer: Anderso n NUTEC H Manufacturer: Anderso n NUTEC H Seria l No. : Seria l No. : Dat e received/place

d i n service : Pr

e 199 0 Dat e received/place

d i n service : Pr

e 199 0 LI- 4 Ho t 21 2 21 3 - 1 LI-2

2 Ho t 21 3 21 2 1 LI- 4 Col d 3

2 3

2 0 LI-2 2 Col d 3

2 3

2 0 Manufacturer: Anderson NUTEC H Manufacturer: Seria l No. : Seria l No. : Dat e received/place

d i n service : Pr

e 199 0 T-coupl e 200

6 Dat

e received/place

d in service : Pr

e 199 0 LI- 8 Ho t 21 2 21 3 - 1 LI-22

A Ho t 21 0 21 2 - 2 LI- 8 Col d 32 . 3 2 0 LI-22 A Col d 3

2 3

2 0 Manufacturer: Anderson NUTEC H Manufacturer: Anderson NUTEC H Seria l Mo. : Seria l No. : Dat e received/place

d i n service : Pr

e 199 0 Dat e received/place

d in service : Pr

e 199 0 Ho t 0 LI-2 4 Ho t 21 0 21 2 - 2 Col d 0 LI-2 4 Col d 3

2 3

2 0 Manufacturer: Anderson NUTEC H Manufacturer: Anderso n NUTEC H Seria l No. : Seria l No. : Dat e received/place

d i n service : ' Pr

e 199 0 Dat e received/place

d in service : Pr

e 199 0 Ho t 0 Lt-25 Ho t 21 2 21 2 0 Col d 0 Lt-25 Col d 3 2 3

2 0 Manufacturer : Anderso n NUTEC H Manufacturer: Anderso n NUTEC H Seria l No. : Seria l No. : Dat e received/place

d i n service : Pr

e 199 0 Dat e received/place

d in service : Pr

e 199 0 LI-1 3 Ho

t 21 0 21 2 - 2 LI-2

8 Ho t 21 3 21 2 1 LI-1 3 Col d 3 3 3

2 1 LI-2 8 Col d 3

2 3

2 0 Manufacturer: Manufacturer: Anderson NUTEC H Seria l No. : Seria l No. : Dat e received

/Dlace d i n service : Pr e 199 0 Dat e received/place

d i n service : Pr

e 199 0 LI-1 5 Ho

t 21 0 21 2 - 2 LI-1 5 Col d 3 2 3

2 0 Manufacturer: Anderson NUTEC H Seria l No. : Dat e received/place

d i n service : Pr

e 199 0 Aftercalibration showe

rheads wer

e cleane d and leak

checke d Q C chec k S . Mil o



### VES01904 5Calibrator : Date : Bil l Hardy Referenc e Thremomete rID : CL-100 0 1/18/201 0 Last ImDinaer Thermocoupl e Calibratio n 200 7 Thermocoupl e Referenc e I Differenc

e (+/ - 2° ) Thermocoupl e Referenc e Differenc e (+/

- 2° ) LI-1 Ho

t 21 0 21 2 - 2 LI-2

0 Ho t 21 1 21 2 - 1 LI-1 Col d 3

2 3

2 0 LI-2 0 Col d 3

2 3

2 0 Manufacturer: Anderso n NUTEC H Manufacturer: Anderson NUTEC H Seria l No. : Seria l No. : Dat e received/place

d i n service : Pr

e 199 0 T-coupl e 200

6 Dat e received/olace

d i n service : Pr e 199 0 LI- 3 Ho t 21 2 21 2 0 LI-2 2 Ho t 21 1 21 2 - 1 LI- 3 Col d 3

2 3

2 0 LI-2 2 Col d 3

2 3

2 0 Manufacturer: Anderso n NUTEC H Manufacturer: Seria l No. : Seria l No. : Dat e received/place

d I n service : Pr

e 199 0 Dat e received/place

d i n service : Pr e 199 0 LI- 4 Ho t 21 0 21 2 - 2 L1-22

A Ho t 21 1 21 2 - 1 LI- 4 Col d 3

2 3

2 0 L1-22 A Col d 3

2 3

2 0 Manufacturer: Anderso n NUTEC H Manufacturer: Anderson NUTEC H Seria l No. : Seria l No. : Dat e received/place

d i n service : Pr

e 199 0 T-couol e 200

6 Dat e received/place

d i n service : Pr e 199 0 LI-1 3 Ho

t 21 2 21 2 0 LI-2 4 Ho t 21 1 21 2 - 1 LI-1 3 Col d 3 3 3

2 1 LI-2 4 Col d 3

3 3

2 1 Manufacturer: Manufacturer: Anderso n NUTEC H Seria l No. : Seria l No. : Dat e received/place

d i n service : Pr

e 199 0 Dat e received/place

d I n service : Pr

e 199 0 LI-1 5 Ho

t 21 1 21 2 - 1 LI-2

5 Ho t 21 0 21 2 - 2 LI-1 5 Col d 3 3 3

2 1 LI-2 5 Col d 3

3 3

2 1 Manufacturer: Anderso n NUTEC H Manufacturer: Anderson NUTEC H Seria l No. : Seria l No. : Dat e rsceived/olace

d i n service : Pr

e 199 0 Dat e received/place

d i n service : Pr e 199 0 LI-1 8 Ho

t 21 0 21 2 - 2 LI-2

8 Ho t 21 1 21 2 - 1 LI-1 8 Col d 3 3 3

2 1 LI-2 8 Col d 3

2 3

2 0 Manufacturer: Anderso n NUTEC H Manufacturer: Anderson NUTEC H Seria l No. : Seria l No. : Dat e received/place

d i n service : Pr

e 199 0 Dat e received/place

d i n service : Pr e 199 0 Afte rcalibration showe

rheads wer

e cleane d and leak

checke d Q C check

S . Milo



### VES01904 6

## AECOM SAMPL E PROB E CALIBRATION DAT A FOR M TYP E "S " PITO

TTUB E ASSEMBL

YAN D NOZZL E Thermocoupl e Calibratio n PROB E 10 : S-NM D Rtltnnc s ThamudiiW

r 1 0 ENS R RT D #213103

5 Omes a CI1000,00602220

0 Omeg a CI1000

. #0802220

0 PROB E 10 : S-NM D Rtltnnc s ThamudiiW

r 1 0 Bcgln g Wal W Tub*Flume s [M' . SOO

" • ) PROB E 10 : S-NM D

. •'.J^,\^ 1 . : FIO.K . P.ill , .*iV.-.^£««.»,-t.'i ? ' ? l*«>m»./:- . L>.-R«toTM\,-^;**TM-;*.-JiiSriTC.. . . w. . . . •.Jw;, ^ =V?-'.^''; : r'^. ^ . fc» .;p*Hi>*i" : .LV^.t'>^.^^KW^i'!i*.=e: . .. . • * - ' . .•;•.• » Data : 1/26/200 9 34 27 4 3 4 274 0 21 2 37 3 21 2 37 3 Q.

O 45 1 60 8 4 5 0 50 5 -0. 1 A m Min i TtfflMihn Q S-MS-4 D 34 27 4 34 274 0 21 2 373 21 2 373 0. 0 45 1 50 6 45 0 50 5 -0. 1 A m Min i TtfflMihn Q S-MS-4 D 3 4 27 4 34 274 0 21 2 37 3 21 2 373 0. 0 45 1 50 6 4 5 0 50 5 -0. 1 (MHM : 3 4 27

4 34 27 4 0 21 2 37 3 21 2 37 3 0. 0 45 1 50 6 45 0 50 5 -0. 1 "Pito t Tub e Calibration : ^

••8M « Indlcaiun

a lav« l pMltto

n fo r otatsmtnlne

Tth* n ealeulet

* Z . Leve l an d perpendicula r Obstructio n Damage d
a , (-10" S a,s+10" )
o 2(-10 ° £aj £+10' ) R , (-5 ° s ft, s + 5"

)

z = ATany(± s 0.125" ) W« ATan9(± £0.O3125" ) D , (3/1 6 < D, s 3/6" ) A A/2D , (1.0 5 s P A /D, £1.5 ) 0.00 0

•Pito t Tub e t o NtibjMHion :

|P i TU Xa

1 ) Plo t t o nozzl t wpa ratta n X 1* ? 2 ) Thermocoupl

e t o pito t separatio n Z >3f4 " 075 3 ) Pito t end I D prob e unio n distanc e Y »3.0 " 3.37 S
iv

_ > V •*.#{ ? j - " * .•*a ? ^grob e Ipfprjjtion ' Manufacturer

: Dat a Receive

d an d place d I n Service : [Conditio n o fProb e vrfie n place d I n service : NE

W p-e-159 5 QA/QC Chec

k Completenes

s . Legibilit y certif y tha t th e Typn S pito t tube/prob

e fD # SM5-4

D I criteri a and/o r applicabl

e desig n feature s an d I s hereb y asalflne d a pito t tub e calibratio

n facto r C„o fQ.B 4 RECONDITIONE

D (circl e one )
Accurac y _X
_

„ meet s o rexceed s al l Specifications

, Specification s _X
_ Reasonablenes s „ X ,

Certifie d bv : Slevn Mil

o 1J2B/0 9 Perwnne i (Signature/Date

) Steve n Mil o 2/18/0 9 Tea m Leade r(Signature/Date

) constructio

n oriteti i fora

n isolate d "S " typ e pito t ar e within give

n tolerance

s prescribe

d in iQualit y Assuranc

e Handboo

k fo rAi rPollutio n Measuremen

t Systems: Volum

e [II , Stationar

y Source-Spedfi

o Methods

. isweOO/R-M/OMc . Septembe r 199 4



### VES01904 7

# AECOM

A/1 5 Thermocoupl e Calibration s - 200 9 Date : 12/16/0 8 BP : 30.0 8 Referenc e Thermomete rID# : Manufacture : Dat e place d i n Service : Calibrator : Steve n Mil o Ambien t Tem p (F) : 6 5 CL-100 0 Fluk e Digita l RT D 213103 5

Fluk e Pr e 198 0
Ic e Bat h Boilin g Wate r Thermocoupl e ID # Referenc e

Tem p X A D

Tem p Tem p

Differenc e To l = + - 2 F Referenc e

Tem p X A D

Tem p Tem p

Differenc e To l = +- 2 F M5-TC 1 21 2 21 2 0 3 2 3 3 1 M5-TC 2 21 2 21 1 - 1 3 2 3 3 1 XAD- 6 3 2 3 2 0 21 3 21 2 - 1 XAD- 7 3 2 3 2 0 21 3 21 2 - 1 Q C chec k

S
. Mil o



### VES01904 8

# AECOM

MS Thermocoupl e Calibration s - 201 0 Date : 1/17/201 0 BP : 30.0 8 Referenc e Thermomete rID# : Manufacture : Dat e place d i n Service : Calibrator : Bil l Hard y Ambien t Tem p (F) : 6 5 CL-100 0 Fluk e Digita l RT D 213103 5

Fluk e Pr e 198 0
Ic e Bat h Boilin g Wate r Thermocoupl e ID # Referenc e

Tem p X A D

Tem p Tem p

Differenc e To l = +- 2 F Referenc e

Tem p X A D

Tem p Tem p

Differenc e Tol'=+- 2 F M5-TC 1 3 2 3 3 1 21 2 21 2 0 M5-TC 2 3 2 3 3 1 21 2 21 1 - 1 XAD- 6 3 2 3 2 0 21 3 21 2 - 1 XAD- 7 3 2 3 2 0 21 2 21 2 0 Q C chec k

S
. Mil o



### VES01904 9

### DAIL YCALIBRATIO N REPOR T

Date : 12/16/2009

Spa n Para m Valu e C0 2 1 1 TH C 9 Calibratio n Erro r= Syste m Bia s = Mid-Ga s Standard S.0 2 5.1 3 Analyze r

Zer o Respons e 0.01 N/ A Star t Time : 08:49:14

En d Time : 10:09:30 Analyze r Mi d Respons e 5.0 1 N/ A Zero

Ca l Erro r 0.1 % 0.0 % Methods : 3A , 6C , 7 E an d 1 0

Jo b Number : 12160 9 Mi d Ca l Erro r -0.1 % 0.0 % Syste m

Zero Respons e 0.0 3 0 . 100 % x(Analyze rRespons e - Cylinde rGa s Standard Value) / (Spa n Value

) 100 % x(Syste m Respons e - Analyze rResponse) / (Spa n Value) Fo rTH C Measurements : Calibratio n Erro r= 100 % x(Syste m Respons e - Cylinde rGas Standard Value ) / (Cylinde rGa s Standard Value ) Syste m Bia s = 100 % x(Syste m Respons e - Cylinde rGa s Standard Value) / (Spa n Value

) Syste m Mi d Respons e 5.0 8 5.1 3 Syste m

Zero Bia s 0.1 % 0.0 % Syste m Mi d Bia s 0.6 % 0.0 %



### VES01905 0

### CALIBRATIO N CHEC KREPOR T

Ru n ID : R1ADate : 12/16/2009 Star t Time : 09:44:39 E n d Time : 12:55:32 E P A Methods : 3A , 6C , 7 E an d 1 0 J o b Number : 12160 9 Analyze rAnalyze rSyste m Syste m Syste m Syste m Syste m Syste m Syste m Syste m Zer o Mi d Pre-Zero Pre-Mi d Pre-Zero Pre-Mi d Post-Zer o Post-Mi d Post-Zero Post-Mi d Para m Respons e Respons e Respons e Respons e Bia s Bia s Respons e Respons e Bia s Bia s Zero Drif t Mi d Drif

t C0 2 0.01 5.0 1 0.0

3 5.0

8 0.1 % 0.6 % 0.0

5 5.1 1 0.3 % 0.9

% 0.2

% 0.3

% TH C W

A N/

A 0 . 5.1 3 0.0 % 0.0

% -0. 1 5.1 3 -1.1 % 0.0 % -1.1 % 0.0 % Syste m Bias = 100

% x(Syste m Respons e - Analyze rResponse) / (Spa n Value

) Syste m Drift= 100

% x(Syste m Pos t Respons e - Syste m Pr e Response) /

(Spa n Value) Fo rTH C Measurements : Syste m Bias = 100

% x(Syste m Respons e - Cylinde rGa s Standard Value) / (Spa n Value

) Syste m Avg-Zer o Respons e 0.0 4 -0.0 5 Syste m

Avg-Mi d Respons e 5. 1 5.1 3



### VES01905 1

### DAIL YCALIBRATIO N REPOR T Star t Time : 

### 0B:54:24 Methods : 3A , 6C , 7 E an d 1 0

Date : 

### 12/17/2009 En d Time : 09:3 

### °:38 Jo b Number : 12170 9 Spa n Para m Valu e C0 2 1 1 TH C 9 Calibratio n Erro r= Syste m Bia s = Mid-Ga s Standard 5.0 2 5.1 3 Analyze r

Zero Respons e 0 N/ A Analyze r

Mi d Respons e 5.1 N/ A Zer o

Ca l Erro r 0.1 % -0.3% Mi d

Ca l Erro r 0.8 % -0.7 % Syste m Zer o Respons e -0.0 2 -0.03 Syste m

Mi d Respons e 5.0 8 5.0 9 Syste m

Zer o Bia s -0.2 % -0.3% Syste m

Mi d Bia s -0.2% -0.4 % 100 % x(Analyze rRespons e - CylinderGa s Standard Value) / (Spa n Value

) 100 % x(Syste m Respons e - Analyze rResponse) / (Spa n Value) Fo rTH C Measurements : Calibratio n Erro r= 100 % x(Syste m Respons e - Cylinde rGas Standard Value) / (CylinderGa s Standard Value) Syste m Bia s = ' 100 % x(Syste m Respons e - Cylinde rGas Standard Value) / (Spa n Value

)



### VES01905 2

### CALIBRATIO N CHEC KREPOR T Star t Time : 

### 11:02:50 EP A Methods : 3A , 6C , 7 E an d 1 0

Ru n ID : R2B Date : 12/17/2009 En d Time : 15:59:08 Jo b Number : 12170 9

Analyze rAnalyze r Zer o Mi d Para m Respons e Respons e C0 2 0 5. 1 TH C N/

A N/

A Syste m Bias ' Syste m Drift' Syste m Syste m Syste m Syste m Syste m Syste m Syste m Syste m Pre-Zero Pre-Mi d Pre-Zer o Pre-Mi d Post-Zer o Post-Mi d Post-Zer o Post-Mi d Respons e Respons e Bia s Bia s Respons e Respons e Bia s Bia s 0.0 2 5.1 0.2 % 0.0

% 0.0

1 5.0

8 0.0

% -0.2% -0.0 7 5.0

6 -0.8% -0.8 % -0.01 5.0 3 -0.1 % -1.1 % 100 % x(Syste m Respons e - Analyze rResponse) / (Spa n Value

) 100 % x(Syste m Pos t Respons e - Syste m P.r e Response) /

(Spa n Value) Fo rTH C Measurements : Syste m Bias = 100

% x(Syste m Respons e - Cylinde rGa s Standard Value ) / (Spa n Value) Zer o Drif t -0.1 % 0.7 % Mi d Drif

t -0.2% -0.3% Syste m

Avg-Zer o Respons e 0.0 2 -0.0 4 Syste m

Avg-MI d Respons e 5.0 9 5.0 5



### VES01905 3

## DAIL

YCALIBRATIO N REPOR T Star t Time : 

### 08:50:13 Methods : 3A , 6C , 7 E an d 1 0 Date : 

### 12118/200S Ent l Time : 

### 09:30:35 Jo b Number : 12180 9
Para m C0 2 TH C Spa n

Valu e 1 1 9 Mid-Ga s

Standard 5.0 2 5.1 3 Analyze r

Zero Respons e 0.0 1 N/ A Analyze r

Mi d Respons e 5.01 N/ A Zero

Ca l Erro r 0.2 % 0.0 % Mi d

Ca l Erro r -0.1 % 0.7 % Syste m Zer o Respons e -0 . 0 . Calibratio n Erro r= 100 % x(Analyze rRespons e - Cylinde rSa s Standard Value) / (Spa n Value

) Syste m Bia s = 100 % x(Syste m Respons e - Analyze rResponse) / (Spa n Value) Fo rTH C Measurements : Calibratio n Erro r= 100 % x(Syste m Respons e - Cylinde rGas Standard Value ) / (Cylinde rGa s Standard Value ) Syste m Bia s = 100 % x(Syste m Respons e - Cylinde rGas Standard Value ) / (Spa n Value

] Syste m Mi d Respons e 4.9 9 5.1 7 Syste m

Zer o Bia s -0.2% 0.0 % Syste m Mi d Bia s -0.2% 0.4 %



### VES01905 4

## CALIBRATIO N CHEC K REPOR Tstar

t Time : 

### 11:12:36 EP A Methods : 3A , 6C , 7 E an d 1 0 Ru n ID : R3B Date : 12/18/2009 En d Time : 15:02:38 Jo b Number : 12180 9

Analyze rAnalyze rSyste m Syste m Syste m Syste m Syste m Syste m Syste m Syste m Zero Mi d Pre-Zer o Pre-Mi d Pre-Zero Pre-Mi d Post-Zer o Post-Mi d Post-Zer o Post-Mi d Para m Respons e Respons e Respons e Respons e Bia s Bia s Respons e Respons e Bia s Bia s Zero Drif t Mi d Drif

t C0 2 0.01 5.01 -0.0 4 4.9

4 -0.5% -0.7 % 0.0

2 4.9

2 0.0

% -0.9% 0.5 % -0.2% TH C N/

A N/

A -0.06 5.1 -0.7 % -0.3% -0.1 4 5.1 1 -1.5% -0.2% -0.9% 0.1 % Syste m Bias = 100

% x(Syste m Respons e - Analyze rResponse) / (Spa n Value) Syste m Drift

= 100 % x(Syste m Pos t Respons e - Syste m Pr e Response)/(Spa n Value ) Fo rTH C Measurements : Syste m Bias = 100

% x(Syste m Respons e - Cylinde rGa s Standard Value) / (Spa n Value

) Syste m Avg-Zer o Respons e -0.0 1 -0. 1 Syste m

Avg-Mi d Respons e 4.9 3 5.1



### VES01905 5

# A2CQM

Comments : 

# Initia l TH C Monito rCalibration s Plan t 

# I.D.V 'goLi ASftU6e~ ^ |Ll.Niof S Projec t No . Sourc e I.D. Pollutan t
_ Dat e r H 

# c Analyze rSeria l No . O

IOO i 7 < ? Hr Operato rT . 

# .SRoez : YK&K i

Analyze rI.D

. Vi 6 Hotel

Q.O Spa n Valu e 1 e» 6



## Initia l Calibratio n (Time \Q:o c 

## l )

Zer o Ga s Cylinde rValu e

(ppm ) 

## 0 >OOQ Syste m

Respons e (ppm ) d O Predicte d Valu e (ppm ) Syste m Respons e (ppm ) Calibratio n

Erro r ( % o fSpan )

Lo wLeve l Ga s Mi d Leve l Ga s 

# 5
. I 3 " 3 £ M 9 

## £
. ' 3

Cylinde rI.D
. Zer o Ga s ULTR AZt.R o f^/Mb e Lo wLeve l Ga s 4 . 7 0 Mi d Leve l Ga s Hig h Leve l Ga s



## Calibratio n Erro r(Svste m Response - Predicte d Value ) X10

0 Calibratio n Gas Predicte d Valu e f(Hig h Respons e - Zero Respo n XMid o rLo wLeve l Ga s ] + Zer

o Response Hig h Leve l Ga s

VES01905 6

# Initia l Monito rCalibration s Plan t I.D . AugeT j \U\mS Projec

t No. (£^i 3 3e3 1 

### k Sourc e I.D . U M i T4 Operatorg jg a CZYAJS^1 

### Pollutan t ^ Oa , AnalyzerLD^ERV^Mfj f> 4 < ? ^ Dat e I

/'

$.00 °j Spa n Value _ AnalyzerSeria l No. /

V /j^ C /,27 < 9 ^

"
Initial Calibration (Tim e \0:<^H ) Cylinde rValue (pp m o r% ) Analyzer Respons e (pp m or% ) Calibration

Erro r ( % o fSpan ) System Respons e (pp m o r% ) Syste

m Bia s ( % o fSpan ) Zer o Ga s x 

# 0, Oo 

### Lo wLeve l Ga s — — 

### - — 

### Mid Leve l Ga s m £06 % 

### Hig h Leve l Ga s il,0 O 

# + 0**+ 

# )l.ol 0, f 

# AECO M

Comments :



### Cylinde rI.D
. Zer o Ga s 

## if

PrtmHi0 funny Lo wLeve l Ga s Mi d Leve l Ga s Hig h Leve l Ga s



### Calibration Error(AnalyzerRespons e - CylinderValue

) X10

0 Spa n Valu e System Bia

s = (Svstem Respons e - AnalyzerResponse

) X10

0 Spa n Value

VES01905 7

# Initia l Monito rCalibration s Plan t 

# i.D .Vfe>l / A SnW6 * T \LU )JO\S 

### Projec

t No. 

## l"

3 3 £ { 

### Sourc e I.D . 

# i T ^ Operator

# T" « £ Roc^-Y^

K i Pollutan t £Analyzerl.D.5^t < ^ 0 5 

### Dat e j. g II I

/ZOO < ? Spa n Value 

## AnalyzerSeria l No. ±W5c/£7o£

_ ^ ° %


### Initia l Calibration (Tim e 0tf>3c?) CylinderValu e (pp m o r% ) Analyze r Respons e (pp m or% ) Calibration

Error ( % o fSpan ) System Respons e (pp m o r% ) System Bia s ( % o fSpan ) Zer o Gas 

# OA Lo wLeve l Ga

s < — , — — 

### Mid Leve l Gas 

# SAo S*e>8 

# -o. a Hig h Leve l Ga

s 1 0 , 1 7 - O a | 

## AECO M

Comments :



### Cylinde rI.D
. Zer o Ga s 

# C C Q.30Ft&4> Lo wLeve l Ga s Mi d Leve l Ga s < Hig h Leve l Ga s



### Calibration Error(AnalvzerRespons e - CylinderValue

) X10 0 Spa n Valu e Syste m Bia s = (Svstem Respons e - AnalvzerResponse

) X10 0 Spa n Valu e

VES01905 8

# AECOM

Comments : 

# Initia l TH C Monito rCalibration s Plan t 

## \BSJUoU.fi



# SbOCfTj

luwoiS

Projec t No . 

# &>

1 

# 3 3 Q 1

# & Sourc e I.D . 

# U ^ f 

# T * f

## Operator T - 

# SEar -g ^S'I C ( Pollutan t ' ' " Dat e 

## \

1 1 7 o o < ? Analyze rSeria l No . NI

OO f ~7 9 9 Analvze rI.D .V f

## 6 2 o



## Spa n Valu e

Initial Calibratio n (Time^.^Q ) Cylinde rValu e (ppm ) Syste m

Respons e (ppm ) Predicte

d Valu e (ppm ) Syste m Response (ppm ) Calibratio n

Erro r ( % o fSpan ) Zer o Ga s 

# 0

'OOO Lo wLeve l Ga s Mi d Leve l Ga s ^^^^^^^^^^^^ ^ Hig h Leve l Ga s

Cylinde rI.D . Zer o Ga s A \ R Lo wLeve l Ga s CC

9.\^ < 

## I'70 Mi d Leve l Ga s Hig h Leve l Ga s 3

Calibratio n Erro r(Svste m Response - Predicte d Value ) X10

0 Calibratio n Ga s Predicte d Valu e f(Hig h Respons e - Zero Respo n XMid orLo wLeve l Ga s ] + Zer

o Respons e Hig h Leve l Ga s

VES01905 9

# AZCOM 

# Initia l Monito rCalibration s

Comments : 

### Plan t I.D . \j£<yL'if\

5vfl uCrf. \LLIWS Projec t No. £0/33g.i£> Sourc e I.D . U f o i ~ <

f Operator : 

### T i 

# Xfotz ; 

# i Pollutan t 

# C 0* AnalvzerI.D . 

# R\fQ*ex lL 

## i°0 Dat e \

3
. / j 3 9 Span Value AnalyzerSeria l No . Initia l Calibration (Time <7 ? : 

### 3p ) CylinderValue (pp m o r% ) Analyze r Response ' (pp m o r% ) Calibration

Error ( % o fSpan ) Syste

m Respons e (pp m o r% ) System Bia s ( % o fSpan) Zer o Gas 

# 0, CO 

## 0>0 \ Lo wLevel Gas 

# •

— ~ 

### Mi d Level Ga s 

# f
. - 6, 

# Q High Leve l Gas 

# 10.7 * +0.2
. >

Cylinde rI.D
. Zer o Ga s M a Lo wLeve l Ga s Mi d Leve l Ga s Hig h Leve l Ga s



### Calibration Error(AnalvzerRespons e - Cylinde

rValue ) X10

0 Spa n Valu e System Bia

s = (Svstem Respons e - AnalvzerResponse

) X10 0 Spa n Value

VES01906 0Comments : 

### Plan t I Sourc e I.D . Pollutan t
_ Dat e 

# Initia l TH C Monito rCalibration s D. 

## V&Ofl 

# Sf\u6eX

lu <7w.- g 

### Projec

t No . 

# <£>Q

(33 SL\ G 

### Operato r

## \ > € 

## Rotz. </vSK

t Analvze rI.D

. V< & Mabe'L2.0 id / Z OO • ? spa n Valu e < R Analyze rSeria l No . O

~?0O i l ^tyInitial Calibratio n (Time &\'>Z>0) Cylinde rValu e (ppm ) Syste m

Response (ppm ) Predicte

d Valu e (ppm ) Syste m Respons e (ppm ) Calibratio n

Erro r ( % o fSpan ) Zer o Ga s 0 u Lo wLeve l Ga s Mi d Leve l Ga s 

# 1 3 3 5 , 3 High Leve l Ga s

Zer o Ga s A ' cx Lo wLeve l Ga s Mi d Leve l Ga s Hig h Leve l Ga s Cylinde rI.D
.



# S 6 otoWWA v z G



### Calibratio n Erro r(Svste m Response - Predicte d Value ) X10

0 Calibratio n Gas Predicte d Valu e f(Hig h Respons e - Zero Respo n XMid orLo wLeve l Ga s ] + Zer

o Respons e Hig h Leve l Ga s

VES01906 1I

o

ri 

### VES01906 2

# AECOM

Appendi xD Laboratory Dat a

VES01906 3

# Metho d 5/26A

VES01906 4AECO M Repor t Environmen t


### Cas e Narrative
Re. : Gravimetri cAnalysi s o f Filte ran d Fron t Hal fProb e Rins e Sample s - Veoli a E S Tec h

Sauget , I L Projec t # : 6013321 6 LA B ID * 09-064,09-067,09-06 9 ANALYTICA L PROCEDURE : Eleve n (11 ) Teflon ®

typ e filter s an d 1 2 fron t hal faceton e rins e sample s wer e analyze d vi a EP AMetho d 5 Gravimetri cAnalysi s a s governe d b yAECOM' s SO P 2629-300
. Consecutiv e gravimetri cweight s o f filter s an d beake rresidue s wer e take n wit h a n annuall ycalibrate d Mettle rbalance' , an d weighe d withi n specifie d limit s a s outline d i n EP AMetho d 5 an d AECOM' s SO P 2629-300
.

1
. Fo rtw o o f thre e shipment s received , 09-067 an d 09-069 , on e fiel d blan k o f bot h filte ran d aceton e wer e analyze d a s specifie d b yEP AMetho d 5 Gravimetri cAnalysi s an d AECOM' s SO P 2629-300
. Th e firs t se t o f samples , 09-064 , containe d on e aceton e blank , bu t n o filte rblan k wa s received
. 2
. Laborator yblank s o fbot h filte ran d aceton e wer e analyze d fo reac h o f th e thre e set s o f sample s pe rth e sam e Metho d an d SO P a s liste d above
. 1
. Fo rth e firs t se t o f sample s received , La b ID : 09-064 , tw o o f th e aceton e sampl e bottles , M5-Acetone-R B an d M5-U3-AR-R3 , di d no t hav e th e leve l o f aceton e marke d o n th e bottle
. Additionally , followin g evaporatio n o f th e firs t o fthes e tw o samples , i.e
. th e fiel d blank , a moist , oily-appearin g residu e wa s observe d i n th e sampl e beaker
. Th e gravimetri cresul t fo rtha t sampl e indicate d a ne t gai n o f 1. 9 mg . 2
. Fo rth e thir d se t o f samples , La b ID : 09-069 , on e o f th e aceton e rins e sampl e bottles , M5-U4-FHR-R2 , wa s foun d t o contai n a piec e o f aluminu m foil , whic h wa s remove d durin g th e aceton e rinse procedur e an d prio rt o weighing
. .QUALIT YCONTROL :

DISCUSSION :

Dat e Sample s Receive d b yth e Laboratory : 12/04,12/1 1 & 12/21/0 9 Dat e Analysi s Started : 12/07/0 9 R:\AirDBaseMVl5DB\Metrio d 5 DatabaseWlETHO D 5 CLIEN TFILESWeolia\09-064_067_069_CaseNarrative.doc



### Pag e 2 o f 1 4 

### VES01906 5

### AECO M Metho d 5 Expose d Filte rDat a Shee t Projec t Manager : Projec t Name : Projec t Number: Analysi s Method : Jef fGorma n \'M f* -• ;T5afe Time R.H(A. t " R TCF

) Analys

t Projec t Manager : Projec t Name : Projec t Number: Analysi s Method : Veolia Star t Monda

y 12/21/200

9 10:3 0 3

4 6

9 W

V Projec t Manager : Projec t Name : Projec t Number: Analysi s Method : 6013321 6 Wt 1 Tuesda y 12/29/200

9 8:4 0 3

6 6

8 W

V Projec t Manager : Projec t Name : Projec t Number: Analysi s Method : Ove n Drie d Wt 2 Wednesda y 12/30/200

9 16:1 0 3

3 6

8 M

W Wt 3 Wt. 4 QAShrie t i PatioS. . Initia

l Woig'KS " i .'Sampl e ' * SprrtpflolD , Filter " Tyi e 1s

t V. l

. Gra n 2n d Wt

- " Grain s _ A*&2W

t "Cram s •>rdW

t I Ai&3WfJ- 4t

h W t ' Gram s 

### .. Gram 6 , FmmW

t Grims 4 Fi

V \\ \ To t i l Groin s QAShrie t i PatioS. . . . .Date

. J, r-Gram's. .filter * Ri m Dat e * SprrtpflolD , Filter " Tyi e 1s

t V. l

. Gra n 2n d Wt

- " Grain s _ A*&2W

t "Cram s Gram

s Gra

m 4t

h W t ' Gram s 

### .. Gram 6 , FmmW

t Grims 4 Fi

V \\ \ To t i l Groin s 9 0 12/22/0

9 0.394

2 T182

9 La

b Filte rBlank 86.2m

m 0.394

2 0.394

2 0.000

0 okbvWt . 0.394 2 0.000

3 8 8 11/25/0

9 0.400

8 T182

3 12/15/0

9 Mf>CPT-PF-FB-U4 86.2m m 0.400

6 0.400

6 0.000

0 okbvWt . 0.400 6 0.000

3 8 7 11/25/0

9 0.403

3 T181 5 12/16/0

9 M5-U4-F-R1 86.2m m 0.404

8 0.404

7 0.000

1 okbvWt . 0.404 8 0.001 5 8 8 11/25/0

9 0.411 5 T181 9 12/17/0 9 M5-U4-F-R

2 88.2m

m 0.413

0 0.413

0 0.000

0 o k byWt. 0.413 0 0.001 5 8 7 11/25/0

9 0.412

4 T181 6 12/18/0

9 M5-U4-F-R

3 86.2m

m 0.416

7 0.416

4 0.000

3 okbvWt . 0.416 6 0.004

2 f D O

- h

FHterTyoe : G=GIas s Q=Quart z 1 . Delt a Weight toleranc

e +/ - O.OOOS g o ftota l weigh

t less tar e weigh t between tw

o consecutiv

e weightings oraverag e weigh t 2 . Filter s mus t b e weighe d wit h m e prope rconditions (R H - 2 5 - 50 % an d R T* 59-7 8 de g f ) 3 . Fillet s mus t b e properly conditione

d (2 4 hou rdesiccation ; Furthe rConditionin g > 6 hours) . 4 . Conditionin g fo rove n method ; Ove n drie d e t 10 S de g c f o 2- 3 hours ; Furthe rconditionin g > 6 hours . 5 . Tota l grams belo

wo requa l to .000

5 (LDL ) I s presente

d a s .0003 .

Veolia_09-069_60l3321 6 emalLxl s 

### VES01906 6

### AECO M Metho d 5 Fron t Hal fAceton e Prob e Rins e Dat a Shee t Balanc e Used : Mettle

r 3 Projec t Manager : Jef

fGorma n s u m - Dat e •Tim

e R.T.TF V Projec t Name : Veoli

a Star t Wednesda

y 12/30/200

9 18:0 0 3 3 6

8 M

W Projec t Number : 6013321 6 Wt . 1 Monda

y 1/4/201 0 16:1 0 3 4 6

8 W

V Analysi s Method : M M M Hea t Applicatio

n Wt. 2 Tuesda y 1/5/201 0 8:3

0 3

4 6

8 W

V Wt 3 Wt. 4 QA.sho» ; i-

< InltlalW

I «* a BeakoY

* Run bat

e , 1s t W t ' Grams , 2n

d W t finms^ , &l&:W

t n J jr_ i •>-

d WI, ' •Gram s 4t

h W t V . »,.g«... s < • &4 W Gran s Flm l W

t r A F

WI W i.w±f ^ ungui s QA.sho» ; Dat

? «.. .. . " M!-, M BeakoY

* Run bat

e , 1s t W t ' Grams , 2n

d W t finms^ , &l&:W

t n J jr_ i •>-

d WI, ' •Gram s 4t

h W t V . »,.g«... s < • &4 W Gran s Flm l W

t r A F

WI W i.w±f ^ ungui s 48 5 12/16/0

9 91.510

6 37 2 — La

b Aceton e Blank — 5 0 91.510

6 91.510

8 0.000

2 okbyWt . 91.510 7 0.000

3 48 5 12/16/0

9 109.695

1 228 4 12/15/0

9 M5-Acetone-RB-U 4 19

8 5

0 109.695

6 109.695

6 0.000

0 okbyWt . 109.695 6 0.000

3 48 5 12/16/0

9 106.701 0 227

8 12/16/0

9 M5-U4-FHR-R1 5 9 5

0 106.703

5 106.704

0 0.000

5 okbyWt . 106.703 8 0.002

8 48 5 12/16/0

9 104.268

2 11 7 12/17/0

9 M5-U4-FHR-R

2 4

9 5

0 104.270

0 104.270

5 0.000

5 o k byWt. 104.270 3 0.002

1 48 5 12/16/0

9 109.716

2 226 6 12/18/0

9 M5-U4-FHR-R

3 6

1 5

0 109.719

1 109.718

8 0.000

3 okbyWt . 109.719 0 0.002

8

Aceton e Manufacturer/Lo

t No. : Fisher/09295

0 Aceton e Rinse = 2 5 mi s twic e - (50 mi

s total) 1 . Delt a Weight toleranc

e +/ - O.OOOS g o ftota l weigh

t (es s tar e weigh t betwee n w o consecutrv e weightings o raverage weight. 2 . Beaker

s mus t be weighe

d wit h th e prope rcondiiion s (R H = 2 5 - 6 0 % an d RT= 59-7

8 de g f ) 3 . Beaker

s mus t be propert

y conditione

d (24 hou rdesiccation ; Furthe rConditionin g > 6 hours) . 4 . Natura l Evaporatio n Metho d « Evaporat

e t o dryness a t roo m temperatur e unde ra hood /

watc h glass cove r 5 . Hea t Applicatio n = Unde ra hood an d watc h glas s ove rsample , apply hea t belo wth e boilin g poin

t of sampl e unti l evaporated l o 2 5 mis ; the n fallo wste p 4 (above

) fo r remainin g portion. . 6 . Tota l grams belo

wo requa l t

o .0005 (LOL

) I s presented a

s .0003 .



### VES01906 7

## Sampl e Traceabilit y Lis t Sit e o fProgram : Veoli a E S Tec h Sampl e Date : 

### U,l / £- 

### & l//O

c 

### r Projec t Location : Sauget , i L P.O
. # : Typ e o fProgram : CP T Dat e Shipped : \2.\ lff/0" ¥ Laborator yAECO M Enviranmor K Harvard , M A f . f- v)*«• £r * Project* : 8013321 6 Progra m Office : Syracus e N Y Shippe r/ Steve n Mil o Recovery : Ji m Morri s Laborator yAECO M Enviranmor K Harvard , M A f . f- v)*«• £r * Progra m Contact : Jef fGorma n FedE xAi rBil l # : Ite m Sampl e I D Cod e Sampl e Matrix Sampl e Descriptio n Analitica l Parameter s Specia l instruction s 1 M5-U4-F-R 1 Filte r IWS , Filler , Ru n 1 Particulat e Matte r ©9-069-3.
. 2 M8-U4-FHR-R 1
. 

### Aceton e MB , F H Aceton e Rinse , Ru n 1 Particulat e Matte r 3 4 M5-U4-F-R 2 Filte r MS , Filter , Ru n 2 Particulat e Matte r 5 M5-U4-FHR-R 2 

### Aceton e WI5 , F H /Aceton e Rinse , Ru n 2 Particulat e Matte r 

### C' V -069- 7 6 7 M5-U4-F-R 3 

### Filte r M5 , Filter , Ru n 3 Particulat e Matte r 8 MS4J4-FHR-R 3 Aceton e M5 , F KAceton e Rinse , Ru n 3 Particulat e Matte r 

### (\<?« c c i> •• 1 ? 9 1 0 1 1 1 2 1 3 1 4 1 5 1 6 1 7 - 1 8 1 9 fur- , fi I f-^ - & U l .4 C 

### ol-os?-- / 2 0 MIS -Acetor»e -RB-U 4 

### Aceton e IMS-Acetone Blan k Particulat e Matte r Fiel d N (>tes

/ Comments Pag e \ o f1 Relinquished By(print) : Date : Signature : Time : 

### 1700 Relinquished B y(print) : Date : Signature : Time : (Relinquishe d By(print) : Date : Signature : Time : [Received b yLa b (print) : Date : Signature : Time : Receive d By(print) : _Date : Signature : Time : 

### ^Mu, U, U Receive d B y(print) : Date : Signature : Time : iReceived By(print) : Date : Signature : Time : Analytica l Laborator yDestination : lAECO M Environment 32 5 Aye rRoa d Harvard , M A0145 1 lAttn : Mr
. Pau l Tavern a (978 ) 772-234 5 Ex t 3 2 

### VES01906 8

### nient/Proj#
_ Projec t Mgr:
_ 

## SAMPL E LOG-I N & RECEIP TCHECKLIS T

La b Pool# : 09-061 Inspecte d & Logge

d i n by: . Dat e & Time :
l^nvbeffo f stJfraPj ^ 

# WBSoSSSSs fib*- HT :#/Vo< ? 

### Due://W/O H HT : It-fa/oX Due : //v A HT : Due : 

### Circl e the appropriat

e response : 1 ) S^fpp^d /

Hand delivere

d i 

### CO C p^Serf t

### /

no t presen t on receip

t 3 ) Sample

s broke n / leakin g / (n{§p $ on receip

t 4 ) Sample

s ^nbj| M /

chille d on receip

t 5 ) Sample

s preserve

d correctl

y / incorrectly_|^noj3

e recommende

d 6 ) Receive

d ^Rjjp /

outsid e holdin g tim

e 7 ) CO C tape

s presen t / r^SDaesen

t on sample

s /N A 9 ) Discrepancie

s /^^discrepancie s note d between COC s an d sample s Additiona l Comments : •

6 38/26/200 8 

### Pag e 1 4 o f1 4


### VES01906 91



# TestAmeric a
TH E LEADE R I N ENVIRONMENTA L TESTIN G
TestAmeric a Laboratories , In c



## ANALYTICA L REPOR T

PROJECT HO . 6013321 S Veoli a - E S Tec h Lo t # : H9L21040 3

Jef f Gorma

n AECOM , In c 510 5 Canrpuswoo

dDriv e Suit e 10 4 Eas t Syracuse , N

Y130S 7

TESTftMERICft . LABORATORIES , INC .

Kevi nS . Woodcoc

k Projec t Manager

Decembe r 30 , 200 9

581 5 Middlebrook

Pik e Knoxville

, T N 3792 1 te l 865.291.300

0 fa x865.584.431 5 www.testamericainc.co m



### VES01907 02 

## ANALYTICA L METHOD S SUMMAR Y

H9L21040 3

ANALYTICA L PARAMETE

RMETHO D Chlorin e Emission s KNO X0050/26

A Mo d HydrogenChlorid e Emission s KHO X0050/26

A Mo d References : KNO XTestAmeric a Laboratorie s Inc. , Knoxvill e Laborator y Standar d Operatin g Procedur e



### VES01907 13 

## SAMPL E SUMMAR Y H9L21040 3

W O # SAMPLEft CLIEN T SAMPL E ID SAMPLE D SAM P DATE TIM

E LRE2 0 LRE2 2 LRE2 3 LRE2 4 LRE2 5 LRE2 6 LRE2 8 LEE2 9 LRE3 S 00 1

00 2 00 3 00 4 00 5 00 6 00 7 00 8 00 9 CPT-HCL-FB-U 4 CPT-CL2-FB-U

4 CPT-U4-HCL-IMP1-4-RI A CPT-17 4 - CL 2 - IMP 5 - 6 -R l CPT-U4-HCL-IMP1-4-R2 A CPT-U4-CL2-IMP5-6-R2 CPT-04-HCL-IMP1-4-R3 A CPT-U4-CL2-IMP5-6-R3 CPT-H20-FB-U

4 12/16/0 9 12/16/0 9 12/17/0 9 12/17/0 9 12/18/0 9 12/18/0 9 12/15/0 9 12/15/0 9 12/15/0 9 MOT E (S ) :

- Th e anaiyiicai result

s o rih e sample s liste d abov e ar e presente

d o n ih e followin g pages

. •Al l calculation

s ar e performe

d befor e rounding i o avoi d round-of ferror s i n calculate

d results .

- Result s note d a s "ND " wer

e no t detecte d a t orabov e liff i stale

d limit .

- Thi s repor

t mus l no i b e reproduced , esccp

t i n full , withou

t th e writte n approval o

fth e laboratory

.

- Result s To rth e followin g parameter

s ar e neve rreporte d o n a dr y weigh t basis : color , corrosiviiy , density , flashpoint

, ignitability . layers, odor, pain t fille rtusr

. pH , porosit

y pressure

, reaciiviiy , redo

xpotential , specific gravity , spoiiests , solids , solubility, temperature , viscosity, an

d weight .



### VES01907 24 

# PROJEC T NARRATIV

E H9L21040 3 Th e result

s reporte d herei n ar e applicable t

o th e sample s submitte

d fo ranalysis only . Thi s repor

tshal l no tb e reproduce

d excepti

nfull , withou

tth e writte n approva

l o f th e laboratory. 

### The origina

l chai n o f custod y documentatio

n i s include d wit h thi s report . Sampl e Receip t Custod y seal s wer e no tpresent . 

### Qualit y Contro l an d Dat aInterpretatio

n Unles s otiierwise noted , all holding time s an d Q C criteriawer

e me tan d th e tes tresult s show n in this repor

tmee tal l applicable NELA C requirements. Sample s wer e analyze

d forchloride b

y ion chromatograph

y using SO Pnumbe

rKNOX WC-00 5 (base

d on EP A method

s 9056,905 7 an

d 26A) . Al l sampl

e result s wer e reporte d a s tota l n g hydroge

n chloride (HCI ) an

d tota l u. gchlorine (Cl 2 

### ) . Result s wer e calculate

d using th e followin g equations : HCI, u g = (Chloride,ug/mL)*(Sample Volume,mL)* [ ^'^"'^WeightHCA „ Q 

### \Molecula

rWeigh tC ! , C l 2, ug = (Chloride,ug

/ mL) * (Sampl

e Volume

, mL) * Benc

h Dilutio n NaO H impinge

rsample s wer e treate d wit h sodiu m thiosulfat

e (NazS^Os

) priort o th e final analysis i n orde

rt o conver tresidua l hypochlorit

e (OC1") t

o chloride ion . Note : A sampl

e volume o f

10 0 m L wa

s use d t o conver tth e result s t o tota l fo rth

e metho d blanks , laborator

y contro l samples, an

d clien treagen tblank s i n orde rt o standardiz

e tlie analyt

e sampl e total .

TesiAmeric

a Knoxville maintain

s th e following certifications , approval s an d accreditations: Arkansa s DEQ La b #88 - 0688 , California DHS ELA P Cert . #2423 , Colorad o DPHE , Connecticu

t DP H La b #PH-0223

, Florid a DO H La

b #E87177 . Georgi a DN R Lab i/906, Hawai i DOH , Illinois EP A La b S20D012

, Indian a DO H La

b #C-TN-02 , Iow

a DN R La b #375 ; Kansa s DH E Cert

. i'E-10349, Kentuck

y DEP La

b #90101 , Louisian

a DEQ Cert

. #03079 , Louisian a DOHH , Marylan d DO E Cert

. #277 , Michiga n DE Q Lab #9933

, Nevad a DEP , Ne

wJerse yDE P La b #TN001 , Ne

wYor k DO H Lab "f , 10781 , Nort

h Carolina DP H La

b #21.705 , Nort h Carolin a DEHN R Cert

. #64 , Ohio EP A VA P La

b &CL0059

, Oklahom a DEQ La

b #9415 , Pennsylvani

a DE P La b #68-00576

, Sout h Carolin a DHE C Cer

t #84001001 , Tennesse

e DO H La b #02014 , Texa s CEQ , Uta

h DO H Lab # QUAN3 , Virginia DGS Lab #00165 , Washingto

n DO E La

b #C1314

, Wes t Virginia DE P Cert

. 2345, Wes

t Virgini a DHH R Cer

t S9955C , Wisconsi n DN R La

b #998044300

, Nava l Faciliiie s Engineerin

g Servic e Cente ran d USD A Soi l Permi

t #S-46424

. This lis t o fapproval s is subjec

t t o chang e an d doe s no t impl y lha t laborator

y certificatio

n is availabl

e fo ral l parameter

s reporte d i n thi s environmenta

l sampl e dat a report .



### VES01907 35 

# PROJEC T NARRATIV

E H9L21040 3 Fo rdemonstratio

n o f analytica

l metho d performanc

e on thes

e samples , TestAmerica Knoxvill e analyze

d matri x spike s (MS) an

d matri x spik e duplicate

s (MSD) . Acceptable recoverie

s o f thes e spike s demonstrat

e tha tquantitatio

n fro m this particula

rstac kga s matri x i s accurat e an d acceptable, Impinge rsample s containing 0.1N HiS0 4 an d O.IN NaO H displa

y matri x interferenc

e effect s causin g poormetho

d performanc

e an d possibl y givin g unreliabl

e dat aunless th

e interferenc

e i s removed. Therefore , th e sample

s wer e diluted i nth

e la b t o remov e th e interferenc

e fo ramor

e accurat e chloride response. Th e sample s ma y b e analyze

d a tincreasing dilution

s along wit

h matri x spike s until matri

x spikes recove

rfrom th

e sampl e within laborator

y contro l limits . The io n chromatograp h calibration rang

e use d t o quantitat

e th e sampl e result s permit s astandar

d ten-fold sampl

e dilutio n whil

e supportin

g th e reportin

g limi twit

h th e low calibration standard. Th e dilution facto

rreporte d on th e sampl e resul tform doe

s no trepresen

tth e benc h dilutio n factor

. I ti s actuall

y th e combinatio

n of factor s require d b y th e metho d t o conver t th e anio n reportin

g limitan

d method detectio

n limitfro

m ug/m L t

o tota l ug . I tma y appea rt o b e elevate d becaus

e itincludes th

e tota l sampl e volume i nmL .



### VES01907 46 

## Q C DAT A ASSOCIATIO N SUMMAR Y

H9L21040 3
Sampl e Preparatio nan dAnalysi s Contro l Number s

SAMPLE j 00 1 00 2 00 3 00 4 00 5 00 6 00 7 00 8 00 9 MATRI

X AI R A I R 

### AI S AI R AI R AI R AI R AI R AI R ANALYTICA L METHO D KNO X0050/26A

Mo d KNO XO0S0/26

A Mo d KNO X0050/26A

Mo d KNO X0050/26A

Mo d KNO X0050/26A

Mo d KNO X0050/26A

Mo d KNO X0050/26A

Mo d KNO X0050/26A

Mo d KNO X0050/26A

Mo d LEAC

H BATC H # PRE

P BATC H # 935819 5 .935735 5 935819 5 935735 5 935819 5 935735 5 

### 935819 5 935B19 5 935735 5 M

S RUN # 935812 0 935607 2 935812 0 935807 2 935812 0 935807 2 935812 0 935B12 0 935807 2

I



## VES01907 57



# Sample Dat aSummar

y

VES01907 68



### AECOM , In c Clien t Sampl e ED : CPT-TJ4-HCL-IMP1-4-R1 A Genera l Chemistry . Lot-Sampl e #... : H9L-210403-00 1 Wor k Orde r #.'.. : LRE2 0 Matri x: AI R Dat e Sampled... : 12/16/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H # Hydroge ncOilorid e 3460 0 4420 . u g KNO X0050/26A

Mo d 12/22/0 9 935819 5 Dilutio nFactor s 44222.4 6 ' MDL . : 190 0



### VES01907 79



### AECOM . m c Clien t Sampl e ID : CPT-04-CL2-IMP5-6-R1

Genera l Chemistr y Lot-Sampl e #... : H9L210403-00 2 Wor k Orde r LRE2 2 Matrix... . : AI R Dat e Sample d: 12/16/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

R.RESUL T R L UNIT S METHO D ' ANALYSI S DAT E BATC H # Chlorin e N D 48 4 u g KNO

X0050/26A

Mo d 12/21/0 9 935735 S Dilutio nFactor : 484 0 HDI > 20 0



### VES01907 81 0



### AECOM , Inc . Clien t Sampl e ID : CPT-04-HCL-IMP1-4-E2 A Genera l Chemistry Lo t -Sampl e #.. . : H9L210403-D0 3 Wor k Orde r : LRE2 3 Matri x: AIR Dat e Sampled. : 12/17/0 9 . Dat e Received.. : 12/19/0 9 PREPARATION - PRE

P PARAMETE

RRESUL T R

L UNIT S METHO D ANALYSI S DAT E BATC H # Hydrogenchlorid e 4310 0 442 0 n g KNO X005Q/26

A Mo d 12/22/0 9 935819 5 Dilutio nFactor : 44222.4 6 MDI , : • 190 0



### VES01907 9

### 1 1

AECOM , In c Clien t Sampl e ID ; CPT-U4-CL2-XME5-6-R2

Genera l Chemistr y Lot-Sampl e #..- : H9L210403-00 4 Wor k Orde r -

. L-RE2 4 Matrix... . t AI R Dat e Sampled... ; 12/17/0 9 Dat e Received. . - . 12/19/0 9 PREPARATION - PRE

P PARAMETE

RRESUL T R L UNIT S METHO D ANALYSI S DATE BATC H # Chlorin e 20 8 B 47 2 ug KNO

X0050/26A

Mo d X2/21/0 9 935735 5 Dilutio nFactor : 472 0 MD L : 20 0 

### NOTB(S ) : R L Reportin

g Limi t B Estimate

d result. Resul

t i s les s tha n RL .



### VES01908 01 2



### AECOM , In c Clien t Sampl e ID : CPT-U4-HCL-IMP1-4-R3 A Genera l Chemistr y Lot-Sampl e #.-. : H9L210403-0.0 5 Wor k Orde r #... : LRE2 5 Matri x: AI R Dat e Sample d: 12/18/0 9 Dat e Received.. : 12/19/0 9 .PREPARATION- PRE P PARAMETE

RRESUL T R

L CHIT S . METHO D ANALYSI S DATE BATC H # Hydroge nchlorid e 364 0 159 0 u g KNO X0050/26

A Mo d 12/22/0 9 935819 5 Dilutio nFactor : 16866.2 4 MD L 71 0



### VES01908 11 3



### Lot-Sampl e # . Dat e Sampled .
PARAMETE

R . AECOM , In c

Clien t Sampl e ID : CPT-U4-CL2-IMP5-6-R3

Genera l Chemistr y

. : H9L210403-00 5 Wor k Orde r #... : LRE26 "

. : 12/18/0 9 Dat e Received.- : 12/19/0 9 Matrxx . AI R

RESUL T R L UNIT S METHO D PREPARATION- PRE P ANALYSI S DATE BATC H # Chlorin e 20 4 B 48 0 u g Dilution . Factor : 480 0 

### KNO X0050/26A

Mo d 12/21/0 9 MD L : 20 0 

### 935735 5 NOTE(S ) : - IU . Reportin

g Limit B Estimate

d result. Resul

t is les s tha n RL .



### VES01908 21 4



### AECOM ; In c Clien t Sampl e ID : CPT-H2O-FB-0 4 Genera l Chemistr y Lot-Sampl e #.. . : H9L2104.03-00 7 Wor k Orde r : LRE2 8 Matri x: AI R Dat e Sample d: 12/15/0 9 Dat e Received . . : 12/19/0 9 PREPARATION- PRE P PARAMETE

R; RESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H # Hydrogenchlorid e N D 10 3 ug KNO X0050/26

A Mo d 12/22/0 9 935819 5 Dilutio nFactor : 1028.4 3 MD L : 4 3



### VES01908 31 5



### • AECOM , la c Clien t Sampl e ID : CPI-HCL-FB-tf 4 Genera l Chemistr y Lot-Sampl e if... : H9L210403-00 8 Wor k Orde r #... : LRE2 S Dat e Sampled... : 12/15/0 9 Dat e Received.. : 12/19/0 9 Matrix . . : : AIR

PARAMETE R 

### RESUL T R L UNIT S Hydioge nchlorid e N D 41 1 ug

Dilutio nFactor. - 4113.7 2 MD L : 17 0 

### PREPARATION- PRE P METHO D ANALYSI S DATE BATC H # KNO X0050/26

A Mo d12/22/0 9 935819 5



### VES01908 4

### 1 6

AECOM , In c Clien t Sampl e ID : CPT~CL2-FB-U 4 Genera l Chemistr y Lot-Sampl e #... : H9L210403-00 9 Wor k Orde r : LRE3 A Matri x: AI R Dat e Sampled-.. : 12/15/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESUL T R

L . UNIT S METHO D ANALYSI S DAT E BATC H # Chlorin e N D .10 0 u g KNO X0050/26

A Mo d 12/21/0 9 935735 5 Dilutio nFactor : 100 0 HD L : 4 2



### VES01908 5

### 1 7

METHO D BLAN KREPOR T Genera l Chemistr y Clien t Lo t # . . . : H9L21040 3 Matrix . . : AI R


### PARAMETE

R REPORTIN G RESUL T LIMI T UNIT S Chlorin e N D METHO D PREPARATION- PRE P ANALYSI S DAT

E ,BATC

H ft Wor k Orde r # : LRLHD1A A M B Lot-Sampl e # : H9L230000-35 5 10. 0 ug KNO X0050/2SA . Mo

d 12/21/0 9 Dilutio nFactor : 10 0 

### 935735 5 Hydroge nchlorid e . Wor k Order,# : LRL131A A M B Lot-Sampl e # : H9L240000-19 5 N D 10. 3 u g KNO X0050/26

A Mo d 12/22/0 9 Dilutio nFactor : 102. 8 

### 935819 5

NOT E IS ) ; Calculations ar

c performe

d befor e rounding t

o avoid roundof

ferror s i n calculate

d results .



### VES01908 61 8



### LABORATOR

YCOHTRO

L SAMPL E EVALDATIO

H REPOR T Genera l Chemistr y Lot-Sampl e #... : H9L21040 3 Matrix . PARAMETE

R Chlorin e PERCEN T RECOVER

Y 9 8 10 3 RECOVER Y LIMIT S RP

D RP D . LIMIT S METHO

D PREPARATION- •

ANALYSI S DAT

E : AI R PREP BATC H #

. WO#:LRLHDIAC-LCS/LRLHDIAD-LCS D LC S Lot-Sample# : H9L230000-35 5 (9 0 - 110 ) KNO XO05O/26

A Mo d 12/21/0 9 935735 5 (9 0 - 110 ) 5. 0 (0-20 ) KNO X0050/26

A Mo d12/21/0 9 935735 5 Dilutio nFactor : 10 0 

### Hydrogenchlorid e

10 0 9 8 WO#:LRL131AC-LCS/LRL131AD-LCS D LC S Lot-Sample# : H9L240000-19 5 (9 0 - 110 ) KNO X0050/26A

Mo d 12/22/0 9 935819 5 (9 0 - 110 ) 2. 0 (0-20 ) KNO X0050/2S

A Mo d 12/22/0 9 935B19 5 Dilutio nFactor : 102. 8


### NOTBCS ) t Calculuions ar

c performe

d befor e roundinc l o avoid roundof ferror s i n calculaie

d results.



### VES01908 71 9



### LABORATOR

YCOHTRO

L SAMPL E DAT A REPOR T Genera l Chemistr y Lot-Sampl e tt... -. H9L21040 3 Matrix . AI R
PARAMETE

R Chlorin e SPIK

E MEASURE

D AMOUN T AMOUN

T UNIT S PERCN T RECVR YRP D METHO

D PREPARATIONANALYSI S DAT

E 75. 0 75. 0 PRE P BATC H # WO#:LRLHDIAC-LCS/LRLHDIAD-LCS D LC S Lot-Sample# : H9L230000-35 5 .73. 7 u

g . 9 8 • ICNO X0050/26

A Mo d12/21/0 9 935735 5 77. 5 u

g 10 3 S. O KNO X0 050/26

A Mo d12/21/0 9 .935735 5 Dilutio nFactor : 10 0 

### Hydrogenchlorid e

77. 1 77. 1 WO#:LRL131AC-LCS/LRL131AD-LCS D LC S Lot-Sample# : H9L240000-19 5 77. 2 ug ' 10 0 KNO X0050/26

A Mo d12/22/0 9 935819 5 75. 6 u

g 9 8 2. 0 KNO X0 050/26

A Mo d12/22/0 9 935819 5 Dilutio nFactor : 102. S 

### NOTE(S) : Calculations ar

e performe

d befor e rounding t

o avoi d round-of

ferror s i n calculate

d results.



### VES01908 8

### 2 0

MATRIXSPIK

E SAMPL

E EVALUATIO

N REPOR T Genera l Chemistr y Clien t Lo t #„.. : H9L21040 3 Dat e Sampled^... : 12/17/0 9 Dat e Received.. : 12/19/0 9 Matrix . . : AI R

• PARAMETE

R Chlorin e PERCEN T RECOVER

Y RECOVER

YLIMIT S RP

D RP D LIMIT S METHO

D PREPARATIONANALYSI S DAT

E PRE P BATC H # 9 8 7 8 WO# : LRE24IAC-MS/.LRE24IAD-MSD . M S Lot-Sampl e # ; H9L21O403-00 4 (7 5 - 125 ) KNO X0050/26

A Mo d 12/21/0 9 935735 5 (7 5 - 125 ) 1 8 (0-20 ) KNO X0050/26

A Mo d 12/21/0 9 935735 5 Dilutio nFactor : 472 0 

### Hydroge nchlorid e

.107 (7 5 11 8 ' (7 5 W0# : LRE23IAC-MS/LRE23IAD-MSD M S Lot-Sampl e # : H9L210403-00 3 125 ) KNO X0050/26

A Mo d 12/22/0 9 935819 5 125 ) 1. 8 (0-20 ) KNO X0050/26

A Mo d 12/22/0 9 935819 5 Dilutio nFactor : 4422 2 

### NOTE(S) : Calculaiion s ar

c performe

d befor e rounding i

o avoid round-of

ferror s i n calculate

d results.



### VES01908 92 1



### MATRI XSPIKE SAMPL

E DAT A REPOR T Genera l Chemistr y Clien t Lo t Dat e Sampled. . H9L21040 3

12/17/0 9 Dat e Received.. : 12/19/0 9 Matrxx . A I R


### SAMPL E SPIKE MEASR

D PARAMETE

RAMOUN

T AM T Chlorin e 20 8

20 8 94 4

94 4 AMOUN

T UNIT S PERCN T RECVR YRP D METHO

D PREPARATIO N - PRE P ANALYSI S DATE BATC H # WO# : LRE24IAC-MS/LRE24lAD-MSD M S Lot-Sampl e # : H9L21O403-00 4 113 0 ug 9 8 KNO X0050/26

A 12/21/0 9 935735 5 94 5 u g 7 8 1 8 KHO X0050/26

A 12/21/0 9 935735 5 Dilutio nFactor : 472 0 

### Hydroge nchlorid e

4310 0 884 0 4310 0 884 0 WO# : LRE231AC-MS/LRE231AD-MS D M S Lot-Sampl e # : H9L21O403-00 3 5260 0 ug 10 7 KNO X0050/26A

12/22/0 9 935819 5 5350 0 ug

- .11 8 1. 8 ICNO X0O50/26

A 12/22/0 9 935819 5 Dilutio nFactor : '4422 2 

### NOT E (S ) Calculaiion s ar c performti l befor e roundin g 1 0 avoi d round-of ferror s i n calculate d results. .



### VES01909 02 2



### Clien t Lo t H9L21040 3 Dat e Sampled... : 12/16/0 9 SAMPL E DDPLICATE EVALUATIO N EEPOR T Genera l Chemistr y Wor k Orde r #... : LRE20-SM P LRE20-DD

P Dat e Received... - 12/19/0 9
PARA M RESUL T DUPLICATE

RESUL T Hydrogenchlorid e 3460 0 3590 0 UNIT S RP D RP D LIMI T METHO

D Matrix. . .

• :-AI R

PREPARATION- PRE P ANALYSI S DAT E BATC H # S D Lot-Sampl e # : H9L210403-00 1 ug 3. 7 (0-20 ) KNO X0050/26

A Mo d 12/22/0 9 , 935819 5 Dilutio nFactor : 44222.4 6



### VES01909 12 3



### Clien t Lo t § . Dat e Sanrpled . PARA M RESUL T Chlorin e N D : H9L21040 3

: 12/16/0 9 DDPLICATE RESULT SAMPL

E DUPLICATE EVALUATIO N REPOR T Genera l Chemistr y Wor k Orde r #... : LRE22-SM P LRE22-DU

P Dat e Received., : 12/19/0 9
UNIT S RP

D RP D LIMI T METHO

D Matri x: AI R

PREPARATION - PRE P ANALYSI S DAT E BATC H # S D Lot-Sampl e # : H9L2.10403-D0 2 21 1 B u

g 20 0 (0-20 ) KNO X0050/26

A Mo d 12/21/0 9 935735 5 Dilutio nFactor : 484 0 

### NOTE(S ) : Calculations ar

c performe

d befor e rounding l o avoid round-offerror s i n calculate

d results. B Estimate

d result. Resul

t is les s tha n RL .



### VES01909 22 4



### Clien t Lo t #... : H9L21040 3 Dat e Sampled... : 12/17/0 9 SAMPL E DUPLICAT E EVALUATIO N REPOR T 

### Genera l Chemistr y Wor k Orde r #... : LRE23-SM P LRE23-DU

P Dat e Received.. : 12/19/0 9
PARA M RESULT DUPLICAT E RESUL T Hydroge nchlorid e 4310 0 4400 0 UNIT S RP D RP D LIMI T METHO

D Matri x: AI R

PREPARATION-

_PRE P ANALYSI S DAT E BATC H # S D Lot-Sampl e ft: H9L210403-0O 3 u g 2. 1 (0-20 ) KNO XOO50/26

A Mo d 12/22/0 9 935819 5 Dilutio nFactor : 44222.46 '



### VES01909 32 5



### Clien t Lo t # . Dat e Sampled . PARA M RESULT Chlairin e 20 8 B H9L21040 3

12/17/0 9 DUPLICATE RESUL T ' SAMPL

E DUPLICATE EVALDATIO H REPOR T Genera l Cnemistr y Wor k Orde r LRE24-SM P LRE24-DU

P Dat e Received.. : 12/19/0 9

N D UNITS RP D RP D LIMI T METHO

D Matri x. -. : AI R

PREPARATION- PREP ANALYSI S DAT E BATC H # S O Lot-Sampl e # : H9L210403-00 4 ug 20 0 (0-20 ) KNO X0050/26

A Mo d 12/21/0 9 335735 5 Dilutio nFactor : 472 0 

### NOTE(S ) : Calculations ar

c performe

d befor e roundin g t o avoi d round-of

ferror s i n calculate

d results . B Estitnate

d result. Resul

t is les s tita n RL .



### VES01909 42 6



### Clien t Lo t #. . Dat e Sampled. . PARA M RESULT H9L21040 3

12/18/0 9 DUPLICATE RESUL T SAMPL

E DUPLICATE EVALUATIO N REPOR T Genera l Chemistr y Wor k Orde r #.„•. : LRE25-SM P LRE25-DU

P Dat e Received.. : 12/19/0 9
Hydrogenchlorid e 364 0 359 0 UNIT S • RP D RP D LIMI T METHO

D Matri x: AI R

PREPARATION- " PRE P ANALYSI S DAT E BATC H # S D Lot-Sampl e # : H9L210403-0O 5 ug 1. 5 "(0-20 ) KNO X0050/26A-Mo

d12/22/0 9 935819 5 Dilutio nFactor : 16866.2 4



### VES01909 5

### 2 7

Clien t Lo t # . Sat e Sampled . PARA M RESULT . : H9L21040 3

. : 12/18/0 9 DUPLICATE • RESUL T SAMPL

E DUPLICATE EVALUATIO N REPOR T Genera l Chemistr y Wor k Orde r #... s LRE26-SM P LRE26-DU

P Dat e Received.. : 12/19/0 9

• Chlorin e 20 4 B N

D Matrix . A I R



### UNITS RP

D RP D . LIMI T METHO

D PREPARATION - PRE P ANALYSI S DAT E BATC H # SD Lot-Sampl e # : H9L210403-00 6 ua ; 20 0 (0-20 ) KNO X0050/26A'Mo

d12/21/0 9 935735 5 Dilutio nFactor : 480 0 NOTE(S ) : . Calculations ar

c performe

d befor e rounding l o avoid round-of ferror s i n calculate

d results. B Estimate

d result . Resul t i s les s tha n RL .



### VES01909 62 8



### Clien t Lo t #. . Dat e Sampled. . PARA M RESUL T . : H9L21040 3

. : 12/15/0 9 DUPLICATE RESUL T SAMPL

E DUPLICATE EVALUATIO N REPOR T Genera l Chemistr y Wor k Orde r #.,. : LRE 2 8 -SM P LRE28-DU

P Dat e Received.. : 12/19/0 9
Hydrogenchlorid e N D N

D Matrix . AI R

UNIT S RP

D RP D LIMI T METHO

D PREPARATION - PRE P ANALYSI S DAT E BATC H # S D LOt-Sampl e # : H9L210403-00 7 ng 0 (0-20 ) KNO X0050/26

A Mo d 12/22/0 9 935819 5 Dilutio nFactor s 1028.4 3



### VES01909 72 9



### Clien t Lo t H9L21040 3 Dat e Sample d: 12/15/0 9 SAMPL E DDPLICAT E EVALUATIO N EEPOR T Genera l Chemistr y Wor k Orde r #... : LRE29-SM P LRE29-DU

P Dat e Received.. : 12/19/0 9
PARA M RESUL T DUPLICATE

RESUL T Hydroge nchlorid e N D N

D Matrix . A I R



### UNIT S RP

D RP D . LIMI T METHO

D PREPARATION - PRE P ANALYSI S DAT E BATC H # S D Lot-Sampl e # : H9L210403-00 S u g 0 (0-20 ) KNO X0050/26

A Mo d 12/22/0 9 935819 5 Dilutio nFactor : 4113.7 2



### VES01909 83 0



### H9L21040 3 12/15/0 9 DUPLICATE RESUL T SAMPL

E DUPLICATE EVALUATIO N REPOR T Genera l Chemistr y Wor k Orde r #... : LRE3A-SM P LRE3A-DU

P Dat e Received.. : 12/19/0 9

N D 

### Matrix . AI R

UNIT S RP

D RP D LIMI T METHO

D PREPARATION- PRE P ANALYSI S DAT E • BATC H ft S D Lot-Sampl e # : H9L210403-00 9 u g 0 (0-20 ) KNO X0050/2S

A Mo d 12/21/0 9 935735 5 Dilutio nFactor : 100 0



### VES01909 93 1



# Sample Receip t

Documentation

VES01910 0

## Sampl e Traceability Lis t AECO M Sit s ofPronram : Veoli a E S Tec h Sampl o Date : vz/1 1 , - \t l iSf/ef t Prolec

t Location : Sauget, IL LabPO#' : Type o fProqram : CP T Dat e Shipped : ^JlSfot Laboratory : Tes t America , Inc, Project* : 6013321 6 Progra m Office : Syracus e NY Shipper

/ Steven . Mil o Recovery : Jef fGorman Laboratory : Knoxville, T N Progra m Contact : . Jef fGorma n FedE xAi rBil l # : He m Sampl e I D Cod e Sampl e Matri x Sampl e Descriptio n . Analytica l Parameter s Specia l Instructions 1 CPT-U4-HCL-.MP1-4- R 1 A . 0.1 N H2S04 Uni t 4 , Impinger

s H , Ru n 1 A HC L 2 ' 3 CPT-U4-CI2-IMP5 ^R' t O . l N NaO H Uni

t 4 , Impinger

s 5-6 , Ru n 1 A 5 a CPT-U4-HCL-IW1P 1 -4 - R 2 A 0.1 N H2S04 Uni t A, Impinger

s 1 -4 , Ru n 2 A HC L p\& O 7 CPT-U4-CI2-IMP5-6- R 2 0. 1 N NaO H Uni t 4 , Impinger

s 5-6 , Ru n 2 c b ypS a -ST f 0

O iA. L-

X3CrX\J 8 g CPT-U4-HCL-IMP1-4- R 3 A 0.1NH2SO 4 Uni t 4 , Impinger

s 1-4 . Ru n 3 A HC L

Hr* ' . ( 0 1 1 CPT-U4-CI2-IMP5-6- R 3 0. 1 N NaO H Uni t 4 , Impinger

s 5-6 , Ru n 3 CI 2 1 2 1 3 1 4 1 5 1 6 1 7 CPT-H20-FB-U 4 DI-H2 0 DI-H2

0 Fiel d Blan k

' HC L and CL 2 1 B CPT-HCL-FB-U 4 0.1 N H2S0 4 0.1 N H2S04 Fiel d Blan k HC L 1 9 CPT-CI2-FB-U 4 O.INNaO H O.INNaO H Fiel d Blan k CI 2 20 Fiel d Notes

/ Comment

s Pag e I off
_ Relinquishe

d B y(print) : Date : Steve n Mil o \Z\\8l<P\ Signature : . Time : JSi wno o Relinquishe d B y (print) : Date : Signature : Time : Relinquishe d B y(print) : Date : Signature : Time : Received b y Lab (print) : Date : Signature : Time : Received B

y (print) : .Date : Signature : Time :



# . aovv9 K^ Receive d B y(print) : Date : Signature : Time : Receive d B y(print) ; Date : Signature : Time : Analytical Laborator yDestination : TestAmeric a Inc. 581 5 Middlebrook

Pik e Knoxville, T N 37921 Attn : Mr. Kevi n Woodcoc k 865-291-300

0


### VES01910 1

## TESTAMERIC A KNOXVILL E SAMPL E RECEIPT/CONDITION UPO N RECEIP T ANOMAL Y CHECKLIS T Lo tNumber: W 'MAM

n U 

## 1 X Revie wItem s N o N A I fNo , wha t wa s th e problem ? Comments/Actions Take n 1 . D o sampl e containe

rlabel s matc h COC ? (IDs , Dates, Times

) 

# 1 •l a D o no t matc h CO C •l b Incomplet

e informatio

n •l c Markin g smeare

d •I d Label to

m Di e N o labe

l •l fCO C no

t receive d D l g Other: 1 . D o sampl e containe

rlabel s matc h COC ? (IDs , Dates, Times

) 

# 1 •l a D o no t matc h CO C •l b Incomplet

e informatio

n •l c Markin g smeare

d •I d Label to

m Di e N o labe

l •l fCO C no

t receive d D l g Other: 1 . D o sampl e containe

rlabel s matc h COC ? (IDs , Dates, Times

) 

# 1 •l a D o no t matc h CO C •l b Incomplet

e informatio

n •l c Markin g smeare

d •I d Label to

m Di e N o labe

l •l fCO C no

t receive d D l g Other: 1 . D o sampl e containe

rlabel s matc h COC ? (IDs , Dates, Times

) 

# 1 •l a D o no t matc h CO C •l b Incomplet

e informatio

n •l c Markin g smeare

d •I d Label to

m Di e N o labe

l •l fCO C no

t receive d D l g Other: 1 . D o sampl e containe

rlabel s matc h COC ? (IDs , Dates, Times

) 

# 1 •l a D o no t matc h CO C •l b Incomplet

e informatio

n •l c Markin g smeare

d •I d Label to

m Di e N o labe

l •l fCO C no

t receive d D l g Other: 1 . D o sampl e containe

rlabel s matc h COC ? (IDs , Dates, Times

) 

# 1 •l a D o no t matc h CO C •l b Incomplet

e informatio

n •l c Markin g smeare

d •I d Label to

m Di e N o labe

l •l fCO C no

t receive d D l g Other: 1 . D o sampl e containe

rlabel s matc h COC ? (IDs , Dates, Times

) 

# 1 •l a D o no t matc h CO C •l b Incomplet

e informatio

n •l c Markin g smeare

d •I d Label to

m Di e N o labe

l •l fCO C no

t receive d D l g Other: 1 . D o sampl e containe

rlabel s matc h COC ? (IDs , Dates, Times

) 

# 1 •l a D o no t matc h CO C •l b Incomplet

e informatio

n •l c Markin g smeare

d •I d Label to

m Di e N o labe

l •l fCO C no

t receive d D l g Other: 2 . I s th e coole rtemperatur

e withi n limits

? ( > freezing temp , o fwate r t o 6°C ; NC , 1668,1613B : 0-4"C ; VOST : 10°C ; MA : 2-6°C ) 

# J 1 D 2 a Tem p Blan k

= 2 . I s th e coole rtemperatur

e withi n limits

? ( > freezing temp , o fwate r t o 6°C ; NC , 1668,1613B : 0-4"C ; VOST : 10°C ; MA : 2-6°C ) 

# J 1 D 2b CoolerTem p = 2 . I s th e coole rtemperatur

e withi n limits

? ( > freezing temp , o fwate r t o 6°C ; NC , 1668,1613B : 0-4"C ; VOST : 10°C ; MA : 2-6°C ) 

# J 1 3 . . Wer e sample s receive d wit h correc t chemica

l preservativ

e (excluding Encore)

? 

# J D 3s i Sampl e preservativ

e = 1 3 . . Wer e sample s receive d wit h correc t chemica

l preservativ

e (excluding Encore)

? 

# J D 3s i Sampl e preservativ

e = 1 4 . Wer e custod y seal s present/intac

t o n coole rand/o r containers

? 

# 1 Ui 4) i No t presen t 0 4 b No t intac t D 4 c Other: 4 . Wer e custod y seal s present/intac

t o n coole rand/o r containers

? 

# 1 Ui 4) i No t presen t 0 4 b No t intac t D 4 c Other: 4 . Wer e custod y seal s present/intac

t o n coole rand/o r containers

? 

# 1 Ui 4) i No t presen t 0 4 b No t intac t D 4 c Other: 5 . Wer e al l ofth e sample

s liste d o n th e CO C received? 

# I •5 a Sample s received-no

t o n CO C •5b Sample

s notreceived-on CO C • 5 . Wer e al l ofth e sample

s liste d o n th e CO C received? 

# I •5 a Sample s received-no

t o n CO C •5b Sample

s notreceived-on CO C • S . Wer e al l ofth e sampl

e container

s receive d intact ? 

# 1 / D 6 a Leakin g D 6 b Broke

n S . Wer e al l ofth e sampl

e container

s receive d intact ? 

# 1 / D 6 a Leakin g D 6 b Broke

n 7 . Wer e VO A sample

s receive d withou t headspace

? V D 7 a Headspac

e (VO A only

) 8 , Wer e sample s receive d i n appropriat

e containers

? V 7 —i- •8 a Imprope

r containe

r 9 . Di d you chec

k fo rresidua

l chlorine , i fnecessary

? I •• 

# / •9

a Coul d no

t b e determine

d du e t o matri xinterferenc

e 9 . Di d you chec

k fo rresidua

l chlorine , i fnecessary

? I •• 

# / •9

a Coul d no

t b e determine

d du e t o matri xinterferenc

e 10 . Wer e sample s received withi n holding time ? J O 10 a Holdin g tim

e expire d 11 . Forra d samples

, wa s sampl e activit y info , provided? •Incomplet e infonnation 12 . For16I3B wate

r sample s is pH<9

? 

# J I fno , wa s p H adjuste

d t o p H 7 - 9 wit h sulfuri c acid? • 12 . For16I3B wate

r sample s is pH<9

? 

# J I fno , wa s p H adjuste

d t o p H 7 - 9 wit h sulfuri c acid? 13 . Ar e th e shipping container

s intact ? •13 a Leakin g 013 b Other: 13 . Ar e th e shipping container

s intact ? •13 a Leakin g 013 b Other: 14 . Wa s CO C relinquished ? (Signed/Dated/Timed ) 

# hf 014 n No t relinquishe

d 15 . Ar e tests/parameter

s liste d foreac h sample ? V •15 a Incomplet

e informatio

n 16 . I s th e matri xofth e sample

s noted ? 

## 1/ •I5 a Incomplet

e informatio

n 17 . I s tli e date/tim

e ofsampl

e collection noted

? 7 D 15 a Incomplet

e informatio

n 18 . I s th e clien t an d projec t name/ # identified ? 

# /

/ 0 15

a Incomplet

e informatio

n 19 . Wa s th e sample ridentifie d o n th e COC ? 

## / Ouote# : . P M Instructions :

. ( ^J\. ^ 

# . r-r - = : Sampl e Receiving 

# AssocWX

W Iflhlffl

Date:) 0 [ 2- i | 0 < 3 QA026R21 .doc , 09040 9

w

w 

## VES01910 23 43 5



# Sample Summar

y

VES01910 43 6



### AECOM , In c Clien t Sampl e ID ; CPT-U4-HCL-IMP1-4-R1 A Genera l Chemistr y Lot-Sampl e ft-..: H9L210403-00 1 Wor k Orde r #. . . : ' LRE2 0 Matri x. : AI R Dat e Sampled.- . 12/16/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H # Hydroge nchlorid e 3460 0 442 0 u g KNO X0050/2G

A Mo d 12/22/0 9 935819 5 Dilutio nFactor : 44222.4 6 HDL.. . s 190 0



### VES01910 53 7



### AECOM , in c Clien t Sampl e ID : CPTr 

### D4-CL2-IMP5-S-R l Genera l Chemistr y Lot-Sampl e tt...: H9L210403-00 2 Dat e Sampled: 12/16/0 9
PARAMETE

RRESUL T Wor

k Orde r #... : LRE2 2 Dat e Received.. : 12/19/0 9
R L UNIT S METHO D Matri x: AI R

PREPARATION

- PRE

P ANALYSI S DAT

E BATC H # Chlorin e N D 48 4 u g KNO

X0050/26

A Mo d 12/21/0 9 93573S 5 Dilutio nFactor : 484 0 MDI . = 20 0



### VES01910 63 8



### AECOM , In c Clien t Sampl e ID : CPT-D4-HCL-IMP1-4-R2 A Genera l Chemistr y Lot-Sampl e it. ..: H9L210403-00 3 Wor k Orde r #...- . LRE2 3 Matri x: AI R Dat e Sampled... : 12/17/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H tt Hydroge nchlorid e 4310 0 442 0 u g KNO X0050/26A

Mo d 12/22/0 9 93B819 5 Dilutio nFactor : 44222.4 6 MD L :190 0



### VES01910 73 9



### AECOM , In c Clxen t Sanipl e ID : CPT-04-CL2-IMP5-6-*R 2 _ Genera l Chemistr y Lot-Sampl e : H9L210403-00 4 Wor k Orde r : LRE2 4 Matri x: AI R Dat e Sampled... : 12/17/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESULT R L UNIT S METHO D ANALYSIS , DATE BATC H g Chlorin e 20 8 B 47 2 u g KNO X0050/26

A Mo d 12/21/0 9 935735 5 Dilutio nFactor : 4720 . MD L : 20 0 

### HOT S (S ) : ] ' R LReportin g limi t B Estimate

d result . Resul t i s les s tha n RL .



### VES01910 84 0



### AECOM , In c • Clien t Sampl e ID : CFT-04-HO.-IMP1-4-R3 A Genera l Chemistr y Lot-Sample*... : H9L210403-0Q5 Wor k Orde r #... : LRE2 5 Matri x: AI R Dat e Sampled... : 12/18/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESUL T R L UNIT S METHO D ANALYSI S DATE BATC H # Hydroge nchlorid e 364 0 169 0 u g KNO XO05O/26

A Mo d 12/22/0 9 935819 5 Dilutio nFactor ; 16866.2 4 MD L .. : 71 0



### VES01910 94 1



### AECOM , In c Clien t Sampl e ID : CPT-TJ4-CL2-IMP5-6-R 3 Genera l Chemistr y Lot-Sampl e #... : H9L210403-00 6 Wor k Orde r ft...: LRE2 6 Matrix... . : AIR Dat e Sampled... : 12/18/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESUL T R L UNIT S METHO D ANALYSI S DATE BATC H # Chlorin e 20 4 B 48 0 u g KNO X0050/26

A Mo d 12/21/0 9 935735 5 Dilutio nFactor. - 480 0 MD L : 20 0 

### NOTE(S ) : R L Reporting Limit B Estimate

d result. Resul

t i s les s tha n RL .



### VES01911 04 2



### AECOM , In c Clien t Sampl e ID : CPT-H20-FB-U 4 Genera l Chemistr y Lot-Sampl e #... : H9L210403-00 7 Wor k Orde r #..- : LRE2 B Dat e Sampled... : 12/15/0 9 Dat e Received.. : 12/19/0 9
PARAMETE

R RESUL T R L UNIT S METHO D Matrix . AIR

PREPARATION- PRE P ANALYSI S DATE BATC H # Hydrogenchlorid e N D 10 3 ug KNO X0050/26

A Mo d 12/22/0 9 Dilutio nFactor : 1026.4 3 MD L : 4 3 

### 935819 5



### VES01911 14 3



### AECOM , In c Clien t Sampl e ID : CPT-HCL-FB-U 4 Genera l Chemistr y Lot-Sampl e ft...: H9L21O403-OO 8 Dat e Sampled... : 12/15/0 9 Wor k Orde r #... : LRE2 9 Dat e Received.. : 12/19/0 9 Matri x: AI R

PARAMETE

R RESUL T R L UNIT S Hydroge nchlorid e N D 41 1 u g Dilutio nFactor : 4113.7 2 ' MD L : 1? 0 

### PREPARATION- PRE P METHO D ANALYSI S DAT E BATC H # ICNO X0050/26

A Mo d12/22/0 9 935819 5



### VES01911 24 4



### AECOM > In c Clien t Sampl e ID : CPT-CL2-PB-D 4 Genera l Chemistr y Lot-Sampl e tt...: H9L210403-00 9 Wor k Orde r #... : LRE3 A Matri x: AI R Dat e Sampled: 12/15/0 9 Dat e Received.. : 12/19/0 9

' PREPARATION- PRE P PARAMETE

RRESUL T R L UNIT S METHO D ANALYSI S DATE BATC H # Chlorin e N D 10 0 u g KNO

X0050/26A

Mo d 12/21/0 9 935735 5 Dilution . Factor : 100 0 MD L : 4 2



### VES01911 3

### 4 5



# Q C Summar

y

VES01911 44 6

METHO D BLAN KREPOR T 

### Genera l Oientistxy Clien t Lo t #... : H9L21040 3 Matri x. - AI R REPORTIN

GPREPARATION- PRE P PARAMETE

RRESUL

T LIMI T UNIT S METHO D ANALYSI S DAT E BATC H # Chlorin e Wor k Orde r # : LRLHD1A A M B Lot-Sample'# : H9L230000-35 5 N D 10. 0 u g ICNO X0050/26

A Mo d 12/21/0 9 935735 5 Dilutio nFactor : 10 0 

### Hydroge nchlorid e Wor k Orde r # : LRL131A A M B Lot-Sampl e # : H9L240000-19 5 N D 10. 3 ug KNO X005O/26

A Mo d 12/22/0 9 Dilutio nFactor : 102. 8
HOTECS ) ; , • ; Calculation

s ar e performe

d befor e roundin g io avoi d round-of

Terror s i n calculaie

d results . 935819 5 

# *

VES01911 54 7



### LABORATOR

YCONTROL , SAMPL

E EVALUATIO

N REPOR T Genera l Chemistr y Lot-Sampl e tt . . . : H9L21040 3 Matri x: AI R
PARAMETE

R Chlorin e PERCEN T RECOVER Y 9 8 10 3 RECOVER

Y LIMIT S RP

D RP D LIMIT S METHO

D PREPARATIONANALYSI S DAT

E PREP BATC H # WO#:LRLHD1AC-LCS/LRLHD1AD-LCS D LC S Lot-Sample# : H9L230000-35 5 (9 0 - 110 ) KNO X0050/26

A Mo d 12/21/0 9 935735 5 (9 0 - 110 ) 5. 0 (0-20 ) KNO X0050/26

A Mo d 12/21/0 9 935735 5 Dilutio nFactor : 10 0 

### Hydroge nchlorid e

10 0 9 8 WO#:LRL13.1AC-LCS/LRL131AD-LCS D LC S Lot-Sample# : H9L240000-19 S (9 0 - 110 ) KNO X0050/2S

A Mo d 12/22/0 9 935819 5 (9 0 - 110 ) 2. 0 (0-20 ) KNO X0050/26

A Mo d 12/22/0 9 935819 5 Dilutio nFactor : 102. 8

HOTE(S ) Calculaiion s ar

e performe

d befor e rounding i o avoid round-of ferror s i n calculate

d results.



### VES01911 64 8



### LABORATOR

YCONTRO

L SAMPL E DAT A REPOR T Genera l Chemistr y Lot-Sampl e #.'.. : H9L21040 3 Matrix . AI R
PARAMETE R Chlorin e 

### SPIK

E MEASURE

D AMOUN T AMOUN

T UNIT S PERCN T RECVR YRP D METHO

D PREPARATION- PRE P

. ANALYSI S DATE BATC H # WO#:LRLHD1AC-LCS/LRLHD1AD-LCS D LC S Lot-Sample# : H9L230000-35 5 75. 0 73. 7 u g 9 8 KNO X0050/26

A Mod . 12/21/0 9 935735 5 75. 0 77. 5 u g 10 3 . 5. 0 KNO X0G5O/26

A Mo d 12/21/0 9 935735 5 Dilutio nFactor : 10 0 

### Hydrogenchlorid e

77. 1 77. 1 WO#;LRL131AC-LCS/LRL131AD-LCS D LC S Lot-Samplet : H9L240000-19 5 77. 2 u

g 100 . KNO X0050/26

A Mo d 12/22/0 9 935B19 5 75. S u

g 9 8 2. 0 KNO X0050/26

A Mo d 12/22/0 9 935819 5 Dilutio nFactor : 102. B


### NOTEtS ) : Calculation

s ar e performe

d befor e rounding t

o avoid round-of

ferror s i n calculate

d results,



### VES01911 74 9



### MATRI XSPIKE SAMPL

E EVALUATIO

N REPOR T Genera l Chemistr y Clien t Lo t # - . . Dat e Sampled.. . : H9L21040 3

: 12/17/0 9 Matrix . AI R

Dat e Received.. : 12/19/0 9
PARAMETE

R Chlorin e PERCEN T RECOVER

Y RECOVER

YLIMIT S RP

D RP D LIMIT S METHO

D PREPARATIONANALYSI S DAT

E PRE P BATC H # 98 7 8 

### W0# : LRE24IAC-MS/LRE24lAD-MSD M S Lot-Sampl e # : H9L21O403-00 4 (7 5 - 125 ) KNO XOO50/2S

A Mo d 12/21/0 9 935735 5 (7 5 - 125 ) 1 8 (0-20 ) KNO X0050/26

A Mo d 12/21/0 9 935735 5 Dilutio nFactor : 472 0 

### Hydrogenchlorid e

10 7 (7 5 11 8 (7 5 W0# : LRE231AC-MS/LRE231AD-MS D M S Lot-Sampl e # : H9L210403-00 3 125 ) KNO X0050/26

A Mo d 12/22/0 9 935819 5 125 ) 1. 8 (0-20 ) KNO X0050/26A

Mo d 12/22/0 9 935819 5 Dilutio nFactor : 4422 2 NOTE(S) ; Calculaiions ar

e performe

d befor e rounding t

o avoi d round-of

ferror s i n calculaie

d results.



### VES01911 85 0



### MATRI XSPIKE SAMPL

E DAT A EEPOR T Genera l Chemistr y Cliea t Lo t #... : H9L21040 3 Dat e Sampled.... : 12/17/0 9 Dat e Received.. : 12/19/0 9 Matri x: AI R

SAMPL E SPIK E MEASR

D PARAMETE

R Chlorin e AMODN

T AM T 20 S 20 8 

### 94 4

94 4 PERCN T RECVR YRP D METHO

D PREPARATION- PRE P ANALYSI S DAT E BATC H # AMOUN T UNIT S . . . WO# : LRE241AC-MS/LRE24lAD-MSD M S Lot-Sampl e # : H9L210403-00 4 113 0 u

g 9 8 KNO X0050/26

A 12/21/0 9 935735 5 94 5 u

g 7 8 1 8 KNO X0050/26

A 12/21/0 9 935735 5 Dilutio nFactor : 472 0 

### Hydrogenchlorid e

.4310 0 8B4 0 4310 0 884 0 WO# : LRE231AC-MS/LRE23lAD-MSD M S Lot-Sampl e # : H9L21O403-00 3 52S0 0 ug 10 7 KNO X0050/26

A 12/22/0 9 935819 5 5350 0 u

g 11 8 1. 8 KNO X0050/26

A 12/22/0 9 935819 5 Dilutio nFactor : 4422 2 NOTE(S) : Calculation

s ar c pcribrme

d befor e rounding l o avoid round-of ferror s i n caioilnie

d results.



### VES01911 95 1



### Clien t Lo t 

# ii...: H9L21040 3 

### Dat e Sampled... : 12/16/0 9 SAMPL E DUPLICAT E EVALUATIO N REPOR T 

### Genera l Chemistr y Wor k Orde r 

# ii...:

LRE20-SMP LRE20-DU P 

### Dat e Received.. : 12/19/0 9 DUPLICATE RESUL T PARA M RESUL T Hydroge nchlorid e 3460 0 3590 0 Matrxx . A I R



### UNIT S RP

D RP D LIMI T METHO

D PREPARATION- PRE P ANALYSI S DATE BATC H #

~~ S D Lot-Sampl e # : H9L210403-OO1

u g

### 3. 7 {0-20 } KNO X0050/26A

Mo d 12/22/0 9 935819 5 Dilutio nFactor : 44222.4 6



### VES01912 05 2



### Clien t Lo t # . Dat e Sampled . PARA M RESUL T Chlorin e N D . : H9L210 4 0 3

. : 12/16/0 9 DDPLICATE RESUL T SAMPL

E DUPLICATE EVALUATIO N REPOR T Genera l Chemistr y Wor k Orde r #... : LRE22-SM P LRB22-DU

P Dat e Received.. : 12/19/0 9
UNIT S RP

D RP D LIMI T METHO

D Matri x: AI R

PREPARATION- PRE P ANALYSI S DAT E BATC H # S D Lot-Sampl e # : H9L210403-0O 2 21 1 B u

g 20 0 (0-20 ) KNO X0050/26

A Mo d 12/21/0 9 935735 5 Dilutio nFactor : 48 4 0 

### NOTE(S) = Calculaiion s ar

c pcrrornie

d beror e roundin

s l o avoi d round-or

ferror s i n calculate

d rcsulis . B Estimate

d result. Resul

t i s les s tha n RL .



### VES01912 15 3



### Clien t Lo t #... : H9L21040 3 Dat e Sampled... : 12/17/0 9 DUPLICATE PARA M RESULT RESUL

T Hydroge nchlorid e 4310 0 4400 0 SAMPL E DUPLICATE EVALUATIO N REPOR T Genera l Chemistr y Wor k Orde r #... : LRE23-SM P LRE23-DU

P Dat e Received.. : 12/19/0 9 Matrix . A I R



### UNIT S RP

D RP D LIMI T METHO

D PREPARATION- PRE P ANALYSI S DAT E BATC H # ' S D Lot-Sampl e # : H9L210403-0O 3 ug 2. 1 (0-20 ) KNO X0050/26

A Mo d 12/22/0 9 935819 5 Dilutio nFactor : 44222.4 6



### VES01912 25 4



### Clien t Lo t # . Dat e Sampled . PARA M RESULT SAMPL E DUPLICATE EVALDATIO H REPOR T Genera l Chemistr y

. : H9L.21040 3 Wor k Orde r #... t LRE24-SM P LRE24-DU

P

. : 12/17/0 9 Dat e Received.. : 12/19/0 9 DUPLICATE RESUL T UNIT S RP D RP D LIMI T METHO

D Matri x: AI R

PREPARATION- PRE P ANALYSI S DATE BATC H # Chlorin e 20 8 B N

D S D Lot-Sampl e # : H9L210403-00 4 u g 20 0 (0-20 ) KNO X0050/26A

Mo d 12/21/0 9 935735 5 Dilutio nPacto n472 0 

### NOTE(S) : Calculaiions ar

e performe

d beror e rounding t

o avoid round-of

Terror s i n calculate

d results . B Estimate

d result . Resul

t is les s tha n RL .



### VES01912 35 5

SAMPL E DUPLICAT E EVALUATIO N REPOR T 

### Genera l Chemistr y Clien t Lo t ft...: H9L21040 3 Wor k Orde r #.. . Dat e Sampled... : 12/18/0 9 LRE25-SM P LRE25-D0 P Dat e Received.. ; 12/19/0 9 Matrxx . . : AI R



### PARA W RESUL T DUPLICATE RESUL T UNITS RP

D RP D LIMI T METHO

D Hydroge nchlorid e

364 0 359 0 

### PREPARATION- PRE P ANALYSI S DAT E BATC H ft S D Lot-Sampl e # : H9L210403-00 5 u g 1. 5 (0-20 ) KNO X0050/26

A Mo d 12/22/0 9 935819 5 Dilutio nFactor : 1S8SS.2 4



### VES01912 45 6



### Clien t Lo t ft. Dat e Sampled . PARfl M RESUL T Chlorin e 204 B 

### . : H9L2104O3

. : 12/18/0 9 DUPLICATE RESUL T SAMPL

E DUPLICAT E EVALUATIO N REPOR T Genera l Chemistr y Wor k Orde r ft...: LRE26-SM P LRE26-DU

P

. Dat e Received.. : 12/19/0 9

N D Matrox . AI R

UNIT S RP

D RP D LIMI T METHO

D PREPARATION- PRE P ANALYSI S DAT E BATC H ft SD Lot-Sampl e ft: H9L210403-00 6 u g 20 0 (0-20 ) KNO X0O5O/26

A Mo d 12/21/0 9 93S735 5 Dilutio nFactor : 480 0 NOTE(S ) : Calculiiion s ar

c pcrrormc

d befor e rounding io avoid round-of ferror s i n calculate

d results. B Estimate

d result . Resul t is les s tha n RL .



### VES01912 5

### 5 7

Clien t LO

C #...: ' H9L21040 3 Dat e Sampled... : 12/15/0 9 DDPLICATE PARA M RESUL T RESUL

T Hydroge nchlorid e N D N

D SAMPL

E DUPLICAT E EVALUATIO N REPOR T Genera l Chemistr y Wor k Orde r LRE2B-SM P LRE2B-DU

P Dat e Received.. : 12/19/0 9 Matrix . AI R

UNIT S RP

D RP D LIMI T METHO

D PREPARATION - PRE P ANALYSI S DATE BATC H # S D Lot-Sampl e # : H9L210403-00 7 u g 0 (0-20 ) KNO X0050/26

A Mo d 12/22/0 9 935819 5 Dilutio nFactor : 1028.4 3



### VES01912 65 8



### Clien t Lo t # . . . : H9L21040 3 Dat e Sampled... : 12/15/0 9 SAMPL E DUPLICAT E EVALUATIO N REPOR T 

### Genera l Chemistr y Wor k Orde r #... r LRE29-SM P LRE29-DU

P Dat e Received.. : 12/19/ 0 9
PARA M RESUL T DUPLICATE RESUL T Hydroge nchlorid e N D N

D Matrxx . . : AI R

UNIT S RP

D RP D LIMI T METHO

D PREPARATION- PRE P ANALYSI S DAT E BATC H # S D Lot-Sampl e # : H9L210403-00 8 u g 0 (0-20 ) KNO X0050/26

A Mo d 12/22/0 9 935819 5 Dilutio nFactor : 4113.7 2



### VES01912 7

### 5 9

Clien t Lo t #=

. Dat e Sampled . PARA M RESUL T Chlorin e N D SAMPL E DUPLICAT E EVALUATIO N REPOR T Genera l Chemistr y H9L21040 3 Wor k Orde r #. . 12/15/0 9 LRE3A-SM P LRE3A-DC

P Dat e Received.. : 12/19/0 9 DUPLICATE RESUL T UNIT S RP D RP D LIMI T METHO

D Matri x: AI R

PREPARATION- PRE P ANALYSI S DATE BATC H # N D S D Lot-Sampl e # : H9L210403-00 9 ug 0 (0-20 ) KNO X0050/26A

Mo d 12/21/0 9 935735 5 Dilutio nFactor : 100 0



### VES01912 8

# Metho d 0023A

VES01912 9

# •Vist a Analytica l Laborator

y


### Januar y 12 , 201 0 

### Vist aProjec tLD. : 3231

3 Mr . Jeffrey Gorman AJECO M Environment 5015 Campuswoo d Driv e Suit e 10 4 East.Syracuse , N Y 13057-4232 DearMr . Gorman , Enclose d ar

e th e result s fo rth e fou rMM 5 samples receive d a tVist aAnalytica l Laborator y on December19, 200 9 underyou rProjectNam e "60133216" . Thes e samples wer e extracted an

d analyzed using Metho d 0023 A fo rtetra-through-oct achlorinated dioxin s an d furans . Th e fron tan d bac khalves wer

e extracted and analyze d separatel y fo rsample

s CPT-U4-M23-XAD-R1 , -R 2 an d -R3 . A standar

d turnaround tim e wa s provide d fo rthis work . The followin g repor

tconsist

s o f aSampl e Inventor

y (Sectio n I) , Analytica l Result s (Sectio n II

) an d th e Appendix , whic h contains th e chain-of-custody , alis to f dat aqualifier s and abbreviations , Vista' s curren

tcertifications , and copie s o f the rawdat

a(i f requested) . 7ist aAnalytica l Laboratory i s committe d t o servin g yo u effectively . I f yo u require additional information , please contac tme a t916-673-152 0 o rb y emai l a tmmaier@vista-analytical.com . Thankyo u fo rchoosin g Vist aa s par to f you ranalytical suppor tteam. Sincerely ,

Marth aM . Maie r Laborator

y Directo r

Vtsta Anaiyiicai

Laboratory

certifies

that the report herein meets all Ihe requirements

set forth by NELAC for those applicable 'fi, test

methods. Results

relate only to the samples

as received

by the laboratory. This

report should not be reproduced

except tnfull without the written approval

of Visla Analytical

Laboratory.

Vist a Analytica

l Laborator

y I 1104Windfiel

d Wa y| E l Dorad o Hills,C A 9576 2 I ph : 916-673-152

0 [ fx : 916-673-010

6 I wwww.vista-analytical.co m Pro jec t 3231 3 Pag e 1 o f1 8 

### VES01913 0

# Wist a

Sectio n I : Sampl

e Inventor

y Repor t Dat e Received : 12/19/200 9 

### Projec tNo. : 3231 3 

### Projec tName: 6013321 6

Lab . Sampl e I D Clien tSampl e I D Componen tID 001 CPT-U4-M23A-XAD-R 1 BH R XA D 00 2 CPT-U4-M23A-PF-R 1 FH R FILTE R 00 3 CPT-U4-M23A-XAD-R 2 BH R XA D 00 4 CPT-U4-M23A-PF-R 2 FH R FILTE R 00 5 CPT-U4-M23A-XAD-R 3 BH R XA D 00 6 CPT-U4-M23A-PF-R 3 FH R FILTE R 00 7 CPT-M23A-U4-F B ACE/MeC12/TO L FILTE R XA D

Smpinvgnmm5.rpi

Projec t 3231 3 Page 2 o f 1 8 

### VES01913 1

# Vvist a

SECTIO N I

I

Projec t 3231 3 Page 3 o f1 8 

### VES01913 2Metho d Blan k 

### Metho d 0023 A Matrix : MM 5 Q C Batc h No. : 268 0 La b Sample : 0-MB00 1 Sampl e Size : Sample Dat e Extracted : 1-Jan-1 0 Dat e Analyzed DB-5 : 9-Jan-1 0 Dat e Analyze d DB-225 : N A Analyt e Cone . (pg/Sample ) D L aEMPC bQualifier s Labele d Standar d % R LCL-UCL d Qualifier s 2,3,7,8-TCD D N D I S 13C-2,3,7,8-TCD D 95. 9 4 0 -13 5 1,2,3,7,8-PeCD D N D 0.41 1 13C-1,2,3,7,8-PeCD D 88.5 4 0 - 13 5 1,2,3,4,7,8-HxCD D N D 13C-1,2,3,6,7,8-HxCD D 93. 6 4 0 -13 5 1,2,3,6,7,8-HxCD D N D 0.53 3 13C-l,2,3,4,6,7,8-HpCD D 98.6 4 0 - 13 5 1,2,3,7,8,9-HxCD D 13C-OCD D 94. 9 4 0 -13 5 1,2,3,4,6,7,8-HpCD D N D 0.66 7 l3C-2,3,7,8-TCD F 90.5 40-13 5 OCD D N D • 1.3 7 ' 13C-l,2,3,7,8-PeCD F 82.9 4 0 - 13 5 2,3,7,8-TCD F N D 0.29 4 13C-l,2,3,6,7,8-HxCD F 95. 1 40-13 5 1,2,3,7,8-PeCD F N D 13C-1,2,3,4,6,7,8-HpCD F 98. 1 4 0 - 13 5 2,3,4,7,8-PeCD F N D 0.31 9 13C-OCD F 94.4 40-13 5 1,2,3,4,7,8-HxCD F N D 0.36 8 :.;^. V A^: f >-;U ' P S 37Cl-2,3,7,8-TCD D 92. 9 70-13 0 1,2,3,6,7,8-HxCD F N D 0.37 5 13C-2,3,4,7,8-PeCD F 84.4 7 0 - 13 0 2,3,4,6,7,8-HxCD F N D 0.41 7 13C-l,2,3,4,7,8-HxCD D 97. 9 70-13 0 1,2,3,7,8,9-HxCD F N D 0.44 2 13C-l,2,3,4,7,8-HxCD F 95.4 7 0 - 13 0 1,2,3,4,6,7,3-HpCD F N D ' -•'0.759 : ' : V"•'• : ^ ; v-" : .'- - 13C-l,2,3,4,7,8,9-HpCD F 97. 9 7 0 - 13 0 1,2,3,4,7,8,9-HpCD F N D 0.89 6 A S 13C-l,2,3,7,8,9-HxCD F 98. 1 4 0 - 13 5 OCD F 0.91 5 Total s Toxi c Equivalen t Quotien t (TEQ ) Dat a e Tota l TCD D N D 0.32 2 TE Q (Min-Max) : 0-1.0 7 Tota l PeCD D N D Tota l HxCD D N D 0.50 6 a. Sampl e specifi cestimate

d detectio

n limit. Tota l HpCD D N D 0.66 7 b . Estimate d maximu

m possible concentration. Tota l TCD F N D 0.29 4 c . Method detectio n limit. Tota l PeCD F 

### N D 0 30

9 d . Lowe rcontro l limit? , uppe

rcontro l Hmit. . • • '

. Tota l HxCD F N D 0.40 0 e . TE Q base

d o n (1989) Internationa

l Toxi cEquivalentFactor s (ITEF) . Tota l HpCD F N D 0.82 8
- Analyst : MA S Approve d By : Marth a M . Maie r 12-Jan-201 0 13:4 1 Projec t 3231 3 Page 4 o f1 8 

### VES01913 3OP RResults 

### Metho d 0023 A
Matrix : MM 5 Q C Batc h No. : 268 0 La b Sample : 0-OPR00 1 Sampl e Size : Sample Dal e Extracted : l-Jan-1 0 Dat e Analyzed DB-5 : 8-Jan-1 0 Dat e Analyze d DB-225 : N A Analyt e Spik e Cone . Cone . (ng/mL ) O P R Limit s Labele d Standar d % R LCL-UC L Qualifie r 2,3,7,8-TCD D 2.5 0 2.0

0 I S 13C-2,3,7,8-TCD D 88. 7 4 0 - 13 5 1,2,3,7,8-PeCD D 12. 5 10.9 8.7 5 - 16.2 5 13C-l,2,3,7,8-PeCD D 85.3 40-13 5 1,2,3,4,7,8-HxCD D 12. 5 10.

8 8.7

5 - 16.2 5 13C-l,2,3,6,7,8-HxCD D 90. 8 40-13 5 1,2,3,6,7,8-HxCD D 12. 5 10.

7 8.7

5 - 16.2 5 13C-l,2,3,4,6,7,8-HpCD D 90.5 40-13 5 1,2,3,7,8,9-HxCD D 12. 5 10.8 8.7 5 - 16.2 5 13C-OCD D 87.3 40-13 5 1,2,3,4,6,7,8-HpCD D 12. 5 10.

7 8.7

5 - 16.2 5 13C-2,3,7,8-TCD F 86.4 40-13 5 OCD D 25.0 20. 8 17. 5 - 32.5 13C-l,2,3,7,8-PeCD F 84.9 4 0 - 13 5 2,3,7,8-TCD F 2.5 0 1.9

8 1.75-3.2 5 13C-l,2,3,6,7,8-HxCD F 90.4 40-13 5 1,2,3,7,8-PeCD F 12. 5 10. 7 8.7 5 - 1 6 2 5 13C-l,2,3,4,6,7,8-HpCD F 88.7 4 0 - 13 5 2,3,4,7,8-PeCD F 12. 5 10.6 8.7 5 - 16.2 5 13C-OCD F 87. 1 40-13 5 1,2,3,4,7,8-HxCD F 12. 5 10.9 8.7 5 - 16.2 5 A S 13C-l,2,3,7,8,9-HxCD F 90.5 40-13 5 1,2,3,6,7,8-HxCD F 12. 5 10.

9 8.7

5 - 16.2 5 2,3,4,6,7,8-HxCD F 12. 5 10.9 8.7 5 - 16.2 5 1,2,3,7,8,9-HxCD F 12. 5 10.9 8.7 5 - 16.2 5 1,2, 3 4,6,7,8-HpCD F 12. 5 10.6 8.7 5 - 16.2 5 1,2,3,4,7,8,9-HpCD F 12. 5 10.

8 8.7

5 - 16.2 5 OCD F 25.0 21. 2 17.5-32. 5 Analyst : MA S Approve d By : Marth a M . Maie r12-Jan-201 0 13:4 1

Projec t 3231 3 Page 5 o f1 8 

### VES01913 4

### Sample ID : CPT-U4-M23A-XAD-R 1 

### Metho d 0O23 A Clien tDat a Sampl e Dat a Laborator y Dat a Name : AECO M Environment Project : 6013321 6 Date Collected : 16-Dec-0 9 Time Collected : N A Matrix : Sampl e Size : MM 5

Sample La b Sample : 32313-001

Q C Batch No. : 268 0 Dat e Analyze d DB-S : 9-Jan-1 0 Dat e Received : Dat e Extracted : Date s Analyze d DB-225 : 19-Dec-0 9

l-Jan-1 0 10-Jan-1 0 Analyt e Cone . (pg/Sample ) D L a EMPC b Qualifier s Labele d Standar d % R LCL-UCL d Qualifier s 2,3,7,8-TCD D 18. 5 I § 13C-2,3,7,8-TCD D 89.9 4 0 -13 5 1,2,3,7,8-PeCD D 27 5 13C-l,2,3,7,8-PeCD D 87. 4 4 0 - 13 5 1,2,3,4,7,8-HxCD D 29 8 13C-l,2,3,6,7,8-HxCD D 92. 9 4 0 - 13 5 1,2,3,6,7,8-HxCD D 85 9 13C-1,2,3,4,6,7,8-HpCD D 93.3 4 0 - 13 5 1,2,3,7,8,9-HxCD D 34 1 13C-OCD D 90. 1 40-13 5 1,2,3,4,6,7,8-HpCD D 258 0 13C-2,3,7,8-TCD F 88. 1 4 0 - 13 5 OCD D 98 5 13C-l,2,3,7,8-PeCD F 87. 7 40-13 5 2,3,7,8-TCD F 86.5 13C-l,2,3,6.7,8-HxCD F 95.3 40-13 5 1,2,3,7,8-PeCD F 12 6 13C-l,2,3,4,6,7,8-HpCD F 92. 0 4 0 - 13 5 2,3,4,7,8-PeCD F 57 8 13C-OCD F 88.4 40-13 5 1,2,3,4,7,8-HxCD F 26 4 £ S 37Cl-2,3,7,8-TCD D 86. 5 7 0 - 13 0 1,2,3,6,7,8-HxCD F 34 3 P 13C-2,3,4,7,8-PeCD F 85. 5 70-13 0 2,3,4,6,7,8-HxCD F 79 6 13C-l,2,3,4,7,8-HxCD D 95.2 70-13 0 1,2,3,7,8,9-HxCD F 85.6 13C-1,2,3,4,7,8-HxCD F 97.5 7 0 - 13 0 1,2,3,4,6,7,8-HpCD F 86 7 13C-l,2,3,4,7,8,9-HpCD F 93.0 7 0 - 13 0 1,2,3,4,7,8,9-HpCD F 11 1 A S 13C-l,2,3,7,8,9-HxCD F 95. 1 4 0 - 13 5 OCD F 16 5 Total s Toxi c Equivalen t Quotien t (TEQ ) Dat a e Tota l TCD D 845 0 846 0 TE Q (Min-Max) : 796-79 6 Tota l PeCD D 1620 0 Tota l HxCD D 1690 0 a . Sample specifi cestimate d detectio

n limit. Tota l HpCD D 599 0 ' b. Estimate d maximu

m possibl e concentration. . Tota l TCD F 1260 0 P c. Method detectio n limit. Tota l PeCD F 1320 0 P : d. Lowe rcontro l limit- uppe

rcontro l limit . Tota l HxCD F 788 0 P e . TE Q base

d on (1989) Internationa l Toxi cEquivalentFactor s (ITEF) . Tota l HpCD F 210 0 Analyst : MA S Approve d By : Marth a M . Maie r12-Jan-201 0 13:4 1 Projec t 3231 3 Pag e 6 o f1 8 

### VES01913 5

# V \ ' 

# t a Sampl e ID : CPT-U4-M23A-PF-R 1 

### Metho d 0023 A Clien tDat a Sampl e Dat a Laborator y Dat a Name : AECO M Environment Project : 6013321 6 Date Collected : 16-Dec-0 9 Tim e Collected : N A Matrix : Sample Size : MM 5

Sample La b Sample : 32313-00 2 Q C Batch No. : 268 0 Dat e Analyze d DB-5 : 9-Jan-1 0 Dat e Received : 19-Dec-09 Dat e Extracted : 1-Jan-1 0 Dat e Analyze d DB-225 : N A Analyt e Cone . (pg/Sample ) D L a EMPC b Qualifier s Labele d Standar d % R LCL-UCL d Qualifier s 2,3,7,8-TCD D N D I S 13C-2,3,7,8-TCD D 94.6 40-13 5 1,2,3,7,8-PeCD D 14. 1 J 13C-l,2,3,7,8-PeCD D 93.4 4 0 - 13 5 1,2,3,4,7,8-HxCD D 13C-l,2,3,6,7,8-HxCD D 97. 1 4 0 - 13 5 1,2,3,6,7,8-HxCD D 64.5 13C-l,2,3,4,6,7,8-HpCD D 10 2 40-13 5 1,2,3,7,8,9-HxCD D 37.2 13C-OCD D 9 6 4 4 0 - 13 5 1,2,3,4,6,7,8-HpCD D 36 4 13C-2,3,7,8-TCD F 93.0 4 0 - 13 5 OCD D 26 3 13C-l,2,3,7,8-PeCD F 92. 1 4 0 - 13 5 2,3,7,8-TCD F 3.6 6 J 13C-l,2,3,6,7,8-HxCD F 97. 1 40-13 5 1,2,3,7,8-PeCD F 6.4 7 13C-l,2,3,4,6,7,8-HpCD F 10 0 4 0 - 13 5 2,3,4,7,8-PeCD F 30. 1 J 13C-OCD F 95.0 40-13 5 1,2,3,4,7,8-HxCD F 17. 8 E § 37Cl-2,3,7,8-TCD D N A 7 0 - 13 0 1,2,3,6,7,8-HxCD F 24. 4 J, P 13C-2,3,4,7,8-PeCD F N A 70 - 13 0 2,3,4,6,7,8-HxCD F 64.4 13C-l,2,3,4,7,8-HxCD D N A 7 0 - 13 0 1,2,3,7,8,9-HxCD F 10. 9 j 13C-l,2,3,4,7,8-HxCD F N A 70 - 13 0 1,2,3,4,6,7,8-HpCD F 90.0 13C-l,2,3,4,7,8,9-HpCD F N A 70-13 0 1,2,3,4,7,8,9-HpCD F 20. 9 J M 13C-l,2,3,7,8,9-HxCD F 99.7 40-13 5 OCD F 44.7 j Total s Toxi c Equivalen t Quotien t (TEQ ) Dat a e Tota l TCD D 18 4 TE Q (Min-Max) : 51.9-52. 3 Tota l PeCD D 58 7 58 9 Tota l HxCD D 115 0 a . Sampl e specifi cestimate

d detection limit. Tota l HpCD D 74 5 ^b\Estiina ^ Tota l TCD F 24 2 25 6 c. Method detectio n limit. Tota l PeCD F 42 3 - ' P d. Lowe rcontro l lirnit- uppe

rcontrol limi t Tota l HxCD F 46 1 P e . TE Q base

d on (1989) Internationa l Toxi cEquivalen

tFactor s (ITEF) . Tota l HpCD F 24 0 Analyst : MA S Approve d By . Marth a M . Maie r12-Jan-201 0 13:4 1 Projec t 3231 3 Pag e 7 o f1 8 

### VES01913 6I i 

# V \ t a Sampl e IB : CPT-U4-M23A-XAD-R 2 

### Method 0O23 A Clien t Dat a Sampl e Dat a Laborator y Dat a Name : AECO M Environment Project : 6013321 6 Date Collected : 17-Dec-0 9 Tim e Collected : N A Matrix : Sample Size : MM 5

Sample La b Sample : 32313-00 3 Q C Batch No. : 268 0 Dat e Analyze d DB-5 : 9-Jan-1 0 Dat e Received : 19-Dec-0 9 Dat e Extracted : 1-Jan-1 0 Date s Analyze d DB-225 : - 10-Jan-1 0 Analyt e Cone . (pg/Sample ) D L a EMPC b Qualifier s Labele d Standar d % R LCL-UCL d Qualifier s 2,3,7,8-TCD D 24. 0 I S 13C-2,3,7,8-TCD D 94. 8 4 0 - 13 5 1,2,3,7,8-PeCD D 32 7 13C-l,2,3,7,8-PeCD D 85.8 40-13 5 1,2,3,4,7,8-HxCD D 26 6 13C-l,2,3,6,7,8-HxCD D 93.6 4 0 - 13 5 1,2,3,6,7,8-HxCD D 79 1 13C-l,2,3,4,6,7,8-HpCD D 93. 0 40-13 5 1,2,3,7,8,9-HxCD D 35 6 13C-OCD D 85.0 4 0 - 13 5 1,2,3,4,6,7,8-HpCD D 209 0 13C-2,3,7,8-TCD F 90. 9 40-13 5 OCD D 71 1 13C-1,2,3,7,8-PeCD F 88.0 4 0 - 13 5 2,3,7,8-TCD F 83.8 13C- 1,2,3,6,7,8-HxCD F 97.7 40 - 13 5 1,2,3,7,8-PeCD F 13C-l,2,3,4,6,7,8-HpCD F 94.4 40-13 5 2,3,4,7,8-PeCD F 48 4 13C-OCD F 84.0 40-13 5 1,2,3,4,7,8-HxCD F F i 37Cl-2,3,7,8-TCD D 90. 1 7 0 - 13 0 1,2,3,6,7,8-HxCD F 26 8 P 13C-2,3,4,7,8-PeCD F 86. 3 70 - 13

0 2,3,4,6,7,8-HxCD F 13C-l,2,3,4,7,8-HxCD D 93. 3 7 0 - 13 0 1,2,3,7,8,9-HxCD F 45. 9 J 13C-l,2,3,4,7,8-HxCD F 10 3 7 0 - 13 0 1,2,3,4,6,7,8-HpCD F 63 8 13C-l,2,3,4,7,8,9-HpCD F 88. 5 7 0 - 13 0 1,2,3,4,7,8,9-HpCD F 57.5 A S 13C-l,2,3,7,8,9-HxCD F 92.8 40-13 5 OCD F 85. 9 J Total s Toxi c Equivalen t Quotien t (TEQ ) Dat a e Tota l TCD D 804 0 TE Q (Min-Max) : 72 3 - 72 3 Tota l PeCD D 1630 0 Tota l HxCD D 1550 0 a Sample specifi cestimate d detectio

n limit. Tota l HpCD D 480 0 b . Estimate d maximu

m possibl

e concentratio

n Tota l TCD F 1350 0 c . Method detectio

n limit . Tota l PeCD F 1300 0 d : IJower.contro l limit - uppe

rcontro l limit. * • Tota l HxCD F 623 0 p e . TE Q base

d on (1989) Internationa l Toxi cEquivalentFactor s (ITEF) . Tota l HpCD F 130 0 Analyst : MA S Approve d By : Marth a M . Maie r12-Jan-201 0 13:4 1 Projec t 3231 3 Page 8 o f1 8 

### VES01913 7

# \ V 

# V 

# t a Sampl e ID : CPT-U4-M23A-PF-R2 

### Method 0O23 A Clien tDat a Sampl e Dat a Laborator y Dat a Name : AECO M Environment Project : 6013321 6 Dat e Collected : 17-Dec-09 Time Collected : N A Matrix : Sample Size : MM 5

Sample La b Sample : 32313-00 4 Q C Batch No. : 268 0 Dat e Analyzed DB-5 : 9-Jan-1 0 Dat e Received : 19-Dec-0 9 Dat e Extracted : l-Jan-1 0 Dat e Analyze d DB-225 : j\J A Analyte Cone . (pg/Sample ) D L a EMPC b Qualifier s Labele d Standar d % R LCL-UCL d Qualifier s 2,3,7,8-TCD D N D ' 0.56 9 I S 13C-2,3,7,8-TCD D 87.4 40-13 5 1,2,3,7,8-PeCD D 12.9 J 13C-l,2,3,7,8-PeCD D 79.7 40-13 5 1,2,3,4,7,8-HxCD D 20.5 J 13C-1,2,3,6,7,8-HxCD D 89. 3 40-13 5 1,2,3,6,7,8-HxCD D 62.5 13C-1,2,3,4,6,7,8-HpCD D 85. 3 40-13 5 l,2,3;7,8,9-HxCD D 28. 6 J 13C-OCD D 78.5 4 0 - 13 5 1,2,3,4,6,7,8-HpCD D 35 2 13C-2,3,7,8-TCD F 84. 2 40-13 5 OCD D 27 6 13C-1,2,3,7,8-PeCD F 76. 9 4 0 - 13 5 2,3,7,8-TCD F 3.6 6 J 13C-1,2,3,6,7,8-HxCD F 90.6 40-13 5 1,2,3,7,8-PeCD F 6.5 7 13C-l,2,3,4,6,7,8-HpCD F 86.0 4 0 - 13 5 2,3,4,7,8-PeCD F 26.4 J 13C-OCD F 79.5 4 0 -13 5 1,2,3,4,7,8-HxCD F 17 9 P S 37Cl-2,3,7,8-TCD D N A 7 0 -13 0 1,2,3,6,7,8-HxCD F 24. 0 J. P 13C-2,3,4,7,8-PeCD F N A 7 0 - 13 0 2,3,4,6,7,8-HxCD F 61. 0 13C-l,2,3,4,7,8-HxCD D : N A 70-13 0 1,2,3,7,8,9-HxCD F 10. 4 j 13C-l,2,3,4,7,8-HxCD F N A 7 0 - 13 0 1,2,3,4,6,7,8-HpCD F 91.6 13C-1,2,3,4,7,8,9-HpCD F . N A 70-13 0 1,2,3,4,7,8,9-HpCD F 21. 4 j A S 13C-l,2,3,7,8,9-HxCD F 89.7 40-13 5 OCD F 47. 0 J Total s Toxi c Equivalen t Quotien t (TEQ ) Dat a e Tota l TCD D 17 4 TE Q (Min-Max) : 47. 8 - 48.4 Tota l PeCD D 52 4 Tota l HxCD D 109 0 a . Sample specifi cestimate d detectio

n limit. Total'HpCD D 72 1 b . Estimate d maximu

m possible concentration. Tota l TCD F 21 8 23 0 c . Method detection limit. Tota l PeCD F 401 d . Lowercontio l limi t- uppe rcontro l limit.-:: ; ; Tota l HxCD F 46 2 p e . TE Q base

d on (1989) Internationa l Toxi cEqu h alen

tFactor s (ITEF) . Tota l HpCD F A242f ; :.; : Analyst : MA S Approve d By : Marth a M . Maie r12-Jan-201 0 13:4 1 Projec t 3231 3 Pag e 9 o f1 8 

### VES01913 8

# t a Sampl e ID : CPT-U4-M23A-XAD-R3 

### Metho d 0O23 A Clien tDat a Name : Project : Date Collected : Time Collected : AECO M Environment

6013321 6 18-Dec-09 N A Sampl e Dat a Matrix : MM 5 Sampl e Size: Sampl e Laborator y Dat a La b Sample : Q C Batch No. : Dat e Analyze d DB-5 : 32313-00 5 Dat

e Received : 19-Dec-0 9 268 0 Dat

e Extracted : J - Jan-1 0 9-Jan-1 0 Date s Analyze d DB-225 : 10-Jan-1 0 Analyt e Cone . (pg/Sample ) D L EMPC U Qualifier s Labele d Standar d % R LCL-UCL " Qualifier s 79.5 4 0 13 5 85. 5 40 - 13

5 96. 8 40 - 13

5 97.2 40 - 13

5 94.5 40 - 13

5 71.4 40 - 13

5 82. 1 40 - 13

5 10 5 40 - 13

5 98.7 40 - 13

5 92.2 40 - 13

5 70. 0 70 - 13

0 69.4 70 - 13

0 81.4 70 - 13

0 82.5 70 - 13

0 52.6 70 - 13

0 96. 1 40 - 13

5 2,3,7,8-TCD D 2 0 3 1,2,3,7,8-PeCD D 29 3 1,2,3,4,7,8-HxCD D 25 9 1.2.3.6.7.8

- HxCD D 81 7 1.2.3.7.8.9

- HxCD D 34

7 1,2,3,4,6,7,8-HpCD D 238 0 OCD D 81 2 2,3,7,8-TCD F 85.5 1,2,3,7,8-PeCD F 14 1 2,3,4,7,8-PeCD F 64 7 1,2,3,4,7,8-HxCD F 26 3 1,2,3,6,7,8-HxCD F 34 3 2.3.4.6.7.8

- HxCD F 74

9 1.2.3.7.8.9

- HxCD F 70. 8 1.2.3.4.6.7.8

- HpCD F 87

0 1.2.3.4.7.8.9

- HpCD F 96. 6 OCD F 13 5 I S 13C-2,3,7,8-TCD D 13C-l,2,3,7,8-PeCD D 13C-l,2,3,6,7,8-HxCD D 13C-l,2,3,4,6,7,8-HpCD D 13C-OCD D 13C-2,3,7,8-TCD F 13C-1,2,3,7,8-PeCD F ; M 13C-l,2,3,6,7,8-HxCD F 13C-1,2,3,4,6,7,8-HpCD F 13C-OCD F ? S 37Cl-2,3,7,8-TCD D 13C-2,3,4,7,8-PeCD F . 13C-l,2,3,4,7,8-ILxCD D 13C - 1,2,3,4,7,8-HxCD F 13C-l,2,3A7,8,9-HpCD F A S 13C-1,2,3,7,8,9-HxCD F Total s Toxi c Equivalen t Quotien t (TEQ ) Dat a Tota l TCD D Tota l PeCD D Tota l HxCD D Tota l HpCD D Tota l TCD F Tota l PeCD F Tota l HxCD F Tota l HpCD F 753 0 15i00 1560 0 568 0 1390 0 1520 0 786 0 200 0 TE Q (Min-Max) : 825-82 5

aSampl e specifi cestimate

d detectio

n limit. b . Estimate

d maximu

m possible concentration. c . Method detectio

n limit . d. Lowercontro

l limi t- uppe

rcontro l limi t e . TE Q base

d o n (1989) Internationa l Toxi cEquivalen

tFactor s (ITEF) . Analyst : MA S Approve d By : Marth a M . Maie r12-Jan-201 0 13:4 1 Projec t 3231 3 Pag e 1 0 o f 1 8 

### VES01913 9

# V \>t a Sampl e ID : CPT-U4-M23A-PF-R3 

### Metho d 0 0 23 A Clien tDat a Sampl e Dat a Laborator y Dat a Name : AECO M Environment Project : 6013321 6 Dat e Collected : 18-Dec-0 9 Tim e Collected : N A Matrix : Sample Size : MM 5

Sample La b Sample : 32313-00 6 Q C Batch No. : 268 0 Dat e Analyze d DB-5 : 9-Jan-1 0 Dat e Received : j 9^Dec-0 9 Dat e Extracted : l-Jan-1 0 Dat e Analyze d DB-225 : N A Analyt e Cone . (pg/Sample ) D L a EMPC b Qualifiers Labele d Standar d % R LCL-UCL d Qualifier s 2,3,7,8-TCD D N D 0.381 l § 13C-2.3,7,8-TCD D 85. 7 4 0 - 13 5 1,2,3,7,8-PeCD D 17. 7 J 13C-l,2,3,7,8-PeCD D 82. 2 40-13 5 1,2,3,4,7,8-HxCD D 27. 0 13C-1,2,3,6,7,8-HxCD D 8 9 8 40-13 5 1,2,3,6,7,8-HxCD D 84.3 13C-l,2,3,4,6,7,8-HpCD D 94.7 4 0 - 13 5 1,2,3,7,8,9-HxCD D 4 1 3 13C-OCD D 91. 7 4 0 - 13 5 1,2,3,4,6,7,8-HpCD D 51 5 13C-2,3,7,8-TCD F 87. 8 4 0 - 13 5 OCD D 37 7 13C-l,2,3,7,8-PeCD F 82. 1 40-13 5 2,3,7,8-TCD F 4.8 5 J 13C-l,2,3,6,7,8-HxCD F 91.9 40-13 5 1,2,3,7,8-PeCD F 9.7 8 J 13C-l,2,3,4,6,7,8-HpCD F 92.9 4 0 - 13 5 2,3,4,7,8-PeCD F 45.3 J 13C-OCD F 92.2 40-13 5 1,2,3,4,7,8-HxCD F 28.4 J P S 37Cl-2,3,7,8-TCD D . . '• ' N A 70-13 0 1,2,3,6,7,8-HxCD F 36.3 J, P 13C-2,3,4,7,8-PeCD F N A 7 0 - 13 0 2,3,4,6,7,8-HxCD F 99. 1 13C-l,2,3,4,7,8-HxCD D : •;NA : ' 7 0 - 13 0 1,2,3,7.8,9-HxCD F 15. 8 J 13C-l,2,3,4,7,8-HxCD F N A 70-13 0 1,2,3,4,6,7,8-HpCD F -;AB7:y.# ; i ; -S; : ' : '".,./- v 13C-l,2,3,4,7,8,9-HpCD F •": : ; :N A: - 70-13 0 1,2,3,4,7,8,9-HpCD F 33.5 J M lSC-l^.SJ.S^-HxCD F 90.3 4 0 - 13 5 OCD F 66. 1 J Total s Toxi c Equivalen t Quotien t (TEQ ) Dat a e Tota l TCD D 231 23 5 TE Q (Min-Max) : 72. 9 - 73. 3 Tota l PeCD D 73 9 Tota l HxCD D 151 0 a . Sampl e specifi cestimate

d detectio

n limit. Tota l HpCD D 112 0 b . Estimate d maximu

m possible concentration. Tota l TCD F 36 8 c. Metho d detectio n limit. Tota l PeCD F 661 66 4 > : ;p , ; d . Lowercontro l limi t- uppe

rcontrol'limi t Tota l HxCD F 72 6 P e , TE Q base

d on (1989) Internationa l Toxi cEquivalentFactor s (ITEF) . Tota l HpCD F 39 9 Analyst : MA S Approve d By : Marth a M . Maie r 12-Jan-201 0 13:4 1
Projec t 3231 3 Page 1 1 o f1 8 

### VES01914 0

# W;t a Sampl e DD: CPT-M23A-U4-F B 

### Metho d 0O23 A Clien t Dat e Sampl e Dat a Laborator y Dat a Name : AECO M Environment Project : 6013321 6 Dat e Collected : 18-Dec-0 9 Tim e Collected : N A Matrix : Sampl e Size : MM 5

Sample La b Sample : 32313-00 7 Q C Batch No. : 268 0 Dat e Analyze d DB-5 : 9-Jan-1 0 Dat e Received : 19-Dec-0 9 Dat e Extracted : l-Jan-1 0 Dat e Analyze d DB-225 : N A Anaiyt e Cone . (pg/Sample) D L a EMPC b Qualifier s Labele d Standard % R LCL-UCL d Qualifier s 2,3,7,8-TCD D N D 0.32 9 I S 13C-2,3,7,8-TCD D 91. 9 4 0 - 13 5 1,2,3,7,8-PeCD D N D 0.45 7 13C-l,2,3,7,8-PeCD D 87.9 4 0 - 13 5 1,2,3,4,7,8-HxCD D N D 0.67 4 13C-1,2,3,6,7,8-HxCD D 4 0 - 13 5 1,2,3,6,7,8-HxCD D N D 0.70 9 13C-l,2,3,4,6,7,8-HpCD D 98.8 4 0 - 13 5 1,2,3,7,8,9-HxCD D N D 0.63 4 13C-OCD D 95.6 40-13 5 1,2,3,4,6,7,8-HpCD D N D 0.75 4 13C-2,3,7,8-TCD F 90.4 4 0 - 13 5 OCD D 20.2 13C-l,2,3,7,8-PcCD F 86.6 4 0 - 13 5 2,3,7,8-TCD F N D 0.41 0 13C-l,2,3,6,7,8-HxCD F 95.3 40-13 5 1,2,3,7,8-PeCD F N D 0.43 4 13C-l,2,3,4,6,7,8-HpCD F 95.7 4 0 - 13 5 2,3,4,7,8-PeCD F 1.3 3 J 13C-OCD F 95.6 40-13 5 1,2,3,4,7,8-HxCD F N D 0.63 5 E S 37Cl-2,3,7,8-TCD D 89.0 7 0 - 13 0 1,2,3,6,7,8-HxCD F N D 0.64 8 13C-2,3,4,7,8-PeCD F 87.0 70-13 0 2,3,4,6,7,8-HxCD F "N D 0.72 0 13C-1,2,3,4,7,8-HxCD D 96.2 70-13 0

. 1,2,3,7,8,9-HxCD F N D 0.76 3 13C-l,2,3,4,7,8-HxCD F 94.7 70-13 0 1,2,3,4,6,7,8-HpCD F 6.2 5 J 13C-1,2,3,4,7,8,9-HpCD F , 97.2 70-13 0 1,2,3,4,7,8,9-HpCD F N D 0.87 8 A S 13C-l,2,3,7,8,9-HxCD F 92. 1 4 0 - 13 5 OCD F N D 0.81 0 Total s Toxi c Equivalen t Quotien t (TEQ ) Dat a e Tota l TCD D 1.6 4 TE Q (Min-Max) : 0.748-1.8 6 Tota l PeCD D N D 0.45 7 Tota l HxCD D N D 0.67 2 a . Sample specifi cestimate d detectio

n limi t Tota l HpCD D N D 0.75 4 i b . Estimate d maximu

m possible concentration : ' Tota l TCD F 4.4 9 c. Metho d detection limit. Tota l PeCD F 8.0 3 d. Lowe rcontrol limit- uppe rconSo l limit . Tota l HxCD F 4.71 e . TE Q base

d on (1989) Internationa l Toxi cEquivalentFactor s (ITEF) . Tota l HpCD F 6.2 5 Analyst : MA S Approve d By : Marth a M . Maie r12-Jan-201 0 13:4 1 Projec t 3231 3 Page 1 2 o f1 8 

### VES01914 1

# Wist a

APPENDI X

Page 1 3 of1 8 

### VES01914 2

# Wist a DAT A QUALIFIER S & ABBREVIATION S

B Thi s compoun d wa s als o detecte d i n th e metho d blank. D Dilution E Th e amoun tdetecte d i s abov e th e High Calibration Limit . PThe amoun treporte

d i s th e maximu

m possibl

e concentratio

n du e t o possibl e chlorinate

d diphenylethe

rinterference. HRecover

y wa s outsid e laborator

y acceptanc

e limits . I Chemica l Interferenc

e J Th e amoun tdetecte d i s belo w th e Lo wCalibration Limit . * Se

e CoverLetter Cone. Concentratio n D L Sample-specifi cestimate

d detectio

n limit MD L Th e minimu m concentratio

n o f asubstanc

e tha tca n b e measure

d an d reported wit

h 99% confidenc

e tha tth e analyt e concentratio

n i s greate r tha n zer o in th e matrix tested. EMP C Estimate d Maximu

m Possibl

e Concentratio

n N A Notapplicabl e R L Reporting Limi t- concentration s tha tcorrespon

d t o lo wcalibration poin

t N D NotDetecte d TE Q ToxicEquivalenc y
Unles s otherwis

e noted, soli

d sampl e result s ar e reporte d i n dr y weight . Tissu e sample s ar e reporte d inwe tweight .

Projec t 3231 3 Pag e 1 4 o f1 8 

### VES01914 3

# Vvist a
CERTIFICATION S

Accreditin g Authorit y Certificat e Numbe r 

### Stat e o fAlaska , DE C CA413-200 8 Stat e o fArizon a AZ063 9 Stat e o fArkansas , DE Q 08-043- 0 Stat e o fArkansas , DO H Reciprocit y throug h C A Stat e o fCaliforni a - NELA P Primar y A A 02102C

A Stat e o fColorad o N/ A Stat e o fConnecticut PH-018 2 Stat e o fFlorida , DE P E8777 7 Stat e o fIndian a Departmen

t o fHealt h C-CA-02 Commonwealt

h o fKentuck

y 9006 3 Stat e o fLouisiana , Health an d Hospital s LA0800 0 Stat e o fLouisiana , DE Q 0197 7 Stat e o fMaine 200802 4 Stat e o fMichigan 993 2 Stat e o fMississipp i Reciprocit y throug h C A Nava l Facilitie

s Engineerin g Servic

e Cente r NFESC41 3 Stat e o fNevad a CA004132007 A Stat e o fNe wJerse y CA00 3 Stat e o fNe wMexic o Reciprocit y throug h CA Stat e o fNe wYork , DO H 1141 1 Stat e o fNort h Carolin a 0670 0 Stat e o fNort h Dakota , DO H R-07 8 Stat e o fOklahoma D991 9 Stat e o fOrego n CA200001-00 6 Stat e o fPennsylvani a 68-0049 0 Stat e o fSouth Carolin a 8700200 1 Stat e o fTennessee TN0299 6 Stat e o fTexas T104704189-08-T X U.S . Arm y Corps o

fEngineer

s N/

A Stat e o fUtah CA1640 0 Commonwealt

h o fVirgini a 0001 3 Stat e o fWashingto n C128 5 Stat e o fWisconsi n 99803616 0 Stat e o fWyomin g 8TMS- Q

Projec t 3231 3 Pag e 1 5 of1 8 

### VES01914 4I


### ^2-3/3 , 

# S-Vc, Anklet Sampl e Traceabilit

y Lis t Sit e o fProgram : Veoli a E S Tec h Sampl e Date : tPJ/6- lAfiPJo** Project Location : Sauget , I L La b P O Typ e o fProgram : CP T Date Shipped : * JZ/tfyoH Laboratory : Vist a Analytica l E l Dorad o Hills , C A Pro]ect# : 6013321 6 Progra m Office : Syracus e N Y Shippe r/ Steve n Mil o Recovery : Jef fGorma n Laboratory : Vist a Analytica l E l Dorad o Hills , C A Progra m Contact : Jef fGorma n FedE xAi rBU I # : Ite m Sampl e I D Cod e Sampl e Matri x Sampl e Descriptio n Analytica l Parameter s Specia l Instruction s 1 CPT-U4-M23A-XAD-R 1 XAD2 RESI N M23 XA D Resi n Trap , Ru n 1 PCDDs/PCDF s EP A 0023A 2 CPT-U4-M23A-PF-R 1 FILTE R M23 P M Filter , Ru n 1 PCDDs/PCDF s EP A 0023A 3 • 4 CPT-U4-M23A-XAD-R 2 XAD2 RESI N M23 XA D Resi n Trap , Ru n 2 PCDDs/PCDF s EP A 0023 A 5 CPT-U4-M23A-PF-R 2 FILTE R M23 P M Filter , Ru n 2 PCDDs/PCDF s EP A 0023 A 6 7 CPT-U4-M23A-XAD-R 3 XAD 2 RESI N M23 XA D Resi n Trap , Ru n 3 PCDDs/PCDF s 8 CPT-U4-M23A-PF-R 3 FILTE R M23 P M Filter , Ru n 3 PCDDs/PCDF s 9 1 0 CPT-M23A-PF-U4-F B FILTE R Particulat e Filte rFiel d Blan k PCDDs/PCDF s EP A 0023 A 1 1 C PT- M 2 3 A-XAD-U4- F B XAD 2 RESI N Xad Resi n Tra p Fiel d Blan k PCDDs/PCDF s EP A 0023 A 1 2 CPT-M23A-U4-Fiel d Blan k Acetone/MeCI^Toiuen e M23 Blan k PCDDs/PCDF s EP A 0023 A 1 3 1 4 CPT-U4-M23A-FHR-R 1 Acetone/MeClaToluen e M23A Front Hal fRinse , Ru n 1 PCDDs/PCDF s EP A 0023 A 1 5 CPT-U4-M23A-FHR-R 2 Acelone/MeCi^Toluen e M23A Front Hal fRinse , Ru n 2 PCDDs/PCDF s EP A 0023 A 1 6 CPT-U4-M23A-FHR-R 3 Acetone/MeCl^Toluen e M23A Front Hal fRinse , Ru n 3 PCDDs/PCDF a EPA0023 A 1 7 1 8 CPT-U4-M23A-BHR-R 1 Acetone/MeClaTolUBn e M23A Bac k Hal fRinse , Ru n 1 PCDDs/PCDF s EP A 0023A 1 9 CPT-U4-M23A-BHR-R 2 Acetone/MeClaToluen e M23A Bac k Hal fRinse , Ru n 2 PCDDs/PCDF s EP A 0023 A 2 0 CPT-U4-M23A-BHR-R 3 Acetone/MeCVToluen e M23A Bac k Hal fRinse , Ru n 3 PCDDs/PCDF s EP A 0023 A Fiel d N Dtes

/ Comment

s Pag e 1 of1 Relinquished B

y (print) : Date ; Steve n Mil o M/t</70J Signature : ^ . Time : Relinquished By (print) : Date : Signature : Time : Relinquished B y (print) : Date : Signature : Time : iReceived b y La b (print) : Date : Signature : Time :
Signature : Time : Received By (print) : Date : Signature : Time : Receive d B y (print) : Date : Signature : Time : Vista Analytica l Laboratories , Inc . 1104WindfieldWay E l Dorad o Hills , C A 9576 2 | Attn : Ms . Marth a Maie r916-673-152 0 Projec t 3231 3 Pag e 1 6 o f1 8 

### VES01914 5

### SAMPL E LOG-J N CHECKLIS T
Vist a Project* : \*h 

# V># 

# Vist a WAnalytica l Laborator y

Sample s Arrival : Date/Tim e Initials : Location : 

### (jjv^- ^ Shelf/Rack : Logge d In : Date/Tim e Initials : Location : ^ Shelf/Rack : fO/ A Delivere d By : 

### (^FedS^ ) UP S Ca l 

### DH L n Hari d 

### . Other Delivere d Preservation : Ic e (^Bkte Ice^ ) 

### Dr

y Ic e Non

e Temp° C Time : Thermomete rID : IR- 1 

### Sfffllli^ ^ YE S NO N A Adequat e Sampl e Volum

e Received ? Holdin g Tim e Acceptable ? Shippin g Container(s

) Intact ? Shippin g Custod

y Seal s Intact

? Shippin g Documentation Present? Airbil l Trk # <£U % S U

?
. ^TZ

J O Sampl e ContainerIntact ? Sampl e Custod

y Seal s Intact

? > 

### Chai n o fCustod y / Sample Documentation Present? CO C Anomaly/Sampl e Acceptanc e For m completed ? I fChlorinate

d orDrinking Water Samples , Acceptabl e Preservation ? Na 2 

### S 2 

### 0 3

### Preservatio n Documented ? Shippin g Container^^/ist a ^ Client /•^RetairT ^ Return Dispos e

p p - p £ Projec t 323 1 3 Sample Login 3/2007 rmh Pag e 1 7 o f1 8 

### VES01914 6

### SAMPL E LOG-I N CHECKLIS T Vist a Projec

t #: 

# Vn/ist a W Analytica l Laborator y


### Sample s Arrival : Date/Tim e initials : Location: ^ Shelf/Rack : W 1 A " Logge d In : Date/Tim e Initials : Location : ^ —/ Shelf/Rack : AV/ 1 

### Delivered By : . ^FedEx 5 

### ^ I UP S Ca l D H L

### Delivere d ° ^ Preservation : ^ ^__^-4c e Blue Ic e Dr

y Ic e ('Non e ^ Temp° C I \YV A^V ~ Time : 

### [QZPl Thermomete rID : IR- 1
Adequat e Sampl e Volume Received ? Holdin g Time Acceptable ? Shippin g Container(s

) Intact ? Shippin g Custod

y Seal s Intact

? Shippin g Documentation Present? Airbil l 

# Trk# < 

# g0 6 

# ?( p Sl\7 Vl^ Sampl e Containe rIntact ? Sampl e Custod

y Seal s Intact

? Chai n o fCustod y / Sample Documentation Present? CO C Anomaly/Sampl e Acceptanc e For m completed ? I fChlorinate

d o rDrinking Water Samples , Acceptabl e Preservation ? Na 2 

### S 2 

### 0 3

### Preservatio n Documented ? Shippin g Containe r Vist a CO C
Comments: 

### rf'



### Sampl e Containe r Retai n rf

rf

Retur n

Projec t 323 1 3 Sample Login 3/2007 rmh Page 1 8 o f1 8 

### VES01914 7

# Wast e Fee d

i 

### VES01914 8TestAmeric a Laboratories , Inc
.



## ANALYTICA L REPOR T

PROJECT NO . 6013321 6 Veoli a - E S Tec h Lo t # : H9L21040 4

Jef f Gorma

n AECOM , In c 510 5 Cairrpuswoo

dDriv e Suit e 10 4 Eas t Syracuse , N

Y1305 7

TESTAMERIC

A LABORATORIES , INC .

Kevi nS . Woodcock Projec t Manage r

Januar y

21 , 201 0

581 5 Middlebroo

kPik e Knoxville, T

N 3792 1 te l 865.291.300

0 fa x865.584.431

5 www.tesiamericainc.co m
i 

### VES01914 9

## ANALYTICA L METHOD S SUMMAR Y H9L21040 4

ANALYTICA L PARAMETE

RMETHO D As hConten t AST M D482-00 a Hea t o f CombustionAST M D240-0 2 Hea t o f CombustionD586 5 AST M D5865-0 0 Tota l Chlorin e KNO XWC-001S References : AST M Annua l Boo

k Of AST

M Standards . KNO XTestAmeric a Laboratorie s Inc. , Knoxvill e Laborator y Standar d Operatin g Procedur e

### 3 

## SAMPL E SUMMAR Y H9L21040 4
SAMPLE D SAM P W O # SAMPLE * CLIEN T SAMPL

E ID DAT E LRE3 3 00 1 HBTU-U4-M23A-R 1 12/16/0 9 LRE3 4 00 2 HBTU-TJ 4 -M23A-R

2 12/17/0 9 LRE 3 5 00 3 HBTU-U4-M23A-R 3 12/18/0 9 LRE 3 6 00 4 LBTU-U4-M23A-R 1 12/16/0 9 LRE 3 7 00 5 LBTLT-U4-M23A-R 2 12/17/0 9 LRE 3 8 00 6 LBTU-U 4 -M 2 3A-R 3 12/18/0 9 LRE4 C 00 7 SF-U4-M23A-R 1 12/16/0 9 LRE4 D 00 8 SF-U4-M23A-R 2 12/17/0 9 LRE4 F 00 9 SF-U4-M23A-R 3 12/18/0 9 LRE4 G 01 0 CS-U4-M23A-R 1 12/16/0 9 LRE4 H O i l CS-U4-M23A-R 2 12/17/0 9 LRE4 J 01 2 CS-U4-M23A-R 3 12/18/0 9 LRE4 K 01 3 BS-U4-M23A-R 1 12/16/0 9 LRE4 L 01 4 BS-U4-M23A-R 2 12/17/0 9 LRE4M 01 5 BS-U4-M23A-R 3 12/18/0 9 LRE4 N 01 5 HBTU-U4-M26A-R 1 12/16/0 9 LRE4 P 01 7 HBTU-U4-M2SA-R 2 12/17/0 9 LRE4 Q 01 8 HBTU-U4-M26A-R 3 12/18/0 9 LRE4 R 01 9 LBTU-U4-M 2 6A-R 1 12/16/0 9 ;LRE4T 02 0 LBTU-TJ4-M 2 6A-R 2 12/17/0 9 LRE4V 02 1 LBTU-U4-M26A-R 3 12/18/0 9 LRE4 W 02 2 SF-U4-M26A-R 1 12/16/0 9 LRE4 X 02 3 SF-U4-M26A-R 2 12/17/0 9 LRE4 0 02 4 SF-U4-M26A-R 3 12/18/0 9 LRE4 3 02 5 CS-U4-M26A-R 1 12/16/0 9 LRE4 4 02 6 CS-U4-M26A-R 2 12/17/0 9 LRE4 5 02 7 CS-U4-M26A-R 3 12/1B/0 9 LRE4 6 02 8 BS-U4-M26A-R 1 12/16/0 9 LRE4 7 02 9 BS-TJ4-M26A-R 2 12/17/0 9 LRE4 8 03 0 BS-U4-M26A-R 3 12/18/0 9 NQTE(S ) : :

- Th e analyfea l rcsul u o fth e sample s Iisre d abov e ar e presente

d on the followin g page s
•Al l calculiicn s ar

e performe

d befor e roundin g l o avoi d round-of ferror s i n calculate

d results .

- Result s note d a s "ND " wer

e no t detecte d a t orabov e the state

d limit .

- Thi s repo

n mus t no t b e reproduced , excep

t i n full , withou

t th e writte n approva l o

fth e laboratory

.

- Result s forth e followin g parameter

s ar e neverreporte

d on a dr y weigh t basis : color , corrosiviiy , density , flashpoinL , ignitability , layers , odor, pain t filietiest , pH . porosit

y pressure

, reactivity, redo

xpoiemial , specifi c gravity , spo t tests , solids , solubility , temperature , viscosity, an

d weight .

I



### VES01915 1

### 4 

# PROJEC T NARRATIVE H9L21040 4 Th e result

s reporte

d herein ar

e applicable t

o th e sample

s submitte

d fo ranalysis only . Thi s repor

tshal l no tb e reproduce

d excepti n full , withou tth e writte n approva

l o f th e laboratory. 

### The origina

l chai n o f custod y documentatio

n i s include d wit h thi s report . Sampl e Receip t Custody seal

s wer e notpresent

. 

### Qualit y Contro l an d Dat aInterpretatio

n Unles s otherwis

e rioted, al l holdin g times an d Q C criteriawer

e me tan d th e tes tresult s show n i n thi s repor tmee tal l applicable NELA C requirements . As h Content : Th e as h conten to f th e sample

s wa s determine

d using SO Pnumbe

rKNOX-WC-001 3 (base d o n AST M Methods A4422 , D482 , an d E830) . A te

n gra m aliquoto f

sampl e i s fired i n apre-tare

d crucibl e a

t750 ° ±25 ° C i n aforced-draf tmuffl e furnace . The tota l weigh to f as h residu e an d th e crucibl e is measure d on a4-plac

e analytica

l balance, an

d th e residu e weigh tis determine

d by difference . The ratio o f th e residu e weigh t(mg ) an d th e initial sampl

e weigh t(kg ) is use d t o calculat

e th e as h conten tofth e sample. Th e duplicat

e RP D resultfo rsampl e LBTU-U4-M26A-R 3 is outsid e contro l limits . The laborator

y contro l sample showe

d acceptabl

e result s indicating tha

tth e analysis wa

s i n control . The duplicat e resul ti s attribute

d t o sampl e heterogeneity. Gross Calorifi cValue : Th e hea to f combustion (gros

s calorifi cvalue) ofth e sample s wa s determine

d using SO P numbe rKNOX-WC-001 0 (base d on AST M Method D5865 fo rsolids an d AST M Method D24 0 fo rliquids) . A wast e feed sample i s combuste d i n a n oxyge n bom b tha tha s bee n placed i n abom

b calorimeter. Th e energ y release

d during this combustion proces s is
TestAmeric

a Knoxvill e maintain s th e followin g certifications , approval

s an daccreditations : Arkansa

s DE Q La b#88 - 0688 , Californi

a DH S ELA P Cert . #2423 , Colorad

o DPHE , Connecticu

t DP H La b#PH-0223 , Florid

a DO H La b #E87177 , Georgi

a DN RLa b#906 , Hawai

i DOH , Illinoi

s EP A La b#200012 , Indian

a DO H La b#C-TN-02 , Iow

a DN R La b#375 , Kansa

s DH E Cert . #E-I0349 , Kentuck y DE P La b#90101 , Louisian

a DE Q Cert . #03079 , Louisian

a DOHH , Marylan dDO E Cert . #277 , Michiga

nDE Q La b#9933 , Nevad

a DEP , Ne

w Jerse y DE P La b#TN00i , Ne

w Yor k DO H La b# 1 0781 , Nort

hCarolin a DP H La b#21705 , Nort

hCarolin a DEHN RCert . #64, Ohi

o EP A VA P La b#CL0059 , Oklahom a DE Q La b#9415, Pennsylvani

a DE P La b#68-00576 , Sout

hCarolin a DHE C Cer t #84001001 , Tennesse

e DO H La b#02014 , Texa

s CEQ , Uta

hDO H La b# QUAN3 , Virgini

a DG S La b#00165 , Washingto

nDO E La b#C1314 , Wes t Virgini a DE P Cert . #345 , Wes

t Virgini a DHH RCer t #9955C , Wisconsi

nDN RLa b#998044300 , Nava

l Facilitie s Engineerin g Servic e Cente r an dUSD A Soi l Permi t #S;46424 . Thi

s lis t o f approval s i s subjec t t o chang e an ddoe s no t impl y tha t laborator y certificatio

ni s availabl e fo r al l parameter

s reporte di nthi s environmenta

l sampl e dat a report .

I 

### VES01915 2

# PROJEC T NARRATIVE H9L21040 4 capture d i nth e calorimeter, and th

e temperatur

e rise o f awate rbat h surroundin

g th e bom b is measured. Th e temperatur e rise i s proportiona

l t o th e hea tliberate d during th

e combustion i ncalories . Th e gross calorifi cvalue is calculate d from th

e temperatur

e rise, th e sampl e weight , an d th e calibration coefficiento f th e calorimeter. Certain extraneou s source s o f hea tar e assessed, an

d th e effecto f

thes e hea tsource s i s accounte

d fo ri n th

e calculation , a

s well a s th e affecto f

various accelerant

s tha tar e adde d t o enhanc

e combustion o f

th e sample. Th e gross hea to f combustio

n i s calculated i nunit

s o f cal/ g using th e followin g equation :

Q(gross 

### ) =

### [(AtEE)-(e 1 + 

### e 2 + 

### e 3+e4 

### ) ] m Where : Q (gross) = gros s calorifi cvalu

e a tconstan tvolum e a s determined, cal/g . E E = th

e hea tcapacit y o f th e calorimeter, cal/°C . A t= correcte

d temperatur

e rise a s measure

d by th e calorimeter, °C . e i = Correction fo rhea to f formation o f

nitricaci d i n calories , calculated b y th e calorimeterbased on th e energ y release d b y th e sample. e 2 = Correction fo rsulfur , which is usually 0 . e j = Correction fo rfuse wire . e 4 = Correction fo rspik e addition tha

tis calculate

d b y th e calorimete

rusing th e spik e weigh tbenzoi caci d equivalen t(grams ) time s th e benzoic aci d hea to f combustion (631 8 cal/gram) . m = mas

s o f th e sample, g

. Th e result

s ar e converte

d t o Btu/lb , a

s necessar

y using th

e followin g conversion factor : 1 Btu/l b = 1.

8 cal/gra

m The duplicat

e RP D result

s fo rsample

s LBTU-U4-M26A-R 3 & BS-U4-M26A-R 2 ar e outside control limits . Th e sample and/orduplicat e result s ar e below th

e reporting limit an d ar e reporte d a s estimate

d values . Th e laborator y contro l sampl e showe d acceptabl

e result s indicating tha

tth e analysis wa

s i n control . The result s ar e attribute

d t o sampl e heterogeneit

y an d increase

d method variabilit

y a tlevels below th

e reportin

g limit . Total Chlorine : The sample

s wer e prepare

d fo rtota

l chlorine using SO Pnumbe rKNOX-WC-001 6 (base d onAST M Method E44 2 an d SW-84 6 Metho d 5050) . Th e sampl e is oxidize d by combustion i n a

noxyge n flas ka

tatmospheri

cpressur

e o rabom b containing oxygen unde rpressure. The liberate d halogen compound

s ar e absorbe

d primarily a

s halides i n a sodium carbonate/sodiu m bicarbonat

e buffersolution . The combustion product s ar e collected b

y repeate

d rinsin g o f

th e combustion apparatus, an d analyzed b

y io n

# PROJEC T NARRATIVE H9L21040 4 chromatograph

y i n accordanc

e wit h SO PBCNOX-WC-0005 (base d o n SW-84 6 Method 9056) . The result

s ar e calculated using th

e followin g equation : 

### Q =

### -com

* com_ x

### lOOOff/f e W
concentration o f

analyt e i nth e sample, mg/kg . concentration o f

analyt e inth e combustate, mg/L . tota l volume o f

combustate

, L . weigh to f sampl e combusted , g . Th e duplicat

e RP D resultfo rsampl e BS-U4-M26A-R 3 is outsid e control limits . The laborator

y contro l sample showe

d acceptabl

e result s indicating tha

tth e analysis wa

s in control . The duplicat

e resul tis attiibute

d t o sampl e heterogeneity. Where : C 

### c co m Vco m 

### W

### 7 

## Q C DAT A ASSOCIATIO N SUMMAR Y

H9L21040 4


### Sampl e Preparation , an d Analysi s Contro l Number s

SAMPLE # 00 1 MATRIX

WAST E WAST E WAST E ANALYTICA

L METHO D AST M D482-00 a KNO XWC-001 6 AST M D240-0 2 LEAC H BATC H # PRE

P BATC H # 001120 8 001104 4 001204 8 M

S RUN #

00 2

00 3

00 4

00 5 WAST

E AST

M D482- 0 0 a WAST E KNO

XWC-001 6 WAST E AST

M D240-0 2 WAST E AST

M D482-00 a WAST E KNO

XWC-001 6 . WAST E AST

M D240-0 2 WAST E AST

M D482-00 a WAST E KNO

XWC-001 6 WAST E AST

M D240-0 2 WAST E AST

M D482-00 a WAST E KNO

XWC-001 6 WAST E AST

M D240-0 2 '001120 8 001104 4 001204 8 001120 8 001104 4 001204 8 001120 8 001104 4 001204 8 001120 8 001104 4 001204 8 001110 8

001102 2 001201 9

00 6

00 7

00 8 WAST

E AST

M D482-00 a WAST E KNO

XWC-001 6 WAST E AST

M D240-02 . WAST E AST

M D482-00 a WAST E KNO

XWC-001 6 WAST E AST

M D240-0 2 WAST E • AST

M D482-00 a WAST E KNO

XWC-001 6 WAST E AST

M D240-0 2 001120 8 001104 4 001204 8 001120 8 001104 4 001204 8 001120 8 001104 4 001204 8 00 9 WAST

E AST

M D482-00 a WAST E KNO

XWC-001 6 WAST E AST

M D240-0 2 001120 8 001104 4 001204 8 01 0 SOLI D AST M D482-00 a SOLI D KNO

XWC-001 6 SOLI D AST

M D5865-0 0 000527 4 000703 6 001302 8 01 1 SOLI D AST M D482-O0 a SOLI D KNO

XWC-001 6 SOLI D AST

M D5865-0 0 000527 4 000703 6 001302 8 (Continue do

nnex t page )



### VES01915 58 

## Q C DAT A ASSOCIATIO N SUMMAR Y

H9L21040 4
Sampl e Preparatio nan d Analysi s Contro l Number s

SAMPLE # 01 2

01 3 MATRI

X SOLI D SOLI D SOLI D SOLI D SOLI D SOLI D ANALYTICA L METHO D AST M D482-O0 a KNO XWC-001 6 AST M D5865-0 0 AST M D482-O0 a KNO XWC-001 6 AST M D5865-0 0 LEAC H BATC H # PRE

P BATC H tt 000527 4 000703 6 001302 8 000527 4 000703 6 001302 8 M

S K0N# 

### 000514 2 000701 6 001301 3

01 4

01 5

01 6

01 7 SOLI D AST M D482-00 a SOLI D KNO

XWC-001 6 SOLI D AST

M D5865-0 0 SOLI D AST

M D 4 82-00 a SOLI D KNO

XWC-001 6 SOLI D AST

M D5865-0 0 WAST E AST

M D 4 82-00 a WAST E KNO

XWC-001 6 WAST E AST

M D2 4 0-0 2 WAST E AST

M D482-00 a WAST E KNO

XWC-001 6 WAST E AST

M D240-0 2 000527 4 000703 6 001302 8 000527 4 000703 6 001302 8 001120 8 001104 4 001204 8 001120 8 001104 4 001204 8 001102 2
01 8 WAST

E AST

M D 4 82-00 a WAST E KNO

XWC-001 6 WAST E AST

M D240-0 2 001120 8 001104 4 001204 8 01 9

02 0

02 1 WAST

E AST

M D 4 82-O0 a WAST E KNO

XWC-001 6 WAST E AST

M D240-0 2 WAST E AST

M D482- 0 0 a WAST E KNO

XWC-001 6 WAST E AST

M D240-0 2 WAST E AST

M D482-O0 a WAST E KNO

XWC-001 6 WAST E AST

M D240-0 2 001120 8 001104 4 001204 8 001120 8 001104 4 001204 8 001120 8 001104 4 001204 8 001110 8

001201 9 02 2 WAST

E AST

M D482-00 a WAST E KNO

XWC-001 6 WAST E AST

M D240-0 2 001120 8 001104 4 001204 8 (Continue do

nnex t page )



### VES01915 69 

## Q C DAT A ASSOCIATIO N SUMMAR Y

H9L21040 4


### Sampl e Preparatio nan d Analysi s Contro l Number s
SAMPLE # 

### MATRI

X ANALYTICA

L METHO D LEAC H BATC H # PRE

P BATC H # M

S RUN # 02 3 WAST

E AST

M D482-O0 a WAST E KNO

XWC-001 6 WAST E AST

M D240-0 2 001120 8 001104 4 001204 8 02 4 WAST

E AST

M D482-00 a WAST E KNO

XWC-001 6 WAST E AST

M D240-0 2 001120 8 001104 4 001204 8 02 5 SOLID AST M D482-O0 a SOLID KNO

XWC-001 6 SOLID AST

M D5865-0 0 000527 4 000703 6 001302 8 02 6 SOLID AST M D482-00 a SOLID KNO

XWC-001 6 SOLID AST

M D5865-0 0 000527 4 000703 6 001302 8 02 7 SOLID AST M D482-00 a SOLID KNO

XWC-001 6 SOLID AST

M D5865-0 0 000527 4 000703 6 001302 8 0 2 8 SOLID AST M D482-00 a SOLID KNO

XWC-001 S SOLID AST

M D5865-0. 0 000527 4 000703 6 001302 8 02 9 SOLID AST M D482-O0 a SOLID KNO

XWC-001 6 SOLID AST

M D5865-0 0 000527 4 000703 6 001302 8 000514 2

001301 3 03 0 SOLID AST M D482-00 a SOLID KNO

XWC-001 6 SOLID AST

M D5865-0 0 000527 4 000703 6 001302 8 000701 7



### VES01915 71 0



# Sample Dat aSummar

y

i VES01915 8

### 1 1

AECOM , In c Clien t Sampl e ID : HBTO-tr4-M23A-Rl

Genera l Chemistr y Lot-Sampl e #... : H9L210404-00 1 Wor k Orde r #... : LRE3 3 Dat e Sarcrpied . .. : 12/16/0 9 Dat e Received.. : 12/19/0 9 Matrxx . WAST E

PARAMETE

R As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e RESUL T R L UNIT S 670 0 20 0 mg/k g Dilutio nFactor : 1 

### 868 0 180 0 BTU/l b

Dilutio nFactor ; 1 

### 644 0 24 4 mg/k g Dilutio nFactor : 1.2 2 

### _METHO D AST M D482-00 a MD L : 5 1 

### AST M D240-0 2
MD L : 13 0 

### KHO XWC-001 6 MD L : 7 3 

### PREPARATION- PRE P ANALYSI S DAT E BATC H # 01/11-01/13/1 0 001120 8 01/12/1 0 001204 8
01/11-01/15/1 0 001104 4



### I

VES01915 9

### 1 2

Lot-Sampl e #. . Dat e Sampled. .
PARAMETE

R AECOM , ID. G Clien t Sampl e ID : HBTU-n4-M23A.-R 2 Genera l Chemistr y H9L210404-00 2 Wor k Orde r #...- . LRE3 4 Matrxx . WAST E 12/17/0 9
RESUL T Dat e Received.. : 12/19/0 9
R L UNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 373 0 20 0 mg/k g Dilutio nFactor : 1 

### 859 0 180 0 BTU/l b

Dilutio nFactor : 1 

### 254 0 25 8 mg/k g Dilutio nFactor ; 1.2 9 

### _METHO D AST M D482-00 a MD L : 5 1 

### AST M D240-0 2
MD L : 13 0 

### KNO XWC-001 6 MD L : 7 7 

### PREPARATION- PRE P ANALYSI S DATE BATC H # 01/11-01/13/1 0 001120 8 01/12/1 0 001204 8
01/11-01/15/1 0 001104 4



### VES01916 01 3



### AECOM , In c Clien t Sampl e ID : HBTU-U4-M23A-R 3 Genera l Chemistr y tot-Sample #... : H9L210404-00 3 Wor k Orde r #... ; LRE3 5 Da.t e Sampled . .'. : 12/18/0 9 Dat e Received.. : 12/19/0 9 Matrix . WAST E

PARAMETE

R RESUL T R

L UNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 308 0 20 0 nig/k g Dilutio nFactor : 1 

### 851 0 180 0 BTU/U b Dilutio nFactor : 1 

### 234 0 31 8 rrtg/k g Dilutio nFactor : 1.5 9 

### _METHO D ' AST M D482-00 a MD L : 5 1 

### AST M D240-0 2
MD L : 13 0 

### KNO XWC-001 6 MD L : 9 5 

### PREPARATION- PRE P ANALYSI S DAT E BATC H # 01/11-01/13/1 0 001120 8 01/12/1 0 001204 8
01/11-01/15/1 0 001104 4



### I

VES01916 1

### 1 4

AECOM , In c Clien t Sampl e ID : LBTO-TJ4-M2 3 A-R l

Genera l Cnemistr y Lot-Sainpl e # . . . : H9L210404-00 4 Wor k Orde r #.. . : LRE3 6 Matri x: WAST E Dat e Sampled... : 12/15/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESUL T R

L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 256 0 20 0 mg/k g AST

M D482-00 a 01/11-01/13/1 0 001120 8 Dilutio nFactor : 1 MD L : 5 1 

### Gros s Calorifi c 22 6 B 180 0 BTU/l bAST M D240-0 2 01/12/1 0 001204 8 Valu e Dilutio nFactor : 1 MD L : 13 0 

### Tota l Chlorin e 128 0 21 4 mg/k g KNO

XWC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 1.0 7 MD L : 6 4 

### NOT E ( S ) : R L Repotting Limi t B Estimate

d result. Result i s les

s tha n RL .



### I VES01916 2

### 1 5

AECOM , In c Clien t Sampl e ID : _TU~U4-M23A-R 2

Genera l Chemistr y Lot-Sanrpl e #- . . : H9L210404-00 5 Wor k Orde r #.. . : LRE3 7 Matri x: WAST E Dat e Sampled . . . : 12/17/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESULT R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 273 0 20 0 mg/k g AST

M D482-00 a 01/11-01/13/1 0 001120 8 Dilutio nFactor : 1 MD L •

. : 5 1 

### Gros s Calorifi c 15 4 B 180 0 BTU/l bAST M D240-0 2 01/12/1 0 001204 8 Valu e Dilutio nFactor ; 1 MD L : 13 0 

### Tota l Chlorin e 137 0 21 6 mg/k g KNO

XWC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 1.0 8 MD L : 6 5 

### NOTE(S ) : R L Reportin g Limi l B Estimate

d result. Resul

t i s les s tha n RL .



### I VES01916 31 6



### AECOM , In c Clien t Sampl e ID : LBTtT-Cf4-M23A-R 3 Genera l Chemistr y H9L210404-00 6 Wor k Orde r #... : LRE3 8 Matri x: WAST E 12/18/0 9 Dat e Received.. : 12/19/0 9 Lot-Sampl e #... : Dat e Sampled... :
PARAMETE

R' RESUL T E L UNIT S As hConten t 335 0 20 0 mg/k g Dilutio nFactor : 1 

### PREPARATION- PRE P

_METHO D ' ANALYSI S DAT E BATC

H # AST M D482-00 a 01/11-01/13/1 0 001120 8 MDL . : 5 1 

### Gros s Calorifi c 24 6 B 180 0 BTU/l bAST M D240-0 2 01/12/1 0 001204 8 Valu e Dilutio nFactor : 1 MD L : 13 0 

### Tota l Chlorin e 167 0 21 6 mg/k g KNO

XWC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 1.0 8 MD L : 6 5 

### NOT B (S ) : R LReportin g limi t B Estimatedresult . Result i s les s tha

nRL .

I 

### VES01916 41 7



### AECOM , In c Clien t Sampl e ID : SF-U4-M23A-R 1 Genera l Chemistr y Lot-Saiopl e #... : H9L210404-00 7 Wor k Orde r : LRE4 C Dat e Sampled... : 12/1S/0 9 Dat e Received.. : 12/19/0 9 Matri x: WAST E

PARAMETE

R RESUL T R L UNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 160 0 20 0 mg/k g Dilutio nFactor : 1 4 *. 

### 939 0 180 0 BTU/l b

Dilutio nFactor : 1 

### 124 0 25 2 mg/k g Dilutio nFactor : 1.2 6 

### _METHO D AST M D482-00 a MD L : 5 1 

### AST M D240-0 2
MD L : 13 0 

### KNO XWC-001 5 MD L : 7 6 

### PREPARATION- PRE P ANALYSI S DATE BATC H # 01/11-01/13/1 0 001120 8 01/12/1 0 001204 8
01/11-01/15/1 0 001104 4



### VES01916 5

### 1 8

AECOM , _ c Clien t Sampl e ID : SF-U4-M23A-R 2 Genera l Chemistr y Lot-Sar_3>l e # . . . : H9L210404-00 8 Wor k Orde r #.. . : LRE4 D Matri x: WAST E Dat e Sampled. : 12/17/0 9 Dat e Received.. : 12/19/0 9 PREPARATION - PRE P PARAMETE

RRESUL T R

L UNIT S METHO D ANALYSI S DATE BATC H # As hConten t 289 0 20 0 mg/k g AST

M D482-00 a 01/11-01/13/1 0 001120 8 Dilutio nFactor : 1 MDL . : 5 1 

### Gros s Calorifi c 991 0 180 0 BTU/l bAST M D240-0 2 01/12/1 0 001204 8 Valu e

. Dilutio nFactor : 1 MDL , : 13 0 

### Tota l Chlorin e 222 0 26 6 mg/k g KNO

XWC-001 6 01/11-01/15/1 0 0011D4 4 Dilutio nFactor : 1.3 3 MD L : 8 0



### VES01916 6

### 1 9

AECOM , In c Clien t Sampl e ID : SF-U4-M23A-R 3 Genera l Chemistr y Lot-Sampl e #.. . : H9L210404-00 9 Wor k Orde r #.. . : LRE4 F Matri x: WAST E Dat e Sampled... : 12/18/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESUL T R L UNIT S METHO D ANALYSI S DATE BATC H # As hConten t 192 0 20 0 mg/k g AST

M D482-00 a 0l/ll-0l/l3/1 0 001120 8 Dilutio nFactor : 1 MD L : 5 1 

### Gros s Calorifi c 977 0 180 0 BTU/l bAST M D240-0 2 01/12/1 0 001204 8 Valu e Dilutio nFactor : 1 MD L : 13 0 

### Tota l Chlorin e 144 0 25 8 mg/k g KNO

XWC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 1.2 9 MD L : 7 7



### VES01916 7

### 2 0

AECOM , _ C Clien t Sampl e ID : CS-U4-M23A.-R 1 Genera l Chemistr y Lot-Sample*... : H9L210404-01 0 Wor k Orde r : LRE4GMatri x: SOLI D Dat e Sampled... : 12/16/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESOL T R L ONIT S METHO D ANALYSI S DAT E BATC H # As hConten t 69900 0 20 0 mg/k g AST

M D482-O0 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : • 1 MD L : 5 1 

### Gros s Calorifi c N D 180 0 BTU/l bAST M D5865-00 - 01/13/1 0 • 001302 8 Valu e Dilutio nFactor : 1 MD L : 13 0 

### Tota l Chlorin e 22 4 20 4 rag/kg KNO XWC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1.0 2 MD L : 6 1



### I VES01916 8

### 2 1

AECOM , Ul C Clien t Sampl e ID : CS-U4-M23A-R 2 Genera l Chemistr y tot-Sample #.. . : H9L210404-01 1 Wor k Orde r #.. . : LRE4H Matri x: SOLI D Dat e Sampled— : 12/17/0 9 Dat e Received.. : 12/19/0 9
PARAMETE

RRESUL T R

L UNIT S METHO D As h Conten t 

### 74600 0 20 0 mg/k g Dilutio nFactor : 1 

### 180 0 BTU/l b Dilutio nFactor : 1 

### 2 08 mg/k

g Dilutio nFactor : 1.0 4 

### AST M D482-00 a MD L : E l 

### AST M D5865-0 0
MD L : 1 3 0 

### KNO XWC-001 6 MD L : 6 2 

### PREPARATION- PRE P ANALYSI S DAT

E BATC

H # 01/OS-01/07/1 0 000527 4 01/13/1 0 001302 8
01/07-01/14/1 0 000703 6 Gros s Calorifi c N D Valu e
Tota l Chlorin e N D



### VES01916 9

### 2 2

AECOM , In c Clien t Sampl e ID : CS-U4-M23A-R 3 Genera l Chemistry Lot - Sampl e #.. . : H9L210404-01 2 Wor k Orde r #.. . : LRE4 J Matri x: SOLID Dat e Sampled . .. : 12/18/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESUL T R

L UNIT S METHO D ANALYSI S DATE BATC H # As hConten t 73700 0 20 0 mg/kg • AST M D482-00 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : 1 MD L : 5 1 

### Gros s Calorifi c N D 180 0 BTU/l bAST M D58S5-0 0 01/13/1 0 001302 8 Valu e Dilutio nFactor : 1 MD L : 13 0 

### Tota l Chlorin e 14 6 B 20 0 mg/k g KNO

XWC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1 MD L : S

O NOT E (S ) : R L Reporting Limi t B Estimate

d result . Resul

t i s les s tha n RL .



### VES01917 02 3



### AECOM , Xn

c Clien t Sampl e ID : BS-U4-M23A-R 1 Genera l Qiemistr y Lot-Sampl e #... : H9L210404-01 3 Wor k Orde r #... : LRE4 KMatri x: SOLID Dat e Sample d: 12/16/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESULT R L UNIT S METHO D ANALYSI S DA.T E BATC H # As hConten t 72500 0 20 0 mg/k g AST

M D482-00 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : 1 MD L : 5 1 

### Gros s Calorifi c 21 5 B 180 0 BTU/l bAST M D5865-0 0 01/13/1 0 001302 8 Valu e Dilutio nFactor : 1 MD L : 1 3 0 

### Tota l Chlorin e 65 0 20 8 mg/k g KNO

XWC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1.0 4 MD L : 6 2 

### NOTE(S ) : R L Reportin g Limi t B Estimate

d result. Resul

t is les s tha n RL . •



### VES01917 1

### 2 4

AECOM , In c Clien t Sampl e TD : BS-U4-M23A-R 2 Genera l Chemistr y Lot-Sampl e : H9L210404-01 4 Wor k Orde r #... : LRE4 L Matri x: SOLID Dat e Sampled . .. : 12/17-/0 9 Dat e Received . . : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESULT R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 77600 0 20 0 mg/k g AST

M D482-00 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : 1 MD L : 5 1 

### Gros s Calorifi c 19 8 B 180 0 BTU/l bAST M D58S5-0 0 01/13/1 0 001302 8 Valu e .Dilutio nFactor : 1 MD L : 13 0 

### Tota l Chlorin e 51 7 20 0 mg/k g KNO

XWC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1 MD L : 6 0 HOTE (S ) : : R L Reportin

g Limi t B Estimaie

d result. Resu U i

s les s tha n RL .



### VES01917 22 5



### AECOM , In c Clien t Sanipl e ID : BS-U4-M23A-R 3 Genera l Chemistr y Lot-Sampl e #... : H9L210404-01 5 Wor k Orde r #... : LRE4 M Matri x: SOLID Dat e Sampled... : 12/18/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 79400 0 20 0 mg/k g AST

M D482-00 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : 1 MD L : 5 1 

### Gros s Calorifi c N D 180 0 BTU/l bAST M D5865-0 0 01/13/1 0 • 001302 8 Valu e Dilutio nFactor : 1 MDL . . . : 13 0 

### Tota l C-ilorin e 22 9 20 2 mg/k g KNO

XWC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1.0 1 MD L : €

1



### VES01917 3

### 2 6

AECOM , In c Clien t Sampl e ID : HBT0-U4-M26A-R 1 Genera l Chemistr y Lot-Sampl e #.. . Dat e Sampled.. .
PARAMETE

R As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e H9L210404-01 6 Wor k Orde r #. . 12/16/0 9 Dat e Received .
RESUL T R

L UNIT S 1320 0 20 0 mg/k g Dilutio nFactor : 1 

### 900 0 180 0 BTU/l b

Dilutio nFactor : 1 

### 1250 0 119 0 mg/k g Dilutio nFactor : 5.9 4 

### LRE4N 12/19/0 9
METHO D Matri x: WAST E
PREPARATION- PRE P ANALYSI S DAT

E BATC

H # ASTM. D482-O0 a MD L : 5 1 

### AST M D240-0 2
MD L : 13 0 

### KNO XWC-001 6 MD L : 36 0 

### 01/11-01/13/1 0 001120 8 01/12/1 0 001204 8
01/11-01/15/1 0 001104 4



### I

VES01917 4

### 2 7

AECOM , In c Clien t Sampl e ID : HBTU-U4-M2SA-R 2 Genera l Cnemistr y Lot-Sampl e #... : H9L210404-01 7 Wor k Orde r #... : LRE4 P Dat e Sampled... : 12/17/0 9 Dat e Received.. : 12/19/0 9 Matri x: WAST E

PARAMETE

R RESUL T R

L UNIT S Ash . Conten t
Gros s Calorifi c Valu e
Tota l Chlorin e 317 0 20 0 mg/k g Dilutio nFactor : 1 

### 864 0 180 0 BTU/l b

Dilutio nFactor : 1 

### 247 0 27 0 mg/k g Dilutio nFactor : 1.3 5 

### _METHO D AST M D482-00 a MD L : 5 1 

### AST M D240-0 2
MD L : 1 3 0 

### KNO XWC-001 6 MDL . . . '. : 8 1 

### PREPARATION- PRE P ANALYSI S DATE BATC H # 01/11-01/13/1 0 001120 8 01/12/1 0 001204 8
01/11-01/15/1 0 001104 4



### VES01917 5

### 2 8

AECOM , In c Clien t Sampl e ID : HBTU-U4-M26A-R 3 Genera l Chemistr y Lot-Sample*... : H9L210404-01 8 Wor k Orde r # . . . : LRE4 Q Matri x: WAST E Dat e Sampled... : 12/18/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 329 0 20 0 mg/k g AST

M D482-O0 a 01/11-01/13/1 0 001120 8 Dilutio nFactor : 1 MD L : 5 1 

### Gros s Calorifi c 866 0 180 0 BTU/l bAST M D240-0 2 01/12/1 0 001204 8 Valu e Dilutio nFactor : 1 MD L : 13 0 

### Tota l Chlorin e 231 0 24 0 mg/k g KNO

XWC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 1. 2 MD L : 7 2



### VES01917 6

### 2 9

AECOM , In c Clien t Sampl e ID : LBTU-U4-M26A-R 1 Genera l Chemistr y Lot-Sanrpl e #... : H9L210404-01 9 Wor k Orde r : LRE4 RMatri x: WAST E Dat e Sampled... : 12/15/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESUL T R L UNIT S METHO D • ANALYSI S DAT E BATC H # As hConten t 266 0 20 0 mg/k g AST

M D482-00 a 01/11-01/13/1O 001120 8 Dilutio nFactor : 1 MD L : 5 1 

### Gros s Calorifi c 25 8 B 180 0 BTU/l bAST M D240-0 2 01/12/1 0 001204 8 Valu e Dilutio nFactor : 1 MD L : 13 0 

### Tota l Chlorin e 125 0 21 2 mg/k g KNO

XWC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 1.0 6 MD L : 6 4 

### NOTE(S ) : ' R L Reportin g Limi t B Estimatt

d result. Resul

t i s les s tha n RL .

I 

### VES01917 73 0



### AECOM , In c Clien t Sampl e ID : LBTU-U4-M26A-R 2 Genera l Chemistr y Lo t - Sampl e #.. . : H9L210404-02 0 Wor k Orde r : LRE4 T Matri x: WAST E Dat e Sampled... : 12/17/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESULT R L UNIT S METHO D ANALYSI S DATE BATC H # As hConten t 277 0 20 0 mg/k g AST

M D482-00 a 01/11-01/13/1 0 001120 8 Dilutio nFactor : 1 MD L : 5 1 

### Gros s Calorifi c 25 1 B 180 0 BTU/l bAST M D240-0 2 01/12/1 0 001204 8 Valu e Dilutio nFactor ; 1 MD L : 13 0 

### Tota l Chlorin e 131 0 21 0 mg/k g KNO

XWC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 1.0 5 MD L ..... : S 3 

### NOTE (S ) : R L Reportin

g Limi t B Estimaie

dresult . Resul

t i s les s tha nRL .



### VES01917 83 1



### AECOM , In c Clien t Sampl e ID : LBTU-U4-M26A-R 3 Genera l Chemistr y Lot-Sampl e #.. . : H9L210404-02 1 Wor k Orde r : LEE4V Matri x: WAST E Dat e Sampled... : 12/18/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESUL T R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 415 0 20 0 mg/k g AST

M D482-00 a 01/11-01/13/1 0 001120 8 Dilutio nFactor : 1 MD L : 5 1 

### Gros s Calorifi c 18 9 B 180 0 BTU/l bAST M D240-0 2 01/12/1 0 001204 8 Valu e Dilutio nFactor : 1 MD L : ; 13 0 

### Tota l Chlorin e 162 0 20 8 mg/k g KNO

XWC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor ; 1.0 4 ' ~MD L : 6 2 NOTE (S ) : R L Reporting Limit B Estimate

d result . Resul t i s les s tha n RL .



### VES01917 9

### 3 2

Lot-Sampl e # . Dat e Sampled .
PARAMETE

R As hConten t
Gros s Calorifi c Valu e
Tota l Oxlorin e AECOM , In c Clien t Sampl e ID : SF-U4-M26A-R 1 Genera l Chemistr y H9L210404-02 2 12/15/0 9
RESULT Wor

k Orde r #...; • LRE4 W Dat e Received.. : 12/19/0 9 Matrxx . WAST E

R L UNIT S 148 0 20 0 mg/k g Dilutio nFactor : 1 

### 1010 0 180 0 BTU/l b

Dilutio nFactor : 1 

### 112 0 26 0 mg/k g Dilutio nFactor : 1. 3 

### _METHO D AST M D482-00 a MD L : 5 1 

### AST M D240-0 2
MD L : 13 0 

### KNO XWC-001 6 MD L : 7

B 

### PREPARATION- PRE P ANALYSI S DAT

E BATC

H # 01/11-01/13/1 0 001120 8 01/12/1 0 001204 8
01/11-01/19/1 0 001104 4



### VES01918 03 3



### AECOM , In c Clien t Sampl e ID : SF-U4-M26A-R 2 Genera l Chemistr y Lot-Saunpl e #. . . : H9L210404-02 3 Wor k Orde r #... : LRE4XMatri x: WAST E Dat e Sampled... : 12/17/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESULT RL ; UNIT S METHO D ANALYSI S DATE BATC H # As hConten t 457 0 20 0 mg/k g AST

M D482-O0 a 01/11-01/13/1 0 001120 8 Dilutio nFactor : 1 MD L : 5 1 

### Gros s Calorifi c 943 0 180 0 BTU/l bAST M D240-0 2 01/12/1 0 001204 8 Valu e Dilutio nFactor : 1 MD L : 13 0 

### Tota l Chlorin e 351 0 25 2 mg/k g KNO

XWC-001 6 01/11-01/19/1 0 001104 4 Dilutio nFactor : 1.2 6 MD L : 7 6



### VES01918 1

### 34

AECOM , In c Clien t Sampl e 10 : SF-TJ4-M26A-R 3 Genera l Chemistr y Lot-Sampl e # . . . : H9L210404-02 4 Wor k Orde r #.. . : LRE4 0 Matri x: WAST E Dat e Sampled... : 12/18/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESULT R L UNIT S METHO D ANALYSI S DAT E BATC H g As hConten t 182 0 20 0 mg/k g AST

M D482-00 a 01/11-01/13/1 0 001120 8 Dilutio nFactor : 1 HD L : 5 1 

### Gros s Calorifi c 982 0 180 0 BTU/l bAST M D240-0 2 01/12/1 0 001204 8 Valu e Dilutio nFactor : 1 MD L : 13 0 

### Tota l Chlorin e 140 0 25 2 mg/k g KNO

XWC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 1.2 6 MD L : 7 6



### VES01918 2

### 3 5

Lot-Sampl e # . Dat e Sampled . .
PARAMETE

R AECOM , In c Clien t Sampl e ID : CS-U4-M26A-R 1 Genera l Chemistr y B9L210404-02 5 Wor k Orde r #... : LRE4 3 12/16/0 9 Dat e Received.. : 12/19/0 9 Matrix . SOLID

RESUL T R L UNIT S As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e 78500 0 20 0 mg/k g Dilutio nFactor : 1 

### N D 18 0 0 BTU/l b

Dilutio nFactor : 1 

### N D 20 8 mg/k g Dilutio nFactor : 1.0 4 

### _METHO D AST M D482-00 a HD L : 5 1 

### AST M D5865-0 0
MD L : 13 0 

### KNO XWC-001 5 MD L : 6 2 

### PREPARATION - PRE P ANALYSI S DAT

E BATC

H # 01/05-01/07/1 0 000527 4 01/13/1 0 001302 8
01/07-01/14/1 0 000703 6



### VES01918 33 6



### AECOM , In c Clien t Sampl e ID : CS-U4-M26A-R 2 Genera l C_ttemistr

y Lot-Sampl e #... : H9L210404-02 6 Wor k Orde r #... : LRE4 4 Matri x: SOLID Dat e Sampled... : 12/17/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESUL T R

L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 85700 0 20 0 mg/k g AST

M D482-00 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : 1 MD L : 5 1 

### Gros s Calorifi c N D 180 0 BTU/l bAST M D5865-0 0 01/13/1 0 001302 8 Valu e Dilutio nFactor : 1 MD L : 1 3 0 

### Tota l Chlorin e N D 21 2 mg/k g KNO

XWC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1.0 6 MD L : 6 4



### VES01918 4

### 37

AECOM , In c Clien t Sampl e ID : CS-U4-M26A-R 3 Genera l Chemistr y Lot-Sampl e #... : H9L210404-02 7 Wor k Orde r #.. . : LRE4 5 Matri x. : SOLI D Dat e Sampled... : 12/18/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESULT R L UNIT S METHO D ANALYSI S DAT E BATC H # As hConten t 74400 0 20 0 mg/k g AST

M D482-00 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : 1 MDL . : 5 1 

### Gros s Calorifi c N D 180 0 BTU/l bAST M D5865-0 0 01/13/1 0 001302 8 Valu e Dilutio nFactor : 1 MD L : 13 0 

### Tota l Chlorin e N D 20 8 mg/k g KNO

XWC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1.0 4 MD L : 6 2



### VES01918 53 8



### AECOM , In c Clien t Sampl e ID : BS-U4-M26A-R 1 Genera l Chemistr y LK3t -Santpl e #... : H9L210404-02 8 Wor k Orde r #.. . Dat e Sampled... : 12/16/0 9 Dat e Received. .
PARAMETE

R As hConten t
Gros s Calorifi c Valu e
Tota l Chlorin e RESUL T RL 

### UNIT S 80800 0 20 0 mg/k g Dilutio nFactor : 1 

### 20 0 B 180 0 BTU/l b

Dilutio nFactor : 1 

### 43 3 20 2 mg/k g

. Dilutio nFactor : 1.0 1 

### LRE4 S 12/19/0 9 Matrix . SOLI D



### _METHO

D AST M D482-00 a MD L : 5 1 AST M Dsses '-o o MD L : 13 0 

### KNO XWC-001 6 MD L : S I 

### PREPARATION- PRE P ANALYSI S DAT

E BATC

H # 01/05-01/07/1 0 000527 4 01/13/1 0 001302 8
01/07-01/14/1 0 000703 6
NOTE(S ) : R L Reportin g Limi

t B Estimate

d result. Resul

t is les s tha n RL .



### VES01918 63 9



### AECOM , In c Clien t Sampl e ID : BS-U4-M26A-R 2 Genera l Cnemistr y Lot-Sampl e #... : H9L210404-D2 9 Wor k Orde r #...: - LRE 4 7 • Matri x: SOLI D Dat e Sampled.. . -

. 12/17/0 9 Dat e Received.. : 12/19/0 9 PREPARATION - PRE P PARAMETE

RRESULT R L UNIT S METHO D ANALYSI S DATE BATC H # As hConten t 80100 0 20 0 mg/k g AST

M D482-00 a 01/05-01/07/1 0 000527 4 Dilutio n Factor : 1 MD L : 5 1 

### Gros s Calorifi c 19 6 B 180 0 BTU/l bAST M D5865-0 0 01/13/1 0 001302 8 Valu e Dilutio n Factor : 1 MD L : 13 0 

### Tota l Chlorin e 97 6 21 6 mg/k g KHO

XWC-001 6 01/07-01/14/1 0 000703 6 Dilutio n Factor : 1.0 8 MD L : 6 5 

### NOTE(S ) : R L Reporting Limi t B Estimate

d result. Resul

t is les s tha n RL .



### VES01918 7

### 4 0

AECOM , In c Clien t Sampl e ID : BS-U4-M26A-R 3 Genera l Chemistr y Lot-Saum?l e # . .. : H9L210404-03 0 Wor k Orde r : LRE4 8 Matri x: SOLID Dat e Sampled... : 12/18/0 9 Dat e Received.. : 12/19/0 9 PREPARATION- PRE P PARAMETE

RRESUL T R

L UNIT S METHO D ANALYSI S DATE BATC H # As hConten t 79700 0 20 0 mg/k g AST

M D482-O0 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : 1 MD L : S I 

### Gros s Calorifi c N D 180 0 BTU/l bAST M D5865-0 0 01/13/1 0 001302 8 Valu e Dilutio nFactor : 1 MD L : 13 0 

### Tota l Chlorin e 61 0 20 0 mg/k g KNO

XWC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1 MD L : 6 0



### VES01918 84 1



### Clien t Lo t # . : H9L21040 4 METHO D BLAN KREPOR

T Genera l Chemistr y Matrix . SOLI D
PARAMETE

R As hConten t RESUL T REPORTIN

G LIMI T UNIT S METHO D PREPARATIONANALYSI S DAT

E Wor k Orde r N D • 20 0

Dilutio n Factor : 1 

### PRE P BATC H # If : LRVT31A

A M B Lot-Sampl e # : HOA050000-27 4 mg/k g AST

M D4S2-00 a 01/05-01/07/1 0 000527 4
Tota l Chlorin e Wor k Orde r # : LRW761A A MB . Lot-Sampl e # : HOA070000-03 6 N D 20 0 mg/k g KNO

XWC-001 6 01/07-01/14/1 0 000703 6 Dilutio n Factor : 1 

### NOTE(S ) : Calculations ar

c performe

d befor e rounding t

o avoid round-of

ferror s i n calculate

d results.



### VES01918 9

### 4 2

Clien t La t H9L21040 4 METHO D BLAN KREPOR T Genera l Chemistry 

### Matri x: WAST E
PARAMETE

R RESULT As hConten t N D REPORTIN G LIMI T UNIT S METHO D PREPARATION- PRE P ANALYSI S DAT

E BATC

H # Wor k Orde r # : LR2KQ1A A M B Lot-Sampl e # : H0A110000-20 8 20 0 mg/k

g AST

M D482-00 a 01/11-01/13/1 0 001120 8 Dilutio n Factor : 1 

### Tota l Chlorin e Wor k Orde r # : LR2CJ1A A M B Lot-Sampl e # : HOA110000-04 4 N D 20 0 mg/k g KNO

XWC-001 S 01/11-01/15/1 0 001104 4 Dilutio n Factor : 1 NOTE(S ) : Calculations ar

e performe

d befor e rounding t

o avoid round-of

Terror s t n calculate

d results.



### VES01919 0

### 4 3

LABORATOR

YCONTRO

L SAMPL

E EVALUATIO

N REPOR T Genera l Chemistr y Lot-Sampl e #... : H9L21040 4 Matri x: SOLI D
PARAMETE

R As hConten t PERCEN T RECOVER Y 10 1 10 1 RECOVER Y LIMIT S RP

D RP D LIMIT S METHO

D PREPARATIONANALYSI S DAT

E PREP BATC H W0#:LRVT31AC-LCS/LRVT31AD-LCSD LC S Lot-Sample# : HOA050000-27 4 (9 0 - 110 ) AST M D482-00 a 01/05-01/07/1 0 000527 4 (9 0 - 110 ) 0.1 2 (0-10 ) AST M D482-00 a 01/05-01/07/1 0 000527 4 Dilutio n Factor : 1 

### Gros s Calorifi c Valu e 10 0

10 0 W0#:LR4DC1AA-LCS/LR4DC1AC-LCS D LC S Lot-Samples : HOA130000-02 8 (9 8 - 102 ) (9 8 - 102 ) 0.0 5 (0-2.0 ) Dilutio n Factor : 1 

### AST M D5865-0 0 AST M D5865-0 0 01/13/1 0

01/13/1 0 001302 8

001302 8
NOTE(S ) : Calculaiions ar

e performe

d befor e rounding i o avoi d round-of ferror s i n calculate

d results.



### VES01919 1

### 4 4

LABORATOR

YCOHTRO

L SAMPL

E DAT A REPOR T Genera l Chemistr y Lot-Sampl e #... : H9L21040 4 Matri x: SOLI D

SPIK E MEASURE

D PARAMETE

RAMOUN

T AMOUN

T UNIT S As hConten t 400 0

400 0 PERCN T RECVR YRP D METHO

D PREPARATION ANALYSI S DAT

E PRE P 

### BATC H # WO#:LRVT31AC-LCS/LRVT31AD-LCS D LC S Lot-Sample* : HOA050000-27 4 405 0 mg/k

g 10 1 AST M D482-00 a 01/05-01/07/1 0 000527 4 406 0 mg/k

g 10 1 0.1 2 AST M D482-00 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : 1 

### Gros s Calorifi c Valu e 1140 0

1140 0 W0#:LR4DC1AA-LCS/LR4DC1AC-LCS D LC S Lot-Satnple# : HOA130000-02 8 11 4 0 0 BTU/l b'1 0 0 1140 0 BTU/l b' 10 0

Dilutio nFactor : 1 

### AST M D5865-0 0 0.0 6 AST

M D5865-0 0 01/13/1 0

01/13/1 0 001302 8

001302 8

NOT E (S) : Calculaiion s ar

e performe

d befor e roundin g i o avoid round-of ferror s i n calculate

d results.



### VES01919 24 5



### LABORATOR

YCONTRO

L SAMPL

E EVALUATIO

N REPOR T Genera l Chemistr y Clien t Lo t #... : H9L21040 4 Matri x: SOLID

PERCEN T RECOVER

YPREPARATION- PREP PARAMETE

RRECOVER

YLIMIT S METHO D ANALYSI S DAT E BATC

H # Tota l Chlorin e Wor k Orde r # : LRW761A C LC S Lot-Sample# : HOA070000-03 6 10 1 (8 0 - 120 ) KNO XWC-001 5 01/07-01/14/1 0 000703 6 Dilutio n Factor : 5 NOTE(S ) : . Calculations ar

e performe

d befor e rounding i o avoid round-of ferror s i n calculate

d results.

i 

### VES01919 3

### 4 6

LABORATOR

YCONTRO

L SAMPL

E DAT A REPOR T Genera l Chemistr y Clien t Lo t #... : H9L21040 4 Matri x: SOLI D

SPIKE MEASURE

D PERCN T PREPARATION- PREP PARAMETE

RAMOUN

T AMOUN

T UNIT S RECVR YMETHO

D ANALYSI S DAT E BATC H # Tota l Chlorin e Wor k Orde r # : LRW7S1A C LC S Lot-Sample# : HOA070000-03 6 1000 0 1010 0 mg/k g 10 1 KNO

XWC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 5 

### NOTE(S ) : ' Calcufariom ar

e perfomie

d befor e rounding t

o avoid round-of

ferror s i n calculate

d results.



### VES01919 4

### 4 7

LABORATOR

YCONTRO

L SAMPL

E EVALUATIO

N REPOR T Genera l Chemistr y Lot-Sampl e #. , H9L21040 4 Matri x: WAST E
PARAMETE

R As hConten t PERCEN T RECOVER Y 9 8 10 1 RECOVER Y LIMIT S RP

D RP D LIMIT S METHO

D PREPARATIONANALYSI S DAT

E PREP BATC H # W0#:LR2KQ1AC-LCS/LR2KQ1AD-LCS D LC S Lot-Sample# : HOA110000-20 8 (9 0 - 110 ) AST M D482-00 a 01/11-01/13/1 0 001120 8 (9 0 - 110 ) 2. 4 (0-10 ) AST M D482-00 a 01/11-01/13/1 0 001120 8 Dilutio nFactor : 1 

### Gros s Calorifi c Valu e 10 0

10 0 WO#:LR2981AA-LCS/LR2981AC-LCSD LCS ' Lot-Sample# : H0A120OOO-0 4

102 ) (9 8 (9 8 - 102 ) 0.0 2 (0-2. 0 Dilutio nFactor : 1 

### AST M D240-0 2 AST M D240-0 2 01/12/1 0

01/12/1 0 001204 8

001204 8
NOTE(S) : Calculation s ar

e performe

d befor e rounding t

o avoi d round-of

ferror s i n calculate

d results .



### VES01919 5

### 4 8

LABORATOR

YCOHTRO

L SAMPL

E DAT A REPOR T Genera l Chemistr y Lot-Sampl e #... : H9L21040 4 Matri x: WAST E
PARAMETE

R As hConten t SPIK

E AMOUN T 400 0 400 0 MEASURE

D AMOUN T UNIT S PERCN T RECVR YRP D METHO

D PREPARATIONANALYSI S DAT

E PRE P BATC H # W0#:LR2KQ1AC-LCS/LR2KQ1AD-LCS D LC S Lot-Sample# : HOA110000-20 8 393 0 mg/k

g 9 8 AST M D482-00 a 01/11-01/13/1 0 001120 8 403 0 mg/k

g 10 1 2. 4 AST M D482-00 a 01/11-01/13/1 0 001120 8 Dilutio n Factor : 1 

### Gros s Calorifi c Valu e 2060 0

20GO O WO#:LR2981AA-LCS/LR2981AC-LCSD LC S Lot-Sample# : H0A120000-04 8 2050 0 2050 0 BTU/l b10 0

BTU/l b10 0 Dilutio n Factor : 1 

### AST M D240-0 2 0.0 2 AST

M D240-0 2 01/12/1 0

01/12/1 0 001204 8

001204 8 NOTE(S ) : Calculations ar

e performe

d befor e roundin g t

o avoid round-of

ferror s i n calculate

d results.



### VES01919 64 9



### LABORATOR

YCONTRO

L SAMPL E EVALUATIO

N REPOR T Genera l Chemistr y Clien t Lo t #... : H9L21040 4 Matri x: WAST E PERCEN T RECOVER

YPREPARATION- PREP PARAMETE

RRECOVER

YLIMIT S METHO D ANALYSI S DAT E BATC

H # Tota l Chlorin e Wor k Orde r # : LR2CJ1A C LC S Lot-Sample# : HOA110000-04 4 10 4 (8 0 - 120 ) KNO XWC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 5 

### NOTE(S ) : Calculations ar

e performe

d befor e rounding t

o avoi d round-of

ferror s i n calculate

d results.



### VES01919 75 0



### LABORATOR

YCONTRO

L SAMPL

E DAT A REPOR T Genera l Chemistr y Clien t Lo t # . . . : H9L21040 4 Matri x: WAST E SPIK E MEASURE

D PERCN T PREPARATION- PRE P PARAMETE

RAMOUN

T AMOUN

T UNIT S RECVR YMETHO

D ANALYSI S DAT E BATC

H # Tota l Chlorin e Wor k Orde r # : LR2CJ1A C LC S Lot-Sample# : HOA110000-04 4 1000 0 1040 0 mg/k g 10 4 KNO

XWC-001 6 Ol /ll -Ol/15/l O 001104 4 Dilutio n Factor : 5 

### NOTE(S ) : Calculations ar

e performe

d befor e rounding t

o avoid round-of

ferror s i n calculate

d results.



### VES01919 85 1



### MATRIXSPIKE SAMPL E EVALUATIO

N REPOR T
Clien t Lo t #.. . Dat e Sampled.. . : H9L21040 4

: 12/18/0 9 Genera l Chemistr y

Dat e Received.. : 12/19/0 9 Matri x: WAST E

PARAMETE

R Tota l Chlorin e

10 7 10 6 PERCEN T RECOVER

Y RECOVER

YLIMIT S RP

D RP D LIMIT S METHO

D PREPARATIONANALYSI S DAT

E PREP BATC H # WO# : LRE351AG-MS/LRE351AH-MS D M S Lot-Sampl e # : H9L210404-00 3 (8 0 - 120 ) KNO XWC-001 6 01/11-01/15/1 0 001104 4 (8 0 - 120 ) 2. 5 (0-10 ) KNO XWC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor i 8. 3 

### NOTE(S) : Calculations ar

e performe

d befor e rounding t

o avoid round-of

ferror s i n calculate

d results .



### VES01919 95 2



### MATRI XSPIKE SAMPL

E DAT A REPOR T Genera l Chemistr y Clien t Lo t #... : H9L21040 4 Matri x: WAST E Dat e Sample d: 12/18/0 9 Dat e Received.. : 12/19/0 9

SAMPL E SPIK E MEASR

D PERCN T PREPARATION- PREP PARAMETE

RAMOUN

T AM T AMOUN

T UNIT S RECVR YRP D METHO

D ANALYSI S DAT E BATC H # Tota l Chlorin e WO# : LRE351AG-MS/LRE351AH-MS D M S Lot-Sampl e # : H9L210404-00 3 234 0 16S0 0 2010 0 mg/k g 10 7 KNO XWC-001 S 01/11-01/15/1 0 001104 4 234 0 1620 0 1960 0 mg/k g 10 6 2. 5 KNO XWC-001 6 0l/ll-0l/l5/l 0 001104 4 Dilutio nFactor : 8. 3 

### NOTE(S) : Calculation s ar

e performe

d befor e rounding t

o avoi d round-of

fenor s i n calculate

d results .

i 

### VES01920 05 3



### MATRI XSPIK E SAMPL E EVALUATIO

N REPOR T Genera l Chemistr y Clien t Lo t #... : H9L21040 4 Matri x: SOLI D Dat e Sampled... : 12/18/0 9 Dat e Received.. : 12/19/0 9

PERCEN T RECOVER

YRP

D PREPARATION- PREP PARAMETE

RRECOVER

YLIMIT S RP

D LIMIT S METHO

D ANALYSI S DAT E BATC H # Tota l Chlorin e WO# : LRE4J1AG-MS/LRE4J1AH-MSD M S Lot-Sampl e # : H9L210404-01 2 9 7 (8 0 - 120 ) KNO XWC-001 6 01/07-01/14/1 0 000703 6 10 0 (8 0 - 120 ) 3. 4 (0-10 ) KNO XWC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 4.9 6 

### NOTE(S ) : Calculations ar

e performe

d befor e roundinc t

o avoid round-of

ferror s i n calculate

d results.

1



### VES01920 15 4



### MATRIXSPIKE SAMPL E DAT A REPOR T Genera l Cnemistr y Clien t Lo t #.. , Dat e Sampled.- . H9L21040 4

12/18/0 9 Matri x: SOLI D

Dat e Received . 12/19/0 9

' SAMPL

E SPIK E PARAMETE

RAMOUN

T AM T Tota l Chlorin e '

14 6 992 0 14 6 1000 0 MEASR D AMOUN T UNIT S PERCN T RECVR YRP D METHO

D PREPARATION- PRE P ANALYSI S DATE BATC H # WO# : LRE4J1AG-MS/LRE4J1AH-MSD M S Lot-Sampl e # : H9L210404-01 2 982 0 mg/k

g 9 7 KNO XWC-001 6 01/07-01/14/1 0 000703 6 1020 0 mg/k

g 10 0 3. 4 KNO XWC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : i.Se NOTE(S ) : Calculaiion s ar

e performe

d befor e rounding t

o avoi d round-of

ferror s i n calculate

d results .



### VES01920 2

### 5 5

SAMPL E DUPLICAT E EVALUATIO N REPOR T Genera l Chemistr y Clien t Lo t H9L21040 4 Wor k Orde r # . . . : LRE35-SM P Matri x: WAST E LRE35-DU

P Dat e Sample d.

- 12/18/0 9 Dat e Received. . : 12/19/0 9 DUPLICATE RP D PREPARATION - PRE P PARA M RESUL T RESUL

T UNIT S RP D LIMI T METHO

D ANALYSI S DATE BATC H # Gros s Calorifi c S D Lot-Sampl e # : H9L210404-OO 3 Valu e 851 0 862 0 BTU/l b1. 3 (0-10 ) AST M D240-0 2 01/12/10 - 001204 8 Dilutio nFactor : 1 

### As hConten t S D Lot-Sampl e # : H9L210404-00 3 308 0 305 0 mg/k g 1. 1 (0-10 ) AST M D482-00 a 01/11-01/13/1 0 001120 8 Dilutio nFactor : 1 

### Tota l Chlorin e SD Lot-Sampl e # : H9L210404-00 3 234 0 235 0 mg/k g 0.1 3 (0-10 ) KNO XWC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 1.5 9



### VES01920 3

### 5 6

SAMPL E DUPLICAT E EVALUATIO N REPOR T Genera l Chemistr y Clien t Lo t H9L21040 4 Wor k Orde r #... : LRE4J-SM P Matri x: SOLI D LRE4J-DU

P Dat e Sampled... : 12/18/0 9 Dat e Received.. : 12/19/0 9 DUPLICATE RP D PREPARATION - PRE P PARA M RESULT RESUL T UNIT S RP D LIMI T METHO

D ANALYSI S DAT E BATC H # Gros s Calorifi c S D Lot-Sampl e # : H9L210404-01 2 Valu e N D N

D BTU/l b0 (0-10 ) AST M D5865-0 0 01/13/1 0 001302 8 Dilutio n Factor : 1 

### As hConten t S D Lot-Sampl e # : H9L210404-01 2 73700 0 74100 0 mg/k g 0.5 S (0-10 ) AST M D482-00 a 01/05-01/07/1 0 000527 4 Dilutio n Factor : 1 

### Tota l Chlorin e S D Lot-Sampl e # : H9L210404-01 2 14 6 B 14 9 B mg/k g 1. 9 (0-10 ) KNO XWC-001 6 01/07-01/14/1 0 000703 6 Dilutio n Factor : 1 

### NOTE(S ) : Calculations ar

e performe

d befor e rounding t

o avoid round-of

ferror s i n calculate

d results . B Estimate

d result . Resul

t is les s tha n RL .



### VES01920 4

### 5 7

Clien t Lo t #... : H9L21040 4 Dat e Sampled... : 12/17/0 9 SAMPL E DUPLICAT E EVALUATIO N REPOR T 

### Genera l Chemistr y Wor k Orde r #... : LRE4P-SM P LRE4P-DU

P Dat e Received.. : 12/19/0 9
PARA M RESULT Tota l Chlorin e 247 0 DUPLICATE

RESUL T 253 0 

### Matrix . WAST E

UNIT S RP

D RP D LIMI T METHO

D PREPARATION- PRE P ANALYSI S DAT E BATC H # S D Lot-Sampl e # : H9L210404-01 7 mg/k g 2. 5 (0-10 ) KNO XWC-001 6 01/11-01/15/1 0 001104 4 Dilutio nFactor : 1.3 S



### VES01920 5

### 5 8

Clien t Lo t # . . . : Dat e Sampled... :
PARA M RESULT H9L21040 4

12/18/0 9 DUPLICATE RESUL T SAMPL

E DUPLICAT E EVALUATIO N REPOR T Genera l Chemistry Wor k Orde r #... : LRE4V-SM P LRE4V-DU

P Dat e Received.. : 12/19/0 9

Gros s Calorifi c Valu e 1 8 9 B UNIT S RP D RP D LIMI T 22 9 B . BTU/l b1 9

Dilutio nFactor : l 

### METHO D Matri x: WAST E

PREPARATION- PRE P ANALYSI S DAT E BATC H # S D Lot-Sampl e # : H9L210404-02 1 (0-10 ) AST

M D240-0 2 01/12/1 0 001204 8
As hConten t 415 0 3 6 0 0 mg/k g 1 4 Dilutio nFactor : 1 

### S D Lot-Sampl e # : H9L210404-02 1 (0-10 ) AST

M D482-00 a 01/11-01/13/1 0 001120 8
NOTE(S ) : Calculations ar

e performe

d befor e rounding t

o avoid round-of

ferror s i n calculate

d results. B Estimaie

d result . Resul t i s les s tha n RL .



### VES01920 6

### 5 9

Clien t Lo t #... : H9L21040 4 Dat e Sampled... : 12/17/0 9 SAMPL E DUPLICAT E EVALUATIO N REPOR T Genera l Chemistr y Wor k Orde r #.. . Dat e Received. .
PARA M RESUL T DUPLICATE

RESUL T Gros s Calorifi c Valu e 19 5 B
As hConten t 80100 0 31 7 B

79700 0 LRE47-SM P LRE47-DU

P 12/19/0 9
UNIT S RP

D RP D LIMI T METHO

D Matri x: SOLID

PREPARATION- PRE P ANALYSI S DAT

E BATC

H # BTU/l b4 7 Dilutio nFactor : 1 

### S D Lot-Sampl e # : H9L210404-02 9 (0-10 ) AST

M D5B65-0 0 01/13/1 0 001302 8
S D Lot-Sampl e # : H9L210404-02 9 mg/k g 0.4 1 (0-10 ) AST M D482-00 a 01/05-01/07/1 0 000527 4 Dilutio nFactor : 1


### NOTEIS ) : Calculations ar

e performer

) befor e rouniitng t

o avoi d round-of

ferror s i n calculate

d results. B Estimate

d result. Resul

t is les s tha n RL .



### VES01920 76 0



### Clien t Lo t #... : HSL21040 4 Dat e Sampled... : 12/18/0 9 SAMPL E DDPLICAT E EVALDATIO H REPOR T Genera l Chemistr y Wor k Orde r LRE48-SM P LRE48-DU

P Dat e Received.. : 12/19/0 9
PARA M RESULT Tota l Chlorin e 61 0 Matri x- . SOLI D

UNIT S RP

D RP D LIMI T METHO

D PREPARATION- PRE P ANALYSI S DAT

E BATC H # DUPLICATE RESUL T S D Lot-Sampl e # : H9L210404-03 0 .24 5 mg/k

g 8 5 (0-10 ) KNO XWC-001 6 01/07-01/14/1 0 000703 6 Dilutio nFactor : 1



### VES01920 8