Memorandu m USEP ARegio n5 Lan dan dChemical s Divisio n
To : Fil e Date : Marc h26 , 201 0 From :

Re : Update dCalculation s o f Meta lFee dRate s Use dDurin g th e200 8 Tes t Burn s a t Veoli aEnvironmenta l Services , LLC , Sauget , I L



### I . Introductio

n I naMa y 6 , 200 9 memorandum , th eUnite dState s Environmenta l Protectio n Agenc y (EPA ) estimate dheav y meta l fee drate s fo r tes t burn s conducte di n200 8 b y Veoli aEnvironmenta l Services , LL C (Veolia ) o nthre e incinerator s a t it s facilit y i n Sauget , Illinois . Th eEPA-estimate dfee drate s differe dsignificantl y fro mthos eprovide d b y Veoli abecaus eo f

problem s identifie dwit hVeolia' s samplin g an danalysis . Th eMa y 6 , 200 9 memorandu mconclude dtha t th eanalytica l dat aprovide db y Maxxa mAnalytical , Inc . (Maxxam ) ha dbee nprepare db y dryin g suc hthat th eresult s wer eexpresse di ndry-weigh t form . Unfortunately , i t appeare dthat

Maxxa muse da dryin g procedur ewhic hdi dno t adequatel y documen t

th eorigina lmoistur econten t o f the samples . Th eresult s o f subsequen t

reanalysi s fo r

moistur econten t

b y Maxxa mwer es o differen t tha nmoistur eresult s obtaine dfro mbot hVeolia' s secondary lab , PS C Republi c Environmenta l System s (Pennsylvania ) LL C (PS C Republic ) an dEPA' s Centra l Regiona lLaborator y (CRL ) that EP Aconclude dth etes t bur nfee drate s shoul db e adjuste dto wet-weigh t usin g th ePS C Republi c moistur edata . Thi s mem o include s ne w estimate s base do nacontinue drevie w o f th e200 8 dat a an dmethodolog y as wel las additiona l informatio nsubmitte db y Veolia . Specifically , E P Areviewe dVeolia' s mercur y spik epreparatio nmethodolog y an ddat aan dconclude d tha t a nestimat eo f

spik emercur y concentratio nbase do nVeolia' s spik epreparatio n procedure s (includin g equipmen t specification s an dinterview s wit hVeoli apersonnel ) mos t accuratel y represent s thespik econcentration s use di nthetes t burn . EP Aals o conducte dapreliminar y validatio no f Veolia' s fee ddatafo r metal s as wel las th e moistur edat afro mCRL .

1

### II

. Mercur ySpik eFee d Contributio

n Jus t befor ecommencemen t o f theStac k

3 Tes t Bu mo nAugus t

4 , 2008 , Veoli averball y describe dth espik epreparatio nprocedure s an dprovide dvariou s documentatio n includin g specificatio nsheet s fo r th emercur y spik emateria l an dcalibratio nrecord s fo r scale s an danalytica l balance s (Septembe r 3 , 200 8 Memorandu mt o File) . Whil eon-sit e fo r then-schedule dStac k

4 Tes t Bur no nAugus t

13 , 2008 , Veoli aprovide dawritte n narrativ edescribin g th eprocedur efo r preparin g th emercur y spik esolution . Veoli aals o provide dMetal s Standar dPreparatio nLa b Sheet s documentin g th eprocedur e(Novembe r 25 , 200 8 Memorandu mt o File) . A t that time , i t wa s no t clea r whic hspik ebatche s wer euse dt o mak ethevariou s spik e vial s use dthroughou t

th etests . I nlat e2009 , EP Arequeste dan dreceive dadditiona l documentatio nfo r

spik epreparatio n(Attachmen t 1) . I nMarc h2010 , EP Aals o requeste d an dreceive dacop y o f theMetal s Standar dPreparatio nLa b Shee t fo r th elas t tw o spik e batche s (Attachmen t

2) . Fro mal l o f

thi s information , EP Awa s abl eto calculat e minimu man dmaximu mconcentration s fo r al lmercur y spik ebatches (Attachmen t 3) . Th eresult s o f

off-sit eanalysi s o f

th espik esolution s collecte dbot hbefor ean ddurin g th e tes t burn s approximat eth ecalculate dspik econcentrations , however , thes e results wer e ofte nhighe r

tha nth emaximu mpossibl econcentratio nbase do nth ecompositio no f th e procure dspik ematerial . EP Anote dnumerou s deficiencie s i nfh elaborator y report s o f spik eanalysi s includin g alac k o f qualit y contro l analysi s an dmissin g documentation . Maxxa mrecommende dthat th espik eresult s b e"viewe dwit hdiscretion, " give nthes e issues . E P Abelieve s that

spik econcentration s calculate dfro mspik epreparatio nmethodolog y usin g th estate dcompositio nan dcertifie dminimu mpurit y o f th eorigina lspik emateria l i s mos t representativ eo f

th espik emateria l as use di nth etes t burns . Tabl e1 summarize s themercur y spik erate s fo r eac hru nan da naverag eo f thre e run s fo r

th e200 8 tes t

burns . Tabl e1 . Mercur y Spik eFee dRate s (lbs/hr ) fo r 200 8 Tes t

Burn s Base do n Documentatio no f

Spik ePreparatio n Stac k Ru n1 Ru n2 Ru n3 Averag e 2 0.0007 0 0.0007 0 0.0006 8 0.0006 9 3 0.0007 0 0.0007 1 0.0007 0 0.0007 0 4 0.018 6 0.018 4 0.017 8 0.018 3 

### III . Maxxa mMetal s Fee d Dat a I nMarc h2010 , w ecomplete dadat arevie w o f th e200 8 Tes t

Bur nReport s focusin g o n dat aqualit y (se eAttachmen t 4) . EP Anote dnumerou s deficiencies , includin g lac k o f complet edocumentation , unapprove ddeviatio nfro mapprove dqualit y assuranc e projec t plans , an dmissin g qualit y contro l data . W ebeliev ethere i s greater uncertaint y associate dwit hthes e result s an dmetal s dat afo r wast efee dfro mth etes t bur nshoul db e
2considere destimate dfo r th epurpose s o f

establishin g tes t

fee drates . W ebeliev ethat th e provisiona lmetal s dat aca nb euse dfo r establishin g syste mremova l efficiencie s becaus e th euncertaint y i s generall y mute db y thesubstantia l contributio no f spikin g material s i n eac hmeta l category . 

### IV. Moistur

eDat a A s discusse di nth eMa y 6 , 200 9 memorandum , EP Anote dsubstantia l difference s betwee nth emoistur edat aprovide db y PS C Republi c an dCR Lfro msample s analyze d withi nafe w week s o f

thetes t bur nan dmoistur edat aprovide db y Maxxa mfro msample s analyze dmonth s afte r

thetest . EP Areviewe dthemoistur edat afro mPS C Republi c an d C R Lan dfoun donl y mino r issue s wit hmethodolog y an ddocumentation . W econtinu et o believ ethemoistur econten t provide db y PS C Republi c an dconfirme db y CR Lt o b eth e mos t representativ eo f

tes t conditions . 

### V . Fee d Rat eSummar

y Asummar y o f

meta l tes t

fee drate s i s provide di nTabl e2 .

3Table 2 . 200 8 Tes t Bur n Fee d Rat e Summar

y Veoli a Environmenta

l Services , LLC , Sauget, I L

Uni t Meta

l Grou p Tes

t Fee d Rat e Claime d b y Veoli a fro

m August-Sep

t 200 8 (Ibs/hr ) Syste

m Removal Efficienc y (SRE ) Using Veolia's Claime d Fee d Rate s (% ) Tes

t Fee d Rat e Calculate

d b yEP Ai n Ma y200 9 Usin g Off-sit e Hg-Spik

e Dat a and Off-sit e Wast e Fee d Concentrations Correcte d wit h PS C Republic Moistur e Conten t (Ibs/hr )

Hg SV M LVM Hg SV M LVM 0.004

7 6 3 4 7 0.03 1 65.2 55.3 Tes t Fee d Rat e Calculate d b yEPAin Marc h 201 0 Using Calculate d Hg-Spik

e Composition and Off-sit e Wast e Fee d Concentrations Correcte d wit h PS C Republic Moistur

e Conten t (Ibs/hr ) Syste

m Removal Efficienc yUsing Tes t Fee d Rat e Calculate d b yEPA (% )
Hg 0.004

7 82.63

% 0.0018 5 SV M 6

3 N C 63.6 (Aug),62.9(Sept ) LVM 4

7 N C 47.2 (Aug),46.8(Sept ) 0.0016

5 63.6 (Aug),62.9(Sept

) 47.2 (Aug),46.8(Sept

) 83.22 % N C N C 0.0018 5 64.3 47. 7 0.0018 0 64,3 47.7 55.5 % N C N C 54.47 % N C N C 96.04 % N C N C 0.02 6 63.6 50.3 0.021 4 63.6 50. 3 95.3 % N C N C Tes

t Fee d Percen t o fHighes

t Fee d Rat e Historical betwee

n 7/1/0 4 Feedrat e and 1/1/0

8 (Ibs/hr ) (% )
31 % 124.9 % 55.2 % Veolia's Propose d Extrapolate

d Fee d Rat e (Ibs/hr )

33 % 89.1 % 61.7 % 36 % 109.6 % 71.9 % 0.0054

0 50.6 84.5 0.0054 5 72. 1 77.3 0.0598 1 58.4 69.9 0.01 7

45 9 39 9 0.01 7 45 9 39 9 0.25 7 50 0 50 0

4Attachmen t 1 Spik eCalculation s an dDocumentatio n Novembe r

19 , 200 9 - Dav eKlarich , Veoli a

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Produc t Specificatio n 

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### ) 2 

### -xH 2 

### 0 ( x= 1 - 2 ) Chemica l Abstrac t No : 7783-34-8 EINECS . 233-886-4 TSCA : Ye s Formul a Weight : 324.60 anhy . Technica l Data (Literature Values ) Density . 4.39 g/ml

_Boilin g point : No data foun d Meltin g Point : 79 ° C Flas h point : No data foun d Specificatio n (maximu m allowed ) Residu e afte rreduction : 0.01 % Chlorid e (CI) : 0.002% Sulfat e (S0 4 

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### PT072_0 2

Preparin g RD F Laborator ySample s Februar y9 , 200 5 Fo rAnalysi s 1 Scop e 

### 1. 1 Th e tes tmetho d cover s th e preparatio n ofrefuse-derive d fuel , RD F laborator y sample s fo ranalysis , th e laborator ysample s havin g previousl yobtaine d fro m representativ e RD F samples
. 2 Summar yo fMetho d 

### 2. 1 Sample s moisture i s reduce d byeithe rair-dryin g to allo wmechanica l reductio n ofsampl e withou t significan tchang e t o th e sample' s fur l propertie s o rth e moistur e i s remove d bydryin g i n a mechanica l draft ove n capabl e of maintainin g a controlle d temperature i n th e rang e fro m 9 5 - 105 ° C
. Th e sampl e particl e siz e i s the n reduce d to a for m suitabl e fo ranalysis
. 2. 2 Ifth e air-dryin g procedur e i s used , i ti s importan tt o measur e an d record th e ai r dr ymoistur e an d th e residua l moistur e i n orde rt o calculat e th e tota l moisture o f th e sample
. 2. 3 Ifth e sampl e i s bone-dried , th e tota l moistur e mustb e measure d an d recorded
. 2. 4 I n eithe rcase , th e sampl e mus thav e a tru e moisture readin g i n orde rt o calculat e value s o n bot h an d a s receive d an d dr ybasis
. NOTE : Bon e dryin g i s normall yuse d unles s otherwis e requeste d byth e client
. 3 Apparatu s an d Material s 

### 3. 1 Air-Dryin g Ove n 3.1. 1 Dryin g ove n - Alarg e chambe rmechanica l draf t ove n capabl e of maintainin g a controlle d temperature i n a rang e fro m 2 5 - 40 ° C
. Ai r change s shoul d b e a

tth e rat e o f1 to 4 change s pe rminute
. Ai rflow shoul d b e baffle d to preven tsample s fro m bein g blow n ou tofth e sampl e containers
. 3. 2 Bone-Dryin g Ove n 3.2. 1 Dryin g ove n - Alarg e chambe rmechanica l draf t ove n capabl e of maintainin g a controlle d temperature i n a rang e fro m 9 5 -110 ° C
. Ai r change s shoul d b e a

tth e rat e o f1 to 4 change s pe rminute
. Pag e 2 Ai rflowshoul d b e baffle d to preven tsample s fro m bein g blow n ou tof th e sampl e container
.

### 3. 3 Dryin g Pa n - Anoncorrodin g pa n o rmes h baske tt o b e use d fo rholdin g th e sampl e durin g th e dryin g process . 3. 4 Balanc e - Abalanc e ofsufficien tcapacit yt o weig h th e sampl e an d container
. Th e balanc e shoul d hav e a sensitivityof0. 5 g . 3. 5 Sampl e Reductio n 3.5. 1 Amil l operatin g o n th e principl e ofcuttin g o rshearin g actio n wil l b e use d fo rsampl e particl e siz e reduction
. Itwil l hav e th e capabilityt o regulat e th e particl e siz e o fth e fina l productb ymean s ofeithe rinterchangeabl e screen s o rmil l adjustments
. Th e mil l wil l b e enclose d an d shoul d generat e a minimu m amoun to fheatdurin g th e millin g process . Th e fina l produc

twil l pas s throug h a 0. 5 m m o rsmalle rscree n int o a receive r integra l wit h th e mill
. 3.5. 2 Analysi s Sampl e Container s - Heavy , vapo rimperviou s bags , properl y sealed ; o rnon-corrodin g cans , glas s jars , o rplasti cbottle s wit h airtigh t sealin g covers , mayb e use d t o stor e RD F sample s fo ranalysis
. Container s shoul d b e checke d fo rsuitabilitybymeasurin g weigh tlos s o r gai n ofth e sampl e an d containe rstore d fo ron e (1 ) wee k unde rambien t laborator yconditions
. Weigh tlos s o rgai n shoul d b e les s tha n 0. 5 % o f th e sampl e weigh tstore d i n th e container
. 3.5. 3 Shredde r- Alaborator yshredde rcapabl e o fshreddin g o rcuttin g large r particl e size s ofsoli d waste . Th e fina l productwil l pas s throug h a two (2 ) inc h o rsmalle rscree n into a receive rintegra l wit h th e shredder
. Reagent s 

### 4. 1 Becaus e ofth e nature o fsoli d wastes ; shredding , grindin g and/o rpulverizin g ma yb e difficul t atambien ttemperatures . T o improv e th e proces s o fparticl e siz e reductio n us e ice , dr yice , o rliqui d nitroge n ca n b e use d to coo l th e sampl e durin g th e grindin g process . NOTE : I

ti s importan tthat an ymoisture adde d t o th e sampl e du e t o condensatio n whe n usin g th e abov e coolin g agent s b e remove d prio rto analysis
.

Pag e 3 Samplin g (Whe n th e Laborator ydoe s th e Sampling) 

### 5. 1 RD F product s ar e frequentl ynonhomogeneous
. Fo rthi s reason , significan t

### car e shoul d b e exercise d to obtai n a representativ e sampl e fro m th e RD F lotto b e characterized
. 5. 2 Th e samplin g metho d fo rthi s procedur e shoul d b e base d o n th e agreemen t betwee n th e clien tan d th e laboratory
. 5. 3 Fo rthi s procedur e th e laborator ysampl e siz e wil l normall ynotexcee d 2 kg wit h som e variatio n possibl e dependin g o n th e laborator yequipmen tavailable
. 5. 4 Du e t

o th e heterogeneou s natur e ofRDF , dividin g a laborator ysampl e to a verysmal l size , analysi s sampl e mayresul ti n nonrepresentativ e results
. Sinc e millin g operation s mi xth e sampl e a s wel l a s reduc e particl e size , laborator y sample s shoul d notb e divide d before th e initia l preparatio n step s hav e bee n completed
. Procedur e 

### 6. 1 Weig h th e entire laborator ysampl e int o a tare d pan . Sampl e dept h i n th e dryin g pa n shoul d b e no tgreate rtha n 10 0 m m ( 4 inches ) an d an ylump s o f sampl e shoul d b e broke n up . Us e more tha n on e pa n i fnecessary . Ifa very fin e mesh-typ e pa n i s used , siz e th e mes h suc h that th e sampl e wil l notb e lost
. 6. 2 Air-Dryin g 6.2. 1 Ifsample s ar e t o b e ai rdried , ai rdr ysample s at1 0 -15 ° C abov e ambient , bu tnotgreate rtha n 40 ° C unti l th e weigh tlos s i s les s tha n 0. 1 % ofth e sampl e weigh tpe rhour
. 6. 3 Bone-Dryin g 6.3. 1 Ifth e sample s ar e to b e bon e dried , dr yth e sample s at10 7 + 3 ° C unti l th e weigh tlos s i s les s tha n 0. 1 % ofth e sampl e weigh tpe rhour
. T o spee d th e dryin g process , th e sample s mayb e carefull ystirre d avoidin g los s ofsample
. 6. 4 Recor d th e air-dr ylos s o rtota l moisture respectiv e ofth e metho d use d i n 6. 2 o r6.3
. 6. 5 Separat e an d weig h th e millable s an d nonmillable s fo rclassificatio n an d use , o ranalysis , i fnecessary . Calculat e th e millable s an d nonmillable s a s describe d i n Sectio n 7.2
. Pag e 4 

### 6. 6 Ifth e sampl e wa s air-drie d (6.2) , dr ya representativ e portio n ofth e air drie d millable s fractio n at10 7 + 3 ° C to constan tweigh ta s follows : 6.6. 1 Heata clean , emptydryin g pa n ata minimu m temperature o f10 7 + 3 ° C

### fo ratleas ton e (1 ) hour
. Whe n cooled , transfe rt o a desiccato ran d tar e weig h t o a n accurac yof0. 5 g . 6.6. 2 Plac e th e laborator ysampl e ofRD F i n th e dryin g pan . Weig h th e pa n an d th e sampl e to a n accurac yo f0. 5 g . 6.6. 3 Plac e th e pa n an d th e sampl e i n th e dryin g ove n at10 7 + 3 ° C fo ra minimu m o fon e (1 ) hour
. 6.6. 4 Remov e pa n fro m th e oven , desiccat e to coo l an d weig h to th e neares t 0. 5 g . 6.6. 5 Plac e bac k

int o th e ove n fo ron e (1 ) hou rat10 7 + 3 ° C
. 6.6. 6 Remov e an d plac e i n desiccator , cool , an d reweigh
. 6.6. 7 Repea tstep s 6.6. 5 an d 6.6. 6 unti l th e weigh tlos s i s les s tha n 0. 1 % / hour
. 6.6. 8 Calculat e % R M o n millabl e portio n ofth e sampl e a s describe d i n Sectio n 7.3
. 6. 7 Ifth e sampl e wa s air-drie d (6.2) , dr yth e nonmillable s at10 7 + 3 ° C to constan tweight
. Calculat e th e % R M o n th e nonmillable s a s describe d i n Sectio n 7.3
. 6. 8 Ifth e sampl e wa s boned-drie d step s 6. 6 nee d notb e done
. Th e tota l moisture wa s determine d i n Sectio n 6. 3 an d 6.4
. 6. 9 Reduc e th e air-drie d o rbone-drie d millable s t o a smalle rparticl e siz e usin g a cuttin g o rshearin g typ e shredde ro rmill
. Th e fina l productshoul d pas s thoug h a 0. 5 m m o rsmalle rscreen . Dependin g o n th e specifi cRD F product , thi s ste p mayinvolv e mor e tha n on e stag e o rreduction , that is , passin g th e sampl e throug h a shredde ro rmil l wit h large rsiz e screen s firs t an d the n millin g to pas s th e fina l screen . Fo rman ysamples , dr yic e o rliqui d nitroge n mayb e use d t o freez e th e sampl e prio rt o milling
. 6.1 0 Th e mixe d air-drie d o rbone-dried , finel ygroun d laborator ysampl e ca n b e furthe rsubdivide d t o a n analysis-siz e sample
. Retai n a minimu m of5 0 g a s th e analysi s sample
. An ydivisio n metho d use d wil l insur e that th e retaine d analysi s sampl e i s representativ e ofth e origina l laborator ysample
. Pag e 5 6.1 1 Kee p th e analysi s sampl e i n a labele d sampl e containe rhavin g a moisture-tigh t seal
. 6.1 2 I fth e sample s wer e air-dried , determin e th e residua l moisture o n th e millabl e portio n o fth e sample
.Calculation s 

### 7. 1 Calculat e th e air-dr ymoisture a s follows : AD L= [(W b 

### -Wa)/Wb ] * 10 0 Where : AD L= % ai rdr

ylos s W b = weigh tofsampl e before ai rdryin g W a = weigh tofsampl e afte rai rdryin g 7. 2 Calculat e th e millable s an d th e nonmillable s ofth e sample :

M = Wm/W s * 10 0 Where : M = % millable s W m = weigh tofth e millable s W s = weigh tofth e sample s (millable s an d nonmillables ) N M = Wnm/W s * 10 0 Where : N M = % nonmillable s Wn m = weigh tofth e nonmillable s W s = weigh tofth e sampl e NOTE : Nonmillable s usuall yar e noncombustibl e an d ca n b e use d i n

contributin g to th e as h valu e o rnoncombustibl e valu e portio n of th e sample
.

Pag e 6 7. 3 Calculatio n ofresidua l moistures :

wt . O fA D sampl e afte rdryin g R M - * 10 0

wt . O fA D sampl e before dryin g

### 7. 4 Ifth e sample s wer e air-drie d an d residua l moisture don e o n eithe rth e millables, an d /

o rnonmillables , calculat e th e tota l moistur e a s follows :
T M = A D + 10 0

[ ( 100-A D ) ( R M ) j j Where : T M = Tota l Moisture , % A D = Ai rDr

yloss , % R M = Residua l Mositure , % 7. 5 Reference s 7.5. 1 AST M E82 9

### Veoli aEnvironmenta l Services Trad e Wast

e Incineratio n PAG E NO . 6 0 BOO KNO . 210 1 

### Metals - Standard Preparatio n Concentration(ug/ml ) /

Nam e Cone /

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# X Reviewe d By : Date :Attachmen t 2 Electroni c Messag e Marc h8 , 201 0 - Dav eKlarich , Veoli aEnvironmenta l Services , LL C to Chri s Lambesi s EP A

### Re : Requeste d Informatio n David.Klaric h to : Christophe rLambesi s Cc : Dennis.Warchol , Doug.Harris , Tod d Ramal y 03/08/201 0 05:0 1 P M From : To : Cc : Davi d .Klarich@veoliaes.co m

Christophe rLambesis/R5/USEPA/US@EP A Dennis.Warchol@veoliaes.com , Doug.Harris@veoliaes.com , Tod d Ramaly/R5/USEPA/US@EP A
Chris , I trie dt o contac t yo u toda yb yphone , bu t wa s unabl e t o catc hyo u i n th e office . Attache dbelo wi s th e "Metal s Standar dPreparation " la bshee t I believ e yo u wante d fo r vial s 120 1 - 1298 . I f thi s i s no t wha t yo u wer e lookin g for , o r ther e i s an yadditiona l informatio ntha t I ca n sen dyou , pleas e le t me know . Bac k i n November , 2009 , PS C sen t PT072_0 2 (Preparin g RD F Laborator y Samples ) t o m e whe n I requested , vi a AEC0M , thei r sampl e dryin g procedure s f o r th e Veoli a wast e samples . Thi s wa s include di n th e packag e o f informatio ntha t I sen t yo u i n November . I f yo u di d no t receiv e thi s procedur e o r yo u ar e lookin g fo r additiona l o r differen t procedures , pleas e l e t me know . I wil l giv e yo u a cal l agai ntomorrow . Dav e

(Se e attache dfile : Stwiscannerl0030815340.pdf )

Lambesis.Christo p her@epamail.epa. g o v T o David.Klarich@veoliaes.co m 03/02/201 0 05:0 0 P M Dennis.Warchol@veoliaes.com , Doug.Harrisdveoliaes.com , Ramaly.Todd@epamail.epa.go v c c Subjec t Re : Requeste dInformatio nDave ,

We ar e reviewin g th e spik e documentatio n tha t yo u provided . Th e packag e i s missin g som e information . Ca nyo u sen d th e "Metal s Standar d Preparation " Veoli a la bsheet s fo r th e mercur yspik e mak e u p fo r vial s 120 1 - 129 8 {prepare d b yTre yFormb yan dRa yHasty) . The ywil l probabl y b e foun d o no r afte r pag e 6 0 o f boo k 2101 . Also , ca nyo u pleas e sen d PS C Republi c Laboratory' s SO P fo r percen t moistur e analysi s a s applie d t o th e wast e sample s fro mth e 200 8 tes t burns . Pleas e cal l me i f yo u hav e an yquestions . Christophe r Lambesi s Environmenta l Scientis t U. S EP ARegio n5 Lan d an dChemical s Divisio n (312 ) 886-358 3

From : David.Klarich@veoliaes.co m
To : Christophe r Lambesis/R5/USEPA/US@EP A
Cc : Charle s Hall/R5/USEPA/US@EPA , Geneviev e Damico/R5/USEPA/US@EPA , Tod d Ramaly/R5/USEPA/US@EPA ,

Doug.Harris@veoliaes.com , Dennis.Warchol@veoliaes.co m
Date : 11/19/200 9 02:2 5 P M Subject : Requeste d Informatio n

Chris , Wante d t o le t yo u kno wtha t th e mercur yspik e informatio nan dth e PS C procedur e tha t yo u requeste do nth e Novembe r 3 conferenc e cal l i s bein g maile dtoday . Sorr yfo r th e delay , bu t a s Dou g ha dmentione d durin g th e call , I wa s ou t o f th e offic e fo r a perio do f tim e afte r th e call . I f y o u hav e an yquestion s o nth e document s o r nee d additiona l information , pleas e contac t me . Dav e

## Veoli aEnvironmenta l Services Trad e Wast

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## ss&^ A> ZJ* Reviewe d By : Date :Attachmen t 3 Calculate dSpik eConcentration s Tod dRamaly , EP AMercur ySpik e Concentration s Base d o n Spik e Preparatio n Procedure s Dat a o n Mercur y( I I

) nitrat e hydrate , ACS , 98.0 % mi n (Catalo g Numbe r14497) , manufacture d b yAif a Aesa r( AJohnso n MattheyCompany) , War d Hill , M A Molecula rweigh tmonohydral e dihydrat e H g 200.5 9 1 200.5 9 1 200.5 9 N 14.006 7 2 28.013 4 2 28.013 4 O ' 15.999 4 7 111.995 8 8 127.995 2 H •1.0079 4 2 2.0158 8 4 4.0317 6 Tota l Molecula rWeigh t 342.6150 8 360.6303 6 58.55 % mol e fractio n H g 65.62 % mol e fractio n H g minimu m solutio n strengt h 98.00 % minimu m 98.00 % minimu m 57.38 % % H g i n produc t 54.51 % % H g i n produc t
batc h pre p dat e mercur yconcentratio n i n spik e produc trange s fro m minimu m maximu m Batc h Use d fo rUnit s 2 an d 3 54.51 % t o 58.55 % 6/23/200 8 mas s o fspik e produc t26. 2 g 14.2 8 g H g 15.3 4 g H g 14281.5 2 m g H g 15339.2 5 m g H g brough tu p t o 2 5 liter s 571.2 6 mq/ LH q 613.5 7 mg/ LH g Spik e Sampl e Dat a off-sit e la b (Veoiia ) 71 0 mg/LH g Spik e Vial s 1-70O 100%ofS2,S 3 Uni t2 Run t 98 6 mg/ LH g

Ru n 2 66 7 mg/LH g Ru n 3 54 8 mg/ LH g
Uni t3 Ru n 1 53 4 mg/LH g 66 5 mg/ LH g CR L

Ru n 2 62 7 mg/LH g Ru n 3 65 5 mq/LH q
6/27/200 8 mas s o fspik e produc t 9 1 g 49.6 0 49603.7 4 g H g

m g H g 53.2 8 53277.5 4 g H g

m g H g brough tu p t o 3 liter s 16534.5 8 Apparentl yno t use d E n th e tes t mg/LH g 17759 .1 8 mg/LH g

Batche s Use d fo rUni t 4 S'5/200 8 mas s o fspik e produc t 121.00 4 g 65-9 6 65958.8 1 g H g

m g H g 70.8 4 70843.9 1 g H g

mgH g brouqh tu p t o 7 liter s 9422.6 9 mq/ LH q 10120.5 6 fnq/ LH q Spik e Sampl e Dat a S4-100%-R1,34.B%-R 2 Spik e Vial s 701-97 0 off-sit e la b (Veolia ) C R L t050 0 mg/ L 625 0 mq/ L 8/11/200 8 mas s o fspik e produc t 43.00 9 g 23.4 4 23444.0 4 g H g

m g H g 25.1 8 25180.3 7 g/H g

m g H g brouqh tu p t p 2. 5 liter s 9377.6 2 m q H g 10072.1 5 m q H q Spik e Sampl e Dat a S4-65.2%-R2
. 36%-R 3 Spik e Vial s 1101-119 3 off-sit e la b (Veolia ) 1040 0 mq/ L 8/21/200 8 mas s o fspik e produc t 43.00 1 g 23.4 4 g H g 25.1 8 g/H g 23439.6 8 m g H g 25175.6 9 m g H g brouqh tu p t p 2. 5 liter s 9375.8 7 m q H q 10070.2 8 m q H q Spik e Sampl e Dat a 64 % o fS4-R 3 Spik e Vial s 1201 -129 8 (al l o rpartially ) off-sit e la b (Veoiia ) 1100 0 mq/ L 8/21/200 8 mas s o fspik e produc t 43.00 2 g 23.4 4 g H g 25.1 8 9/H g 23440.2 2 rngH g 25176.2 7 m g H g brough tu p t p 2. 5 liter s 9376.0 9 m q H q 10070.5 1 m q H g Spik e Sampl e Dat a 64 % o fS4-R 3 Spik e Vial s 1201-129 8 (al l o rpartially ) off-sit e la b (Veolia ) 1100 0 mq/ L Calc , Maximu m Maxxa m La b Spik e Spik e Cate
. Minimu m Spik e Concentratio n Concentratio n Concentratio n (mg/L ) (mg/L ) (mg/L ) Uni t4 Ru n 1 942 3 1012 1 1120 0

Ru n 2 939 3 1008 9 1160 0 Ru n 3 937 6 1007 1 1250 0Attachmen t 4 Marc h26 , 201 0 Memorandu mt o File : Dat aRevie w o f Veoli aTria lBur nReport s October , 200 8 Christophe r

Lambesis , EP AMEMORANDU M UNITE D STATE S ENVIRONMENTA LPROTECTIO NAGENC Y REGIO N5 

### To : From : Date : Subject: Christophe r Lambesis , Environmenta l Scientist , LC D Marc h26 , 201 0 \ Dat aRevie w o f

Veoli aTria lBur nReport s October, 200 8 Fil e(] {

Thi s i s asummary o f

USEP ALC D staf

f revie w o f

Veolia' s thre e tria lbu mreport s submitte dOctober , 200 8 titled : "Metals Performance Test Report Prepared

forthe Fixed

Hearth Incinerator Number2 in Accordance with 40 CFR § 63 Subpart EEE" "Metals Performance Test Report Prepared

forthe Fixed

Hearth Incinerator Number3 in Accordance with 40 CFR § 63 Subpart EEE" "Metals Performance Test Report Prepared

forthe Rotary Kiln Incinerator Number4

in Accordance with 40 CFR § 63 Subpart EEE" Th eprimar y focu s o f

thi s revie w wa s give nt o dat aquality , accuracy , precision , and representativeness . Th efollowin g deficiencie s werenote ddurin g thereview : 1 ) Th ereport s d o not

referenc ethetes t

plan s submitte db y Veolia . 2 ) Maxxa mLaboratory di dno t denot e thebul k

an dcontainerize dsolid s wast e fee d analysi s as wet

o r dr y weight . USEP Adetermine dtha t theMaxxa mlaboratory result s ar edry weigh t

reported . Maxxa mdrie dthesample s befor eanalysi s withou t performin g percent

moistureanalysis . 3 ) Th emercury spik econcentration s use di ntria lbu mcalculation s shoul dbethe laboratory' s intende dpreparatio nconcentration s followe db y confirmatio n analysis . Thes ereport s incorrectl y us etheconfirmator y result s as thespik e concentrations . 4 ) Th ereport s d o not

includ eanalytica l method s standardoperatio nprocedures . 5 ) Th ereport s stat

e tha t theanalytica l datahas beenvalidate dan dal l datai s acceptable . However , th edatahas not

beenproperl y validate dan dther e ar eman y quality contro l problem s (seeexample s below) . Th eanalytica l dataneed s to be validate db y aqualifie dprofessiona l an dal l quality contro l problem s needt o b e addresse dclearly . 6 ) Th ewast

e profil ereports , calle dTW ILa b Report , report s sampl eaverage s an dd o not repor t individua lsampl eresults . The y do not repor t an y quality contro l data . The y hav eimprope r

cross-out s an dhav equestionabl eresult s tha t ma y be detectio nlimit s insteado f quantitate dvalues . 7 ) Therear

eno quality contro l datafo r any spikeanalysis .X ) Ther ear

en o chain-of-custod y forms for any spik eanalysis . 9 ) Ther ear

en o complete dchain-of-custod y form s fo r sample s sen

t t o Maxxa mo r PS C Republi c laboratories . 10 ) Th ePS C Republi c holdin g time s for percent moistureanalysi s exten dfro m9 to 1 6 days . Percent

moistureanalysi s shoul db eperforme das soo nas possibl eafte r sampling . 11 ) Th esubcontracte dlaboratories , PS C Republi c an dMaxxa mMississauga , d o not hav eNELA C accreditatio nfo r specifi c media . 12) Th eChemica lWast emanagement WasteProfil eReport s contai nresult s tha t appea r t o beanalytica l detectio nlimit s an dno t detecte dresults . 13 ) Th eUni t

2 repor t state s tha

t themercury blank

spik efo r

stac k analysi s hadalo w recovery . Thi s shoul dbeexplained . 14 ) Th eUni t

2 , week on erepor

t state s tha

t th emetal s analysi s fo r

fee dwaste result s require dsampl edilutio ndu eto sampl ematrix . Thi s need s to bechecke dan d explained . 15 ) Th eUni t

2 , week on erepor

t doe s not

repor t any duplicat eanalysi s result s fo r the metal s analysi s fo r

fee dwaste results . 16) Th eUni t

2 , wee k on erepor

t state s tha

t themetal s analysi s fo r fee dwaste result s had0 % spik erecovery fo r arsenic . Th earseni c spik eanalysi s wa s reporte das O.Oppm . 17 ) Th eUni t

3 report , stac k

sampl eanalysi s repor

t has anunclear

explanatio no f

th e mercury spik erecoveries . 18) Th eUni t

3 report , fee dwaste analytica l result s hav eseveral section s tha t hav e qualit y contro l comment s tha t appea r to hav ebee nconceale db y white-out . 19) Th eUni t

3 report , fee dwaste analytica l result s hav egeneral comment s o npag e 1 1 o f 1 4 tha t explai nth

emercury spik eanalyse s ar eno t reliable . 20 ) Th eUni t

3 report , fee dwaste analytica l result s fo r metal s an dmercury d o no t hav eduplicat eresults . 21 ) Th eUni t

4 report , stac k

sampl eanalytica l result s stat e repor t themercury spik e resul t i s lo w an dthemetal s result s hav eseveral quality contro l irregularities . 22 ) Th eUni t

4 report , fee dwaste analytica l result s report anon-calculabl eresul t fo r chromiu mrecovery an dirregularitie s wit hmercury qualit y control . Give nth enumerou s explaine dan dunexplaine ddeficiencie s i nthes e reports , w ebeliev e ther e i s greater

uncertainty associate dwit hthes e results . A s such , thi s datashoul db e regarde das provisional .