5420 Mainway Drive, Unit 5, Burlington ON, L7L 6A4

Including For Each Analytical Sequence:

- The scanned instrument runlogs

- Instrument output (SICP chromatograms) indicating the integrations used for quantification including:

- GC chromatographic resolution checks, where appropriate

- SICPs for the run

- SICP chromatograms indicating both the automated and manual peak integration, 

 where this has been edited

- Reference peak profiles indicating the mass resolution

- Pre-run mass calibration check printouts

- Post-run mass calibration check printouts

SVOC DATA PACKAGE

APPENDIX 1: INSTRUMENT OUTPUT

DOCUMENTS
ALS Environmental - Burlington, ON L1535265 Appendix 141208 Appendix Page 1 of 625
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7:36

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

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7:36

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,748.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

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100 A9.78E6 

7:34

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,940.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

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100 A1.06E6 

7:34

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,236.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

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100 7:11 7:20 7:27 7:37 7:45 7:52 8:00 8:10 8:17 8:26 8:35 8:50 8:58 9:07 9:15 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A03 #1-2851 Acq:15-NOV-2014 13:53:10 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#1-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

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50 

100 A5.66E5 

8:45

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,712.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A5.32E5 

8:54

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,752.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

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100 A4.72E6 

8:50

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

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100 A4.37E6 

8:50

A3.15E6

8:42

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

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100 7:11 7:20 7:27 7:37 7:45 7:52 8:00 8:10 8:17 8:26 8:35 8:50 8:58 9:07 9:15 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A03 #1-2851 Acq:15-NOV-2014 13:53:10 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#1-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

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50 

100 A1.20E6 

10:11

A4.27E5

10:28

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.09E5 

10:11

A1.42E5

10:28

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.43E6 

10:10

A3.34E6

10:26

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.02E6 

10:10

A5.32E5

10:26

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:51 9:59 10:06 10:14 10:24 10:37 10:51 11:06 11:15 11:23 11:34 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A03 #1-2851 Acq:15-NOV-2014 13:53:10 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#1-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.79E5 

10:28

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,164.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.93E5 

10:28

A5.48E4

10:11

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,224.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.75E6 

10:26

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.85E6 

10:26

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:51 9:59 10:06 10:14 10:24 10:37 10:51 11:06 11:15 11:23 11:34 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A03 #1-2851 Acq:15-NOV-2014 13:53:10 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#1-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.11E5 

11:19

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.46E5 

11:19

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.72E6 

11:16

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.75E6 

11:16

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:51 9:59 10:06 10:14 10:24 10:37 10:51 11:06 11:15 11:23 11:34 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A03 #1-2851 Acq:15-NOV-2014 13:53:10 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#1-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.39E6 

12:52

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.28E5 

12:52

A1.03E5

12:57

A1.00E4

13:02

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.29E7 

12:49

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.14E5 

12:49

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:26 12:56 13:15 13:29 13:46 14:00 14:22 14:37 14:52 15:08 15:36 15:5

12:11 12:42 

13:56

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A03 #1-2851 Acq:15-NOV-2014 13:53:10 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#1-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.05E6 

15:11

A9.77E5

14:48

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.84E5 

15:11

A1.62E5

14:48

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.09E6 

15:09

A7.22E6

14:46

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.29E6 

15:09

A1.18E6

14:46

A9.33E4

15:36

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:26 12:56 13:15 13:29 13:46 14:00 14:22 14:37 14:52 15:08 15:36 15:5

12:11 12:42 

13:56

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A03 #1-2851 Acq:15-NOV-2014 13:53:10 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#1-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.20E6 

17:37

A2.56E5

17:00

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.22E5 

17:37

A9.91E4

17:00

A9.66E3

17:44

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.12E7 

17:34

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.19E6 

17:34

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:42 16:55 17:07 17:25 17:35 17:49 17:59 18:09 18:20 18:32 18:45 18:56 

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A03 #1-2851 Acq:15-NOV-2014 13:53:10 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#1-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A9.26E5 

20:15

A7.77E5

19:44

A1.05E6

20:31

A6.09E4

19:54

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.24E5 

20:15

A2.30E5

19:48

A2.33E5

20:31

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.05E7 

20:12

A7.22E6

19:42

A7.80E6

20:28

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.37E6 

20:12

A1.98E6

19:45

A1.58E6

20:28

A1.29E5

19:49

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:39 19:52 20:00 20:12 20:23 20:39 20:46 21:01 21:12 21:21 21:30 21:3

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A03 #1-2851 Acq:15-NOV-2014 13:53:10 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#1-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A7.13E5 

22:48

A5.22E5

22:23

A2.23E5

22:27

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.73E5 

22:47

A1.28E5

22:22

A6.43E4

22:27

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A6.24E6 

22:45

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.44E6 

22:45

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:09 22:39 23:01 23:29 23:49 24:09 24:41 25:18 25:45 26:10 26:37 27:00 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A03 #1-2851 Acq:15-NOV-2014 13:53:10 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#1-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.64E5 

22:27

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.32E5 

22:27

A1.11E4

22:45

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.90E6 

22:23

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A8.52E5 

22:24

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:09 22:39 23:01 23:29 23:49 24:09 24:41 25:18 25:45 26:10 26:37 27:00 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A03 #1-2851 Acq:15-NOV-2014 13:53:10 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#1-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A4.34E6 

15:36

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A8.08E5 

15:35

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 13:29 13:46 14:00 14:22 15:08 15:5

12:26 12:56 13:15 14:37 14:52 15:36 

12:11 12:35 12:51 13:31 14:01 14:17 14:55 15:11 15:34 1

13:56

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A03 #1-2851 Acq:15-NOV-2014 13:53:10 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#1-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A6.14E6 

7:34

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1788.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A7.29E5 

7:34

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,636.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.02E7 

7:32

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,700.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.10E6 

7:32

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,828.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:10 7:23 7:32 7:47 7:55 8:09 8:17 8:25 8:32 8:42 8:50 8:59 9:06 9:

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A04 #1-2850 Acq:15-NOV-2014 14:27:20 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#2-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.82E6 

8:43

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,328.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.65E6 

8:52

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,484.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.48E6 

8:49

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.21E6 

8:49

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:10 7:23 7:32 7:47 7:55 8:09 8:17 8:25 8:32 8:42 8:50 8:59 9:06 9:

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A04 #1-2850 Acq:15-NOV-2014 14:27:20 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#2-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.76E6 

10:09

A2.14E6

10:27

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.06E6 

10:09

A7.15E5

10:27

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.51E6 

10:08

A3.34E6

10:24

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.10E6 

10:08

A5.30E5

10:24

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:52 9:59 10:06 10:14 10:23 10:36 10:45 10:53 11:02 11:09 11:18 11:26 11:34 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A04 #1-2850 Acq:15-NOV-2014 14:27:20 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#2-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.00E6 

10:27

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,112.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.49E6 

10:27

A3.44E5

10:09

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,200.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.61E6 

10:23

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.77E6 

10:24

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:52 9:59 10:06 10:14 10:23 10:36 10:45 10:53 11:02 11:09 11:18 11:26 11:34 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A04 #1-2850 Acq:15-NOV-2014 14:27:20 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#2-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.54E6 

11:17

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.71E6 

11:17

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.46E6 

11:14

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.41E6 

11:14

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:52 9:59 10:06 10:14 10:23 10:36 10:45 10:53 11:02 11:09 11:18 11:26 11:34 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A04 #1-2850 Acq:15-NOV-2014 14:27:20 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#2-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A7.11E6 

12:50

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A6.70E5 

12:50

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.42E7 

12:47

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.10E5 

12:47

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:11 12:27 12:56 13:30 13:47 14:01 14:20 14:34 14:49 15:05 15:22 15:36 15:

12:42 13:16 12:58 

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A04 #1-2850 Acq:15-NOV-2014 14:27:20 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#2-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A5.32E6 

15:09

A5.09E6

14:46

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.97E5 

15:09

A8.48E5

14:46

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.35E6 

15:07

A7.49E6

14:44

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.42E6 

15:07

A1.20E6

14:44

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:11 12:27 12:56 13:30 13:47 14:01 14:20 14:34 14:49 15:05 15:22 15:36 15:

12:42 13:16 12:58 

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A04 #1-2850 Acq:15-NOV-2014 14:27:20 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#2-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A6.57E6 

17:35

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.29E6 

17:35

A9.98E4

16:58

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.20E7 

17:32

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.35E6 

17:32

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:39 16:53 17:16 17:27 17:48 17:59 18:11 18:21 18:31 18:41 19:01 

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A04 #1-2850 Acq:15-NOV-2014 14:27:20 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#2-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A5.93E6 

20:29

A4.73E6

20:13

A4.15E6

19:42

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.33E6 

20:29

A1.07E6

20:13

A9.30E5

19:42

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.08E7 

20:10

A1.06E7

19:43

A8.32E6

20:26

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.43E6 

20:10

A2.16E6

19:43

A1.86E6

20:26

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:38 19:52 20:05 20:23 20:39 20:49 21:00 21:09 21:28 21:36 

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A04 #1-2850 Acq:15-NOV-2014 14:27:20 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#2-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.00E6 

22:45

A1.46E6

22:25

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A9.39E5 

22:45

A3.94E5

22:25

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A7.05E6 

22:43

A5.98E6

22:18

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.63E6 

22:43

A1.30E6

22:18

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:08 22:27 22:47 23:09 23:39 23:59 24:27 24:46 25:07 25:32 25:58 26:32 27:05 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A04 #1-2850 Acq:15-NOV-2014 14:27:20 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#2-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.72E6 

22:25

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A8.72E5 

22:25

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.56E6 

22:22

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.00E6 

22:21

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:08 22:27 22:47 23:09 23:39 23:59 24:27 24:46 25:07 25:32 25:58 26:32 27:05 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A04 #1-2850 Acq:15-NOV-2014 14:27:20 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#2-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A3.98E6 

15:34

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A7.67E5 

15:34

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 12:56 13:47 14:34 15:05 15:

12:11 12:49 13:30 14:06 14:23 14:40 15:22 15:36 12:27 13:06 13:53 

14:47 15:08 12:18 13:24 

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A04 #1-2850 Acq:15-NOV-2014 14:27:20 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#2-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.12E7 

7:34

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,3316.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.42E6 

7:34

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,760.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.81E6 

7:32

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,448.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.03E6 

7:32

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,44.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:16 7:23 7:31 7:44 7:53 8:05 8:16 8:28 8:39 8:46 8:54 9:08 9:14 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A05 #1-2850 Acq:15-NOV-2014 15:01:35 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#3-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A5.22E6 

8:43

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,312.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.88E6 

8:52

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,412.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.49E6 

8:49

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.33E6 

8:49

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:16 7:23 7:31 7:44 7:53 8:05 8:16 8:28 8:39 8:46 8:54 9:08 9:14 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A05 #1-2850 Acq:15-NOV-2014 15:01:35 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#3-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.09E7 

10:09

A4.02E6

10:27

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.06E6 

10:09

A1.39E6

10:27

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.35E6 

10:08

A3.29E6

10:23

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.08E6 

10:08

A5.31E5

10:23

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:54 10:10 10:24 10:32 10:41 10:53 11:05 11:14 11:22 11:33 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A05 #1-2850 Acq:15-NOV-2014 15:01:35 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#3-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.65E6 

10:26

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,172.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.58E6 

10:27

A6.32E5

10:09

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,212.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.54E6 

10:23

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.68E6 

10:23

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:54 10:10 10:24 10:32 10:41 10:53 11:05 11:14 11:22 11:33 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A05 #1-2850 Acq:15-NOV-2014 15:01:35 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#3-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.93E6 

11:17

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.19E6 

11:17

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.62E6 

11:14

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.56E6 

11:14

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:54 10:10 10:24 10:32 10:41 10:53 11:05 11:14 11:22 11:33 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A05 #1-2850 Acq:15-NOV-2014 15:01:35 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#3-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.32E7 

12:50

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.31E6 

12:50

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.29E7 

12:48

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.59E5 

12:48

A8.22E4

12:57

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:19 13:07 13:22 13:42 14:11 14:28 14:57 15:11 15:27 15

12:44 13:24 13:56 15:42

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A05 #1-2850 Acq:15-NOV-2014 15:01:35 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#3-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.03E7 

15:09

A9.33E6

14:46

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.79E6 

15:09

A1.71E6

14:46

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.19E6 

15:07

A7.15E6

14:44

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.32E6 

15:07

A1.14E6

14:44

A7.54E4

14:48

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:19 13:07 13:22 13:42 14:11 14:28 14:57 15:11 15:27 15

12:44 13:24 13:56 15:42

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A05 #1-2850 Acq:15-NOV-2014 15:01:35 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#3-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.13E7 

17:35

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.33E6 

17:35

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.11E7 

17:32

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.17E6 

17:32

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:36 16:46 16:57 17:14 17:23 17:38 17:48 18:07 18:20 18:35 18:49 19:0

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A05 #1-2850 Acq:15-NOV-2014 15:01:35 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#3-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A8.51E6 

20:13

A1.01E7

20:29

A7.46E6

19:43

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.33E6 

20:29

A1.94E6

20:13

A1.55E6

19:43

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A9.48E6 

20:10

A9.49E6

19:43

A7.18E6

20:26

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.19E6 

20:10

A2.09E6

19:43

A1.56E6

20:16

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:41 19:51 19:59 20:07 20:15 20:26 20:34 20:43 20:55 21:04 21:15 21:31 

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A05 #1-2850 Acq:15-NOV-2014 15:01:35 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#3-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.43E6 

22:45

A1.70E6

22:25

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.04E6 

22:45

A4.04E5

22:25

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.91E6 

22:43

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A9.39E5 

22:43

A5.24E5

22:18

A2.56E5

22:21

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:15 22:47 23:22 23:42 24:14 24:35 25:13 25:35 25:54 26:13 26:37 27:04 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A05 #1-2850 Acq:15-NOV-2014 15:01:35 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#3-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.05E6 

22:25

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A9.62E5 

22:25

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.63E6 

22:22

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A6.32E5 

22:21

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:15 22:47 23:22 23:42 24:14 24:35 25:13 25:35 25:54 26:13 26:37 27:04 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A05 #1-2850 Acq:15-NOV-2014 15:01:35 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#3-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A4.12E6 

15:34

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A8.43E5 

15:34

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 13:07 13:22 14:11 15:27 

13:42 14:28 14:57 15:33 15

12:19 12:44 13:27 13:58 15:11 13:12 14:14 14:34 15:

12:21 13:39 12:52

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A05 #1-2850 Acq:15-NOV-2014 15:01:35 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#3-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.38E7 

7:34

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,2540.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.93E6 

7:34

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,988.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.57E6 

7:31

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,604.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.01E6 

7:31

A5.44E4

8:49

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,256.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:05 7:14 7:27 7:35 7:48 8:01 8:11 8:25 8:41 8:48 8:57 9:10 9:1

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A06 #1-2849 Acq:15-NOV-2014 15:35:55 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.01E7 

8:52

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,256.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.84E6 

8:52

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,516.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.59E6 

8:48

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.34E6 

8:48

A3.09E6

8:40

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:05 7:14 7:27 7:35 7:48 8:01 8:11 8:25 8:41 8:48 8:57 9:10 9:1

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A06 #1-2849 Acq:15-NOV-2014 15:35:55 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.25E7 

10:09

A8.18E6

10:26

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.37E6 

10:09

A2.96E6

10:26

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.28E6 

10:08

A3.29E6

10:23

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.09E6 

10:08

A4.99E5

10:23

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:49 9:59 10:14 10:23 10:30 10:40 10:55 11:11 11:20 11:36 1

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A06 #1-2849 Acq:15-NOV-2014 15:35:55 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.15E7 

10:26

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,192.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.35E7 

10:26

A1.17E6

10:09

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,188.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.58E6 

10:23

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.81E6 

10:23

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:49 9:59 10:14 10:23 10:30 10:40 10:55 11:11 11:20 11:36 1

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A06 #1-2849 Acq:15-NOV-2014 15:35:55 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.04E7 

11:17

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.10E7 

11:17

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.81E6 

11:14

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.86E6 

11:14

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:49 9:59 10:14 10:23 10:30 10:40 10:55 11:11 11:20 11:36 1

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A06 #1-2849 Acq:15-NOV-2014 15:35:55 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.86E7 

12:49

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.76E6 

12:49

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.37E7 

12:47

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.63E5 

12:47

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:06 12:35 12:51 13:13 13:41 13:56 14:16 14:46 15:07 15:31 15:4

13:16 14:31

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A06 #1-2849 Acq:15-NOV-2014 15:35:55 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.04E7 

15:09

A1.97E7

14:46

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.86E6 

15:09

A3.59E6

14:46

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A7.88E6 

15:07

A7.10E6

14:44

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.32E6 

14:44

A1.38E6

15:07

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:06 12:35 12:51 13:13 13:41 13:56 14:16 14:46 15:07 15:31 15:4

13:16 14:31

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A06 #1-2849 Acq:15-NOV-2014 15:35:55 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.17E7 

17:35

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A4.65E6 

17:35

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.08E7 

17:32

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.17E6 

17:32

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:36 16:45 16:55 17:06 17:18 17:29 17:40 17:50 18:03 18:13 18:28 18:37 18:47 18:57 

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A06 #1-2849 Acq:15-NOV-2014 15:35:55 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.43E7 

20:29

A1.01E7

20:13

A9.45E6

19:42

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A3.29E6 

20:29

A2.34E6

20:13

A2.19E6

19:42

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A5.69E6 

20:10

A6.35E6

19:43

A4.30E6

20:16

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.23E6 

20:10

A1.11E6

19:43

A8.97E5

20:26

A1.14E5

19:46

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:41 19:49 19:57 20:12 20:23 20:34 20:44 20:57 21:12 21:27 21:37 

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A06 #1-2849 Acq:15-NOV-2014 15:35:55 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.98E6 

22:46

A3.45E6

22:21

A2.36E6

22:25

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.18E6 

22:46

A8.37E5

22:20

A5.70E5

22:25

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.22E6 

22:43

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.94E5 

22:43

A2.62E4

22:27

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:20 22:53 23:16 23:42 24:10 24:43 25:09 25:31 25:51 26:17 26:36 27:0

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A06 #1-2849 Acq:15-NOV-2014 15:35:55 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.98E6 

22:25

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.17E6 

22:25

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.52E6 

22:21

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.25E5 

22:21

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:20 22:53 23:16 23:42 24:10 24:43 25:09 25:31 25:51 26:17 26:36 27:0

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A06 #1-2849 Acq:15-NOV-2014 15:35:55 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A4.32E6 

15:33

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A8.03E5 

15:33

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 12:51 13:13 14:16 14:46 

12:06 12:35 13:20 13:56 15:31 15:

13:41 14:31 15:07 12:24 13:02 14:17 14:48 15:35 15

12:48 13:36

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A06 #1-2849 Acq:15-NOV-2014 15:35:55 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A5.96E7 

7:34

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,2948.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A6.68E6 

7:34

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1020.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.81E6 

7:32

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,196.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.04E6 

7:32

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,280.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:07 7:17 7:28 7:35 7:42 7:49 7:57 8:05 8:16 8:23 8:30 8:38 8:57 9:05 9:14 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A07 #1-2849 Acq:15-NOV-2014 16:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#5-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.45E7 

8:52

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,404.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.43E7 

8:52

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,444.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.46E6 

8:49

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.33E6 

8:49

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:07 7:17 7:28 7:35 7:42 7:49 7:57 8:05 8:16 8:23 8:30 8:38 8:57 9:05 9:14 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A07 #1-2849 Acq:15-NOV-2014 16:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#5-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.97E7 

10:09

A1.93E7

10:27

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.03E7 

10:09

A7.01E6

10:27

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.47E6 

10:08

A3.27E6

10:24

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.11E6 

10:08

A5.01E5

10:24

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:56 10:11 10:19 10:27 10:42 10:57 11:08 11:18 11:27 11:34 1

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A07 #1-2849 Acq:15-NOV-2014 16:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#5-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.92E7 

10:27

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,156.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.48E7 

10:27

A3.25E6

10:09

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,320.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.52E6 

10:24

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.78E6 

10:24

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:56 10:11 10:19 10:27 10:42 10:57 11:08 11:18 11:27 11:34 1

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A07 #1-2849 Acq:15-NOV-2014 16:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#5-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.51E7 

11:17

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.66E7 

11:17

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.69E6 

11:14

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.73E6 

11:14

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:56 10:11 10:19 10:27 10:42 10:57 11:08 11:18 11:27 11:34 1

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A07 #1-2849 Acq:15-NOV-2014 16:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#5-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A7.99E7 

12:50

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A6.87E6 

12:50

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.37E7 

12:48

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.01E6 

12:48

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:26 12:51 13:06 13:30 13:45 14:00 14:27 14:43 15:00 15:15 15:29 15:44 

12:12 13:01

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A07 #1-2849 Acq:15-NOV-2014 16:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#5-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A6.03E7 

15:09

A5.45E7

14:47

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.84E6 

15:09

A8.83E6

14:47

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.53E6 

15:07

A7.21E6

14:45

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.47E6 

15:07

A1.19E6

14:45

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:26 12:51 13:06 13:30 13:45 14:00 14:27 14:43 15:00 15:15 15:29 15:44 

12:12 13:01

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A07 #1-2849 Acq:15-NOV-2014 16:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#5-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A7.39E7 

17:35

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.40E7 

17:35

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.30E7 

17:32

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.64E6 

17:32

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:36 16:55 17:10 17:25 17:35 17:47 18:04 18:15 18:31 18:46 18:55 19

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A07 #1-2849 Acq:15-NOV-2014 16:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#5-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A7.71E7 

20:29

A6.02E7

20:13

A6.85E7

19:46

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.62E7 

20:29

A1.29E7

20:13

A1.48E7

19:46

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.17E7 

20:10

A1.27E7

19:43

A9.56E6

20:26

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.66E6 

20:10

A2.73E6

19:43

A2.10E6

20:26

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:37 19:46 19:59 20:06 20:16 20:30 20:39 20:47 20:56 21:07 21:19 21:29 21:3

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A07 #1-2849 Acq:15-NOV-2014 16:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#5-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.79E7 

22:46

A3.58E7

22:21

A1.77E7

22:25

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.15E7 

22:46

A8.88E6

22:20

A5.02E6

22:25

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A7.94E6 

22:43

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.82E6 

22:43

A6.05E5

22:21

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:12 22:31 22:54 23:26 23:50 24:14 24:38 25:00 25:28 25:50 26:22 26:41 2

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A07 #1-2849 Acq:15-NOV-2014 16:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#5-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.92E7 

22:25

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.19E7 

22:25

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A6.05E6 

22:21

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.32E6 

22:21

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:12 22:31 22:54 23:26 23:50 24:14 24:38 25:00 25:28 25:50 26:22 26:41 2

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A07 #1-2849 Acq:15-NOV-2014 16:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#5-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A4.43E6 

15:34

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A8.50E5 

15:34

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 12:51 14:00 14:27 15:00 15:15 15:29 15:44 

12:26 13:06 13:30 13:45 14:43 

14:14 15:03 15:32 15:47 12:16 12:43 12:59 13:38 14:47

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A07 #1-2849 Acq:15-NOV-2014 16:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#5-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.93E8 

7:34

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,5204.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.08E7 

7:34

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1272.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.02E7 

7:32

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,616.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.07E6 

7:32

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,336.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:18 7:26 7:34 7:41 7:52 8:06 8:13 8:20 8:30 8:44 8:53 9:05 9:14 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A08 #1-2850 Acq:15-NOV-2014 16:44:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#6-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.26E8 

8:43

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,396.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.18E8 

8:52

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,564.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.60E6 

8:48

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.38E6 

8:48

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:18 7:26 7:34 7:41 7:52 8:06 8:13 8:20 8:30 8:44 8:53 9:05 9:14 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A08 #1-2850 Acq:15-NOV-2014 16:44:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#6-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.34E8 

10:09

A9.03E7

10:27

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.88E7 

10:09

A3.00E7

10:27

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.03E6 

10:08

A3.18E6

10:24

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.18E6 

10:08

A5.18E5

10:24

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:47 10:01 10:09 10:18 10:27 10:40 10:50 10:59 11:08 11:19 11:31 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A08 #1-2850 Acq:15-NOV-2014 16:44:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#6-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.49E8 

10:26

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,216.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.83E8 

10:27

A1.43E7

10:09

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,280.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.63E6 

10:24

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.84E6 

10:24

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:47 10:01 10:09 10:18 10:27 10:40 10:50 10:59 11:08 11:19 11:31 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A08 #1-2850 Acq:15-NOV-2014 16:44:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#6-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.30E8 

11:17

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.38E8 

11:17

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.89E6 

11:14

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.98E6 

11:14

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:47 10:01 10:09 10:18 10:27 10:40 10:50 10:59 11:08 11:19 11:31 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A08 #1-2850 Acq:15-NOV-2014 16:44:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#6-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.67E8 

12:50

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.19E7 

12:50

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.55E7 

12:53

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.04E6 

12:48

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:31 12:55 13:29 13:45 14:08 14:23 14:37 14:58 15:16 15:42 

12:11 12:47 13:11 15:00 

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A08 #1-2850 Acq:15-NOV-2014 16:44:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#6-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.26E8 

15:09

A3.07E8

14:47

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.63E7 

15:09

A4.27E7

14:47

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.51E6 

15:07

A7.52E6

14:45

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.44E6 

15:07

A1.30E6

14:45

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:31 12:55 13:29 13:45 14:08 14:23 14:37 14:58 15:16 15:42 

12:11 12:47 13:11 15:00 

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A08 #1-2850 Acq:15-NOV-2014 16:44:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#6-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A4.01E8 

17:35

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A6.99E7 

17:35

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.46E7 

17:32

A8.55E6

17:29

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.96E6 

17:32

A1.75E6

17:28

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:36 16:49 16:59 17:11 17:25 17:36 17:51 18:06 18:16 18:34 18:43 18:57 

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A08 #1-2850 Acq:15-NOV-2014 16:44:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#6-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A4.01E8 

20:29

A3.44E8

20:13

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A7.86E7 

20:29

A6.93E7

19:46

A6.28E7

20:13

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.41E7 

19:43

A1.14E7

20:10

A9.67E6

20:26

A7.86E6

19:40

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A3.30E6 

19:43

A2.58E6

20:10

A1.75E6

19:39

A2.10E6

20:26

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:44 19:53 20:03 20:13 20:29 20:40 20:49 21:06 21:19 21:35 

19:36 21:27

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A08 #1-2850 Acq:15-NOV-2014 16:44:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#6-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.90E8 

22:45

A2.31E8

22:21

A7.79E7

22:24

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.83E7 

22:45

A4.72E7

22:21

A2.01E7

22:24

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A9.03E6 

22:43

A8.54E6

22:18

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.15E6 

22:43

A1.97E6

22:18

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:10 22:37 22:57 23:22 23:51 24:12 24:44 25:08 25:26 26:02 26:23 26:42 27:00 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A08 #1-2850 Acq:15-NOV-2014 16:44:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#6-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.86E8 

22:24

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.77E7 

22:24

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.65E6 

22:21

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:10 22:37 22:57 23:22 23:51 24:12 24:44 25:08 25:26 26:02 26:23 26:42 27:00 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A08 #1-2850 Acq:15-NOV-2014 16:44:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#6-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A4.56E6 

15:34

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A8.81E5 

15:33

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 12:55 14:58 

12:31 13:05 13:29 13:45 14:03 14:23 14:37 15:16 15:42 12:11 12:35 12:50 13:30 13:57 14:39 15:02 15:20 

14:25

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A08 #1-2850 Acq:15-NOV-2014 16:44:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CS#6-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.84E7 

7:36

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,3372.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.32E6 

7:36

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1056.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.54E7 

7:34

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,876.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.61E6 

7:34

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,512.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:19 7:32 7:42 7:48 7:57 8:04 8:14 8:24 8:36 8:50 9:00 9:10 9

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A09 #1-2850 Acq:15-NOV-2014 17:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-RS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.32E5 

8:45

A1.36E5

8:54

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,396.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.18E5 

8:45

A1.42E5

8:54

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,604.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A6.95E6 

8:50

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A6.67E6 

8:50

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:19 7:32 7:42 7:48 7:57 8:04 8:14 8:24 8:36 8:50 9:00 9:10 9

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A09 #1-2850 Acq:15-NOV-2014 17:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-RS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.92E7 

10:11

A7.01E6

10:28

A1.75E6

11:08

A1.39E6

9:46

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.63E6 

10:11

A2.52E6

10:28

A3.93E5

11:08

A4.10E5

9:46

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.57E7 

10:10

A4.91E6

10:25

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.06E6 

10:10

A7.83E5

10:25

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:56 10:04 10:12 10:20 10:30 10:40 10:48 10:56 11:03 11:15 11:30 11:37 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A09 #1-2850 Acq:15-NOV-2014 17:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-RS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.00E7 

10:28

A7.31E5

11:08

A7.31E5

10:35

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,244.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.18E7 

10:28

A1.99E6

11:08

A1.41E6

9:46

A1.25E6

10:35

A1.06E6

10:11

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,328.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.51E6 

10:25

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.80E6 

10:25

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:56 10:04 10:12 10:20 10:30 10:40 10:48 10:56 11:03 11:15 11:30 11:37 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A09 #1-2850 Acq:15-NOV-2014 17:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-RS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.07E6 

11:19

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.54E6 

11:19

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.91E6 

11:16

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.93E6 

11:16

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:56 10:04 10:12 10:20 10:30 10:40 10:48 10:56 11:03 11:15 11:30 11:37 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A09 #1-2850 Acq:15-NOV-2014 17:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-RS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.57E7 

12:51

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.53E6 

12:51

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.36E7 

12:49

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.59E6 

12:49

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:17 12:32 12:47 13:04 13:18 13:36 13:54 14:17 14:33 14:54 15:08 15:31 15:5

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A09 #1-2850 Acq:15-NOV-2014 17:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-RS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.88E7 

14:48

A1.91E7

15:11

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.43E6 

14:48

A3.55E6

15:11

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.36E7 

14:46

A1.33E7

15:09

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.43E6 

14:46

A2.29E6

15:09

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:17 12:32 12:47 13:04 13:18 13:36 13:54 14:17 14:33 14:54 15:08 15:31 15:5

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A09 #1-2850 Acq:15-NOV-2014 17:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-RS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.24E7 

17:33

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A4.61E6 

17:33

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.59E7 

17:34

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A5.28E6 

17:33

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:43 16:57 17:11 17:25 17:37 17:54 18:07 18:17 18:27 18:39 18:49 18:59 1

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A09 #1-2850 Acq:15-NOV-2014 17:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-RS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.93E7 

19:44

A1.87E7

20:21

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A4.64E6 

19:44

A4.44E6

20:21

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.07E7 

20:12

A1.71E7

19:41

A2.01E7

20:27

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A4.81E6 

20:12

A5.02E6

19:45

A4.45E6

20:27

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:40 19:49 19:56 20:14 20:24 20:32 20:43 20:51 21:01 21:12 21:21 21:32 21

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A09 #1-2850 Acq:15-NOV-2014 17:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-RS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.30E7 

22:47

A1.80E7

22:22

A8.29E6

22:26

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.85E6 

22:47

A4.50E6

22:22

A2.44E6

22:26

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.82E7 

22:44

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.46E6 

22:44

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:27 22:48 23:08 23:40 24:10 24:32 25:01 25:38 26:09 26:34 26:56 2

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A09 #1-2850 Acq:15-NOV-2014 17:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-RS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.17E7 

22:26

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.52E6 

22:26

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.29E7 

22:23

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.05E6 

22:23

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:27 22:48 23:08 23:40 24:10 24:32 25:01 25:38 26:09 26:34 26:56 2

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A09 #1-2850 Acq:15-NOV-2014 17:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-RS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A8.20E6 

15:35

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A1.58E6 

15:35

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 13:04 13:36 14:17 14:54 15:31 

12:47 13:18 13:54 14:33 15:08 15:5

12:17 12:32 13:39 14:10 15:28 13:01 13:16 14:40 15:

12:19 14:22

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A09 #1-2850 Acq:15-NOV-2014 17:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-RS#4-0112 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.91E7 

7:35

A1.06E7

7:15

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,31796.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.00E6 

7:10

A3.61E6

7:35

A2.15E6

7:15

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,2444.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.84E7 

7:33

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1128.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.95E6 

7:33

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1288.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:13 7:22 7:29 7:38 7:49 8:03 8:11 8:18 8:26 8:34 8:45 8:56 9:04 9

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A10 #1-2849 Acq:15-NOV-2014 17:53:01 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:WG1980014-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.70E4 

8:53

A5.52E4

8:26

A3.02E3

8:16

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,868.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 

A1.12E5

8:53

A7.27E4

8:26

A1.17E4

8:49

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1488.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A6.41E6 

8:41

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A5.74E6 

8:41

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:13 7:22 7:29 7:38 7:49 8:03 8:11 8:18 8:26 8:34 8:45 8:56 9:04 9

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A10 #1-2849 Acq:15-NOV-2014 17:53:01 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:WG1980014-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.20E7 

10:11

A7.52E6

10:28

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.06E6 

10:11

A2.77E6

10:28

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.55E7 

10:09

A6.71E6

10:25

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.08E6 

10:09

A1.16E6

10:25

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:55 10:03 10:17 10:25 10:36 10:44 10:51 11:01 11:08 11:15 11:26 11:35 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A10 #1-2849 Acq:15-NOV-2014 17:53:01 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:WG1980014-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.14E7 

10:28

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,264.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.34E7 

10:28

A1.23E6

10:10

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,376.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.22E7 

10:25

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.26E7 

10:25

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:55 10:03 10:17 10:25 10:36 10:44 10:51 11:01 11:08 11:15 11:26 11:35 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A10 #1-2849 Acq:15-NOV-2014 17:53:01 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:WG1980014-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.78E6 

11:18

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.04E7 

11:18

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.17E3 

11:16

A1.09E3

10:15

A828.69

9:48

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.02E3 

11:15

A614.55

10:32

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:55 10:03 10:17 10:25 10:36 10:44 10:51 11:01 11:08 11:15 11:26 11:35 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A10 #1-2849 Acq:15-NOV-2014 17:53:01 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:WG1980014-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.61E7 

12:51

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.46E6 

12:51

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.41E7 

12:48

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.55E6 

12:48

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:08 12:26 12:44 13:10 13:34 13:50 14:04 14:21 14:40 15:09 15:28 15:47 

13:03 13:23

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A10 #1-2849 Acq:15-NOV-2014 17:53:01 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:WG1980014-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.68E7 

14:47

A1.62E7

15:10

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.03E6 

14:47

A3.03E6

15:10

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.37E7 

15:08

A1.11E7

14:45

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.41E6 

15:08

A2.00E6

14:45

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:08 12:26 12:44 13:10 13:34 13:50 14:04 14:21 14:40 15:09 15:28 15:47 

13:03 13:23

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A10 #1-2849 Acq:15-NOV-2014 17:53:01 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:WG1980014-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A8.93E6 

17:32

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.76E6 

17:32

A1.12E5

16:59

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.00E7 

17:33

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.02E6 

17:33

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:42 16:55 17:06 17:16 17:25 17:36 17:50 18:09 18:19 18:31 18:42 18:52 19:02 

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A10 #1-2849 Acq:15-NOV-2014 17:53:01 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:WG1980014-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A6.92E6 

19:44

A6.00E6

20:20

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.59E6 

19:44

A1.32E6

20:20

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A9.29E6 

20:11

A7.76E6

19:44

A5.59E6

20:18

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.07E6 

20:11

A1.56E6

19:44

A1.20E6

20:18

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:40 19:49 20:06 20:13 20:21 20:29 20:42 20:50 21:03 21:12 21:22 21:34 2

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A10 #1-2849 Acq:15-NOV-2014 17:53:01 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:WG1980014-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.64E6 

22:47

A4.32E6

22:22

A1.93E6

22:26

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.35E6 

22:47

A1.05E6

22:22

A5.03E5

22:26

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.41E6 

22:44

A3.92E6

22:19

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.01E6 

22:44

A9.15E5

22:19

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:20 22:41 23:09 23:32 23:51 24:25 24:58 25:19 25:48 26:24 26:57 2

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A10 #1-2849 Acq:15-NOV-2014 17:53:01 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:WG1980014-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.50E6 

22:26

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.08E6 

22:26

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.76E6 

22:23

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A6.24E5 

22:23

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:20 22:41 23:09 23:32 23:51 24:25 24:58 25:19 25:48 26:24 26:57 2

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A10 #1-2849 Acq:15-NOV-2014 17:53:01 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:WG1980014-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A1.39E3 

15:18

A504.77

15:35

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A927.34 

15:19

A135.92

15:21

A112.20

12:09

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 13:10 13:34 13:50 14:21 15:09 15:47 

12:08 12:26 12:57 13:15 14:04 14:40 15:28 12:42 13:31 13:45 14:25 15:29 15:49 

12:13 13:03 15:14 12:28 13:23

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A10 #1-2849 Acq:15-NOV-2014 17:53:01 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:WG1980014-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.96E6 

7:09

A1.38E6

7:34

A5.43E5

7:20

A2.05E5

7:40

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,3748.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A8.67E5 

7:09

A3.64E5

7:15

A1.73E5

7:34

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,996.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.08E7 

7:32

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,884.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.09E6 

7:32

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1128.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:20 7:28 7:38 7:46 7:55 8:09 8:16 8:25 8:33 8:44 8:53 9:00 9:11 9:

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A6.43E4 

8:44

A7.53E3

8:26

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A5.45E4 

8:54

A1.03E4

8:26

A3.45E3

8:59

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,600.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.44E6 

8:41

A2.08E6

8:49

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.99E6 

8:41

A1.96E6

8:49

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:20 7:28 7:38 7:46 7:55 8:09 8:16 8:25 8:33 8:44 8:53 9:00 9:11 9:

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 

A1.32E4

10:10

A1.72E4

10:27

A8.03E3

11:34

A9.43E3

10:49

A9.74E3

9:59

A5.16E3

9:47

A3.91E3

10:37

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 

A2.34E3

10:28

A2.61E3

9:54

A2.98E3

10:14

A1.72E3

10:49

A1

1

A1.28E3

10:03

A1.95E3

11:34

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.34E6 

10:09

A4.80E6

10:24

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.29E5 

10:09

A8.08E5

10:24

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:54 10:08 10:22 10:30 10:41 10:49 10:59 11:12 11:20 11:30 11:38 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 

A6.40E3

10:28

A5.10E3

9:50

A7.16E3

10:01

A3.99E3

10:41

A1.85E

11:38

A842.13

11:08

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,180.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 

A1.45E4

10:28

A5.43E3

9:50

A5.76E3

10:00

A2.70E3

10:11

A1.97E3

11:34

A2.16E3

10:42

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,188.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.48E6 

10:24

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.75E6 

10:24

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:54 10:08 10:22 10:30 10:41 10:49 10:59 11:12 11:20 11:30 11:38 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.73E4 

11:19

A4.79E3

9:52

A4.31E3

11:22

A2.83E3

10:48

A4.84E

11:38

A3.00E3

10:14

A2.25E3

11:04

A1.83E3

10:38

A1.45E3

10:28

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 

A2.18E4

11:19

A1.04E4

11:34

A8.33E3

10:14

A7.13E3

10:50

A1.53E4

9:52

A5.93E3

10:27

A8.63E3

10:38

A3.53E3

11:04

A4.44E3

11:22

A2.04E3

10:02

A

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.61E6 

11:15

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.60E6 

11:15

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:54 10:08 10:22 10:30 10:41 10:49 10:59 11:12 11:20 11:30 11:38 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.15E5 

12:51

A2.82E4

12:20

A2.99E4

12:56

A2.27E4

13:45

A6.39E3

14:14

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.10E4 

12:51

A5.54E3

12:17

A4.06E3

13:45

A3.58E3

12:12

A3.27E3

12:55

A1.79E3

15:34

A1.98E3

14:04

A2.26E3

14:49

A2.33E3

12:32

A1.46E3

13:18

A1.94E3

15:14

A539.50

14:29

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A7.83E6 

12:48

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A5.13E5 

12:48

A4.75E5

12:54

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:13 12:36 13:00 13:24 13:45 14:14 14:29 14:44 15:04 15:18 15:34 

14:00 15:

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.82E4 

15:10

A1.04E4

14:47

A1.34E4

12:52

A7.80E3

13:21

A4.47E3

15:13

A3.64E3

14:49

A4.46E3

12:46

A1.70E3

14:27

A3.48E3

12:22

A2.14E3

15:36

A1.51E3

13:57

A1.85E3

13:30

A1.86E3

13:09

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.74E3 

13:21

A8.27E3

12:52

A7.47E3

15:10

A2.71E3

14:46

A3.74E3

13:58

A2.35E3

14:26

A1.84E3

15:32

A2.80E3

12:16

A1.40E3

13:34

A1.47E3

12:55

A976.07

15:06

A372.06

13:15

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.03E7 

15:08

A4.05E6

14:45

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.82E6 

15:08

A6.42E5

14:45

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:13 12:36 13:00 13:24 13:45 14:14 14:29 14:44 15:04 15:18 15:34 

14:00 15:

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.32E5 

16:59

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A8.63E4 

16:59

A5.63E3

17:03

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A3.30E6 

17:33

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A5.99E5 

17:33

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:36 16:54 17:06 17:21 17:32 17:42 18:00 18:18 18:30 18:40 18:51 19:0

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A5.66E3 

19:47

A4.73E3

20:21

A724.66

21:00

A562.25

21:19

A625.54

21:32

A466.15

19:35

A159.65

20:07

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 

A2.03E3

20:28

A1.85E3

19:46

A1.49E3

20:11

A1.62E

21:36

A924.08

20:45

A605.05

21:05

A543.35

20:24

A704.00

20:00

A731.94

21:19

A644.50

19:39

A470.78

20:35

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A5.20E6 

20:11

A1.89E6

19:44

A1.49E6

20:27

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.11E6 

20:11

A2.52E5

19:41

A3.09E5

20:27

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:39 19:47 20:05 20:22 20:35 20:44 20:54 21:04 21:14 21:22 21:36 

19:57 20:14

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A7.00E3 

22:46

A870.17

26:40

A756.45

25:38

A

A464.30

25:07

A491.57

23:13

A548.39

23:38

A260.95

24:20

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.37E3 

22:22

A898.74

23:26

A767.57

22:53

A807.78

26:10

A727.18

25:12

A642.17

24:33

A664.36

27:01

A507.65

22:26

A415.31

23:32

A232.93

26:23

A235.37

25:06

A206.05

24:35

A1

2

A201.01

26:51

A218.94

23:04

A134.48

24:01

A199.66

25:33

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A9.22E5 

22:44

A7.35E5

22:20

A3.88E4

22:52

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.19E5 

22:44

A1.63E5

22:20

A1.15E4

22:50

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:13 22:36 22:56 23:14 23:35 23:58 24:26 24:46 25:12 25:47 26:18 26:55 2

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.93E3 

22:26

A1.83E3

22:37

A989.63

25:25

A782.26

26:23

A791.39

24:51

A566.23

25:55

A504.46

24:24

A541.96

26:50

A669.79

23:12

A310.33

23:44

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.83E3 

22:44

A860.12

26:10

A979.71

25:30

A599.12

24:06

A1.04E3

26:45

A879.38

24:34

A628.75

23:34

A513.84

23:00

A46

27

A689.81

22:31

A340.96

25:24

A364.60

26:17

A445.93

24:58

A386.05

24:04

A278.55

24:32

A233.55

26:48

A204.10

25:51

A159.09

23:14

A99.24

22:14

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.93E5 

22:23

A2.70E4

22:34

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A7.54E4 

22:23

A2.01E4

22:26

A2.71E3

22:39

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:13 22:36 22:56 23:14 23:35 23:58 24:26 24:46 25:12 25:47 26:18 26:55 2

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A1.15E6 

15:35

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A2.10E5 

15:35

A9.02E3

15:40

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 12:13 12:36 14:14 14:55 

12:37 12:51 13:10 13:24 13:45 14:10 14:29 15:08 15:34 15:

13:11 13:26 13:55 14:52 15:22

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
8:14 8:16 8:18 8:20 8:22 8:24 8:26 8:28 8:30 8:32 8:34 8:36 8:38 8:40 8:42 8:44 8:46 8:48 8:50 8:52 8:54 8:56 8:58 9:00 9:02 9:04 

%

0 

20 40 60 80 

100 120 140 

A6.43E4

A5.10E4

A7.53E3

A455.83

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

8:14 8:16 8:18 8:20 8:22 8:24 8:26 8:28 8:30 8:32 8:34 8:36 8:38 8:40 8:42 8:44 8:46 8:48 8:50 8:52 8:54 8:56 8:58 9:00 9:02 9:04 

%

0 

20 40 60 80 

100 120 140 

A5.45E4 A5.90E4

A1.03E4

A3.45E3

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,600.0,3.00%,F,T) 

after_modification

8:14 8:16 8:18 8:20 8:22 8:24 8:26 8:28 8:30 8:32 8:34 8:36 8:38 8:40 8:42 8:44 8:46 8:48 8:50 8:52 8:54 8:56 8:58 9:00 9:02 9:04 

%

0 

20 40 60 80 

100 120 140 

8:38 8:44 8:53 9:00 9:

8:16 8:22 8:25 8:28 8:33 8:36 8:41 9:02

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

8:14 8:16 8:18 8:20 8:22 8:24 8:26 8:28 8:30 8:32 8:34 8:36 8:38 8:40 8:42 8:44 8:46 8:48 8:50 8:52 8:54 8:56 8:58 9:00 9:02 9:04 

%

0 

20 40 60 80 

100 120 140 

A6.93E4

A5.53E4

A7.72E3

A671.02 A3.20E3 A2.94E3 A

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,292.0,3.00%,F,T) 

before_modification

8:14 8:16 8:18 8:20 8:22 8:24 8:26 8:28 8:30 8:32 8:34 8:36 8:38 8:40 8:42 8:44 8:46 8:48 8:50 8:52 8:54 8:56 8:58 9:00 9:02 9:04 

%

0 

20 40 60 80 

100 120 140 

A5.67E4 A6.19E4

A1.16E4

A4.22E3 

A1.50E3

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,488.0,3.00%,F,T) 

before_modification

File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
8:24 8:26 8:28 8:30 8:32 8:34 8:36 8:38 8:40 8:42 8:44 8:46 8:48 8:50 8:52 8:54 8:56 8:58 9:00 9:02 9:04 9:06 9:08 9:10 9:12 9:14 

%

0 

20 40 60 80 

100 120 140 

A6.43E4

A5.10E4

A7.53E3

A455.83

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

8:24 8:26 8:28 8:30 8:32 8:34 8:36 8:38 8:40 8:42 8:44 8:46 8:48 8:50 8:52 8:54 8:56 8:58 9:00 9:02 9:04 9:06 9:08 9:10 9:12 9:14 

%

0 

20 40 60 80 

100 120 140 

A5.45E4

A5.90E4

A1.03E4

A3.45E3

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,600.0,3.00%,F,T) 

after_modification

8:24 8:26 8:28 8:30 8:32 8:34 8:36 8:38 8:40 8:42 8:44 8:46 8:48 8:50 8:52 8:54 8:56 8:58 9:00 9:02 9:04 9:06 9:08 9:10 9:12 9:14 

%

0 

20 40 60 80 

100 120 140 

A6.93E4

A5.53E4

A7.72E3

A3.20E3 A671.02 A2.94E3 A1.87E3

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,292.0,3.00%,F,T) 

before_modification

8:24 8:26 8:28 8:30 8:32 8:34 8:36 8:38 8:40 8:42 8:44 8:46 8:48 8:50 8:52 8:54 8:56 8:58 9:00 9:02 9:04 9:06 9:08 9:10 9:12 9:14 

%

0 

20 40 60 80 

100 120 140 

A5.67E4 A6.19E4

A1.16E4

A4.22E3 A5.36E3

A1.50E3

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,488.0,3.00%,F,T) 

before_modification

File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13

%

0 

20 40 60 80 

100 120 140 

A1.15E5

A2.10E4 A2.99E4 A1.42E4 A1.10E4 A1.75E4 A9.03E3

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13

%

0 

20 40 60 80 

100 120 140 

A1.10E4

A3.27E3 A1

A1.89E3 A2.54E3 A2.79E3 A3.96E3 A1.96E3 A2.33E3 A1.64E3 A1.75E3 

A660.00 

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13

%

0 

20 40 60 80 

100 120 140 

12:30 12:36 12:51 13:00 13:04 13:10 

12:23 12:27 12:32 12:43 12:48 12:54 12:56 12:58 13:07 

12:39

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13

%

0 

20 40 60 80 

100 120 140 

A1.04E5

A1.90E4

A1.09E4 A8.02E3 A1.78E4 A9.57E3

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13

%

0 

20 40 60 80 

100 120 140 

A8.22E3

A1.37E3 A1.50E3 A1.29E3 A1.05E3 A7

A342.14 A773.50 A373.34 A927.79 

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13:16 

%

0 

20 40 60 80 

100 120 140 

A2.99E4

A1.10E4

A1.75E4

A6.09E3 A9.03E3

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13:16 

%

0 

20 40 60 80 

100 120 140 A2.54E3 A2.79E3 

A2.33E3 

A1.96E3 A1.75E3

A1.64E3 

A632.61

A660.00

A173.6

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13:16 

%

0 

20 40 60 80 

100 120 140 

A1.78E4

A8.02E3

A9.57E3

A3.85E3

A2.88E3 A2.98E3

A1.25E3

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13:16 

%

0 

20 40 60 80 

100 120 140 

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

A1.23E4

A1.05E4

A4.44E3

A4.25E3

A4.06E3 A3.07E3

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 A1.52E3 

A1.96E3

A1.40E3

A1.92E3

A1.09E3

A796.76

A573.99 A1.31E3 A617.76

A592.18 

A386.37

A217.95 A370.93

A198.8

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

17:04 17:06 17:11 17:16 17:19 17:21 17:24 17:27 17:32 17:34 17:38 17:42 17:46 17:49 17:52 

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

A3.37E3

A2.33E3

A1.11E3

A326.26

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 A397.12 

A202.89

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 17

%

0 

20 40 60 80 

100 120 140 

A1.23E4

A1.05E4

A4.44E3

A4.25E3

A4.06E3 A3.07E3

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 17

%

0 

20 40 60 80 

100 120 140 A1.76E3 A1.52E3 

A1.96E3

A1.40E3

A1.92E3

A1.09E3

A796.76

A573.99 A1.31E3 A617.76

A592.18 A746.76

A386.37

A217.95 A370.93

A198.83 

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 17

%

0 

20 40 60 80 

100 120 140 

A5.04E3

A3.37E3

A2.33E3

A1.11E3

A326.26

A210.83

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 17

%

0 

20 40 60 80 

100 120 140 

A397.12

A202.89

A296.47

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A5.66E3 A7.30E3

A627.30

A552.75 A703.72 A466.15 A444.09 

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 A1.85E3 

A2.16E3

A1.18E3 

A944.00

A656.50

A737.00 A689.00 A704.00 A578.00 A520.00 A644.50 A494.50 A408.50

A410.44 A371.00 A601.50 A326.50 A438.50

A196.

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

19:25 19:30 19:35 19:39 19:47 19:50 19:54 19:57 20:01 20

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A7.16E3 A6.68E3

A616.00 A863.64 A604.26 A609.09 A488.45 A395.76

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A1.47E3

A1.44E3

A864.90

A1.06E3 A756.64

A834.66 A564.79 A1.16E3

A359.76

A122.45

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A5.66E3 A7.30E3

A627.30

A552.75 A703.72 A466.15 A444.09 A159

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A944.00 

A656.50

A737.00

A689.00

A704.00

A578.00 A520.00 A644.50 A494.50

A347.00 A408.50

A410.44 A371.00 A601.50 A326.50

A438.50

A299.0

A196.00

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A7.16E3

A6.68E3

A616.00 A863.64 A604.26 A609.09 A488.45 A395.76

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A864.90

A756.64 A1.06E3

A834.66 A564.79

A1.16E3

A359.76 

A314.55

A122.45

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A4.73E3

A3.30E3 A3.64E3

A159.65

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A1.04E3

A1.18E3 A976.00

A719.50 A999.00 A1.37E3

A1.02E3 A712.78

A679.94

A689.00 A543.35 A704.00 

A436.50 A494.50 A408.50 A465.54

A326.50

A438.50 

A170.24

A299.00

A196.00

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A3.91E3

A3.28E3

A2.54E3

A863.64 A604.26

A350.80 A655.13 

A17

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A397.01 A259.97

A119.05

A122.45

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A4.73E3

A3.30E3 A3.64E3

A159.65

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A326.50

A224

A438.50 

A170.24

A299.00

A196.00

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A3.44E3

A3.91E3

A3.28E3 A2.54E3

A863.64 A604.26 A350.80 A655.13 A392

A177.70

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A1.15E3

A1.56E3

A397.01 A259.97

A119.05

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A4.73E3

A3.30E3 A3.64E3

A159.65

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 A924.08 

A679.94

A754.65

A543.35 A821

A651.21

A436.50

A465.54 A408.50 A683.74

A224.56

A170.24 A283.79

A299.00 

A196.00 

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A3.91E3

A3.28E3 A2.54E3

A350.80 A655.13 A392.19

A177.70 

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A5.79E3

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A1.37E3

A947.03 A853.32

A702.34

A507.65 A675.13

A445

A883.75 

A607.21

A376.73

A260.43

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A6.26E3

A2.66E3

A1.19E3

A5

A653.67 A687.96

A380.50 A435.98 A601.02 A327.89

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A1.35E3

A931.23

A808.42

A680.22

A492.48 A638.25

A882.63 A400

A507.69 

A369.35

A260.43

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A5.93E3

A1.83E3

A1.72E3

A495.34 A4

A169.98 

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 A1.83E3 

A888.98

A1.25E3

A466.97 A689.81

A281.52 

A112.04 A99.24 

A77.02

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

22:13 22:19 22:22 22:26 22:28 22:36 22:39 22:44 

22:07 22:10 22:17 22:41 22:

22:32

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A7.59E3

A1.67E3

A1.55E3

A495.58 A822.95 A3

A170.17

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 A1.92E3 

A920.91

A1.30E3

A502.69 A735.87

A311.33 

A125.93 A117.76 A113.17 

A119.26

A39.75

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 

%

0 

20 40 60 80 

100 120 140 

A7.00E3

A5.79E3

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 

%

0 

20 40 60 80 

100 120 140 A607.21 A420.61 

A376.73

A218.94 

A175.95 A135.16

A67.65

A23.6

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 

%

0 

20 40 60 80 

100 120 140 

A6.36E3

A6.26E3

A2.66E3

A1.19E3

A1.36E3 A596.97 A1.04E3

A435.98 A327.89 A601.02 A211.74 A227.92

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 

%

0 

20 40 60 80 

100 120 140 

A369.35

A128.12 

A106.34

A29.49

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A15 #1-2852 Acq:15-NOV-2014 20:44:24 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-11 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.50E7 

7:34

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,64824.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A5.56E6 

7:34

A6.32E5

8:25

A3.43E5

8:44

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,15504.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.58E7 

7:32

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,940.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.62E6 

7:32

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1976.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:11 7:19 7:26 7:34 7:43 7:50 7:58 8:05 8:13 8:28 8:35 8:43 8:54 9:02 9:15 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A16 #1-2850 Acq:15-NOV-2014 21:18:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-4 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.36E7 

8:43

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,12428.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.08E7 

8:43

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,14744.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A5.90E6 

8:40

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A5.20E6 

8:40

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,428.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:11 7:19 7:26 7:34 7:43 7:50 7:58 8:05 8:13 8:28 8:35 8:43 8:54 9:02 9:15 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A16 #1-2850 Acq:15-NOV-2014 21:18:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-4 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.26E6 

10:27

A3.15E6

10:10

A1.97E6

9:53

A1.54E6

10:32

A1

11

A7.87E5

11:24

A7.29E5

10:48

A4.59E5

10:58

A4.62E5

9:59

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.45E6 

10:27

A5.77E5

9:53

A6.35E5

10:10

A3.77E5

10:41

A3

11

A1.98E5

11:24

A1.08E5

10:51

A1.25E5

11:07

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.39E7 

10:09

A5.86E6

10:24

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.88E6 

10:09

A1.00E6

10:24

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:53 9:59 10:07 10:17 10:29 10:41 10:51 11:08 11:20 11:29 11:3

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A16 #1-2850 Acq:15-NOV-2014 21:18:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-4 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.36E6 

10:27

A6.32E5

9:53

A4.53E5

11:08

A3.83E5

10:38

A4.48E5

10:04

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,448.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.45E6 

10:27

A2.07E6

9:53

A1.14E6

10:32

A1.31E6

11:24

A1.06E6

10:04

A8.47E5

10:48

A5.93E5

10:58

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,776.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.08E7 

10:24

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.12E7 

10:24

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:53 9:59 10:07 10:17 10:29 10:41 10:51 11:08 11:20 11:29 11:3

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A16 #1-2850 Acq:15-NOV-2014 21:18:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-4 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.47E6 

11:18

A4.72E5

10:27

A4.28E5

11:24

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.30E6 

11:18

A2.04E6

10:27

A1.09E6

11:24

A2.88E5

10:29

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 

A6.89E3

11:15

A1.63E3

10:37

A1.47E3

10:08

A1.91E3

11:27

A1.77E3

9:50

A1.19E3

10:50

A902.13

11:03

A908.30

10:19

A517

11:4

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 

A1.22E4

9:49

A8.90E3

11:15

A3.41E3

10:29

A2.47E3

11:05

A3.87E3

10:07

A2.33E3

10:16

A1.57E3

10:52

A1.21E3

11:26

A694.14

10:42

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:53 9:59 10:07 10:17 10:29 10:41 10:51 11:08 11:20 11:29 11:3

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A16 #1-2850 Acq:15-NOV-2014 21:18:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-4 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.11E7 

12:50

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A6.80E6 

12:50

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.19E7 

12:48

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.54E6 

12:48

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:20 12:38 13:11 13:27 13:42 13:57 14:15 14:29 14:49 15:07 15:22 15:39 15

12:15 12:52

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A16 #1-2850 Acq:15-NOV-2014 21:18:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-4 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.64E6 

14:47

A1.03E6

15:10

A1.60E5

14:09

A1.46E5

13:20

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.82E5 

14:47

A1.77E5

13:20

A1.98E5

15:10

A9.65E4

14:09

A3.05E4

14:42

A1.75E4

15:22

A1.52E

15:48

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.18E7 

15:08

A9.38E6

14:45

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.13E6 

15:08

A1.68E6

14:45

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:20 12:38 13:11 13:27 13:42 13:57 14:15 14:29 14:49 15:07 15:22 15:39 15

12:15 12:52

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A16 #1-2850 Acq:15-NOV-2014 21:18:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-4 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A5.69E5 

18:13

A3.75E5

16:59

A3.98E5

18:16

A4.36E5

17:35

A9.96E4

17:32

A7.89E4

17:06

A7.41E4

18:23

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A3.38E5 

18:13

A2.77E5

18:15

A1.75E5

16:59

A1.13E5

17:35

A6.28E4

16:50

A4.00E4

17:05

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.30E7 

17:32

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.65E6 

17:32

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:50 17:00 17:16 17:31 17:41 17:53 18:12 18:24 18:44 19:01 

16:38

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A16 #1-2850 Acq:15-NOV-2014 21:18:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-4 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A7.95E6 

19:45

A6.25E5

19:59

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A9.70E6 

19:46

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.56E7 

20:12

A1.11E7

19:40

A9.21E6

20:27

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A3.63E6 

20:11

A2.54E6

19:40

A2.04E6

20:27

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:39 19:48 20:01 20:12 20:25 20:35 20:46 20:54 21:04 21:18 21:28 21:3

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A16 #1-2850 Acq:15-NOV-2014 21:18:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-4 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.06E4 

22:46

A3.36E4

22:22

A6.91E3

23:08

A1.74E3

26:38

A1.40E3

25:42

A1.1

27:

A1.07E3

24:57

A2.31E3

23:43

A2.29E3

26:07

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.67E4 

22:20

A3.16E4

22:46

A7.30E3

22:49

A3.97E3

23:20

A2.19E3

25:35

A1.83E3

25:09

A1.83E3

26:03

A870.19

24:15

A919.89

26:42

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A7.90E6 

22:44

A7.29E6

22:19

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.85E6 

22:44

A1.69E6

22:19

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 23:38 24:11 24:44 25:12 25:44 26:10 26:37 26:59 

22:26 22:48 23:07 25:03

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A16 #1-2850 Acq:15-NOV-2014 21:18:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-4 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.35E4 

22:26

A5.73E3

22:46

A2.79E3

23:11

A2.26E3

24:47

A1.69E3

25:13

A2.49E3

26:02

A1.71E3

26:35

A516.93

24:17

A539.13

23:41

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.33E3 

22:44

A2.91E3

24:13

A2.56E3

25:13

A2.29E3

23:32

A1.74E3

24:27

A2.31E3

23:57

A845.27

22:27

A494.38

25:26

A560.66

26:39

A408.32

23:03

A214.41

23:47

A

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.17E6 

22:22

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.16E6 

22:22

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 23:38 24:11 24:44 25:12 25:44 26:10 26:37 26:59 

22:26 22:48 23:07 25:03

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A16 #1-2850 Acq:15-NOV-2014 21:18:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-4 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A2.11E4 

14:02

A1.36E4

13:56

A4.37E3

15:35

A1.78E3

14:43

A1.54E3

14:06

A1.04E3

13:15

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A2.89E3 

14:18

A2.53E3

15:31

A1.50

15:5

A1.83E3

14:00

A1.01E3

15:18

A868.34

14:21

A509.86

13:09

A528.89

13:45

A595.48

12:48

A324.92

14:09

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 12:20 13:11 14:49 15:07 15

12:38 13:35 13:57 14:15 15:22 15:39 12:09 13:01 13:16 14:29 

12:27 12:45 13:49 14:55 15:46 14:12 15:12 

12:56

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A16 #1-2850 Acq:15-NOV-2014 21:18:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-4 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13

%

0 

20 40 60 80 

100 120 140 

A3.08E6

A3.02E5 A3.53E5

A3.49E5 A2.38E5

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13

%

0 

20 40 60 80 

100 120 140 

A2.56E5

A4.46E4

A3.76E4 A2.73E4 A1.97E4 A1.58E4 A1.22E4

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13

%

0 

20 40 60 80 

100 120 140 

A2.57E6

A3.21E5

A1.82E5

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13

%

0 

20 40 60 80 

100 120 140 

A2.26E5

A4.74E4

A2.76E4 A1.33E4 A1.19E4

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A16 #1-2850 Acq:15-NOV-2014 21:18:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-4 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A7.95E6

A6.25E5

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A9.70E6

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A1.51E7

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A9.42E6

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A16 #1-2850 Acq:15-NOV-2014 21:18:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-4 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A7.95E6

A6.25E5

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A9.70E6

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A1.51E7

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A9.42E6

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A16 #1-2850 Acq:15-NOV-2014 21:18:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-4 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A5.20E4

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

///

after_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 A1.48E5 

A1.21E5

A8.87E4 A4.75E4

A4.28E4

A5.00E4 A7.65E4

A3.01E4

A2.59E4

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A9.50E4

A5.40E4

A2.91E4

A1.89E3

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A3.59E3

A894.27

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A16 #1-2850 Acq:15-NOV-2014 21:18:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-4 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A3.36E4

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A1.67E4 

A1.19E4 A1.02E4

A9.28E3 A9.16E3 A1.20E4 A1.49E4

A1.11E4 A6.67E3 A8.21E3 A1.12E4 

A9.35E3

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

22:26 22:39 22:42 

22:10 22:13 22:17 22:31 22:35 22:06 22:20 22:37 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A6.62E4

A9.79E3 A8.57E3 A9.92E3

A8.12E3

A5.13E3 A7.52E3 A1.37E4 A5.14E3

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A1.61E4

A1.19E4 A9.53E3 A9.13E3 

A9.16E3 A1.20E4

A1.11E4 A6.67E3 A1.28E4

A6.54E3

A8.05E3

A6.00E3 

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A16 #1-2850 Acq:15-NOV-2014 21:18:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-4 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A1.35E4

A1.34E4 A5.31E3

A2.90E3 A5.7

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A1.77E4

A5.37E3

A8.40E3

A2.80E3

A1.93E3 A6.45E3 A2.30E3 A4.31E3 A4.25E3 A2.09E3 A2.57E3

A1.6

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 A3.65E3 A3.07E3 

A2.60E3

A1.

A901.62

A624.01 

A319.93

A166.19

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A16 #1-2850 Acq:15-NOV-2014 21:18:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-4 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 

%

0 

20 40 60 80 

100 120 140 

A3.06E4

A3.36E4

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg111416mb

after_modification

22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 

%

0 

20 40 60 80 

100 120 140 

A1.67E4 A3.16E4

A1.02E4

A9.28E3 A1.49E4

A8.21E3

A1.12E4 A7.30E3 A1.30E4 A9.35E3 A1.17E4

A5.52E3

A6.51E3 

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 

%

0 

20 40 60 80 

100 120 140 

A3.77E4 A6.62E4

A1.27E4

A7.52E3 A1.37E4 A5.14E3 A5.13E3 A3.06E3 A3.89E3

A801.63

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 

%

0 

20 40 60 80 

100 120 140 

A1.61E4

A9.53E3

A9.13E3 A2.10E4

A1.28E4

A6.54E3

A8.05E3

A6.00E3 A3.95E3

A5.60E3

A1.79E3

A288.84

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A16 #1-2850 Acq:15-NOV-2014 21:18:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-4 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.36E8 

7:36

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,182432.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.45E7 

7:37

A2.04E6

7:11

A1.48E6

8:26

A7.66E5

8:45

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,61044.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.27E7 

7:34

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1372.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.37E6 

7:35

A1.19E5

8:33

A1.30E5

7:42

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,2432.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:16 7:28 7:36 7:49 8:03 8:16 8:27 8:35 8:45 8:54 9:02 9:09 9:1

7:07

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.25E8 

8:44

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,3476.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.15E8 

8:44

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,29648.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.55E6 

8:50

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,4.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.32E6 

8:50

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,872.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:16 7:28 7:36 7:49 8:03 8:16 8:27 8:35 8:45 8:54 9:02 9:09 9:1

7:07

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.57E6 

10:28

A4.95E6

10:11

A4.43E6

9:54

A2

1

A2.34E6

10:33

A1.84E6

11:24

A1.32E6

10:48

A8.23E5

10:59

A1.03E6

10:00

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.87E6 

10:28

A1.32E6

9:54

A1.31E6

10:11

A8

1

A4.36E5

10:33

A3.91E5

11:24

A2.82E5

10:48

A1.79E5

10:59

A2.41E5

10:00

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.11E7 

10:09

A4.80E6

10:25

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.52E6 

10:09

A8.03E5

10:25

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 10:01 10:09 10:17 10:29 10:37 10:45 10:55 11:04 11:12 11:22 11:32 1

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.87E6 

10:28

A1.51E6

10:00

A9.29E5

9:47

A7.63E5

10:38

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1164.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.29E7 

10:28

A4.73E6

9:54

A3.06E6

11:24

A2.31E6

10:05

A1.79E6

10:33

A1.48E6

10:48

A1.10E6

10:59

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1432.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.01E6 

10:25

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.28E6 

10:25

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 10:01 10:09 10:17 10:29 10:37 10:45 10:55 11:04 11:12 11:22 11:32 1

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.17E7 

11:18

A7.99E5

10:27

A9.35E5

11:24

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.36E7 

11:18

A3.22E6

10:27

A2.28E6

11:24

A8.90

11:3

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.87E6 

11:15

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.83E6 

11:15

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 10:01 10:09 10:17 10:29 10:37 10:45 10:55 11:04 11:12 11:22 11:32 1

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.47E8 

12:51

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.70E7 

12:51

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.88E7 

12:48

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.28E6 

12:48

A8.58E5

12:53

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:21 12:51 13:13 13:32 13:50 14:17 14:47 15:09 15:32 15:5

12:38 14:31

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.35E6 

14:47

A8.43E6

15:10

A8.88E5

14:09

A7.64E5

14:57

A5.51E5

14:34

A4.59E5

13:21

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.61E6 

15:10

A1.36E6

14:47

A5.64E5

13:21

A4.60E5

14:09

A2.67E5

14:34

A2.23E5

15:23

A1.28E5

12:16

A7.69E

15:48

A9.02E4

14:57

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.32E7 

15:08

A1.02E7

14:45

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.45E6 

15:08

A1.80E6

14:45

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:21 12:51 13:13 13:32 13:50 14:17 14:47 15:09 15:32 15:5

12:38 14:31

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A4.54E6 

17:36

A1.78E6

17:32

A6.49E5

17:55

A6.29E5

16:59

A5.15E5

16:41

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.33E6 

17:36

A5.41E5

17:55

A7.02E5

16:50

A3.06E5

17:04

A2.33E5

16:37

A1

1

A1.22E5

17:18

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.80E7 

17:33

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A3.69E6 

17:33

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:36 16:46 16:56 17:11 17:21 17:33 17:46 17:57 18:08 18:20 18:32 18:43 18:55 

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A3.76E6 

19:43

A1.85E6

20:14

A1.03E6

19:46

A7.36E5

20:20

A2.90E5

21:30

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 

A2.03E6

19:43

A5.56E5

21:30

A4.18E5

20:14

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.55E7 

20:11

A1.72E7

19:40

A1.39E7

20:27

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A5.88E6 

20:11

A4.41E6

19:44

A3.20E6

20:27

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:33 19:49 19:58 20:10 20:17 20:28 20:36 20:45 21:03 21:20 21:32 21:

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A9.29E5 

22:47

A3.95E5

22:22

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.31E5 

22:46

A1.79E5

22:22

A6.37E4

22:26

A2.55E4

23:00

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.33E7 

22:44

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.17E6 

22:44

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:31 22:49 23:11 24:08 26:34 26:53 

22:09 23:33 24:36 25:01 25:39 26:01

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.86E5 

22:26

A1.46E5

22:13

A4.44E4

22:44

A1.22E4

23:10

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A8.81E4 

22:25

A2.97E4

22:43

A5.23E4

22:14

A6.69E3

22:48

A3.65E3

25:44

A6.40E3

23:17

A3.09E3

23:46

A3

2

A2.72E3

26:15

A2.59E3

24:58

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A9.52E6 

22:22

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.24E6 

22:22

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:31 22:49 23:11 24:08 26:34 26:53 

22:09 23:33 24:36 25:01 25:39 26:01

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A6.36E6 

15:34

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A1.23E6 

15:34

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 12:51 15:32 15:5

12:21 13:32 14:17 14:47 15:07 12:42 12:59 13:13 13:36 13:50 14:07 14:28 15:43 1

12:20 14:45 15:02 15:17

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

A1.78E6

A3.07E5

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 A1.33E6 

A8.01E5

A3.06E5 A2.46E5

A2.01E5 A2.29E5 A1.72E5

A1.22E5

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

A1.68E6

A2.40E5

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

A4.59E5

A1.75E5 A1.35E5

A7.79E4 A1.21E5 A5.37E4

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A4.54E6

A1.78E6

A6.49E5

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A1.33E6

A8.01E5

A5.41E5

A2.46E5

A2.01E5 A1.72E5 A2.29E5 A1.22E5

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A4.39E6

A1.68E6

A6.03E5

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A1.00E6

A4.59E5

A4.03E5

A1.35E5

A7.79E4 A1.21E5 A5.37E4

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20

%

0 

20 40 60 80 

100 120 140 

A3.76E6

A1.03E6

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20

%

0 

20 40 60 80 

100 120 140 

A2.03E6

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20

%

0 

20 40 60 80 

100 120 140 

A4.89E6

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20

%

0 

20 40 60 80 

100 120 140 

A2.21E6

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 

%

0 

20 40 60 80 

100 120 140 

A1.03E6

A2.16E5

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 

%

0 

20 40 60 80 

100 120 140 

A6.68E4

A3.64E4 A2.50E4 A1.01E4 A1

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 

%

0 

20 40 60 80 

100 120 140 

A1.62E5 A4.63E4 A9.36E4 A7.42E4

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 

%

0 

20 40 60 80 

100 120 140 

A1.43E5 A3.48E4 A6.28E4

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A1.85E6

A1.03E6

A7.36E5

A2.16E5 A1.11E5

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A4.18E5

A1.70E5

A6.68E4 A3.64E4 A1.78E4 A1.82E4

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A1.71E6

A5.84E5

A1.62E5

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A3.64E5

A1.15E5

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 

%

0 

20 40 60 80 

100 120 140 

A7.36E5

A2.16E5 A1.11E5

A3.93E4

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 

%

0 

20 40 60 80 

100 120 140 

A1.70E5

A6.68E4

A3.64E4

A1.78E4 A1.82E4 A1.63E4 A8.33E3

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 

%

0 

20 40 60 80 

100 120 140 

A5.84E5

A1.62E5

A3.82E4

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 

%

0 

20 40 60 80 

100 120 140 

A1.15E5

A1.84E4

A3.49E3 A4.27E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A1.11E5

A3.93E4

A1.02E4 A1.81E4

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A1.82E4

A1.78E4

A8.33E3

A5.06E3

A1.43E3

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A3.82E4

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A3.95E5

A3.44E4

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A1.79E5

A6.37E4 A8.26E4

A1.46E4 A2.26E4 A5.22E4 A3.52E4 A1.89E4

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

22:20 22:31 22:06 22:13 22:18 22:26 22:34 22:37 

22:09 22:15 22:41 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A5.03E5

A1.94E5 A1.41E5

A3.71E4 A3.81E4 A6.39E4

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A1.73E5

A9.71E4 A5.64E4

A3.52E4 A1.65E4 A3.52E4 A1.42E4

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A1.86E5

A1.46E5

A4.44E4

A2.46E4 A2.93E4 A2.11

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A8.81E4

A5.05E4 A2.97E4 A5.23E4 A6.14E4

A3.25E4 A2.24E4 A1.49E4 A2.46E4

A

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A3.27E5

A1.54E5

A1.46E5

A7.36E4

A5.51E4 A3.80E4

A2.46E4 A2.93E4 A1.61

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A8.51E4

A4.18E4 A2.48E4

A3.00E4 A4.69E4

A2.15E4 A1.61E4

A1.35E4

A

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 

A9.29E5

A3.95E5

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 

A3.31E5

A1.79E5

A6.37E4

A2.26E4 A5.22E4 A1.89E4 A1.53E4 A2.55E4 A1.59E4 

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 

A1.02E6

A5.03E5

A1.41E5

A6.39E4

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 

A2.58E5

A1.73E5

A5.64E4

A1.65E4 A3.52E4 A1.42E4

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A17 #1-2850 Acq:15-NOV-2014 21:52:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.65E6 

7:34

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,8836.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.98E5 

7:34

A5.02E4

7:08

A7.00E3

8:21

A1.37E4

8:44

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1796.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.50E5 

7:32

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,64.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.35E4 

7:32

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,740.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:11 7:23 7:36 7:48 7:58 8:11 8:20 8:28 8:37 8:47 8:57 9:05 9:13 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.60E6 

8:43

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1896.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.43E6 

8:43

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,2532.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.28E5 

8:49

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.19E5 

8:49

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:11 7:23 7:36 7:48 7:58 8:11 8:20 8:28 8:37 8:47 8:57 9:05 9:13 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.60E5 

10:27

A1.50E5

10:10

A1.20E5

9:53

A6.47E4

10:32

A6

1

A3.27E4

11:24

A1.66E4

10:58

A2.97E4

9:49

A2.73E4

10:47

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.51E4 

10:27

A3.49E4

9:53

A2.78E4

10:10

A1.24E4

11:35

A1.20E4

10:32

A8.20E3

9:48

A6.96E3

9:58

A3.32E3

10:58

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.18E6 

10:24

A2.73E5

10:08

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.03E5 

10:24

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:55 10:07 10:16 10:30 10:40 10:55 11:03 11:12 11:25 11:35 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.42E5 

10:27

A4.07E4

9:53

A2.01E4

10:04

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,324.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.55E5 

10:27

A1.19E5

9:53

A5.30E4

11:24

A7.29E4

10:04

A4.54E4

10:32

A4.30E4

10:47

A2.34E4

10:58

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,492.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.65E6 

10:24

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.81E6 

10:24

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:55 10:07 10:16 10:30 10:40 10:55 11:03 11:12 11:25 11:35 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.11E5 

11:18

A3.18E4

11:24

A1.97E4

10:27

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.88E5 

11:18

A7.05E4

10:27

A4.89E4

11:24

A3.15E

11:38

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.14E5 

11:15

A7.90E3

11:19

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.14E5 

11:15

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:55 10:07 10:16 10:30 10:40 10:55 11:03 11:12 11:25 11:35 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.76E6 

12:50

A1.00E6

12:53

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.89E5 

12:50

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.80E5 

12:48

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.53E4 

12:48

A2.55E4

12:54

A1.19E4

14:58

A3.10E3

13:45

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:20 12:35 12:59 13:18 13:43 14:03 14:24 14:46 15:02 15:20 15:42 

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.76E5 

15:09

A1.52E5

14:47

A1.88E4

13:20

A8.18E3

14:51

A8.27E3

14:09

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.75E4 

15:09

A2.84E4

14:47

A2.08E4

13:20

A7.44E3

14:33

A5.66E3

12:15

A8.78E3

14:09

A4.99E3

15:30

A2.65E3

14:53

A2.25E3

13:10

A3.11E3

12:51

A1.42E3

13:48

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.83E6 

15:07

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.51E6 

15:07

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:20 12:35 12:59 13:18 13:43 14:03 14:24 14:46 15:02 15:20 15:42 

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A3.00E5 

16:58

A5.70E4

17:36

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.22E5 

16:58

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.24E5 

17:33

A1.12E4

17:43

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A4.08E4 

17:33

A4.01E3

17:43

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:45 16:56 17:10 17:22 17:35 17:47 17:56 18:07 18:23 18:34 18:46 18:56 

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.67E4 

20:14

A1.35E4

19:44

A2.99E3

20:29

A2.26E3

21:03

A1.

21

A2.42E3

19:39

A2.18E3

21:20

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 

A2.42E3

19:43

A2.10E3

20:19

A2.06E3

21:28

A1.92E3

20:54

A1.

21

A1.83E3

21:07

A1.11E3

20:44

A1.05E3

20:01

A992.31

20:32

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A5.56E6 

20:10

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.19E6 

20:10

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:36 19:46 19:56 20:11 20:26 20:43 20:51 21:00 21:15 21:28 21:

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.05E4 

22:47

A1.91E3

25:09

A1.54E3

23:45

A1.85E3

26:46

A1.61E3

24:26

A1.23E3

26:02

A752.94

23:19

A387.62

25:24

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.89E3 

22:24

A2.35E3

22:22

A1.29E3

23:19

A1.15E3

25:23

A1.78E3

24:36

A779.08

26:52

A1.97E3

22:48

A528.98

23:49

A613.75

25:53

A301.63

23:15

A257.88

24:32

A260.26

25:14

A138.96

26:32

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A8.92E4 

22:44

A4.47E4

22:19

A8.60E3

22:31

A2.24E3

23:18

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A6.89E3 

22:43

A8.32E3

22:21

A1.75E3

24:13

A1.88E3

23:46

A1.79E3

23:10

A1.05E3

24:46

A929.50

25:13

A916.50

22:15

A660.37

26:34

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:25 22:52 23:14 23:36 24:09 24:28 24:46 25:16 25:36 26:02 26:28 26:50 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.92E3 

22:27

A2.30E3

25:11

A4.66E3

22:42

A1.97E3

26:14

A891.59

23:34

A1.31E3

26:46

A568.83

25:21

A420.40

24:42

A446.82

24:16

A296.71

23:08

A383.67

25:47

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 

A1.27E3

25:04

A1.05E3

23:36

A88

27

A1.19E3

26:06

A915.36

26:32

A795.74

25:38

A2.99E3

22:27

A1.19E3

24:21

A1.34E3

22:58

A813.91

24:58

A485.96

25:47

A511.36

22:17

A555.32

23:27

A484.25

22:47

A440.64

24:33

A255.12

26:25

A165.07

23:59

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.96E4 

22:24

A7.32E3

22:28

A1.22E3

23:00

A1.72E3

23:52

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.06E3 

22:22

A4.02E3

22:27

A1.49E3

24:31

A1.24E3

25:20

A1.11E3

26:58

A1.33E3

26:30

A1.31E3

23:46

A966.34

25:47

A1.01E3

23:02

A696.79

22:17

A272.11

24:14

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:25 22:52 23:14 23:36 24:09 24:28 24:46 25:16 25:36 26:02 26:28 26:50 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A8.10E4 

15:34

A7.71E3

15:37

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A2.00E4 

15:34

A998.23

15:42

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 12:20 14:18 15:20 

12:35 13:18 13:43 14:03 14:32 14:58 

12:59 15:12 15:49 

12:11 13:54 14:12 14:36 14:54 15:27 

12:56 13:27

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:40 9:42 9:44 9:46 9:48 9:50 9:52 9:54 9:56 9:58 10:00 10:02 10:04 10:06 10:08 10:10 10:12 10:14 10:16 10:18 10:20 10:22 10:24 10:26 10:28 10:30 

%

0 

20 40 60 80 

100 120 140 

A1.50E5

A1.20E5

A6.35E4

A2.97E4 A2.83E4

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

9:40 9:42 9:44 9:46 9:48 9:50 9:52 9:54 9:56 9:58 10:00 10:02 10:04 10:06 10:08 10:10 10:12 10:14 10:16 10:18 10:20 10:22 10:24 10:26 10:28 10:30 

%

0 

20 40 60 80 

100 120 140 

A2.78E4

A2.13E4

A2.02E4

A8.20E3 

A6.96E3

A4.01E3

A711.55

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

9:40 9:42 9:44 9:46 9:48 9:50 9:52 9:54 9:56 9:58 10:00 10:02 10:04 10:06 10:08 10:10 10:12 10:14 10:16 10:18 10:20 10:22 10:24 10:26 10:28 10:30 

%

0 

20 40 60 80 

100 120 140 

A1.54E5

A1.20E5

A6.33E4

A6.99E4

A2.95E4 A2.81E4 A1.36E4

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

9:40 9:42 9:44 9:46 9:48 9:50 9:52 9:54 9:56 9:58 10:00 10:02 10:04 10:06 10:08 10:10 10:12 10:14 10:16 10:18 10:20 10:22 10:24 10:26 10:28 10:30 

%

0 

20 40 60 80 

100 120 140 

A3.00E4

A2.22E4

A2.24E4

A8.93E3 

A8.12E3 A5.46E3

A1.66E3

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:20 12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 

%

0 

20 40 60 80 

100 120 140 

A4.76E6

A1.00E6

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

12:20 12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 

%

0 

20 40 60 80 

100 120 140 

A4.89E5

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

12:20 12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 

%

0 

20 40 60 80 

100 120 140 

12:20 12:35 12:41 12:43 12:46 12:59 13:07 

12:24 12:28 12:31 12:37 12:50 12:52 13:02 13:04 

12:56

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

12:20 12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 

%

0 

20 40 60 80 

100 120 140 

A5.51E6

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

12:20 12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 

%

0 

20 40 60 80 

100 120 140 

A4.82E5

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13

%

0 

20 40 60 80 

100 120 140 

A1.00E6

A1.51E5 A1.50E5

A3.60E4 A4.21E4 

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13

%

0 

20 40 60 80 

100 120 140 

A1.19E4 A1.66E4

A3.84E3 A4.09E3 A2.52E3 A3.22E3 A5

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13

%

0 

20 40 60 80 

100 120 140 

A9.92E4

A4.10E4 A3.46E4 A6.48E4

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13

%

0 

20 40 60 80 

100 120 140 

A9.86E3 A1.14E4

A4.91E3 A3.67E3 A5.23E3 A2.47E3 A1.28E3 A3

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17

%

0 

20 40 60 80 

100 120 140 

A1.41E4

A4.87E3

A6.52E3 A7.16

A4.74E3 A3.77E3 A3.59E3 A5.30E3 A1.53E3

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17

%

0 

20 40 60 80 

100 120 140 A1.22E4 

A4.42E3 A2.98E3

A2.84E3

A2.47E3 A4.26E3

A1.95E3 A1.55E3

A2.41E3 A1.65E3 A3.40E3 A1.44E3 A1.13E3

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17

%

0 

20 40 60 80 

100 120 140 

17:08 17:10 17:14 17:17 17:19 17:22 17:26 17:28 17:35 17:40 17:42 17:44 17:47 17:52 

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17

%

0 

20 40 60 80 

100 120 140 

A3.29E3

A2.62

A2.46E3

A556.36 A552.25

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17

%

0 

20 40 60 80 

100 120 140 

A734.23

A328.14 A580.67

A185.07

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A5.70E4

A1.41E4

A4.87E3

A6.52E3 A7.16E3

A4.74E3 A3.77E3 A3.59E3 A5.30E3 A1.53E3

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A1.22E4

A4.42E3

A2.84E3

A2.47E3 A4.26E3

A1.95E3 A1.55E3

A2.41E3 A1.65E3 A3.40E3 A1.44E3 A1.13E3

A526.5

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A5.45E4

A3.29E3

A2.62E3 A2.46E3

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A3.90E3 A4.31E3

A899.54

A734.23

A328.14 A580.67

A185.07

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A1.35E4

A1.62E4

A1.04E3 A2.42E3 A1.77E3 A2.76E3 A2.37E3

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A2.42E3

A1.53E3

A2.75E3

A2.02E3 A1.09E3 

A891.39 A1.05E3 A1.09E3 A570.37 A789.10 A812.32 A916.82

A248.57 A287.14

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

19:23 19:30 19:36 19:38 19:40 19:44 19:46 19:49 19:53 19:56 19:59 

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A1.26E4

A1.40E4

A3.62E3 A3.19E3 A1.63E3 A2.05E3 A1.50E3 A861.41 A324.28

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A4.06E3

A3.18E3

A1.88E3 A1.94E3

A1.60E3 A1.76E3 A1.18E3

A886.22 

A1.22E3 A627.06

A761.36 

A314.61 A285.25 A222.19

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 

%

0 

20 40 60 80 

100 120 140 

A1.35E4

A1.62E4

A1.04E3 A2.42E3 A1.77E3 A1.19E3 A2.76E3 A2.37E3

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 

%

0 

20 40 60 80 

100 120 140 

A1.53E3 

A2.75E3

A2.02E3

A1.09E3

A1.05E3 A891.39 A1.09E3

A570.37

A789.10 A812.32

A916.82

A248.57

A287.14

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 

%

0 

20 40 60 80 

100 120 140 

A1.26E4

A1.40E4

A3.62E3

A3.19E3 A1.63E3

A2.05E3 A1.50E3 A861.41

A324.28 A306.01

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 

%

0 

20 40 60 80 

100 120 140 

A3.18E3

A1.88E3

A1.94E3

A1.60E3 A1.76E3

A1.18E3

A886.22 

A1.22E3 

A627.06

A761.36 

A314.61 A285.25

A222.19

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A1.67E4

A1.62E4 A1.44E4

A2.99E3

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A2.17E3

A1.85E3

A2.02E3 A1.76E3

A1.09E3 A1.23E3

A1.62E3

A1.05E3 A876.28

A646.38 A992.31

A570.37 A770

A789.10 A812.32

A248.57 

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A1.15E4

A1.40E4

A6.99E3

A2.78E3

A1.76E3

A861.41 A641.79

A306.01 A324.28

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A981.68 A886.22

A830.18 A845.77

A463.08

A314.61 A285.25

A222.19

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 

%

0 

20 40 60 80 

100 120 140 

A1.44E4

A2.99E3

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 

%

0 

20 40 60 80 

100 120 140 

A1.62E3

A1.05E3 A876.28

A646.38 A992.31

A770.97 A789.10

A812.32 

A992.35

A248.57

A

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 

%

0 

20 40 60 80 

100 120 140 

A6.99E3

A2.78E3

A1.76E3

A861.41 A641.79

A324.28

A306.01

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 

%

0 

20 40 60 80 

100 120 140 

A314.61 A285.25

A222.19

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20

%

0 

20 40 60 80 

100 120 140 A2.99E3 

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20

%

0 

20 40 60 80 

100 120 140 A3.98E3 

A2.17E3

A1.85E3

A1.76E3

A1.23E3

A1.62E3 A1.11E3

A1.05E3 A876.28

A646.38 A992.31 

A770.97

A812.32 A644.33

A992.35

A209.54

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20

%

0 

20 40 60 80 

100 120 140 A1.76E3 

A641.79

A324.28

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20

%

0 

20 40 60 80 

100 120 140 

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A8.34E3

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A2.35E3

A2.35E3

A2.32E3 A1.80E3

A998.96

A1.08E3 A868.82 A2.11E3

A1.70E3 A988.33

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A8.89E3 

A4.27E3

A4.29E3 A3.18E3

A2.14E3

A1.50E3

A1.45E3 A2.05E3

A973.29 A749.95 A814.83

A892

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A2.29E3

A2.24E3

A2.32E3

A1.49E3

A1.70E3 A981.69 A762.96 

A609.22 A1.08E3

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A5.92E3

A4.66E3

A1.51E3 A1.54

A811.33 A1.17E3 

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A1.91E3

A2.99E3 A1.07E3 

A1.12E3 A892.85

A511.36 A546.07 A793.02 A579.37

A513.06 A484.

A599.99 

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

22:09 22:12 22:15 22:20 22:25 22:32 22:36 22:39 22:42 

22:28 22:45 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A8.21E3

A2.12E3

A2.64E3 A3.89E3 A1.51E3 A1.37E3 A1.33E3 A1.21

A812.37

A875.00 A833.82 A922.18 

A784.38 A345.14 

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 A1.28E3 

A1.92E3 A695.62 

A616.60 A520.16

A301.54 A367.99 A286.61 A254.

A209.70 A207.66

A113.03

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 

A1.05E4

A8.34E3

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 A1.97E3 

A998.96 A91

A2.11E3

A1.08E3 A868.82

A753.00

A545.79

A375.33

A259.77 A350.33

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 

A8.89E3 A9.85E3

A4.27E3

A3.18E3

A2.14E3

A1.50E3

A2.05E3

A749.95 A987.42 A1.18E3 A645.29

A892.90 A366.81 A572.62

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A18 #1-2850 Acq:15-NOV-2014 22:27:09 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-3 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.72E6 

7:35

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,4348.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.99E5 

7:35

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,932.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.93E5 

7:33

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,292.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.65E4 

7:33

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,492.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:11 7:18 7:29 7:40 7:48 7:57 8:05 8:18 8:30 8:39 8:52 9:04 9:13 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.32E5 

8:44

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,624.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.23E5 

8:44

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1032.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.08E5 

8:41

A3.54E4

8:46

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.89E5 

8:41

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:11 7:18 7:29 7:40 7:48 7:57 8:05 8:18 8:30 8:39 8:52 9:04 9:13 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.87E5 

10:10

A6.92E4

10:27

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.00E5 

10:10

A1.54E4

10:28

A1.32E4

10:14

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.61E5 

10:09

A3.82E5

10:24

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.38E4 

10:09

A7.06E4

10:24

A5.73E3

10:30

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:49 10:01 10:11 10:18 10:27 10:34 10:43 10:53 11:00 11:09 11:19 11:26 11:35 1

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.44E4 

10:27

A2.13E4

10:01

A1.72E4

9:49

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.77E4 

10:27

A2.66E4

10:10

A1.11E4

9:50

A1.69E3

10:00

A2.86E3

10:30

A3.50E3

11:24

A7.05E3

10:50

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,336.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.93E5 

10:24

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.36E5 

10:24

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:49 10:01 10:11 10:18 10:27 10:34 10:43 10:53 11:00 11:09 11:19 11:26 11:35 1

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.97E4 

11:18

A5.48E3

11:29

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.02E5 

11:18

A1.44E4

9:52

A5.46E3

10:49

A7.31E3

11:25

A9.02E3

10:33

A9.42E3

10:14

A6.56

11:3

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.33E3 

11:15

A202.66

11:24

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.08E3 

11:16

A3

1

A372.75

10:47

A292.17

10:11

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:49 10:01 10:11 10:18 10:27 10:34 10:43 10:53 11:00 11:09 11:19 11:26 11:35 1

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.79E6 

12:50

A9.89E5

12:55

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.33E5 

12:50

A8.64E4

12:55

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.11E6 

12:48

A1.52E5

12:59

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.67E4 

12:48

A3.06E4

12:54

A7.09E3

13:07

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:20 12:47 13:07 13:24 13:41 13:58 14:28 14:53 15:18 15:33 15

12:17 12:33 14:12 15

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A6.40E6 

14:47

A5.02E6

15:10

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.08E6 

14:47

A8.94E5

15:10

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.40E5 

15:08

A5.68E5

14:45

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.66E5 

15:08

A7.81E4

14:45

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:20 12:47 13:07 13:24 13:41 13:58 14:28 14:53 15:18 15:33 15

12:17 12:33 14:12 15

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.07E6 

17:36

A2.49E5

17:32

A2.25E5

16:59

A1.29E5

17:06

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.28E5 

17:36

A9.78E4

16:59

A5.62E4

17:32

A2.40E4

17:06

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.02E6 

17:33

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.69E5 

17:33

A2.80E4

17:38

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:38 16:50 17:01 17:14 17:33 17:50 18:03 18:16 18:29 18:41 18:52 19:02 

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.39E5 

19:44

A8.82E4

20:14

A8.47E4

19:46

A3.68E4

20:21

A1.28E4

20:31

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A3.57E4 

19:44

A1.42E4

19:47

A2.11E4

20:15

A4.00E3

19:50

A2.86E3

20:18

A1.57E3

21:20

A1.14E3

20:33

A1.35E3

19:39

A853.62

21:10

A998.50

20:07

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.10E6 

20:11

A6.13E5

20:27

A8.00E5

19:45

A6.44E4

20:32

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.54E5 

20:11

A1.12E5

19:41

A1.25E5

20:27

A1.07E4

19:52

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:33 19:43 19:52 20:04 20:16 20:26 20:34 20:46 20:55 21:11 21:26 21:37 

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A6.79E3 

22:22

A879

27:

A1.40E3

26:38

A719.82

26:04

A555.93

25:07

A431.45

24:24

A778.17

23:17

A259.18

25:36

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A6.45E3 

22:34

A2.47E3

24:39

A3.63E3

23:17

A1.82E3

25:26

A1.93E3

23:57

A3.67E3

22:22

A1.4

27

A1.69E3

26:24

A1.09E3

22:48

A763.75

25:40

A434.97

25:05

A288.06

23:36

A540.67

22:12

A246.23

24:31

A174.95

24:05

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.49E5 

22:44

A3.90E5

22:20

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.08E5 

22:44

A8.46E4

22:19

A9.93E3

22:50

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:18 22:46 23:12 23:44 24:20 24:46 25:15 25:41 26:03 26:40 26:59 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.02E3 

22:28

A882.65

26:54

A762.66

24:17

A950.85

25:46

A691.12

22:24

A522.60

25:13

A684.06

22:53

A766.67

24:44

A481.29

23:38

A344.10

26:51

A284.74

26:13

A147.22

24:16

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 

A961.80

23:21

A936.58

26:38

A1.52E3

25:06

A923.15

23:57

A690.61

25:33

A628.02

26:13

A690.65

22:12

A643.83

24:35

A468.38

22:38

A417

27:0

A670.59

23:03

A261.97

23:54

A337.32

25:13

A249.13

25:58

A480.87

24:44

A211.86

24:19

A229.43

22:17

A1

2

A108.78

22:47

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.53E5 

22:24

A3.28E4

22:30

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.54E4 

22:24

A1.54E4

22:27

A1.91E3

22:48

A

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:18 22:46 23:12 23:44 24:20 24:46 25:15 25:41 26:03 26:40 26:59 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A397.39 

15:34

A35.73

15:36

A56.08

12:13

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A92.62 

12:05

A28.20

12:13

A74.15

12:29

A

A18.36

15:27

A31.14

15:44

A12.16

12:39

A9.7615:04

A15.67

14:48

A4.3114:26

A2.7312:46

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 12:20 12:47 13:07 13:58 14:53 15:18 15:33 15

12:14 12:30 13:10 13:24 13:41 14:05 14:28 15:09 1

12:53 14:39 15:27 12:33 13:29 13:44 14:12 15

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:58 10:00 10:02 10:04 10:06 10:08 10:10 10:12 10:14 10:16 10:18 10:20 10:22 10:24 10:26 10:28 10:30 10:32 10:34 10:36 10:38 10:40 10:42 10:44 10:46 10

%

0 

20 40 60 80 

100 120 140 

A5.44E4

A2.13E4

A5.06E3

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

9:58 10:00 10:02 10:04 10:06 10:08 10:10 10:12 10:14 10:16 10:18 10:20 10:22 10:24 10:26 10:28 10:30 10:32 10:34 10:36 10:38 10:40 10:42 10:44 10:46 10

%

0 

20 40 60 80 

100 120 140 

A6.77E4

A2.66E4

A1.69E3 A857.61 A2.86E3 

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,336.0,3.00%,F,T) 

after_modification

9:58 10:00 10:02 10:04 10:06 10:08 10:10 10:12 10:14 10:16 10:18 10:20 10:22 10:24 10:26 10:28 10:30 10:32 10:34 10:36 10:38 10:40 10:42 10:44 10:46 10

%

0 

20 40 60 80 

100 120 140 

10:01 10:04 10:06 10:11 10:13 10:18 10:22 10:27 10:32 10:34 10:37 10:40 10:43 10:46 1

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

9:58 10:00 10:02 10:04 10:06 10:08 10:10 10:12 10:14 10:16 10:18 10:20 10:22 10:24 10:26 10:28 10:30 10:32 10:34 10:36 10:38 10:40 10:42 10:44 10:46 10

%

0 

20 40 60 80 

100 120 140 

A5.12E4

A1.53E4

A2.25E3 A1.80E3

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,292.0,3.00%,F,T) 

before_modification

9:58 10:00 10:02 10:04 10:06 10:08 10:10 10:12 10:14 10:16 10:18 10:20 10:22 10:24 10:26 10:28 10:30 10:32 10:34 10:36 10:38 10:40 10:42 10:44 10:46 10

%

0 

20 40 60 80 

100 120 140 

A6.81E4

A2.63E4

A3.76E3 A3.25E3 

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,328.0,3.00%,F,T) 

before_modification

File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
10:48 10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 

%

0 

20 40 60 80 

100 120 140 

A8.97E4

A5.48E3 A5.72E3

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

10:48 10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 

%

0 

20 40 60 80 

100 120 140 

A1.02E5

A5.46E3 A7.31E3 A4.38E3 A7.05E3 A

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

10:48 10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 

%

0 

20 40 60 80 

100 120 140 

A1.01E5

A2.78E3 A7.44E3 A7.40E3 A2.97E3 

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

10:48 10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 

%

0 

20 40 60 80 

100 120 140 

A1.06E5

A5.88E3 A8.74E3 A5.65E3 A8.65E3 A2.12E3 A

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:20 12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 

%

0 

20 40 60 80 

100 120 140 

A4.79E6

A9.89E5

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg1411116mb

after_modification

12:20 12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 

%

0 

20 40 60 80 

100 120 140 

A4.33E5

A8.64E4

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

12:20 12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 

%

0 

20 40 60 80 

100 120 140 

12:29 12:47 13:07 12:25 12:30 12:39 12:43 12:50 12:53 12:57 13:01 13:1

12:33 13:04

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

12:20 12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 

%

0 

20 40 60 80 

100 120 140 

A4.75E6

A1.01E6

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

12:20 12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 

%

0 

20 40 60 80 

100 120 140 

A4.27E5

A8.05E4

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13

%

0 

20 40 60 80 

100 120 140 

A9.89E5

A3.63E5

A1.20E5 A

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13

%

0 

20 40 60 80 

100 120 140 

A8.64E4

A1.46E4 A1.12E4

A1.12E4 A8.25E3

A2.50E3 A4.11E3

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13

%

0 

20 40 60 80 

100 120 140 

A1.01E6

A3.09E5

A8.33E4

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13

%

0 

20 40 60 80 

100 120 140 

A8.05E4

A1.18E4 A8.76E3

A6.79E3 A4.55E3 

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

A2.49E5

A1.29E5

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

A5.62E4

A2.40E4 A2.04E4

A7.59E3

A2.87E3 A6.37E3 A

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

17:14 17:33 17:46 17:50 

17:03 17:07 17:10 17:12 17:20 17:23 17:26 17:29 17:35 17:38 17:42

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

A2.48E5

A1.23E5

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

A5.16E4

A2.08E4 A2.22E4

A4.60E3

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A1.07E6

A2.49E5

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A2.28E5

A5.62E4

A2.04E4

A7.59E3

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A1.15E6

A2.48E5

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A2.15E5

A5.16E4

A2.22E4

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A1.39E5

A8.47E4

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A3.57E4

A1.42E4

A4.00E3

A1.30E3 A1.35E3 A3.26E3 A1.84E3 A732.0

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

19:25 19:27 19:30 19:33 19:39 19:43 19:50 19:52 19:56 19:58 20:04 

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A2.35E5

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A3.37E4

A1.85E4

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 

%

0 

20 40 60 80 

100 120 140 

A8.47E4

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 

%

0 

20 40 60 80 

100 120 140 

A1.42E4

A4.00E3

A3.26E3

A1.84E3

A1.30E3 A1.47E3 A1.35E3 A732.00 

A816.50 A859.00 A608.37

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 

%

0 

20 40 60 80 

100 120 140 

A4.90E3

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 

%

0 

20 40 60 80 

100 120 140 

A1.85E4

A1.23E3 A1.43E3 A837.79 A802.72 A720.84

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A8.82E4

A8.47E4

A3.68E4

A1.28E4

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A1.42E4

A2.11E4

A4.00E3 A4.84E3

A3.26E3 A2.86E3

A1.84E3 A1.66E3

A980.00 A1.78E3 A1.14E3 A859.00 A2.10E3 A828.00 A1.15E3 

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A7.95E4

A3.18E4

A4.90E3 A6.23E3

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A1.85E4

A1.58E4

A4.50E3

A720.84 A797.14

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A3.68E4

A1.28E4

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A4.84E3

A3.43E3

A2.86E3

A1.84E3 A1.66E3

A1.78E3 A1.14E3 A980.00

A859.00

A2.10E3 A828.00 A1.15E3 A795.23 A1.20

A1.08E3

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A3.18E4

A4.90E3 A6.23E3

A2.83E3

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A4.50E3

A720.84 A797.14

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

A1.28E4

A1.83E3

A

A1.16E3 

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 A1.14E3 

A1.78E3

A980.00

A732.00 A998.50 A1.15E3

A828.00 A795.23 A1.20E3 A647.22 A895.35 

A776.44 

A1.08E3

A586.24 A38

A242.65

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

A6.23E3

A2.83E3

A457.44

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

A797.14

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A6.79E3

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A3.67E3 

A1.

A1.76E3 A900.83

A661.37

A538.53

A540.67 A493.65 A426.58

A158.83 A234.55 

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A9.67E3

A5.33E3

A2.08E3

A1.26E3 A1.67E3

A1.30E3 A621.05

A382.67 A711.07 A361.02

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A3.50E3

A1.

A1.76E3 A900.83

A695.30

A540.67 A465.62 A529.65

A158.83 A270.53

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 

%

0 

20 40 60 80 

100 120 140 

A3.02E3

A691.12 

A562.67 A559.81 

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 

%

0 

20 40 60 80 

100 120 140 

A690.65 A1.22E3

A577.91 A468.38 A518.98

A771.57 A523.97

A271.53

A229.43 A

A108.78

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 

%

0 

20 40 60 80 

100 120 140 

22:12 22:18 22:21 22:26 22:33 22:36 22:46 

22:08 22:38 22:42 22:44

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 

%

0 

20 40 60 80 

100 120 140 

A4.09E3

A1.84E3

A1.28E3

A880.00 A1.40E3

A562.99 A1.05E3 A688.93 

A408.50 A372.32 

A274.33 A134.83

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 

%

0 

20 40 60 80 

100 120 140 

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 

A6.79E3

A9.46E3

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 

A1.09E3

A775.31

A661.37 A669.10 A592.12

A538.53

A559.98 A368.66

A426.58

A250.57 A226.45 A234.55

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 A9.67E3 

A6.49E3

A5.33E3

A1.67E3 A1.67E3

A621.05

A427.54 A752.01 A381.49 A361.02

A163.16

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 A884.71 

A695.30 A536.71

A393.50 A465.62 A310.73

A394.31

A270.53

A129.06 A105.65

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A19 #1-2850 Acq:15-NOV-2014 23:01:22 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.62E6 

7:35

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.72E5 

7:35

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,700.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.12E6 

7:33

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,260.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.91E4 

7:33

A1.97E4

7:36

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,116.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:11 7:18 7:28 7:41 7:50 7:59 8:13 8:25 8:34 8:45 8:54 9:02 9:09 9:16 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.19E5 

8:44

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,424.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.09E5 

8:44

A2.65E3

8:59

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,688.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.64E5 

8:41

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.40E5 

8:41

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:11 7:18 7:28 7:41 7:50 7:59 8:13 8:25 8:34 8:45 8:54 9:02 9:09 9:16 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.82E5 

10:10

A3.94E4

10:28

A3.37E4

10:15

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.59E4 

10:10

A1.22E4

10:28

A4.97E3

10:15

A6.41E3

9:46

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.18E5 

10:09

A3.72E5

10:25

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.07E5 

10:09

A5.32E4

10:25

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:47 9:59 10:12 10:23 10:34 10:45 10:56 11:08 11:17 11:27 11:34 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.28E4 

10:28

A9.35E3

10:00

A7.63E3

9:47

A479.40

10:11

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.13E4 

10:28

A2.17E4

10:10

A7.68E3

9:50

A2.60E3

10:00

A4.42E3

10:15

A2.45E3

11:35

A2.84E3

10:41

A1.93E3

11:24

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,288.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.37E5 

10:25

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.92E5 

10:25

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:47 9:59 10:12 10:23 10:34 10:45 10:56 11:08 11:17 11:27 11:34 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.79E4 

11:18

A4.52E3

10:37

A2.09E3

11:04

A5.09E

11:39

A3.20E3

10:49

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.94E4 

11:18

A1.43E4

9:52

A5.36E3

10:50

A7.65E3

10:14

A7.60E3

11:34

A

A3.31E3

10:38

A3.13E3

10:28

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A402.29 

11:17

A38.98

10:17

A201.98

9:46

A30.18

10:55

A16.28

10:26

A16.76

11:20

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A124.05 

11:15

A66.79

9:54

A93.52

10:06

A49.76

10:26

A39.03

10:43

A19

11

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:47 9:59 10:12 10:23 10:34 10:45 10:56 11:08 11:17 11:27 11:34 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.29E6 

12:51

A8.24E5

12:55

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.87E5 

12:51

A7.62E4

12:56

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.23E6 

12:49

A1.81E5

13:00

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.64E4 

12:48

A5.42E4

12:54

A7.90E3

12:58

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:08 12:25 12:45 13:02 13:18 13:45 14:00 14:20 14:48 15:12 15:33 15:5

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.43E6 

14:47

A7.17E6

15:10

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.46E6 

14:47

A1.24E6

15:10

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A7.66E5 

15:08

A7.02E5

14:46

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.35E5 

15:08

A9.47E4

14:46

A7.93E3

15:15

A1.05E4

14:49

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:08 12:25 12:45 13:02 13:18 13:45 14:00 14:20 14:48 15:12 15:33 15:5

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A3.35E6 

17:36

A5.17E5

17:33

A2.14E5

16:59

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A6.81E5 

17:36

A1.20E5

17:33

A9.25E4

16:59

A7.24E4

17:12

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.12E6 

17:33

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.99E5 

17:33

A9.55E3

17:41

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:38 16:56 17:07 17:16 17:27 17:46 17:58 18:11 18:28 18:47 18:59 

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A4.62E5 

19:44

A2.24E5

20:15

A2.14E5

19:47

A1.08E5

20:21

A3.80E4

19:55

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.60E5 

19:44

A5.09E4

20:15

A1.96E4

20:21

A4.63E3

19:55

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A8.98E5 

20:11

A4.97E5

19:41

A6.32E5

20:27

A2.64E4

20:34

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.54E5 

20:11

A1.14E5

19:40

A9.01E4

20:27

A2.24E4

20:15

A1.05E4

19:50

A1.36E4

20:36

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:37 19:46 19:53 20:01 20:10 20:21 20:34 20:41 20:51 21:02 21:16 21:26 21:35 

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.64E4 

22:47

A1.95E3

22:29

A2.78E3

22:55

A1.39E3

25:59

A684.87

26:48

A626.37

24:20

A561.06

23:36

A445.87

24:46

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A6.71E3 

22:48

A3.70E3

22:23

A2.65E3

22:55

A1.36E3

22:13

A882.69

26:44

A604.97

26:17

A588.73

23:30

A736.61

25:38

A638.01

25:09

A297.08

24:21

A261.98

23:01

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.99E5 

22:44

A4.24E5

22:20

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.17E5 

22:44

A1.01E5

22:20

A1.23E4

22:49

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:10 22:32 22:56 23:26 23:53 24:17 24:47 25:15 25:39 25:58 26:18 26:45 27:03 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.58E3 

22:27

A1.02E3

26:17

A946.36

25:45

A654.08

24:09

A922.

27:0

A686.63

23:39

A303.02

24:43

A451.03

25:18

A471.02

23:07

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 

A1.26E3

26:45

A1.04E3

24:21

A902.66

24:47

A1.03E3

25:35

A1.00E3

22:28

A586.16

23:48

A492.28

26:05

A372.60

26:43

A467.96

23:22

A178.79

24:33

A174.96

22:15

A137.42

23:55

A47.66

25:25

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.75E5 

22:23

A4.05E4

22:32

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.60E4 

22:23

A1.18E4

22:29

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:10 22:32 22:56 23:26 23:53 24:17 24:47 25:15 25:39 25:58 26:18 26:45 27:03 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A1.57E3 

15:36

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A52.49 

12:04

A30.60

12:12

A30.24

12:19

A38

15

A23.07

12:32

A38.65

15:19

A36.59

15:01

A17.64

14:46

A4.4014:28

A5.5512:43

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 13:02 13:45 14:48 15:33 15:5

12:25 12:45 13:18 14:00 14:20 15:12 

12:08 12:30 12:47 13:33 14:04 14:35 14:52 15:08 15:30 15:49

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13

%

0 

20 40 60 80 

100 120 140 

A4.29E6

A8.24E5

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13

%

0 

20 40 60 80 

100 120 140 

A3.87E5

A7.62E4

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13

%

0 

20 40 60 80 

100 120 140 

13:02 12:25 12:41 12:45 12:52 13:07 13

12:30 12:33 12:36 12:39 12:47 12:56 

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13

%

0 

20 40 60 80 

100 120 140 

A5.11E6

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13

%

0 

20 40 60 80 

100 120 140 

A3.84E5

A7.26E4

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13

%

0 

20 40 60 80 

100 120 140 

A8.24E5

A5.10E4 A3.01E

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13

%

0 

20 40 60 80 

100 120 140 

A7.62E4

A1.61E4

A1.32E4

A3.67E3 A3.84E3 A4.

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13

%

0 

20 40 60 80 

100 120 140 

A4.62E4 A2.64E

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13

%

0 

20 40 60 80 

100 120 140 

A7.26E4

A1.40E4

A1.02E4

A2.50E3 A2.31E3 A2.

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A4.62E5

A2.14E5

A3.80E4

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A1.60E5

A4.63E3

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

19:24 19:26 19:30 19:33 19:37 19:39 19:42 19:46 19:48 19:51 19:53 19:56 19:59 20:01 

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A7.12E5

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A1.52E5

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A2.14E5

A3.80E4 A1.72E4

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A4.63E3

A4.81E3 A2.48E3 A3.50E3 A2.97E3 A2.49E3 A1.38E3 

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A2.76E4

A1.15E4

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A4.07E3 A8.82E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A2.24E5

A2.14E5

A1.08E5

A3.80E4

A1.72E4 A1.11E4

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A5.09E4

A1.96E4

A5.43E3 A4.63E3

A2.48E3 A4.81E3 A5.38E3 A2.49E3 A1.38E3 A2.34E3 A2.30E3 A1.30E3 

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A2.18E5

A1.01E5

A2.76E4

A1.15E4 A1.28E4

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A4.70E4

A1.30E4

A4.07E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A1.08E5

A3.80E4

A1.72E4 A1.11E4

A6.22E3 A4.09E3 

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A1.96E4

A5.43E3

A4.63E3

A4.81E3 A5.38E3 A2.48E3

A1.38E3 A2.30E3 A2.49E3 A1.18E3 A2.34E3 A1.30E3 A2.33E3 A1.

A591.84 

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A1.01E5

A2.76E4

A1.15E4 A1.28E4

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A1.30E4

A4.07E3

A1.42E3 A856.21 A446.07

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A1.11E4

A6.22E3 A4.09E3

A3.39E3

A2.57E3

A3.04E3 A2.57E

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A4.81E3

A5.38E3

A1.38E3 A2.30E3

A1.44E3

A2.34E3 A2.33E3 A1.19E3

A1.30E3 A1.04E3 A1.18E3 A1.05E3

A1.21E3

A599.86

A591.84

A54

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A1.28E4

A2.24E3

A813.74

A531.74 A323.07

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 A1.42E3 

A856.21

A294.12

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A2.22E4

A1.95E3

A1.44E3 A1.62E3

A1.18E3 A2.18E3 A889.24

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A3.70E3

A2.64E3

A1.36E3

A448.06

A527.74 A489.43 A407.24

A439.33 A279.06 A303.91 A244.17

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A2.20E4

A1.80E3

A1.62E3 A1.31E3 A

A717.50 A1.52E3 A889.24

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A3.65E3

A2.58E3

A1.36E3

A412.23 A522.70 A477.54 A362.45

A439.34 A238.76 A244.17 A206.02

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A4.58E3

A847.21

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 A394.36 

A230.13

A162.23

A174.96

A133.28 A103.70

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

2

22:06 22:10 22:14 22:22 22:29 22:32 22:35 22:38 22:44 

22:18 22:26 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A5.51E3

A2.97E3 A2.06E3 A1.52E3

A1.70E3

A1.50E3

A1.01E3 A731.47 A500.70 

A847.12 A396.83 

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A552.87

A316.97

A212.47

A252.09 A190.29

A117.53 A205.39

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 

%

0 

20 40 60 80 

100 120 140 A2.64E4 

A2.22E4

A1.95E3 A2.78E3 A1.62E3 

A2.18E3 A1.01E3 A611.94 

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 

%

0 

20 40 60 80 

100 120 140 

A3.70E3

A2.64E3

A2.65E3

A448.06 A489.43 A407.24

A

A279.06 A303.91 A129.23 A261.98

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 

%

0 

20 40 60 80 

100 120 140 A2.51E4 

A2.20E4

A1.80E3

A1.31E3 A1.36E3 A2.06E3 A1.52E3 

A579.91

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 

%

0 

20 40 60 80 

100 120 140 

A3.65E3

A2.58E3

A1.88E3

A477.54 A412.23 A362.45 A402.13 

A238.76 A206.02 A

A53.49 A113.83

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A20 #1-2850 Acq:15-NOV-2014 23:35:39 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.44E6 

7:35

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,3996.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.58E5 

7:35

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,776.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.07E6 

7:33

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,140.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.20E4 

7:33

A6.37E3

8:41

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,464.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:14 7:23 7:29 7:41 7:52 8:02 8:10 8:24 8:33 8:41 8:51 9:01 9:10 9:

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A21 #1-2851 Acq:16-NOV-2014 00:09:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.04E5 

8:44

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,428.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.28E4 

8:44

A4.01E3

8:50

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,700.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.23E5 

8:41

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.07E5 

8:41

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:14 7:23 7:29 7:41 7:52 8:02 8:10 8:24 8:33 8:41 8:51 9:01 9:10 9:

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A21 #1-2851 Acq:16-NOV-2014 00:09:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.77E5 

10:11

A3.80E4

10:28

A2.31E4

10:15

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.88E4 

10:11

A1.01E4

10:28

A7.15E3

10:15

A5.34E3

9:47

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.20E5 

10:10

A3.82E5

10:25

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.16E5 

10:10

A4.47E4

10:25

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:51 10:00 10:14 10:24 10:32 10:45 10:53 11:06 11:22 11:30 11:39 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A21 #1-2851 Acq:16-NOV-2014 00:09:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.91E4 

10:28

A1.33E4

9:48

A9.15E3

10:05

A3.97E3

10:18

A1.64E3

10:31

A2.69E

11:38

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,192.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.67E4 

10:28

A1.86E4

10:11

A3.25E3

9:53

A2.32E3

11:26

A2.70E3

10:32

A3.15E3

10:15

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,280.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.31E5 

10:25

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.38E5 

10:25

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:51 10:00 10:14 10:24 10:32 10:45 10:53 11:06 11:22 11:30 11:39 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A21 #1-2851 Acq:16-NOV-2014 00:09:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.45E4 

11:19

A6.19E3

9:52

A2.74E3

11:25

A2.35E3

10:49

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.95E4 

11:19

A1.13E4

9:53

A9.51E3

11:34

A8.62E3

11:23

A7.65E3

10:50

A6.72E3

10:15

A3

1

A3.38E3

10:28

A5.79E3

10:38

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A897.51 

11:16

A17.70

9:59

A96.59

9:50

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A790.17 

11:24

A436.77

11:16

A88.41

9:47

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:51 10:00 10:14 10:24 10:32 10:45 10:53 11:06 11:22 11:30 11:39 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A21 #1-2851 Acq:16-NOV-2014 00:09:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.01E6 

12:51

A9.18E5

12:55

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.07E5 

12:51

A2.97E4

12:58

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.17E6 

12:49

A1.13E6

12:54

A2.33E5

13:01

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.11E5 

12:49

A5.60E4

12:54

A1.00E4

13:05

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:13 12:42 13:03 13:28 13:49 14:14 14:31 14:52 15:10 15:39 

12:27 15:24

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A21 #1-2851 Acq:16-NOV-2014 00:09:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A6.85E6 

14:48

A5.73E6

15:10

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.19E6 

14:48

A9.97E5

15:10

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.32E5 

15:08

A6.92E5

14:46

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.24E5 

15:08

A9.03E4

14:46

A1.02E4

14:49

A8.42E3

15:14

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:13 12:42 13:03 13:28 13:49 14:14 14:31 14:52 15:10 15:39 

12:27 15:24

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A21 #1-2851 Acq:16-NOV-2014 00:09:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A3.87E6 

17:37

A6.71E5

17:33

A1.99E5

16:59

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A7.45E5 

17:37

A1.84E5

17:33

A8.19E4

16:59

A7.15E4

17:12

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.01E6 

17:34

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.85E5 

17:34

A9.11E3

17:40

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:36 16:49 17:00 17:10 17:23 17:34 17:45 18:03 18:18 18:28 18:42 18:52 19:

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A21 #1-2851 Acq:16-NOV-2014 00:09:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A7.15E5 

19:44

A3.84E5

20:15

A3.51E5

19:47

A1.90E5

20:21

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.23E5 

19:44

A8.55E4

20:15

A4.44E4

20:21

A1.42E4

19:51

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A9.54E5 

20:12

A4.85E5

19:41

A6.38E5

20:28

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.23E5 

20:12

A1.32E5

19:45

A1.18E5

20:19

A1.97E4

19:48

A1.62E4

20:31

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:34 19:44 19:53 20:08 20:19 20:31 20:40 20:48 20:59 21:10 21:27 2

21:19

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A21 #1-2851 Acq:16-NOV-2014 00:09:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.02E4 

22:47

A2.36E4

22:23

A1.17E3

23:05

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A9.17E3 

22:47

A1.56E3

22:29

A1.03E3

25:49

A923.85

26:47

A1.20E3

26:15

A1.02E3

25:06

A760.29

23:26

A699.92

24:24

A1.31E3

22:56

A448.72

23:55

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.86E5 

22:44

A3.91E5

22:20

A2.09E4

22:52

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A8.93E4 

22:44

A6.31E4

22:20

A1.17E4

22:48

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:14 22:39 23:11 23:47 24:16 24:36 24:58 25:18 25:40 26:17 26:41 2

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A21 #1-2851 Acq:16-NOV-2014 00:09:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.69E3 

22:28

A1.70E3

22:16

A953.7

27:05

A795.50

22:49

A699.04

26:21

A864.27

24:48

A1.11E3

23:17

A789.98

25:40

A662.46

24:20

A512.98

23:49

A391.51

25:15

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.62E3 

22:26

A868.94

24:42

A898.39

23:57

A630.53

26:52

A567.22

23:02

A658.44

25:30

A602.10

22:15

A4

2

A460.93

26:08

A321.67

23:31

A276.13

25:04

A437.32

24:17

A96.56

22:56

A58.98

25:40

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.51E5 

22:24

A2.25E4

22:32

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.77E4 

22:24

A9.60E3

22:29

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:14 22:39 23:11 23:47 24:16 24:36 24:58 25:18 25:40 26:17 26:41 2

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A21 #1-2851 Acq:16-NOV-2014 00:09:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A543.52 

15:37

A90.54

12:13

A36.70

14:55

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A173.27 

15:36

A50.17

12:12

A38.75

12:36

A15.30

14:48

A17.37

15:30

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 12:42 13:28 14:14 15:39 

12:13 13:03 13:49 14:52 15:10 

12:27 12:44 13:33 13:55 14:10 14:31 14:50 15:32 15:48 

13:18 14:26 15:09

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A21 #1-2851 Acq:16-NOV-2014 00:09:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 11

%

0 

20 40 60 80 

100 120 140 

A5.45E4

A2.74E3 A3.31E3 A3.64E3 A5.65E3 

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 11

%

0 

20 40 60 80 

100 120 140 

A4.95E4

A8.62E3 A9.51E3 A7.65E3 A5.12E3 A7.25E3 

A1.84E3

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 11

%

0 

20 40 60 80 

100 120 140 

10:53 10:58 11:06 11:11 11:16 11:19 11:22 11:27 11:30 11:34 11:39 

11:01 11:03

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 11

%

0 

20 40 60 80 

100 120 140 

A5.79E4

A1.85E3 A2.72E3 A3.26E3 A3.56E3 A5.43E3 

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 11

%

0 

20 40 60 80 

100 120 140 

A4.91E4

A9.41E3 A7.47E3 A8.37E3 A4.96E3 A7.24E3 

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A21 #1-2851 Acq:16-NOV-2014 00:09:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A7.15E5

A3.51E5

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A2.23E5

A1.42E4

A6.47E3 A9.86E3 A7.17E3

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A1.07E6

A6.20E4

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A2.34E5

A1.44E4

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A21 #1-2851 Acq:16-NOV-2014 00:09:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A3.51E5

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A1.42E4

A6.47E3 A9.86E3 A7.17E3 A4.18E3 A4.37E3 A4.24E3 A4.50

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A6.20E4

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A1.44E4 A4.29E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A21 #1-2851 Acq:16-NOV-2014 00:09:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A3.84E5

A3.51E5

A1.90E5

A4.81E4

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A8.55E4

A4.44E4

A1.42E4

A6.47E3

A7.17E3 A4.24E3 A3.17E3 A6.07E3 A3.18E3 A4.50E3

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A3.66E5

A1.77E5

A6.20E4 A3.87E4

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A7.22E4

A3.36E4

A4.29E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A21 #1-2851 Acq:16-NOV-2014 00:09:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A1.90E5

A4.81E4

A8.67E3 A4.75E3 A1.40E4

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A4.44E4

A6.47E3

A7.17E3

A3.17E3 A6.07E3 A3.18E3

A4.24E3 A4.50E3 A2.33E3 A1.19E3 A1.51E3 

A950.50 

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A1.77E5

A6.20E4

A3.87E4

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A3.36E4

A4.29E3

A3.63E3

A844.14 A798.60

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A21 #1-2851 Acq:16-NOV-2014 00:09:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

A4.81E4

A8.67E3 A1.40E4

A5.65E3

A4.75E3

A3.88E3 A4.19E3

A1.17E3 A2.51

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

A6.07E3

A3.18E3 A3.17E3

A2.33E3

A4.50E3

A1.95E3 A1.79E3 A1.19E3 A1.51E3

A950.50 A970.16 A865.51

A1.02E3 A1.31E3 A1.04E

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

A3.87E4

A4.90E3

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

A3.63E3

A844.14

A117.48

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A21 #1-2851 Acq:16-NOV-2014 00:09:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22

%

0 

20 40 60 80 

100 120 140 

A2.36E4

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22

%

0 

20 40 60 80 

100 120 140 

A9.23E3

A1.56E3

A1.69E3

A1.27E3 A700.50 A888.48 A449.30 A862.84 A256.31

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22

%

0 

20 40 60 80 

100 120 140 

22:31 22:35 22:39 22:05 22:09 22:14 22:17 22:19 22:22 22:27 22:41 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22

%

0 

20 40 60 80 

100 120 140 

A2.53E4

A5.82E3

A6.62E3

A1.83E3

A675.14 A1.19E3 A2.48E3

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22

%

0 

20 40 60 80 

100 120 140 

A8.96E3 

A1.42E3

A885.70 A1.43E3 A1.27E3 A700.50

A217.55 A518.96 A297.27

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A21 #1-2851 Acq:16-NOV-2014 00:09:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 

%

0 

20 40 60 80 

100 120 140 

A5.69E3

A1.70E3

A920.61 A7

A505.84 

A200.89 A311.11

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 

%

0 

20 40 60 80 

100 120 140 

A192.96

A104.64 

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 

%

0 

20 40 60 80 

100 120 140 

A8.55E3

A1.74E3

A1.70E3

A1.56E3 A1.48E3 A1.63E3 A906.77

A6

A479.43 

A200.95 A311.17 

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 

%

0 

20 40 60 80 

100 120 140 

A392.03

A266.46

A203.12 

A97.02

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A21 #1-2851 Acq:16-NOV-2014 00:09:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 

A3.02E4

A2.36E4

A1.17E3

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 

A9.17E3

A9.23E3

A1.56E3

A1.69E3 

A862.84 A1.31E3 A579.24 A449.30 

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 

A3.07E4

A2.53E4

A5.82E3

A1.83E3 A2.42E3

A675.14 A1.19E3 A2.48E3 A1.02E3

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 

A8.96E3 A8.08E3

A1.42E3

A1.43E3

A217.55 A518.96 A553.06 A221.74 

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115A21 #1-2851 Acq:16-NOV-2014 00:09:54 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.90E6 

7:36

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,2584.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.23E6 

7:36

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,748.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A8.78E6 

7:34

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,436.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A8.92E5 

7:34

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,372.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:13 7:24 7:31 7:40 7:52 8:04 8:11 8:21 8:30 8:40 8:48 8:57 9:05 9:12 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A23 #1-2851 Acq:16-NOV-2014 01:18:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0452 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.57E6 

8:54

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,344.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.51E6 

8:54

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,448.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.25E6 

8:50

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.10E6 

8:50

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:13 7:24 7:31 7:40 7:52 8:04 8:11 8:21 8:30 8:40 8:48 8:57 9:05 9:12 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A23 #1-2851 Acq:16-NOV-2014 01:18:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0452 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.55E6 

10:11

A3.58E6

10:28

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.79E6 

10:11

A1.21E6

10:28

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.12E6 

10:10

A2.82E6

10:25

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.98E5 

10:10

A4.69E5

10:25

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:49 9:57 10:07 10:16 10:27 10:41 10:49 10:58 11:06 11:13 11:21 11:33 11:

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A23 #1-2851 Acq:16-NOV-2014 01:18:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0452 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.00E6 

10:28

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,164.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.85E6 

10:28

A5.15E5

10:11

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,192.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.83E6 

10:25

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.02E6 

10:25

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:49 9:57 10:07 10:16 10:27 10:41 10:49 10:58 11:06 11:13 11:21 11:33 11:

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A23 #1-2851 Acq:16-NOV-2014 01:18:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0452 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.39E6 

11:19

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.67E6 

11:19

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.22E6 

11:16

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.15E6 

11:16

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:49 9:57 10:07 10:16 10:27 10:41 10:49 10:58 11:06 11:13 11:21 11:33 11:

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A23 #1-2851 Acq:16-NOV-2014 01:18:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0452 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.13E7 

12:51

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.04E6 

12:51

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.18E7 

12:49

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.02E5 

12:49

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:12 12:38 13:05 13:24 13:47 14:10 14:24 14:46 15:01 15:25 15:43 1

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A23 #1-2851 Acq:16-NOV-2014 01:18:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0452 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.05E6 

15:11

A8.52E6

14:48

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.64E6 

15:11

A1.51E6

14:48

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A7.21E6 

15:09

A6.42E6

14:46

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.20E6 

15:09

A1.08E6

14:46

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:12 12:38 13:05 13:24 13:47 14:10 14:24 14:46 15:01 15:25 15:43 1

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A23 #1-2851 Acq:16-NOV-2014 01:18:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0452 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.14E7 

17:37

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.24E6 

17:37

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.06E7 

17:34

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.12E6 

17:34

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:35 16:54 17:03 17:14 17:24 17:42 17:52 18:03 18:17 18:32 18:42 18:57 19

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A23 #1-2851 Acq:16-NOV-2014 01:18:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0452 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.15E7 

20:31

A8.01E6

20:15

A7.05E6

19:44

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.68E6 

20:31

A1.86E6

20:15

A1.65E6

19:44

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A9.53E6 

20:12

A9.66E6

19:45

A7.73E6

20:28

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.11E6 

20:12

A2.14E6

19:45

A1.65E6

20:28

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:39 19:49 20:00 20:13 20:27 20:38 20:51 21:05 21:14 21:24 21:35 

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A23 #1-2851 Acq:16-NOV-2014 01:18:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0452 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A7.36E6 

22:47

A5.00E6

22:22

A3.14E6

22:27

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.76E6 

22:47

A1.22E6

22:22

A8.36E5

22:27

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A6.24E6 

22:45

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.46E6 

22:45

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:25 22:52 23:23 23:50 24:09 24:41 25:02 25:31 26:06 26:33 26:55 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A23 #1-2851 Acq:16-NOV-2014 01:18:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0452 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A7.06E6 

22:27

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.71E6 

22:27

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.34E6 

22:23

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.01E6 

22:23

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:25 22:52 23:23 23:50 24:09 24:41 25:02 25:31 26:06 26:33 26:55 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A23 #1-2851 Acq:16-NOV-2014 01:18:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0452 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A4.28E6 

15:35

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A8.26E5 

15:35

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 12:12 12:38 13:05 13:24 13:47 14:10 14:24 14:46 15:01 15:25 15:43 

12:31 14:06 14:32 14:48 15:13 15:41 1

12:07 12:52 13:22 13:49 14:13 1

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115A23 #1-2851 Acq:16-NOV-2014 01:18:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0452 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
Instrument: HRMS‐4

Run File:

MID Procedure:

Reference Compound: PFK

15‐Nov‐14 15‐Nov‐14 15‐Nov‐14 15‐Nov‐14 15‐Nov‐14 15‐Nov‐14 15‐Nov‐14 15‐Nov‐14 15‐Nov‐14 15‐N

Segment 13:59:15 14:33:30 15:07:49 15:42:10 16:16:24 16:50:43 17:24:55 17:59:06 18:33:27 20:

MID Time Window 1 9209 9161 9098 9128 9080 8881 8862 8778 8757 MID Time Window 2 8915 8880 8959 8768 8756 8913 8866 8441 8823 MID Time Window 3 8801 8787 9018 8714 8863 8803 8539 8883 8854 MID Time Window 4 9346 8987 9025 8985 9301 8833 9165 9350 8784 MID Time Window 5 9202 9257 9216 9307 9102 8979 9105 8954 9463 MID Time Window 6 9285 9297 9024 9634 9215 9400 9288 9317 9033 

15‐Nov‐14 15‐Nov‐14 15‐Nov‐14 15‐Nov‐14 16‐Nov‐14 16‐Nov‐14

Segment 21:59:03 22:33:17 23:07:33 23:41:48 0:16:11 1:24:47

MID Time Window 1 8357 8735 8798 9073 8904 8931MID Time Window 2 8597 8655 8423 8594 8741 8541MID Time Window 3 8660 8517 8726 8685 8355 8629MID Time Window 4 8845 8791 8838 8734 8821 8563MID Time Window 5 9337 9322 8798 8981 8980 9104MID Time Window 6 9372 9040 9151 8883 9011 9021

Mass Resolution

Mass Resolution Examination ‐ Thermo DFS

4‐141115AC429‐DB5MS‐3

Mass Resolution

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
ALS Environmental - Burlington, ON L1535265 Appendix 141208 Appendix Page 272 of 625
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.03E7 

7:34

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,2976.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.28E6 

7:34

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,560.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.26E6 

7:32

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,376.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.83E5 

7:32

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,708.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:13 7:24 7:33 7:48 7:55 8:07 8:16 8:23 8:30 8:39 8:47 8:58 9:14 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B01 #1-2851 Acq:16-NOV-2014 01:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0453 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.81E6 

8:52

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,392.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.72E6 

8:52

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,432.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.53E6 

8:49

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.25E6 

8:49

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:13 7:24 7:33 7:48 7:55 8:07 8:16 8:23 8:30 8:39 8:47 8:58 9:14 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B01 #1-2851 Acq:16-NOV-2014 01:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0453 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.01E7 

10:09

A3.90E6

10:26

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.91E6 

10:09

A1.33E6

10:26

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.63E6 

10:08

A3.16E6

10:23

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.85E5 

10:08

A4.94E5

10:23

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:47 9:56 10:04 10:14 10:24 10:32 10:44 10:53 11:06 11:14 11:23 11:32 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B01 #1-2851 Acq:16-NOV-2014 01:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0453 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.44E6 

10:26

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,208.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.40E6 

10:26

A5.06E5

10:09

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,260.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.50E6 

10:23

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.49E6 

10:23

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:47 9:56 10:04 10:14 10:24 10:32 10:44 10:53 11:06 11:14 11:23 11:32 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B01 #1-2851 Acq:16-NOV-2014 01:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0453 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.77E6 

11:17

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.01E6 

11:17

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.36E6 

11:14

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.37E6 

11:14

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:47 9:56 10:04 10:14 10:24 10:32 10:44 10:53 11:06 11:14 11:23 11:32 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B01 #1-2851 Acq:16-NOV-2014 01:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0453 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.16E7 

12:50

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.11E6 

12:50

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.22E7 

12:47

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.77E5 

12:47

A7.14E4

12:56

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:34 13:02 13:18 13:37 13:51 14:10 14:26 14:43 15:12 15:33 15

12:18 12:48 13:43 15

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B01 #1-2851 Acq:16-NOV-2014 01:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0453 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.47E6 

15:09

A8.85E6

14:46

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.73E6 

15:09

A1.55E6

14:46

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A7.65E6 

15:07

A6.47E6

14:44

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.32E6 

15:07

A1.11E6

14:44

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:34 13:02 13:18 13:37 13:51 14:10 14:26 14:43 15:12 15:33 15

12:18 12:48 13:43 15

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B01 #1-2851 Acq:16-NOV-2014 01:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0453 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.11E7 

17:35

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.31E6 

17:35

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.12E7 

17:32

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.21E6 

17:32

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:42 17:00 17:13 17:24 17:35 17:45 18:06 18:24 18:35 18:45 18:56 19

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B01 #1-2851 Acq:16-NOV-2014 01:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0453 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.30E7 

20:29

A9.33E6

20:13

A7.82E6

19:43

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A3.02E6 

20:29

A2.14E6

20:13

A1.83E6

19:43

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.07E7 

20:10

A1.05E7

19:43

A8.66E6

20:26

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.42E6 

20:10

A2.26E6

19:43

A1.73E6

20:16

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:41 19:50 19:59 20:09 20:19 20:33 20:44 20:53 21:05 21:17 21:26 21:3

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B01 #1-2851 Acq:16-NOV-2014 01:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0453 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A8.56E6 

22:46

A6.09E6

22:21

A3.59E6

22:25

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.06E6 

22:46

A1.49E6

22:21

A9.51E5

22:25

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A7.41E6 

22:43

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.75E6 

22:43

A1.52E6

22:18

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:19 22:38 23:13 23:38 24:01 24:28 25:01 25:37 26:00 26:21 26:46 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B01 #1-2851 Acq:16-NOV-2014 01:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0453 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A8.48E6 

22:25

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.04E6 

22:25

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.19E6 

22:22

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.15E6 

22:22

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:19 22:38 23:13 23:38 24:01 24:28 25:01 25:37 26:00 26:21 26:46 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B01 #1-2851 Acq:16-NOV-2014 01:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0453 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A4.37E6 

15:34

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A8.43E5 

15:34

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 13:37 13:51 14:10 15:12 15:33 15

12:34 13:02 14:26 14:43 

12:18 13:18 13:52 14:08 15:5

12:48 13:33 14:23 15:04 

12:09

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B01 #1-2851 Acq:16-NOV-2014 01:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0453 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.42E7 

7:35

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,4752.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.74E6 

7:35

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1736.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.23E6 

7:33

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1436.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.22E5 

7:33

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,312.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:10 7:24 7:34 7:43 7:55 8:07 8:22 8:31 8:42 8:55 9:03 9:13 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.09E6 

8:44

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,260.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.04E6 

8:44

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1052.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.07E6 

8:41

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.82E6 

8:41

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:10 7:24 7:34 7:43 7:55 8:07 8:22 8:31 8:42 8:55 9:03 9:13 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.62E6 

10:10

A5.35E5

10:28

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.03E6 

10:10

A1.59E5

10:28

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.69E6 

10:09

A3.96E6

10:25

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.93E5 

10:09

A6.49E5

10:25

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:51 10:01 10:11 10:20 10:31 10:40 10:48 11:02 11:10 11:25 11:37 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.83E5 

10:28

A1.17E5

10:00

A8.45E4

9:50

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,100.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.62E5 

10:28

A2.87E5

10:10

A4.68E4

9:50

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,256.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.64E6 

10:25

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.00E6 

10:25

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:51 10:01 10:11 10:20 10:31 10:40 10:48 11:02 11:10 11:25 11:37 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.59E5 

11:19

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.04E6 

11:19

A7.84E4

11:27

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.24E3 

11:16

A1.81E3

11:19

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.29E4 

11:16

A1.85E3

11:19

A821.38

10:28

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:51 10:01 10:11 10:20 10:31 10:40 10:48 11:02 11:10 11:25 11:37 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A5.24E7 

12:51

A1.17E7

12:56

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.87E6 

12:51

A7.57E5

12:56

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.21E7 

12:48

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.08E5 

12:48

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:23 12:41 13:02 13:18 13:58 14:12 14:30 14:52 15:13 15:29 15:46 

12:06 13:32 

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A7.73E7 

14:47

A5.96E7

15:10

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.22E7 

14:47

A9.87E6

15:10

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.91E6 

15:08

A7.21E6

14:45

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.82E6 

15:08

A1.20E6

14:45

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:23 12:41 13:02 13:18 13:58 14:12 14:30 14:52 15:13 15:29 15:46 

12:06 13:32 

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.10E7 

17:36

A4.03E6

17:32

A1.17E6

17:06

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.26E6 

17:36

A8.66E5

17:32

A2.15E5

17:06

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.04E7 

17:33

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.05E6 

17:33

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:45 16:58 17:09 17:24 17:34 17:44 18:02 18:12 18:29 18:39 18:49 18:59 1

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.56E6 

19:44

A7.29E5

20:14

A6.59E5

19:46

A3.05E5

20:21

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A5.10E5 

19:44

A1.68E5

20:14

A6.37E4

20:21

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A9.73E6 

20:11

A4.78E6

19:41

A5.81E6

20:27

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.21E6 

20:11

A1.08E6

19:41

A1.25E6

20:17

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:37 19:52 20:00 20:14 20:23 20:32 20:45 20:59 21:11 21:22 21:31 21

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A7.59E4 

22:46

A5.83E4

22:22

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.54E4 

22:46

A5.69E3

22:35

A4.06E3

23:58

A4.22E3

23:18

A3.87E3

24:39

A3.45E3

22:13

A1.88E3

22:53

A1.88E3

25:27

A2.18E3

26:23

A758.83

25:55

A494.34

24:24

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.24E6 

22:44

A3.50E6

22:20

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A9.69E5 

22:44

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:09 22:28 23:04 23:23 23:44 24:10 24:30 24:58 25:21 26:00 26:23 26:44 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A8.73E3 

22:26

A7.16E3

22:14

A6.57E3

22:44

A2.09E3

22:47

A1.47E3

25:27

A1.12E3

23:15

A718.00

25:59

A1.02E3

26:46

A678.68

23:40

A468.90

24:32

A354.57

25:01

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.51E3 

22:44

A1.85E3

22:46

A2.26E3

24:39

A1.85E3

23:58

A1.48E3

26:03

A1.53E3

23:17

A822.48

26:51

A1.60E3

25:27

A835.70

22:21

A349.65

22:52

A247.37

24:53

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.34E6 

22:23

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.16E5 

22:23

A3.10E4

22:31

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:09 22:28 23:04 23:23 23:44 24:10 24:30 24:58 25:21 26:00 26:23 26:44 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A1.34E4 

15:35

A571.02

15:41

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A1.95E3 

15:35

A106.16

15:38

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 14:30 15:13 15:46 

12:23 12:41 13:18 13:58 14:12 14:26 14:52 

13:02 13:32 13:47 15:08 15:29 1

12:14 14:03 14:42 12:30 12:43 13:09

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

A4.03E6

A1.17E6

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141117mb

after_modification

17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

A8.66E5

A2.15E5 A2.80E5

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

A4.00E6

A1.16E6

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

A8.47E5

A2.01E5 A2.42E5

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A1.10E7

A4.03E6

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A2.26E6

A8.66E5

A2.80E5

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A1.10E7

A4.00E6

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A2.21E6

A8.47E5

A2.42E5

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A1.56E6

A6.59E5

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A5.10E5

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A2.22E6

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A5.00E5

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 

%

0 

20 40 60 80 

100 120 140 

A6.59E5

A6.25E4

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 

%

0 

20 40 60 80 

100 120 140 

A2.18E4 A7.48E3 A9.48E3

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 

%

0 

20 40 60 80 

100 120 140 

A5.24E4

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 

%

0 

20 40 60 80 

100 120 140 

A2.14E4 A8.79E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A7.29E5

A6.59E5

A3.05E5

A6.25E4 A7.47E4

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A1.68E5

A6.37E4

A7.48E3 A9.48E3 A9.81E3

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A7.13E5

A2.70E5

A5.24E4 A4.91E4

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A1.54E5

A4.81E4

A8.79E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A3.05E5

A6.25E4 A7.47E4

A3.65E4

A7.01E3 A9.66E3

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A6.37E4

A7.48E3 A9.81E3 A9.48E3 A3.53E3 A4.73E3 A4.93E3 A4.65E3 A2.49E3 A2.96E3 A2.42E3 A2.23

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A2.70E5

A5.24E4 A4.91E4

A2.92E4

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A4.81E4

A5.79E3

A7.27E3 A3.14E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A7.47E4

A7.01E3

A7.74E3 A5.76E3

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A9.81E3

A4.73E3 A3.53E3

A4.93E3 A4.65E3 A2.47E3

A2.49E3 A2.96E3

A2.42E3 A2.11E3 A2.23E3 A928.72 A994.

A385.35

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A4.91E4

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A7.27E3

A565.83

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A5.83E4

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A1.16E4

A5.69E3

A2

A3.45E3 A1.88E3

A1.47E3 A1.48E3

A410.13 A596.67 A544.82

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

22:09 22:11 22:16 22:18 22:20 22:22 22:28 22:32 22:39 22:42 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A5.84E4

A1.33E4

A3.74E3 A1.68E3 A1.44E3 A1.23E3

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A1.14E4

A5.34E3

A2

A3.45E3 A1.79E3

A1.34E3 A1.22E3

A410.13 A596.67 A589.60

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A8.73E3

A7.16E3 A6.57E3 A5.57E3

A1.69E3 A2.

A1.34E3 

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A4.47E3

A1.09E3

A835.70 A989.46

A661.40

A270.80 A234.54 

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A1.66E4

A7.16E3 A6.48E3 A5.49E3

A3.02E3

A2.71E3

A1.65E3 A2.

A1.16E3

A1.34E3 

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A4.63E3

A1.11E3 

A1.11E3 A845.23

A643.80 A403.62 

A282.79

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 

%

0 

20 40 60 80 

100 120 140 

A7.59E4

A5.83E4

A1.78E3 A1.90E3

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 

%

0 

20 40 60 80 

100 120 140 

A1.54E4

A1.16E4

A5.69E3

A2.33E3 A2.28E3

A1.88E3 A1.88E3 A1.47E3 A1.48E3

A544.82 A460.34 A420.60 

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 

%

0 

20 40 60 80 

100 120 140 

A7.34E4

A5.84E4

A3.74E3 A1.68E3 A2.48E3

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 

%

0 

20 40 60 80 

100 120 140 

A1.47E4 A1.14E4

A5.34E3

A2.07E3 A2.03E3

A1.79E3

A1.34E3 A1.37E3 A1.22E3

A589.60 A395.07

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B04 #1-2849 Acq:16-NOV-2014 03:35:44 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.15E7 

7:35

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,2532.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.38E6 

7:35

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1540.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.03E7 

7:33

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1756.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.01E6 

7:33

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,520.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:17 7:24 7:38 7:51 7:59 8:08 8:18 8:27 8:35 8:42 8:49 8:59 9:06 9:

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B05 #1-2852 Acq:16-NOV-2014 04:10:04 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.51E5 

8:44

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,340.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.04E5 

8:44

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1088.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.92E6 

8:41

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.41E6 

8:41

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:17 7:24 7:38 7:51 7:59 8:08 8:18 8:27 8:35 8:42 8:49 8:59 9:06 9:

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B05 #1-2852 Acq:16-NOV-2014 04:10:04 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.72E6 

10:11

A3.65E5

10:28

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.96E5 

10:11

A1.12E5

10:28

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.35E6 

10:09

A3.62E6

10:25

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.09E6 

10:09

A5.79E5

10:25

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:52 9:59 10:11 10:21 10:28 10:37 10:45 10:57 11:07 11:17 11:27 11:36 1

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B05 #1-2852 Acq:16-NOV-2014 04:10:04 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.91E5 

10:28

A1.12E5

10:00

A5.75E4

9:49

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,236.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.79E5 

10:28

A2.05E5

10:11

A4.87E4

9:50

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,200.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.10E6 

10:25

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.21E6 

10:25

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:52 9:59 10:11 10:21 10:28 10:37 10:45 10:57 11:07 11:17 11:27 11:36 1

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B05 #1-2852 Acq:16-NOV-2014 04:10:04 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.32E5 

11:19

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.50E5 

11:19

A4.15E4

11:25

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.12E4 

11:16

A2.94E3

11:22

A610.96

11:32

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.29E4 

11:16

A3.19E3

11:20

A496

11:

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:52 9:59 10:11 10:21 10:28 10:37 10:45 10:57 11:07 11:17 11:27 11:36 1

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B05 #1-2852 Acq:16-NOV-2014 04:10:04 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.86E7 

12:51

A7.96E6

12:56

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.92E6 

12:51

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.43E7 

12:49

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.91E5 

12:49

A8.11E5

12:54

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:10 12:24 12:39 13:10 13:27 13:53 14:08 14:22 14:46 15:12 15:38 1

12:55 14:39

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B05 #1-2852 Acq:16-NOV-2014 04:10:04 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.19E8 

14:47

A9.47E7

15:10

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.83E7 

14:47

A1.47E7

15:10

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.83E6 

15:08

A8.40E6

14:45

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.64E6 

15:08

A1.48E6

14:45

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:10 12:24 12:39 13:10 13:27 13:53 14:08 14:22 14:46 15:12 15:38 1

12:55 14:39

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B05 #1-2852 Acq:16-NOV-2014 04:10:04 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A3.35E7 

17:36

A8.63E6

17:32

A2.70E6

17:06

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A6.88E6 

17:36

A2.31E6

17:32

A7.08E5

17:11

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.15E7 

17:33

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.30E6 

17:33

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:36 16:48 17:00 17:14 17:30 17:41 17:54 18:06 18:16 18:28 18:37 18:49 19

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B05 #1-2852 Acq:16-NOV-2014 04:10:04 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A5.22E6 

19:44

A2.22E6

20:14

A2.00E6

19:46

A8.62E5

20:20

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.68E6 

19:44

A5.14E5

20:14

A2.13E5

20:20

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A8.12E6 

20:11

A8.65E6

19:45

A5.91E6

20:18

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.84E6 

20:11

A1.92E6

19:45

A1.27E6

20:27

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:36 19:45 19:56 20:07 20:18 20:35 20:48 20:57 21:10 21:19 21:31 21:

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B05 #1-2852 Acq:16-NOV-2014 04:10:04 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.12E5 

22:47

A2.86E4

22:13

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.17E4 

22:47

A9.91E3

22:13

A5.36E3

23:17

A4.87E3

24:39

A4.31E3

25:27

A2.79E3

23:58

A2.23E3

22:39

A2.01E3

26:24

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.90E6 

22:44

A4.05E6

22:20

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.14E6 

22:44

A9.17E5

22:20

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:41 23:32 23:56 24:21 24:54 25:29 25:50 26:22 26:56 

22:22 22:45 23:06 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B05 #1-2852 Acq:16-NOV-2014 04:10:04 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.62E4 

22:27

A686.58

26:34

A953.41

25:50

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A8.79E3 

22:44

A3.63E3

22:15

A2.80E3

22:40

A2.00E3

25:28

A1.83E3

23:17

A1.98E3

24:39

A2.26E3

23:58

A705.89

26:49

A679.07

26:24

A221.56

25:58

A233.11

25:20

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.80E6 

22:23

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A6.17E5 

22:23

A1.50E4

22:33

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:41 23:32 23:56 24:21 24:54 25:29 25:50 26:22 26:56 

22:22 22:45 23:06 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B05 #1-2852 Acq:16-NOV-2014 04:10:04 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A6.45E3 

15:36

A2.00E3

15:39

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A1.69E3 

15:35

A825.11

15:39

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 12:10 12:39 13:10 14:46 15:12 1

12:24 12:49 13:27 13:53 14:08 14:22 14:54 15:38 13:08 15:10 15:40 

12:12 12:31 13:29 13:49 14:40

13:04

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B05 #1-2852 Acq:16-NOV-2014 04:10:04 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A5.22E6

A2.00E6

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A1.68E6

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A7.29E6

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A1.64E6

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B05 #1-2852 Acq:16-NOV-2014 04:10:04 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A2.00E6

A1.96E5

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A6.17E4 A4.16E4 A2.45E4

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A1.75E5

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A6.67E4

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B05 #1-2852 Acq:16-NOV-2014 04:10:04 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A2.22E6

A2.00E6

A8.62E5

A1.96E5 A1.67E5

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A5.14E5

A2.13E5

A4.16E4 A4.43E4

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A2.17E6

A8.57E5

A1.75E5

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A4.77E5

A1.65E5

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B05 #1-2852 Acq:16-NOV-2014 04:10:04 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 

%

0 

20 40 60 80 

100 120 140 

A8.62E5

A1.96E5 A1.67E5

A5.24E4 A1.87E4

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 

%

0 

20 40 60 80 

100 120 140 

A2.13E5

A4.16E4 A4.43E4

A1.75E4 A1.10E4 A8.10E3 A1.16E4 A4.90E3 A5.37E3

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 

%

0 

20 40 60 80 

100 120 140 

A8.57E5

A1.75E5 A1.39E5

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 

%

0 

20 40 60 80 

100 120 140 

A1.65E5

A2.09E4

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B05 #1-2852 Acq:16-NOV-2014 04:10:04 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A1.67E5

A5.24E4

A1.87E4

A2.71E4 A2.10E4

A1.25E4 A1.13E4 A6.36E3 

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A4.43E4

A1.75E4 A1.10E4

A1.16E4

A4.90E3

A5.37E3 A3.63E3 A3.11E3 A2.34E3 A3.62E3 A2.29E

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A1.39E5

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A2.09E4

A2.63E3

A1.13E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B05 #1-2852 Acq:16-NOV-2014 04:10:04 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.20E7 

7:34

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,3220.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.44E6 

7:34

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1472.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.06E7 

7:32

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,364.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.03E6 

7:32

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,476.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:12 7:20 7:29 7:36 7:43 7:53 8:01 8:11 8:19 8:28 8:41 8:49 9:02 9:15 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B06 #1-2851 Acq:16-NOV-2014 04:44:17 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.04E6 

8:44

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,812.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.58E5 

8:44

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,928.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.88E6 

8:41

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.41E6 

8:41

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:12 7:20 7:29 7:36 7:43 7:53 8:01 8:11 8:19 8:28 8:41 8:49 9:02 9:15 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B06 #1-2851 Acq:16-NOV-2014 04:44:17 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.09E6 

10:10

A3.00E5

10:28

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.59E5 

10:10

A9.31E4

10:28

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.60E6 

10:09

A4.11E6

10:24

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.14E6 

10:09

A6.28E5

10:24

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:58 10:08 10:20 10:39 10:51 10:59 11:14 11:24 11:32 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B06 #1-2851 Acq:16-NOV-2014 04:44:17 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.23E5 

10:27

A9.45E4

10:00

A5.82E4

9:49

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,176.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.14E5 

10:27

A1.95E5

10:10

A4.22E4

9:49

A3.94E4

10:00

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,272.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.89E6 

10:24

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.01E6 

10:24

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:58 10:08 10:20 10:39 10:51 10:59 11:14 11:24 11:32 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B06 #1-2851 Acq:16-NOV-2014 04:44:17 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.21E5 

11:18

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.06E5 

11:18

A9.37E4

11:25

A3.47E4

10:27

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.81E3 

11:15

A2.12E3

11:18

A638.10

9:52

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.10E4 

11:16

A967.97

11:24

A9

1

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:58 10:08 10:20 10:39 10:51 10:59 11:14 11:24 11:32 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B06 #1-2851 Acq:16-NOV-2014 04:44:17 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.69E7 

12:50

A8.15E6

12:55

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.83E6 

12:50

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.38E7 

12:48

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.54E5 

12:48

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:08 12:40 12:59 13:13 13:31 14:17 14:30 14:56 15:25 15:

12:09 12:24 13:50 15:39

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B06 #1-2851 Acq:16-NOV-2014 04:44:17 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.81E7 

14:47

A7.69E7

15:10

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.51E7 

14:47

A1.24E7

15:10

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.07E7 

15:08

A8.10E6

14:45

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.86E6 

15:08

A1.36E6

14:45

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:08 12:40 12:59 13:13 13:31 14:17 14:30 14:56 15:25 15:

12:09 12:24 13:50 15:39

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B06 #1-2851 Acq:16-NOV-2014 04:44:17 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A4.00E7 

17:36

A1.05E7

17:32

A2.51E6

17:06

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A8.24E6 

17:36

A2.88E6

17:32

A8.69E5

17:11

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.16E7 

17:33

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.31E6 

17:33

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 17:38 17:52 18:03 18:18 18:35 18:47 18:58 

16:46 16:56 17:10 17:24

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B06 #1-2851 Acq:16-NOV-2014 04:44:17 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A7.33E6 

19:44

A3.63E6

20:14

A3.70E6

19:45

A1.82E6

20:20

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.59E6 

19:43

A8.23E5

20:14

A4.04E5

20:20

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A9.29E6 

20:11

A8.60E6

19:44

A6.07E6

20:27

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.12E6 

20:11

A1.82E6

19:44

A1.16E6

20:27

A1.17E5

20:31

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:38 19:52 20:03 20:11 20:20 20:30 20:40 20:48 21:05 21:16 21:25 21:34 

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B06 #1-2851 Acq:16-NOV-2014 04:44:17 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.01E5 

22:46

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A6.04E4 

22:46

A8.69E3

22:50

A1.22E4

22:13

A5.80E3

23:17

A4.05E3

23:58

A4.71E3

24:38

A3.34E3

26:24

A3.81E3

25:27

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.46E6 

22:44

A3.52E6

22:19

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.06E6 

22:44

A8.23E5

22:19

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:12 22:36 22:59 23:23 23:47 24:05 24:35 24:57 25:31 25:54 26:23 26:54 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B06 #1-2851 Acq:16-NOV-2014 04:44:17 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.67E4 

22:26

A3.04E4

22:39

A2.97E3

22:50

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A8.08E3 

22:44

A4.40E3

22:14

A2.33E3

22:40

A1.67E3

26:24

A2.12E3

25:27

A1.54E3

23:57

A1.77E3

23:17

A880.52

24:38

A2

2

A244.97

25:52

A271.44

26:51

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.52E6 

22:23

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.49E5 

22:23

A3.19E4

22:31

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:12 22:36 22:59 23:23 23:47 24:05 24:35 24:57 25:31 25:54 26:23 26:54 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B06 #1-2851 Acq:16-NOV-2014 04:44:17 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A1.68E4 

15:35

A995.22

15:45

A649.79

15:18

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A1.91E3 

15:34

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 12:08 13:31 14:56 15:

12:40 12:59 13:13 14:30 14:54 15:10 15:25 

12:06 12:24 13:44 14:17 15:44

12:12 12:42 13:02 13:24 14:02 14:38 15:14 1

14:24

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B06 #1-2851 Acq:16-NOV-2014 04:44:17 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
10:48 10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 

%

0 

20 40 60 80 

100 120 140 

A6.21E5

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

10:48 10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 

%

0 

20 40 60 80 

100 120 140 

A6.06E5

A9.37E4

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

10:48 10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 

%

0 

20 40 60 80 

100 120 140 

10:51 10:53 10:57 10:59 11:04 11:08 11:14 11:18 11:24 11:32 11:37 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

10:48 10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 

%

0 

20 40 60 80 

100 120 140 

A6.19E5

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

10:48 10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 

%

0 

20 40 60 80 

100 120 140 

A6.01E5

A9.02E4

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B06 #1-2851 Acq:16-NOV-2014 04:44:17 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A7.33E6

A3.70E6

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A2.59E6

A1.10E5

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A1.12E7

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A2.54E6

A1.07E5

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B06 #1-2851 Acq:16-NOV-2014 04:44:17 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A3.70E6

A4.58E5

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A1.10E5 A8.81E4

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A1.07E5

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B06 #1-2851 Acq:16-NOV-2014 04:44:17 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A4.67E4

A3.26E4

A3.04E4

A1.19E4

A7.04E3

A4.26E3 

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A8.08E3

A1.12E4

A4.40E3

A1.94E3 A2.33E3 A2.40E3 A1.64E3

A1.5

A1.52E3 A1.01E3

A462.09 A660.58 

A439.75

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A4.72E4

A3.26E4

A3.00E4

A1.51E4

A7.70E3 A1.16E4

A7.01E3

A2.61E3 A4.25E3 

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A8.08E3

A1.05E4

A3.83E3

A1.62E3 A3.73E3

A2.23E3 A1.51E3 A1.5

A764.42

A332.78 

A654.89

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B06 #1-2851 Acq:16-NOV-2014 04:44:17 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.26E7 

7:35

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,2960.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.50E6 

7:35

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1288.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.01E7 

7:32

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1448.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.82E5 

7:32

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,700.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:08 7:21 7:29 7:36 7:46 7:56 8:04 8:13 8:20 8:30 8:38 8:54 9:01 9:12 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B07 #1-2851 Acq:16-NOV-2014 05:18:40 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.70E5 

8:44

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,308.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A8.99E5 

8:44

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,448.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.59E6 

8:41

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.24E6 

8:41

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:08 7:21 7:29 7:36 7:46 7:56 8:04 8:13 8:20 8:30 8:38 8:54 9:01 9:12 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B07 #1-2851 Acq:16-NOV-2014 05:18:40 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.40E6 

10:10

A3.16E5

10:28

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.89E5 

10:10

A8.14E4

10:28

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.17E6 

10:09

A3.88E6

10:25

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.03E6 

10:09

A6.61E5

10:25

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 10:04 10:17 10:26 10:34 10:48 10:58 11:07 11:15 11:28 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B07 #1-2851 Acq:16-NOV-2014 05:18:40 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.40E5 

10:28

A9.06E4

10:01

A8.21E4

9:50

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,140.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.03E5 

10:28

A2.33E5

10:10

A5.13E4

9:50

A5.42E4

10:00

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,272.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.54E6 

10:25

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.65E6 

10:25

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 10:04 10:17 10:26 10:34 10:48 10:58 11:07 11:15 11:28 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B07 #1-2851 Acq:16-NOV-2014 05:18:40 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.48E5 

11:19

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.93E5 

11:19

A5.33E4

11:28

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.13E4 

11:16

A568.85

11:19

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.03E3 

11:16

A1.78E3

11:18

A1.74E3

11:28

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 10:04 10:17 10:26 10:34 10:48 10:58 11:07 11:15 11:28 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B07 #1-2851 Acq:16-NOV-2014 05:18:40 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.95E7 

12:51

A5.56E6

12:55

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.97E6 

12:51

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.32E7 

12:49

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.24E5 

12:49

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:08 12:24 12:50 13:06 13:27 13:44 14:01 14:18 14:35 14:55 15:19 15:33 15:47 

14:20

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B07 #1-2851 Acq:16-NOV-2014 05:18:40 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.76E7 

14:48

A3.53E7

15:10

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.11E6 

14:47

A6.25E6

15:10

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.98E6 

15:08

A7.78E6

14:46

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.73E6 

15:08

A1.35E6

14:46

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:08 12:24 12:50 13:06 13:27 13:44 14:01 14:18 14:35 14:55 15:19 15:33 15:47 

14:20

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B07 #1-2851 Acq:16-NOV-2014 05:18:40 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.25E7 

17:36

A2.41E6

17:33

A8.61E5

17:06

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.45E6 

17:36

A6.60E5

17:32

A2.64E5

17:12

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.17E7 

17:33

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.27E6 

17:33

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:38 16:55 17:11 17:21 17:35 17:51 18:09 18:22 18:35 18:51 19:02 

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B07 #1-2851 Acq:16-NOV-2014 05:18:40 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.10E6 

19:44

A1.09E6

20:15

A9.68E5

19:46

A4.18E5

20:21

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A7.44E5 

19:44

A2.49E5

20:15

A8.94E4

20:21

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A9.07E6 

20:11

A7.87E6

19:44

A5.79E6

20:27

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.02E6 

20:11

A1.67E6

19:44

A1.19E6

20:27

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:36 19:44 19:59 20:11 20:18 20:36 21:05 21:13 21:29 21:3

20:44 20:53

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B07 #1-2851 Acq:16-NOV-2014 05:18:40 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A9.51E4 

22:47

A8.33E4

22:22

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.58E4 

22:47

A1.36E4

22:22

A6.18E3

23:18

A5.22E3

23:58

A5.18E3

24:39

A2.70E3

25:28

A2.08E3

22:16

A1.91E3

22:53

A3.39E3

26:22

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.62E6 

22:44

A3.73E6

22:19

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.11E6 

22:44

A8.57E5

22:19

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:11 22:35 23:06 23:24 23:44 24:17 24:50 25:09 25:30 25:50 26:15 26:34 26:56 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B07 #1-2851 Acq:16-NOV-2014 05:18:40 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.57E4 

22:26

A1.01E4

22:15

A4.02E3

22:41

A1

2

A1.27E3

23:02

A478.08

25:15

A409.52

25:56

A540.09

23:59

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.54E3 

22:45

A2.38E3

24:39

A2.40E3

23:57

A1.84E3

23:17

A1.74E3

25:27

A1.45E3

22:35

A1.26E3

26:24

A983.83

25:01

A792.49

24:34

A577.77

23:51

A382.17

26:49

A323.74

22:19

A323.59

22:51

A187.68

25:38

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.52E6 

22:23

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.19E5 

22:23

A3.59E4

22:30

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:11 22:35 23:06 23:24 23:44 24:17 24:50 25:09 25:30 25:50 26:15 26:34 26:56 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B07 #1-2851 Acq:16-NOV-2014 05:18:40 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A3.10E3 

15:34A3.96E3

15:37

A1.12

15:4

A456.55

15:18

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A232.12 

15:36

A89.48

12:13

A37.00

12:30

A18.49

15:40

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 12:24 12:50 13:06 13:27 14:01 14:18 14:55 15:19 15:33 15:47 

12:08 13:44 

12:40 13:01 13:24 13:55 14:10 14:35 14:49 15:39 12:20 14:20 15:17

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B07 #1-2851 Acq:16-NOV-2014 05:18:40 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 11

%

0 

20 40 60 80 

100 120 140 

A8.48E5

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 11

%

0 

20 40 60 80 

100 120 140 

A8.93E5

A5.33E4

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 11

%

0 

20 40 60 80 

100 120 140 

10:50 10:54 10:58 11:02 11:07 11:10 11:15 11:20 11:22 11:28 11:32 11:39 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 11

%

0 

20 40 60 80 

100 120 140 

A8.41E5

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 11

%

0 

20 40 60 80 

100 120 140 

A8.84E5

A5.01E4

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B07 #1-2851 Acq:16-NOV-2014 05:18:40 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13

%

0 

20 40 60 80 

100 120 140 

A3.95E7

A5.56E6

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141117mb

after_modification

12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13

%

0 

20 40 60 80 

100 120 140 

A3.97E6

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13

%

0 

20 40 60 80 

100 120 140 

A3.93E7

A5.95E6

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13

%

0 

20 40 60 80 

100 120 140 

A3.96E6

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B07 #1-2851 Acq:16-NOV-2014 05:18:40 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13

%

0 

20 40 60 80 

100 120 140 

A5.56E6

A1.72E5

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141117mb

after_modification

12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13

%

0 

20 40 60 80 

100 120 140 

A4.47E4

A2.35E4 A1.95E4 A1.69E4 A1.14E4

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13

%

0 

20 40 60 80 

100 120 140 

A5.95E6

A4.97E5

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13

%

0 

20 40 60 80 

100 120 140 

A4.20E4

A2.13E4 A1.68E4 A1.44E4

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B07 #1-2851 Acq:16-NOV-2014 05:18:40 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A2.10E6

A9.68E5

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A7.44E5

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A3.10E6

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A7.26E5

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B07 #1-2851 Acq:16-NOV-2014 05:18:40 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 

%

0 

20 40 60 80 

100 120 140 

A9.68E5

A1.08E5

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 

%

0 

20 40 60 80 

100 120 140 

A2.14E4 A8.41E3 A8.07E3

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 

%

0 

20 40 60 80 

100 120 140 

A7.83E4

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 

%

0 

20 40 60 80 

100 120 140 

A3.05E4

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B07 #1-2851 Acq:16-NOV-2014 05:18:40 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A8.33E4

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A1.36E4

A7.30E3

A6.63E3

A2.08E3

A1.04E3 A1.76E3 A1.10E3 A1.16E

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A8.36E4

A1.82E4

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A1.32E4

A6.64E3

A6.12E3

A2.04E3

A1.10E3 A825.50 A1.17E3 A590.7

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B07 #1-2851 Acq:16-NOV-2014 05:18:40 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A1.57E4

A1.01E4

A4.02E3 A4.82E3

A2.64E3 A3.0

A5.06E3 A3.59E3 A3.53E3

A2.09E3 

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A4.54E3

A3.71E3

A1.45E3 A1.47E3 A2.24E3 A1.20E3 A1.05E3 A77

A447.84

A261.43 A323.74 

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

22:11 22:19 22:22 22:35 22:06 22:14 22:16 22:29 22:33 22:39 22:42 

22:25

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A1.51E4

A1.00E4

A3.43E3 A4.06E3

A4.80E3 A2.95E3 A2.18E3 A2.92E3 A2.3

A2.09E3 

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A4.42E3

A3.42E3

A1.28E3 A1.26E3 A1.72E3 A968.95 A935.83 A73

A298.38

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B07 #1-2851 Acq:16-NOV-2014 05:18:40 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 

A9.51E4

A8.33E4

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 

A2.58E4

A1.36E4

A7.30E3

A6.63E3

A1.04E3 A1.76E3 A1.91E3 A1.89E3 A1.57E3 A1.16E3 A840.33

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 

A8.95E4

A8.36E4

A2.56E3

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 

A2.36E4

A1.32E4

A6.64E3

A6.12E3

A825.50 A1.17E3 A909.74 A728.97 A474.00

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B07 #1-2851 Acq:16-NOV-2014 05:18:40 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.37E7 

7:34

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,12020.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.67E6 

7:34

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,3156.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.86E5 

7:32

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,144.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.23E4 

7:32

A2.28E3

7:48

A3.03E

9:14

A2.79E3

7:29

A2.01E3

8:33

A1.95E3

7:18

A1.17E3

8:49

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,224.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:12 7:26 7:34 7:49 7:56 8:03 8:11 8:19 8:28 8:40 8:51 8:59 9:10 9:

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.95E6 

8:44

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,252.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.83E6 

8:44

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,364.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.01E5 

8:50

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.77E4 

8:50

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:12 7:26 7:34 7:49 7:56 8:03 8:11 8:19 8:28 8:40 8:51 8:59 9:10 9:

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.89E6 

10:11

A3.35E5

10:28

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.02E5 

10:11

A9.51E4

10:28

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.69E6 

10:25

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.09E5 

10:25

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:56 10:02 10:15 10:26 10:36 10:44 10:58 11:06 11:15 11:24 11:36 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.08E5 

10:28

A1.02E5

10:00

A6.24E4

9:49

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,152.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.08E5 

10:28

A2.62E5

10:11

A8.52E4

9:54

A4.79E4

11:25

A5.18E4

10:05

A4.32E4

10:33

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,272.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.81E6 

10:25

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.83E6 

10:25

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:56 10:02 10:15 10:26 10:36 10:44 10:58 11:06 11:15 11:24 11:36 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.54E5 

11:19

A3.26E4

11:25

A1.98E4

11:09

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.16E5 

11:19

A5.32E4

10:27

A5.95E4

11:24

A2.94E4

11:09

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.14E4 

11:16

A1.15E4

11:19

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.04E5 

11:16

A1.70E4

11:22

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:56 10:02 10:15 10:26 10:36 10:44 10:58 11:06 11:15 11:24 11:36 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.43E7 

12:51

A3.51E6

12:56

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.37E6 

12:51

A2.64E5

12:56

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.60E5 

12:49

A3.76E4

13:00

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.96E4 

12:54

A6.13E3

12:56

A3.94E3

15:00

A2.05E3

13:47

A1.92E3

12:27

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 13:04 13:18 13:42 14:09 14:53 15:08 15:24 15:39 

12:08 12:31 12:45 13:56 14:25 14:42

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.09E7 

14:47

A8.47E6

15:10

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.89E6 

14:47

A1.50E6

15:10

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.38E6 

15:08

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.49E6 

15:08

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 13:04 13:18 13:42 14:09 14:53 15:08 15:24 15:39 

12:08 12:31 12:45 13:56 14:25 14:42

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.66E6 

17:37

A3.14E5

17:33

A1.55E5

16:59

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A6.46E5 

17:37

A6.98E4

16:59

A6.24E4

17:12

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.52E5 

17:34

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A3.89E4 

17:34

A1.43E3

17:40

A1.08E3

16:55

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:36 16:48 17:01 17:19 17:34 17:52 18:10 18:21 18:32 18:49 18:58 19

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A3.63E5 

19:45

A3.24E5

20:15

A2.59E5

19:47

A6.57E4

19:53

A3.99E4

20:22

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.70E5 

19:44

A6.67E4

20:15

A1.08E4

20:21

A6.55E3

19:56

A5.00E3

20:07

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A5.39E6 

20:11

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.11E6 

20:11

A4.57E4

20:17

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:35 19:43 19:53 20:11 20:19 20:28 20:41 20:52 21:02 21:10 21:19 21:34 

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.08E4 

22:48

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.27E4 

22:48

A1.82E3

22:15

A1.65E3

22:40

A1.16E3

26:06

A1.26E3

26:39

A1.48E3

24:23

A888.39

25:21

A1.06E3

23:06

A421.79

23:50

A380.83

24:53

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A7.17E4 

22:45

A3.86E4

22:21

A5.96E3

22:51

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A8.33E3 

22:45

A5.05E3

22:25

A2.43E3

22:55

A669.44

24:09

A632.46

25:58

A445.21

23:20

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:09 22:29 22:54 23:21 23:46 24:26 24:45 25:08 25:34 26:07 26:27 26:53 

24:05

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.59E3 

22:27

A4.30E3

22:17

A3.39E3

22:47

A976.79

22:58

A600.01

25:22

A486.62

26:16

A466.49

23:47

A368.13

24:36

A291.19

25:47

A327.38

26:42

A211

27:

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.11E3 

22:29

A946.14

24:56

A91

27

A799.01

22:31

A668.10

24:13

A502.62

25:31

A544.52

26:42

A438.70

22:56

A350.96

24:40

A281.00

26:05

A407.38

23:25

A157.29

23:57

A148.33

25:16

A151.94

22:12

A55.41

22:46

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.12E4 

22:26

A7.91E3

22:30

A873.29

22:45

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.94E3 

22:25

A2.45E3

22:31

A1.41E3

26:01

A1.11E3

22:12

A601.79

24:02

A676.86

22:47

A618.66

25:35

A354.14

23:23

A261.79

25:07

A276.25

26:47

A202.09

24:32

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:09 22:29 22:54 23:21 23:46 24:26 24:45 25:08 25:34 26:07 26:27 26:53 

24:05

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A9.10E4 

15:35

A8.80E3

15:44

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A1.66E4 

15:35

A1.11E3

15:41

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 13:42 14:53 

12:45 13:04 13:18 13:44 14:09 14:25 14:54 15:08 15:24 15:39 

12:08 12:31 13:02 13:27 13:58 14:39 15:13 15:45 

12:34

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13

%

0 

20 40 60 80 

100 120 140 

A1.43E7

A3.51E6

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13

%

0 

20 40 60 80 

100 120 140 

A1.37E6

A2.64E5

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13

%

0 

20 40 60 80 

100 120 140 

13:04 

12:25 12:31 12:37 12:41 12:45 12:47 12:51 12:53 12:57 13:02 13:09 

12:34 12:54 13:

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13

%

0 

20 40 60 80 

100 120 140 

A1.44E7

A3.56E6

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13

%

0 

20 40 60 80 

100 120 140 

A1.36E6

A2.40E5

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13:16 

%

0 

20 40 60 80 

100 120 140 

A3.51E6

A9.45E4 A1.15E5

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13:16 

%

0 

20 40 60 80 

100 120 140 

A2.64E5

A1.56E4 A2.22E4 A1.73E4 

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13:16 

%

0 

20 40 60 80 

100 120 140 

A3.56E6

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13:16 

%

0 

20 40 60 80 

100 120 140 

A2.40E5

A1.06E4 A1.21E4

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A3.63E5

A2.59E5

A6.57E4

A2.13E4

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A1.70E5

A6.63E3 A6.55E3 A2.77E3 

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

19:24 19:28 19:33 19:35 19:37 19:41 19:43 19:46 19:50 19:53 19:56 20:00 

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A7.30E5

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A1.60E5

A9.13E3 A4.67E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A2.59E5

A6.57E4

A2.13E4 A1.31E4

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A6.55E3 A6.63E3 A2.77E3 A5.00E

A5.60E3 A2.57E3 A3.70E3

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A1.75E4

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A9.13E3 A4.67E3 A4.23E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A3.24E5

A2.59E5

A6.57E4 A3.99E4

A2.13E4 A1.15E4

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A6.67E4

A9.25E3 A1.08E4

A6.55E3 A1.64E4

A2.77E3 A5.00E3 A3.72E3 A3.70E3 A2.36E3 A1.38E

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A3.05E5

A5.36E4

A1.75E4

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A5.95E4

A4.92E3 A4.67E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 

%

0 

20 40 60 80 

100 120 140 

A6.57E4

A3.99E4

A2.13E4

A1.15E4 A1.91E4

A3.42E3

A2.99E3 A3.11E3 

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 

%

0 

20 40 60 80 

100 120 140 

A1.64E4

A6.55E3

A4.33E3

A2.77E3 A3.72E3

A5.00E3

A2.36E3 A3.70E3

A2.98E3

A1.43E3 A1.90E3 A1.84E3 A2.72

A1.19E3 

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 

%

0 

20 40 60 80 

100 120 140 

A5.36E4

A1.75E4

A9.81E3 A4.58E3 A1.14E4

A2.15E3

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 

%

0 

20 40 60 80 

100 120 140 

A3.92E3

A1.44E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A1.15E4

A1.91E4

A3.42E3

A2.99E3

A3.11E3 A2.32E3 

A2.12E3 

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 A2.36E3 

A3.70E3

A2.98E3

A1.90E3

A1.43E3

A1.38E3

A2.72E3

A1.19E3 A820

A823.00 

A573.60 

A818.49 

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A9.81E3

A4.58E3 A1.14E4

A5.24E3

A2.15E3

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22

%

0 

20 40 60 80 

100 120 140 

A4.01E4

A1.99E3 A911.95

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22

%

0 

20 40 60 80 

100 120 140 

A7.11E3

A7.98E3

A1.82E3 A1.65E3 

A1.46E3 A1.30E3

A1.34E3 A1.18E3 A1.08E3 A851.50

A228.33

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22

%

0 

20 40 60 80 

100 120 140 

A4.12E4

A7.50E3 A1.01E4

A2.19E3 A3.36E3

A1.99E3 A912.17 A935.21 A1.06E3

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22

%

0 

20 40 60 80 

100 120 140 

A6.71E3

A7.45E3

A1.69E3

A1.13E3 A1.30E3 A811.38 

A1.17E3 A761.94 A887.80 A764.99

A174.59

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A3.59E3

A4.30E3

A2.37E3 A3.39

A652.82 

A476.02

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A799.01

A777.72

A324.66 A402.97

A153.03

A151.94 A119.25

A55.41

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

22:06 22:22 22:29 22:43 

22:09 22:13 22:19 22:24 22:27 22:32 22:35 22:45 22:15 22:39

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A4.62E3

A3.79E3 A3.56E3

A4.28E3 A3.14E3

A2.36E3 A2.82E3 A2.90

A2.36E3

A1.05E3 

A654.00 A718.56 A476.06 

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A920.20

A883.64

A456.43 

A541.87 A227.31 A300.02 A170.76

A86.77

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23:08 

%

0 

20 40 60 80 

100 120 140 

A5.08E4

A4.01E4

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23:08 

%

0 

20 40 60 80 

100 120 140 

A1.27E4

A7.11E3

A7.98E3

A1.65E3 A1.25E3 A1.30E3 A1.18E3 A1.08E3 A1.06E3 A595.92 A1.05E3 

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23:08 

%

0 

20 40 60 80 

100 120 140 

A4.99E4

A4.12E4

A7.50E3

A2.96E3 A3.36E3 A2.47E3

A935.21 A1.06E3

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23:08 

%

0 

20 40 60 80 

100 120 140 

A1.13E4

A6.71E3

A7.45E3

A1.13E3

A811.38 A783.79 A887.80 A764.99

A296.71

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B08 #1-2852 Acq:16-NOV-2014 05:52:53 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A5.52E6 

7:34

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,7876.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A6.50E5 

7:34

A2.76E4

7:09

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1416.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.13E5 

7:32

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,8.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.68E4 

7:32

A3.25E3

7:24

A2.32E3

7:47

A2.45E3

8:13

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,268.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:11 7:21 7:31 7:40 7:49 7:59 8:12 8:22 8:31 8:45 8:55 9:09 9:

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.44E6 

8:44

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,332.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.39E6 

8:44

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,336.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A8.37E4 

8:49

A4.19E3

8:46

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A8.54E4 

8:49

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:11 7:21 7:31 7:40 7:49 7:59 8:12 8:22 8:31 8:45 8:55 9:09 9:

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.29E5 

10:10

A2.10E5

10:27

A7.02E4

9:53

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.61E5 

10:10

A6.36E4

10:28

A2.26E4

9:53

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.62E6 

10:24

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.15E5 

10:24

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 10:00 10:08 10:17 10:25 10:36 10:47 11:04 11:12 11:28 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.13E5 

10:27

A3.74E4

9:53

A3.20E4

10:04

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,184.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.85E5 

10:27

A7.06E4

9:53

A5.33E4

10:10

A3.24E4

11:24

A1.86E4

10:41

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,236.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.71E6 

10:24

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.66E6 

10:24

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 10:00 10:08 10:17 10:25 10:36 10:47 11:04 11:12 11:28 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.89E5 

11:18

A5.29E4

11:24

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.07E5 

11:18

A4.81E4

11:24

A3.26E4

10:27

A1.82E4

10:37

A2.06E4

11:38

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.44E4 

11:15

A7.42E3

11:22

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.02E4 

11:15

A1.10E4

11:19

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 10:00 10:08 10:17 10:25 10:36 10:47 11:04 11:12 11:28 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A6.46E6 

12:51

A1.39E6

12:54

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A6.25E5 

12:51

A5.66E4

12:55

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.67E5 

12:49

A1.50E4

13:04

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.19E4 

12:48

A2.32E3

15:04

A2.08E3

13:29

A1.20E3

15:23

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:19 12:52 13:26 14:12 14:46 15:16 15:41 1

12:33 13:07 13:52 14:27 15:01 15:5

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.57E6 

14:47

A2.16E6

15:10

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.21E5 

14:47

A3.71E5

15:10

A2.78E4

13:21

A2.20E4

14:53

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.11E6 

15:08

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.54E6 

15:08

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:19 12:52 13:26 14:12 14:46 15:16 15:41 1

12:33 13:07 13:52 14:27 15:01 15:5

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.62E6 

17:37

A2.75E5

17:34

A1.51E5

16:59

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A3.86E5 

17:36

A6.16E4

16:59

A1.20E4

17:12

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.50E5 

17:33

A5.19E3

17:45

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.70E4 

17:33

A7.84E3

17:36

A5.19E3

17:38

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:36 16:47 17:03 17:16 17:33 17:42 17:54 18:07 18:18 18:27 18:37 18:53 19:

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.88E5 

19:44

A1.94E5

20:14

A1.28E5

19:48

A1.58E4

20:21

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A8.77E4 

19:45

A4.59E4

20:14

A4.76E3

19:51

A5.05E3

20:20

A3.29E3

20:07

A3.05E3

20:31

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A3.91E6 

20:11

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A8.82E5 

20:11

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:39 19:50 20:00 20:14 20:24 20:34 20:46 20:59 21:10 21:18 21:26 21:34 

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.91E4 

22:48

A3.77E3

22:14

A1.42E3

23:07

A578.95

25:49

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.08E3 

22:23

A4.66E3

22:49

A2.03E3

22:51

A1.45E3

22:14

A1.13E3

26:52

A759.33

25:32

A684.27

26:23

A634.90

24:59

A637.61

23:12

A489.71

22:41

A418.78

23:38

A296.62

24:25

A1

2

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.78E4 

22:45

A2.70E3

24:36

A1.68E3

23:19

A915.27

22:13

A539.01

26:49

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A8.23E3 

22:45

A3.10E3

22:22

A2.44E3

22:48

A

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:19 22:45 23:04 23:24 23:44 24:08 24:28 25:06 25:39 26:15 26:40 2

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A8.07E3 

22:30

A2.11E3

22:34

A533.54

23:06

A554.94

26:41

A495.27

22:20

A740.00

26:00

A638.

27:0

A410.22

25:03

A378.02

25:27

A230.11

24:34

A422.83

23:33

A140.27

23:59

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A799.31 

22:26

A687.55

23:05

A

A768.88

24:18

A606.91

23:50

A809.51

26:10

A409.37

26:43

A554.08

25:22

A448.45

23:24

A371.27

22:50

A428.36

24:40

A43

27

A214.22

22:17

A247.38

26:18

A185.20

25:34

A130.86

23:56

A100.30

25:07

A135.51

26:49

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.43E4 

22:27

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.19E3 

22:28

A1.89E3

22:58

A1.23E3

24:27

A1.15E3

22:23

A1.02E3

26:11

A627.78

27:01

A835.72

23:23

A548.14

24:08

A1.04E3

22:18

A447.17

24:54

A414.35

22:44

A307.00

26:06

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:19 22:45 23:04 23:24 23:44 24:08 24:28 25:06 25:39 26:15 26:40 2

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A8.79E4 

15:34

A5.80E3

15:44

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A1.89E4 

15:35

A1.27E3

15:43

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 14:12 

12:19 12:52 13:26 14:06 14:22 14:46 15:16 15:41 1

12:15 12:33 12:51 13:07 13:30 13:45 14:54 15:12 15:26 

12:35 14:26 15:5

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 

%

0 

20 40 60 80 

100 120 140 

A2.75E5

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 

%

0 

20 40 60 80 

100 120 140 

A1.77E4 A1.20E4 A8.00E3 A4.01E3 A4.32E3 

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 

%

0 

20 40 60 80 

100 120 140 

17:06 17:09 17:13 17:16 17:20 17:22 17:25 17:27 17:29 17:33 17:36 17:40 17:42 17:46 17:49 17:51 17:5

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 

%

0 

20 40 60 80 

100 120 140 

A6.82E4

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 

%

0 

20 40 60 80 

100 120 140 

A1.51E4 A1.04E4 A6.51E3 A3.36E3

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 17

%

0 

20 40 60 80 

100 120 140 

A1.62E6

A2.75E5

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 17

%

0 

20 40 60 80 

100 120 140 

A3.86E5

A1.20E4 A8.00E3

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 17

%

0 

20 40 60 80 

100 120 140 

A1.85E6

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 17

%

0 

20 40 60 80 

100 120 140 

A3.75E5

A1.04E4

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A2.88E5

A1.28E5

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A8.77E4

A4.76E3

A5.57E3

A1.70E3 A2.17E3 A2.13E3 A3.47E3 

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

19:24 19:28 19:31 19:36 19:39 19:44 19:50 19:56 20:00 20:03 2

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A4.56E5

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A9.17E4

A5.47E3 A4.16E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 

%

0 

20 40 60 80 

100 120 140 

A1.28E5

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 

%

0 

20 40 60 80 

100 120 140 

A4.76E3

A7.51E3

A5.57E3

A1.70E3 A2.29E3 A3.47E3 A3.29E3

A2.17E3 A1.42E3 A2.13E3 A1.19E3

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 

%

0 

20 40 60 80 

100 120 140 

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 

%

0 

20 40 60 80 

100 120 140 

A4.16E3

A5.47E3

A1.20E3 A744.48 A1.11E3 A1.12E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 A2.88E5 

A1.94E5

A1.28E5

A1.58E4

A7.29E3

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A8.77E4

A4.59E4

A4.76E3

A5.57E3 A5.05E3 A4.55E3

A2.29E3 A3.47E3 A3.29E3 A2.90E3 A1.82E3 A3.05E3 

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A1.75E5

A8.91E3

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A3.36E4

A4.16E3

A1.43E3 A851.93

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A1.58E4

A7.29E3

A4.55E3 A2.68E3

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A2.14E3

A1.57E3

A3.05E3

A1.82E3

A1.17E3 A1.37E3

A652.82

A683.0

A445.56

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A8.91E3

A7.59E3

A2.64E3

A1.98E3

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A851.93

A1.12E3

A186.69

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A7.29E3

A4.55E3 A2.68E3

A2.62E3 A1.59E3

A3.98E3 

A1.49E

A673.13 

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A1.17E3

A652.82

A683.09 A493.49

A445.56 A50

A264.21

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A1.98E3

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 

%

0 

20 40 60 80 

100 120 140 

A851.93

A186.69

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 

%

0 

20 40 60 80 

100 120 140 

A9.86E4

A7.81E4 A3.41E4

A1.69E4 

A7.92E3 A9.70E3 

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 

%

0 

20 40 60 80 

100 120 140 

A1.84E4 A2.03E4

A1.19E4

A9.47E3 A6.79E3

A4.28E3 A8.97E3

A3.73E3 A

A2.67E3 

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 

%

0 

20 40 60 80 

100 120 140 

A5.10E4 A8.84E4

A1.86E4 A1.57E4 A7.82E3 A1.70E4 

264.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 

%

0 

20 40 60 80 

100 120 140 

A1.73E4 A3.01E4

A1.16E4

A9.52E3

A7.24E3 A8.88E3

A3.19E3 A4

A2.35E3 

265.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20

%

0 

20 40 60 80 

100 120 140 

A7.81E4

A3.41E4

A2.83E4

A1.69E4

A9.28E3

A1

A7.92E3 

A3.15E3

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20

%

0 

20 40 60 80 

100 120 140 

A1.84E4 A2.03E4

A1.19E4

A9.47E3

A6.79E3

A4.28E3 A8.97E3

A3.73E3 A4.29E3

A3.59E3 A2.68E3 

A600.1

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20

%

0 

20 40 60 80 

100 120 140 

A5.10E4 A8.84E4

A5.64E4

A1.86E4 A1.57E4

A1.18E4 A1

A6.38E3 

264.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20

%

0 

20 40 60 80 

100 120 140 

A1.73E4 A3.01E4

A1.16E4

A9.52E3

A7.24E3

A8.88E3

A3.19E3 A4.14E3

A3.76E3 A2.83E3 

265.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20

%

0 

20 40 60 80 

100 120 140 

A3.91E6

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20

%

0 

20 40 60 80 

100 120 140 

A8.82E5

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20

%

0 

20 40 60 80 

100 120 140 

A4.10E6

264.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20

%

0 

20 40 60 80 

100 120 140 

A8.83E5

265.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B09 #1-2851 Acq:16-NOV-2014 06:27:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.15E4 

7:38

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1144.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,384.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.54E3 

7:32

A620.69

7:24

A418.74

8:43

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.58E3 

8:41

A2.54E3

8:02

A

A1.50E3

7:26

A1.11E3

7:54

A1.03E3

8:14

A1.11E3

9:01

A1.14E3

7:41

A423.66

8:44

A259

9:

A130.55

8:23

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:18 7:27 7:36 7:48 8:01 8:09 8:18 8:26 8:40 8:47 9:04 9:14 

7:08

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B10 #1-2850 Acq:16-NOV-2014 07:01:33 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.13E4 

8:54

A1.60E3

8:31

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,312.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.07E4 

8:54

A1.30E3

8:35

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,412.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 

A17.43

8:30

A14.14

7:32

A18.24

8:35

A7.31

8:21

A7.89

9:13

A9.45

8:58

A11.62

8:46

A13.19

7:12

A6.74

8:03

A4.98

7:54

A3.00

7:45

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A137.61 

8:32

A97.25

7:12

A35.00

8:36

A1

9

A13.56

7:45

A8.65

8:59

A4.57

7:15

A7.19

8:00

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:18 7:27 7:36 7:48 8:01 8:09 8:18 8:26 8:40 8:47 9:04 9:14 

7:08

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B10 #1-2850 Acq:16-NOV-2014 07:01:33 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 

A1.18E4

10:10

A6.06E3

9:50

A3.67E3

11:33

A4.32E3

10:28

A4.67E3

10:49

A3.96E3

10:38

A3.41E3

10:03

A1.47E3

11:23

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 

A1.80E3

10:10

A1.05E3

9:50

A677.82

11:36

A773.01

10:37

A474.30

10:21

A475.17

10:53

A266.10

11:12

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.53E3 

10:24

A951.04

10:31

A622.59

10:08

A481.62

11:22

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A182.63 

10:24

A66.79

10:26

A87.67

9:47

A130.05

10:02

A72.69

10:15

A

A22.02

10:38

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:55 10:10 10:19 10:27 10:42 10:57 11:11 11:18 11:33 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B10 #1-2850 Acq:16-NOV-2014 07:01:33 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 

A4.89E3

9:55

A1.59E3

10:07

A1.47E3

10:23

A1.62E3

11:24

A1.13E3

11:11

A963.0

11:39

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,148.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 

A1.63E3

9:48

A1.95E3

10:41

A1.38E

11:39

A1.67E3

11:24

A589.67

10:23

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,212.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.56E3 

10:24

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.00E4 

10:24

A923.89

11:10

A669.67

10:29

A355.24

10:53

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:55 10:10 10:19 10:27 10:42 10:57 11:11 11:18 11:33 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B10 #1-2850 Acq:16-NOV-2014 07:01:33 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 

A4.12E3

11:19

A3.83E3

9:53

A2.60E3

10:29

A1.59E3

10:56

A1.96E

11:39

A1.05E3

11:22

A835.23

9:49

A710.46

10:15

A745.61

10:39

A383.75

10:28

A487.86

9:59

A290.31

11:07

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 

A4.38E3

11:19

A8.37E3

9:52

A6.23E3

10:15

A5.69E3

10:38

A2.63E3

11:33

A3.91E3

10:49

A

A1.26E3

10:27

A467.46

9:55

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A56.03 

9:47

A46.16

9:58

A82.39

10:23

A42.46

10:12

A52.05

10:27

A23.96

10:38

A3.3910:51

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A101.56 

10:30

A94.39

9:48

A117.56

9:59

A66.93

10:13

A54.80

10:24

A38.06

10:52

A42.79

10:35

A

A13.71

11:25

A3.9010:57

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:55 10:10 10:19 10:27 10:42 10:57 11:11 11:18 11:33 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B10 #1-2850 Acq:16-NOV-2014 07:01:33 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.29E4 

12:51

A1.00E4

12:19

A1.31E4

12:57

A4.15E3

12:26

A2.19E3

13:16

A2.3

15:

A3.56E3

15:19

A2.51E3

14:35

A1.11E3

14:13

A983.17

13:46

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.84E3 

12:54

A1.92E3

12:19

A1.49E3

14:27

A1.08E3

14:04

A1.01E3

13:41

A1.26E3

13:03

A1.16E3

15:18

A756.17

12:21

A355.31

14:48

A516.18

15:37

A499.72

13:32

A133.35

14:14

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A147.97 

13:27

A126.23

12:13

A44.40

12:32

A3

1

A17.64

15:26

A11.14

15:01

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.02E3 

15:00

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:45 12:59 13:30 13:44 14:07 14:21 14:41 14:55 15:30 

12:17 12:31 13:14 14:24 14:58 15:15 15:46 

13:28

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B10 #1-2850 Acq:16-NOV-2014 07:01:33 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.90E4 

15:10

A2.03E4

14:48

A5.82E3

14:59

A2.45E3

15:24

A4.56E3

14:21

A1.59E3

13:30

A1.32E3

12:39

A1.17E3

12:14

A1.61E3

13:53

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A5.67E3 

14:48

A2.65E3

15:11

A1.22E3

13:01

A1.3

15:

A1.22E3

14:15

A2.06E3

13:22

A832.40

12:30

A930.86

12:10

A740.99

14:42

A1.12E3

13:42

A589.03

15:32

A400.19

15:06

A212.82

12:58

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.54E4 

15:08

A2.72E3

15:15

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A955.97 

15:08

A237.02

15:13

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:45 12:59 13:30 13:44 14:07 14:21 14:41 14:55 15:30 

12:17 12:31 13:14 14:24 14:58 15:15 15:46 

13:28

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B10 #1-2850 Acq:16-NOV-2014 07:01:33 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.31E5 

16:59

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A5.24E4 

16:59

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.40E3 

17:40

A810.45

17:44

A330.33

17:31

A70.58

17:51

A129.90

16:44

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A514.27 

17:38

A382.60

18:30

A322.27

17:53

A288.44

16:59

A170.01

18:08

A162.76

17:40

A157.74

16:41

A56.77

17:13

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:36 16:47 17:01 17:13 17:25 17:46 17:55 18:06 18:21 18:39 18:51 19:00 

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B10 #1-2850 Acq:16-NOV-2014 07:01:33 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.50E3 

19:49

A1.09E3

20:19

A757.00

20:01

A462.35

20:50

A667.09

21:14

A400.23

20:40

A348.67

20:25

A447.49

21:32

A272.00

20:11

A522.50

19:36

A233.05

21:04

A98.73

20:52

A82.9

21:3

A44.01

21:16

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A521.00 

19:53

A620.17

21:26

A683.50

20:16

A321.33

20:39

A337.94

21:33

A707.59

21:14

A406.00

19:50

A282.05

20:59

A230.47

20:28

A332.50

20:01

A334.00

20:12

A144.50

19:42

A75.60

21:11

A118.74

20:41

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A6.00E3 

20:13

A1.75E3

20:16

A1.54E3

20:35

A1.05E3

19:47

A725.09

20:49

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A90.02 

21:02

A39.76

20:13

A69.86

21:31

A20.58

19:35

A18

21

A39.64

19:45

A24.32

21:22

A11.75

21:03

A12.50

20:05

A10.76

19:55

A9.4020:53

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:35 19:45 19:55 20:05 20:13 20:21 20:30 20:43 20:57 21:06 21:16 21:33 21

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B10 #1-2850 Acq:16-NOV-2014 07:01:33 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.45E3 

26:08

A1.01E3

22:47

A637.87

26:43

A580.88

23:32

A383.63

24:13

A584.45

25:07

A363.51

22:54

A349.09

26:00

A529.72

22:29

A411.45

26:53

A228.08

25:10

A261.20

24:08

A121.16

24:34

A125.70

26:26

A124.01

23:24

A59.60

25:54

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A596.77 

26:54

A516.46

24:47

A605.08

26:24

A432.40

25:23

A642.74

23:59

A576.86

22:22

A454.12

23:27

A

A350.92

24:37

A233.71

26:05

A344.88

22:48

A280.30

25:19

A531.77

22:14

A117.87

23:48

A71.21

26:59

A133.79

23:14

A93.43

24:25

A98.40

22:28

A28.39

25:07

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.36E3 

22:27

A528.48

25:15

A50.85

23:46

A100.45

22:22

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A567

27:

A182.40

26:48

A294.51

22:24

A107.95

25:37

A62.59

25:08

A82.69

23:05

A22.07

23:50

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:17 22:37 23:05 23:28 23:59 24:21 24:46 25:04 25:23 25:43 26:05 26:30 26:48 2

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B10 #1-2850 Acq:16-NOV-2014 07:01:33 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A934.17 

22:41

A587.20

26:30

A624.59

25:41

A463.76

24:55

A455.4

27:04

A395.02

26:35

A328.91

25:55

A273.91

24:23

A287.30

22:44

A246.73

24:57

A212.

27:0

A165.05

23:57

A142.43

26:20

A242.21

22:15

A190.10

23:11

A68.16

25:31

A53.76

25:06

A31.47

24:27

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.12E3 

25:13

A1.10

27:0

A876.93

24:40

A1.11E3

23:57

A745.70

22:32

A439.40

25:23

A403.47

24:28

A480.64

23:01

A393.54

23:31

A290.16

26:07

A236.01

26:42

A353.34

24:55

A303.35

22:26

A129

27:

A103.66

25:32

A119.78

24:08

A109.41

23:05

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A384.83 

25:22

A593.81

22:35

A296.10

22:29

A107.23

22:25

A36.52

25:24

A83.62

23:11

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 

A711.49

25:36

A829.11

24:44

A581.66

22:38

A337.03

26:22

A291.87

26:48

A242.22

25:30

A145.15

24:32

A99.67

22:13

A196.35

22:40

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:17 22:37 23:05 23:28 23:59 24:21 24:46 25:04 25:23 25:43 26:05 26:30 26:48 2

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B10 #1-2850 Acq:16-NOV-2014 07:01:33 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A441.56 

13:50

A72.97

12:11

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A90.93 

12:08

A64.52

12:14

A42.11

12:25

A12.36

13:53

A12.51

14:20

A18.

15:5

A20.42

12:36

A18.57

15:30

A15.13

15:11

A10.41

14:45

A7.9012:43

A4.0714:27

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 12:59 13:30 14:21 14:55 

12:45 13:44 14:07 14:41 15:30 

12:17 12:31 13:19 13:53 14:33 14:59 15:15 15:46 

13:01 

12:18

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B10 #1-2850 Acq:16-NOV-2014 07:01:33 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.21E7 

7:34

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,10032.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.52E6 

7:34

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,2396.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.18E5 

7:32

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.75E4 

7:32

A3.56E3

7:35

A2.19E3

7:47

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,328.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:09 7:22 7:31 7:39 7:47 7:57 8:04 8:11 8:20 8:31 8:38 8:51 9:00 9:14 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.66E6 

8:43

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,528.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.55E6 

8:44

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1900.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A8.05E4 

8:49

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A7.19E4 

8:49

A3.56E3

8:45

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:09 7:22 7:31 7:39 7:47 7:57 8:04 8:11 8:20 8:31 8:38 8:51 9:00 9:14 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.66E6 

10:10

A2.98E5

10:27

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.36E5 

10:10

A8.56E4

10:27

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.45E6 

10:24

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.05E5 

10:24

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:59 10:06 10:15 10:25 10:35 10:45 10:54 11:05 11:19 11:29 11:38 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.86E5 

10:27

A9.86E4

10:00

A7.90E4

9:49

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.83E5 

10:27

A2.02E5

10:10

A8.92E4

9:53

A5.29E4

10:04

A2.80E4

11:24

A3.06E4

10:41

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,252.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.47E6 

10:24

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.58E6 

10:24

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:59 10:06 10:15 10:25 10:35 10:45 10:54 11:05 11:19 11:29 11:38 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.35E5 

11:18

A3.43E4

11:24

A1.51E4

11:09

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.61E5 

11:18

A3.87E4

10:27

A4.91E4

11:24

A2.66E4

11:09

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.41E4 

11:15

A5.89E3

11:23

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.41E4 

11:15

A5.28E3

11:22

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:59 10:06 10:15 10:25 10:35 10:45 10:54 11:05 11:19 11:29 11:38 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.16E7 

12:50

A3.20E6

12:55

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.09E6 

12:50

A2.08E5

12:55

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.43E5 

12:48

A1.63E4

13:02

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.89E4 

12:48

A5.53E3

12:56

A1.99E3

14:58

A928.55

13:32

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 14:07 14:38 14:52 15:11 15

12:12 12:33 12:47 13:10 13:40 14:23 15:25 15:41 

13:25 13:59

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A6.82E6 

14:47

A5.56E6

15:09

A6.01E5

14:57

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.22E6 

14:47

A9.75E5

15:09

A1.06E5

14:57

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.82E6 

15:08

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.63E6 

15:07

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 14:07 14:38 14:52 15:11 15

12:12 12:33 12:47 13:10 13:40 14:23 15:25 15:41 

13:25 13:59

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A6.99E5 

17:36

A1.30E5

16:59

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.51E5 

17:37

A5.46E4

16:59

A1.60E4

17:06

A8.57E3

17:47

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.37E5 

17:33

A6.26E3

17:43

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.56E4 

17:33

A2.08E3

17:41

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:37 16:47 17:03 17:23 17:41 17:52 18:12 18:29 18:42 18:54 

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.32E5 

19:45

A1.09E5

20:14

A5.88E4

19:47

A1.45E4

20:23

A3.96E3

20:01

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.64E4 

19:44

A2.15E4

20:14

A7.48E3

19:50

A5.04E3

20:21

A890.50

20:04

A1.15E3

20:39

A595.81

21:19

A889.01

20:50

A693.00

19:38

A527.45

21:32

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A4.25E6 

20:11

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A8.11E5 

20:11

A1.05E5

20:15

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:34 19:49 19:59 20:06 20:16 20:31 20:42 20:54 21:09 21:20 21:34 

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.23E4 

22:48

A1.20E4

22:24

A2.03E3

22:57

A977.52

26:22

A510.12

23:39

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.64E3 

22:47

A3.22E3

22:30

A1.97E3

23:00

A624.15

26:17

A5

2

A480.84

25:27

A525.50

22:14

A410.76

23:45

A357.20

25:02

A263.93

24:23

A452.82

23:18

A101.34

26:46

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.10E4 

22:45

A1.36E3

23:03

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A7.47E3 

22:46

A738.18

24:46

A820.96

23:06

A746.01

22:26

A2

2

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:17 22:44 23:11 23:31 23:53 24:17 24:52 25:18 25:39 25:58 26:16 26:38 27:00 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.53E3 

22:29

A1.38E3

22:20

A538.20

23:08

A469.90

24:15

A425.23

25:40

A400.94

25:10

A789.98

26:13

A643

27

A358.11

22:14

A153.41

24:42

A133.43

23:36

A220.07

26:39

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.02E3 

22:05

A530.10

24:40

A644.16

23:02

A553.13

22:20

A9

2

A727.29

24:15

A593.59

25:32

A375.43

26:44

A329.43

23:42

A235.95

26:11

A248.86

23:00

A195.00

24:57

A291

27:

A245.34

24:28

A116.27

22:34

A48.12

23:49

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A7.81E3 

22:27

A867.83

23:56

A337.23

26:02

A434.45

22:58

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.69E3 

22:52

A1.08E3

24:15

A1.31E3

22:12

A885.47

26:04

A681.41

24:58

A884.66

23:27

A874.58

22:32

A522.

27:0

A353.12

25:37

A307.83

22:57

A197.66

23:36

A185.67

26:20

A106.69

25:00

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:17 22:44 23:11 23:31 23:53 24:17 24:52 25:18 25:39 25:58 26:16 26:38 27:00 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A7.61E4 

15:35

A1.02E4

15:41

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A1.12E4 

15:34

A4.77E3

15:38

A1.08E3

15:40

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 15

14:38 14:52 15:11 15:44 

14:07 15:27 

12:12 12:33 12:47 13:10 13:40 14:33 15:02 

13:36 13:58 14:16

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:20 12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 

%

0 

20 40 60 80 

100 120 140 

A1.16E7

A3.20E6

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

12:20 12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 

%

0 

20 40 60 80 

100 120 140 

A1.09E6

A2.08E5

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

12:20 12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 

%

0 

20 40 60 80 

100 120 140 

12:26 12:33 12:38 12:41 12:47 12:50 12:57 13:01 13:10 

12:23 12:35 12:52 12:55 13:06

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

12:20 12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 

%

0 

20 40 60 80 

100 120 140 

A1.15E7

A3.46E6

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

12:20 12:22 12:24 12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 

%

0 

20 40 60 80 

100 120 140 

A1.09E6

A1.98E5

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13

%

0 

20 40 60 80 

100 120 140 

A3.20E6

A7.87E4

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13

%

0 

20 40 60 80 

100 120 140 

A2.08E5

A3.06E4

A3.08E4 A1.41E4

A1.62E4 A4.78

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13

%

0 

20 40 60 80 

100 120 140 

A3.46E6

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

12:26 12:28 12:30 12:32 12:34 12:36 12:38 12:40 12:42 12:44 12:46 12:48 12:50 12:52 12:54 12:56 12:58 13:00 13:02 13:04 13:06 13:08 13:10 13:12 13:14 13

%

0 

20 40 60 80 

100 120 140 

A1.98E5

A2.68E4

A2.51E4 A1.10E4

A1.16E4

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17

%

0 

20 40 60 80 

100 120 140 

A6.99E5

A3.53E5

A7.74E4

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17

%

0 

20 40 60 80 

100 120 140 

A1.51E5

A7.10E4

A1.19E4 A3.71E3 A8.57E3 A6.32E3

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17

%

0 

20 40 60 80 

100 120 140 

17:06 17:08 17:11 17:16 17:18 17:23 17:28 17:31 17:36 17:39 17:41 17:43 17:45 17:52 17

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17

%

0 

20 40 60 80 

100 120 140 

A1.06E6

A7.23E4

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17

%

0 

20 40 60 80 

100 120 140 

A1.39E5

A6.38E4

A7.72E3 A4.29E3

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17

%

0 

20 40 60 80 

100 120 140 

A6.99E5

A3.53E5

A7.74E4

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17

%

0 

20 40 60 80 

100 120 140 

A1.51E5

A7.10E4

A1.19E4 A3.71E3 A8.57E3 A4.30E3 A6.32E3

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17

%

0 

20 40 60 80 

100 120 140 

A1.06E6

A7.23E4

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17

%

0 

20 40 60 80 

100 120 140 

A1.39E5

A6.38E4

A7.72E3 A4.29E3

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A1.32E5

A5.88E4

A3.96E3

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A2.64E4

A1.47E4

A7.48E3

A3.92E3 A2.73E3 A2.65E3 A1.38E3 A1.98E3 A693.00 A1.26E3 A890.50 

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

19:27 19:30 19:34 19:37 19:44 19:49 19:51 19:55 19:59 20:02 20:04 

19:42

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A2.25E5

A4.81E3

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A2.56E4

A1.35E4

A6.29E3

A3.18E3

A2.52E3 A1.34E3 A2.13E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A5.88E4

A3.96E3 A2.65E3 A

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 A2.64E4 

A1.47E4 

A7.48E3

A3.92E3

A2.73E3

A2.65E3 A1.38E3 A1.98E3 A1.26E3 A890.50 A1

A1.11E3 A693.00

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A4.81E3 A6.62E3

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 A2.56E4 

A1.35E4

A6.29E3

A3.18E3

A2.52E3 A2.13E3 A1.34E3

A519.91

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A1.09E5

A5.88E4

A1.45E4

A3.96E3 A5.03E3 A2.65E3 

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A2.64E4

A1.47E4 A2.15E4

A7.48E3

A5.04E3 A3.92E3 A2.88E3

A2.73E3 A3.50E3

A1.98E3 A2.64E3 A890.50 A1.21E3 A1.32E3 A1.72E3 

A926.46 

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A9.64E4

A9.81E3

A4.81E3 A6.62E3 A2.87E3 A4.03E3

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A1.35E4

A1.74E4

A6.29E3

A3.18E3

A3.69E3

A2.13E3

A519.91

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20

%

0 

20 40 60 80 

100 120 140 

A1.45E4

A5.03E3

A3.96E3

A3.01E3 A4.10E3

A1.83E3 A2.54E3 

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20

%

0 

20 40 60 80 

100 120 140 

A3.92E3

A2.88E3

A3.50E3

A2.73E3

A1.55E3

A2.64E3 A1.98E3

A1.32E3 A1.72E3 A890.50 A1.21E3 A1.15E3

A984.11 

A1.04E3 A573.23 

A926.46

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20

%

0 

20 40 60 80 

100 120 140 

A9.81E3

A4.81E3

A6.62E3

A2.87E3

A4.03E3

A583.80 A462.12

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20

%

0 

20 40 60 80 

100 120 140 

A2.13E3

A519.91

A350.44

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 A5.03E3 

A3.01E3

A2.65E3 A4.10E3

A1.83E3

A2.54E3

A2.

A1.05E3 

A408.19 

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

A1.32E3 A1.72E3

A890.50

A1.21E3 A1.15E3

A965.79

A1.04E3 A984.11 A889.01

A926.46 A573.23

A659.48

A435.68

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 A4.03E3 

A583.80

A462.12

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 

%

0 

20 40 60 80 

100 120 140 

A1.20E4

A768.30 A840.06

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 

%

0 

20 40 60 80 

100 120 140 

A4.46E3 

A3.22E3

A1.31E3 

A913.83 A959.81

A573.22 A507.93

A455.17 A247.

A273.00

A208.83 A194.62

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 

%

0 

20 40 60 80 

100 120 140 

A1.33E4

A7.30E3

A3.84E3

A1.99E3 A2.17E3

A1.39E3

A919.00 A768.52 A839.83 A1.16E3

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 

%

0 

20 40 60 80 

100 120 140 

A4.34E3

A3.04E3

A1.26E3

A913.83 

A831.01

A738.23

A442.04

A352.65 A273.00 A177.

A208.83

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22

%

0 

20 40 60 80 

100 120 140 

A1.53E3

A1.52E3 A1.38E3

A497.38 A358.11

A230.42 A155.56

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141118mb

after_modification

22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22

%

0 

20 40 60 80 

100 120 140 

A309.17

A257.16 A286.31

A196.4

A180.49 A116.27

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22

%

0 

20 40 60 80 

100 120 140 

22:08 22:14 22:17 22:20 22:25 22:28 22:33 22:36 22:39 22:42 22:44 22:46 22:49 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22

%

0 

20 40 60 80 

100 120 140 

A2.02E3

A2.41E3

A1.70E3

A1.48E3 A1.39E3

A1.51E3 A1.33E3 A1.02E3 A991.07 A1.50E

A498.19 A

A357.33 A460.59

A230.00 

A155.67

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22

%

0 

20 40 60 80 

100 120 140 A252.47 

A183.74 A200.26 A163.7

A81.34 

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23:08 

%

0 

20 40 60 80 

100 120 140 

A2.23E4

A1.20E4

A2.03E3

A1.48E3 A1.35E3 

A687.04

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23:08 

%

0 

20 40 60 80 

100 120 140 

A2.64E3

A4.46E3 A2.29E3

A3.22E3

A1.31E3 A1.09E3 A1.97E3 A959.81

A680.28

A507.93

A455.17 A247.60 A397.50 

A231.81 

A79.2

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23:08 

%

0 

20 40 60 80 

100 120 140 

A2.85E4

A1.33E4

A7.30E3

A3.84E3

A1.98E3 A2.17E3 A1.37E3

A919.00 A634.04

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23:08 

%

0 

20 40 60 80 

100 120 140 

A2.41E3

A4.34E3

A2.13E3

A3.04E3

A1.26E3

A909.77

A831.01 A1.51E3

A487.00 A442.04

A352.65

A177.69 A201.57 

A79.91

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B11 #1-2851 Acq:16-NOV-2014 07:35:56 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.49E8 

7:35

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,169000.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A6.75E7 

7:35

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,26816.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A8.51E6 

7:33

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1244.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.67E5 

7:33

A8.38E4

7:42

A6.24E4

8:33

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,2604.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:08 7:20 7:29 7:36 7:45 7:57 8:07 8:14 8:25 8:38 8:49 9:02 9:12 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B12 #1-2851 Acq:16-NOV-2014 08:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A6.95E7 

8:44

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,15716.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A6.30E7 

8:44

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,20444.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.15E6 

8:50

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.83E6 

8:50

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,424.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:08 7:20 7:29 7:36 7:45 7:57 8:07 8:14 8:25 8:38 8:49 9:02 9:12 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B12 #1-2851 Acq:16-NOV-2014 08:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.67E8 

10:11

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.58E7 

10:11

A3.05E6

10:28

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.13E6 

10:09

A3.70E6

10:25

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.13E6 

10:09

A6.59E5

10:25

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:55 10:06 10:20 10:28 10:37 10:46 10:59 11:10 11:19 11:31 11:4

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B12 #1-2851 Acq:16-NOV-2014 08:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.01E7 

10:28

A4.17E6

10:00

A1.10E6

9:50

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,816.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.34E7 

10:28

A6.88E6

10:11

A2.75E6

9:54

A2.07E6

11:25

A1.16E6

10:42

A1.36E6

10:05

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,912.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.09E6 

10:25

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.24E6 

10:25

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:55 10:06 10:20 10:28 10:37 10:46 10:59 11:10 11:19 11:31 11:4

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B12 #1-2851 Acq:16-NOV-2014 08:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.45E7 

11:19

A9.11E5

11:09

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.59E7 

11:19

A2.31E6

10:28

A1.77E6

11:09

A2.04E6

11:25

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.38E6 

11:16

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.28E6 

11:16

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:55 10:06 10:20 10:28 10:37 10:46 10:59 11:10 11:19 11:31 11:4

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B12 #1-2851 Acq:16-NOV-2014 08:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.44E8 

12:51

A7.21E7

12:56

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A5.72E7 

12:51

A5.12E6

12:56

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.37E7 

12:49

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.30E5 

12:49

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:55 14:49 15:37 15

12:18 12:33 13:14 13:35 13:50 14:11 14:28 15:14 

12:48

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B12 #1-2851 Acq:16-NOV-2014 08:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.88E8 

14:48

A3.45E8

15:11

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A7.26E7 

14:48

A5.38E7

15:11

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.67E6 

15:09

A7.00E6

14:46

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.76E6 

15:09

A1.25E6

14:46

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:55 14:49 15:37 15

12:18 12:33 13:14 13:35 13:50 14:11 14:28 15:14 

12:48

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B12 #1-2851 Acq:16-NOV-2014 08:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.60E8 

17:36

A3.62E7

17:32

A1.08E7

17:06

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.84E7 

17:36

A1.11E7

17:32

A4.28E6

17:11

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.01E7 

17:33

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.15E6 

17:33

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:35 16:50 17:02 17:12 17:24 17:34 17:44 18:01 18:17 18:28 18:37 18:53 

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B12 #1-2851 Acq:16-NOV-2014 08:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A5.04E7 

19:44

A2.38E7

20:15

A1.97E7

19:47

A7.48E6

20:21

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.22E7 

19:44

A6.10E6

20:15

A4.06E6

19:47

A1.83E6

20:21

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.27E7 

20:12

A9.72E6

19:45

A7.61E6

20:27

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.83E6 

20:11

A2.12E6

19:45

A1.65E6

20:27

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:40 19:55 20:10 20:22 20:30 20:42 20:54 21:06 21:14 21:26 21:35 

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B12 #1-2851 Acq:16-NOV-2014 08:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A6.86E6 

22:47

A6.59E6

22:22

A1.38E6

22:13

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.75E6 

22:47

A3.84E5

22:13

A2.98E5

22:39

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A6.84E6 

22:44

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.58E6 

22:44

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:19 22:38 22:57 23:18 23:40 23:58 24:31 25:08 25:53 26:15 26:38 26:57 

25:31 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B12 #1-2851 Acq:16-NOV-2014 08:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.47E6 

22:26

A9.56E5

22:14

A2.68E5

22:31

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.74E5 

22:26

A3.51E5

22:39

A2.04E4

22:20

A1.89E4

22:50

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.52E6 

22:23

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.04E6 

22:23

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:19 22:38 22:57 23:18 23:40 23:58 24:31 25:08 25:53 26:15 26:38 26:57 

25:31 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B12 #1-2851 Acq:16-NOV-2014 08:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A4.74E6 

15:35

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A8.87E5 

15:35

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 15

12:55 15:37 

12:18 12:33 13:00 13:14 13:35 13:50 14:28 14:49 15:14 1

12:44 14:11 14:47 15:02 15:29 15:47 

12:14 13:20 13:38 14:26 14:42

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B12 #1-2851 Acq:16-NOV-2014 08:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A5.04E7

A1.97E7

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A1.22E7

A4.06E6

A1.44E6

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

19:24 19:31 19:34 19:40 19:51 19:55 20:00 2

19:28 19:38 19:42 19:45 

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A6.88E7

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A1.56E7

A1.35E6

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B12 #1-2851 Acq:16-NOV-2014 08:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A1.97E7

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A4.06E6

A1.44E6

A6.65E5

A7.01E5 A4.54

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A1.40E6

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A1.35E6

A5.46E5

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B12 #1-2851 Acq:16-NOV-2014 08:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A2.38E7

A1.97E7

A7.48E6

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A6.10E6

A4.06E6

A1.83E6

A4.54E5 A5.30E5

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A2.34E7

A6.39E6

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A5.54E6

A1.17E6

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B12 #1-2851 Acq:16-NOV-2014 08:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A7.48E6

A1.29E6

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A1.83E6

A4.54E5 A5.30E5 A7.01E5

A3.49E4

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A6.39E6

A1.40E6 A7.75E5

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A1.17E6

A1.85E5 A1.04E5 A1.00E5

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B12 #1-2851 Acq:16-NOV-2014 08:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

A1.29E6

A2.55E5

A2.57E5 A8.94E4

A6.69E4 A1.06E5 A5.

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

A4.54E5

A5.30E5

A3.49E4 A7.47E4 A4.47E4 A5.00E4 A4.04E4 

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

A7.75E5

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B12 #1-2851 Acq:16-NOV-2014 08:10:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-7 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.03E8 

7:35

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,115132.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.92E7 

7:35

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,34636.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A8.98E6 

7:33

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1560.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.63E5 

7:33

A8.21E4

8:33

A8.29E4

7:41

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,3880.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:07 7:16 7:25 7:35 7:46 7:53 8:09 8:20 8:28 8:36 8:47 8:55 9:02 9:12 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B13 #1-2852 Acq:16-NOV-2014 08:44:36 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A7.52E7 

8:45

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,3500.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A6.90E7 

8:45

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,4392.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.55E6 

8:42

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,8.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.26E6 

8:51

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,204.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:07 7:16 7:25 7:35 7:46 7:53 8:09 8:20 8:28 8:36 8:47 8:55 9:02 9:12 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B13 #1-2852 Acq:16-NOV-2014 08:44:36 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.22E7 

10:11

A8.16E6

10:28

A4.73E6

9:47

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.38E6 

10:11

A2.61E6

10:28

A1.31E6

9:47

A6

1

A4.62E5

9:57

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.06E6 

10:09

A3.16E6

10:26

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.04E6 

10:09

A5.05E5

10:26

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 10:02 10:14 10:28 10:35 10:44 10:56 11:10 11:19 11:30 11:38 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B13 #1-2852 Acq:16-NOV-2014 08:44:36 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.33E6 

10:28

A1.47E6

10:00

A8.77E5

9:47

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.21E7 

10:28

A2.87E6

9:54

A3.15E6

10:11

A1.91E6

11:25

A1.15E6

10:33

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,636.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.06E6 

10:25

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.17E6 

10:25

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 10:02 10:14 10:28 10:35 10:44 10:56 11:10 11:19 11:30 11:38 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B13 #1-2852 Acq:16-NOV-2014 08:44:36 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.23E7 

11:19

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.33E7 

11:19

A2.05E6

10:28

A1.54E6

11:25

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.98E6 

11:16

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.02E6 

11:16

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 10:02 10:14 10:28 10:35 10:44 10:56 11:10 11:19 11:30 11:38 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B13 #1-2852 Acq:16-NOV-2014 08:44:36 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.32E8 

12:51

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.63E7 

12:51

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.35E7 

12:49

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.68E5 

12:49

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:26 12:44 13:00 13:23 13:43 14:04 14:18 14:35 15:05 15:24 15:48 

12:08 12:46 14:00 14:33 15:22

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B13 #1-2852 Acq:16-NOV-2014 08:44:36 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.09E8 

14:48

A7.91E7

15:11

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.64E7 

14:48

A1.24E7

15:11

A1.49E6

14:10

A1.01E6

13:21

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A6.91E6 

15:09

A6.27E6

14:46

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.20E6 

15:09

A1.08E6

14:46

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:26 12:44 13:00 13:23 13:43 14:04 14:18 14:35 15:05 15:24 15:48 

12:08 12:46 14:00 14:33 15:22

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B13 #1-2852 Acq:16-NOV-2014 08:44:36 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A5.42E7 

17:37

A1.69E7

17:32

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.08E7 

17:37

A4.42E6

17:32

A9.34E5

17:11

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A4.85E6 

17:33

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A9.47E5 

17:33

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:45 16:54 17:07 17:23 17:39 17:59 18:16 18:26 18:39 18:52 19:0

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B13 #1-2852 Acq:16-NOV-2014 08:44:36 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.65E7 

19:44

A7.87E6

20:15

A5.89E6

19:47

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A4.08E6 

19:44

A1.92E6

20:15

A1.35E6

19:47

A3.33E5

20:21

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A3.62E6 

20:12

A3.55E6

19:45

A2.31E6

20:28

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A8.05E5 

20:12

A5.67E5

19:41

A4.77E5

20:28

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:37 19:49 20:05 20:13 20:23 20:32 20:45 20:53 21:03 21:12 21:28 

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B13 #1-2852 Acq:16-NOV-2014 08:44:36 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.78E6 

22:48

A2.03E6

22:23

A4.16E5

22:13

A1.96E5

22:40

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.09E5 

22:23

A4.13E5

22:48

A1.19E5

22:13

A8.40E4

22:39

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.94E6 

22:45

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.46E5 

22:45

A2.49E4

22:27

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:24 22:50 23:15 23:37 24:12 24:33 24:58 25:18 25:42 26:03 26:23 26:42 27:01 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B13 #1-2852 Acq:16-NOV-2014 08:44:36 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A6.25E5 

22:27

A6.83E4

22:47

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.51E5 

22:27

A2.70E4

22:36

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.23E6 

22:24

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.66E5 

22:24

A1.69E4

22:32

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:24 22:50 23:15 23:37 24:12 24:33 24:58 25:18 25:42 26:03 26:23 26:42 27:01 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B13 #1-2852 Acq:16-NOV-2014 08:44:36 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A3.15E6 

15:35

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A5.96E5 

15:35

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 12:44 13:43 14:04 14:35 14:52 15:24 15:48 

12:26 12:53 13:23 13:50 14:18 

12:08 13:06 13:30 14:44 15:02 15:17 15:34 15:

12:22 12:37 14:02 14:33

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B13 #1-2852 Acq:16-NOV-2014 08:44:36 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

A1.69E7

A2.23E6

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

A4.42E6

A9.34E5

A4.37E5

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

A1.67E7

A2.22E6

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

A4.34E6

A8.26E5

A3.97E5

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B13 #1-2852 Acq:16-NOV-2014 08:44:36 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 17

%

0 

20 40 60 80 

100 120 140 

A5.42E7

A1.69E7

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 17

%

0 

20 40 60 80 

100 120 140 

A1.08E7

A4.42E6

A9.34E5

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 17

%

0 

20 40 60 80 

100 120 140 

A5.30E7

A1.67E7

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 17

%

0 

20 40 60 80 

100 120 140 

A1.07E7

A4.34E6

A8.26E5

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B13 #1-2852 Acq:16-NOV-2014 08:44:36 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A1.65E7

A5.89E6

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A4.08E6

A1.35E6

A4.14E5

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A2.19E7

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A5.20E6

A4.25E5

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B13 #1-2852 Acq:16-NOV-2014 08:44:36 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A5.89E6

A6.97E5

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A1.35E6

A4.14E5

A1.89E5

A1.48E5 A1.4

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A4.25E5

A1.46E5

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B13 #1-2852 Acq:16-NOV-2014 08:44:36 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A7.87E6

A5.89E6

A1.25E6

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A1.92E6

A1.35E6

A3.33E5

A1.49E5

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A7.65E6

A9.79E5

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A1.73E6

A1.50E5

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B13 #1-2852 Acq:16-NOV-2014 08:44:36 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A1.25E6

A6.97E5

A3.20E5

A5.18E4 A3.16E4 A3.80E4

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A3.33E5

A1.49E5

A1.48E5

A1.09E5

A2.55E4

A3.07E4

A2.23E4 A2.04E4 

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A9.79E5

A1.30E5

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A1.50E5

A5.54E4 A2.91E4

A7.35E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B13 #1-2852 Acq:16-NOV-2014 08:44:36 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

A3.20E5

A5.18E4

A3.16E4

A3.80E4

A3.01E4 A4.16E4 A2.69E4 

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 A1.49E5 

A1.09E5

A3.07E4

A2.23E4 A2.04E4 A2.04E4

A1.11E4 A9.69E3 

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

A1.30E5

A6.23E3

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

A7.35E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B13 #1-2852 Acq:16-NOV-2014 08:44:36 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22

%

0 

20 40 60 80 

100 120 140 

A2.03E6 

A4.16E5

A1.96E5

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22

%

0 

20 40 60 80 

100 120 140 

A5.09E5 

A1.19E5

A8.40E4 A3.52E4 A1.59E4

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22

%

0 

20 40 60 80 

100 120 140 

22:05 22:13 22:18 22:24 22:36 

22:09 22:28 22:34 22:42

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22

%

0 

20 40 60 80 

100 120 140 

A1.98E6 

A4.19E5

A1.25E5

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22

%

0 

20 40 60 80 

100 120 140 

A5.01E5 

A1.18E5

A3.52E4 A7.14E4 A1.36E4

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B13 #1-2852 Acq:16-NOV-2014 08:44:36 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A6.25E5

A4.99E5

A6

A2.49E4 

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A1.51E5

A7.58E4 A1.03E5

A2.56E4 A2.70E4

A2.14E4

A1.42E4 A1.00E

A1.07E4 

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A6.26E5

A4.80E5 A3.10E5

A6

A2.49E4

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 

%

0 

20 40 60 80 

100 120 140 

A1.32E5

A6.35E4 A9.20E4

A2.03E4 A2.17E4

A1.63E4

A7.12E

A7.91E3 A4.73E3 

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B13 #1-2852 Acq:16-NOV-2014 08:44:36 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-8 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.25E7 

7:34

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,11460.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.57E6 

7:34

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,3096.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.24E5 

7:32

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.16E4 

7:32

A4.51E3

8:32

A2.02E3

7:35

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,368.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:09 7:18 7:30 7:43 7:55 8:03 8:13 8:21 8:28 8:37 8:45 8:59 9:06 9:14 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.10E6 

8:44

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,388.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.90E6 

8:44

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,2344.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A8.34E4 

8:49

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A7.82E4 

8:49

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:09 7:18 7:30 7:43 7:55 8:03 8:13 8:21 8:28 8:37 8:45 8:59 9:06 9:14 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.49E6 

10:10

A3.65E5

10:28

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.38E5 

10:10

A9.67E4

10:28

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.24E6 

10:24

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.71E5 

10:25

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:55 10:04 10:16 10:26 10:33 10:40 10:48 10:58 11:08 11:18 11:27 11:37 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.46E5 

10:28

A7.81E4

10:00

A5.77E4

9:49

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,280.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.55E5 

10:28

A1.68E5

10:10

A9.08E4

9:53

A5.39E4

11:24

A3.30E4

10:41

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,392.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.05E6 

10:24

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.18E6 

10:24

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:55 10:04 10:16 10:26 10:33 10:40 10:48 10:58 11:08 11:18 11:27 11:37 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.09E5 

11:18

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.11E5 

11:18

A6.94E4

11:24

A6.69E4

10:27

A3.92E4

11:09

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.14E5 

11:16

A5.18E3

11:21

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.09E5 

11:16

A7.02E3

11:22

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:55 10:04 10:16 10:26 10:33 10:40 10:48 10:58 11:08 11:18 11:27 11:37 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.52E7 

12:50

A5.05E6

12:56

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.43E6 

12:50

A3.26E5

12:56

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.12E5 

12:48

A4.97E4

12:58

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.01E4 

12:54

A3.32E3

13:02

A1.77E3

12:35

A1.49E3

14:55

A874.94

13:22

A776.50

13:59

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:15 12:29 12:45 13:14 13:38 13:57 14:20 15:05 15:27 15:47 

14:46

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.68E7 

14:47

A1.31E7

15:10

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.10E6 

14:47

A2.54E6

15:10

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.79E6 

15:08

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.78E6 

15:08

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:15 12:29 12:45 13:14 13:38 13:57 14:20 15:05 15:27 15:47 

14:46

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.46E6 

17:36

A3.48E5

17:33

A3.28E5

17:06

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A6.15E5 

17:36

A7.40E4

16:59

A8.05E4

17:12

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.31E5 

17:33

A2.01E4

17:40

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.72E4 

17:30

A2.44E3

17:40

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:38 16:48 16:59 17:09 17:20 17:35 17:48 17:59 18:13 18:23 18:33 18:47 18:57 

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A5.33E5 

19:45

A3.57E5

20:14

A2.70E5

19:47

A6.79E4

20:22

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.18E5 

19:44

A8.40E4

20:14

A5.64E4

19:47

A1.36E4

20:21

A1.07E4

19:53

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A6.91E6 

20:11

A2.96E5

20:16

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.62E6 

20:11

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:54 20:47 21:06 21:16 21:24 21

19:39 20:03 20:21 20:31 20:39 20:56

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.81E4 

22:48

A9.70E3

22:15

A2.01E3

22:59

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.07E4 

22:47

A5.71E3

22:23

A3.93E3

22:51

A1.34E3

26:32

A1

2

A1.36E3

22:18

A745.57

24:46

A553.61

25:40

A614.87

26:04

A896.77

23:19

A519.24

24:19

A389.78

23:48

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A9.39E4 

22:44

A6.68E4

22:21

A4.11E3

22:57

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.30E4 

22:45

A3.87E3

22:23

A5.25E3

22:50

A2.30E3

24:47

A805.96

25:28

A606.01

23:46

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:16 22:41 23:02 23:36 24:06 24:28 24:47 25:12 25:35 25:54 26:20 26:40 27:0

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A9.01E3 

22:28

A2.84E3

22:47

A745.78

26:20

A822.34

23:29

A623.78

26:46

A573.25

25:37

A683

27

A476.95

25:06

A354.90

24:30

A208.85

24:03

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.17E3 

22:28

A639.68

24:14

A916.53

26:52

A927.50

24:55

A568.58

25:32

A982.75

22:17

A552.78

23:18

A441.88

22:48

A787.57

26:06

A692.21

24:23

A520.42

23:53

A311.76

26:40

A232.13

25:15

A257

27:

A194.45

24:49

A38.28

23:11

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.89E4 

22:25

A1.20E4

22:27

A3.58E3

22:38

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.97E3 

22:25

A845.01

23:11

A848.65

25:36

A853.82

22:44

A588.86

25:01

A568

27

A477.48

26:24

A409.67

24:15

A246.13

23:17

A100.64

23:43

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:16 22:41 23:02 23:36 24:06 24:28 24:47 25:12 25:35 25:54 26:20 26:40 27:0

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A1.06E5 

15:35

A7.59E3

15:39

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A2.34E4 

15:35A4.37E3

15:37

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 12:45 13:57 14:20 15:05 15:47 

12:15 12:29 12:53 13:14 13:38 13:59 14:58 15:27 

12:11 12:33 13:17 14:17 14:43 15:41 

12:56

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
10:48 10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 

%

0 

20 40 60 80 

100 120 140 

A5.09E5

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

10:48 10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 

%

0 

20 40 60 80 

100 120 140 

A5.11E5

A3.92E4 A6.94E4 A7.28E4 A2.92E4

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

10:48 10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 

%

0 

20 40 60 80 

100 120 140 

10:51 10:53 10:56 10:58 11:05 11:08 11:10 11:15 11:18 11:24 11:27 11:30 11:37 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

10:48 10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 

%

0 

20 40 60 80 

100 120 140 

A5.10E5

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

10:48 10:50 10:52 10:54 10:56 10:58 11:00 11:02 11:04 11:06 11:08 11:10 11:12 11:14 11:16 11:18 11:20 11:22 11:24 11:26 11:28 11:30 11:32 11:34 11:36 11:38 

%

0 

20 40 60 80 

100 120 140 

A5.11E5

A3.89E4 A6.94E4 A7.30E4 A2.95E4

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17

%

0 

20 40 60 80 

100 120 140 

A3.48E5

A3.28E5

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17

%

0 

20 40 60 80 

100 120 140 

A6.11E4 A8.05E4

A8.74E3 A4.80E3

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17

%

0 

20 40 60 80 

100 120 140 

A3.18E5

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17

%

0 

20 40 60 80 

100 120 140 

A5.26E4 A6.62E4

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A2.46E6

A3.48E5

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A6.15E5

A8.05E4

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A2.81E6

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A5.71E5

A6.62E4

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A5.33E5

A2.70E5

A1.47E4

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A1.18E5

A5.64E4

A1.07E4 A4.47E3 A1.44E4 A4.54E3

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A7.94E5

A2.62E4

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A1.71E5

A5.79E3 A5.75E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A2.70E5

A1.47E4 A9.56E3 A8.34E3

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A5.64E4

A1.07E4 A1.44E4 A4.47E3 A4.54E3

A1.41E3 A3.34E3 A2.09E3 A5.7

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A2.62E4

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A5.79E3 A5.75E3 A2.45E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A3.57E5

A2.70E5

A6.79E4

A1.47E4

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A8.40E4

A5.64E4

A1.36E4 A1.07E4 A1.44E4 A6.10E3 A4.54E3 A5.76E3 A4.87E3 A2.45E3 

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A3.30E5

A5.16E4 A2.62E4

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 

%

0 

20 40 60 80 

100 120 140 

A6.36E4

A6.36E3 A5.75E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 

%

0 

20 40 60 80 

100 120 140 

A6.79E4

A1.47E4

A1.20E4 A9.56E3 A8.34E3

A7.82E3

A3.

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 

%

0 

20 40 60 80 

100 120 140 

A1.07E4

A6.10E3

A1.44E4

A4.54E3

A4.87E3

A5.76E3 A2.45E3

A2.02E3 A1.93E3 A1.71E3 A2.26E3 

A871.73 A

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 

%

0 

20 40 60 80 

100 120 140 

A5.16E4

A2.62E4

A2.47E3 A3.27E3

A2.34E3

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 

%

0 

20 40 60 80 

100 120 140 

A5.75E3

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

A1.20E4

A8.34E3

A4.87E3

A7.82E3

A2.98E3 A3.33E3 A3.78E3

A1

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

A2.45E3

A5.76E3 A2.11E3

A1.93E3 A2.02E3 A1.67E3

A1.71E3 A2.26E3

A2.02E3

A871.73 

A1.05E3 A786.61 

A56

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

A3.27E3

A2.34E3

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22

%

0 

20 40 60 80 

100 120 140 

A3.97E4

A9.70E3

A2.28E3

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22

%

0 

20 40 60 80 

100 120 140 

A5.71E3

A2.20E3 

A2.60E3

A1.36E3 A1.72E3 A2.33E3 A2.45E3 A885.17 A1.21E3

A445.

A371.67

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22

%

0 

20 40 60 80 

100 120 140 

22:16 22:33 22:35 22:41 22:07 22:10 22:20 22:23 22:25 22:31 22:39 

22:13

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22

%

0 

20 40 60 80 

100 120 140 

A4.19E4

A1.32E4

A4.03E3

A2.28E3 A2.93E3 A1.54E3 A967.73

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22

%

0 

20 40 60 80 

100 120 140 

A5.57E3

A2.09E3

A2.60E3

A885.17 A1.20E3 A1.32E3 A1.52E3 A1.94E3 A1.96E3

A371.67 A260.

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 

%

0 

20 40 60 80 

100 120 140 

A9.01E3

A4.72E3

A2.84E3

A1.11E3 

A857.31

A537.34

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 

%

0 

20 40 60 80 

100 120 140 

A1.17E3

A1.11E3

A757.90 A982.75 A484.06 A437.13

A396.35 A441.

A559.23 

A624.59 A543.06 A217.15

A197.60

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 

%

0 

20 40 60 80 

100 120 140 

A1.10E4

A7.39E3

A4.72E3

A3.21E3 A3.07E3

A2.30E3

A1.21E3 A1.05E3 A1.11E3 A1.05E3

A858.17 A657.34 

A535.83 

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 

%

0 

20 40 60 80 

100 120 140 

A973.97

A888.86

A481.35 A647.59 A289.77 A284.24 A313.

A221.27 A271.95

A315.50 A281.88

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23:08 

%

0 

20 40 60 80 

100 120 140 

A5.81E4

A3.97E4

A2.01E3 A2.28E3 A2.05E3

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23:08 

%

0 

20 40 60 80 

100 120 140 

A1.07E4

A5.71E3

A2.20E3 A3.93E3

A1.72E3 A2.33E3 A2.45E3 A1.93E3

A445.65 A435.23 A568.75 A

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23:08 

%

0 

20 40 60 80 

100 120 140 

A5.61E4

A4.19E4

A4.03E3 A2.93E3 A1.54E3 A858.64

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23:08 

%

0 

20 40 60 80 

100 120 140 

A9.89E3

A5.57E3

A2.09E3

A3.32E3

A1.52E3 A1.94E3 A1.96E3 A1.24E3

A260.17

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17

%

0 

20 40 60 80 

100 120 140 

A2.31E5

A1.24E5

A2.01E4

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17

%

0 

20 40 60 80 

100 120 140 

A2.72E4 A3.93E4

A2.44E3 A1.77E3 A1.42E3 A1.52E3

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17

%

0 

20 40 60 80 

100 120 140 

A2.30E5

A1.24E5

A1.99E4

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17

%

0 

20 40 60 80 

100 120 140 

A2.70E4 A3.90E4

A2.37E3 A1.69E3 A1.36E3 A1.46E3

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:12 19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20

%

0 

20 40 60 80 

100 120 140 A1.38E5 

A9.04E4

A1.28E4

A3.78E3 A3.06

A3.27E3

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:12 19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20

%

0 

20 40 60 80 

100 120 140 

A8.85E3

A1.13E4

A3.77E3

A6.60E3

A1.78E3

A1.

A477.90

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:12 19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20

%

0 

20 40 60 80 

100 120 140 

A1.35E5

A8.65E4

A8.06E3

264.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:12 19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20

%

0 

20 40 60 80 

100 120 140 

A1.12E4 A9.37E3

A6.05E3

A1.67E3

A98

265.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A1.38E5

A9.04E4

A1.28E4

A3.78E3 A3.06E3

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A1.77E4

A8.85E3 A1.13E4

A3.77E3

A6.60E3

A1.78E3

A1.10E3

A477.90

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A1.35E5

A8.65E4

A8.06E3

264.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20

%

0 

20 40 60 80 

100 120 140 

A2.12E4

A1.12E4 A9.37E3

A6.05E3

A1.67E3

A985.35

265.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 

%

0 

20 40 60 80 

100 120 140 

A2.96E5

A1.26E5

A1.

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 

%

0 

20 40 60 80 

100 120 140 

A2.97E4

A2.92E4

A3.15E4

A1.78E4

A7.37E3

A6.60E3 

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 

%

0 

20 40 60 80 

100 120 140 

A2.21E5

A4.97E4

264.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 

%

0 

20 40 60 80 

100 120 140 

A3.07E4

A1.74E4

A1.42E4

A6.05E3 

265.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20

%

0 

20 40 60 80 

100 120 140 

A1.26E5

A1.81E4

A2.56E4 A2.77E4

A1.12E4 

A3.06E3

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20

%

0 

20 40 60 80 

100 120 140 

A1.41E4

A7.37E3

A3.80E3

A4.81E3

A2.82E3

A2.38E3 A5.03E3 

A1.65

A1.10E3 

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20

%

0 

20 40 60 80 

100 120 140 

A2.21E5

A4.97E4

A1.68E4 A2.59E4

A7.54E3 

264.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20

%

0 

20 40 60 80 

100 120 140 

A3.07E4

A1.74E4

A1.42E4

A4.14E3

A2.33E3 A4.59E3 

A1.19E3 A985.35 

265.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22

%

0 

20 40 60 80 

100 120 140 

A6.68E4

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22

%

0 

20 40 60 80 

100 120 140 

A1.09E4

A3.87E3

A2.03E3

A1.54E3

A716.10 A438.33

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22

%

0 

20 40 60 80 

100 120 140 

A3.14E4

A3.61E4

A1.02E4

A7.19E3 A4.81E3

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22

%

0 

20 40 60 80 

100 120 140 

A1.09E4

A3.86E3

A2.02E3

A1.52E3

A677.44 A438.33

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 

%

0 

20 40 60 80 

100 120 140 

A9.39E4

A6.68E4

A4.11E3 A2.66E3 

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 

%

0 

20 40 60 80 

100 120 140 

A1.30E4

A1.09E4

A3.87E3

A5.25E3

A2.03E3

A1.54E3

A716.10 A1.25E3

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 

%

0 

20 40 60 80 

100 120 140 

A9.70E4

A3.14E4

A3.61E4

A1.02E4

A7.19E3 A3.58E3 A4.81E3 A2.79E3 A1.90E3 

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 

%

0 

20 40 60 80 

100 120 140 

A1.29E4

A1.09E4

A3.86E3

A5.14E3

A2.02E3

A1.52E3

A677.44 A1.16E3

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B14 #1-2850 Acq:16-NOV-2014 09:18:48 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.13E8 

7:35

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,84120.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A5.76E7 

7:35

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,34156.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A7.69E6 

7:33

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1268.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A8.09E5 

7:33

A6.93E4

8:33

A8.34E4

7:41

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,3108.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:06 7:12 7:21 7:36 7:52 8:00 8:09 8:21 8:31 8:38 8:45 8:54 9:05 9:12 9

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B15 #1-2851 Acq:16-NOV-2014 09:53:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A8.49E7 

8:44

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,2484.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A7.86E7 

8:44

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,7168.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.03E6 

8:50

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.80E6 

8:50

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,116.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:06 7:12 7:21 7:36 7:52 8:00 8:09 8:21 8:31 8:38 8:45 8:54 9:05 9:12 9

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B15 #1-2851 Acq:16-NOV-2014 09:53:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.52E8 

10:11

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.34E7 

10:11

A3.37E6

10:28

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.33E6 

10:09

A3.37E6

10:25

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.79E5 

10:09

A5.79E5

10:25

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:56 10:04 10:12 10:21 10:30 10:37 10:46 10:56 11:04 11:21 11:30 11:38 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B15 #1-2851 Acq:16-NOV-2014 09:53:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.18E7 

10:28

A3.56E6

10:00

A1.01E6

9:50

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,580.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.56E7 

10:28

A7.24E6

10:11

A3.07E6

9:54

A2.32E6

11:25

A1.19E6

10:42

A1.53E6

10:05

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1276.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.71E6 

10:25

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.70E6 

10:25

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:56 10:04 10:12 10:21 10:30 10:37 10:46 10:56 11:04 11:21 11:30 11:38 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B15 #1-2851 Acq:16-NOV-2014 09:53:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.71E7 

11:19

A9.26E5

11:10

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.88E7 

11:19

A2.31E6

10:28

A1.85E6

11:10

A1.97E6

11:25

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.91E6 

11:16

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.88E6 

11:16

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:56 10:04 10:12 10:21 10:30 10:37 10:46 10:56 11:04 11:21 11:30 11:38 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B15 #1-2851 Acq:16-NOV-2014 09:53:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.94E8 

12:51

A8.54E7

12:56

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.58E7 

12:51

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.26E7 

12:49

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.99E5 

12:49

A6.05E4

14:46

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:58 13:38 13:55 14:23 14:40 15:11 15:28 15:48 

12:20 12:43 13:21 14:55 

14:12

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B15 #1-2851 Acq:16-NOV-2014 09:53:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.74E8 

14:48

A4.34E8

15:11

A2.89E7

14:58

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.37E8 

14:48

A9.71E7

15:11

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.05E7 

15:09

A7.36E6

14:46

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.90E6 

15:09

A1.25E6

14:46

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:58 13:38 13:55 14:23 14:40 15:11 15:28 15:48 

12:20 12:43 13:21 14:55 

14:12

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B15 #1-2851 Acq:16-NOV-2014 09:53:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.34E8 

17:36

A4.29E7

17:33

A1.61E7

17:07

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.53E7 

17:36

A1.09E7

17:33

A5.51E6

17:11

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.13E7 

17:33

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.33E6 

17:33

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:36 16:52 17:07 17:25 17:38 17:55 18:13 18:23 18:35 18:50 19:0

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B15 #1-2851 Acq:16-NOV-2014 09:53:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A5.39E7 

19:44

A2.43E7

20:15

A1.55E7

19:47

A5.53E6

20:21

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.26E7 

19:44

A6.12E6

20:15

A3.32E6

19:47

A1.47E6

20:21

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.56E7 

20:12

A1.14E7

19:45

A9.04E6

20:28

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A3.64E6 

20:12

A2.14E6

19:41

A1.98E6

20:28

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:38 19:50 19:59 20:09 20:21 20:35 20:50 21:01 21:09 21:18 21:26 21:3

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B15 #1-2851 Acq:16-NOV-2014 09:53:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.59E6 

22:47

A5.23E6

22:22

A1.16E6

22:13

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.37E6 

22:47

A1.36E6

22:22

A3.40E5

22:13

A2.31E5

22:38

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A8.66E6 

22:44

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.06E6 

22:44

A1.94E6

22:20

A9.51E4

24:48

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:15 22:38 22:59 23:26 23:50 24:21 24:57 25:23 25:48 26:21 26:58 2

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B15 #1-2851 Acq:16-NOV-2014 09:53:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.18E6 

22:26

A9.63E5

22:39

A1.86E5

22:47

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.12E5 

22:26

A2.94E5

22:39

A7.34E4

22:45

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.85E6 

22:23

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.36E6 

22:23

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:15 22:38 22:59 23:26 23:50 24:21 24:57 25:23 25:48 26:21 26:58 2

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B15 #1-2851 Acq:16-NOV-2014 09:53:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A4.90E6 

15:35

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A9.37E5 

15:35

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 15:11 

13:38 13:55 14:23 14:40 15:28 12:58 13:21 15:07 15:48 

12:20 13:44 14:02 15:32 

12:43 13:27 14:19 14:37 1

12:07 12:26 13:06 12:47 14:06

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B15 #1-2851 Acq:16-NOV-2014 09:53:13 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-9 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.86E8 

7:35

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,81948.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A7.20E7 

7:35

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,24448.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A8.82E6 

7:33

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1344.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.28E5 

7:33

A9.70E4

7:41

A5.92E4

8:33

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,3796.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:12 7:20 7:36 7:44 7:57 8:05 8:18 8:29 8:40 8:49 8:56 9:05 9:13 9

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B16 #1-2850 Acq:16-NOV-2014 10:27:30 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A8.31E7 

8:44

A5.70E7

8:54

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A7.69E7 

8:44

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,23876.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.33E6 

8:41

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,4.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.83E6 

8:50

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,188.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:12 7:20 7:36 7:44 7:57 8:05 8:18 8:29 8:40 8:49 8:56 9:05 9:13 9

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B16 #1-2850 Acq:16-NOV-2014 10:27:30 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.88E8 

10:11

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.89E7 

10:11

A3.11E6

10:28

A2.20E6

9:47

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.47E6 

10:09

A3.77E6

10:25

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.98E5 

10:09

A6.52E5

10:25

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:59 10:12 10:21 10:30 10:40 10:49 11:02 11:13 11:22 11:35 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B16 #1-2850 Acq:16-NOV-2014 10:27:30 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.06E7 

10:28

A3.70E6

10:00

A1.06E6

9:50

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,944.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.41E7 

10:28

A9.55E6

10:11

A2.77E6

9:54

A1.85E6

11:25

A1.14E6

10:33

A1.42E6

10:05

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1272.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.24E6 

10:25

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.41E6 

10:25

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:59 10:12 10:21 10:30 10:40 10:49 11:02 11:13 11:22 11:35 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B16 #1-2850 Acq:16-NOV-2014 10:27:30 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.40E7 

11:19

A8.42E5

11:10

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.51E7 

11:19

A2.09E6

10:28

A1.65E6

11:10

A1.82E6

11:28

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.31E6 

11:16

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.25E6 

11:16

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:59 10:12 10:21 10:30 10:40 10:49 11:02 11:13 11:22 11:35 11

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B16 #1-2850 Acq:16-NOV-2014 10:27:30 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.34E8 

12:51

A8.21E7

12:56

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A5.75E7 

12:51

A5.86E6

12:56

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.17E7 

12:49

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A7.89E5 

12:49

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:09 12:54 13:08 13:39 14:05 14:21 14:39 15:12 15:38 15:

12:24 14:00 14:56 13:24

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B16 #1-2850 Acq:16-NOV-2014 10:27:30 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.30E8 

14:48

A2.38E8

15:10

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.92E7 

14:48

A3.36E7

15:10

A4.07E6

14:58

A3.63E6

14:10

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.57E6 

15:08

A5.86E6

14:46

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.70E6 

15:08

A1.02E6

14:46

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:09 12:54 13:08 13:39 14:05 14:21 14:39 15:12 15:38 15:

12:24 14:00 14:56 13:24

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B16 #1-2850 Acq:16-NOV-2014 10:27:30 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A3.02E7 

17:36

A2.69E6

17:07

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A6.29E6 

17:36

A7.07E5

17:11

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A4.88E6 

17:33

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A9.45E5 

17:33

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:36 16:48 16:59 17:19 17:37 17:57 18:15 18:27 18:39 18:57 

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B16 #1-2850 Acq:16-NOV-2014 10:27:30 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A9.22E6 

19:44

A5.10E6

20:15

A4.03E6

19:47

A2.01E6

20:21

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A3.19E6 

19:44

A1.25E6

20:15

A4.84E5

20:21

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A5.45E6 

20:12

A3.11E6

19:45

A2.45E6

20:28

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.20E6 

20:12

A5.28E5

19:41

A5.74E5

20:18

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:37 19:48 19:57 20:07 20:16 20:23 20:33 20:44 20:54 21:05 21:16 21:28 

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B16 #1-2850 Acq:16-NOV-2014 10:27:30 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.74E6 

22:47

A1.64E6

22:22

A3.31E5

22:13

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.12E5 

22:47

A4.04E5

22:22

A9.22E4

22:13

A3.75E4

22:40

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.76E6 

22:45

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.23E5 

22:45

A3.78E5

22:20

A1.79E4

24:48

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:20 22:48 23:09 23:30 24:03 24:24 25:00 25:31 26:01 26:27 26:58 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B16 #1-2850 Acq:16-NOV-2014 10:27:30 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.45E5 

22:27

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A9.40E4 

22:26

A7.81E4

22:40

A6.87E3

22:48

A1.18E4

22:20

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.14E6 

22:23

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.38E5 

22:23

A1.29E4

22:29

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:20 22:48 23:09 23:30 24:03 24:24 25:00 25:31 26:01 26:27 26:58 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B16 #1-2850 Acq:16-NOV-2014 10:27:30 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A2.93E6 

15:35

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A5.97E5 

15:35

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 13:08 14:05 14:21 15:12 15:5

12:09 12:54 13:39 13:54 14:39 14:54 15:36 

12:24 13:17 14:08 14:22 15:21 

12:22 13:24 15:25

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B16 #1-2850 Acq:16-NOV-2014 10:27:30 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
8:14 8:16 8:18 8:20 8:22 8:24 8:26 8:28 8:30 8:32 8:34 8:36 8:38 8:40 8:42 8:44 8:46 8:48 8:50 8:52 8:54 8:56 8:58 9:00 9:02 9:04 

%

0 

20 40 60 80 

100 120 140 

A8.31E7

A5.70E7

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

8:14 8:16 8:18 8:20 8:22 8:24 8:26 8:28 8:30 8:32 8:34 8:36 8:38 8:40 8:42 8:44 8:46 8:48 8:50 8:52 8:54 8:56 8:58 9:00 9:02 9:04 

%

0 

20 40 60 80 

100 120 140 

A7.69E7

A5.53E7

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,23876.0,3.00%,F,T) 

after_modification

8:14 8:16 8:18 8:20 8:22 8:24 8:26 8:28 8:30 8:32 8:34 8:36 8:38 8:40 8:42 8:44 8:46 8:48 8:50 8:52 8:54 8:56 8:58 9:00 9:02 9:04 

%

0 

20 40 60 80 

100 120 140 

8:15 8:18 8:21 8:25 8:29 8:34 8:37 8:40 8:49 8:51 8:53 8:56 9:00 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

8:14 8:16 8:18 8:20 8:22 8:24 8:26 8:28 8:30 8:32 8:34 8:36 8:38 8:40 8:42 8:44 8:46 8:48 8:50 8:52 8:54 8:56 8:58 9:00 9:02 9:04 

%

0 

20 40 60 80 

100 120 140 

A8.25E7

A5.61E7

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,1364.0,3.00%,F,T) 

before_modification

8:14 8:16 8:18 8:20 8:22 8:24 8:26 8:28 8:30 8:32 8:34 8:36 8:38 8:40 8:42 8:44 8:46 8:48 8:50 8:52 8:54 8:56 8:58 9:00 9:02 9:04 

%

0 

20 40 60 80 

100 120 140 

A7.70E7

A5.53E7

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,2392.0,3.00%,F,T) 

before_modification

File:4-141115B16 #1-2850 Acq:16-NOV-2014 10:27:30 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
8:24 8:26 8:28 8:30 8:32 8:34 8:36 8:38 8:40 8:42 8:44 8:46 8:48 8:50 8:52 8:54 8:56 8:58 9:00 9:02 9:04 9:06 9:08 9:10 9:12 9:14 

%

0 

20 40 60 80 

100 120 140 

A5.70E7

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

8:24 8:26 8:28 8:30 8:32 8:34 8:36 8:38 8:40 8:42 8:44 8:46 8:48 8:50 8:52 8:54 8:56 8:58 9:00 9:02 9:04 9:06 9:08 9:10 9:12 9:14 

%

0 

20 40 60 80 

100 120 140 

A7.69E7

A5.53E7

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,23876.0,3.00%,F,T) 

after_modification

8:24 8:26 8:28 8:30 8:32 8:34 8:36 8:38 8:40 8:42 8:44 8:46 8:48 8:50 8:52 8:54 8:56 8:58 9:00 9:02 9:04 9:06 9:08 9:10 9:12 9:14 

%

0 

20 40 60 80 

100 120 140 

A5.61E7

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,1364.0,3.00%,F,T) 

before_modification

8:24 8:26 8:28 8:30 8:32 8:34 8:36 8:38 8:40 8:42 8:44 8:46 8:48 8:50 8:52 8:54 8:56 8:58 9:00 9:02 9:04 9:06 9:08 9:10 9:12 9:14 

%

0 

20 40 60 80 

100 120 140 

A5.53E7

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,2392.0,3.00%,F,T) 

before_modification

File:4-141115B16 #1-2850 Acq:16-NOV-2014 10:27:30 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A9.22E6

A4.03E6

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A3.19E6

A3.08E5

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

19:25 19:28 19:33 19:37 19:57 20:0

19:31 19:35 19:41 19:43 19:48 19:52 20:01 

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A1.33E7

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A3.07E6

A3.34E5

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B16 #1-2850 Acq:16-NOV-2014 10:27:30 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A4.03E6

A5.61E5

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A3.08E5

A1.23E5 A1.91E5 A1.

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A5.28E5

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A3.34E5

A1.03E5 A9.37E4 A3.

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B16 #1-2850 Acq:16-NOV-2014 10:27:30 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A1.64E6

A3.31E5

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A4.04E5

A9.22E4

A3.83E4 A3.75E4 A1.29E4 A8.92E3

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

22:06 22:12 22:20 22:26 22:30 22:32 22:36 22:39 22

22:09 22:15 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A1.59E6

A3.30E5

A1.28E5

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 

%

0 

20 40 60 80 

100 120 140 

A3.95E5

A9.17E4

A3.83E4 A2.80E4 A1.17E4

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B16 #1-2850 Acq:16-NOV-2014 10:27:30 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A3.45E5

A2.23E5

A1.21E4

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A9.40E4

A6.57E4

A7.81E4

A2.72E4

A1.16E4

A2.27E4 A1.33E4

A7.63E3 A1.18E4 A6.8

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A3.82E5

A2.23E5 A3.02E5

A7.35E4

A6.69E4

A5.04

A1.21E4 A8.55E3

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A8.81E4

A5.96E4

A7.25E4

A2.46E4

A1.03E4

A2.01E4

A7.29E3 A1.11E4

A8.65E3 A5.6

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B16 #1-2850 Acq:16-NOV-2014 10:27:30 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 

A1.74E6

A1.64E6

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 

A4.12E5

A4.04E5

A3.75E4 A2.88E4

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 

A1.61E6

A1.59E6

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23

%

0 

20 40 60 80 

100 120 140 

A3.97E5

A3.95E5

A2.80E4

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B16 #1-2850 Acq:16-NOV-2014 10:27:30 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-10 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.21E8 

7:34

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,14760.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.25E7 

7:35

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,7776.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.00E5 

7:33

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.42E4 

7:33

A4.39E3

8:32

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,612.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:14 7:24 7:36 7:47 7:55 8:03 8:11 8:21 8:28 8:36 8:50 9:01 9:13 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B17 #1-2852 Acq:16-NOV-2014 11:01:47 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A8.13E6 

8:44

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,484.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A7.56E6 

8:44

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1012.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A7.66E4 

8:50

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A6.55E4 

8:50

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:04 7:14 7:24 7:36 7:47 7:55 8:03 8:11 8:21 8:28 8:36 8:50 9:01 9:13 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B17 #1-2852 Acq:16-NOV-2014 11:01:47 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.25E7 

10:10

A3.55E6

10:28

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.32E6 

10:10

A1.13E6

10:28

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.83E6 

10:25

A1.94E5

10:09

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.99E5 

10:25

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 10:00 10:10 10:17 10:24 10:38 10:47 10:55 11:03 11:12 11:19 11:28 11:38 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B17 #1-2852 Acq:16-NOV-2014 11:01:47 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.37E6 

10:28

A8.96E5

10:00

A3.57E5

9:50

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,304.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.41E6 

10:28

A2.01E6

10:10

A4.73E5

10:00

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,504.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.64E6 

10:25

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.68E6 

10:25

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 10:00 10:10 10:17 10:24 10:38 10:47 10:55 11:03 11:12 11:19 11:28 11:38 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B17 #1-2852 Acq:16-NOV-2014 11:01:47 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.88E6 

11:19

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.28E6 

11:19

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.86E4 

11:16

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.07E4 

11:16

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 10:00 10:10 10:17 10:24 10:38 10:47 10:55 11:03 11:12 11:19 11:28 11:38 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B17 #1-2852 Acq:16-NOV-2014 11:01:47 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.02E8 

12:51

A5.83E7

12:56

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.06E7 

12:51

A4.70E6

12:56

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.28E5 

12:49

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.41E4 

12:49

A3.47E3

12:35

A3.06E3

14:56

A3.37E3

13:17

A2.81E3

15:21

A2.84E3

14:08

A1.19E3

12:11

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:35 13:08 13:35 13:55 15:05 15:27 

12:20 12:51 13:53 14:09 14:28 14:47 15:19 15:43

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B17 #1-2852 Acq:16-NOV-2014 11:01:47 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.16E8 

14:48

A3.67E8

15:10

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.29E7 

14:48

A6.05E7

15:10

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A6.05E6 

15:08

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.07E6 

15:08

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:35 13:08 13:35 13:55 15:05 15:27 

12:20 12:51 13:53 14:09 14:28 14:47 15:19 15:43

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B17 #1-2852 Acq:16-NOV-2014 11:01:47 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A3.57E7 

17:36

A1.40E7

17:33

A4.39E6

17:06

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A7.50E6 

17:36

A3.36E6

17:32

A1.14E6

17:11

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.02E5 

17:33

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.84E4 

17:33

A5.50E3

16:55

A1.15E3

17:38

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:39 16:58 17:07 17:18 17:30 17:43 17:58 18:08 18:21 18:31 18:51 19:0

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B17 #1-2852 Acq:16-NOV-2014 11:01:47 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A4.29E6 

19:44

A2.20E6

19:47

A1.90E6

20:15

A8.69E5

20:21

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.50E6 

19:44

A4.53E5

20:15

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.77E6 

20:11

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A5.74E5 

20:11

A3.40E4

20:18

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:34 19:44 19:56 20:12 20:24 20:40 20:51 21:08 21:18 21:30 21

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B17 #1-2852 Acq:16-NOV-2014 11:01:47 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.93E5 

22:48

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.80E4 

22:48

A5.35E3

22:29

A2.58E3

22:56

A1.55E3

26:26

A1.35E3

25:53

A682.66

24:09

A536.57

24:52

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.41E4 

22:45

A5.36E3

22:28

A2.13E3

22:54

A1.43E

27:04

A2.05E3

24:38

A1.30E3

25:08

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.44E3 

22:46

A2.55E3

22:20

A1.66E3

24:20

A1.38E3

22:28

A1.26E3

26:08

A874.50

25:40

A614.15

23:04

A

A180.16

26:11

A234.93

23:35

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:38 23:05 23:24 23:44 24:18 24:42 25:02 25:31 25:51 26:15 26:36 27

22:18

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B17 #1-2852 Acq:16-NOV-2014 11:01:47 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.07E4 

22:27

A5.69E3

22:44

A1.49E3

25:15

A2.27E3

22:58

A897.35

26:58

A767.90

26:31

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.78E3 

22:14

A3.11E3

22:44

A923.69

22:12

A797.26

24:51

A1.21E3

22:37

A1.06E3

24:14

A1.41E3

25:54

A1.09E3

25:21

A687.06

26:21

A601.47

23:07

A35

27

A354.80

23:40

A202.47

24:44

A228.69

24:17

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A7.72E3 

22:25

A1.47E3

23:30

A317.66

24:52

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.91E3 

26:50

A1.16E3

23:59

A1.14E3

22:21

A1.65E3

23:02

A1.32E3

25:00

A1.43E3

25:33

A727.22

22:27

A5

2

A567.89

24:19

A501.78

23:42

A605.35

23:17

A350.87

26:38

A129.96

24:45

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:38 23:05 23:24 23:44 24:18 24:42 25:02 25:31 25:51 26:15 26:36 27

22:18

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B17 #1-2852 Acq:16-NOV-2014 11:01:47 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A6.06E4 

15:35

A2.85E3

15:41

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A1.26E4 

15:35

A1.85E3

15:39

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 15:05 

12:35 13:02 13:35 13:55 14:28 14:55 15:27 

12:16

12:20 12:58 13:16 13:42 14:09 14:33 14:50 15:12 15:35 

12:48 13:57 15:19 15:44

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B17 #1-2852 Acq:16-NOV-2014 11:01:47 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17

%

0 

20 40 60 80 

100 120 140 

A1.40E7

A4.39E6

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17

%

0 

20 40 60 80 

100 120 140 

A3.36E6

A8.46E5 A1.14E6

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17

%

0 

20 40 60 80 

100 120 140 

A1.40E7

A4.37E6

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17

%

0 

20 40 60 80 

100 120 140 

A3.30E6

A8.09E5 A1.04E6

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B17 #1-2852 Acq:16-NOV-2014 11:01:47 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A3.57E7

A1.40E7

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A7.50E6

A3.36E6

A1.14E6

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A3.47E7

A1.40E7

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 

%

0 

20 40 60 80 

100 120 140 

A7.38E6

A3.30E6

A1.04E6

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B17 #1-2852 Acq:16-NOV-2014 11:01:47 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A4.29E6

A2.20E6

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A1.50E6

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A6.63E6

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A1.47E6

A6.67E4

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B17 #1-2852 Acq:16-NOV-2014 11:01:47 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A2.20E6 

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141116mb

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A5.77E4 A2.56E4 A2.99E4

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A6.67E4 A1.86E4 A2.35E4

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B17 #1-2852 Acq:16-NOV-2014 11:01:47 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A1.07E4

A5.69E3

A2.02E3 A1.41E3 

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A2.78E3

A3.25E3

A2.80E3

A3.25E3 A3.11E3

A1.71E3

A923.69 A1.21E3

A1.25E

A1.12E3 A733.53 A749.42 A677.60

A690.95 A361.89 

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A2.33E4

A1.89E4

A1.55E4

A1.14E4

A4.01E3 A4.34E3

A6.72E3

A3.80E3 A1.93E3

A2.02E3 A1.41E3 

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A2.85E3

A3.28E3

A2.88E3

A3.26E3 A3.02E3

A1.67E3

A986.29 A1.18E3

A1.14E

A818.55 A1.18E3 A700.74 A719.28

A794.87

A357.57 

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B17 #1-2852 Acq:16-NOV-2014 11:01:47 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23:08 

%

0 

20 40 60 80 

100 120 140 

A1.93E5

A1.61E5

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23:08 

%

0 

20 40 60 80 

100 120 140 

A3.80E4

A1.77E4

A1.72E4

A5.35E3 A4.75E3

A2.89E3 A3.52E3 A2.58E3 A2.06E3 A1.34E3 A1.78E3 A1.53E3 A1.28E3

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23:08 

%

0 

20 40 60 80 

100 120 140 

A1.79E5

A1.59E5

A9.42E3 A7.04E3

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23:08 

%

0 

20 40 60 80 

100 120 140 

A3.42E4

A1.72E4

A1.67E4

A4.87E3

A3.50E3

A2.43E3 A2.21E3 A936.34 A1.47E3 A1.08E3 A887.35 A626.99

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B17 #1-2852 Acq:16-NOV-2014 11:01:47 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-1 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.15E7 

7:35

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,11528.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.00E7 

7:35

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1776.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.58E5 

7:32

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.37E4 

7:32

A2.34E3

7:38

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,520.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:16 7:26 7:37 7:49 8:02 8:11 8:19 8:33 8:42 8:56 9:09 9:1

7:04

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A7.32E6 

8:44

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,444.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A6.76E6 

8:44

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,564.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A7.59E4 

8:50

A4.65E4

8:41

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A7.19E4 

8:50

A4.38E4

8:41

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:16 7:26 7:37 7:49 8:02 8:11 8:19 8:33 8:42 8:56 9:09 9:1

7:04

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.64E7 

10:10

A2.50E6

10:28

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.77E6 

10:10

A7.69E5

10:28

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.81E6 

10:25

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.00E5 

10:25

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:52 10:05 10:13 10:25 10:35 10:45 10:58 11:09 11:19 11:28 11:38 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.99E6 

10:28

A9.20E5

10:00

A3.49E5

9:50

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,248.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.64E6 

10:28

A1.39E6

10:10

A3.57E5

10:00

A3.04E5

9:50

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,300.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.36E6 

10:25

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.45E6 

10:25

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:52 10:05 10:13 10:25 10:35 10:45 10:58 11:09 11:19 11:28 11:38 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.59E6 

11:19

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.15E6 

11:19

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.67E4 

11:16

A6.37E3

11:20

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.18E4 

11:16

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:52 10:05 10:13 10:25 10:35 10:45 10:58 11:09 11:19 11:28 11:38 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.78E8 

12:51

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.48E7 

12:51

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.41E5 

12:49

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.12E4 

12:49

A5.31E3

12:54

A3

1

A2.11E3

14:45

A1.96E3

12:26

A1.52E3

15:11

A703.23

13:50

A624.26

14:20

A578.62

13:11

A507.87

13:31

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:24 12:39 12:54 13:25 13:45 14:00 14:23 14:51 15:10 15:24 15:41 

12:10 13:10 14:22

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.66E8 

14:48

A4.44E8

15:11

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.35E8 

14:48

A1.04E8

15:11

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A6.47E6 

15:08

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.13E6 

15:08

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:24 12:39 12:54 13:25 13:45 14:00 14:23 14:51 15:10 15:24 15:41 

12:10 13:10 14:22

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.48E8 

17:36

A3.84E7

17:32

A1.13E7

17:06

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.64E7 

17:36

A9.56E6

17:32

A3.28E6

17:11

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A5.33E4 

17:33

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.07E4 

17:33

A929.56

17:36

A891.31

18:28

A1.11E3

18:10

A546.85

16:46

A395.66

18:42

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:36 16:55 17:13 17:28 17:40 17:51 18:01 18:13 18:28 18:40 18:57 

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.75E7 

19:44

A7.26E6

20:15

A6.87E6

19:47

A3.07E6

20:21

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A4.31E6 

19:44

A1.68E6

20:15

A1.58E6

19:47

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A3.01E6 

20:12

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A6.64E5 

20:12

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:35 19:43 19:51 19:59 20:10 20:19 20:31 20:46 20:55 21:11 21:26 21:3

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.90E5 

22:48

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.32E5 

22:48

A1.30E5

22:23

A2.70E4

22:14

A8.36E3

22:57

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.05E4 

22:21

A1.04E3

24:41

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.77E3 

22:45

A1.33E3

22:20

A653.13

24:15

A836.52

23:15

A481.96

26:27

A415.14

25:04

A261.56

25:32

A

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:22 22:42 23:03 23:36 23:56 24:18 24:44 25:10 25:29 25:51 26:10 26:32 26:53 

27

24:15

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A9.80E4 

22:27

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.89E4 

22:28

A7.07E3

22:16

A8.96E3

22:41

A1.49E3

22:46

A1.05E3

25:01

A1.34E3

26:22

A617.97

24:33

A546.51

23:53

A526.92

23:26

A495.57

25:44

A

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A7.34E3 

22:25

A651.57

22:41

A301.33

24:48

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.17E3 

26:35

A987.04

24:52

A1.02E3

22:23

A841.45

22:48

A624.32

26:23

A494.83

25:49

A433.38

24:24

A406.08

23:40

A358.91

24:54

A370.06

22:25

A1

2

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:22 22:42 23:03 23:36 23:56 24:18 24:44 25:10 25:29 25:51 26:10 26:32 26:53 

27

24:15

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A6.05E4 

15:35

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A1.04E4 

15:35

A946.32

13:44

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 12:24 12:54 13:25 13:45 14:00 14:51 15:10 15:24 15:41 

12:39 13:01 13:49 14:23 14:45 15:37 

12:16 13:30 14:09 

12:45 14:12

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A1.75E7

A6.87E6

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141118mb

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A4.31E6

A1.58E6

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A2.39E7

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A5.70E6

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A6.87E6

A7.81E5

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141118mb

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A1.58E6

A2.79E5

A1.25E5

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A6.56E5

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20

%

0 

20 40 60 80 

100 120 140 

A2.64E5

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A7.26E6

A6.87E6

A3.07E6

A7.81E5 A6.03E5

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A1.68E6

A1.58E6

A7.13E5

A1.25E5 A1.48E5

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A7.10E6

A2.84E6

A6.56E5

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20

%

0 

20 40 60 80 

100 120 140 

A1.57E6

A5.47E5

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A3.07E6

A7.81E5 A6.03E5

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A7.13E5

A1.25E5 A1.48E5

A2.35E4 A7.76E4 A2.83E4

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A2.84E6

A6.56E5 A4.46E5

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20

%

0 

20 40 60 80 

100 120 140 

A5.47E5

A5.09E4

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

A6.03E5

A1.24E5

A4.28E4 A2.75E4 A5.90E4 A3.25E4 A2.55E4 

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

A1.48E5

A7.76E4

A2.83E4

A1.47E4

A6.89E3

A6.57E3 A7.18E3 A5.68E3 

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

A4.46E5

252.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20:48 20:50 20

%

0 

20 40 60 80 

100 120 140 

A5.09E4

A1.01E4

253.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22

%

0 

20 40 60 80 

100 120 140 

A4.87E5

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141118mb

after_modification

21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22

%

0 

20 40 60 80 

100 120 140 

A1.30E5

A2.70E4

A9.79E3 A2.36E3 A4.93E3 A6.42E3 A5.43E3

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22

%

0 

20 40 60 80 

100 120 140 

22:12 22:22 22:42 22:08 22:19 22:30 22:32 22:10 22:14 22:24 22:26 22:35 22:39 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) 

21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22

%

0 

20 40 60 80 

100 120 140 

A5.26E5

A1.06E5

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22

%

0 

20 40 60 80 

100 120 140 

A1.26E5

A2.69E4

A9.79E3

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A9.80E4

A3.69E3

A2.18E3

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141118mb

after_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A1.89E4

A6.87E3

A7.07E3 A8.96E3

A3.82E3 A2.68E3

A4.10E3

A2.55E3 A1.62E3 A1.49E3

A551.22 A792.65

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A8.29E4 A1.09E5

A7.11E4

A1.23E4

A3.70E3 

A2.17E3

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A1.86E4

A6.48E3

A6.67E3 A9.40E3

A3.80E3 A2.79E3

A3.85E3

A1.44E3 A1.64E3 A2.25E3 

A455.76 A816.53

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23:08 

%

0 

20 40 60 80 

100 120 140 

A4.90E5

A4.87E5

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141118mb

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23:08 

%

0 

20 40 60 80 

100 120 140 

A1.32E5

A1.30E5

A8.36E3 A4.93E3 A6.42E3 A5.43E3 A4.89E3

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23:08 

%

0 

20 40 60 80 

100 120 140 

A4.78E5

A5.26E5

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23:06 23:08 

%

0 

20 40 60 80 

100 120 140 

A1.22E5

A1.26E5

A4.14E3

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22

%

0 

20 40 60 80 

100 120 140 

A1.05E4

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22

%

0 

20 40 60 80 

100 120 140 

A1.33E3 A880.88

A498.83

A138.97 A107.50 A89.50 A172.45 A105.26 A69.87

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22

%

0 

20 40 60 80 

100 120 140 

A1.06E4

A1.04E3

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:52 21:54 21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22

%

0 

20 40 60 80 

100 120 140 

A1.32E3 A948.71

A599.08

A138.97 A107.50 A89.50 A171.15

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22

%

0 

20 40 60 80 

100 120 140 

A7.34E3

A817.81 A651.57 

A321.15

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22

%

0 

20 40 60 80 

100 120 140 

A370.06

A247.07

A232.03 A276.76

A125.72 A158.00

A162.82 

A122.38

A35.12 

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22

%

0 

20 40 60 80 

100 120 140 

A7.84E3

A1.91E3

A717.18 A572.85 

A261.60

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:56 21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22

%

0 

20 40 60 80 

100 120 140 

A361.54

A219.28

A210.14 A219.98

A158.00 A117.00

A162.08 A118.86 

A22.7

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23

%

0 

20 40 60 80 

100 120 140 

A1.05E4

A1.38E4

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23

%

0 

20 40 60 80 

100 120 140 

A3.77E3

A1.33E3 A880.88

A498.83 

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23

%

0 

20 40 60 80 

100 120 140 

A1.06E4

A1.38E4

A3.11E3

A1.04E3

A916.27 A456.11

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22:48 22:50 22:52 22:54 22:56 22:58 23:00 23:02 23:04 23

%

0 

20 40 60 80 

100 120 140 

A3.70E3

A1.32E3 A948.71

A599.08 

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 

%

0 

20 40 60 80 

100 120 140 

A3.01E6

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 

%

0 

20 40 60 80 

100 120 140 

A6.64E5

A1.84E4

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 

%

0 

20 40 60 80 

100 120 140 

A3.09E6

264.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 

%

0 

20 40 60 80 

100 120 140 

A6.82E5

265.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B18 #1-2850 Acq:16-NOV-2014 11:36:08 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-2 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A7.87E7 

7:35

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,3972.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A8.85E6 

7:35

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,5176.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.89E5 

7:33

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.04E4 

7:33

A4.63E3

7:41

A3.31E3

8:33

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,372.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:06 7:16 7:23 7:34 7:42 7:49 7:59 8:13 8:20 8:29 8:39 8:48 8:58 9:06 9:15 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B19 #1-2851 Acq:16-NOV-2014 12:10:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A6.71E6 

8:44

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,416.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A6.23E6 

8:44

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,460.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A8.20E4 

8:41

A5.12E3

8:55

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A7.73E4 

8:50

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:06 7:16 7:23 7:34 7:42 7:49 7:59 8:13 8:20 8:29 8:39 8:48 8:58 9:06 9:15 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B19 #1-2851 Acq:16-NOV-2014 12:10:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.88E7 

10:11

A1.96E6

10:28

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.45E6 

10:11

A6.04E5

10:28

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.84E6 

10:25

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.89E5 

10:25

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:55 10:03 10:16 10:31 10:41 10:53 11:01 11:09 11:20 11:28 11:38 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B19 #1-2851 Acq:16-NOV-2014 12:10:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.36E6 

10:28

A7.75E5

10:00

A3.43E5

9:50

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,284.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.88E6 

10:28

A1.00E6

10:11

A2.97E5

10:00

A2.42E5

9:50

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,276.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.49E6 

10:25

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.54E6 

10:25

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:55 10:03 10:16 10:31 10:41 10:53 11:01 11:09 11:20 11:28 11:38 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B19 #1-2851 Acq:16-NOV-2014 12:10:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.13E6 

11:19

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.62E6 

11:19

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A9.04E4 

11:16

A3.67E3

11:20

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.29E4 

11:16

A7.64E3

11:20

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:55 10:03 10:16 10:31 10:41 10:53 11:01 11:09 11:20 11:28 11:38 

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B19 #1-2851 Acq:16-NOV-2014 12:10:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.79E8 

12:51

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.27E7 

12:51

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.21E5 

12:49

A2.07E4

12:58

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.74E4 

12:49

A3.75E3

12:54

A4.82E3

12:23

A2.49E3

14:59

A1.11E3

13:59

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:32 13:07 13:29 14:33 14:58 15:26 1

12:11 12:53 13:45 14:02 14:18 15:42

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B19 #1-2851 Acq:16-NOV-2014 12:10:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.68E8 

14:48

A4.21E8

15:11

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.13E8 

14:48

A8.60E7

15:11

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A7.12E6 

15:09

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.29E6 

15:09

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:32 13:07 13:29 14:33 14:58 15:26 1

12:11 12:53 13:45 14:02 14:18 15:42

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B19 #1-2851 Acq:16-NOV-2014 12:10:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.11E8 

17:37

A7.59E7

17:32

A1.23E7

17:07

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A3.71E7 

17:36

A1.58E7

17:32

A4.74E6

17:11

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.47E5 

17:33

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A2.64E4 

17:33

A1.75E3

18:26

A1.96E3

16:54

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:36 16:47 16:56 17:07 17:23 17:39 17:49 17:59 18:13 18:24 18:35 18:49 19

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B19 #1-2851 Acq:16-NOV-2014 12:10:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A3.32E7 

19:44

A1.40E7

20:15

A1.46E7

19:47

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.13E7 

19:44

A3.41E6

20:15

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A4.10E6 

20:12

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A9.07E5 

20:12

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:35 19:48 20:00 20:15 20:29 20:38 20:49 21:00 21:16 21:25 21:36 

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B19 #1-2851 Acq:16-NOV-2014 12:10:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.14E6 

22:48

A1.03E6

22:23

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.30E5 

22:47

A6.17E4

22:14

A4.36E4

22:53

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A5.82E4 

22:45

A7.30E3

22:25

A2.15E3

22:55

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.12E4 

22:44

A1.81E3

22:25

A2.22E3

24:48

A1.60E3

22:53

A363.26

23:45

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:20 22:39 22:58 23:32 23:53 24:19 24:53 25:16 26:05 26:23 26:42 27:02 

25:41

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B19 #1-2851 Acq:16-NOV-2014 12:10:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.86E5 

22:27

A1.55E5

22:41

A4.81E4

22:47

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.80E4 

22:28

A6.80E3

22:32

A1.84E3

24:59

A902.65

24:02

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.15E4 

22:25

A5.32E3

22:28

A896.43

24:55

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.48E3 

22:25

A1.45E3

22:23

A1.53E3

25:06

A872

27:0

A1.08E3

26:11

A609.85

24:28

A548.00

22:30

A303.10

23:45

A235.85

23:14

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:20 22:39 22:58 23:32 23:53 24:19 24:53 25:16 26:05 26:23 26:42 27:02 

25:41

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B19 #1-2851 Acq:16-NOV-2014 12:10:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A7.03E4 

15:35

A9.18E3

15:40

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A1.40E4 

15:35

A528.74

15:39

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 14:33 14:58 15:26 

15:21 1

12:32 12:46 13:07 13:29 13:45 14:28 14:51 15:42 

12:21 14:12 15:13 12:07 12:44 13:02 13:18 13:49 15:30 15:5

12:15

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B19 #1-2851 Acq:16-NOV-2014 12:10:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

A7.59E7

A1.23E7

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141117mb

after_modification

17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

A1.58E7

A4.74E6

A2.43E6

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

A7.53E7

A1.23E7

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:02 17:04 17:06 17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 

%

0 

20 40 60 80 

100 120 140 

A1.56E7

A4.42E6

A2.30E6

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B19 #1-2851 Acq:16-NOV-2014 12:10:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 17

%

0 

20 40 60 80 

100 120 140 

A2.11E8

A7.59E7

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

eg141117mb

after_modification

17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 17

%

0 

20 40 60 80 

100 120 140 

A3.71E7

A1.58E7

A4.74E6

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 17

%

0 

20 40 60 80 

100 120 140 

A2.08E8

A7.53E7

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

17:08 17:10 17:12 17:14 17:16 17:18 17:20 17:22 17:24 17:26 17:28 17:30 17:32 17:34 17:36 17:38 17:40 17:42 17:44 17:46 17:48 17:50 17:52 17:54 17:56 17

%

0 

20 40 60 80 

100 120 140 

A3.67E7

A1.56E7

A4.42E6

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B19 #1-2851 Acq:16-NOV-2014 12:10:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A1.86E5

A1.52E5

A1.55E5

A4.81E

A2.33E4

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

eg141116mb

after_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A4.80E4

A3.92E4

A3.41E4

A6.03E3 A6.80E3

A9.86E3 A4.41E3

A4.56E3 A3.

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A2.36E5

A1.52E5

A1.50E5

A1.13E4 A4.37E

A2.33E4 A1.55E4

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

21:58 22:00 22:02 22:04 22:06 22:08 22:10 22:12 22:14 22:16 22:18 22:20 22:22 22:24 22:26 22:28 22:30 22:32 22:34 22:36 22:38 22:40 22:42 22:44 22:46 22

%

0 

20 40 60 80 

100 120 140 

A4.10E4

A2.92E4

A3.01E4

A4.21E3 A5.37E3

A5.95E3 A3.44E3

A2.

A2.04E3

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B19 #1-2851 Acq:16-NOV-2014 12:10:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20

%

0 

20 40 60 80 

100 120 140 

A5.79E4

A1.31E4 A8.51E3 A5.65E3 A3.32E

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20

%

0 

20 40 60 80 

100 120 140 

A1.22E4

A7.24E3

A5.77E3

A2.67E3

A2.54E3 A2.29E3 A1.32E3 A1.2

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20

%

0 

20 40 60 80 

100 120 140 A1.08E5 

A5.12E4

A1.12E4 A8.14E3

A2.82E

264.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20

%

0 

20 40 60 80 

100 120 140 

A1.06E4 A1.29E4

A6.10E3

A4.76E3

A2.44E3

A1.77E3 A1.25E3 A1.1

265.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B19 #1-2851 Acq:16-NOV-2014 12:10:29 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-5 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A8.78E7 

7:34

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,7648.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A9.57E6 

7:34

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,4260.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.98E5 

7:32

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A1.41E4 

7:32

A3.25E3

7:40

A915.30

8:38

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,260.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:06 7:14 7:22 7:36 7:50 7:57 8:08 8:21 8:30 8:42 8:52 9:00 9:08 9:15 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B20 #1-2851 Acq:16-NOV-2014 12:44:50 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A6.81E6 

8:44

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,544.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A6.25E6 

8:44

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,516.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A7.79E4 

8:50

A3.33E3

8:44

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A7.22E4 

8:50

A5.29E3

8:45

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:06 7:14 7:22 7:36 7:50 7:57 8:08 8:21 8:30 8:42 8:52 9:00 9:08 9:15 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B20 #1-2851 Acq:16-NOV-2014 12:44:50 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.82E7 

10:10

A2.00E6

10:27

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.93E6 

10:10

A5.65E5

10:27

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.85E6 

10:25

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.93E5 

10:25

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:58 10:08 10:16 10:27 10:38 10:49 10:58 11:08 11:17 11:29 11:

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B20 #1-2851 Acq:16-NOV-2014 12:44:50 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.24E6 

10:27

A8.84E5

10:00

A3.50E5

9:49

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,204.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A2.76E6 

10:27

A1.33E6

10:10

A3.48E5

10:00

A3.05E5

9:49

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,320.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.43E6 

10:25

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.36E6 

10:25

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:58 10:08 10:16 10:27 10:38 10:49 10:58 11:08 11:17 11:29 11:

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B20 #1-2851 Acq:16-NOV-2014 12:44:50 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.61E6 

11:18

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.09E6 

11:18

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.26E4 

11:15

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A7.72E4 

11:15

A8.13E3

11:20

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:58 10:08 10:16 10:27 10:38 10:49 10:58 11:08 11:17 11:29 11:

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B20 #1-2851 Acq:16-NOV-2014 12:44:50 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A3.49E8 

12:50

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.85E7 

12:50

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.45E5 

12:48

A2.35E4

12:57

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A2.64E4 

12:48

A1.04E4

12:54

A4.20E3

14:45

A3.94E3

14:08

A2.12E3

13:07

A1.07E3

12:20

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:12 12:40 12:56 13:13 13:33 13:57 14:18 14:37 14:57 15:18 15:37 15:

12:26

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B20 #1-2851 Acq:16-NOV-2014 12:44:50 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A4.01E8 

14:47

A3.43E8

15:10

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A7.43E7 

14:47

A5.41E7

15:10

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.87E6 

15:08

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.49E6 

15:08

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:12 12:40 12:56 13:13 13:33 13:57 14:18 14:37 14:57 15:18 15:37 15:

12:26

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B20 #1-2851 Acq:16-NOV-2014 12:44:50 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A6.29E7 

17:36

A1.60E7

17:32

A5.36E6

17:06

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.26E7 

17:36

A4.55E6

17:32

A1.73E6

17:11

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.38E5 

17:33

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A3.16E4 

17:33

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:36 16:52 17:03 17:13 17:22 17:32 17:46 18:01 18:21 18:31 18:43 18:55 

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B20 #1-2851 Acq:16-NOV-2014 12:44:50 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A8.95E6 

19:44

A4.38E6

20:14

A4.21E6

19:46

A1.73E6

20:21

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A3.13E6 

19:44

A9.79E5

20:14

A4.11E5

20:21

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A4.35E6 

20:11

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A9.59E5 

20:11

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 19:35 19:44 19:55 20:09 20:19 20:28 20:40 20:52 21:01 21:12 21:23 21:33 2

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B20 #1-2851 Acq:16-NOV-2014 12:44:50 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A3.49E5 

22:48

A3.05E5

22:23

A1.80E4

22:36

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A6.71E4 

22:47

A1.96E4

22:14

A5.18E3

22:43

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A2.91E4 

22:45

A1.47E4

22:48

A1.89E3

22:31

A1.24E3

23:05

A1.07E3

24:36

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A8.85E3 

22:20

A3.45E3

22:45

A760.42

25:27

A791.25

22:52

A1.05E3

25:52

A675.27

22:26

A607.54

23:23

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:16 22:42 23:09 23:31 23:51 24:13 24:32 24:51 25:31 25:52 26:21 26:59 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B20 #1-2851 Acq:16-NOV-2014 12:44:50 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.92E4 

22:28

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A6.19E3 

22:27

A3.26E3

22:44

A1.46E3

22:17

A1.04E3

24:09

A824.86

22:50

A546.23

25:01

A781.59

25:35

A479.28

26:54

A347.19

23:20

A576.81

26:23

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.64E4 

22:24

A4.04E3

22:28

A2.16E3

22:42

A

A370.44

25:06

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.14E3 

22:24

A1.30E3

26:16

A1.40E3

25:02

A1.96E3

22:28

A853.51

24:11

A1.33E3

23:30

A415.28

25:11

A393.59

26:40

A312.74

22:57

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:16 22:42 23:09 23:31 23:51 24:13 24:32 24:51 25:31 25:52 26:21 26:59 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B20 #1-2851 Acq:16-NOV-2014 12:44:50 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A7.43E4 

15:35

A2.94E4

15:37

A2.61E3

15:44

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A1.41E4 

15:35

A1.46E3

15:42

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 12:56 13:13 13:33 13:57 14:18 15:18 15:37 15:

12:40 14:37 14:57 

12:12 12:28 12:46 13:10 13:24 13:49 14:22 15:22 1

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B20 #1-2851 Acq:16-NOV-2014 12:44:50 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:12 19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20

%

0 

20 40 60 80 

100 120 140 

A4.85E4 A6.86E4

A7.50E3 A2.74E3 A2.26E3

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:12 19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20

%

0 

20 40 60 80 

100 120 140 

A1.36E4

A8.56E3

A4.66E3

A1.30E3 A889.27

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:12 19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20

%

0 

20 40 60 80 

100 120 140 

A4.81E4 A7.61E4

A7.45E3

A2.21E3 A2.62E3

264.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:12 19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20

%

0 

20 40 60 80 

100 120 140 

A1.52E4

A1.29E4

A988.25

A331.32

265.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B20 #1-2851 Acq:16-NOV-2014 12:44:50 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A4.85E4 A6.86E4

A7.50E3 A2.74E3 A2.26E3 

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A1.36E4

A8.56E3

A4.66E3

A1.30E3 A889.27

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A4.81E4 A7.61E4

A7.45E3

A2.21E3 A2.62E3

264.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:14 19:16 19:18 19:20 19:22 19:24 19:26 19:28 19:30 19:32 19:34 19:36 19:38 19:40 19:42 19:44 19:46 19:48 19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 

%

0 

20 40 60 80 

100 120 140 

A1.52E4

A1.29E4

A988.25

265.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B20 #1-2851 Acq:16-NOV-2014 12:44:50 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 

%

0 

20 40 60 80 

100 120 140 

A9.89E4

A7.16E4

A2.03E4

A9.50E3 A

A2.74E3 

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 

%

0 

20 40 60 80 

100 120 140 

A9.49E3

A7.19E3 A1.35E4

A1.08E4

A7.08E3

A4.07E3 

A2.53E3 

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 

%

0 

20 40 60 80 

100 120 140 

A4.90E4 A1.14E5

A1.86E4

A2.08E4

A1.14E4 A

264.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:50 19:52 19:54 19:56 19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 

%

0 

20 40 60 80 

100 120 140 

A2.53E4

A1.09E4

A1.31E4

A8.90E3

A7.68E3

A4.05E3 

A2.28E3 

265.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B20 #1-2851 Acq:16-NOV-2014 12:44:50 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20

%

0 

20 40 60 80 

100 120 140 

A7.16E4

A2.03E4

A9.50E3 A6.66E3

A4.68E3 

A2.45E3 

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) 

eg141116mb

after_modification

19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20

%

0 

20 40 60 80 

100 120 140 

A9.49E3

A7.19E3

A1.35E4

A1.08E4

A7.08E3

A4.07E3 A4.39E3

A2.53E3 A1.28E3 

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

after_modification

19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20

%

0 

20 40 60 80 

100 120 140 

A4.90E4

A1.14E5

A1.86E4

A2.08E4

A1.14E4 A6.17E3

A4.14E3 

A2.44E3 

264.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

19:58 20:00 20:02 20:04 20:06 20:08 20:10 20:12 20:14 20:16 20:18 20:20 20:22 20:24 20:26 20:28 20:30 20:32 20:34 20:36 20:38 20:40 20:42 20:44 20:46 20

%

0 

20 40 60 80 

100 120 140 

A1.09E4

A1.31E4

A8.90E3

A7.68E3

A4.05E3

A4.16E3

A2.28E3 A1.58E3 

265.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(128,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

before_modification

File:4-141115B20 #1-2851 Acq:16-NOV-2014 12:44:50 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Text:L1535265-6 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A6.94E6 

7:36

128.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,1104.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A8.36E5 

7:37

127.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,584.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A7.09E6 

7:34

136.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,368.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A6.76E5 

7:34

134.0987 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,12.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:05 7:13 7:21 7:29 7:41 7:50 8:01 8:09 8:18 8:25 8:33 8:41 8:48 9:00 9:07 9:16 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B22 #1-2850 Acq:16-NOV-2014 13:53:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0454 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A4.02E6 

8:54

142.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,308.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.82E6 

8:54

141.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,472.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A3.15E6 

8:51

152.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 A2.89E6 

8:51

150.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

7:00 7:12 7:24 7:36 7:48 8:00 8:12 8:24 8:36 8:48 9:00 9:12 

%

0 

50 

100 7:05 7:13 7:21 7:29 7:41 7:50 8:01 8:09 8:18 8:25 8:33 8:41 8:48 9:00 9:07 9:16 

130.9914 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B22 #1-2850 Acq:16-NOV-2014 13:53:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0454 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.00E6 

10:12

A3.16E6

10:29

152.0626 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A1.35E6 

10:12

A9.72E5

10:29

151.0548 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A6.54E6 

10:10

A2.71E6

10:26

160.1128 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A8.60E5 

10:10

A4.71E5

10:26

161.1162 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:58 10:05 10:12 10:22 10:37 10:46 10:55 11:05 11:12 11:25 11:36 1

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B22 #1-2850 Acq:16-NOV-2014 13:53:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0454 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.51E6 

10:29

154.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,136.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A5.31E6 

10:29

153.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,220.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.96E6 

10:26

164.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.94E6 

10:26

162.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:58 10:05 10:12 10:22 10:37 10:46 10:55 11:05 11:12 11:25 11:36 1

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B22 #1-2850 Acq:16-NOV-2014 13:53:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0454 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.71E6 

11:20

166.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A4.95E6 

11:20

165.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.52E6 

11:17

176.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 A3.54E6 

11:17

174.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

9:48 10:00 10:12 10:24 10:36 10:48 11:00 11:12 11:24 11:36 

%

0 

50 

100 9:48 9:58 10:05 10:12 10:22 10:37 10:46 10:55 11:05 11:12 11:25 11:36 1

168.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B22 #1-2850 Acq:16-NOV-2014 13:53:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0454 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.58E6 

12:52

178.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A7.77E5 

12:52

177.0704 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A9.22E6 

12:50

188.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A6.04E5 

12:50

A5.51E5

12:55

186.1269 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:18 12:40 12:57 13:23 13:51 14:05 14:45 15:32 

14:29 15:12 12:42 15:5

14:03

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B22 #1-2850 Acq:16-NOV-2014 13:53:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0454 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

50 

100 A8.20E6 

15:12

A7.62E6

14:49

202.0783 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.46E6 

15:12

A1.36E6

14:49

203.0816 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A7.08E6 

15:10

A6.30E6

14:47

212.141 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 A1.24E6 

15:10

A1.02E6

14:47

213.1444 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

50 

100 12:18 12:40 12:57 13:23 13:51 14:05 14:45 15:32 

14:29 15:12 12:42 15:5

14:03

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B22 #1-2850 Acq:16-NOV-2014 13:53:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0454 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A7.87E6 

17:38

228.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.55E6 

17:38

229.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A8.57E6 

17:34

240.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 A1.72E6 

17:34

241.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

16:36 16:48 17:00 17:12 17:24 17:36 17:48 18:00 18:12 18:24 18:36 18:48 19:00 

%

0 

50 

100 16:44 16:55 17:13 17:25 17:40 17:51 18:00 18:10 18:21 18:35 18:46 19:01 

230.985 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B22 #1-2850 Acq:16-NOV-2014 13:53:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0454 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A9.12E6 

20:32

A6.33E6

20:16

A7.10E6

19:48

252.0939 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A2.08E6 

20:32

A1.42E6

20:16

A1.59E6

19:48

253.0973 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A7.47E6 

20:13

A7.11E6

19:46

A6.31E6

20:29

264.1692 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 A1.63E6 

20:13

A1.50E6

19:46

A1.38E6

20:29

265.1726 (+RP) Win 1000PPM BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

19:36 19:48 20:00 20:12 20:24 20:36 20:48 21:00 21:12 21:24 21:36 

%

0 

50 

100 20:03 20:19 20:29 20:38 20:48 21:04 21:16 21:30 21:3

19:40 19:53

268.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B22 #1-2850 Acq:16-NOV-2014 13:53:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0454 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A6.47E6 

22:48

A4.26E6

22:23

A3.03E6

22:27

276.0939 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.62E6 

22:48

A1.05E6

22:23

A8.35E5

22:27

277.0973 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A6.30E6 

22:45

A5.54E6

22:21

288.1692 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.41E6 

22:45

A1.34E6

22:21

289.1726 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:27 23:04 23:32 23:53 24:17 24:39 24:58 25:17 25:51 26:16 26:35 27:00 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B22 #1-2850 Acq:16-NOV-2014 13:53:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0454 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A6.58E6 

22:28

278.1096 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.61E6 

22:28

279.1129 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A4.65E6 

22:24

292.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 A1.04E6 

22:24

293.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

22:00 23:00 24:00 25:00 26:00 27:00 

%

0 

50 

100 22:27 23:04 23:32 23:53 24:17 24:39 24:58 25:17 25:51 26:16 26:35 27:00 

280.9818 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B22 #1-2850 Acq:16-NOV-2014 13:53:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0454 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A4.44E6 

15:36

244.1974 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 A8.51E5 

15:36

245.2008 (+RP) Win 1000PPM SMO(1,3) BSUB(256,15,-3.0) PKD(3,3,2,0.01%,0.0,3.00%,F,T) 

12:00 13:00 14:00 15:00 

%

0 

20 40 60 80 

100 12:40 

12:18 12:57 13:23 13:4013:51 14:05 14:29 14:45 15:12 15:32 

12:35 14:13 14:49 

12:06 13:25 13:59 15:06 15:41 14:20 

192.9882 (+RP) Win 1000PPM PKD(3,3,2,0.01%,10000000.0,3.00%,F,T) File:4-141115B22 #1-2850 Acq:16-NOV-2014 13:53:18 EI+ Magnet Finnigan-MAT LCQSample#1 File Text:Operator: EG Sample:H4-14-CCV-0454 

ALS Environmental - Burlington, ON L1535265 Appendix 141208 
Instrument: HRMS‐4

Run File:

MID Procedure:

Reference Compound: PFK

16‐Nov‐14 16‐Nov‐14 16‐Nov‐14 16‐Nov‐14 16‐Nov‐14 16‐Nov‐14 16‐Nov‐14 16‐Nov‐14 16‐Nov‐14 16‐N

Segment 1:59:04 3:41:59 4:16:12 4:50:35 5:24:47 5:59:12 6:33:27 7:42:07 8:16:30 8:

MID Time Window 1 8925 8708 8767 8945 8953 8767 8811 9045 8798 MID Time Window 2 8663 8718 8579 8612 8572 8672 8703 8692 8680 MID Time Window 3 8681 8660 8575 8796 8703 8571 8520 8430 8634 MID Time Window 4 8758 9148 8922 8629 9191 9192 8712 8796 8774 MID Time Window 5 8981 9182 9254 9085 9134 8955 8814 9445 9230 MID Time Window 6 9375 9055 9065 8776 9047 8846 8973 9399 9110 

16‐Nov‐14 16‐Nov‐14 16‐Nov‐14 16‐Nov‐14 16‐Nov‐14 16‐Nov‐14

Segment 10:33:41 11:08:02 11:42:23 12:16:44 12:50:57 13:59:24

MID Time Window 1 8928 8697 9097 9139 8992 8888MID Time Window 2 8720 8749 8670 8922 8694 8612MID Time Window 3 8683 8624 8971 8626 8835 8555MID Time Window 4 9162 8812 8997 8852 9078 8652MID Time Window 5 8688 8745 9103 9433 9193 8632MID Time Window 6 9149 8600 9382 9066 9034 8954

Mass Resolution

Mass Resolution Examination ‐ Thermo DFS

4‐141115BC429‐DB5MS‐3

Mass Resolution

ALS Environmental - Burlington, ON L1535265 Appendix 141208