# PI'N~LE~ Environmental Testing

PLLD. 709293



## October 17,2007

NMED-GWQB 1190 St. FrancisDrive SantaFe, NM 87502

ProjectNamelNumber: ATSF/ABQ



## Attention: DavidL. Mayerson

On09/28/07, 

## PinnacleLaboratories Inc., (ADHS LicenseNo. AZ0643), received arequestto analyzenon-aq 

## samples. Thesamples wereanalyzedwithEPAmethodologyorequivalent methods. Theresults oftheseanalyses andthequalitycontrol data, whichfollow eachsetof analyses, are enclosed.

All sampleswere analyzedbyFlowers Chemical**La~oratories,** 

## Inc. (FCL), Altamonte Springs, FL.

Ifyouhave anyquestions orcomments, pleasedonothesitateto contactus at(505) 344-3777.

H. Mitchell Rubenstein, Ph.D. GeneralManager

MR:jt

Enclosure

2709-D Pan American Fwy, NE Albuquerque, NM 87107 505.344.3777 505.344.4413 FAX 

### 877.PIN.1998 TOLL FREE 

### www.pinnaclelabs.org www.pinnaclelabsonline.com



## 1" 

# PIN**~LE~** Environmental Testing

CLIENT :NMED-GWQB DATE

## RECENED :09/28/07
PROJECT# :(NONE)
PROJECTNAME :ATSF/ABQ REPORTDATE : 10/17/07

PLID: 709293
PINNACLE CLIENT DATE ID# DESCRIPTION MATRIX COLLECTED
01 709293-01 CS-G10-3-1 NON-AQ 09/28/07
02 709293-02 D1 NON-AQ 09/28/07
03 709293-03 CS-G04-1 NON-AQ 09/28/07
04 709293-04 CS-G06-1 NON-AQ 09/28/07

---TOTALS---

MATRIX NON-AQ #SAMPLES 

## 4

2709-D Pan American 

### Fwy, NE Albuquerque, NM 87107 505.344.3777 505.344.4413 FAX 

### 877.PIN.1998 TOLL FREE 

### www.pinnaclelabs.org www.pinnaclelabsonline.com



## 2P.O. Box 150597, Altamonte Springs FL 32715-0597 Phone 407-339-5984 Fax 407-260-6110 www.flowerslabs.com 8253 South U.S. Highway 1, Port St. Lucie FL 34952-2860 Phone 772-343-8006 Fax 772-343-8089 P.O. Box 1200, Madison FL 32341 Phone 850-973-6878 Fax850-973-6878



### Pinnacle Laboratories 2709 D Pan American Freeway NE Albuquerque.NM 87107

Date Received: Oct 1, 2007 PO#: 709293 Client Project#: NMGW Date Sampled: Sep 28, 2007 Oct 12, 2007; Invoice: 49487


### ReportSummary

FCL Project Manager: June S. Flowers


### Laboratory

### # Sample Description 49487S01 CS-G10-3-3/709293-01

49487S02 D11709293-02

49487S03 CS-G04-11709293-03

49487S04 CS-G06-11709293-04 

### Analysis EPA6020 EPA8270 SM2540B XBNE EPA6020 EPA8270 SM2540B XBNE EPA6020 EPA8270 SM2540B XBNE EPA6020 EPA8270 SM2540B XBNE 

### Chemist EVB CLS RMV CDG EVB CLS RMV CDG EVB CLS RMV CDG EVB CLS RMV CDG 

### Location Main Lab Main Lab Main Lab Main Lab Main Lab Main Lab Main Lab Main Lab Main Lab Main Lab Main Lab Main Lab Main Lab Main Lab Main Lab Main Lab 

### SampleMatrix Soil

Soil

Soil

Soil



### Certificate ofResults Sample integritywas certified priorto analysis. Test results meetall requirements ofthe NELAC Standards exceptas noted in the Quality Control Report. Uncertainties forthese data are available on request. This report may not be reproduced in part; results relate onlyto itemstested.

FLOOH: E83018 (Main Lab) FLOOH: E86562 (South Lab) FLOOH: E82405 (North Lab) NJOEP: FL015 Page 1 of9



## 3P.O. Box 150597, Altamonte Springs FL 32715-0597 Phone 407

- 339

- 5984 Fax 407

- 260

- 6110 www.f1owerslabs.com 8253 South U.S. Highway 1. Port St. Lucie FL 34952-2860 Phone 772

- 343

- 8006 Fax 772

- 343

- 8089 P.O. Box 1200. Madison FL 32341 Phone 850-973-6878 Fax 850-973-6878

Pinnacle Laboratories PO#: 709293 2709 0 Pan American Freeway NE Client Project#: NMGW Albuquerque,NM 87107 Date Sampled: Sep28, 2007 Oct 12,2007; Invoice: 49487

Analysis Report

lab

### #: 49487S01 Sampled: 09/28/0710:27AM Desc: CS-G10-3-31709293-01 Parameter Result Units DF MDl PQl QC Batch Method CAS

### # Analyzed % Moisture 5.39 %Wt 1.00 0.000250 0.000500 10090704 SM2540B 10/02/07 Zinc 30.7 mg/Kg 1.00 1.00 2.00 10091027 EPA6020 7440-66-6 10/04/07 1-methyl-Naphthalene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 090-12-0 10/10/07 2-methyl-Naphthalene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 91-57-6 10/10/07 Acenaphthene 6.00 U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 83-32-9 10/10/07 Acenaphthylene 14.5 ug/Kg 1.00 6.00 12.0 10091194 EPA8270 208-96-8 10/10/07 Anthracene 79.8 ug/Kg 1.00 6.00 12.0 10091194 EPA8270 120-12-7 10110/07 Benzo(a)anthracene 53.4 ug/Kg 1.00 6.00 12.0 10091194 EPA8270 56-55-3 10/10/07 Benzo(a)pyrene 32.0 ug/Kg 1.00 6.00 12.0 10091194 EPA8270 50-32-8 10/10/07 Benzo(b)f1uoranthene 104 ug/Kg 1.00 6.00 12.0 10091194 EPA8270 205-99-2 10/10/07 Benzo(g,h,i)perylene 57.9 ug/Kg 1.00 6.00 12.0 10091194 EPA8270 191-24-2 10/10/07 Benzo(k)f1uoranthene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 207-08-9 10/10/07 Chrysene 90.4 ug/Kg 1.00 6.00 12.0 10091194 EPA8270 218-01-9 10/10/07 Oibenz(a,h)anthracene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 53-70-3 10/10/07 Fluoranthene 230 ug/Kg 1.00 6.00 12.0 10091194 EPA8270 206-44-0 10/10/07 Fluorene 6.00U ug/Kg 1.00 6.00 12.0 10091194 EPA8270 86-73-7 10/10/07 Indeno(1,2,3-cd)pyrene 28.9 uglKg 1.00 6.00 12.0 10091194 EPA8270 193-39-5 10/10/07 Naphthalene 14.8 ug/Kg 1.00 6.00 12.0 10091194 EPA8270 91-20-3 10/10/07 Phenanthrene 138 ugfKg 1.00 6.00 12.0 10091194 EPA8270 85-01-8 10/10/07 Pyrene 213 ugfKg 1.00 6.00 12.0 10091194 EPA8270 129-00-0 10/10/07 Surr:2-Fluorobiphenyl (79-120%) 75.62% 1.00 0.0100 0.0200 10091194 EPA8270 321-60-8 10/10/07 Surr:Nitrobenzene-d5 (79-120%) 105.08% 1.00 0.0100 0.0200 10091194 EPA8270 10/10/07 Surr:Terphenyl-d14 (79-120%) 130.42% 1.00 0.0100 0.0200 10091194 EPA8270 10/10f07 Base_NeutraLExtraction 30.0 

### 9 1.00 10091246 XBNE 10/08/07

Lab

### #: 49487S02 Sampled: 09f28/07 11 :00AM Desc: 011709293-02 Parameter Result Units DF MDl PQl QC Batch Method CAS

### # Analyzed

FLOOH: E83018 (Main Lab) FLDOH: E86562 (South Lab) FLOOH: E82405 (North Lab) NJDEP: FL015 Page 2 of9P.O. Box 150597, Altamonte Springs FL 32715-0597 Phone 407

- 339

- 5984 Fax 407

- 260

- 6110 www.f1owerslabs.com 8253 South U.S. Highway 1. Port St. Lucie FL 34952-2860 Phone 772

- 343

- 8006 Fax 772

- 343

- 8089 P.O. Box 1200. Madison FL 32341 Phone 850-973-6878 Fax 850-973-6876

Pinnacle Laboratories PO#: 709293 2709 D Pan American Freeway NE Client Project#: NMGW Albuquerque,NM 87107 Date Sampled: Sep 28, 2007 Oct 12, 2007; Invoice: 49487

Lab#: 49487S02 Sampled: 09/28/0711 :00AM Oesc: D11709293-02 Parameter Result Units OF MOL PQL QC Batch Method CAS

### # Analyzed % Moisture 5.54 %Wt 1.00 0.000250 0.000500 10090704 SM2540B 10/02/07 Zinc 19.7 

### mg/Kg 1.00 1.00 2.00 10091027 EPA6020 7440-66-6 10/04/07 1-methyl-Naphthalene 6.00 U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 090-12-0 10/10/07 2-methyl-Naphthalene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 91-57-6 10/10/07 Acenaphthene 6.00 U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 83-32-9 10110/07 Acenaphthylene 6.00 U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 208-96-8 10110/07 Anthracene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 120-12-7 10110/07 Benzo(a)anthracene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 56-55-3 10/10/07 Benzo(a)pyrene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 50-32-8 10/10/07 Benzo(b)f1uoranthene 14.8 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 205-99-2 10/10/07 Benzo(g,h,i)perylene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 191-24-2 10110/07 Benzo(k)fluoranthene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 207-08-9 10110/07 Chrysene 8.50 I 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 218-01-9 10/10/07 Dibenz(a,h)anthracene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 53-70-3 10/10/07 Fluoranthene 10.71 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 206-44-0 10/10/07 Fluorene 6.00 U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 86-73-7 10/10/07 Indeno(1,2,3-cd)pyrene 6.0OU 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 193-39-5 10/10/07 Naphthalene 6.00 U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 91-20-3 10/10/07 Phenanthrene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 85-01-8 10/10/07 pyrene 8.30 I 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 129-00-0 10110/07 Surr:2-Fluorobiphenyl (79-120%) 63.94% 1.00 0.0100 0.0200 10091194 EPA8270 321-60-8 10/10/07 Surr:Nitrobenzene-d5 (79-120%) 61.94% 1.00 0.0100 0.0200 10091194 EPA8270 10110/07 Surr:Terphenyl-d14 (79-120%) 100.36% 1.00 0.0100 0.0200 10091194 EPA8270 10/10/07 Base_NeutraLExtraction 30.0 

### 9 1.00 10091246 XBNE 10/08/07

Lab

### #: 49487S03 Sampled: 09/28/07 11 :25AM Oesc: CS-G04-11709293-03 Parameter Result Units OF MOL PQL QC Batch Method CAS

### # Analyzed % Moisture 6.33 %Wt 1.00 0.000250 0.000500 10090704 SM2540B 10/02/07 Zinc 15.1 

### mg/Kg 1.00 1.00 2.00 10091027 EPA6020 7440-66-6 10/04/07

FLOOH: E83018 (Main Lab) FLOOH: E86562 (South Lab) FLOOH: E82405 (North Lab) NJOEP: FL015 Page30f9P.O. Box 150597, Altamonte Springs FL 32715-0597 Phone 407

- 339

- 5984 Fax 407

- 260

- 6110 www.f1owerslabs.com 8253 South U.S. Highway 1, Port St. Lucie FL 34952-2860 Phone 772

- 343

- 8006 Fax 772

- 343

- 8089 P.O. Box 1200, Madison FL 32341 Phone 850-973-6878 Fax 850-973-6878

Pinnacle Laboratories PO#: 709293 2709 D Pan American Freeway NE Client Project#: NMGW Albuquerque,NM 87107 Date Sampled: Sep28, 2007 Oct 12, 2007; Invoice: 49487

lab#:49487S03 Sampled: 09/28/0711 :25AM Cese:**CS~G04-11709293-03** Parameter Result Units CF MCl PQl QC Batch Method CAS# Analyzed 1-methyl-Naphthalene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 090-12-0 10/10/07 2-methyl-Naphthalene 6.00U uglKg 1.00 6.00 12.0 10091194 EPA8270 91-57-6 10/10/07 Acenaphthene 6.00 U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 83-32-9 10/10/07 Acenaphthylene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 208-96-8 10/10/07 Anthracene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 120-12-7 10/10/07 Benzo(a)anthracene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 56-55-3 10/10/07 Benzo(a)pyrene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 50-32-8 10/10/07 Benzo(b)f1uoranthene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270**205-9~2** 10/10/07 Benzo(g,h,i)perylene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 191-24-2 10/10/07 Benzo(k)f1uoranthene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 207-08-9 10/10/07 Chrysene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 218-01-9 10/10/07 Dibenz(a,h)anthracene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 53-70-3 10/10/07 Fluoranthene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 206-44-0 10/10/07 Fluorene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 86-73-7 10/10/07 Indeno(1,2,3-cd)pyrene 6.00 U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 193-39-5 10110/07 Naphthalene 6.00 U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 91-20-3 10/10/07 Phenanthrene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 85-01-6 10/10/07 Pyrene 6.00U 

### ug/Kg 1.00 6.00 12.0 10091194 EPA8270 129-00-0 10/10/07 Surr:2-Fluorobiphenyl (79-120%) 81.30% 1.00 0.0100 0.0200 10091194 EPA8270 321-60-8 10/10/07 Surr:Nitrobenzene-d5 (79-120%) 87.83% 1.00 0.0100 0.0200 10091194 EPA8270 10/10/07 Surr:Terphenyl-d14 (79-120%) 112.53% 1.00 0.0100 0.0200 10091194 EPA8270 10/10/07 Base_NeutraLExtraction 30.0 

### 9 1.00 10091246 XBNE 10/08/07

lab#: 49487S04 Sampled: 09/28/0701:47PM Cese: CS-G06-11709293-04 Parameter Result Units CF MCl PQl QC Batch Method CAS # Analyzed % Moisture 21.2 %Wt 1.00 0.000250 0.000500 10090704 SM2540B 10/02/07 Zinc 18.3 

### mg/Kg 1.00 1.00 2.00 10091027 EPA6020 7440-66-6 10/04/07 1-methyl-Naphthalene 48.21 

### ug/Kg 5.00 30.0 60.0 10091194 EPA8270 090-12-0 10/10/07 2-methyl-Naphthalene 30.0U 

### ug/Kg 5.00 30.0 60.0 10091194 EPA8270 91-57-6 10/10/07

FLOOH: E83018 (Main Lab) FLOOH: E86562 (South Lab) FLOOH: E82405(North Lab) NJOEP: FL015 Page4of9P.O. Box 150597, Altamonte Springs FL 32715-0597 Phone 407

- 339

- 5984 Fax 407

- 260

- 6110 www.f1owerslabs.com 8253 South U.S. Highway 1. Port St. Lucie FL 34952-2860 Phone 772

- 343

- 8006 Fax 772

- 343

- 8089 P.O. Box 1200, Madison FL 32341 Phone 850-973-6878 Fax 850-973-6878

,**,.,-.'~'** ,.'**_~** ....." I .11 1 ""-! Pinnacle Laboratories PO#: 709293 2709 D Pan American Freeway NE Client Project

### #: NMGW Albuquerque,NM 87107 Date Sampled: Sep28, 2007 Oct 12, 2007; Invoice: 49487

Lab#: 49487S04 Sampled: 09/28/0701:47 PM Oesc:**CS~G06-11709293-o4** Parameter Result Units OF MOL PQL QC Batch Method CAS

### # Analyzed Acenaphthene 1350 ug/Kg 5.00 30.0 60.0 10091194 EPA8270 83-32-9 10110/07 Acenaphthylene 174 

### ug/Kg 5.00 30.0 60.0 10091194 EPA8270 208-96-8 10/10/07 Anthracene 30.0 U 

### ug/Kg 5.00 30.0 60.0 10091194 EPA8270 120-12-7 10/10/07 Benzo(a)anthracene 1150 

### ug/Kg 5.00 30.0 60.0 10091194 EPA8270 56-55-3 10/10/07 Benzo(a)pyrene 459 

### ug/Kg 5.00 30.0 60.0 10091194 EPA8270 50-32-8 10/10/07 Benzo(b)f1uoranthene 1120 

### ug/Kg 5.00 30.0 60.0 10091194 EPA8270 205-99-2 10/10/07 Benzo(g,h,i)perylene 123 ug/Kg 5.00 30.0 60.0 10091194 EPA8270 191-24-2 10/10/07 Benzo(k)f1uoranthene 30.0U 

### ug/Kg 5.00 30.0 60.0 10091194 EPA8270 207-08-9 10/10/07 Chrysene 998 

### ug/Kg 5.00 30.0 60.0 10091194 EPA8270 218-01-9 10/10/07 Dibenz(a,h)anthracene 30.0U 

### ug/Kg 5.00 30.0 60.0 10091194 EPA8270 53-70-3 10/10/07 Fluoranthene 7990 

### ug/Kg 5.00 30.0 60.0 10091194 EPA8270 206-44-0 10/10/07 Fluorene 1630 

### ug/Kg 5.00 30.0 60.0 10091194 EPA8270 86-73-7 10/10/07 Indeno(1,2,3-cd)pyrene 144 ug/Kg 5.00 30.0 60.0 10091194 EPA8270 193-39-5 10/10/07 Naphthalene 30.0U 

### ug/Kg 5.00 30.0 60.0 10091194 EPA8270 91-20-3 10/10/07 Phenanthrene 1260 

### ug/Kg 5.00 30.0 60.0 10091194 EPA8270 85-01-8 10/10/07 Pyrene 6450 

### ug/Kg 5.00 30.0 60.0 10091194 EPA8270 129·00-0 10/10/07 Surr:2-Fluorobiphenyl (79-120%) 70.34% 5.00 0.0500 0.100 10091194 EPA8270 321-60-8 10/10/07 Surr:Nitrobenzene-d5 (79-120%) 79.11% 5.00 0.0500 0.100 10091194 EPA8270 10/10/07 Surr:Terphenyl-d14 (79-120%) 128.74% 5.00 0.0500 0.100 10091194 EPA8270 10/10/07 Base_NeutraLExtraction 30.0 

### 9 1.00 10091246 XBNE 10/08/07

FLOOH: E83018 (Main Lab) FLOOH: E86562 (South Lab) FLOOH: E82405 (North Lab) NJOEP: FL015 Page50f9P.O. Box 150597, Altamonte SprIngs FL 32715-0597 Phone 407

- 339

- 5984 Fax 407

- 260

- 6110 www.f1owerslabs.com 8253 South U.S. Highway 1, Port St. Lucie FL 34952-2860 Phone 772

- 343

- 8006 Fax 772

- 343

- 8089 P.O. Box 1200. Madison FL 32341 Phone 850-973·6878 Fax 850-973-6878



### Pinnacle Laboratories 2709 D Pan American Freeway NE Albuquerque,NM 87107

QualityConttolBatch: 10091027 Blank Zinc Analyst: EVB Result Units 1.00U mg/Kg PO#: 709293 Client Project

### #: NMGW Date Sampled: Sep28, 2007 Oct 12, 2007; Invoice: 49487

Quality Report

Laboratory Control Sample Zinc

Matrix Spike Zinc

MatrixSpike Duplicate Zinc Result 0.267

Result 0.284

Result 0.281 Units mg/Kg



### Units mg/Kg



### Units mg/Kg 

### Spike 0.250
Spike 0.250
Spike 0.250 %REC %RECLim 106.64 70.72-128.29

%REC %RECLim Sample 83.43 35.26-158.48 0.0751

%REC %RECLim Sample RPD 82.37 35.26-158.48 0.0751 0.94 RPDLim 36.34
QualityControl Batch: 10091194 Blank Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)f1uoranthene Benzo(g,h,i)perylene Benzo(k)f1uoranthene Chrysene Dibenz(a,h)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene Analyst: CLS Result Units 6.00U ug/Kg 6.00U ug/Kg 6.00U ug/Kg 6.00U ug/Kg 6.00U ug/Kg 6.00U ug/Kg 6.00U ug/Kg 6.00U ug/Kg 6.00U ug/Kg 6.00U ug/Kg 6.00U ug/Kg 6.00U ug/Kg 6.00U ug/Kg

CXl FLDOH: E83018 (Main Lab) FLDOH: E86562 (South Lab) FLDOH: E82405 (North Lab) NJDEP: FL015 Page6of9P.O. Box 150597, Altamonte Springs FL 32715-0597 Phone 407

- 339

- 5984 Fax 407

- 260

- 6110 www.f1owerslabs.com 8253 South U.S. Highway 1, Port St. Lucie FL 34952-2860 Phone 772

- 343

- 8006 Fax 772

- 343

- 8089 P.O. Box 1200, Madison FL 32341 Phone 850-973-6878 Fax 850-973-6878

Pinnacle Laboratories 2709 D Pan American Freeway NE Albuquerque,NM 87107



### QualityControl Batch: 10091194 

### Blank Naphthalene Phenanthrene Pyrene 1-methyl-Naphthalene 2-methyl-Naphthalene Surr:Nitrobenzene-d5 Surr:Terphenyl-d14 Surr:2-Fluorobiphenyl 

### Analyst: CLS 

### Result Units 6.00U 

### ug/Kg 6.00U ug/Kg 6.00U ug/Kg 6.00U 

### ug/Kg 6.00U ug/Kg 878 ug/Kg 

### 1840 ug/Kg 1110 ug/Kg PO#: 709293 Client Project#: NMGW Date Sampled: Sep 28, 2007 Oct 12, 2007; Invoice: 49487



### Laboratory Control Sample Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)f1uoranthene Benzo(g,h,i)perylene Benzo(k)f1uoranthene Chrysene Dibenz(a,h)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene Naphthalene Phenanthrene Pyrene 1-methyl-Naphthalene 2-methyl-Naphthalene Surr:Nitrobenzene-d5 

### Result 1520 1430 1640 1750 1680 1570 1730 2280 1920 1690 1800 1560 1760 1470 1590 2250 1170 1060 1250 

### Units ug/Kg 

### ug/Kg ug/Kg 

### ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg 

### ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg 

### ug/Kg Spike 1670 1670 1670 1670 1670 1670 1670 1670 1670 1670 1670 1670 1670 1670 1670 1670 1670 1670 1670 

### %REC 91.22 85.77 98.62 104.91 101.04 93.89 103.50 136.64 114.94 101.13 107.71 93.79 105.60 88.28 95.55 135.24 70.33 63.45 74.76 

### %RECLim 80.00-120.00 80.00-120.00 80.00-120.00 80.00-120.00 80.00-120.00 80.00-120.00 80.00-120.00 80.00-120.00 80.00-120.00 80.00-120.00 80.00-120.00 80.00-120.00 80.00-120.00 80.00-120.00 80.00-120.00 80.00-120.00 80.00-120.00 80.00-120.00 80.00-120.00



### co FLOOH: E83018 (Main Lab) FLOOH: E86562 (South Lab) FLOOH: E82405 (North Lab) NJOEP: FL015 Page7of9P.O. Box 150597. Altamonte Springs FL 32715-0597 Phone 407

- 339

- 5984 Fax 407

- 260

- 6110 www.f1owerslabs.com 8253 South U.S. Highway 1. Port St. Lucie FL 34952-2860 Phone 772

- 343

- 8006 Fax 772

- 343

- 8089 P.O. Box 1200. Madison FL 32341 Phone 850-973-6878 Fax 850-973-6878



### Pinnacle Laboratories 2709 D Pan American Freeway NE Albuquerque,NM 87107 PO#: 709293 Client Project

### #: NMGW Date Sampled: Sap 28, 2007 Oct 12, 2007; Invoice: 49487

Quality.ControIBatch:10091194 LaboratoryControl Sample Surr:Terphenyl-d14 Surr:2-Fluorobiphenyl . Analyst:CLs Result Units 2070 ug/Kg 1280 ug/Kg 

### Spike 1670 1670 %REC 123.93 76.98 %RECLim 80.00-120.00 80.00-120.00

.....>. 

## o FLOOH: E83018 (Main Lab) FLOOH: E86562 (South Lab) FLOOH: E82405 (North Lab) NJDEP: FL015 PageS of9P.O. Box 150597, Altamonte Springs FL 32715-0597 Phone 407-339-5984 Fax407-260-6110 www.flowerslabs.com 8253 South U.S. Highway 1, Port St. Lucie FL 34952-2860 Phone 772-343-8006 Fax 772-343-8089 P.O. Box 1200, Madison FL 32341 Phone 850-973-6878 Fax850-973-6878

Pinnacle Laboratories 2709 D Pan American Freeway NE Albuquerque.NM 87107

Narrative Report PO

### #: 709293 Client Project

### #: NMGW Date Sampled: Sep28, 2007 Oct 12, 2007; Invoice: 49487

Sample Handling Sample handling and holding time criteriawere metfor all samples. Samples collected bysubmitter. No unusual events occurred during analysis. Results are reported on awetweight basisfor aqueous matrices and on a dryweight basisfor sludge and soil matrices unless otherwise noted. Sample results reported as dissolved were field filtered.

Quality Control Enclosed analyses met method or FCLcriteria, unless otherwise denoted on the sample results. Applied data qualifiers are defined below.

Additional Comments Surrogate and LCS recoveries arewithin method recovery limits of70-130%.

Attachments Chain ofCustody

Qualifier 

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### Y Meaning Compound was analyzed forbut notdetected. One ormore QC samples associated with this data value exceeded QC limits. Surrogate recovery limits have been exceeded. No known qualitycontrol criteria existforthe component. Reported valuefailed to meetestablished qualitycontrol criteria for eitherprecision oraccuracy. Sample matrixinterfered with the abilityto make an accurate determination on the spiked sample. Sample held beyond the accepted holding time. Off-scale high; reported concentration exceedsthe higheststandard. Analyte was detected in boththe sample and the associated method blank. Too numerousto count. Numericvalue represents filtration volume. Absent Present Value reported is lessthan the statistical method detection limit. Reported forinformational purposes only. Value reported is greaterthan the statistical method detection limit, but less than the reported MOL. The greatestofthe dilutions performed did notyield sufficientoxygen depletion forvalid data. The leastofthe dilutions performed did notyield sufficientoxygen residual forvalid data. Result is greaterthan (over) the specified value. Reported value is between the laboratory method detection limitand the laboratorypractical quantitation limit. Results based upon colony plate count outside ideal range. The laboratoryanalysis was from an improperly preserved sample. The data may not be accurate.

FLDOH: E83018 (Main Lab) FLDOH: E86562 (South Lab) FLDOH: E82405 (North Lab) NJDEP: FL015 Page 90f9



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PROJECT INFORMATION SAMPLE RECEIPT SAMPLES SENTTO: RELINQUISED 

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