# APPENDIX D

LABORATORY DATA

# 2714 Exchange Drive

Wilmington, NC 28405

Ph.: 910-794-1613

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# 12 August 2011

Sarah Sharman

Weston Solutions

1625 Pumphrey Avenue

Auburn, AL 36832

Ph.: 334-466-5600

Email: Sarah.Sharman@westonsolutions.com



# Subject: Certificate of Results

Dear Sarah;

Attached to this na rrative are the analytical results you requested on samples submitted

for the determination of polychlorinated dibenzo- p -dioxins and dibenzofurans. The insert

below summarizes the relevant information pert aining to your project. In particular, QC

annotations bring to your atte ntion specific analytical obser vations and assessments made

during the sample handling and data interpretati on phases. Results reported relate only to

the items tested.

Project Information Summary When applicable, see QC Annotations for details

Client Project No. 02774.015.001.0001 (Formosa)

AP Project # A3423

Analytical Protocol Method 23

No. Samples Submitted 4

No. Samples Analyzed 4

No. Laboratory Method Blanks 1

No. OPRs / Batch CS3 1

No. Outstanding Samples 0

Date Received 9-Aug-2011

Condition Received good

Temperature upon Receipt (C) 3

Extraction within Holding Time yes

Analysis within Holding Time yes

Data meet QA/QC Requirements yes

Exceptions none

Analytical Difficulties none

# 2714 Exchange Drive

Wilmington, NC 28405

Ph.: 910-794-1613

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# Analytical Perspectives remains committed to serving you in the most effective manner.

Should you have any questions or need addi tional information and technical support,

please do not hesitate to cont act us. Thank you for choosing Analytical Perspectives as

part of your analytical support team.

Sincerely,

Kimberly Mace, Ph.D.

Project Scientist

QC Annotations:

See Appendix A & B for data qualifier, data attribute, and lab identifier information.

# 2714 Exchange Drive

Wilmington, NC 28405

Ph.: 910-794-1613

3 / 3 

# APPENDIX A: DATA QUALIFIERS / DATA ATTRIBUTES

* The reported concentration exceeds the calibration range (upper point of the calibration curve). 1



# > Indicates high recoveries. Shown with the numeric value at the top of the range. 1



# B The analyte is found in the method blank, at a level that is <=10x the sample concentration.

C Two or more congeners co-elute. In EDDs C denotes the lowest IUPAC congener in a coelution group and additional co-eluters for the group are shown with the number of the lowest

IUPAC co-eluter.

E The reported concentration exceeds the calibration range (upper point of the calibration curve).

EMPC Represents an Estimated Maximum Possible Con centration. EMPC’s arise in cases where the

signal/noise ratio is not sufficient for peak identification (the determined ion-abundance ratio is

outside the allowed theoretical range), where ther e is a co-eluting interference, or where a single

ion is utilized for quantitation due to PFK interference.

ETH Indicates the presence of a diphenyl ether that a ppears to interfere with the quantitation of a

furan. The reported concentration is the maximum.

H/h If the standard recovery is below the method or SOP specified value “H” is assigned. If the

obtained value is less than half the specified value “h” is assigned. 1



# J Indicates that an analyte has a concentration below the reporting limit (lowest point of the

calibration curve).

ND Indicates a non-detect.

NR Indicates a value that is not reportable.

PR Due to interference, the associa ted congener is poorly resolved.

QI Indicates the presence of a quantitative interference.

Ra The new ratio – [Ra] -- for 2,3,7,8-TCDD following the 37 

# Cl 4 

# -2,3,7,8-TCDD correction is

shown between squared brackets in the DL column. 1



# SI Denotes “Single Ion Mode” and is utilized fo r PCBs where the secondary ion trace has a

significantly elevated noise level due to background PFK. Responses for such peaks are

calculated using an EMPC approach based so lely on the primary ion area(s) and may be

considered estimates. 1



# U The analyte was not detected. The estimated detection limit (EDL) may be reported for this

analyte.

V The labeled standard recovery was found to be outside of the method control limits.

X Indicates results reported from reinjection, refractionation, or repeat analyses.

APPENDIX B: LAB ID IDENTIFIERS

AR Indicates use of the archived portion of the sample extract.

CU Indicates a sample that required additional clean-up prior to MS injection/processing.

D Indicates a dilution of the sample extract. The number that follows the “D” indicates the

dilution factor.

DE Indicates a dilution performed with the addition of ES (extraction standard) solution.

DUP Designation for a duplicate sample.

MS Designation for a matrix spike.

MSD Designation for a matrix spike duplicate.

RJ Indicates a reinjection of the sample extract.

S Indicates a sample split. The number that fo llows the “S” indicates the split factor.

1 

# Denotes data qualifiers/attributes who se use will be phased out over timeA3423 - TEQProject ID: 02774.015.001.0001 (Formosa)Sample SummaryPart 1Method 23AnalyteMethod Blank FPC-C-R1 FPC-C-R2 FPC-C-R3 FPC-C-RFBpgpgpgpgpg2,3,7,8-TCDD(1.71)31.333.829.4(1.96)1,2,3,7,8-PeCDD(1.53)164186149(2.35)1,2,3,4,7,8-HxCDD(1.43)288350273(2.29)1,2,3,6,7,8-HxCDD(1.55)494602477(2.46)1,2,3,7,8,9-HxCDD[1.61]171219170(2.66)1,2,3,4,6,7,8-HpCDD(2.57)171022501780(3.83)OCDD(3.59)1610234019507.972,3,7,8-TCDF(1.5)203203176(1.98)1,2,3,7,8-PeCDF(1.41)133014401210(1.93)2,3,4,7,8-PeCDF(1.25)288297251(1.74)1,2,3,4,7,8-HxCDF(1.1)464051004330(1.56)1,2,3,6,7,8-HxCDF(1.11)136015501330(1.54)2,3,4,6,7,8-HxCDF(1.1)333348284(1.61)1,2,3,7,8,9-HxCDF(1.42)125206141(2.23)1,2,3,4,6,7,8-HpCDF(1.13)615073806410(1.75)1,2,3,4,7,8,9-HpCDF(1.92)195021001630(3.01)OCDF(6.06)99501310010200(7.42)ITEF TEQ (ND=0; EMPC=0)01200134011200.00797ITEF TEQ (ND=0; EMPC=EMPC)0.1611200134011200.00797ITEF TEQ (ND=DL/2; EMPC=0)2.161200134011202.92ITEF TEQ (ND=DL/2; EMPC=EMPC)2.241200134011202.92ITEF TEQ (ND=DL; EMPC=EMPC)4.321200134011205.83Checkcode344-106-PKD 049-212-JWT 148-791-GZG 447-485-HLB 005-808-RSSLab IDMB1_8918_DF_SDS A3423_8918_DF_001 A3423_8918_DF_002 A3423_8918_DF_003 A3423_8918_DF_004( ) = DL[ ] = EMPCA3423 - WHO-2005-TEQProject ID: 02774.015.001.0001 (Formosa)Sample SummaryPart 1Method 23AnalyteMethod Blank FPC-C-R1 FPC-C-R2 FPC-C-R3 FPC-C-RFBpgpgpgpgpg2,3,7,8-TCDD(1.71)31.333.829.4(1.96)1,2,3,7,8-PeCDD(1.53)164186149(2.35)1,2,3,4,7,8-HxCDD(1.43)288350273(2.29)1,2,3,6,7,8-HxCDD(1.55)494602477(2.46)1,2,3,7,8,9-HxCDD[1.61]171219170(2.66)1,2,3,4,6,7,8-HpCDD(2.57)171022501780(3.83)OCDD(3.59)1610234019507.972,3,7,8-TCDF(1.5)203203176(1.98)1,2,3,7,8-PeCDF(1.41)133014401210(1.93)2,3,4,7,8-PeCDF(1.25)288297251(1.74)1,2,3,4,7,8-HxCDF(1.1)464051004330(1.56)1,2,3,6,7,8-HxCDF(1.11)136015501330(1.54)2,3,4,6,7,8-HxCDF(1.1)333348284(1.61)1,2,3,7,8,9-HxCDF(1.42)125206141(2.23)1,2,3,4,6,7,8-HpCDF(1.13)615073806410(1.75)1,2,3,4,7,8,9-HpCDF(1.92)195021001630(3.01)OCDF(6.06)99501310010200(7.42)WHO-2005 TEQ (ND=0; EMPC=0)01190133011100.00239WHO-2005 TEQ (ND=0; EMPC=EMPC)0.1611190133011100.00239WHO-2005 TEQ (ND=DL/2; EMPC=0)2.41190133011103.3WHO-2005 TEQ (ND=DL/2; EMPC=EMPC)2.481190133011103.3WHO-2005 TEQ (ND=DL; EMPC=EMPC)4.81190133011106.6Checkcode344-106-PKD 049-212-JWT 148-791-GZG 447-485-HLB 005-808-RSSLab IDMB1_8918_DF_SDS A3423_8918_DF_001 A3423_8918_DF_002 A3423_8918_DF_003 A3423_8918_DF_004( ) = DL[ ] = EMPCA3423 - TotalsProject ID: 02774.015.001.0001 (Formosa)Sample SummaryPart 2Method 23AnalyteMethod Blank FPC-C-R1 FPC-C-R2 FPC-C-R3 FPC-C-RFBpgpgpgpgpgTotalsTCDDs04745554650PeCDDs0111011609520HxCDDs02170253021000HpCDDs02180284022800OCDD01610234019507.97TCDFs02050234019300PeCDFs04840536044500HxCDFs099601090093000HpCDFs01080012400102000OCDF0995013100102000Total PCDD/Fs (ND=0; EMPC=0)04510053500438007.97Total PCDD/Fs (ND=0; EMPC=EMPC)1.614520053500439007.97Total PCDD/Fs (2378-X ND=DL; EMPC=EMPC)3245200535004390048.3Total 2378s (ND=0; EMPC=0)03080037700308007.97Total 2378s (ND=0.5; EMPC=0)1630800377003080028.1Total 2378s (ND=1; EMPC=0)32.130800377003080048.3Total 2378s (ND=0; EMPC=1)1.613080037700308007.97Total 2378s (ND=0.5; EMPC=1)16.830800377003080028.1Total 2378s (ND=1; EMPC=1)3230800377003080048.3Checkcode344-106-PKD 049-212-JWT 148-791-GZG 447-485-HLB 005-808-RSSLab IDMB1_8918_DF_SDS A3423_8918_DF_001 A3423_8918_DF_002 A3423_8918_DF_003 A3423_8918_DF_004( ) = DL[ ] = EMPCA3423 - OthersProject ID: 02774.015.001.0001 (Formosa)Sample SummaryPart 3Method 23AnalyteMethod Blank FPC-C-R1 FPC-C-R2 FPC-C-R3 FPC-C-RFBpgpgpgpgpgOther PCDD/Fs (ND=0, EMPC=0)Other TCDD04435214350Other PeCDD09489708030Other HxCDD01220136011800Other HpCDD04685864980Other TCDF01850214017500Other PeCDF03230362029900Other HxCDF03500371032100Other HpCDF02670287022100Other PCDD/Fs (ND=0, EMPC=EMPC)Other TCDD04875284460Other PeCDD09489708360Other HxCDD01220136011800Other HpCDD04685864980Other TCDF01850214017500Other PeCDF03230362030100Other HxCDF03500371032100Other HpCDF02670287022100Checkcode344-106-PKD 049-212-JWT 148-791-GZG 447-485-HLB 005-808-RSSLab IDMB1_8918_DF_SDS A3423_8918_DF_001 A3423_8918_DF_002 A3423_8918_DF_003 A3423_8918_DF_004( ) = DL[ ] = EMPCA3423 - DLsProject ID: 02774.015.001.0001 (Formosa)Sample SummaryPart 5 (DLs)Method 23AnalyteMethod Blank FPC-C-R1 FPC-C-R2 FPC-C-R3 FPC-C-RFBpgpgpgpgpg2,3,7,8-TCDD1.712.142.091.911.961,2,3,7,8-PeCDD1.532.112.442.542.351,2,3,4,7,8-HxCDD1.432.11.812.222.291,2,3,6,7,8-HxCDD1.552.181.862.312.461,2,3,7,8,9-HxCDD1.672.382.012.62.661,2,3,4,6,7,8-HpCDD2.573.463.763.83OCDD3.595.714.846.75.622,3,7,8-TCDF1.52.331.632.571.981,2,3,7,8-PeCDF1.414.34.163.181.932,3,4,7,8-PeCDF1.253.933.882.921.741,2,3,4,7,8-HxCDF1.15.956.527.051.561,2,3,6,7,8-HxCDF1.116.286.446.991.542,3,4,6,7,8-HxCDF1.16.096.677.021.611,2,3,7,8,9-HxCDF1.428.078.669.592.231,2,3,4,6,7,8-HpCDF1.133.453.033.131.751,2,3,4,7,8,9-HpCDF1.925.685.25.623.01OCDF6.066.737.6910.27.42Total TCDD1.712.142.091.911.96Total PeCDD1.532.112.442.542.35Total HxCDD1.542.211.882.362.46Total HpCDD2.573.463.763.83Total TCDF1.52.331.632.571.98Total PeCDF1.334.114.023.051.83Total HxCDF1.176.5377.561.71Total HpCDF1.464.43.964.192.28Checkcode344-106-PKD 049-212-JWT 148-791-GZG 447-485-HLB 005-808-RSSLab IDMB1_8918_DF_SDS A3423_8918_DF_001 A3423_8918_DF_002 A3423_8918_DF_003 A3423_8918_DF_0044 .3 2 1 20 0 1 34 0 1 12 0 5 .8 302004006008001,0001,2001,400pg M et ho d B la nk F P C- C-R1 F P C- C-R2 F P C- C-R3

F P C- C-RF BITEF-TEQProject ID: 02774.015.001.0001 (Formosa)A3423ND=0; EMPC=0ND=0; EMPC=EMPCND=DL/2; EMPC=0ND=DL/2; EMPC=EMPCND=DL; EMPC=EMPC4 .8 1 19 0 1 33 0 1 11 0 6 .602004006008001,0001,2001,400pg M et ho d B la nk F P C- C-R1 F P C- C-R2 F P C- C-R3

F P C- C-RF BWHO-2005-TEQProject ID: 02774.015.001.0001 (Formosa)A3423ND=0; EMPC=0ND=0; EMPC=EMPCND=DL/2; EMPC=0ND=DL/2; EMPC=EMPCND=DL; EMPC=EMPC3 2 4 52 00 5 35 00 4 39 00 4 8. 3010,00020,00030,00040,00050,00060,000pg M et ho d B la nk F P C- C-R1 F P C- C-R2 F P C- C-R3

F P C- C-RF BTotalsProject ID: 02774.015.001.0001 (Formosa)A3423Total PCDD/Fs (ND=0; EMPC=0)Total PCDD/Fs (ND=0; EMPC=EMPC)Total PCDD/Fs (2378-X ND=DL; EMPC=EMPC)Method Specification Limits: Tetra-Hexa ES: 40-130%, Hepta-Octa ES: 25-130% (F = fail)

9 4 - 1 03 8 9 - 9 8 9 4 - 1 00 8 8 - 1 00 9 2 - 1 02

8 8 - 9 4

8 4 - 9 3 8 8 - 9 8 8 6 - 9 6 8 6 - 9 8 9 0 - 9 8 8 9 - 9 7 9 1 - 9 9

8 9 - 9 4 9 0 - 9 7

8 7 - 9 4

8 3 - 9 40102030405060708090100% Rec. 1 3 C-T C DD 1 3 C-Pe C DD 1 3 C-Hx C DD 1 3 C-Hx C DD 1 3 C-Hx C DD 1 3 C-HpC D D 1 3 C-O C DD 1 3 C-T C DF 1 3 C-Pe C DF 1 3 C-Pe C DF 1 3 C-Hx C DF 1 3 C-Hx C DF 1 3 C-Hx C DF 1 3 C-Hx C DF 1 3 C-HpC D F 1 3 C-HpC D F 1 3 C-O C DFMean Recoveries of Extraction Standards (N=5)Project ID: 02774.015.001.0001 (Formosa)A3423MeanStd. Dev.Method Specification Limits: Tetra-Octa SS: 70-130% (F = fail)

1 0 0-10 7 8 9 - 9 6 1 0 7-11 0 1 0 2-10 7 1 0 0-10 6020406080100120% Rec. 3 7 Cl - TC DD 1 3 C-Pe C DD 1 3 C-Pe C DF 1 3 C-Hx C DF 1 3 C-HpC D FMean Recoveries of Sampling Standards (N=5)Project ID: 02774.015.001.0001 (Formosa)A3423MeanStd. Dev.A3423 Page 11 of 13A3423 Page 12 of 13A3423 Page 13 of 13Sample ID: Method BlankMethod 23Client DataSample DataLaboratory DataSoftware date: 11 Aug 11Name:Weston Solutions Matrix:Air Lab Project ID: A3423 Date Received: 09-Aug-2011Project ID:02774.015.001.0001 (Formosa)Weight/Volume: 1 Lab Sample ID MB1_8918_DF_SDS Date Extracted: 09-Aug-2011Date Collected:03-Aug-2011QC Batch No: 8918 Date Analyzed: 10-Aug-2011Split:2 Dilution:-Time Analyzed: 18:55:47AnalyteConc. (pg)DL (pg) EMPC (pg) Qualifiers StandardES Recoveries Qualifiers2378-TCDDND1.71ES 2378-TCDD97.612378-PeCDDND1.53ES 12378-PeCDD92.4123478-HxCDDND1.43ES 123478-HxCDD94.7123678-HxCDDND1.55ES 123678-HxCDD87.9123789-HxCDDEMPC1.61JES 123789-HxCDD92.21234678-HpCDDND2.57ES 1234678-HpCDD88.9OCDDND3.59ES OCDD87.12378-TCDFND1.5ES 2378-TCDF93.312378-PeCDFND1.41ES 12378-PeCDF89.323478-PeCDFND1.25ES 23478-PeCDF92123478-HxCDFND1.1ES 123478-HxCDF90.4123678-HxCDFND1.11ES 123678-HxCDF88.7234678-HxCDFND1.1ES 234678-HxCDF90.9123789-HxCDFND1.42ES 123789-HxCDF89.11234678-HpCDFND1.13ES 1234678-HpCDF89.71234789-HpCDFND1.92ES 1234789-HpCDF86.9OCDFND6.06ES OCDF85.6TotalsStandardSS/AS RecoveriesSS 37Cl-2378-TCDD102Total TCDDND1.71NDSS 12347-PeCDD95.1Total PeCDDND1.53NDSS 12346-PeCDF107Total HxCDDND1.61SS 123469-HxCDF104Total HpCDDND2.57NDSS 1234689-HpCDF102AS 1368-TCDD95.7Total TCDFND1.5NDAS 1368-TCDF94.4Total PeCDFND1.33NDTotal HxCDFND1.17NDTotal HpCDFND1.46NDTotal PCDD/FsND1.61ITEF TEQsTEQ: ND=000.1612714 Exchange DriveTEQ: ND=DL/22.162.162.24Wilmington, NC 28405 , USATEQ: ND=DL4.334.334.32info@ultratrace.comTel: +1 910 794-1613 (Fax: -3919); Toll-Free 866 846-8290 www.ultratrace.comCheckcode: 344-106-PKDAP D/F 2010 Rev. OReport Created: 11-Aug-2011 10:16 Analyst: APSample ID: FPC-C-R1Method 23Client DataSample DataLaboratory DataSoftware date: 11 Aug 11Name:Weston Solutions Matrix:Air Lab Project ID: A3423 Date Received: 09-Aug-2011Project ID:02774.015.001.0001 (Formosa)Weight/Volume: 1 Lab Sample ID A3423_8918_DF_001 Date Extracted: 09-Aug-2011Date Collected:02-Aug-2011QC Batch No: 8918 Date Analyzed: 10-Aug-2011Split:2 Dilution:-Time Analyzed: 19:48:55AnalyteConc. (pg)DL (pg) EMPC (pg) Qualifiers StandardES Recoveries Qualifiers2378-TCDD31.3ES 2378-TCDD9412378-PeCDD164ES 12378-PeCDD89.1123478-HxCDD288ES 123478-HxCDD94.4123678-HxCDD494ES 123678-HxCDD92.2123789-HxCDD171ES 123789-HxCDD961234678-HpCDD1710ES 1234678-HpCDD88.1OCDD1610ES OCDD85.62378-TCDF203ES 2378-TCDF87.712378-PeCDF1330ES 12378-PeCDF89.223478-PeCDF288ES 23478-PeCDF88.3123478-HxCDF4640ES 123478-HxCDF93123678-HxCDF1360ES 123678-HxCDF92.2234678-HxCDF333ES 234678-HxCDF91.5123789-HxCDF125ES 123789-HxCDF89.61234678-HpCDF6150ES 1234678-HpCDF89.61234789-HpCDF1950ES 1234789-HpCDF87.8OCDF9950ES OCDF88.8TotalsStandardSS/AS RecoveriesSS 37Cl-2378-TCDD103Total TCDD474518SS 12347-PeCDD95.4Total PeCDD11101110SS 12346-PeCDF107Total HxCDD21702170SS 123469-HxCDF102Total HpCDD21802180SS 1234689-HpCDF103AS 1368-TCDD90.4Total TCDF20502050AS 1368-TCDF89.5Total PeCDF48404840Total HxCDF99609960Total HpCDF1080010800Total PCDD/Fs 45100 45200ITEF TEQsTEQ: ND=0120012002714 Exchange DriveTEQ: ND=DL/212004.521200Wilmington, NC 28405 , USATEQ: ND=DL12009.051200info@ultratrace.comTel: +1 910 794-1613 (Fax: -3919); Toll-Free 866 846-8290 www.ultratrace.comCheckcode: 049-212-JWTAP D/F 2010 Rev. OReport Created: 11-Aug-2011 10:17 Analyst: APSample ID: FPC-C-R2Method 23Client DataSample DataLaboratory DataSoftware date: 11 Aug 11Name:Weston Solutions Matrix:Air Lab Project ID: A3423 Date Received: 09-Aug-2011Project ID:02774.015.001.0001 (Formosa)Weight/Volume: 1 Lab Sample ID A3423_8918_DF_002 Date Extracted: 09-Aug-2011Date Collected:02-Aug-2011QC Batch No: 8918 Date Analyzed: 10-Aug-2011Split:2 Dilution:-Time Analyzed: 20:42:03AnalyteConc. (pg)DL (pg) EMPC (pg) Qualifiers StandardES Recoveries Qualifiers2378-TCDD33.8ES 2378-TCDD98.912378-PeCDD186ES 12378-PeCDD88.7123478-HxCDD350ES 123478-HxCDD94.9123678-HxCDD602ES 123678-HxCDD91.6123789-HxCDD219ES 123789-HxCDD95.71234678-HpCDD2250ES 1234678-HpCDD91.1OCDD2340ES OCDD88.42378-TCDF203ES 2378-TCDF92.912378-PeCDF1440ES 12378-PeCDF86.523478-PeCDF297ES 23478-PeCDF86123478-HxCDF5100ES 123478-HxCDF92.7123678-HxCDF1550ES 123678-HxCDF91.4234678-HxCDF348ES 234678-HxCDF91.8123789-HxCDF206ES 123789-HxCDF89.91234678-HpCDF7380ES 1234678-HpCDF92.71234789-HpCDF2100ES 1234789-HpCDF91.4OCDF13100ES OCDF89.5TotalsStandardSS/AS RecoveriesSS 37Cl-2378-TCDD104Total TCDD555562SS 12347-PeCDD88.9Total PeCDD11601160SS 12346-PeCDF107Total HxCDD25302530SS 123469-HxCDF102Total HpCDD28402840SS 1234689-HpCDF103AS 1368-TCDD94.6Total TCDF23402340AS 1368-TCDF92.2Total PeCDF53605360Total HxCDF1090010900Total HpCDF1240012400Total PCDD/Fs 53500 53500ITEF TEQsTEQ: ND=0134013402714 Exchange DriveTEQ: ND=DL/213404.581340Wilmington, NC 28405 , USATEQ: ND=DL13409.151340info@ultratrace.comTel: +1 910 794-1613 (Fax: -3919); Toll-Free 866 846-8290 www.ultratrace.comCheckcode: 148-791-GZGAP D/F 2010 Rev. OReport Created: 11-Aug-2011 10:18 Analyst: APSample ID: FPC-C-R3Method 23Client DataSample DataLaboratory DataSoftware date: 11 Aug 11Name:Weston Solutions Matrix:Air Lab Project ID: A3423 Date Received: 09-Aug-2011Project ID:02774.015.001.0001 (Formosa)Weight/Volume: 1 Lab Sample ID A3423_8918_DF_003 Date Extracted: 09-Aug-2011Date Collected:03-Aug-2011QC Batch No: 8918 Date Analyzed: 10-Aug-2011Split:2 Dilution:-Time Analyzed: 21:35:10AnalyteConc. (pg)DL (pg) EMPC (pg) Qualifiers StandardES Recoveries Qualifiers2378-TCDD29.4ES 2378-TCDD10312378-PeCDD149ES 12378-PeCDD98.2123478-HxCDD273ES 123478-HxCDD100123678-HxCDD477ES 123678-HxCDD99.8123789-HxCDD170ES 123789-HxCDD1021234678-HpCDD1780ES 1234678-HpCDD93.6OCDD1950ES OCDD92.72378-TCDF176ES 2378-TCDF97.512378-PeCDF1210ES 12378-PeCDF95.923478-PeCDF251ES 23478-PeCDF98.1123478-HxCDF4330ES 123478-HxCDF97.7123678-HxCDF1330ES 123678-HxCDF97.1234678-HxCDF284ES 234678-HxCDF99.4123789-HxCDF141ES 123789-HxCDF93.51234678-HpCDF6410ES 1234678-HpCDF97.21234789-HpCDF1630ES 1234789-HpCDF94OCDF10200ES OCDF93.5TotalsStandardSS/AS RecoveriesSS 37Cl-2378-TCDD100Total TCDD465475SS 12347-PeCDD95.9Total PeCDD952985SS 12346-PeCDF108Total HxCDD21002100SS 123469-HxCDF106Total HpCDD22802280SS 1234689-HpCDF99.5AS 1368-TCDD99.7Total TCDF19301930AS 1368-TCDF98.7Total PeCDF44504470Total HxCDF93009300Total HpCDF1020010200Total PCDD/Fs 43800 43900ITEF TEQsTEQ: ND=0112011202714 Exchange DriveTEQ: ND=DL/211204.51120Wilmington, NC 28405 , USATEQ: ND=DL11208.991120info@ultratrace.comTel: +1 910 794-1613 (Fax: -3919); Toll-Free 866 846-8290 www.ultratrace.comCheckcode: 447-485-HLBAP D/F 2010 Rev. OReport Created: 11-Aug-2011 10:18 Analyst: APSample ID: FPC-C-RFBMethod 23Client DataSample DataLaboratory DataSoftware date: 11 Aug 11Name:Weston Solutions Matrix:Air Lab Project ID: A3423 Date Received: 09-Aug-2011Project ID:02774.015.001.0001 (Formosa)Weight/Volume: 1 Lab Sample ID A3423_8918_DF_004 Date Extracted: 09-Aug-2011Date Collected:03-Aug-2011QC Batch No: 8918 Date Analyzed: 10-Aug-2011Split:2 Dilution:-Time Analyzed: 22:28:17AnalyteConc. (pg)DL (pg) EMPC (pg) Qualifiers StandardES Recoveries Qualifiers2378-TCDDND1.96ES 2378-TCDD10012378-PeCDDND2.35ES 12378-PeCDD95123478-HxCDDND2.29ES 123478-HxCDD97.6123678-HxCDDND2.46ES 123678-HxCDD94.4123789-HxCDDND2.66ES 123789-HxCDD96.41234678-HpCDDND3.83ES 1234678-HpCDD88.3OCDD7.97JES OCDD83.92378-TCDFND1.98ES 2378-TCDF97.812378-PeCDFND1.93ES 12378-PeCDF93.523478-PeCDFND1.74ES 23478-PeCDF93.2123478-HxCDFND1.56ES 123478-HxCDF94123678-HxCDFND1.54ES 123678-HxCDF93.8234678-HxCDFND1.61ES 234678-HxCDF94.8123789-HxCDFND2.23ES 123789-HxCDF89.61234678-HpCDFND1.75ES 1234678-HpCDF911234789-HpCDFND3.01ES 1234789-HpCDF87.9OCDFND7.42ES OCDF83.4TotalsStandardSS/AS RecoveriesSS 37Cl-2378-TCDD107Total TCDDND1.96NDSS 12347-PeCDD95.1Total PeCDDND2.35NDSS 12346-PeCDF110Total HxCDDND2.46NDSS 123469-HxCDF107Total HpCDDND3.83NDSS 1234689-HpCDF106AS 1368-TCDD100Total TCDFND1.98NDAS 1368-TCDF99.9Total PeCDFND1.83NDTotal HxCDFND1.71NDTotal HpCDFND2.28NDTotal PCDD/Fs7.977.97ITEF TEQsTEQ: ND=00.007970.007972714 Exchange DriveTEQ: ND=DL/22.922.912.92Wilmington, NC 28405 , USATEQ: ND=DL5.835.825.83info@ultratrace.comTel: +1 910 794-1613 (Fax: -3919); Toll-Free 866 846-8290 www.ultratrace.comCheckcode: 005-808-RSSAP D/F 2010 Rev. OReport Created: 11-Aug-2011 10:19 Analyst: AP