PI'N~LE~ Environmental Testing

PL LD. 709293

October 17,2007

NMED-GWQB

1190 St. Francis Drive

Santa Fe, NM 87502

Project NamelNumber: ATSF/ABQ

Attention: David L. Mayerson

On 09/28/07, Pinnacle Laboratories Inc., (ADHS License No. AZ0643), received a request to

analyze non-aq samples. The samples were analyzed with EPA methodology or equivalent

methods. The results ofthese analyses and the quality control data, which follow each set of

analyses, are enclosed.

All samples were analyzed by Flowers Chemical La~oratories, Inc. (FCL), Altamonte Springs,

FL.

Ifyou have any questions or comments, please do not hesitate to contact us at (505) 344-3777.

H. Mitchell Rubenstein, Ph.D.

General Manager

MR:jt

Enclosure

2709-D Pan American Fwy, NE Albuquerque, NM 87107 505.344.3777 505.344.4413 FAX 877.PIN.1998 TOLL FREE

www.pinnaclelabs.org www.pinnaclelabsonline.com

1

000503
"

PIN ~LE~ Environmental Testing

CLIENT :NMED-GWQB DATE RECENED :09/28/07

PROJECT # :(NONE)

PROJECT NAME :ATSF/ABQ REPORT DATE : 10/17/07

PL ID: 709293

PINNACLE CLIENT DATE

ID# DESCRIPTION MATRIX COLLECTED

01 709293-01 CS-G10-3-1 NON-AQ 09/28/07

02 709293-02 D1 NON-AQ 09/28/07

03 709293-03 CS-G04-1 NON-AQ 09/28/07

04 709293-04 CS-G06-1 NON-AQ 09/28/07

---TOTALS---

MATRIX

NON-AQ

#SAMPLES

4

2709-D Pan American Fwy, NE Albuquerque, NM 87107 505.344.3777 505.344.4413 FAX 877.PIN.1998 TOLL FREE

www.pinnaclelabs.org www.pinnaclelabsonline.com

2

000504
P.O. Box 150597, Altamonte Springs FL 32715-0597 Phone 407-339-5984 Fax 407-260-6110 www.flowerslabs.com

8253 South U.S. Highway 1, Port St. Lucie FL 34952-2860 Phone 772-343-8006 Fax 772-343-8089

P.O. Box 1200, Madison FL 32341 Phone 850-973-6878 Fax 850-973-6878

Pinnacle Laboratories

2709 D Pan American Freeway NE

Albuquerque.NM 87107

Date Received: Oct 1, 2007

PO#: 709293

Client Project #: NMGW

Date Sampled: Sep 28, 2007

Oct 12, 2007; Invoice: 49487

Report Summary

FCL Project Manager: June S. Flowers

Laboratory # Sample Description

49487S01 CS-G10-3-3/709293-01

49487S02 D11709293-02

49487S03 CS-G04-11709293-03

49487S04 CS-G06-11709293-04

Analysis

EPA6020

EPA8270

SM2540B

XBNE

EPA6020

EPA8270

SM2540B

XBNE

EPA6020

EPA8270

SM2540B

XBNE

EPA6020

EPA8270

SM2540B

XBNE

Chemist

EVB

CLS

RMV

CDG

EVB

CLS

RMV

CDG

EVB

CLS

RMV

CDG

EVB

CLS

RMV

CDG

Location

Main Lab

Main Lab

Main Lab

Main Lab

Main Lab

Main Lab

Main Lab

Main Lab

Main Lab

Main Lab

Main Lab

Main Lab

Main Lab

Main Lab

Main Lab

Main Lab

SampleMatrix

Soil

Soil

Soil

Soil

Certificate of Results

Sample integrity was certified prior to analysis. Test results meet all requirements of the NELAC Standards except as noted in

the Quality Control Report. Uncertainties for these data are available on request. This report may not be reproduced in part;

results relate only to items tested.

FLOOH: E83018 (Main Lab) FLOOH: E86562 (South Lab) FLOOH: E82405 (North Lab) NJOEP: FL015 Page 1 of9

3

000505
P.O. Box 150597, Altamonte Springs FL 32715-0597 Phone 407 - 339 - 5984 Fax 407 - 260 - 6110 www.f1owerslabs.com

8253 South U.S. Highway 1. Port St. Lucie FL 34952-2860 Phone 772 - 343 - 8006 Fax 772 - 343 - 8089

P.O. Box 1200. Madison FL 32341 Phone 850-973-6878 Fax 850-973-6878

Pinnacle Laboratories PO#: 709293

2709 0 Pan American Freeway NE Client Project #: NMGW

Albuquerque,NM 87107 Date Sampled: Sep 28, 2007

Oct 12,2007; Invoice: 49487

Analysis Report

lab #: 49487S01 Sampled: 09/28/0710:27 AM Desc: CS-G10-3-31709293-01

Parameter Result Units DF MDl PQl QC Batch Method CAS # Analyzed

% Moisture 5.39 %Wt 1.00 0.000250 0.000500 10090704 SM2540B 10/02/07

Zinc 30.7 mg/Kg 1.00 1.00 2.00 10091027 EPA6020 7440-66-6 10/04/07

1-methyl-Naphthalene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 090-12-0 10/10/07

2-methyl-Naphthalene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 91-57-6 10/10/07

Acenaphthene 6.00 U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 83-32-9 10/10/07

Acenaphthylene 14.5 ug/Kg 1.00 6.00 12.0 10091194 EPA8270 208-96-8 10/10/07

Anthracene 79.8 ug/Kg 1.00 6.00 12.0 10091194 EPA8270 120-12-7 10110/07

Benzo(a)anthracene 53.4 ug/Kg 1.00 6.00 12.0 10091194 EPA8270 56-55-3 10/10/07

Benzo(a)pyrene 32.0 ug/Kg 1.00 6.00 12.0 10091194 EPA8270 50-32-8 10/10/07

Benzo(b)f1uoranthene 104 ug/Kg 1.00 6.00 12.0 10091194 EPA8270 205-99-2 10/10/07

Benzo(g,h,i)perylene 57.9 ug/Kg 1.00 6.00 12.0 10091194 EPA8270 191-24-2 10/10/07

Benzo(k)f1uoranthene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 207-08-9 10/10/07

Chrysene 90.4 ug/Kg 1.00 6.00 12.0 10091194 EPA8270 218-01-9 10/10/07

Oibenz(a,h)anthracene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 53-70-3 10/10/07

Fluoranthene 230 ug/Kg 1.00 6.00 12.0 10091194 EPA8270 206-44-0 10/10/07

Fluorene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 86-73-7 10/10/07

Indeno(1,2,3-cd)pyrene 28.9 uglKg 1.00 6.00 12.0 10091194 EPA8270 193-39-5 10/10/07

Naphthalene 14.8 ug/Kg 1.00 6.00 12.0 10091194 EPA8270 91-20-3 10/10/07

Phenanthrene 138 ugfKg 1.00 6.00 12.0 10091194 EPA8270 85-01-8 10/10/07

Pyrene 213 ugfKg 1.00 6.00 12.0 10091194 EPA8270 129-00-0 10/10/07

Surr:2-Fluorobiphenyl (79-120%) 75.62% 1.00 0.0100 0.0200 10091194 EPA8270 321-60-8 10/10/07

Surr:Nitrobenzene-d5 (79-120%) 105.08% 1.00 0.0100 0.0200 10091194 EPA8270 10/10/07

Surr:Terphenyl-d14 (79-120%) 130.42% 1.00 0.0100 0.0200 10091194 EPA8270 10/10f07

Base_NeutraLExtraction 30.0 9 1.00 10091246 XBNE 10/08/07

Lab #: 49487S02 Sampled: 09f28/07 11 :00 AM Desc: 011709293-02

Parameter Result Units DF MDl PQl QC Batch Method CAS # Analyzed

FLOOH: E83018 (Main Lab) FLDOH: E86562 (South Lab) FLOOH: E82405 (North Lab) NJDEP: FL015 Page 2 of9

000506
P.O. Box 150597, Altamonte Springs FL 32715-0597 Phone 407 - 339 - 5984 Fax 407 - 260 - 6110 www.f1owerslabs.com

8253 South U.S. Highway 1. Port St. Lucie FL 34952-2860 Phone 772 - 343 - 8006 Fax 772 - 343 - 8089

P.O. Box 1200. Madison FL 32341 Phone 850-973-6878 Fax 850-973-6876

Pinnacle Laboratories PO#: 709293

2709 D Pan American Freeway NE Client Project #: NMGW

Albuquerque,NM 87107 Date Sampled: Sep 28, 2007

Oct 12, 2007; Invoice: 49487

Lab#: 49487S02 Sampled: 09/28/07 11 :00 AM Oesc: D11709293-02

Parameter Result Units OF MOL PQL QC Batch Method CAS # Analyzed

% Moisture 5.54 %Wt 1.00 0.000250 0.000500 10090704 SM2540B 10/02/07

Zinc 19.7 mg/Kg 1.00 1.00 2.00 10091027 EPA6020 7440-66-6 10/04/07

1-methyl-Naphthalene 6.00 U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 090-12-0 10/10/07

2-methyl-Naphthalene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 91-57-6 10/10/07

Acenaphthene 6.00 U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 83-32-9 10110/07

Acenaphthylene 6.00 U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 208-96-8 10110/07

Anthracene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 120-12-7 10110/07

Benzo(a)anthracene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 56-55-3 10/10/07

Benzo(a)pyrene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 50-32-8 10/10/07

Benzo(b)f1uoranthene 14.8 ug/Kg 1.00 6.00 12.0 10091194 EPA8270 205-99-2 10/10/07

Benzo(g,h,i)perylene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 191-24-2 10110/07

Benzo(k)fluoranthene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 207-08-9 10110/07

Chrysene 8.50 I ug/Kg 1.00 6.00 12.0 10091194 EPA8270 218-01-9 10/10/07

Dibenz(a,h)anthracene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 53-70-3 10/10/07

Fluoranthene 10.71 ug/Kg 1.00 6.00 12.0 10091194 EPA8270 206-44-0 10/10/07

Fluorene 6.00 U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 86-73-7 10/10/07

Indeno(1,2,3-cd)pyrene 6.0OU ug/Kg 1.00 6.00 12.0 10091194 EPA8270 193-39-5 10/10/07

Naphthalene 6.00 U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 91-20-3 10/10/07

Phenanthrene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 85-01-8 10/10/07

pyrene 8.30 I ug/Kg 1.00 6.00 12.0 10091194 EPA8270 129-00-0 10110/07

Surr:2-Fluorobiphenyl (79-120%) 63.94% 1.00 0.0100 0.0200 10091194 EPA8270 321-60-8 10/10/07

Surr:Nitrobenzene-d5 (79-120%) 61.94% 1.00 0.0100 0.0200 10091194 EPA8270 10110/07

Surr:Terphenyl-d14 (79-120%) 100.36% 1.00 0.0100 0.0200 10091194 EPA8270 10/10/07

Base_NeutraLExtraction 30.0 9 1.00 10091246 XBNE 10/08/07

Lab #: 49487S03 Sampled: 09/28/07 11 :25 AM Oesc: CS-G04-11709293-03

Parameter Result Units OF MOL PQL QC Batch Method CAS # Analyzed

% Moisture 6.33 %Wt 1.00 0.000250 0.000500 10090704 SM2540B 10/02/07

Zinc 15.1 mg/Kg 1.00 1.00 2.00 10091027 EPA6020 7440-66-6 10/04/07

FLOOH: E83018 (Main Lab) FLOOH: E86562 (South Lab) FLOOH: E82405 (North Lab) NJOEP: FL015 Page30f9

000507
P.O. Box 150597, Altamonte Springs FL 32715-0597 Phone 407 - 339 - 5984 Fax 407 - 260 - 6110 www.f1owerslabs.com

8253 South U.S. Highway 1, Port St. Lucie FL 34952-2860 Phone 772 - 343 - 8006 Fax 772 - 343 - 8089

P.O. Box 1200, Madison FL 32341 Phone 850-973-6878 Fax 850-973-6878

Pinnacle Laboratories PO#: 709293

2709 D Pan American Freeway NE Client Project #: NMGW

Albuquerque,NM 87107 Date Sampled: Sep 28, 2007

Oct 12, 2007; Invoice: 49487

lab #:49487S03 Sampled: 09/28/07 11:25 AM Cese: CS~G04-11709293-03

Parameter Result Units CF MCl PQl QC Batch Method CAS # Analyzed

1-methyl-Naphthalene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 090-12-0 10/10/07

2-methyl-Naphthalene 6.00U uglKg 1.00 6.00 12.0 10091194 EPA8270 91-57-6 10/10/07

Acenaphthene 6.00 U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 83-32-9 10/10/07

Acenaphthylene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 208-96-8 10/10/07

Anthracene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 120-12-7 10/10/07

Benzo(a)anthracene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 56-55-3 10/10/07

Benzo(a)pyrene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 50-32-8 10/10/07

Benzo(b)f1uoranthene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 205-9~2 10/10/07

Benzo(g,h,i)perylene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 191-24-2 10/10/07

Benzo(k)f1uoranthene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 207-08-9 10/10/07

Chrysene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 218-01-9 10/10/07

Dibenz(a,h)anthracene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 53-70-3 10/10/07

Fluoranthene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 206-44-0 10/10/07

Fluorene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 86-73-7 10/10/07

Indeno(1,2,3-cd)pyrene 6.00 U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 193-39-5 10110/07

Naphthalene 6.00 U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 91-20-3 10/10/07

Phenanthrene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 85-01-6 10/10/07

Pyrene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 129-00-0 10/10/07

Surr:2-Fluorobiphenyl (79-120%) 81.30% 1.00 0.0100 0.0200 10091194 EPA8270 321-60-8 10/10/07

Surr:Nitrobenzene-d5 (79-120%) 87.83% 1.00 0.0100 0.0200 10091194 EPA8270 10/10/07

Surr:Terphenyl-d14 (79-120%) 112.53% 1.00 0.0100 0.0200 10091194 EPA8270 10/10/07

Base_NeutraLExtraction 30.0 9 1.00 10091246 XBNE 10/08/07

lab #: 49487S04 Sampled: 09/28/0701:47 PM Cese: CS-G06-11709293-04

Parameter Result Units CF MCl PQl QC Batch Method CAS # Analyzed

% Moisture 21.2 %Wt 1.00 0.000250 0.000500 10090704 SM2540B 10/02/07

Zinc 18.3 mg/Kg 1.00 1.00 2.00 10091027 EPA6020 7440-66-6 10/04/07

1-methyl-Naphthalene 48.21 ug/Kg 5.00 30.0 60.0 10091194 EPA8270 090-12-0 10/10/07

2-methyl-Naphthalene 30.0U ug/Kg 5.00 30.0 60.0 10091194 EPA8270 91-57-6 10/10/07

FLOOH: E83018 (Main Lab) FLOOH: E86562 (South Lab) FLOOH: E82405 (North Lab) NJOEP: FL015 Page4of9

000508
P.O. Box 150597, Altamonte Springs FL 32715-0597 Phone 407 - 339 - 5984 Fax 407 - 260 - 6110 www.f1owerslabs.com

8253 South U.S. Highway 1. Port St. Lucie FL 34952-2860 Phone 772 - 343 - 8006 Fax 772 - 343 - 8089

P.O. Box 1200, Madison FL 32341 Phone 850-973-6878 Fax 850-973-6878

, ,.,-.'~' ,.' _~....." I .11 1

""-!

Pinnacle Laboratories PO#: 709293

2709 D Pan American Freeway NE Client Project #: NMGW

Albuquerque,NM 87107 Date Sampled: Sep 28, 2007

Oct 12, 2007; Invoice: 49487

Lab#: 49487S04 Sampled: 09/28/0701:47 PM Oesc: CS~G06-11709293-o4

Parameter Result Units OF MOL PQL QC Batch Method CAS # Analyzed

Acenaphthene 1350 ug/Kg 5.00 30.0 60.0 10091194 EPA8270 83-32-9 10110/07

Acenaphthylene 174 ug/Kg 5.00 30.0 60.0 10091194 EPA8270 208-96-8 10/10/07

Anthracene 30.0 U ug/Kg 5.00 30.0 60.0 10091194 EPA8270 120-12-7 10/10/07

Benzo(a)anthracene 1150 ug/Kg 5.00 30.0 60.0 10091194 EPA8270 56-55-3 10/10/07

Benzo(a)pyrene 459 ug/Kg 5.00 30.0 60.0 10091194 EPA8270 50-32-8 10/10/07

Benzo(b)f1uoranthene 1120 ug/Kg 5.00 30.0 60.0 10091194 EPA8270 205-99-2 10/10/07

Benzo(g,h,i)perylene 123 ug/Kg 5.00 30.0 60.0 10091194 EPA8270 191-24-2 10/10/07

Benzo(k)f1uoranthene 30.0U ug/Kg 5.00 30.0 60.0 10091194 EPA8270 207-08-9 10/10/07

Chrysene 998 ug/Kg 5.00 30.0 60.0 10091194 EPA8270 218-01-9 10/10/07

Dibenz(a,h)anthracene 30.0U ug/Kg 5.00 30.0 60.0 10091194 EPA8270 53-70-3 10/10/07

Fluoranthene 7990 ug/Kg 5.00 30.0 60.0 10091194 EPA8270 206-44-0 10/10/07

Fluorene 1630 ug/Kg 5.00 30.0 60.0 10091194 EPA8270 86-73-7 10/10/07

Indeno(1,2,3-cd)pyrene 144 ug/Kg 5.00 30.0 60.0 10091194 EPA8270 193-39-5 10/10/07

Naphthalene 30.0U ug/Kg 5.00 30.0 60.0 10091194 EPA8270 91-20-3 10/10/07

Phenanthrene 1260 ug/Kg 5.00 30.0 60.0 10091194 EPA8270 85-01-8 10/10/07

Pyrene 6450 ug/Kg 5.00 30.0 60.0 10091194 EPA8270 129·00-0 10/10/07

Surr:2-Fluorobiphenyl (79-120%) 70.34% 5.00 0.0500 0.100 10091194 EPA8270 321-60-8 10/10/07

Surr:Nitrobenzene-d5 (79-120%) 79.11% 5.00 0.0500 0.100 10091194 EPA8270 10/10/07

Surr:Terphenyl-d14 (79-120%) 128.74% 5.00 0.0500 0.100 10091194 EPA8270 10/10/07

Base_NeutraLExtraction 30.0 9 1.00 10091246 XBNE 10/08/07

FLOOH: E83018 (Main Lab) FLOOH: E86562 (South Lab) FLOOH: E82405 (North Lab) NJOEP: FL015 Page50f9

000509
P.O. Box 150597, Altamonte SprIngs FL 32715-0597 Phone 407 - 339 - 5984 Fax 407 - 260 - 6110 www.f1owerslabs.com

8253 South U.S. Highway 1, Port St. Lucie FL 34952-2860 Phone 772 - 343 - 8006 Fax 772 - 343 - 8089

P.O. Box 1200. Madison FL 32341 Phone 850-973·6878 Fax 850-973-6878

Pinnacle Laboratories

2709 D Pan American Freeway NE

Albuquerque,NM 87107

QualityConttolBatch: 10091027

Blank

Zinc

Analyst: EVB

Result Units

1.00U mg/Kg

PO#: 709293

Client Project #: NMGW

Date Sampled: Sep 28, 2007

Oct 12, 2007; Invoice: 49487

Quality Report

Laboratory Control Sample

Zinc

Matrix Spike

Zinc

Matrix Spike Duplicate

Zinc

Result

0.267

Result

0.284

Result

0.281

Units

mg/Kg

Units

mg/Kg

Units

mg/Kg

Spike

0.250

Spike

0.250

Spike

0.250

%REC %RECLim

106.64 70.72-128.29

%REC %RECLim Sample

83.43 35.26-158.48 0.0751

%REC %RECLim Sample RPD

82.37 35.26-158.48 0.0751 0.94

RPDLim

36.34

Quality Control Batch: 10091194

Blank

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene

Benzo(b)f1uoranthene

Benzo(g,h,i)perylene

Benzo(k)f1uoranthene

Chrysene

Dibenz(a,h)anthracene

Fluoranthene

Fluorene

Indeno(1,2,3-cd)pyrene

Analyst: CLS

Result Units

6.00U ug/Kg

6.00U ug/Kg

6.00U ug/Kg

6.00U ug/Kg

6.00U ug/Kg

6.00U ug/Kg

6.00U ug/Kg

6.00U ug/Kg

6.00U ug/Kg

6.00U ug/Kg

6.00U ug/Kg

6.00U ug/Kg

6.00U ug/Kg

CXl

FLDOH: E83018 (Main Lab) FLDOH: E86562 (South Lab) FLDOH: E82405 (North Lab) NJDEP: FL015 Page6of9

000510
P.O. Box 150597, Altamonte Springs FL 32715-0597 Phone 407 - 339 - 5984 Fax 407 - 260 - 6110 www.f1owerslabs.com

8253 South U.S. Highway 1, Port St. Lucie FL 34952-2860 Phone 772 - 343 - 8006 Fax 772 - 343 - 8089

P.O. Box 1200, Madison FL 32341 Phone 850-973-6878 Fax 850-973-6878

Pinnacle Laboratories

2709 D Pan American Freeway NE

Albuquerque,NM 87107

Quality Control Batch: 10091194

Blank

Naphthalene

Phenanthrene

Pyrene

1-methyl-Naphthalene

2-methyl-Naphthalene

Surr:Nitrobenzene-d5

Surr:Terphenyl-d14

Surr:2-Fluorobiphenyl

Analyst: CLS

Result Units

6.00U ug/Kg

6.00U ug/Kg

6.00U ug/Kg

6.00U ug/Kg

6.00U ug/Kg

878 ug/Kg

1840 ug/Kg

1110 ug/Kg

PO#: 709293

Client Project #: NMGW

Date Sampled: Sep 28, 2007

Oct 12, 2007; Invoice: 49487

Laboratory Control Sample

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene

Benzo(b)f1uoranthene

Benzo(g,h,i)perylene

Benzo(k)f1uoranthene

Chrysene

Dibenz(a,h)anthracene

Fluoranthene

Fluorene

Indeno(1,2,3-cd)pyrene

Naphthalene

Phenanthrene

Pyrene

1-methyl-Naphthalene

2-methyl-Naphthalene

Surr:Nitrobenzene-d5

Result

1520

1430

1640

1750

1680

1570

1730

2280

1920

1690

1800

1560

1760

1470

1590

2250

1170

1060

1250

Units

ug/Kg

ug/Kg

ug/Kg

ug/Kg

ug/Kg

ug/Kg

ug/Kg

ug/Kg

ug/Kg

ug/Kg

ug/Kg

ug/Kg

ug/Kg

ug/Kg

ug/Kg

ug/Kg

ug/Kg

ug/Kg

ug/Kg

Spike

1670

1670

1670

1670

1670

1670

1670

1670

1670

1670

1670

1670

1670

1670

1670

1670

1670

1670

1670

%REC

91.22

85.77

98.62

104.91

101.04

93.89

103.50

136.64

114.94

101.13

107.71

93.79

105.60

88.28

95.55

135.24

70.33

63.45

74.76

%RECLim

80.00-120.00

80.00-120.00

80.00-120.00

80.00-120.00

80.00-120.00

80.00-120.00

80.00-120.00

80.00-120.00

80.00-120.00

80.00-120.00

80.00-120.00

80.00-120.00

80.00-120.00

80.00-120.00

80.00-120.00

80.00-120.00

80.00-120.00

80.00-120.00

80.00-120.00

co

FLOOH: E83018 (Main Lab) FLOOH: E86562 (South Lab) FLOOH: E82405 (North Lab) NJOEP: FL015 Page 7 of9

000511
P.O. Box 150597. Altamonte Springs FL 32715-0597 Phone 407 - 339 - 5984 Fax 407 - 260 - 6110 www.f1owerslabs.com

8253 South U.S. Highway 1. Port St. Lucie FL 34952-2860 Phone 772 - 343 - 8006 Fax 772 - 343 - 8089

P.O. Box 1200. Madison FL 32341 Phone 850-973-6878 Fax 850-973-6878

Pinnacle Laboratories

2709 D Pan American Freeway NE

Albuquerque,NM 87107

PO#: 709293

Client Project #: NMGW

Date Sampled: Sap 28, 2007

Oct 12, 2007; Invoice: 49487

Quality.ControIBatch:10091194

Laboratory Control Sample

Surr:Terphenyl-d14

Surr:2-Fluorobiphenyl

. Analyst:CLs

Result Units

2070 ug/Kg

1280 ug/Kg

Spike

1670

1670

%REC

123.93

76.98

%RECLim

80.00-120.00

80.00-120.00

.....>.

o

FLOOH: E83018 (Main Lab) FLOOH: E86562 (South Lab) FLOOH: E82405 (North Lab) NJDEP: FL015 PageS of9

000512
P.O. Box 150597, Altamonte Springs FL 32715-0597 Phone 407-339-5984 Fax 407-260-6110 www.flowerslabs.com

8253 South U.S. Highway 1, Port St. Lucie FL 34952-2860 Phone 772-343-8006 Fax 772-343-8089

P.O. Box 1200, Madison FL 32341 Phone 850-973-6878 Fax 850-973-6878

Pinnacle Laboratories

2709 D Pan American Freeway NE

Albuquerque.NM 87107

Narrative Report

PO #: 709293

Client Project #: NMGW

Date Sampled: Sep 28, 2007

Oct 12, 2007; Invoice: 49487

Sample Handling

Sample handling and holding time criteria were met for all samples. Samples collected by submitter. No unusual events

occurred during analysis. Results are reported on a wet weight basis for aqueous matrices and on a dry weight basis for

sludge and soil matrices unless otherwise noted. Sample results reported as dissolved were field filtered.

Quality Control

Enclosed analyses met method or FCL criteria, unless otherwise denoted on the sample results. Applied data qualifiers are

defined below.

Additional Comments

Surrogate and LCS recoveries are within method recovery limits of 70-130%.

Attachments

Chain of Custody

Qualifier

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Q

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ZTNTC

A

P

T

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G

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Meaning

Compound was analyzed for but not detected.

One or more QC samples associated with this data value exceeded QC limits.

Surrogate recovery limits have been exceeded.

No known quality control criteria exist for the component.

Reported value failed to meet established quality control criteria for either precision or accuracy.

Sample matrix interfered with the ability to make an accurate determination on the spiked sample.

Sample held beyond the accepted holding time.

Off-scale high; reported concentration exceeds the highest standard.

Analyte was detected in both the sample and the associated method blank.

Too numerous to count. Numeric value represents filtration volume.

Absent

Present

Value reported is less than the statistical method detection limit. Reported for informational purposes only.

Value reported is greater than the statistical method detection limit, but less than the reported MOL.

The greatest of the dilutions performed did not yield sufficient oxygen depletion for valid data.

The least of the dilutions performed did not yield sufficient oxygen residual for valid data.

Result is greater than (over) the specified value.

Reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.

Results based upon colony plate count outside ideal range.

The laboratory analysis was from an improperly preserved sample. The data may not be accurate.

FLDOH: E83018 (Main Lab) FLDOH: E86562 (South Lab) FLDOH: E82405 (North Lab) NJDEP: FL015 Page 90f9

11

000513
( Pinnacle Laboratories, Inc. Interlab Chain of Custody Date: Page:__of__

Network Project Manager: Jacinta Tenorio ANALYSIS REQUEST

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PROJECT INFORMATION SAMPLE RECEIPT SAMPLES SENT TO: RELINQUISED BY: 1, RELINQUISED BY: 2.

PROJECT#: ~2-q3 Total Number of Containers PENSACOLA· STL·FL ~alure: • II ,.-::1 AAA 'f~:: R1v Signature: lime:

PROJ.NAME: NMBlAJ Chain of Custody Seals ESL·OR A 1A1~ \IV ....-:;./ v 'v "V

QC LEVEL:.CSrD? IV Received Intact? ATEL-AZ

~~-rMAJal'?8(A- Printed Name: Date:

ec"REQ'lICC .~ MS MSD BLANK Received Good CondJCold ATEL· MARION

TAT:~TANDA~ RUSHl! LAB NUMBER: ATEL • MELMORE Pinnacle Laboratolies, Inc. Company

FCL K RECEIVED BY: 1. RECEIVED BY: 2.

DUE DATE: 10112- COMMENTS: EHL Signature: lime: Signature: lime:

RUSH SURCHARGE: - GEL

CLIENT DISCOUNT: - WCAS Printed Name: Date: Printed Name: Date:

SPECIAL CERTIF1~N WOHL

REQUIRED: YESt1J"O· Company Company

......

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000514
DISTRIBUTION: White - PU, Canary' Originator

COMMENTS:

METHANOL PRESERVATION 0 METALS 0 TOTAL 0 DISSOLVED

CERTIFICATION REQUIRED 0 NM 0 SDWA 0 AZ 0 OTHER

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