United States Department of Agriculture

January 2022

Dear Reader:

We are pleased to present the Pesticide Data Program’s (PDP) 30th Annual Summary for calendar 

year 2020 and to celebrate the program’s 30-year anniversary! Since the program’s inception in 1991, 

over 310,000 samples have been collected and analyzed from 126 different commodities generating 

42 million pesticide-commodity data points. Thirty years of PDP residue data (available through our 

website) represent one of the largest sources of food pesticide residue data available. 

The U.S. Department of Agriculture (USDA), Agricultural Marketing Service (AMS) conducts the 

PDP each year to collect new/updated data on pesticide residues in food. This Annual Summary 

report shows that when pesticide residues are found on foods, they are nearly always at levels below 

the tolerance, or maximum amount of a pesticide allowed to remain in or on a food, that is set by the 

U.S. Environmental Protection Agency (EPA).

The PDP provides high-quality, nationally representative pesticide residue data that contribute to the 

information available to help ensure consumer confidence in the foods they provide to their families. 

More than 99 percent of the products sampled through PDP had residues below the EPA tolerances. 

Ultimately, if EPA determines a pesticide use is not safe for human consumption, EPA will mitigate 

exposure to the pesticide through actions such as amending label instructions or changing or revoking 

a tolerance.

The PDP tests a wide variety of domestic and imported foods, with a strong focus on foods that are 

consumed by infants and children. EPA relies on PDP data to conduct dietary risk assessments and to 

review the maximum amount of a pesticide allowed to remain in or on a food. USDA uses the data 

to better understand the relationship of pesticide residues to agricultural practices and to implement 

USDA’s Integrated Pest Management objectives. USDA also works with U.S. growers to improve 

agricultural practices and to facilitate the adoption of integrated pest management techniques, 

including judicious use of pesticides, throughout the food supply chain.

The PDP is not designed for enforcement of EPA pesticide residue tolerances. Rather, the U.S. Food 

and Drug Administration (FDA) is responsible for enforcing EPA tolerances. The PDP provides FDA 

and EPA with monthly reports of pesticide residue testing and informs the FDA if residues detected 

exceed the EPA tolerance or have no EPA tolerance established.

To collect the data in this report, the PDP works with State agencies representing all census regions 

of the country and nearly half of the U.S. population. In 2020, analyzed samples were collected in 

California, Colorado, Florida, Maryland, Michigan, New York, North Carolina, Ohio, Texas, and 

Washington.

For more information about PDP, please visit our website at https://www.ams.usda.gov/datasets/pdp. 

For additional information about pesticides and food, please visit EPA’s website at http://www.epa.

gov/safepestcontrol and FDA’s website at http://www.fda.gov/Food/Chemicals-Metals-PesticidesFood/Pesticides.

Agricultural Marketing Service

1400 Independence Avenue, SW, Washington, DC 20250-0201

Voice (202) 720-8998 Fax (202) 720-7135

An Equal Opportunity Provider and Employer
Pesticide Data Program—Annual Summary, Calendar Year 2020

iii

Contents

Page No.

Acknowledgements........................................................................................................................ vii

Executive Summary...................................................................................................................... ix

Acronyms and Abbreviations........................................................................................................ xi

Section I--Introduction............................................................................................................... 1

Section II--Sampling Operations............................................................................................... 4

Conceptual Framework.................................................................................................... 4

Sampling Procedures....................................................................................................... 5

2020 Sampling Operations.............................................................................................. 6

Fresh and Processed Commodities.................................................................................. 9

Sampling Limitations...................................................................................................... 12

Section III--Laboratory Operations......................................................................................... 13

Overview.......................................................................................................................... 13

Fresh and Processed Commodities.................................................................................. 13

Quality Assurance Program............................................................................................. 13

Section IV--Database Management.......................................................................................... 16

Electronic Data Path........................................................................................................ 16

Data Reporting................................................................................................................ 18

Online Database Search Tool.......................................................................................... 18

Section V--Sample Results and Discussion.............................................................................. 18

Overview......................................................................................................................... 18

Import Versus Domestic Residue Comparisons.............................................................. 19

Postharvest Applications................................................................................................. 20

Discussion of Results ..................................................................................................... 20

Environmental Contaminants.......................................................................................... 21

Tolerance Violations........................................................................................................ 22

Look Ahead..................................................................................................................... 23
Pesticide Data Program—Annual Summary, Calendar Year 2020

v

Figures Page No.

 1 Pesticide Data Program (PDP) Program Operations Support and Data Users................... 2

 2 Program Participants........................................................................................................... 3

 3 Monthly Sample Collection in 2020................................................................................... 7

 4 Commodity Origin.............................................................................................................. 10

 5 Origin of Selected Fresh Commodities: Cantaloupe and Tangerine Samples.................... 12

 6 Pesticide Data Program (PDP) Data Pathway..................................................................... 17

Tables

 1 Pesticide Data Program (PDP) Commodity Collection Schedule for 2020........................ 6

 2 Distribution of Samples Collected by Each Participating State.......................................... 8

 3 Acceptable Products for Collected Commodities................................................................ 9

 4 Sample Preparation Steps for Analysis................................................................................ 14

 

Appendixes A-H

Appendix A Commodity History

Appendix B Distribution of Residues by Pesticide in Fruit and Vegetables

Appendix C Distribution of Residues for Environmental Contaminants

Appendix D Sample Origin by State or Country

Appendix E Import Versus Domestic Pesticide Residue Comparisons

Appendix F Pesticide Residues by Commodity

Appendix G Number of Pesticides Detected per Sample

Appendix H Samples Reported to the U.S. Food and Drug Administration 

 as Exceeding the Tolerance or Without Established Tolerance
Pesticide Data Program—Annual Summary, Calendar Year 2020

vii

Acknowledgements

The States participating in the Pesticide Data 

Program (PDP) deserve special recognition for 

their contributions to the program. The dedication 

and flexibility of sample collectors allow the U.S. 

Department of Agriculture’s (USDA) Agricultural 

Marketing Service (AMS) to adjust sampling 

protocols when responding to changing trends 

in commodity distribution and availability. PDP 

acknowledges the contributions of the State 

laboratories in providing testing services to the 

program and the USDA, National Agricultural 

Statistics Service for providing statistical support. 

PDP also acknowledges the exceptional support 

of the Health Effects Division staff of the U.S. 

Environmental Protection Agency, Office of 

Pesticide Programs, and the U.S. Food and Drug 

Administration, Center for Food Safety and 

Applied Nutrition, Office of Food Safety, in 

helping to set the direction for PDP. 

 

Data presented in this report are the latest available 

and were collected and processed through the 

efforts of the following organizations:

USDA Program Administration

Agricultural Marketing Service

Science and Technology Program

1400 Independence Ave., SW

South Building, Mail Stop 0270

Washington, DC 20250

Ruihong Guo, Ph.D., Deputy Administrator

Science and Technology Program, AMS

(202) 720-8556

Brenda Foos, Director

Monitoring Programs Division, AMS

1400 Independence Ave, SW

Room 2911-S, Stop 0276

Washington, DC 20250

(202) 572-8167

Electronic-mail Address:

amsmpo.data@usda.gov

Website:

http://www.ams.usda.gov/pdp

Participating State Agencies

California Department of Food and Agriculture

California Department of Pesticide Regulation

Colorado Department of Agriculture

Florida Department of Agriculture and

 Consumer Services

Maryland Department of Agriculture

Michigan Department of Agriculture and 

 Rural Development

New York Department of Agriculture and 

 Markets

North Carolina Department of Agriculture &

 Consumer Services

Ohio Department of Agriculture

Texas Department of Agriculture

Washington State Department of Agriculture

Participating Laboratories

California Department of Food and Agriculture

Division of Inspection Services

Center for Analytical Chemistry

3292 Meadowview Rd.

Sacramento, CA 95832

 

Florida Department of Agriculture and

 Consumer Services

Chemical Residue Laboratory

3125 Conner Blvd., Bldg. 3

Tallahassee, FL 32399-1650

Michigan Department of Agriculture and 

 Rural Development

Laboratory Division

1615 South Harrison Rd.

East Lansing, MI 48823-5224

New York Department of Agriculture 

 and Markets

Food Laboratory

1220 Washington Ave, Bldg. 6

Albany, NY 12226
Pesticide Data Program—Annual Summary, Calendar Year 2020

viii

Ohio Department of Agriculture

Consumer Protection Laboratory

8995 East Main St.

Reynoldsburg, OH 43068

Texas Department of Agriculture

Pesticide Laboratory

1500 Research Parkway, Ste. B100

College Station, TX 77845

United States Department of Agriculture

Agricultural Marketing Service

National Science Laboratories

801 Summit Crossing Pl.

Gastonia, NC 28054

Washington State Department of Agriculture

Chemical and Hop Laboratory

21 N. 1st Ave., Ste. 106

Yakima, WA 98902
Pesticide Data Program—Annual Summary, Calendar Year 2020

ix

Executive Summary

In 1991, the U.S. Department of Agriculture 

(USDA), Agricultural Marketing Service (AMS) 

was charged with designing and implementing 

the Pesticide Data Program (PDP) to collect 

data on pesticide residues in food, and Congress 

mandated the program in the 1996 Food Quality 

Protection Act. PDP provides high-quality data on 

pesticide residues in food, particularly foods most 

likely consumed by infants and children. This 

30th Pesticide Data Program summary presents 

results for samples collected in 2020.

Before a company can sell or distribute any 

pesticide in the United States, the Environmental 

Protection Agency (EPA) reviews studies on 

the pesticide to ensure that it will not pose 

unreasonable risks to human health or the 

environment, while considering the economic, 

social, and environmental costs and benefits of 

the use of any pesticide. Once EPA has made 

that determination, it will license or register that 

pesticide for use in strict accordance with label 

directions. Before allowing a pesticide to be 

used on a food commodity, EPA sets limits on 

how much of a pesticide may be used on food 

during growing, processing, and storage, and how 

much can remain on the food that reaches the 

consumer. In setting the tolerance, or maximum 

residue limit in food, EPA makes a safety finding 

that the pesticide can be used with a reasonable 

certainty of no harm by considering the toxicity 

of the pesticide, how much of the pesticide is 

applied and how often, how much of the pesticide 

remains in or on food by the time it is marketed 

and prepared, and all possible routes of exposure 

including use on crops, exposure from drinking 

water, and residential exposure.

PDP data are provided to EPA for its consideration 

in setting and reviewing tolerances. FDA monitors 

food in interstate commerce to ensure that these 

limits are not exceeded. EPA also sets standards 

to protect workers from exposure to pesticides on 

the job. 

AMS’s Monitoring Programs Division (MPD) 

is responsible for the administration, planning, 

and coordination of day-to-day PDP operations. 

MPD regularly engages with EPA and other 

Government agencies to establish program priorities 

and direction. In 2020, sampling and/or testing 

program operations were carried out with the support 

of 10 States: California, Colorado, Florida, Maryland, 

Michigan, New York, North Carolina, Ohio, Texas, 

and Washington. These States had a prominent role 

in program planning and policy setting, particularly 

policies relating to quality assurance.

PDP commodity sampling is based on a rigorous 

statistical design that ensures the data are reliable for 

use in exposure assessments and can be used to draw 

various conclusions about the Nation’s food supply. 

The pesticides and commodities to be included each 

year in the sampling are selected based on EPA data 

needs, and the types and amounts of food consumed 

by infants and children are considered. The number 

of samples collected by each State is apportioned 

according to that State’s population. Samples are 

randomly chosen close to the time and point of 

consumption (i.e., distribution centers rather than at 

the farm gate) and reflect what is typically available 

to the consumer throughout the year. Samples are 

selected without regard to country of origin, variety, 

growing season, or organic labeling.

Fresh and processed fruit and vegetables accounted 

for 100 percent of the total 9,600 samples collected 

in 2020. Fresh and processed fruit and vegetables 

tested during 2020 were: apple juice, bananas, 

blueberries (fresh and frozen), broccoli, cantaloupe, 

carrots, cauliflower, collard greens, eggplant, green 

beans, kiwi fruit, orange juice, radishes, summer 

squash, sweet bell peppers, tangerines, tomato paste 

and winter squash. Domestic samples accounted for 

59.5 percent of the samples, while 34.9 percent were 

imports, 4.9 percent were of mixed national origin, 

and 0.7 percent were of unknown origin. COVID19-related closures disrupted PDP sampling for 

most of the year in 2020, which may have impacted 

the seasonal observations within the data this year. 

Specific COVID-19-related sampling information 

can be found in Section II. Sampling Operations.

Because PDP data are used for risk assessments, PDP 

laboratory methods are geared to detect very low 

levels of pesticide residues, even when those levels 

are well below the tolerances established by EPA. 

Prior to testing, PDP analysts washed samples for 15 
Pesticide Data Program—Annual Summary, Calendar Year 2020

x

to 20 seconds with gently running cold water as 

a consumer may do; no chemicals, soaps, or any 

special washes were used. 

This summary report includes the distribution of 

residues by pesticide. The full results for more 

than 2.6 million analyses, representing each 

pesticide monitored on each commodity, are too 

numerous to be included in their entirety in this 

summary. The complete PDP database file for 2020 

along with annual summaries and database files for 

previous years are available on the PDP website 

at http://www.ams.usda.gov/pdp or by contacting 

MPD at amsmpo.data@usda.gov. PDP data are 

also available using the PDP database search tool 

that can be accessed at: https://apps.ams.usda.gov/

pdp.

In 2020, over 99 percent of the samples tested 

had residues below the tolerances established by 

the EPA with 30.0 percent having no detectable 

residue. Appendixes B and C provide a distribution 

of residues by pesticide for the commodities tested. 

Residues exceeding the tolerance were detected in 

0.49 percent (47 samples) of the total samples tested 

(9,600 samples). Of these 47 samples, 35 were 

domestic (74.5 percent), 11 were imported (23.4 

percent), and 1 was of unknown origin (2.1 percent). 

Residues with no established tolerance were found 

in 3.2 percent (303 samples) of the total samples 

tested (9,600 samples). Of these 303 samples, 199 

were domestic (65.7 percent), 100 were imported 

(33.0 percent), and 4 were of unknown origin (1.3 

percent).

PDP is a voluntary program and is not designed for 

enforcement of tolerances. However, PDP informs 

the U.S. Food and Drug Administration and EPA of 

presumptive tolerance violations if detected residues 

exceed the EPA tolerance or if residues are detected 

that have no EPA tolerance established.

PDP laboratories also test foods for low levels of 

environmental contaminants that are no longer 

used as pesticides in the United States, but due to 

their persistence in the environment, particularly 

in soil, can be taken up by plants. Results for 

environmental contaminants in all commodities are 

listed in Appendix C. More information on results 

is provided in the Sample Results and Discussion 

section of this summary.

In accordance with Federal civil rights law and U.S. Department of Agriculture (USDA) civil rights regulations 

and policies, the USDA, its Agencies, offices, and employees, and institutions participating in or administering 

USDA programs are prohibited from discriminating based on race, color, national origin, religion, sex, gender 

identity (including gender expression), sexual orientation, disability, age, marital status, family/parental status, 

income derived from a public assistance program, political beliefs, or reprisal or retaliation for prior civil rights 

activity, in any program or activity conducted or funded by USDA (not all bases apply to all programs). Remedies 

and complaint filing deadlines vary by program or incident.

Persons with disabilities who require alternative means of communication for program information (e.g., Braille, 

large print, audiotape, American Sign Language, etc.) should contact the responsible Agency or USDA’s TARGET 

Center at (202) 720-2600 (voice and TTY) or contact USDA through the Federal Relay Service at (800) 877-8339. 

Additionally, program information may be made available in languages other than English.

To file a program discrimination complaint, complete the USDA Program Discrimination Complaint Form, AD3027, found online at How to File a Program Discrimination Complaint and at any USDA office or write a letter 

addressed to USDA and provide in the letter all of the information requested in the form. To request a copy of the 

complaint form, call (866) 632-9992. Submit your completed form or letter to USDA by: (1) mail: U.S. Department 

of Agriculture, Office of the Assistant Secretary for Civil Rights, 1400 Independence Avenue, SW, Washington, 

D.C. 20250-9410; (2) fax: (202) 690-7442; or (3) email: program.intake@usda.gov.

USDA is an equal opportunity provider, employer, and lender.

Mention of a trade name or brand name does not constitute endorsement or recommendation by USDA over 

similar products or vendors.
Pesticide Data Program—Annual Summary, Calendar Year 2020

xi

Acronyms and Abbreviations

% C.V. Percent Coefficient of Variation

A2LA American Association for Laboratory Accreditation

AL Action Level

AMS Agricultural Marketing Service

BQL Below Quantifiable Level

CSV Comma-Separated Values

EPA U.S. Environmental Protection Agency

e-SIF Electronic Sample Information Form

FAO Food and Agriculture Organizations of the United Nations

FAPAS Food Analysis Performance Assessment Scheme

FDA U.S. Food and Drug Administration

FQPA Food Quality Protection Act

GEMS Global Environmental Monitoring Systems – Food Contamination Monitoring and 

 Assessment Programme

GC Gas Chromatography

HCB Hexachlorobenzene

ISO International Organization for Standardization

LC Liquid Chromatography

LOD Limit of Detection

LOQ Limit of Quantitation

MPD Monitoring Programs Division

MRL Maximum Residue Limit

MRM Multiresidue Method

MS Mass Spectrometry

NASS National Agricultural Statistics Service

NCI Negative Chemical Ionization

NSL National Science Laboratories
Pesticide Data Program—Annual Summary, Calendar Year 2020

xii

PDP Pesticide Data Program

PPS Probability proportionate-to-size

PT Proficiency Testing

QA Quality Assurance

QAU Quality Assurance Unit

QuEChERS Quick, Easy, Cheap, Effective, Rugged and Safe

QC Quality Control

RDE Remote Data Entry

SIF Sample Information Form

SOP Standard Operating Procedure

SQL Structured Query Language

USDA United States Department of Agriculture

WHO World Health Organization
Pesticide Data Program—Annual Summary, Calendar Year 2020

1

Pesticide Data Program (PDP)

Annual Summary, Calendar Year 2020

This summary consists of the following sections: (I.) Introduction, (II.) Sampling Operations, 

(III.) Laboratory Operations, (IV.) Database Management, and (V.) Sample Results and Discussion

I. Introduction

The U.S. Department of Agriculture’s (USDA) 

Agricultural Marketing Service (AMS) initiated the 

Pesticide Data Program (PDP) in 1991 to collect 

data on pesticide residues in food, and the program 

now has an important role in the implementation 

of the 1996 Food Quality Protection Act (FQPA). 

The law directs the Secretary of Agriculture to 

collect pesticide residue data on commodities most 

frequently consumed by infants and children. PDP 

data are used primarily by the U.S. Environmental 

Protection Agency (EPA) to assess dietary 

exposure during the review of the safety of existing 

pesticide tolerances (also referred to as maximum 

residue limits in other countries). EPA establishes 

the tolerances after developing a risk assessment 

that considers the following: the pesticide exposure 

through diet and drinking water and from uses in 

and around the home; the cumulative exposure to 

two or more pesticides that cause a common toxic 

effect; the possibility of increased susceptibility to 

infants and children or other sensitive populations 

from exposure to the pesticide; and the possibility 

that the pesticide produces an effect in people 

similar to an effect produced by a naturally 

occurring estrogen or produces other endocrine 

disruption. PDP data also are used by the U.S. 

Food and Drug Administration (FDA) to assist 

in planning commodity surveys for pesticide 

residues as a part of its enforcement and regulatory 

programs.

Because PDP collects data on food commodities 

primarily for consumer exposure assessment, 

program operations differ markedly from those 

followed by regulatory monitoring programs for 

tolerance enforcement. Commodities chosen for 

inclusion in the program are based on EPA data 

needs. PDP samples are collected closer to the 

point of consumption and are prepared emulating 

consumer practices. PDP sampling does not impede 

commodity distribution. Laboratory operations 

are designed to achieve detection of low levels 

rather than quick sample turnaround. As PDP data 

are used in dietary risk assessment, the program 

prioritizes testing for pesticides with registered 

uses for the commodities in the program, as well 

as for pesticides that may not have U.S. tolerances 

but are used in other countries on commodities that 

are imported to the United States.

Primary contributors to PDP’s policy development 

and planning of operations include the participating 

States, other government agencies, and program 

stakeholders (Figure 1(a)), while primary data 

users include EPA, FDA, and a wide range of other 

agencies and groups (Figure 1(b)). Federal, State, 

and foreign government agencies and industries 

have used PDP data to promote the export of 

U.S. commodities to international markets. 

Additionally, PDP methodologies are consistent 

with international guidelines that have been adopted 

by the Codex Committee on Pesticide Residues 

for good laboratory practices (CAC/GL 40-1993), 

performance criteria for methods of analysis 

(CXG 90-2017) and use of mass spectrometry 

(CAC/GL 56-2005). PDP monitoring data are also 

incorporated into the World Health Organization’s 

(WHO) Global Environment Monitoring System - 

Food Contamination Monitoring and Assessment 

Programme (GEMS/Food), a data platform used 

by the Joint Food and Agriculture Organization 

of the United Nations (FAO)/WHO Meeting on 

Pesticide Residues to evaluate dietary exposure 

and recommend the establishment of pesticide 

maximum residue limits (MRLs) to the Codex 

Committee on Pesticide Residues.

In 2020, sampling services were provided by 10 

States (California, Colorado, Florida, Maryland, 

Michigan, New York, North Carolina, Ohio, Texas, 

and Washington; see Figure 2). Laboratory services 

were provided by the States of California, Florida, 

Michigan, New York, Ohio, Texas, and Washington. 

Together, these States represent about 50 percent of 

the Nation’s population and all four census regions 

of the United States. They also represent major 

U.S. producers of fruit and vegetables.
Pesticide Data Program—Annual Summary, Calendar Year 2020

2

Figure 1. Pesticide Data Program (PDP) Program Operations Support and Data Users. This figure illustrates (a) 

agencies/groups that support PDP program policy and planning activities and (b) agencies/groups that use PDP data. 

Program Operations

Participating 

States

National

Agricultural Statistics 

Service

Industry and

Grower Groups

Environmental

Protection

Agency

(a) PDP Policy and Planning Contributors

Data

Food and Drug 

Administration Environmental 

Protection Agency

Academic 

Institutions

Agricultural 

Industry

Foreign 

Agricultural 

Service

Economic 

Research 

Service

Chemical 

Manufacturers, 

Environmental 

Interest Groups, Food 

Safety Organizations

Other 

Government 

Agencies

Participating 

States

(b) PDP Data Users

Food and Drug 

Administration
Pesticide Data Program—Annual Summary, Calendar Year 2020

3

The AMS Monitoring Programs Division (MPD) 

is responsible for overall management of PDP, 

including cooperative agreements with the States, 

sampling and laboratory testing approaches, 

and data management and analysis. Each year 

MPD works closely with EPA and FDA to select 

commodities and pesticides for testing; both 

commodities and pesticides are prioritized by PDP 

based on EPA and/or FDA data needs. Typically, 

the selected commodities represent the highest 

U.S. consumption, with an emphasis on foods 

consumed by infants and children. Due to budget 

limitations, the high consumption commodities are 

cycled through the program approximately every 

1 The U.S. National Residue Program (NRP) administered by the U.S. Department of Agriculture’s (USDA), Food Safety and 

Inspection Service (FSIS) monitors pesticide residues for meat, poultry, and egg products.

5 years rather than tested continuously. Specialized 

commodities (e.g., fresh herbs) are added to the 

rotation as data are needed. Fresh fruit and vegetable 

commodities remain in the program for 2 years to 

capture two full growing seasons, thereby capturing 

any changes due to seasonality or year-to-year 

variations. Processed products, as well as dairy, fish, 

and grains, are tested for 1 full year. All commodity 

rotations are provided in the PDP Program Plans 

prior to the start of sampling and are shown in Table 

1 for 2020. A total of 126 commodities have been 

tested by PDP from the beginning of the program (in 

1991) through 2021 (Appendix A).1

 

Washington

California

Colorado

Texas

Ohio

New York

Florida

Maryland

Michigan

Participating State

Location of Participating State Laboratories

North Carolina

Figure 2. Program Participants. During 2020, USDA’s Agricultural Marketing Service established cooperative agreements 

with 10 States to sample and/or test Pesticide Data Program commodities. Together, these States represent about 50 percent of 

the Nation’s population and all four census regions of the United States. These States are the major U.S. producers of fruit and 

vegetables. State laboratories were responsible for analyzing fresh and processed fruit and vegetable samples. 
Pesticide Data Program—Annual Summary, Calendar Year 2020

4

Fruit and vegetable samples are collected at terminal 

markets2 and distribution centers from which 

food commodities are supplied to supermarkets 

and grocery stores. Sampling at these locations 

allows for residue measurements that include 

pesticides applied during crop production and those 

applied after harvest (such as fungicides, growth 

regulators, and sprouting inhibitors) and considers 

residue degradation while food commodities are 

in storage. Participation as a PDP sampling site is 

voluntary, which sets it apart from State and Federal 

enforcement programs. In 2020, over 570 sites 

granted access and provided information, including 

site volume data, to sample collectors. Voluntary 

cooperation is important to PDP and makes it 

possible to adjust sampling protocols in response to 

fluctuations in food distribution and production.

Pesticides prioritized for screening by PDP 

include those with current registered uses for the 

commodity being tested and compounds for which 

toxicity data and preliminary estimates of dietary 

exposure indicate the need for more extensive/

updated residue data. PDP also monitors pesticides 

for which EPA has modified use directions (i.e., 

reduced application rates or frequency) as part of 

risk management activities. In addition, PDP tests 

for selected pesticides that may not have U.S. 

tolerances but are used in other countries that 

export commodities to the United States. Appendix 

B lists the specific pesticides tested in the fruit and 

vegetable samples. Environmental contaminants, 

or pesticides whose uses have been canceled in 

the United States, but their residues persist in the 

environment, are consolidated into Appendix C, 

which summarizes findings for these chemicals 

across all commodities.

II. Sampling Operations

• Conceptual Framework

The goal of the PDP sampling program is to obtain 

a statistically valid representation of the U.S. food 

supply. PDP data reflect actual pesticide residue 

exposure from food. Using a rigorous statistical 

design, PDP has developed extensive procedures 

that ensure samples are randomly selected from the 

national food distribution system and reflect what is 

typically available to the consumer.

Ten States currently participate in PDP – California, 

Colorado, Florida, Maryland, Michigan, New York, 

North Carolina, Ohio, Texas, and Washington. 

The initial participating States in 1991 (California, 

Florida, Michigan, New York, Texas, and 

Washington) were selected based on agricultural 

production, analytical capabilities, population, 

and regional/geographic distribution – all four 

U.S. Census Regions (West, South, Midwest, 

and Northeast) were represented. Later, in 1993, 

Colorado joined to represent the Mountain Division 

of the Western Region and Ohio to further represent 

the densely populated East North Central Division 

of the Midwest Region. In 1993, North Carolina 

was included to better represent the South Atlantic 

Division of the Southern Region. Maryland was 

added in 1997 to represent the South Atlantic 

Division of the Southern Region. Today, these 

States together represent about 50 percent of the 

Nation’s population and all four census regions of 

the United States.

Commodities chosen for inclusion in the program 

are based on EPA data needs. Foods selected for 

testing are high-consumption items with a strong 

focus on the foods that compose the diets of infants 

and children. Each fresh commodity is sampled and 

tested for 2 years in order to capture annual and 

seasonal variability. High-consumption items are 

rotated in and out of the program every 5 years–for 

example, apples, lettuce, and oranges are retested 

and the data refreshed every 5 years.

PDP collects a minimum of 600 samples per 

commodity per year in order to provide an accurate 

statistical representation for a given commodity. 

PDP collects additional samples to allow 

apportionment among the participating States over 

a 12-month period and to allow for a small sample 

overage for any missed, damaged, or unusable 

samples. Participating State population figures are 

used to apportion the number of samples scheduled 

for collection by each state (for more detail see the 

2020 Sampling Operations later in this section). 

PDP sampling operations may be adjusted according 

2 Terminal markets are facilities where wholesalers receive large quantities of fresh fruit and vegetables by rail, truck, and air 

from around the world for sale to grocers, restaurants, institutions, and other businesses. Terminal markets are often located in 

metropolitan areas at or near major transportation hubs.
Pesticide Data Program—Annual Summary, Calendar Year 2020

5

to product availability. For example, cherries, 

nectarines, and peaches may be oversampled 

during the summer months to make up for low 

availability during winter months. In some cases, 

frozen product is allowed as an alternative to fresh 

(e.g., cranberries).

PDP samples are collected at terminal markets 

and warehouse distribution centers, close to the 

point of consumption. Participating State agencies 

compile and maintain lists of these sampling 

sites. In 2020, 573 sites granted access to sample 

collectors. The States provide AMS and USDA, 

National Agricultural Statistics Service (NASS) 

with annual volume information for commodities 

distributed at these sites. Based on this information, 

sites are assigned volume indicators compared to 

other sites in the same State. This volume indicator 

is used to ensure larger sites are selected more 

frequently than smaller sites. This information is 

used to weigh the site to determine the probability 

for sample selection. For example, a weight of 

10 may be given to a site that distributes 100,000 

pounds of produce annually and a weight of 1 

is given to a site that distributes 10,000 pounds. 

This site selection method, termed probabilityproportionate-to-size (PPS), then results in the 

larger site being 10 times more likely to be selected 

for sampling than the smaller site.

Each participating State works with NASS to 

develop statistical procedures for site weighting 

and selection. States are also given the option to 

have NASS perform their quarterly site selection. 

The number of sampling sites and the volume of 

produce distributed by the sites vary greatly among 

States. Sampling plans that include sampling 

dates, sites (primary and alternate), targeted 

commodities, and testing laboratories are prepared 

by each State on a quarterly basis. Collection of 

commodities is randomly assigned to weeks of 

the month, prior to selection of specific sampling 

dates within a week. Because sampling sites are 

selected for an entire quarter, States may assign 

the sites to particular months based on geographic 

location.

Sample information is captured at the time of 

collection for inclusion in the PDP database. PDP 

sample origin data identify the State or country 

where the commodity was produced. A comparison 

of PDP sample origin data to State production 

and import data by USDA’s NASS shows PDP 

sampling is representative of the U.S. food supply.

• Sampling Procedures

While obtaining PDP samples, collectors randomly 

select the scheduled commodities. Collectors 

use established procedures to prevent crosscontamination and maintain chain-of-custody. PDP 

State sample collectors are trained to adhere to 

detailed program Standard Operating Procedures 

(SOPs) that provide criteria for site selection and 

specific instructions for sample selection, shipping 

and handling, and chain-of-custody. SOPs are 

updated as needed and serve as a technical reference 

in conducting program sampling reviews to 

ensure program goals and objectives are met. PDP 

sampling SOPs are available on the website: www.

ams.usda.gov/datasets/pdp. On a quarterly basis, 

sample collectors are provided with Commodity 

Fact Sheets that list specific collection details for 

the individual commodities in the program.

Temperature-sensitive samples are packed in 

heavy-duty, temperature-controlled containers. 

Holding temperatures are preserved throughout 

transit time with the inclusion of ample frozen cold 

packs and insulating materials. Non-temperaturesensitive samples do not require temperaturecontrolled containers; however, they are shipped in 

heavy-duty, well-cushioned containers. To preserve 

sample integrity, most samples are shipped the 

same day by overnight delivery. Non-refrigerated 

processed commodities such as tomato paste are 

often shipped by ground transportation to reduce 

shipping costs.

Electronic Sample Information Forms (e-SIFs) 

are used for chain-of-custody and to capture 

information needed to characterize the sample. 

Sample collectors use tablets or laptop computers in 

the field to record sample identification information 

such as: (1) State of sample collection, (2) collection 

date, (3) sampling site code, (4) commodity code, 

and (5) testing laboratory code. Information from 

these five data elements is combined to form a 

unique PDP identification number for each sample.
Pesticide Data Program—Annual Summary, Calendar Year 2020

6

Other available information about each sample is 

also recorded, such as collector name; the country 

of origin; product variety; production claims such 

as organic; expiration date; and grower, packer, 

and/or distributor locations. The e-SIFs are sent 

electronically the same day as sample collection or, 

at the latest, by the next morning after collection to 

ensure that sample information is received at each 

laboratory by the time samples arrive for analysis. 

Refer to Section IV on Database Management for 

more information on the e-SIF system.

Because most PDP samples are collected at 

distribution centers, terminal markets, and other 

wholesalers, entire cases must be obtained while 

a significantly smaller portion is sent to the 

laboratory for testing. For example, if a 20-pound 

case of apples is collected and a 5-pound sample 

is sent for testing, the remaining 15 pounds are 

typically donated. In most cases, the excess 

samples are donated to organizations such as local 

food banks, shelters, senior assisted living centers, 

churches, and other charities. PDP often provides 

the only fresh commodity donations available to 

these organizations. In 2020, PDP State participants 

donated over 40,000 pounds of food to local 

charities. 

• 2020 Sampling Operations

The number of fruit and vegetable samples collected 

in each participating State is determined by State 

population. The monthly collection schedule for all 

2020 commodities is shown in Table 1; however, 

not all samples scheduled were collected due to 

the Coronavirus COVID-19 pandemic. In March 

of 2020, the global COVID-19 pandemic began 

impacting PDP sampling operations. Within the 

first 2 weeks of impacts, 7 of the 10 PDP sampling 

States suspended collection. Sampling operations 

were severely impacted in April, when only 33 

percent of samples were collected. The first makeup samples were collected in May as some States 

re-opened. MPD issued guidance prioritizing 

Commodity Jan-Mar Apr-Jun Jul-Sep Oct-Dec End Date

Apple Juice Dec-20

Bananas Dec-20

Blueberries Sep-22

Blueberries, Frozen Sep-22

Broccoli Dec-21

Cantaloupe Jun-21

Carrots Mar-22

Cauliflower Sep-21

Collard Greens Sep-20

Eggplant Dec-21

Green Beans Sep-22

Kiwi Fruit Mar-20

Orange Juice Sep-20

Radishes Dec-20

Summer Squash Sep-22

Sweet Bell Peppers Jun-21

Tangerines Sep-21

Tomato Paste Sep-20

Winter Squash Dec-21

Table 1. Pesticide Data Program (PDP) Commodity Collection Schedule for 2020. Samples are 

most often collected for a 2-year time period. Commodities are initiated or terminated in different 

quarters of the year so that new commodities are not brought into the program all at the same time. 

This table illustrates time ranges for the listed commodities. See Appendix A for the complete PDP 

commodity history (May 1991 through December 2021). 
Pesticide Data Program—Annual Summary, Calendar Year 2020

7

missed commodities to minimize potential impacts 

on seasonality. Three tiers were established, one 

for highly seasonal commodities (cantaloupe, 

sweet bell pepper, tangerines, winter squash), one 

for moderately seasonal commodities (carrots, 

eggplant, radishes), and one for commodities with 

little to no seasonal influences (bananas, broccoli, 

cauliflower, collard greens). By September, 

sampling operations had resumed in 9 of the 10 

PDP collection States, with Florida being the 

exception. In October, all 10 States resumed 

sample collection, and this was the first month 

since February with no missed samples. California 

suspended sample collection in December and the 

State did not collect 9 of its 14 commodities for the 

month. These represented the only missed samples 

in December. Figure 3 illustrates the number of 

collected, missed, and make-up samples by month. 

While yearly sample targets were met (minimum 

600 samples per commodity), results could 

potentially have been impacted by interruptions to 

the 2020 sampling schedule. PDP tried to minimize 

seasonality affects by prioritizing commodities 

most likely to be affected by seasonality for makeup samples.

The total number of samples collected in each State 

for each commodity is listed in Table 2. Table 3 

lists the acceptable product types for each collected 

commodity as seen on Commodity Fact Sheets 

provided to sample collectors. For all commodities, 

domestic or imported and organically grown or 

conventionally grown products are acceptable. In 

2020, 7.4 percent of the tested samples were organic 

(706 of 9,600); summaries of findings by claim may 

be found by using the PDP web app: https://apps.

ams.usda.gov/pdp.

State population figures are used to assign the 

number of fruit and vegetable samples scheduled for 

collection each month. During 2020, the monthly 

number of samples assigned for each State included: 

California, 13; Colorado, 2; Florida, 7; Maryland, 4; 

Michigan, 6; New York, 9; Ohio, 6; Texas, 8; and 

Washington, 4. This schedule resulted in a monthly 

target of 59 samples per commodity or 708 samples 

per commodity per year.

Additionally, North Carolina collected 4 samples 

per month for selected commodities–apple juice, 

blueberries, collard greens, green beans, orange 

Figure 3. Monthly Sample Collection in 2020. This figure illustrates the impacts of the COVID-19 pandemic on PDP 

sampling operations.

Scheduled Collected Scheduled Missed Make-up Samples

0

10

20

30

40

50

60

70

80

90

100

JAN

FEB

MAR

APR

MAY

JUN

AUG

SEP

OCT

NOV

DEC

JUL

Percent of Target Monthly Samples (%)
Pesticide Data Program—Annual Summary, Calendar Year 2020

8

juice, summer squash and tomato paste, which 

resulted in a total of 63 samples per commodity per 

month for these products.

In 2020, fruit and vegetable samples were randomly 

collected by trained State inspectors at terminal 

markets and large chain store distribution centers 

throughout the country. Surrogate or “proxy” sites 

(retail markets) are used to collect these samples 

when the commodity of interest is unavailable 

at a terminal market or distribution center. In 

these instances, the commodity is selected in the 

rear storage area of the retail facility so possible 

contamination by the consumer is eliminated 

and to allow capture of sample information from 

product boxes. In 2020, 32.0 percent of fruit and 

vegetable samples were collected at proxy sites. The 

commodities most often collected at these facilities 

were orange juice, tomato paste, and apple juice. 

The total number of samples per commodity and 

the percentage of each that were either domestic, 

imported, or of unknown origin are shown in Figure 

4. The origin of some fresh commodities can vary 

greatly throughout the year. A graphic example 

of this variation can be found in Figure 5, where 

differences in origin (domestic versus import) are 

depicted by month for cantaloupe and tangerine 

(mandarin) samples.

State BB BN BR CF CN CR EP GB GL KW PP RD SS TA WS

Total 

Fresh

California 24 160 152 161 172 105 148 26 101 39 152 152 26 160 153 1,731

Colorado 4 24 24 24 24 18 24 6 18 6 24 24 6 24 24 274

Florida 21 71 59 62 59 42 54 21 21 21 59 68 21 58 56 693

Maryland 12 50 44 48 42 36 42 12 36 12 44 48 12 48 48 534

Michigan 17 72 72 72 72 54 72 18 54 18 72 72 18 72 72 827

New York 25 108 108 108 108 81 108 27 81 27 108 108 27 108 108 1,240

N. Carolina 11 13 40 12 76

Ohio 18 72 72 72 72 54 71 18 54 18 72 72 18 72 72 827

Texas 24 98 96 97 97 73 94 24 73 24 96 97 24 97 96 1,110

Washington 12 48 48 48 48 36 48 12 36 12 48 48 12 48 48 552

TOTAL 168 703 675 692 694 499 661 177 514 177 675 689 176 687 677 7,864

State AJ BZ OJ TP

Total 

Processed

Total 

Fresh & 

Proccessed 

F&V

California 151 2 100 102 355 2,086

Colorado 24 18 18 60 334

Florida 59 1 21 21 102 795

Maryland 44 31 32 107 641

Michigan 72 1 54 54 181 1,008

New York 108 2 78 80 268 1,508

N. Carolina 48 1 37 36 122 198

Ohio 72 54 54 180 1,007

Texas 97 73 73 243 1,353

Washington 49 33 36 118 670

TOTAL 724 7 499 506 1,736 9,600

Table 2. Distribution of Samples Collected by Each Participating State. This table includes those 

commodities collected at terminal markets, distribution centers, and retail markets. 

Commodity Legend

AJ = Apple Juice GL = Collard Greens

BB = Blueberries, Fresh KW = Kiwi Fruit

BN = Bananas OJ = Orange Juice

BR = Broccoli PP = Sweet Bell Peppers

BZ = Blueberries, Frozen RD = Radishes

CF = Cauliflower SS = Summer Squash

CN = Cantaloupe TA = Tangerines

CR = Carrots TP = Tomato Paste

EP = Eggplant WS = Winter Squash

GB = Green Beans
Pesticide Data Program—Annual Summary, Calendar Year 2020

9

Commodity Acceptable Products

Apple Juice 100% apple juice. Single strength, ready-to-serve in cartons, jars, cans, pouches, 

or plastic containers. Reconstituted from concentrate or not from concentrate. May 

be pasteurized. Individual single-serving box containers are acceptable as long as 

the sample size requirement is met. May contain ascorbic acid/Vitamin C as added 

ingredient.

Bananas Whole, fresh bananas.

Blueberries Any fresh, whole blueberry; cultivated (Highbush) or wild (Lowbush). Fresh are 

preferred, but frozen are acceptable. 

Blueberries, Frozen Frozen blueberries; cultivated (Highbush) or wild (Lowbush). Individually quick frozen 

(IQF) or frozen in own juices. Fresh are preferred, but frozen are acceptable.

Broccoli Fresh broccoli. Broccoli crowns (bunch with top florets plus a little of the stem) 

are preferred. Broccoli with stems (bunch with top florets plus a lot of the stem) is 

acceptable if broccoli crowns are not available.

Cantaloupe Whole, fresh cantaloupe.

Carrots Fresh, whole carrots, with or without tops. 

Cauliflower Any fresh whole cauliflower. White in color.

Collard Greens Fresh collard greens. Pre-bagged or loose.

Eggplant Whole, fresh eggplant. Traditional types that are oval or pear in shape with a black, 

purplish-black, or purple skin color. 

Green Beans Fresh green string beans. Whole or pre-cut.

Kiwi Fruit Whole, fresh fuzzy kiwifruit. Gold or green.

Orange Juice 100% Orange juice. Ready-to-serve containers of orange juice that are refrigerated. 

With or without pulp. Reconstituted from concentrate or not from concentrate.

Radishes Whole, fresh globe-shaped radishes, with or without tops. Red, white, or watermelon. 

Summer Squash Fresh whole zucchini, yellow squash, or crookneck squash.

Sweet Bell Peppers Whole, fresh bell peppers. Colors may include, but are not limited to: green, orange, 

purple, red, or yellow.

Tangerines Any fresh, whole tangerine (mandarin or mandarin orange). Clementine, Minneola, 

Mediterranean mandarin, Satsuma mandarin, or tangelo.

Tomato Paste Any canned tomato paste. May be salted or salt-free. May contain "spices," listed as 

a generic ingredient on the can.

Winter Squash Whole winter squash varieties include but are not limited to: Acorn, banana, Boston 

marrow, buttercup, butternut, Hubbard, kabocha, and spaghetti. 

Table 3. Acceptable Products for Collected Commodities. This table lists the acceptable products for 

each collected commodity as seen on the Commodity Fact Sheets provided to sample collectors. For all 

commodities, domestic or imported and organically grown or conventionally grown products are acceptable.

Fresh and processed fruit and vegetable samples 

originated from 34 States and 34 foreign countries 

(refer to Appendix D).

• Fresh and Processed Commodities

All samples collected and analyzed in 2020 (9,600) 

were fruit and vegetables, including fresh and 

processed products. The fresh commodities collected 

for PDP were bananas, blueberries, broccoli, 

cantaloupe, carrots, cauliflower, collard greens, 

eggplant, green beans, kiwi fruit, radishes, summer 

squash, sweet bell peppers, tangerines (mandarins), 

and winter squash. The processed commodities 

included apple juice, frozen blueberries, orange 

juice, and tomato paste. 

Fresh and frozen fruit and vegetable samples 

weighed either 3 or 5 pounds, except for blueberries 

where the sample size was 1 pound. Three pounds 

were collected for smaller, low-weight commodities 

such as collard greens and kiwi fruit, and 5 pounds 
Pesticide Data Program—Annual Summary, Calendar Year 2020

10

Cantaloupe (694 Samples)

A. Fresh Fruit and Vegetable Samples

Collard Greens (514 Samples) Green Beans (177 Samples)

Summer Squash (176 Samples)

Carrots (499 Samples) Cauliflower (692 Samples)

Bananas (703 Samples) Broccoli (675 Samples)

Domestic 95.5%

Domestic 95.4%

Import 39.2%

Import 2.0%

Import 100%

Import 4.0%

Unknown 0.6%

Domestic 63.3%

Domestic 59.0%

Import 25.3%

Unknown 1.8%

Domestic 74.7%

Radishes (689 Samples)

Import 19.6%

Domestic 78.2%

Kiwi Fruit (177 Samples)

Import 21.1%

Blueberries (168 Samples)

Domestic 49.2%

Domestic 80.1%

Unknown 0.3%

Unknown 2.5%

Import 33.9%

Unknown 2.8%

Import 50.8% Unknown 0.7%

Domestic 6.5%

Import 93.5%

Domestic 60.5% Unknown 0.4%

Import 39.1%

Eggplant (661 Samples)

Domestic 43.2%

Import 53.4%

Unknown 3.4%
Pesticide Data Program—Annual Summary, Calendar Year 2020

11

Sweet Bell Peppers (675 Samples)

Figure 4. Commodity Origin. This figure depicts the proportion of commodity origin (domestic, import, unknown, 

and mixed national origin) for each fresh and processed fruit and vegetable product tested in 2020.

Tangerines (687 Samples)

Domestic 48.0%

Unknown 0.6%

Import 52.0%

Domestic 52.7%

Import 46.7%

Blueberries, Frozen (7 Samples)

Domestic 28.6%

Apple Juice (724 Samples)

Unknown 0.4%

Import 71.4%

Orange Juice (499 Samples)

Domestic 42.7%

Import 31.2%

Domestic 36.3%

Unknown 0.8%

Mixed National 25.7%

B. Processed Fruit and Vegetable Commodities

Tomato Paste (506 Samples)

Domestic 98.4%

Import 0.8%

Winter Squash (677 Samples)

Domestic 49.5%

Import 50.2%

Unknown 0.3%

Import 5.0%

Mixed National 57.9%

Unknown 0.8%
Pesticide Data Program—Annual Summary, Calendar Year 2020

12

Figure 5. Origin of Selected Fresh Commodity: Cantaloupe and Tangerine Samples. Differences in origin 

(domestic vs. import) are illustrated by month. 

Domestic Imported Unknown

Origin of Cantaloupe Samples

JAN

FEB

MAR

APR

MAY

JUN

AUG

SEP

OCT

NOV

DEC

60

10

20

30

40

50

Number of Samples

Origin of Tangerine Samples

JANFEB

MAR

APR

MAY

JUN

JUL

AUG

SEP

OCT

NOV

DEC

60

10

20

30

40

50

Number of Samples

70

JUL

90

80

70

90

80

were collected for larger, high-weight commodities 

such as cantaloupe and sweet bell peppers. For 

processed commodities, a sample size of 1 quart (32 

ounces) was collected for apple juice and orange 

juice and 1-pound samples were collected for frozen 

blueberries and tomato paste.

• Sampling Limitations 

Ten States from all four census regions of the United 

States participate in PDP. The States that participate 

account for about 50 percent of the U.S. population 

and the major agricultural production areas of the 

country, making them representative of the United 

States as a whole.

PDP collects samples from over 570 distribution 

centers and terminal markets within the participating 

States. The total number of distribution centers and 

terminal markets within the participating States is 

difficult to establish since existing sites may go out 

of business or merge and new sites may open during 

the year. However, there is no evidence to believe 

that sites within the States that participate differ 
Pesticide Data Program—Annual Summary, Calendar Year 2019

13

significantly from those that do not participate. 

Since these sites are similar throughout the State, 

they are representative of all sites in the State.

Sometimes it is necessary to replace the site that 

was originally selected using PPS. In those cases, 

an alternate site of similar size is selected from 

the quarterly site list by the State personnel to 

replace the original site. Whenever possible, a site 

of similar size in the same region as the original 

site is chosen as the replacement. Additionally, 

the availability of a specific commodity may 

necessitate a change in site selection. For example, 

cantaloupe may be collected from an alternate site 

if the primary site is out of stock.

III. Laboratory Operations

• Overview

Seven State laboratories performed analyses 

for PDP. These laboratories are equipped with 

instrumentation capable of detecting residues at 

very low levels. Laboratory staff members receive 

intensive training and must demonstrate analytical 

proficiency on an ongoing basis. Laboratory 

scientists continually test new technologies and 

develop new techniques to improve the levels of 

detection. Any major change in methodology and/

or instrumentation is evaluated, and its soundness 

demonstrated and documented by means of method 

validation modules in accordance with PDP SOPs.

• Fresh and Processed Commodities

A total of 9,600 fresh and processed fruit and 

vegetable samples were tested for 584 parent 

pesticides, metabolites, degradates, and/or isomers, 

plus 21 environmental contaminants using MultiResidue Methods (MRMs). Pesticides prioritized 

for screening by PDP include those with current 

registered uses for the commodity being tested and 

compounds for which toxicity data and preliminary 

estimates of dietary exposure indicate the need for 

more extensive residue data.

Upon arrival at the testing facility, samples of 

fresh commodities were visually examined for 

acceptability and discarded if determined to be 

inedible (decayed, extensively bruised, or spoiled). 

Laboratories are permitted to refrigerate incoming 

fresh fruit and vegetable samples of the same 

commodity up to 72 hours to allow for different 

sample arrival times from collection sites. Frozen 

and canned commodities may be held in storage 

(freezer or shelf) until the entire sample set is ready 

for analysis.

Each sample is prepared according to the procedures 

detailed in Table 4, which lists the steps for 

preparing each commodity for analysis as defined 

in the Laboratory Sample Processing and Analysis 

SOP. For all commodities, the sample is chopped, 

mixed, or blended until a visually homogeneous 

mixture is attained.

Samples are separated into analytical portions 

(aliquots) for analysis. If testing cannot be 

performed immediately, the entire analytical set 

is frozen at -40°C or lower according to PDP’s 

Quality Assurance/ Quality Control (QA/QC) 

requirements. Surplus aliquots not used for the 

initial testing are retained frozen in the event that 

replication of analysis or verification testing is 

required.

For analysis of fruit and vegetable samples, testing 

laboratories use various Quick, Easy, Cheap, 

Effective, Rugged and Safe (QuEChERS)-based 

approaches.3 All MRMs are determined, prior to 

use and through appropriate method validation 

procedures, to produce equivalent data for PDP 

analytical purposes. PDP laboratories use gas 

chromatography (GC) and liquid chromatography 

(LC) instrumentation, coupled with tandem mass 

spectrometry (MS) detection systems for the 

simultaneous identification/confirmation and 

quantitation of pesticides. The use of these GC-MS/

MS and LC- MS/MS systems allows the program 

to capture data for a broad spectrum of pesticides, 

including emerging product chemistries.

• Quality Assurance Program

The primary objectives of the QA/QC program 

are to ensure the reliability of PDP data and the 

performance equivalency of the participating 

laboratories. Direction for the PDP QA program 

3

 M. Anastassiades, S.J. Lehotay, D. Stajnbaher and F.J. Schenck, “Quick, Easy, Cheap, Effective, Rugged and Safe 

(QuEChERS) Method,” J AOAC Int 86 (2003) 412.
Pesticide Data Program—Annual Summary, Calendar Year 2020

14

Commodity Sample Preparation Steps

Bananas If necessary, banana samples may be stored in a secure location at room temperature 

for up to 72 hours for ripening purposes. To accelerate ripening, the bananas can be 

stored in a paper bag. Peel each fruit. 

Blueberries Wash blueberries by the handful or by using a colander and drain. 

Blueberries, Frozen The samples may be chopped while frozen, or to prevent damage to the chopper/

homogenizer blades, the sample may be thawed in a refrigerator or in a room 

temperature water bath. Open the containers and pour the entire contents into the 

chopper/homogenizer. 

Broccoli Visually examine and discard any damaged portion or wilted florets. Do not discard 

leaves unless they are wilted. Trim away inedible portions of stems. If the stem is less 

than 3 inches, do not trim. If the stem is longer than 3 inches, thinly slice away the 

tough outer layer on the stalk. Wash and drain.

Cantaloupe Cut each cantaloupe in half and remove seeds and rind. Halves may be further 

divided at this point to facilitate removal of the rind.

Carrots If carrots have any visible dirt, hold each carrot under cold running tap water and 

gently scrub the entire surface with a clean vegetable brush to remove any loose soil 

and grit. Rinse and drain. With a clean, dry knife, remove stem cap portion from each 

carrot.

Cauliflower Visually examine the head and remove wrapper leaves and any damaged portions. 

Rinse, turn the head top side down to drain.

Collard Greens Visually examine the sample and remove only the damaged or wilted leaves and any 

woody stems. Wash and drain. Note: Bagged pre-washed greens do not require 

washing by the laboratory.

Eggplant Wash and drain. Using a clean, dry knife, remove the end pieces.

Green Beans Wash and drain. Do not peel. Using a clean, dry knife, remove any stems that are 

present.

Juices: Apple Juice, 

Orange Juice

For fresh and reconstituted juices, ensure that the sample is evenly mixed to obtain 

a homogeneous mixture. For concentrates, dilute juice in a dry, clean container with 

cold running tap water, according to label directions.

Kiwi Fruit Wash and drain. Do not peel.

Radishes Hold each radish under cold running tap water and remove any loose soil and grit 

(discard the leaf portion). Rinse and drain. Note: Bagged pre-washed radishes do not 

require washing by the laboratory. Remove any tops or roots that are present.

Summer Squash Wash and drain. Using a clean, dry knife, remove end pieces.

Sweet Bell Peppers Wash and drain. Remove stem, core, and seeds.

Tangerines Peel each fruit and remove any excess white membrane.

Tomato Paste, Canned If the lid of the can has visible dirt or dust, rinse the lid under cold running tap water for 

5 to 10 seconds. Dry the lid with a paper towel. Open each can and pour the entire 

contents of each can including the liquid into a blender/homogenizer. 

Winter Squash Wash and drain. When possible, using a clean, dry knife, remove stem and/or end 

pieces.

Table 4. Sample Preparation Steps for Analysis. This table lists the steps for preparing each collected commodity 

for analysis as defined in the Laboratory Standard Operating Procedure. The wash and drain steps refer to a wash 

under cold running water for approximately 15-20 seconds to assure that all surfaces are rinsed, then a drain for 

at least 2 minutes. For all commodities, the sample is chopped, mixed, or blended until a visually homogeneous 

mixture is attained.
Pesticide Data Program—Annual Summary, Calendar Year 2020

15

4 “ISO” is not an acronym because the initials would be different in various official languages. “ISO” is adopted from the 

Greek word “isos” meaning equal.

is provided through SOPs based on EPA Good 

Laboratory Practices, along with program-specific 

QA/QC requirements. The PDP SOPs provide 

uniform administrative and sampling procedures, 

as well as guidelines for laboratory operations 

and data analyses. The SOPs are revised annually 

to accommodate changes in the program and 

are aligned with International Organization 

for Standardization (ISO)4 requirements. PDP 

laboratories are accredited to ISO 17025 by the 

American Association for Laboratory Accreditation 

(A2LA), an internationally recognized accrediting 

body. 

A Technical Advisory Group, comprised of 

laboratory Technical Program Managers and 

Quality Assurance Officers, is responsible for 

annually reviewing program SOPs and addressing 

QA issues. For day-to-day QA oversight, PDP 

relies on the Quality Assurance Unit (QAU) at 

each participating facility. The QAU operates 

independently from the laboratory staff and is 

responsible for reviewing all data generated for 

PDP and for performing quarterly, internal program 

audits. Preliminary data review procedures are 

performed onsite by each laboratory’s QAU. MPD 

staff conduct a final review of data for conformance 

with SOPs.

Method Performance Requirements: Laboratories 

are required to determine and verify the limits of 

detection (LODs) and limits of quantitation (LOQs) 

for each pesticide/commodity pair. LODs depend 

on matrix, analyte, and methods used (extraction 

and instrumental). LODs for each pesticide/

commodity pair are shown in the applicable crop 

results appendix. Additional method performance/

validation requirements include modules for 

consistent instrument response (linearity), method 

range, and precision and accuracy.

Identification/Confirmation: Identification/confirmation is performed using MS technologies. 

Residue amounts greater than or equal to LOD 

and below LOQ are reported as below quantifiable 

level (BQL). BQLs are assigned values at one-half 

the LOQ and are used along with values greater 

than or equal to LOQ and non-detects in dietary 

risk assessments when appropriate.

Routine Quality Control Procedures: PDP 

procedures for QC are used to assess method and 

analyst performance during sample preparation, 

extraction, and cleanup. To maximize sample 

output and decrease the QC/sample ratio, samples 

are analyzed in analytical sets that include the test 

samples and the following components:

• Reagent Blank - For analysis of fruit and 

vegetables, an amount of distilled water, equivalent 

to the natural moisture content of the commodity, is 

run through the entire analytical process to confirm 

glassware cleanliness and system integrity.

• Matrix Blank - A previously analyzed sample 

of the same commodity, which contains either 

very low concentrations of known residues or no 

detectable residues, is divided into two portions. 

The first portion is used to determine background 

information on naturally occurring chemicals and 

the second to prepare a matrix spike.

• Matrix Spike(s) - Prior to extraction, a portion of 

the matrix blank is spiked with marker pesticides to 

determine the precision and accuracy of the analyst 

and instrument performance. Marker pesticides 

are compounds selected from different pesticide 

classes (e.g., organochlorines, organophosphates, 

carbamates, conazoles, imidazolinones, macrocyclic lactones, neonicotinyls, phenoxy acid 

herbicides, pyrethroids, strobilurins, sulfonyl urea 

herbicides, triazines, uracils), with physical and 

chemical characteristics representative of their 

corresponding pesticide class. Marker pesticides 

may be used to monitor recovery instead of spiking 

all pesticides. This use of marker pesticides 

optimizes the resources required to analyze the 

thousands of analyte/matrix combinations in the 

program while still allowing evaluation of daily 

recovery patterns.

In addition, each laboratory must perform matrix 

spikes at least quarterly for each analyte/crop 

combination it reports. Some laboratories choose to 

rotate spikes of all compounds on a set-by-set basis 

or spike all compounds analyzed with each set, so 

that the amount of spike recovery data obtained 

exceeds the minimal requirements previously 

stated. During 2020, PDP laboratories quantitated 
Pesticide Data Program—Annual Summary, Calendar Year 2020

16

a total of 81,157 matrix spikes, with an overall 

mean recovery of 96.1 percent and an overall 20.1 

percent coefficient of variation (% C.V.). The % 

C.V. is calculated as the standard deviation divided 

by the mean.

• Process Control Spike - A compound with physical 

and chemical characteristics similar to those of 

the pesticides being tested is used to evaluate the 

analytical process on a sample-by-sample basis. 

Each of the analytical set components, except 

the reagent and matrix blanks, is spiked with 

process controls. During 2020, PDP laboratories 

quantitated a total of 20,187 process controls on 

9,600 samples, with an overall mean recovery of 

100 percent and an overall 15.6 percent C.V. Of 

these process controls, 22 (0.11 percent) were 

reruns due to initial failure to meet PDP recovery 

criteria. The rerun values are not included in these 

statistics.

Proficiency Testing: All facilities are required 

to participate in PDP’s Proficiency Testing 

(PT) program. In order to properly benchmark 

performance, PDP laboratories participate in 

the international Food Analysis Performance 

Assessment Scheme (FAPAS), administered by 

the Food and Environment Research Agency, 

Sand Hutton, York, United Kingdom. In 2020, 

PDP laboratories that routinely analyze fruit and 

vegetable samples via MRMs participated in one 

FAPAS round for apple purée that contained 12 

fortified analytes. Laboratories were evaluated 

based on z-scores for reported compounds, as well 

as any reported false negatives or false positives. 

PDP laboratories typically obtained z-scores 

less than two, which is deemed satisfactory 

performance.

In addition, PDP laboratories participate in an 

internal PT program that is tailored to current 

PDP commodities and testing profiles. For this 

internal program, the California Department of 

Food and Agriculture QAU prepares and issues 

rounds designed in collaboration with MPD. 

Spiking compounds are selected with specificity 

and levels for each commodity. Fortification levels 

of selected analytes are generally 1 to 10 times the 

program LOQ for that commodity/compound pair. 

For each multiresidue round, one compound per 

set is typically repeated within the round to provide 

an indicator of repeatability. The resulting data 

are used to determine performance equivalency 

among the testing laboratories and to evaluate 

individual laboratory performance.

During 2020, PDP laboratories received two 

multiresidue fruit and vegetable PT rounds 

(mushrooms and cantaloupe), each consisting of 

three test samples. The mushroom samples were 

fortified with a total of 12 different compounds 

with azoxystrobin spiked on 2 different samples. 

The cantaloupe samples were fortified with a total 

of 11 different compounds with fludioxonil spiked 

on 2 different samples at the same level to evaluate 

within and between laboratory variability.

Onsite Reviews: In addition to the onsite 

assessments performed by A2LA that are required 

to maintain ISO 17025 accreditation, MPD staff 

chemists perform onsite reviews of laboratory 

operations to determine compliance with PDP 

SOPs and provide a report of findings identifying 

potential areas of improvement. Improvements 

in sampling, chain-of-custody, laboratory, 

recordkeeping, and electronic data transmission 

procedures are made as a result of onsite reviews. 

The 2020 onsite reviews were postponed due to 

COVID-19-related travel restrictions.

IV. Database Management

PDP maintains an electronic database that serves 

as a central data repository. The data captured 

and stored in the PDP database include sample 

collection and product information, residue 

findings, and process control recoveries for each 

sample analyzed, in addition to QA/QC fortified 

recoveries for each set of samples. Each calendaryear survey is stored in a separate database 

structure, which allows easier administration 

and data reporting. The PDP data pathway is 

illustrated in Figure 6.

• Electronic Data Path

PDP utilizes the Remote Data Entry (RDE) system, 

which is a customized software application 

that allows participating State and Federal 

laboratories to electronically enter and transmit 

data. The RDE system is distributed with all user 

interface software and database files residing on 
Pesticide Data Program—Annual Summary, Calendar Year 2020

17

- Collection in 10 States

- Samples taken close to consumer consumption

- Standardized sample information forms

- Data entry on tablet/laptop computers

- Chemists review data on-screen

- Upload data to central database

- 7 State laboratories

- Fruit and vegetable samples prepared for

 consumption

- Detect residues at low levels

- Pesticide residue data generated

- Multi-tiered quality assurance data review

 process

- Customized data entry software

- Import data from other systems

- Access controlled by user login

- Extensive data cross-checks

- Data reconciliation

- Standard & ad hoc reporting

- Annual Summary

- Data available online

YEAR-END REVIEW

INTERNET

SAMPLE COLLECTION DATA REVIEW AT HQ

LABORATORY ANALYSIS

LABORATORY REMOTE DATA 

ENTRY (RDE) DATA REPORTING

INTERNET

Figure 6. Pesticide Data Program (PDP) Data Pathway: An illustration of PDP data path from sample collection 

through laboratory analysis and reporting.
Pesticide Data Program—Annual Summary, Calendar Year 2020

18

laboratory computers. The laboratory users need 

only Microsoft® Office tools to interface with the 

RDE system. Access is controlled through separate 

user login/password accounts and user access 

rights for the various system functions based on 

position requirements. The RDE system utilizes 

file encryption to secure all data stored in and 

transmitted from the RDE system.

A separate Windows®-based system allows 

sample collectors to capture the standardized 

Sample Information Form (SIF) electronically 

on laptop or tablet computers. The e-SIF system 

generates formatted text files containing sample 

information that are e-mailed to MPD staff for 

central processing and distribution to the analyzing 

laboratories for import into the RDE system.

The RDE data entry screens have extensive editing 

functions and cross-checks built into the software 

to ensure valid values are entered for all critical 

data elements. This task is made easier by the 

practice of capturing and storing standardized 

codes for all critical alphanumeric data elements 

rather than their complete names, meanings, or 

descriptions. This coding scheme allows for faster 

and more accurate data entry, saves disk storage 

space, and allows the user to perform ad-hoc 

queries (data searches) on the database easily. The 

data entry screens also perform checks on numeric 

fields, dates, and other character fields to ensure 

entries are within established boundaries.

MPD staff chemists review the data online and then 

mark the data as ready-for-upload to the central 

PDP database. A separate upload application 

converts and passes the data to the PDP database, 

which is maintained using Microsoft® SQL Server 

and Access database tools. Access to the central 

PDP database is limited to MPD personnel and is 

controlled through password protection and user 

access rights.

• Data Reporting

The MPD staff frequently receives requests for 

data from government agencies and interested 

outside parties. Adhoc queries and custom reports 

are generated to fill such requests. An electronic 

library of data queries is maintained to generate 

standardized data summaries, including the data 

tables, charts, and appendixes in this annual 

summary. Subsets of the PDP calendar-year 

databases are made available for download from 

the PDP website. The data files on the website 

are delimited text files that contain a portion of 

the sampling data, all reported residue findings, 

and reference lists that can be used to interpret 

the standardized codes seen in the PDP data. The 

data files can be imported into defined database 

structures and manipulated using common 

database management software packages.

• Online Database Search Tool

An online PDP Database search tool is available 

for public use. The search tool allows anyone 

with internet access to search for PDP pesticide 

residue findings on commodities tested across 

all published years. Search criteria are selected 

from lists of all reported commodities, pesticides, 

and survey years. One of five output preferences 

is selected to show individual residue findings 

or summary data. The generated dataset can be 

exported to a comma-separated values (CSV) 

file. The search tool can be reached from any PDP 

website page or directly at https://apps.ams.usda.

gov/pdp.

V. Sample Results and Discussion

• Overview

In 2020, PDP conducted surveys on a variety 

of foods including fresh and processed fruit 

and vegetables. Of the 9,600 samples analyzed 

in 2020, 7,864 were fresh fruit and vegetable 

samples and 1,736 were processed products. 

PDP testing methods are designed to detect low 

levels of pesticide residues. In 2020, over 99 

percent of the samples tested had residues below 

the tolerances established by the EPA, with 30.0 

percent having no detectable pesticide residue. 

The data reported by PDP illustrate that residues 

found in agricultural products sampled are at 

levels that do not pose risk to consumers’ health 

and are safe according to EPA and FDA.

Appendix B tabulates the distribution of residue 

results for fruit and vegetables. Information 

included in this appendix are the number of 
Pesticide Data Program—Annual Summary, Calendar Year 2020

19

samples analyzed for each compound, number 

and percent of samples with detections, range of 

concentrations detected, range of analytical LODs, 

and EPA tolerance levels.

PDP laboratories tested foods for low levels 

of environmental contaminants. The selected 

contaminants were pesticides and are no longer 

used in the United States, but due to their 

persistence in the environment, particularly 

in soil, these contaminants can be still taken 

up by plants. Appendix C tabulates the results 

for environmental contaminants across all 

commodities. Environmental contaminants are 

consolidated into a single appendix because they 

have no registered uses and are not applied to 

crops in the United States. These compounds are 

subject to FDA Action Levels (ALs) rather than 

tolerances. Because environmental contaminants 

continue to persist in the environment, they may 

be present in food commodities at generally low 

levels.

Most of the collected and analyzed samples (59.5 

percent) were produced in the United States, 34.9 

percent were imports, 4.9 percent were of mixed 

national origin, and 0.7 percent were of unknown 

origin. Appendix D shows the distribution of 

sample origin by State or country. Of all samples 

collected and analyzed, approximately 29.7 

percent (2,855 of 9,600) were grown, packed, and/

or distributed in or from California, which is the 

leading agricultural production and most populous 

State. Appendix E includes a comparison of 

residues for selected commodities with significant 

domestic and import components.

Food monitoring data, together with dietary 

consumption surveys, are used by EPA to estimate 

dietary exposure to pesticides to ensure the safety 

of existing pesticide uses. EPA uses all results 

reported by PDP, including sample results reported 

as below the LOD and those above the tolerance. 

PDP laboratories are required to establish LODs 

and report any instrumental response below 

the LOD as a non-detect. LODs are established 

experimentally for each pesticide/commodity pair 

and are reported with each data set. The number 

of non-detects can be used in conjunction with 

percent-crop-treated data to determine what 

proportion of these values may be counted as zero 

towards the dietary exposure. All individual sample 

data can be downloaded from the PDP website 

at http://www.ams.usda.gov/pdp or obtained by 

contacting MPD.

• Import Versus Domestic Residue Comparisons

Information about the origin of each PDP sample 

is recorded when the sample is collected. Figure 4 

illustrates the portion of the domestic and import 

component for each of the PDP fruit and vegetable 

commodities in 2020. The data generated by PDP 

reflect pesticide residues in foods, both domestic 

and imported products, available to the U.S. 

consumer. Many fresh and processed commodities 

are almost entirely of domestic origin, such as 

collard greens (95.5 percent) and cauliflower (95.4 

percent) with only minor import (2.0 percent and 

4.0 percent, respectively) and unknown origins (2.5 

percent and 0.6 percent, respectively). Other fresh 

commodities, such as cantaloupe and tangerines, 

are available from domestic growers part of the 

year and imported during the remaining months, 

as illustrated in Figure 5.

Comparison of selected residues detected in 

imported versus domestic cantaloupe, tangerine, 

and winter squash can be found in Appendix E. 

These sample sets were selected to compare data 

where residues of the listed pesticides are present 

in greater than 5 percent of the total samples for 

the commodity. The comparison of individual 

pesticides between the countries of origin show 

that the residue profiles for domestic and imported 

crops are significantly different, as would be 

expected due to different pest pressures.

The cantaloupe data in Appendix E show that 

acetamiprid, fluopyram, metalaxyl/mefenoxam, 

propamocarb hydrochloride, and thiabendazole 

were detected more frequently in imported samples 

than in domestic samples. For example, acetamiprid 

was detected in 40.8 percent of the Guatemalan 

samples and 8.3 percent of the domestic samples, 

while fluopyram was detected in 21.1 percent of 

the samples from Guatemala and 1.8 percent of 

the U.S. samples. Bifenthrin and imidacloprid 
Pesticide Data Program—Annual Summary, Calendar Year 2020

20

were detected more frequently in domestic 

samples than in imports. Bifenthrin was detected 

in 10.8 percent of U.S. samples and 0 percent of 

Guatemalan samples, while imidacloprid was 

detected in 24.0 percent of U.S. samples and 12.7 

percent of samples from Guatemala. Dinotefuran, 

oxamyl oxime, and thiamethoxam were detected 

with relatively equal frequency in both the U.S. 

and Guatemalan cantaloupe. 

The data for tangerines in Appendix E 

illustrates that acetamiprid, fludioxonil, and 

pyrimethanil were detected more frequently in 

imported samples than in domestic samples and 

azoxystrobin was detected more frequently in 

domestic samples. Compounds like imazalil and 

thiabendazole were detected with relatively equal 

frequency. Acetamiprid was detected in 30.3 

percent of the samples from Chile, 29.5 percent of 

the Peruvian samples, and 1.5 percent of the U.S. 

samples. Fludioxonil was detected in 47.4 percent 

of the samples from Chile, 3.1 percent of Peruvian 

samples, and 31.5 percent of the U.S. samples. 

Pyrimethanil was detected in 27.0 percent of 

the Chilean samples, 6.2 percent of the Peruvian 

samples, and 6.7 percent of the U.S. samples. 

Azoxystrobin was detected in 33.6 percent of the 

U.S. samples, 7.2 percent of the Chilean samples, 

and was not detected in any of the samples from 

Peru. Imazalil was detected in more than 90 

percent of the samples from the United States, 

Chile, and Peru while thiabendazole was detected 

at 82.4 percent of the samples from the United 

States, 71.7 percent of the Chilean samples, and 

83.7 percent of the Peruvian samples.

The winter squash data in Appendix E shows that 

compounds like imidacloprid and propamocarb 

were detected more frequently in imported 

samples than in domestic samples. Imidacloprid 

was detected in 55.5 percent of the samples from 

Mexico and 17.9 percent of the U.S. samples, 

while propamocarb was detected in 14.7 percent 

of the Mexican samples and 3.6 percent of the 

domestic samples. Bifenthrin and cyflufenamid 

were detected more frequently in domestic 

samples than in imports. Bifenthrin was detected 

in 24.8 percent of U.S. samples and 18.1 percent 

of Mexican samples, while cyflufenamid was 

detected in 21.5 percent of U.S. samples and was 

not detected in any of the samples from Mexico. 

Metalaxyl/mefenoxam and thiamethoxam were 

detected with relatively equal frequency in both 

the U.S. and Mexican winter squash.

All pesticides detected in this comparison 

of domestic and imported commodities had 

tolerances for the given commodity in the United 

States as shown in Appendix E; however, the 

profiles of residue findings were markedly 

different in U.S. samples versus imported samples. 

The differences in residue detections between 

countries were likely due to the pesticides used 

in response to pest pressures based on differing 

environmental and climatic conditions as well as 

crop production and protection practices.

• Postharvest Applications

Pesticides can be applied before and after harvest 

depending on the crop and approved label use. 

PDP data capture both preharvest and postharvest 

uses because samples are collected at points 

when all pesticide applications have already 

occurred. Pesticides applied postharvest are 

used primarily as fungicides (e.g., azoxystrobin, 

imazalil, o-phenylphenol, and thiabendazole) 

and growth regulators/sprouting inhibitors 

(e.g., chlorpropham). Some detections reported 

in Appendix B most likely reflect postharvest 

applications to the raw agricultural commodity.

• Discussion of Results

There are many pesticides registered for use 

on the same crop; however, not all registered 

pesticides are used at the same time or location. 

In 2020, 30.0 percent of the samples tested had no 

detectable pesticide residue, and over 99 percent 

of the samples tested had residues below the 

tolerances established by the EPA. Pesticide use 

is primarily dictated by local pest pressures and 

environmental conditions conducive to growth 

of pest populations, as well as the planting of 

susceptible varieties.

These differences are captured by PDP data, 

which reflect actual residues present in food 
Pesticide Data Program—Annual Summary, Calendar Year 2020

21

grown in various regions of the United States and 

foreign countries. Thus, in evaluating consumer 

exposure to pesticides through the diet, EPA uses 

all available information provided by registrants, 

PDP, and others to verify that tolerances meet the 

safety standards set by FQPA. The presence of 

residues at levels below the established tolerance 

serves to ensure and verify the safety of the 

Nation’s food supply.

Food commodities with pesticides detected in 

at least 5 percent of samples tested are shown in 

Appendix F. The data shown include the range 

and mean of values detected and EPA tolerance 

references for each commodity/pesticide pair.

By virtue of the MRMs employed, PDP provides 

critical data that can be used by EPA to evaluate 

exposure to multiple residues from the same 

commodity. The data are crucial for assessments 

that consider cumulative exposure to pesticides 

determined to have common mechanisms of 

toxicity. The distribution of multiple pesticides 

occurring in samples tested during 2020 is 

presented in Appendix G. These data indicate 

that 30.0 percent of all samples tested contained 

no detectable pesticides, 22.3 percent contained 

1 pesticide, and 47.7 percent contained more 

than 1 pesticide. Parent compounds and their 

metabolites are combined to report the number of 

“pesticides” rather than the number of “residues.” 

Environmental contaminants, listed in Appendix C, 

have been excluded from this count of pesticides.

One sample of sweet bell peppers contained 

residues of 18 pesticides. No residues found on the 

sweet bell pepper sample exceeded the established 

tolerances. Multiple residue detections can result 

from the application of more than one pesticide 

on a crop during a growing season; in addition, 

several other factors can contribute to multiple 

detections. For example, unintentional spray drift 

in the field, planting of crops in fields previously 

treated with the pesticide, and/or transfer of 

residues of postharvest fungicides or growth 

regulators applied to other commodities stored in 

the same storage facilities could all contribute to 

residue detections.

In most cases, samples analyzed by PDP are 

composites of 3 to 5 pounds of commodity 

from the same lot. Therefore, the estimated 

concentrations for multiple residue detections in 

these composite sample results may or may not 

reflect the number or levels of pesticides in a 

single-serving item of a commodity.

• Environmental Contaminants

Environmental contaminants include pesticides 

whose uses have been canceled in the United 

States, but their residues persist in the 

environment, particularly in soil, where they may 

be taken up by plants. These data are also used 

to facilitate international trade. Residue results 

for environmental contaminants may be found in 

Appendix C.

DDT, DDD, and DDE: PDP screened samples 

for various metabolites of DDT including DDT 

o,p’; DDT p,p’; DDD o,p’; DDD p,p’; DDE o,p’; 

and DDE p,p’. Use of DDT has been prohibited 

in the United States since 1972; however, due 

to its persistence in the environment, lowlevel residues of DDT and its DDD and DDE 

metabolites were detected in some commodities 

tested. DDD o,p’ was detected in collard greens 

(0.2 percent) and winter squash (0.1 percent). 

DDE p,p’ was detected in broccoli (3.9 percent), 

carrots (4.6 percent), collard greens (1 percent), 

green beans (1.7 percent), radishes (3.5 percent), 

summer squash (3.4 percent), and winter squash 

(2.8 percent). DDT o,p’ was detected in summer 

squash (2.2 percent) and winter squash (0.7 

percent). DDT p,p’ was detected in radishes 

(0.1 percent), summer squash (1.1 percent), and 

winter squash (1 percent). No residues of DDD 

p,p’, or DDE o,p’ were detected in any samples. 

All residues detected were lower than established 

FDA ALs.

Other Contaminants: PDP screened samples for 

other environmental contaminants including: 

aldrin, which readily metabolizes to dieldrin; 

BHC (alpha/beta/delta/epsilon); chlordane (cis, 

trans) and its metabolite oxychlordane; dieldrin; 

endrin; heptachlor and its epoxide metabolite; 

hexachlorobenzene (HCB); lindane (BHC 
Pesticide Data Program—Annual Summary, Calendar Year 2020

22

gamma); and mirex. HCB was used as a seed 

protectant until 1965 and, due to its persistence, 

remains in soil and grasses. In 1974, all aldrin 

and dieldrin uses were canceled in the United 

States and, in 1978, all heptachlor and mirex uses 

were canceled. In 1986, chlordane uses, except 

termiticide uses, were canceled. Despite these 

cancellations and because they persist in the 

environment, trace residues of chlordane (cis and 

trans), dieldrin, endrin, heptachlor (parent and 

epoxide), and oxychlordane were detected in some 

of the tested commodities.

Chlordane (cis) was detected in 3.4 percent of 

summer squash samples and 0.7 percent of winter 

squash samples, while chlordane (trans) was 

detected in 0.1 percent of apple juice samples, 1.1 

percent of summer squash samples, and 0.7 percent 

of winter squash samples. Dieldrin was detected 

in 0.9 percent of cantaloupe samples, 0.4 percent 

of carrot samples, 0.2 percent of collard green 

samples, 0.1 percent of radish samples, 18 percent 

of summer squash samples, and 9.3 percent of 

winter squash samples. Endrin was detected in 3.4 

percent of summer squash samples and 0.4 percent 

of winter squash samples. Heptachlor (parent) was 

detected in 0.2 percent of collard green samples. 

Heptachlor epoxide was detected in 1 percent of 

winter squash samples. Mirex was detected in 0.4 

percent of cantaloupe samples. Oxychlordane was 

detected in 0.1 percent of winter squash samples. 

No residues of Aldrin, BHC (alpha/beta/delta/

epsilon), HCB, or lindane (BHC gamma) were 

detected in any samples.

• Tolerance Violations

A tolerance is defined under Section 408 of the 

Federal Food, Drug, and Cosmetic Act as the 

maximum quantity of a pesticide residue allowable 

on a raw agricultural commodity. Tolerances are 

also applicable to processed foods. The FQPA of 

1996 amended the Federal Insecticide, Fungicide 

and Rodenticide Act to require EPA to periodically 

review each pesticide registration using the most 

currently available data. Timely pesticide data 

provided by PDP enable the EPA to refine risk 

estimates used in the pesticide registration review 

process.

A tolerance violation occurs when a residue is 

found that exceeds the tolerance level or when 

a certain residue is found for which there is no 

established tolerance. Apart from meat, poultry, 

and egg products, for which USDA’s Food 

Safety and Inspection Service is responsible, 

FDA enforces tolerances for all imported foods 

and domestic foods that move through interstate 

commerce. Unlike enforcement programs, PDP 

emphasizes determination of residues at low 

levels of detection levels rather than quick turnaround times. When PDP identifies samples with 

residues exceeding the tolerance or with residues 

for which there is no established tolerance, these 

detections are reported to FDA’s headquarters 

office. This notification is made in accordance with 

a Memorandum of Understanding between USDA 

and FDA for the purpose of identifying areas where 

closer surveillance may be needed. FDA assesses 

PDP apparent violation data for appropriateness for 

follow up under its regulatory pesticide program. 

Due to the time period required for completion 

of PDP analyses and data reporting, FDA follow 

up will usually be at a subsequent harvest or 

commodity availability period.

Residues exceeding the established tolerance or 

ALs are noted with an “X” in Appendix B. Similarly, 

residues for which a tolerance is not established 

are noted with a “V” in Appendixes B and C. The 

“X” and “V” annotations are followed by a number 

indicating the number of samples reported to FDA. 

The EPA tolerances cited in this summary and 

appendixes apply to 2020 and not to the current 

year. There may be instances where tolerances may 

have been recently changed that would influence 

whether a residue is violative.

An established tolerance may apply to more than 

one residue because pesticides may break down 

into more than one metabolite or contain more 

than one isomer. If a pesticide also has a metabolite 

of interest, PDP assigns the metabolite the same 

tolerance as the parent compound. However, 

if the metabolite has a higher tolerance in the 

CFR, the higher of the two values is used for the 

metabolite. If a pesticide has multiple isomers the 

tolerance is the sum of parent and isomer(s) of 

interest. For example, the tolerance for endosulfan 
Pesticide Data Program—Annual Summary, Calendar Year 2020

23

combines residues of endosulfan I, endosulfan 

II, and endosulfan sulfate; and organophosphate 

tolerances may combine the parent compound and 

the sulfone and sulfoxide metabolites. Therefore, 

where applicable, the pesticide violations in 

Appendix H are combined residues of parent and 

any isomers and/or metabolites to count the total 

number of samples with tolerance violations.

A total of 341 samples with 378 pesticides was 

reported to FDA as Presumptive Tolerance 

Violations. Pesticides exceeding the tolerance 

were detected in 0.49 percent (47 samples) of the 

total samples tested (9,600 samples). Of these 

47 samples, 35 were domestic (74.5 percent), 

11 were imported (23.4 percent), and 1 was of 

unknown origin (2.1 percent), representing 0.6 

percent of the total domestic samples, 0.3 percent 

of the total imported samples, and 1.5 percent of 

the total unknown origin samples, respectively. 

The samples containing pesticides that exceeded 

established tolerances included: 1 sample of 

blueberries, 5 samples of carrots, 2 samples of 

eggplant, 10 samples of green beans, 16 samples 

of collard greens, 6 samples of sweet bell peppers, 

4 samples of radishes, 2 samples of tangerines, and 

1 sample of winter squash. Commodities that did 

not have any samples exceeding the established 

tolerances were the following: apple juice, 

bananas, broccoli, cantaloupe, cauliflower, kiwi, 

orange juice, summer squash, and tomato paste.

Residues with no established tolerance were found 

in 3.2 percent (303 samples) of the total samples 

tested (9,600 samples). Of these 303 samples, 199 

were domestic (65.7 percent), 100 were imported 

(33.0 percent), and 4 samples were of unknown 

origin (1.3 percent), representing 3.5 percent 

of the total domestic samples, 3.0 percent of the 

total imported samples, and 6.0 percent of the 

total unknown origin samples, respectively. These 

samples included 295 fresh fruit and vegetable 

samples and 8 processed fruit/vegetable samples. 

The 8 processed fruit/vegetable samples were 

orange juice and tomato paste. There were 283 

samples that contained 1 pesticide for which 

no tolerance was established; 16 samples with 2 

pesticides for which no tolerance was established; 

3 samples with 3 pesticides for which no tolerance 

was established; and 1 sample with 4 pesticides for 

which no tolerance was established. Nine of the 

303 samples also contained 1 or more pesticides 

that exceeded an established tolerance. The 

pesticide residue levels and commodities are listed 

in Appendix H. In most cases, these pesticides 

with no established tolerance were detected at 

low levels. Some pesticide residues may have 

resulted from unintentional spray drift in the field; 

planting of crops in fields previously treated with 

the pesticide; transfer of pesticide residues, postharvest fungicides, or other growth regulators 

applied to other commodities kept in the same 

storage facilities; or exposure to pesticides during 

transportation through the distribution chain. 

Commodities that did not have any samples with 

pesticides for which no tolerance was established 

were apple juice and bananas.

• Look Ahead

At the time this report was drafted, 2021 PDP 

sampling and testing was underway. Commodities 

included in the 2021 survey are: blueberries, 

broccoli, butter, cantaloupe, carrots, cauliflower, 

celery, corn grain, eggplant, grape juice, green 

beans, peaches, pears, plums, summer squash, 

sweet bell peppers, tangerines (mandarins), 

watermelon, and winter squash. It is anticipated 

that the 2021 PDP data will be published in an 

annual summary approximately 1 year after the 

date of this report.

♦♦♦♦♦♦
Appendix A

Commodity History

Appendix A identifies commodities sampled by the Pesticide Data Program (PDP) through 

December 2021. Updates to this list are posted on the PDP Web site at

www.ams.usda.gov/pdp.
Fresh Commodities

Commodity Start Date End Date

Apples 1 Sep-91 Dec-96

Apples (S-1) Jan-99 Dec-99

Apples (S-2) Jan-99 May-99

Apples Oct-00 Sep-02

Apples (T-1) Jan-03 Dec-03

Apples Jan-04 Dec-05

Apples Jan-09 Dec-10

Apples (B-1) Aug-12 Oct-12

Apples Oct-14 Sep-16

Asparagus Jan-02 Jun-03

Asparagus Jul-08 Jun-10

Asparagus Jul-17 Jun-19

Avocados Jul-12 Dec-12

Bananas Sep-91 Sep-95

Bananas Jan-01 Dec-02

Bananas (TSP) Jul-03 Dec-03

Bananas Jan-06 Dec-07

Bananas Apr-12 Mar-14

Bananas Jan-19 Dec-20

Basil Apr-19 Sep-19

Blueberries (cultivated) 2 Jan-07 Dec-08

Blueberries (cultivated) 2 Jan-14 Dec-14

Blueberries (cultivated) 2 Oct-20 Ongoing

Broccoli Oct-92 Dec-94

Broccoli Jan-01 Dec-02

Broccoli Oct-06 Sep-08

Broccoli Jan-13 Dec-14

Broccoli Jan-20 Dec-21

Cabbage Jan-10 Dec-11

Cabbage Jul-17 Jun-19

Cantaloupe Jul-98 Jun-00

Cantaloupe Oct-03 Sep-05

Cantaloupe Jan-10 Mar-10

Cantaloupe Oct-10 Jun-12

Cantaloupe Jul-19 Jun-21

Carrots 1 Oct-92 Sep-96

Carrots Oct-00 Sep-02

Carrots Jan-06 Dec-07

Carrots Jan-13 Dec-14

Carrots Apr-20 Ongoing

Cauliflower Oct-04 Sep-06

Cauliflower Oct-11 Sep-13

APPENDIX A. COMMODITY HISTORY

AS OF DECEMBER 2021

Appendix A. Page 1 of 10
Commodity Start Date End Date

Cauliflower Oct-19 Sep-21

Celery Feb-92 Mar-94

Celery Jan-01 Dec-02

Celery Jan-07 Dec-08

Celery Jan-13 Dec-14

Celery Jul-21 Ongoing

Cherries 3 May-00 Aug-01

Cherries 2 May-07 Sep-07

Cherries Apr-14 Mar-16

Cilantro Oct-09 Sep-10

Cilantro Oct-18 Mar-19

Collard Greens Oct-19 Sep-20

Cranberries Oct-06 Dec-06

Cranberries 2 Oct-16 Mar-18

Cucumbers Jan-99 Dec-00

Cucumbers Oct-02 Sep-04

Cucumbers Jan-09 Dec-10

Cucumbers Jul-15 Jun-17

Eggplant Jan-05 Dec-06

Eggplant Jan-20 Dec-21

Grapefruit Aug-91 Dec-93

Grapefruit Jan-05 Dec-06

Grapefruit Oct-15 Sep-17

Grapes 1 May-91 Dec-96

Grapes Jan-00 Dec-01

Grapes (TSP) Jul-03 Dec-03

Grapes Jan-04 Dec-05

Grapes Jan-09 Dec-10

Grapes Jan-15 Dec-16

Green Beans Feb-92 Dec-95

Green Beans Jan-00 Dec-01

Green Beans Apr-04 Mar-05

Green Beans Jan-07 Dec-08

Green Beans Jul-13 Sep-16

Green Beans Oct-20 Ongoing

Green Onions Oct-08 Sep-09

Green Onions Jan-18 Dec-18

Greens (collard & kale) Oct-06 Sep-08

Hot Peppers Oct-10 Sep-11

Hot Peppers Jan-19 Dec-19

Kale Jan-17 Dec-18

Kiwi Fruit Apr-18 Mar-20

Lettuce May-91 Dec-94

Lettuce Oct-99 Sep-01

Lettuce Jan-04 Dec-05

Lettuce Jan-10 Dec-11

Lettuce Jul-15 Jun-17

Appendix A. Page 2 of 10
Commodity Start Date End Date

Lettuce, Organic Jan-09 Dec-09

Mangoes Apr-10 Sep-10

Mangoes Oct-17 Sep-18

Mushrooms Oct-01 Sep-03

Mushrooms Oct-11 Sep-13

Mustard Greens Jan-19 Dec-19

Nectarines 

4 Jul-00 Sep-01

Nectarines Jan-07 Dec-08

Nectarines Jan-13 Dec-15

Onions Jan-02 Dec-03

Onions Oct-11 Sep-12

Onions Jan-17 Dec-17

Oranges 

1 Aug-91 Dec-96

Oranges Jan-00 Dec-01

Oranges Jan-04 Dec-05

Oranges Jan-09 Dec-10

Oranges Jan-15 Dec-16

Papaya Jul-11 Jun-12

Peaches Feb-92 Sep-96

Peaches (S-3) Jan-00 Sep-00

Peaches 

5 Jan-01 Sep-02

Peaches (T-1) May-03 Sep-03

Peaches Oct-06 Sep-08

Peaches (B-1) Aug-12 Oct-12

Peaches Jul-13 Jun-15

Peaches Jan-21 Ongoing

Pears Jan-97 Jun-99

Pears (S-1) Jul-98 Jun-99

Pears Oct-03 Sep-05

Pears Jan-09 Dec-10

Pears (B-1) Oct-12 Nov-12

Pears Jan-15 Dec-16

Pears Jan-21 Ongoing

Pineapples Jul-00 Jun-02

Plums 

6 Jan-05 Dec-06

Plums Oct-11 Sep-13

Plums Jul-21 Ongoing

Potatoes May-91 Dec-95

Potatoes (S-4) Dec-96 Dec-97

Potatoes Jul-00 Jun-02

Potatoes Jan-08 Dec-09

Potatoes Jan-15 Dec-16

Radishes Jan-19 Dec-20

Raspberries 

2 Jan-13 Dec-13

Snap Peas Jan-11 Dec-12

Snap Peas Jan-17 Dec-18

Spinach 

1 Jan-95 Sep-97

Appendix A. Page 3 of 10
Commodity Start Date End Date

Spinach Jul-02 Dec-03

Spinach 7 Jan-06 Sep-06

Spinach Jan-08 Dec-09

Spinach Jan-15 Dec-16

Strawberries 2 Jan-98 Sep-00

Strawberries Jan-04 Dec-05

Strawberries Jan-08 Dec-09

Strawberries Oct-14 Sep-16

Summer Squash Oct-06 Sep-08

Summer Squash Oct-12 Sep-14

Summer Squash Oct-20 Ongoing

Sweet Corn (on-the-cob) Oct-08 Sep-10

Sweet Corn (on-the-cob) Oct-14 Sep-15

Sweet Bell Peppers Jan-99 Dec-00

Sweet Bell Peppers Oct-02 Sep-04

Sweet Bell Peppers Jan-10 Mar-12

Sweet Bell Peppers Jul-19 Jun-21

Sweet Potatoes 1 Jan-96 Jun-98

Sweet Potatoes Jan-03 Dec-04

Sweet Potatoes Oct-08 Sep-10

Sweet Potatoes Apr-16 Mar-18

Tangerines Jan-11 Dec-12

Tangerines Oct-19 Sep-21

Tomatoes 1 Jul-96 Jun-99

Tomatoes Jan-03 Dec-04

Tomatoes Jan-07 Dec-08

Tomatoes Oct-14 Sep-16

Tomatoes, Cherry/Grape Jan-11 Dec-12

Watermelon 8 Oct-05 Sep-06

Watermelon Apr-10 Sep-10

Watermelon Jul-14 Jun-15

Watermelon Oct-21 Ongoing

Winter Squash 2 Jan-97 Jun-99

Winter Squash Jul-04 Jun-06

Winter Squash Oct-11 Mar-13

Winter Squash Jan-20 Dec-21

NOTES

1

 Excludes sampling hiatus September - November 1996.

2

 Frozen collected when fresh unavailable.

3

 Sampling adjusted for market availability. Cherries were sampled for 2 years 

 (May-00 - Aug-01) for a total of 6 months.

4

 Sampling adjusted for market availability. Nectarines were sampled for 2 years 

 (Jul-00 - Sep-01) for a total of 6 months.

5

 Sampling adjusted for market availability. Peaches were sampled for 2 years

 (Jan-01 - Sep-02) for a total of 16 months.

6

 Dried plums (prunes) were collected when fresh plums were not available.

Appendix A. Page 4 of 10
Commodity Start Date End Date

7

 Spinach ended earlier than planned due to the unavailability of product.

8

 Samples collected in California, Florida, and Texas only.

(B-1) Special project testing for bifenthrin in multi-residue screen.

(S-1) Special single serving project testing for organophosphates.

(S-2) Special single serving project testing for carbamates.

(S-3) Special single serving project testing for carbamate, organochlorine, 

 organophosphate, organonitrogen, and sulfur compounds.

(S-4) Special single serving project testing for aldicarb.

(T-1) Triazole parent and metabolite compounds only.

(TSP) Triazole Sampling Project. Samples sent to contract laboratory.

Appendix A. Page 5 of 10
Processed Commodities

Commodity Start Date End Date

Apple Juice 

1 Jul-96 Dec-98

Apple Juice Jan-02 Dec-02

Apple Juice Jul-07 Jun-08

Apple Juice Jul-12 Jun-13

Apple Juice Jan-20 Dec-20

Applesauce Jul-02 Dec-02

Applesauce Jan-06 Dec-06

Applesauce Oct-16 Sep-17

Asparagus, Canned Jul-03 Dec-03

Beans, Canned (4 varieties) 

2 Oct-08 Sep-10

Beets, Canned Jan-11 Dec-11

Blueberries (cultivated), Frozen 

3 Jan-07 Dec-08

Blueberries (cultivated/wild), Frozen 

3 Jan-14 Dec-14

Blueberries (cultivated), Frozen 

3 Oct-20 Ongoing

Cherries, Frozen 

4 Apr-14 Mar-16

Corn Syrup 

4 Jan-98 Jun-99

Cranberries, Canned Apr-18 Sep-18

Cranberries, Frozen 

3 Oct-16 Mar-18

Garbanzo Beans, Canned Oct-17 Sep-18

Garbanzo Beans, Dried Jan-19 Dec-19

Grape Juice Jan-98 Dec-99

Grape Juice Jan-08 Dec-08

Grape Juice Oct-13 Sep-14

Grape Juice Jan-21 Dec-21

Green Beans, Canned/Frozen 

1 Jan-96 Jun-98

Green Beans, Canned Jan-03 Mar-04

Green Beans, Frozen Apr-05 Dec-05

Green Beans, Canned/Frozen Jan-14 Dec-14

Olives, Canned Oct-16 Sep-18

Orange Juice Jan-97 Dec-98

Orange Juice Oct-04 Sep-06

Orange Juice Oct-10 Sep-11

Orange Juice Jan-12 Jun-12

Orange Juice Oct-19 Sep-20

Peaches, Canned Dec-96 Dec-97

Peaches, Canned Jan-03 Dec-04

Peaches, Canned Jan-18 Dec-18

Peaches, Canned (T-1) Jan-03 Mar-03

Peaches, Canned (T-1) Oct-03 Dec-03

Pear Juice, Concentrate/Puree Jul-02 Jun-03

Pears, Canned Jul-99 Jun-00

Peas, Canned/Frozen Apr-94 Jun-96

Peas, Canned/Frozen 

5 Oct-01 Sep-03

Peas, Canned/Frozen Oct-18 Sep-19

Peas, Frozen Jan-06 Dec-06

Pineapple, Canned Jan-17 Dec-17

Appendix A. Page 6 of 10
Commodity Start Date End Date

Plums, Dried (Prunes) 6 Jan-05 Dec-06

Plums, Dried (Prunes) Oct-17 Sep-18

Potatoes, Frozen Jan-06 Dec-07

Raisins Jul-06 Jun-07

Raisins Jan-18 Dec-18

Raspberries, Frozen 3 Jan-13 Dec-13

Spinach, Canned Oct-97 Dec-98

Spinach, Canned Jan-04 Jun-04

Spinach, Canned/Frozen Jul-10 Jun-11

Spinach, Canned/Frozen Oct-18 Sep-19

Spinach, Frozen Jan-99 Dec-99

Strawberries, Frozen 3 Jan-98 Sep-00

Strawberries, Frozen Oct-18 Sep-19

Sweet Corn, Canned/Frozen Apr-94 Mar-96

Sweet Corn, Canned/Frozen 5 Oct-01 Sep-03

Sweet Corn, Frozen 3 Oct-08 Sep-10

Sweet Corn, Frozen 3 Oct-14 Sep-15

Tomato Paste, Canned Jan-01 Jun-01

Tomato Paste, Canned Jan-09 Dec-09

Tomato Paste, Canned Oct-19 Sep-20

Tomatoes, Canned Jul-99 Jun-00

Tomatoes, Canned Oct-16 Sep-17

Winter Squash, Frozen 3 Jan-97 Jun-99

Baby Food / Formula Products

Commodity Start Date End Date

Baby Food, Applesauce Jul-12 Jun-13

Baby Food, Carrots Jan-12 Dec-12

Baby Food, Green Beans Oct-10 Sep-11

Baby Food, Peaches Jan-12 Dec-12

Baby Food, Pears Oct-10 Sep-11

Baby Food, Peas Jul-12 Jun-13

Baby Food, Sweet Potatoes Oct-10 Sep-11

Infant Formula, Dairy-Based Oct-13 Sep-14

Infant Formula, Soy-Based Oct-13 Sep-14

NOTES

1 Excludes sampling hiatus September - November 1996.

2 Bean varieties included black, garbanzo, kidney, and pinto.

3 Frozen collected when fresh unavailable.

4 Excludes sampling hiatus January 1999.

5 Canned samples collected in first year and frozen samples in second year of testing.

6 Dried plums (prunes) were collected when fresh plums were not available.

(T-1) Triazole parent and metabolite compounds only.

Appendix A. Page 7 of 10
Grains

Commodity Start Date End Date

Barley Oct-01 Sep-03

Corn Oct-06 Sep-08

Corn Jul-21 Ongoing

Oats Jul-99 Apr-00

Oats Jan-10 Jun-10

Oats Apr-14 Aug-14

Oats Jan-19 Dec-19

Rice Oct-00 Sep-02

Rice1 Oct-08 Sep-09

Rice Apr-14 Aug-14

Rice Oct-18 Sep-19

Soybeans Sep-96 Feb-98

Soybeans Oct-03 Sep-05

Soybeans Sep-10 Apr-11

Soybeans (S-1) Oct-05 Dec-05

Wheat Feb-95 Jan-98

Wheat Sep-04 Jun-06

Wheat Jul-12 Sep-12

Wheat Flour Jan-03 Dec-04

Wheat Flour Jan-18 Dec-18

Wheat Flour (T-1) Jan-03 Dec-03

Nuts and Nut Products

Commodity Start Date End Date

Almonds Jul-07 Mar-08

Peanut Butter Jan-00 Dec-00

Peanut Butter (TSP) Jul-03 Dec-03

Peanut Butter Jan-06 Dec-06

Peanut Butter Apr-15 Aug-15

Dairy Products

Commodity Start Date End Date

Butter Jan-03 Dec-03

Butter Jan-12 Dec-13

Butter Oct-21 Ongoing

Heavy Cream Jul-05 Dec-05

Heavy Cream Jan-07 Dec-07

Heavy Cream Jun-18 Aug-18

Milk 2 Jan-96 Oct-98

Milk (TSP) Jul-03 Dec-03

Milk Jan-04 Dec-05

Milk Jan-11 Dec-11

Milk Jan-16 Dec-17

Appendix A. Page 8 of 10
Fish Products

Commodity Type Start Date End Date

Fish 3 Catfish Apr-08 Jun-10

Fish Salmon Jul-13 Jun-14

Meat / Poultry / Pork Products

Commodity Type Start Date End Date

Poultry Young Chickens Apr-00 Mar-01

Poultry Young & Mature Chickens Jan-06 Dec-06

Beef Cows, Heifers, Steers Jun-01 Jul-02

Beef 4 Cows, Heifers, Steers Dec-08 May-09

Pork Gilt, Barrow Jan-05 Jun-05

Other Products

Commodity Start Date End Date

Eggs (TSP) Jul-03 Dec-03

Eggs Jul-10 Jun-11

Eggs Apr-16 Aug-16

Honey Oct-07 Sep-08

Honey Apr-17 Aug-17

Drinking Water

States Start Date End Date

Finished Water Only (27 sites)

California, Colorado, Kansas, New York, Texas Mar-01 Dec-03

Raw Intake and Finished Water (70 sites) Jan-04 Apr-13

Alabama, Arizona, California, Florida, Georgia, Illinois, Indiana, Iowa, Kansas,

Kentucky, Louisiana, Maryland, Michigan, Minnesota, Missouri, Montana, New Jersey, 

New York, North Carolina, North Dakota, Ohio, Oregon, Pennsylvania, South Carolina, 

Tennessee, Texas, Virginia, Washington State, and Washington, D.C.

Bottled Water 

10 Participating States Jan-05 Dec-06

10 Participating States Jan-17 Dec-17

Groundwater 

1,495 Private Wells in 45 States plus Washington, DC Jan-07 Feb-13

16 Municipal Water Facilities in 13 States Mar-10 Feb-13

Appendix A. Page 9 of 10
NOTES

1

 Includes sampling hiatus May-July 2009.

2

 Excludes sampling hiatus September - November 1996.

3 Excludes sampling hiatus April-June 2009.

4

 Survey ended 7 months early due to budgetary constraints.

(S-1) Special survey for fungicides used to combat soybean rust.

(T-1) Triazole parent and metabolite compounds only.

(TSP) Triazole Sampling Project. Samples sent to contract laboratory.

Appendix A. Page 10 of 10
Appendix B

Distribution of Residues by Pesticide

in Fruit and Vegetables

Appendix B shows residue detections for all fruit and vegetable pesticide/commodity pairs 

tested, including range of values detected, range of Limits of Detection (LODs), and U.S. 

Environmental Protection Agency (EPA) tolerances for each pair. The EPA tolerances cited in 

this summary and appendixes apply to 2020 and not to the current year. There may be 

instances where tolerances have been recently set, modified, or revoked that would have an 

effect on whether a residue is violative or not.

In 2020, the Pesticide Data Program (PDP) analyzed 9,600 fruit and vegetable samples, of 

which 7,864 were fresh products and 1,736 were processed products.

PDP reports tolerance violations to FDA as part of an interagency Memorandum of 

Understanding between the U.S. Department of Agriculture and FDA. Residues reported to 

FDA are shown in the “Tolerance Violation” column and are annotated as “X” (if the residue 

exceeded the established tolerance) or “V” (if the residue did not have a tolerance listed in the 

Code of Federal Regulations, Title 40, Part 180). In both cases, these annotations are followed 

by a number indicating the number of samples reported to FDA.

Results for environmental contaminants across all commodities, including fruit and vegetables, 

have been consolidated in a separate appendix because they have no registered uses and are 

not applied to crops (see Appendix C). 
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

2,3,5-Trimethacarb (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

2,6-DIPN (plant growth regulator) 

Green Beans 177 0 0.005 - 0.010 NT

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 - 0.010 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 - 0.010 NT

TOTAL 1,732 0

Abamectin (insecticide)

Apple Juice 724 0 0.004 0.02

Bananas 703 0 0.004 0.01

Blueberries, Cultivated, Fresh 168 0 0.050 0.05

Blueberries, Frozen 7 0 0.050 0.05

Cantaloupe 694 0 0.050 0.01

Green Beans 177 0 0.020 0.08

Orange Juice 499 0 0.020 0.02

Summer Squash 89 0 0.020 0.01

Tomato Paste 290 0 0.020 0.07

Winter Squash 677 0 0.020 0.01

TOTAL 4,028 0

Acephate (insecticide)

Apple Juice 724 0 0.075 0.02

Bananas 703 0 0.075 0.02

Blueberries, Cultivated, Fresh 168 0 0.003 0.02

Blueberries, Frozen 7 0 0.003 0.02

Cantaloupe 693 0 0.003 0.02

Carrots 499 0 0.075 0.02

Cauliflower 664 5 0.8 0.015 - 0.069 0.005 2.0

Collard Greens 514 1 0.2 0.006 0.003 0.02

Eggplant 661 1 0.2 0.10 0.005 - 0.075 X-1 0.02

Green Beans 177 8 4.5 0.006 - 6.8 0.005 X-7 0.02

Kiwi Fruit 177 0 0.15 0.02

Orange Juice 499 0 0.005 0.02

Radishes 689 0 0.050 0.02

Summer Squash 176 0 0.005 - 0.015 0.02

Sweet Bell Peppers 675 24 3.6 0.051 - 0.86 0.050 4.0

Tangerines 687 0 0.060 0.02

Tomato Paste 506 0 0.005 - 0.060 0.02

Winter Squash 677 1 0.1 0.052 0.005 X-1 0.02

TOTAL 8,896 40

Acequinocyl (acaricide) 

Carrots 499 0 0.20 NT

TOTAL 499 0

APPENDIX B. DISTRIBUTION OF RESIDUES BY PESTICIDE IN FRUIT AND VEGETABLES

Appendix B. Page 1 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Acetamiprid (insecticide) 

Apple Juice 724 91 12.6 0.012 - 0.034 0.007 1.0

Bananas 703 0 0.007 0.5

Blueberries, Cultivated, Fresh 168 65 38.7 0.002 - 0.54 0.002 1.6

Blueberries, Frozen 7 0 0.002 1.6

Broccoli 628 4 0.6 0.002 - 0.007 0.001 - 0.006 1.2

Cantaloupe 694 94 13.5 0.002 - 0.026 0.002 0.50

Carrots 499 0 0.005 0.01

Cauliflower 692 1 0.1 0.007 0.003 1.2

Collard Greens 514 57 11.1 0.002 - 1.1 0.002 15

Eggplant 661 85 12.9 0.002 - 0.17 0.001 - 0.005 0.20

Green Beans 177 3 1.7 0.002 - 0.016 0.001 0.60

Kiwi Fruit 177 0 0.005 0.01

Orange Juice 499 0 0.001 1.0

Radishes 689 0 0.010 0.01

Summer Squash 176 15 8.5 0.002 - 0.015 0.001 - 0.002 0.50

Sweet Bell Peppers 675 52 7.7 0.011 - 0.28 0.010 X-1 0.20

Tangerines 687 90 13.1 0.002 - 0.064 0.002 1.0

Tomato Paste 506 19 3.8 0.001 - 0.009 0.001 - 0.002 0.40

Winter Squash 677 40 5.9 0.001 - 0.017 0.001 0.50

TOTAL 9,553 616

Acetochlor (herbicide) 

Blueberries, Cultivated, Fresh 168 0 0.005 NT

Blueberries, Frozen 7 0 0.005 NT

Broccoli 675 0 0.001 - 0.003 NT

Cantaloupe 694 0 0.005 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.001 NT

Collard Greens 514 0 0.005 NT

Eggplant 661 0 0.001 - 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.050 NT

Orange Juice 499 0 0.001 NT

Summer Squash 176 0 0.001 - 0.030 NT

Tangerines 687 0 0.050 NT

Tomato Paste 506 0 0.001 - 0.050 NT

Winter Squash 677 0 0.001 NT

TOTAL 6,809 0

Acibenzolar S methyl (fungicide) 

Apple Juice 724 0 0.025 0.05

Bananas 703 0 0.025 0.1

Blueberries, Cultivated, Fresh 168 0 0.020 0.15

Blueberries, Frozen 7 0 0.020 0.15

Broccoli 675 0 0.004 - 0.012 1.0

Cantaloupe 694 0 0.020 2.0

Carrots 499 0 0.040 NT

Cauliflower 692 0 0.004 1.0

Eggplant 661 0 0.004 - 0.040 1.0

Kiwi Fruit 177 0 0.080 NT

Radishes 689 0 0.010 NT

Summer Squash 87 0 0.030 2.0

Sweet Bell Peppers 675 0 0.010 1.0

Tangerines 687 0 0.030 0.02

Tomato Paste 216 0 0.030 3.0

TOTAL 7,354 0

Appendix B. Page 2 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Aclonifen (herbicide) 

Green Beans 177 0 0.001 - 0.003 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 - 0.003 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 - 0.003 NT

TOTAL 1,732 0

Afidopyropen (insecticide) 

Apple Juice 724 0 0.005 0.02

Broccoli 675 0 0.001 - 0.003 0.50

Cauliflower 692 0 0.001 0.50

Eggplant 350 0 0.001 0.2

Summer Squash 87 0 0.010 0.70

Tangerines 687 0 0.010 0.15

Tomato Paste 216 0 0.010 0.2

TOTAL 3,431 0

Alachlor (herbicide) 

Broccoli 675 0 0.002 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.002 NT

Eggplant 661 0 0.002 - 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Summer Squash 176 0 0.001 - 0.020 NT

Tangerines 687 0 0.020 NT

Tomato Paste 506 0 0.001 - 0.020 NT

Winter Squash 677 0 0.001 NT

TOTAL 5,426 0

Aldicarb (insecticide) 

Blueberries, Cultivated, Fresh 79 0 0.030 NT

Blueberries, Frozen 4 0 0.030 NT

Broccoli 675 0 0.001 - 0.003 NT

Cantaloupe 428 0 0.030 NT

Carrots 499 0 0.020 NT

Cauliflower 692 0 0.001 NT

Collard Greens 271 0 0.030 NT

Eggplant 661 0 0.001 - 0.020 NT

Green Beans 177 0 0.005 NT

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 0 0.005 0.3

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.002 - 0.005 NT

Sweet Bell Peppers 675 0 0.010 NT

Tangerines 687 0 0.002 NT

Tomato Paste 506 0 0.002 - 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 7,572 0

Aldicarb sulfone (metabolite of Aldicarb)

Blueberries, Cultivated, Fresh 168 0 0.005 NT

Blueberries, Frozen 7 0 0.005 NT

Cantaloupe 694 0 0.005 NT

Appendix B. Page 3 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Carrots 499 0 0.025 NT

Cauliflower 664 0 0.003 - 0.010 NT

Collard Greens 514 0 0.005 NT

Eggplant 661 0 0.003 - 0.025 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.025 NT

Orange Juice 499 0 0.003 0.3

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.003 - 0.010 NT

Sweet Bell Peppers 675 0 0.010 NT

Tangerines 687 0 0.020 NT

Tomato Paste 506 0 0.003 - 0.020 NT

Winter Squash 677 0 0.003 NT

TOTAL 7,470 0

Aldicarb sulfoxide (metabolite of Aldicarb)

Blueberries, Cultivated, Fresh 168 0 0.005 NT

Blueberries, Frozen 7 0 0.005 NT

Cantaloupe 694 0 0.005 NT

Carrots 499 0 0.055 NT

Collard Greens 514 0 0.005 NT

Eggplant 661 0 0.002 - 0.055 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.055 NT

Orange Juice 499 0 0.003 0.3

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.003 NT

Sweet Bell Peppers 656 0 0.010 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 5,797 0

Allethrin (insecticide) 

Carrots 499 0 0.080 NT

Eggplant 311 0 0.080 NT

Kiwi Fruit 177 0 0.080 NT

Radishes 689 0 0.010 NT

Sweet Bell Peppers 675 0 0.010 NT

TOTAL 2,351 0

Allidochlor (herbicide) 

Green Beans 177 0 0.005 NT

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 1,732 0

Ametoctradin (fungicide) 

Broccoli 675 12 1.8 0.004 - 0.51 0.003 9.0

Carrots 499 0 0.010 NT

Cauliflower 692 3 0.4 0.002 0.001 9.0

Eggplant 661 0 0.003 - 0.010 1.5

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Appendix B. Page 4 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Summer Squash 89 1 1.1 0.017 0.001 3.0

Sweet Bell Peppers 675 11 1.6 0.012 - 0.066 0.010 1.5

Tangerines 687 0 0.001 NT

Tomato Paste 506 0 0.001 1.5

Winter Squash 677 19 2.8 0.001 - 0.027 0.001 3.0

TOTAL 6,703 46

Ametryn (herbicide) 

Bananas 703 0 0.001 0.25

Carrots 499 0 0.005 NT

Eggplant 311 0 0.005 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.001 - 0.005 NT

Sweet Bell Peppers 675 0 0.010 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 NT

TOTAL 5,776 0

Amicarbazone (herbicide) 

Green Beans 177 0 0.005 NT

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 1,732 0

Aminocarb (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Anilofos (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Aspon (insecticide) 

Radishes 689 0 0.005 NT

Sweet Bell Peppers 675 0 0.005 NT

TOTAL 1,364 0

Asulam (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Appendix B. Page 5 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Atraton (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Atrazine (herbicide) 

Blueberries, Cultivated, Fresh 168 0 0.002 NT

Blueberries, Frozen 7 0 0.002 NT

Broccoli 675 3 0.4 0.002 - 0.003 0.001 V-3 NT

Cantaloupe 694 0 0.002 NT

Carrots 499 1 0.2 0.001 0.001 V-1 NT

Cauliflower 692 0 0.001 NT

Collard Greens 514 33 6.4 0.002 - 0.029 0.002 V-33 NT

Eggplant 661 0 0.001 NT

Green Beans 177 1 0.6 0.002 0.001 V-1 NT

Kiwi Fruit 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.001 - 0.010 NT

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 0 0.010 NT

Tomato Paste 506 0 0.001 - 0.010 NT

Winter Squash 677 0 0.001 NT

TOTAL 8,173 38

Aviglycine hydrochloride (plant growth regulator) 

Apple Juice 724 0 0.001 0.08

TOTAL 724 0

Azaconazole (fungicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Azamethiphos (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Azimsulfuron (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,442 0

Appendix B. Page 6 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Azinphos (insecticide) 

Green Beans 177 0 0.005 NT

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 1,732 0

Azinphos methyl (insecticide) 

Apple Juice 724 0 0.010 NT

Bananas 703 0 0.010 NT

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Broccoli 675 0 0.006 NT

Cantaloupe 694 0 0.010 NT

Carrots 499 0 0.005 NT

Cauliflower 692 0 0.006 NT

Collard Greens 514 0 0.010 NT

Eggplant 661 0 0.005 - 0.006 NT

Green Beans 177 0 0.005 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.005 NT

Radishes 668 0 0.020 NT

Summer Squash 176 0 0.005 - 0.010 NT

Sweet Bell Peppers 675 0 0.020 NT

Tangerines 687 0 0.050 NT

Tomato Paste 506 0 0.005 - 0.050 NT

Winter Squash 677 0 0.005 NT

TOTAL 9,579 0

Azinphos methyl oxygen analog (metabolite of Azinphos methyl)

Apple Juice 724 0 0.005 NT

Bananas 703 0 0.005 NT

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Cantaloupe 694 0 0.010 NT

Carrots 499 0 0.010 NT

Collard Greens 514 0 0.010 NT

Eggplant 311 0 0.010 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.003 NT

Sweet Bell Peppers 675 0 0.010 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 6,893 0

Azoxystrobin (fungicide) 

Bananas 703 368 52.3 0.003 - 0.020 0.002 0.1

Blueberries, Cultivated, Fresh 168 40 23.8 0.002 - 1.4 0.002 10.0

Blueberries, Frozen 7 1 14.3 0.026 0.002 10.0

Broccoli 675 99 14.7 0.002 - 1.3 0.001 3.0

Cantaloupe 666 9 1.4 0.002 - 0.004 0.002 0.3

Carrots 499 25 5 0.010 - 0.043 0.010 1.0

Cauliflower 692 2 0.3 0.002 - 0.038 0.001 3.0

Appendix B. Page 7 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Collard Greens 514 115 22.4 0.002 - 11 0.002 25

Eggplant 661 48 7.3 0.002 - 0.043 0.001 - 0.010 3.0

Green Beans 177 42 23.7 0.001 - 0.92 0.001 3.0

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 3 0.6 0.004 - 0.010 0.001 - 0.005 15.0

Radishes 689 75 10.9 0.002 - 0.19 0.002 1.0

Summer Squash 176 3 1.7 0.002 - 0.004 0.001 0.3

Sweet Bell Peppers 675 200 29.6 0.002 - 0.11 0.002 3.0

Tangerines 687 123 17.9 0.002 - 0.13 0.002 15.0

Tomato Paste 506 367 72.5 0.001 - 0.023 0.001 - 0.002 0.6

Winter Squash 677 27 4 0.001 - 0.034 0.001 0.3

TOTAL 8,848 1,547

Beflubutamid (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Benalaxyl (fungicide) 

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 0.20

Winter Squash 677 2 0.3 0.009 - 0.010 0.003 V-2 NT

TOTAL 1,732 2

Bendiocarb (insecticide) 

Bananas 703 0 0.005 NT

Blueberries, Cultivated, Fresh 168 0 0.003 NT

Blueberries, Frozen 7 0 0.003 NT

Broccoli 675 0 0.003 NT

Cantaloupe 694 0 0.003 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.001 NT

Collard Greens 514 0 0.003 NT

Eggplant 661 0 0.001 - 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.001 - 0.002 NT

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 NT

TOTAL 8,876 0

Benfluralin (herbicide) 

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Cantaloupe 694 0 0.010 NT

Collard Greens 514 0 0.010 NT

Green Beans 177 0 0.001 - 0.003 NT

Orange Juice 499 0 0.001 NT

Appendix B. Page 8 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Summer Squash 89 0 0.001 - 0.003 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 - 0.003 NT

TOTAL 3,115 0

Benoxacor (herbicide safener) 

Blueberries, Cultivated, Fresh 168 0 0.010 0.01

Blueberries, Frozen 7 0 0.010 0.01

Broccoli 675 0 0.001 0.01

Cantaloupe 694 0 0.010 0.01

Carrots 499 0 0.015 0.01

Cauliflower 692 0 0.001 0.01

Collard Greens 514 0 0.010 0.01

Eggplant 661 0 0.001 - 0.015 0.01

Green Beans 177 0 0.003 0.01

Kiwi Fruit 177 0 0.015 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.005 0.01

Summer Squash 176 0 0.003 - 0.020 0.01

Sweet Bell Peppers 675 0 0.005 0.01

Tangerines 687 0 0.020 NT

Tomato Paste 506 0 0.003 - 0.020 0.01

Winter Squash 677 0 0.003 0.01

TOTAL 8,173 0

Bensulfuron methyl (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Bensulide (herbicide) 

Blueberries, Cultivated, Fresh 168 0 0.004 NT

Blueberries, Frozen 7 0 0.004 NT

Cantaloupe 694 0 0.004 0.15

Carrots 499 0 0.005 0.10

Collard Greens 514 1 0.2 0.046 0.004 0.15

Eggplant 311 0 0.005 0.10

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.001 - 0.010 0.15

Sweet Bell Peppers 675 0 0.010 0.10

Tangerines 687 0 0.050 NT

Tomato Paste 506 0 0.001 - 0.050 0.10

Winter Squash 677 0 0.001 0.15

TOTAL 6,456 1

Bensulide oxygen analog (metabolite of Bensulide)

Blueberries, Cultivated, Fresh 168 0 0.002 NT

Blueberries, Frozen 7 0 0.002 NT

Cantaloupe 694 0 0.002 0.15

Carrots 499 0 0.010 0.10

Collard Greens 514 2 0.4 0.003 - 0.031 0.002 0.15

Appendix B. Page 9 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Eggplant 311 0 0.010 0.10

Kiwi Fruit 177 0 0.010 NT

Summer Squash 87 0 0.002 0.15

Tangerines 687 0 0.002 NT

Tomato Paste 216 0 0.002 0.10

TOTAL 3,360 2

Bentazon (herbicide) 

Carrots 499 0 0.030 NT

Eggplant 311 0 0.030 NT

Kiwi Fruit 177 0 0.030 NT

Summer Squash 87 0 0.050 NT

Tangerines 687 0 0.10 NT

Tomato Paste 216 0 0.10 NT

TOTAL 1,977 0

Benthiavalicarb isopropyl (fungicide) 

Carrots 499 0 0.010 NT

Eggplant 311 0 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 0.45

Winter Squash 677 0 0.001 NT

TOTAL 2,719 0

Benzobicyclon (herbicide) 

Green Beans 177 0 0.001 - 0.003 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 - 0.003 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 - 0.003 NT

TOTAL 1,732 0

Benzovindiflupyr (fungicide) 

Apple Juice 724 0 0.003 0.20

Carrots 499 0 0.020 NT

Eggplant 311 0 0.020 1.5

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 176 2 1.1 0.001 - 0.002 0.001 - 0.005 0.30

Tangerines 687 1 0.1 0.006 0.005 V-1 NT

Tomato Paste 506 2 0.4 0.002 0.001 - 0.005 1.5

Winter Squash 677 18 2.7 0.001 - 0.007 0.001 0.30

TOTAL 4,256 23

Bifenazate (acaricide) 

Apple Juice 724 0 0.010 0.7

Carrots 499 0 0.005 NT

Eggplant 311 0 0.005 4.0

Green Beans 177 0 0.003 6.0

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.003 0.75

Sweet Bell Peppers 675 9 1.3 0.010 - 0.11 0.010 4.0

Appendix B. Page 10 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomato Paste 290 0 0.003 4.0

Winter Squash 677 0 0.003 0.75

TOTAL 4,807 9

Bifenox (herbicide) 

Green Beans 177 0 0.001 - 0.003 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 - 0.003 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 - 0.003 NT

TOTAL 1,732 0

Bifenthrin (insecticide) 

Apple Juice 724 0 0.002 0.5

Bananas 703 0 0.002 0.1

Blueberries, Cultivated, Fresh 168 10 6 0.004 - 0.11 0.002 1.8

Blueberries, Frozen 7 4 57.1 0.033 - 0.085 0.002 1.8

Broccoli 675 22 3.3 0.002 - 0.16 0.001 0.6

Cantaloupe 662 53 8 0.002 - 0.006 0.002 0.4

Carrots 499 0 0.005 0.10

Cauliflower 692 0 0.001 0.6

Collard Greens 514 107 20.8 0.002 - 5.3 0.002 X-2 3.5

Eggplant 661 51 7.7 0.002 - 0.078 0.001 - 0.005 X-1 0.05

Green Beans 177 38 21.5 0.002 - 0.17 0.001 0.6

Kiwi Fruit 177 0 0.010 0.05

Orange Juice 499 0 0.001 0.05

Radishes 689 2 0.3 0.007 - 0.014 0.005 0.10

Summer Squash 176 19 10.8 0.001 - 0.11 0.001 - 0.005 0.4

Sweet Bell Peppers 675 50 7.4 0.005 - 0.11 0.005 0.5

Tangerines 687 0 0.005 0.05

Tomato Paste 505 264 52.3 0.001 - 0.040 0.001 - 0.005 0.15

Winter Squash 677 147 21.7 0.001 - 0.15 0.001 0.4

TOTAL 9,567 767

Bioallethrin (insecticide) 

Green Beans 127 0 0.010 NT

Orange Juice 499 0 0.010 NT

Summer Squash 34 0 0.010 NT

Tomato Paste 290 0 0.010 NT

Winter Squash 615 0 0.010 NT

TOTAL 1,565 0

Biphenyl (fungicide) 

Carrots 499 0 0.075 NT

Eggplant 311 0 0.075 NT

Kiwi Fruit 177 0 0.075 NT

TOTAL 987 0

Bitertanol (fungicide) 

Bananas 703 0 0.001 0.5

Green Beans 177 0 0.010 NT

Orange Juice 499 0 0.010 NT

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.010 NT

Sweet Bell Peppers 675 0 0.010 NT

Tomato Paste 290 0 0.010 NT

Winter Squash 677 0 0.010 NT

TOTAL 3,799 0

Appendix B. Page 11 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Boscalid (fungicide) 

Apple Juice 724 2 0.3 0.008 0.005 3.0

Bananas 703 1 0.1 0.008 0.005 0.40

Blueberries, Cultivated, Fresh 168 88 52.4 0.004 - 3.0 0.003 13.0

Blueberries, Frozen 7 4 57.1 0.037 - 0.25 0.003 13.0

Broccoli 675 72 10.7 0.002 - 0.78 0.001 6.0

Cantaloupe 694 0 0.003 3.0

Carrots 499 90 18 0.020 - 0.11 0.020 2.0

Cauliflower 692 2 0.3 0.002 - 0.005 0.001 6.0

Collard Greens 514 85 16.5 0.003 - 0.34 0.003 60

Eggplant 661 11 1.7 0.002 - 0.018 0.001 - 0.010 3.0

Green Beans 177 20 11.3 0.004 - 0.37 0.003 5.0

Kiwi Fruit 177 3 1.7 0.030 - 0.087 0.015 V-3 NT

Orange Juice 499 0 0.003 2.0

Radishes 689 2 0.3 0.011 - 0.017 0.010 2.0

Summer Squash 176 4 2.3 0.003 - 0.005 0.003 - 0.005 3.0

Sweet Bell Peppers 675 58 8.6 0.010 - 0.33 0.010 3.0

Tangerines 687 1 0.1 0.010 0.005 2.0

Tomato Paste 506 0 0.003 - 0.005 3.0

Winter Squash 677 26 3.8 0.003 - 0.030 0.003 3.0

TOTAL 9,600 469

Bromacil (herbicide) 

Blueberries, Cultivated, Fresh 168 0 0.003 NT

Blueberries, Frozen 7 0 0.003 NT

Cantaloupe 694 0 0.003 NT

Carrots 499 0 0.020 NT

Collard Greens 514 1 0.2 0.004 0.003 V-1 NT

Eggplant 311 0 0.020 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 0 0.003 0.1

Summer Squash 176 0 0.003 - 0.010 NT

Tangerines 687 0 0.010 0.1

Tomato Paste 496 0 0.003 - 0.010 NT

Winter Squash 677 0 0.003 NT

TOTAL 5,082 1

Bromobutide (herbicide) 

Green Beans 177 0 0.005 NT

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 1,732 0

Bromophos ethyl (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Bromopropylate (acaricide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Appendix B. Page 12 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 3,096 0

Bromuconazole (fungicide) 

Green Beans 177 0 0.001 - 0.003 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 - 0.003 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 - 0.003 NT

TOTAL 1,732 0

Bupirimate (fungicide) 

Carrots 499 0 0.005 NT

Eggplant 311 0 0.005 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,083 0

Buprofezin (insecticide) 

Apple Juice 724 0 0.001 3.0

Bananas 703 51 7.3 0.002 - 0.14 0.001 0.20

Blueberries, Cultivated, Fresh 168 7 4.2 0.001 - 0.003 0.001 2.5

Blueberries, Frozen 7 0 0.001 2.5

Broccoli 675 2 0.3 0.014 - 0.68 0.001 12

Cantaloupe 694 8 1.2 0.001 0.001 0.50

Carrots 499 0 0.001 NT

Cauliflower 692 0 0.001 12

Collard Greens 514 3 0.6 0.001 - 0.002 0.001 60

Eggplant 661 0 0.001 2.0

Green Beans 177 7 4 0.002 - 0.031 0.001 X-1 0.02

Kiwi Fruit 177 1 0.6 0.002 0.001 V-1 NT

Orange Juice 499 0 0.001 4

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.001 0.50

Sweet Bell Peppers 675 6 0.9 0.010 - 0.053 0.010 2.0

Tangerines 687 1 0.1 0.001 0.001 4

Tomato Paste 506 0 0.001 2.0

Winter Squash 677 6 0.9 0.002 - 0.009 0.001 0.50

TOTAL 9,600 92

Butachlor (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Appendix B. Page 13 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Butocarboxim (insecticide, acaricide)

Carrots 499 0 0.020 NT

Eggplant 311 0 0.020 NT

Kiwi Fruit 177 0 0.010 NT

Radishes 689 0 0.010 NT

Sweet Bell Peppers 675 0 0.010 NT

TOTAL 2,351 0

Butocarboxim sulfone (metabolite of Butocarboxim)

Carrots 499 0 0.015 NT

Eggplant 311 0 0.015 NT

Kiwi Fruit 177 0 0.015 NT

TOTAL 987 0

Butocarboxim sulfoxide (metabolite of Butocarboxim)

Carrots 499 0 0.010 NT

Eggplant 311 0 0.010 NT

Kiwi Fruit 177 0 0.010 NT

TOTAL 987 0

Butralin (herbicide) 

Green Beans 177 0 0.001 - 0.005 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 - 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 - 0.005 NT

TOTAL 1,732 0

Butylate (herbicide) 

Carrots 499 0 0.020 NT

Eggplant 311 0 0.020 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 2,719 0

Cadusafos (insecticide) 

Bananas 703 0 0.001 0.01

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 2,435 0

Captan (fungicide) (parent of THPI)

Cantaloupe 651 0 0.025 0.05

Carrots 499 0 0.10 0.05

Eggplant 311 0 0.10 0.05

Sweet Bell Peppers 635 0 0.020 0.05

TOTAL 2,096 0

Appendix B. Page 14 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Carbaryl (insecticide) 

Apple Juice 724 17 2.3 0.008 - 0.068 0.005 12

Bananas 703 0 0.005 5.0

Blueberries, Cultivated, Fresh 168 0 0.007 3.0

Blueberries, Frozen 7 0 0.007 3.0

Broccoli 675 4 0.6 0.005 - 0.030 0.003 10

Cantaloupe 694 3 0.4 0.006 - 0.031 0.003 3.0

Carrots 499 0 0.005 2.0

Cauliflower 692 0 0.001 - 0.006 10

Collard Greens 489 2 0.4 0.003 0.003 10

Eggplant 661 37 5.6 0.002 - 0.35 0.001 - 0.005 5.0

Green Beans 177 3 1.7 0.003 - 0.013 0.003 10

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 3 0.6 0.003 - 0.004 0.003 10

Radishes 689 0 0.010 2.0

Summer Squash 176 0 0.002 - 0.003 3.0

Sweet Bell Peppers 675 10 1.5 0.010 - 0.37 0.010 5.0

Tangerines 687 9 1.3 0.006 - 0.075 0.005 10

Tomato Paste 506 0 0.003 - 0.005 5.0

Winter Squash 677 1 0.1 0.003 0.003 3.0

TOTAL 9,575 89

Carbendazim - MBC (fungicide) (metabolite of Benomyl and Thiophanate Methyl)

Apple Juice 724 28 3.9 0.013 - 0.034 0.008 2.0

Bananas 703 0 0.008 2.0

Blueberries, Cultivated, Fresh 168 9 5.4 0.001 - 0.010 0.001 V-9 NT

Blueberries, Frozen 7 0 0.001 NT

Broccoli 675 2 0.3 0.020 - 0.15 0.003 V-2 NT

Cantaloupe 694 9 1.3 0.001 - 0.041 0.001 1.0

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.001 NT

Collard Greens 514 0 0.001 NT

Green Beans 177 41 23.2 0.002 - 0.24 0.001 2.0

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 1 0.2 0.002 0.001 V-1 NT

Radishes 689 1 0.1 0.085 0.010 V-1 NT

Summer Squash 176 2 1.1 0.003 - 0.004 0.001 - 0.010 1.0

Sweet Bell Peppers 675 1 0.1 0.012 0.010 V-1 NT

Tangerines 687 1 0.1 0.13 0.050 V-1 NT

Tomato Paste 506 0 0.001 - 0.050 NT

Winter Squash 677 16 2.4 0.001 - 0.027 0.001 1.0

TOTAL 8,939 111

Carbofuran (insecticide) (parent of 3-Hydroxycarbofuran)

Apple Juice 724 0 0.003 NT

Bananas 703 0 0.003 0.1

Blueberries, Cultivated, Fresh 168 0 0.002 NT

Blueberries, Frozen 7 0 0.002 NT

Broccoli 675 0 0.003 NT

Cantaloupe 694 0 0.002 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.003 NT

Collard Greens 514 0 0.002 NT

Eggplant 661 0 0.001 - 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Appendix B. Page 15 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.001 - 0.002 NT

Sweet Bell Peppers 675 0 0.010 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 NT

TOTAL 9,600 0

Carbophenothion (insecticide) 

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 1,732 0

Carboxin (fungicide) 

Carrots 499 0 0.005 NT

Eggplant 311 0 0.005 NT

Green Beans 177 0 0.003 - 0.005 0.2

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.003 - 0.025 NT

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 0 0.025 NT

Tomato Paste 506 0 0.003 - 0.025 NT

Winter Squash 677 0 0.003 NT

TOTAL 5,073 0

Carfentrazone (herbicide) 

Apple Juice 724 0 0.006 0.10

Bananas 703 0 0.006 0.10

Blueberries, Cultivated, Fresh 168 0 0.005 0.10

Blueberries, Frozen 7 0 0.005 0.10

Broccoli 675 0 0.005 - 0.030 0.10

Cantaloupe 694 0 0.005 0.10

Carrots 499 0 0.020 0.10

Cauliflower 669 0 0.005 - 0.030 0.10

Collard Greens 514 0 0.005 0.10

Eggplant 661 0 0.005 - 0.020 0.10

Green Beans 177 0 0.003 0.10

Kiwi Fruit 177 0 0.020 0.10

Orange Juice 499 0 0.003 0.10

Radishes 689 0 0.005 0.10

Summer Squash 176 0 0.003 - 0.005 0.10

Sweet Bell Peppers 675 0 0.005 0.10

Tangerines 687 0 0.005 0.10

Tomato Paste 506 0 0.003 - 0.005 0.10

Winter Squash 677 0 0.003 0.10

TOTAL 9,577 0

Carpropamid (fungicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Appendix B. Page 16 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Chlorantraniliprole (insecticide) 

Apple Juice 724 9 1.2 0.012 0.007 1.2

Bananas 703 0 0.007 4.0

Blueberries, Cultivated, Fresh 168 10 6 0.011 - 0.086 0.010 2.5

Blueberries, Frozen 7 1 14.3 0.043 0.010 2.5

Broccoli 675 19 2.8 0.006 - 0.10 0.005 4.0

Cantaloupe 694 0 0.010 0.5

Carrots 499 0 0.020 0.30

Cauliflower 692 1 0.1 0.011 0.002 4.0

Collard Greens 514 98 19.1 0.010 - 6.9 0.010 11

Eggplant 661 40 6.1 0.003 - 0.010 0.002 - 0.020 1.4

Green Beans 177 26 14.7 0.005 - 0.11 0.005 2.0

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.005 1.4

Radishes 689 14 2 0.020 - 0.077 0.020 0.30

Summer Squash 176 1 0.6 0.006 0.005 0.5

Sweet Bell Peppers 675 10 1.5 0.021 - 0.052 0.020 1.4

Tangerines 687 0 0.005 1.4

Tomato Paste 506 2 0.4 0.005 - 0.006 0.005 1.4

Winter Squash 677 3 0.4 0.006 - 0.007 0.005 0.5

TOTAL 9,600 234

Chlorbromuron (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Chlordimeform (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Chlorethoxyfos (insecticide) 

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 176 0 0.003 - 0.005 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.003 - 0.005 NT

Winter Squash 677 0 0.003 NT

TOTAL 2,722 0

Chlorfenapyr (insecticide) 

Apple Juice 724 0 0.018 0.01

Bananas 703 0 0.018 0.01

Blueberries, Cultivated, Fresh 168 0 0.015 0.01

Blueberries, Frozen 7 0 0.015 0.01

Broccoli 675 0 0.002 0.01

Appendix B. Page 17 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cantaloupe 694 0 0.015 0.01

Carrots 499 0 0.020 0.01

Cauliflower 692 0 0.002 0.01

Collard Greens 514 0 0.015 0.01

Eggplant 661 2 0.3 0.004 0.002 - 0.020 2

Green Beans 177 0 0.005 - 0.010 0.01

Kiwi Fruit 177 0 0.040 0.01

Orange Juice 499 0 0.005 0.01

Radishes 689 0 0.005 0.01

Summer Squash 176 0 0.005 - 0.025 0.01

Sweet Bell Peppers 675 65 9.6 0.005 - 0.32 0.005 2

Tangerines 687 0 0.025 0.01

Tomato Paste 506 0 0.005 - 0.025 2

Winter Squash 677 0 0.005 - 0.010 0.01

TOTAL 9,600 67

Chlorfenvinphos (insecticide) 

Broccoli 675 0 0.002 - 0.005 NT

Cauliflower 692 0 0.002 - 0.005 NT

Eggplant 350 0 0.002 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,813 0

Chlorfluazuron (insect growth regulator) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Chlorimuron ethyl (herbicide) 

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 176 0 0.003 - 0.005 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.003 - 0.005 NT

Winter Squash 677 0 0.003 NT

TOTAL 2,722 0

Chlorobenzilate (acaricide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Chloroneb (fungicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Appendix B. Page 18 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Chlorothalonil (fungicide) 

Blueberries, Cultivated, Fresh 168 0 0.020 1.0

Blueberries, Frozen 7 0 0.020 1.0

Cantaloupe 694 0 0.020 5.0

Collard Greens 514 10 1.9 0.025 - 7.7 0.020 V-10 NT

Green Beans 177 29 16.4 0.005 - 0.41 0.005 5

Summer Squash 89 8 9 0.005 - 0.029 0.005 5.0

Sweet Bell Peppers 675 64 9.5 0.005 - 0.20 0.005 6.0

Tomato Paste 290 0 0.005 - 0.010 5

Winter Squash 677 69 10.2 0.005 - 0.49 0.005 5.0

TOTAL 3,291 180

Chlorotoluron (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Chloroxuron (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Chlorpropham (herbicide, growth regulator)

Blueberries, Cultivated, Fresh 168 0 0.020 NT

Blueberries, Frozen 7 0 0.020 NT

Broccoli 675 26 3.9 0.002 - 0.016 0.001 V-26 NT

Cantaloupe 694 0 0.020 NT

Carrots 499 0 0.010 NT

Cauliflower 692 7 1 0.002 - 0.003 0.001 V-7 NT

Collard Greens 514 1 0.2 0.048 0.020 V-1 NT

Eggplant 661 5 0.8 0.002 - 0.020 0.001 - 0.010 V-5 NT

Green Beans 177 4 2.3 0.002 - 0.015 0.001 V-4 NT

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 0 0.001 NT

Radishes 689 1 0.1 0.008 0.005 V-1 NT

Summer Squash 176 0 0.001 - 0.005 NT

Sweet Bell Peppers 675 5 0.7 0.005 - 0.014 0.005 V-5 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 22 3.2 0.001 - 0.052 0.001 V-22 NT

TOTAL 8,173 71

Chlorpyrifos (insecticide) 

Apple Juice 724 0 0.010 0.1

Bananas 703 0 0.010 0.1

Blueberries, Cultivated, Fresh 168 1 0.6 0.005 0.005 0.1

Appendix B. Page 19 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Blueberries, Frozen 7 0 0.005 0.1

Broccoli 675 8 1.2 0.002 - 0.20 0.001 1.0

Cantaloupe 694 1 0.1 0.006 0.005 0.1

Carrots 499 0 0.010 0.1

Cauliflower 692 0 0.001 1.0

Collard Greens 514 2 0.4 0.009 - 0.021 0.005 1.0

Eggplant 661 0 0.001 - 0.010 0.1

Green Beans 177 4 2.3 0.003 - 0.045 0.003 0.1

Kiwi Fruit 177 0 0.010 2.0

Orange Juice 499 0 0.003 1.0

Radishes 689 58 8.4 0.005 - 0.10 0.005 2.0

Summer Squash 176 0 0.003 - 0.015 0.1

Sweet Bell Peppers 675 20 3 0.006 - 0.31 0.005 1.0

Tangerines 687 0 0.015 1.0

Tomato Paste 506 0 0.003 - 0.015 0.1

Winter Squash 677 2 0.3 0.006 - 0.011 0.003 0.1

TOTAL 9,600 96

Chlorpyrifos oxygen analog (metabolite of Chlorpyrifos)

Apple Juice 724 0 0.004 0.1

Bananas 703 0 0.004 0.1

Blueberries, Cultivated, Fresh 168 0 0.004 0.1

Blueberries, Frozen 7 0 0.004 0.1

Broccoli 624 0 0.001 - 0.003 1.0

Cantaloupe 694 0 0.002 0.1

Carrots 499 0 0.005 0.1

Cauliflower 648 0 0.001 - 0.006 1.0

Collard Greens 485 1 0.2 0.002 0.002 1.0

Eggplant 661 0 0.001 - 0.005 0.1

Green Beans 177 0 0.001 0.1

Kiwi Fruit 177 0 0.005 2.0

Orange Juice 499 0 0.001 1.0

Radishes 689 0 0.010 2.0

Summer Squash 176 0 0.001 - 0.005 0.1

Sweet Bell Peppers 675 0 0.010 1.0

Tangerines 687 0 0.005 1.0

Tomato Paste 506 0 0.001 - 0.005 0.1

Winter Squash 677 0 0.001 0.1

TOTAL 9,476 1

Chlorpyrifos methyl (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Chlorpyrifos methyl oxygen analog (insecticide metabolite)

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Appendix B. Page 20 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Chlorsulfuron (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Chlorthiophos (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Clethodim (herbicide) 

Apple Juice 724 0 0.006 0.20

Carrots 499 0 0.035 1.0

Cauliflower 692 0 0.002 3.0

Eggplant 661 0 0.002 - 0.035 1.0

Green Beans 177 0 0.010 3.5

Orange Juice 499 0 0.010 NT

Radishes 689 0 0.010 1.0

Summer Squash 176 0 0.005 - 0.010 0.50

Sweet Bell Peppers 675 0 0.010 1.0

Tangerines 687 0 0.20 NT

Tomato Paste 506 0 0.010 - 0.20 1.0

Winter Squash 677 0 0.010 0.50

TOTAL 6,662 0

Clethodim 5-OH sulfone (herbicide metabolite)

Apple Juice 724 0 0.010 0.20

Carrots 499 0 0.10 1.0

Eggplant 311 0 0.10 1.0

TOTAL 1,534 0

Clethodim sulfone (herbicide metabolite)

Apple Juice 724 0 0.015 0.20

Carrots 499 0 0.040 1.0

Eggplant 311 0 0.040 1.0

TOTAL 1,534 0

Clethodim sulfoxide (herbicide metabolite)

Apple Juice 724 0 0.015 0.20

Carrots 499 0 0.040 1.0

Eggplant 311 0 0.040 1.0

TOTAL 1,534 0

Clodinafop propargyl (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Appendix B. Page 21 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Clofentezine (insecticide) 

Apple Juice 724 0 0.005 0.50

Carrots 499 0 0.080 NT

Eggplant 311 0 0.040 - 0.080 NT

Green Beans 177 0 0.005 NT

Kiwi Fruit 177 0 0.040 NT

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 3,443 0

Clomazone (herbicide) 

Blueberries, Cultivated, Fresh 168 0 0.005 NT

Blueberries, Frozen 7 0 0.005 NT

Broccoli 675 0 0.002 0.10

Cantaloupe 694 0 0.005 0.05

Carrots 499 0 0.020 NT

Cauliflower 692 0 0.002 0.10

Collard Greens 514 0 0.005 NT

Eggplant 661 0 0.002 - 0.020 NT

Green Beans 177 0 0.001 0.05

Kiwi Fruit 177 0 0.070 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.001 - 0.005 0.1

Sweet Bell Peppers 675 0 0.005 0.05

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 0.1

TOTAL 8,173 0

Cloquintocet-mexyl (herbicide safener) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Cloransulam methyl (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Clothianidin (insecticide) (also a metabolite of Thiamethoxam)

Apple Juice 724 0 0.020 1.0

Bananas 703 0 0.020 0.03

Blueberries, Cultivated, Fresh 168 1 0.6 0.016 0.010 0.30

Blueberries, Frozen 7 0 0.010 0.30

Broccoli 675 31 4.6 0.005 - 0.037 0.005 4.5

Cantaloupe 694 9 1.3 0.010 - 0.028 0.010 0.2

Carrots 499 0 0.035 0.8

Cauliflower 692 16 2.3 0.003 - 0.056 0.002 4.5

Appendix B. Page 22 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Collard Greens 514 80 15.6 0.010 - 0.28 0.010 3.0

Eggplant 661 62 9.4 0.003 - 0.087 0.002 - 0.035 0.25

Green Beans 177 0 0.001 0.02

Kiwi Fruit 177 0 0.035 0.02

Orange Juice 499 1 0.2 0.002 0.001 0.40

Radishes 689 0 0.010 0.8

Summer Squash 176 12 6.8 0.001 - 0.005 0.001 - 0.025 0.2

Sweet Bell Peppers 675 134 19.9 0.010 - 0.25 0.010 0.80

Tangerines 687 0 0.025 0.40

Tomato Paste 506 125 24.7 0.001 - 0.013 0.001 - 0.025 0.80

Winter Squash 677 13 1.9 0.001 - 0.012 0.001 0.2

TOTAL 9,600 484

Coumaphos (insecticide) 

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Broccoli 675 0 0.002 - 0.005 NT

Cantaloupe 694 0 0.010 NT

Cauliflower 692 0 0.002 - 0.005 NT

Collard Greens 514 0 0.010 NT

Eggplant 350 0 0.002 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 6,196 0

Coumaphos oxygen analog (metabolite of Coumaphos)

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Broccoli 675 0 0.003 NT

Cantaloupe 694 0 0.010 NT

Cauliflower 692 0 0.003 NT

Collard Greens 514 0 0.010 NT

Eggplant 350 0 0.003 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,832 0

Crotoxyphos (insecticide, acaricide)

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 1,732 0

Crufomate (insecticide) 

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Appendix B. Page 23 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 1,732 0

Cumyluron (herbicide) 

Radishes 689 0 0.010 NT

Sweet Bell Peppers 675 0 0.010 NT

TOTAL 1,364 0

Cyanazine (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Cyantraniliprole (insecticide) 

Apple Juice 724 0 0.012 1.5

Broccoli 675 10 1.5 0.008 - 0.25 0.008 3.0

Carrots 499 0 0.15 0.40

Cauliflower 692 3 0.4 0.004 0.002 3.0

Eggplant 661 13 2 0.004 - 0.014 0.002 - 0.15 2.0

Green Beans 177 7 4 0.003 - 0.15 0.003 2.0

Kiwi Fruit 177 0 0.15 NT

Orange Juice 499 0 0.003 0.70

Summer Squash 176 0 0.003 - 0.005 0.70

Tangerines 687 0 0.005 0.70

Tomato Paste 506 0 0.003 - 0.005 2.0

Winter Squash 677 0 0.003 0.70

TOTAL 6,150 33

Cyazofamid (fungicide) 

Broccoli 675 1 0.1 0.010 0.006 1.5

Carrots 499 3 0.6 0.023 - 0.025 0.020 0.09

Cauliflower 692 0 0.006 1.5

Eggplant 661 0 0.006 - 0.020 0.9

Green Beans 177 1 0.6 0.10 0.010 0.5

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 0 0.010 NT

Summer Squash 176 0 0.010 0.10

Tangerines 687 0 0.010 NT

Tomato Paste 480 0 0.010 0.9

Winter Squash 677 0 0.010 0.10

TOTAL 5,400 5

Cyclaniliprole (insecticide) 

Apple Juice 724 0 0.008 0.30

Carrots 499 0 0.010 EX1

Eggplant 311 0 0.010 0.20

Summer Squash 87 0 0.010 0.15

Tangerines 687 0 0.010 0.4

Tomato Paste 216 0 0.010 0.20

TOTAL 2,524 0

Cyflufenamid (fungicide) 

Apple Juice 724 0 0.003 0.06

Carrots 499 0 0.005 NT

Appendix B. Page 24 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Eggplant 311 0 0.005 0.20

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 176 5 2.8 0.003 - 0.025 0.001 - 0.005 0.10

Sweet Bell Peppers 675 0 0.010 0.20

Tangerines 687 0 0.005 NT

Tomato Paste 506 1 0.2 0.001 0.001 - 0.005 0.20

Winter Squash 677 72 10.6 0.001 - 0.056 0.001 0.10

TOTAL 5,797 78

Cyflumetofen (acaricide) 

Apple Juice 724 0 0.003 0.30

Carrots 499 0 0.015 NT

Eggplant 311 1 0.3 0.015 0.015 2

Green Beans 177 0 0.003 - 0.005 NT

Kiwi Fruit 177 0 0.010 - 0.050 NT

Orange Juice 499 0 0.003 0.30

Summer Squash 176 0 0.003 - 0.020 NT

Tangerines 687 0 0.10 0.30

Tomato Paste 506 0 0.003 - 0.10 0.7

Winter Squash 677 0 0.003 - 0.005 NT

TOTAL 4,433 1

Cyfluthrin (insecticide) 

Apple Juice 724 0 0.015 0.5

Bananas 703 0 0.015 0.05

Blueberries, Cultivated, Fresh 168 0 0.004 0.05

Blueberries, Frozen 7 0 0.004 0.05

Broccoli 675 4 0.6 0.012 0.008 2.5

Cantaloupe 694 0 0.004 0.1

Carrots 499 0 0.025 0.20

Cauliflower 692 0 0.008 2.5

Collard Greens 514 110 21.4 0.004 - 1.9 0.004 7.0

Eggplant 661 2 0.3 0.031 - 0.035 0.025 - 0.50 0.5

Green Beans 177 0 0.003 0.05

Kiwi Fruit 177 0 0.045 0.05

Orange Juice 499 0 0.003 0.2

Radishes 689 2 0.3 0.007 0.005 1.0

Summer Squash 176 0 0.003 - 0.050 0.1

Sweet Bell Peppers 675 25 3.7 0.005 - 0.098 0.005 0.50

Tangerines 687 0 0.050 0.2

Tomato Paste 506 0 0.003 - 0.050 0.5

Winter Squash 677 6 0.9 0.003 - 0.005 0.003 0.1

TOTAL 9,600 149

Cyhalothrin, Total (Cyhalothrin-L + R157836 epimer) (insecticide)

Apple Juice 724 0 0.006 0.30

Bananas 703 0 0.006 0.01

Blueberries, Cultivated, Fresh 168 1 0.6 0.027 0.005 X-1 0.01

Blueberries, Frozen 7 0 0.005 0.01

Broccoli 675 30 4.4 0.005 - 0.078 0.003 0.4

Cantaloupe 694 0 0.005 0.05

Carrots 499 0 0.015 0.01

Cauliflower 692 0 0.003 0.4

Collard Greens 514 18 3.5 0.005 - 0.52 0.005 X-12 0.01

Appendix B. Page 25 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Eggplant 661 6 0.9 0.005 - 0.024 0.003 - 0.015 0.20

Green Beans 177 25 14.1 0.003 - 0.033 0.003 0.20

Kiwi Fruit 177 0 0.015 0.01

Orange Juice 499 0 0.003 0.01

Radishes 689 2 0.3 0.009 - 0.014 0.008 0.01

Summer Squash 176 2 1.1 0.003 - 0.007 0.003 - 0.005 0.05

Sweet Bell Peppers 675 33 4.9 0.008 - 0.97 0.008 X-1 0.20

Tangerines 687 0 0.005 0.01

Tomato Paste 506 76 15 0.003 - 0.009 0.003 - 0.005 0.1

Winter Squash 677 19 2.8 0.003 - 0.014 0.003 0.05

TOTAL 9,600 212

Cymoxanil (fungicide)

Blueberries, Cultivated, Fresh 168 0 0.005 NT

Blueberries, Frozen 7 0 0.005 NT

Cantaloupe 694 0 0.005 0.05

Carrots 499 0 0.020 NT

Cauliflower 650 0 0.010 NT

Collard Greens 514 1 0.2 0.006 0.005 V-1 NT

Eggplant 661 0 0.010 - 0.020 0.2

Green Beans 177 0 0.010 NT

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 0 0.010 NT

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.010 - 0.050 0.05

Sweet Bell Peppers 675 0 0.010 0.2

Tangerines 687 0 0.10 NT

Tomato Paste 506 0 0.010 - 0.10 0.2

Winter Squash 677 0 0.010 0.05

TOTAL 7,456 1

Cypermethrin (insecticide) 

Apple Juice 724 0 0.050 2

Bananas 703 0 0.050 0.05

Blueberries, Cultivated, Fresh 168 19 11.3 0.015 - 0.30 0.010 0.8

Blueberries, Frozen 7 3 42.9 0.027 - 0.15 0.010 0.8

Broccoli 675 9 1.3 0.037 - 1.5 0.022 2.0

Cantaloupe 694 0 0.010 0.2

Carrots 499 0 0.035 0.1

Cauliflower 692 0 0.022 2.0

Collard Greens 514 100 19.5 0.010 - 4.4 0.010 14.0

Eggplant 661 3 0.5 0.045 - 0.053 0.022 - 0.075 0.2

Green Beans 177 21 11.9 0.008 - 0.17 0.005 0.5

Kiwi Fruit 177 0 0.070 0.05

Orange Juice 499 0 0.005 0.35

Radishes 689 7 1 0.012 - 0.020 0.010 0.1

Summer Squash 176 3 1.7 0.006 - 0.008 0.005 - 0.050 0.2

Sweet Bell Peppers 675 61 9 0.010 - 0.27 0.010 0.2

Tangerines 687 0 0.050 0.35

Tomato Paste 506 0 0.005 - 0.050 0.2

Winter Squash 677 11 1.6 0.005 - 0.022 0.005 0.2

TOTAL 9,600 237

Cyphenothrin (insecticide) 

Apple Juice 724 0 0.035 NT

Bananas 703 0 0.035 NT

Appendix B. Page 26 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Blueberries, Cultivated, Fresh 168 1 0.6 0.059 0.015 V-1 NT

Blueberries, Frozen 7 0 0.015 NT

Cantaloupe 694 0 0.015 NT

Carrots 499 0 0.060 NT

Collard Greens 514 0 0.015 NT

Eggplant 311 0 0.060 NT

Green Beans 177 0 0.015 - 0.020 NT

Kiwi Fruit 177 0 0.060 NT

Orange Juice 499 0 0.020 NT

Radishes 689 0 0.008 NT

Summer Squash 155 0 0.015 - 0.050 NT

Sweet Bell Peppers 675 0 0.008 NT

Tangerines 687 0 0.050 NT

Tomato Paste 472 0 0.020 - 0.050 NT

Winter Squash 642 0 0.015 - 0.020 NT

TOTAL 7,793 1

Cyprazine (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Cyproconazole (fungicide) 

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Cantaloupe 694 0 0.010 NT

Carrots 499 0 0.005 NT

Collard Greens 514 0 0.010 NT

Eggplant 311 0 0.005 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,102 0

Cyprodinil (fungicide) 

Apple Juice 724 5 0.7 0.003 0.002 1.7

Blueberries, Cultivated, Fresh 168 52 31 0.005 - 0.45 0.005 5.0

Blueberries, Frozen 7 4 57.1 0.011 - 0.11 0.005 5.0

Broccoli 675 15 2.2 0.002 - 0.062 0.001 1.0

Cantaloupe 694 12 1.7 0.005 - 0.014 0.005 0.70

Carrots 499 2 0.4 0.019 - 0.039 0.015 0.75

Cauliflower 692 1 0.1 0.008 0.001 1.0

Collard Greens 514 7 1.4 0.008 - 0.41 0.005 10.0

Green Beans 177 0 0.003 0.6

Kiwi Fruit 177 22 12.4 0.038 - 0.87 0.015 1.8

Orange Juice 499 0 0.003 NT

Radishes 689 1 0.1 0.007 0.005 0.75

Summer Squash 176 2 1.1 0.003 - 0.009 0.003 - 0.005 0.70

Sweet Bell Peppers 675 13 1.9 0.005 - 0.043 0.005 1.5

Tangerines 687 0 0.005 NT

Appendix B. Page 27 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomato Paste 506 3 0.6 0.005 - 0.006 0.003 - 0.005 1.5

Winter Squash 677 13 1.9 0.004 - 0.020 0.003 0.70

TOTAL 8,236 152

Cyprosulfamide (herbicide safener) 

Eggplant 311 0 0.010 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.003 NT

Summer Squash 176 0 0.003 - 0.005 NT

Tangerines 687 0 0.010 NT

Tomato Paste 506 0 0.003 - 0.010 NT

Winter Squash 677 0 0.003 NT

TOTAL 3,210 0

Cyromazine (insect growth regulator) 

Carrots 499 0 0.10 NT

Eggplant 311 0 0.10 3

Green Beans 177 0 0.005 2.0

Kiwi Fruit 177 0 0.10 NT

Orange Juice 499 0 0.005 NT

Radishes 629 0 0.020 0.5

Summer Squash 176 1 0.6 0.009 0.005 - 0.050 1.0

Tomato Paste 290 0 0.005 1

Winter Squash 677 1 0.1 0.037 0.005 1.0

TOTAL 3,435 2

Daimuron (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

DCPA (herbicide) 

Blueberries, Cultivated, Fresh 168 0 0.002 NT

Blueberries, Frozen 7 0 0.002 NT

Broccoli 675 175 25.9 0.002 - 0.28 0.001 5.0

Cantaloupe 694 29 4.2 0.002 - 0.019 0.002 1.0

Carrots 499 0 0.020 NT

Cauliflower 692 26 3.8 0.002 - 0.005 0.001 5.0

Collard Greens 514 168 32.7 0.002 - 0.16 0.002 5.0

Eggplant 661 0 0.001 - 0.020 1.0

Green Beans 177 1 0.6 0.002 0.001 2.0

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 0 0.001 NT

Radishes 689 146 21.2 0.005 - 0.24 0.005 2.0

Summer Squash 176 1 0.6 0.007 0.001 - 0.005 1.0

Sweet Bell Peppers 675 0 0.005 2.0

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 1.0

Winter Squash 677 4 0.6 0.005 - 0.039 0.001 1.0

TOTAL 8,173 550

DEF - Tribufos (herbicide, plant growth regulator)

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Appendix B. Page 28 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Deltamethrin (includes parent Tralomethrin) (insecticide) 

Apple Juice 724 0 0.020 0.2

Bananas 703 0 0.020 0.05

Blueberries, Cultivated, Fresh 168 0 0.015 0.05

Blueberries, Frozen 7 0 0.015 0.05

Broccoli 675 0 0.012 0.05

Cantaloupe 694 0 0.015 0.2

Carrots 499 0 0.070 0.2

Cauliflower 692 0 0.012 0.05

Collard Greens 514 0 0.015 0.05

Eggplant 661 0 0.004 - 0.070 0.3

Green Beans 177 1 0.6 0.005 0.001 0.05

Kiwi Fruit 177 0 0.12 0.05

Orange Juice 499 0 0.001 0.30

Radishes 689 0 0.008 0.2

Summer Squash 176 0 0.001 - 0.050 0.2

Sweet Bell Peppers 675 12 1.8 0.008 - 0.070 0.008 0.3

Tangerines 687 0 0.050 0.05

Tomato Paste 506 0 0.001 - 0.050 1.0

Winter Squash 677 5 0.7 0.002 - 0.005 0.001 0.2

TOTAL 9,600 18

Demeton-O (metabolite of the insecticide Demeton)

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Demeton-S (metabolite of Demeton)

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 1,732 0

Demeton-S methyl (insecticide metabolite)

Green Beans 177 0 0.005 NT

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 1,732 0

Demeton-S sulfone (metabolite of Demeton-S)

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Appendix B. Page 29 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Demeton-S sulfoxide (metabolite of Demeton-S)

Green Beans 177 0 0.001 NT

Summer Squash 89 0 0.001 NT

Winter Squash 62 0 0.001 NT

TOTAL 328 0

Desethyl atrazine (herbicide metabolite)

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 1,732 0

Desmedipham (herbicide) 

Carrots 499 0 0.060 NT

Eggplant 311 0 0.060 NT

Kiwi Fruit 177 0 0.060 NT

Summer Squash 87 0 0.005 NT

Tangerines 687 0 0.005 NT

Tomato Paste 206 0 0.005 NT

TOTAL 1,967 0

Desmetryn (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Dialifos (insecticide) 

Green Beans 177 0 0.005 NT

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 1,732 0

Diazinon (insecticide) 

Apple Juice 724 0 0.001 0.50

Bananas 703 0 0.001 0.20

Blueberries, Cultivated, Fresh 168 0 0.005 0.50

Blueberries, Frozen 7 0 0.005 0.50

Broccoli 675 1 0.1 0.011 0.001 0.70

Cantaloupe 694 0 0.005 0.75

Carrots 499 0 0.010 0.75

Cauliflower 692 0 0.001 0.70

Collard Greens 514 1 0.2 2.1 0.005 X-1 0.70

Eggplant 661 0 0.001 - 0.010 NT

Green Beans 177 0 0.001 0.50

Kiwi Fruit 177 0 0.010 0.75

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.002 0.50

Summer Squash 176 0 0.001 - 0.005 0.50

Sweet Bell Peppers 675 3 0.4 0.002 - 0.010 0.002 0.5

Appendix B. Page 30 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 0.75

Winter Squash 677 0 0.001 0.75

TOTAL 9,600 5

Diazinon oxygen analog (metabolite of Diazinon)

Apple Juice 724 0 0.003 0.50

Bananas 703 0 0.003 0.20

Broccoli 675 0 0.001 0.70

Carrots 499 0 0.010 0.75

Cauliflower 692 0 0.001 0.70

Eggplant 661 0 0.001 - 0.010 NT

Green Beans 177 0 0.001 0.50

Kiwi Fruit 177 0 0.010 0.75

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.001 0.50

Summer Squash 89 0 0.001 0.50

Sweet Bell Peppers 675 0 0.001 0.5

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 0.75

Winter Squash 677 0 0.001 0.75

TOTAL 8,130 0

Dichlobenil (herbicide) 

Apple Juice 724 0 0.001 0.5

Blueberries, Cultivated, Fresh 168 0 0.010 0.15

Blueberries, Frozen 7 0 0.010 0.15

Broccoli 675 0 0.001 NT

Cantaloupe 694 0 0.010 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.001 NT

Collard Greens 514 0 0.010 NT

Eggplant 661 0 0.001 - 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.001 - 0.002 NT

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 0 0.002 NT

Tomato Paste 506 0 0.001 - 0.002 NT

Winter Squash 677 0 0.001 NT

TOTAL 8,897 0

Dichlofenthion (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Dichlormid (herbicide safener)

Carrots 499 0 0.040 0.05

Eggplant 311 0 0.040 0.05

Green Beans 177 0 0.020 0.05

Kiwi Fruit 177 0 0.040 NT

Appendix B. Page 31 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Orange Juice 499 0 0.020 NT

Summer Squash 176 0 0.005 - 0.020 0.05

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.005 - 0.020 0.05

Winter Squash 677 0 0.020 0.05

TOTAL 3,709 0

Dichlorobenzophenone o,p' (insecticide) (also a breakdown product of Dicofol)

Green Beans 177 0 0.001 NT

Summer Squash 55 0 0.001 NT

Winter Squash 62 0 0.001 NT

Green Beans 177 0 0.001 NT

Summer Squash 55 0 0.001 NT

Winter Squash 62 0 0.001 NT

TOTAL 588 0

Dichlorvos - DDVP (insecticide) (also a metabolite of Naled)

Apple Juice 724 0 0.050 0.5

Bananas 703 0 0.050 0.5

Blueberries, Cultivated, Fresh 168 0 0.020 0.5

Blueberries, Frozen 7 0 0.020 0.5

Broccoli 675 0 0.003 1

Cantaloupe 694 0 0.020 0.5

Carrots 499 0 0.010 0.5

Cauliflower 692 0 0.010 1

Collard Greens 514 0 0.020 3

Eggplant 661 0 0.003 - 0.010 0.5

Green Beans 177 0 0.020 - 0.040 0.5

Kiwi Fruit 177 0 0.010 0.5

Orange Juice 499 0 0.020 3

Radishes 689 0 0.010 0.5

Summer Squash 176 0 0.005 - 0.040 0.5

Sweet Bell Peppers 675 2 0.3 0.018 - 0.043 0.010 0.5

Tangerines 687 0 0.005 3

Tomato Paste 506 0 0.005 - 0.020 0.5

Winter Squash 677 0 0.020 - 0.040 0.5

TOTAL 9,600 2

Diclobutrazol (fungicide) 

Green Beans 177 0 0.001 - 0.005 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 - 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 - 0.005 NT

TOTAL 1,732 0

Diclofop methyl (herbicide) 

Blueberries, Cultivated, Fresh 168 0 0.001 NT

Blueberries, Frozen 7 0 0.001 NT

Cantaloupe 694 0 0.001 NT

Collard Greens 514 0 0.001 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 3,115 0

Appendix B. Page 32 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Dicloran (fungicide) 

Blueberries, Cultivated, Fresh 168 0 0.016 NT

Blueberries, Frozen 7 0 0.016 NT

Broccoli 675 2 0.3 0.004 0.002 V-2 NT

Cantaloupe 694 0 0.016 NT

Carrots 499 0 0.020 10

Cauliflower 692 0 0.002 NT

Collard Greens 514 0 0.016 NT

Eggplant 661 0 0.002 - 0.020 NT

Green Beans 177 14 7.9 0.002 - 6.0 0.001 20

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.001 - 0.010 NT

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 0 0.010 NT

Tomato Paste 506 0 0.001 - 0.010 5

Winter Squash 677 0 0.001 NT

TOTAL 8,173 16

Diclosulam (herbicide) 

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 1,732 0

Dicofol (insecticide) 

Apple Juice 724 0 0.007 10.0

TOTAL 724 0

Dicofol o,p' (isomer of Dicofol) 

Carrots 499 0 0.015 NT

Eggplant 311 0 0.015 2.0

Kiwi Fruit 177 0 0.015 NT

TOTAL 987 0

Dicofol p,p' (isomer of Dicofol) 

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Broccoli 675 0 0.001 NT

Cantaloupe 694 0 0.010 2.0

Carrots 499 0 0.025 NT

Cauliflower 692 0 0.001 NT

Collard Greens 514 0 0.010 NT

Eggplant 661 0 0.001 - 0.025 2.0

Kiwi Fruit 177 0 0.025 NT

Summer Squash 87 0 0.005 2.0

Tangerines 687 0 0.005 6.0

Tomato Paste 216 0 0.005 2.0

TOTAL 5,077 0

Dicrotophos (insecticide) 

Broccoli 675 0 0.001 NT

Cauliflower 692 0 0.001 NT

Appendix B. Page 33 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Eggplant 350 0 0.001 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 3,449 0

Diethofencarb (fungicide) 

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 1,732 0

Difenoconazole (fungicide) 

Apple Juice 724 1 0.1 0.002 0.001 5.0

Bananas 703 2 0.3 0.002 0.001 0.2

Blueberries, Cultivated, Fresh 168 16 9.5 0.013 - 0.42 0.010 4.0

Blueberries, Frozen 7 0 0.010 4.0

Broccoli 675 8 1.2 0.004 - 0.18 0.003 2.0

Cantaloupe 694 0 0.010 0.70

Carrots 499 6 1.2 0.005 - 0.065 0.005 0.6

Cauliflower 692 0 0.001 2.0

Collard Greens 514 12 2.3 0.014 - 0.98 0.010 35

Eggplant 661 43 6.5 0.002 - 0.046 0.001 - 0.005 0.60

Green Beans 177 3 1.7 0.002 - 0.004 0.001 V-3 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 0.60

Radishes 689 0 0.005 0.6

Summer Squash 176 0 0.001 - 0.002 0.70

Sweet Bell Peppers 675 120 17.8 0.005 - 0.49 0.005 0.60

Tangerines 687 0 0.002 0.60

Tomato Paste 506 309 61.1 0.001 - 0.020 0.001 - 0.002 0.60

Winter Squash 677 21 3.1 0.001 - 0.015 0.001 0.70

TOTAL 9,600 541

Diflubenzuron (insecticide) 

Blueberries, Cultivated, Fresh 168 0 0.002 NT

Blueberries, Frozen 7 0 0.002 NT

Broccoli 602 0 0.003 - 0.006 NT

Cantaloupe 694 0 0.002 NT

Carrots 499 0 0.080 0.20

Cauliflower 575 0 0.001 - 0.006 NT

Collard Greens 514 0 0.002 9.0

Eggplant 661 1 0.2 0.004 0.001 - 0.080 1.0

Green Beans 177 2 1.1 0.001 - 0.032 0.001 V-2 NT

Kiwi Fruit 177 0 0.080 NT

Orange Juice 499 131 26.3 0.001 - 0.004 0.001 3.0

Summer Squash 176 0 0.001 - 0.020 NT

Tangerines 687 0 0.020 3.0

Tomato Paste 506 0 0.001 - 0.020 NT

Winter Squash 677 1 0.1 0.002 0.001 V-1 NT

TOTAL 6,619 135

Appendix B. Page 34 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Dimepiperate (herbicide) 

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 1,732 0

Dimethenamid (herbicide) 

Blueberries, Cultivated, Fresh 168 0 0.002 NT

Blueberries, Frozen 7 0 0.002 NT

Broccoli 675 0 0.001 NT

Cantaloupe 694 0 0.002 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.001 NT

Collard Greens 514 0 0.002 NT

Eggplant 661 0 0.001 - 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 0.01

Summer Squash 176 0 0.001 - 0.005 NT

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 0.01

TOTAL 8,173 0

Dimethipin (plant growth regulator) 

Green Beans 177 0 0.010 - 0.020 NT

Orange Juice 499 0 0.010 NT

Summer Squash 89 0 0.010 - 0.020 NT

Tomato Paste 290 0 0.010 NT

Winter Squash 677 0 0.010 - 0.020 NT

TOTAL 1,732 0

Dimethoate (insecticide) (parent of Omethoate)

Blueberries, Cultivated, Fresh 168 0 0.005 1.0

Blueberries, Frozen 7 0 0.005 1.0

Broccoli 675 5 0.7 0.003 - 0.14 0.003 2.0

Cantaloupe 694 0 0.005 1.0

Carrots 499 0 0.010 NT

Cauliflower 692 1 0.1 0.012 0.001 2.0

Collard Greens 514 1 0.2 0.009 0.005 V-1 NT

Eggplant 661 1 0.2 0.002 0.001 - 0.010 V-1 NT

Green Beans 177 4 2.3 0.002 - 0.11 0.001 2.0

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 2 0.4 0.001 - 0.002 0.001 2.0

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.001 - 0.005 NT

Sweet Bell Peppers 675 8 1.2 0.011 - 0.17 0.010 2.0

Tangerines 687 4 0.6 0.005 - 0.012 0.005 2.0

Tomato Paste 506 0 0.001 - 0.005 2.0

Winter Squash 677 0 0.001 NT

TOTAL 8,173 26

Appendix B. Page 35 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Dimethomorph (fungicide) 

Blueberries, Cultivated, Fresh 168 0 0.003 NT

Blueberries, Frozen 7 0 0.003 NT

Broccoli 675 18 2.7 0.001 - 0.41 0.001 - 0.003 6.0

Cantaloupe 694 0 0.003 0.5

Carrots 499 0 0.010 NT

Cauliflower 692 1 0.1 0.002 0.001 6.0

Collard Greens 514 54 10.5 0.003 - 2.4 0.003 30.0

Eggplant 661 5 0.8 0.002 - 0.056 0.001 - 0.010 1.5

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.003 - 0.020 0.5

Sweet Bell Peppers 675 8 1.2 0.011 - 0.033 0.010 1.5

Tangerines 687 0 0.020 NT

Tomato Paste 506 1 0.2 0.003 0.003 - 0.020 1.5

Winter Squash 677 6 0.9 0.003 - 0.008 0.003 0.5

TOTAL 8,173 93

Dimethylvinphos (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Dimetilan (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Dimoxystrobin (fungicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Diniconazole (fungicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Dinotefuran (insecticide) 

Apple Juice 724 0 0.030 2.0

Bananas 703 0 0.030 0.01

Blueberries, Cultivated, Fresh 168 0 0.003 0.2

Blueberries, Frozen 7 0 0.003 0.2

Appendix B. Page 36 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Broccoli 675 2 0.3 0.042 - 0.058 0.006 - 0.040 1.4

Cantaloupe 694 234 33.7 0.003 - 0.13 0.003 0.5

Carrots 499 0 0.015 0.01

Cauliflower 664 1 0.2 0.053 0.006 1.4

Collard Greens 514 8 1.6 0.006 - 0.017 0.003 15.0

Eggplant 661 74 11.2 0.010 - 0.12 0.006 - 0.015 0.7

Green Beans 177 13 7.3 0.003 - 0.031 0.003 X-3 0.01

Kiwi Fruit 177 0 0.015 0.9

Orange Juice 499 0 0.003 0.01

Radishes 689 0 0.010 0.01

Summer Squash 176 17 9.7 0.003 - 0.30 0.003 - 0.040 0.5

Sweet Bell Peppers 675 51 7.6 0.010 - 0.44 0.010 0.7

Tangerines 687 0 0.040 0.01

Tomato Paste 506 20 4 0.003 - 0.009 0.003 - 0.040 1.0

Winter Squash 677 28 4.1 0.003 - 0.042 0.003 0.5

TOTAL 9,572 448

Dioxacarb (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Dioxathion (insecticide) 

Green Beans 177 0 0.005 NT

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 1,732 0

Diphenamid (herbicide) 

Broccoli 675 0 0.002 NT

Cauliflower 692 0 0.002 NT

Eggplant 350 0 0.002 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,813 0

Diphenylamine - DPA (plant growth regulator) 

Apple Juice 724 50 6.9 0.010 - 0.077 0.006 10.0

Blueberries, Cultivated, Fresh 168 0 0.002 NT

Blueberries, Frozen 7 0 0.002 NT

Broccoli 675 0 0.003 NT

Cantaloupe 694 0 0.002 NT

Carrots 499 0 0.020 NT

Cauliflower 692 0 0.003 NT

Collard Greens 514 0 0.002 NT

Eggplant 661 0 0.003 - 0.020 NT

Green Beans 177 0 0.001 NT

Appendix B. Page 37 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Kiwi Fruit 177 0 0.065 NT

Orange Juice 499 1 0.2 0.002 0.001 V-1 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 256 3 1.2 0.001 - 0.002 0.001 V-3 NT

Winter Squash 677 0 0.001 NT

TOTAL 7,873 54

Dipropetryn (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Disulfoton (insecticide) 

Carrots 499 0 0.050 NT

Eggplant 311 0 0.050 NT

Green Beans 177 0 0.001 0.75

Kiwi Fruit 177 0 0.050 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,083 0

Disulfoton oxygen analog (metabolite of Disulfoton)

Blueberries, Cultivated, Fresh 136 0 0.001 NT

Blueberries, Frozen 7 0 0.001 NT

Broccoli 675 0 0.001 0.75

Cantaloupe 669 0 0.001 NT

Carrots 499 0 0.005 NT

Cauliflower 692 0 0.001 0.75

Collard Greens 514 0 0.001 NT

Eggplant 648 0 0.001 - 0.005 NT

Kiwi Fruit 177 0 0.005 NT

Summer Squash 87 0 0.001 NT

Tangerines 687 0 0.001 NT

Tomato Paste 216 0 0.001 NT

TOTAL 5,007 0

Disulfoton sulfone (metabolite of Disulfoton)

Blueberries, Cultivated, Fresh 168 0 0.020 NT

Blueberries, Frozen 7 0 0.020 NT

Broccoli 675 0 0.001 0.75

Cantaloupe 693 0 0.020 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.001 0.75

Collard Greens 514 0 0.020 NT

Eggplant 661 0 0.001 - 0.010 NT

Green Beans 177 0 0.001 0.75

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Appendix B. Page 38 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.010 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 7,182 0

Disulfoton sulfone oxygen analog (metabolite of Disulfoton)

Broccoli 512 0 0.001 0.75

Carrots 499 0 0.010 NT

Cauliflower 533 0 0.001 0.75

Eggplant 612 0 0.001 - 0.010 NT

Kiwi Fruit 177 0 0.010 NT

TOTAL 2,333 0

Disulfoton sulfoxide (metabolite of Disulfoton)

Blueberries, Cultivated, Fresh 168 0 0.005 NT

Blueberries, Frozen 7 0 0.005 NT

Broccoli 675 0 0.001 0.75

Cantaloupe 694 0 0.005 NT

Carrots 499 0 0.005 NT

Cauliflower 692 0 0.001 0.75

Collard Greens 514 0 0.005 NT

Eggplant 661 0 0.001 - 0.005 NT

Green Beans 177 0 0.001 0.75

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tangerines 687 0 0.002 NT

Tomato Paste 506 0 0.001 - 0.002 NT

Winter Squash 677 0 0.001 NT

TOTAL 6,722 0

Disulfoton sulfoxide oxygen analog (metabolite of Disulfoton)

Carrots 499 0 0.010 NT

Eggplant 311 0 0.010 NT

Kiwi Fruit 177 0 0.010 NT

TOTAL 987 0

Ditalimfos (fungicide) 

Green Beans 177 0 0.005 NT

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 1,732 0

Dithiopyr (herbicide) 

Carrots 499 0 0.010 NT

Eggplant 311 0 0.010 NT

Green Beans 177 0 0.003 - 0.005 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 - 0.005 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 - 0.005 NT

TOTAL 2,719 0

Appendix B. Page 39 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Diuron (herbicide) 

Apple Juice 724 0 0.006 0.1

Bananas 703 0 0.006 0.1

Blueberries, Cultivated, Fresh 168 1 0.6 0.004 0.002 0.1

Blueberries, Frozen 7 0 0.002 0.1

Broccoli 675 0 0.004 NT

Cantaloupe 694 0 0.002 NT

Carrots 499 0 0.015 NT

Cauliflower 692 0 0.004 NT

Collard Greens 482 2 0.4 0.002 - 0.004 0.002 V-2 NT

Eggplant 661 0 0.004 - 0.015 NT

Green Beans 177 0 0.010 NT

Kiwi Fruit 177 0 0.015 NT

Orange Juice 499 0 0.010 0.05

Summer Squash 176 0 0.010 NT

Tangerines 687 0 0.010 0.05

Tomato Paste 506 0 0.010 NT

Winter Squash 677 0 0.010 NT

TOTAL 8,204 3

DMST (4-dimethylaminosulphotosluidide) (metabolite of Tolyfluanid)

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 1,732 0

Dodine (fungicide) 

Apple Juice 724 0 0.005 5.0

Bananas 703 0 0.005 0.50

Green Beans 177 0 0.010 NT

Orange Juice 499 0 0.010 NT

Summer Squash 89 0 0.010 NT

Tomato Paste 290 0 0.010 NT

Winter Squash 677 0 0.010 NT

TOTAL 3,159 0

Edifenphos (fungicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Emamectin (insecticide) 

Green Beans 177 0 0.010 NT

Orange Juice 499 0 0.010 NT

Summer Squash 89 0 0.010 0.02

Tomato Paste 290 0 0.010 0.150

Winter Squash 677 0 0.010 0.02

TOTAL 1,732 0

Emamectin benzoate 1 (insecticide) 

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Appendix B. Page 40 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Broccoli 675 1 0.1 0.002 0.001 - 0.003 0.05

Cantaloupe 694 0 0.010 0.02

Carrots 499 0 0.005 NT

Cauliflower 692 0 0.001 - 0.003 0.05

Collard Greens 514 1 0.2 0.039 0.010 0.2

Eggplant 661 0 0.001 - 0.005 0.02

Radishes 689 0 0.010 NT

Sweet Bell Peppers 675 0 0.010 0.02

TOTAL 5,274 2

Endosulfan I (insecticide) 

Apple Juice 724 0 0.004 1.0

Blueberries, Cultivated, Fresh 168 0 0.010 0.3

Blueberries, Frozen 7 0 0.010 0.3

Broccoli 675 0 0.005 3.0

Cantaloupe 694 0 0.010 1.0

Carrots 499 0 0.030 0.2

Cauliflower 692 0 0.005 2.0

Collard Greens 514 0 0.010 2.0

Eggplant 661 0 0.005 - 0.030 1.0

Green Beans 177 0 0.001 2.0

Kiwi Fruit 177 0 0.030 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.001 - 0.010 1.0

Sweet Bell Peppers 675 0 0.005 2.0

Tangerines 687 0 0.010 NT

Tomato Paste 494 0 0.001 - 0.010 1.0

Winter Squash 677 0 0.001 1.0

TOTAL 8,885 0

Endosulfan II (isomer of Endosulfan)

Apple Juice 724 0 0.015 1.0

Blueberries, Cultivated, Fresh 168 0 0.015 0.3

Blueberries, Frozen 7 0 0.015 0.3

Broccoli 675 0 0.001 3.0

Cantaloupe 694 0 0.015 1.0

Carrots 499 0 0.030 0.2

Cauliflower 692 0 0.001 2.0

Collard Greens 514 0 0.015 2.0

Eggplant 661 0 0.001 - 0.030 1.0

Green Beans 177 0 0.001 2.0

Kiwi Fruit 177 0 0.085 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.001 - 0.005 1.0

Sweet Bell Peppers 675 0 0.005 2.0

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 1.0

Winter Squash 677 0 0.001 1.0

TOTAL 8,897 0

Endosulfan sulfate (metabolite of Endosulfan)

Apple Juice 724 0 0.004 1.0

Blueberries, Cultivated, Fresh 168 0 0.005 0.3

Blueberries, Frozen 7 0 0.005 0.3

Broccoli 675 0 0.018 3.0

Appendix B. Page 41 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cantaloupe 694 0 0.005 1.0

Carrots 499 0 0.030 0.2

Cauliflower 664 0 0.018 - 0.070 2.0

Collard Greens 514 0 0.005 2.0

Eggplant 661 0 0.018 - 0.035 1.0

Green Beans 177 1 0.6 0.001 0.001 2.0

Kiwi Fruit 177 0 0.040 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 176 1 0.6 0.002 0.001 - 0.015 1.0

Sweet Bell Peppers 675 0 0.005 2.0

Tangerines 687 0 0.015 NT

Tomato Paste 506 0 0.001 - 0.015 1.0

Winter Squash 677 3 0.4 0.001 - 0.017 0.001 1.0

TOTAL 8,869 5

EPN (insecticide) 

Bananas 703 0 0.020 NT

Carrots 499 0 0.040 NT

Eggplant 311 0 0.040 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.040 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 3,422 0

Epoxiconazole (fungicide) 

Bananas 703 19 2.7 0.002 - 0.005 0.001 0.5

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 5 0.7 0.002 - 0.016 0.001 V-5 NT

TOTAL 2,435 24

EPTC (herbicide) 

Broccoli 675 0 0.001 NT

Carrots 499 8 1.6 0.13 - 0.36 0.035 X-5 0.1

Cauliflower 692 0 0.001 - 0.003 NT

Eggplant 661 0 0.001 - 0.035 NT

Green Beans 177 1 0.6 0.008 0.003 0.08

Kiwi Fruit 177 0 0.035 NT

Radishes 689 0 0.010 0.1

Summer Squash 176 0 0.003 - 0.005 NT

Sweet Bell Peppers 675 0 0.010 NT

Tangerines 687 0 0.005 0.1

Tomato Paste 216 0 0.005 0.08

Winter Squash 62 0 0.003 NT

TOTAL 5,386 9

Esfenvalerate+Fenvalerate Total (insecticide) 

Apple Juice 724 0 0.020 1.0

Bananas 703 0 0.020 0.05

Blueberries, Cultivated, Fresh 168 0 0.005 1.0

Blueberries, Frozen 7 1 14.3 0.030 0.005 1.0

Appendix B. Page 42 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Broccoli 675 5 0.7 0.004 - 0.023 0.002 1.0

Cantaloupe 694 0 0.005 0.5

Cauliflower 692 0 0.002 0.5

Collard Greens 514 3 0.6 0.033 - 0.28 0.005 3.0

Eggplant 350 2 0.6 0.008 - 0.009 0.008 - 0.015 0.5

Radishes 689 11 1.6 0.006 - 0.019 0.005 0.3

Summer Squash 87 0 0.050 0.5

Sweet Bell Peppers 675 16 2.4 0.006 - 0.044 0.005 0.5

Tangerines 687 0 0.050 0.05

Tomato Paste 216 0 0.050 0.5

TOTAL 6,881 38

Esfenvalerate (isomer of Fenvalerate)

Carrots 499 0 0.020 0.5

Eggplant 311 0 0.020 0.5

Green Beans 177 0 0.005 1.0

Kiwi Fruit 177 5 2.8 0.042 - 0.22 0.035 0.5

Orange Juice 499 0 0.005 0.05

Summer Squash 89 0 0.005 0.5

Tomato Paste 290 16 5.5 0.005 - 0.010 0.005 0.5

Winter Squash 677 0 0.005 0.5

TOTAL 2,719 21

Esprocarb (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Ethaboxam (fungicide) 

Carrots 499 0 0.010 NT

Eggplant 311 0 0.010 0.90

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 176 1 0.6 0.011 0.001 - 0.005 0.30

Tomato Paste 290 0 0.001 NT

Winter Squash 677 5 0.7 0.002 - 0.079 0.001 0.30

TOTAL 2,629 6

Ethalfluralin (herbicide) 

Blueberries, Cultivated, Fresh 168 0 0.005 NT

Blueberries, Frozen 7 0 0.005 NT

Broccoli 675 0 0.002 NT

Cantaloupe 694 0 0.005 0.05

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.002 NT

Collard Greens 514 0 0.005 NT

Eggplant 661 0 0.002 - 0.010 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.003 NT

Summer Squash 176 0 0.001 - 0.003 0.05

Tangerines 687 0 0.001 NT

Tomato Paste 506 0 0.001 - 0.003 NT

Winter Squash 677 0 0.003 0.05

TOTAL 6,809 0

Appendix B. Page 43 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Ethametsulfuron methyl (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Ethidimuron (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Ethiofencarb (insecticide) 

Broccoli 675 0 0.002 NT

Cauliflower 692 0 0.002 NT

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.003 NT

Sweet Bell Peppers 675 0 0.010 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 4,463 0

Ethiofencarb sulfone (metabolite of Ethiofencarb)

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 1,732 0

Ethiofencarb sulfoxide (metabolite of Ethiofencarb)

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Ethion (insecticide) 

Broccoli 675 0 0.003 NT

Carrots 499 0 0.015 NT

Cauliflower 692 0 0.003 NT

Eggplant 661 0 0.001 - 0.015 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.015 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.010 NT

Appendix B. Page 44 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 5,800 0

Ethion mono oxon (metabolite of Ethion)

Broccoli 512 0 0.001 - 0.003 NT

Cauliflower 533 0 0.001 - 0.006 NT

Eggplant 301 0 0.001 NT

TOTAL 1,346 0

Ethiprole (insecticide) 

Green Beans 177 0 0.005 NT

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 1,732 0

Ethofumesate (herbicide) 

Carrots 499 0 0.005 7.0

Eggplant 311 0 0.005 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 2,719 0

Ethoprop (insecticide) 

Bananas 703 3 0.4 0.002 - 0.010 0.001 0.02

Broccoli 675 0 0.001 NT

Carrots 499 0 0.005 NT

Cauliflower 692 0 0.001 - 0.003 NT

Eggplant 661 0 0.001 - 0.005 NT

Green Beans 177 0 0.001 0.02

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.001 - 0.005 NT

Sweet Bell Peppers 675 0 0.010 NT

Tangerines 687 0 0.010 NT

Tomato Paste 506 0 0.001 - 0.010 NT

Winter Squash 677 0 0.001 NT

TOTAL 7,493 3

Ethoxyquin (plant growth regulator) 

Bananas 703 0 0.010 NT

Summer Squash 87 0 0.005 NT

Tangerines 628 0 0.005 NT

Tomato Paste 216 0 0.005 NT

TOTAL 1,634 0

Ethylan (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Appendix B. Page 45 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Etofenprox (insecticide) 

Apple Juice 724 0 0.003 5.0

Bananas 703 0 0.003 5.0

Blueberries, Cultivated, Fresh 168 0 0.025 5.0

Blueberries, Frozen 7 0 0.025 5.0

Broccoli 675 0 0.001 - 0.002 5.0

Cantaloupe 694 0 0.025 5.0

Carrots 499 0 0.020 5.0

Cauliflower 692 0 0.001 - 0.002 5.0

Collard Greens 514 0 0.025 5.0

Eggplant 661 0 0.001 - 0.020 5.0

Green Beans 177 0 0.001 5.0

Kiwi Fruit 177 8 4.5 0.039 - 0.14 0.035 5.0

Orange Juice 499 0 0.001 5.0

Summer Squash 176 0 0.001 - 0.010 5.0

Tangerines 687 0 0.010 5.0

Tomato Paste 506 0 0.001 - 0.010 5.0

Winter Squash 677 10 1.5 0.001 - 0.002 0.001 5.0

TOTAL 8,236 18

Etoxazole (acaricide) 

Apple Juice 724 0 0.001 0.20

Broccoli 675 1 0.1 0.002 0.001 V-1 NT

Carrots 499 0 0.10 NT

Cauliflower 692 0 0.001 NT

Eggplant 661 10 1.5 0.002 - 0.003 0.001 - 0.10 0.20

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.20 NT

Orange Juice 499 0 0.001 0.10

Radishes 689 0 0.004 NT

Summer Squash 176 0 0.001 0.02

Sweet Bell Peppers 675 2 0.3 0.011 0.004 0.20

Tangerines 687 1 0.1 0.002 0.001 0.10

Tomato Paste 506 0 0.001 0.20

Winter Squash 677 0 0.001 0.02

TOTAL 7,514 14

Etridiazole (fungicide) 

Carrots 499 0 0.015 NT

Eggplant 311 0 0.015 NT

Green Beans 177 0 0.005 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.005 NT

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.005 NT

Sweet Bell Peppers 675 2 0.3 0.006 - 0.008 0.005 V-2 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.005 0.15

Winter Squash 677 0 0.005 NT

TOTAL 5,073 2

Etrimfos (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Appendix B. Page 46 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Famoxadone (fungicide) 

Blueberries, Cultivated, Fresh 168 0 0.025 NT

Blueberries, Frozen 7 0 0.025 NT

Broccoli 675 0 0.002 - 0.015 NT

Cantaloupe 694 0 0.025 0.30

Carrots 499 0 0.050 NT

Cauliflower 692 0 0.002 - 0.015 NT

Collard Greens 514 2 0.4 0.029 - 0.053 0.025 V-2 NT

Eggplant 598 0 0.008 - 0.050 4.0

Green Beans 177 0 0.010 NT

Kiwi Fruit 177 0 0.050 NT

Orange Juice 499 0 0.010 NT

Summer Squash 176 0 0.010 - 0.050 0.30

Tangerines 687 0 0.10 NT

Tomato Paste 506 1 0.2 0.011 0.010 - 0.10 1.0

Winter Squash 677 0 0.010 0.30

TOTAL 6,746 3

Famphur (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Fenamidone (fungicide) 

Blueberries, Cultivated, Fresh 168 0 0.005 NT

Blueberries, Frozen 7 0 0.005 NT

Broccoli 675 5 0.7 0.004 - 0.18 0.002 5.0

Cantaloupe 694 0 0.005 0.15

Carrots 499 1 0.2 0.015 0.015 0.15

Cauliflower 692 0 0.002 5.0

Collard Greens 514 47 9.1 0.005 - 2.3 0.005 60

Eggplant 661 0 0.002 - 0.015 1.0

Green Beans 177 0 0.001 0.80

Kiwi Fruit 177 0 0.060 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.001 0.15

Sweet Bell Peppers 675 0 0.010 1.0

Tangerines 687 0 0.001 NT

Tomato Paste 506 0 0.001 2.2

Winter Squash 677 0 0.001 0.15

TOTAL 8,173 53

Fenamiphos (insecticide) 

Bananas 703 0 0.002 0.1

Broccoli 675 0 0.001 - 0.003 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.001 - 0.006 NT

Eggplant 661 0 0.001 - 0.010 NT

Appendix B. Page 47 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 6,503 0

Fenamiphos sulfone (metabolite of Fenamiphos)

Bananas 703 0 0.002 0.1

Broccoli 655 0 0.005 - 0.010 NT

Carrots 499 0 0.005 NT

Cauliflower 692 0 0.005 NT

Eggplant 661 0 0.002 - 0.005 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 6,483 0

Fenamiphos sulfoxide (metabolite of Fenamiphos)

Bananas 703 0 0.006 0.1

Broccoli 675 0 0.002 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.002 NT

Eggplant 661 0 0.002 - 0.010 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.003 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 6,503 0

Fenarimol (fungicide) 

Apple Juice 724 0 0.005 0.3

Bananas 703 0 0.005 0.25

Broccoli 675 0 0.002 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.002 NT

Eggplant 661 0 0.002 - 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.015 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 0.20

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 1 0.1 0.005 0.005 V-1 NT

Appendix B. Page 48 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 0.20

TOTAL 8,130 1

Fenazaquin (insecticide, acaricide)

Apple Juice 724 0 0.001 0.6

Blueberries, Cultivated, Fresh 168 0 0.005 2

Blueberries, Frozen 7 0 0.005 2

Cantaloupe 669 0 0.005 0.3

Carrots 499 0 0.005 NT

Collard Greens 271 0 0.005 NT

Eggplant 311 0 0.005 0.3

Green Beans 177 0 0.001 0.4

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 0.5

Summer Squash 176 0 0.001 - 0.005 0.3

Tangerines 687 0 0.005 0.5

Tomato Paste 506 0 0.001 - 0.005 0.3

Winter Squash 677 0 0.001 - 0.003 0.3

TOTAL 5,548 0

Fenbuconazole (fungicide) 

Apple Juice 724 0 0.002 0.4

Bananas 703 0 0.002 0.3

Blueberries, Cultivated, Fresh 168 1 0.6 0.012 0.005 0.3

Blueberries, Frozen 7 0 0.005 0.3

Broccoli 628 0 0.003 - 0.006 NT

Cantaloupe 694 0 0.005 NT

Carrots 499 0 0.005 NT

Cauliflower 626 0 0.001 - 0.006 NT

Collard Greens 514 0 0.005 NT

Eggplant 661 0 0.001 - 0.005 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 1 0.2 0.002 0.001 1.0

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 1.0

Tangerines 687 0 0.001 1.0

Tomato Paste 506 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 9,487 2

Fenchlorphos (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Fenhexamid (fungicide) 

Blueberries, Cultivated, Fresh 168 44 26.2 0.015 - 2.0 0.013 5

Blueberries, Frozen 7 0 0.013 5

Cantaloupe 694 0 0.013 NT

Carrots 499 0 0.015 NT

Collard Greens 514 0 0.013 NT

Appendix B. Page 49 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Eggplant 311 0 0.015 2

Green Beans 177 0 0.010 NT

Kiwi Fruit 177 0 0.015 30

Orange Juice 499 0 0.010 NT

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.010 NT

Sweet Bell Peppers 675 16 2.4 0.013 - 0.088 0.010 2

Tangerines 687 0 0.010 NT

Tomato Paste 506 0 0.010 2

Winter Squash 677 0 0.010 NT

TOTAL 6,456 60

Fenitrothion (insecticide) 

Broccoli 675 0 0.002 NT

Cauliflower 692 0 0.002 NT

Eggplant 350 0 0.002 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 3,449 0

Fenobucarb - BPMC (insecticide) 

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 1,732 0

Fenoxaprop ethyl (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Fenoxycarb (insecticide) 

Carrots 499 0 0.020 NT

Eggplant 311 0 0.020 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 2,542 0

Fenpicoxamid (fungicide) 

Bananas 703 0 0.001 0.15

TOTAL 703 0

Fenpropathrin (insecticide) 

Apple Juice 724 0 0.006 5.0

Bananas 703 0 0.006 NT

Blueberries, Cultivated, Fresh 168 1 0.6 0.39 0.020 3.0

Appendix B. Page 50 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Blueberries, Frozen 7 2 28.6 0.048 - 0.26 0.020 3.0

Broccoli 675 0 0.002 3.0

Cantaloupe 694 0 0.02 0.5

Carrots 499 0 0.020 NT

Cauliflower 692 0 0.002 3.0

Collard Greens 514 0 0.020 NT

Eggplant 661 5 0.8 0.004 - 0.018 0.002 - 0.020 1.0

Green Beans 177 2 1.1 0.003 - 0.058 0.001 V-2 NT

Kiwi Fruit 177 0 0.020 5

Orange Juice 499 2 0.4 0.001 0.001 2.0

Radishes 689 0 0.005 NT

Summer Squash 176 1 0.6 0.002 0.001 - 0.005 0.5

Sweet Bell Peppers 675 14 2.1 0.013 - 0.080 0.005 1.0

Tangerines 687 0 0.005 2.0

Tomato Paste 506 10 2 0.001 - 0.006 0.001 - 0.005 1.0

Winter Squash 677 13 1.9 0.001 - 0.031 0.001 0.5

TOTAL 9,600 50

Fenpropidin (fungicide) 

Bananas 703 7 1 0.002 - 0.006 0.001 10

Green Beans 177 0 0.040 NT

Orange Juice 499 0 0.040 NT

Summer Squash 89 0 0.040 NT

Tomato Paste 290 0 0.040 NT

Winter Squash 677 0 0.040 NT

TOTAL 2,435 7

Fenpropimorph (fungicide) 

Bananas 703 74 10.5 0.005 - 0.018 0.003 2.0

Blueberries, Cultivated, Fresh 168 0 0.001 NT

Blueberries, Frozen 7 0 0.001 NT

Cantaloupe 632 0 0.001 NT

Collard Greens 450 1 0.2 0.001 0.001 V-1 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.010 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 5,056 75

Fenpyrazamine (fungicide) 

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 176 0 0.001 - 0.003 NT

Tangerines 687 0 0.001 NT

Tomato Paste 506 0 0.001 - 0.003 NT

Winter Squash 451 0 0.003 NT

TOTAL 2,496 0

Fenpyroximate (acaricide) 

Apple Juice 724 0 0.001 0.30

Blueberries, Cultivated, Fresh 168 0 0.005 3

Blueberries, Frozen 7 0 0.005 3

Broccoli 675 0 0.003 NT

Cantaloupe 694 0 0.005 0.10

Appendix B. Page 51 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Carrots 499 0 0.005 NT

Cauliflower 692 0 0.001 NT

Collard Greens 514 0 0.005 NT

Eggplant 661 22 3.3 0.003 - 0.036 0.003 - 0.005 0.20

Green Beans 177 0 0.001 0.40

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 1.0

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.001 0.4

Sweet Bell Peppers 675 31 4.6 0.010 - 0.13 0.010 0.20

Tomato Paste 290 0 0.001 0.20

Winter Squash 677 0 0.001 0.4

TOTAL 7,907 53

Fensulfothion (insecticide, fumigant)

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Fenthion (insecticide) 

Broccoli 675 0 0.006 NT

Carrots 499 0 0.030 NT

Cauliflower 692 0 0.002 - 0.006 NT

Eggplant 661 0 0.002 - 0.030 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.015 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 5,800 0

Fenthion oxygen analog sulfone (metabolite of Fenthion)

Carrots 499 0 0.015 NT

Eggplant 311 0 0.015 NT

Kiwi Fruit 177 0 0.015 NT

TOTAL 987 0

Fenthion oxygen analog sulfoxide (metabolite of Fenthion)

Carrots 499 0 0.015 NT

Eggplant 311 0 0.015 NT

Kiwi Fruit 177 0 0.015 NT

TOTAL 987 0

Fenthion sulfone (metabolite of Fenthion)

Carrots 499 0 0.12 NT

Eggplant 311 0 0.12 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.12 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Appendix B. Page 52 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 2,719 0

Fenthion sulfoxide (metabolite of Fenthion)

Carrots 499 0 0.020 NT

Eggplant 311 0 0.020 NT

Green Beans 177 0 0.010 NT

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 0 0.010 NT

Summer Squash 89 0 0.010 NT

Tomato Paste 290 0 0.010 NT

Winter Squash 677 0 0.010 NT

TOTAL 2,719 0

Fenuron (herbicide) 

Green Beans 177 0 0.005 - 0.020 NT

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 - 0.020 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 - 0.020 NT

TOTAL 1,732 0

Fipronil (insecticide) 

Broccoli 675 1 0.1 0.002 0.001 V-1 NT

Carrots 499 0 0.015 NT

Cauliflower 692 0 0.001 NT

Eggplant 661 0 0.001 - 0.015 NT

Green Beans 177 1 0.6 0.061 0.001 V-1 NT

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 1 0.1 0.014 0.005 V-1 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 5,800 3

Fipronil sulfone - MB46136 (metabolite of Fipronil)

Blueberries, Cultivated, Fresh 168 0 0.050 NT

Blueberries, Frozen 7 0 0.050 NT

Cantaloupe 694 0 0.050 NT

Collard Greens 514 0 0.050 NT

Green Beans 177 1 0.6 0.009 0.001 V-1 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 3,115 1

Flazasulfuron (herbicide) 

Green Beans 177 0 0.005 NT

Orange Juice 499 0 0.005 0.01

Summer Squash 176 0 0.005 NT

Tangerines 687 0 0.005 0.01

Tomato Paste 506 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 2,722 0

Appendix B. Page 53 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Flonicamid (insecticide) 

Apple Juice 724 0 0.010 0.20

Blueberries, Cultivated, Fresh 168 0 0.006 1.5

Blueberries, Frozen 7 0 0.006 1.5

Broccoli 675 6 0.9 0.003 - 0.035 0.003 1.5

Cantaloupe 694 4 0.6 0.010 - 0.012 0.006 1.5

Carrots 499 0 0.005 0.60

Cauliflower 664 1 0.2 0.005 0.003 1.5

Collard Greens 486 11 2.3 0.014 - 1.7 0.006 16

Eggplant 661 12 1.8 0.002 - 0.046 0.001 - 0.005 3.0

Green Beans 177 4 2.3 0.011 - 0.17 0.010 4.0

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.010 1.5

Radishes 689 44 6.4 0.010 - 0.12 0.010 0.60

Summer Squash 176 12 6.8 0.014 - 0.31 0.010 - 0.050 1.5

Sweet Bell Peppers 675 75 11.1 0.011 - 0.44 0.010 3.0

Tangerines 687 0 0.050 1.5

Tomato Paste 506 0 0.010 - 0.050 2.0

Winter Squash 677 0 0.010 1.5

TOTAL 8,841 169

Florpyrauxifen-Benzyl (herbicide) 

Green Beans 177 0 0.010 - 0.020 EX2

Orange Juice 499 0 0.010 EX2

Summer Squash 89 0 0.010 - 0.020 EX2

Tomato Paste 290 0 0.010 EX2

Winter Squash 677 0 0.010 - 0.020 EX2

TOTAL 1,732 0

Fluazifop butyl (herbicide) 

Bananas 703 0 0.001 0.01

Broccoli 675 0 0.001 NT

Carrots 499 0 0.005 2.0

Cauliflower 692 0 0.001 NT

Eggplant 661 0 0.001 - 0.005 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 0.03

Summer Squash 176 0 0.001 - 0.005 NT

Tangerines 687 0 0.005 0.03

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 NT

TOTAL 6,129 0

Fluazinam (fungicide) 

Apple Juice 724 0 0.005 2.0

Carrots 499 0 0.025 0.70

Eggplant 311 0 0.025 0.09

Kiwi Fruit 177 0 0.025 NT

TOTAL 1,711 0

Flubendiamide (insecticide) 

Apple Juice 724 0 0.004 1.5

Blueberries, Cultivated, Fresh 168 0 0.004 1.5

Blueberries, Frozen 7 0 0.004 1.5

Broccoli 675 17 2.5 0.002 - 0.43 0.001 - 0.003 3.0

Appendix B. Page 54 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cantaloupe 624 0 0.004 0.20

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.003 3.0

Collard Greens 514 6 1.2 0.004 - 0.46 0.004 25

Eggplant 661 2 0.3 0.003 - 0.009 0.003 - 0.010 0.60

Green Beans 177 2 1.1 0.002 - 0.003 0.001 0.50

Orange Juice 499 0 0.001 NT

Summer Squash 176 1 0.6 0.001 0.001 - 0.020 0.20

Tangerines 687 0 0.020 NT

Tomato Paste 506 0 0.001 - 0.020 0.60

Winter Squash 677 33 4.9 0.001 - 0.023 0.001 0.20

TOTAL 7,286 61

Flucythrinate (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Fludioxonil (fungicide) 

Apple Juice 724 50 6.9 0.012 - 0.10 0.007 5.0

Blueberries, Cultivated, Fresh 168 50 29.8 0.025 - 1.7 0.025 3.0

Blueberries, Frozen 7 1 14.3 0.043 0.025 3.0

Broccoli 675 7 1 0.010 - 0.076 0.006 2

Cantaloupe 694 0 0.025 0.03

Carrots 499 1 0.2 0.067 0.065 - 0.13 7.0

Cauliflower 692 1 0.1 0.010 0.006 2

Collard Greens 514 4 0.8 0.026 - 0.046 0.025 15

Eggplant 648 0 0.006 - 0.065 0.50

Green Beans 177 0 0.010 0.4

Kiwi Fruit 177 20 11.3 0.070 - 3.1 0.065 20

Orange Juice 499 3 0.6 0.019 - 0.022 0.010 10

Radishes 689 2 0.3 0.006 - 0.022 0.005 0.75

Summer Squash 176 0 0.005 - 0.010 0.45

Sweet Bell Peppers 675 18 2.7 0.007 - 0.33 0.005 0.50

Tangerines 687 197 28.7 0.005 - 0.21 0.005 10

Tomato Paste 506 0 0.005 - 0.010 5.0

Winter Squash 677 1 0.1 0.016 0.010 0.45

TOTAL 8,884 355

Fluensulfone (nematicide) 

Apple Juice 724 0 0.070 0.4

Carrots 499 0 0.010 4

Eggplant 311 0 0.010 0.7

Summer Squash 87 0 0.005 0.7

Tangerines 687 0 0.005 0.3

Tomato Paste 216 0 0.005 1.5

TOTAL 2,524 0

Flufenacet (herbicide) 

Carrots 499 0 0.005 NT

Eggplant 311 0 0.005 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Appendix B. Page 55 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.001 - 0.005 NT

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 NT

TOTAL 5,073 0

Flufenoxuron (insecticide) 

Apple Juice 724 0 0.002 0.50

Blueberries, Cultivated, Fresh 168 0 0.001 NT

Blueberries, Frozen 7 0 0.001 NT

Cantaloupe 694 0 0.001 NT

Collard Greens 514 0 0.001 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 0.30

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 3,839 0

Flufenpyr ethyl (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Flumetsulam (herbicide) 

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 1,732 0

Flumiclorac pentyl (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Flumioxazin (herbicide) 

Apple Juice 724 0 0.030 0.02

Blueberries, Cultivated, Fresh 168 0 0.010 0.07

Blueberries, Frozen 7 0 0.010 0.07

Broccoli 675 0 0.010 0.02

Cantaloupe 694 0 0.010 0.03

Carrots 499 0 0.040 NT

Cauliflower 692 0 0.003 0.02

Collard Greens 514 0 0.010 NT

Eggplant 661 0 0.003 - 0.040 0.02

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.040 NT

Appendix B. Page 56 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Orange Juice 499 0 0.001 0.02

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.001 - 0.005 0.03

Sweet Bell Peppers 675 0 0.005 0.02

Tangerines 687 0 0.005 0.02

Tomato Paste 506 0 0.001 - 0.005 0.02

Winter Squash 677 0 0.001 0.03

TOTAL 8,897 0

Fluometuron (herbicide) 

Carrots 499 0 0.010 NT

Eggplant 311 0 0.010 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.003 NT

Summer Squash 176 0 0.003 - 0.004 NT

Tangerines 687 0 0.004 NT

Tomato Paste 506 0 0.003 - 0.004 NT

Winter Squash 677 0 0.003 NT

TOTAL 3,709 0

Fluopicolide (fungicide) 

Blueberries, Cultivated, Fresh 168 0 0.005 NT

Blueberries, Frozen 7 0 0.005 NT

Broccoli 675 27 4 0.002 - 0.27 0.001 5.0

Cantaloupe 694 5 0.7 0.005 - 0.007 0.005 0.50

Carrots 499 11 2.2 0.011 - 0.037 0.010 0.15

Cauliflower 692 6 0.9 0.002 0.001 5.0

Collard Greens 514 115 22.4 0.005 - 1.5 0.005 18

Eggplant 661 38 5.7 0.002 - 0.040 0.001 - 0.010 1.6

Green Beans 177 2 1.1 0.002 - 0.003 0.001 0.90

Kiwi Fruit 177 0 0.015 NT

Orange Juice 499 0 0.001 0.01

Radishes 689 24 3.5 0.013 - 0.28 0.010 X-3 0.15

Summer Squash 176 9 5.1 0.002 - 0.034 0.001 - 0.010 0.50

Sweet Bell Peppers 675 31 4.6 0.010 - 0.11 0.010 1.6

Tangerines 687 0 0.010 0.01

Tomato Paste 506 0 0.001 - 0.010 1.6

Winter Squash 677 23 3.4 0.001 - 0.032 0.001 0.50

TOTAL 8,173 291

Fluopyram (fungicide) 

Apple Juice 724 1 0.1 0.003 0.002 0.80

Bananas 703 1 0.1 0.003 0.002 1.0

Blueberries, Cultivated, Fresh 168 1 0.6 0.032 0.005 7.0

Blueberries, Frozen 7 3 42.9 0.015 - 0.14 0.005 7.0

Broccoli 675 38 5.6 0.002 - 0.022 0.001 4.0

Cantaloupe 669 39 5.8 0.005 - 0.033 0.005 1.0

Carrots 499 18 3.6 0.005 - 0.023 0.005 0.30

Cauliflower 692 20 2.9 0.002 - 0.010 0.001 - 0.006 4.0

Collard Greens 514 62 12.1 0.005 - 1.1 0.005 50

Eggplant 661 105 15.9 0.002 - 0.099 0.001 - 0.005 4.0

Green Beans 177 5 2.8 0.001 - 0.010 0.001 4.0

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 1.0

Radishes 689 1 0.1 0.021 0.010 0.30

Summer Squash 176 26 14.8 0.002 - 0.11 0.001 - 0.002 0.60

Appendix B. Page 57 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Sweet Bell Peppers 675 117 17.3 0.010 - 0.18 0.010 4.0

Tangerines 687 1 0.1 0.002 0.002 1.0

Tomato Paste 506 67 13.2 0.001 - 0.018 0.001 - 0.002 1.0

Winter Squash 677 21 3.1 0.001 - 0.030 0.001 0.60

TOTAL 9,575 526

Fluorodifen (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Fluoxastrobin (fungicide) 

Broccoli 675 0 0.001 NT

Carrots 499 0 0.015 NT

Cauliflower 663 0 0.001 NT

Eggplant 661 19 2.9 0.002 - 0.024 0.001 - 0.015 1.0

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.015 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.002 NT

Summer Squash 176 0 0.001 0.50

Sweet Bell Peppers 675 6 0.9 0.002 - 0.050 0.002 1.0

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 1.5

Winter Squash 677 0 0.001 0.50

TOTAL 6,761 25

Flupyradifurone (insecticide) 

Apple Juice 724 0 0.015 0.70

Broccoli 675 33 4.9 0.003 - 0.25 0.003 6

Carrots 499 0 0.10 0.90

Cauliflower 692 124 17.9 0.002 - 0.026 0.001 6

Eggplant 661 50 7.6 0.002 - 0.17 0.001 - 0.10 1.5

Green Beans 177 0 0.001 3.0

Kiwi Fruit 177 0 0.10 NT

Orange Juice 499 2 0.4 0.001 - 0.002 0.001 3.0

Summer Squash 176 24 13.6 0.002 - 0.038 0.001 - 0.005 0.40

Tangerines 687 1 0.1 0.009 0.005 3.0

Tomato Paste 506 3 0.6 0.001 - 0.002 0.001 - 0.005 1.5

Winter Squash 677 20 3 0.001 - 0.019 0.001 0.40

TOTAL 6,150 257

Fluquinconazole (fungicide) 

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Cantaloupe 694 0 0.010 NT

Collard Greens 514 0 0.010 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.010 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,479 0

Appendix B. Page 58 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Fluridone (herbicide) 

Apple Juice 724 0 0.001 0.1

Blueberries, Cultivated, Fresh 168 0 0.001 0.1

Blueberries, Frozen 7 0 0.001 0.1

Broccoli 675 0 0.001 0.1

Cantaloupe 694 0 0.001 0.1

Carrots 499 0 0.005 0.1

Cauliflower 692 0 0.001 0.1

Collard Greens 514 0 0.001 0.1

Eggplant 661 0 0.001 - 0.005 0.1

Green Beans 177 0 0.001 0.1

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 0.1

Radishes 689 0 0.010 0.1

Summer Squash 176 0 0.001 - 0.002 0.1

Sweet Bell Peppers 675 0 0.010 0.1

Tangerines 687 0 0.002 0.1

Tomato Paste 506 0 0.001 - 0.002 0.1

Winter Squash 677 0 0.001 0.1

TOTAL 8,897 0

Fluroxypyr-meptyl (herbicide) 

Apple Juice 724 0 0.005 0.02

TOTAL 724 0

Flusilazole (fungicide) 

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Cantaloupe 694 0 0.010 NT

Carrots 499 0 0.010 NT

Collard Greens 243 0 0.010 NT

Eggplant 311 0 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.010 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 5,195 0

Fluthiacet methyl (herbicide) 

Carrots 499 0 0.010 NT

Eggplant 311 0 0.010 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.003 NT

Summer Squash 176 0 0.003 - 0.005 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.003 - 0.005 NT

Winter Squash 677 0 0.003 NT

TOTAL 3,709 0

Appendix B. Page 59 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Flutianil (fungicide) 

Apple Juice 724 0 0.002 0.15

Summer Squash 87 0 0.005 0.2

TOTAL 811 0

Flutolanil (fungicide) 

Blueberries, Cultivated, Fresh 168 0 0.002 NT

Blueberries, Frozen 7 0 0.002 NT

Cantaloupe 694 0 0.002 NT

Carrots 499 0 0.005 - 0.010 NT

Collard Greens 483 0 0.002 0.1

Eggplant 311 0 0.005 - 0.010 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 3,894 0

Flutriafol (fungicide) 

Apple Juice 724 8 1.1 0.003 0.002 0.40

Bananas 703 0 0.002 0.30

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Broccoli 675 9 1.3 0.002 - 0.010 0.001 1.5

Cantaloupe 694 7 1 0.011 - 0.021 0.010 0.30

Carrots 499 0 0.010 NT

Cauliflower 692 4 0.6 0.002 0.001 1.5

Collard Greens 514 8 1.6 0.012 - 0.11 0.010 7.0

Eggplant 661 18 2.7 0.002 - 0.021 0.001 - 0.010 1.0

Green Beans 177 3 1.7 0.001 - 0.004 0.001 V-3 NT

Kiwi Fruit 177 0 0.025 NT

Orange Juice 499 0 0.001 NT

Summer Squash 176 19 10.8 0.001 - 0.015 0.001 - 0.002 0.30

Tangerines 687 0 0.002 NT

Tomato Paste 506 15 3 0.001 - 0.011 0.001 - 0.002 1.5

Winter Squash 677 22 3.2 0.001 - 0.021 0.001 0.30

TOTAL 8,236 113

Fluvalinate (insecticide) 

Apple Juice 724 0 0.008 NT

Bananas 703 0 0.008 NT

Blueberries, Cultivated, Fresh 168 0 0.050 NT

Blueberries, Frozen 7 0 0.050 NT

Cantaloupe 694 0 0.050 NT

Carrots 499 0 0.020 NT

Collard Greens 514 0 0.050 NT

Eggplant 311 0 0.020 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.035 NT

Orange Juice 499 0 0.001 NT

Radishes 658 0 0.005 NT

Summer Squash 176 0 0.001 - 0.050 NT

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 0 0.050 NT

Tomato Paste 506 0 0.001 - 0.050 NT

Winter Squash 677 0 0.001 NT

TOTAL 7,852 0

Appendix B. Page 60 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Fluxapyroxad (fungicide) 

Apple Juice 724 17 2.3 0.003 - 0.008 0.002 0.8

Bananas 703 4 0.6 0.003 0.002 3.0

Broccoli 675 13 1.9 0.002 - 0.071 0.001 4.0

Carrots 499 15 3 0.011 - 0.034 0.010 0.90

Cauliflower 692 0 0.003 4.0

Eggplant 661 21 3.2 0.002 - 0.035 0.001 - 0.010 0.7

Green Beans 177 9 5.1 0.002 - 0.022 0.001 2.0

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 1.0

Summer Squash 176 3 1.7 0.001 - 0.004 0.001 - 0.005 0.50

Tangerines 687 1 0.1 0.005 0.005 1.0

Tomato Paste 506 185 36.6 0.001 - 0.019 0.001 - 0.005 0.7

Winter Squash 677 9 1.3 0.002 - 0.029 0.001 0.50

TOTAL 6,853 277

Folpet (fungicide) 

Apple Juice 724 0 0.15 5.0

Cantaloupe 694 0 0.030 3.0

Sweet Bell Peppers 655 0 0.015 NT

TOTAL 2,073 0

Fomesafen (herbicide) 

Summer Squash 87 0 0.005 0.025

Tangerines 687 0 0.005 NT

TOTAL 774 0

Fonofos (insecticide) 

Broccoli 675 0 0.001 - 0.003 NT

Carrots 499 0 0.015 NT

Cauliflower 692 0 0.003 NT

Eggplant 661 0 0.001 - 0.015 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.030 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 5,800 0

Foramsulfuron (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Forchlorfenuron (plant growth regulator) 

Carrots 499 0 0.005 NT

Eggplant 311 0 0.005 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 0.04

Orange Juice 499 0 0.001 NT

Appendix B. Page 61 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Radishes 689 0 0.002 NT

Summer Squash 176 1 0.6 0.001 0.001 V-1 NT

Sweet Bell Peppers 675 0 0.002 NT

Tangerines 687 0 0.001 NT

Tomato Paste 477 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 5,044 1

Formetanate hydrochloride (insecticide) 

Apple Juice 724 0 0.010 0.50

Carrots 499 0 0.010 NT

Eggplant 311 0 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 1.5

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.010 NT

Tangerines 687 5 0.7 0.016 - 0.13 0.005 X-2 0.03

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 NT

TOTAL 5,710 5

Fosthiazate (nematicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 0.02

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Furalaxyl (fungicide) 

Green Beans 177 0 0.005 NT

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 1,732 0

Furathiocarb (insecticide) 

Radishes 689 0 0.010 NT

Sweet Bell Peppers 675 0 0.010 NT

TOTAL 1,364 0

Halosulfuron (herbicide) 

Carrots 499 0 0.050 NT

Eggplant 311 0 0.050 0.05

Kiwi Fruit 177 0 0.050 NT

Summer Squash 87 0 0.010 0.5

Tangerines 687 0 0.010 NT

Tomato Paste 216 0 0.010 0.05

TOTAL 1,977 0

Halosulfuron methyl 2 (herbicide) 

Apple Juice 724 0 0.004 0.05

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Appendix B. Page 62 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.001 0.5

Sweet Bell Peppers 675 0 0.010 0.05

Tomato Paste 290 0 0.001 0.05

Winter Squash 677 0 0.001 0.5

TOTAL 3,820 0

Heptenophos (insecticide, acaricide)

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Hexaconazole (fungicide) 

Green Beans 177 0 0.005 NT

Orange Juice 499 0 0.005 NT

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.005 NT

Sweet Bell Peppers 675 0 0.010 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 3,096 0

Hexazinone (herbicide) 

Carrots 499 0 0.005 NT

Eggplant 311 0 0.005 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 2,719 0

Hexythiazox (insecticide, acaricide)

Apple Juice 724 0 0.002 0.4

Blueberries, Cultivated, Fresh 168 0 0.002 6

Blueberries, Frozen 7 0 0.002 6

Broccoli 675 0 0.006 NT

Cantaloupe 694 0 0.002 NT

Carrots 499 0 0.015 NT

Cauliflower 692 1 0.1 0.003 0.002 V-1 NT

Collard Greens 514 0 0.002 NT

Eggplant 661 0 0.006 - 0.015 1.5

Green Beans 177 0 0.001 0.3

Kiwi Fruit 177 0 0.015 NT

Orange Juice 499 0 0.001 0.6

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.001 - 0.005 NT

Sweet Bell Peppers 675 0 0.010 1.5

Tangerines 626 0 0.010 0.6

Tomato Paste 506 0 0.001 - 0.010 0.50

Winter Squash 677 0 0.001 NT

TOTAL 8,836 1

Appendix B. Page 63 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Hydroprene (insect growth regulator) 

Apple Juice 724 0 0.008 0.2

Bananas 703 0 0.008 0.2

Broccoli 675 0 0.005 0.2

Carrots 499 0 0.015 0.2

Cauliflower 692 0 0.002 0.2

Eggplant 661 0 0.002 - 0.015 0.2

Green Beans 177 0 0.003 0.2

Kiwi Fruit 177 0 0.015 0.2

Orange Juice 499 0 0.003 0.2

Summer Squash 176 0 0.003 - 0.005 0.2

Tangerines 687 0 0.005 0.2

Tomato Paste 506 0 0.003 - 0.005 0.2

Winter Squash 677 0 0.003 0.2

TOTAL 6,853 0

3-Hydroxycarbofuran (metabolite of Carbofuran)

Apple Juice 724 0 0.008 NT

Bananas 703 0 0.008 0.1

Blueberries, Cultivated, Fresh 168 1 0.6 0.004 0.003 V-1 NT

Blueberries, Frozen 7 0 0.003 NT

Cantaloupe 694 0 0.003 NT

Carrots 499 0 0.005 NT

Cauliflower 670 0 0.004 NT

Collard Greens 514 0 0.003 NT

Eggplant 661 0 0.004 - 0.005 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.001 - 0.005 NT

Sweet Bell Peppers 675 0 0.010 NT

Tangerines 687 0 0.020 NT

Tomato Paste 506 0 0.001 - 0.020 NT

Winter Squash 677 0 0.001 NT

TOTAL 8,903 1

5-Hydroxythiabendazole (metabolite of Thiabendazole)

Carrots 499 0 0.005 10.0

Green Beans 177 0 0.001 0.02

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 7 1.4 0.001 - 0.005 0.001 10.0

Summer Squash 89 0 0.001 0.02

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 0.02

TOTAL 2,408 7

Hydroxy Acequinocyl (metabolite of Acequinocyl)

Green Beans 177 0 0.001 0.25

Summer Squash 89 0 0.001 0.30

Winter Squash 62 0 0.001 0.30

TOTAL 328 0

Imazalil (fungicide) 

Bananas 703 26 3.7 0.007 - 0.070 0.004 3.0

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Appendix B. Page 64 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Broccoli 675 0 0.001 NT

Cantaloupe 694 0 0.010 NT

Carrots 499 0 0.005 NT

Cauliflower 692 0 0.001 - 0.003 NT

Collard Greens 514 0 0.010 NT

Eggplant 661 2 0.3 0.002 0.001 - 0.005 V-2 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 96 19.2 0.003 - 0.085 0.003 10.0

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.003 - 0.005 NT

Sweet Bell Peppers 675 0 0.010 NT

Tangerines 687 641 93.3 0.005 - 1.3 0.005 10.0

Tomato Paste 506 0 0.003 - 0.005 NT

Winter Squash 677 1 0.1 0.007 0.003 V-1 NT

TOTAL 8,876 766

Imazethapyr (herbicide) 

Blueberries, Cultivated, Fresh 168 0 0.020 NT

Blueberries, Frozen 7 0 0.020 NT

Cantaloupe 694 0 0.020 NT

Collard Greens 514 0 0.020 NT

TOTAL 1,383 0

Imazosulfuron (herbicide) 

Carrots 499 0 0.025 NT

Eggplant 311 0 0.025 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.025 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 0.02

Winter Squash 677 0 0.003 NT

TOTAL 2,719 0

Imidacloprid (insecticide) 

Apple Juice 724 0 0.020 0.5

Bananas 703 0 0.020 0.50

Blueberries, Cultivated, Fresh 168 21 12.5 0.003 - 0.18 0.003 3.5

Blueberries, Frozen 7 3 42.9 0.012 - 0.038 0.003 3.5

Broccoli 675 120 17.8 0.003 - 0.12 0.003 - 0.006 3.5

Cantaloupe 694 159 22.9 0.003 - 0.18 0.003 0.5

Carrots 499 1 0.2 0.024 0.020 0.40

Cauliflower 692 134 19.4 0.003 - 0.059 0.003 3.5

Collard Greens 514 153 29.8 0.003 - 0.34 0.003 3.5

Eggplant 661 188 28.4 0.002 - 0.13 0.001 - 0.020 1.0

Green Beans 177 6 3.4 0.005 - 0.042 0.003 4.0

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 5 1 0.003 - 0.013 0.003 0.70

Radishes 689 16 2.3 0.011 - 0.099 0.010 0.40

Summer Squash 176 80 45.5 0.003 - 0.14 0.003 - 0.010 0.5

Sweet Bell Peppers 675 145 21.5 0.010 - 1.6 0.010 X-1 1.0

Tangerines 687 17 2.5 0.010 - 0.044 0.010 0.70

Tomato Paste 506 203 40.1 0.003 - 0.024 0.003 - 0.010 6.0

Winter Squash 677 234 34.6 0.003 - 0.20 0.003 0.5

TOTAL 9,600 1,485

Appendix B. Page 65 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Imidacloprid desnitro (metabolite of Imidacloprid)

Green Beans 177 17 9.6 0.001 - 0.014 0.001 4.0

Summer Squash 89 44 49.4 0.001 - 0.012 0.001 0.5

Winter Squash 62 18 29 0.001 - 0.007 0.001 0.5

TOTAL 328 79

Imidacloprid urea (metabolite of Imidacloprid)

Apple Juice 724 0 0.012 0.5

Carrots 499 0 0.015 0.40

Eggplant 311 0 0.015 1.0

Green Beans 177 3 1.7 0.002 - 0.008 0.001 4.0

Kiwi Fruit 177 0 0.015 NT

Orange Juice 499 0 0.001 0.70

Summer Squash 89 8 9 0.002 - 0.004 0.001 0.5

Tomato Paste 290 0 0.001 6.0

Winter Squash 677 16 2.4 0.001 - 0.006 0.001 0.5

TOTAL 3,443 27

Imiprothrin (insecticide) 

Apple Juice 724 0 0.015 NT

Bananas 703 0 0.015 NT

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Cantaloupe 694 0 0.010 NT

Carrots 499 0 0.045 NT

Collard Greens 514 0 0.010 NT

Eggplant 311 0 0.045 NT

Green Beans 177 0 0.010 NT

Kiwi Fruit 177 0 0.095 NT

Orange Juice 499 0 0.010 NT

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.010 - 0.10 NT

Sweet Bell Peppers 675 0 0.010 NT

Tangerines 687 0 0.40 NT

Tomato Paste 506 0 0.010 - 0.40 NT

Winter Squash 677 0 0.010 NT

TOTAL 7,883 0

Indaziflam (herbicide) 

Apple Juice 724 0 0.001 0.01

Bananas 703 0 0.001 0.01

Blueberries, Cultivated, Fresh 168 0 0.001 0.01

Blueberries, Frozen 7 0 0.001 0.01

Cantaloupe 694 0 0.001 NT

Collard Greens 514 0 0.001 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 0.01

Summer Squash 176 0 0.001 NT

Tangerines 687 1 0.1 0.002 0.001 0.01

Tomato Paste 506 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 5,532 1

Indoxacarb (insecticide) 

Apple Juice 724 0 0.005 1.0

Blueberries, Cultivated, Fresh 168 0 0.020 1.5

Blueberries, Frozen 7 0 0.020 1.5

Appendix B. Page 66 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cantaloupe 694 0 0.020 0.60

Carrots 499 0 0.025 NT

Collard Greens 514 53 10.3 0.020 - 0.92 0.020 12

Eggplant 311 0 0.025 0.50

Green Beans 177 0 0.005 0.9

Kiwi Fruit 177 0 0.025 NT

Orange Juice 499 0 0.005 NT

Radishes 689 1 0.1 0.013 0.010 V-1 NT

Summer Squash 176 0 0.005 - 0.050 0.60

Sweet Bell Peppers 675 12 1.8 0.011 - 0.11 0.010 0.50

Tangerines 687 0 0.050 NT

Tomato Paste 506 3 0.6 0.007 - 0.009 0.005 - 0.050 0.50

Winter Squash 677 0 0.005 0.60

TOTAL 7,180 69

Ipconazole (fungicide) 

Carrots 499 0 0.005 NT

Eggplant 311 0 0.005 NT

Green Beans 177 0 0.003 0.01

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.003 NT

Summer Squash 176 0 0.003 - 0.010 NT

Tangerines 687 0 0.010 NT

Tomato Paste 506 0 0.003 - 0.010 NT

Winter Squash 677 0 0.003 NT

TOTAL 3,709 0

Iprobenfos - IBP (fungicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Iprodione (fungicide) 

Blueberries, Cultivated, Fresh 168 10 6 0.054 - 1.4 0.040 15.0

Blueberries, Frozen 7 1 14.3 0.094 0.040 15.0

Broccoli 675 0 0.009 25.0

Cantaloupe 694 0 0.040 NT

Carrots 499 64 12.8 0.015 - 0.087 0.015 5.0

Cauliflower 664 0 0.009 NT

Collard Greens 514 0 0.040 NT

Eggplant 630 0 0.015 - 0.030 NT

Green Beans 177 1 0.6 0.15 0.003 2.0

Kiwi Fruit 177 0 0.025 10.0

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.003 - 0.075 NT

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 0 0.075 NT

Tomato Paste 506 0 0.003 - 0.075 NT

Winter Squash 677 0 0.003 NT

TOTAL 8,114 76

Iprovalicarb (fungicide) 

Carrots 499 0 0.010 NT

Eggplant 311 0 0.010 NT

Appendix B. Page 67 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.003 NT

Summer Squash 176 0 0.003 - 0.005 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.003 - 0.005 1.0

Winter Squash 677 0 0.003 NT

TOTAL 3,709 0

Isocarbophos (insecticide) 

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 1,732 0

Isofenphos (insecticide) 

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.003 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 3,096 0

Isofenphos methyl (metabolite if Isofenphos)

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Isofetamid (fungicide) 

Apple Juice 724 0 0.001 0.60

Summer Squash 87 0 0.001 NT

Tangerines 687 0 0.002 NT

Tomato Paste 216 0 0.002 NT

TOTAL 1,714 0

Isoprocarb (insecticide) 

Green Beans 177 0 0.005 NT

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 1,732 0

Isopropalin (herbicide) 

Green Beans 177 0 0.010 NT

Orange Juice 499 0 0.010 NT

Summer Squash 89 0 0.010 NT

Tomato Paste 290 0 0.010 NT

Winter Squash 677 0 0.010 NT

TOTAL 1,732 0

Appendix B. Page 68 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Isoprothiolane (fungicide) 

Green Beans 177 4 2.3 0.001 - 0.002 0.001 V-4 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 3,096 4

Isoproturon (herbicide) 

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 1,732 0

Isopyrazam (fungicide) 

Bananas 703 0 0.003 0.05

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 176 0 0.001 - 0.005 NT

Tangerines 687 1 0.1 0.006 0.005 V-1 NT

Tomato Paste 506 0 0.001 - 0.005 0.50

Winter Squash 677 0 0.001 NT

TOTAL 3,425 1

Isoxaben (herbicide) 

Apple Juice 724 0 0.001 0.01

TOTAL 724 0

Isoxadifen ethyl (herbicide safener) 

Carrots 499 0 0.005 NT

Eggplant 311 0 0.005 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Summer Squash 176 0 0.001 - 0.005 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 NT

TOTAL 3,709 0

Kinoprene (insecticide) 

Carrots 499 0 0.10 NT

Eggplant 311 0 0.10 NT

Kiwi Fruit 177 0 0.10 NT

TOTAL 987 0

Kresoxim-methyl (fungicide) 

Apple Juice 724 0 0.009 0.5

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Broccoli 675 0 0.002 NT

Cantaloupe 694 0 0.010 0.40

Carrots 499 0 0.015 NT

Appendix B. Page 69 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cauliflower 692 0 0.002 NT

Collard Greens 514 0 0.010 NT

Eggplant 661 0 0.002 - 0.015 NT

Green Beans 177 0 0.005 NT

Kiwi Fruit 177 0 0.015 NT

Orange Juice 499 0 0.005 NT

Summer Squash 176 0 0.005 0.40

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.005 NT

Winter Squash 677 0 0.005 0.40

TOTAL 7,533 0

Lactofen (herbicide) 

Green Beans 177 0 0.003 0.01

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 0.02

Winter Squash 677 0 0.003 NT

TOTAL 1,732 0

Lenacil (herbicide) 

Radishes 689 0 0.005 NT

Sweet Bell Peppers 675 0 0.005 NT

TOTAL 1,364 0

Leptophos oxygen analog (insecticide metabolite)

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 1,732 0

Linuron (herbicide) 

Blueberries, Cultivated, Fresh 168 0 0.008 NT

Blueberries, Frozen 7 0 0.008 NT

Broccoli 675 1 0.1 0.010 0.002 V-1 NT

Cantaloupe 694 0 0.008 NT

Carrots 499 158 31.7 0.010 - 0.17 0.010 1.0

Cauliflower 692 0 0.002 NT

Collard Greens 514 5 1 0.009 - 0.023 0.008 V-5 NT

Eggplant 661 0 0.002 - 0.010 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.019 NT

Summer Squash 176 0 0.003 - 0.010 NT

Sweet Bell Peppers 675 0 0.019 NT

Tangerines 687 0 0.010 NT

Tomato Paste 506 0 0.003 - 0.010 NT

Winter Squash 677 1 0.1 0.003 0.003 V-1 NT

TOTAL 8,173 165

Lufenuron (insecticide) 

Carrots 499 0 0.010 NT

Eggplant 311 0 0.010 NT

Kiwi Fruit 177 0 0.010 NT

TOTAL 987 0

Appendix B. Page 70 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Malathion (insecticide) 

Apple Juice 724 0 0.004 8

Blueberries, Cultivated, Fresh 168 3 1.8 0.005 - 0.012 0.002 8

Blueberries, Frozen 7 5 71.4 0.004 - 0.057 0.002 8

Broccoli 675 1 0.1 0.002 0.001 8

Cantaloupe 694 0 0.002 8

Carrots 499 0 0.005 8

Cauliflower 692 0 0.001 8

Collard Greens 514 2 0.4 0.002 - 0.007 0.002 8

Eggplant 661 14 2.1 0.002 - 0.010 0.001 - 0.005 8

Green Beans 177 0 0.003 8

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.003 8

Radishes 689 0 0.010 8

Summer Squash 176 0 0.003 - 0.010 8

Sweet Bell Peppers 675 2 0.3 0.027 - 0.035 0.010 8

Tangerines 687 0 0.010 8

Tomato Paste 506 0 0.003 - 0.010 8

Winter Squash 677 0 0.003 8

TOTAL 8,897 27

Malathion oxygen analog (metabolite of Malathion)

Apple Juice 724 0 0.010 8

Blueberries, Cultivated, Fresh 110 0 0.002 8

Blueberries, Frozen 6 1 16.7 0.003 0.002 8

Broccoli 675 0 0.002 8

Cantaloupe 693 1 0.1 0.007 0.002 8

Carrots 499 0 0.005 8

Cauliflower 692 0 0.002 8

Collard Greens 514 0 0.002 8

Eggplant 661 0 0.002 - 0.005 8

Green Beans 177 0 0.001 8

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 8

Radishes 689 0 0.010 8

Summer Squash 176 0 0.001 - 0.002 8

Sweet Bell Peppers 675 0 0.010 8

Tangerines 687 0 0.002 8

Tomato Paste 506 0 0.001 - 0.002 8

Winter Squash 677 0 0.001 8

TOTAL 8,837 2

Mandipropamid (fungicide) 

Blueberries, Cultivated, Fresh 168 0 0.002 NT

Blueberries, Frozen 7 0 0.002 NT

Broccoli 675 13 1.9 0.005 - 0.13 0.003 3.0

Cantaloupe 694 0 0.002 0.6

Carrots 499 0 0.020 NT

Cauliflower 692 0 0.003 3.0

Collard Greens 514 75 14.6 0.002 - 2.1 0.002 25

Eggplant 661 1 0.2 0.032 0.003 - 0.020 1.0

Green Beans 177 0 0.003 0.90

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 0 0.003 0.50

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.003 - 0.005 0.6

Appendix B. Page 71 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Sweet Bell Peppers 675 11 1.6 0.005 - 0.030 0.005 1.0

Tangerines 687 0 0.005 0.50

Tomato Paste 506 0 0.003 - 0.005 1.0

Winter Squash 677 2 0.3 0.004 - 0.007 0.003 0.6

TOTAL 8,173 102

Mecarbam (insecticide, acaricide)

Green Beans 177 0 0.005 NT

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 1,732 0

Mefenacet (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 3,096 0

Mefenpyr diethyl (herbicide safener) 

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 1,732 0

Mepanipyrim (fungicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 0.5

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Mephosfolan (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Mepronil (fungicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Appendix B. Page 72 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Mesotrione (herbicide) 

Apple Juice 724 0 0.040 0.01

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 0 0.020 0.01

Summer Squash 87 0 0.050 NT

Tangerines 687 0 0.050 0.01

Tomato Paste 216 0 0.050 NT

TOTAL 2,390 0

Metaflumizone (insecticide) 

Apple Juice 724 0 0.020 0.04

Carrots 499 0 0.010 NT

Eggplant 311 0 0.010 1.5

Green Beans 177 0 0.010 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.010 0.04

Summer Squash 176 0 0.005 - 0.010 NT

Tangerines 687 0 0.005 0.04

Tomato Paste 506 0 0.005 - 0.010 1.2

Winter Squash 677 0 0.010 NT

TOTAL 4,433 0

Metalaxyl/Mefenoxam 3 (fungicide) 

Apple Juice 724 0 0.002 0.2

Blueberries, Cultivated, Fresh 168 6 3.6 0.001 - 0.021 0.001 2.0

Blueberries, Frozen 7 0 0.001 2.0

Broccoli 675 12 1.8 0.002 - 0.006 0.001 2.0

Cantaloupe 694 93 13.4 0.001 - 0.041 0.001 1.0

Carrots 499 0 0.015 0.5

Cauliflower 692 5 0.7 0.002 - 0.027 0.001 1.0

Collard Greens 514 38 7.4 0.001 - 0.15 0.001 0.1

Eggplant 661 7 1.1 0.002 - 0.005 0.001 - 0.015 1.0

Green Beans 177 20 11.3 0.001 - 0.020 0.001 0.2

Kiwi Fruit 177 0 0.030 0.10

Orange Juice 499 0 0.001 1.0

Radishes 689 25 3.6 0.006 - 0.071 0.005 0.5

Summer Squash 176 14 8 0.001 - 0.031 0.001 - 0.010 1.0

Sweet Bell Peppers 675 121 17.9 0.005 - 0.23 0.005 1.0

Tangerines 687 0 0.010 1.0

Tomato Paste 506 18 3.6 0.002 - 0.014 0.001 - 0.010 3.0

Winter Squash 677 37 5.5 0.001 - 0.17 0.001 1.0

TOTAL 8,897 396

Metaldehyde (molluscicide) 

Carrots 499 0 0.055 NT

Eggplant 311 0 0.055 NT

Kiwi Fruit 177 0 0.11 NT

TOTAL 987 0

Metamitron (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Appendix B. Page 73 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Metconazole (fungicide) 

Bananas 703 0 0.002 0.1

Carrots 499 0 0.010 NT

Eggplant 311 0 0.010 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 3,422 0

Methacrifos (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Methamidophos (insecticide) (also a metabolite of Acephate)

Apple Juice 724 0 0.025 0.02

Bananas 703 0 0.025 0.02

Blueberries, Cultivated, Fresh 168 0 0.005 0.02

Blueberries, Frozen 7 0 0.005 0.02

Cantaloupe 694 0 0.005 0.02

Carrots 499 0 0.035 0.02

Cauliflower 692 8 1.2 0.006 - 0.024 0.004 0.5

Collard Greens 514 1 0.2 0.010 0.005 0.02

Eggplant 661 0 0.001 - 0.035 0.02

Green Beans 177 11 6.2 0.002 - 1.1 0.001 X-6 0.02

Kiwi Fruit 177 0 0.035 0.02

Orange Juice 499 0 0.001 0.02

Radishes 689 2 0.3 0.011 - 0.018 0.010 0.02

Summer Squash 176 0 0.001 - 0.020 0.02

Sweet Bell Peppers 675 31 4.6 0.010 - 0.23 0.010 1

Tangerines 687 0 0.10 0.02

Tomato Paste 506 0 0.001 - 0.10 0.02

Winter Squash 677 1 0.1 0.013 0.001 0.02

TOTAL 8,925 54

Methfuroxam (fungicide) 

Orange Juice 499 0 0.001 NT

Summer Squash 55 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 594 0 0.001 NT

TOTAL 1,438 0

Methidathion (insecticide) 

Apple Juice 724 0 0.003 0.05

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Broccoli 675 0 0.001 NT

Cantaloupe 694 0 0.010 NT

Carrots 499 0 0.015 NT

Cauliflower 692 0 0.001 NT

Collard Greens 514 0 0.010 NT

Appendix B. Page 74 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Eggplant 661 0 0.001 - 0.015 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.015 0.1

Orange Juice 499 0 0.003 4.0

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.003 NT

Sweet Bell Peppers 675 0 0.010 NT

Tangerines 687 0 0.002 6.0

Tomato Paste 506 0 0.002 - 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 8,810 0

Methiocarb (insecticide)

Broccoli 675 0 0.001 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.001 NT

Eggplant 661 0 0.001 - 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.010 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 5,800 0

Methiocarb sulfone (metabolite of Methiocarb)

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 1,732 0

Methiocarb sulfoxide (metabolite of Methiocarb)

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Methomyl (insecticide) 

Apple Juice 724 0 0.008 1

Blueberries, Cultivated, Fresh 168 0 0.030 6

Blueberries, Frozen 7 0 0.030 6

Broccoli 675 3 0.4 0.009 - 0.035 0.008 3

Cantaloupe 694 0 0.030 0.2

Carrots 499 0 0.015 0.2

Cauliflower 692 9 1.3 0.010 - 0.048 0.008 2

Collard Greens 486 7 1.4 0.038 - 4.3 0.030 6

Eggplant 661 10 1.5 0.022 - 0.13 0.002 - 0.015 0.2

Green Beans 177 9 5.1 0.017 - 0.45 0.010 2

Kiwi Fruit 177 0 0.015 NT

Orange Juice 499 0 0.010 2

Radishes 689 2 0.3 0.014 - 0.039 0.010 0.2

Appendix B. Page 75 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Summer Squash 176 3 1.7 0.011 - 0.029 0.005 - 0.010 0.2

Sweet Bell Peppers 675 34 5 0.011 - 0.20 0.010 2

Tangerines 687 1 0.1 0.013 0.010 2

Tomato Paste 506 0 0.010 1

Winter Squash 677 0 0.010 0.2

TOTAL 8,869 78

Methomyl oxime (insecticide metabolite)

Apple Juice 724 0 0.035 1

Carrots 499 0 0.10 0.2

Eggplant 311 0 0.10 0.2

Summer Squash 87 0 0.10 0.2

Tangerines 687 0 0.10 2

Tomato Paste 216 0 0.10 1

TOTAL 2,524 0

Methoprene (insect growth regulator) 

Broccoli 675 0 0.015 EX3

Carrots 499 0 0.060 EX3

Cauliflower 692 0 0.050 EX3

Eggplant 661 0 0.050 - 0.060 EX3

Kiwi Fruit 177 0 0.060 EX3

TOTAL 2,704 0

Methoprotryne (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Methoxychlor (insecticide) 

Broccoli 675 0 0.003 - 0.006 NT

Carrots 499 0 0.020 NT

Cauliflower 692 0 0.003 NT

Eggplant 648 0 0.003 - 0.020 NT

Kiwi Fruit 177 0 0.040 NT

Summer Squash 55 0 0.001 NT

Winter Squash 62 0 0.001 NT

TOTAL 2,808 0

Methoxychlor olefin (metabolite of Methoxychlor)

Broccoli 675 0 0.001 NT

Cauliflower 692 0 0.001 NT

Eggplant 350 0 0.001 NT

TOTAL 1,717 0

Methoxychlor p,p' (isomer of Methoxychlor)

Green Beans 92 0 0.001 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 34 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 615 0 0.001 NT

TOTAL 2,894 0

Appendix B. Page 76 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Methoxyfenozide (insecticide) 

Apple Juice 724 19 2.6 0.002 - 0.009 0.001 2.0

Blueberries, Cultivated, Fresh 168 2 1.2 0.004 - 0.016 0.003 3.0

Blueberries, Frozen 7 0 0.003 3.0

Broccoli 675 8 1.2 0.002 - 0.12 0.001 - 0.003 7.0

Cantaloupe 694 0 0.003 0.3

Carrots 499 0 0.020 0.90

Cauliflower 692 1 0.1 0.002 0.001 7.0

Collard Greens 514 66 12.8 0.003 - 5.7 0.003 30

Eggplant 661 8 1.2 0.005 - 0.017 0.003 - 0.020 2.0

Green Beans 177 12 6.8 0.003 - 0.098 0.003 1.5

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.003 3.0

Radishes 689 9 1.3 0.021 - 0.17 0.010 0.90

Summer Squash 176 1 0.6 0.004 0.002 - 0.003 0.3

Sweet Bell Peppers 675 28 4.1 0.010 - 0.065 0.010 2.0

Tangerines 687 0 0.010 3.0

Tomato Paste 506 77 15.2 0.003 - 0.019 0.003 - 0.010 2.0

Winter Squash 677 15 2.2 0.003 - 0.026 0.003 0.3

TOTAL 8,897 246

Metobromuron (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Metolachlor (herbicide) 

Blueberries, Cultivated, Fresh 168 0 0.001 0.40

Blueberries, Frozen 7 0 0.001 0.40

Broccoli 675 1 0.1 0.002 0.001 0.60

Cantaloupe 694 0 0.001 0.50

Carrots 499 0 0.010 0.40

Cauliflower 692 0 0.001 0.60

Collard Greens 514 0 0.001 1.8

Eggplant 661 0 0.001 - 0.010 0.10

Green Beans 177 0 0.001 0.30

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 0.30

Summer Squash 176 0 0.001 - 0.005 0.50

Sweet Bell Peppers 675 0 0.005 0.10

Tangerines 687 0 0.005 NT

Tomato Paste 506 12 2.4 0.001 - 0.002 0.001 - 0.005 0.30

Winter Squash 677 0 0.001 0.50

TOTAL 8,173 13

Metolachlor oxanilic acid (OA) (herbicide metabolite)

Summer Squash 87 0 0.050 0.50

Tangerines 687 0 0.050 NT

Tomato Paste 216 0 0.050 0.30

TOTAL 990 0

Appendix B. Page 77 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Metolcarb (insecticide, acaricide)

Green Beans 177 0 0.010 NT

Orange Juice 499 0 0.010 NT

Summer Squash 89 0 0.010 NT

Tomato Paste 290 0 0.010 NT

Winter Squash 677 0 0.010 NT

TOTAL 1,732 0

Metoxuron (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Metrafenone (fungicide) 

Apple Juice 724 0 0.005 1.5

Carrots 499 0 0.005 NT

Eggplant 311 0 0.005 0.90

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.001 - 0.010 0.50

Sweet Bell Peppers 675 1 0.1 0.035 0.010 0.90

Tangerines 687 0 0.010 NT

Tomato Paste 506 2 0.4 0.001 - 0.002 0.001 - 0.010 0.90

Winter Squash 677 4 0.6 0.002 - 0.006 0.001 0.50

TOTAL 5,620 7

Metribuzin (herbicide) 

Blueberries, Cultivated, Fresh 168 0 0.005 NT

Blueberries, Frozen 7 0 0.005 NT

Broccoli 675 1 0.1 0.003 0.002 V-1 NT

Cantaloupe 694 0 0.005 NT

Carrots 499 0 0.020 0.3

Cauliflower 692 0 0.002 NT

Collard Greens 514 6 1.2 0.006 - 0.042 0.005 V-6 NT

Eggplant 661 0 0.002 - 0.020 NT

Green Beans 177 0 0.005 NT

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 NT

Tangerines 451 0 0.005 NT

Tomato Paste 427 0 0.005 0.1

Winter Squash 677 0 0.005 NT

TOTAL 6,407 7

Metsulfuron methyl (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 647 0 0.001 NT

TOTAL 1,702 0

Appendix B. Page 78 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Mevinphos (insecticide) 

Broccoli 675 0 0.002 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.002 NT

Eggplant 661 0 0.002 - 0.010 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.003 - 0.010 NT

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 0 0.010 NT

Tomato Paste 506 0 0.003 - 0.010 NT

Winter Squash 677 0 0.003 NT

TOTAL 6,790 0

Mexacarbate (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

MGK-264 (insecticide) 

Apple Juice 724 0 0.002 5

Bananas 703 0 0.002 5

Blueberries, Cultivated, Fresh 168 0 0.10 5

Blueberries, Frozen 7 0 0.10 5

Broccoli 675 0 0.002 5

Cantaloupe 694 0 0.10 5

Carrots 499 0 0.015 5

Cauliflower 692 0 0.002 5

Collard Greens 514 0 0.10 5

Eggplant 661 0 0.005 - 0.015 5

Green Beans 177 0 0.001 5

Kiwi Fruit 177 0 0.030 5

Orange Juice 499 0 0.001 5

Radishes 661 0 0.010 5

Summer Squash 176 0 0.001 - 0.025 5

Sweet Bell Peppers 675 0 0.010 5

Tangerines 687 0 0.025 5

Tomato Paste 506 0 0.001 - 0.025 5

Winter Squash 677 0 0.001 5

TOTAL 9,572 0

MGK-326 (insecticide) 

Carrots 499 0 0.015 NT

Eggplant 311 0 0.015 NT

TOTAL 810 0

Molinate (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Appendix B. Page 79 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Monocrotophos (insecticide) 

Carrots 499 0 0.020 NT

Eggplant 311 0 0.020 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.003 NT

Sweet Bell Peppers 675 0 0.010 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 4,083 0

Monolinuron (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Monuron (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Myclobutanil (fungicide) 

Apple Juice 724 0 0.004 0.5

Bananas 703 77 11 0.007 - 0.098 0.004 4.0

Blueberries, Cultivated, Fresh 168 3 1.8 0.005 - 0.093 0.003 V-3 NT

Blueberries, Frozen 7 0 0.003 NT

Broccoli 675 0 0.003 0.03

Cantaloupe 694 0 0.003 0.20

Carrots 499 16 3.2 0.002 - 0.024 0.001 0.03

Cauliflower 692 0 0.001 0.03

Collard Greens 514 0 0.003 0.03

Eggplant 661 0 0.001 - 0.003 4.0

Green Beans 177 5 2.8 0.003 - 0.068 0.003 1.0

Kiwi Fruit 177 0 0.001 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.005 0.03

Summer Squash 176 3 1.7 0.005 - 0.012 0.003 - 0.010 0.20

Sweet Bell Peppers 675 57 8.4 0.006 - 0.19 0.005 4.0

Tangerines 687 0 0.010 NT

Tomato Paste 506 11 2.2 0.003 - 0.007 0.003 - 0.010 1.0

Winter Squash 677 29 4.3 0.003 - 0.015 0.003 0.20

TOTAL 9,600 201

Naled (insecticide) 

Apple Juice 724 0 0.015 0.5

Bananas 703 0 0.015 0.5

Blueberries, Cultivated, Fresh 168 0 0.020 0.5

Blueberries, Frozen 7 0 0.020 0.5

Appendix B. Page 80 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Carrots 499 0 0.20 0.5

Eggplant 311 0 0.20 0.5

TOTAL 2,412 0

1-Naphthol (metabolite of Carbaryl)

Apple Juice 724 0 0.35 12

Bananas 703 0 0.35 5.0

Blueberries, Cultivated, Fresh 168 0 0.015 3.0

Blueberries, Frozen 7 0 0.015 3.0

Cantaloupe 368 0 0.015 3.0

Carrots 499 0 0.20 2.0

Collard Greens 514 0 0.015 10

Eggplant 311 0 0.20 5.0

TOTAL 3,294 0

Napropamide (herbicide) 

Broccoli 675 1 0.1 0.079 0.002 0.1

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.002 0.1

Eggplant 661 0 0.002 - 0.010 0.1

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.020 0.1

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.001 NT

Sweet Bell Peppers 675 0 0.010 0.1

Tangerines 687 0 0.001 NT

Tomato Paste 506 0 0.001 0.1

Winter Squash 677 0 0.001 NT

TOTAL 6,790 1

Neburon (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Nicosulfuron (herbicide) 

Green Beans 127 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 121 0 0.001 - 0.005 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 615 0 0.001 NT

TOTAL 2,555 0

Nitenpyram (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Appendix B. Page 81 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Nitrapyrin (nitrification inhibitor) 

Green Beans 94 0 0.001 - 0.003 NT

Orange Juice 499 0 0.001 0.06

Summer Squash 176 0 0.001 - 0.005 NT

Tangerines 687 0 0.005 0.06

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 - 0.003 NT

TOTAL 2,639 0

Nitrofen (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Norflurazon (herbicide) 

Apple Juice 724 0 0.030 0.1

Blueberries, Cultivated, Fresh 168 0 0.002 0.2

Blueberries, Frozen 7 0 0.002 0.2

Broccoli 675 0 0.001 NT

Cantaloupe 694 0 0.002 NT

Carrots 499 0 0.005 NT

Cauliflower 692 0 0.001 NT

Collard Greens 514 0 0.002 NT

Eggplant 661 0 0.001 - 0.005 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.003 0.2

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.003 - 0.010 NT

Sweet Bell Peppers 675 0 0.010 NT

Tangerines 687 0 0.010 0.2

Tomato Paste 506 0 0.003 - 0.010 NT

Winter Squash 677 0 0.003 NT

TOTAL 8,897 0

Norflurazon desmethyl (metabolite of Norflurazon)

Apple Juice 724 0 0.020 0.1

Blueberries, Cultivated, Fresh 168 0 0.005 0.2

Blueberries, Frozen 7 0 0.005 0.2

Broccoli 675 1 0.1 0.002 0.001 V-1 NT

Cantaloupe 694 0 0.005 NT

Carrots 499 0 0.010 NT

Cauliflower 692 1 0.1 0.002 0.001 V-1 NT

Collard Greens 514 0 0.005 NT

Eggplant 661 0 0.001 - 0.010 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.003 0.2

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.003 NT

Sweet Bell Peppers 675 0 0.010 NT

Tangerines 657 0 0.005 0.2

Appendix B. Page 82 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomato Paste 506 0 0.003 - 0.005 NT

Winter Squash 677 0 0.003 NT

TOTAL 8,780 2

Novaluron (insecticide) 

Apple Juice 724 0 0.003 3.0

Bananas 703 0 0.003 0.01

Blueberries, Cultivated, Fresh 168 1 0.6 0.072 0.009 7.0

Blueberries, Frozen 7 0 0.009 7.0

Broccoli 675 11 1.6 0.002 - 0.023 0.001 0.7

Cantaloupe 694 0 0.009 0.20

Carrots 499 0 0.010 0.05

Cauliflower 692 0 0.001 0.7

Collard Greens 514 3 0.6 0.016 - 0.23 0.009 25

Eggplant 648 4 0.6 0.002 - 0.037 0.001 - 0.010 2

Green Beans 177 4 2.3 0.007 - 0.011 0.001 - 0.003 0.70

Kiwi Fruit 177 0 0.010 0.01

Orange Juice 499 0 0.001 0.01

Radishes 689 0 0.010 0.01

Summer Squash 176 1 0.6 0.006 0.001 - 0.005 0.20

Sweet Bell Peppers 675 52 7.7 0.010 - 0.092 0.010 2

Tangerines 687 0 0.025 0.01

Tomato Paste 506 14 2.8 0.001 - 0.005 0.001 - 0.025 2

Winter Squash 677 21 3.1 0.001 - 0.030 0.001 - 0.003 0.20

TOTAL 9,587 111

Nuarimol (fungicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Octhilinone (fungicide) 

Green Beans 146 0 0.001 - 0.005 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 - 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 642 0 0.001 - 0.005 NT

TOTAL 1,666 0

Omethoate (insecticide) (also a metabolite of Dimethoate)

Blueberries, Cultivated, Fresh 168 2 1.2 0.023 - 0.030 0.020 1.0

Blueberries, Frozen 7 0 0.020 1.0

Broccoli 675 3 0.4 0.022 - 0.11 0.002 2.0

Cantaloupe 694 0 0.020 1.0

Carrots 499 0 0.010 NT

Cauliflower 692 1 0.1 0.004 0.002 2.0

Collard Greens 514 0 0.020 NT

Eggplant 661 0 0.002 - 0.010 NT

Green Beans 177 4 2.3 0.003 - 0.035 0.001 2.0

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 2.0

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.001 - 0.015 NT

Sweet Bell Peppers 656 5 0.8 0.016 - 0.039 0.010 2.0

Appendix B. Page 83 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tangerines 687 0 0.030 2.0

Tomato Paste 506 0 0.001 - 0.030 2.0

Winter Squash 677 0 0.001 NT

TOTAL 8,154 15

Orthosulfamuron (herbicide) 

Green Beans 92 0 0.003 NT

Orange Juice 425 0 0.003 NT

Tomato Paste 225 0 0.003 NT

Winter Squash 420 0 0.003 NT

TOTAL 1,162 0

Oryzalin (herbicide) 

Apple Juice 724 0 0.012 0.05

Blueberries, Cultivated, Fresh 168 0 0.020 0.05

Blueberries, Frozen 7 0 0.020 0.05

Cantaloupe 694 0 0.020 NT

Carrots 499 0 0.10 NT

Collard Greens 514 0 0.020 NT

Eggplant 311 0 0.10 NT

Kiwi Fruit 177 0 0.10 0.05

Radishes 689 0 0.020 NT

Sweet Bell Peppers 675 0 0.10 NT

Tangerines 687 0 0.20 0.05

Tomato Paste 216 0 0.20 NT

TOTAL 5,361 0

Oxadiazon (herbicide) 

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Cantaloupe 694 0 0.010 NT

Collard Greens 514 0 0.010 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 3,115 0

Oxadixyl (fungicide) 

Broccoli 675 0 0.003 NT

Cauliflower 692 0 0.003 NT

Eggplant 350 0 0.003 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.010 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,813 0

Oxamyl (insecticide) 

Apple Juice 724 0 0.015 2

Bananas 703 0 0.015 0.3

Blueberries, Cultivated, Fresh 168 0 0.003 NT

Blueberries, Frozen 7 0 0.003 NT

Appendix B. Page 84 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cantaloupe 694 3 0.4 0.006 - 0.018 0.003 2.0

Carrots 499 0 0.005 0.1

Cauliflower 692 0 0.006 NT

Collard Greens 514 3 0.6 0.011 - 0.96 0.003 V-3 NT

Eggplant 311 7 2.3 0.009 - 0.042 0.005 2.0

Green Beans 177 0 0.005 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.005 3

Radishes 689 0 0.010 NT

Summer Squash 176 4 2.3 0.006 - 0.060 0.005 2.0

Sweet Bell Peppers 675 36 5.3 0.010 - 1.2 0.010 2.0

Tangerines 687 0 0.005 3

Tomato Paste 506 0 0.005 2

Winter Squash 677 1 0.1 0.029 0.005 2.0

TOTAL 8,575 54

Oxamyl oxime (metabolite of Oxamyl)

Apple Juice 724 0 0.060 2

Bananas 703 0 0.060 0.3

Blueberries, Cultivated, Fresh 168 0 0.007 NT

Blueberries, Frozen 7 0 0.007 NT

Cantaloupe 694 41 5.9 0.007 - 1.4 0.007 2.0

Carrots 499 0 0.040 0.1

Collard Greens 514 1 0.2 0.052 0.007 V-1 NT

Eggplant 311 7 2.3 0.045 - 0.12 0.040 2.0

Green Beans 177 0 0.005 NT

Kiwi Fruit 177 0 0.040 NT

Orange Juice 499 0 0.005 3

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.005 - 0.050 2.0

Sweet Bell Peppers 675 150 22.2 0.010 - 0.48 0.010 2.0

Tangerines 687 0 0.050 3

Tomato Paste 506 0 0.005 - 0.050 2

Winter Squash 677 3 0.4 0.005 - 0.013 0.005 2.0

TOTAL 7,883 202

Oxathiapiprolin (fungicide) 

Apple Juice 724 0 0.003 0.10

Carrots 499 0 0.020 0.10

Eggplant 311 0 0.020 0.50

Green Beans 177 0 0.001 0.10

Orange Juice 499 0 0.001 0.06

Summer Squash 176 0 0.001 - 0.010 0.20

Tangerines 687 0 0.010 0.06

Tomato Paste 506 0 0.001 - 0.010 0.50

Winter Squash 677 1 0.1 0.003 0.001 0.20

TOTAL 4,256 1

Oxycarboxin (fungicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Appendix B. Page 85 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Oxydemeton methyl (insecticide) 

Blueberries, Cultivated, Fresh 168 0 0.002 NT

Blueberries, Frozen 7 0 0.002 NT

Cantaloupe 693 0 0.002 0.2

Carrots 499 0 0.005 NT

Collard Greens 514 0 0.002 NT

Eggplant 311 0 0.005 1.0

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 1.0

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.001 1.0

Sweet Bell Peppers 675 0 0.010 0.75

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 0.3

TOTAL 5,465 0

Oxydemeton methyl sulfone (metabolite of Oxydemeton methyl)

Blueberries, Cultivated, Fresh 168 0 0.002 NT

Blueberries, Frozen 7 0 0.002 NT

Cantaloupe 694 0 0.002 0.2

Carrots 499 0 0.005 NT

Collard Greens 514 0 0.002 NT

Eggplant 311 0 0.005 1.0

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 1.0

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.001 - 0.020 1.0

Sweet Bell Peppers 675 0 0.010 0.75

Tangerines 687 0 0.020 NT

Tomato Paste 506 0 0.001 - 0.020 NT

Winter Squash 677 0 0.001 0.3

TOTAL 6,456 0

Oxyfluorfen (herbicide) 

Apple Juice 724 0 0.030 0.05

Bananas 703 0 0.030 0.05

Blueberries, Cultivated, Fresh 168 0 0.050 NT

Blueberries, Frozen 7 0 0.050 NT

Broccoli 675 2 0.3 0.004 - 0.005 0.001 0.05

Cantaloupe 694 0 0.050 NT

Carrots 499 0 0.040 NT

Cauliflower 692 0 0.001 0.05

Collard Greens 514 0 0.050 NT

Eggplant 661 0 0.001 - 0.040 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.040 0.05

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 8,610 2

Appendix B. Page 86 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Paclobutrazol (plant growth regulator) 

Carrots 499 0 0.010 NT

Eggplant 311 0 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,083 0

Parathion (insecticide) 

Blueberries, Cultivated, Fresh 168 0 0.005 NT

Blueberries, Frozen 7 0 0.005 NT

Broccoli 675 0 0.003 NT

Cantaloupe 694 0 0.005 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.003 NT

Collard Greens 514 0 0.005 NT

Eggplant 661 0 0.003 - 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.060 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 7,183 0

Parathion oxygen analog (metabolite of Parathion)

Broccoli 675 0 0.001 NT

Carrots 499 0 0.005 NT

Cauliflower 692 0 0.001 NT

Eggplant 661 0 0.001 - 0.005 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 4,436 0

Parathion methyl (insecticide) 

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Broccoli 675 0 0.002 NT

Cantaloupe 694 0 0.010 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.002 NT

Collard Greens 514 0 0.010 NT

Eggplant 661 0 0.002 - 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 0 0.001 NT

Appendix B. Page 87 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.001 - 0.005 NT

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 NT

TOTAL 8,173 0

Parathion methyl oxygen analog (metabolite of Parathion methyl)

Blueberries, Cultivated, Fresh 168 0 0.020 NT

Blueberries, Frozen 7 0 0.020 NT

Cantaloupe 694 0 0.020 NT

Carrots 499 0 0.025 NT

Collard Greens 514 0 0.020 NT

Eggplant 311 0 0.025 NT

Green Beans 177 0 0.010 NT

Kiwi Fruit 177 0 0.025 NT

Orange Juice 499 0 0.010 NT

Summer Squash 89 0 0.010 NT

Tomato Paste 290 0 0.010 NT

Winter Squash 677 0 0.010 NT

TOTAL 4,102 0

Pebulate (herbicide) 

Radishes 689 0 0.005 NT

Sweet Bell Peppers 675 0 0.005 NT

TOTAL 1,364 0

Penconazole (fungicide) 

Carrots 499 0 0.010 NT

Eggplant 311 0 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,083 0

Pencycuron (fungicide) 

Carrots 499 0 0.005 NT

Eggplant 311 0 0.005 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.003 NT

Sweet Bell Peppers 675 0 0.010 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 4,083 0

Pendimethalin (herbicide) 

Apple Juice 724 0 0.010 0.1

Blueberries, Cultivated, Fresh 168 0 0.050 0.1

Appendix B. Page 88 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Blueberries, Frozen 7 0 0.050 0.1

Broccoli 675 23 3.4 0.002 - 0.014 0.001 0.1

Cantaloupe 693 0 0.050 0.10

Carrots 499 0 0.020 0.5

Cauliflower 692 2 0.3 0.002 0.001 0.1

Collard Greens 514 0 0.050 0.20

Eggplant 661 0 0.001 - 0.020 0.1

Green Beans 177 2 1.1 0.002 - 0.003 0.001 0.10

Kiwi Fruit 177 0 0.035 0.10

Orange Juice 499 0 0.001 0.1

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.001 - 0.005 NT

Sweet Bell Peppers 675 1 0.1 0.006 0.005 0.1

Tangerines 687 0 0.005 0.1

Tomato Paste 506 0 0.001 - 0.005 0.1

Winter Squash 677 1 0.1 0.001 0.001 V-1 NT

TOTAL 8,896 29

Penflufen (fungicide) 

Green Beans 177 0 0.001 0.01

Orange Juice 499 0 0.001 NT

Summer Squash 176 0 0.001 NT

Tangerines 687 0 0.001 NT

Tomato Paste 506 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 2,722 0

Penoxsulam (herbicide) 

Apple Juice 724 0 0.003 0.01

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.010 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 3,820 0

Pentachloroaniline - PCA (metabolite of Quintozene)

Blueberries, Cultivated, Fresh 168 0 0.004 NT

Blueberries, Frozen 7 0 0.004 NT

Broccoli 675 3 0.4 0.002 - 0.004 0.001 0.1

Cantaloupe 694 3 0.4 0.004 - 0.006 0.004 V-3 NT

Carrots 499 8 1.6 0.006 - 0.018 0.005 V-8 NT

Cauliflower 692 0 0.001 0.1

Collard Greens 514 1 0.2 0.004 0.004 0.2

Eggplant 661 0 0.001 - 0.005 0.1

Green Beans 177 0 0.001 0.1

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 176 1 0.6 0.001 0.001 - 0.005 V-1 NT

Sweet Bell Peppers 675 1 0.1 0.007 0.005 0.1

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 0.1

Winter Squash 677 6 0.9 0.002 - 0.004 0.001 V-6 NT

TOTAL 8,173 23

Appendix B. Page 89 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Pentachlorobenzene - PCB (metabolite of Quintozene)

Blueberries, Cultivated, Fresh 168 0 0.005 NT

Blueberries, Frozen 7 0 0.005 NT

Broccoli 675 0 0.003 - 0.010 0.1

Cantaloupe 694 0 0.005 NT

Carrots 499 2 0.4 0.005 0.002 V-2 NT

Cauliflower 692 0 0.003 - 0.020 0.1

Collard Greens 514 0 0.005 0.2

Eggplant 661 0 0.002 - 0.020 0.1

Green Beans 177 0 0.001 0.1

Kiwi Fruit 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.001 - 0.002 NT

Sweet Bell Peppers 675 0 0.005 0.1

Tangerines 687 0 0.002 NT

Tomato Paste 506 0 0.001 - 0.002 0.1

Winter Squash 677 1 0.1 0.002 0.001 V-1 NT

TOTAL 8,173 3

Pentachlorophenyl methyl sulfide - PCPMS (metabolite of Quintozene)

Broccoli 675 1 0.1 0.002 0.001 0.1

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.003 0.1

Green Beans 177 0 0.003 0.1

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.003 - 0.015 NT

Sweet Bell Peppers 675 0 0.005 0.1

Tangerines 687 0 0.015 NT

Tomato Paste 506 0 0.003 - 0.015 0.1

Winter Squash 677 0 0.003 NT

TOTAL 6,129 1

Penthiopyrad (fungicide) 

Apple Juice 724 1 0.1 0.002 0.001 0.50

Broccoli 675 7 1 0.004 - 0.47 0.001 - 0.003 5

Carrots 499 50 10 0.001 - 0.052 0.001 3.0

Cauliflower 692 1 0.1 0.004 0.001 - 0.006 5

Eggplant 661 40 6.1 0.001 - 0.050 0.001 3.0

Green Beans 177 19 10.7 0.002 - 0.33 0.001 4.0

Kiwi Fruit 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Radishes 689 2 0.3 0.011 - 0.037 0.010 3.0

Summer Squash 176 0 0.001 0.60

Sweet Bell Peppers 675 27 4 0.010 - 0.10 0.010 3.0

Tangerines 687 0 0.001 NT

Tomato Paste 506 29 5.7 0.001 - 0.010 0.001 3.5

Winter Squash 677 10 1.5 0.001 - 0.007 0.001 0.60

TOTAL 7,514 186

Permethrin Total (insecticide)

Green Beans 177 1 0.6 0.004 0.003 V-1 NT

Orange Juice 499 0 0.003 NT

Radishes 689 3 0.4 0.011 - 0.10 0.005 V-3 NT

Appendix B. Page 90 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Summer Squash 176 1 0.6 0.008 0.003 - 0.050 1.5

Sweet Bell Peppers 675 43 6.4 0.005 - 0.46 0.005 0.50

Tangerines 687 0 0.050 NT

Tomato Paste 506 0 0.003 - 0.050 2.0

Winter Squash 677 15 2.2 0.003 - 0.033 0.003 1.5

TOTAL 4,086 63

Permethrin cis (isomer of Permethrin)

Apple Juice 724 0 0.010 0.05

Bananas 703 0 0.010 NT

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Broccoli 675 54 8 0.002 - 0.12 0.001 2.0

Cantaloupe 694 0 0.010 1.5

Carrots 499 0 0.010 NT

Cauliflower 692 3 0.4 0.002 0.001 0.5

Collard Greens 514 10 1.9 0.014 - 0.085 0.010 15

Eggplant 661 34 5.1 0.002 - 0.047 0.001 - 0.010 0.50

Kiwi Fruit 177 0 0.020 2.0

TOTAL 5,514 101

Permethrin trans (isomer of Permethrin)

Apple Juice 724 0 0.010 0.05

Bananas 703 0 0.010 NT

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Broccoli 675 44 6.5 0.002 - 0.13 0.001 2.0

Cantaloupe 694 0 0.010 1.5

Carrots 499 0 0.010 NT

Cauliflower 692 2 0.3 0.002 0.001 0.5

Collard Greens 514 10 1.9 0.014 - 0.082 0.010 15

Eggplant 661 37 5.6 0.002 - 0.069 0.001 - 0.010 0.50

Kiwi Fruit 177 0 0.010 2.0

TOTAL 5,514 93

Phenmedipham (herbicide) 

Summer Squash 87 0 0.005 NT

Tangerines 687 0 0.005 NT

Tomato Paste 216 0 0.005 NT

TOTAL 990 0

Phenothrin (insecticide) 

Apple Juice 724 0 0.010 0.01

Bananas 703 0 0.010 0.01

Blueberries, Cultivated, Fresh 168 0 0.050 0.01

Blueberries, Frozen 7 0 0.050 0.01

Broccoli 675 0 0.002 0.01

Cantaloupe 694 0 0.050 0.01

Carrots 499 0 0.075 0.01

Cauliflower 692 0 0.002 0.01

Collard Greens 514 0 0.050 0.01

Eggplant 661 0 0.002 - 0.075 0.01

Green Beans 177 0 0.005 - 0.010 0.01

Kiwi Fruit 177 0 0.15 0.01

Orange Juice 499 0 0.005 0.01

Radishes 689 0 0.005 0.01

Summer Squash 176 0 0.005 - 0.025 0.01

Appendix B. Page 91 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Sweet Bell Peppers 675 0 0.005 0.01

Tangerines 687 0 0.025 0.01

Tomato Paste 475 0 0.005 - 0.025 0.01

Winter Squash 643 0 0.005 - 0.010 0.01

TOTAL 9,535 0

Phenthoate (insecticide) 

Broccoli 675 0 0.001 NT

Cauliflower 692 0 0.001 NT

Eggplant 350 0 0.001 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 3,449 0

o-Phenylphenol (fungicide) 

Apple Juice 724 0 0.002 25

Blueberries, Cultivated, Fresh 168 0 0.005 NT

Blueberries, Frozen 7 0 0.005 NT

Cantaloupe 694 26 3.7 0.010 - 0.27 0.005 10

Carrots 499 0 0.040 20

Collard Greens 514 0 0.005 NT

Eggplant 311 0 0.040 NT

Kiwi Fruit 177 0 0.040 NT

Orange Juice 499 4 0.8 0.005 - 0.014 0.005 10

Tomato Paste 290 0 0.005 10

TOTAL 3,883 30

Phorate (insecticide) 

Broccoli 675 0 0.003 NT

Carrots 499 0 0.085 NT

Cauliflower 672 0 0.001 - 0.006 NT

Eggplant 661 0 0.003 - 0.085 NT

Green Beans 177 0 0.003 0.05

Kiwi Fruit 177 0 0.17 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.003 - 0.030 NT

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 0 0.030 NT

Tomato Paste 506 0 0.003 - 0.030 NT

Winter Squash 677 0 0.003 NT

TOTAL 6,770 0

Phorate oxygen analog (metabolite of Phorate)

Broccoli 675 0 0.001 NT

Cauliflower 692 0 0.001 NT

Eggplant 350 0 0.001 NT

Green Beans 177 0 0.005 0.05

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 3,449 0

Appendix B. Page 92 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Phorate oxygen analog sulfone (metabolite of Phorate)

Broccoli 675 0 0.001 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.001 NT

Eggplant 661 0 0.001 - 0.010 NT

Green Beans 177 0 0.001 0.05

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Summer Squash 176 0 0.001 - 0.010 NT

Tangerines 687 0 0.010 NT

Tomato Paste 506 0 0.001 - 0.010 NT

Winter Squash 677 0 0.001 NT

TOTAL 5,426 0

Phorate oxygen analog sulfoxide (metabolite of Phorate)

Broccoli 675 0 0.001 NT

Carrots 499 0 0.005 NT

Cauliflower 692 0 0.001 NT

Eggplant 661 0 0.001 - 0.005 NT

Green Beans 177 0 0.001 0.05

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Summer Squash 176 0 0.001 - 0.010 NT

Tangerines 687 0 0.010 NT

Tomato Paste 506 0 0.001 - 0.010 NT

Winter Squash 677 0 0.001 NT

TOTAL 5,426 0

Phorate sulfone (metabolite of Phorate)

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Broccoli 675 0 0.002 NT

Cantaloupe 573 0 0.010 NT

Carrots 499 0 0.030 NT

Cauliflower 692 0 0.002 NT

Collard Greens 241 0 0.010 NT

Eggplant 661 0 0.002 - 0.030 NT

Green Beans 177 0 0.003 0.05

Kiwi Fruit 177 0 0.030 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.003 - 0.025 NT

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 0 0.050 NT

Tomato Paste 506 0 0.003 - 0.050 NT

Winter Squash 677 0 0.003 NT

TOTAL 7,779 0

Phorate sulfoxide (metabolite of Phorate)

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Broccoli 675 0 0.001 NT

Cantaloupe 693 0 0.010 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.001 NT

Collard Greens 514 0 0.010 NT

Eggplant 661 0 0.001 - 0.010 NT

Appendix B. Page 93 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Green Beans 177 0 0.001 0.05

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.001 - 0.002 NT

Sweet Bell Peppers 675 0 0.010 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 NT

TOTAL 8,172 0

Phosalone (insecticide) 

Apple Juice 724 0 0.003 NT

Blueberries, Cultivated, Fresh 168 0 0.001 NT

Blueberries, Frozen 7 0 0.001 NT

Broccoli 675 0 0.005 NT

Cantaloupe 694 0 0.001 NT

Carrots 499 0 0.015 NT

Cauliflower 692 0 0.002 - 0.005 NT

Collard Greens 514 0 0.001 NT

Eggplant 661 0 0.002 - 0.015 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.015 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.003 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 7,907 0

Phosmet (insecticide) 

Apple Juice 724 1 0.1 0.008 0.005 10

Bananas 703 0 0.005 NT

Blueberries, Cultivated, Fresh 168 0 0.010 10

Blueberries, Frozen 7 3 42.9 0.015 - 0.035 0.010 10

Cantaloupe 694 0 0.010 NT

Carrots 499 0 0.025 NT

Collard Greens 514 0 0.010 NT

Eggplant 536 0 0.005 - 0.025 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.025 25

Orange Juice 499 0 0.001 5

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 657 0 0.020 5

Tomato Paste 506 0 0.001 - 0.020 NT

Winter Squash 677 0 0.001 NT

TOTAL 7,991 4

Phosmet oxygen analog (metabolite of Phosmet)

Apple Juice 724 0 0.005 10

Bananas 703 0 0.005 NT

Blueberries, Cultivated, Fresh 168 0 0.004 10

Blueberries, Frozen 7 2 28.6 0.008 - 0.020 0.004 10

Cantaloupe 694 0 0.004 NT

Appendix B. Page 94 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Carrots 499 0 0.010 NT

Collard Greens 514 0 0.004 NT

Eggplant 311 0 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 25

Orange Juice 499 0 0.001 5

Summer Squash 176 0 0.001 - 0.005 NT

Tangerines 687 0 0.005 5

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 NT

TOTAL 6,519 2

Phosphamidon (insecticide) 

Broccoli 675 0 0.001 NT

Cauliflower 692 0 0.001 - 0.003 NT

Eggplant 350 0 0.001 NT

Green Beans 177 0 0.005 NT

Orange Juice 499 0 0.005 NT

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.005 NT

Sweet Bell Peppers 675 0 0.010 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 4,813 0

Phoxim (insecticide) 

Carrots 499 0 0.025 NT

Eggplant 311 0 0.025 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.025 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 2,719 0

Picolinafen (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Picoxystrobin (fungicide) 

Broccoli 657 0 0.001 - 0.006 2.0

Carrots 499 0 0.001 0.50

Cauliflower 600 0 0.001 - 0.006 2.0

Eggplant 661 0 0.001 0.70

Green Beans 177 0 0.005 2.0

Kiwi Fruit 177 0 0.001 NT

Orange Juice 499 0 0.005 NT

Summer Squash 176 0 0.005 0.30

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.005 0.70

Winter Squash 677 0 0.005 0.30

TOTAL 5,316 0

Appendix B. Page 95 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Pinoxaden (herbicide) 

Green Beans 177 0 0.020 NT

Orange Juice 499 0 0.020 NT

Summer Squash 89 0 0.020 NT

Tomato Paste 290 0 0.020 NT

Winter Squash 677 0 0.020 NT

TOTAL 1,732 0

Piperonyl butoxide (insecticide) 

Apple Juice 724 0 0.004 10

Bananas 703 0 0.004 10

Blueberries, Cultivated, Fresh 168 0 0.005 10

Blueberries, Frozen 7 0 0.005 10

Broccoli 675 1 0.1 0.003 0.002 10

Cantaloupe 694 0 0.005 10

Carrots 499 0 0.015 10

Cauliflower 692 0 0.002 10

Collard Greens 514 0 0.005 10

Eggplant 661 3 0.5 0.003 - 0.025 0.002 - 0.015 10

Green Beans 177 0 0.003 10

Kiwi Fruit 177 0 0.015 10

Orange Juice 499 0 0.003 10

Radishes 689 0 0.005 10

Summer Squash 176 0 0.003 - 0.025 10

Sweet Bell Peppers 675 12 1.8 0.006 - 0.087 0.005 10

Tangerines 687 0 0.025 10

Tomato Paste 506 0 0.003 - 0.025 10

Winter Squash 677 1 0.1 0.009 0.003 10

TOTAL 9,600 17

Pirimicarb (insecticide) 

Broccoli 675 0 0.001 NT

Carrots 499 0 0.005 NT

Cauliflower 692 0 0.001 NT

Eggplant 661 0 0.001 - 0.005 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 5,800 0

Pirimicarb desmethyl (metabolite of Pirimicarb)

Carrots 499 0 0.001 NT

Eggplant 311 0 0.001 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.010 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,083 0

Appendix B. Page 96 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Pirimiphos ethyl (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Pirimiphos methyl (insecticide) 

Blueberries, Cultivated, Fresh 168 0 0.001 NT

Blueberries, Frozen 7 0 0.001 NT

Broccoli 675 1 0.1 0.008 0.001 V-1 NT

Cantaloupe 694 0 0.001 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.001 NT

Collard Greens 514 0 0.001 NT

Eggplant 661 0 0.001 - 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 7,183 1

Prallethrin (insecticide) 

Apple Juice 724 0 0.008 1.0

Bananas 703 0 0.008 1.0

Blueberries, Cultivated, Fresh 168 0 0.008 1.0

Blueberries, Frozen 7 0 0.008 1.0

Cantaloupe 694 0 0.008 1.0

Carrots 499 0 0.045 1.0

Collard Greens 514 0 0.008 1.0

Eggplant 311 0 0.045 1.0

Green Beans 177 0 0.020 1.0

Kiwi Fruit 177 0 0.10 1.0

Orange Juice 499 0 0.020 1.0

Radishes 689 0 0.010 1.0

Summer Squash 89 0 0.020 1.0

Sweet Bell Peppers 675 0 0.010 1.0

Tangerines 687 0 0.030 1.0

Tomato Paste 506 0 0.020 - 0.030 1.0

Winter Squash 677 0 0.020 1.0

TOTAL 7,796 0

Pretilachlor (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Appendix B. Page 97 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Primisulfuron methyl (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Prochloraz (fungicide) 

Green Beans 177 0 0.005 NT

Orange Juice 499 0 0.005 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.005 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 3,096 0

Procymidone (fungicide) 

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Cantaloupe 694 0 0.010 NT

Carrots 499 0 0.010 NT

Collard Greens 514 0 0.010 NT

Eggplant 311 0 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 5,466 0

Prodiamine (herbicide) 

Carrots 499 0 0.005 NT

Eggplant 311 0 0.005 NT

Kiwi Fruit 177 0 0.005 NT

TOTAL 987 0

Profenofos (insecticide) 

Blueberries, Cultivated, Fresh 168 0 0.075 NT

Blueberries, Frozen 7 0 0.075 NT

Broccoli 675 0 0.003 NT

Cantaloupe 694 0 0.075 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.001 NT

Collard Greens 514 0 0.075 NT

Eggplant 661 0 0.001 - 0.010 NT

Green Beans 177 1 0.6 0.003 0.001 V-1 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.001 - 0.005 NT

Sweet Bell Peppers 675 0 0.010 NT

Tangerines 687 0 0.005 NT

Appendix B. Page 98 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 NT

TOTAL 8,173 1

Profluralin (herbicide) 

Green Beans 177 0 0.005 NT

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 1,732 0

Profoxydim (herbicide) 

Green Beans 127 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 34 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 615 0 0.003 NT

TOTAL 1,565 0

Promecarb (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Prometon (herbicide) 

Broccoli 675 0 0.001 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.001 NT

Eggplant 661 0 0.001 - 0.010 NT

Kiwi Fruit 177 0 0.010 NT

TOTAL 2,704 0

Prometryn (herbicide) 

Broccoli 675 0 0.001 NT

Carrots 499 1 0.2 0.023 0.010 0.45

Cauliflower 692 0 0.001 NT

Eggplant 661 0 0.001 - 0.010 NT

Green Beans 177 0 0.001 0.05

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,436 1

Pronamide (herbicide) 

Apple Juice 724 0 0.004 0.1

Blueberries, Cultivated, Fresh 168 0 0.002 0.05

Blueberries, Frozen 7 0 0.002 0.05

Broccoli 675 9 1.3 0.002 - 0.012 0.001 - 0.003 V-9 NT

Cantaloupe 694 3 0.4 0.003 - 0.005 0.002 V-3 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.001 NT

Appendix B. Page 99 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Collard Greens 514 14 2.7 0.002 - 0.020 0.002 V-14 NT

Eggplant 661 0 0.001 - 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.015 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.001 - 0.005 NT

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 NT

TOTAL 8,897 26

Propachlor (herbicide) 

Broccoli 675 0 0.001 - 0.003 NT

Cauliflower 692 0 0.001 NT

Eggplant 350 0 0.001 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 3,449 0

Propamocarb (fungicide) 

Green Beans 177 7 4 0.002 - 0.060 0.001 V-7 NT

Orange Juice 499 0 0.001 NT

Radishes 689 2 0.3 0.16 - 0.58 0.010 V-2 NT

Summer Squash 89 11 12.4 0.002 - 0.18 0.001 1.5

Sweet Bell Peppers 675 49 7.3 0.010 - 0.36 0.010 4

Tomato Paste 290 0 0.001 5.0

Winter Squash 677 62 9.2 0.001 - 0.34 0.001 1.5

TOTAL 3,096 131

Propamocarb hydrochloride 4 (fungicide) 

Blueberries, Cultivated, Fresh 168 0 0.002 NT

Blueberries, Frozen 7 0 0.002 NT

Cantaloupe 694 57 8.2 0.002 - 0.014 0.002 1.5

Carrots 499 0 0.005 NT

Collard Greens 514 3 0.6 0.006 - 0.054 0.002 V-3 NT

Eggplant 311 16 5.1 0.006 - 0.38 0.005 4

Kiwi Fruit 177 0 0.005 NT

Summer Squash 87 5 5.7 0.001 - 0.032 0.001 1.5

Tangerines 687 0 0.001 NT

Tomato Paste 216 0 0.001 5.0

TOTAL 3,360 81

Propanil (herbicide) 

Green Beans 177 0 0.001 - 0.003 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 - 0.003 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 - 0.003 NT

TOTAL 1,732 0

Propaquizafop (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Appendix B. Page 100 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Propargite (insecticide) 

Blueberries, Cultivated, Fresh 168 0 0.050 NT

Blueberries, Frozen 7 0 0.050 NT

Broccoli 675 0 0.006 NT

Cantaloupe 694 0 0.050 NT

Carrots 499 0 0.040 NT

Cauliflower 692 0 0.006 NT

Collard Greens 514 1 0.2 0.099 0.050 V-1 NT

Eggplant 661 0 0.006 - 0.040 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.040 NT

Orange Juice 499 0 0.001 10.0

Radishes 689 0 0.020 NT

Summer Squash 176 0 0.001 - 0.025 NT

Sweet Bell Peppers 656 0 0.020 NT

Tangerines 687 0 0.025 NT

Tomato Paste 506 2 0.4 0.002 0.001 - 0.025 V-2 NT

Winter Squash 677 1 0.1 0.002 0.001 V-1 NT

TOTAL 8,154 4

Propazine (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Propetamphos (insecticide) 

Bananas 703 0 0.010 NT

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Broccoli 675 0 0.001 - 0.003 NT

Cantaloupe 694 0 0.010 NT

Carrots 499 0 0.020 NT

Cauliflower 692 0 0.001 - 0.003 NT

Collard Greens 514 0 0.010 NT

Eggplant 661 0 0.001 - 0.020 NT

Green Beans 177 0 0.005 NT

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 0 0.005 NT

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.005 NT

Sweet Bell Peppers 675 0 0.010 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 8,789 0

Propham (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Appendix B. Page 101 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Propiconazole (fungicide) 

Bananas 703 0 0.003 0.2

Blueberries, Cultivated, Fresh 168 0 0.010 1.3

Blueberries, Frozen 7 0 0.010 1.3

Broccoli 675 0 0.005 - 0.015 NT

Cantaloupe 694 0 0.010 NT

Carrots 499 6 1.2 0.023 - 0.032 0.020 0.3

Cauliflower 692 0 0.005 NT

Collard Greens 514 1 0.2 0.063 0.010 20

Eggplant 661 0 0.005 - 0.020 NT

Green Beans 177 0 0.001 0.70

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 2 0.4 0.001 - 0.005 0.001 8.0

Radishes 689 0 0.010 0.3

Summer Squash 176 0 0.001 - 0.005 NT

Sweet Bell Peppers 675 0 0.010 NT

Tangerines 687 57 8.3 0.005 - 0.066 0.005 8.0

Tomato Paste 506 0 0.001 - 0.005 3.0

Winter Squash 677 0 0.001 NT

TOTAL 8,876 66

Propoxycarbazone (herbicide) 

Orange Juice 499 0 0.005 NT

Tomato Paste 290 0 0.005 NT

TOTAL 789 0

Proquinazid (fungicide) 

Green Beans 177 0 0.005 NT

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 1,732 0

Prosulfuron (herbicide) 

Carrots 499 0 0.005 NT

Eggplant 311 0 0.005 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.003 NT

Summer Squash 176 0 0.003 - 0.010 NT

Tangerines 687 0 0.010 NT

Tomato Paste 506 0 0.003 - 0.010 NT

Winter Squash 677 0 0.003 NT

TOTAL 3,709 0

Prothioconazole (fungicide) 

Kiwi Fruit 177 0 0.10 NT

Summer Squash 57 0 0.10 0.30

Tangerines 687 0 0.10 NT

Tomato Paste 216 0 0.10 NT

TOTAL 1,137 0

Appendix B. Page 102 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Prothioconazole desthio (metabolite of Prothioconazole) 

Green Beans 177 0 0.001 NT

Summer Squash 89 0 0.001 0.30

Winter Squash 62 0 0.001 0.30

TOTAL 328 0

Prothiofos (insecticide) 

Carrots 499 0 0.040 NT

Eggplant 311 0 0.040 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.040 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 648 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,056 0

Pydiflumetofen (fungicide) 

Apple Juice 724 0 0.002 0.2

Carrots 499 0 0.010 0.5

Eggplant 311 0 0.010 0.60

Green Beans 177 0 0.001 1

Orange Juice 499 0 0.001 1

Summer Squash 176 11 6.2 0.001 - 0.016 0.001 - 0.005 0.50

Tangerines 687 0 0.005 1

Tomato Paste 506 0 0.001 - 0.005 0.60

Winter Squash 677 17 2.5 0.002 - 0.14 0.001 0.50

TOTAL 4,256 28

Pymetrozine (insecticide) 

Broccoli 675 0 0.005 0.5

Carrots 499 0 0.085 NT

Cauliflower 692 0 0.005 0.5

Eggplant 661 1 0.2 0.005 0.005 - 0.085 0.2

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.085 NT

Orange Juice 499 0 0.001 NT

Radishes 669 0 0.010 NT

Summer Squash 89 0 0.001 0.1

Sweet Bell Peppers 675 0 0.010 0.2

Tomato Paste 290 0 0.001 0.2

Winter Squash 677 0 0.001 0.1

TOTAL 5,780 1

Pyraclofos (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Pyraclostrobin (fungicide) 

Apple Juice 724 2 0.3 0.005 0.003 1.5

Bananas 703 0 0.003 0.04

Appendix B. Page 103 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Blueberries, Cultivated, Fresh 168 44 26.2 0.004 - 0.35 0.003 4.0

Blueberries, Frozen 7 1 14.3 0.026 0.003 4.0

Broccoli 675 66 9.8 0.002 - 0.34 0.001 - 0.003 5.0

Cantaloupe 694 0 0.003 0.5

Carrots 499 59 11.8 0.005 - 0.025 0.005 0.4

Cauliflower 692 0 0.001 5.0

Collard Greens 514 107 20.8 0.004 - 2.4 0.003 16

Eggplant 661 26 3.9 0.002 - 0.041 0.001 - 0.005 1.4

Green Beans 177 30 16.9 0.002 - 0.17 0.001 0.5

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 2.0

Radishes 689 58 8.4 0.003 - 0.17 0.003 0.4

Summer Squash 176 19 10.8 0.001 - 0.025 0.001 0.5

Sweet Bell Peppers 675 167 24.7 0.003 - 0.46 0.003 1.4

Tangerines 687 7 1 0.001 - 0.007 0.001 2.0

Tomato Paste 506 0 0.001 1.4

Winter Squash 677 46 6.8 0.001 - 0.010 0.001 0.5

TOTAL 9,600 632

Pyraflufen ethyl (herbicide) 

Apple Juice 724 0 0.002 0.01

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Cantaloupe 694 0 0.010 NT

Carrots 499 0 0.030 NT

Collard Greens 514 0 0.010 NT

Eggplant 311 0 0.030 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.030 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,826 0

Pyrazon (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Pyrazophos (fungicide) 

Carrots 499 0 0.010 NT

Eggplant 311 0 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.010 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,083 0

Appendix B. Page 104 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Pyrethrins (insecticide) 

Carrots 499 0 0.20 1.0

Eggplant 311 0 0.20 1.0

Green Beans 177 0 0.005 1.0

Kiwi Fruit 177 0 0.20 1.0

Summer Squash 89 0 0.005 1.0

Winter Squash 62 0 0.005 1.0

TOTAL 1,315 0

Pyridaben (insecticide, acaricide)

Apple Juice 724 0 0.001 0.75

Blueberries, Cultivated, Fresh 168 0 0.005 2.5

Blueberries, Frozen 7 0 0.005 2.5

Cantaloupe 694 0 0.005 NT

Carrots 499 0 0.001 NT

Collard Greens 514 0 0.005 NT

Eggplant 311 0 0.001 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.001 NT

Orange Juice 499 0 0.001 0.9

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.001 - 0.005 NT

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 1 0.1 0.005 0.005 0.9

Tomato Paste 506 0 0.001 - 0.005 0.15

Winter Squash 677 0 0.001 NT

TOTAL 7,180 1

Pyridalyl (insecticide) 

Carrots 499 0 0.020 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Summer Squash 176 0 0.001 - 0.005 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 1.0

Winter Squash 677 0 0.001 NT

TOTAL 3,398 0

Pyridaphenthion (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Pyrifluquinazon (insecticide) 

Apple Juice 724 0 0.001 0.07

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 0.70

Summer Squash 176 0 0.001 - 0.005 0.07

Tangerines 687 0 0.005 0.70

Tomato Paste 506 0 0.001 - 0.005 0.30

Winter Squash 677 0 0.001 0.07

TOTAL 3,446 0

Appendix B. Page 105 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Pyrimethanil (fungicide) 

Apple Juice 724 195 26.9 0.003 - 2.5 0.002 15

Bananas 703 13 1.8 0.003 0.002 0.10

Blueberries, Cultivated, Fresh 168 8 4.8 0.060 - 0.95 0.050 8.0

Blueberries, Frozen 7 1 14.3 0.14 0.050 8.0

Broccoli 675 4 0.6 0.002 - 0.63 0.001 V-4 NT

Cantaloupe 694 0 0.050 NT

Carrots 499 10 2 0.005 - 0.035 0.005 V-10 NT

Cauliflower 692 0 0.003 NT

Collard Greens 514 0 0.050 NT

Eggplant 661 4 0.6 0.002 - 0.007 0.001 - 0.005 V-4 NT

Green Beans 177 1 0.6 0.009 0.005 V-1 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 2 0.4 0.006 - 0.008 0.005 10

Radishes 689 1 0.1 0.12 0.003 V-1 NT

Summer Squash 176 0 0.005 NT

Sweet Bell Peppers 675 0 0.003 NT

Tangerines 687 118 17.2 0.005 - 0.50 0.005 10

Tomato Paste 506 0 0.005 0.50

Winter Squash 677 0 0.005 NT

TOTAL 9,600 357

Pyriofenone (fungicide) 

Green Beans 177 0 0.001 NT

Summer Squash 176 0 0.001 - 0.005 0.30

Winter Squash 62 0 0.001 0.30

TOTAL 415 0

Pyriproxyfen (insecticide, growth regulator)

Apple Juice 724 0 0.005 0.20

Bananas 703 11 1.6 0.008 0.005 0.20

Blueberries, Cultivated, Fresh 168 0 0.001 1.0

Blueberries, Frozen 7 0 0.001 1.0

Broccoli 675 0 0.001 - 0.002 0.70

Cantaloupe 694 0 0.001 0.10

Carrots 499 0 0.005 0.15

Cauliflower 692 0 0.001 - 0.002 0.70

Collard Greens 514 0 0.001 2.0

Eggplant 661 9 1.4 0.002 - 0.021 0.001 - 0.005 0.80

Green Beans 177 5 2.8 0.002 - 0.060 0.001 0.20

Kiwi Fruit 177 0 0.005 0.35

Orange Juice 499 0 0.001 0.50

Radishes 689 0 0.005 0.15

Summer Squash 176 0 0.001 0.10

Sweet Bell Peppers 675 21 3.1 0.005 - 0.038 0.005 0.80

Tangerines 687 7 1 0.001 - 0.003 0.001 0.50

Tomato Paste 506 0 0.001 0.80

Winter Squash 677 0 0.001 0.10

TOTAL 9,600 53

Pyroxasulfone (herbicide) 

Carrots 499 0 0.005 NT

Eggplant 311 0 0.005 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Appendix B. Page 106 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 2,719 0

Pyroxsulam (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Quinalphos (insecticide) 

Carrots 499 0 0.005 NT

Eggplant 311 0 0.005 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,083 0

Quinoxyfen (fungicide) 

Blueberries, Cultivated, Fresh 168 0 0.020 1.0

Blueberries, Frozen 7 0 0.020 1.0

Broccoli 675 0 0.001 NT

Cantaloupe 694 0 0.020 0.08

Carrots 499 0 0.005 NT

Cauliflower 692 0 0.001 NT

Collard Greens 514 0 0.020 NT

Eggplant 661 1 0.2 0.009 0.001 - 0.005 1.7

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 176 3 1.7 0.001 - 0.006 0.001 V-3 NT

Sweet Bell Peppers 675 10 1.5 0.010 - 0.032 0.010 1.7

Tangerines 687 0 0.001 NT

Tomato Paste 506 0 0.001 1.7

Winter Squash 677 6 0.9 0.001 - 0.017 0.001 0.20

TOTAL 8,173 20

Quintozene - PCNB (fungicide) (parent of HCB, PCA, PCB and PCPMS)

Broccoli 675 1 0.1 0.002 0.001 0.1

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.001 0.1

Eggplant 661 0 0.003 - 0.010 0.1

Green Beans 177 0 0.001 0.1

Kiwi Fruit 177 0 0.025 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.001 - 0.005 NT

Sweet Bell Peppers 675 0 0.005 0.1

Tangerines 687 0 0.005 NT

Appendix B. Page 107 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomato Paste 506 0 0.001 - 0.005 0.1

Winter Squash 677 0 0.001 NT

TOTAL 6,790 1

Quizalofop ethyl (herbicide) 

Green Beans 177 0 0.001 0.25

Orange Juice 499 0 0.001 NT

Summer Squash 176 0 0.001 - 0.025 NT

Tangerines 687 0 0.025 NT

Tomato Paste 506 0 0.001 - 0.025 NT

Winter Squash 677 0 0.001 NT

TOTAL 2,722 0

Resmethrin (insecticide) 

Apple Juice 724 0 0.010 3.0

Bananas 703 0 0.010 3.0

Carrots 499 0 0.030 3.0

Eggplant 311 0 0.030 3.0

Green Beans 177 0 0.003 3.0

Kiwi Fruit 177 0 0.030 3.0

Orange Juice 499 0 0.003 3.0

Radishes 689 0 0.020 3.0

Summer Squash 89 0 0.003 3.0

Sweet Bell Peppers 656 0 0.020 3.0

Tangerines 687 0 0.050 3.0

Tomato Paste 506 0 0.003 - 0.050 3.0

Winter Squash 645 0 0.003 3.0

TOTAL 6,362 0

Resmethrin trans (isomer of Resmethrin)

Blueberries, Cultivated, Fresh 168 0 0.050 3.0

Blueberries, Frozen 7 0 0.050 3.0

Broccoli 675 0 0.002 - 0.003 3.0

Cantaloupe 694 0 0.050 3.0

Collard Greens 514 0 0.050 3.0

Eggplant 350 0 0.001 - 0.002 3.0

TOTAL 2,408 0

Rimsulfuron (herbicide) 

Apple Juice 724 0 0.005 0.01

Green Beans 127 0 0.003 NT

Orange Juice 499 0 0.003 0.01

Radishes 689 0 0.010 NT

Summer Squash 121 0 0.003 - 0.005 NT

Sweet Bell Peppers 675 0 0.010 NT

Tangerines 687 0 0.010 0.01

Tomato Paste 506 0 0.003 - 0.010 0.05

Winter Squash 615 0 0.003 NT

TOTAL 4,643 0

Rotenone (insecticide) 

Green Beans 177 0 0.003 EX4

Orange Juice 499 0 0.003 EX4

Summer Squash 89 0 0.003 EX4

Tomato Paste 290 0 0.003 EX4

Winter Squash 677 0 0.003 EX4

TOTAL 1,732 0

Appendix B. Page 108 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Saflufenacil (herbicide) 

Apple Juice 724 0 0.005 0.03

Bananas 703 0 0.005 0.03

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Cantaloupe 694 0 0.010 NT

Collard Greens 514 0 0.010 NT

Green Beans 177 0 0.003 0.03

Orange Juice 499 0 0.003 0.03

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.003 - 0.020 NT

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 0 0.020 0.03

Tomato Paste 506 0 0.003 - 0.020 NT

Winter Squash 677 0 0.003 NT

TOTAL 6,896 0

S-Bioallethrin (insecticide) 

Green Beans 50 0 0.010 NT

Summer Squash 55 0 0.010 NT

Winter Squash 62 0 0.010 NT

TOTAL 167 0

Sedaxane (fungicide) 

Carrots 499 0 0.050 NT

Eggplant 311 0 0.050 NT

Green Beans 177 0 0.005 0.01

Kiwi Fruit 177 0 0.050 NT

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 2,719 0

Sethoxydim (herbicide) 

Apple Juice 724 0 0.001 0.2

Blueberries, Cultivated, Fresh 168 0 0.003 4.0

Blueberries, Frozen 7 0 0.003 4.0

Cantaloupe 694 1 0.1 0.003 0.003 4.0

Carrots 499 0 0.010 4.0

Collard Greens 514 0 0.003 5.0

Eggplant 311 0 0.010 4.0

Green Beans 177 0 0.003 15

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.003 0.5

Summer Squash 176 0 0.003 - 0.005 4.0

Tangerines 687 0 0.005 0.5

Tomato Paste 506 0 0.003 - 0.005 4.0

Winter Squash 677 0 0.003 4.0

TOTAL 5,816 1

Sethoxydim sulfoxide (herbicide metabolite)

Apple Juice 724 0 0.004 0.2

TOTAL 724 0

Appendix B. Page 109 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Siduron (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Simazine (herbicide) 

Apple Juice 724 0 0.002 0.20

Blueberries, Cultivated, Fresh 168 0 0.005 0.20

Blueberries, Frozen 7 0 0.005 0.20

Broccoli 675 0 0.001 - 0.003 NT

Cantaloupe 694 0 0.005 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.001 - 0.006 NT

Collard Greens 514 0 0.005 NT

Eggplant 661 0 0.001 - 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 0.25

Summer Squash 176 0 0.001 - 0.005 NT

Tangerines 687 1 0.1 0.006 0.005 V-1 NT

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 NT

TOTAL 7,533 1

Simeconazole (fungicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Simetryn (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 3,096 0

Spinetoram (insecticide) 

Apple Juice 724 0 0.010 0.20

Bananas 703 0 0.010 0.25

Blueberries, Cultivated, Fresh 168 7 4.2 0.004 - 0.016 0.003 0.90

Blueberries, Frozen 7 0 0.003 0.90

Broccoli 675 8 1.2 0.004 - 0.030 0.003 2.0

Cantaloupe 694 0 0.003 0.30

Carrots 499 0 0.010 0.10

Cauliflower 692 2 0.3 0.002 - 0.005 0.001 - 0.003 2.0

Collard Greens 498 51 10.2 0.004 - 0.20 0.003 10

Eggplant 661 2 0.3 0.002 0.001 - 0.010 0.40

Green Beans 177 0 0.010 0.30

Appendix B. Page 110 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.010 0.30

Radishes 689 2 0.3 0.012 - 0.014 0.010 0.10

Summer Squash 89 0 0.010 0.30

Sweet Bell Peppers 675 2 0.3 0.011 - 0.030 0.010 0.40

Tangerines 687 0 0.005 0.30

Tomato Paste 506 0 0.005 - 0.010 0.40

Winter Squash 677 0 0.010 0.30

TOTAL 9,497 74

Spinetoram J (metabolite of Spinetoram) 

Summer Squash 87 0 0.005 0.30

TOTAL 87 0

Spinetoram L (metabolite of Spinetoram) 

Summer Squash 87 0 0.005 0.30

TOTAL 87 0

Spinosad (insecticide) (total of spinosyns A and D)

Apple Juice 724 0 0.005 0.20

Bananas 703 0 0.005 0.25

Broccoli 675 11 1.6 0.004 - 0.028 0.003 2.0

Carrots 499 0 0.010 0.10

Cauliflower 692 0 0.003 2.0

Eggplant 661 0 0.003 - 0.010 0.40

Green Beans 177 1 0.6 0.006 0.003 0.30

Kiwi Fruit 177 0 0.010 0.02

Orange Juice 499 0 0.003 0.30

Radishes 689 1 0.1 0.006 0.004 0.10

Summer Squash 89 0 0.003 0.3

Sweet Bell Peppers 662 7 1.1 0.005 - 0.071 0.004 0.40

Tomato Paste 290 0 0.003 0.40

Winter Squash 677 0 0.003 0.3

TOTAL 7,214 20

Spinosad A (isomer of Spinosad) 

Blueberries, Cultivated, Fresh 168 11 6.5 0.004 - 0.044 0.003 0.90

Blueberries, Frozen 7 0 0.003 0.90

Cantaloupe 694 0 0.003 0.3

Collard Greens 514 6 1.2 0.006 - 0.023 0.003 10.0

Summer Squash 87 0 0.002 0.3

Tangerines 687 0 0.002 0.30

Tomato Paste 216 0 0.002 0.40

TOTAL 2,373 17

Spinosad D (isomer of Spinosad) 

Summer Squash 87 0 0.002 0.3

Tangerines 687 0 0.002 0.30

Tomato Paste 216 0 0.002 0.40

TOTAL 990 0

Spirodiclofen (acaricide) 

Apple Juice 724 0 0.004 0.80

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Broccoli 655 1 0.2 0.010 0.006 V-1 NT

Cantaloupe 694 0 0.010 NT

Appendix B. Page 111 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Carrots 499 0 0.010 NT

Cauliflower 692 1 0.1 0.010 0.006 V-1 NT

Collard Greens 514 0 0.010 NT

Eggplant 661 0 0.006 - 0.010 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.003 0.60

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.003 - 0.005 NT

Sweet Bell Peppers 675 0 0.010 NT

Tangerines 687 0 0.005 0.50

Tomato Paste 506 0 0.003 - 0.005 NT

Winter Squash 677 0 0.003 NT

TOTAL 8,877 2

Spiromesifen Total (parent + enol metabolite) (insecticide) 

Broccoli 547 0 0.002 2.0

Cauliflower 692 0 0.002 2.0

Eggplant 350 2 0.6 0.004 0.002 0.45

TOTAL 1,589 2

Spiromesifen (insecticide) 

Blueberries, Cultivated, Fresh 168 0 0.010 2.0

Blueberries, Frozen 7 0 0.010 2.0

Cantaloupe 662 0 0.010 0.10

Carrots 499 0 0.020 NT

Collard Greens 482 0 0.010 12

Eggplant 311 0 0.020 0.45

Green Beans 177 0 0.003 0.80

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.002 NT

Summer Squash 176 0 0.003 - 0.010 0.10

Sweet Bell Peppers 675 85 12.6 0.002 - 0.21 0.002 0.45

Tangerines 687 0 0.010 NT

Tomato Paste 506 0 0.003 - 0.010 0.80

Winter Squash 677 0 0.003 0.10

TOTAL 6,392 85

Spiromesifen alcohol (metabolite of Spiromesifen)

Green Beans 177 0 0.001 0.80

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 0.10

Tomato Paste 290 0 0.001 0.80

Winter Squash 677 0 0.001 0.10

TOTAL 1,732 0

Spiromesifen enol 5 (metabolite of Spiromesifen)

Carrots 499 0 0.010 NT

Eggplant 311 0 0.010 0.45

Kiwi Fruit 177 0 0.010 NT

TOTAL 987 0

Spirotetramat (insecticide) 

Apple Juice 724 0 0.003 0.70

Bananas 703 0 0.003 4.0

Blueberries, Cultivated, Fresh 168 13 7.7 0.005 - 0.47 0.002 3.0

Blueberries, Frozen 7 0 0.002 3.0

Appendix B. Page 112 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Broccoli 675 7 1 0.003 - 0.007 0.002 - 0.005 2.5

Cantaloupe 694 0 0.002 0.30

Carrots 499 0 0.005 0.15

Cauliflower 692 0 0.002 - 0.010 2.5

Collard Greens 514 13 2.5 0.002 - 0.16 0.002 8.0

Eggplant 661 1 0.2 0.003 0.002 - 0.005 2.5

Green Beans 177 0 0.001 2.5

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 0.60

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.001 - 0.002 0.30

Sweet Bell Peppers 675 1 0.1 0.011 0.010 2.5

Tangerines 687 1 0.1 0.002 0.002 0.60

Tomato Paste 506 0 0.001 - 0.002 2.5

Winter Squash 677 0 0.001 0.30

TOTAL 9,600 36

Spiroxamine (fungicide) 

Bananas 703 0 0.001 3.0

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Cantaloupe 694 0 0.010 NT

Carrots 499 0 0.005 NT

Collard Greens 489 0 0.010 NT

Eggplant 311 0 0.005 1.2

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.001 - 0.002 NT

Sweet Bell Peppers 675 0 0.010 1.2

Tangerines 544 0 0.002 NT

Tomato Paste 506 0 0.001 - 0.002 1.2

Winter Squash 677 0 0.001 NT

TOTAL 6,991 0

Sulfallate (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Sulfentrazone (herbicide) 

Carrots 499 0 0.035 NT

Eggplant 311 0 0.035 0.15

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.035 0.15

Orange Juice 499 0 0.003 0.15

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.003 - 0.025 NT

Sweet Bell Peppers 675 0 0.005 0.15

Tangerines 687 0 0.050 0.15

Tomato Paste 506 0 0.003 - 0.050 0.15

Winter Squash 677 0 0.003 NT

TOTAL 5,073 0

Appendix B. Page 113 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Sulfometuron methyl (herbicide) 

Green Beans 177 0 0.010 NT

Orange Juice 499 0 0.010 NT

Summer Squash 89 0 0.010 NT

Tomato Paste 290 0 0.010 NT

Winter Squash 677 0 0.010 NT

TOTAL 1,732 0

Sulfosulfuron (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Sulfoxaflor (insecticide) 

Apple Juice 724 0 0.01 0.50

Carrots 499 0 0.10 0.05

Cauliflower 692 1 0.1 0.005 0.004 0.08

Eggplant 661 14 2.1 0.002 - 0.094 0.001 - 0.10 0.70

Green Beans 177 8 4.5 0.003 - 0.036 0.003 4.0

Orange Juice 499 0 0.003 0.70

Summer Squash 176 1 0.6 0.003 0.003 - 0.050 0.40

Tangerines 687 0 0.15 0.70

Tomato Paste 506 0 0.003 - 0.15 2.60

Winter Squash 677 1 0.1 0.011 0.003 0.40

TOTAL 5,298 25

Sulprofos (insecticide) 

Broccoli 675 0 0.002 NT

Cauliflower 692 0 0.002 NT

Eggplant 350 0 0.002 NT

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 3,449 0

TCMTB (fungicide) 

Carrots 499 0 0.020 NT

Eggplant 311 0 0.020 NT

Green Beans 177 0 0.005 NT

Kiwi Fruit 177 0 0.010 - 0.020 NT

Orange Juice 499 0 0.005 NT

Summer Squash 148 0 0.005 - 0.10 NT

Tangerines 687 0 0.10 NT

Tomato Paste 506 0 0.005 - 0.10 NT

Winter Squash 677 0 0.005 NT

TOTAL 3,681 0

Tebuconazole (fungicide) 

Apple Juice 724 0 0.004 1

Bananas 703 0 0.004 0.05

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Appendix B. Page 114 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Blueberries, Frozen 7 0 0.010 NT

Broccoli 675 1 0.1 0.003 0.001 V-1 NT

Cantaloupe 694 0 0.010 0.4

Carrots 499 1 0.2 0.023 0.015 V-1 NT

Cauliflower 692 0 0.001 NT

Collard Greens 514 12 2.3 0.013 - 1.9 0.010 2.5

Eggplant 661 10 1.5 0.002 - 0.078 0.001 - 0.015 1.3

Green Beans 177 11 6.2 0.003 - 0.054 0.001 0.1

Kiwi Fruit 177 0 0.015 NT

Orange Juice 499 0 0.001 1.0

Radishes 689 0 0.005 NT

Summer Squash 176 3 1.7 0.008 - 0.009 0.001 - 0.005 0.4

Sweet Bell Peppers 675 25 3.7 0.005 - 0.24 0.005 1.3

Tangerines 687 2 0.3 0.005 0.005 V-2 NT

Tomato Paste 506 0 0.001 - 0.005 1.3

Winter Squash 677 50 7.4 0.001 - 0.016 0.001 0.4

TOTAL 9,600 115

Tebufenozide (insecticide) 

Apple Juice 724 0 0.001 1.5

Blueberries, Cultivated, Fresh 168 0 0.002 3.0

Blueberries, Frozen 7 0 0.002 3.0

Broccoli 611 0 0.005 - 0.010 5.0

Cantaloupe 694 0 0.002 NT

Carrots 499 0 0.005 NT

Cauliflower 625 0 0.002 - 0.010 5.0

Collard Greens 514 0 0.002 10.0

Eggplant 648 0 0.002 - 0.010 1.0

Green Beans 177 0 0.005 NT

Kiwi Fruit 177 0 0.005 0.5

Orange Juice 499 0 0.005 2.0

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.005 NT

Sweet Bell Peppers 675 8 1.2 0.007 - 0.038 0.005 1.0

Tangerines 687 0 0.010 2.0

Tomato Paste 506 0 0.005 - 0.010 1.0

Winter Squash 677 0 0.005 NT

TOTAL 8,753 8

Tebufenpyrad (insecticide, acaricide)

Carrots 499 0 0.005 NT

Eggplant 311 0 0.005 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.010 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,083 0

Tebupirimfos (insecticide) 

Broccoli 675 0 0.001 NT

Cauliflower 692 0 0.001 NT

Eggplant 350 0 0.001 NT

Green Beans 177 0 0.001 NT

Appendix B. Page 115 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 3,449 0

Tebutam (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Tebuthiuron (herbicide) 

Broccoli 648 0 0.001 - 0.006 NT

Carrots 499 0 0.010 NT

Cauliflower 670 0 0.003 - 0.006 NT

Eggplant 661 0 0.001 - 0.010 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,210 0

Tecnazene (plant growth regulator) 

Broccoli 675 0 0.001 NT

Cauliflower 692 0 0.001 NT

Eggplant 350 0 0.001 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,813 0

Teflubenzuron (insecticide) 

Apple Juice 724 0 0.006 1.0

Carrots 499 0 0.020 NT

Eggplant 311 0 0.020 NT

Green Beans 177 0 0.005 NT

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 0 0.005 0.60

Summer Squash 89 0 0.005 NT

Tangerines 687 0 0.050 NT

Tomato Paste 475 0 0.005 - 0.050 1.5

Winter Squash 677 0 0.005 NT

TOTAL 4,315 0

Tefluthrin (insecticide) 

Apple Juice 724 0 0.001 NT

Bananas 703 0 0.001 NT

Blueberries, Cultivated, Fresh 168 0 0.002 NT

Blueberries, Frozen 7 0 0.002 NT

Appendix B. Page 116 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Broccoli 675 0 0.001 NT

Cantaloupe 694 0 0.002 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.001 NT

Collard Greens 514 0 0.002 NT

Eggplant 661 0 0.001 - 0.010 NT

Green Beans 177 0 0.001 - 0.003 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.001 - 0.005 NT

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 - 0.003 NT

TOTAL 9,600 0

Temephos (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Tepraloxydim (herbicide) 

Green Beans 177 0 0.01 NT

Orange Juice 499 0 0.01 NT

Summer Squash 89 0 0.01 NT

Tangerines 687 0 0.01 NT

Tomato Paste 506 0 0.01 NT

Winter Squash 677 0 0.01 NT

TOTAL 2,635 0

Terbacil (herbicide) 

Apple Juice 724 0 0.004 0.3

Blueberries, Cultivated, Fresh 168 0 0.010 0.2

Blueberries, Frozen 7 0 0.010 0.2

Broccoli 675 0 0.003 NT

Cantaloupe 694 0 0.010 NT

Carrots 499 0 0.020 NT

Cauliflower 692 0 0.003 NT

Collard Greens 514 0 0.010 NT

Eggplant 661 0 0.003 - 0.020 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.008 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.008 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 7,907 0

Terbufos (insecticide) 

Bananas 703 0 0.005 0.025

Carrots 499 0 0.010 NT

Appendix B. Page 117 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Eggplant 311 0 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Summer Squash 176 0 0.001 - 0.005 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,412 0

Terbufos oxygen analog (metabolite of Terbufos)

Bananas 703 0 0.006 0.025

Carrots 499 0 0.005 NT

Eggplant 311 0 0.005 NT

Kiwi Fruit 177 0 0.005 NT

Summer Squash 87 0 0.001 NT

Tangerines 687 0 0.005 NT

Tomato Paste 216 0 0.005 NT

TOTAL 2,680 0

Terbufos oxygen analog sulfone (metabolite of Terbufos)

Bananas 703 0 0.006 0.025

Carrots 499 0 0.005 NT

Eggplant 311 0 0.005 NT

Green Beans 127 0 0.010 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.010 NT

Summer Squash 121 0 0.005 - 0.010 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.005 - 0.010 NT

Winter Squash 615 0 0.010 NT

TOTAL 4,245 0

Terbufos oxygen analog sulfoxide (metabolite of Terbufos)

Bananas 703 0 0.006 0.025

Summer Squash 87 0 0.005 NT

Tangerines 687 0 0.005 NT

Tomato Paste 216 0 0.005 NT

TOTAL 1,693 0

Terbufos sulfone (metabolite of Terbufos)

Bananas 703 0 0.010 0.025

Broccoli 675 0 0.001 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.001 NT

Eggplant 661 0 0.001 - 0.010 NT

Green Beans 177 0 0.005 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 NT

Tangerines 687 0 0.025 NT

Tomato Paste 506 0 0.005 - 0.025 NT

Winter Squash 677 0 0.005 NT

TOTAL 6,042 0

Terbufos sulfoxide (metabolite of Terbufos)

Bananas 703 0 0.010 0.025

Carrots 499 0 0.005 NT

Appendix B. Page 118 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Eggplant 311 0 0.005 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.003 NT

Summer Squash 176 0 0.002 - 0.003 NT

Tangerines 687 0 0.002 NT

Tomato Paste 506 0 0.002 - 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 4,412 0

Terbuthylazine (herbicide) 

Carrots 499 0 0.005 NT

Eggplant 311 0 0.005 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,083 0

Terbutryn (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 125 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,567 0

Tetrachlorvinphos (insecticide) 

Broccoli 675 0 0.005 - 0.010 NT

Cauliflower 692 0 0.002 - 0.010 NT

Eggplant 350 0 0.002 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tangerines 687 0 0.010 NT

Tomato Paste 506 0 0.001 - 0.010 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,352 0

Tetraconazole (fungicide) 

Blueberries, Cultivated, Fresh 168 0 0.010 0.25

Blueberries, Frozen 7 0 0.010 0.25

Broccoli 648 0 0.001 - 0.003 NT

Cantaloupe 694 0 0.010 0.15

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.001 - 0.006 NT

Collard Greens 514 0 0.010 NT

Eggplant 593 0 0.003 - 0.010 0.30

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Summer Squash 176 3 1.7 0.003 - 0.011 0.001 0.15

Appendix B. Page 119 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tangerines 687 0 0.001 NT

Tomato Paste 506 0 0.001 0.30

Winter Squash 677 0 0.001 0.15

TOTAL 6,714 3

Tetradifon (insecticide) 

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Broccoli 675 0 0.002 NT

Cantaloupe 694 0 0.010 NT

Carrots 499 0 0.020 NT

Cauliflower 692 0 0.002 NT

Collard Greens 514 0 0.010 NT

Eggplant 661 0 0.002 - 0.020 NT

Green Beans 177 0 0.003 - 0.005 NT

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.003 - 0.005 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 - 0.005 NT

TOTAL 7,183 0

Tetrahydrophthalimide - THPI (metabolite of Captafol and Captan)

Apple Juice 724 209 28.9 0.012 - 1.7 0.007 25.0

Blueberries, Cultivated, Fresh 168 10 6 0.011 - 0.21 0.010 20.0

Blueberries, Frozen 7 4 57.1 0.069 - 0.45 0.010 20.0

Broccoli 675 0 0.004 0.05

Cantaloupe 694 0 0.010 0.05

Cauliflower 672 0 0.004 0.05

Collard Greens 514 3 0.6 0.043 - 0.42 0.010 X-2 0.05

Eggplant 333 0 0.012 - 0.024 0.05

Green Beans 177 3 1.7 0.007 - 0.012 0.005 0.05

Orange Juice 499 0 0.005 NT

Summer Squash 89 1 1.1 0.008 0.005 0.05

Tomato Paste 290 0 0.005 0.05

Winter Squash 677 1 0.1 0.014 0.005 0.05

TOTAL 5,519 231

Tetramethrin (insecticide) 

Apple Juice 724 0 0.006 NT

Bananas 703 0 0.006 NT

Blueberries, Cultivated, Fresh 168 0 0.005 NT

Blueberries, Frozen 7 0 0.005 NT

Cantaloupe 694 0 0.005 NT

Carrots 499 0 0.025 NT

Collard Greens 514 0 0.005 NT

Eggplant 311 0 0.025 NT

Green Beans 177 0 0.005 NT

Kiwi Fruit 177 0 0.10 NT

Orange Juice 499 0 0.005 NT

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.005 - 0.010 NT

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 0 0.010 NT

Appendix B. Page 120 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomato Paste 506 0 0.005 - 0.010 NT

Winter Squash 677 0 0.005 NT

TOTAL 7,883 0

Thiabendazole (fungicide) (parent of 5-hydroxythiabendazole)

Apple Juice 724 161 22.2 0.005 - 0.20 0.003 5.0

Bananas 703 288 41 0.005 - 0.21 0.003 3.0

Blueberries, Cultivated, Fresh 168 1 0.6 0.008 0.002 V-1 NT

Blueberries, Frozen 7 0 0.002 NT

Broccoli 675 0 0.003 0.02

Cantaloupe 694 35 5 0.002 - 0.27 0.002 15.0

Carrots 499 1 0.2 0.006 0.005 10.0

Cauliflower 692 5 0.7 0.002 - 0.005 0.001 0.02

Collard Greens 482 0 0.002 NT

Eggplant 661 0 0.003 - 0.005 NT

Green Beans 177 1 0.6 0.003 0.001 0.02

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 133 26.7 0.001 - 0.12 0.001 10.0

Radishes 689 0 0.010 0.02

Summer Squash 176 0 0.001 - 0.005 0.02

Sweet Bell Peppers 675 0 0.010 NT

Tangerines 687 530 77.1 0.011 - 1.2 0.010 10.0

Tomato Paste 506 1 0.2 0.002 0.001 - 0.010 V-1 NT

Winter Squash 677 2 0.3 0.002 - 0.014 0.001 0.02

TOTAL 9,568 1,158

Thiacloprid (insecticide) 

Apple Juice 724 0 0.007 0.30

Blueberries, Cultivated, Fresh 168 0 0.001 NT

Blueberries, Frozen 7 0 0.001 NT

Broccoli 675 0 0.001 NT

Cantaloupe 694 0 0.001 NT

Carrots 499 0 0.005 NT

Cauliflower 692 0 0.001 NT

Collard Greens 514 0 0.001 NT

Eggplant 661 7 1.1 0.002 - 0.049 0.001 - 0.005 V-7 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.001 - 0.005 NT

Sweet Bell Peppers 675 48 7.1 0.010 - 0.12 0.010 1.0

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 NT

TOTAL 8,897 55

Thiamethoxam (insecticide) (also a parent of Clothianidin)

Apple Juice 724 0 0.025 0.2

Bananas 703 0 0.025 0.03

Blueberries, Cultivated, Fresh 168 3 1.8 0.003 - 0.12 0.003 0.30

Blueberries, Frozen 7 0 0.003 0.30

Broccoli 675 128 19 0.003 - 0.059 0.002 4.5

Cantaloupe 694 71 10.2 0.003 - 0.040 0.003 0.2

Carrots 499 0 0.005 0.05

Cauliflower 664 172 25.9 0.003 - 0.027 0.002 4.5

Collard Greens 514 105 20.4 0.003 - 0.69 0.003 3.0

Appendix B. Page 121 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Eggplant 661 179 27.1 0.003 - 0.10 0.002 - 0.005 0.25

Green Beans 177 0 0.001 0.02

Kiwi Fruit 177 0 0.005 0.02

Orange Juice 499 1 0.2 0.001 0.001 0.40

Radishes 689 8 1.2 0.014 - 0.087 0.010 X-1 0.05

Summer Squash 176 52 29.5 0.001 - 0.17 0.001 - 0.010 0.2

Sweet Bell Peppers 675 152 22.5 0.010 - 0.48 0.010 X-4 0.25

Tangerines 687 0 0.020 0.40

Tomato Paste 506 64 12.6 0.001 - 0.008 0.001 - 0.020 0.80

Winter Squash 677 97 14.3 0.001 - 0.022 0.001 0.2

TOTAL 9,572 1,032

Thiazopyr (herbicide) 

Blueberries, Cultivated, Fresh 168 0 0.008 NT

Blueberries, Frozen 7 0 0.008 NT

Cantaloupe 694 0 0.008 NT

Collard Greens 514 0 0.008 NT

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 176 0 0.001 - 0.003 NT

Tangerines 687 0 0.001 NT

Tomato Paste 506 0 0.001 - 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 4,105 0

Thidiazuron (plant growth regulator) 

Green Beans 177 0 0.005 NT

Orange Juice 499 0 0.005 NT

Summer Squash 89 0 0.005 NT

Tomato Paste 290 0 0.005 NT

Winter Squash 677 0 0.005 NT

TOTAL 1,732 0

Thiencarbazone methyl (herbicide) 

Carrots 499 0 0.020 NT

Eggplant 311 0 0.020 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.020 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 2,719 0

Thifensulfuron methyl (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Thiobencarb (herbicide) 

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Broccoli 675 1 0.1 0.034 0.003 V-1 NT

Cantaloupe 694 0 0.010 NT

Appendix B. Page 122 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Cauliflower 692 2 0.3 0.002 - 0.009 0.001 V-2 NT

Collard Greens 514 0 0.010 NT

Eggplant 350 0 0.001 NT

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 4,832 3

Thiodicarb (insecticide) 

Blueberries, Cultivated, Fresh 168 0 0.003 NT

Blueberries, Frozen 7 0 0.003 NT

Carrots 499 0 0.020 NT

Collard Greens 514 0 0.003 NT

Eggplant 311 0 0.020 NT

Green Beans 177 0 0.010 NT

Kiwi Fruit 177 0 0.010 - 0.020 NT

Orange Juice 499 0 0.010 NT

Summer Squash 89 0 0.010 NT

Tomato Paste 290 0 0.010 NT

Winter Squash 677 0 0.010 NT

TOTAL 3,408 0

Thionazin (insecticide, fumigant)

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 NT

Summer Squash 89 0 0.003 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 1,732 0

Thiophanate methyl (fungicide) 

Apple Juice 724 0 0.020 2.0

Bananas 703 0 0.020 2.0

Carrots 499 0 0.10 - 0.20 NT

Eggplant 311 1 0.3 0.11 0.10 V-1 NT

Summer Squash 87 0 0.020 1.0

Tangerines 687 0 0.020 NT

Tomato Paste 216 0 0.020 NT

TOTAL 3,227 1

Tolclofos methyl (fungicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Tolfenpyrad (insecticide) 

Apple Juice 724 0 0.002 1.0

Carrots 499 0 0.025 NT

Eggplant 311 1 0.3 0.043 0.025 1.5

Green Beans 177 0 0.003 NT

Orange Juice 499 0 0.003 1.5

Summer Squash 176 0 0.003 - 0.005 0.70

Appendix B. Page 123 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tangerines 687 0 0.005 1.5

Tomato Paste 506 0 0.003 - 0.005 1.5

Winter Squash 677 0 0.003 0.70

TOTAL 4,256 1

Tolylfluanid (fungicide) 

Apple Juice 724 0 0.003 5.0

Carrots 499 0 0.050 NT

Eggplant 311 0 0.050 NT

Kiwi Fruit 177 0 0.050 NT

TOTAL 1,711 0

Tri-Allate (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.001 - 0.005 NT

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,086 0

Triadimefon (fungicide) (also a parent of Triadimenol)

Broccoli 675 0 0.001 NT

Carrots 499 0 0.005 NT

Cauliflower 692 0 0.001 NT

Eggplant 661 0 0.001 - 0.005 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.003 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.003 NT

Winter Squash 677 0 0.003 NT

TOTAL 5,800 0

Triadimenol (fungicide) (also a metabolite of Triadimefon)

Bananas 703 0 0.007 0.2

Carrots 499 0 0.040 NT

Eggplant 311 0 0.040 NT

Green Beans 177 0 0.020 - 0.040 NT

Kiwi Fruit 177 0 0.040 NT

Orange Juice 499 0 0.020 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.020 - 0.040 NT

Sweet Bell Peppers 675 0 0.005 NT

Tomato Paste 290 0 0.020 NT

Winter Squash 677 0 0.020 - 0.040 NT

TOTAL 4,786 0

Triasulfuron (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Appendix B. Page 124 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Triazophos (insecticide) 

Carrots 499 0 0.010 NT

Eggplant 311 0 0.010 NT

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.010 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 4,083 0

Tribenuron methyl (herbicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Trichlorfon (insecticide) 

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Cantaloupe 694 0 0.010 NT

Carrots 499 0 0.050 NT

Collard Greens 514 0 0.010 NT

Eggplant 311 0 0.050 - 0.10 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.050 - 0.10 NT

Orange Juice 499 0 0.003 NT

Summer Squash 176 0 0.003 - 0.040 NT

Tangerines 687 0 0.040 NT

Tomato Paste 506 0 0.003 - 0.040 NT

Winter Squash 677 0 0.003 NT

TOTAL 5,092 0

Trichloronate (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Tricyclazole (fungicide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Appendix B. Page 125 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tridemorph (fungicide) 

Bananas 703 0 0.025 1.0

TOTAL 703 0

Trifloxystrobin (fungicide) 

Apple Juice 724 0 0.001 0.5

Bananas 703 0 0.001 0.10

Blueberries, Cultivated, Fresh 168 0 0.002 1.5

Blueberries, Frozen 7 0 0.002 1.5

Broccoli 675 1 0.1 0.005 0.003 2.0

Cantaloupe 694 0 0.002 0.50

Carrots 499 0 0.005 0.1

Cauliflower 692 1 0.1 0.002 0.001 2.0

Collard Greens 514 6 1.2 0.002 - 0.84 0.002 30

Eggplant 661 1 0.2 0.002 0.001 - 0.005 0.5

Green Beans 177 0 0.001 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.001 0.6

Radishes 689 0 0.005 0.1

Summer Squash 176 0 0.001 0.50

Sweet Bell Peppers 675 21 3.1 0.005 - 0.062 0.005 0.5

Tangerines 687 0 0.001 0.6

Tomato Paste 506 51 10.1 0.001 - 0.011 0.001 0.5

Winter Squash 677 10 1.5 0.001 - 0.007 0.001 0.50

TOTAL 9,600 91

Trifloxysulfuron (herbicide) 

Blueberries, Cultivated, Fresh 136 0 0.020 NT

Blueberries, Frozen 7 0 0.020 NT

Cantaloupe 664 0 0.020 NT

Collard Greens 514 0 0.020 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 0.03

Summer Squash 176 0 0.001 - 0.010 NT

Tangerines 687 0 0.010 0.03

Tomato Paste 506 0 0.001 - 0.010 0.01

Winter Squash 677 0 0.001 NT

TOTAL 4,043 0

Triflumezopyrim (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Triflumizole (fungicide) 

Apple Juice 724 0 0.001 0.50

Blueberries, Cultivated, Fresh 168 0 0.010 2.0

Blueberries, Frozen 7 0 0.010 2.0

Broccoli 675 0 0.002 8.0

Cantaloupe 694 1 0.1 0.019 0.010 0.5

Carrots 499 0 0.005 NT

Cauliflower 692 0 0.002 8.0

Collard Greens 514 0 0.010 40

Eggplant 661 0 0.002 - 0.005 NT

Appendix B. Page 126 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.005 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.003 NT

Summer Squash 176 2 1.1 0.011 - 0.016 0.003 - 0.010 0.5

Sweet Bell Peppers 675 0 0.003 NT

Tangerines 687 0 0.010 NT

Tomato Paste 506 0 0.003 - 0.010 1.5

Winter Squash 677 1 0.1 0.004 0.003 0.5

TOTAL 8,897 4

Trifluralin (herbicide) 

Blueberries, Cultivated, Fresh 168 0 0.001 NT

Blueberries, Frozen 7 0 0.001 NT

Broccoli 675 4 0.6 0.002 0.001 0.05

Cantaloupe 694 0 0.001 0.05

Carrots 499 4 0.8 0.010 - 0.042 0.010 1.0

Cauliflower 692 0 0.001 0.05

Collard Greens 514 14 2.7 0.001 - 0.003 0.001 0.05

Eggplant 661 0 0.001 - 0.010 0.05

Green Beans 177 0 0.001 0.05

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 0.05

Radishes 689 4 0.6 0.007 - 0.010 0.005 0.05

Summer Squash 176 0 0.001 - 0.005 0.05

Sweet Bell Peppers 675 0 0.005 0.05

Tangerines 687 0 0.005 0.05

Tomato Paste 506 1 0.2 0.001 0.001 - 0.005 0.05

Winter Squash 677 1 0.1 0.001 0.001 0.05

TOTAL 8,173 28

Triforine (fungicide) 

Blueberries, Cultivated, Fresh 168 0 0.010 1.0

Blueberries, Frozen 7 0 0.010 1.0

Cantaloupe 694 0 0.010 NT

Collard Greens 514 0 0.010 NT

TOTAL 1,383 0

Triticonazole (fungicide) 

Carrots 499 0 0.010 NT

Eggplant 311 0 0.010 NT

Green Beans 177 0 0.003 NT

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.003 NT

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.003 - 0.005 NT

Sweet Bell Peppers 675 0 0.010 NT

Tangerines 687 0 0.010 NT

Tomato Paste 506 0 0.003 - 0.010 NT

Winter Squash 677 0 0.003 NT

TOTAL 5,073 0

Uniconazole (fungicide) 

Carrots 499 0 0.020 NT

Eggplant 311 0 0.020 0.01

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Appendix B. Page 127 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 0.01

Winter Squash 677 0 0.001 NT

TOTAL 2,542 0

Valifenalate (fungicide) 

Green Beans 177 0 0.001 NT

Summer Squash 176 0 0.001 - 0.010 0.3

Winter Squash 62 0 0.001 0.3

TOTAL 415 0

Vamidothion (insecticide) 

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 1,732 0

Vernolate (herbicide) 

Green Beans 177 0 0.010 - 0.040 NT

Orange Juice 499 0 0.010 NT

Radishes 689 0 0.010 NT

Summer Squash 89 0 0.010 - 0.040 NT

Sweet Bell Peppers 675 0 0.010 NT

Tomato Paste 290 0 0.010 NT

Winter Squash 677 0 0.010 - 0.040 NT

TOTAL 3,096 0

Vinclozolin (fungicide) 

Blueberries, Cultivated, Fresh 168 0 0.010 NT

Blueberries, Frozen 7 0 0.010 NT

Broccoli 675 0 0.001 NT

Cantaloupe 694 0 0.010 NT

Carrots 499 0 0.010 NT

Cauliflower 692 0 0.001 NT

Collard Greens 514 0 0.010 NT

Eggplant 661 0 0.001 - 0.010 NT

Green Beans 177 0 0.001 2.0

Kiwi Fruit 177 0 0.010 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 89 0 0.001 NT

Sweet Bell Peppers 675 0 0.005 3.0

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 7,183 0

Zoxamide (fungicide) 

Carrots 499 0 0.020 NT

Eggplant 311 0 0.020 1.0

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.010 NT

Summer Squash 176 0 0.001 - 0.002 1.0

Sweet Bell Peppers 675 0 0.010 1.0

Tangerines 687 0 0.002 NT

Appendix B. Page 128 of 129
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^ 

 Tolerance 

Violation

EPA 

Tolerance 

Level, ppm

Tomato Paste 506 0 0.001 - 0.002 2.0

Winter Squash 677 3 0.4 0.001 - 0.060 0.001 1.0

TOTAL 4,896 3

NOTES

^ = When a range is not listed, only one distinct detected concentration or LOD value was reported for the pesticide/commodity pair.

NT = No tolerance level was set for that pesticide/commodity pair.

EX1 = Exempt from the requirement of a tolerance in or on raw agricultural commodities that have no established tolerance when residues

are present as a result of subsequent uptake by crops rotated into fields where crops with tolerances were treated with cyclaniliprole.

EX2 = Exempt from the requirement of a tolerance in or on all food and feed commodities when applied as an herbicide in accordance

with good agricultural practices.

EX3 = Exempt from the requirement of a tolerance in or on all food commodities when used to control insect larvae.

EX4 = Exempt from the requirement of a tolerance when applied to growing crops in accordance with good agricultural practices.

1 Emamectin benzoate is the salt form of the active, Emamectin.

2 Halosulfuron methyl is the salt form of the active, Halosulfuron.

3 Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one of the spatial

isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable via multiresidue methods.

4 Propamocarb analytically determined as the salt (hydrochloride).

5 Enol metabolite calculated as the parent, Spiromesifen.

(X) = Residue was found which exceeds EPA tolerance or FDA action level. Following "X" are the number of occurrences. Refer to

pages 1 and 2 in Appendix H to see the sample origin (domestic, imported, or unknown) for each occurrence.

(V) = Residue was found where no tolerance was established by EPA. Following "V" are the number of occurrences. Refer to

pages 3 through 5 in Appendix H to see the number of occurrences broken down by sample origin (domestic, imported, or

unknown) for a commodity/pesticide pair.

Many of the listed tolerances are the sum of a parent compound and metabolite(s)/isomer(s). The reader is 

advised to refer to EPA for the complete listing of compounds in tolerance expressions. The cited tolerances

apply to 2020 and not to the current year. There may be instances where a tolerance was recently set or revoked 

that would have an effect on whether a residue is violative or not. 

Appendix B. Page 129 of 129
Appendix C

Distribution of Residues 

for Environmental Contaminants

Appendix C shows residue detections across all commodities for 21 compounds identified as 

environmental contaminants, including range of values detected, range of Limits of Detection 

(LODs), and U.S. Environmental Protection Agency (EPA) tolerances or U.S. Food and Drug 

Administration (FDA) Action Levels for each pair. Results for environmental contaminants have 

been consolidated in this appendix because they have no registered uses and are not applied to 

crops.

The EPA tolerances cited in this summary and appendixes apply to 2020 and not to the current 

year. There may be instances where tolerances have been recently set, modified or revoked 

that would have an effect on whether a residue is violative or not.

Action Levels (ALs) are shown in this appendix, where applicable, and denote AL values 

established by FDA. ALs are used for environmental contaminants when tolerances are not 

available.

PDP reports tolerance violations to FDA as part of an interagency Memorandum of 

Understanding between the U.S. Department of Agriculture and FDA. Residues reported to 

FDA are shown in the “Pesticide/Commodity” column to the right of the commodity and are 

annotated as “X” (if the residue exceeded the established tolerance) or “V” (if the residue did not 

have a tolerance listed in the Code of Federal Regulations, Title 40, Part 180). In both cases, 

these annotations are followed by a number indicating the number of samples reported to FDA. 
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

Aldrin (insecticide) (parent of Dieldrin)

Apple Juice 724 0 0.004 0.03 AL

Bananas 703 0 0.004 0.02 AL

Blueberries, Cultivated, Fresh 168 0 0.003 0.05 AL

Blueberries, Frozen 7 0 0.003 0.05 AL

Broccoli 675 0 0.001 0.03 AL

Cantaloupe 694 0 0.003 0.1 AL

Carrots 499 0 0.020 0.1 AL

Cauliflower 692 0 0.001 0.03 AL

Collard Greens 514 0 0.003 0.05 AL

Eggplant 661 0 0.001 - 0.020 0.05 AL

Green Beans 177 0 0.001 0.05 AL

Kiwi Fruit 177 0 0.040 0.05 AL

Orange Juice 499 0 0.001 0.02 AL

Radishes 689 0 0.005 0.1 AL

Summer Squash 176 0 0.001 - 0.005 0.1 AL

Sweet Bell Peppers 675 0 0.005 0.05 AL

Tangerines 687 0 0.005 0.02 AL

Tomato Paste 506 0 0.001 - 0.005 0.05 AL

Winter Squash 677 0 0.001 0.1 AL

TOTAL 9,600 0

BHC alpha (insecticide) (isomer of BHC)

Apple Juice 724 0 0.001 0.05 AL

Blueberries, Cultivated, Fresh 168 0 0.012 0.05 AL

Blueberries, Frozen 7 0 0.012 0.05 AL

Broccoli 675 0 0.001 0.05 AL

Cantaloupe 694 0 0.012 0.05 AL

Carrots 499 0 0.005 0.3 AL

Cauliflower 692 0 0.001 0.05 AL

Collard Greens 514 0 0.012 0.05 AL

Eggplant 661 0 0.001 - 0.005 0.05 AL

Green Beans 177 0 0.001 0.05 AL

Kiwi Fruit 177 0 0.010 0.05 AL

Orange Juice 499 0 0.001 0.05 AL

Radishes 689 0 0.005 0.05 AL

Summer Squash 176 0 0.001 - 0.010 0.05 AL

Sweet Bell Peppers 675 0 0.005 0.05 AL

Tangerines 687 0 0.010 0.05 AL

Tomato Paste 506 0 0.001 - 0.010 0.05 AL

Winter Squash 677 0 0.001 0.05 AL

TOTAL 8,897 0

BHC beta (isomer of BHC)

Apple Juice 724 0 0.003 0.05 AL

Blueberries, Cultivated, Fresh 168 0 0.014 0.05 AL

Blueberries, Frozen 7 0 0.014 0.05 AL

Cantaloupe 694 0 0.014 0.5 AL

Collard Greens 514 0 0.014 0.05 AL

Green Beans 177 0 0.001 0.05 AL

Orange Juice 499 0 0.001 0.05 AL

Radishes 689 0 0.005 0.05 AL

Summer Squash 176 0 0.001 - 0.005 0.05 AL

Sweet Bell Peppers 675 0 0.005 0.05 AL

Tangerines 687 0 0.005 0.05 AL

APPENDIX C. DISTRIBUTION OF RESIDUES FOR ENVIRONMENTAL CONTAMINANTS

Appendix C. Page 1 of 7
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

Tomato Paste 506 0 0.001 - 0.005 0.05 AL

Winter Squash 677 0 0.001 0.05 AL

TOTAL 6,193 0

BHC delta (isomer of BHC)

Carrots 499 0 0.005 0.3 AL

Eggplant 311 0 0.005 0.05 AL

Green Beans 177 0 0.001 0.05 AL

Orange Juice 499 0 0.001 0.05 AL

Summer Squash 89 0 0.001 0.05 AL

Tomato Paste 290 0 0.001 0.05 AL

Winter Squash 677 0 0.001 0.05 AL

TOTAL 2,542 0

BHC epsilon (isomer of BHC)

Carrots 499 0 0.005 0.3 AL

Eggplant 311 0 0.005 0.05 AL

TOTAL 810 0

Chlordane cis (insecticide) (isomer of Chlordane)

Apple Juice 724 0 0.002 0.1 AL

Bananas 703 0 0.002 0.1 AL

Blueberries, Cultivated, Fresh 168 0 0.010 0.1 AL

Blueberries, Frozen 7 0 0.010 0.1 AL

Broccoli 675 0 0.001 0.1 AL

Cantaloupe 694 0 0.010 0.1 AL

Carrots 499 0 0.010 0.1 AL

Cauliflower 692 0 0.001 0.1 AL

Collard Greens 514 0 0.010 0.1 AL

Eggplant 661 0 0.001 - 0.010 0.1 AL

Green Beans 177 0 0.001 0.1 AL

Kiwi Fruit 177 0 0.010 0.1 AL

Orange Juice 499 0 0.001 0.1 AL

Radishes 689 0 0.005 0.1 AL

Summer Squash 89 3 3.4 0.002 - 0.008 0.001 0.1 AL

Sweet Bell Peppers 675 0 0.005 0.1 AL

Tangerines 687 0 0.010 0.1 AL

Tomato Paste 506 0 0.001 - 0.010 0.1 AL

Winter Squash 677 5 0.7 0.004 - 0.029 0.001 0.1 AL

TOTAL 9,513 8

Chlordane trans (isomer of Chlordane)

Apple Juice 724 1 0.1 0.019 0.002 0.1 AL

Bananas 703 0 0.002 0.1 AL

Blueberries, Cultivated, Fresh 168 0 0.010 0.1 AL

Blueberries, Frozen 7 0 0.010 0.1 AL

Broccoli 675 0 0.001 0.1 AL

Cantaloupe 694 0 0.010 0.1 AL

Carrots 499 0 0.010 0.1 AL

Cauliflower 692 0 0.001 0.1 AL

Collard Greens 514 0 0.010 0.1 AL

Eggplant 661 0 0.001 - 0.010 0.1 AL

Green Beans 177 0 0.001 0.1 AL

Kiwi Fruit 177 0 0.010 0.1 AL

Orange Juice 499 0 0.001 0.1 AL

Radishes 689 0 0.005 0.1 AL

Summer Squash 89 1 1.1 0.002 0.001 0.1 AL

Sweet Bell Peppers 675 0 0.005 0.1 AL

Appendix C. Page 2 of 7
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

Tangerines 687 0 0.005 0.1 AL

Tomato Paste 506 0 0.001 - 0.005 0.1 AL

Winter Squash 677 5 0.7 0.002 - 0.004 0.001 0.1 AL

TOTAL 9,513 7

DDD o,p' (metabolite of DDT)

Blueberries, Cultivated, Fresh 168 0 0.001 0.1 AL

Blueberries, Frozen 7 0 0.001 0.1 AL

Broccoli 675 0 0.001 0.5 AL

Cantaloupe 694 0 0.001 0.1 AL

Cauliflower 692 0 0.001 0.5 AL

Collard Greens 514 1 0.2 0.001 0.001 0.5 AL

Eggplant 350 0 0.001 0.1 AL

Green Beans 177 0 0.001 0.2 AL

Orange Juice 499 0 0.001 0.1 AL

Summer Squash 89 0 0.001 0.1 AL

Tomato Paste 290 0 0.001 0.05 AL

Winter Squash 677 1 0.1 0.002 0.001 0.1 AL

TOTAL 4,832 2

DDD p,p' (metabolite of DDT)

Blueberries, Cultivated, Fresh 168 0 0.005 0.1 AL

Blueberries, Frozen 7 0 0.005 0.1 AL

Broccoli 675 0 0.001 0.5 AL

Cantaloupe 694 0 0.005 0.1 AL

Carrots 499 0 0.005 3 AL

Cauliflower 692 0 0.001 0.5 AL

Collard Greens 514 0 0.005 0.5 AL

Eggplant 661 0 0.001 - 0.005 0.1 AL

Kiwi Fruit 177 0 0.005 0.1 AL

Radishes 689 0 0.005 0.2 AL

Summer Squash 87 0 0.005 0.1 AL

Sweet Bell Peppers 675 0 0.005 0.1 AL

Tangerines 687 0 0.005 0.1 AL

Tomato Paste 216 0 0.005 0.05 AL

TOTAL 6,441 0

DDE o,p' (metabolite of DDT)

Apple Juice 724 0 0.002 0.1 AL

Blueberries, Cultivated, Fresh 168 0 0.001 0.1 AL

Blueberries, Frozen 7 0 0.001 0.1 AL

Cantaloupe 694 0 0.001 0.1 AL

Collard Greens 514 0 0.001 0.5 AL

Green Beans 177 0 0.001 0.2 AL

Orange Juice 499 0 0.001 0.1 AL

Summer Squash 89 0 0.001 0.1 AL

Tomato Paste 290 0 0.001 0.05 AL

Winter Squash 677 0 0.001 0.1 AL

TOTAL 3,839 0

DDE p,p' (metabolite of DDT)

Apple Juice 724 0 0.001 0.1 AL

Blueberries, Cultivated, Fresh 168 0 0.010 0.1 AL

Blueberries, Frozen 7 0 0.010 0.1 AL

Broccoli 675 26 3.9 0.002 0.001 0.5 AL

Cantaloupe 694 0 0.010 0.1 AL

Carrots 499 23 4.6 0.010 - 0.031 0.010 3 AL

Cauliflower 692 0 0.001 0.5 AL

Appendix C. Page 3 of 7
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

Collard Greens 514 5 1 0.012 - 0.018 0.010 0.5 AL

Eggplant 661 0 0.001 - 0.010 0.1 AL

Green Beans 177 3 1.7 0.002 - 0.006 0.001 0.2 AL

Kiwi Fruit 177 0 0.005 0.1 AL

Orange Juice 499 0 0.001 0.1 AL

Radishes 689 24 3.5 0.005 - 0.019 0.005 0.2 AL

Summer Squash 89 3 3.4 0.002 - 0.012 0.001 0.1 AL

Sweet Bell Peppers 675 0 0.005 0.1 AL

Tangerines 687 0 0.005 0.1 AL

Tomato Paste 506 0 0.001 - 0.005 0.05 AL

Winter Squash 677 19 2.8 0.001 - 0.011 0.001 0.1 AL

TOTAL 8,810 103

DDT o,p' (insecticide) 

Apple Juice 724 0 0.004 0.1 AL

Broccoli 675 0 0.001 0.5 AL

Cauliflower 692 0 0.001 - 0.003 0.5 AL

Eggplant 350 0 0.001 - 0.003 0.1 AL

Green Beans 177 0 0.001 0.2 AL

Orange Juice 466 0 0.001 0.1 AL

Summer Squash 89 2 2.2 0.001 - 0.004 0.001 0.1 AL

Tomato Paste 290 0 0.001 0.05 AL

Winter Squash 677 5 0.7 0.001 - 0.003 0.001 0.1 AL

TOTAL 4,140 7

DDT p,p' (insecticide) 

Apple Juice 724 0 0.002 0.1 AL

Blueberries, Cultivated, Fresh 168 0 0.001 0.1 AL

Blueberries, Frozen 7 0 0.001 0.1 AL

Broccoli 675 0 0.001 - 0.003 0.5 AL

Cantaloupe 694 0 0.001 0.1 AL

Carrots 499 0 0.010 3 AL

Cauliflower 692 0 0.001 - 0.006 0.5 AL

Eggplant 661 0 0.003 - 0.010 0.1 AL

Green Beans 143 0 0.001 0.2 AL

Kiwi Fruit 177 0 0.040 0.1 AL

Orange Juice 499 0 0.001 0.1 AL

Radishes 689 1 0.1 0.005 0.005 0.2 AL

Summer Squash 89 1 1.1 0.003 0.001 0.1 AL

Sweet Bell Peppers 655 0 0.005 0.1 AL

Tomato Paste 290 0 0.001 0.05 AL

Winter Squash 677 7 1 0.001 - 0.004 0.001 - 0.008 0.1 AL

TOTAL 7,339 9

Dieldrin (insecticide) (also a metabolite of Aldrin)

Apple Juice 724 0 0.004 0.03 AL

Bananas 703 0 0.004 0.02 AL

Blueberries, Cultivated, Fresh 168 0 0.010 0.05 AL

Blueberries, Frozen 7 0 0.010 0.05 AL

Broccoli 675 0 0.002 0.03 AL

Cantaloupe 694 6 0.9 0.011 - 0.048 0.010 0.1 AL

Carrots 499 2 0.4 0.020 - 0.023 0.020 0.1 AL

Cauliflower 692 0 0.002 0.03 AL

Collard Greens 514 1 0.2 0.016 0.010 0.05 AL

Eggplant 661 0 0.002 - 0.020 0.05 AL

Green Beans 177 0 0.003 0.05 AL

Kiwi Fruit 177 0 0.040 0.05 AL

Orange Juice 499 0 0.003 0.02 AL

Appendix C. Page 4 of 7
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

Radishes 689 1 0.1 0.006 0.005 0.1 AL

Summer Squash 89 16 18 0.003 - 0.045 0.003 0.1 AL

Sweet Bell Peppers 675 0 0.005 0.05 AL

Tangerines 687 0 0.025 0.02 AL

Tomato Paste 506 0 0.003 - 0.025 0.05 AL

Winter Squash 677 63 9.3 0.003 - 0.11 0.003 0.1 AL

TOTAL 9,513 89

Endrin (insecticide) 

Blueberries, Cultivated, Fresh 168 0 0.010 0.05 AL

Blueberries, Frozen 7 0 0.010 0.05 AL

Broccoli 675 0 0.005 0.03 AL

Cantaloupe 694 0 0.010 0.03 AL

Carrots 499 0 0.020 0.1 AL

Cauliflower 692 0 0.005 0.1 AL

Collard Greens 514 0 0.010 0.05 AL

Eggplant 661 0 0.005 - 0.020 0.05 AL

Green Beans 177 0 0.003 0.05 AL

Kiwi Fruit 177 0 0.035 0.05 AL

Orange Juice 499 0 0.003 0.02 AL

Radishes 689 0 0.005 0.1 AL

Summer Squash 176 6 3.4 0.003 - 0.007 0.003 - 0.005 0.1 AL

Sweet Bell Peppers 675 0 0.005 0.05 AL

Tangerines 687 0 0.005 0.02 AL

Tomato Paste 506 0 0.003 - 0.005 0.05 AL

Winter Squash 677 3 0.4 0.003 - 0.005 0.003 0.1 AL

TOTAL 8,173 9

Heptachlor (insecticide) 

Apple Juice 724 0 0.001 NT

Blueberries, Cultivated, Fresh 168 0 0.002 0.05 AL

Blueberries, Frozen 7 0 0.002 0.05 AL

Broccoli 675 0 0.001 0.05 AL

Cantaloupe 694 0 0.002 0.05 AL

Carrots 499 0 0.025 NT

Cauliflower 692 0 0.001 0.05 AL

Collard Greens 514 1 0.2 0.003 0.002 0.05 AL

Eggplant 661 0 0.001 - 0.025 0.03 AL

Green Beans 177 0 0.001 0.05 AL

Kiwi Fruit 177 0 0.10 0.05 AL

Orange Juice 499 0 0.001 0.05 AL

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.001 0.05 AL

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 0 0.001 0.05 AL

Tomato Paste 506 0 0.001 NT

Winter Squash 677 0 0.001 0.05 AL

TOTAL 8,897 1

Heptachlor epoxide (metabolite of Heptachlor)

Apple Juice 724 0 0.002 NT

Blueberries, Cultivated, Fresh 168 0 0.005 0.05 AL

Blueberries, Frozen 7 0 0.005 0.05 AL

Broccoli 675 0 0.002 0.05 AL

Cantaloupe 694 0 0.005 0.05 AL

Carrots 499 0 0.040 NT

Cauliflower 692 0 0.002 0.05 AL

Collard Greens 514 0 0.005 0.05 AL

Appendix C. Page 5 of 7
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

Eggplant 661 0 0.002 - 0.040 0.03 AL

Green Beans 177 0 0.001 0.05 AL

Kiwi Fruit 177 0 0.040 0.05 AL

Orange Juice 499 0 0.001 0.05 AL

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.001 0.05 AL

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 0 0.001 0.05 AL

Tomato Paste 506 0 0.001 NT

Winter Squash 677 7 1 0.002 - 0.011 0.001 0.05 AL

TOTAL 8,897 7

Hexachlorobenzene - HCB (fungicide) (metabolite and impurity of Quintozene)

Carrots 499 0 0.005 NT

Eggplant 311 0 0.005 0.1

Green Beans 177 0 0.001 0.1

Orange Juice 499 0 0.001 NT

Radishes 689 0 0.005 NT

Summer Squash 176 0 0.001 - 0.005 NT

Sweet Bell Peppers 675 0 0.005 0.1

Tangerines 687 0 0.005 NT

Tomato Paste 506 0 0.001 - 0.005 0.1

Winter Squash 677 0 0.001 NT

TOTAL 4,896 0

Lindane - BHC gamma (insecticide) (also an isomer of BHC)

Blueberries, Cultivated, Fresh 168 0 0.013 0.5 AL

Blueberries, Frozen 7 0 0.013 0.5 AL

Broccoli 675 0 0.001 NT

Cantaloupe 694 0 0.013 NT

Carrots 499 0 0.005 0.5 AL

Cauliflower 692 0 0.001 NT

Collard Greens 514 0 0.013 NT

Eggplant 661 0 0.001 - 0.005 NT

Green Beans 177 0 0.001 0.5 AL

Kiwi Fruit 177 0 0.045 0.5 AL

Orange Juice 499 0 0.001 0.5 AL

Radishes 689 0 0.005 0.5 AL

Summer Squash 176 0 0.001 - 0.005 NT

Sweet Bell Peppers 675 0 0.005 NT

Tangerines 687 0 0.005 0.5 AL

Tomato Paste 506 0 0.001 - 0.005 NT

Winter Squash 677 0 0.001 NT

TOTAL 8,173 0

Mirex (insecticide) 

Blueberries, Cultivated, Fresh 168 0 0.001 NT

Blueberries, Frozen 7 0 0.001 NT

Cantaloupe (V-2) 694 3 0.4 0.002 0.001 NT

Collard Greens 514 0 0.001 NT

Green Beans 177 0 0.001 NT

Orange Juice 499 0 0.001 NT

Summer Squash 89 0 0.001 NT

Tomato Paste 290 0 0.001 NT

Winter Squash 677 0 0.001 NT

TOTAL 3,115 3

Appendix C. Page 6 of 7
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm ^

Range of LODs, 

ppm ^

EPA 

Tolerance 

Level, ppm

Oxychlordane (metabolite of Chlordane)

Bananas 703 0 0.007 0.1 AL

Green Beans 177 0 0.005 0.1 AL

Orange Juice 499 0 0.005 0.1 AL

Summer Squash 89 0 0.005 0.1 AL

Tomato Paste 290 0 0.005 0.1 AL

Winter Squash 677 1 0.1 0.006 0.005 0.1 AL

TOTAL 2,435 1

NOTES

^ = When a range is not listed, only one distinct detected concentration or LOD value was reported for the pesticide/commodity pair.

AL = Numbers shown are Action Levels established by FDA for some pesticides. Under the Food Quality Protection Act, responsibility

for establishing tolerances in lieu of action levels has been transferred to EPA. In the interim, action levels are used.

NT = No tolerance level was set for that pesticide/commodity pair.

(V) = Residue was found where no tolerance was established by EPA. Following "V" are the number of occurrences. Refer to

page 3 in Appendix H to see the number of occurrences broken down by sample origin (domestic, imported, or unknown).

Appendix C. Page 7 of 7
Appendix D

Sample Origin by State or Country

(Determined by Grower, Packer, or Distributor)

Appendix D gives the number of samples per State or country of origin and the number of 

samples of unknown origin. Where available, the origin of fresh commodities is taken from the 

grower or packer information. For processed commodities, origin is determined primarily by 

packer or distributor.

As shown in Appendix D, samples originated from 34 States and 34 foreign countries. There 

were 298 domestic samples from unknown States and 19 imported samples from unknown 

countries. There were an additional 67 samples from unknown origins. Overall, 59.5 percent of 

samples were from U.S. sources, 34.9 percent were imports from single countries, 4.9 percent 

were of mixed national origin, and 0.7 percent were of unknown origin.
Part 1. Domestic Samples

# of % of

BB BN BR CF CN CR EP GB GL KW PP RD SS TA WS AJ BZ OJ TP Samples Total

Alabama 1 1 2 < 0.1

Arizona 7 9 39 15 3 1 1 4 37 1 2 7 8 2 8 144 1.5

Arkansas 1 3 2 2 2 2 24 2 12 50 0.5

California 5 417 579 292 285 120 25 159 80 152 136 10 261 141 51 21 121 2855 29.7

Colorado 3 1 7 6 1 1 19 6 17 9 1 71 0.7

Connecticut 1 1 17 19 0.2

Delaware 1 1 2 < 0.1

Florida 1 14 34 11 52 25 4 2 45 87 14 35 16 15 127 4 486 5.1

Georgia 5 1 1 1 69 12 75 47 4 12 1 15 4 1 248 2.6

Idaho 4 4 < 0.1

Illinois 6 3 3 1 7 4 12 161 197 2.1

Indiana 1 1 2 2 16 22 0.2

Maine 1 2 1 5 9 0.1

Maryland 1 3 1 2 12 6 28 4 2 3 6 1 5 74 0.8

Massachusetts 1 1 1 2 5 0.1

Michigan 1 11 10 2 32 4 108 2 36 38 2 27 273 2.8

Minnesota 1 2 9 2 1 17 32 0.3

Mississippi 1 1 < 0.1

Missouri 1 2 3 < 0.1

Nebraska 2 2 < 0.1

Nevada 4 4 < 0.1

New Hampshire 1 1 < 0.1

New Jersey 14 2 10 1 10 1 1 2 6 4 1 12 64 0.7

New York 17 2 1 6 1 2 9 1 1 13 16 1 2 12 84 0.9

North Carolina 3 1 7 5 10 10 5 6 1 1 19 68 0.7

Ohio 1 2 4 9 15 2 16 4 84 2 6 27 11 2 27 212 2.2

Oregon 1 5 1 1 27 1 6 42 0.4

Pennsylvania 4 2 1 4 2 1 1 2 4 10 8 39 0.4

South Carolina 1 1 48 2 52 0.5

Tennessee 2 1 3 < 0.1

Texas 1 27 23 16 12 16 11 32 2 19 2 7 4 31 7 28 238 2.5

Virginia 1 5 1 7 0.1

Washington 1 4 4 1 5 1 4 3 1 14 54 92 1.0

Wisconsin 4 2 1 1 8 0.1

Unknown State 26 28 23 4 54 12 37 2 28 30 11 8 20 7 6 2 298 3.1

# of Domestic 11 541 660 420 373 390 112 491 87 356 539 76 330 335 309 2 181 498 5,711

% of Total 7 80 95 61 75 59 63 96 49 53 78 43 48 49 43 29 36 98 59.5

Part 2. Imported Samples

# of % of

BB BN BR CF CN CR EP GB GL KW PP RD SS TA WS AJ BZ OJ TP Samples Total

Argentina 18 11 29 0.3

Australia 12 12 0.1

Austria 1 1 < 0.1

Brazil 6 8 14 0.1

APPENDIX D. SAMPLE ORIGIN BY STATE OR COUNTRY

(Determined by Grower, Packer, or Distributor)

Fresh F&V Processed F&V

Fresh F&V Processed F&V

Appendix D. Page 1 of 4
# of % of

BB BN BR CF CN CR EP GB GL KW PP RD SS TA WS AJ BZ OJ TP Samples Total

Canada 9 5 72 7 7 63 60 18 2 3 246 2.6

Chile 4 1 1 152 9 1 168 1.8

China 132 2 134 1.4

Colombia 40 40 0.4

Costa Rica 156 25 181 1.9

Dominican Republic 1 1 2 < 0.1

Ecuador 119 1 120 1.3

El Salvador 2 2 < 0.1

Greece 40 40 0.4

Guatemala 1 218 1 142 1 13 2 2 3 383 4.0

Honduras 82 66 3 19 170 1.8

Israel 7 2 9 0.1

Italy 49 1 50 0.5

Lebanon 1 1 < 0.1

Mexico 37 49 122 23 36 46 250 47 3 240 84 92 3 299 17 1348 14.0

Morocco 20 20 0.2

Netherlands 2 2 4 < 0.1

New Zealand 1 3 4 < 0.1

Nicaragua 1 1 < 0.1

Panama 9 9 0.1

Peru 96 11 1 129 1 238 2.5

South Africa 17 5 22 0.2

Spain 1 1 < 0.1

Turkey 46 46 0.5

Ukraine 10 10 0.1

Uruguay 1 22 23 0.2

Unknown Country 17 1 1 19 0.2

# of Imports 157 703 132 28 271 126 259 60 10 90 315 145 94 357 340 226 5 25 4 3,347

% of Total 93 100 20 4 39 25 39 34 2 51 47 21 53 52 50 31 71 5 1 34.9

Part 3. Mixed National Origin Samples

# of % of

BB BN BR CF CN CR EP GB GL KW PP RD SS TA WS AJ BZ OJ TP Samples Total

Argentina / Austria / Chile / China / Hungary / Italy / Poland / Turkey / USA 4 4 < 0.1

Argentina / Chile / China / USA 2 2 < 0.1

Argentina / China 3 3 < 0.1

Argentina / China / New Zealand / Poland / South Africa 1 1 < 0.1

Argentina / China / USA 1 1 < 0.1

Argentina / Poland / USA 2 2 < 0.1

Argentina / Turkey 6 6 0.1

Argentina / Ukraine 1 1 < 0.1

Belize / Brazil / Costa Rica / Mexico / USA 12 12 0.1

Belize / Brazil / Mexico / USA 2 2 < 0.1

Brazil / Chile 4 4 < 0.1

Brazil / Chile / China 2 2 < 0.1

Brazil / Chile / China / Hungary / Italy / Poland / Turkey / Ukraine 4 4 < 0.1

Brazil / Chile / China / Hungary / Italy / Poland / Turkey / Ukraine / USA 10 10 0.1

Brazil / China 1 1 < 0.1

Brazil / Costa Rica / Mexico 1 1 < 0.1

Brazil / Costa Rica / Mexico / USA 15 15 0.2

Brazil / Costa Rica / USA 18 18 0.2

Brazil / Mexico 1 1 < 0.1

Brazil / Mexico / USA 25 25 0.3

Fresh F&V Processed F&V

Fresh F&V Processed F&V

Appendix D. Page 2 of 4
# of % of

BB BN BR CF CN CR EP GB GL KW PP RD SS TA WS AJ BZ OJ TP Samples Total

Brazil / Poland 1 1 < 0.1

Brazil / USA 181 181 1.9

Canada / USA 15 15 0.2

Chile / China 3 3 < 0.1

Chile / China / Mexico / Poland / Spain / Turkey / USA 3 3 < 0.1

Chile / China / Poland / Turkey / USA 1 1 < 0.1

Chile / China / Turkey 1 1 < 0.1

Chile / China / Turkey / USA 7 7 0.1

Chile / China / USA 3 3 < 0.1

Chile / Hungary / Poland 1 1 < 0.1

Chile / Poland / Turkey 2 2 < 0.1

Chile / Poland / Turkey / USA 1 1 < 0.1

Chile / Poland / USA 1 1 < 0.1

Chile / South Africa 3 3 < 0.1

Chile / Turkey / USA 2 2 < 0.1

Chile / Ukraine / USA 3 3 < 0.1

Chile / USA 1 1 < 0.1

China / Italy / Ukraine 1 1 < 0.1

China / Mexico 1 1 < 0.1

China / New Zealand 1 1 < 0.1

China / New Zealand / Poland 1 1 < 0.1

China / New Zealand / USA 1 1 < 0.1

China / Poland 7 7 0.1

China / Poland / Turkey / USA 4 4 < 0.1

China / Poland / USA 3 3 < 0.1

China / Spain 1 1 < 0.1

China / Turkey 16 16 0.2

China / Turkey / USA 3 3 < 0.1

China / Ukraine 8 8 0.1

China / USA 32 32 0.3

Mexico / Spain / USA 1 1 < 0.1

Mexico / USA 33 33 0.3

Moldova / Ukraine 1 1 < 0.1

New Zealand / USA 1 1 < 0.1

Poland / Turkey / USA 2 2 < 0.1

Poland / Ukraine 2 2 < 0.1

Poland / USA 2 2 < 0.1

Spain / Ukraine 1 1 < 0.1

Turkey / China ` 1 1 < 0.1

Turkey / USA 8 8 0.1

# of Mixed National Origin Samples 186 289 475

% of Total 26 58 4.9

Part 4. Unknown Origin Samples

# of % of

BB BN BR CF CN CR EP GB GL KW PP RD SS TA WS AJ BZ OJ TP Samples Total

Unknown Origin 2 4 3 12 5 13 4 5 6 2 3 4 4 67 0.7

% of Total < 1 1 < 1 2 3 3 1 1 3 < 1 < 1 1 1 0.7

Sample Totals: 168 703 675 692 694 499 661 177 514 177 675 689 176 687 677 724 7 499 506 9,600

Fresh F&V Processed F&V

Fresh F&V Processed F&V

Appendix D. Page 3 of 4
Commodity Legend

AJ = Apple Juice CR = Carrots PP = Sweet Bell Peppers

BB = Blueberries, Cultivated EP = Eggplant RD = Radishes

BN = Bananas GB = Green Beans SS = Summer Squash

BR = Broccoli GL = Collard Greens TA = Tangerines

BZ = Blueberries, Frozen KW = Kiwi Fruit TP = Tomato Paste

CF = Cauliflower OJ = Orange Juice WS = Winter Squash

CN = Cantaloupe

Appendix D. Page 4 of 4
Appendix E 

Import Versus Domestic Pesticide Residue Comparisons

 

The Pesticide Data Program is designed to provide a comprehensive statistical picture of 

pesticide residues in the U.S. food supply, representing all sources, including imports. Most 

commodities consumed are generally produced in the United States with import components 

that vary by commodity. However, several commodities tested over the past several years were 

cyclical; that is, part of the year the commodity was produced domestically and part of the year it 

was imported. 

Appendix E compares residue data reported for samples originating in the United States with 

those of the same commodity from major exporting countries in 2020. Residue data for 

domestic cantaloupe are compared with data for samples originating in Guatemala. Residue 

data for domestic tangerines are compared with data for samples originating in both Chile and 

Peru. Residue data for domestic winter squash are compared with data for samples originating 

in Mexico. These commodities were selected because they are fresh products collected all 12 

months of the year and they have more than 100 data points (samples) for each of the countries 

compared. Only residues detected in more than 5 percent of all samples are included in each 

comparison. All pesticides detected were registered in the United States. However, the profiles 

of residue findings were markedly different in the United States samples versus samples from 

these exporting countries. The differences in residue detections between countries were likely 

due to the pesticides used in response to pest pressures based on differing environmental and 

climatic conditions as well as crop production and protection practices. 
Pesticide Origin

# of 

Samples 

Analyzed

# of 

Samples w/ 

Detections

% of 

Samples w/ 

Detections

Range of 

Detections, ppm

EPA 

Tolerance, 

ppm

Acetamiprid United States 420 35 8.3 0.0015 - 0.016 0.50

Guatemala 142 58 40.8 0.0016 - 0.026 0.50

Bifenthrin United States 418 45 10.8 0.002 - 0.0059 0.4

Guatemala 122 0 0.4

Dinotefuran United States 420 150 35.7 0.0034 - 0.13 0.5

Guatemala 142 56 39.4 0.0033 - 0.05 0.5

Fluopyram United States 395 7 1.8 0.0055 - 0.021 1.0

Guatemala 142 30 21.1 0.005 - 0.016 1.0

Imidacloprid United States 420 101 24.0 0.0033 - 0.078 0.5

Guatemala 142 18 12.7 0.0033 - 0.025 0.5

Metalaxyl/Mefenoxam United States 420 20 4.8 0.0011 - 0.035 1.0

Guatemala 142 51 35.9 0.0011 - 0.041 1.0

Oxamyl oxime United States 420 25 6.0 0.007 - 1.4 2.0

Guatemala 142 15 10.6 0.0067 - 0.10 2.0

Propamocarb hydrochloride United States 420 7 1.7 0.0021 - 0.0058 1.5

Guatemala 142 29 20.4 0.002 - 0.014 1.5

Thiabendazole United States 420 4 1.0 0.0064 - 0.029 15.0

Guatemala 142 22 15.5 0.0021 - 0.27 15.0

Thiamethoxam United States 420 31 7.4 0.0035 - 0.024 0.2

Guatemala 142 21 14.8 0.0034 - 0.040 0.2

NOTE: The Limits of Detection (LODs) for pesticide detections in cantaloupe are listed in Appendix B.

Appendix E. Import Versus Domestic Pesticide Residue Comparisons

2020 Distribution of Residues for Cantaloupe Samples

Originating in Guatemala Versus United States

(Only Pesticides with Residue Detections in at least 5 Percent of all Samples)

Appendix E. Page 1 of 3
Pesticide Origin

# of 

Samples 

Analyzed

# of 

Samples w/ 

Detections

% of 

Samples w/ 

Detections

Range of 

Detections, ppm

EPA 

Tolerance, 

ppm

Acetamiprid United States 330 5 1.5 0.0025 - 0.015 1.0

Chile 152 46 30.3 0.002 - 0.064 1.0

Peru 129 38 29.5 0.002 - 0.047 1.0

Azoxystrobin United States 330 111 33.6 0.002 - 0.13 15.0

Chile 152 11 7.2 0.0024 - 0.13 15.0

Peru 129 0 15.0

Fludioxonil United States 330 104 31.5 0.005 - 0.21 10

Chile 152 72 47.4 0.0056 - 0.091 10

Peru 129 4 3.1 0.018 - 0.078 10

Imazalil United States 330 300 90.9 0.0054 - 0.65 10.0

Chile 152 146 96.1 0.0061 - 1.3 10.0

Peru 129 125 96.9 0.010 - 1.2 10.0

Propiconazole United States 330 21 6.4 0.0051 - 0.046 8.0

Chile 152 0 8.0

Peru 129 6 4.7 0.0052 - 0.031 8.0

Pyrimethanil United States 330 22 6.7 0.0057 - 0.033 10

Chile 152 41 27.0 0.0051 - 0.28 10

Peru 129 8 6.2 0.035 - 0.17 10

Thiabendazole United States 330 272 82.4 0.011 - 0.78 10.0

Chile 152 109 71.7 0.012 - 0.86 10.0

Peru 129 108 83.7 0.012 - 1.2 10.0

NOTE: The Limits of Detection (LODs) for pesticide detections in tangerines are listed in Appendix B.

2020 Distribution of Residues for Tangerine Samples

Originating in Chile and Peru Versus United States

(Only Pesticides with Residue Detections in at least 5 Percent of all Samples)

Appendix E. Page 2 of 3
Pesticide Origin

# of 

Samples 

Analyzed

# of 

Samples w/ 

Detections

% of 

Samples w/ 

Detections

Range of 

Detections, ppm

EPA 

Tolerance, 

ppm

Acetamiprid USA 335 11 3.3 0.0013 - 0.0047 0.50

Mexico 299 20 6.7 0.0014 - 0.017 0.50

Bifenthrin USA 335 83 24.8 0.0013 - 0.15 0.4

Mexico 299 54 18.1 0.0013 - 0.016 0.4

Chlorothalonil USA 335 40 11.9 0.0051 - 0.49 5.0

Mexico 299 22 7.4 0.005 - 0.079 5.0

Cyflufenamid USA 335 72 21.5 0.0014 - 0.056 0.10

Mexico 299 0 0.10

Imidacloprid USA 335 60 17.9 0.0028 - 0.20 0.5

Mexico 299 166 55.5 0.0027 - 0.13 0.5

Metalaxyl/Mefenoxam USA 335 18 5.4 0.002 - 0.17 1.0

Mexico 299 19 6.4 0.0013 - 0.024 1.0

Propamocarb USA 335 12 3.6 0.0014 - 0.21 1.5

Mexico 299 44 14.7 0.0045 - 0.34 1.5

Pyraclostrobin USA 335 12 3.6 0.0013 - 0.010 0.5

Mexico 299 29 9.7 0.0013 - 0.0072 0.5

Tebuconazole USA 335 7 2.1 0.0015 - 0.016 0.4

Mexico 299 39 13.0 0.0013 - 0.014 0.4

Thiamethoxam USA 335 45 13.4 0.0013 - 0.022 0.2

Mexico 299 46 15.4 0.0013 - 0.020 0.2

NOTE: The Limits of Detection (LODs) for pesticide detections in winter squash are listed in Appendix B.

2020 Distribution of Residues for Winter Squash Samples

Originating in Mexico Versus United States

(Only Pesticides with Residue Detections in at least 5 Percent of all Samples)

Appendix E. Page 3 of 3
Appendix F 

Pesticide Residues by Commodity

(Pairs With Residue Detections in at Least 5 Percent of Samples)

Appendix F shows 199 commodity/pesticide pairs (including metabolites, isomers, and 

degradates) with detections in at least 5 percent of the samples tested. The data shown include 

the range and mean of values detected and U.S. Environmental Protection Agency (EPA) 

tolerance references for each pair. The EPA tolerances cited in this summary and appendixes 

apply to 2020 and not to the current year. There may be instances where tolerances have been 

recently set, modified, or revoked that would have an effect on whether a residue is violative or 

not. 
APPENDIX F. PESTICIDE RESIDUES A

 BY COMMODITY

(Pairs With Residue Detections in at Least 5 Percent of Samples)

% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

1 Apple Juiice (6 pesticides)

Acetamiprid * I 12.6 724 91 0.012 - 0.034 0.013 1.0

Diphenylamine (DPA) F 6.9 724 50 0.010 - 0.077 0.017 10.0

Fludioxonil F 6.9 724 50 0.012 - 0.10 0.019 5.0

Pyrimethanil F 26.9 724 195 0.003 - 2.5 0.23 15

Tetrahydrophthalimide (THPI) 1 FM 28.9 724 209 0.012 - 1.7 0.10 25.0

Thiabendazole F 22.2 724 161 0.005 - 0.20 0.03 5.0

2 Bananas (5 pesticides)

Azoxystrobin F 52.3 703 368 0.003 - 0.020 0.004 0.1

Buprofezin I 7.3 703 51 0.002 - 0.14 0.022 0.20

Fenpropimorph F 10.5 703 74 0.005 - 0.018 0.006 2.0

Myclobutanil F 11 703 77 0.007 - 0.098 0.033 4.0

Thiabendazole F 41 703 288 0.005 - 0.21 0.050 3.0

3 Blueberries, Cultivated, Fresh (17 pesticides)

Acetamiprid * I 38.7 168 65 0.002 - 0.54 0.089 1.6

Azoxystrobin F 23.8 168 40 0.002 - 1.4 0.12 10.0

Bifenthrin * I 6 168 10 0.004 - 0.11 0.024 1.8

Boscalid F 52.4 168 88 0.004 - 3.0 0.21 13.0

Carbendazim (MBC) 2 F 5.4 168 9 0.001 - 0.010 0.004 NT

Chlorantraniliprole I 6 168 10 0.011 - 0.086 0.049 2.5

Cypermethrin * I 11.3 168 19 0.015 - 0.30 0.094 0.8

Cyprodinil F 31 168 52 0.005 - 0.45 0.074 5.0

Difenoconazole F 9.5 168 16 0.013 - 0.42 0.10 4.0

Fenhexamid F 26.2 168 44 0.015 - 2.0 0.21 5

Fludioxonil F 29.8 168 50 0.025 - 1.7 0.23 3.0

Imidacloprid I 12.5 168 21 0.003 - 0.18 0.035 3.5

Iprodione F 6 168 10 0.054 - 1.4 0.47 15.0

Pyraclostrobin F 26.2 168 44 0.004 - 0.35 0.036 4.0

Spinosad A * IM 6.5 168 11 0.004 - 0.044 0.010 0.90

Spirotetramat I 7.7 168 13 0.005 - 0.47 0.082 3.0

Tetrahydrophthalimide (THPI) 1 FM 6 168 10 0.011 - 0.21 0.084 20.0

4 Broccoli (8 pesticides)

Azoxystrobin F 14.7 675 99 0.002 - 1.3 0.055 3.0

Boscalid F 10.7 675 72 0.002 - 0.78 0.045 6.0

DCPA H 25.9 675 175 0.002 - 0.28 0.007 5.0

Fluopyram F 5.6 675 38 0.002 - 0.022 0.003 4.0

Imidacloprid I 17.8 675 120 0.003 - 0.12 0.012 3.5

Permethrin (parent)

 Permethrin cis 3 IM 8 675 54 0.002 - 0.12 0.016 2.0

 Permethrin trans 3 IM 6.5 675 44 0.002 - 0.13 0.016 2.0

Appendix F. Page 1 of 6
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

Pyraclostrobin F 9.8 675 66 0.002 - 0.34 0.035 5.0

Thiamethoxam * I 19 675 128 0.003 - 0.059 0.006 4.5

5 Cantaloupe (10 pesticides)

Acetamiprid * I 13.5 694 94 0.002 - 0.026 0.005 0.50

Bifenthrin * I 8 662 53 0.002 - 0.006 0.003 0.4

Dinotefuran * I 33.7 694 234 0.003 - 0.13 0.023 0.5

Fluopyram F 5.8 669 39 0.005 - 0.033 0.009 1.0

Imidacloprid I 22.9 694 159 0.003 - 0.18 0.014 0.5

Metalaxyl/Mefenoxam 4 F 13.4 694 93 0.001 - 0.041 0.008 1.0

Oxamyl oxime IM 5.9 694 41 0.007 - 1.4 0.21 2.0

Propamocarb hydrochloride 5 F 8.2 694 57 0.002 - 0.014 0.004 1.5

Thiabendazole F 5 694 35 0.002 - 0.27 0.035 15.0

Thiamethoxam * I 10.2 694 71 0.003 - 0.040 0.010 0.2

6 Carrots (6 pesticides)

Azoxystrobin F 5 499 25 0.010 - 0.043 0.017 1.0

Boscalid F 18 499 90 0.020 - 0.11 0.040 2.0

Iprodione F 12.8 499 64 0.015 - 0.087 0.034 5.0

Linuron H 31.7 499 158 0.010 - 0.17 0.038 1.0

Penthiopyrad F 10 499 50 0.001 - 0.052 0.010 3.0

Pyraclostrobin F 11.8 499 59 0.005 - 0.025 0.010 0.4

7 Cauliflower (3 pesticides)

Flupyradifurone I 17.9 692 124 0.002 - 0.026 0.003 6

Imidacloprid I 19.4 692 134 0.003 - 0.059 0.010 3.5

Thiamethoxam * I 25.9 664 172 0.003 - 0.027 0.005 4.5

8 Collard Greens (21 pesticides)

Acetamiprid * I 11.1 514 57 0.002 - 1.1 0.071 15

Atrazine H 6.4 514 33 0.002 - 0.029 0.005 NT

Azoxystrobin F 22.4 514 115 0.002 - 11 0.76 25

Bifenthrin * I 20.8 514 107 0.002 - 5.3 0.30 3.5

Boscalid F 16.5 514 85 0.003 - 0.34 0.022 60

Chlorantraniliprole I 19.1 514 98 0.010 - 6.9 0.31 11

Cyfluthrin * I 21.4 514 110 0.004 - 1.9 0.14 7.0

Cypermethrin * I 19.5 514 100 0.010 - 4.4 0.33 14.0

DCPA H 32.7 514 168 0.002 - 0.16 0.021 5.0

Dimethomorph F 10.5 514 54 0.003 - 2.4 0.12 30.0

Fenamidone F 9.1 514 47 0.005 - 2.3 0.26 60

Fluopicolide F 22.4 514 115 0.005 - 1.5 0.097 18

Fluopyram F 12.1 514 62 0.005 - 1.1 0.044 50

Imidacloprid I 29.8 514 153 0.003 - 0.34 0.037 3.5

Indoxacarb I 10.3 514 53 0.020 - 0.92 0.16 12

Mandipropamid F 14.6 514 75 0.002 - 2.1 0.32 25

Metalaxyl/Mefenoxam 4 F 7.4 514 38 0.001 - 0.15 0.014 0.1

Appendix F. Page 2 of 6
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

Methoxyfenozide I 12.8 514 66 0.003 - 5.7 0.43 30

Pyraclostrobin F 20.8 514 107 0.004 - 2.4 0.30 16

Spinetoram I 10.2 498 51 0.004 - 0.20 0.031 10

Thiamethoxam (parent) * I 20.4 514 105 0.003 - 0.69 0.032 3.0

 Clothianidin 6

 * I 15.6 514 80 0.010 - 0.28 0.047 3.0

9 Eggplant (15 pesticides)

Acetamiprid * I 12.9 661 85 0.002 - 0.17 0.024 0.20

Azoxystrobin F 7.3 661 48 0.002 - 0.043 0.006 3.0

Bifenthrin * I 7.7 661 51 0.002 - 0.078 0.015 0.05

Carbaryl I 5.6 661 37 0.002 - 0.35 0.090 5.0

Chlorantraniliprole I 6.1 661 40 0.003 - 0.010 0.004 1.4

Difenoconazole F 6.5 661 43 0.002 - 0.046 0.007 0.60

Dinotefuran * I 11.2 661 74 0.010 - 0.12 0.029 0.7

Fluopicolide F 5.7 661 38 0.002 - 0.040 0.007 1.6

Fluopyram F 15.9 661 105 0.002 - 0.099 0.020 4.0

Flupyradifurone I 7.6 661 50 0.002 - 0.17 0.031 1.5

Imidacloprid I 28.4 661 188 0.002 - 0.13 0.013 1.0

Penthiopyrad F 6.1 661 40 0.001 - 0.050 0.010 3.0

Permethrin (parent)

 Permethrin cis 3 IM 5.1 661 34 0.002 - 0.047 0.016 0.50

 Permethrin trans 3 IM 5.6 661 37 0.002 - 0.069 0.021 0.50

Propamocarb hydrochloride 5 F 5.1 311 16 0.006 - 0.38 0.076 4

Thiamethoxam (parent) * I 27.1 661 179 0.003 - 0.10 0.016 0.25

 Clothianidin 6 * I 9.4 661 62 0.003 - 0.087 0.011 0.25

10 Green Beans (19 pesticides)

Azoxystrobin F 23.7 177 42 0.001 - 0.92 0.059 3.0

Bifenthrin * I 21.5 177 38 0.002 - 0.17 0.039 0.6

Boscalid F 11.3 177 20 0.004 - 0.37 0.089 5.0

Carbendazim (MBC) 2 F 23.2 177 41 0.002 - 0.24 0.046 2.0

Chlorantraniliprole I 14.7 177 26 0.005 - 0.11 0.025 2.0

Chlorothalonil F 16.4 177 29 0.005 - 0.41 0.087 5

Cyhalothrin, Total 7 * I 14.1 177 25 0.003 - 0.033 0.015 0.20

Cypermethrin * I 11.9 177 21 0.008 - 0.17 0.029 0.5

Dicloran F 7.9 177 14 0.002 - 6.0 0.90 20

Dinotefuran * I 7.3 177 13 0.003 - 0.031 0.014 0.01

Fluxapyroxad F 5.1 177 9 0.002 - 0.022 0.008 2.0

Imidacloprid desnitro IM 9.6 177 17 0.001 - 0.014 0.005 4.0

Metalaxyl/Mefenoxam 4 F 11.3 177 20 0.001 - 0.020 0.006 0.2

Methamidophos * I 6.2 177 11 0.002 - 1.1 0.24 0.2

Methomyl I 5.1 177 9 0.017 - 0.45 0.16 2

Methoxyfenozide I 6.8 177 12 0.003 - 0.098 0.028 1.5

Penthiopyrad F 10.7 177 19 0.002 - 0.33 0.039 4.0

Pyraclostrobin F 16.9 177 30 0.002 - 0.17 0.027 0.5

Tebuconazole F 6.2 177 11 0.003 - 0.054 0.022 0.1

Appendix F. Page 3 of 6
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

11 Kiwi Fruit (2 pesticides)

Cyprodinil F 12.4 177 22 0.038 - 0.87 0.38 1.8

Fludioxonil F 11.3 177 20 0.070 - 3.1 0.83 20

12 Orange Juice (3 pesticides)

Diflubenzuron I 26.3 499 131 0.001 - 0.004 0.002 3.0

Imazalil F 19.2 499 96 0.003 - 0.085 0.027 10.0

Thiabendazole F 26.7 499 133 0.001 - 0.12 0.019 10.0

13 Radishes (5 pesticides)

Azoxystrobin F 10.9 689 75 0.002 - 0.19 0.022 1.0

Chlorpyrifos * I 8.4 689 58 0.005 - 0.10 0.021 2.0

DCPA H 21.2 689 146 0.005 - 0.24 0.044 2.0

Flonicamid I 6.4 689 44 0.010 - 0.12 0.037 0.60

Pyraclostrobin F 8.4 689 58 0.003 - 0.17 0.027 0.4

14 Summer Squash (15 pesticides)

Acetamiprid * I 8.5 176 15 0.002 - 0.015 0.008 0.50

Bifenthrin * I 10.8 176 19 0.001 - 0.11 0.014 0.4

Chlorothalonil F 9 89 8 0.005 - 0.029 0.011 5.0

Dinotefuran * I 9.7 176 17 0.003 - 0.30 0.055 0.5

Flonicamid I 6.8 176 12 0.014 - 0.31 0.072 1.5

Fluopicolide F 5.1 176 9 0.002 - 0.034 0.009 0.50

Fluopyram F 14.8 176 26 0.002 - 0.11 0.032 0.60

Flupyradifurone I 13.6 176 24 0.002 - 0.038 0.008 0.40

Flutriafol F 10.8 176 19 0.001 - 0.015 0.005 0.30

Imidacloprid (parent) I 45.5 176 80 0.003 - 0.14 0.025 0.5

 Imidacloprid desnitro 8 IM 49.4 89 44 0.001 - 0.012 0.003 0.5

 Imidacloprid urea 8 IM 9 89 8 0.002 - 0.004 0.002 0.5

Metalaxyl/Mefenoxam 4 F 8 176 14 0.001 - 0.031 0.008 1.0

Propamocarb (parent) F 12.4 89 11 0.002 - 0.18 0.051 1.5

 Propamocarb hydrochloride 5 F 5.7 87 5 0.001 - 0.032 0.012 1.5

Pydiflumetofen F 6.2 176 11 0.001 - 0.016 0.008 0.50

Pyraclostrobin F 10.8 176 19 0.001 - 0.025 0.010 0.5

Thiamethoxam (parent) * I 29.5 176 52 0.001 - 0.17 0.023 0.2

 Clothianidin 6 * I 6.8 176 12 0.001 - 0.005 0.003 0.2

15 Sweet Bell Peppers (23 pesticides)

Acetamiprid * I 7.7 675 52 0.011 - 0.28 0.048 0.20

Azoxystrobin F 29.6 675 200 0.002 - 0.11 0.016 3.0

Bifenthrin * I 7.4 675 50 0.005 - 0.11 0.028 0.5

Boscalid F 8.6 675 58 0.010 - 0.33 0.049 3.0

Chlorfenapyr * I 9.6 675 65 0.005 - 0.32 0.071 2

Chlorothalonil F 9.5 675 64 0.005 - 0.20 0.031 6.0

Cypermethrin * I 9 675 61 0.010 - 0.27 0.044 0.2

Appendix F. Page 4 of 6
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

Difenoconazole F 17.8 675 120 0.005 - 0.49 0.034 0.60

Dinotefuran * I 7.6 675 51 0.010 - 0.44 0.061 0.7

Flonicamid I 11.1 675 75 0.011 - 0.44 0.055 3.0

Fluopyram F 17.3 675 117 0.010 - 0.18 0.034 4.0

Imidacloprid I 21.5 675 145 0.010 - 1.6 0.055 1.0

Metalaxyl/Mefenoxam 4 F 17.9 675 121 0.005 - 0.23 0.033 1.0

Methomyl I 5 675 34 0.011 - 0.20 0.068 2

Myclobutanil F 8.4 675 57 0.006 - 0.19 0.032 4.0

Novaluron * I 7.7 675 52 0.010 - 0.092 0.030 2

Oxamyl (parent) I 5.3 675 36 0.010 - 1.2 0.098 2.0

 Oxamyl oxime 9 IM 22.2 675 150 0.010 - 0.48 0.076 2.0

Permethrin Total I 6.4 675 43 0.005 - 0.46 0.068 0.50

Propamocarb F 7.3 675 49 0.010 - 0.36 0.086 4

Pyraclostrobin F 24.7 675 167 0.003 - 0.46 0.029 1.4

Spiromesifen I 12.6 675 85 0.002 - 0.21 0.018 0.45

Thiacloprid I 7.1 675 48 0.010 - 0.12 0.041 1.0

Thiamethoxam (parent) * I 22.5 675 152 0.010 - 0.48 0.046 0.25

 Clothianidin 6 * I 19.9 675 134 0.010 - 0.25 0.046 0.80

16 Tangerines (7 pesticides)

Acetamiprid * I 13.1 687 90 0.002 - 0.064 0.011 1.0

Azoxystrobin F 17.9 687 123 0.002 - 0.13 0.028 15.0

Fludioxonil F 28.7 687 197 0.005 - 0.21 0.026 10

Imazalil F 93.3 687 641 0.005 - 1.3 0.17 10.0

Propiconazole F 8.3 687 57 0.005 - 0.066 0.018 8.0

Pyrimethanil F 17.2 687 118 0.005 - 0.50 0.060 10

Thiabendazole F 77.1 687 530 0.011 - 1.2 0.18 10.0

17 Tomato Paste (12 pesticides)

Azoxystrobin F 72.5 506 367 0.001 - 0.023 0.006 0.6

Bifenthrin * I 52.3 505 264 0.001 - 0.040 0.009 0.15

Cyhalothrin, Total 7 * I 15 506 76 0.003 - 0.009 0.004 0.1

Difenoconazole F 61.1 506 309 0.001 - 0.020 0.005 0.60

Esfenvalerate * I 5.5 290 16 0.005 - 0.010 0.006 0.5

Fluopyram F 13.2 506 67 0.001 - 0.018 0.005 1.0

Fluxapyroxad F 36.6 506 185 0.001 - 0.019 0.005 0.7

Imidacloprid I 40.1 506 203 0.003 - 0.024 0.006 6.0

Methoxyfenozide I 15.2 506 77 0.003 - 0.019 0.005 2.0

Penthiopyrad F 5.7 506 29 0.001 - 0.010 0.003 3.5

Thiamethoxam (parent) * I 12.6 506 64 0.001 - 0.008 0.003 0.80

 Clothianidin 6 * I 24.7 506 125 0.001 - 0.013 0.004 0.80

Trifloxystrobin F 10.1 506 51 0.001 - 0.011 0.003 0.5

18 Winter Squash (10 pesticides)

Acetamiprid * I 5.9 677 40 0.001 - 0.017 0.003 0.50

Bifenthrin * I 21.7 677 147 0.001 - 0.15 0.008 0.4

Appendix F. Page 5 of 6
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

Chlorothalonil F 10.2 677 69 0.005 - 0.49 0.046 5.0

Cyflufenamid F 10.6 677 72 0.001 - 0.056 0.009 0.10

Imidacloprid (parent) I 34.6 677 234 0.003 - 0.20 0.016 0.5

 Imidacloprid desnitro IM 29 62 18 0.001 - 0.007 0.003 0.5

Metalaxyl/Mefenoxam 4 F 5.5 677 37 0.001 - 0.17 0.019 1.0

Propamocarb F 9.2 677 62 0.001 - 0.34 0.10 1.5

Pyraclostrobin F 6.8 677 46 0.001 - 0.010 0.003 0.5

Tebuconazole F 7.4 677 50 0.001 - 0.016 0.004 0.4

Thiamethoxam * I 14.3 677 97 0.001 - 0.022 0.004 0.2

NOTES

A Excludes environmental contaminants, which are listed in Appendix C.

NT No tolerance established.

* Residue may result from food handling establishment (FHE) application.

1 Metabolite of captafol and captan.

2 Metabolite of benomyl and thiophanate methyl.

3 Isomer of parent, permethrin.

4 Metalaxyl/mefenoxam are spatial isomers which are analytically indistinguishable via multiresidue methods, but have

separate registrations.

5 Propamocarb analytically determined as the salt (hydrochloride).

6 Metabolite of parent, thiamethoxam.

7 Includes cyhalothrin lambda plus R157836 epimer.

8 Metabolite of parent, imidacloprid. 

9 Metabolite of parent, oxamyl. 

Pesticide Types:

F = Fungicide, FM = Fungicide Metabolite

H = Herbicide

I = Insecticide, IM = Insecticide Metabolite

Appendix F. Page 6 of 6
Appendix G 

Number of Pesticides Detected per Sample

Appendix G shows the percentage of samples versus the number of pesticides detected per 

sample. The graph and data on page 1 show the overall number of samples and percentages 

(of total number of samples analyzed) for each detection group across all commodities. The 

table on page 2 shows the number of pesticides detected by individual commodity. For the 

9,600 samples analyzed, 30.0 percent of the samples had no detectable pesticides, 22.3

percent had 1 pesticide, and 47.7 percent of the samples had more than 1 pesticide. 

This appendix reports the number of distinct pesticides rather than residues. A parent 

compound and its metabolites are reported as a single pesticide.
0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18

0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18

# of

Samples 2,878 2,141 1,712 1,127 635 398 269 172 109 46 44 23 22 10 7 2 4 0 1

% of Total

Samples 30.0 22.3 17.8 11.7 6.6 4.1 2.8 1.8 1.1 0.5 0.5 0.2 0.2 0.1 0.1 0.02 0.04 - 0.01

TOTAL NUMBER OF SAMPLES = 9,600

NOTES

1

 Environmental contaminants, listed in Appendix C, have been excluded from the count of pesticides detected in this appendix. Parent

 compounds and their metabolites are combined to report the number of "pesticides" rather than the number of "residues."

APPENDIX G. NUMBER OF PESTICIDES 1

 DETECTED PER SAMPLE

40

Number of Pesticides Detected per Sample

Number of Pesticides Detected per Sample

30

20

10

Percent of Samples

22.3

4.1

6.6

11.7

Multiple pesticide detections may result from the application of more than one pesticide, 

spray drift, crop rotation, and/or cross-contamination.

30.0

17.8

2.8

1.8

1.1

0.5 0.5 0.2 0.2 0.1 0.1 0.02 0.04 0.01

Appendix G. Page 1 of 2
Commodity (# of samples) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18

Fresh Fruit and Vegetables: Percent

Bananas (703) 26.2 27.6 35.4 8.0 2.3 0.4 0.1 -- -- -- -- -- -- -- -- -- -- -- --

Blueberries, Cultivated (168) 22.7 27.3 37.4 9.7 2.5 0.3 -- -- -- -- -- -- -- -- -- -- -- -- --

Broccoli (675) 19.9 29.8 21.0 16.3 6.2 4.4 2.1 -- -- -- 0.1 -- 0.1 -- -- -- -- -- --

Cantaloupe (694) 27.2 28.7 24.4 13.7 4.6 1.0 0.4 -- -- -- -- -- -- -- -- -- -- -- --

Carrots (499) 39.7 31.9 16.4 5.8 2.4 2.6 1.0 0.2 -- -- -- -- -- -- -- -- -- -- --

Cauliflower (692) 41.0 41.3 13.9 2.7 1.0 -- -- -- -- -- -- -- -- -- -- -- -- -- --

Collard Greens (514) 15.8 14.6 11.1 10.3 9.7 10.3 6.2 7.2 5.3 1.8 2.5 1.4 1.2 0.8 1.2 0.4 0.4 -- --

Eggplant (661) 26.5 23.9 15.4 13.9 7.7 6.1 3.6 1.5 0.8 0.3 0.2 0.2 -- -- -- -- -- -- --

Green Beans (177) 20.3 18.1 11.3 12.4 15.3 5.6 6.8 3.4 4.5 -- 1.1 -- 0.6 0.6 -- -- -- -- --

Kiwi Fruit (177) 73.4 19.8 6.8 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

Radishes (689) 58.9 21.9 7.7 7.8 2.3 1.2 0.1 -- -- -- -- -- -- -- -- -- -- -- --

Summer Squash (176) 18.2 17.6 21.0 18.8 10.2 4.5 3.4 1.1 2.3 1.1 1.1 0.6 -- -- -- -- -- -- --

Sweet Bell Peppers (675) 13.8 11.6 13.0 14.2 10.7 9.8 8.0 7.1 4.4 2.5 2.1 1.2 1.0 0.3 0.1 -- -- -- 0.1

Tangerines (687) 2.5 8.3 37.4 30.6 16.7 3.8 0.6 0.1 -- -- -- -- -- -- -- -- -- -- --

Winter Squash (677) 23.9 24.1 18.9 12.3 8.6 4.3 2.7 2.2 1.6 0.4 0.3 0.3 0.1 0.1 -- -- 0.1 -- --

Processed Fruit and Vegetables:

Apple Juice (724) 53.9 18.9 7.5 8.3 3.9 2.6 2.9 1.5 0.6 -- -- -- -- -- -- -- -- -- --

Blueberries, Frozen (7) 14.3 14.3 -- 14.3 -- 14.3 -- -- -- -- -- 28.6 14.3 -- -- -- -- -- --

Orange Juice (499) 50.3 25.9 19.2 4.2 0.4 -- -- -- -- -- -- -- -- -- -- -- -- -- --

Tomato Paste (506) 16.8 6.9 9.5 13.4 13.2 13.8 12.5 6.1 2.6 2.2 1.6 0.4 0.8 0.2 -- -- -- -- --

Percent of Total Samples 30.0 22.3 17.8 11.7 6.6 4.1 2.8 1.8 1.1 0.5 0.5 0.2 0.2 0.1 0.1 0.02 0.04 -- 0.01

Actual Number of Samples 2,878 2,141 1,712 1,127 635 398 269 172 109 46 44 23 22 10 7 2 4 0 1

NOTES

1

 Environmental contaminants, listed in Appendix C, have been excluded from the count of pesticides detected in this appendix. Parent

 compounds and their metabolites are combined to report the number of "pesticides" rather than the number of "residues." 

Number of Pesticides 1

 Detected per Sample

APPENDIX G. NUMBER OF PESTICIDES DETECTED PER SAMPLE

TOTAL NUMBER OF FRUIT & VEGETABLE SAMPLES = 9,600

Appendix G. Page 2 of 2
Appendix H

Samples Reported to the

U.S. Food and Drug Administration as

Exceeding the Tolerance

or Without Established Tolerance

(per Code of Federal Regulations, Title 40, Part 180)

Appendix H shows pesticide residues reported to the U.S. Food and Drug Administration (FDA) 

as exceeding the tolerance or residues for which no established tolerance was listed under the 

Code of Federal Regulations, Title 40, Part 180. In 2020, a total of 341 samples with 378 

pesticides were reported to the FDA as Presumptive Tolerance Violations.

Pesticides exceeding the tolerance were detected in 47 samples including 1 sample of fresh 

blueberries, 5 samples of carrots, 2 samples of eggplant, 10 samples of green beans, 16 

samples of collard greens, 6 samples of sweet bell peppers, 4 samples of radishes, 2 samples 

of tangerines, and 1 sample of winter squash. Of those 47 samples, 11 were reported as 

imported produce. One green bean sample contained 3 residues that exceeded the established 

tolerances. Five green bean samples, 1 collard green sample, and 1 sweet bell pepper sample

contained 2 residues each that exceeded the established tolerances. 

In addition, 303 samples were found to have pesticides for which no tolerance was established, 

including 295 fresh fruit and vegetable samples and 8 processed fruit/vegetable samples. 

o 283 samples contained 1 pesticide for which no tolerance was established.

o 16 samples contained 2 pesticides for which no tolerances were established.

o 3 samples contained 3 pesticides for which no tolerances were established.

o 1 sample contained 4 pesticides for which no tolerances were established.

 

Nine of the 303 samples also contained one or more pesticides that exceeded an established 

tolerance. 

The columns under the Sample Origin heading provide the number of samples that were of 

domestic, imported, or unknown origin for each pesticide/commodity pair listed.

Appendix H also notes if metabolites (or isomers) were detected as part of the same sample. In 

instances where both parent and metabolite (or isomer) were detected, the Pesticide Data 

Program accounted for both as part of the same tolerance expression.

The EPA tolerances cited in this summary and appendixes apply to 2020 and not to the current 

year. There may be instances where tolerances have been recently set, modified, or revoked 

that would have an effect on whether a residue is violative or not. 

A number of the findings shown in this appendix are less than 0.01 ppm. Levels below 0.01 

ppm are deemed by the U.S. FDA to be “not of regulatory significance”.
Residues Exceeding Established Tolerance

Commodity / Pesticide

Limit of 

Detection, 

ppm

Concentration 

Detected, 

ppm

EPA 

Tolerance 

Level, ppm Country of Origin

1 Blueberries, Cultivated, Fresh / Cyhalothrin, Total 1 0.005 0.027 0.01 Mexico

2 Carrots / EPTC 0.035 0.36 0.1 U.S.

3 Carrots / EPTC 0.035 0.27 0.1 U.S.

4 Carrots / EPTC 0.035 0.24 0.1 U.S.

5 Carrots / EPTC 0.035 0.22 0.1 U.S.

6 Carrots / EPTC 0.035 0.2 0.1 U.S.

7 Collard Greens / Bifenthrin 0.002 5.3 3.5 U.S.

8 Collard Greens / Bifenthrin 2 0.002 4.8 3.5 U.S.

9 Collard Greens / Cyhalothrin, Total 1 0.005 0.52 0.01 U.S.

10 Collard Greens / Cyhalothrin, Total 1 0.005 0.22 0.01 U.S.

11 Collard Greens / Cyhalothrin, Total 1 0.005 0.17 0.01 U.S.

12 Collard Greens / Cyhalothrin, Total 1 0.005 0.17 0.01 Unknown

13 Collard Greens / Cyhalothrin, Total 1 0.005 0.16 0.01 U.S.

14 Collard Greens / Cyhalothrin, Total 1 0.005 0.048 0.01 U.S.

15 Collard Greens / Cyhalothrin, Total 1 0.005 0.045 0.01 U.S.

16 Collard Greens / Cyhalothrin, Total 1 0.005 0.028 0.01 U.S.

17 Collard Greens / Cyhalothrin, Total 1 0.005 0.027 0.01 U.S.

18 Collard Greens / Cyhalothrin, Total 1 0.005 0.023 0.01 U.S.

19 Collard Greens / Cyhalothrin, Total 1 0.005 0.021 0.01 U.S.

20 Collard Greens / Cyhalothrin, Total 1 0.005 0.02 0.01 U.S.

21 Collard Greens / Diazinon 0.005 2.1 0.70 U.S.

22 Collard Greens / Tetrahydrophthalimide (THPI) 2, 3 0.01 0.42 0.05 U.S.

23 Collard Greens / Tetrahydrophthalimide (THPI) 3 0.01 0.2 0.05 U.S.

24 Eggplant / Acephate 0.075 0.1 0.02 U.S.

25 Eggplant / Bifenthrin 0.005 0.078 0.05 U.S.

26 Green Beans / Acephate 4, 5 0.005 6.8 0.02 U.S.

27 Green Beans / Acephate 4, 6 0.005 4.5 0.02 U.S.

28 Green Beans / Acephate 4, 7 0.005 0.61 0.02 Mexico

29 Green Beans / Acephate 4, 8 0.005 0.19 0.02 Mexico

30 Green Beans / Acephate 4, 9 0.005 0.13 0.02 Mexico

31 Green Beans / Acephate 4, 10 0.005 0.073 0.02 Mexico

APPENDIX H. SAMPLES REPORTED TO FDA AS EXCEEDING THE TOLERANCE

OR WITHOUT ESTABLISHED TOLERANCE

(per Code of Federal Regulations, Title 40, Part 180)

Appendix H. Page 1 of 6
Commodity / Pesticide

Limit of 

Detection, 

ppm

Concentration 

Detected, 

ppm

EPA 

Tolerance 

Level, ppm Country of Origin

32 Green Beans / Acephate 0.005 0.031 0.02 Mexico

33 Green Beans / Buprofezin 6 0.001 0.031 0.02 U.S.

34 Green Beans / Dinotefuran 0.003 0.031 0.01 U.S.

35 Green Beans / Dinotefuran 0.003 0.023 0.01 U.S.

36 Green Beans / Dinotefuran 0.003 0.021 0.01 Mexico

37 Green Beans / Methamidophos 4, 5 0.001 1.1 0.02 U.S.

38 Green Beans / Methamidophos 4, 6 0.001 1.1 0.02 U.S.

39 Green Beans / Methamidophos 4, 7 0.001 0.2 0.02 Mexico

40 Green Beans / Methamidophos 4, 8 0.001 0.088 0.02 Mexico

41 Green Beans / Methamidophos 4, 10 0.001 0.044 0.02 Mexico

42 Green Beans / Methamidophos 4, 9 0.001 0.038 0.02 Mexico

43 Radishes / Fluopicolide 0.01 0.28 0.15 U.S.

44 Radishes / Fluopicolide 0.01 0.21 0.15 U.S.

45 Radishes / Fluopicolide 0.01 0.21 0.15 U.S.

46 Radishes / Thiamethoxam 0.01 0.087 0.05 U.S.

47 Sweet Bell Peppers / Acetamiprid 0.01 0.28 0.20 U.S.

48 Sweet Bell Peppers / Cyhalothrin, Total 1, 11 0.008 0.97 0.20 Dominican Republic

49 Sweet Bell Peppers / Imidacloprid 11 0.01 1.6 1.0 Dominican Republic

50 Sweet Bell Peppers / Thiamethoxam 0.01 0.48 0.25 Mexico

51 Sweet Bell Peppers / Thiamethoxam 0.01 0.35 0.25 U.S.

52 Sweet Bell Peppers / Thiamethoxam 0.01 0.33 0.25 Mexico

53 Sweet Bell Peppers / Thiamethoxam 0.01 0.27 0.25 El Salvador

54 Tangerines / Formetanate hydrochloride 0.005 0.13 0.03 U.S.

55 Tangerines / Formetanate hydrochloride 0.005 0.13 0.03 U.S.

56 Winter Squash / Acephate 0.005 0.052 0.02 U.S.

Appendix H. Page 2 of 6
Commodity / Pesticide U.S. Import Unk.

1 Blueberries, Cultivated, Fresh (5 pesticides)

3-Hydroxycarbofuran 168 1 0.6 0.004 0.003 0 1 0

Carbendazim (MBC) 12 168 9 5.4 0.001 - 0.010 0.001 2 7 0

Cyphenothrin 168 1 0.6 0.059 0.015 0 1 0

Myclobutanil 168 3 1.8 0.005 - 0.093 0.003 0 3 0

Thiabendazole 168 1 0.6 0.008 0.002 0 1 0

2 Broccoli (15 pesticides)

Atrazine 675 3 0.4 0.002 - 0.003 0.001 2 0 1

Carbendazim (MBC) 12 675 2 0.3 0.020 - 0.15 0.003 1 1 0

Chlorpropham 675 26 3.9 0.002 - 0.016 0.001 24 2 0

Dicloran 675 2 0.3 0.004 0.002 1 1 0

Etoxazole 675 1 0.1 0.002 0.001 1 0 0

Fipronil 675 1 0.1 0.002 0.001 0 1 0

Linuron 675 1 0.1 0.010 0.002 1 0 0

Metribuzin 675 1 0.1 0.003 0.002 1 0 0

Norflurazon desmethyl 675 1 0.1 0.002 0.001 1 0 0

Pirimiphos methyl 675 1 0.1 0.008 0.001 1 0 0

Pronamide 675 9 1.3 0.002 - 0.012 0.001 - 0.003 9 0 0

Pyrimethanil 675 4 0.6 0.002 - 0.63 0.001 1 3 0

Spirodiclofen 655 1 0.2 0.010 0.006 1 0 0

Tebuconazole 675 1 0.1 0.003 0.001 1 0 0

Thiobencarb 675 1 0.1 0.034 0.003 1 0 0

3 Cantaloupe (3 pesticides)

Mirex 694 3 0.4 0.002 0.001 3 0 0

Pentachloroaniline (PCA) 694 3 0.4 0.004 - 0.006 0.004 3 0 0

Pronamide 694 3 0.4 0.003 - 0.005 0.002 3 0 0

4 Carrots (4 pesticides)

Atrazine 499 1 0.2 0.001 0.001 1 0 0

Pyrimethanil 499 10 2 0.005 - 0.035 0.005 9 1 0

Quintozene (PCNB) (parent) 13

 Pentachloroaniline (PCA) 499 8 1.6 0.006 - 0.018 0.005 2 6 0

 Pentachlorobenzene (PCB) 499 2 0.4 0.005 0.002 0 2 0

Tebuconazole 499 1 0.2 0.023 0.015 0 1 0

5 Cauliflower (5 pesticides)

Chlorpropham 692 7 1 0.002 - 0.003 0.001 7 0 0

Hexythiazox 692 1 0.1 0.003 0.002 1 0 0

Norflurazon desmethyl 692 1 0.1 0.002 0.001 1 0 0

Spirodiclofen 692 1 0.1 0.010 0.006 1 0 0

Thiobencarb 692 2 0.3 0.002 - 0.009 0.001 1 1 0

Sample Origin

Distribution of Residues with No Tolerance Listed in 40 CFR, Part 180, 

Range of 

LODs, ppm ^

Number of 

Samples

Samples 

Reported

% of 

Samples 

Range of Values 

Detected, ppm ^

by Commodity/Pesticide

Appendix H. Page 3 of 6
Commodity / Pesticide U.S. Import Unk.

Sample Origin Range of 

LODs, ppm ^

Number of 

Samples

Samples 

Reported

% of 

Samples 

Range of Values 

Detected, ppm ^

6 Collard Greens (15 pesticides)

Atrazine 514 33 6.4 0.002 - 0.029 0.002 32 1 0

Bromacil 514 1 0.2 0.004 0.003 1 0 0

Chlorothalonil 514 10 1.9 0.025 - 7.7 0.020 10 0 0

Chlorpropham 514 1 0.2 0.048 0.020 0 1 0

Cymoxanil 514 1 0.2 0.006 0.005 1 0 0

Dimethoate 514 1 0.2 0.009 0.005 0 1 0

Diuron 482 2 0.4 0.002 - 0.004 0.002 2 0 0

Famoxadone 514 2 0.4 0.029 - 0.053 0.025 2 0 0

Fenpropimorph 450 1 0.2 0.001 0.001 1 0 0

Linuron 514 5 1 0.009 - 0.023 0.008 3 2 0

Metribuzin 514 6 1.2 0.006 - 0.042 0.005 6 0 0

Oxamyl (parent) 14 514 3 0.6 0.011 - 0.96 0.003 2 1 0

 Oxamyl oxime 514 1 0.2 0.052 0.007 0 1 0

Pronamide 514 14 2.7 0.002 - 0.020 0.002 14 0 0

Propamocarb hydrochloride 514 3 0.6 0.006 - 0.054 0.002 3 0 0

Propargite 514 1 0.2 0.099 0.050 1 0 0

7 Eggplant (6 pesticides)

Chlorpropham 661 5 0.8 0.002 - 0.020 0.001 - 0.010 2 3 0

Dimethoate 661 1 0.2 0.002 0.001 - 0.010 1 0 0

Imazalil 661 2 0.3 0.002 0.001 - 0.005 0 2 0

Pyrimethanil 661 4 0.6 0.002 - 0.007 0.001 - 0.005 1 3 0

Thiacloprid 661 7 1.1 0.002 - 0.049 0.001 - 0.005 1 6 0

Thiophanate methyl 311 1 0.3 0.11 0.10 1 0 0

8 Green Beans (12 pesticides)

Atrazine 177 1 0.6 0.002 0.001 1 0 0

Chlorpropham 177 4 2.3 0.002 - 0.015 0.001 1 1 2

Difenoconazole 177 3 1.7 0.002 - 0.004 0.001 0 3 0

Diflubenzuron 177 2 1.1 0.001 - 0.032 0.001 2 0 0

Fenpropathrin 177 2 1.1 0.003 - 0.058 0.001 0 2 0

Fipronil (parent) 15 177 1 0.6 0.061 0.001 0 1 0

 Fipronil sulfone (MB46136) 177 1 0.6 0.009 0.001 0 1 0

Flutriafol 177 3 1.7 0.001 - 0.004 0.001 3 0 0

Isoprothiolane 177 4 2.3 0.001 - 0.002 0.001 4 0 0

Permethrin Total 16 177 1 0.6 0.004 0.003 0 1 0

Profenofos 177 1 0.6 0.003 0.001 0 1 0

Propamocarb 177 7 4 0.002 - 0.060 0.001 3 4 0

Pyrimethanil 177 1 0.6 0.009 0.005 0 1 0

9 Kiwi Fruit (2 pesticides)

Boscalid 177 3 1.7 0.030 - 0.087 0.015 1 2 0

Buprofezin 177 1 0.6 0.002 0.001 1 0 0

10 Orange Juice (2 pesticides)

Carbendazim (MBC) 12 499 1 0.2 0.002 0.001 0 1 0

Diphenylamine (DPA) 499 1 0.2 0.002 0.001 1 0 0

Appendix H. Page 4 of 6
Commodity / Pesticide U.S. Import Unk.

Sample Origin Range of 

LODs, ppm ^

Number of 

Samples

Samples 

Reported

% of 

Samples 

Range of Values 

Detected, ppm ^

11 Radishes (6 pesticides)

Carbendazim (MBC) 12 689 1 0.1 0.085 0.010 0 1 0

Chlorpropham 689 1 0.1 0.008 0.005 1 0 0

Indoxacarb 689 1 0.1 0.013 0.010 0 1 0

Permethrin Total 16 689 3 0.4 0.011 - 0.10 0.005 1 2 0

Propamocarb 689 2 0.3 0.16 - 0.58 0.010 0 2 0

Pyrimethanil 689 1 0.1 0.12 0.003 0 1 0

12 Summer Squash (3 pesticides)

Forchlorfenuron 176 1 0.6 0.001 0.001 0 1 0

Pentachloroaniline (PCA) 176 1 0.6 0.001 0.001 - 0.005 1 0 0

Quinoxyfen 176 3 1.7 0.001 - 0.006 0.001 1 2 0

13 Sweet Bell Peppers (4 pesticides)

Carbendazim (MBC) 12 675 1 0.1 0.012 0.010 0 1 0

Chlorpropham 675 5 0.7 0.005 - 0.014 0.005 1 4 0

Etridiazole 675 2 0.3 0.006 - 0.008 0.005 0 2 0

Fipronil 675 1 0.1 0.014 0.005 0 1 0

14 Tangerines (6 pesticides)

Benzovindiflupyr 687 1 0.1 0.006 0.005 0 1 0

Carbendazim (MBC) 12 687 1 0.1 0.13 0.050 1 0 0

Fenarimol 687 1 0.1 0.005 0.005 0 1 0

Isopyrazam 687 1 0.1 0.006 0.005 0 1 0

Simazine 687 1 0.1 0.006 0.005 1 0 0

Tebuconazole 687 2 0.3 0.005 0.005 1 1 0

15 Tomato Paste (3 pesticides)

Diphenylamine (DPA) 256 3 1.2 0.001 - 0.002 0.001 3 0 0

Propargite 506 2 0.4 0.002 0.001 - 0.025 2 0 0

Thiabendazole 506 1 0.2 0.002 0.001 - 0.010 0 0 1

16 Winter Squash (9 pesticides)

Benalaxyl 677 2 0.3 0.009 - 0.010 0.003 0 2 0

Chlorpropham 677 22 3.2 0.001 - 0.052 0.001 8 14 0

Diflubenzuron 677 1 0.1 0.002 0.001 1 0 0

Epoxiconazole 677 5 0.7 0.002 - 0.016 0.001 0 5 0

Imazalil 677 1 0.1 0.007 0.003 0 1 0

Linuron 677 1 0.1 0.003 0.003 1 0 0

Pendimethalin 677 1 0.1 0.001 0.001 1 0 0

Propargite 677 1 0.1 0.002 0.001 1 0 0

Quintozene (PCNB) (parent) 

 Pentachloroaniline (PCA) 677 6 0.9 0.002 - 0.004 0.001 4 2 0

 Pentachlorobenzene (PCB) 677 1 0.1 0.002 0.001 0 1 0

Appendix H. Page 5 of 6
Commodity / Pesticide U.S. Import Unk.

Sample Origin Range of 

LODs, ppm ^

Number of 

Samples

Samples 

Reported

% of 

Samples 

Range of Values 

Detected, ppm ^

NOTES

1 Includes cyhalothrin lambda plus its R157836 epimer.

2 Collard Green sample had 2 tolerance exceeders: bifenthrin and tetrahydrophthalimide.

3 Tetrahydrophthalimide (THPI) is a metabolite of captafol and captan.

4 Food Handling Estabilishment (FHE) tolerance of 0.02 ppm was applied to both acephate and its metabolite/degradate methamidophos.

5 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

6 Green Bean sample had 3 tolerance exceeders: acephate and its methamidophos metabolite and buprofezin.

7 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

8 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

9 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

10 Green Bean sample had 2 tolerance exceeders: acephate and its methamidophos metabolite.

11 Sweet Bell Pepper sample had 2 tolerance exceeders: cyhalothrin and imidacloprid.

12 Carbendazim (MBC) is a metabolite of benomyl and thiophanate methyl.

13 Two Carrot samples contained both the PCA and PCB metabolites of quintozene.

14 One Collard Green sample contained both oxamyl and its oxime metabolite.

15 One Green Bean sample contacted both fipronil and its sulfone metabolite.

16 Includes permethrin cis and trans isomers.

^ When a range is not listed, only one distinct detected concentration or LOD value was reported for the pesticide/commodity pair.

Note:

For those pesticide/commodity pairs where the minimum detected value is less than the limit of quantitation (three times

the limit of detection), the reported values are estimates. In a few cases, this may apply to the maximum detected value.

Appendix H. Page 6 of 6
PESTICIDE DATA PROGRAM

 Annual Summary, Calendar Year 2020

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