United States Department of Agriculture

December 2014

Dear Reader:

We are pleased to present the Pesticide Data Program’s (PDP) 23rd Annual Summary for 

calendar year 2013. The U.S. Department of Agriculture (USDA), Agricultural Marketing 

Service (AMS), conducts this program each year to collect data on pesticide residues in 

food. This report shows that overall pesticide residues found in foods are at levels below the 

tolerances set by the U.S. Environmental Protection Agency (EPA).

The PDP provides reliable data that helps assure consumers that the food they feed their 

families is safe. Over 99 percent of the products sampled through PDP had residues below 

the EPA tolerances. Ultimately, if EPA determines a pesticide is not safe for our families, it is 

removed from the market. This system of checks and balances provides Americans with the 

safest food supply in the world.

The PDP tests a wide variety of domestic and imported foods using a sound statistical program 

and the most current laboratory methods. The EPA uses the PDP data when looking at dietary 

pesticide exposure, a critical step to verify that all sources of exposure to pesticides meet U.S. 

safety standards. 

The PDP is not designed for enforcement of EPA pesticide residue tolerances. Rather, the 

U.S. Food and Drug Administration (FDA) is responsible for enforcing EPA tolerances. PDP 

provides FDA and EPA with monthly reports of pesticide residue testing and informs the FDA if 

residues detected exceed the EPA tolerance or have no EPA tolerance established. In instances 

where a PDP fi nding is extraordinary and may pose a safety risk, FDA and EPA are notifi ed 

immediately. In such cases, USDA may also work with U.S. growers in an outreach effort to 

communicate possible pesticide regulatory decisions or improved agricultural practices.

The PDP works with State agencies representing all regions of the country and more than half 

of the U.S. population. In 2013, samples were collected and analyzed in California, Colorado, 

Florida, Maryland, Michigan, Minnesota, Montana, New York, North Carolina, Ohio, Texas, 

Washington, and Wisconsin. The data reported by PDP corroborate that residues found in 

agricultural products sampled are at levels that do not pose risk to consumers’ health (i.e., are 

safe according to EPA). 

For more information about PDP, please visit our website at www.ams.usda.gov. For more 

information about pesticides and food, please visit EPA’s website at 

http://www.epa.gov/pesticides/food.

Agricultural Marketing Service

1400 Independence Avenue, SW, Washington, DC 20250-0201

Voice (202) 720-8998 Fax (202) 720-7135

An Equal Opportunity Provider and Employer
Pesticide Data Program—Annual Summary, Calendar Year 2013

iii

Contents

Page No.

Acknowledgements........................................................................................................................ vii

Executive Summary...................................................................................................................... ix

Acronyms and Abbreviations........................................................................................................ xi

Section I--Introduction............................................................................................................... 1

Section II--Sampling Operations............................................................................................... 4

 Background...................................................................................................................... 4

 Fresh and Processed Commodities.................................................................................. 6

 Butter............................................................................................................................... 10

 Infant Formula................................................................................................................. 11 

 Salmon............................................................................................................................. 11

 Drinking Water................................................................................................................. 12

Section III--Laboratory Operations......................................................................................... 13

 Overview.......................................................................................................................... 13 

 Fresh and Processed Commodities.................................................................................. 13

 Baby Food........................................................................................................................ 14

 Infant Formula................................................................................................................. 14

 Butter............................................................................................................................... 14

 Salmon............................................................................................................................. 15

 Potable Groundwater from Domestic and School/Childcare Facility............................. 15

 Municipal Drinking Water............................................................................................... 15

 Quality Assurance Program............................................................................................. 15

Section IV--Database Management.......................................................................................... 17

 Electronic Data Path........................................................................................................ 17

 Data Reporting............................................................................................................... 19

Section V--Sample Results and Discussion.............................................................................. 19

 Overview......................................................................................................................... 19

 Baby Food........................................................................................................................ 20

 Infant Formula................................................................................................................. 20

 Import vs. Domestic Residue Comparisons.................................................................... 20

 Postharvest Applications................................................................................................. 21

 Discussion of Results ..................................................................................................... 21

 Special Projects............................................................................................................... 22

 Potable Groundwater....................................................................................................... 22

 Municipal Drinking Water............................................................................................... 23

 Environmental Contaminants.......................................................................................... 23

 Tolerance Violations........................................................................................................ 24
Pesticide Data Program—Annual Summary, Calendar Year 2013

v

Figures Page No.

 1 PDP Program Operations Support and Data Users............................................................. 2 

 2 Program Participants........................................................................................................... 3

 3 Commodity Origin.............................................................................................................. 9

 4 Origin of Selected Fresh Commodities: Raspberry and Summer Squash Samples............ 11

 5 PDP Data Pathway............................................................................................................... 18

Tables

 1 PDP Commodity Collection Schedule for 2013.................................................................. 5 

 2 Distribution of Samples Collected and Analyzed by Each Participating State................... 7

 3 Acceptable Products for Collected Commodities................................................................ 8

 

Appendixes A-M

 Appendix A Commodity History

 Appendix B Distribution of Residues by Pesticide in Fruit and Vegetables

 Appendix C Distribution of Residues by Pesticide in Infant Formula

 Appendix D Distribution of Residues by Pesticide in Butter

 Appendix E Distribution of Residues by Pesticide in Salmon

 Appendix F Distribution of Residues by Pesticide in Groundwater

 Appendix G Distribution of Residues by Pesticide in Drinking Water

 Appendix H Distribution of Residues for Environmental Contaminants

 Appendix I Sample Origin by State or Country

 Appendix J Import vs. Domestic Pesticide Residue Comparisons

 Appendix K Pesticide Residues by Commodity

 Appendix L Number of Pesticides Detected per Sample

 Appendix M Fruit and Vegetable Samples Reported to the U.S. Food and Drug 

 Administration as Exceeding the Tolerance or Without Established 

 Tolerance
Pesticide Data Program—Annual Summary, Calendar Year 2013

vii

Acknowledgements

The States participating in the Pesticide Data 

Program (PDP) deserve special recognition for 

their contributions to the program. The dedication 

and fl exibility of sample collectors allow the U.S. 

Department of Agriculture’s (USDA) Agricultural 

Marketing Service (AMS) to adjust sampling 

protocols when responding to changing trends 

in commodity distribution and availability. PDP 

acknowledges the contributions of the State 

laboratories in providing testing services to the 

program and the USDA National Agricultural 

Statistics Service for providing statistical support. 

PDP also acknowledges the exceptional support 

of the Health Effects Division staff of the U.S. 

Environmental Protection Agency, Offi ce of 

Pesticide Programs, and the Food and Drug 

Administration, Center of Food Safety and 

Nutrition, Offi ce of Food Safety, in helping to set 

the direction for PDP. 

 

Data presented in this report are the latest available 

and were collected and processed through the 

efforts of the following organizations:

USDA Program Administration

Agricultural Marketing Service

Science and Technology Program

1400 Independence Ave., SW

South Building, Mail Stop 0270

Washington, DC 20250

Ruihong Guo, Ph.D., Deputy Administrator, 

Science and Technology Program

 (202) 720-8556, Facsimile (202) 720-6496

Diana Haynes, Director

Monitoring Programs Division, AMS

1400 Independence Ave, SW

Room 0611-S, Stop 0276

Washington, DC 20250: 

(202) 572-8167, Facsimile (202) 619-1724

Electronic-mail Address:

amsmpo.data@ams.usda.gov

Website:

http://www.ams.usda.gov/pdp

Participating State Agencies

California Department of Food and Agriculture

California Department of Pesticide Regulation

Colorado Department of Agriculture

Florida Department of Agriculture and

 Consumer Services

Maryland Department of Agriculture

Michigan Department of Agriculture and 

 Rural Development

Minnesota Department of Agriculture

Montana Department of Agriculture

New York Department of Agriculture and 

 Markets

North Carolina Department of Agriculture &

 Consumer Services

Ohio Department of Agriculture

Texas Department of Agriculture

Washington State Department of Agriculture

Wisconsin Department of Agriculture, Trade, 

 and Consumer Protection

Participating Laboratories

California Department of Food and Agriculture

Division of Inspection Services

Center for Analytical Chemistry

3292 Meadowview Rd.

Sacramento, CA 95832

 

Florida Department of Agriculture and

 Consumer Services

Chemical Residue Laboratory

3125 Conner Blvd., Bldg. 3

Tallahassee, FL 32399-1650

Michigan Department of Agriculture and 

 Rural Development

Laboratory Division

1615 South Harrison Rd.

East Lansing, MI 48823-5224
Pesticide Data Program—Annual Summary, Calendar Year 2013

viii

Minnesota Department of Agriculture

Laboratory Services Division

601 N. Robert St.

St. Paul, MN 55155-2531

Montana Department of Agriculture

Laboratory Bureau

McCall Hall, Montana State University

Bozeman, MT 59717

New York Department of Agriculture 

 and Markets

Food Laboratory

6 Harriman Campus Road

Albany, NY 12235

Ohio Department of Agriculture

Consumer Analytical Laboratory

8995 East Main St.

Reynoldsburg, OH 43068

Texas Department of Agriculture

Pesticide Laboratory

1500 Research Parkway, Ste. B100

College Station, TX 77845

Washington State Department of Agriculture

Chemical and Hop Laboratory

21 N. 1st Ave., Ste. 106

Yakima, WA 98902
Pesticide Data Program—Annual Summary, Calendar Year 2013

ix

Executive Summary

In 1991, the U.S. Department of Agriculture 

(USDA), Agricultural Marketing Service (AMS), 

was charged with designing and implementing the 

Pesticide Data Program (PDP) to collect data on 

pesticide residues in food. PDP provides highquality data on residues in food, particularly foods 

most likely consumed by infants and children. This 

23rd Pesticide Data Program summary presents 

results for samples collected in 2013.

This information is provided to the U.S. 

Environmental Protection Agency (EPA). Before 

a company can sell or distribute any pesticide in 

the United States of America, EPA must review 

studies on the pesticide to determine that it will 

not pose unreasonable risks to human health 

or the environment. Once EPA has made that 

determination, it will license or register that 

pesticide for use in strict accordance with label 

directions. 

Before allowing a pesticide to be used on a food 

commodity, EPA sets limits on how much of a 

pesticide may be used on food during growing, 

processing, and storage, and how much can remain 

on the food that reaches the consumer. Government 

inspectors monitor food in interstate commerce to 

ensure that these limits are not exceeded. EPA also 

sets standards to protect workers from exposure to 

pesticides on the job. 

AMS, through its Monitoring Programs Division 

(MPD), is responsible for the administration, 

planning, and coordination of day-to-day PDP 

operations. MPD meets regularly with EPA and 

other Government agencies to establish program 

priorities and direction. Sampling and/or testing 

program operations were carried out with the 

support of 13 States: California, Colorado, Florida, 

Maryland, Michigan, Minnesota, Montana, New 

York, North Carolina, Ohio, Texas, Washington, 

and Wisconsin. These States had a prominent role 

in program planning and policy setting, particularly 

policies relating to quality assurance.

Drinking water sampling from public utilities was 

conducted by utility personnel while homeowners 

sampled their own well (ground) water. In 2013, 

a groundwater survey of schools and childcare 

facilities also was performed in which school and 

childcare facility personnel sampled the well water 

serving the facility. 

PDP commodity sampling is based on a rigorous 

statistical design that ensures the data are reliable 

for use in exposure assessments and can be used 

to draw various conclusions about the Nation’s 

food supply. The pesticides and commodities to 

be included each year in the sampling are selected 

based on EPA data needs and take into account the 

types and amounts of food consumed by infants 

and children. The number of samples collected by 

the States is apportioned according to that State’s 

population. Samples are randomly chosen close to 

the time and point of consumption (i.e., distribution 

centers rather than at the farm gate) and refl ect what 

is typically available to the consumer throughout 

the year. Samples are selected without regard to 

country of origin, variety, or organic labeling.

Fresh and processed fruit and vegetables accounted 

for 84.4 percent of the total 10,104 samples 

collected in 2013. Other samples collected included 

butter, 7.5 percent; infant formula, 3.5 percent; 

salmon, 3.5 percent; and water, 1.1 percent. Fresh 

and processed fruit and vegetables tested during 

2013 were: apple juice, baby food (applesauce 

and peas), bananas, broccoli, carrots, caulifl ower, 

celery, grape juice, greens beans, mushrooms, 

nectarines, peaches, plums, raspberries (fresh 

and frozen), summer squash, and winter squash. 

Excluding water samples, which were all from 

domestic sources, domestic samples accounted 

for 70.8 percent of the samples while 26.6 percent 

were imports, 1.9 percent were of mixed origin, 

and 0.7 percent were of unknown origin.

Because PDP data are mainly used for risk 

assessments, PDP laboratory methods are geared 

to detect the smallest possible levels of pesticide 

residues, even when those levels are well below 

the tolerances established by EPA. Prior to testing, 

PDP analysts washed samples for 15-20 seconds 

with gently running cold water as a consumer 

would do; no chemicals, soap, or any special wash 

was used. Results for more than 2 million analyses 
Pesticide Data Program—Annual Summary, Calendar Year 2013

x

were reported by the laboratories in 2013 and are 

too numerous to be included in their entirety in 

this summary. The PDP database fi le for 2013 and 

annual summaries/database fi les for previous years 

are available on the PDP website at http://www.

ams.usda.gov/pdp or by contacting MPD.

In 2013, over 40 percent of the samples tested 

had no detectable pesticide residue. Appendixes 

B through G provide a distribution of residues by 

pesticide for the commodities tested. Excluding 

water, residues exceeding the tolerance were 

detected in 0.23 percent (23 samples) of the 

total samples tested (9,990 samples). Of these 

23 samples, 17 were imported (74 percent) and 

6 were domestic (26 percent). Residues with no 

established tolerance were found in 3.0 percent 

(301 samples) of the total samples tested (9,990 

samples). Of these 301 samples, 151 were domestic 

(50.2 percent), 148 were imported (49.2 percent), 

and 2 were of unknown origin (0.6 percent). PDP 

is a voluntary program and is not designed for 

enforcement of tolerances. However, PDP informs 

the U.S. Food and Drug Administration if residues 

detected exceed the EPA tolerance or have no EPA 

tolerance established. 

PDP laboratories also test foods for low levels of 

environmental contaminants that are no longer used 

in the United States, but due to their persistence in 

the environment, particularly in soil, can be taken up 

by plants. Results for environmental contaminants 

in all commodities are listed in Appendix H. More 

information on results is provided in the Sample 

Results and Discussion section of this summary.

Also in 2013, 100 (treated and untreated) drinking 

water samples were collected at water treatment 

facilities in 6 States and 14 groundwater samples 

were collected from private domestic wells and 

school/childcare facilities in 5 States. Low levels 

of detectable residues, measured in parts per 

trillion, were detected in both drinking water 

and groundwater. The majority of pesticides, 

metabolites, and isomers included in the PDP 

testing profi les were not detected. During 2013, no 

detections in treated water or groundwater exceeded 

established Maximum Contaminant Levels, 

Health Advisories, Human Health Benchmarks 

for Pesticides, or Freshwater Aquatic Organism 

criteria. Additional information is provided in 

the Sample Results and Discussion section of this 

Annual Summary. 

PDP continually strives to improve methods for 

collecting, testing, and reporting data. These data 

are freely available to EPA and other Federal and 

State agencies charged with regulating and setting 

policies on the use of pesticides and to the public 

by hard copy, Internet, or custom reports generated 

by MPD. Additional copies of the PDP Annual 

Summary may be obtained by mailing the form 

provided at the end of the Summary. 

The U.S. Department of Agriculture (USDA) prohibits discrimination in all its programs and activities on the basis of race, color, national origin, age, disability, 

and where applicable, sex, marital status, familial status, parental status, religion, sexual orientation, genetic information, political beliefs, reprisal, or because 

all or part of an individual’s income is derived from any public assistance program (not all prohibited bases apply to all programs). Persons with disabilities 

who require alternative means for communication of program information (Braille, large print, audiotape, etc.) should contact USDA’s TARGET Center at 

(202) 720-2600 (voice and TDD). To fi le a complaint of discrimination, write to USDA, Director, Offi ce of Civil Rights, 1400 Independence Avenue, S.W., 

Washington, D.C. 20250-9410, or call (800) 795-3272 (voice) or (202) 720-6382 (TDD). USDA is an equal opportunity provider and employer.

Disclaimer: Mention of a trade name or brand name does not constitute endorsement or recommendation by USDA over 

similar products or vendors.
Pesticide Data Program—Annual Summary, Calendar Year 2013

xi

Acronyms and Abbreviations

% C.V. Percent Coeffi cient of Variation

A2LA American Association for Laboratory Accreditation

AL Action Level

AMS Agricultural Marketing Service

BQL Below Quantifi able Level

EPA Environmental Protection Agency

e-SIF Electronic Sample Information Form

FAO Freshwater Aquatic Organism

FAPAS Food Analysis Performance Assessment Scheme

FDA Food and Drug Administration

FQPA Food Quality Protection Act

GC Gas Chromatography

HCB Hexachlorobenzene

HHBP Human Health Benchmarks for Pesticides

ISO International Organization for Standardization

LC Liquid Chromatography

LOD Limit of Detection

LOQ Limit of Quantitation

MCL Maximum Contaminant Level

MPD Monitoring Programs Division

MRM Multiresidue Method

MS Mass Spectrometry

NASS National Agricultural Statistics Service

PDP Pesticide Data Program

PT Profi ciency Testing

QA Quality Assurance

QAU Quality Assurance Unit
Pesticide Data Program—Annual Summary, Calendar Year 2013

xii

QuEChERS Quick, Easy, Cheap, Effective, Rugged and Safe

QC Quality Control

RDE Remote Data Entry

SDWA Safe Drinking Water Act

SIF Sample Information Form

SOP Standard Operating Procedure

USDA United States Department of Agriculture
Pesticide Data Program—Annual Summary, Calendar Year 2013

1

Pesticide Data Program (PDP)

Annual Summary, Calendar Year 2013

This summary consists of the following sections: (I.) Introduction, (II.) Sampling Operations, 

(III.) Laboratory Operations, (IV.) Database Management, and (V.) Sample Results and Discussion

I. Introduction

The U.S. Department of Agriculture (USDA) 

Agricultural Marketing Service (AMS) initiated 

the Pesticide Data Program (PDP) in 1991 to 

collect data on pesticide residues in food and 

now has an important role in the implementation 

of the 1996 Food Quality Protection Act (FQPA). 

The law directs the Secretary of Agriculture to 

collect pesticide residue data on commodities most 

frequently consumed by infants and children. PDP 

data are used primarily by the U.S. Environmental 

Protection Agency (EPA) to assess dietary 

exposure during the review of the safety of existing 

pesticide tolerances (Maximum Residue Limits). 

PDP data also are used by the U.S. Food and 

Drug Administration (FDA) to assist in planning 

commodity surveys for pesticide residues from an 

enforcement/regulatory perspective.

Because PDP collects data on food commodities 

primarily for exposure assessment, program 

operations differ markedly from those followed 

by regulatory monitoring programs for tolerance 

enforcement. PDP samples are collected closer 

to the point of consumption and are prepared 

emulating consumer practices. Sampling is based 

on EPA data needs and does not impede commodity 

distribution. Laboratory operations are designed to 

achieve the lowest detectable levels rather than quick 

sample turnaround. As a dietary risk assessment 

support program, PDP tests for registered uses 

for the commodities in the program, as well as for 

pesticides that may not have U.S. tolerances but are 

used in other countries on commodities exported to 

the United States.

Figure 1(a) illustrates contributors to PDP 

policy development and planning operations. 

Primary contributors to these activities include 

the participating States, EPA, USDA’s National 

Agricultural Statistics Service (NASS), and 

additional stakeholders including industry and 

grower groups. Figure 1(b) depicts PDP primary 

data users including EPA, FDA, USDA’s Economic 

Research Service, and Foreign Agricultural Service, 

participating States, academic institutions, chemical 

manufacturers, environmental interest groups, 

food safety organizations, and groups within the 

private sector representing food producers. Other 

Federal, State, and foreign government agencies 

and industries have used PDP data to promote 

the export of U.S. commodities to international 

markets. Additionally, the Codex Alimentarius 

Committee on Pesticides Residues recognizes PDP 

methodologies as offi cial and validated methods 

for the determination of pesticide residues in foods.

In 2013, sampling services were provided by 11 

States (California, Colorado, Florida, Maryland, 

Michigan, New York, North Carolina, Ohio, Texas, 

Washington, and Wisconsin). Sampling services 

for drinking water were provided by participating 

facility personnel at eight individual sites in six 

States. A voluntary groundwater survey was 

continued in 2013 with homeowners and school/

childcare facilities at 14 sites in 5 States.

Laboratory services were provided by the States 

of California, Florida, Michigan, Minnesota, 

Montana, New York, Ohio, Texas, and Washington. 

The AMS Monitoring Programs Division (MPD) is 

responsible for overall management of PDP.

Figure 2 shows the States that participate in 

program sampling and/or testing. Together, 

these States represent about 50 percent of the 

Nation’s population and all 4 census regions of 

the United States. They also represent major U.S. 

producers of fruit and vegetables. MPD works 

closely with EPA and FDA to select commodities 

and pesticides for testing and with EPA in the 

selection of drinking water and groundwater sites. 

The selected commodities represent the highest 

U.S. consumption, with an emphasis on foods 

consumed by infants and children. Commodities 

are cycled through the program approximately 

every 5 years. High-consumption fresh fruit and 

vegetable commodities remain in the program for 2 

years to capture two full growing seasons, thereby 
Pesticide Data Program—Annual Summary, Calendar Year 2013

2

Figure 1. PDP Program Operations Support and Data Users. This fi gure illustrates (a) agencies/groups 

that support PDP program policy and planning activities and (b) agencies/groups that use PDP data. 

Program Operations

Participating 

States

National

Agricultural Statistics 

Service

Industry and

Grower Groups

Environmental

Protection

Agency

(a) PDP Policy and Planning Contributions

Data

Food and Drug 

Administration Environmental 

Protection 

Agency

Academic 

Institutions

Agricultural 

Industry

Foreign 

Agricultural 

Service

Economic 

Research 

Service

Chemical 

Manufacturers, 

Environmental 

Interest Groups, Food 

Safety Organizations

Other 

Government 

Agencies

Participating 

States

(b) PDP Data Users
Pesticide Data Program—Annual Summary, Calendar Year 2013

3

capturing any changes due to seasonality or yearto-year variations. Processed products, as well as 

dairy, meat, fi sh, and grains, are tested for 1 full 

year. Appendix A provides a list of commodities 

tested by PDP from the beginning of the program 

in 1991 through 2014.

Fruit and vegetable samples are collected at 

terminal markets1

 and large chain store distribution 

centers from which food commodities are supplied 

to supermarkets and grocery stores. Sampling at 

these locations allows for residue measurements that 

include pesticides applied during crop production 

and those applied after harvest (such as fungicides, 

growth regulators, and sprouting inhibitors) and 

takes into account residue degradation while food 

commodities are in storage. Participation as a 

PDP sampling site is voluntary, which sets it apart 

from State and Federal enforcement programs. In 

2013, over 600 sites granted access and provided 

information, including site volume data, to sample 

collectors. Voluntary cooperation is important 

to PDP and makes it possible to adjust sampling 

protocols in response to fl uctuations in food 

distribution and production.

Pesticides screened by PDP include those with 

current registered uses and compounds for which 

toxicity data and preliminary estimates of dietary 

exposure indicate the need for more extensive 

Figure 2. Program Participants. During 2013, AMS established cooperative agreements with 13 States to sample and/or test 

PDP commodities. Together, these States represent about 50 percent of the Nation’s population and all 4 census regions of the 

U.S. They also represent major U.S. producers of fruit and vegetables. State laboratories are responsible for analyzing

fresh and processed fruit and vegetable, infant formula, butter, salmon, groundwater, and drinking water samples.

Washington

California

Colorado

Texas

Ohio

Wisconsin

New York

Florida

Maryland

Michigan

Participating State

Location of Participating State Laboratories

North Carolina

Montana Minnesota

Testing Services Only

1

 Terminal markets are facilities where wholesalers receive large quantities of fresh fruit and vegetables by rail, truck 

and air from around the world for sale to grocers, restaurants, institutions, and other businesses. Terminal markets are 

often located in metropolitan areas at or near major transportation hubs.
Pesticide Data Program—Annual Summary, Calendar Year 2013

4

residue data. PDP also monitors pesticides for 

which EPA has modifi ed use directions (i.e., 

reduced application rates or frequency) as part of 

risk management activities. In addition, PDP tests 

for selected pesticides that may not have U.S. 

tolerances, but are used in other countries that export 

commodities to the United States. The following 

appendixes list the specifi c pesticides tested in the 

program: fruit and vegetables (Appendix B), infant 

formula (Appendix C), butter (Appendix D), salmon 

(Appendix E), potable groundwater (Appendix 

F), and municipal drinking water (Appendix G). 

Environmental contaminants, or pesticides whose 

uses have been canceled in the United States 

but their residues persist in the environment, are 

consolidated into Appendix H, which summarizes 

fi ndings for these chemicals across all commodities. 

II. Sampling Operations

♦ Background

The goal of the PDP sampling program is to obtain 

a statistically defensible representation of the U.S. 

food supply. PDP data refl ect actual pesticide residue 

exposure from food. Using a rigorous statistical 

design, PDP has developed extensive procedures 

that ensure samples are randomly selected from the 

national food distribution system and refl ect what is 

typically available to the consumer.

At all sampling locations, information is usually 

available about the identity and origin of the 

sample. Sample information is captured at the time 

of collection for inclusion in the PDP database. 

PDP sample origin data identify the State or country 

where the commodity was produced. A comparison 

of PDP sample origin data to State production 

and import data by USDA’s NASS shows PDP 

sampling is representative of the U.S. food supply. 

PDP sampling operations are adjusted according to 

product availability. The number of fruit, vegetable, 

infant formula, butter, and salmon samples 

collected in each participating State is determined 

by State population. The number and location of 

groundwater samples are determined based on 

geographic region, location in an agricultural area, 

and the willingness of the well owners to participate 

in the program. The quarterly collection schedule 

for all 2013 commodities is shown in Table 1. 

In 2013, fruit, vegetables, infant formula, butter, 

and salmon were randomly collected by trained 

State inspectors at terminal markets and large chain 

store distribution centers throughout the country. 

Surrogate or “proxy” sites (retail markets) are 

used to collect these samples when the commodity 

of interest is unavailable at a terminal market 

or distribution center. In these instances, the 

commodity is selected in the rear storage area of 

the retail facility so possible contamination by 

the consumer is eliminated and allows capture of 

sample information from product boxes. In 2013, 

29.7 percent of fruit, vegetable, infant formula, 

butter, and salmon samples were collected at proxy 

sites. The commodities most often collected at these 

facilities were infant formula, grape juice, baby 

foods (applesauce and peas), frozen raspberries, 

apple juice, and salmon. 

Treated and untreated drinking water samples were 

collected onsite by trained personnel at selected 

water treatment facilities across the country. 

Potable groundwater samples were collected 

from private domestic wells by homeowners and 

school/childcare facility personnel. Participation 

in the groundwater survey is voluntary, with site 

selections based on agricultural chemical usage in 

the surrounding watershed and geographic location. 

The number and location of drinking water samples 

from water treatment facilities are determined by 

EPA pesticide registration information needs. Each 

local watershed has its own unique characteristics; 

therefore, sample collection for this commodity is 

not intended to refl ect national trends; rather, PDP 

collects samples in areas where it is known that 

targeted pesticides are used. 

PDP State sample collectors are trained to adhere 

to detailed program Standard Operating Procedures 

(SOPs) that provide criteria for site selection and 

specifi c instructions for sample selection, shipping 

and handling, and chain-of-custody. SOPs are 

updated as needed and serve as a technical reference 

in conducting program sampling reviews to ensure 

program goals and objectives are met. SOPs for 

PDP sampling are available on the Internet at www.

ams.usda.gov/pdp. On a quarterly basis, sample 

collectors are provided with commodity Fact 

Sheets and Quick Reference Guides that list specifi c 
Pesticide Data Program—Annual Summary, Calendar Year 2013

5

collection details for individual commodities that 

have been added to the program.

Temperature-sensitive samples are packed in 

heavy-duty, temperature-controlled containers. 

Holding temperatures are preserved throughout 

transit time with the inclusion of ample frozen cold 

packs and insulating materials. Non-temperaturesensitive samples do not require temperaturecontrolled containers; however, they are shipped in 

heavy-duty, well-cushioned containers. To preserve 

sample integrity, most samples are shipped the 

same day as collection by overnight delivery. 

Non-refrigerated processed commodities such as 

apple juice, grape juice, infant formula, and baby 

foods (applesauce and peas) are often shipped by 

ground transportation to reduce shipping costs. 

Groundwater samples and raw intake and treated 

drinking water samples are collected in specially 

prepared bottles containing dechlorinating 

agents to halt potential compound degradation, 

packed with proper cushioning and cold packs, 

and shipped the same day as collection to their 

respective laboratory by overnight delivery. 

Electronic Sample Information Forms (e-SIFs) 

are used for chain-of-custody and to capture 

information needed to characterize the sample. 

Sample collectors use tablets or laptop computers 

in the fi eld to record sample identifi cation 

information such as: (1) State of sample collection, 

(2) collection date, (3) sampling site code, (4) 

commodity code, and (5) testing laboratory 

code. Information from these fi ve data elements 

Commodity Jan-Mar Apr-Jun Jul-Sep Oct-Dec End Date

Apple Juice Jun-13

Baby Food-Apple Sauce Jun-13

Baby Food-Peas Jun-13

Bananas Mar-14

Broccoli Dec-14

Butter Dec-13

Carrots Dec-14

Caulifl ower Sep-13

Celery Dec-14

Dairy-based Formula Sep-14

Fish, Salmon Jun-14

Grape Juice Sep-14

Green Beans Jun-15

Mushrooms Sep-13

Nectarines Dec-15

Peaches Jun-15

Plums Sep-13

Raspberries Dec-13

Raspberries, Frozen Dec-13

Soy-based Formula Sep-14

Summer Squash Sep-14

Water, Finished Apr-13

Water, Groundwater Feb-13

Water, Untreated Apr-13

Winter Squash Mar-13

Table 1. Pesticide Data Program (PDP) Commodity Collection Schedule for 2013. Samples are 

most often collected for a 2-year time period. Commodities are initiated or terminated in different 

quarters of the year, so that new commodities are not brought into the program all at the same time. 

This table illustrates time ranges for the listed commodities. See Appendix A for the complete PDP 

commodity history (May 1991 through December 2014).
Pesticide Data Program—Annual Summary, Calendar Year 2013

6

is combined to form a unique PDP identifi cation 

number for each sample. Other available 

information about each sample is also recorded, 

such as collector name; the State or country of 

origin; product variety; production claims such as 

organic; postharvest chemical applications; and 

grower, packer, and/or distributor locations. The 

e-SIFs are electronically mailed the same day 

as sample collection or, at the latest, by the next 

morning after collection to ensure that sample 

information is received at each laboratory by the 

time samples arrive for analysis. Refer to Section 

IV on Database Management for more information 

on the e-SIF system. 

Participating State agencies compile and maintain 

lists of sampling sites. In 2013, over 600 sites 

granted access to sample collectors. The States 

provide AMS and NASS with annual volume 

information for commodities distributed at the 

sites. This information is used to weight the site to 

determine the probability for sample selection. For 

example, a weight of 10 may be given to a site that 

distributes 100,000 pounds of produce annually 

and a weight of 1 is given to a site that distributes 

10,000 pounds. The probability-proportionate-tosize method of site selection then results in the 

larger site being 10 times more likely to be selected 

for sampling than the smaller site. 

Participating States work with NASS to develop 

statistical procedures for site weighting and 

selection. States are also given the option to have 

NASS perform their quarterly site selection. The 

number of sampling sites and the volume of produce 

distributed by the sites vary greatly among States. 

Sampling plans that include sampling dates, sites 

(primary and alternate), targeted commodities, and 

testing laboratories are prepared by each State on 

a quarterly basis. Collection of commodities is 

randomly assigned to weeks of the month, prior to 

selection of specifi c sampling dates within a week. 

Because sampling sites are selected for an entire 

quarter, States may assign the sites to particular 

months based on geographic location.

State population fi gures are used to assign the 

number of fruit, vegetable, and other specialty 

samples scheduled for collection each month. 

At the beginning of 2013, these population- and 

distribution-network-based numbers resulted in 

the following monthly collection assignments for 

each State: California, 13; Colorado, 2; Florida, 7; 

Maryland, 4; Michigan, 6; New York, 9; Ohio, 6; 

Texas, 9; Washington, 4; and Wisconsin, 2. This 

schedule resulted in a monthly target of 62 samples 

per commodity or 744 samples per commodity per 

year. Due to budgetary restrictions, PDP adjusted 

sampling rates during the year. By the end of 

2013, the monthly collection assignment for each 

State was as follows: California, 13; Colorado, 2; 

Florida, 7; Maryland, 4; Michigan, 6; New York, 

9; Ohio, 6; Texas, 8; and Washington, 4. The 

schedule results in a monthly target of 59 samples 

per commodity or 708 samples per commodity 

per year. Additionally, North Carolina collected 

four samples per month for selected commodities 

-- apple juice, baby foods (applesauce and peas), 

butter, green beans, and peaches. 

The total number of samples collected in each State 

for each commodity is listed in Table 2. Figure 2 

illustrates the participating collection States and 

the laboratories to which samples were shipped. 

Table 3 lists the acceptable product types for 

each collected commodity as seen on Commodity 

Fact Sheets provided to sample collectors. For all 

commodities, domestic or imported and organically 

grown or conventionally grown products are 

acceptable.

The total number of samples per commodity and 

the percentage of each that were either domestic, 

imported, or of unknown origin are shown in Figure 

3. The origin of some fresh commodities can vary 

greatly throughout the year. Graphic examples 

of this variation can be found in Figure 4 where 

differences in origin (domestic versus import) are 

depicted by month for raspberries and summer 

squash. Fresh and processed fruit and vegetable, 

infant formula, butter, and salmon samples 

originated from 36 States and 34 foreign countries 

(refer to Appendix I). Groundwater and drinking 

water samples are excluded from Appendix I 

because they rely on differential sampling frames. 

♦ Fresh and Processed Commodities 

Of all samples collected and analyzed in 2013, 

84.4 percent (8,526 of 10,104) were fruit and 
Pesticide Data Program—Annual Summary, Calendar Year 2013

7

State BN BR CE CF CR GB MU NE PC PU RS SS WS

Total 

Fresh

California 156 154 156 117 156 78 117 124 64 118 151 156 39 1,586

Colorado 24 24 24 18 24 12 18 17 8 14 24 24 6 237

Florida 84 84 84 63 84 42 63 71 31 66 75 84 21 852

Maryland 48 48 48 36 48 24 36 38 17 32 48 48 12 483

Michigan 66 66 66 48 66 36 48 51 24 61 61 66 18 677

New York 108 108 108 81 108 54 81 91 54 81 105 108 27 1,114

N. Carolina 24 12 36

Ohio 66 66 66 48 68 36 48 46 24 43 53 66 18 648

Texas 98 100 98 75 100 48 75 62 35 58 94 99 28 970

Washington 48 48 48 36 48 24 36 36 16 28 34 48 12 462

Wisconsin 10 10 10 10 10 10 7 6 7 10 6 96

TOTAL 708 708 708 532 712 378 532 543 285 507 652 709 187 7,161

State AJ GJ IA IE RZ

Total 

Processed

Total 

Fresh & 

Proccessed 

F&V

California 78 39 78 78 3 276 1,862

Colorado 12 5 12 12 41 278

Florida 42 21 42 42 9 156 1,008

Maryland 24 12 24 24 84 567

Michigan 30 18 30 30 5 113 790

New York 54 27 54 53 3 191 1,305

N. Carolina 24 24 24 72 108

Ohio 30 18 30 30 13 121 769

Texas 51 24 51 51 3 180 1,150

Washington 24 12 24 24 14 98 560

Wisconsin 10 10 10 3 33 129

TOTAL 379 176 379 378 53 1,365 8,526

Infant Formula

DF YF

39 41

6 6

21 21

12 12

18 18

27 27

18 18

24 24

12 12

177 179

Commodity Legend

AJ = Apple Juice FS = Fish, Salmon PU = Plums

BN = Bananas GB = Green Beans RS = Raspberries

BR = Broccoli GJ = Grape Juice RZ = Raspberries, Frozen

BU = Butter IA = Baby Food - Applesauce SS = Summer Squash

CE = Celery IE = Baby Food - Peas WS = Winter Squash

CF = Caulifl ower MU = Mushrooms YF = Soy-based Infant Formula

CR = Carrots NE = Nectarines

DF = Dairy-based Infant Formula PC = Peaches

Table 2. Distribution of Samples Collected and Analyzed by Each Participating State. This table includes 

those commodities collected at terminal markets, distribution centers, and retail markets. This table does not 

show the 14 groundwater samples that were collected at residential or school/daycare wells or the 100 fi nished/

untreated drinking water samples that were collected at water treatment facilities. 

Dairy

BU

156

23

84

48

66

108

48

66

99

48

10

756

Fish

FS

78

12

42

24

36

54

35

47

24

352
Pesticide Data Program—Annual Summary, Calendar Year 2013

8

Commodity Acceptable Products

Apple Juice 100% apple juice. Single strength (juice may have been reconstituted from concentrate). Readyto-serve in cartons, jars, cans, or plastic containers. Individual single-service box containers 

are acceptable as long as they are all from the same lot number. All apple juice must be 100% 

pasturized.

Baby Food - ApplesaucePureed Stage 1 (First Food) or Stage 2 (Second Food) apples/applesauce baby food. Container 

may be glass or plastic. May contain docosahexaenoic acid (DHA), arachidonic acid (ARA), 

choline, vitamin E or gelatin.

Baby Food - Peas Pureed Stage 1 (First Food) or Stage 2 (Second Food) peas baby food. Container may be glass 

or plastic. May contain DHA, ARA, choline, vitamin E or gelatin.

Bananas Whole, fresh bananas.

Broccoli Fresh Broccoli. Broccoli crowns (bunch with top fl orets plus a little of the stem) are preferred. 

Broccoli with stems (bunch with top fl orets plus a lot of the stem) is acceptable if broccoli crowns 

are not available.

Butter Salted or unsalted sweet butter in cubes or sticks.

Carrots Fresh, whole carrots, with or without tops.

Caulifl ower Any fresh, whole caulifl ower.

Celery Fresh, whole celery.

Grape Juice 100% Grape Juice. Concord, red or white grape juice. Added nutritional ingredients such as 

citric acid and ascorbic acid. Ready-to-serve or frozen concentrate are rotated according to 

a fi xed schedule. Ready-to-serve: single strength (grape juice may have been reconstitutued 

from concentrate). Shelf-stable or refrigerated. Individual single-serving boxes with the same lot 

number. Frozen concentrate includes cans of concentrated grape juice that are frozen. Nonconcentrated grape juice may not be substituted for frozen grape juice concentrate.

Green Beans Fresh green string beans. Whole or pre-cut.

Infant Formula, DairyBasedAny dairy-based infant formula. Powdered, concentrated liquid, or ready-to-eat. Samples may 

contain ARA, DHA, Choline, vitamins, minerals (e.g., iron, zinc, etc.), probiotics, and prebiotics. 

Formula with pre-digested proteins (i.e., hydrolyzed proteins).

Infant Formula, SoyBasedAny soy-based infant formula. Powdered, concentrated liquid, or ready-to-eat. Samples may 

contain ARA, DHA, Choline, vitamins, minerals (e.g., iron, zinc, etc.), probiotics, and prebiotics. 

Formula with pre-digested proteins (i.e., hydrolyzed proteins).

Mushrooms Any fresh whole, white (Agaricus/button) or brown (crimini or portabella) mushroom.

Nectarines Any fresh, whole nectarines.

Peaches Fresh, whole peaches. Red or white. Clingstone, freestone or semi-freestone. Attempt to select 

peaches that are not overly ripe or soft to the touch.

Plums Fresh, whole plums. Any color except green is acceptable. Hybrids of plums with apricots, such 

as plumcots, pluots or dinosaur eggs (this includes interspecifi c plums with a PLU of 3278).

Raspberries Any fresh, whole raspberry. Red, black, purple or golden (yellow). Fresh are preferred but frozen 

are acceptable.

Raspberries, Frozen Frozen raspberries. Red, black, purple or golden (yellow). Individually quick frozen (IQF) or 

frozen are acceptable.

Salmon Fresh or frozen raw (uncooked) salmon. Filets, nuggets, strips or steaks; bones-in or no bones; 

Atlantic or Pacifi c; farm-raised or wild caught.

Summer Squash Fresh whole zucchini, yellow squash or crookneck squash.

Winter Squash Whole winter squash varieties include but are not limited to: Acorn, banana, Boston marrow, 

buttercup, butternut, Hubbard and spaghetti.

Table 3. Acceptable Products for Collected Commodities. This table lists the acceptable products for each 

collected commodity as seen on Commodity Fact Sheets provided to sample collectors. For all commodities, 

domestic or imported and organically grown or conventionally grown products are acceptable.
Pesticide Data Program—Annual Summary, Calendar Year 2013

9

Caulifl ower (532 Samples)

A. Fresh Fruit and Vegetable Samples

Plums (507 Samples) Raspberries (652 Samples)

Mushrooms (532 Samples) Nectarines (543 Samples) Peaches (285 Samples)

Celery (708 Samples) Green Beans (378 Samples)

Broccoli (708 Samples) Carrots (712 Samples)

Summer Squash (709 Samples)

Domestic 89.1%

Domestic 96.8% Domestic 92.1% Domestic 82.0%

Domestic 80.9%

Import 41.8% Import 10.7%

Import 2.8% Import 6.9%

Import 14.3%

Import 18.4%

Unknown 0.7%

Unknown 3.7%

Unknown 1.0%

Domestic 55.6%

Domestic 67.3%

Domestic 46.3%

Domestic 94.0%

Domestic 57.6%

Import 42.7%

Import 32.5% Import 53.5%

Import 5.6%

Unknown 0.6% Unknown 0.4%

Unknown 0.2%

Import 11.6%

Bananas (708 Samples)

Import 100% Domestic 88.0%

Unknown 1.7%

Unknown 0.4%

Unknown 0.2%

Unknown 0.2%

Unknown 0.4%
Pesticide Data Program—Annual Summary, Calendar Year 2013

10

vegetables, including fresh and processed products. 

The fresh commodities collected for PDP were 

bananas, broccoli, carrots, caulifl ower, celery, green 

beans, mushrooms, nectarines, peaches, plums, 

raspberries, summer squash, and winter squash. 

The processed commodities included ready-toserve apple juice, baby food (applesauce and peas), 

grape juice (ready-to-serve and concentrate), and 

frozen raspberries. All fresh fruit and vegetable 

samples weighed either 3 or 5 pounds with the 

exception of raspberry samples that weighed 1 

dry U.S. pint (~0.6 pound). Three pounds were 

collected for smaller, low-weight commodities 

such as green beans and mushrooms and 5 pounds 

were collected for larger, high-weight commodities 

such as bananas and winter squash. For processed 

samples, apple juice and grape juice samples were 

1 quart or 32 ounces.

♦ Butter

In 2013, PDP collected and analyzed 756 butter 

samples. Samples were collected from routine PDP 

sampling sites, which included major distribution 

centers and terminal markets, as well as proxy sites. 

The sample size for butter was 1 pound. Analysis 

was performed by the New York laboratory. Results 

for butter are shown in Appendix D.

B. Processed Fruit and Vegetable Commodities

Figure 3. Commodity Origin. This fi gure depicts the proportion of commodity origin (domestic, import, 

unknown and mixed national origin) for each fresh and processed fruit and vegetable product tested in 2013.

Baby Food

Applesauce (379 Samples)

Domestic 95.5% Import 4.0%

Grape Juice (176 Samples)

Domestic 39.8%

Apple Juice (379 Samples)

Domestic 13.2%

Baby Food

Peas (378 Samples)

Domestic 99.5%

Unknown 0.3%

Import 85.0%

Winter Squash (187 Samples)

Domestic 15.0%

Unknown 0.5% Unknown 0.5%

Import 86.8%

Raspberries, Frozen (53 Samples)

Mixed National 39.3%

Import 20.6%

Domestic 91.5%

Mixed National 7.9%

Unknown 0.6%
Pesticide Data Program—Annual Summary, Calendar Year 2013

11

♦ Infant Formula 

In 2013, PDP tested two types of infant formula 

(dairy-based and soy-based). Acceptable samples 

included concentrated liquid, powdered, and 

ready-to-eat; domestic or imported; organic or 

conventional products. The minimum weight was 

enough to reconstitute to 32 ounces. PDP collected 

and tested 177 dairy-based samples and 179 soybased samples. For the 179 soy-based infant 

formula samples, 31 were concentrated liquid, 87 

were powdered, and 61 were ready-to-eat. For the 

177 dairy-based infant formula samples, 38 were 

concentrated liquid, 77 were powdered, and 62 

were ready-to-eat. Samples were collected from 

routine PDP sampling sites, which included major 

distribution centers and terminal markets as well as 

proxy sites. Dairy-based samples were tested at the 

New York laboratory and soy-based samples at the 

California laboratory.

♦ Salmon 

In 2013, EPA requested collection of salmon data 

to examine levels of pesticides present in salmon, 

whether from environmental contaminants or 

from pesticides used in aquaculture. Current, 

comprehensive data on pesticide residues on fi sh 

available to the U.S. consumer are largely unavailable. 

Sampling was designed to capture domestic and 

Figure 4. Origin of Selected Fresh Commodities: Raspberry and Summer Squash Samples. Differences in 

origin (domestic vs. import) are illustrated by month. 

Origin of Raspberry Samples

Origin of Summer Squash Samples

Domestic Imported Unknown

JAN

FEB

MAR

APR

MAY

JUN

JUL

AUG

SEPOCT

NOV

DEC

60

10

20

30

40

50

JAN

FEB

MAR

APR

MAY

JUN

JUL

AUG

SEPOCTNOV

DEC

60

10

20

30

40

50
Pesticide Data Program—Annual Summary, Calendar Year 2013

12

imported products, including farm-raised and wildcaught salmon. PDP sampled salmon available at 

designated sampling locations regardless of country 

of origin, in order to capture results for salmon 

consumed by the American public. 

PDP collected and analyzed 352 salmon samples in 

2013. Each sample consisted of 2 pounds of fresh 

or frozen raw salmon. Proxy/retail sites provided 

73.6 percent of salmon samples. Whole salmon 

samples were not collected; rather, only fi llets, 

nuggets, strips, or steaks were obtained for testing. 

Both bones-in and no bones were acceptable sample 

types. To ensure salmon samples arrived at the 

laboratory in acceptable condition, samples were 

fi rst frozen overnight and then shipped the following 

day by overnight air with ample frozen cold packs 

and insulating materials surrounding all sample 

units. Analysis was performed by the Washington 

laboratory. 

Farm-raised or wild-caught, and domestic or 

imported salmon were collected on a random, as 

available basis. The majority of samples were wildcaught and imported. Approximately 32 percent of 

the samples were farm-raised and 57 percent were 

wild-caught. The remainder of the samples had 

no available source information. Approximately 

27 percent of the samples originated in the United 

States, 73 percent were imported, and less than 

1 percent was of unknown origin. Distribution of 

residues in salmon may be found in Appendix E.

♦ Drinking Water

Potable Groundwater

Approximately 15 percent of the U.S. population 

obtains its domestic water from private wells. 

Many of these wells are located in agricultural areas 

and may be susceptible to pesticide contamination, 

making it necessary to monitor these shallow 

groundwater wells to determine potential exposure 

to pesticides through water consumption for this 

segment of the population.

Some pesticides bind tightly to soils and therefore 

are unlikely to be found in groundwater; others, such 

as water-soluble pesticides, can move through soil 

to reach the water table. Movement of pesticides 

in soils and rock is much slower than in surface 

water. For example, pesticide movement in soils 

and rock is measured in centimeters per year while 

movement in surface water is measured in meters 

per year. Because of these differences in mobility, 

pesticide concentrations in groundwater are much 

less variable, and samples do not need to be taken 

as frequently. Consequently, for these groundwater 

studies, a single annual sample was taken rather than 

the bimonthly samples taken for surface water.

A total of 14 samples from 14 sites were collected 

and tested for the 2013 groundwater program. 

These included 11 private residence wells in 4 

States (California, Minnesota, Washington, and 

Wisconsin). Three school/childcare facility wells 

were sampled in 2013 in two States (New York and 

California). Groundwater sampling and testing was 

discontinued in April 2013. 

For private residences, samples were collected at the 

kitchen faucet after a signifi cant volume of water 

had been used (i.e., after morning showers) to ensure 

that water from the pressure tank or any storage 

tanks was depleted and that the water sampled was 

from the well and not stagnant. It is assumed that 

most households do not spray household pesticides 

around the kitchen faucet; therefore, the chance of 

contamination is minimal.

Schools and childcare facilities are often located 

on or outside of town perimeters due to lower land 

costs. Bringing utilities to these remote locations can 

be expensive; therefore, onsite wells are often used 

for water supplies. As children are most susceptible 

to pesticides during their growth and developmental 

years and spend a signifi cant portion of their lives at 

these locations, it is critical to have adequate data to 

evaluate children’s potential exposure to pesticides 

through the consumption of water. The expense of 

testing for a large suite of pesticide residues at partper-trillion levels is cost-prohibitive to most schools 

and homeowners, as well as to county and State 

governments. PDP collaborated with these groups 

on sample collection and provided them with their 

individual sample results.

When pesticides are detected in groundwater, the 

source is not always the immediate surface above, 

but can be where the water is entering, or recharging, 
Pesticide Data Program—Annual Summary, Calendar Year 2013

13

the aquifer, often miles away. Thus, if pesticides 

are being used in the recharge zone, they may be 

transported through the aquifer to the well. The 

transport times from recharge points (where surface 

water and precipitation enter the ground in route to 

the aquifer) to the wells can take a signifi cant amount 

of time, from many days to years. During this time, 

microbial and chemical degradation of the pesticide 

can occur. From the observation of the data in this 

report, it is often the pesticide metabolites that are 

detected and not the parent pesticide compound. 

Municipal Drinking Water

In 2001, PDP began testing municipal waters 

drawing from surface water sources because 

surface water is more vulnerable to pesticides than 

municipal waters that draw from groundwater 

sources. Most municipal systems that draw water 

from groundwater obtain water from fairly deep (i.e., 

>200 feet) aquifers that are not generally susceptible 

to pesticide contamination. 

The sample collection sites are community water 

systems that draw water from surface water sources. 

Site selection was made in collaboration with EPA’s 

Offi ce of Pesticide Programs. All selected sites met 

the following criteria: (1) use of surface water as the 

primary source of water and (2) location in regions of 

heavy agriculture where known amounts of targeted 

pesticides of interest were applied. Water treatment 

method was not a part of the selection criteria.

Samples were collected bimonthly by trained water 

treatment facility personnel. Paired samples of the 

raw intake water (untreated) and disinfected and 

fi nished drinking water (treated) were collected for 

analysis. Treated water samples were collected after 

the untreated samples at a time interval consistent 

with the hydraulic residence. Hydraulic residence is 

the average time from entry into the treatment facility 

until distribution as treated water. Dechlorination and 

preservative chemicals were added to the samples at 

the time of collection. Samples were packed with 

frozen cold packs and shipped overnight to the 

testing laboratories. 

During 2013, 100 total treated and untreated drinking 

water samples were collected from 8 community 

water systems in 6 States – Kentucky (1 site); 

Louisiana (1 site); Missouri (1 site); New Jersey (1 

site); North Carolina (2 sites); and North Dakota (2 

sites). The Louisiana site was sampled only once 

for surveillance purposes, checking for carbamate 

and organophosphate detections. Drinking water 

sampling and testing was discontinued in April 2013.

Each watershed refl ects the local topography, 

watershed size, geomorphology, soil types, 

geology, land use, land management practices, 

crop production, pesticides applied, and application 

methods. Due to the complexities associated with 

water quality assessments, these data refl ect only the 

unique characteristics of the watersheds from which 

the samples were obtained.

III. Laboratory Operations 

♦ Overview

Nine State laboratories performed analyses 

for PDP. These laboratories are equipped with 

instrumentation capable of detecting residues at 

very low levels. Laboratory staff members receive 

intensive training and must demonstrate analytical 

profi ciency on an ongoing basis. Program scientists 

continually test new technologies and develop new 

techniques to improve the levels of detection. Major 

changes in methodology and/or instrumentation are 

evaluated and their soundness demonstrated and 

documented by means of method validation modules 

in accordance with PDP SOPs.

♦ Fresh and Processed Commodities

Fruit and vegetable samples were tested for 386 

parent pesticides, metabolites, degradates, and/or 

isomers, plus 21 environmental contaminants using 

Multiresidue Methods (MRMs). Upon arrival at the 

testing facility, samples of fresh commodities were 

visually examined for acceptability and discarded 

if determined to be inedible (decayed, extensively 

bruised, or spoiled). Except for bananas, fresh 

produce samples were washed under gently running 

cold water, emulating the practices of the average 

consumer to more closely represent actual exposure 

to residues. Samples were not cooked, bleached, or 

washed with detergents. Additionally, any inedible 

or damaged portions were removed prior to further 

preparation. For example: bananas were peeled; 
Pesticide Data Program—Annual Summary, Calendar Year 2013

14

stem caps were removed from carrots; peaches 

were pitted, etc. Processed commodities were not 

washed or cooked prior to homogenization and 

were homogenized with all liquid that was present 

in the sample package. Grape juice concentrates 

were reconstituted according to package directions 

while ready-to-serve apple juice and grape juice 

were simply mixed prior to removal of a portion for 

analysis. Ready-to-eat infant formula samples were 

mixed prior to removal of a portion for analysis. 

Concentrated liquid infant formula samples were 

diluted in a dry, clean container with reagent 

water, according to label directions, and mixed 

well to ensure a homogeneous mixture. Powdered 

infant formula samples were reconstituted in a 

dry, clean container with reagent water, according 

to label directions, and mixed well to ensure a 

homogeneous mixture. Detailed information on 

sample preparation for each commodity is available 

in the Laboratory Operations (PDP-LABOP) SOP 

on the PDP website at www.ams.usda.gov/pdp. 

Laboratories are permitted to refrigerate incoming 

fresh fruit and vegetable samples of the same 

commodity up to 72 hours to allow for different 

sample arrival times from collection sites. Frozen 

and canned commodities may be held in storage 

(freezer or shelf) until the entire sample set is ready 

for analysis.

Samples are homogenized using choppers and/

or blenders and separated into analytical portions 

(aliquots) for analysis. If testing cannot be 

performed immediately, the entire analytical set 

is frozen at -40°C or lower, according to PDP’s 

Quality Assurance/Quality Control (QA/QC) 

requirements. Surplus aliquots not used for the 

initial testing are retained frozen in the event that 

replication of analysis or verifi cation testing is 

required.

For analysis of fruit and vegetables, testing 

laboratories used various Quick, Easy, Cheap, 

Rugged and Safe (QuEChERS2

)-based approaches. 

All MRMs are determined, prior to use and 

through appropriate method validation procedures, 

to produce equivalent data for PDP analytical 

purposes.

PDP laboratories primarily use gas chromatography (GC) and liquid chromatography (LC) 

instrumentation, coupled with tandem mass 

spectrometry (MS) detection systems for the 

simultaneous identifi cation/confi rmation and 

quantitation of pesticides. The use of these GC-MS/

MS and LC-MS/MS systems allows the program 

to capture data for a broad spectrum of pesticides, 

including emerging product chemistries.

♦ Baby Food

In 2013, PDP laboratories analyzed baby food 

applesauce (379 samples) and baby food peas 

(378 samples) for a total of 207 parent pesticides, 

metabolites, degradates, and/or isomers, plus 

13 environmental contaminants. The baby food 

applesauce samples were analyzed by the Florida 

laboratory, while baby food peas were analyzed by 

the Texas laboratory. Multiple containers of a given 

sample (of the same lot number) were combined, 

homogenized, and extracted using modifi cations of 

the QuEChERS method. Analyses were performed 

utilizing GC-mass selective detector, GC-MS/MS, 

and LC-MS/MS. 

♦ Infant Formula

The California laboratory tested 179 soy-based 

infant formula samples and the New York laboratory 

tested 177 dairy-based infant formula samples 

for a total of 312 parent pesticides, metabolites, 

degradates, and/or isomers, plus 18 environmental 

contaminants. Analyses were performed using GCMS/MS and LC-MS/MS.

♦ Butter

The New York laboratory tested 756 butter samples 

for 170 parent pesticides, metabolites, degradates, 

and/or isomers, plus 14 environmental contaminants. 

Upon arrival at the testing facility, samples were 

visually examined for acceptability and discarded if 

warm to the touch, rancid, or leaking. Samples were 

extracted using a modifi cation of the QuEChERS 

method and analyzed using GC-MS/MS and LCMS/MS.

2

 M. Anastassiades, S.J. Lehotay, D. Stajnbaher and F.J. Schenck, “Quick, Easy, Cheap, Effective, Rugged and Safe 

(QuEChERS) Method”, J AOAC Int 86 (2003) 412.
Pesticide Data Program—Annual Summary, Calendar Year 2013

15

♦ Salmon

The Washington State laboratory analyzed 352 

samples of salmon for 189 parent pesticides, 

metabolites, degradates, and/or isomers, plus 15 

environmental contaminants. Upon arrival at 

the testing laboratory, the samples were visually 

examined for acceptability prior to extraction 

using a modifi cation of the QuEChERS method 

followed by analysis via GC-MS/MS and LC-MS/

MS.

♦ Potable Groundwater from Domestic and 

School/Childcare Facility Wells

In 2013, PDP conducted two groundwater testing 

studies: one for private domestic wells and one for 

school/childcare facilities. Onsite wells providing 

drinking water to school/childcare facilities are 

regulated by EPA’s Offi ce of Water under the Safe 

Drinking Water Act (SDWA) as non-transient, 

non-community water systems. SDWA requires 

testing for the 23 compounds that have established 

Maximum Contaminant Levels (MCLs). These 

compounds include only parent compounds – 

no metabolites are required to be tested. In both 

surface and groundwater, metabolites are detected 

more often than parent compounds. Furthermore, 

metabolites are often more water soluble and stable 

than parent compounds and are usually detected at 

higher concentrations than the parent compounds. 

EPA does not have established MCL levels or 

testing requirements for these metabolites. 

The Minnesota and Montana laboratories analyzed 

groundwater samples for 201 parent pesticides, 

metabolites, degradates, and/or isomers, plus 8 

environmental contaminants. These compounds 

were determined to be of interest to EPA based on 

data needs for risk assessment as required under 

FQPA. Each sample consisted of three 1-liter 

amber glass bottles. Upon arrival at the testing 

laboratory, samples were visually examined 

for acceptability (no leakage). Samples were 

refrigerated until time of analysis, which began 

within 5 working days of collection. One liter of 

the sample was extracted for compounds amenable 

to GC-MS analysis, and one liter was extracted for 

compounds amenable to LC-MS/MS. A third bottle 

was held in reserve in case of breakage or laboratory 

accident. 

♦ Municipal Drinking Water

The Minnesota and Montana laboratories analyzed 

drinking water for 201 parent pesticides, metabolites, 

degradates, and/or isomers, plus 8 environmental 

contaminants. These compounds were determined 

to be of interest to EPA based on data needs for risk 

assessment as required under FQPA. Samples were 

collected at water treatment facilities. Each sample 

consisted of two 1-liter amber glass bottles of treated 

water and two 1-liter amber glass bottles of raw 

untreated water. Upon arrival at the testing laboratory, 

samples were visually examined for acceptability 

and discarded if warm to the touch or leaking. 

Samples were refrigerated until time of analysis and 

extracted within 96 hours of collection. A 1-liter 

bottle was extracted for compounds amenable to GCMS analysis and the other for compounds amenable 

to LC-MS/MS analysis. The extraction methods 

used were initially based on Solid Phase Extraction 

methods developed by the U.S. Geological Survey. 

These methods were modifi ed to capture specifi c 

analytes of interest and were independently validated 

by each testing laboratory.

♦ Quality Assurance Program

The primary objectives of the QA/QC program 

are to ensure the reliability of PDP data and the 

performance equivalency of the participating 

laboratories. Direction for the PDP QA program 

is provided through SOPs initially based on EPA 

Good Laboratory Practices, along with programspecifi c QA/QC requirements. The PDP SOPs 

provide uniform administrative and sampling 

procedures, as well as laboratory operations and data 

analyses guidelines. The program SOPs are revised 

annually to accommodate changes in the program 

and are aligned with International Organization for 

Standardization (ISO)3

 requirements. PDP State 

laboratories are accredited to ISO 17025 by the 

American Association for Laboratory Accreditation 

(A2LA), an internationally recognized accrediting 

body.

 3 “ISO” is not an acronym because the initials would be different in various offi cial languages. “ISO” is adopted from the 

Greek word “isos” meaning equal.
Pesticide Data Program—Annual Summary, Calendar Year 2013

16

Laboratory Technical Advisory Group and Quality 

Assurance Offi cers: A Technical Advisory Group, 

comprised of laboratory Technical Program 

Managers and Quality Assurance Offi cers, is 

responsible for annually reviewing program SOPs 

and addressing QA issues. For day-to-day QA 

oversight, PDP relies on the Quality Assurance Unit 

(QAU) at each participating facility. The QAU 

operates independently from the laboratory staff 

and is responsible for reviewing all data generated 

for PDP and for performing quarterly, internal 

program audits. Preliminary data review procedures 

are performed onsite by each laboratory’s QAU. 

Final review procedures are performed by MPD 

staff assigned to each laboratory that is responsible 

for collating and reviewing data for conformance 

with SOPs.

Method Performance Requirements: Laboratories 

are required to determine and verify the limits of 

detection (LODs) and limits of quantitation (LOQs) 

for each pesticide/commodity pair. LODs depend 

on matrix, analyte, and methods used (extraction 

and instrumental). LODs for each pesticide/

commodity pair are shown in the applicable crop 

results appendix. Additional method performance/

validation requirements include modules for 

consistent instrument response (linearity), method 

range, and precision and accuracy.

Identifi cation/Confi rmation: Identifi cation and 

confi rmation is performed primarily by MS 

technologies. Residue amounts greater than 

or equal to LOD and below LOQ are reported 

as below quantifi able level (BQL). BQLs are 

assigned values at one-half the LOQ, and are used 

along with values greater than or equal to LOQ 

and non-detects in dietary risk assessments, when 

appropriate.

Routine Quality Control Procedures: PDP 

procedures for QC are intended to assess 

method and analyst performance during sample 

preparation, extraction, and cleanup. To maximize 

sample output and decrease the QC/sample ratio, 

samples are analyzed in analytical sets that include 

the test samples and the following components:

• Reagent Blank - For analysis of fruit and 

vegetables, baby food, infant formula, butter, and 

salmon, an amount of distilled water, equivalent to 

the natural moisture content of the commodity, is 

run through the entire analytical process to confi rm 

glassware cleanliness and system integrity.

• Matrix Blank - A previously analyzed sample 

of the same commodity, which contains either 

very low concentrations of known residues or no 

detectable residues, is divided into two portions. 

The fi rst portion is used to determine background 

information on naturally occurring chemicals and 

the second to prepare a matrix spike.

• Matrix Spike(s) - Prior to extraction, a portion of 

matrix blank is spiked with marker pesticides to 

determine the precision and accuracy of the analyst 

and instrument performance. Marker pesticides 

are compounds selected from different pesticide 

classes (e.g., organochlorines, organophosphates, 

carbamates, conazoles, imidazolinones, macrocyclic lactones, neonicotinyls, phenoxy acid 

herbicides, pyrethroids, strobilurins, sulfonyl urea 

herbicides, triazines, uracils), with physical and 

chemical characteristics representative of their 

corresponding pesticide class. Marker pesticides 

may be used to monitor recovery instead of spiking 

all pesticides. This use of marker pesticides 

optimizes the resources required to analyze the 

thousands of analyte/matrix combinations in the 

program while still allowing evaluation of daily 

recovery patterns. In addition, each laboratory 

must perform matrix spikes at least quarterly 

for each analyte/crop combination it reports. 

Some laboratories choose to rotate spikes of 

all compounds on a set-to-set basis or spike all 

compounds analyzed with each set, so that the 

amount of spike recovery data obtained actually 

exceeds the minimal requirements previously 

stated. During 2013, PDP laboratories quantitated 

a total of 72,355 matrix spikes, with an overall 

mean recovery of 96 percent and an overall 25 

percent coeffi cient of variation (% C.V.). The % 

C.V. is calculated as the standard deviation divided 

by the mean.

• Process Control Spike - A compound with physical 

and chemical characteristics similar to those of 

the pesticides being tested is used to evaluate the 

analytical process on a sample-by-sample basis. 

Each of the analytical set components, except 
Pesticide Data Program—Annual Summary, Calendar Year 2013

17

the reagent and matrix blanks, is spiked with 

process controls. During 2013, PDP laboratories 

quantitated a total of 23,388 process controls on 

10,104 samples, with an overall mean recovery of 

100 percent and an overall 18 % C.V. Of these 

process controls, 70 (0.3 percent) were reruns due 

to initial failure to meet PDP recovery criteria. The 

rerun values are not included in these statistics.

Profi ciency Testing: All facilities are required 

to participate in PDP’s Profi ciency Testing 

(PT) program. In order to properly benchmark 

performance, PDP laboratories participate in 

an international PT program, the Food Analysis 

Performance Assessment Scheme (FAPAS) 

PT program, administered by the Food and 

Environment Research Agency, Sand Hutton, 

York, United Kingdom. In 2013, PDP laboratories 

that routinely analyze fruit and vegetables via 

MRMs participated in one FAPAS round for 

grapes that contained seven fortifi ed analytes. 

Laboratories were evaluated based on z-scores 

for reported compounds, as well as any reported 

false negatives or false positives. PDP laboratories 

typically obtained z-scores less than two, which is 

deemed satisfactory performance.

In addition, PDP laboratories participate in an 

internal PT program that is tailored to current 

PDP commodities and testing profi les. For this 

internal program, the California Department of 

Food and Agriculture QAU prepares and issues 

rounds designed by MPD. Spiking compounds 

are selected with specifi city and levels for each 

commodity. Fortifi cation levels of selected 

analytes are generally 1 to 10 times the program 

LOQ for that commodity/compound pair. For 

each multiresidue round, one compound per set is 

typically repeated within the round to provide an 

indicator of repeatability. The resulting data are 

used to determine performance equivalency among 

the testing laboratories and to evaluate individual 

laboratory performance. 

During 2013, PDP laboratories received three 

multiresidue fruit and vegetable PT rounds (carrots, 

celery, and tomatoes), each consisting of three 

test samples. The carrot samples were fortifi ed 

with 12 different compounds with imidacloprid 

spiked on 2 different samples at the same level to 

evaluate within and between laboratory variability. 

The celery samples were fortifi ed with 12 different 

pesticides with fl udioxonil spiked on 2 different 

samples. The tomato samples were fortifi ed with 10 

different pesticides with trifl oxystrobin spiked on 2 

different samples.

Onsite Reviews: In addition to the onsite assessments 

performed by A2LA that are required to maintain 

ISO 17025 accreditation, MPD staff chemists 

perform onsite reviews of laboratory operations 

to determine compliance specifi cally with PDP 

SOPs. Improvements in sampling, chain-ofcustody, laboratory, recordkeeping, and electronic 

data transmission procedures are made as a result of 

onsite reviews.

IV. Database Management

 

PDP maintains an electronic database at the MPD 

in Washington, D.C., that serves as a central data 

repository. The data captured and stored in the PDP 

database include sample collection and product 

information, residue fi ndings, and process control 

recoveries for each sample analyzed, in addition 

to QA/QC fortifi ed recoveries for each set of 

samples. Each calendar-year survey is stored in a 

separate database structure, which allows easier 

administration and data reporting. The PDP data 

path is illustrated in Figure 5.

♦ Electronic Data Path

 

PDP utilizes the Remote Data Entry (RDE) system, 

which is a customized software application that 

allows participating State and Federal laboratories 

to enter and transmit data electronically. The RDE 

system is centralized with all user interface software 

and database fi les residing in Washington, D.C. 

The laboratory users need only a Web browser to 

interface with the RDE system. Access is controlled 

through separate user login/password accounts and 

user access rights for the various system functions 

based on position requirements. The RDE system 

utilizes Secure Sockets Layer technology to encrypt 

all data passed between users’ computers and the 

central Web server. 

A separate Windows®-based system allows sample 

collectors to capture the standardized Sample 
Pesticide Data Program—Annual Summary, Calendar Year 2013

18

- Collection in 11 States

- Samples taken close to consumer consumption

- Standardized Sample Information Forms

- Data entry on hand-held/laptop computers

- Chemists review data on-screen

- Upload data to central database

- 9 State laboratories

- Fruit and vegetable samples prepared for

 consumption

- Detect residues at low levels

- Pesticide residue data generated

- Multi-tiered quality assurance data review

 process

- Web-based data entry software

- Import data from other systems

- Access controlled by user login

- Extensive data cross-checks

- Data reconciliation

- Standard & adhoc reporting

- Annual Summary

- Custom data sets

YEAR-END REVIEW

INTERNET

SAMPLE COLLECTION DATA REVIEW AT HQ

LABORATORY ANALYSIS

LABORATORY REMOTE DATA 

ENTRY (RDE)

DATA REPORTING

Figure 5. PDP Data Pathway. An illustration of PDP data path from sample collection through laboratory 

analysis and reporting.

view

INTER

RY A

Y RE

-END

PORT

INTERNET
Pesticide Data Program—Annual Summary, Calendar Year 2013

19

Information Form (SIF) electronically on laptop 

or tablet computers. The e-SIF system generates 

formatted text fi les containing sample information 

that are e-mailed to PDP headquarters and then 

imported into the Web-based RDE system.

The RDE data entry screens have extensive editing 

functions and cross-checks built into the software to 

ensure valid values are entered for all critical data 

elements. This task is made easier by the practice 

of capturing and storing standardized codes for all 

critical alphanumeric data elements rather than their 

complete names, meanings, or descriptions. This 

coding scheme allows for faster and more accurate 

data entry, saves disk storage space, and allows 

the user to perform ad-hoc queries (data searches) 

on the database easily. The data entry screens also 

perform automatic edits on numeric fi elds, dates, 

and other character fi elds to ensure entries are 

within prescribed boundaries. 

At PDP headquarters, the RDE system allows staff 

chemists to review the data online and then to mark 

the data as ready-for-upload to the central PDP 

database. A separate upload application converts 

and passes the data to the PDP database, which 

is maintained using Microsoft® Access and SQL 

Server database tools. Access to the central PDP 

database is limited to MPD personnel only and is 

controlled through password protection and user 

access rights.

♦ Data Reporting 

The MPD staff frequently receives requests for data 

from Government agencies and interested outside 

parties. Ad-hoc queries and custom reports are 

generated to fi ll such requests. An electronic library 

of data queries is maintained to generate standardized 

data summaries, including the data tables, charts, 

and appendixes in this annual summary. Subsets of 

the PDP calendar year databases are made available 

for download from the PDP website. The data fi les 

on the website are delimited text fi les that contain 

a portion of the sampling data, all reported residue 

fi ndings, and reference lists that can be used to 

interpret the standardized codes used in the PDP 

data. The data fi les can be imported into defi ned 

database structures and manipulated using common 

database management software packages.

V. Sample Results and Discussion

♦ Overview

In 2013, PDP conducted surveys on a variety 

of foods including fresh and processed fruit 

and vegetables, infant formula, butter, salmon, 

groundwater, and treated and untreated drinking 

water. Of the total 10,104 samples collected and 

analyzed, 8,526 were fresh and processed fruit and 

vegetable commodities, 356 were infant formula 

samples, 756 were butter samples, 352 were salmon 

samples, 14 were groundwater samples, and 100 

were drinking water samples. Over 40 percent of the 

samples tested had no detectable pesticide residue. 

Appendix B tabulates the distribution of residues in 

fruit and vegetables for the complete 2013 data set. 

Information included in this appendix are: number 

of samples analyzed for a particular compound; 

number and percent of samples with detections; 

range of concentrations detected; range of analytical 

limit of detections (LODs); and EPA tolerance 

levels. Appendixes C, D, E, F, and G, provide the 

distribution of residues for infant formula, butter, 

salmon, groundwater, and treated and untreated 

drinking water, respectively. 

PDP laboratories tested foods for low levels of 

environmental contaminants that are no longer used 

in the United States, but due to their persistence in 

the environment, particularly in soil, can be taken 

up by plants. Appendix H tabulates the results for 

environmental contaminants across all commodities. 

Environmental contaminants are consolidated into 

a single appendix because they have no registered 

uses and are not applied to crops in the U.S. These 

compounds are subject to FDA Action Levels (ALs), 

rather than tolerances. Because environmental 

contaminants continue to persist in the environment, 

they are practically unavoidable and may be present 

in food commodities at generally low levels. All 

individual sample data can be downloaded from the 

PDP Website at http://www.ams.usda.gov/pdp or 

obtained by contacting MPD.

For fresh and processed fruit and vegetables, infant 

formula, butter, and salmon, 70.8 percent of all 

samples were produced in the United States, 26.6 

percent were imports, 1.9 percent were of mixed 

origin, and 0.7 percent were of unknown origin. 
Pesticide Data Program—Annual Summary, Calendar Year 2013

20

Appendix I shows the distribution of sample origin 

by State or country. Of all fresh and processed fruit 

and vegetables, infant formula, butter, and salmon 

samples collected and analyzed, approximately 35.8 

percent (3,577 of 9,990) were grown, packed, and/

or distributed in or from California. Groundwater 

and drinking water are excluded from Appendix 

I since the samples targeted rely on differential 

sampling frames and are not collected from routine 

PDP sample collection locations (i.e., terminal 

markets and large chain store distribution centers 

throughout the country). Treated and untreated 

drinking water samples are collected from 

community water treatment facilities. Groundwater 

samples are collected from private domestic wells 

and school/childcare facilities. Appendix J includes 

a comparison of residues for selected commodities 

with a signifi cant import component.

Food monitoring data, together with dietary 

consumption surveys, are used by EPA to estimate 

dietary exposure to pesticides to ensure the safety 

of existing pesticide uses. EPA uses all results 

reported by PDP, including sample results reported 

as below the LOD and those above the tolerance. 

PDP laboratories are required to establish LODs 

and report any instrumental response below the 

LOD as a non-detect. LODs are established 

experimentally for each pesticide/commodity pair 

and are reported with each data set. The number of 

non-detects can be used in conjunction with percent 

crop treated data to determine what proportion of 

these values may be counted as zero towards the 

dietary exposure.

♦ Baby Food

Samples of baby food applesauce and peas were 

tested as processed products – contents of individual 

containers within a sample were combined then 

mixed until homogeneous, and then an analytical 

portion was removed to be tested by the laboratory’s 

MRM. Results for baby food commodities are 

shown in Appendixes B, H, I, K, L, and M. 

♦ Infant Formula

Both dairy-based and soy-based infant formulas 

were tested as processed products. For readyto-eat samples, the sample was evenly mixed in 

order to obtain a homogeneous mixture prior to 

removing an analytical portion. Concentrated liquid 

infant formula samples were diluted in a dry, clean 

container with reagent water, according to label 

directions, and mixed well to ensure a homogeneous 

mixture. Powdered infant formula samples were 

reconstituted in a dry, clean container with reagent 

water, according to label directions, and mixed well 

to ensure a homogeneous mixture. Results for infant 

formula are contained in Appendixes C, H, I, and L.

♦ Import versus Domestic Residue Comparisons 

Information about the origin of each PDP sample 

is recorded when the sample is collected. Figure 

3 illustrates the portion of the domestic and import 

component for each of the PDP fruit and vegetable 

commodities in 2013. The data generated by PDP 

refl ect pesticide residues in foods, both domestic and 

imported products, available to the U.S. consumer. 

Many fresh and processed commodities are almost 

entirely of domestic origin, such as baby food peas 

(99.5 percent); caulifl ower (96.8 percent); baby food 

applesauce (95.5 percent); peaches (94.0 percent); 

and celery (92.1 percent) with only minor import (0 

percent, 2.8 percent, 4.0 percent, 5.6 percent, and 

6.9 percent, respectively) and unknown origins (0.5 

percent, 0.4 percent, 0.5 percent, 0.4 percent, and 1.0 

percent, respectively). Some fresh and processed 

fruit and vegetables are entirely or almost entirely 

imported in origin such as bananas (100 percent); 

frozen raspberries (86.8 percent); and winter squash 

(85.0 percent) with only minor domestic (0 percent, 

13.2 percent, and 15.0 percent, respectively) and 

unknown origins (0 percent for all 3 commodities). 

Other fresh commodities, such as raspberries and 

summer squash, are from domestic growers part of 

the year and imported during the remaining months, 

as illustrated in Figure 4.

Comparisons of selected residues detected in 

imported versus domestic nectarines, raspberries, 

and summer squash can be found in Appendix J. 

These sample sets were selected to compare data 

where residues are present in greater than 10 percent 

of the commodity and allow for the comparison of 

individual residues. These data also show that the 

residue profi les for domestic and imported crops are 

signifi cantly different. 
Pesticide Data Program—Annual Summary, Calendar Year 2013

21

The nectarine data in Appendix J illustrate that in 

2013 iprodione and tebuconazole were detected 

more frequently in imported samples than in 

domestic samples. Iprodione was detected in 96.0 

percent of the samples from Chile and 0.6 percent of 

the U.S. samples, and tebuconazole was detected in 

78.0 percent of the Chilean samples and 7.3 percent 

of the domestic samples. Lambda cyhalothrin, 

spinosad, acetamiprid, pyrimethanil, thiabendazole, 

and fenhexamid also were detected more frequently 

in imported samples than in domestic samples. 

Fludioxonil was detected more frequently in 

domestic samples than in imports. Fludioxonil 

was detected in 81.7 percent of U.S. samples and 

8.3 percent of samples from Chile. Propiconazole, 

boscalid, pyraclostrobin, and indoxacarb also were 

detected more frequently in domestic samples than 

in imports. Methoxyfenozide was detected with 

relatively equal frequency in both the U.S. and 

Chilean nectarines.

The data for raspberries in Appendix J illustrate that 

in 2013 spinetoram was detected more frequently 

in U.S. samples than in samples from Mexico. 

Spinetoram was detected in 18.2 percent of domestic 

samples and 2.8 percent of the samples from Mexico. 

Bifenazate, boscalid, cypermethrin, cyprodinil, 

myclobutanil, pyraclostrobin, and spinosad were 

detected with relatively equal frequency in both the 

U.S. and Mexican raspberries.

The summer squash data in Appendix J illustrate 

that in 2013 endosulfan sulfate and imidacloprid 

were detected more frequently in imported samples 

than in domestic samples. Endosulfan sulfate was 

detected in 25.5 percent of the samples from Mexico 

and 11.9 percent of the United States samples and 

imidacloprid was detected in 25.2 percent of the 

Mexican samples and 8.4 percent of the domestic 

samples. Propamocarb hydrochloride was detected 

more frequently in domestic samples than in 

imports. Propamocarb hydrochloride was detected 

in 17.3 percent of U.S. samples and 2.7 percent of 

the samples from Mexico.

All pesticides detected, except thiabendazole in 

nectarines, were registered in the United States; 

however, the profi les of residue fi ndings were 

markedly different in the U.S. samples versus 

samples from these exporting countries. The 

differences in residue detections between countries 

were likely due to the pesticides used in response 

to pest pressures based on differing environmental, 

climatic, and growing conditions.

♦ Postharvest Applications

Pesticides can be applied before and after harvest 

depending on the crop and approved label use. 

PDP data capture both preharvest and postharvest 

uses because samples are collected at points 

when all pesticide applications have already 

occurred. Pesticides applied postharvest are 

used primarily as fungicides (e.g., azoxystrobin, 

imazalil, o-phenylphenol, and thiabendazole) 

and growth regulators/sprouting inhibitors 

(e.g., chlorpropham). Some detections reported 

in Appendix B most likely refl ect postharvest 

applications to the raw agricultural commodity.

♦ Discussion of Results

There are many pesticides registered for use on 

the same crop; however, not all crops are sprayed 

and not all available pesticides are used at the 

same time or location. Over 40 percent of the 

samples tested had no detectable pesticide residue. 

Pesticide use is primarily dictated by local pest 

pressures and environmental conditions conducive 

to growth of pest populations, as well as the 

planting of susceptible varieties. These differences 

are captured by PDP data which refl ect actual 

residues present in food grown in various regions 

of the U.S. and overseas. Thus, in evaluating 

consumer exposure to pesticides through the diet, 

EPA uses all available information provided by 

registrants, PDP, and others to verify that tolerances 

meet the safety standards set by FQPA. Over 99 

percent of the products sampled through PDP had 

residues below the EPA tolerances. The reporting 

of residues present at levels below the established 

tolerance serves to ensure and verify the safety of 

the Nation’s food supply.

Food commodities with pesticides detected in 

at least 5 percent of samples tested are shown in 

Appendix K. The data shown include the range and 

mean of values detected and U.S. EPA tolerance 

references for each pair. 
Pesticide Data Program—Annual Summary, Calendar Year 2013

22

By virtue of the MRMs employed, PDP provides 

novel data that can be used by EPA to evaluate 

exposure to multiple residues from the same 

commodity. The data are crucial for assessments 

that consider cumulative exposure to pesticides 

determined to have common mechanisms of 

toxicity. The distribution of multiple pesticides 

occurring in samples tested during 2013 is presented 

in Appendix L. These data indicate that 40.5 percent 

of all samples tested, excluding groundwater and 

treated and untreated drinking water, contained 

no detectable pesticides, 23.5 percent contained 

1 pesticide, and 36.0 percent contained more 

than 1 pesticide. Parent compounds and their 

metabolites are combined to report the number of 

“pesticides” rather than the number of “residues.” 

Environmental contaminants, listed in Appendix H, 

have been excluded from this count of pesticides. 

One sample each of nectarines and peaches 

contained residues of 13 pesticides. None of the 

residues found on either the nectarine or peach 

sample exceeded the established tolerance. Multiple 

residue detections can result from the application of 

more than one pesticide on a crop during a growing 

season; in addition, a number of other factors can 

contribute to multiple detections. For example, 

unintentional spray drift in the fi eld, planting of 

crops in fi elds previously treated with the pesticide, 

and/or transfer of residues of postharvest fungicides 

or growth regulators applied to other commodities 

stored in the same storage facilities could all 

contribute to residue detections.

In most cases, samples analyzed by PDP are 

composites of 3 to 5 pounds of commodity from the 

same lot. Therefore, the estimated concentrations 

for multiple residue detections in these composite 

sample results may or may not refl ect the number 

or levels of pesticides in a single serving item of a 

commodity.

♦ Special Projects

Butter: The New York laboratory conducted testing 

for pesticide residues on 756 butter samples. Overall, 

nine different residues (including metabolites 

and isomers), representing eight pesticides, were 

detected in the butter samples (Appendix D and H). 

The most frequently detected residue was novaluron 

which was detected in 269 samples (37.2 percent). 

Trans permethrin was detected in 214 samples 

(28.3 percent), cis permethrin in 206 samples (27.2 

percent), and cyhalothrin in 154 samples (20.4 

percent). Bifenthrin was detected in 112 samples 

(14.8 percent), spinosad in 24 samples (3.2 percent), 

and piperonyl butoxide in 16 samples (2.1 percent). 

Chlorpropham was detected in two samples (0.3 

percent). All residue detections were lower than 

the established tolerances, where tolerances were 

established. The environmental contaminant DDE 

p,p’ was detected in 503 (66.5 percent) of the butter 

samples (Appendix H). All DDE p,p’ detections 

were lower than FDA’s established AL. 

Salmon: The Washington laboratory conducted 

testing for pesticide residues on 352 salmon 

samples. Four residues (including metabolites 

and isomers), representing four pesticides were 

detected in the salmon samples (Appendix E and 

H). Azinphos methyl oxygen analog, carbendazim, 

and cypermethrin were each detected in one sample 

(Appendix E). All residue detections were lower 

than the established tolerances, where tolerances 

were established. The environmental contaminant 

DDT p,p’ was detected in two of the salmon samples 

(Appendix H). Both residue detections were lower 

than FDA’s established AL. 

♦ Potable Groundwater

In 2013, 11 groundwater samples were collected 

from private domestic wells and 3 from school/

childcare facilities. Overall, PDP detected 25 

different residues (including metabolites), 

representing 17 pesticides, in the groundwater 

samples. Most of the detections were for herbicides 

or their metabolites. The samples with detectable 

residues came from seven different sites. Residue 

profi les are shown in Appendixes F and H. 

In April 2012, EPA’s Offi ce of Water issued “Human 

Health Benchmarks for Pesticides (HHBPs)” 

available at www.epa.gov/pesticides/hhbp. These 

benchmarks are for 350 pesticides for which there 

are no MCLs or Health Advisories. While not an 

enforceable limit, these values provide context to 

safe levels of non-regulated pesticides. In 2013, 

none of the groundwater data exceeded any of the 

EPA HHBPs.
Pesticide Data Program—Annual Summary, Calendar Year 2013

23

♦ Municipal Drinking Water

PDP analyzed 100 water samples (50 untreated 

samples and 50 fi nished samples) from community 

water systems. Appendix G and H show the 

concentration of detected residues in treated and 

untreated water. Thirty-six different residues 

(including metabolites), representing 27 pesticides, 

were detected in treated drinking water and 

40 different residues (including metabolites), 

representing 31 pesticides, were detected in the 

untreated intake water. The majority of pesticides 

included in the PDP testing profi les were not 

detected; those compounds that were detected were 

primarily commonly used herbicides and their 

metabolites.

Water treatment technologies vary widely and may 

be based on the local water chemistry, targeted 

contaminants needing removal, and cost. In most 

cases, treated samples had fewer residues and lower 

concentrations than their untreated counterpart. In 

these cases, the effectiveness of water treatment in 

removing/reducing pesticide levels is seen. In a few 

cases, treated samples contained a trace of a residue 

that was not detected in the untreated sample or 

contained a residue at a higher concentration than 

the paired untreated sample. The data acquired to 

date indicate that in these cases the water treatment 

process removed matrix interferences. This provided 

a more effi cient extraction or more sensitive 

measurement in the treated water. Depending on 

the treatment process employed and the chemical 

properties of the pesticide, an individual pesticide 

may be entirely, partially, or not removed during the 

treatment process.

Appendix G also lists the MCLs, HA values, Fresh 

Aquatic Organism (FAO) criteria and EPA’s new 

HHBPs. During 2013, none of the detections in the 

fi nished water samples exceeded established EPA 

MCL or HA levels; however, many of the compounds 

in the PDP testing profi les do not have established 

regulatory standards. The EPA MCLs apply only 

to treated drinking water, not ambient, untreated 

water. Therefore, for comparative purposes, FAO 

criteria and HHBPs, which are much lower than 

human-based MCLs or HA levels, also are given. 

These criteria and benchmarks are lower than MCL 

or HA levels due primarily to higher exposure to 

these compounds because aquatic organisms live 

all or most of their lives in water. During 2013, 

no detections in either treated or untreated water 

exceeded established FAO or HHBP levels. 

Additional information regarding EPA drinking 

water standards is available at: http://water.epa.

gov/drink/standardsriskmanagement.cfm. 

♦ Environmental Contaminants

Environmental contaminants include pesticides 

whose uses have been canceled in the United 

States, but their residues persist in the 

environment, particularly in soil, where they may 

be taken up by plants. These data are also used 

to facilitate international trade. Residue results 

for environmental contaminants may be found in 

Appendix H.

DDT, DDD, and DDE: PDP screened samples for 

various metabolites of DDT including: DDT o,p’; 

DDT p,p’; DDD o,p’; DDD p,p’; DDE o,p’; and 

DDE p,p’. Use of DDT has been prohibited in 

the United States since 1972; however, due to its 

persistence in the environment, low level residues 

of DDT and its DDD and DDE metabolites were 

detected in some commodities tested. DDE p,p’ 

was detected in butter (66.5 percent), carrots (23.5 

percent), celery (17.2 percent), summer squash 

(2.7 percent), winter squash (2.1 percent), green 

beans (0.3 percent), and nectarines (0.2 percent). 

DDT p,p’ was detected in carrots (9 percent), 

summer squash (2.2 percent), celery (1.3 percent), 

and salmon (0.6 percent). DDT o,p’ was detected 

in carrots (6.2 percent) and summer squash (2.5 

percent) and DDE o,p’ was detected in carrots (0.3 

percent). DDD o,p’ was detected in summer squash 

(0.3 percent) and DDD p,p’ was detected in celery 

(0.1 percent) and summer squash (0.1 percent). 

All residues detected were lower than established 

FDA ALs. Drinking water (treated and untreated) 

and groundwater samples were not tested for DDT 

or any of its metabolites.

Other Extraneous Pesticides: PDP screened samples 

for other environmental contaminants including: 

aldrin, which readily metabolizes to dieldrin; BHC 

(alpha/beta/delta); chlordane (total, cis/trans) and 

its metabolite oxychlordane; dieldrin; endrin; 

heptachlor and its epoxide metabolite (total, cis, 
Pesticide Data Program—Annual Summary, Calendar Year 2013

24

trans); and hexachlorobenzene (HCB). HCB was 

used as a seed protectant until 1965 and, due to its 

persistence, remains in soil and grasses. In 1974, 

all aldrin and dieldrin uses were canceled in the 

United States and, in 1978, all heptachlor uses were 

canceled. In 1986, chlordane uses, except termiticide 

uses, were canceled. Despite these cancellations and 

because they persist in the environment, residues 

of BHC beta, chlordane, dieldrin, endrin, and 

heptachlor epoxide were detected in some of the 

tested commodities.

For example, dieldrin was detected in 2.7 percent 

of summer squash samples, 1.3 percent of carrots 

samples, and 1.1 percent of winter squash samples, 

while chlordane (cis) and chlordane (trans) were 

detected in 0.4 percent and 0.3 percent, respectively, 

in summer squash, and 0.5 percent each in winter 

squash. Chlordane (total) was detected in 0.6 percent 

of carrot samples. Endrin was detected in 1.1 percent 

of winter squash samples, and BHC (beta) was 

detected in 0.3 percent of carrot samples. Heptachlor 

epoxide (total) was detected in 0.3 percent and 

0.5 percent of summer squash and winter squash, 

respectively. Heptachlor epoxide (cis) was detected 

in 0.6 percent of carrot samples; no Action Level 

is established for heptachlor or its metabolites in 

carrots. There were no detections of any of these 

extraneous residues in drinking water (treated or 

untreated) or groundwater.

♦ Tolerance Violations

A tolerance is defi ned under Section 408 of the 

Federal Food, Drug, and Cosmetic Act as the 

maximum quantity of a pesticide residue allowable 

on a raw agricultural commodity. Tolerances are 

also applicable to processed foods. The FQPA of 

1996 amended the Federal Insecticide, Fungicide 

and Rodenticide Act to require EPA to periodically 

review each pesticide registration using the most 

currently available data. Timely pesticide data 

provided by PDP enable the EPA to refi ne risk 

estimates used in the pesticide reregistration process. 

A tolerance violation occurs when a residue is found 

that exceeds the tolerance level or when a certain 

residue is found for which there is no established 

tolerance. With the exception of meat, poultry, and 

egg products, for which USDA’s Food Safety and 

Inspection Service is responsible, FDA enforces 

tolerances for all imported foods and domestic 

foods that move through interstate commerce. 

Unlike enforcement programs, PDP emphasizes 

determination of residues at the lowest detectable 

levels rather than quick turn-around times. When 

PDP identifi es samples with residues exceeding 

the tolerance or with residues for which there is no 

established tolerance, these detections are reported 

to FDA’s headquarters offi ce. This notifi cation 

is made in accordance with a Memorandum of 

Understanding between USDA and FDA for 

the purpose of identifying areas where closer 

surveillance may be needed. FDA assesses PDP 

apparent violation data for appropriateness for 

follow-up under its regulatory pesticide program. 

Due to the time period required for completion of 

PDP analyses and data reporting, FDA follow-up 

will usually be at a subsequent harvest or commodity 

availability period. In instances where a PDP fi nding 

is extraordinary and may pose a safety risk, FDA and 

EPA are immediately notifi ed.

Residues exceeding the established tolerance are 

noted with an “X” in Appendix B. Similarly, 

residues for which a tolerance is not established 

are noted with a “V” in Appendixes B, D, and H. 

The “X” and “V” annotations are followed by a 

number indicating the number of samples reported 

to FDA. The EPA tolerances cited in this summary 

and appendixes apply to 2013 and not to the current 

year. There may be instances where tolerances may 

have been recently set or revoked that would have an 

effect on whether a residue is violative.

An established tolerance may apply to more than 

one residue because pesticides may break down into 

more than one metabolite or contain more than one 

isomer. For example, the tolerance for endosulfan 

combines residues of endosulfan I, endosulfan II, and 

endosulfan sulfate; and organophosphate tolerances 

may combine the parent compound and the sulfone 

and sulfoxide metabolites. Therefore, where 

applicable, the pesticide violations in Appendix M 

are combined residues of parent and any isomers 

and/or metabolites to count the total number of 

samples with tolerance violations.

Excluding water, a total of 317 samples with 350 

pesticides were reported to FDA as Presumptive 
Pesticide Data Program—Annual Summary, Calendar Year 2013

25

Tolerance Violations. Pesticides exceeding the 

tolerance were detected in 0.23 percent (23 

samples) of the total samples tested (9,990 

samples). Of these 23 samples, 17 were imported 

(74 percent), and 6 were domestic (26 percent). 

The samples containing pesticides that exceeded 

established tolerances included: 1 sample of 

broccoli, 1 sample of celery, 4 samples of green 

beans, 11 nectarine samples, 1 sample of plums, 

1 sample of fresh raspberries, and 4 samples of 

summer squash.

Residues with no established tolerance were found 

in 3.0 percent (301 samples) of the total samples 

tested (9,990 samples). Of these 301 samples, 151 

were domestic (50.2 percent), 148 were imported 

(49.2 percent), and 2 were of unknown origin 

(0.6 percent). These samples included 286 fresh 

fruit and vegetable samples, 13 processed fruit/

vegetable samples, and 2 butter samples. The 13 

processed fruit/vegetable samples were baby food 

applesauce, grape juice, and frozen raspberries. 

There were 276 samples that contained 1 pesticide 

for which no tolerance was established, 24 

samples with 2 pesticides for which no tolerance 

was established, and 1 sample with 3 pesticides for 

which no tolerance was established. Seven of the 

301 samples also contained 1 pesticide each that 

exceeded an established tolerance. In most cases, 

these pesticides with no established tolerance 

were detected at very low levels. Some pesticide 

residues may have resulted from unintentional 

spray drift in the fi eld, planting of crops in fi elds 

previously treated with the pesticide, or transfer 

of pesticide residues of postharvest fungicides or 

growth regulators applied to other commodities 

stored in the same storage facilities. The pesticide 

levels and commodities are listed in Appendix M.

♦♦♦♦♦♦
Appendix A

Commodity History

Appendix A identifi es commodities sampled by the Pesticide Data Program (PDP) through 

December 2014. Updates to this list are posted on the PDP Web site at www.ams.usda.gov/pdp. 
Fresh Commodities

Commodity Start Date End Date

Apples 1 Sep-91 Dec-96

Apples (S-1) Jan-99 Dec-99

Apples (S-2) Jan-99 May-99

Apples Oct-00 Sep-02

Apples (T-1) Jan-03 Dec-03

Apples Jan-04 Dec-05

Apples Jan-09 Dec-10

Apples (B-1) Aug-12 Oct-12

Apples Oct-14 Ongoing

Asparagus Jan-02 Jun-03

Asparagus Jul-08 Jun-10

Avocados Jul-12 Dec-12

Bananas Sep-91 Sep-95

Bananas Jan-01 Dec-02

Bananas (TSP) Jul-03 Dec-03

Bananas Jan-06 Dec-07

Bananas Apr-12 Mar-14

Blueberries (cultivated) 2 Jan-07 Dec-08

Blueberries (cultivated) 2 Jan-14 Dec-14

Broccoli Oct-92 Dec-94

Broccoli Jan-01 Dec-02

Broccoli Oct-06 Sep-08

Broccoli Jan-13 Dec-14

Cabbage Jan-10 Dec-11

Cantaloupe Jul-98 Jun-00

Cantaloupe Oct-03 Sep-05

Cantaloupe Jan-10 Mar-10

Cantaloupe Oct-10 Jun-12

Carrots 1 Oct-92 Sep-96

Carrots Oct-00 Sep-02

Carrots Jan-06 Dec-07

Carrots Jan-13 Dec-14

Cauliflower Oct-04 Sep-06

Cauliflower Oct-11 Sep-13

Celery Feb-92 Mar-94

Celery Jan-01 Dec-02

Celery Jan-07 Dec-08

Celery Jan-13 Dec-14

Cherries 3 May-00 Aug-01

Cherries 2 May-07 Sep-07

Cherries Apr-14 Ongoing

Cilantro Oct-09 Sep-10

Cranberries Oct-06 Dec-06

Cucumbers Jan-99 Dec-00

Cucumbers Oct-02 Sep-04

Cucumbers Jan-09 Dec-10

Eggplant Jan-05 Dec-06

Grapefruit Aug-91 Dec-93

Grapefruit Jan-05 Dec-06

Grapes 1 May-91 Dec-96

Grapes Jan-00 Dec-01

Grapes (TSP) Jul-03 Dec-03

APPENDIX A. COMMODITY HISTORY

AS OF DECEMBER 2014

Appendix A. Page 1 of 7
Commodity Start Date End Date

Grapes Jan-04 Dec-05

Grapes Jan-09 Dec-10

Green Beans Feb-92 Dec-95

Green Beans Jan-00 Dec-01

Green Beans Apr-04 Mar-05

Green Beans Jan-07 Dec-08

Green Beans Jul-13 Ongoing

Green Onions (scallions) Oct-08 Sep-09

Greens (collard & kale) Oct-06 Sep-08

Hot Peppers Oct-10 Sep-11

Lettuce May-91 Dec-94

Lettuce Oct-99 Sep-01

Lettuce Jan-04 Dec-05

Lettuce Jan-10 Dec-11

Lettuce, Organic Jan-09 Dec-09

Mangoes Apr-10 Sep-10

Mushrooms Oct-01 Sep-03

Mushrooms Oct-11 Sep-13

Nectarines 4 Jul-00 Sep-01

Nectarines Jan-07 Dec-08

Nectarines Jan-13 Ongoing

Onions Jan-02 Dec-03

Onions Oct-11 Sep-12

Oranges 1 Aug-91 Dec-96

Oranges Jan-00 Dec-01

Oranges Jan-04 Dec-05

Oranges Jan-09 Dec-10

Papaya Jul-11 Jun-12

Peaches Feb-92 Sep-96

Peaches (S-3) Jan-00 Sep-00

Peaches 5 Jan-01 Sep-02

Peaches (T-1) May-03 Sep-03

Peaches Oct-06 Sep-08

Peaches (B-1) Aug-12 Oct-12

Peaches Jul-13 Ongoing

Pears Jan-97 Jun-99

Pears (S-1) Jul-98 Jun-99

Pears Oct-03 Sep-05

Pears Jan-09 Dec-10

Pears (B-1) Oct-12 Nov-12

Pineapples Jul-00 Jun-02

Plums 6 Jan-05 Dec-06

Plums Oct-11 Sep-13

Potatoes May-91 Dec-95

Potatoes (S-4) Dec-96 Dec-97

Potatoes Jul-00 Jun-02

Potatoes Jan-08 Dec-09

Raspberries 2 Jan-13 Dec-13

Snap Peas Jan-11 Dec-12

Spinach 1 Jan-95 Sep-97

Spinach Jul-02 Dec-03

Spinach 7 Jan-06 Sep-06

Spinach Jan-08 Dec-09

Strawberries 2 Jan-98 Sep-00

Strawberries Jan-04 Dec-05

Strawberries Jan-08 Dec-09

Appendix A. Page 2 of 7
Commodity Start Date End Date

Strawberries Oct-14 Ongoing

Summer Squash Oct-06 Sep-08

Summer Squash Oct-12 Sep-14

Sweet Corn (on-the-cob) Oct-08 Sep-10

Sweet Corn (on-the-cob) Oct-14 Ongoing

Sweet Bell Peppers Jan-99 Dec-00

Sweet Bell Peppers Oct-02 Sep-04

Sweet Bell Peppers Jan-10 Mar-12

Sweet Potatoes 1 Jan-96 Jun-98

Sweet Potatoes Jan-03 Dec-04

Sweet Potatoes Oct-08 Sep-10

Tangerines Jan-11 Dec-12

Tomatoes 1 Jul-96 Jun-99

Tomatoes Jan-03 Dec-04

Tomatoes Jan-07 Dec-08

Tomatoes Oct-14 Ongoing

Tomatoes, Cherry/Grape Jan-11 Dec-12

Watermelon 8 Oct-05 Sep-06

Watermelon Apr-10 Sep-10

Watermelon Jul-14 Ongoing

Winter Squash 2 Jan-97 Jun-99

Winter Squash Jul-04 Jun-06

Winter Squash Oct-11 Mar-13

1

 Excludes sampling hiatus September - November 1996.

2

 Frozen collected when fresh unavailable.

3

 Sampling adjusted for market availability. Cherries were sampled for 2 years 

 (May-00 - Aug-01) for a total of 6 months.

4

 Sampling adjusted for market availability. Nectarines were sampled for 2 years 

 (Jul-00 - Sep-01) for a total of 6 months.

5

 Sampling adjusted for market availability. Peaches were sampled for 2 years

 (Jan-01 - Sep-02) for a total of 16 months.

6

 Dried plums (prunes) were collected when fresh plums were not available.

7

 Spinach ended earlier than planned due to the unavailability of product.

8

 Samples collected in California, Florida, and Texas only.

(B-1) Special project testing for bifenthrin in multi-residue screen.

(S-1) Special single serving project testing for organophosphates.

(S-2) Special single serving project testing for carbamates.

(S-3) Special single serving project testing for carbamate, organochlorine, 

 organophosphate, organonitrogen, and sulfur compounds.

(S-4) Special single serving project testing for aldicarb.

(T-1) Triazole parent and metabolite compounds only.

(TSP) Triazole Sampling Project. Samples sent to contract laboratory.

Appendix A. Page 3 of 7
Processed Commodities

Commodity Start Date End Date

Apple Juice 1 Jul-96 Dec-98

Apple Juice Jan-02 Dec-02

Apple Juice Jul-07 Jun-08

Apple Juice Jul-12 Jun-13

Applesauce Jul-02 Dec-02

Applesauce Jan-06 Dec-06

Asparagus, Canned Jul-03 Dec-03

Beans, Canned (4 varieties) Oct-08 Sep-10

Beets, Canned Jan-11 Dec-11

Blueberries (cultivated), Frozen 2 Jan-07 Dec-08

Blueberries (cultivated), Frozen 2 Jan-14 Dec-14

Cherries, Frozen 2 Apr-14 Ongoing

Corn Syrup 3 Jan-98 Jun-99

Grape Juice Jan-98 Dec-99

Grape Juice Jan-08 Dec-08

Grape Juice Oct-13 Sep-14

Green Beans, Canned/Frozen 1 Jan-96 Jun-98

Green Beans, Canned Jan-03 Mar-04

Green Beans, Frozen Apr-05 Dec-05

Green Beans, Canned/Frozen Jan-14 Dec-14

Orange Juice Jan-97 Dec-98

Orange Juice Oct-04 Sep-06

Orange Juice Oct-10 Sep-11

Orange Juice Jan-12 Jun-12

Peaches, Canned Dec-96 Dec-97

Peaches, Canned Jan-03 Dec-04

Peaches, Canned (T-1) Jan-03 Mar-03

Peaches, Canned (T-1) Oct-03 Dec-03

Pear Juice, Concentrate/Puree Jul-02 Jun-03

Pears, Canned Jul-99 Jun-00

Peas, Canned/Frozen Apr-94 Jun-96

Peas, Canned/Frozen 4 Oct-01 Sep-03

Peas, Frozen Jan-06 Dec-06

Plums, Dried (Prunes) 5 Jan-05 Dec-06

Potatoes, Frozen Jan-06 Dec-07

Raisins Jul-06 Jun-07

Raspberries, Frozen 2 Jan-13 Dec-13

Spinach, Canned Oct-97 Dec-98

Spinach, Frozen Jan-99 Dec-99

Spinach, Canned Jan-04 Jun-04

Spinach, Canned/Frozen Jul-10 Jun-11

Strawberries, Frozen 2 Jan-98 Sep-00

Sweet Corn, Canned/Frozen Apr-94 Mar-96

Sweet Corn, Canned/Frozen 4 Oct-01 Sep-03

Sweet Corn, Frozen 2 Oct-08 Sep-10

Appendix A. Page 4 of 7
Commodity Start Date End Date

Sweet Corn, Frozen 2 Oct-14 Ongoing

Tomato Paste, Canned Jan-01 Jun-01

Tomato Paste, Canned Jan-09 Dec-09

Tomatoes, Canned Jul-99 Jun-00

Winter Squash, Frozen 2 Jan-97 Jun-99

Baby Food / Formula Products

Commodity Start Date End Date

Baby Food, Applesauce Jul-12 Jun-13

Baby Food, Carrots Jan-12 Dec-12

Baby Food, Green Beans Oct-10 Sep-11

Baby Food, Peaches Jan-12 Dec-12

Baby Food, Pears Oct-10 Sep-11

Baby Food, Peas Jul-12 Jun-13

Baby Food, Sweet Potatoes Oct-10 Sep-11

Infant Formula, Dairy-based Oct-13 Sep-14

Infant Formula, Soy-based Oct-13 Sep-14

1 Excludes sampling hiatus September - November 1996.

2 Frozen collected when fresh unavailable.

3 Excludes sampling hiatus January 1999.

4 Canned samples collected in first year and frozen samples in second year of testing.

5 Dried plums (prunes) were collected when fresh plums were not available.

(T-1) Triazole parent and metabolite compounds only.

(TSP) Triazole Sampling Project. Samples sent to contract laboratory.

Appendix A. Page 5 of 7
Grains

Commodity Start Date End Date

Barley Oct-01 Sep-03

Corn Oct-06 Sep-08

Oats Jul-99 Apr-00

Oats Jan-10 Jun-10

Oats Apr-14 Aug-14

Rice Oct-00 Sep-02

Rice1 Oct-08 Sep-09

Rice Apr-14 Aug-14

Soybeans Sep-96 Feb-98

Soybeans Oct-03 Sep-05

Soybeans Sep-10 Apr-11

Soybeans (S-1) Oct-05 Dec-05

Wheat Feb-95 Jan-98

Wheat Sep-04 Jun-06

Wheat Jul-12 Sep-12

Wheat Flour Jan-03 Dec-04

Wheat Flour (T-1) Jan-03 Dec-03

Nuts and Nut Products

Commodity Start Date End Date

Almonds Jul-07 Mar-08

Peanut Butter Jan-00 Dec-00

Peanut Butter (TSP) Jul-03 Dec-03

Peanut Butter Jan-06 Dec-06

Dairy Products

Commodity Start Date End Date

Butter Jan-03 Dec-03

Butter Jan-12 Dec-13

Heavy Cream Jul-05 Dec-05

Heavy Cream Jan-07 Dec-07

Milk 2 Jan-96 Oct-98

Milk (TSP) Jul-03 Dec-03

Milk Jan-04 Dec-05

Milk Jan-11 Dec-11

Meat / Poultry / Pork Products

Commodity Type Start Date End Date

Poultry Young Chickens Apr-00 Mar-01

Poultry Young & Mature Chickens Jan-06 Dec-06

Beef Cows, Heifers, Steers Jun-01 Jul-02

Beef 3 Cows, Heifers, Steers Dec-08 May-09

Pork Gilt, Barrow Jan-05 Jun-05

Appendix A. Page 6 of 7
Fish Products

Commodity Type Start Date End Date

Fish 4 Catfish Apr-08 Jun-10

Fish Salmon Jul-13 Jun-14

Other Products

Commodity Start Date End Date

Eggs (TSP) Jul-03 Dec-03

Eggs Jul-10 Jun-11

Honey Oct-07 Sep-08

Drinking Water

States Start Date End Date

Finished Water Only (27 sites)

California, Colorado, Kansas, New York, Texas Mar-01 Dec-03

Raw Intake and Finished Water (70 sites) Jan-04 Apr-13

Alabama, Arizona, California, Florida, Georgia, Illinois, Indiana, Iowa, Kansas,

Kentucky, Louisiana, Maryland, Michigan, Minnesota, Missouri, Montana, New Jersey, 

New York, North Carolina, North Dakota, Ohio, Oregon, Pennsylvania, South Carolina, 

Tennessee, Texas, Virginia, Washington State, and Washington, D.C.

Bottled Water 

10 Participating States Jan-05 Dec-06

Groundwater 

1,495 Private Wells in 45 States plus Washington, DC Jan-07 Feb-13

16 Municipal Water Facilities in 13 States Mar-10 Feb-13

1

 Includes sampling hiatus May-July 2009.

2

 Excludes sampling hiatus September - November 1996.

3

 Survey ended 7 months early due to budgetary constraints.

4 Excludes sampling hiatus April-June 2009.

(S-1) Special survey for fungicides used to combat soybean rust.

(T-1) Triazole parent and metabolite compounds only.

(TSP) Triazole Sampling Project. Samples sent to contract laboratory.

Appendix A. Page 7 of 7
Appendix B

Distribution of Residues by Pesticide

in Fruit and Vegetables

Appendix B shows residue detections for all fruit and vegetable pesticide/commodity pairs 

tested, including range of values detected, range of Limits of Detection (LODs), and U.S. 

Environmental Protection Agency (EPA) tolerances for each pair. The EPA tolerances cited 

in this appendix apply to 2013 and not to the current year. There may be instances where 

tolerances have been recently set or revoked that would have an effect on whether a residue 

is violative or not.

In 2013, 8,526 fruit and vegetable samples were analyzed, of which 7,161 were fresh product 

and 1,365 were processed product.

Action Levels (ALs) are shown in this appendix, where applicable, and denote Action 

Level values established by FDA. Under the Food Quality Protection Act, responsibility for 

establishing tolerances in lieu of ALs has been transferred to EPA. In the interim, ALs are 

used.

The Pesticide Data Program reports tolerance violations to the U.S. Food and Drug 

Administration (FDA) as part of an interagency Memorandum of Understanding between 

the U.S. Department of Agriculture and FDA. Residues reported to FDA are shown in the 

“Pesticide/Commodity” column to the right of the commodity and are annotated as “X” (if the 

residue exceeded the established tolerance) or “V” (if the residue did not have a tolerance 

listed in the Code of Federal Regulations, Title 40, Part 180). In both cases, these annotations 

are followed by a number indicating the number of samples reported to FDA. 

Results for environmental contaminants across all commodities, including fruit and vegetables, 

have been consolidated in a separate appendix because they have no registered uses and 

are not applied to crops (see Appendix H). 
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Abamectin (insecticide, acaricide)

Celery 346 0 0.020 ^ 0.10

Plums 507 0 0.020 ^ 0.09

Raspberries (X-1) 351 1 0.3 0.095 ^ 0.020 ^ 0.01

Raspberries, Frozen 10 0 0.020 ^ 0.01

Summer Squash 363 0 0.020 ^ 0.01

Winter Squash 187 0 0.012 ^ 0.01

TOTAL 1,764 1

Acephate (insecticide)

Apple Juice 379 0 0.030 ^ 0.02

Baby Food - Applesauce 379 0 0.010 ^ 0.02

Baby Food - Peas 378 0 0.030 ^ 0.02

Bananas 708 0 0.075 ^ 0.02

Broccoli 649 0 0.050 ^ 0.02

Carrots 712 0 0.10 ^ 0.02

Cauliflower 532 16 3 0.005 - 0.097 0.005 ^ 2.0

Celery 708 156 22 0.003 - 0.45 0.002 - 0.010 10

Grape Juice 176 0 0.030 ^ 0.02

Green Beans 378 98 25.9 0.030 - 2.6 0.030 ^ 3.0

Mushrooms 532 0 0.030 ^ 0.02

Nectarines 271 0 0.040 ^ 0.02

Peaches 285 0 0.010 ^ 0.02

Plums 507 0 0.010 ^ 0.02

Raspberries 652 0 0.010 - 0.075 0.02

Raspberries, Frozen 53 0 0.010 - 0.075 0.02

Summer Squash (X-1) 709 2 0.3 0.011 - 0.039 0.010 - 0.030 0.02

Winter Squash 187 0 0.006 ^ 0.02

TOTAL 8,195 272

Acequinocyl (acaricide) 

Green Beans 347 0 0.20 ^ 0.25

TOTAL 347 0

Acetamiprid (insecticide) 

Apple Juice 379 57 15 0.003 - 0.019 0.003 ^ 1.0

Baby Food - Applesauce 379 89 23.5 0.011 - 0.053 0.010 ^ 1.0

Baby Food - Peas 378 0 0.020 ^ 0.40

Bananas 708 0 0.002 ^ 0.01

Broccoli 708 0 0.010 ^ 1.20

Carrots 712 0 0.002 ^ 0.01

Cauliflower 532 1 0.2 0.002 ^ 0.001 ^ 1.20

Celery 708 77 10.9 0.002 - 0.061 0.001 - 0.003 3.00

Grape Juice 148 0 0.003 ^ 0.35

Green Beans 378 2 0.5 0.010 ^ 0.002 ^ 0.60

Mushrooms 532 0 0.003 ^ 0.01

Nectarines 543 73 13.4 0.017 - 0.23 0.010 ^ 1.20

Peaches 285 15 5.3 0.011 - 0.14 0.010 ^ 1.20

Plums 507 5 1 0.003 - 0.012 0.003 ^ 0.20

Raspberries 652 36 5.5 0.003 - 1.5 0.002 - 0.003 1.6

Raspberries, Frozen 53 0 0.002 - 0.003 1.6

Summer Squash 709 7 1 0.003 - 0.025 0.003 - 0.020 0.50

Winter Squash 187 4 2.1 0.003 - 0.006 0.002 ^ 0.50

TOTAL 8,498 366

Acetochlor (herbicide) 

Baby Food - Peas 378 0 0.020 ^ 0.05

Grape Juice 176 0 0.005 ^ NT

Green Beans 378 0 0.005 ^ NT

TOTAL 932 0

Acibenzolar S methyl (plant activator) 

Apple Juice 379 0 0.020 ^ 0.05

Cauliflower 532 0 0.004 ^ 1.0

APPENDIX B. DISTRIBUTION OF RESIDUES BY PESTICIDE IN FRUIT AND VEGETABLES

Appendix B. Page 1 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Celery 362 0 0.012 ^ 0.25

Green Beans 378 0 0.020 ^ NT

Mushrooms 503 0 0.020 ^ NT

Summer Squash 346 0 0.10 ^ 2.0

TOTAL 2,500 0

Acrinathrin (insecticide, acaricide)

Apple Juice 379 0 0.010 ^ NT

Grape Juice 176 0 0.010 ^ NT

TOTAL 555 0

Alachlor (herbicide) 

Cauliflower 532 0 0.005 ^ NT

Celery 708 0 0.005 ^ NT

Green Beans 378 0 0.020 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

TOTAL 2,849 0

Aldicarb (insecticide) 

Apple Juice 114 0 0.010 - 0.020 NT

Baby Food - Applesauce 379 0 0.010 ^ NT

Bananas 708 0 0.020 ^ NT

Broccoli 708 0 0.010 ^ NT

Cauliflower 532 0 0.001 - 0.003 NT

Celery 708 0 0.003 - 0.010 NT

Mushrooms 266 0 0.010 - 0.030 NT

Nectarines 543 0 0.003 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.010 - 0.020 NT

Raspberries, Frozen 53 0 0.010 - 0.020 NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 6,005 0

Aldicarb sulfone (metabolite of Aldicarb)

Apple Juice 379 0 0.003 ^ NT

Baby Food - Applesauce 379 0 0.010 ^ NT

Bananas 708 0 0.025 ^ NT

Broccoli 708 0 0.010 ^ NT

Cauliflower 516 0 0.010 - 0.020 NT

Celery 708 0 0.003 - 0.010 NT

Grape Juice 176 0 0.005 ^ NT

Mushrooms 532 0 0.003 - 0.005 NT

Nectarines 543 0 0.050 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.010 - 0.025 NT

Raspberries, Frozen 53 0 0.010 - 0.025 NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 6,696 0

Aldicarb sulfoxide (metabolite of Aldicarb)

Apple Juice 379 0 0.003 ^ NT

Baby Food - Applesauce 379 0 0.010 ^ NT

Bananas 708 0 0.050 ^ NT

Broccoli 708 0 0.010 ^ NT

Cauliflower 532 0 0.006 ^ NT

Celery 708 0 0.002 - 0.010 NT

Grape Juice 176 0 0.005 ^ NT

Mushrooms 532 0 0.003 - 0.005 NT

Nectarines 543 0 0.050 ^ NT

Appendix B. Page 2 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.010 - 0.050 NT

Raspberries, Frozen 53 0 0.010 - 0.050 NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 6,712 0

Allethrin (insecticide) 

Apple Juice 346 0 0.025 ^ EX

Baby Food - Applesauce 357 0 0.020 ^ EX

Baby Food - Peas 378 0 0.10 ^ EX

Bananas 708 0 0.080 ^ EX

Broccoli 707 0 0.020 ^ EX

Carrots 712 0 0.008 ^ EX

Celery 346 0 0.020 ^ EX

Green Beans 378 0 0.050 ^ EX

Mushrooms 502 0 0.025 ^ EX

Nectarines 543 0 0.008 ^ EX

Peaches 285 0 0.020 ^ EX

Plums 507 0 0.020 ^ EX

Raspberries 652 0 0.020 - 0.080 EX

Raspberries, Frozen 53 0 0.020 - 0.080 EX

Summer Squash 709 0 0.020 - 0.10 EX

Winter Squash 187 0 0.012 ^ EX

TOTAL 7,370 0

Ametoctradin (fungicide) 

Celery 346 0 0.003 ^ 40.0

Green Beans 378 0 0.001 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 709 5 0.7 0.007 - 0.034 0.003 - 0.005 3.0

TOTAL 2,301 5

Ametryn (herbicide) 

Baby Food - Applesauce 379 0 0.010 ^ NT

Celery 346 0 0.005 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.005 ^ NT

TOTAL 2,428 0

Atrazine (herbicide) 

Apple Juice 379 0 0.002 ^ NT

Baby Food - Applesauce 357 0 0.001 ^ NT

Broccoli 707 0 0.005 ^ NT

Cauliflower 532 0 0.003 ^ NT

Celery 708 0 0.001 - 0.005 0.25

Grape Juice 148 0 0.002 ^ NT

Mushrooms 532 0 0.002 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 5,066 0

Avermectin (insecticide, acaricide)

Carrots 712 0 0.060 ^ 0.01

Nectarines 543 0 0.050 ^ 0.09

TOTAL 1,255 0

Appendix B. Page 3 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Azinphos (insecticide) 

Celery 346 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 1,764 0

Azinphos methyl (insecticide) 

Apple Juice 379 0 0.003 ^ 1.5

Baby Food - Applesauce 358 0 0.004 ^ 1.5

Baby Food - Peas 378 0 0.090 ^ NT

Bananas 708 0 0.004 ^ NT

Carrots 712 0 0.009 ^ NT

Cauliflower 532 0 0.012 ^ NT

Celery 708 0 0.005 - 0.012 NT

Grape Juice 176 0 0.010 ^ NT

Green Beans 378 0 0.020 ^ NT

Mushrooms 532 0 0.003 - 0.010 NT

Nectarines (V-3) 543 3 0.6 0.008 - 0.080 0.005 ^ NT

Peaches 285 0 0.020 ^ 2.0

Plums 507 0 0.005 ^ 2.0

Raspberries 652 0 0.004 - 0.005 2.0

Raspberries, Frozen 53 1 1.9 0.008 ^ 0.004 - 0.005 2.0

Summer Squash 709 0 0.005 - 0.090 NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 7,797 4

Azinphos methyl oxygen analog (metabolite of Azinphos methyl)

Apple Juice 379 0 0.010 ^ 1.5

Baby Food - Peas 378 0 0.015 ^ NT

Bananas 708 0 0.005 ^ NT

Carrots 712 0 0.008 ^ NT

Celery 346 0 0.010 ^ NT

Grape Juice 176 0 0.010 ^ NT

Green Beans 378 0 0.003 ^ NT

Mushrooms 532 0 0.010 ^ NT

Nectarines 543 0 0.001 ^ NT

Plums 507 0 0.010 ^ 2.0

Raspberries 652 0 0.005 - 0.010 2.0

Raspberries, Frozen 53 0 0.005 - 0.010 2.0

Summer Squash 709 0 0.010 - 0.015 NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 6,260 0

Azoxystrobin (fungicide) 

Apple Juice 379 0 0.003 ^ NT

Baby Food - Applesauce 379 0 0.002 ^ NT

Baby Food - Peas 378 0 0.005 ^ 0.5

Bananas 708 151 21.3 0.005 - 0.077 0.005 ^ 2.0

Broccoli 708 75 10.6 0.002 - 0.46 0.002 ^ 3.0

Carrots 712 55 7.7 0.010 - 0.031 0.006 ^ 0.5

Cauliflower 532 2 0.4 0.002 ^ 0.001 ^ 3.0

Celery 708 123 17.4 0.002 - 0.42 0.001 - 0.003 30.0

Grape Juice 148 0 0.003 ^ 2.0

Green Beans 378 116 30.7 0.001 - 0.076 0.001 ^ 3.0

Mushrooms 532 0 0.003 ^ NT

Nectarines 543 19 3.5 0.002 - 0.055 0.001 ^ 1.5

Peaches 285 17 6 0.002 - 0.13 0.002 ^ 1.5

Plums 507 3 0.6 0.006 - 0.018 0.003 ^ 1.5

Raspberries 652 52 8 0.003 - 0.34 0.003 - 0.005 5.0

Raspberries, Frozen 53 4 7.5 0.015 - 0.20 0.003 - 0.005 5.0

Summer Squash 709 11 1.6 0.004 - 0.050 0.003 - 0.005 0.3

Winter Squash 187 2 1.1 0.003 ^ 0.002 ^ 0.3

TOTAL 8,498 630

Appendix B. Page 4 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Bendiocarb (insecticide) 

Apple Juice 379 0 0.003 ^ SU

Baby Food - Applesauce 379 0 0.005 ^ SU

Baby Food - Peas 378 0 0.015 ^ SU

Bananas 708 0 0.009 ^ SU

Broccoli 708 0 0.005 ^ SU

Carrots 712 0 0.002 ^ SU

Cauliflower 532 0 0.005 - 0.015 SU

Celery 708 0 0.005 - 0.015 SU

Grape Juice 176 0 0.003 ^ SU

Green Beans 378 0 0.015 ^ SU

Mushrooms 532 0 0.003 ^ SU

Nectarines 543 0 0.001 ^ SU

Peaches 285 0 0.005 ^ SU

Plums 507 0 0.005 ^ SU

Raspberries 652 0 0.005 - 0.009 SU

Raspberries, Frozen 53 0 0.005 - 0.009 SU

Summer Squash 709 0 0.005 - 0.015 SU

Winter Squash 187 0 0.003 ^ SU

TOTAL 8,526 0

Benfluralin (herbicide) 

Apple Juice 379 0 0.010 ^ NT

Celery 346 0 0.005 ^ NT

Grape Juice 176 0 0.010 ^ NT

Mushrooms 532 0 0.010 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

TOTAL 2,664 0

Benoxacor (herbicide safener) 

Apple Juice 379 0 0.010 ^ NT

Baby Food - Peas 378 0 0.030 ^ 0.01

Bananas 708 0 0.012 ^ NT

Carrots 712 0 0.015 ^ 0.01

Cauliflower 532 0 0.001 ^ 0.01

Celery 708 0 0.001 - 0.010 0.01

Grape Juice 176 0 0.010 ^ NT

Green Beans 378 0 0.020 ^ 0.01

Mushrooms 532 0 0.010 ^ NT

Nectarines 543 0 0.005 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.010 - 0.012 0.01

Raspberries, Frozen 53 0 0.010 - 0.012 0.01

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ 0.01

TOTAL 6,808 0

Bensulide (herbicide) 

Apple Juice 379 0 0.004 ^ NT

Carrots 676 0 0.006 - 0.020 0.10

Celery 346 0 0.003 ^ 0.15

Grape Juice 176 0 0.004 ^ NT

Green Beans 378 0 0.015 ^ NT

Mushrooms 532 0 0.004 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 709 0 0.003 - 0.005 0.15

Winter Squash 187 0 0.002 ^ 0.15

TOTAL 4,251 0

Appendix B. Page 5 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Bensulide oxygen analog (herbicide metabolite)

Apple Juice 379 0 0.002 ^ NT

Carrots 712 0 0.002 ^ 0.10

Grape Juice 176 0 0.002 ^ NT

Green Beans 378 0 0.002 ^ NT

Mushrooms 532 0 0.002 ^ NT

Summer Squash 346 0 0.005 ^ 0.15

TOTAL 2,523 0

Bentazon (herbicide) 

Baby Food - Peas 378 0 0.50 ^ 3.0

Bananas 708 0 0.015 ^ NT

Green Beans 378 0 0.10 ^ 0.5

Raspberries 301 0 0.015 ^ NT

Raspberries, Frozen 43 0 0.015 ^ NT

TOTAL 1,808 0

Benthiavalicarb isopropyl (fungicide) 

Bananas 708 0 0.005 ^ NT

Raspberries 301 0 0.005 ^ NT

Raspberries, Frozen 43 0 0.005 ^ NT

TOTAL 1,052 0

Bifenazate (acaricide) 

Celery 346 0 0.005 ^ NT

Plums 507 3 0.6 0.007 - 0.022 0.005 ^ 0.20

Raspberries 351 105 29.9 0.005 - 1.5 0.005 ^ 5.0

Raspberries, Frozen 10 0 0.005 ^ 5.0

Summer Squash 363 0 0.005 ^ 0.75

Winter Squash 187 0 0.003 ^ 0.75

TOTAL 1,764 108

Bifenox (herbicide) 

Celery 288 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

TOTAL 1,519 0

Bifenthrin (insecticide) 

Apple Juice 379 0 0.005 ^ 0.5

Baby Food - Applesauce 379 10 2.6 0.002 ^ 0.001 ^ 0.5

Baby Food - Peas 378 0 0.020 ^ 0.05

Bananas 708 0 0.008 ^ 0.1

Broccoli 707 5 0.7 0.007 - 0.078 0.005 ^ 0.6

Carrots 712 0 0.001 ^ 0.10

Cauliflower 532 0 0.002 ^ 0.6

Celery 708 11 1.6 0.003 - 0.062 0.002 - 0.010 3.0

Grape Juice 176 0 0.005 ^ 0.2

Green Beans 378 40 10.6 0.040 - 0.13 0.040 ^ 0.6

Mushrooms 532 0 0.005 ^ 0.05

Nectarines 543 1 0.2 0.010 ^ 0.001 ^ 0.5

Peaches 285 3 1.1 0.084 - 0.15 0.005 ^ 0.5

Plums 507 0 0.010 ^ 0.05

Raspberries 652 23 3.5 0.009 - 0.72 0.008 - 0.010 1.0

Raspberries, Frozen 53 7 13.2 0.017 - 0.20 0.008 - 0.010 1.0

Summer Squash 709 18 2.5 0.012 - 0.10 0.010 - 0.020 0.4

Winter Squash 187 22 11.8 0.005 - 0.072 0.003 ^ 0.4

TOTAL 8,525 140

Bitertanol (fungicide) 

Baby Food - Applesauce 379 0 0.010 ^ NT

Broccoli 708 0 0.010 ^ NT

Celery 346 0 0.040 ^ NT

Peaches 285 0 0.010 ^ NT

Appendix B. Page 6 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Plums 507 0 0.040 ^ NT

Raspberries 351 0 0.040 ^ NT

Raspberries, Frozen 10 0 0.040 ^ NT

Summer Squash 363 0 0.040 ^ NT

TOTAL 2,949 0

Boscalid (fungicide) 

Apple Juice 379 2 0.5 0.003 - 0.006 0.003 ^ 3.0

Baby Food - Applesauce 379 12 3.2 0.011 - 0.035 0.010 ^ 3.0

Baby Food - Peas 378 0 0.010 ^ 0.6

Bananas 708 1 0.1 0.016 ^ 0.013 ^ 0.40

Broccoli 708 11 1.6 0.021 - 0.39 0.010 ^ 3.0

Carrots 712 164 23 0.025 - 0.17 0.015 - 0.050 1.0

Celery 693 62 8.9 0.006 - 0.10 0.005 - 0.020 45

Grape Juice 176 14 8 0.006 - 0.079 0.003 ^ 3.5

Green Beans 378 35 9.3 0.006 - 0.87 0.005 ^ 1.6

Mushrooms 532 0 0.003 ^ NT

Nectarines 543 82 15.1 0.002 - 0.19 0.001 ^ 3.5

Peaches 285 105 36.8 0.010 - 0.35 0.010 ^ 3.5

Plums 507 9 1.8 0.005 - 0.026 0.005 ^ 3.5

Raspberries 652 160 24.5 0.005 - 3.0 0.005 - 0.013 6.0

Raspberries, Frozen 53 6 11.3 0.021 - 0.63 0.005 - 0.013 6.0

Summer Squash 709 10 1.4 0.005 - 0.075 0.005 - 0.015 1.6

Winter Squash 187 4 2.1 0.005 ^ 0.003 ^ 1.6

TOTAL 7,979 677

Bromacil (herbicide) 

Apple Juice 379 0 0.003 ^ NT

Bananas 708 0 0.005 ^ NT

Celery 346 0 0.010 ^ NT

Grape Juice 176 0 0.003 ^ NT

Mushrooms 532 0 0.003 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.005 - 0.010 NT

Raspberries, Frozen 53 0 0.005 - 0.010 NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 156 0 0.009 ^ NT

TOTAL 3,872 0

Bromopropylate (acaricide) 

Baby Food - Applesauce 379 0 0.001 ^ NT

Broccoli 707 0 0.005 ^ NT

Celery 346 0 0.010 ^ NT

Nectarines 543 0 0.001 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

TOTAL 3,491 0

Bromuconazole (fungicide) 

Celery 346 0 0.010 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

TOTAL 1,577 0

Bupirimate (fungicide) 

Apple Juice 379 0 0.001 ^ NT

Baby Food - Applesauce 379 0 0.001 ^ NT

Bananas 708 0 0.002 ^ NT

Broccoli 707 0 0.005 ^ NT

Celery 346 0 0.040 ^ NT

Grape Juice 176 0 0.001 ^ NT

Appendix B. Page 7 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Nectarines 543 0 0.003 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.040 ^ NT

Raspberries 652 0 0.002 - 0.040 NT

Raspberries, Frozen 53 0 0.002 - 0.040 NT

Summer Squash 363 0 0.040 ^ NT

TOTAL 5,098 0

Buprofezin (insecticide) 

Apple Juice 379 0 0.001 ^ 3.0

Baby Food - Applesauce 379 0 0.010 ^ 3.0

Bananas 708 46 6.5 0.001 - 0.097 0.001 ^ 0.20

Broccoli 708 8 1.1 0.017 - 0.12 0.010 ^ 12.0

Cauliflower 532 0 0.001 ^ 12.0

Celery 708 14 2 0.002 - 0.021 0.001 - 0.005 35

Grape Juice 176 0 0.001 ^ 2.5

Green Beans 378 1 0.3 0.002 ^ 0.001 ^ 0.02

Mushrooms 532 0 0.001 ^ NT

Nectarines 543 25 4.6 0.002 - 0.068 0.001 ^ 1.9

Peaches 285 16 5.6 0.011 - 0.030 0.010 ^ 9.0

Plums 507 2 0.4 0.006 - 0.028 0.005 ^ 1.9

Raspberries (V-1) 652 1 0.2 0.002 ^ 0.001 - 0.005 NT

Raspberries, Frozen 53 0 0.001 - 0.005 NT

Summer Squash 709 1 0.1 0.006 ^ 0.005 ^ 0.50

Winter Squash 187 0 0.003 ^ 0.50

TOTAL 7,436 114

Butocarboxim (insecticide, acaricide)

Baby Food - Applesauce 379 0 0.010 ^ NT

Bananas 708 0 0.010 ^ NT

Broccoli 708 0 0.010 ^ NT

Nectarines 543 0 0.001 ^ NT

Peaches 285 0 0.010 ^ NT

Raspberries 301 0 0.010 ^ NT

Raspberries, Frozen 43 0 0.010 ^ NT

TOTAL 2,967 0

Butocarboxim sulfone (metabolite of Butocarboxim)

Bananas 708 0 0.021 ^ NT

Raspberries 301 0 0.021 ^ NT

Raspberries, Frozen 43 0 0.021 ^ NT

TOTAL 1,052 0

Butocarboxim sulfoxide (metabolite of Butocarboxim)

Bananas 708 0 0.006 ^ NT

Nectarines 543 0 0.030 ^ NT

Raspberries 301 0 0.006 ^ NT

Raspberries, Frozen 43 0 0.006 ^ NT

TOTAL 1,595 0

Cadusafos (insecticide) 

Celery 346 0 0.003 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

TOTAL 1,577 0

Captan (fungicide) (parent of THPI)

Baby Food - Applesauce 291 0 0.004 - 0.020 25.0

Bananas 708 0 0.19 ^ NT

Carrots 712 0 0.20 ^ 0.05

Nectarines 543 4 0.7 0.15 - 0.76 0.050 ^ 25.0

Peaches 285 39 13.7 0.027 - 1.2 0.020 ^ 15.0

Appendix B. Page 8 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Raspberries 301 3 1 0.25 - 1.0 0.19 ^ 25.0

Raspberries, Frozen 43 4 9.3 0.27 - 2.2 0.19 ^ 25.0

TOTAL 2,883 50

Carbaryl (insecticide) 

Apple Juice 379 8 2.1 0.004 - 0.041 0.003 ^ 12

Baby Food - Applesauce 379 1 0.3 0.021 ^ 0.010 ^ 12

Baby Food - Peas 378 0 0.020 ^ 10

Bananas 708 0 0.005 ^ 5.0

Broccoli 708 0 0.010 ^ 10

Carrots 712 0 0.002 ^ 2.0

Cauliflower 532 0 0.001 ^ 10

Celery 708 6 0.8 0.008 - 0.67 0.001 - 0.005 3.0

Grape Juice 176 45 25.6 0.003 - 0.026 0.003 ^ 10

Green Beans 378 1 0.3 0.027 ^ 0.002 ^ 10

Mushrooms 532 0 0.003 ^ NT

Nectarines 543 4 0.7 0.016 - 0.71 0.004 ^ 10

Peaches 285 4 1.4 0.010 - 1.3 0.010 ^ 10

Plums 507 1 0.2 0.007 ^ 0.005 ^ 10

Raspberries 652 0 0.005 ^ 12.0

Raspberries, Frozen 53 6 11.3 0.007 - 0.052 0.005 ^ 12.0

Summer Squash 709 2 0.3 0.006 ^ 0.005 - 0.020 3.0

Winter Squash 187 0 0.003 ^ 3.0

TOTAL 8,526 78

Carbendazim - MBC (fungicide) (metabolite of Benomyl and Thiophanate Methyl)

Apple Juice 379 106 28 0.001 - 0.035 0.001 ^ 2.0

Baby Food - Applesauce 379 38 10 0.010 - 0.058 0.010 ^ 2.0

Bananas 708 0 0.005 ^ 2.0

Broccoli (V-1) 708 1 0.1 0.049 ^ 0.010 ^ NT

Carrots 712 0 0.003 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery (V-1) 708 1 0.1 0.002 ^ 0.001 - 0.005 NT

Grape Juice 176 5 2.8 0.002 - 0.004 0.001 ^ 5.0

Mushrooms (V-5) 532 5 0.9 0.011 - 0.56 0.001 ^ NT

Nectarines (V-2) 543 2 0.4 0.005 - 0.026 0.003 ^ NT

Peaches 285 13 4.6 0.016 - 0.12 0.010 ^ 3.0

Plums 507 1 0.2 0.010 ^ 0.005 ^ 0.5

Raspberries (V-3) 652 3 0.5 0.007 - 0.015 0.005 ^ NT

Raspberries, Frozen (V-8) 53 8 15.1 0.006 - 0.22 0.005 ^ NT

Summer Squash 363 9 2.5 0.009 - 0.042 0.005 ^ 1.0

Winter Squash 187 5 2.7 0.003 - 0.045 0.002 ^ 1.0

TOTAL 7,424 197

Carbofuran (insecticide) (parent of 3-Hydroxycarbofuran)

Apple Juice 379 0 0.003 ^ NT

Baby Food - Applesauce 379 0 0.010 ^ NT

Baby Food - Peas 378 0 0.005 ^ NT

Bananas 708 0 0.006 ^ 0.1

Broccoli (V-1) 708 1 0.1 0.026 ^ 0.010 ^ NT

Carrots 712 0 0.001 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.005 NT

Grape Juice 176 0 0.003 ^ 0.4

Green Beans (V-2) 378 2 0.5 0.002 ^ 0.001 ^ NT

Mushrooms 532 0 0.003 ^ NT

Nectarines 543 0 0.001 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.005 - 0.006 NT

Raspberries, Frozen 53 0 0.005 - 0.006 NT

Summer Squash 709 0 0.005 ^ 0.8

Winter Squash 187 0 0.003 ^ 0.8

TOTAL 8,526 3

Appendix B. Page 9 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Carbophenothion (insecticide) 

Cauliflower 532 0 0.002 - 0.008 NT

Celery 708 0 0.002 - 0.010 NT

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 2,658 0

Carbophenothion methyl (insecticide) 

Celery 346 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

TOTAL 1,577 0

Carboxin (fungicide) 

Celery 346 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 1,764 0

Carfentrazone (herbicide) 

Apple Juice 379 4 1.1 0.006 - 0.013 0.005 ^ 0.10

Baby Food - Applesauce 379 0 0.001 ^ 0.10

Baby Food - Peas 378 0 0.005 ^ 0.10

Bananas 708 0 0.016 ^ 0.20

Broccoli 707 0 0.005 ^ 0.10

Carrots 712 0 0.002 ^ 0.10

Cauliflower 532 0 0.005 ^ 0.10

Celery 693 0 0.003 - 0.005 0.10

Grape Juice 176 0 0.005 ^ 0.10

Green Beans 378 0 0.005 ^ 0.10

Mushrooms 503 0 0.005 ^ NT

Nectarines 543 0 0.002 ^ 0.10

Peaches 285 0 0.005 ^ 0.10

Plums 507 0 0.003 ^ 0.10

Raspberries 652 0 0.003 - 0.016 0.10

Raspberries, Frozen 53 0 0.003 - 0.016 0.10

Summer Squash 709 0 0.003 - 0.005 0.10

Winter Squash 187 0 0.002 ^ 0.10

TOTAL 8,481 4

Chlorantraniliprole (insecticide) 

Apple Juice 379 1 0.3 0.015 ^ 0.010 ^ 1.2

Baby Food - Applesauce 379 0 0.020 ^ 1.2

Baby Food - Peas 378 0 0.005 ^ 2.0

Broccoli 708 9 1.3 0.021 - 0.19 0.020 ^ 4.0

Carrots 712 0 0.005 ^ 0.30

Cauliflower 532 2 0.4 0.003 - 0.018 0.002 ^ 4.0

Celery 708 203 28.7 0.003 - 0.29 0.002 - 0.010 13

Grape Juice 176 0 0.010 ^ 2.5

Green Beans 378 46 12.2 0.001 - 0.020 0.001 ^ 2.0

Mushrooms 532 0 0.010 ^ NT

Nectarines 543 7 1.3 0.083 ^ 0.050 ^ 4.0

Peaches 285 72 25.3 0.021 - 0.15 0.020 ^ 4.0

Plums 507 4 0.8 0.010 - 0.019 0.010 ^ 4.0

Raspberries 351 2 0.6 0.044 - 0.054 0.010 ^ 1.8

Raspberries, Frozen 10 0 0.010 ^ 1.8

Summer Squash 709 2 0.3 0.006 ^ 0.005 - 0.010 0.5

Winter Squash 187 1 0.5 0.010 ^ 0.006 ^ 0.5

TOTAL 7,474 349

Appendix B. Page 10 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Chlorethoxyfos (insecticide) 

Celery 346 0 0.010 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.009 ^ NT

TOTAL 1,764 0

Chlorfenapyr (insecticide) 

Apple Juice 379 0 0.015 ^ 0.01

Baby Food - Applesauce 357 0 0.005 ^ 0.01

Baby Food - Peas 378 0 0.050 ^ 0.01

Bananas 708 0 0.040 ^ 0.01

Broccoli 707 0 0.005 ^ 0.01

Carrots 712 0 0.10 ^ 0.01

Cauliflower 532 0 0.002 ^ 0.01

Celery 362 0 0.002 ^ 0.01

Grape Juice 176 0 0.015 ^ 0.01

Green Beans 378 0 0.025 ^ 0.01

Mushrooms 532 0 0.015 ^ 0.01

Nectarines 543 0 0.025 ^ 0.01

Peaches 285 0 0.005 ^ 0.01

Raspberries 301 0 0.040 ^ 0.01

Raspberries, Frozen 43 0 0.040 ^ 0.01

Summer Squash 346 0 0.050 ^ 0.01

TOTAL 6,739 0

Chlorfenvinphos (insecticide) 

Cauliflower 532 0 0.004 ^ NT

Celery 708 0 0.004 - 0.010 NT

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 2,658 0

Chlorobenzilate (acaricide) 

Celery 346 0 0.003 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

TOTAL 1,577 0

Chloroneb (fungicide) 

Celery 346 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

TOTAL 1,577 0

Chlorothalonil (fungicide) 

Apple Juice 313 0 0.020 ^ NT

Baby Food - Applesauce 357 0 0.001 ^ NT

Mushrooms 532 1 0.2 0.026 ^ 0.020 ^ 1.0

Peaches 285 2 0.7 0.024 - 0.088 0.005 ^ 0.5

Plums 507 2 0.4 0.011 - 0.015 0.010 ^ 0.2

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

TOTAL 2,355 5

Appendix B. Page 11 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Chlorpropham (herbicide, growth regulator)

Apple Juice 379 0 0.020 ^ NT

Baby Food - Applesauce 357 0 0.001 ^ NT

Bananas 708 0 0.020 ^ NT

Broccoli (V-3) 707 3 0.4 0.008 - 0.013 0.005 ^ NT

Cauliflower (V-9) 532 9 1.7 0.002 - 0.007 0.001 ^ NT

Celery (V-4) 708 4 0.6 0.002 - 0.009 0.001 - 0.005 NT

Grape Juice 176 0 0.020 ^ NT

Green Beans 378 0 0.020 ^ NT

Mushrooms 532 0 0.020 ^ NT

Nectarines 543 0 0.060 ^ NT

Peaches (V-3) 285 3 1.1 0.011 - 0.013 0.005 ^ NT

Plums (V-1) 507 1 0.2 0.006 ^ 0.005 ^ NT

Raspberries (V-7) 652 7 1.1 0.006 - 0.13 0.005 - 0.020 NT

Raspberries, Frozen 53 0 0.005 - 0.020 NT

Summer Squash 709 0 0.005 - 0.20 NT

Winter Squash (V-2) 187 2 1.1 0.010 ^ 0.006 ^ NT

TOTAL 7,413 29

Chlorpyrifos (insecticide) 

Apple Juice 379 0 0.005 ^ 0.01

Baby Food - Applesauce 379 5 1.3 0.002 ^ 0.001 ^ 0.01

Baby Food - Peas 378 0 0.15 ^ 0.05

Bananas 708 0 0.005 ^ 0.1

Broccoli 707 5 0.7 0.006 - 0.034 0.005 ^ 1.0

Carrots 712 3 0.4 0.010 - 0.046 0.006 ^ 0.1

Cauliflower 532 2 0.4 0.002 - 0.010 0.001 ^ 1.0

Celery 708 5 0.7 0.002 - 0.004 0.001 - 0.010 0.1

Grape Juice 176 0 0.005 ^ 0.01

Green Beans 378 1 0.3 0.059 ^ 0.035 ^ 0.05

Mushrooms 532 0 0.005 ^ 0.1

Nectarines 543 21 3.9 0.005 - 0.036 0.003 ^ 0.05

Peaches 285 4 1.4 0.005 - 0.008 0.005 ^ 0.05

Plums 507 1 0.2 0.011 ^ 0.010 ^ 0.05

Raspberries 652 1 0.2 0.031 ^ 0.005 - 0.010 0.1

Raspberries, Frozen 53 4 7.5 0.006 - 0.019 0.005 - 0.010 0.1

Summer Squash 709 1 0.1 0.032 ^ 0.010 - 0.075 0.1

Winter Squash 187 0 0.006 ^ 0.1

TOTAL 8,525 53

Chlorpyrifos oxygen analog (metabolite of Chlorpyrifos)

Apple Juice 379 0 0.002 ^ 0.01

Baby Food - Peas 378 0 0.005 ^ 0.05

Bananas 708 0 0.009 ^ 0.1

Carrots 712 0 0.001 ^ 0.1

Cauliflower 532 0 0.001 - 0.003 1.0

Celery 708 0 0.001 - 0.010 0.1

Grape Juice 176 0 0.002 ^ 0.01

Green Beans 378 0 0.001 ^ 0.05

Mushrooms 532 0 0.002 ^ 0.1

Nectarines 543 0 0.001 ^ 0.05

Plums 507 0 0.010 ^ 0.05

Raspberries 652 0 0.009 - 0.010 0.1

Raspberries, Frozen 53 0 0.009 - 0.010 0.1

Summer Squash 709 0 0.005 - 0.010 0.1

Winter Squash 187 0 0.006 ^ 0.1

TOTAL 7,154 0

Chlozolinate (fungicide) 

Celery 288 0 0.010 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 290 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 303 0 0.010 ^ NT

TOTAL 1,398 0

Appendix B. Page 12 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Clethodim (herbicide) 

Baby Food - Peas 356 0 0.20 ^ 3.5

Carrots 712 0 0.001 ^ 1.0

Cauliflower 532 0 0.002 ^ 3.0

Celery 592 0 0.002 - 0.040 0.60

Green Beans 378 0 0.40 ^ 3.5

Nectarines 543 0 0.001 ^ NT

Plums 416 0 0.040 ^ NT

Raspberries 264 0 0.040 ^ 0.30

Raspberries, Frozen 7 0 0.040 ^ 0.30

Summer Squash 543 0 0.040 - 0.20 0.50

TOTAL 4,343 0

Clethodim sulfone (metabolite of Clethodim)

Celery 346 0 0.005 ^ 0.60

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ 0.30

Raspberries, Frozen 10 0 0.005 ^ 0.30

Summer Squash 363 0 0.005 ^ 0.50

TOTAL 1,577 0

Clethodim sulfoxide (metabolite of Clethodim)

Celery 230 0 0.005 ^ 0.60

Plums 416 0 0.005 ^ NT

Raspberries 264 0 0.005 ^ 0.30

Raspberries, Frozen 7 0 0.005 ^ 0.30

Summer Squash 273 0 0.005 ^ 0.50

TOTAL 1,190 0

Clofentezine (insecticide) 

Celery 346 0 0.020 ^ NT

Nectarines 542 11 2 0.002 - 0.052 0.001 ^ 1.0

Plums 507 0 0.020 ^ NT

Raspberries 351 0 0.020 ^ NT

Raspberries, Frozen 10 0 0.020 ^ NT

Summer Squash 363 0 0.020 ^ NT

Winter Squash 187 0 0.012 ^ NT

TOTAL 2,306 11

Clomazone (herbicide) 

Apple Juice 379 0 0.005 ^ NT

Baby Food - Applesauce 379 0 0.001 - 0.005 NT

Baby Food - Peas 378 0 0.050 ^ 0.05

Bananas 708 0 0.070 ^ NT

Broccoli 707 0 0.005 ^ NT

Cauliflower 532 0 0.002 ^ NT

Celery 708 0 0.002 - 0.003 NT

Grape Juice 176 0 0.005 ^ NT

Green Beans 378 0 0.005 ^ 0.05

Mushrooms 532 0 0.005 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.003 - 0.070 NT

Raspberries, Frozen 53 0 0.003 - 0.070 NT

Summer Squash 709 1 0.1 0.006 ^ 0.003 - 0.050 0.1

Winter Squash 187 0 0.003 ^ 0.1

TOTAL 7,270 1

Clothianidin (insecticide) (also a metabolite of Thiamethoxam)

Apple Juice 379 0 0.010 ^ 1.0

Baby Food - Applesauce 379 0 0.010 ^ 1.0

Baby Food - Peas 378 0 0.060 ^ 0.02

Bananas 708 0 0.035 ^ NT

Broccoli 708 4 0.6 0.011 - 0.015 0.010 ^ 4.5

Carrots 712 0 0.005 ^ 0.8

Cauliflower 516 1 0.2 0.011 ^ 0.005 - 0.010 4.5

Appendix B. Page 13 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Celery 708 1 0.1 0.003 ^ 0.002 - 0.010 4.0

Grape Juice 176 0 0.010 ^ 0.60

Green Beans 378 1 0.3 0.019 ^ 0.005 ^ 0.02

Mushrooms 532 0 0.010 ^ NT

Nectarines 543 5 0.9 0.008 - 0.031 0.005 ^ 0.5

Peaches 285 26 9.1 0.010 - 0.13 0.010 ^ 0.80

Plums 507 0 0.005 ^ 0.5

Raspberries 652 0 0.005 - 0.035 0.35

Raspberries, Frozen 53 0 0.005 - 0.035 0.35

Summer Squash 709 6 0.8 0.006 - 0.012 0.005 - 0.050 0.2

Winter Squash 187 1 0.5 0.005 ^ 0.003 ^ 0.2

TOTAL 8,510 45

Coumaphos (insecticide) 

Baby Food - Applesauce 357 0 0.001 ^ NT

Broccoli 707 0 0.005 ^ NT

Cauliflower 532 0 0.002 ^ NT

Celery 708 0 0.002 - 0.005 NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 4,007 0

Coumaphos oxygen analog (metabolite of Coumaphos)

Cauliflower 532 0 0.008 ^ NT

Celery 362 0 0.008 ^ NT

TOTAL 894 0

Crotoxyphos (insecticide, acaricide)

Celery 346 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 1,764 0

Crufomate (insecticide) 

Celery 346 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 1,764 0

Cyazofamid (fungicide) 

Bananas 708 0 0.020 ^ NT

Carrots 712 32 4.5 0.013 - 0.030 0.008 ^ 0.09

Celery 346 0 0.010 ^ NT

Green Beans 378 0 0.010 ^ 0.5

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.010 - 0.020 NT

Raspberries, Frozen 53 0 0.010 - 0.020 NT

Summer Squash 709 3 0.4 0.011 - 0.059 0.010 - 0.050 0.10

Winter Squash 187 8 4.3 0.010 - 0.10 0.006 ^ 0.10

TOTAL 4,252 43

Cyfluthrin (insecticide) 

Apple Juice 379 0 0.004 ^ 0.5

Baby Food - Applesauce 357 0 0.001 - 0.005 0.5

Baby Food - Peas 378 0 0.050 ^ 0.25

Bananas 708 0 0.042 ^ 0.05

Appendix B. Page 14 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Broccoli 707 5 0.7 0.006 - 0.14 0.005 ^ 2.5

Carrots 712 0 0.015 ^ 0.20

Cauliflower 532 1 0.2 0.072 ^ 0.008 ^ 2.5

Celery 693 2 0.3 0.005 - 0.007 0.005 - 0.025 6.0

Grape Juice 176 0 0.004 ^ 1.0

Green Beans (X-1) 378 1 0.3 0.11 ^ 0.10 ^ 0.05

Mushrooms 532 0 0.004 ^ 0.05

Nectarines 543 1 0.2 0.025 ^ 0.015 ^ 0.3

Peaches 285 38 13.3 0.006 - 0.12 0.005 ^ 0.3

Plums 507 0 0.005 ^ 0.3

Raspberries 652 0 0.005 - 0.042 0.05

Raspberries, Frozen 53 0 0.005 - 0.042 0.05

Summer Squash 709 3 0.4 0.008 - 0.010 0.005 - 0.10 0.1

Winter Squash 187 0 0.030 ^ 0.1

TOTAL 8,488 51

Cyhalothrin, Total (Cyhalothrin-L + R157836 epimer) (insecticide)

Apple Juice 379 0 0.005 ^ 0.30

Baby Food - Applesauce 379 2 0.5 0.003 ^ 0.002 ^ 0.30

Baby Food - Peas 378 0 0.075 ^ 0.01

Bananas 708 0 0.012 ^ 0.01

Broccoli 707 11 1.6 0.009 - 0.033 0.008 ^ 0.4

Cauliflower 532 2 0.4 0.005 ^ 0.003 ^ 0.4

Celery 708 3 0.4 0.005 ^ 0.003 - 0.010 0.01

Grape Juice 176 0 0.005 ^ 0.01

Green Beans 378 0 0.075 ^ 0.20

Mushrooms 532 0 0.005 ^ 0.01

Peaches 285 28 9.8 0.008 - 0.14 0.008 ^ 0.50

Plums 507 0 0.010 ^ 0.50

Raspberries 652 0 0.010 - 0.012 0.01

Raspberries, Frozen 53 0 0.010 - 0.012 0.01

Summer Squash 709 0 0.010 - 0.075 0.05

Winter Squash 187 0 0.012 ^ 0.05

TOTAL 7,270 46

Cyhalothrin, Lambda (includes gamma isomer)

Carrots 712 0 0.002 ^ 0.01

Nectarines 543 126 23.2 0.003 - 0.055 0.002 ^ 0.50

TOTAL 1,255 126

Cymoxanil (fungicide)

Apple Juice 379 0 0.005 ^ NT

Bananas 708 0 0.020 ^ NT

Cauliflower 516 0 0.005 - 0.010 NT

Celery 693 0 0.002 - 0.010 6.0

Green Beans 378 0 0.010 ^ NT

Mushrooms 532 0 0.005 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.010 - 0.020 4.0

Raspberries, Frozen 53 0 0.010 - 0.020 4.0

Summer Squash 709 0 0.010 - 0.050 0.05

Winter Squash 187 0 0.006 ^ 0.05

TOTAL 5,314 0

Cypermethrin (insecticide) 

Apple Juice 379 0 0.010 ^ 2

Baby Food - Applesauce 379 0 0.002 ^ 2

Baby Food - Peas 378 0 0.080 ^ 0.1

Bananas 708 0 0.069 ^ 0.05

Broccoli (X-1) 707 13 1.8 0.010 - 6.6 0.010 ^ 2.0

Carrots 712 0 0.020 ^ 0.1

Cauliflower 532 0 0.022 ^ 2.0

Celery 708 35 4.9 0.010 - 0.044 0.010 - 0.022 10.00

Grape Juice 176 0 0.010 ^ 2

Green Beans 378 0 0.30 ^ 0.5

Mushrooms 532 0 0.010 ^ 0.05

Appendix B. Page 15 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Nectarines 543 0 0.020 ^ 1

Peaches 285 6 2.1 0.010 - 0.078 0.010 ^ 1

Plums 507 0 0.010 ^ 1

Raspberries 652 92 14.1 0.010 - 0.47 0.010 - 0.069 0.8

Raspberries, Frozen 53 3 5.7 0.15 - 0.33 0.010 - 0.069 0.8

Summer Squash 709 3 0.4 0.011 - 0.015 0.010 - 0.20 0.2

Winter Squash 187 0 0.024 ^ 0.2

TOTAL 8,525 152

Cyphenothrin (insecticide) 

Apple Juice 379 0 0.015 ^ NT

Baby Food - Peas 378 0 0.050 ^ NT

Bananas 708 0 0.029 ^ NT

Carrots 712 0 0.010 ^ NT

Celery 346 0 0.010 ^ NT

Grape Juice 176 0 0.015 ^ NT

Green Beans 378 0 0.050 ^ NT

Mushrooms 502 0 0.015 ^ NT

Nectarines 543 0 0.010 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.010 - 0.029 NT

Raspberries, Frozen 53 0 0.010 - 0.029 NT

Summer Squash 709 0 0.010 - 0.050 NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 6,230 0

Cyproconazole (fungicide) 

Apple Juice 379 0 0.010 ^ NT

Bananas 708 0 0.005 ^ NT

Celery 346 0 0.010 ^ NT

Grape Juice 176 0 0.010 ^ NT

Mushrooms 532 0 0.010 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.005 - 0.010 NT

Raspberries, Frozen 53 0 0.005 - 0.010 NT

Summer Squash 363 0 0.010 ^ NT

TOTAL 3,716 0

Cyprodinil (fungicide) 

Apple Juice 379 0 0.005 ^ 1.7

Baby Food - Applesauce 379 14 3.7 0.002 - 0.008 0.001 ^ 1.7

Bananas 708 0 0.012 ^ NT

Broccoli 707 0 0.005 ^ 1.0

Carrots 712 0 0.001 ^ 0.75

Celery 317 0 0.003 ^ 30

Grape Juice 148 0 0.005 ^ 3.0

Green Beans 378 0 0.055 ^ 0.6

Mushrooms 532 0 0.005 ^ NT

Nectarines 543 36 6.6 0.003 - 0.22 0.002 ^ 2.0

Peaches 285 22 7.7 0.011 - 1.0 0.005 ^ 2.0

Plums 507 18 3.6 0.003 - 0.044 0.003 ^ 2.0

Raspberries 652 75 11.5 0.003 - 1.7 0.003 - 0.012 10

Raspberries, Frozen 53 9 17 0.024 - 0.92 0.003 - 0.012 10

Summer Squash 709 9 1.3 0.003 - 0.077 0.003 - 0.055 0.70

Winter Squash 187 1 0.5 0.011 ^ 0.003 ^ 0.70

TOTAL 7,196 184

Cyromazine (insect growth regulator) 

Cauliflower 372 0 0.008 ^ 10.0

Celery 648 91 14 0.005 - 0.32 0.005 - 0.016 7.0

Green Beans 378 0 0.10 ^ 2.0

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 709 24 3.4 0.005 - 0.061 0.005 - 0.16 1.0

Appendix B. Page 16 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Winter Squash 187 7 3.7 0.005 - 0.022 0.003 ^ 1.0

TOTAL 3,162 122

DCPA (herbicide) 

Apple Juice 379 0 0.002 ^ NT

Baby Food - Applesauce 379 0 0.001 ^ NT

Bananas 708 0 0.010 ^ NT

Broccoli 707 70 9.9 0.005 - 0.063 0.005 ^ 5.0

Cauliflower 532 18 3.4 0.002 - 0.006 0.001 ^ 5.0

Celery (V-16) 708 16 2.3 0.002 - 0.011 0.001 - 0.003 NT

Grape Juice 176 0 0.002 ^ NT

Green Beans 378 0 0.010 ^ 2.0

Mushrooms 532 0 0.002 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries (V-3) 652 3 0.5 0.003 - 0.005 0.003 - 0.010 NT

Raspberries, Frozen 53 0 0.003 - 0.010 NT

Summer Squash 709 0 0.003 - 0.025 1.0

Winter Squash 187 0 0.002 ^ 1.0

TOTAL 6,892 107

DEF - Tribufos (herbicide, plant growth regulator)

Celery 346 0 0.003 ^ NT

Grape Juice 176 0 0.002 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 1,940 0

Deltamethrin (includes parent Tralomethrin) (insecticide) 

Apple Juice 379 0 0.015 ^ 0.2

Baby Food - Applesauce 379 0 0.002 ^ 0.2

Baby Food - Peas 378 0 0.050 ^ 0.05

Bananas 708 0 0.12 ^ 0.05

Broccoli 707 0 0.008 ^ 0.05

Carrots 712 0 0.020 ^ 0.2

Cauliflower 532 21 3.9 0.020 ^ 0.012 ^ 0.05

Celery 708 78 11 0.020 ^ 0.005 - 0.040 0.05

Grape Juice 176 0 0.015 ^ 0.05

Green Beans 378 0 0.050 ^ 0.05

Mushrooms 532 0 0.015 ^ 0.05

Nectarines 543 0 0.020 ^ 0.05

Peaches 285 0 0.008 ^ 0.05

Plums 507 0 0.005 ^ 0.05

Raspberries 652 0 0.005 - 0.12 0.05

Raspberries, Frozen 53 0 0.005 - 0.12 0.05

Summer Squash 709 0 0.005 - 0.10 0.2

Winter Squash 187 0 0.012 ^ 0.2

TOTAL 8,525 99

Demeton-O (metabolite of the insecticide Demeton)

Celery 346 0 0.020 ^ NT

Plums 507 0 0.020 ^ NT

Raspberries 351 0 0.020 ^ NT

Raspberries, Frozen 10 0 0.020 ^ NT

Summer Squash 363 0 0.020 ^ NT

TOTAL 1,577 0

Demeton-S (metabolite of Demeton)

Celery 346 0 0.030 ^ NT

Plums 507 0 0.030 ^ NT

Raspberries 322 0 0.030 ^ NT

Raspberries, Frozen 7 0 0.030 ^ NT

Appendix B. Page 17 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Summer Squash 363 0 0.030 ^ NT

Winter Squash 187 0 0.009 ^ NT

TOTAL 1,732 0

Demeton-S sulfone (metabolite of Demeton-S)

Apple Juice 165 0 0.004 ^ NT

Celery 346 0 0.003 ^ NT

Mushrooms 155 0 0.004 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 2,084 0

Dialifos (insecticide) 

Celery 346 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

TOTAL 1,577 0

Diazinon (insecticide) 

Apple Juice 379 0 0.005 ^ 0.50

Baby Food - Applesauce 379 0 0.002 ^ 0.50

Baby Food - Peas 378 0 0.20 ^ 0.50

Bananas 708 0 0.010 ^ 0.20

Broccoli 708 0 0.002 ^ 0.70

Carrots 712 38 5.3 0.002 - 0.038 0.001 ^ 0.75

Cauliflower 473 0 0.001 ^ 0.70

Celery 558 1 0.2 0.051 ^ 0.001 - 0.003 0.70

Grape Juice 176 0 0.005 ^ 0.75

Green Beans 378 1 0.3 0.093 ^ 0.001 ^ 0.50

Mushrooms 532 0 0.005 ^ 0.75

Nectarines 543 0 0.001 ^ 0.20

Peaches 285 0 0.002 ^ 0.20

Plums 507 0 0.003 ^ 0.20

Raspberries 652 0 0.003 - 0.010 0.75

Raspberries, Frozen 53 0 0.003 - 0.010 0.75

Summer Squash 709 0 0.003 - 0.20 0.50

Winter Squash 187 0 0.002 ^ 0.75

TOTAL 8,317 40

Diazinon oxygen analog (metabolite of Diazinon)

Baby Food - Applesauce 379 0 0.001 ^ 0.50

Baby Food - Peas 378 0 0.030 ^ 0.50

Bananas 708 0 0.008 ^ 0.20

Broccoli 708 0 0.001 ^ 0.70

Carrots 712 0 0.001 ^ 0.75

Cauliflower 532 0 0.001 ^ 0.70

Celery 708 0 0.001 - 0.005 0.70

Green Beans 378 0 0.001 ^ 0.50

Nectarines 543 0 0.001 ^ 0.20

Peaches 285 0 0.001 ^ 0.20

Plums 507 0 0.005 ^ 0.20

Raspberries 652 0 0.005 - 0.008 0.75

Raspberries, Frozen 53 0 0.005 - 0.008 0.75

Summer Squash 709 0 0.005 - 0.060 0.50

Winter Squash 187 0 0.003 ^ 0.75

TOTAL 7,439 0

Dichlobenil (herbicide) 

Apple Juice 379 0 0.010 ^ 0.5

Baby Food - Applesauce 357 0 0.001 ^ 0.5

Bananas 708 0 0.007 ^ NT

Appendix B. Page 18 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Broccoli 707 0 0.005 ^ NT

Cauliflower 532 0 0.002 ^ NT

Celery 708 0 0.002 - 0.003 NT

Grape Juice 176 0 0.010 ^ 0.15

Peaches 285 0 0.005 ^ 0.15

Plums 507 0 0.003 ^ 0.15

Raspberries 652 0 0.003 - 0.007 0.10

Raspberries, Frozen 53 0 0.003 - 0.007 0.10

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 5,614 0

Dichlofluanid (fungicide, acaricide)

Bananas 708 0 0.035 ^ NT

Raspberries 301 0 0.035 ^ NT

Raspberries, Frozen 43 0 0.035 ^ NT

TOTAL 1,052 0

Dichlorvos - DDVP (insecticide) (also a metabolite of Naled)

Apple Juice 379 0 0.020 ^ 0.5

Baby Food - Peas 378 0 0.060 ^ 0.5

Bananas 708 0 0.005 ^ 0.5

Carrots 243 0 0.007 ^ 0.5

Celery 708 0 0.010 - 0.020 0.5

Grape Juice 176 0 0.020 ^ 0.5

Green Beans 378 0 0.060 ^ 0.5

Mushrooms 532 0 0.020 ^ 0.5

Nectarines 543 0 0.010 ^ 0.5

Plums 507 0 0.020 ^ 0.5

Raspberries 652 0 0.005 - 0.020 0.5

Raspberries, Frozen 53 0 0.005 - 0.020 0.5

Summer Squash 709 0 0.020 - 0.060 0.5

Winter Squash 187 0 0.012 ^ 0.5

TOTAL 6,153 0

Diclofop methyl (herbicide) 

Grape Juice 146 0 0.001 ^ NT

TOTAL 146 0

Dicloran (fungicide) 

Apple Juice 379 0 0.016 ^ NT

Baby Food - Applesauce 379 0 0.001 ^ NT

Bananas 708 0 0.020 ^ NT

Broccoli (V-1) 707 1 0.1 0.035 ^ 0.005 ^ NT

Carrots 711 0 0.006 ^ 10

Cauliflower 532 0 0.002 ^ NT

Celery 708 266 37.6 0.004 - 2.5 0.002 - 0.010 15

Grape Juice 176 0 0.016 ^ 10

Green Beans 378 20 5.3 0.11 - 1.5 0.10 ^ 20

Mushrooms 532 0 0.016 ^ NT

Nectarines 543 0 0.006 ^ 20

Peaches 285 0 0.005 ^ 20

Plums 507 0 0.010 ^ 15

Raspberries 652 0 0.010 - 0.020 NT

Raspberries, Frozen 53 0 0.010 - 0.020 NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 - 0.020 NT

TOTAL 7,800 287

Dicofol Total (insecticide) 

Green Beans 378 0 0.15 ^ 3.0

Nectarines 543 0 0.003 ^ 5.0

Summer Squash 346 0 0.15 ^ 2.0

TOTAL 1,267 0

Appendix B. Page 19 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Dicofol o,p' (isomer of Dicofol) 

Bananas 708 0 0.015 ^ NT

Cauliflower 532 0 0.002 ^ NT

Celery 708 0 0.002 - 0.010 NT

Plums 507 0 0.010 ^ 5.0

Raspberries 652 0 0.010 - 0.015 5.0

Raspberries, Frozen 53 0 0.010 - 0.015 5.0

Summer Squash 363 0 0.010 ^ 2.0

TOTAL 3,523 0

Dicofol p,p' (isomer of Dicofol) 

Apple Juice 379 0 0.010 ^ 10.0

Bananas 708 0 0.024 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.005 NT

Grape Juice 176 0 0.010 ^ 5.0

Mushrooms 532 0 0.010 ^ NT

Peaches 269 0 0.005 ^ 5.0

Plums 507 0 0.005 ^ 5.0

Raspberries 652 0 0.005 - 0.024 5.0

Raspberries, Frozen 53 0 0.005 - 0.024 5.0

Summer Squash 363 0 0.005 ^ 2.0

Winter Squash 187 0 0.006 ^ 2.0

TOTAL 5,066 0

Dicrotophos (insecticide) 

Cauliflower 532 0 0.002 ^ NT

Celery 708 0 0.002 - 0.003 NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 2,658 0

Diethofencarb (fungicide) 

Celery 346 0 0.003 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

TOTAL 1,577 0

Difenoconazole (fungicide) 

Apple Juice 379 0 0.010 ^ 1.0

Baby Food - Applesauce 379 0 0.005 ^ 1.0

Bananas 708 0 0.005 ^ 0.2

Broccoli 708 1 0.1 0.019 ^ 0.005 ^ 1.9

Carrots 712 11 1.5 0.002 - 0.007 0.001 ^ 0.50

Cauliflower 532 0 0.003 ^ 1.9

Celery (V-2) 708 2 0.3 0.004 - 0.006 0.003 - 0.005 NT

Grape Juice 176 0 0.010 ^ 4.0

Green Beans 378 0 0.005 ^ NT

Nectarines 543 5 0.9 0.002 - 0.004 0.001 ^ 2.5

Peaches 285 6 2.1 0.007 - 0.038 0.005 ^ 2.5

Plums 507 0 0.005 ^ 2.5

Raspberries (V-1) 652 1 0.2 0.098 ^ 0.005 ^ NT

Raspberries, Frozen 53 0 0.005 ^ NT

Summer Squash 709 3 0.4 0.005 - 0.009 0.005 ^ 0.70

Winter Squash 187 0 0.003 ^ 0.70

TOTAL 7,616 29

Diflubenzuron (insecticide) 

Apple Juice 379 0 0.003 ^ NT

Bananas 708 0 0.15 ^ NT

Appendix B. Page 20 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Carrots 712 0 0.002 ^ NT

Cauliflower 516 0 0.002 ^ NT

Celery 708 0 0.002 - 0.020 NT

Grape Juice 176 0 0.003 ^ NT

Mushrooms 532 0 0.003 ^ 0.2

Nectarines 543 2 0.4 0.005 ^ 0.003 ^ 0.07

Plums 507 0 0.020 ^ 0.07

Raspberries 652 0 0.020 - 0.15 NT

Raspberries, Frozen 53 0 0.020 - 0.15 NT

Summer Squash 363 0 0.020 ^ NT

Winter Squash 187 0 0.012 ^ NT

TOTAL 6,036 2

Dimethenamid (herbicide) 

Apple Juice 379 0 0.003 ^ NT

Bananas 708 0 0.007 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.003 NT

Grape Juice 176 0 0.003 ^ NT

Mushrooms 532 0 0.003 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.003 - 0.007 NT

Raspberries, Frozen 53 0 0.003 - 0.007 NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ 0.01

TOTAL 4,797 0

Dimethoate (insecticide) (parent of Omethoate)

Apple Juice 379 0 0.005 ^ NT

Baby Food - Applesauce 379 0 0.010 ^ NT

Baby Food - Peas 378 0 0.010 ^ 2.0

Bananas 708 0 0.005 ^ NT

Broccoli 708 4 0.6 0.011 - 0.21 0.010 ^ 2.0

Cauliflower 532 2 0.4 0.004 - 0.036 0.002 ^ 2.0

Celery 708 30 4.2 0.003 - 0.21 0.002 - 0.003 2.0

Grape Juice 176 0 0.005 ^ NT

Green Beans 378 20 5.3 0.001 - 0.63 0.001 ^ 2.0

Mushrooms 532 0 0.005 ^ NT

Nectarines (V-1) 543 1 0.2 0.005 ^ 0.003 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.003 - 0.005 NT

Raspberries, Frozen 53 0 0.003 - 0.005 NT

Summer Squash 709 0 0.003 - 0.010 NT

Winter Squash (V-1) 187 1 0.5 0.021 ^ 0.002 ^ NT

TOTAL 7,814 58

Dimethomorph (fungicide) 

Apple Juice 379 0 0.003 ^ NT

Baby Food - Applesauce 379 0 0.010 ^ NT

Broccoli 708 3 0.4 0.018 - 0.067 0.010 ^ 6.0

Cauliflower 532 1 0.2 0.002 ^ 0.001 ^ 6.0

Celery 708 8 1.1 0.002 - 0.004 0.001 - 0.005 30.0

Grape Juice 176 0 0.003 ^ 3.0

Green Beans (V-1) 378 1 0.3 0.036 ^ 0.001 ^ NT

Mushrooms 502 0 0.003 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 709 1 0.1 0.020 ^ 0.005 - 0.010 0.5

Winter Squash 187 1 0.5 0.005 ^ 0.003 ^ 0.5

TOTAL 5,811 15

Diniconazole (fungicide) 

Celery 346 0 0.020 ^ NT

Plums 507 0 0.020 ^ NT

Appendix B. Page 21 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Raspberries 351 0 0.020 ^ NT

Raspberries, Frozen 10 0 0.020 ^ NT

Summer Squash 363 0 0.020 ^ NT

TOTAL 1,577 0

Dinotefuran (insecticide) 

Apple Juice 379 1 0.3 0.011 ^ 0.003 ^ 1.0

Bananas 708 0 0.015 ^ 0.01

Cauliflower 532 0 0.006 ^ 1.4

Celery 708 23 3.2 0.010 - 0.071 0.006 - 0.020 5.0

Grape Juice 176 0 0.003 ^ 0.9

Green Beans (X-2) 378 2 0.5 0.17 ^ 0.040 ^ 0.01

Mushrooms 532 0 0.003 ^ 0.01

Nectarines 543 1 0.2 0.10 ^ 0.060 ^ 1.0

Plums 507 0 0.010 ^ 1.0

Raspberries 652 0 0.010 - 0.015 NT

Raspberries, Frozen 53 0 0.010 - 0.015 NT

Summer Squash 709 33 4.7 0.010 - 0.40 0.010 - 0.10 0.5

Winter Squash 187 4 2.1 0.010 - 0.043 0.006 ^ 0.5

TOTAL 6,064 64

Dioxacarb (insecticide) 

Nectarines 543 0 0.004 ^ NT

TOTAL 543 0

Dioxathion (insecticide) 

Celery 346 0 0.020 ^ NT

Plums 453 0 0.020 - 0.040 NT

Raspberries 351 0 0.020 ^ NT

Raspberries, Frozen 10 0 0.020 ^ NT

Summer Squash 363 0 0.020 ^ NT

Winter Squash 187 0 0.012 ^ NT

TOTAL 1,710 0

Diphenamid (herbicide) 

Baby Food - Applesauce 357 0 0.001 ^ NT

Broccoli 707 0 0.005 ^ NT

Cauliflower 532 0 0.002 ^ NT

Celery 362 0 0.002 ^ NT

Peaches 285 0 0.005 ^ NT

TOTAL 2,243 0

Diphenylamine - DPA (plant growth regulator) 

Apple Juice 379 67 17.7 0.002 - 0.066 0.002 ^ 10.0

Baby Food - Applesauce 379 10 2.6 0.005 - 0.035 0.005 ^ 10.0

Bananas 708 0 0.060 ^ NT

Broccoli 707 0 0.005 ^ NT

Cauliflower 532 0 0.003 ^ NT

Celery 708 0 0.003 ^ NT

Grape Juice 176 0 0.002 ^ NT

Mushrooms 532 0 0.002 ^ NT

Peaches (V-1) 285 1 0.4 0.007 ^ 0.005 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.003 - 0.060 NT

Raspberries, Frozen 53 0 0.003 - 0.060 NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 6,168 78

Disulfoton (insecticide) 

Apple Juice 33 0 0.010 ^ NT

Baby Food - Applesauce 379 0 0.001 ^ NT

Bananas 708 0 0.050 ^ NT

Broccoli 707 0 0.005 ^ 0.75

Cauliflower 532 0 0.002 ^ 0.75

Celery 708 0 0.002 - 0.010 NT

Appendix B. Page 22 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Mushrooms 31 0 0.010 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.010 - 0.050 NT

Raspberries, Frozen 53 0 0.010 - 0.050 NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 5,145 0

Disulfoton oxon (metabolite of Disulfoton)

Apple Juice 379 0 0.001 ^ NT

Bananas 708 0 0.002 ^ NT

Cauliflower 532 0 0.002 ^ 0.75

Celery 362 0 0.002 ^ NT

Grape Juice 176 0 0.001 ^ NT

Green Beans 378 0 0.001 ^ 0.75

Mushrooms 532 0 0.001 ^ NT

Raspberries 301 0 0.002 ^ NT

Raspberries, Frozen 43 0 0.002 ^ NT

TOTAL 3,411 0

Disulfoton sulfone (metabolite of Disulfoton)

Apple Juice 379 0 0.020 ^ NT

Baby Food - Applesauce 379 0 0.010 ^ NT

Bananas 708 0 0.010 ^ NT

Broccoli 708 0 0.050 ^ 0.75

Cauliflower 532 0 0.002 ^ 0.75

Celery 708 0 0.002 - 0.003 NT

Grape Juice 148 0 0.020 ^ NT

Mushrooms 532 0 0.020 ^ NT

Peaches 285 0 0.050 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.003 - 0.010 NT

Raspberries, Frozen 53 0 0.003 - 0.010 NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 6,141 0

Disulfoton sulfone oxygen analog (metabolite of Disulfoton)

Bananas 708 0 0.010 ^ NT

Cauliflower 532 0 0.001 - 0.006 0.75

Celery 362 0 0.001 - 0.006 NT

Green Beans 378 0 0.005 ^ 0.75

Raspberries 301 0 0.010 ^ NT

Raspberries, Frozen 43 0 0.010 ^ NT

TOTAL 2,324 0

Disulfoton sulfoxide (metabolite of Disulfoton)

Apple Juice 379 0 0.005 ^ NT

Bananas 708 0 0.005 ^ NT

Cauliflower 532 0 0.002 - 0.006 0.75

Celery 708 0 0.002 - 0.003 NT

Grape Juice 176 0 0.005 ^ NT

Green Beans 378 0 0.001 ^ 0.75

Mushrooms 532 0 0.005 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.003 - 0.005 NT

Raspberries, Frozen 53 0 0.003 - 0.005 NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 5,175 0

Disulfoton sulfoxide oxygen analog (metabolite of Disulfoton)

Bananas 708 0 0.010 ^ NT

Cauliflower 532 0 0.001 - 0.003 0.75

Celery 362 0 0.001 - 0.003 NT

Appendix B. Page 23 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Green Beans 378 0 0.001 ^ 0.75

Raspberries 301 0 0.010 ^ NT

Raspberries, Frozen 43 0 0.010 ^ NT

TOTAL 2,324 0

Diuron (herbicide) 

Apple Juice 379 0 0.003 ^ 0.1

Baby Food - Peas 378 0 0.10 ^ 0.1

Bananas 708 0 0.030 ^ 0.1

Cauliflower 532 0 0.008 - 0.025 NT

Celery 708 0 0.008 - 0.020 NT

Grape Juice 148 0 0.003 ^ 0.05

Green Beans 378 0 0.010 ^ NT

Mushrooms 532 0 0.003 ^ NT

Nectarines 543 0 0.020 ^ NT

Plums 507 0 0.020 ^ NT

Raspberries 652 0 0.020 - 0.030 0.1

Raspberries, Frozen 53 0 0.020 - 0.030 0.1

Summer Squash 363 0 0.020 ^ NT

Winter Squash 187 0 0.012 ^ NT

TOTAL 6,068 0

DMST (4-dimethylaminosulphotosluidide) (metabolite of Tolyfluanid)

Celery 346 0 0.003 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

TOTAL 1,577 0

Dodine (fungicide) 

Apple Juice 379 0 0.010 ^ 5.0

Celery 346 0 0.020 ^ NT

Grape Juice 148 0 0.010 ^ NT

Nectarines 453 0 0.015 ^ 5.0

Plums 507 0 0.020 ^ 5.0

Raspberries 351 0 0.020 ^ NT

Raspberries, Frozen 10 0 0.020 ^ NT

Summer Squash 363 0 0.020 ^ NT

Winter Squash 187 0 0.012 ^ NT

TOTAL 2,744 0

Emamectin (insecticide) 

Celery 346 0 0.010 ^ 0.100

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ 0.02

Winter Squash 187 0 0.006 ^ 0.02

TOTAL 1,764 0

Emamectin benzoate 1

 (insecticide) 

Apple Juice 379 0 0.010 ^ 0.025

Cauliflower 532 0 0.001 ^ 0.050

Celery 362 0 0.001 ^ 0.100

Grape Juice 176 0 0.010 ^ 0.03

TOTAL 1,449 0

Endosulfan I (insecticide) 

Apple Juice 379 0 0.010 ^ 1.0

Baby Food - Applesauce 357 0 0.001 ^ 1.0

Bananas 708 0 0.030 ^ NT

Broccoli 707 0 0.005 ^ 3.0

Carrots 712 0 0.004 ^ 0.2

Cauliflower 532 0 0.006 ^ 2.0

Celery 708 3 0.4 0.010 - 0.067 0.006 - 0.010 8.0

Appendix B. Page 24 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Grape Juice 176 0 0.010 ^ NT

Green Beans 378 1 0.3 0.19 ^ 0.12 ^ 2.0

Mushrooms 532 0 0.010 ^ NT

Nectarines 543 0 0.004 ^ 2.0

Peaches 285 0 0.005 ^ 2.0

Plums 507 0 0.010 ^ 2.0

Raspberries 652 0 0.010 - 0.030 NT

Raspberries, Frozen 53 0 0.010 - 0.030 NT

Summer Squash 709 6 0.8 0.011 - 0.039 0.010 - 0.25 1.0

Winter Squash 187 1 0.5 0.010 ^ 0.006 ^ 1.0

TOTAL 8,125 11

Endosulfan II (isomer of Endosulfan)

Apple Juice 379 0 0.015 ^ 1.0

Baby Food - Applesauce 357 0 0.001 ^ 1.0

Bananas 708 0 0.042 ^ NT

Broccoli 707 0 0.005 ^ 3.0

Carrots 712 0 0.010 ^ 0.2

Cauliflower 532 0 0.001 - 0.004 2.0

Celery 708 4 0.6 0.002 - 0.067 0.001 - 0.010 8.0

Grape Juice 176 0 0.015 ^ NT

Green Beans 378 2 0.5 0.043 - 0.085 0.025 ^ 2.0

Mushrooms 502 0 0.015 ^ NT

Nectarines 543 0 0.010 ^ 2.0

Peaches 285 1 0.4 0.011 ^ 0.005 ^ 2.0

Plums 507 0 0.010 ^ 2.0

Raspberries 652 0 0.010 - 0.042 NT

Raspberries, Frozen 53 0 0.010 - 0.042 NT

Summer Squash 709 0 0.010 - 0.050 1.0

Winter Squash 187 1 0.5 0.015 ^ 0.009 ^ 1.0

TOTAL 8,095 8

Endosulfan sulfate (metabolite of Endosulfan)

Apple Juice 379 0 0.005 ^ 1.0

Baby Food - Applesauce 379 1 0.3 0.002 ^ 0.001 ^ 1.0

Bananas 708 0 0.020 ^ NT

Broccoli 707 1 0.1 0.011 ^ 0.005 ^ 3.0

Carrots 712 5 0.7 0.003 - 0.010 0.002 ^ 0.2

Cauliflower 532 0 0.004 - 0.012 2.0

Celery 708 2 0.3 0.008 - 0.028 0.005 - 0.012 8.0

Grape Juice 146 0 0.005 ^ NT

Green Beans 378 2 0.5 0.14 - 0.23 0.025 ^ 2.0

Mushrooms 532 0 0.005 ^ NT

Nectarines 543 0 0.002 ^ 2.0

Peaches 285 1 0.4 0.024 ^ 0.005 ^ 2.0

Plums 507 0 0.005 ^ 2.0

Raspberries 652 0 0.005 - 0.020 NT

Raspberries, Frozen 53 0 0.005 - 0.020 NT

Summer Squash 709 124 17.5 0.005 - 0.12 0.005 - 0.050 1.0

Winter Squash 187 33 17.6 0.005 - 0.070 0.003 ^ 1.0

TOTAL 8,117 169

Epoxiconazole (fungicide) 

Celery 346 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

TOTAL 1,577 0

EPTC (herbicide) 

Apple Juice 99 0 0.010 ^ NT

Baby Food - Peas 378 0 0.005 ^ 0.08

Bananas 708 0 0.035 ^ NT

Carrots 712 1 0.1 0.007 ^ 0.004 ^ 0.1

Cauliflower 532 0 0.006 ^ NT

Appendix B. Page 25 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Celery 362 0 0.001 - 0.006 NT

Green Beans 378 4 1.1 0.001 - 0.009 0.001 ^ 0.08

Mushrooms 124 0 0.010 ^ NT

Raspberries 301 0 0.035 ^ NT

Raspberries, Frozen 43 0 0.035 ^ NT

TOTAL 3,637 5

Esfenvalerate+Fenvalerate Total (insecticide) 

Apple Juice 379 0 0.005 ^ 1.0

Baby Food - Applesauce 379 0 0.001 ^ 1.0

Baby Food - Peas 378 0 0.075 ^ 0.5

Broccoli 707 7 1 0.008 - 0.089 0.005 ^ 1.0

Cauliflower 532 0 0.008 ^ 0.5

Celery 708 1 0.1 0.018 ^ 0.002 - 0.008 0.05

Grape Juice 176 0 0.005 ^ 0.05

Green Beans 378 3 0.8 0.083 - 0.10 0.075 ^ 1.0

Mushrooms 532 0 0.005 ^ 0.05

Peaches 285 33 11.6 0.005 - 0.13 0.005 ^ 3.0

Plums 507 2 0.4 0.007 - 0.010 0.005 ^ 3.0

Raspberries 351 0 0.005 ^ 1.0

Raspberries, Frozen 10 0 0.005 ^ 1.0

Summer Squash 709 0 0.005 - 0.075 0.5

Winter Squash 187 0 0.008 ^ 0.5

TOTAL 6,218 46

Esfenvalerate (isomer of Fenvalerate)

Bananas 708 0 0.035 ^ 0.05

Carrots 712 0 0.015 ^ 0.5

Nectarines 543 19 3.5 0.025 ^ 0.015 ^ 3.0

Raspberries 301 0 0.035 ^ 1.0

Raspberries, Frozen 43 0 0.035 ^ 1.0

TOTAL 2,307 19

Ethalfluralin (herbicide) 

Apple Juice 379 0 0.005 ^ NT

Baby Food - Peas 378 0 0.025 ^ NT

Bananas 708 0 0.010 ^ NT

Cauliflower 532 0 0.002 ^ NT

Celery 708 0 0.002 - 0.005 NT

Grape Juice 176 0 0.005 ^ NT

Green Beans 378 0 0.010 ^ NT

Mushrooms 532 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.005 - 0.010 NT

Raspberries, Frozen 53 0 0.005 - 0.010 NT

Summer Squash 709 0 0.005 - 0.020 0.05

Winter Squash 187 0 0.006 ^ 0.05

TOTAL 5,899 0

Ethiofencarb (insecticide) 

Baby Food - Applesauce 379 0 0.010 ^ NT

Broccoli 708 0 0.010 ^ NT

Cauliflower 532 0 0.002 ^ NT

Celery 30 0 0.002 ^ NT

Peaches 285 0 0.010 ^ NT

TOTAL 1,934 0

Ethion (insecticide) 

Apple Juice 379 0 0.001 ^ NT

Baby Food - Applesauce 379 0 0.010 ^ NT

Bananas 708 0 0.007 ^ NT

Broccoli 708 0 0.010 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.003 NT

Grape Juice 176 0 0.001 ^ NT

Peaches 285 0 0.010 ^ NT

Appendix B. Page 26 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.003 - 0.007 NT

Raspberries, Frozen 53 0 0.003 - 0.007 NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 5,637 0

Ethion mono oxon (metabolite of Ethion)

Apple Juice 379 0 0.001 ^ NT

Cauliflower 532 0 0.002 ^ NT

Celery 708 0 0.002 - 0.003 NT

Grape Juice 176 0 0.001 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 3,213 0

Ethofumesate (herbicide) 

Bananas 708 0 0.005 ^ NT

Carrots 712 2 0.3 0.025 ^ 0.015 ^ 7.0

Celery 346 0 0.003 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.003 - 0.005 NT

Raspberries, Frozen 53 0 0.003 - 0.005 NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 3,528 2

Ethoprop (insecticide) 

Apple Juice 379 0 0.002 ^ NT

Baby Food - Applesauce 379 0 0.010 ^ NT

Bananas 708 8 1.1 0.002 - 0.015 0.002 ^ 0.02

Broccoli 708 0 0.010 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.003 NT

Grape Juice 28 0 0.002 ^ NT

Green Beans 378 0 0.001 ^ 0.02

Mushrooms 532 0 0.002 ^ NT

Nectarines 543 0 0.001 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.002 - 0.003 NT

Raspberries, Frozen 53 0 0.002 - 0.003 NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 6,942 8

Ethylan (insecticide) 

Celery 346 0 0.003 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

TOTAL 1,577 0

Etofenprox (insecticide) 

Celery 346 0 0.003 ^ NT

Grape Juice 176 0 0.025 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

TOTAL 1,753 0

Appendix B. Page 27 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Etoxazole (acaricide) 

Apple Juice 349 0 0.005 ^ 0.20

Baby Food - Applesauce 379 0 0.004 ^ 0.20

Broccoli 708 0 0.004 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.003 NT

Grape Juice 176 0 0.005 ^ 0.50

Green Beans 378 0 0.001 ^ NT

Nectarines 543 4 0.7 0.002 - 0.012 0.001 ^ 1.0

Peaches 285 8 2.8 0.004 - 0.010 0.004 ^ 1.0

Plums 507 0 0.003 ^ 0.15

Raspberries 351 14 4 0.003 - 0.23 0.003 ^ 1.5

Raspberries, Frozen 10 0 0.003 ^ 1.5

Summer Squash 709 0 0.003 - 0.005 0.02

Winter Squash 187 0 0.002 ^ 0.02

TOTAL 5,822 26

Etridiazole (fungicide) 

Baby Food - Applesauce 379 0 0.001 ^ NT

Baby Food - Peas 378 0 0.10 ^ 0.1

Bananas 708 0 0.010 ^ NT

Broccoli 687 0 0.005 ^ NT

Green Beans 378 0 0.30 ^ 0.1

Peaches 285 0 0.005 ^ NT

Raspberries 301 0 0.010 ^ NT

Raspberries, Frozen 43 0 0.010 ^ NT

TOTAL 3,159 0

Famoxadone (fungicide) 

Apple Juice 379 0 0.025 ^ NT

Bananas 708 0 0.033 ^ NT

Cauliflower 483 0 0.003 ^ NT

Celery 692 0 0.003 - 0.010 25

Grape Juice 176 0 0.025 ^ 2.5

Mushrooms 503 0 0.025 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.010 - 0.033 10

Raspberries, Frozen 53 0 0.010 - 0.033 10

Summer Squash 709 1 0.1 0.023 ^ 0.010 - 0.050 0.30

Winter Squash 187 1 0.5 0.028 ^ 0.006 ^ 0.30

TOTAL 5,049 2

Fenamidone (fungicide) 

Apple Juice 379 0 0.005 ^ NT

Bananas 708 0 0.060 ^ NT

Carrots 712 0 0.020 ^ 0.15

Cauliflower 532 0 0.002 ^ 5.0

Celery 708 11 1.6 0.004 - 0.070 0.002 - 0.010 60

Grape Juice 176 0 0.005 ^ 1.0

Green Beans (V-1) 378 1 0.3 0.001 ^ 0.001 ^ NT

Mushrooms 503 0 0.005 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.010 - 0.060 NT

Raspberries, Frozen 53 0 0.010 - 0.060 NT

Summer Squash 709 0 0.010 - 0.050 0.15

Winter Squash 187 0 0.006 ^ 0.15

TOTAL 6,204 12

Fenamiphos (insecticide) 

Baby Food - Applesauce 379 0 0.005 ^ NT

Bananas 708 0 0.020 ^ 0.1

Broccoli 708 0 0.005 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.003 NT

Grape Juice 176 0 0.050 ^ 0.1

Peaches 285 0 0.005 ^ NT

Appendix B. Page 28 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.003 - 0.020 NT

Raspberries, Frozen 53 0 0.003 - 0.020 NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 5,258 0

Fenamiphos sulfone (metabolite of Fenamiphos)

Baby Food - Applesauce 379 0 0.005 ^ NT

Bananas 708 0 0.004 ^ 0.1

Broccoli 708 0 0.005 ^ NT

Cauliflower 532 0 0.004 ^ NT

Celery 708 0 0.004 - 0.005 NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.004 - 0.005 NT

Raspberries, Frozen 53 0 0.004 - 0.005 NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 5,082 0

Fenamiphos sulfoxide (metabolite of Fenamiphos)

Baby Food - Applesauce 379 0 0.005 ^ NT

Bananas 708 0 0.004 ^ 0.1

Broccoli 708 0 0.005 ^ NT

Cauliflower 532 0 0.004 ^ NT

Celery 708 0 0.004 - 0.020 NT

Grape Juice 176 0 0.050 ^ 0.1

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.020 ^ NT

Raspberries 652 0 0.004 - 0.020 NT

Raspberries, Frozen 53 0 0.004 - 0.020 NT

Summer Squash 363 0 0.020 ^ NT

Winter Squash 187 0 0.012 ^ NT

TOTAL 5,258 0

Fenarimol (fungicide) 

Baby Food - Applesauce 379 0 0.001 ^ 0.3

Bananas 708 0 0.013 ^ 0.25

Broccoli 707 0 0.005 ^ NT

Cauliflower 532 0 0.002 ^ NT

Celery 708 0 0.002 - 0.003 NT

Green Beans 378 0 0.005 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.003 - 0.013 NT

Raspberries, Frozen 53 0 0.003 - 0.013 NT

Summer Squash 709 0 0.003 - 0.025 0.20

Winter Squash 187 0 0.008 ^ 0.20

TOTAL 5,805 0

Fenazaquin (insecticide, acaricide)

Apple Juice 379 0 0.005 ^ 0.2

Celery 346 0 0.003 ^ NT

Grape Juice 176 0 0.005 ^ NT

Mushrooms 501 0 0.005 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

TOTAL 2,633 0

Fenbuconazole (fungicide) 

Apple Juice 379 0 0.005 ^ 0.4

Baby Food - Applesauce 379 1 0.3 0.006 ^ 0.005 ^ 0.4

Bananas 708 0 0.005 ^ 0.3

Appendix B. Page 29 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Broccoli 708 0 0.005 ^ NT

Cauliflower (V-1) 532 1 0.2 0.002 ^ 0.001 ^ NT

Celery 708 0 0.001 - 0.010 NT

Grape Juice 176 0 0.005 ^ 1.0

Mushrooms 532 0 0.005 ^ NT

Nectarines 543 24 4.4 0.003 - 0.10 0.002 ^ 1.0

Peaches 285 65 22.8 0.005 - 0.19 0.005 ^ 1.0

Plums 507 0 0.010 ^ 1.0

Raspberries 652 0 0.005 - 0.010 NT

Raspberries, Frozen 53 0 0.005 - 0.010 NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash (V-2) 187 2 1.1 0.010 ^ 0.006 ^ NT

TOTAL 6,712 93

Fenbutatin oxide (insecticide, acaricide)

Nectarines 543 0 0.012 ^ NT

TOTAL 543 0

Fenchlorphos (insecticide) 

Celery 346 0 0.003 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 1,764 0

Fenhexamid (fungicide) 

Apple Juice 379 0 0.013 ^ NT

Bananas 708 0 0.011 ^ NT

Cauliflower 532 0 0.010 ^ NT

Celery 376 0 0.009 - 0.040 NT

Grape Juice 176 11 6.2 0.020 - 0.082 0.013 ^ 4.0

Green Beans 378 0 0.002 ^ NT

Mushrooms 532 0 0.013 ^ NT

Nectarines 543 63 11.6 0.008 - 0.98 0.005 ^ 10.0

Plums 507 19 3.7 0.040 - 0.52 0.040 ^ 1.5

Raspberries 652 12 1.8 0.013 - 0.72 0.011 - 0.040 20.0

Raspberries, Frozen 53 9 17 0.015 - 0.69 0.011 - 0.040 20.0

Summer Squash 709 0 0.010 - 0.040 NT

Winter Squash 187 0 0.024 ^ NT

TOTAL 5,732 114

Fenitrothion (insecticide) 

Cauliflower 532 0 0.010 - 0.020 NT

Celery 708 0 0.003 - 0.020 NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 2,658 0

Fenobucarb - BPMC (insecticide) 

Celery 346 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 1,764 0

Fenpropathrin (insecticide) 

Apple Juice 379 0 0.020 ^ 5.0

Baby Food - Applesauce 379 25 6.6 0.002 ^ 0.001 ^ 5.0

Baby Food - Peas 378 0 0.12 ^ 0.02

Appendix B. Page 30 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Bananas 708 0 0.020 ^ NT

Broccoli 707 0 0.005 ^ 3.0

Carrots 712 0 0.003 ^ NT

Cauliflower 486 0 0.003 ^ 3.0

Celery 708 0 0.003 - 0.005 NT

Grape Juice 176 0 0.020 ^ 5.0

Green Beans (V-1) 378 1 0.3 0.067 ^ 0.050 ^ NT

Mushrooms 532 0 0.020 ^ NT

Nectarines 543 14 2.6 0.005 - 0.16 0.003 ^ 1.4

Peaches 285 26 9.1 0.006 - 1.0 0.005 ^ 1.4

Plums 507 5 1 0.012 - 0.026 0.005 ^ 1.4

Raspberries 652 1 0.2 0.043 ^ 0.005 - 0.020 12

Raspberries, Frozen 53 0 0.005 - 0.020 12

Summer Squash 709 0 0.005 - 0.10 0.5

Winter Squash 187 1 0.5 0.020 ^ 0.012 ^ 0.5

TOTAL 8,479 73

Fenpropimorph (fungicide) 

Apple Juice 379 0 0.001 ^ NT

Baby Food - Applesauce 379 0 0.010 ^ NT

Broccoli 708 0 0.010 ^ NT

Celery 346 0 0.003 ^ NT

Grape Juice 176 0 0.001 ^ NT

Peaches 269 0 0.010 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

TOTAL 3,488 0

Fenpyroximate (acaricide) 

Apple Juice 379 0 0.005 ^ 0.30

Baby Food - Applesauce 379 0 0.010 ^ 0.30

Broccoli 708 0 0.010 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery 362 0 0.001 - 0.003 NT

Grape Juice 176 0 0.005 ^ 1.0

Mushrooms 532 0 0.005 ^ NT

Nectarines 543 2 0.4 0.002 - 0.009 0.001 ^ 2.0

Peaches 285 0 0.010 ^ 2.0

TOTAL 3,896 2

Fensulfothion (insecticide, fumigant)

Celery 346 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 1,764 0

Fenthion (insecticide) 

Baby Food - Applesauce 379 0 0.001 ^ NT

Bananas 708 0 0.015 ^ NT

Broccoli 707 0 0.005 ^ NT

Cauliflower 532 0 0.002 ^ NT

Celery 708 0 0.002 - 0.003 NT

Grape Juice 176 0 0.010 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.003 - 0.015 NT

Raspberries, Frozen 53 0 0.003 - 0.015 NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 5,257 0

Appendix B. Page 31 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Fenthion oxygen analog sulfone (metabolite of Fenthion)

Bananas 708 0 0.007 ^ NT

Grape Juice 146 0 0.15 ^ NT

Raspberries 301 0 0.007 ^ NT

Raspberries, Frozen 43 0 0.007 ^ NT

TOTAL 1,198 0

Fenthion oxygen analog sulfoxide (metabolite of Fenthion)

Bananas 708 0 0.007 ^ NT

Grape Juice 176 0 0.050 ^ NT

Raspberries 301 0 0.007 ^ NT

Raspberries, Frozen 43 0 0.007 ^ NT

TOTAL 1,228 0

Fenthion sulfone (metabolite of Fenthion)

Bananas 708 0 0.030 ^ NT

Grape Juice 146 0 0.075 ^ NT

Raspberries 301 0 0.030 ^ NT

Raspberries, Frozen 43 0 0.030 ^ NT

TOTAL 1,198 0

Fenthion sulfoxide (metabolite of Fenthion)

Bananas 708 0 0.010 ^ NT

Grape Juice 146 0 0.020 ^ NT

Raspberries 301 0 0.010 ^ NT

Raspberries, Frozen 43 0 0.010 ^ NT

TOTAL 1,198 0

Fenuron (herbicide) 

Carrots 712 0 0.005 ^ NT

Nectarines 543 0 0.025 ^ NT

TOTAL 1,255 0

Fipronil (insecticide) 

Baby Food - Applesauce 379 0 0.001 ^ NT

Bananas 708 0 0.010 ^ NT

Broccoli 707 0 0.005 ^ NT

Celery 318 0 0.002 - 0.010 NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 591 0 0.010 ^ NT

Raspberries, Frozen 53 0 0.010 ^ NT

Summer Squash 303 0 0.010 ^ NT

TOTAL 3,851 0

Fipronil sulfone - MB46136 (metabolite of Fipronil)

Apple Juice 379 0 0.050 ^ NT

Grape Juice 176 0 0.050 ^ NT

TOTAL 555 0

Flonicamid (insecticide) 

Apple Juice 379 0 0.006 ^ 0.20

Baby Food - Applesauce 379 0 0.010 ^ 0.20

Bananas 708 0 0.005 ^ NT

Broccoli 708 1 0.1 0.11 ^ 0.010 ^ 1.5

Carrots 712 0 0.004 ^ 0.60

Cauliflower 532 7 1.3 0.002 - 0.007 0.001 ^ 1.5

Celery 708 69 9.7 0.002 - 0.10 0.001 - 0.030 4.0

Grape Juice 148 0 0.006 ^ NT

Green Beans 378 0 0.10 ^ NT

Mushrooms 532 0 0.006 ^ NT

Nectarines 543 0 0.010 ^ 0.60

Peaches 285 0 0.010 ^ 0.60

Plums 507 0 0.030 ^ 0.60

Raspberries 652 0 0.005 - 0.030 NT

Raspberries, Frozen 53 0 0.005 - 0.030 NT

Appendix B. Page 32 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Summer Squash 709 10 1.4 0.032 - 0.14 0.030 - 0.10 0.4

Winter Squash 187 0 0.018 ^ 0.4

TOTAL 8,120 87

Fluazifop butyl (herbicide) 

Carrots 712 0 0.001 ^ 2.0

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.003 NT

Nectarines 543 0 0.001 ^ 0.05

Plums 507 0 0.003 ^ 0.05

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 3,913 0

Fluazinam (fungicide) 

Carrots 712 0 0.010 ^ 0.70

TOTAL 712 0

Flubendiamide (insecticide) 

Apple Juice 379 0 0.035 ^ 1.5

Baby Food - Peas 378 0 0.005 ^ 0.05

Celery 346 3 0.9 0.006 - 0.008 0.005 ^ 11

Grape Juice 176 0 0.035 ^ 1.4

Green Beans 378 5 1.3 0.004 - 0.11 0.003 ^ 0.50

Mushrooms 532 0 0.035 ^ NT

Nectarines 541 23 4.3 0.005 - 0.081 0.003 ^ 1.6

Plums 453 6 1.3 0.007 - 0.017 0.005 ^ 1.6

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 709 3 0.4 0.005 - 0.016 0.005 ^ 0.20

Winter Squash 187 0 0.003 ^ 0.20

TOTAL 4,440 40

Fludioxonil (fungicide) 

Apple Juice 379 0 0.025 ^ 5.0

Baby Food - Applesauce 357 5 1.4 0.002 - 0.013 0.001 ^ 5.0

Baby Food - Peas 378 0 0.015 ^ 0.01

Bananas 708 0 0.015 ^ NT

Broccoli 707 0 0.005 ^ 2.0

Carrots 712 0 0.008 - 0.027 0.75

Cauliflower 532 0 0.012 ^ 2.0

Celery 708 0 0.010 - 0.012 15

Grape Juice 176 0 0.025 ^ 2.0

Green Beans 378 0 0.050 ^ 0.4

Mushrooms 532 0 0.025 ^ NT

Nectarines 271 213 78.6 0.033 - 3.4 0.020 ^ 5.0

Peaches 285 218 76.5 0.006 - 2.4 0.005 ^ 5.0

Plums 507 225 44.4 0.012 - 1.7 0.010 ^ 5.0

Raspberries 652 42 6.4 0.011 - 0.56 0.010 - 0.015 5.0

Raspberries, Frozen 53 9 17 0.023 - 0.51 0.010 - 0.015 5.0

Summer Squash 709 1 0.1 0.011 ^ 0.010 - 0.060 0.45

Winter Squash 187 0 0.006 ^ 0.45

TOTAL 8,231 713

Flufenoxuron (insecticide) 

Apple Juice 379 0 0.002 ^ 0.50

Celery 346 0 0.010 ^ NT

Grape Juice 176 0 0.002 ^ 0.70

Mushrooms 532 0 0.002 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

TOTAL 2,664 0

Appendix B. Page 33 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Flumioxazin (herbicide) 

Apple Juice 379 0 0.010 ^ 0.02

Bananas 708 0 0.020 ^ NT

Cauliflower 532 0 0.002 - 0.005 NT

Celery 362 0 0.002 - 0.010 0.02

Grape Juice 176 0 0.010 ^ 0.02

Green Beans 378 0 0.080 ^ NT

Nectarines 543 0 0.023 ^ 0.02

Raspberries 301 0 0.020 ^ NT

Raspberries, Frozen 43 0 0.020 ^ NT

Summer Squash 346 0 0.18 ^ 0.03

TOTAL 3,768 0

Fluopicolide (fungicide) 

Apple Juice 379 0 0.015 ^ NT

Bananas 708 0 0.007 ^ NT

Carrots 712 19 2.7 0.010 - 0.025 0.006 - 0.020 0.15

Cauliflower 516 0 0.002 ^ 5.0

Celery 708 18 2.5 0.003 - 0.009 0.002 - 0.003 25

Grape Juice 176 0 0.015 ^ 2.0

Green Beans (V-1) 378 1 0.3 0.007 ^ 0.002 ^ NT

Mushrooms 532 0 0.015 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.003 - 0.007 NT

Raspberries, Frozen 53 0 0.003 - 0.007 NT

Summer Squash 709 24 3.4 0.003 - 0.057 0.003 - 0.010 0.50

Winter Squash 187 5 2.7 0.003 - 0.008 0.002 ^ 0.50

TOTAL 6,217 67

Fluoxastrobin (fungicide) 

Baby Food - Applesauce 379 0 0.002 ^ NT

Bananas 708 0 0.025 ^ NT

Broccoli 708 0 0.002 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.003 4.0

Green Beans 378 0 0.001 ^ NT

Peaches 285 0 0.002 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.003 - 0.025 NT

Raspberries, Frozen 53 0 0.003 - 0.025 NT

Summer Squash 709 0 0.003 - 0.005 0.50

Winter Squash 187 0 0.002 ^ 0.50

TOTAL 5,806 0

Fluquinconazole (fungicide) 

Apple Juice 379 0 0.010 ^ NT

Celery 346 0 0.010 ^ NT

Grape Juice 176 0 0.010 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

TOTAL 2,132 0

Fluridone (herbicide) 

Apple Juice 379 0 0.001 ^ 0.1

Baby Food - Applesauce 379 0 0.010 ^ 0.1

Baby Food - Peas 378 0 0.005 ^ 0.1

Bananas 708 0 0.001 ^ NT

Broccoli 708 0 0.010 ^ 0.1

Carrots 712 0 0.001 ^ 0.1

Celery 346 0 0.003 ^ 0.1

Grape Juice 176 0 0.001 ^ 0.1

Green Beans 378 1 0.3 0.003 ^ 0.001 ^ 0.1

Mushrooms 532 0 0.001 ^ NT

Appendix B. Page 34 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Nectarines 543 0 0.001 ^ 0.1

Peaches 285 0 0.010 ^ 0.1

Plums 507 0 0.003 ^ 0.1

Raspberries 652 0 0.001 - 0.003 0.1

Raspberries, Frozen 53 0 0.001 - 0.003 0.1

Summer Squash 709 1 0.1 0.010 ^ 0.003 - 0.005 0.1

Winter Squash 187 0 0.002 ^ 0.1

TOTAL 7,632 2

Flusilazole (fungicide) 

Apple Juice 379 0 0.010 ^ NT

Baby Food - Applesauce 379 0 0.002 ^ NT

Bananas 708 0 0.008 ^ NT

Broccoli 707 0 0.010 ^ NT

Celery 346 0 0.003 ^ NT

Grape Juice 176 0 0.010 ^ NT

Mushrooms 532 0 0.010 ^ NT

Nectarines 543 0 0.003 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.003 - 0.008 NT

Raspberries, Frozen 53 0 0.003 - 0.008 NT

Summer Squash 363 0 0.003 ^ NT

TOTAL 5,630 0

Flutolanil (fungicide) 

Apple Juice 379 0 0.003 ^ NT

Celery 346 0 0.003 ^ NT

Grape Juice 176 0 0.003 ^ NT

Mushrooms 532 0 0.003 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 2,851 0

Flutriafol (fungicide) 

Apple Juice 379 0 0.010 ^ 0.40

Celery 346 0 0.010 ^ NT

Grape Juice 176 0 0.010 ^ 1.5

Plums 507 0 0.010 ^ 1.5

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ 0.30

TOTAL 2,132 0

Fluvalinate (insecticide) 

Apple Juice 379 0 0.050 ^ NT

Baby Food - Applesauce 357 0 0.001 ^ NT

Baby Food - Peas 378 0 0.30 ^ NT

Bananas 708 0 0.036 ^ NT

Broccoli 707 0 0.005 ^ NT

Carrots 712 0 0.007 ^ NT

Celery 346 0 0.010 ^ NT

Grape Juice 176 0 0.050 ^ NT

Green Beans 378 0 0.15 ^ NT

Mushrooms 532 0 0.050 ^ NT

Nectarines 543 0 0.007 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.010 - 0.036 NT

Raspberries, Frozen 53 0 0.010 - 0.036 NT

Summer Squash 709 0 0.010 - 0.30 NT

Winter Squash 187 0 0.012 ^ NT

TOTAL 7,609 0

Appendix B. Page 35 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Fluxapyroxad (fungicide) 

Green Beans 378 0 0.005 ^ 2.0

Nectarines 543 5 0.9 0.003 - 0.057 0.002 ^ 2.0

TOTAL 921 5

Folpet (fungicide) 

Apple Juice 379 0 0.030 ^ 5.0

Baby Food - Applesauce 357 0 0.003 ^ 5.0

Bananas 240 0 0.030 - 0.15 NT

Mushrooms 504 0 0.030 ^ NT

Nectarines 543 0 0.064 ^ NT

Peaches 285 0 0.015 ^ NT

TOTAL 2,308 0

Fonofos (insecticide) 

Baby Food - Applesauce 379 0 0.001 ^ NT

Broccoli 707 0 0.005 ^ NT

Cauliflower 532 0 0.002 ^ NT

Celery 708 0 0.002 - 0.003 NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 4,029 0

Forchlorfenuron (plant growth regulator) 

Baby Food - Applesauce 379 0 0.002 ^ NT

Celery 346 0 0.003 ^ NT

Nectarines 543 0 0.001 ^ NT

Peaches 220 0 0.010 ^ NT

Plums 507 0 0.003 ^ 0.01

Raspberries (V-3) 351 3 0.9 0.003 - 0.004 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 2,906 3

Formetanate hydrochloride (insecticide) 

Bananas 708 0 0.010 ^ NT

Celery 346 0 0.010 ^ NT

Nectarines 543 0 0.030 ^ 0.40

Peaches 285 1 0.4 0.010 ^ 0.010 ^ 0.40

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.010 ^ NT

Raspberries, Frozen 53 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 3,644 1

Fosthiazate (nematicide) 

Celery 346 0 0.003 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

TOTAL 1,577 0

Halosulfuron (herbicide) 

Baby Food - Peas 378 0 0.050 ^ 0.05

Bananas 708 0 0.099 - 0.50 NT

Green Beans 378 0 0.005 ^ NT

Raspberries 301 0 0.099 - 0.50 0.05

Raspberries, Frozen 43 0 0.099 - 0.50 0.05

Appendix B. Page 36 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Summer Squash 346 0 0.050 ^ 0.5

TOTAL 2,154 0

Halosulfuron methyl 2

 (herbicide) 

Baby Food - Applesauce 379 0 0.010 ^ 0.05

Broccoli 708 0 0.010 ^ NT

Peaches 285 0 0.010 ^ NT

TOTAL 1,372 0

Haloxyfop (herbicide) 

Plums 507 0 0.040 ^ NT

Raspberries 351 0 0.040 ^ NT

Raspberries, Frozen 10 0 0.040 ^ NT

TOTAL 868 0

Hexaconazole (fungicide) 

Baby Food - Applesauce 379 0 0.010 ^ NT

Broccoli 708 0 0.010 ^ NT

Celery 346 0 0.020 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.020 ^ NT

Raspberries 351 0 0.020 ^ NT

Raspberries, Frozen 10 0 0.020 ^ NT

Summer Squash 363 0 0.020 ^ NT

Winter Squash 187 0 0.012 ^ NT

TOTAL 3,136 0

Hexazinone (herbicide) 

Bananas 708 0 0.004 ^ NT

Raspberries 301 0 0.004 ^ NT

Raspberries, Frozen 43 0 0.004 ^ NT

TOTAL 1,052 0

Hexythiazox (insecticide, acaricide)

Apple Juice 379 0 0.002 ^ 0.25

Baby Food - Applesauce 379 0 0.010 ^ 0.25

Baby Food - Peas 378 0 0.10 ^ NT

Bananas 708 0 0.012 ^ NT

Broccoli 708 0 0.010 ^ NT

Celery 346 0 0.005 ^ NT

Grape Juice 176 0 0.002 ^ 1.0

Green Beans 378 0 0.30 ^ 0.3

Mushrooms 532 0 0.002 ^ NT

Nectarines 543 4 0.7 0.058 ^ 0.035 ^ 1.0

Peaches 285 15 5.3 0.011 - 0.15 0.010 ^ 1.0

Plums 507 2 0.4 0.005 - 0.012 0.005 ^ 1.0

Raspberries 652 59 9 0.005 - 0.38 0.005 - 0.012 1.0

Raspberries, Frozen 53 1 1.9 0.069 ^ 0.005 - 0.012 1.0

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 6,574 81

Hydroprene (insect growth regulator) 

Apple Juice 379 0 0.10 ^ 0.2

Baby Food - Peas 378 0 0.080 ^ 0.2

Carrots 708 0 0.001 ^ 0.2

Cauliflower 532 0 0.002 - 0.005 0.2

Celery 362 0 0.002 ^ 0.2

Grape Juice 176 0 0.10 ^ 0.2

Green Beans 378 0 0.080 ^ 0.2

Nectarines 543 0 0.001 ^ 0.2

Summer Squash 346 0 0.080 ^ 0.2

TOTAL 3,802 0

3-Hydroxycarbofuran (metabolite of Carbofuran)

Apple Juice 379 0 0.003 ^ NT

Appendix B. Page 37 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Baby Food - Applesauce 379 0 0.010 ^ NT

Baby Food - Peas 378 0 0.010 ^ NT

Bananas 708 0 0.002 ^ 0.1

Broccoli (V-1) 708 1 0.1 0.017 ^ 0.010 ^ NT

Carrots 712 0 0.030 ^ NT

Cauliflower 532 0 0.001 - 0.008 NT

Celery 708 0 0.001 - 0.010 NT

Grape Juice 176 0 0.003 ^ 0.4

Green Beans (V-1) 378 1 0.3 0.004 ^ 0.002 ^ NT

Mushrooms 532 0 0.003 ^ NT

Nectarines 543 0 0.050 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.002 - 0.010 NT

Raspberries, Frozen 53 0 0.002 - 0.010 NT

Summer Squash 709 0 0.010 ^ 0.8

Winter Squash 187 0 0.006 ^ 0.8

TOTAL 8,526 2

5-Hydroxythiabendazole (metabolite of Thiabendazole)

Celery 346 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 1,764 0

Imazalil (fungicide) 

Apple Juice 379 0 0.010 ^ NT

Baby Food - Applesauce 379 0 0.010 ^ NT

Bananas 708 257 36.3 0.005 - 0.10 0.005 ^ 3.0

Broccoli 690 0 0.010 ^ NT

Cauliflower 532 0 0.009 ^ NT

Celery 708 0 0.001 - 0.030 NT

Grape Juice 176 0 0.010 ^ NT

Mushrooms 532 0 0.010 ^ NT

Nectarines (V-22) 543 22 4.1 0.007 - 0.29 0.004 ^ NT

Peaches 285 0 0.010 ^ NT

Plums (V-1) 507 1 0.2 0.013 ^ 0.005 ^ NT

Raspberries 652 0 0.005 ^ NT

Raspberries, Frozen 53 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 6,694 280

Imazethapyr (herbicide) 

Apple Juice 379 0 0.020 ^ NT

Grape Juice 176 0 0.020 ^ NT

Mushrooms 532 0 0.020 ^ NT

TOTAL 1,087 0

Imidacloprid (insecticide) 

Apple Juice 379 2 0.5 0.006 - 0.007 0.003 ^ 0.5

Baby Food - Applesauce 379 0 0.010 ^ 0.5

Baby Food - Peas 378 0 0.030 ^ 4.0

Bananas 708 1 0.1 0.010 ^ 0.009 ^ 0.50

Broccoli 708 69 9.7 0.010 - 1.5 0.010 ^ 3.5

Carrots 712 3 0.4 0.008 ^ 0.005 ^ 0.40

Cauliflower 532 212 39.8 0.002 - 0.36 0.001 ^ 3.5

Celery 708 38 5.4 0.002 - 0.046 0.001 - 0.010 6.0

Grape Juice 176 17 9.7 0.004 - 0.041 0.003 ^ 1.5

Green Beans 378 2 0.5 0.024 - 0.025 0.005 ^ 4.0

Mushrooms 532 0 0.003 ^ NT

Nectarines 543 10 1.8 0.017 - 0.045 0.010 ^ 3.0

Peaches 285 14 4.9 0.011 - 0.29 0.010 ^ 3.0

Appendix B. Page 38 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Plums 507 1 0.2 0.012 ^ 0.010 ^ 3.0

Raspberries 652 9 1.4 0.010 - 0.046 0.009 - 0.010 2.5

Raspberries, Frozen 53 1 1.9 0.089 ^ 0.009 - 0.010 2.5

Summer Squash 709 110 15.5 0.010 - 0.19 0.010 - 0.030 0.5

Winter Squash 187 42 22.5 0.010 - 0.13 0.006 ^ 0.5

TOTAL 8,526 531

Imidacloprid urea (metabolite of Imidacloprid)

Bananas 708 0 0.022 ^ 0.50

Raspberries 301 0 0.022 ^ 2.5

Raspberries, Frozen 43 0 0.022 ^ 2.5

TOTAL 1,052 0

Imiprothrin (insecticide) 

Apple Juice 379 0 0.010 ^ NT

Baby Food - Peas 378 0 0.040 ^ NT

Bananas 708 0 0.090 ^ NT

Carrots 712 0 0.009 ^ NT

Celery 346 0 0.010 ^ NT

Grape Juice 176 0 0.010 ^ NT

Green Beans 378 0 0.030 ^ NT

Mushrooms 532 0 0.010 ^ NT

Nectarines 543 0 0.009 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.010 - 0.090 NT

Raspberries, Frozen 53 0 0.010 - 0.090 NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 5,914 0

Indaziflam (herbicide) 

Apple Juice 379 0 0.001 ^ 0.01

Celery 346 0 0.003 ^ NT

Grape Juice 176 0 0.001 ^ 0.01

Nectarines 543 1 0.2 0.003 ^ 0.002 ^ 0.01

Plums 507 0 0.003 ^ 0.01

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 2,862 1

Indoxacarb (insecticide) 

Apple Juice 379 0 0.020 ^ 1.0

Baby Food - Applesauce 379 0 0.010 ^ 1.0

Bananas 708 0 0.021 ^ NT

Broccoli 708 13 1.8 0.011 - 0.065 0.010 ^ 12

Celery 346 0 0.010 ^ 14

Grape Juice 176 0 0.020 ^ 2.0

Green Beans 378 0 0.050 ^ NT

Mushrooms 532 0 0.020 ^ NT

Nectarines 541 98 18.1 0.003 - 0.083 0.002 ^ 0.90

Peaches 285 19 6.7 0.010 - 0.035 0.010 ^ 0.90

Plums 507 0 0.010 ^ 0.90

Raspberries 652 0 0.010 - 0.021 NT

Raspberries, Frozen 53 0 0.010 - 0.021 NT

Summer Squash 709 2 0.3 0.012 - 0.021 0.005 - 0.010 0.60

Winter Squash 187 0 0.006 ^ 0.60

TOTAL 6,540 132

Ipconazole (fungicide) 

Baby Food - Peas 378 0 0.020 ^ NT

Green Beans 378 0 0.002 ^ NT

TOTAL 756 0

Appendix B. Page 39 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Iprodione (fungicide) 

Apple Juice 379 0 0.040 ^ NT

Baby Food - Applesauce (V-1) 357 1 0.3 0.002 ^ 0.001 ^ NT

Bananas 708 0 0.022 ^ NT

Broccoli 707 0 0.005 ^ 25.0

Carrots 712 58 8.1 0.033 - 1.4 0.020 - 0.067 5.0

Cauliflower 532 0 0.009 ^ NT

Celery (V-1) 376 1 0.3 0.006 ^ 0.005 - 0.009 NT

Grape Juice 146 0 0.040 ^ 60.0

Green Beans 378 0 0.15 ^ 2.0

Mushrooms 532 0 0.040 ^ NT

Nectarines 543 221 40.7 0.008 - 7.2 0.005 ^ 20.0

Peaches 285 19 6.7 0.005 - 1.8 0.005 ^ 20.0

Plums 507 262 51.7 0.005 - 6.4 0.005 ^ 20.0

Raspberries 652 20 3.1 0.007 - 2.9 0.005 - 0.022 15.0

Raspberries, Frozen 53 8 15.1 0.023 - 0.44 0.005 - 0.022 15.0

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 7,417 590

Iprovalicarb (fungicide) 

Bananas 708 0 0.010 ^ NT

Celery 346 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.005 - 0.010 NT

Raspberries, Frozen 53 0 0.005 - 0.010 NT

Summer Squash 363 0 0.005 ^ NT

TOTAL 2,629 0

Isofenphos (insecticide) 

Celery 346 0 0.003 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 1,764 0

Isoprocarb (insecticide) 

Celery 346 0 0.010 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 1,764 0

Isoproturon (herbicide) 

Celery 346 0 0.003 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

TOTAL 1,577 0

Kresoxim-methyl (fungicide) 

Apple Juice 379 0 0.010 ^ 0.5

Bananas 708 0 0.008 ^ NT

Cauliflower 532 0 0.003 - 0.010 NT

Celery 708 0 0.002 - 0.010 NT

Grape Juice 176 0 0.010 ^ 1.0

Green Beans 378 0 0.020 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.008 - 0.010 NT

Raspberries, Frozen 53 0 0.008 - 0.010 NT

Summer Squash 709 0 0.010 - 0.025 0.40

Appendix B. Page 40 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Winter Squash 187 0 0.006 ^ 0.40

TOTAL 4,989 0

Lactofen (herbicide) 

Celery 346 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 1,764 0

Lenacil (herbicide) 

Baby Food - Applesauce 379 0 0.001 ^ NT

Broccoli 707 0 0.005 ^ NT

Celery 346 0 0.005 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

TOTAL 2,948 0

Leptophos oxygen analog (insecticide metabolite)

Celery 346 0 0.020 ^ NT

Plums 507 0 0.020 ^ NT

Raspberries 351 0 0.020 ^ NT

Raspberries, Frozen 10 0 0.020 ^ NT

Summer Squash 363 0 0.020 ^ NT

Winter Squash 187 0 0.012 ^ NT

TOTAL 1,764 0

Lindane - BHC gamma (insecticide) 

Apple Juice 379 0 0.013 ^ NT

Baby Food - Applesauce 379 0 0.001 ^ NT

Baby Food - Peas 378 0 0.15 ^ 0.5 AL

Bananas 708 0 0.044 ^ NT

Carrots 712 0 0.001 ^ 0.5 AL

Cauliflower 532 0 0.001 ^ NT

Celery 376 0 0.001 - 0.003 NT

Grape Juice 176 0 0.013 ^ NT

Green Beans 378 0 0.075 ^ 0.5 AL

Mushrooms 532 0 0.013 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.003 - 0.044 0.5 AL

Raspberries, Frozen 53 0 0.003 - 0.044 0.5 AL

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 6,597 0

Linuron (herbicide) 

Apple Juice 379 0 0.003 ^ NT

Baby Food - Applesauce 357 0 0.004 ^ NT

Bananas 708 0 0.007 ^ NT

Broccoli 688 0 0.019 ^ NT

Carrots 712 152 21.3 0.033 - 0.52 0.020 ^ 1.0

Cauliflower 532 0 0.003 ^ NT

Celery 708 107 15.1 0.005 - 0.090 0.003 - 0.010 0.5

Grape Juice 176 0 0.003 ^ NT

Mushrooms 532 0 0.003 ^ NT

Peaches 285 0 0.019 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.007 - 0.010 NT

Raspberries, Frozen 53 0 0.007 - 0.010 NT

Summer Squash 363 0 0.010 ^ NT

Appendix B. Page 41 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Winter Squash 187 0 0.006 ^ NT

TOTAL 6,839 259

Lufenuron (insecticide) 

Apple Juice 379 0 0.020 ^ NT

Bananas 708 0 0.010 ^ NT

Grape Juice 176 0 0.020 ^ NT

Raspberries 301 0 0.010 ^ NT

Raspberries, Frozen 43 0 0.010 ^ NT

TOTAL 1,607 0

Malathion (insecticide) 

Apple Juice 379 0 0.002 ^ 8

Baby Food - Applesauce 379 0 0.010 ^ 8

Baby Food - Peas 378 0 0.010 ^ 8

Bananas 708 0 0.010 ^ NT

Broccoli 708 0 0.010 ^ 8

Carrots 712 0 0.001 ^ 8

Cauliflower 532 0 0.001 ^ 8

Celery 708 75 10.6 0.002 - 0.17 0.001 - 0.005 8

Grape Juice 176 0 0.002 ^ 8

Green Beans 378 0 0.002 ^ 8

Mushrooms 532 0 0.002 ^ 8

Nectarines 543 0 0.002 ^ 8

Peaches 285 0 0.010 ^ 8

Plums 507 0 0.005 ^ 8

Raspberries 652 42 6.4 0.005 - 0.16 0.005 - 0.010 8

Raspberries, Frozen 53 1 1.9 0.010 ^ 0.005 - 0.010 8

Summer Squash 709 0 0.005 - 0.010 8

Winter Squash 187 0 0.003 ^ 8

TOTAL 8,526 118

Malathion oxygen analog (metabolite of Malathion)

Apple Juice 379 0 0.002 ^ 8

Baby Food - Applesauce 379 0 0.010 ^ 8

Baby Food - Peas 378 0 0.005 ^ 8

Bananas 708 0 0.002 ^ NT

Broccoli 708 0 0.010 ^ 8

Carrots 712 0 0.001 ^ 8

Cauliflower 532 0 0.003 ^ 8

Celery 708 0 0.003 ^ 8

Grape Juice 176 0 0.002 ^ 8

Green Beans 378 0 0.001 ^ 8

Mushrooms 532 0 0.002 ^ 8

Nectarines 543 0 0.002 ^ 8

Peaches 285 0 0.010 ^ 8

Plums 507 0 0.003 ^ 8

Raspberries 652 1 0.2 0.003 ^ 0.002 - 0.003 8

Raspberries, Frozen 53 0 0.002 - 0.003 8

Summer Squash 709 0 0.003 - 0.005 8

Winter Squash 187 0 0.002 ^ 8

TOTAL 8,526 1

Mandipropamid (fungicide) 

Apple Juice 379 0 0.002 ^ NT

Baby Food - Applesauce 379 0 0.005 ^ NT

Bananas 708 0 0.010 ^ NT

Broccoli 708 17 2.4 0.007 - 0.23 0.005 ^ 3

Cauliflower 516 0 0.005 - 0.015 3

Celery 708 5 0.7 0.008 - 0.21 0.005 - 0.030 20

Grape Juice 148 2 1.4 0.003 - 0.004 0.002 ^ 1.4

Green Beans 378 3 0.8 0.002 - 0.012 0.001 ^ 0.90

Mushrooms 532 0 0.002 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.005 - 0.010 NT

Appendix B. Page 42 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Raspberries, Frozen 53 0 0.005 - 0.010 NT

Summer Squash 709 4 0.6 0.005 - 0.010 0.005 ^ 0.6

Winter Squash 187 0 0.003 ^ 0.6

TOTAL 6,849 31

Mepanipyrim (fungicide) 

Celery 346 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

TOTAL 1,577 0

Mesotrione (herbicide) 

Plums 507 0 0.040 ^ NT

TOTAL 507 0

Metaflumizone (insecticide) 

Bananas 708 0 0.010 ^ NT

Celery 346 0 0.020 ^ NT

Plums 507 0 0.020 ^ NT

Raspberries 652 0 0.010 - 0.020 NT

Raspberries, Frozen 53 0 0.010 - 0.020 NT

Summer Squash 363 0 0.020 ^ NT

TOTAL 2,629 0

Metalaxyl/Mefenoxam 3

 (fungicide) 

Apple Juice 379 0 0.001 ^ 0.2

Baby Food - Applesauce 379 0 0.001 ^ 0.2

Baby Food - Peas 378 0 0.025 ^ 0.2

Bananas 708 0 0.030 ^ NT

Broccoli 707 6 0.8 0.006 - 0.046 0.005 ^ 2.0

Carrots 711 77 10.8 0.008 - 0.035 0.005 ^ 0.5

Cauliflower 532 4 0.8 0.002 - 0.007 0.001 ^ 1.0

Celery 708 1 0.1 0.002 ^ 0.001 - 0.005 5.0

Grape Juice 148 1 0.7 0.002 ^ 0.001 ^ 2.0

Green Beans 378 19 5 0.001 - 0.018 0.001 ^ 0.2

Mushrooms 532 0 0.001 ^ NT

Nectarines 543 0 0.001 ^ 1.0

Peaches 285 0 0.005 ^ 1.0

Plums 507 0 0.003 ^ 1.0

Raspberries 652 0 0.003 - 0.030 0.70

Raspberries, Frozen 53 0 0.003 - 0.030 0.70

Summer Squash 709 30 4.2 0.003 - 0.40 0.003 - 0.050 1.0

Winter Squash 187 17 9.1 0.003 - 0.057 0.002 ^ 1.0

TOTAL 8,496 155

Metaldehyde (molluscicide) 

Bananas 708 0 0.22 ^ NT

Raspberries 301 0 0.22 ^ 0.15

Raspberries, Frozen 43 0 0.22 ^ 0.15

TOTAL 1,052 0

Metconazole (fungicide) 

Celery 346 0 0.010 ^ NT

Nectarines 543 0 0.002 ^ 0.20

Plums 507 0 0.010 ^ 0.20

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 2,307 0

Appendix B. Page 43 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Methamidophos (insecticide) (also a metabolite of Acephate)

Apple Juice 379 0 0.005 ^ 0.02

Baby Food - Applesauce 379 0 0.010 ^ 0.02

Baby Food - Peas 378 0 0.10 ^ 0.02

Bananas 708 0 0.008 ^ 0.02

Broccoli 708 0 0.050 ^ 1.0

Carrots 243 0 0.017 ^ 0.02

Cauliflower 532 18 3.4 0.002 - 0.046 0.001 ^ 0.5 4

Celery 708 65 9.2 0.002 - 0.031 0.001 - 0.005 1 5

Grape Juice 148 0 0.005 ^ 0.02

Green Beans 378 100 26.5 0.020 - 0.86 0.020 ^ 1 6

Mushrooms 532 0 0.005 ^ 0.02

Nectarines 271 0 0.025 ^ 0.02

Peaches 285 0 0.050 ^ 0.02

Plums 507 0 0.005 ^ 0.02

Raspberries 652 0 0.005 - 0.008 0.02

Raspberries, Frozen 53 0 0.005 - 0.008 0.02

Summer Squash 709 0 0.005 - 0.10 0.02

Winter Squash 187 3 1.6 0.005 - 0.025 0.003 ^ 0.02

TOTAL 7,757 186

Methidathion (insecticide) 

Apple Juice 379 0 0.010 ^ 0.05

Baby Food - Applesauce 379 0 0.010 ^ 0.05

Bananas 708 0 0.006 ^ NT

Broccoli 708 0 0.010 ^ NT

Cauliflower 532 0 0.002 ^ NT

Celery 708 0 0.002 - 0.003 NT

Grape Juice 176 0 0.010 ^ NT

Nectarines 543 0 0.001 ^ 0.05

Peaches 285 0 0.010 ^ 0.05

Plums 507 0 0.003 ^ 0.05

Raspberries 652 0 0.003 - 0.006 NT

Raspberries, Frozen 53 0 0.003 - 0.006 NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 6,180 0

Methidathion oxygen analog (metabolite of Methidathion)

Cauliflower 532 0 0.003 ^ NT

Celery 332 0 0.010 ^ NT

TOTAL 864 0

Methiocarb (insecticide)

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.010 NT

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 2,658 0

Methiocarb sulfone (metabolite of Methiocarb)

Apple Juice 379 0 0.001 ^ NT

Grape Juice 176 0 0.001 ^ NT

TOTAL 555 0

Methiocarb sulfoxide (metabolite of Methiocarb)

Apple Juice 379 0 0.001 ^ NT

Celery 346 0 0.005 ^ NT

Grape Juice 176 0 0.001 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

TOTAL 2,132 0

Appendix B. Page 44 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Methomyl (insecticide) 

Apple Juice 379 0 0.010 ^ 1

Baby Food - Applesauce 379 0 0.010 ^ 1

Baby Food - Peas 378 0 0.005 ^ 5

Bananas 708 0 0.013 ^ NT

Broccoli 708 0 0.010 ^ 3

Carrots 712 0 0.004 ^ 0.2

Cauliflower 532 5 0.9 0.004 - 0.042 0.002 ^ 2

Celery 708 20 2.8 0.004 - 0.19 0.002 - 0.020 3

Grape Juice 146 0 0.030 ^ 5

Green Beans 378 10 2.6 0.002 - 0.17 0.001 ^ 2

Mushrooms 501 0 0.010 - 0.030 NT

Nectarines 543 21 3.9 0.005 - 0.28 0.003 ^ 5

Peaches 285 1 0.4 0.042 ^ 0.010 ^ 5

Plums 507 0 0.020 ^ NT

Raspberries 652 0 0.013 - 0.020 NT

Raspberries, Frozen 53 0 0.013 - 0.020 NT

Summer Squash 709 6 0.8 0.007 - 0.043 0.005 - 0.020 0.2

Winter Squash 187 0 0.012 ^ 0.2

TOTAL 8,465 63

Methoprene (insect growth regulator) 

Baby Food - Peas 378 0 0.20 ^ EX

Cauliflower 516 0 0.015 ^ EX

Celery 362 0 0.015 ^ EX

Green Beans 378 0 0.40 ^ EX

TOTAL 1,634 0

Methoxychlor Total (insecticide) 

Bananas 708 0 0.008 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery 362 0 0.001 ^ NT

Raspberries 301 0 0.008 ^ NT

Raspberries, Frozen 43 0 0.008 ^ NT

TOTAL 1,946 0

Methoxychlor olefin (metabolite of Methoxychlor)

Cauliflower 532 0 0.001 ^ NT

Celery 362 0 0.001 ^ NT

TOTAL 894 0

Methoxychlor p,p' (isomer of Methoxychlor)

Baby Food - Applesauce 357 0 0.001 ^ NT

Broccoli 665 0 0.005 ^ NT

Celery 317 0 0.005 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.009 ^ NT

TOTAL 3,042 0

Methoxyfenozide (insecticide) 

Apple Juice 379 2 0.5 0.003 - 0.004 0.003 ^ 1.5

Baby Food - Applesauce 379 1 0.3 0.031 ^ 0.010 ^ 1.5

Baby Food - Peas 378 0 0.010 ^ 0.2

Bananas 708 0 0.006 ^ NT

Broccoli 708 0 0.010 ^ 7.0

Carrots 712 5 0.7 0.003 ^ 0.002 ^ 0.90

Cauliflower 532 0 0.001 ^ 7.0

Celery 708 111 15.7 0.002 - 0.096 0.001 - 0.005 25

Grape Juice 176 17 9.7 0.003 - 0.008 0.003 ^ 1.0

Green Beans 378 4 1.1 0.003 - 0.020 0.002 ^ 1.5

Mushrooms 532 0 0.003 ^ NT

Appendix B. Page 45 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Nectarines 543 113 20.8 0.003 - 0.18 0.002 ^ 3.0

Peaches 285 53 18.6 0.010 - 0.11 0.010 ^ 3.0

Plums 507 30 5.9 0.005 - 0.059 0.005 ^ 0.30

Raspberries (V-1) 652 1 0.2 0.026 ^ 0.005 - 0.006 NT

Raspberries, Frozen 53 0 0.005 - 0.006 NT

Summer Squash 709 1 0.1 0.007 ^ 0.005 - 0.010 0.3

Winter Squash 187 9 4.8 0.005 - 0.013 0.003 ^ 0.3

TOTAL 8,526 347

Metolachlor (herbicide) 

Apple Juice 379 0 0.001 ^ NT

Baby Food - Applesauce 379 0 0.001 ^ NT

Baby Food - Peas 378 0 0.005 ^ 0.30

Bananas 708 0 0.007 ^ NT

Broccoli 707 0 0.005 ^ 0.60

Carrots 712 5 0.7 0.002 ^ 0.001 ^ 0.40

Cauliflower 532 0 0.001 ^ 0.60

Celery 708 7 1 0.002 - 0.004 0.001 - 0.003 0.10

Grape Juice 176 0 0.001 ^ NT

Green Beans 378 0 0.005 ^ 0.30

Mushrooms 532 0 0.001 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.003 - 0.007 0.10

Raspberries, Frozen 53 0 0.003 - 0.007 0.10

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.003 ^ 0.10

TOTAL 7,636 12

Metribuzin (herbicide) 

Apple Juice 379 0 0.005 ^ NT

Baby Food - Peas 378 0 0.20 ^ 0.1

Bananas 708 0 0.004 ^ NT

Carrots 712 1 0.1 0.012 ^ 0.002 ^ 0.3

Cauliflower 532 0 0.002 ^ NT

Celery 708 0 0.002 - 0.005 NT

Grape Juice 176 0 0.005 ^ NT

Green Beans 378 0 0.002 ^ NT

Mushrooms 532 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.004 - 0.005 NT

Raspberries, Frozen 53 0 0.004 - 0.005 NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 6,265 1

Mevinphos (insecticide) 

Apple Juice 379 0 0.002 ^ NT

Baby Food - Applesauce 357 0 0.001 ^ NT

Baby Food - Peas 378 0 0.020 ^ NT

Bananas 708 0 0.006 ^ NT

Broccoli 707 0 0.005 ^ NT

Celery 708 0 0.002 - 0.005 NT

Grape Juice 176 0 0.002 ^ NT

Green Beans 378 0 0.002 ^ NT

Mushrooms 532 0 0.002 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.003 - 0.006 NT

Raspberries, Frozen 53 0 0.003 - 0.006 NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 6,370 0

Appendix B. Page 46 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

MGK-264 (insecticide) 

Baby Food - Peas 378 0 0.040 ^ 5

Bananas 708 0 0.030 ^ 5

Carrots 712 0 0.001 ^ 5

Celery 346 0 0.003 ^ 5

Grape Juice 176 0 0.10 ^ 5

Green Beans 378 0 0.020 ^ 5

Nectarines 543 0 0.001 ^ 5

Plums 507 1 0.2 0.005 ^ 0.003 ^ 5

Raspberries 652 0 0.003 - 0.030 5

Raspberries, Frozen 53 0 0.003 - 0.030 5

Summer Squash 709 0 0.003 - 0.040 5

Winter Squash 187 0 0.003 ^ 5

TOTAL 5,349 1

Mirex (insecticide) 

Grape Juice 176 0 0.001 ^ NT

TOTAL 176 0

Monocrotophos (insecticide) 

Baby Food - Applesauce 379 0 0.010 ^ NT

Bananas 708 0 0.004 ^ NT

Broccoli 708 0 0.010 ^ NT

Celery 346 0 0.005 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.004 - 0.005 NT

Raspberries, Frozen 53 0 0.004 - 0.005 NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 4,188 0

Myclobutanil (fungicide) 

Apple Juice 379 0 0.003 ^ 0.5

Baby Food - Applesauce 379 36 9.5 0.002 ^ 0.001 ^ 0.5

Baby Food - Peas 378 0 0.010 ^ 0.03

Bananas 708 116 16.4 0.002 - 0.11 0.001 ^ 4.0

Broccoli 707 0 0.005 ^ 0.03

Carrots 712 7 1 0.003 - 0.011 0.002 ^ 0.03

Cauliflower 532 0 0.001 ^ 0.03

Celery (X-1) 708 15 2.1 0.002 - 0.083 0.001 - 0.010 0.03

Grape Juice 176 0 0.003 ^ 1.0

Green Beans 378 20 5.3 0.006 - 0.089 0.005 ^ 1.0

Mushrooms 532 0 0.003 ^ NT

Nectarines 539 34 6.3 0.003 - 0.078 0.002 ^ 2.0

Peaches 285 10 3.5 0.005 - 0.072 0.005 ^ 2.0

Plums 507 0 0.010 ^ 2.0

Raspberries 652 97 14.9 0.001 - 0.21 0.001 - 0.010 2.0

Raspberries, Frozen 53 1 1.9 0.037 ^ 0.001 - 0.010 2.0

Summer Squash 709 14 2 0.011 - 0.081 0.010 - 0.020 0.20

Winter Squash 187 1 0.5 0.010 ^ 0.006 ^ 0.20

TOTAL 8,521 351

Naled (insecticide) 

Apple Juice 379 0 0.020 ^ 0.5

Carrots 712 0 0.025 ^ 0.5

Grape Juice 148 0 0.020 ^ 0.5

Mushrooms 503 0 0.020 ^ 0.5

Nectarines 543 0 0.015 ^ 0.5

TOTAL 2,285 0

1-Naphthol (metabolite of Carbaryl)

Apple Juice 379 0 0.015 ^ 12

Baby Food - Peas 378 0 0.010 ^ 10

Carrots 712 0 0.017 - 0.057 2.0

Appendix B. Page 47 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Green Beans 347 0 0.060 ^ 10

Mushrooms 503 0 0.015 ^ NT

Nectarines 543 4 0.7 0.025 - 2.1 0.015 ^ 10

Summer Squash 346 0 0.020 ^ 3.0

TOTAL 3,208 4

Napropamide (herbicide) 

Apple Juice 379 0 0.005 ^ NT

Baby Food - Applesauce 379 0 0.010 ^ NT

Bananas 708 0 0.020 ^ NT

Broccoli 708 0 0.010 ^ 0.1

Cauliflower 532 0 0.002 ^ 0.1

Celery 708 0 0.002 - 0.005 NT

Grape Juice 176 0 0.005 ^ 0.1

Mushrooms 532 0 0.005 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.005 - 0.020 0.1

Raspberries, Frozen 53 0 0.005 - 0.020 0.1

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.008 ^ NT

TOTAL 6,169 0

Nitrofen (herbicide) 

Celery 346 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

TOTAL 1,577 0

Norflurazon (herbicide) 

Apple Juice 379 0 0.002 ^ 0.1

Baby Food - Applesauce 379 0 0.010 ^ 0.1

Bananas 708 0 0.005 ^ NT

Broccoli 708 0 0.010 ^ NT

Celery 376 0 0.001 - 0.010 NT

Grape Juice 176 0 0.002 ^ 0.1

Mushrooms 532 0 0.002 ^ NT

Nectarines 543 0 0.001 ^ 0.1

Peaches 285 0 0.010 ^ 0.1

Plums 507 0 0.010 ^ 0.1

Raspberries 652 0 0.005 - 0.010 0.2

Raspberries, Frozen 53 0 0.005 - 0.010 0.2

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 5,848 0

Norflurazon desmethyl (metabolite of Norflurazon)

Apple Juice 379 0 0.005 ^ 0.1

Baby Food - Applesauce 379 0 0.010 ^ 0.1

Bananas 708 0 0.010 ^ NT

Broccoli 708 0 0.010 ^ NT

Celery 376 0 0.001 - 0.010 NT

Grape Juice 176 0 0.005 ^ 0.1

Mushrooms 532 0 0.005 ^ NT

Nectarines 543 1 0.2 0.008 ^ 0.005 ^ 0.1

Peaches 285 0 0.010 ^ 0.1

Plums 507 0 0.010 ^ 0.1

Raspberries 652 0 0.010 ^ 0.2

Raspberries, Frozen 53 0 0.010 ^ 0.2

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 5,848 1

Appendix B. Page 48 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Novaluron (insecticide) 

Baby Food - Applesauce 379 0 0.010 ^ 2.0

Baby Food - Peas 378 0 0.050 ^ 0.01

Bananas 708 0 0.010 ^ 0.01

Broccoli 708 0 0.010 ^ 0.50

Carrots 712 0 0.005 ^ 0.01

Cauliflower 502 0 0.001 ^ 0.50

Celery 692 0 0.001 - 0.080 0.01

Green Beans 378 0 0.050 ^ 0.60

Nectarines 543 0 0.001 ^ 1.9

Peaches 285 0 0.010 ^ 1.9

Plums 507 0 0.080 ^ 1.9

Raspberries 652 0 0.010 - 0.080 0.01

Raspberries, Frozen 53 0 0.010 - 0.080 0.01

Summer Squash 709 0 0.050 - 0.080 0.15

Winter Squash 187 0 0.048 ^ 0.15

TOTAL 7,393 0

Omethoate (insecticide) (also a metabolite of Dimethoate)

Apple Juice 379 0 0.020 ^ NT

Baby Food - Applesauce 379 0 0.010 ^ NT

Baby Food - Peas 378 0 0.015 ^ 2.0

Bananas 708 0 0.019 ^ NT

Broccoli 708 4 0.6 0.018 - 0.15 0.010 ^ 2.0

Cauliflower 532 0 0.002 ^ 2.0

Celery 708 52 7.3 0.004 - 0.049 0.002 - 0.008 2.0

Grape Juice 176 0 0.020 ^ NT

Green Beans 378 15 4 0.007 - 0.081 0.006 ^ 2.0

Mushrooms 532 0 0.020 ^ NT

Nectarines 543 0 0.060 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.005 - 0.019 NT

Raspberries, Frozen 53 0 0.005 - 0.019 NT

Summer Squash 709 0 0.005 - 0.015 NT

Winter Squash (V-1) 187 1 0.5 0.052 ^ 0.003 ^ NT

TOTAL 7,814 72

Oryzalin (herbicide) 

Apple Juice 379 0 0.020 ^ 0.05

Baby Food - Applesauce 379 0 0.020 ^ 0.05

Bananas 708 0 0.050 ^ NT

Broccoli 708 0 0.10 ^ NT

Grape Juice 176 0 0.020 ^ 0.05

Nectarines 543 0 0.010 ^ 0.05

Peaches 285 0 0.020 ^ 0.05

Raspberries 301 0 0.050 ^ 0.05

Raspberries, Frozen 43 0 0.050 ^ 0.05

TOTAL 3,522 0

Oxadiazon (herbicide) 

Celery 346 0 0.003 ^ NT

Grape Juice 146 0 0.010 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

TOTAL 1,723 0

Oxadixyl (fungicide) 

Baby Food - Applesauce 379 0 0.010 ^ NT

Broccoli 708 0 0.010 ^ NT

Cauliflower 532 0 0.003 ^ NT

Celery 693 0 0.003 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.003 ^ NT

Appendix B. Page 49 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 4,015 0

Oxamyl (insecticide) 

Apple Juice 379 0 0.003 ^ 2

Baby Food - Applesauce 379 0 0.010 ^ 2

Bananas 708 0 0.008 ^ 0.3

Broccoli 708 0 0.010 ^ NT

Carrots 712 0 0.029 ^ 0.1

Cauliflower 532 0 0.006 ^ NT

Celery 708 40 5.6 0.003 - 0.071 0.002 - 0.012 10.0

Grape Juice 176 0 0.003 ^ NT

Green Beans (V-1) 378 1 0.3 0.002 ^ 0.002 ^ NT

Mushrooms 532 0 0.003 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.008 - 0.010 NT

Raspberries, Frozen 53 0 0.008 - 0.010 NT

Summer Squash 709 35 4.9 0.011 - 0.46 0.010 ^ 2.0

Winter Squash 187 0 0.006 ^ 2.0

TOTAL 7,605 76

Oxamyl oxime (metabolite of Oxamyl)

Apple Juice 379 0 0.003 ^ 2

Baby Food - Applesauce 379 1 0.3 0.010 ^ 0.010 ^ 2

Bananas 708 4 0.6 0.022 - 0.032 0.020 ^ 0.3

Broccoli 708 0 0.010 ^ NT

Celery 346 5 1.4 0.021 - 0.029 0.020 ^ 10.0

Grape Juice 118 0 0.003 ^ NT

Green Beans 378 0 0.050 ^ NT

Mushrooms 532 0 0.003 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.020 ^ NT

Raspberries 652 0 0.020 ^ NT

Raspberries, Frozen 53 0 0.020 ^ NT

Summer Squash 709 12 1.7 0.022 - 0.13 0.020 - 0.060 2.0

Winter Squash 187 0 0.012 ^ 2.0

TOTAL 5,941 22

Oxydemeton methyl (insecticide) 

Apple Juice 379 0 0.002 ^ NT

Baby Food - Applesauce 379 0 0.010 ^ NT

Bananas 708 0 0.005 ^ NT

Broccoli 708 0 0.010 ^ 1.0

Celery 346 0 0.003 ^ NT

Grape Juice 176 0 0.002 ^ NT

Green Beans 378 0 0.002 ^ NT

Mushrooms 532 0 0.002 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.003 - 0.005 NT

Raspberries, Frozen 53 0 0.003 - 0.005 NT

Summer Squash 709 0 0.003 - 0.010 1.0

TOTAL 5,812 0

Oxydemeton methyl sulfone (metabolite of Oxydemeton methyl)

Apple Juice 379 0 0.002 ^ NT

Baby Food - Applesauce 379 0 0.010 ^ NT

Broccoli 708 0 0.010 ^ 1.0

Cauliflower 532 0 0.012 ^ 1.0

Celery 708 0 0.005 - 0.012 NT

Grape Juice 176 0 0.002 ^ NT

Green Beans 378 0 0.001 ^ NT

Appendix B. Page 50 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Mushrooms 532 0 0.002 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 709 0 0.005 - 0.010 1.0

Winter Squash 187 0 0.003 ^ 0.3

TOTAL 5,841 0

Oxyfluorfen (herbicide) 

Apple Juice 379 0 0.050 ^ 0.05

Baby Food - Applesauce 379 0 0.001 ^ 0.05

Broccoli 707 0 0.005 ^ 0.05

Cauliflower 532 0 0.001 ^ 0.05

Celery 708 0 0.001 - 0.010 NT

Grape Juice 176 0 0.050 ^ 0.05

Nectarines 543 0 0.006 ^ 0.05

Peaches 285 0 0.005 ^ 0.05

Plums 507 0 0.010 ^ 0.05

Raspberries 351 0 0.010 ^ 0.05

Raspberries, Frozen 10 0 0.010 ^ 0.05

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.008 ^ NT

TOTAL 5,127 0

Paclobutrazol (plant growth regulator) 

Apple Juice 379 0 0.010 ^ NT

Baby Food - Applesauce 379 0 0.001 ^ NT

Bananas 708 0 0.007 ^ NT

Broccoli 707 0 0.005 ^ NT

Celery 346 0 0.010 ^ NT

Grape Juice 176 0 0.010 ^ NT

Nectarines 543 0 0.025 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.007 - 0.010 NT

Raspberries, Frozen 53 0 0.007 - 0.010 NT

Summer Squash 363 0 0.010 ^ NT

TOTAL 5,098 0

Parathion (insecticide) 

Baby Food - Applesauce 379 0 0.001 ^ NT

Bananas 708 0 0.060 ^ NT

Broccoli 707 0 0.005 ^ NT

Cauliflower 532 0 0.003 ^ NT

Celery 708 0 0.003 - 0.010 NT

Grape Juice 176 0 0.005 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.005 - 0.060 NT

Raspberries, Frozen 53 0 0.005 - 0.060 NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 5,257 0

Parathion methyl (insecticide) 

Apple Juice 379 0 0.010 ^ NT 7

Baby Food - Applesauce 379 0 0.001 ^ NT 7

Bananas 708 0 0.016 ^ NT

Broccoli 707 0 0.005 ^ NT 7

Cauliflower 532 0 0.008 - 0.032 NT 7

Celery 708 0 0.002 - 0.016 NT 7

Grape Juice 176 0 0.010 ^ NT 7

Mushrooms 532 0 0.010 ^ NT

Peaches 285 0 0.005 ^ NT 7

Appendix B. Page 51 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Plums 507 0 0.005 ^ NT 7

Raspberries 652 0 0.005 - 0.016 NT

Raspberries, Frozen 53 0 0.005 - 0.016 NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.009 ^ NT

TOTAL 6,168 0

Parathion methyl oxygen analog (metabolite of Parathion methyl)

Apple Juice 379 0 0.020 ^ NT 7

Cauliflower 532 0 0.005 ^ NT 7

Celery 708 0 0.005 - 0.010 NT 7

Grape Juice 176 0 0.020 ^ NT 7

Mushrooms 532 0 0.020 ^ NT

Plums 507 0 0.010 ^ NT 7

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 3,745 0

Parathion oxygen analog (metabolite of Parathion)

Cauliflower 532 0 0.003 ^ NT

Celery 708 0 0.003 - 0.010 NT

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 2,658 0

Pebulate (herbicide) 

Baby Food - Applesauce 379 0 0.001 ^ NT

Broccoli 707 0 0.005 ^ NT

Peaches 285 0 0.005 ^ NT

TOTAL 1,371 0

Penconazole (fungicide) 

Baby Food - Applesauce 379 0 0.001 ^ NT

Bananas 708 0 0.006 ^ NT

Broccoli 707 0 0.005 ^ NT

Celery 346 0 0.010 ^ NT

Nectarines (V-1) 543 1 0.2 0.026 ^ 0.003 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.006 - 0.010 NT

Raspberries, Frozen 53 0 0.006 - 0.010 NT

Summer Squash 363 0 0.010 ^ NT

TOTAL 4,543 1

Pencycuron (fungicide) 

Baby Food - Applesauce 379 0 0.010 ^ NT

Bananas 708 0 0.005 ^ NT

Broccoli 708 0 0.010 ^ NT

Celery 346 0 0.005 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.005 ^ NT

Raspberries, Frozen 53 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

TOTAL 4,001 0

Pendimethalin (herbicide) 

Apple Juice 379 0 0.10 ^ 0.10

Baby Food - Applesauce 379 0 0.001 ^ 0.10

Baby Food - Peas 378 0 0.040 ^ 0.10

Appendix B. Page 52 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Bananas 708 0 0.032 ^ NT

Broccoli 707 4 0.6 0.005 - 0.012 0.005 ^ 0.1

Carrots 712 30 4.2 0.010 ^ 0.006 ^ 0.5

Cauliflower 532 0 0.001 ^ 0.1

Celery (V-5) 708 5 0.7 0.002 - 0.007 0.001 - 0.005 NT

Grape Juice 176 0 0.10 ^ 0.1

Green Beans 378 0 0.040 ^ 0.10

Mushrooms 532 0 0.10 ^ NT

Nectarines 543 0 0.006 ^ 0.10

Peaches 285 0 0.005 ^ 0.10

Plums 507 0 0.005 ^ 0.10

Raspberries 652 0 0.005 - 0.032 NT

Raspberries, Frozen 53 0 0.005 - 0.032 NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 8,179 39

Penflufen (fungicide) 

Green Beans 378 0 0.001 ^ 0.01

TOTAL 378 0

Pentachloroaniline - PCA (metabolite of Quintozene)

Apple Juice 379 0 0.004 ^ NT

Baby Food - Applesauce 379 0 0.001 ^ NT

Broccoli 707 0 0.005 ^ 0.1

Carrots (V-35) 712 35 4.9 0.003 - 0.010 0.002 ^ NT

Cauliflower 532 0 0.001 ^ 0.1

Celery (V-1) 708 1 0.1 0.002 ^ 0.001 - 0.003 NT

Grape Juice 176 0 0.004 ^ NT

Green Beans 378 0 0.060 ^ 0.1

Mushrooms 532 0 0.004 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash (V-11) 709 11 1.6 0.003 - 0.018 0.003 - 0.12 NT

TOTAL 6,365 47

Pentachlorobenzene - PCB (metabolite of Quintozene)

Apple Juice 379 0 0.005 ^ NT

Baby Food - Applesauce 357 0 0.001 ^ NT

Broccoli 707 0 0.005 ^ 0.1

Carrots (V-1) 712 1 0.1 0.008 ^ 0.001 ^ NT

Cauliflower 514 0 0.008 ^ 0.1

Celery 708 0 0.005 - 0.008 NT

Grape Juice 176 0 0.005 ^ NT

Green Beans 378 0 0.015 ^ 0.1

Mushrooms 532 0 0.005 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 709 0 0.005 - 0.010 NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 6,512 1

Pentachlorophenyl methyl sulfide (metabolite of Quintozene)

Apple Juice 379 0 0.005 ^ NT

Baby Food - Applesauce 379 0 0.001 ^ NT

Broccoli 707 0 0.005 ^ 0.1

Carrots 712 0 0.002 ^ NT

Celery 362 0 0.001 - 0.003 NT

Grape Juice 176 0 0.005 ^ NT

Green Beans 378 0 0.025 ^ 0.1

Mushrooms 532 0 0.005 ^ NT

Peaches 285 0 0.005 ^ NT

Appendix B. Page 53 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Summer Squash 346 0 0.050 ^ NT

TOTAL 4,256 0

Penthiopyrad (fungicide) 

Carrots 712 32 4.5 0.003 - 0.029 0.002 ^ 3.0

Celery 346 9 2.6 0.004 - 0.13 0.003 ^ 30

Green Beans 378 18 4.8 0.002 - 0.19 0.001 ^ 4.0

Nectarines 543 3 0.6 0.002 - 0.044 0.001 ^ 4.0

Plums 507 0 0.003 ^ 4.0

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 709 5 0.7 0.003 - 0.007 0.003 - 0.005 0.60

TOTAL 3,556 67

Permethrin Total (insecticide)

Baby Food - Applesauce 379 0 0.002 ^ 0.05

Baby Food - Peas 378 0 0.040 ^ NT

Broccoli 707 12 1.7 0.011 - 0.95 0.010 ^ 2.0

Carrots 712 0 0.004 ^ NT

Green Beans 378 0 0.040 ^ NT

Nectarines (V-1) 543 1 0.2 0.21 ^ 0.004 ^ NT

Peaches 285 22 7.7 0.015 - 0.68 0.010 ^ 1.0

Summer Squash 346 0 0.040 ^ 1.5

TOTAL 3,728 35

Permethrin cis (isomer of Permethrin)

Apple Juice 379 0 0.010 ^ 0.05

Bananas 708 0 0.010 ^ NT

Cauliflower 532 2 0.4 0.002 ^ 0.001 ^ 0.5

Celery 708 303 42.8 0.002 - 0.24 0.001 - 0.005 5.0

Grape Juice 176 0 0.010 ^ NT

Mushrooms 532 11 2.1 0.010 - 0.11 0.010 ^ 5.0

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.005 - 0.010 NT

Raspberries, Frozen 53 0 0.005 - 0.010 NT

Summer Squash 363 1 0.3 0.006 ^ 0.005 ^ 1.5

Winter Squash 187 1 0.5 0.010 ^ 0.006 ^ 1.5

TOTAL 4,797 318

Permethrin trans (isomer of Permethrin)

Apple Juice 379 0 0.010 ^ 0.05

Bananas 708 0 0.010 ^ NT

Cauliflower 532 2 0.4 0.002 ^ 0.001 ^ 0.5

Celery 708 283 40 0.002 - 0.27 0.001 - 0.005 5.0

Grape Juice 176 0 0.010 ^ NT

Mushrooms 532 12 2.3 0.010 - 0.14 0.010 ^ 5.0

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.005 - 0.010 NT

Raspberries, Frozen 53 0 0.005 - 0.010 NT

Summer Squash 363 0 0.005 ^ 1.5

Winter Squash 187 2 1.1 0.010 ^ 0.006 ^ 1.5

TOTAL 4,797 299

Phenothrin (insecticide) 

Apple Juice 379 0 0.050 ^ 0.01

Baby Food - Applesauce 379 0 0.005 ^ 0.01

Baby Food - Peas 378 0 0.015 ^ 0.01

Bananas 708 0 0.018 ^ 0.01

Broccoli 707 0 0.005 ^ 0.01

Carrots 712 0 0.003 ^ 0.01

Cauliflower 532 0 0.002 - 0.008 0.01

Celery 708 0 0.002 - 0.005 0.01

Grape Juice 176 0 0.050 ^ 0.01

Green Beans 378 0 0.030 ^ 0.01

Mushrooms 532 0 0.050 ^ 0.01

Nectarines 543 0 0.003 ^ 0.01

Appendix B. Page 54 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Peaches 285 0 0.005 ^ 0.01

Plums 507 0 0.005 ^ 0.01

Raspberries 652 0 0.005 - 0.018 0.01

Raspberries, Frozen 53 0 0.005 - 0.018 0.01

Summer Squash 709 0 0.005 - 0.030 0.01

Winter Squash 187 0 0.003 ^ 0.01

TOTAL 8,525 0

Phenthoate (insecticide) 

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.003 NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

TOTAL 2,471 0

o-Phenylphenol (fungicide) 

Apple Juice 379 3 0.8 0.006 - 0.008 0.005 ^ 25

Carrots 712 1 0.1 0.007 ^ 0.004 ^ 20

Grape Juice 176 0 0.005 ^ NT

Mushrooms (V-7) 532 7 1.3 0.005 - 0.035 0.005 ^ NT

Nectarines 543 0 0.004 ^ 5

Plums 507 1 0.2 0.012 ^ 0.005 ^ 20

TOTAL 2,849 12

Phorate (insecticide) 

Apple Juice 379 0 0.010 ^ NT

Baby Food - Applesauce 379 0 0.001 ^ NT

Bananas 708 0 0.042 ^ NT

Broccoli 707 0 0.005 ^ NT

Celery 708 0 0.002 - 0.010 NT

Grape Juice 176 0 0.010 ^ NT

Green Beans 378 0 0.060 ^ 0.05

Mushrooms 532 0 0.010 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.010 - 0.042 NT

Raspberries, Frozen 53 0 0.010 - 0.042 NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 6,014 0

Phorate oxygen analog (metabolite of Phorate)

Apple Juice 379 0 0.010 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.005 NT

Grape Juice 176 0 0.010 ^ NT

Green Beans 378 0 0.001 ^ 0.05

Mushrooms 532 0 0.010 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 4,123 0

Phorate oxygen analog sulfone (metabolite of Phorate)

Bananas 708 0 0.010 ^ NT

Green Beans 378 0 0.002 ^ 0.05

Raspberries 301 0 0.010 ^ NT

Raspberries, Frozen 43 0 0.010 ^ NT

TOTAL 1,430 0

Phorate oxygen analog sulfoxide (metabolite of Phorate)

Bananas 708 0 0.005 ^ NT

Appendix B. Page 55 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Green Beans 378 0 0.002 ^ 0.05

Raspberries 301 0 0.005 ^ NT

Raspberries, Frozen 43 0 0.005 ^ NT

TOTAL 1,430 0

Phorate sulfone (metabolite of Phorate)

Apple Juice 379 0 0.010 ^ NT

Bananas 708 0 0.030 ^ NT

Cauliflower 532 0 0.003 ^ NT

Celery 708 0 0.003 - 0.005 NT

Grape Juice 176 0 0.010 ^ NT

Green Beans 378 0 0.005 ^ 0.05

Mushrooms 532 0 0.010 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.005 - 0.030 NT

Raspberries, Frozen 53 0 0.005 - 0.030 NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 5,175 0

Phorate sulfoxide (metabolite of Phorate)

Apple Juice 379 0 0.010 ^ NT

Baby Food - Applesauce 379 0 0.010 ^ NT

Bananas 708 0 0.005 ^ NT

Broccoli 708 0 0.010 ^ NT

Cauliflower 532 0 0.002 ^ NT

Celery 708 0 0.002 - 0.005 NT

Grape Juice 176 0 0.010 ^ NT

Green Beans 378 1 0.3 0.001 ^ 0.001 ^ 0.05

Mushrooms 532 0 0.010 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.005 ^ NT

Raspberries, Frozen 53 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 6,547 1

Phosalone (insecticide) 

Apple Juice 379 0 0.001 ^ 10.0

Baby Food - Applesauce 379 0 0.001 ^ 10.0

Bananas 708 0 0.026 ^ NT

Broccoli 707 0 0.005 ^ NT

Cauliflower 532 0 0.002 ^ NT

Celery 708 0 0.002 - 0.005 NT

Grape Juice 176 0 0.001 ^ 10.0

Peaches 285 0 0.005 ^ 15.0

Plums 507 0 0.005 ^ 15.0

Raspberries 652 0 0.005 - 0.026 NT

Raspberries, Frozen 53 0 0.005 - 0.026 NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 5,636 0

Phosmet (insecticide) 

Apple Juice 379 0 0.010 ^ 10

Baby Food - Applesauce 379 3 0.8 0.002 ^ 0.001 ^ 10

Baby Food - Peas 378 0 0.12 ^ 1

Bananas 708 0 0.049 ^ NT

Broccoli 668 0 0.005 ^ NT

Carrots (V-4) 711 4 0.6 0.005 - 0.017 0.003 - 0.010 NT

Celery 346 0 0.005 ^ NT

Grape Juice 176 14 8 0.011 - 0.015 0.010 ^ 10

Green Beans 378 0 0.010 ^ NT

Mushrooms 532 0 0.010 ^ NT

Nectarines 543 16 2.9 0.083 - 0.31 0.050 ^ 5

Appendix B. Page 56 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Peaches 285 42 14.7 0.005 - 0.45 0.005 ^ 10

Plums 507 13 2.6 0.008 - 0.032 0.005 ^ 5

Raspberries 652 0 0.005 - 0.049 NT

Raspberries, Frozen 53 0 0.005 - 0.049 NT

Summer Squash 709 0 0.005 - 0.12 NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 7,591 92

Phosmet oxygen analog (metabolite of Phosmet)

Baby Food - Peas 378 0 0.010 ^ 1

Bananas 708 0 0.006 ^ NT

Carrots 712 0 0.002 ^ NT

Green Beans 378 0 0.001 ^ NT

Nectarines 543 4 0.7 0.002 - 0.004 0.001 ^ 5

Raspberries 301 0 0.006 ^ NT

Raspberries, Frozen 43 0 0.006 ^ NT

Summer Squash 346 0 0.010 ^ NT

TOTAL 3,409 4

Phosphamidon (insecticide) 

Baby Food - Applesauce 379 0 0.010 ^ NT

Broccoli 708 0 0.010 ^ NT

Cauliflower 532 0 0.003 ^ NT

Celery 708 0 0.003 - 0.005 NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 4,030 0

Phoxim (insecticide) 

Bananas 708 0 0.049 ^ NT

Celery 346 0 0.003 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.003 - 0.049 NT

Raspberries, Frozen 53 0 0.003 - 0.049 NT

Summer Squash 363 0 0.003 ^ NT

TOTAL 2,629 0

Piperonyl butoxide (insecticide) 

Apple Juice 379 0 0.005 ^ 8

Baby Food - Applesauce 379 0 0.001 ^ 8

Baby Food - Peas 378 0 0.010 ^ 8

Bananas 708 0 0.013 ^ EX

Broccoli 707 0 0.005 ^ EX

Carrots 712 0 0.003 ^ EX

Cauliflower 532 0 0.005 ^ EX

Celery 708 6 0.8 0.008 - 0.23 0.005 ^ EX

Grape Juice 176 0 0.005 ^ 8

Green Beans 378 0 0.030 ^ 8

Mushrooms 532 19 3.6 0.007 - 0.48 0.005 ^ EX

Nectarines 543 0 0.003 ^ EX

Peaches 285 1 0.4 0.008 ^ 0.005 ^ 8

Plums 507 1 0.2 0.006 ^ 0.005 ^ 8

Raspberries 652 6 0.9 0.009 - 0.15 0.005 - 0.013 8

Raspberries, Frozen 53 0 0.005 - 0.013 8

Summer Squash 709 0 0.005 - 0.030 EX

Winter Squash 187 0 0.003 ^ EX

TOTAL 8,525 33

Pirimicarb (insecticide) 

Baby Food - Applesauce 379 0 0.005 ^ NT

Bananas 708 0 0.003 ^ NT

Appendix B. Page 57 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Broccoli 708 0 0.005 ^ NT

Cauliflower 514 0 0.001 ^ NT

Celery 708 0 0.001 - 0.010 NT

Nectarines 543 0 0.005 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.003 - 0.010 NT

Raspberries, Frozen 53 0 0.003 - 0.010 NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 5,607 0

Pirimicarb desmethyl (insecticide metabolite)

Baby Food - Applesauce 379 0 0.010 ^ NT

Bananas 708 0 0.002 ^ NT

Broccoli 708 0 0.010 ^ NT

Celery 346 0 0.003 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.002 - 0.003 NT

Raspberries, Frozen 53 0 0.002 - 0.003 NT

Summer Squash 363 0 0.003 ^ NT

TOTAL 4,001 0

Pirimiphos methyl (insecticide) 

Apple Juice 379 0 0.001 ^ NT

Baby Food - Applesauce 379 0 0.001 ^ NT

Broccoli 707 0 0.005 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.005 NT

Grape Juice 176 0 0.001 ^ NT

Mushrooms 532 0 0.001 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 5,116 0

Prallethrin (insecticide) 

Baby Food - Peas 378 0 0.10 ^ 1.0

Bananas 708 0 0.10 ^ 1.0

Carrots 712 0 0.015 ^ 1.0

Celery 346 0 0.020 ^ 1.0

Green Beans 378 0 0.20 ^ 1.0

Nectarines 543 0 0.015 ^ 1.0

Plums 507 0 0.020 ^ 1.0

Raspberries 652 0 0.020 - 0.10 1.0

Raspberries, Frozen 53 0 0.020 - 0.10 1.0

Summer Squash 709 0 0.020 - 0.10 1.0

Winter Squash 187 0 0.012 ^ 1.0

TOTAL 5,173 0

Prochloraz (fungicide) 

Baby Food - Applesauce 379 0 0.001 ^ NT

Broccoli 707 0 0.005 ^ NT

Celery 346 0 0.010 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

TOTAL 2,948 0

Appendix B. Page 58 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Procymidone (fungicide) 

Baby Food - Applesauce 379 0 0.001 ^ NT

Bananas 708 0 0.010 ^ NT

Broccoli 707 0 0.005 ^ NT

Celery 346 0 0.010 ^ NT

Grape Juice 176 0 0.010 ^ 5.0

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.010 ^ NT

Raspberries, Frozen 53 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

TOTAL 4,176 0

Profenofos (insecticide) 

Baby Food - Applesauce 379 0 0.010 ^ NT

Broccoli 708 0 0.010 ^ NT

Cauliflower 532 0 0.002 ^ NT

Celery 708 0 0.002 - 0.005 NT

Grape Juice 176 0 0.075 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

TOTAL 4,019 0

Profluralin (herbicide) 

Celery 346 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

TOTAL 1,577 0

Promecarb (insecticide) 

Celery 346 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 1,764 0

Prometryn (herbicide) 

Carrots 712 0 0.003 ^ 0.45

Cauliflower 532 0 0.001 ^ NT

Celery 708 35 4.9 0.002 - 0.024 0.001 - 0.003 0.50

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.005 ^ NT

TOTAL 3,370 35

Pronamide (herbicide) 

Apple Juice 379 0 0.002 ^ 0.1

Baby Food - Applesauce 379 0 0.001 ^ 0.1

Baby Food - Peas 378 0 0.005 ^ 0.05

Bananas 708 0 0.012 ^ NT

Broccoli (V-1) 707 1 0.1 0.007 ^ 0.005 ^ NT

Cauliflower (V-1) 532 1 0.2 0.002 ^ 0.001 ^ NT

Celery (V-2) 708 2 0.3 0.004 - 0.007 0.001 - 0.003 NT

Grape Juice 176 0 0.002 ^ 0.1

Green Beans 378 0 0.005 ^ NT

Mushrooms 532 0 0.002 ^ NT

Appendix B. Page 59 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Nectarines 543 0 0.001 ^ 0.1

Peaches 285 0 0.005 ^ 0.1

Plums 507 0 0.003 ^ 0.1

Raspberries 652 0 0.003 - 0.012 0.05

Raspberries, Frozen 53 0 0.003 - 0.012 0.05

Summer Squash (V-1) 363 1 0.3 0.003 ^ 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 7,467 5

Propachlor (herbicide) 

Cauliflower 532 0 0.001 - 0.003 NT

Celery 362 0 0.001 - 0.003 NT

TOTAL 894 0

Propamocarb hydrochloride 8

 (fungicide) 

Apple Juice 379 0 0.003 ^ NT

Baby Food - Applesauce 379 0 0.010 ^ NT

Broccoli (V-3) 708 3 0.4 0.011 - 0.041 0.010 ^ NT

Celery (V-3) 346 3 0.9 0.011 - 0.035 0.010 ^ NT

Grape Juice 148 0 0.003 ^ NT

Green Beans (V-6) 378 6 1.6 0.001 - 0.14 0.001 ^ NT

Mushrooms 532 0 0.003 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 709 76 10.7 0.006 - 0.56 0.005 - 0.010 1.5

Winter Squash 187 38 20.3 0.010 - 0.61 0.006 ^ 1.5

TOTAL 4,919 126

Propanil (herbicide) 

Celery 346 0 0.010 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

TOTAL 1,577 0

Propaquizafop (herbicide) 

Celery 346 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

TOTAL 1,577 0

Propargite (insecticide) 

Apple Juice 379 0 0.050 ^ NT

Bananas 708 0 0.018 ^ NT

Broccoli 707 0 0.020 ^ NT

Cauliflower 532 0 0.020 ^ NT

Celery 708 0 0.005 - 0.020 NT

Grape Juice 176 0 0.050 ^ 10.0

Mushrooms 532 0 0.050 ^ NT

Nectarines 543 3 0.6 0.17 - 0.52 0.030 ^ 4.0

Peaches 285 0 0.020 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.005 - 0.018 NT

Raspberries, Frozen 53 0 0.005 - 0.018 NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 6,332 3

Appendix B. Page 60 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Propetamphos (insecticide) 

Apple Juice 379 0 0.010 ^ 0.1

Baby Food - Applesauce 379 0 0.010 ^ 0.1

Baby Food - Peas 378 0 0.050 ^ 0.1

Bananas 708 0 0.010 ^ 0.1

Broccoli 708 0 0.010 ^ 0.1

Carrots 712 0 0.005 ^ 0.1

Cauliflower 532 0 0.002 ^ 0.1

Celery 708 0 0.002 - 0.005 0.1

Grape Juice 146 0 0.010 ^ 0.1

Green Beans 378 0 0.10 ^ 0.1

Mushrooms 501 0 0.010 ^ 0.1

Nectarines 543 0 0.001 ^ 0.1

Peaches 285 0 0.010 ^ 0.1

Plums 507 0 0.005 ^ 0.1

Raspberries 652 0 0.005 - 0.010 0.1

Raspberries, Frozen 53 0 0.005 - 0.010 0.1

Summer Squash 709 0 0.005 - 0.050 0.1

Winter Squash 187 0 0.003 ^ 0.1

TOTAL 8,465 0

Propham (herbicide) 

Celery 346 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.005 ^ NT

TOTAL 1,764 0

Propiconazole (fungicide) 

Apple Juice 379 0 0.010 ^ NT

Baby Food - Applesauce 379 0 0.010 ^ NT

Bananas 708 0 0.018 ^ 0.2

Broccoli 708 0 0.010 ^ NT

Carrots 712 4 0.6 0.017 ^ 0.010 ^ 0.25

Cauliflower 532 0 0.008 ^ NT

Celery 708 194 27.4 0.010 - 0.15 0.008 - 0.010 5.0

Grape Juice 176 0 0.010 ^ 1.3

Green Beans 378 0 0.005 ^ 0.70

Mushrooms 532 0 0.010 ^ 0.1

Nectarines 543 143 26.3 0.007 - 0.64 0.004 ^ 4.0

Peaches 285 130 45.6 0.011 - 0.91 0.010 ^ 4.0

Plums 507 30 5.9 0.011 - 0.39 0.010 ^ 0.60

Raspberries 652 3 0.5 0.027 - 0.13 0.010 - 0.018 1.0

Raspberries, Frozen 53 0 0.010 - 0.018 1.0

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 7,802 504

Propoxur (insecticide) 

Apple Juice 379 0 0.003 ^ NT

Mushrooms 268 0 0.003 ^ NT

TOTAL 647 0

Prothioconazole (fungicide) 

Baby Food - Peas 378 0 0.50 ^ NT

Green Beans 346 0 0.50 ^ NT

TOTAL 724 0

Prothiofos (insecticide) 

Apple Juice 379 0 0.010 ^ NT

Baby Food - Applesauce 379 0 0.001 ^ NT

Broccoli 707 0 0.005 ^ NT

Celery 346 0 0.010 ^ NT

Nectarines 543 0 0.025 ^ NT

Appendix B. Page 61 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

TOTAL 3,870 0

Pymetrozine (insecticide) 

Bananas 708 0 0.007 ^ NT

Cauliflower 532 0 0.005 ^ 0.5

Celery 708 4 0.6 0.003 - 0.005 0.003 - 0.005 0.6

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.003 - 0.007 NT

Raspberries, Frozen 53 0 0.003 - 0.007 NT

Summer Squash 363 0 0.003 ^ 0.1

Winter Squash 187 4 2.1 0.003 ^ 0.002 ^ 0.1

TOTAL 3,710 8

Pyraclostrobin (fungicide) 

Apple Juice 379 0 0.003 ^ 1.5

Baby Food - Applesauce 379 0 0.003 ^ 1.5

Baby Food - Peas 378 0 0.005 ^ 0.2

Bananas 708 0 0.001 ^ 0.04

Broccoli 708 12 1.7 0.003 - 0.48 0.003 ^ 5.0

Carrots 711 110 15.5 0.008 - 0.035 0.005 - 0.017 0.4

Cauliflower 532 0 0.004 ^ 5.0

Celery 708 124 17.5 0.003 - 0.47 0.003 - 0.004 29.0

Grape Juice 176 0 0.003 ^ 2.0

Green Beans 378 29 7.7 0.001 - 0.52 0.001 ^ 0.5

Mushrooms 532 0 0.003 ^ NT

Nectarines 542 56 10.3 0.002 - 0.10 0.001 ^ 2.5

Peaches 285 108 37.9 0.003 - 0.23 0.003 ^ 2.5

Plums 507 8 1.6 0.003 - 0.015 0.003 ^ 2.5

Raspberries 652 141 21.6 0.001 - 0.40 0.001 - 0.003 4.0

Raspberries, Frozen 53 7 13.2 0.002 - 0.34 0.001 - 0.003 4.0

Summer Squash 709 50 7.1 0.003 - 0.029 0.003 - 0.005 0.5

Winter Squash 187 5 2.7 0.003 ^ 0.002 ^ 0.5

TOTAL 8,524 650

Pyraflufen ethyl (herbicide) 

Apple Juice 379 0 0.010 ^ 0.01

Celery 346 0 0.003 ^ NT

Grape Juice 176 0 0.010 ^ 0.01

Nectarines 543 0 0.001 ^ 0.01

Plums 507 0 0.003 ^ 0.01

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 2,862 0

Pyrazophos (fungicide) 

Baby Food - Applesauce 379 0 0.010 ^ NT

Bananas 708 0 0.006 ^ NT

Broccoli 708 0 0.010 ^ NT

Celery 346 0 0.005 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.005 - 0.006 NT

Raspberries, Frozen 53 0 0.005 - 0.006 NT

Summer Squash 363 0 0.005 ^ NT

TOTAL 4,001 0

Pyrethrins (insecticide) 

Bananas 708 0 0.20 ^ 1.0

Raspberries 301 0 0.20 ^ 1.0

Appendix B. Page 62 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Raspberries, Frozen 43 0 0.20 ^ 1.0

TOTAL 1,052 0

Pyridaben (insecticide, acaricide)

Apple Juice 379 0 0.005 ^ 0.5

Baby Food - Applesauce 379 21 5.5 0.002 ^ 0.001 ^ 0.5

Bananas 708 0 0.001 ^ NT

Broccoli 707 0 0.005 ^ NT

Celery 346 0 0.003 ^ NT

Grape Juice 176 0 0.005 ^ 1.5

Mushrooms 532 0 0.005 ^ NT

Nectarines 543 5 0.9 0.002 - 0.031 0.001 ^ 2.5

Peaches 285 7 2.5 0.008 - 0.018 0.005 ^ 2.5

Plums 507 0 0.003 ^ 2.5

Raspberries 652 0 0.001 - 0.003 NT

Raspberries, Frozen (V-1) 53 1 1.9 0.004 ^ 0.001 - 0.003 NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 5,817 34

Pyrimethanil (fungicide) 

Apple Juice 379 21 5.5 0.11 - 0.23 0.10 ^ 14

Baby Food - Applesauce 379 32 8.4 0.003 - 0.13 0.003 ^ 14

Bananas 708 34 4.8 0.002 - 0.011 0.002 ^ 0.10

Broccoli 708 0 0.003 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery (V-1) 708 1 0.1 0.002 ^ 0.001 - 0.005 NT

Grape Juice 118 0 0.10 ^ 5.0

Green Beans (V-2) 378 2 0.5 0.003 - 0.006 0.001 ^ NT

Mushrooms 532 0 0.10 ^ NT

Nectarines 542 68 12.5 0.002 - 1.0 0.001 ^ 10

Peaches 285 35 12.3 0.10 - 0.58 0.003 ^ 10

Plums 507 37 7.3 0.005 - 1.4 0.005 ^ 10

Raspberries (V-14) 652 14 2.1 0.002 - 0.041 0.002 - 0.005 NT

Raspberries, Frozen (V-4) 53 4 7.5 0.007 - 0.14 0.002 - 0.005 NT

Summer Squash 709 0 0.005 - 0.10 NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 7,377 248

Pyriproxyfen (insecticide, growth regulator)

Apple Juice 379 0 0.001 ^ 0.20

Baby Food - Applesauce 357 0 0.001 ^ 0.20

Baby Food - Peas 378 0 0.010 ^ 0.20

Bananas 708 0 0.002 ^ 0.20

Broccoli 707 0 0.005 ^ 0.70

Carrots 712 0 0.001 ^ 0.15

Cauliflower 532 0 0.003 ^ 0.70

Celery 708 0 0.003 - 0.012 3.0

Grape Juice 176 0 0.001 ^ 2.5

Green Beans 378 2 0.5 0.002 - 0.003 0.001 ^ 0.20

Mushrooms 532 0 0.001 ^ 0.10

Nectarines 543 0 0.001 ^ 1.0

Peaches 285 0 0.005 ^ 1.0

Plums 507 1 0.2 0.003 ^ 0.003 ^ 1.0

Raspberries 652 0 0.002 - 0.003 1.0

Raspberries, Frozen 53 0 0.002 - 0.003 1.0

Summer Squash 709 0 0.003 - 0.010 0.10

Winter Squash 187 0 0.002 ^ 0.10

TOTAL 8,503 3

Quinalphos (insecticide) 

Baby Food - Applesauce 379 0 0.001 ^ NT

Bananas 708 0 0.003 ^ NT

Broccoli 707 0 0.005 ^ NT

Celery 346 0 0.005 ^ NT

Appendix B. Page 63 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.003 - 0.005 NT

Raspberries, Frozen 53 0 0.003 - 0.005 NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 4,187 0

Quinoxyfen (fungicide) 

Apple Juice 379 0 0.020 ^ NT

Baby Food - Applesauce 379 0 0.010 ^ NT

Broccoli 708 0 0.010 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.003 NT

Grape Juice 146 0 0.020 ^ 0.60

Mushrooms 532 0 0.020 ^ NT

Nectarines 543 6 1.1 0.002 - 0.022 0.001 ^ 0.70

Peaches 285 0 0.010 ^ 0.70

Plums 507 2 0.4 0.006 - 0.017 0.003 ^ 0.70

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash (V-4) 363 4 1.1 0.004 - 0.010 0.003 ^ NT

Winter Squash 187 8 4.3 0.003 - 0.007 0.002 ^ 0.20

TOTAL 5,630 20

Quintozene - PCNB (fungicide) (parent of HCB, PCA, PCB and PCPMS)

Apple Juice 379 0 0.004 ^ NT

Baby Food - Applesauce 379 0 0.001 ^ NT

Bananas 708 0 0.021 ^ NT

Broccoli 707 0 0.005 ^ 0.1

Carrots 712 0 0.006 ^ NT

Cauliflower 532 0 0.001 ^ 0.1

Celery 708 0 0.001 - 0.005 NT

Grape Juice 176 0 0.004 ^ NT

Green Beans 378 0 0.025 ^ 0.1

Mushrooms 532 0 0.004 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.005 - 0.021 NT

Raspberries, Frozen 53 0 0.005 - 0.021 NT

Summer Squash 709 0 0.005 - 0.050 NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 7,604 0

Quizalofop ethyl (herbicide) 

Celery 346 0 0.010 ^ NT

Green Beans 378 0 0.35 ^ 0.25

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 2,142 0

Resmethrin (insecticide) 

Baby Food - Applesauce 379 0 0.004 ^ 3.0

Baby Food - Peas 378 0 0.12 ^ 3.0

Bananas 708 0 0.028 ^ 3.0

Broccoli 687 0 0.020 ^ 3.0

Celery 346 0 0.010 ^ 3.0

Green Beans 283 0 0.20 ^ 3.0

Peaches 285 0 0.020 ^ 3.0

Plums 476 0 0.010 ^ 3.0

Raspberries 652 0 0.010 - 0.028 3.0

Raspberries, Frozen 53 0 0.010 - 0.028 3.0

Appendix B. Page 64 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Summer Squash 649 0 0.010 - 0.25 3.0

Winter Squash 187 0 0.006 ^ 3.0

TOTAL 5,083 0

Resmethrin cis (isomer of Resmethrin)

Apple Juice 379 0 0.050 ^ 3.0

Carrots 712 0 0.002 ^ 3.0

Cauliflower 518 0 0.002 ^ 3.0

Celery 346 0 0.002 ^ 3.0

Grape Juice 176 0 0.050 ^ 3.0

Mushrooms 532 0 0.050 ^ 3.0

Nectarines 543 0 0.002 ^ 3.0

TOTAL 3,206 0

Resmethrin trans (isomer of Resmethrin)

Apple Juice 379 0 0.050 ^ 3.0

Carrots 712 0 0.002 ^ 3.0

Cauliflower 532 0 0.002 ^ 3.0

Celery 362 0 0.002 ^ 3.0

Grape Juice 176 0 0.050 ^ 3.0

Mushrooms 532 0 0.050 ^ 3.0

Nectarines 543 0 0.002 ^ 3.0

TOTAL 3,236 0

Rimsulfuron (herbicide) 

Apple Juice 33 0 0.010 ^ 0.01

Mushrooms 93 0 0.010 ^ NT

Nectarines 543 0 0.003 ^ 0.01

Plums 507 0 0.010 ^ 0.01

Raspberries 351 0 0.010 ^ 0.01

Raspberries, Frozen 10 0 0.010 ^ 0.01

TOTAL 1,537 0

Rotenone (insecticide) 

Celery 346 0 0.040 ^ NT

Plums 507 0 0.040 ^ NT

Raspberries 351 0 0.040 ^ NT

Raspberries, Frozen 10 0 0.040 ^ NT

Summer Squash 363 0 0.040 ^ NT

TOTAL 1,577 0

Saflufenacil (herbicide) 

Apple Juice 379 0 0.010 ^ 0.03

Baby Food - Peas 356 0 0.010 ^ 0.03

Celery 346 0 0.010 ^ NT

Grape Juice 176 0 0.010 ^ 0.03

Green Beans 378 0 0.010 ^ 0.03

Mushrooms 532 0 0.010 ^ NT

Nectarines 543 0 0.005 ^ 0.03

Plums 507 0 0.010 ^ 0.03

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 4,128 0

Sethoxydim (herbicide) 

Apple Juice 379 0 0.003 ^ 0.2

Baby Food - Peas 378 0 0.020 ^ 10

Bananas 708 0 0.007 ^ NT

Carrots 712 0 0.001 ^ 4.0

Celery 346 0 0.005 ^ 4.0

Grape Juice 176 0 0.003 ^ 1.0

Green Beans 378 0 0.005 ^ 15

Mushrooms 532 0 0.003 ^ NT

Nectarines 543 0 0.001 ^ 0.2

Appendix B. Page 65 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.005 - 0.007 5.0

Raspberries, Frozen 53 0 0.005 - 0.007 5.0

Summer Squash 709 0 0.005 - 0.020 4.0

Winter Squash 187 0 0.003 ^ 4.0

TOTAL 6,260 0

Simazine (herbicide) 

Apple Juice 379 0 0.005 ^ 0.20

Bananas 708 0 0.005 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.005 NT

Grape Juice 176 0 0.005 ^ 0.20

Mushrooms 532 0 0.005 ^ NT

Nectarines 543 0 0.004 ^ NT

Plums 507 0 0.005 ^ 0.20

Raspberries 652 0 0.005 ^ 0.20

Raspberries, Frozen 53 0 0.005 ^ 0.20

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 5,340 0

Spinetoram (insecticide) 

Apple Juice 379 0 0.005 ^ 0.20

Bananas 708 0 0.005 ^ 0.25

Carrots 712 0 0.015 ^ 0.10

Cauliflower 532 0 0.001 ^ 2.0

Celery 708 3 0.4 0.002 - 0.018 0.001 - 0.010 8.0

Grape Juice 176 0 0.005 ^ 0.50

Green Beans 347 2 0.6 0.001 - 0.008 0.001 ^ 0.30

Mushrooms 532 0 0.005 ^ NT

Nectarines 543 49 9 0.013 - 0.16 0.008 ^ 0.20

Plums 507 0 0.010 ^ 0.20

Raspberries 652 86 13.2 0.005 - 0.37 0.005 - 0.010 0.70

Raspberries, Frozen 53 1 1.9 0.038 ^ 0.005 - 0.010 0.70

Summer Squash 363 0 0.010 ^ 0.30

Winter Squash 187 0 0.006 ^ 0.30

TOTAL 6,399 141

Spinosad (insecticide) (total of spinosyns A and D)

Baby Food - Peas 378 0 0.005 ^ 0.02

Carrots 712 0 0.005 ^ 0.10

Cauliflower 532 0 0.001 ^ 2.0

Celery 708 12 1.7 0.002 - 0.087 0.001 - 0.003 8.0

Green Beans 347 6 1.7 0.002 - 0.044 0.002 ^ 0.30

Nectarines 543 174 32 0.010 - 0.11 0.006 ^ 0.20

Plums 507 1 0.2 0.005 ^ 0.003 ^ 0.20

Raspberries 351 41 11.7 0.003 - 0.21 0.003 ^ 0.7

Raspberries, Frozen 10 0 0.003 ^ 0.7

Summer Squash 709 1 0.1 0.004 ^ 0.003 - 0.005 0.3

TOTAL 4,797 235

Spinosad A (isomer of Spinosad) 

Apple Juice 379 0 0.005 ^ 0.20

Baby Food - Applesauce 379 2 0.5 0.003 - 0.005 0.002 ^ 0.20

Bananas 708 0 0.005 ^ 0.25

Broccoli 686 2 0.3 0.009 - 0.31 0.002 ^ 2.0

Grape Juice 176 0 0.005 ^ 0.50

Mushrooms 532 0 0.005 ^ 0.02

Raspberries 301 24 8 0.008 - 0.44 0.005 ^ 0.7

Raspberries, Frozen 43 0 0.005 ^ 0.7

Winter Squash 187 0 0.002 ^ 0.3

TOTAL 3,391 28

Spinosad D (isomer of Spinosad) 

Apple Juice 379 1 0.3 0.007 ^ 0.005 ^ 0.20

Appendix B. Page 66 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Baby Food - Applesauce 379 0 0.002 ^ 0.20

Bananas 708 0 0.005 ^ 0.25

Broccoli 686 2 0.3 0.002 - 0.052 0.002 ^ 2.0

Grape Juice 176 0 0.007 ^ 0.50

Mushrooms 532 0 0.005 - 0.007 0.02

Raspberries 301 17 5.6 0.005 - 0.10 0.005 ^ 0.7

Raspberries, Frozen 43 0 0.005 ^ 0.7

Winter Squash 187 0 0.002 ^ 0.3

TOTAL 3,391 20

Spirodiclofen (acaricide) 

Apple Juice 379 0 0.010 ^ 0.80

Baby Food - Applesauce 379 0 0.010 ^ 0.80

Bananas 708 0 0.006 ^ NT

Broccoli 708 0 0.010 ^ NT

Celery 346 0 0.005 ^ NT

Grape Juice 176 0 0.010 ^ 2.0

Mushrooms 532 0 0.010 ^ NT

Nectarines 543 5 0.9 0.11 ^ 0.065 ^ 1.0

Peaches 285 88 30.9 0.010 - 0.29 0.010 ^ 1.0

Plums 507 12 2.4 0.005 - 0.017 0.005 ^ 1.0

Raspberries 652 0 0.005 - 0.006 NT

Raspberries, Frozen 53 0 0.005 - 0.006 NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 5,818 105

Spiromesifen Total (parent + enol metabolite) (insecticide) 

Cauliflower 532 0 0.006 ^ 2.0

Celery 362 0 0.008 - 0.020 6.0

TOTAL 894 0

Spiromesifen (insecticide) 

Apple Juice 379 0 0.010 ^ NT

Baby Food - Applesauce 379 0 0.002 ^ NT

Baby Food - Peas 378 0 0.020 ^ NT

Broccoli 688 0 0.002 ^ 2.0

Celery 346 0 0.005 ^ 6.0

Grape Juice 176 0 0.010 ^ NT

Green Beans 378 1 0.3 0.025 ^ 0.020 ^ 0.80

Mushrooms 532 0 0.010 ^ NT

Peaches 285 0 0.002 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries (V-1) 351 1 0.3 0.008 ^ 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 709 0 0.005 - 0.040 0.10

Winter Squash 187 0 0.003 ^ 0.10

TOTAL 5,305 2

Spirotetramat (insecticide) 

Apple Juice 379 0 0.002 ^ 0.70

Baby Food - Peas 378 0 0.010 ^ 2.5

Celery 346 4 1.2 0.003 - 0.006 0.003 ^ 9.0

Grape Juice 176 0 0.002 ^ 1.3

Green Beans 378 0 0.001 ^ 2.5

Mushrooms 532 0 0.002 ^ NT

Nectarines 543 0 0.001 ^ 4.5

Plums 507 4 0.8 0.003 - 0.008 0.003 ^ 4.5

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 709 0 0.003 - 0.010 0.30

Winter Squash 187 1 0.5 0.003 ^ 0.002 ^ 0.30

TOTAL 4,496 9

Appendix B. Page 67 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Spiroxamine (fungicide) 

Baby Food - Applesauce 379 0 0.010 ^ NT

Bananas 708 0 0.002 ^ 3.0

Broccoli 708 0 0.010 ^ NT

Celery 346 0 0.003 ^ NT

Grape Juice 176 0 0.010 ^ 1.0

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.002 - 0.003 NT

Raspberries, Frozen 53 0 0.002 - 0.003 NT

Summer Squash 363 0 0.003 ^ NT

TOTAL 4,177 0

Sulfallate (herbicide) 

Celery 346 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

TOTAL 1,577 0

Sulfentrazone (herbicide) 

Baby Food - Peas 378 0 0.15 ^ 0.15

Bananas 708 0 0.035 ^ NT

Celery 346 0 0.010 ^ NT

Green Beans 378 0 0.015 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.010 - 0.035 0.15

Raspberries, Frozen 53 0 0.010 - 0.035 0.15

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 3,572 0

Sulprofos (insecticide) 

Cauliflower 532 0 0.002 ^ NT

Celery 708 0 0.002 - 0.005 NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 2,658 0

Tebuconazole (fungicide) 

Apple Juice 379 0 0.010 ^ 0.05

Baby Food - Applesauce 379 0 0.001 ^ 0.05

Bananas 708 0 0.006 ^ 0.05

Broccoli (V-1) 707 1 0.1 0.037 ^ 0.005 ^ NT

Cauliflower 532 0 0.002 ^ NT

Celery (V-1) 708 1 0.1 0.010 ^ 0.002 - 0.010 NT

Grape Juice 176 0 0.010 ^ 5.0

Green Beans (X-1) 378 24 6.3 0.001 - 0.20 0.001 ^ 0.1

Nectarines (X-11) 543 201 37 0.002 - 3.4 0.001 ^ 1.0

Peaches 285 32 11.2 0.005 - 0.28 0.005 ^ 1.0

Plums (X-1) 507 84 16.6 0.010 - 2.5 0.010 ^ 1.0

Raspberries 652 0 0.006 - 0.010 NT

Raspberries, Frozen 53 0 0.006 - 0.010 NT

Summer Squash 709 2 0.3 0.007 - 0.009 0.005 - 0.010 0.09

Winter Squash 187 1 0.5 0.010 ^ 0.006 ^ 0.09

TOTAL 6,903 346

Tebufenozide (insecticide) 

Apple Juice 379 0 0.002 ^ 1.0

Baby Food - Applesauce 379 6 1.6 0.006 - 0.008 0.005 ^ 1.0

Bananas 708 0 0.003 ^ NT

Appendix B. Page 68 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Broccoli 528 0 0.025 ^ 5.0

Cauliflower 532 0 0.003 - 0.010 5.0

Celery 708 0 0.005 - 0.010 2.0

Grape Juice 176 0 0.002 ^ 3.0

Mushrooms 532 0 0.002 ^ NT

Peaches 285 0 0.005 - 0.050 NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.003 - 0.005 3.0

Raspberries, Frozen 53 0 0.003 - 0.005 3.0

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 5,989 6

Tebufenpyrad (insecticide, acaricide)

Apple Juice 379 0 0.010 ^ NT

Baby Food - Applesauce 379 0 0.002 ^ NT

Bananas 708 0 0.005 ^ NT

Broccoli 707 0 0.010 ^ NT

Celery 346 0 0.005 ^ NT

Grape Juice 176 0 0.010 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.005 ^ NT

Raspberries, Frozen 53 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

TOTAL 4,555 0

Tebuthiuron (herbicide) 

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.003 NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 2,658 0

Tecnazene (plant growth regulator) 

Baby Food - Applesauce 379 0 0.001 ^ NT

Broccoli 707 0 0.005 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.010 NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

TOTAL 3,842 0

Teflubenzuron (insecticide) 

Bananas 708 0 0.010 ^ NT

Raspberries 301 0 0.010 ^ NT

Raspberries, Frozen 43 0 0.010 ^ NT

TOTAL 1,052 0

Tefluthrin (insecticide) 

Apple Juice 379 0 0.002 ^ NT

Baby Food - Applesauce 379 0 0.001 ^ NT

Baby Food - Peas 378 0 0.010 ^ NT

Bananas 708 0 0.009 ^ NT

Broccoli 707 0 0.005 ^ NT

Carrots 712 0 0.002 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.003 NT

Grape Juice 176 0 0.002 ^ NT

Green Beans 378 0 0.050 ^ NT

Appendix B. Page 69 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Mushrooms 532 0 0.002 ^ NT

Nectarines 543 0 0.002 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.003 - 0.009 NT

Raspberries, Frozen 53 0 0.003 - 0.009 NT

Summer Squash 709 0 0.003 - 0.050 NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 8,525 0

Tepraloxydim (herbicide) 

Baby Food - Peas 378 0 0.060 ^ NT

Green Beans 378 0 0.005 ^ NT

TOTAL 756 0

Terbacil (herbicide) 

Apple Juice 379 0 0.010 ^ 0.3

Baby Food - Applesauce 357 0 0.002 ^ 0.3

Bananas 708 0 0.010 ^ NT

Broccoli 668 0 0.008 ^ NT

Cauliflower 514 0 0.003 ^ NT

Celery 708 0 0.003 - 0.010 NT

Grape Juice 176 0 0.010 ^ NT

Nectarines 543 0 0.020 ^ NT

Peaches 285 0 0.008 ^ 0.2

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.005 - 0.010 0.2

Raspberries, Frozen 53 0 0.005 - 0.010 0.2

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.008 ^ NT

TOTAL 6,100 0

Terbufos (insecticide) 

Celery 603 0 0.002 - 0.003 NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 2,021 0

Terbufos sulfone (metabolite of Terbufos)

Cauliflower 532 0 0.002 ^ NT

Celery 708 0 0.002 - 0.010 NT

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 2,658 0

Terbuthylazine (herbicide) 

Baby Food - Applesauce 379 0 0.001 ^ NT

Bananas 708 0 0.002 ^ NT

Broccoli 707 0 0.005 ^ NT

Celery 346 0 0.003 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 652 0 0.002 - 0.003 NT

Raspberries, Frozen 53 0 0.002 - 0.003 NT

Summer Squash 363 0 0.003 ^ NT

TOTAL 4,000 0

Terbutryn (herbicide) 

Grape Juice 176 0 0.025 ^ NT

TOTAL 176 0

Appendix B. Page 70 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Tetrachlorvinphos (insecticide) 

Baby Food - Peas 378 0 0.050 ^ NT

Cauliflower 532 0 0.003 ^ NT

Celery 708 0 0.003 - 0.005 NT

Green Beans 378 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 3,414 0

Tetraconazole (fungicide) 

Apple Juice 379 0 0.010 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.010 NT

Grape Juice 176 0 0.010 ^ 0.20

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 3,213 0

Tetradifon (insecticide) 

Apple Juice 379 0 0.010 ^ NT

Baby Food - Applesauce 357 0 0.001 ^ NT

Bananas 708 0 0.020 ^ NT

Broccoli 707 0 0.005 ^ NT

Cauliflower 532 0 0.002 ^ NT

Celery 708 0 0.002 - 0.010 NT

Grape Juice 176 0 0.010 ^ NT

Mushrooms 532 0 0.010 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.010 - 0.020 NT

Raspberries, Frozen 53 0 0.010 - 0.020 NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 6,146 0

Tetrahydrophthalimide - THPI (metabolite of Captafol and Captan)

Apple Juice 379 98 25.9 0.010 - 0.56 0.010 ^ 25.0

Cauliflower 532 0 0.004 ^ 0.05

Celery 693 0 0.004 - 0.012 0.05

Grape Juice 176 0 0.010 ^ 25.0

Mushrooms 532 0 0.010 ^ NT

Plums 507 3 0.6 0.012 - 0.024 0.010 ^ 10.0

Raspberries 351 8 2.3 0.012 - 0.29 0.010 ^ 25.0

Raspberries, Frozen 10 1 10 1.7 ^ 0.010 ^ 25.0

Summer Squash (X-2) 363 4 1.1 0.011 - 0.11 0.010 ^ 0.05

Winter Squash 187 0 0.009 ^ 0.05

TOTAL 3,730 114

Tetramethrin (insecticide) 

Apple Juice 379 0 0.005 ^ NT

Baby Food - Applesauce 379 0 0.005 ^ NT

Baby Food - Peas 378 0 0.050 ^ NT

Bananas 708 0 0.099 ^ NT

Broccoli 707 0 0.005 ^ NT

Carrots 712 0 0.001 ^ NT

Celery 346 0 0.005 ^ NT

Grape Juice 176 0 0.005 ^ NT

Green Beans 378 0 0.050 ^ NT

Mushrooms 532 0 0.005 ^ NT

Appendix B. Page 71 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Nectarines 543 0 0.001 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.005 - 0.099 NT

Raspberries, Frozen 53 0 0.005 - 0.099 NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 7,285 0

Thiabendazole (fungicide) (parent of 5-hydroxythiabendazole)

Apple Juice 379 95 25.1 0.003 - 0.27 0.003 ^ 5.0

Baby Food - Applesauce 379 26 6.9 0.019 - 0.12 0.010 ^ 5.0

Bananas 708 389 54.9 0.006 - 0.16 0.006 ^ 3.0

Broccoli 708 0 0.010 ^ NT

Carrots 712 0 0.002 ^ 10.0

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.005 NT

Grape Juice (V-1) 176 1 0.6 0.003 ^ 0.003 ^ NT

Mushrooms 532 254 47.7 0.003 - 2.0 0.003 ^ 40.0

Nectarines (V-74) 543 74 13.6 0.003 - 1.8 0.002 ^ NT

Peaches 285 0 0.010 ^ NT

Plums (V-9) 507 9 1.8 0.005 - 0.091 0.005 ^ NT

Raspberries 652 0 0.005 - 0.006 NT

Raspberries, Frozen 53 0 0.005 - 0.006 NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 7,424 848

Thiacloprid (insecticide) 

Apple Juice 379 14 3.7 0.001 - 0.002 0.001 ^ 0.30

Baby Food - Applesauce 379 8 2.1 0.010 - 0.025 0.010 ^ 0.30

Bananas 708 0 0.005 ^ NT

Broccoli 708 0 0.010 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery 693 0 0.001 - 0.003 NT

Grape Juice 176 0 0.001 ^ NT

Nectarines 543 0 0.005 ^ 0.5

Peaches 285 0 0.010 ^ 0.5

Plums 507 0 0.003 ^ 0.05

Raspberries 652 0 0.003 - 0.005 NT

Raspberries, Frozen 53 0 0.003 - 0.005 NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 6,165 22

Thiamethoxam (insecticide) (also a parent of Clothianidin)

Apple Juice 379 3 0.8 0.003 - 0.004 0.003 ^ 0.2

Baby Food - Applesauce 379 0 0.010 ^ 0.2

Baby Food - Peas 378 0 0.060 ^ 0.02

Bananas 708 0 0.010 ^ 0.02

Broccoli 708 10 1.4 0.011 - 0.076 0.010 ^ 4.5

Carrots 712 0 0.015 ^ 0.05

Cauliflower 532 4 0.8 0.008 ^ 0.005 - 0.030 4.5

Celery 708 86 12.1 0.003 - 0.16 0.003 - 0.005 4.0

Grape Juice 176 0 0.003 ^ 0.20

Green Beans 378 0 0.005 ^ 0.02

Mushrooms 532 0 0.003 ^ 0.02

Nectarines 543 0 0.025 ^ 0.5

Peaches 285 0 0.010 ^ 0.5

Plums 507 2 0.4 0.004 - 0.005 0.003 ^ 0.5

Raspberries 652 1 0.2 0.060 ^ 0.003 - 0.010 0.35

Raspberries, Frozen 53 2 3.8 0.021 - 0.025 0.003 - 0.010 0.35

Summer Squash (X-1) 709 106 15 0.003 - 0.36 0.003 - 0.060 0.2

Winter Squash 187 29 15.5 0.003 - 0.011 0.002 ^ 0.2

TOTAL 8,526 243

Appendix B. Page 72 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Thiazopyr (herbicide) 

Apple Juice 379 0 0.008 ^ NT

Grape Juice 176 0 0.008 ^ NT

Mushrooms 532 0 0.008 ^ NT

TOTAL 1,087 0

Thiobencarb (herbicide) 

Apple Juice 379 0 0.010 ^ NT

Cauliflower 532 0 0.003 ^ NT

Celery 708 0 0.003 - 0.010 0.2

Grape Juice 176 0 0.010 ^ NT

Mushrooms 532 0 0.010 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 3,745 0

Thiodicarb (insecticide) 

Apple Juice 379 0 0.003 ^ NT

Celery 346 0 0.010 ^ 35

Grape Juice 176 0 0.003 ^ NT

Mushrooms 532 0 0.003 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 2,851 0

Thionazin (insecticide, fumigant)

Celery 346 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 351 0 0.005 ^ NT

Raspberries, Frozen 10 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 1,764 0

Thiophanate methyl (fungicide) 

Green Beans 378 5 1.3 0.008 - 0.020 0.005 ^ 2.0

Summer Squash 346 0 0.040 ^ 1.0

TOTAL 724 5

Tolclofos methyl (fungicide) 

Celery 346 0 0.010 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 351 0 0.010 ^ NT

Raspberries, Frozen 10 0 0.010 ^ NT

Summer Squash 363 0 0.010 ^ NT

TOTAL 1,577 0

Tolylfluanid (fungicide) 

Bananas 708 0 0.047 ^ NT

Raspberries 301 0 0.047 ^ NT

Raspberries, Frozen 43 0 0.047 ^ NT

TOTAL 1,052 0

Tri-Allate (herbicide) 

Baby Food - Applesauce 379 0 0.001 ^ NT

Baby Food - Peas 378 0 0.050 ^ 0.2

Broccoli 707 0 0.005 ^ NT

Celery 346 0 0.003 ^ NT

Green Beans 378 0 0.075 ^ NT

Peaches 285 0 0.005 ^ NT

Appendix B. Page 73 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 363 0 0.003 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 3,891 0

Triadimefon (fungicide) (also a parent of Triadimenol)

Baby Food - Applesauce 379 0 0.001 ^ NT

Bananas 708 0 0.005 ^ NT

Broccoli 707 0 0.005 ^ NT

Cauliflower 532 0 0.003 ^ NT

Celery 708 0 0.001 - 0.010 NT

Nectarines 543 0 0.015 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.010 ^ NT

Raspberries 652 0 0.005 - 0.010 NT

Raspberries, Frozen 53 0 0.005 - 0.010 NT

Summer Squash 363 0 0.010 ^ NT

Winter Squash 187 0 0.006 ^ NT

TOTAL 5,624 0

Triadimenol (fungicide) (also a metabolite of Triadimefon)

Baby Food - Applesauce 379 0 0.001 ^ NT

Bananas 708 0 0.017 ^ 0.2

Broccoli 707 0 0.005 ^ NT

Celery 346 0 0.030 ^ NT

Nectarines 543 0 0.050 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.030 ^ NT

Raspberries 652 0 0.017 - 0.030 NT

Raspberries, Frozen 53 0 0.017 - 0.030 NT

Summer Squash 363 0 0.030 ^ NT

Winter Squash 187 0 0.018 ^ NT

TOTAL 4,730 0

Triazophos (insecticide) 

Apple Juice 379 0 0.001 ^ NT

Baby Food - Applesauce 379 0 0.002 ^ NT

Bananas 708 0 0.005 ^ NT

Broccoli 707 0 0.010 ^ NT

Celery 346 0 0.005 ^ NT

Grape Juice 176 0 0.001 ^ NT

Nectarines 543 0 0.003 ^ NT

Peaches 285 0 0.010 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.005 ^ NT

Raspberries, Frozen 53 0 0.005 ^ NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 5,285 0

Trichlorfon (insecticide) 

Apple Juice 379 0 0.010 ^ NT

Grape Juice 176 0 0.010 ^ NT

Mushrooms 532 0 0.010 ^ NT

TOTAL 1,087 0

Trifloxystrobin (fungicide) 

Apple Juice 379 0 0.003 ^ 0.5

Baby Food - Applesauce 379 0 0.005 ^ 0.5

Bananas 708 0 0.005 ^ 0.10

Broccoli 708 0 0.005 ^ NT

Carrots 712 0 0.001 ^ 0.1

Cauliflower 532 0 0.001 ^ NT

Celery 708 18 2.5 0.002 - 0.023 0.001 - 0.003 3.5

Appendix B. Page 74 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Grape Juice 176 0 0.003 ^ 2.0

Green Beans (V-6) 378 6 1.6 0.001 - 0.023 0.001 ^ NT

Mushrooms 532 0 0.003 ^ NT

Nectarines 543 7 1.3 0.005 - 0.022 0.003 ^ 2

Peaches 285 5 1.8 0.009 - 0.19 0.005 ^ 2

Plums 507 1 0.2 0.003 ^ 0.003 ^ 2

Raspberries 652 0 0.003 - 0.005 NT

Raspberries, Frozen (V-1) 53 1 1.9 0.011 ^ 0.003 - 0.005 NT

Summer Squash 709 5 0.7 0.003 - 0.012 0.003 - 0.005 0.50

Winter Squash 187 1 0.5 0.003 ^ 0.002 ^ 0.50

TOTAL 8,148 44

Trifloxysulfuron (herbicide) 

Apple Juice 379 0 0.005 ^ NT

Grape Juice 176 0 0.020 ^ NT

Mushrooms 501 0 0.005 - 0.020 NT

TOTAL 1,056 0

Triflumizole (fungicide) 

Apple Juice 379 0 0.010 ^ 0.5

Baby Food - Applesauce 379 0 0.003 ^ 0.5

Bananas 708 0 0.002 ^ NT

Broccoli 708 0 0.003 ^ 8.0

Celery 346 0 0.005 ^ NT

Grape Juice 176 0 0.010 ^ 2.5

Green Beans 378 0 0.001 ^ NT

Peaches 285 0 0.003 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.002 - 0.005 NT

Raspberries, Frozen 53 0 0.002 - 0.005 NT

Summer Squash 709 7 1 0.006 - 0.023 0.005 - 0.062 0.5

Winter Squash 187 0 0.003 ^ 0.5

TOTAL 5,467 7

Trifluralin (herbicide) 

Apple Juice 379 0 0.001 ^ NT

Baby Food - Applesauce 379 0 0.001 ^ NT

Baby Food - Peas 378 0 0.010 ^ 0.05

Bananas 708 0 0.009 ^ NT

Broccoli 707 2 0.3 0.010 - 0.013 0.005 ^ 0.05

Carrots 712 171 24 0.003 - 0.18 0.002 ^ 1.0

Cauliflower 532 1 0.2 0.002 ^ 0.001 ^ 0.05

Celery 708 13 1.8 0.002 - 0.009 0.001 - 0.005 0.05

Grape Juice 176 0 0.001 ^ 0.05

Green Beans 378 0 0.005 ^ 0.05

Mushrooms 532 0 0.001 ^ NT

Nectarines 543 0 0.002 ^ 0.05

Peaches 285 0 0.005 ^ 0.05

Plums 507 0 0.005 ^ 0.05

Raspberries 652 0 0.005 - 0.009 NT

Raspberries, Frozen 53 0 0.005 - 0.009 NT

Summer Squash 709 1 0.1 0.010 ^ 0.005 - 0.010 0.05

Winter Squash 187 0 0.006 ^ 0.05

TOTAL 8,525 188

Triforine (fungicide) 

Apple Juice 379 0 0.010 ^ NT

Grape Juice 176 0 0.010 ^ NT

Nectarines 543 0 0.025 ^ NT

TOTAL 1,098 0

Triticonazole (fungicide) 

Baby Food - Applesauce 379 0 0.010 ^ NT

Broccoli 708 0 0.010 ^ NT

Celery 346 0 0.040 ^ NT

Peaches 285 0 0.010 ^ NT

Appendix B. Page 75 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Plums 507 0 0.040 ^ NT

Raspberries 351 0 0.040 ^ NT

Raspberries, Frozen 10 0 0.040 ^ NT

Summer Squash 363 0 0.040 ^ NT

TOTAL 2,949 0

Uniconazole (insect growth regulator) 

Celery 346 0 0.040 ^ NT

Plums 507 0 0.040 ^ NT

Raspberries 351 0 0.040 ^ NT

Raspberries, Frozen 10 0 0.040 ^ NT

Summer Squash 363 0 0.040 ^ NT

Winter Squash 187 0 0.024 ^ NT

TOTAL 1,764 0

Vernolate (herbicide) 

Baby Food - Applesauce 379 0 0.010 ^ NT

Broccoli 708 0 0.010 ^ NT

Peaches 220 0 0.010 ^ NT

TOTAL 1,307 0

Vinclozolin (fungicide) 

Apple Juice 379 0 0.010 ^ NT

Baby Food - Applesauce 379 0 0.001 ^ NT

Bananas 708 0 0.010 ^ NT

Broccoli 707 0 0.005 ^ NT

Carrots 712 0 0.002 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.005 NT

Grape Juice 176 0 0.010 ^ 6.0

Mushrooms 532 0 0.010 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.005 ^ NT

Raspberries 652 0 0.005 - 0.010 NT

Raspberries, Frozen 53 0 0.005 - 0.010 NT

Summer Squash 363 0 0.005 ^ NT

Winter Squash 187 0 0.003 ^ NT

TOTAL 6,880 0

Zoxamide (fungicide) 

Celery 346 0 0.003 ^ NT

Green Beans 378 0 0.002 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 709 0 0.003 - 0.010 1.0

TOTAL 2,301 0

NOTES

^ Only one distinct detected concentration or LOD value was reported for the pair.

NT = No tolerance level was set for that pesticide/commodity pair.

EX = Exempt from the requirement of a tolerance in or on all food commodities.

SU = Safe for use in spot and/or crevice treatments in food handling establishments.

1 Emamectin benzoate is the salt form of the active, Emamectin.

2 Halosulfuron methyl is the salt form of the active, Halosulfuron.

Many of the listed tolerances are the sum of a parent compound and metabolite(s)/isomer(s). The reader is 

advised to refer to EPA for the complete listing of compounds in tolerance expressions. The cited tolerances

apply to 2013 and not to the current year. There may be instances where a tolerance was recently set or 

revoked that would have an effect on whether a residue is violative or not. 

Appendix B. Page 76 of 77
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

3 Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one of the spatial

isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable via multiresidue methods.

4 Specific tolerance established for methamidophos in cauliflower as a possible result of an acephate application.

5 Specific tolerance established for methamidophos in celery as a possible result of an acephate application.

6 Specific tolerance established for methamidophos in green beans as a possible result of an acephate application.

7 Specific tolerances for parathion methyl and its oxygen analog metabolite have been revoked since December 31, 1999, but 

are subject to a channels of trade provision per Code of Federal Regulations, Title 40, Part 180.121.

8 Propamocarb analytically determined as the salt (hydrochloride).

(X) = Residue was found which exceeds EPA tolerance or FDA action level. Following "X" are the number of occurrences. Refer to

page 1 in Appendix M to see the sample origin (domestic, imported, or unknown) for each occurrence.

(V) = Residue was found where no tolerance was established by EPA. Following "V" are the number of occurrences. Refer to

pages 2 and 3 in Appendix M to see the number of occurrences broken down by sample origin (domestic, imported, or

unknown) for a commodity/pesticide pair.

Appendix B. Page 77 of 77
Appendix C

Distribution of Residues by Pesticide

in Infant Formula

Appendix C shows residue detections for all compounds tested in dairy-based and soy-based 

infant formula, including range of values detected, range of Limits of Detection (LODs), and U.S. 

Environmental Protection Agency (EPA) tolerance references for each pair. The EPA tolerances 

cited in this appendix apply to 2013 and not to the current year. There may be instances where 

tolerances have been recently set or revoked that would have an effect on whether a residue is 

violative or not. 

In 2013, the Pesticide Data Program (PDP) analyzed 177 dairy-based formula samples and 179 

soy-based formula samples. PDP detected just one pesticide in the infant formula samples, the 

insecticide synergist MGK-264, at a concentration of 0.003 ppm where the established tolerance 

was 5 ppm.

Results for environmental contaminants across all commodities, including infant formula, have been 

consolidated in a separate appendix because they have no registered uses and are not applied to 

crops (see Appendix H). 
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Abamectin (I)

 Infant Formula, Soy-based 179 0.020 ^ 0.01

Acephate (I)

 Infant Formula, Dairy-based 177 0.002 ^ 0.1

 Infant Formula, Soy-based 179 0.010 ^ 1.0

Acetamiprid (I)

 Infant Formula, Dairy-based 177 0.001 ^ 0.30

 Infant Formula, Soy-based 179 0.003 ^ 0.03

Acetochlor (H)

 Infant Formula, Soy-based 179 0.005 ^ 1.0

Acibenzolar S methyl (L)

 Infant Formula, Dairy-based 177 0.004 - 0.012 NT

Alachlor (H)

 Infant Formula, Dairy-based 177 0.002 ^ 0.02

 Infant Formula, Soy-based 179 0.005 ^ 1.0

Aldicarb (I)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.010 ^ 0.02

Aldicarb sulfone (IM)

 Infant Formula, Dairy-based 177 0.003 - 0.010 NT

 Infant Formula, Soy-based 179 0.010 ^ 0.02

Aldicarb sulfoxide (IM)

 Infant Formula, Dairy-based 177 0.002 - 0.006 NT

 Infant Formula, Soy-based 179 0.010 ^ 0.02

Allethrin (I)

 Infant Formula, Soy-based 179 0.020 ^ EX

Ametoctradin (F)

 Infant Formula, Soy-based 179 0.003 ^ NT

Ametryn (H)

 Infant Formula, Soy-based 179 0.005 ^ NT

Atrazine (H)

 Infant Formula, Dairy-based 177 0.001 ^ 0.02

 Infant Formula, Soy-based 179 0.005 ^ NT

Azinphos ethyl (I)

 Infant Formula, Soy-based 179 0.005 ^ NT

Azinphos methyl (I)

 Infant Formula, Dairy-based 177 0.012 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ NT

Azinphos methyl oxygen analog (IM)

 Infant Formula, Soy-based 147 0.010 ^ NT

Azoxystrobin (F)

 Infant Formula, Dairy-based 177 0.001 ^ 0.006

 Infant Formula, Soy-based 179 0.003 ^ 0.5

Bendiocarb (I)

 Infant Formula, Dairy-based 177 0.001 ^ SU

 Infant Formula, Soy-based 179 0.005 ^ SU

Benfluralin (H)

 Infant Formula, Soy-based 179 0.005 ^ NT

Benoxacor (S)

 Infant Formula, Dairy-based 177 0.001 ^ 0.01

 Infant Formula, Soy-based 179 0.010 ^ 0.01

APPENDIX C. DISTRIBUTION OF RESIDUES BY PESTICIDE IN INFANT FORMULA

Appendix C. Page 1 of 16
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Bensulide (H)

 Infant Formula, Soy-based 179 0.003 ^ NT

Bifenox (H)

 Infant Formula, Soy-based 179 0.005 ^ NT

Bifenthrin (I)

 Infant Formula, Dairy-based 177 0.002 ^ 0.1

 Infant Formula, Soy-based 179 0.010 ^ 0.2

Bitertanol (F)

 Infant Formula, Soy-based 179 0.040 ^ NT

Boscalid (F)

 Infant Formula, Soy-based 179 0.005 ^ 0.1

Bromacil (H)

 Infant Formula, Soy-based 179 0.010 ^ NT

Bromopropylate (A)

 Infant Formula, Soy-based 179 0.010 ^ NT

Bromuconazole (F)

 Infant Formula, Soy-based 179 0.010 ^ NT

Bupirimate (F)

 Infant Formula, Soy-based 179 0.040 ^ NT

Buprofezin (I)

 Infant Formula, Dairy-based 177 0.001 ^ 0.01

 Infant Formula, Soy-based 179 0.005 ^ NT

Cadusafos (I)

 Infant Formula, Soy-based 179 0.003 ^ NT

Carbaryl (I)

 Infant Formula, Dairy-based 177 0.001 ^ 1.0

 Infant Formula, Soy-based 179 0.005 ^ 0.5

Carbendazim (MBC) (F)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ 0.2

Carbofuran (I)

 Infant Formula, Dairy-based 177 0.001 ^ 0.1

 Infant Formula, Soy-based 179 0.005 ^ 1.0

Carbophenothion (I)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.010 ^ NT

Carbophenothion methyl (I)

 Infant Formula, Soy-based 179 0.005 ^ NT

Carboxin (F)

 Infant Formula, Soy-based 179 0.005 ^ 0.2

Carfentrazone ethyl (H)

 Infant Formula, Dairy-based 177 0.005 ^ 0.05

 Infant Formula, Soy-based 179 0.003 ^ 0.10

Chlorantraniliprole (I)

 Infant Formula, Dairy-based 177 0.002 ^ 0.1

 Infant Formula, Soy-based 179 0.010 ^ 2.0

Chlorethoxyfos (I)

 Infant Formula, Soy-based 179 0.010 ^ NT

Chlorfenapyr (I)

 Infant Formula, Dairy-based 177 0.002 ^ 0.01

Chlorfenvinphos (I)

 Infant Formula, Dairy-based 177 0.004 ^ NT

 Infant Formula, Soy-based 179 0.010 ^ NT

Appendix C. Page 2 of 16
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Chlorobenzilate (A)

 Infant Formula, Soy-based 179 0.003 ^ NT

Chloroneb (F)

 Infant Formula, Soy-based 179 0.005 ^ 0.2

Chlorothalonil (F)

 Infant Formula, Soy-based 179 0.010 ^ 0.2

Chlorpropham (H)

 Infant Formula, Dairy-based 177 0.001 ^ 0.30

 Infant Formula, Soy-based 179 0.005 ^ NT

Chlorpyrifos (I)

 Infant Formula, Dairy-based 177 0.001 ^ 0.01

 Infant Formula, Soy-based 179 0.010 ^ 0.3

Chlorpyrifos oxygen analog (IM)

 Infant Formula, Dairy-based 177 0.001 ^ 0.01

 Infant Formula, Soy-based 179 0.010 ^ 0.3

Clethodim (H)

 Infant Formula, Dairy-based 177 0.002 ^ 0.05

Clofentezine (I)

 Infant Formula, Soy-based 179 0.020 ^ NT

Clomazone (H)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ 0.05

Clothianidin (I)

 Infant Formula, Dairy-based 177 0.002 ^ 0.02

 Infant Formula, Soy-based 179 0.005 ^ 0.02

Coumaphos (I)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ NT

Coumaphos oxygen analog (IM)

 Infant Formula, Dairy-based 177 0.008 ^ NT

Crotoxyphos (I)

 Infant Formula, Soy-based 179 0.005 ^ NT

Crufomate (I)

 Infant Formula, Soy-based 179 0.005 ^ NT

Cyazofamid (I)

 Infant Formula, Soy-based 179 0.010 ^ NT

Cyfluthrin (I)

 Infant Formula, Dairy-based 177 0.008 ^ 0.2

 Infant Formula, Soy-based 179 0.005 ^ 0.03

Cyhalothrin, Total (Cyhalothrin-L + R157836 epimer) (I)

 Infant Formula, Dairy-based 177 0.003 ^ 0.4

 Infant Formula, Soy-based 179 0.010 ^ 0.01

Cymoxanil (F)

 Infant Formula, Dairy-based 177 0.003 ^ NT

 Infant Formula, Soy-based 179 0.010 ^ NT

Cypermethrin (I)

 Infant Formula, Dairy-based 177 0.022 ^ 0.10

 Infant Formula, Soy-based 179 0.010 ^ 0.05

Cyphenothrin (I)

 Infant Formula, Soy-based 179 0.010 ^ NT

Cyproconazole (F)

 Infant Formula, Soy-based 179 0.010 ^ 0.05

Cyprodinil (F)

 Infant Formula, Soy-based 179 0.003 ^ 0.6

Appendix C. Page 3 of 16
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

DCPA (H)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ 2.0

DEF (Tribufos) (H)

 Infant Formula, Soy-based 179 0.003 ^ NT

Deltamethrin (includes parent Tralomethrin) (I)

 Infant Formula, Dairy-based 177 0.012 - 0.040 0.02

 Infant Formula, Soy-based 179 0.005 ^ 0.1

Demeton-O (IM)

 Infant Formula, Soy-based 179 0.020 ^ NT

Demeton-S (IM)

 Infant Formula, Soy-based 179 0.030 ^ NT

Demeton-S sulfone (IM)

 Infant Formula, Soy-based 147 0.003 ^ NT

Dialifos (I)

 Infant Formula, Soy-based 179 0.005 ^ NT

Diazinon (I)

 Infant Formula, Soy-based 179 0.003 ^ NT

Diazinon oxygen analog (IM)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ NT

Dichlobenil (H)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ NT

Dichlorvos (DDVP) (I)

 Infant Formula, Dairy-based 177 0.003 ^ 0.02

 Infant Formula, Soy-based 179 0.020 ^ 0.5

Dicloran (F)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.010 ^ NT

Dicofol o,p' (I)

 Infant Formula, Dairy-based 177 0.002 ^ 0.75

 Infant Formula, Soy-based 179 0.010 ^ 0.5

Dicofol p,p' (I)

 Infant Formula, Dairy-based 177 0.001 ^ 0.75

 Infant Formula, Soy-based 179 0.005 ^ 0.5

Dicrotophos (I)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ NT

Diethofencarb (F)

 Infant Formula, Soy-based 179 0.003 ^ NT

Difenoconazole (F)

 Infant Formula, Dairy-based 177 0.003 ^ 0.01

 Infant Formula, Soy-based 179 0.005 ^ 0.15

Diflubenzuron (I)

 Infant Formula, Dairy-based 177 0.002 ^ 0.05

 Infant Formula, Soy-based 179 0.020 ^ 0.05

Dimethenamid (H)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ 0.01

Dimethoate (I)

 Infant Formula, Dairy-based 177 0.002 ^ 0.002

 Infant Formula, Soy-based 179 0.003 ^ 2.0

Appendix C. Page 4 of 16
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Dimethomorph (F)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ NT

Diniconazole (F)

 Infant Formula, Soy-based 179 0.020 ^ NT

Dinotefuran (I)

 Infant Formula, Dairy-based 177 0.006 ^ 0.05

 Infant Formula, Soy-based 179 0.010 ^ 0.01

Dioxathion (I)

 Infant Formula, Soy-based 179 0.020 ^ NT

Diphenamid (H)

 Infant Formula, Dairy-based 177 0.002 ^ NT

Diphenylamine (DPA) (F)

 Infant Formula, Dairy-based 177 0.003 ^ 0.01

 Infant Formula, Soy-based 179 0.003 ^ NT

Disulfoton (I)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.010 ^ NT

Disulfoton oxon (IM)

 Infant Formula, Dairy-based 177 0.002 ^ NT

Disulfoton sulfone (IM)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ NT

Disulfoton sulfone oxygen analog (IM)

 Infant Formula, Dairy-based 177 0.003 ^ NT

Disulfoton sulfoxide (IM)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ NT

Disulfoton sulfoxide oxygen analog (IM)

 Infant Formula, Dairy-based 177 0.001 ^ NT

Diuron (H)

 Infant Formula, Dairy-based 177 0.008 ^ NT

 Infant Formula, Soy-based 179 0.020 ^ NT

DMST (4-dimethylaminosulphotosluidide) (FM)

 Infant Formula, Soy-based 179 0.003 ^ NT

Dodine (F)

 Infant Formula, Soy-based 179 0.020 ^ NT

Emamectin (I)

 Infant Formula, Soy-based 179 0.010 ^ NT

Emamectin benzoate (I)

 Infant Formula, Dairy-based 177 0.001 ^ 0.003

Endosulfan I (I)

 Infant Formula, Dairy-based 177 0.006 ^ NT

 Infant Formula, Soy-based 179 0.010 ^ 2.0

Endosulfan II (IM)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.010 ^ 2.0

Endosulfan sulfate (IM)

 Infant Formula, Dairy-based 177 0.012 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ 2.0

Epoxiconazole (F)

 Infant Formula, Soy-based 179 0.005 ^ NT

EPTC (H)

 Infant Formula, Dairy-based 177 0.001 ^ NT

Appendix C. Page 5 of 16
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Esfenvalerate+Fenvalerate Total (I)

 Infant Formula, Dairy-based 177 0.002 ^ 0.3

 Infant Formula, Soy-based 179 0.005 ^ 0.05

Ethalfluralin (H)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ 0.05

Ethion (I)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ NT

Ethion mono oxon (IM)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 147 0.003 ^ NT

Ethofumesate (H)

 Infant Formula, Soy-based 179 0.003 ^ NT

Ethoprop (I)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ NT

Ethylan (I)

 Infant Formula, Soy-based 179 0.003 ^ NT

Etofenprox (I)

 Infant Formula, Soy-based 179 0.003 ^ NT

Etoxazole (A)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ NT

Etridiazole (F)

 Infant Formula, Soy-based 179 0.020 ^ 0.1

Famoxadone (F)

 Infant Formula, Soy-based 179 0.010 ^ NT

Fenamidone (F)

 Infant Formula, Dairy-based 177 0.002 ^ 0.02

 Infant Formula, Soy-based 179 0.010 ^ 0.02

Fenamiphos (I)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ NT

Fenamiphos sulfone (IM)

 Infant Formula, Dairy-based 177 0.004 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ NT

Fenamiphos sulfoxide (IM)

 Infant Formula, Dairy-based 177 0.004 ^ NT

 Infant Formula, Soy-based 179 0.020 ^ NT

Fenarimol (F)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ NT

Fenazaquin (I)

 Infant Formula, Soy-based 179 0.003 ^ NT

Fenbuconazole (F)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.010 ^ NT

Fenchlorphos (I)

 Infant Formula, Soy-based 179 0.003 ^ NT

Fenhexamid (F)

 Infant Formula, Soy-based 179 0.040 ^ NT

Appendix C. Page 6 of 16
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Fenitrothion (I)

 Infant Formula, Dairy-based 177 0.003 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ NT

Fenobucarb (BPMC) (I)

 Infant Formula, Soy-based 179 0.005 ^ NT

Fenpropathrin (I)

 Infant Formula, Dairy-based 177 0.003 ^ 0.08

 Infant Formula, Soy-based 179 0.005 ^ NT

Fenpropimorph (F)

 Infant Formula, Soy-based 179 0.003 ^ NT

Fenpyroximate (A)

 Infant Formula, Dairy-based 177 0.001 - 0.003 0.015

Fensulfothion (I)

 Infant Formula, Soy-based 179 0.005 ^ NT

Fenthion (I)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ NT

Fipronil (I)

 Infant Formula, Dairy-based 177 0.002 ^ 0.05

Flonicamid (I)

 Infant Formula, Dairy-based 177 0.001 ^ 0.03

 Infant Formula, Soy-based 179 0.030 ^ NT

Fluazifop butyl (H)

 Infant Formula, Dairy-based 177 0.001 ^ 0.05

 Infant Formula, Soy-based 179 0.003 ^ 2.5

Fludioxonil (F)

 Infant Formula, Dairy-based 177 0.012 ^ 0.01

 Infant Formula, Soy-based 179 0.010 ^ 0.4

Flufenacet (H)

 Infant Formula, Soy-based 179 0.010 ^ 0.1

Flufenoxuron (I)

 Infant Formula, Soy-based 179 0.010 ^ NT

Flumioxazin (H)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.020 ^ 0.02

Fluopicolide (F)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ NT

Fluoxastrobin (F)

 Infant Formula, Dairy-based 177 0.001 ^ 0.02

 Infant Formula, Soy-based 179 0.003 ^ 0.05

Fluquinconazole (F)

 Infant Formula, Soy-based 179 0.010 ^ NT

Fluridone (H)

 Infant Formula, Soy-based 179 0.003 ^ 0.1

Flusilazole (F)

 Infant Formula, Soy-based 179 0.003 ^ 0.04

Flutolanil (F)

 Infant Formula, Soy-based 179 0.003 ^ 0.20

Flutriafol (F)

 Infant Formula, Soy-based 179 0.010 ^ 0.35

Fluvalinate (I)

 Infant Formula, Soy-based 179 0.010 ^ NT

Appendix C. Page 7 of 16
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Fonofos (I)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ NT

Forchlorfenuron (P)

 Infant Formula, Soy-based 179 0.003 ^ NT

Formetanate hydrochloride (I)

 Infant Formula, Soy-based 179 0.010 ^ NT

Fosthiazate (T)

 Infant Formula, Soy-based 179 0.003 ^ NT

Hexaconazole (F)

 Infant Formula, Soy-based 179 0.020 ^ NT

Hexythiazox (I)

 Infant Formula, Soy-based 179 0.005 ^ NT

Hydroprene (R)

 Infant Formula, Soy-based 179 0.010 ^ 0.2

3-Hydroxycarbofuran (IM)

 Infant Formula, Dairy-based 177 0.001 ^ 0.1

 Infant Formula, Soy-based 179 0.010 ^ 1.0

5-Hydroxythiabendazole (FM)

 Infant Formula, Soy-based 179 0.005 ^ 0.1

Imazalil (F)

 Infant Formula, Dairy-based 177 0.001 ^ 0.02

 Infant Formula, Soy-based 179 0.005 ^ NT

Imidacloprid (I)

 Infant Formula, Dairy-based 177 0.003 ^ 0.10

 Infant Formula, Soy-based 179 0.010 ^ 3.5

Imiprothrin (I)

 Infant Formula, Soy-based 179 0.010 ^ NT

Indaziflam (H)

 Infant Formula, Soy-based 179 0.003 ^ NT

Indoxacarb (I)

 Infant Formula, Soy-based 179 0.010 ^ 0.80

Iprodione (F)

 Infant Formula, Soy-based 179 0.005 ^ 2.0

Iprovalicarb (F)

 Infant Formula, Soy-based 179 0.005 ^ NT

Isofenphos (I)

 Infant Formula, Soy-based 179 0.003 ^ NT

Isoprocarb (I)

 Infant Formula, Soy-based 179 0.010 ^ NT

Isoproturon (H)

 Infant Formula, Soy-based 179 0.003 ^ NT

Kresoxim-methyl (F)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.010 ^ NT

Lactofen (H)

 Infant Formula, Soy-based 179 0.005 ^ 0.01

Lenacil (H)

 Infant Formula, Soy-based 179 0.005 ^ NT

Leptophos oxygen analog (IM)

 Infant Formula, Soy-based 179 0.020 ^ NT

Lindane (BHC gamma) (I)

 Infant Formula, Dairy-based 177 0.001 ^ 0.3 AL

 Infant Formula, Soy-based 179 0.003 ^ 0.5

Appendix C. Page 8 of 16
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Linuron (H)

 Infant Formula, Dairy-based 177 0.003 ^ 0.05

 Infant Formula, Soy-based 179 0.010 ^ 1.0

Malathion (I)

 Infant Formula, Dairy-based 177 0.001 ^ 0.5

 Infant Formula, Soy-based 179 0.005 ^ 8

Malathion oxygen analog (IM)

 Infant Formula, Dairy-based 177 0.010 ^ 0.5

 Infant Formula, Soy-based 179 0.003 ^ 8

Mandipropamid (F)

 Infant Formula, Dairy-based 177 0.015 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ NT

Melamine (RM)

 Infant Formula, Dairy-based 177 0.015 ^ 0.05

Mepanipyrim (F)

 Infant Formula, Soy-based 179 0.005 ^ NT

Metalaxyl/Mefenoxam (F) 

 Infant Formula, Dairy-based 177 0.001 ^ 0.02

 Infant Formula, Soy-based 179 0.003 ^ 1.0

Metconazole (F)

 Infant Formula, Soy-based 179 0.010 ^ 0.05

Methamidophos (I)

 Infant Formula, Dairy-based 177 0.004 ^ 0.1

 Infant Formula, Soy-based 179 0.005 ^ 1.0

Methidathion (I)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ NT

Methiocarb (I)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.010 ^ NT

Methiocarb sulfoxide (IM)

 Infant Formula, Soy-based 179 0.005 ^ NT

Methomyl (I)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.020 ^ 0.2

Methoprene (R)

 Infant Formula, Dairy-based 177 0.050 ^ EX

Methoxychlor Total (I)

 Infant Formula, Dairy-based 177 0.001 ^ NT

Methoxychlor olefin (IM)

 Infant Formula, Dairy-based 177 0.001 ^ NT

Methoxychlor p,p' (IM)

 Infant Formula, Soy-based 179 0.005 ^ NT

Methoxyfenozide (I)

 Infant Formula, Dairy-based 177 0.001 ^ 0.10

 Infant Formula, Soy-based 179 0.005 ^ 1.0

Metolachlor (H)

 Infant Formula, Dairy-based 177 0.001 ^ 0.02

 Infant Formula, Soy-based 179 0.003 ^ 0.20

Metribuzin (H)

 Infant Formula, Dairy-based 177 0.002 ^ 0.05

 Infant Formula, Soy-based 179 0.005 ^ 0.3

Appendix C. Page 9 of 16
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Mevinphos (I)

 Infant Formula, Dairy-based 177 0.005 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ NT

MGK-264 (I)

 Infant Formula, Soy-based 179 1 0.6 0.003 ^ 0.003 ^ 5

Monocrotophos (I)

 Infant Formula, Soy-based 179 0.005 ^ NT

Myclobutanil (F)

 Infant Formula, Dairy-based 177 0.001 ^ 0.2

 Infant Formula, Soy-based 179 0.010 ^ 0.25

Napropamide (H)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ NT

Nitrofen (H)

 Infant Formula, Soy-based 179 0.005 ^ NT

Norflurazon (H)

 Infant Formula, Dairy-based 177 0.001 ^ 0.1

 Infant Formula, Soy-based 179 0.010 ^ 0.1

Norflurazon desmethyl (HM)

 Infant Formula, Dairy-based 177 0.001 ^ 0.1

 Infant Formula, Soy-based 179 0.010 ^ 0.1

Novaluron (I)

 Infant Formula, Dairy-based 177 0.001 ^ 1.0

 Infant Formula, Soy-based 179 0.080 ^ 0.07

Omethoate (IM)

 Infant Formula, Dairy-based 177 0.002 ^ 0.002

 Infant Formula, Soy-based 179 0.005 ^ 2.0

Oxadiazon (H)

 Infant Formula, Soy-based 179 0.003 ^ NT

Oxadixyl (F)

 Infant Formula, Dairy-based 177 0.003 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ NT

Oxamyl (I)

 Infant Formula, Dairy-based 177 0.002 - 0.006 NT

 Infant Formula, Soy-based 179 0.010 ^ 0.1

Oxamyl oxime (IM)

 Infant Formula, Soy-based 179 0.020 ^ 0.1

Oxydemeton methyl (I)

 Infant Formula, Soy-based 179 0.003 ^ NT

Oxydemeton methyl sulfone (IM)

 Infant Formula, Dairy-based 177 0.012 ^ 0.01

 Infant Formula, Soy-based 179 0.005 ^ NT

Oxyfluorfen (H)

 Infant Formula, Dairy-based 177 0.001 ^ 0.01

 Infant Formula, Soy-based 179 0.010 ^ 0.05

Paclobutrazol (P)

 Infant Formula, Soy-based 179 0.010 ^ NT

Parathion (I)

 Infant Formula, Dairy-based 177 0.003 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ NT

Parathion methyl (I)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ 0.1

Appendix C. Page 10 of 16
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Parathion methyl oxygen analog (IM)

 Infant Formula, Dairy-based 177 0.005 ^ NT

 Infant Formula, Soy-based 179 0.010 ^ 0.1

Parathion oxygen analog (IM)

 Infant Formula, Dairy-based 177 0.003 ^ NT

 Infant Formula, Soy-based 179 0.010 ^ NT

Penconazole (F)

 Infant Formula, Soy-based 179 0.010 ^ NT

Pencycuron (F)

 Infant Formula, Soy-based 179 0.005 ^ NT

Pendimethalin (H)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ 0.10

Pentachloroaniline (PCA) (FM)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ 0.1

Pentachlorobenzene (PCB) (FM)

 Infant Formula, Dairy-based 177 0.008 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ 0.1

Penthiopyrad (F)

 Infant Formula, Soy-based 147 0.003 ^ 0.40

Permethrin cis (IM)

 Infant Formula, Dairy-based 177 0.001 ^ 0.88

 Infant Formula, Soy-based 179 0.005 ^ 0.05

Permethrin trans (IM)

 Infant Formula, Dairy-based 177 0.001 ^ 0.88

 Infant Formula, Soy-based 179 0.005 ^ 0.05

Phenothrin (I)

 Infant Formula, Dairy-based 177 0.002 ^ 0.01

 Infant Formula, Soy-based 179 0.005 ^ 0.01

Phenthoate (I)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ NT

Phorate (I)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.010 ^ 0.05

Phorate oxygen analog (IM)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 147 0.005 ^ 0.05

Phorate sulfone (IM)

 Infant Formula, Dairy-based 177 0.003 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ 0.05

Phorate sulfoxide (IM)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ 0.05

Phosalone (I)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ NT

Phosmet (I)

 Infant Formula, Soy-based 179 0.005 ^ NT

Phosphamidon (I)

 Infant Formula, Dairy-based 177 0.003 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ NT

Appendix C. Page 11 of 16
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Phoxim (I)

 Infant Formula, Soy-based 179 0.003 ^ NT

Piperonyl butoxide (I)

 Infant Formula, Dairy-based 177 0.005 ^ 0.25

Pirimicarb (I)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.010 ^ NT

Pirimicarb desmethyl (IM)

 Infant Formula, Soy-based 179 0.003 ^ NT

Pirimiphos methyl (I)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ NT

Prallethrin (I)

 Infant Formula, Soy-based 179 0.020 ^ 1.0

Prochloraz (F)

 Infant Formula, Soy-based 179 0.010 ^ NT

Procymidone (F)

 Infant Formula, Soy-based 179 0.010 ^ NT

Profenofos (I)

 Infant Formula, Dairy-based 177 0.002 ^ 0.01

 Infant Formula, Soy-based 179 0.005 ^ NT

Profluralin (H)

 Infant Formula, Soy-based 179 0.005 ^ NT

Promecarb (I)

 Infant Formula, Soy-based 179 0.005 ^ NT

Prometryn (H)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ NT

Pronamide (H)

 Infant Formula, Dairy-based 177 0.001 ^ 0.02

 Infant Formula, Soy-based 179 0.003 ^ NT

Propachlor (H)

 Infant Formula, Dairy-based 177 0.001 ^ 0.02

Propamocarb hydrochloride (F)

 Infant Formula, Soy-based 179 0.010 ^ NT

Propanil (H)

 Infant Formula, Soy-based 150 0.010 ^ NT

Propaquizafop (H)

 Infant Formula, Soy-based 179 0.005 ^ NT

Propargite (I)

 Infant Formula, Dairy-based 177 0.006 ^ 0.08

 Infant Formula, Soy-based 179 0.005 ^ 0.2

Propetamphos (I)

 Infant Formula, Dairy-based 177 0.002 ^ 0.1

 Infant Formula, Soy-based 179 0.005 ^ 0.1

Propham (H)

 Infant Formula, Soy-based 179 0.005 ^ NT

Propiconazole (F)

 Infant Formula, Dairy-based 177 0.008 ^ 0.05

 Infant Formula, Soy-based 179 0.010 ^ 2.0

Prothiofos (I)

 Infant Formula, Soy-based 179 0.010 ^ NT

Appendix C. Page 12 of 16
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Pymetrozine (I)

 Infant Formula, Dairy-based 177 0.005 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ NT

Pyraclostrobin (F)

 Infant Formula, Dairy-based 177 0.004 ^ 0.1

 Infant Formula, Soy-based 179 0.003 ^ 0.04

Pyraflufen ethyl (H)

 Infant Formula, Soy-based 179 0.003 ^ 0.01

Pyrazophos (F)

 Infant Formula, Soy-based 179 0.005 ^ NT

Pyridaben (I)

 Infant Formula, Soy-based 179 0.003 ^ NT

Pyrimethanil (F)

 Infant Formula, Dairy-based 177 0.001 ^ 0.05

 Infant Formula, Soy-based 179 0.005 ^ NT

Pyriproxyfen (I)

 Infant Formula, Dairy-based 177 0.003 ^ 0.10

 Infant Formula, Soy-based 179 0.003 ^ 0.20

Quinalphos (I)

 Infant Formula, Soy-based 179 0.005 ^ NT

Quinoxyfen (F)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ NT

Quintozene (PCNB) (F)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ 0.1

Quizalofop ethyl (H)

 Infant Formula, Soy-based 179 0.010 ^ 0.05

Resmethrin (I)

 Infant Formula, Soy-based 179 0.010 ^ 3.0

Resmethrin cis (IM)

 Infant Formula, Dairy-based 177 0.002 ^ 3.0

Resmethrin trans (IM)

 Infant Formula, Dairy-based 177 0.002 ^ 3.0

Rotenone (I)

 Infant Formula, Soy-based 179 0.040 ^ NT

Sethoxydim (H)

 Infant Formula, Soy-based 179 0.005 ^ 16

Simazine (H)

 Infant Formula, Dairy-based 177 0.001 ^ 0.03

 Infant Formula, Soy-based 179 0.005 ^ NT

Spinetoram (I)

 Infant Formula, Dairy-based 177 0.001 ^ 0.30

 Infant Formula, Soy-based 179 0.010 ^ 0.04

Spinosad (I)

 Infant Formula, Dairy-based 177 0.001 ^ 7.0

 Infant Formula, Soy-based 179 0.003 - 0.005 0.02

Spirodiclofen (A)

 Infant Formula, Soy-based 179 0.005 ^ NT

Spiromesifen (I)

 Infant Formula, Soy-based 179 0.005 ^ 0.02

Spirotetramat (I)

 Infant Formula, Soy-based 179 0.003 ^ 5.0

Appendix C. Page 13 of 16
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Spiroxamine (F)

 Infant Formula, Soy-based 179 0.003 ^ NT

Sulfallate (H)

 Infant Formula, Soy-based 179 0.005 ^ NT

Sulfentrazone (H)

 Infant Formula, Soy-based 179 0.010 ^ 0.15

Sulprofos (I)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ NT

Tebuconazole (F)

 Infant Formula, Dairy-based 177 0.002 ^ 0.1

 Infant Formula, Soy-based 179 0.010 ^ 0.08

Tebufenozide (I)

 Infant Formula, Dairy-based 177 0.010 ^ 0.04

 Infant Formula, Soy-based 179 0.005 ^ NT

Tebufenpyrad (I)

 Infant Formula, Soy-based 179 0.005 ^ NT

Tebuthiuron (H)

 Infant Formula, Dairy-based 177 0.001 ^ 0.8

 Infant Formula, Soy-based 179 0.003 ^ NT

Tecnazene (P)

 Infant Formula, Dairy-based 177 0.003 ^ NT

 Infant Formula, Soy-based 179 0.010 ^ NT

Tefluthrin (I)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.003 ^ NT

Terbacil (H)

 Infant Formula, Dairy-based 177 0.003 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ NT

Terbufos (I)

 Infant Formula, Soy-based 179 0.003 ^ NT

Terbufos sulfone (IM)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.010 ^ NT

Terbuthylazine (H)

 Infant Formula, Soy-based 179 0.003 ^ NT

Tetrachlorvinphos (I)

 Infant Formula, Dairy-based 177 0.003 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ NT

Tetraconazole (F)

 Infant Formula, Dairy-based 177 0.001 ^ 0.03

 Infant Formula, Soy-based 179 0.010 ^ 0.15

Tetradifon (I)

 Infant Formula, Dairy-based 177 0.002 ^ NT

 Infant Formula, Soy-based 179 0.010 ^ NT

Tetrahydrophthalimide (THPI) (FM)

 Infant Formula, Dairy-based 177 0.004 ^ 0.10

 Infant Formula, Soy-based 179 0.010 ^ 0.05

Tetramethrin (I)

 Infant Formula, Soy-based 179 0.005 ^ NT

Thiabendazole (F)

 Infant Formula, Dairy-based 177 0.001 ^ 0.1

 Infant Formula, Soy-based 179 0.005 ^ 0.1

Appendix C. Page 14 of 16
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Thiacloprid (I)

 Infant Formula, Dairy-based 177 0.003 ^ 0.030

 Infant Formula, Soy-based 179 0.003 ^ NT

Thiamethoxam (I)

 Infant Formula, Dairy-based 177 0.005 ^ 0.02

 Infant Formula, Soy-based 179 0.003 ^ 0.02

Thiobencarb (H)

 Infant Formula, Dairy-based 177 0.003 ^ 0.05

 Infant Formula, Soy-based 179 0.010 ^ NT

Thiodicarb (I)

 Infant Formula, Soy-based 179 0.010 ^ 0.2

Thionazin (I)

 Infant Formula, Soy-based 179 0.005 ^ NT

Tolclofos methyl (F)

 Infant Formula, Soy-based 179 0.010 ^ NT

Tri Allate (H)

 Infant Formula, Soy-based 179 0.003 ^ NT

Triadimefon (F)

 Infant Formula, Dairy-based 177 0.003 ^ NT

 Infant Formula, Soy-based 179 0.010 ^ NT

Triadimenol (F)

 Infant Formula, Soy-based 179 0.030 ^ NT

Triazophos (I)

 Infant Formula, Soy-based 179 0.005 ^ NT

Trifloxystrobin (F)

 Infant Formula, Dairy-based 177 0.001 ^ 0.02

 Infant Formula, Soy-based 179 0.003 ^ 0.08

Triflumizole (F)

 Infant Formula, Soy-based 179 0.005 ^ NT

Trifluralin (H)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ 0.05

Triticonazole (F)

 Infant Formula, Soy-based 179 0.040 ^ NT

Uniconazole (R)

 Infant Formula, Soy-based 179 0.040 ^ NT

Vinclozolin (F)

 Infant Formula, Dairy-based 177 0.001 ^ NT

 Infant Formula, Soy-based 179 0.005 ^ NT

Zoxamide (F)

 Infant Formula, Soy-based 179 0.003 ^ NT

Many of the listed tolerances are the sum of a parent compound and metabolite(s)/isomer(s). The reader is 

advised to refer to EPA for the complete listing of compounds in tolerance expressions. The cited tolerances

apply to 2013 and not to the current year. There may be instances where a tolerance was recently set or 

revoked that would have an effect on whether a residue is violative or not. 

Appendix C. Page 15 of 16
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

NOTES

^ = Only one distinct detected concentration or LOD value was reported for the pair.

NT = No tolerance level was set for that pesticide/commodity pair.

EX = Exempt from the requirement of a tolerance in or on all food commodities.

SU = Safe for use in spot and/or crevice treatments in food handling establishments.

AL = Number shown is an Action Level established by FDA. Under the Food Quality Protection Act, responsibility for

 establishing tolerances in lieu of action levels has been transferred to EPA. In the interim, action levels are used.

Pesticide Types:

A = Acaricide

F = Fungicide, FM = Fungicide Metabolite

H = Herbicide, HM = Herbicide Metabolite

I = Insecticide, IM = Insecticide Metabolite

L = Plant Activator

P = Plant Growth Regulator

R = Insect Growth Regulator, RM = Insect Growth Regulator Metabolite

S = Herbicide Safener

T = Nematicide

Appendix C. Page 16 of 16
Appendix D

Distribution of Residues by Pesticide

in Butter 

Appendix D shows residue detections for all compounds tested in butter, including range of 

values detected, range of Limits of Detection (LODs), and U.S. Environmental Protection 

Agency (EPA) tolerance references for each pair. The EPA tolerances cited in this appendix 

apply to 2013 and not to the current year. There may be instances where tolerances have 

been recently set or revoked that would have an effect on whether a residue is violative or 

not. 

In 2013, the Pesticide Data Program (PDP) analyzed 756 butter samples. PDP detected 

eight different residues (including metabolites), representing seven pesticides, in the butter 

samples. All residue detections were lower than the established tolerances for those 

compounds with established tolerances.

The Pesticide Data Program reports tolerance violations to the U.S. Food and Drug 

Administration (FDA) as part of an interagency Memorandum of Understanding between 

the U.S. Department of Agriculture and FDA. Residues reported to FDA are shown in the 

“Pesticide/Commodity” column to the right of the commodity and are annotated as “X” (if the 

residue exceeded the established tolerance) or “V” (if the residue did not have a tolerance 

listed in the Code of Federal Regulations, Title 40, Part 180). In both cases, these annotations 

are followed by a number indicating the number of samples reported to FDA. 

Results for environmental contaminants across all commodities, including butter, have been 

consolidated in a separate appendix because they have no registered uses and are not 

applied to crops (see Appendix H). PDP detected one environmental contaminant, DDE p,p’, 

in the butter samples.
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Acephate I 740 0.002 - 0.012 0.02

Acetamiprid I 756 0.001 ^ 0.01

Acibenzolar S methyl L 756 0.015 ^ NT

Alachlor H 756 0.002 ^ NT

Aldicarb I 756 0.001 - 0.004 NT

Aldicarb sulfone IM 707 0.004 - 0.024 NT

Aldicarb sulfoxide IM 756 0.002 - 0.007 NT

Atrazine H 756 0.004 - 0.007 NT

Azinphos methyl I 756 0.001 ^ NT

Azoxystrobin F 739 0.001 ^ NT

Bendiocarb I 756 0.005 ^ SU

Benoxacor S 756 0.001 ^ NT

Bifenthrin I 756 112 14.8 0.003 - 0.006 0.002 ^ 1.0

Buprofezin I 756 0.001 ^ NT

Carbaryl I 756 0.001 ^ NT

Carbendazim (MBC) F 756 0.001 ^ NT

Carbofuran I 756 0.001 ^ NT

Carfentrazone ethyl H 756 0.005 - 0.018 NT

Chlorantraniliprole I 756 0.002 ^ NT

Chlorfenapyr I 738 0.003 ^ 0.01

Chlorfenvinphos total I 756 0.004 ^ NT

Chlorpropham (V-2) H 756 2 0.3 0.002 - 0.004 0.001 - 0.004 NT

Chlorpyrifos I 756 0.001 ^ 0.25

Chlorpyrifos oxygen analog IM 756 0.001 - 0.004 0.25

Clethodim H 724 0.009 ^ NT

Clomazone H 756 0.003 ^ NT

Clothianidin I 756 0.002 - 0.012 NT

Coumaphos I 756 0.002 ^ 0.5

Coumaphos oxygen analog IM 756 0.009 ^ 0.5

Cyfluthrin I 756 0.009 - 0.060 5.0

Cyhalothrin, Total (Cyhalothrin-L + R157836 

epimer) I 756 154 20.4 0.006 - 0.036 0.004 - 0.012 10.0

Cymoxanil F 756 0.002 - 0.006 NT

Cypermethrin I 756 0.027 - 0.090 2.5

Cyromazine R 634 0.003 - 0.010 NT

DCPA H 756 0.001 ^ NT

Diazinon I 505 0.001 ^ NT

Diazinon oxygen analog IM 740 0.001 ^ NT

Dichlobenil H 756 0.003 ^ NT

Dichlorvos (DDVP) I 756 0.004 ^ 0.5

Dicloran F 739 0.003 - 0.009 NT

Dicofol o,p' I 756 0.003 ^ 22.0

Dicofol p,p' I 756 0.001 ^ 22.0

Dicrotophos I 756 0.002 ^ NT

Difenoconazole F 756 0.004 ^ NT

Diflubenzuron I 756 0.002 - 0.006 NT

Dimethenamid H 756 0.001 ^ NT

APPENDIX D. DISTRIBUTION OF RESIDUES BY PESTICIDE IN BUTTER

Appendix D. Page 1 of 4
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Dimethoate I 756 0.003 - 0.010 NT

Dimethomorph F 756 0.001 ^ NT

Dinotefuran I 756 0.007 - 0.024 0.01

Diphenamid H 756 0.003 ^ NT

Diphenylamine (DPA) F 756 0.004 ^ NT

Disulfoton I 756 0.009 ^ NT

Disulfoton oxon IM 756 0.010 ^ NT

Disulfoton sulfone IM 756 0.002 ^ NT

Disulfoton sulfone oxygen analog IM 740 0.001 - 0.007 NT

Disulfoton sulfoxide IM 756 0.002 ^ NT

Disulfoton sulfoxide oxygen analog IM 756 0.001 - 0.007 NT

Diuron H 756 0.009 ^ NT

Emamectin benzoate I 756 0.001 ^ NT

Endosulfan I I 756 0.007 ^ 2.0

Endosulfan II IM 739 0.001 ^ 2.0

Endosulfan sulfate IM 756 0.015 - 0.030 2.0

EPTC H 671 0.007 ^ NT

Ethalfluralin H 756 0.027 ^ NT

Ethion I 739 0.005 ^ 0.5

Ethion mono oxon IM 756 0.002 ^ 0.5

Ethoprop I 756 0.001 ^ NT

Etoxazole A 724 0.004 ^ 0.01

Famoxadone F 723 0.004 - 0.007 0.06

Fenamidone F 756 0.003 ^ NT

Fenamiphos I 756 0.001 ^ NT

Fenamiphos sulfone IM 756 0.004 ^ NT

Fenamiphos sulfoxide IM 756 0.004 ^ NT

Fenarimol F 756 0.003 - 0.009 NT

Fenbuconazole F 756 0.001 ^ NT

Fenhexamid F 756 0.011 ^ NT

Fenitrothion I 756 0.004 - 0.024 NT

Fenpropathrin I 756 0.004 ^ 2.0

Fenpyroximate A 537 0.004 - 0.007 NT

Fenthion I 756 0.010 ^ NT

Flonicamid I 756 0.001 - 0.004 NT

Fludioxonil F 738 0.014 ^ NT

Flumioxazin H 756 0.001 ^ NT

Fluopicolide F 756 0.001 ^ NT

Fluoxastrobin F 756 0.001 ^ 0.50

Hydroprene R 756 0.006 ^ 0.2

3-Hydroxycarbofuran IM 739 0.005 ^ NT

Imazalil F 756 0.011 ^ NT

Imidacloprid I 756 0.001 ^ NT

Kresoxim-methyl F 741 0.012 ^ NT

Lindane (BHC gamma) I 756 0.001 ^ 0.3 AL

Linuron H 756 0.004 - 0.012 NT

Malathion I 756 0.003 ^ 0.5

Malathion oxygen analog IM 756 0.002 ^ 0.5

Mandipropamid F 756 0.005 - 0.018 NT

Appendix D. Page 2 of 4
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Metalaxyl/Mefenoxam * F 739 0.001 ^ NT

Methamidophos I 756 0.001 ^ 0.02

Methidathion oxygen analog IM 756 0.004 ^ NT

Methiocarb I 756 0.004 ^ NT

Methomyl I 742 0.003 - 0.010 NT

Methoxychlor Total I 689 0.001 - 0.014 NT

Methoxychlor olefin IM 756 0.011 ^ NT

Methoxyfenozide I 756 0.001 ^ NT

Metolachlor H 756 0.001 ^ NT

Metribuzin H 756 0.002 ^ NT

Mevinphos Total I 740 0.002 - 0.060 NT

Myclobutanil F 756 0.001 ^ NT

Napropamide H 741 0.002 - 0.012 NT

Novaluron I 723 269 37.2 0.002 - 0.013 0.001 ^ 20

Omethoate IM 740 0.003 - 0.010 NT

Oxadixyl F 721 0.012 ^ NT

Oxamyl I 739 0.002 - 0.007 NT

Oxydemeton methyl sulfone IM 756 0.014 ^ NT

Oxyfluorfen H 738 0.001 ^ NT

Parathion I 756 0.004 - 0.012 NT

Parathion methyl I 756 0.003 - 0.019 NT

Parathion methyl oxygen analog IM 756 0.005 ^ NT

Parathion oxygen analog IM 756 0.004 ^ NT

Pendimethalin H 756 0.001 - 0.004 NT

Pentachloroaniline (PCA) FM 756 0.001 ^ NT

Pentachlorobenzene (PCB) FM 756 0.009 ^ NT

Pentachlorophenyl methyl sulfide FM 756 0.001 ^ NT

Permethrin cis IM 756 206 27.2 0.002 - 0.008 0.001 - 0.004 3.0

Permethrin trans IM 756 214 28.3 0.002 - 0.010 0.001 - 0.005 3.0

Phenothrin I 756 0.003 - 0.009 0.01

Phenthoate I 756 0.001 - 0.005 NT

Phorate I 756 0.002 - 0.014 NT

Phorate oxygen analog IM 756 0.001 ^ NT

Phorate sulfone IM 756 0.004 ^ NT

Phorate sulfoxide IM 756 0.002 ^ NT

Phosalone I 756 0.003 ^ NT

Phosphamidon I 756 0.004 ^ NT

Piperonyl butoxide I 756 16 2.1 0.009 ^ 0.005 ^ 0.25

Pirimicarb I 756 0.001 - 0.004 NT

Pirimiphos methyl I 756 0.001 ^ NT

Profenofos I 756 0.002 ^ NT

Prometryn H 756 0.001 ^ NT

Pronamide H 756 0.001 - 0.004 NT

Propachlor H 756 0.001 - 0.004 NT

Propetamphos I 756 0.002 ^ 0.1

Propiconazole F 756 0.030 ^ NT

Pymetrozine I 756 0.005 ^ NT

Pyrimethanil F 756 0.001 ^ NT

Pyriproxyfen I 756 0.004 ^ 0.10

Appendix D. Page 3 of 4
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Quinoxyfen F 756 0.001 ^ NT

Quintozene (PCNB) F 756 0.001 - 0.004 NT

Resmethrin cis IM 739 0.003 ^ 3.0

Resmethrin trans IM 756 0.003 ^ 3.0

Simazine H 756 0.001 ^ NT

Spinetoram I 756 0.001 - 0.004 7.5

Spinosad I 756 24 3.2 0.002 - 0.013 0.001 - 0.004 85

Sulprofos I 724 0.007 - 0.014 NT

Tebuconazole F 756 0.007 ^ NT

Tebufenozide I 756 0.012 ^ NT

Tebuthiuron H 756 0.001 ^ NT

Tecnazene P 756 0.001 ^ NT

Tefluthrin I 756 0.001 ^ NT

Terbacil H 756 0.004 ^ NT

Terbufos sulfone IM 756 0.003 ^ NT

Tetrachlorvinphos I 756 0.004 ^ 0.05

Tetraconazole F 756 0.001 ^ 0.75

Tetradifon I 756 0.003 ^ NT

Tetrahydrophthalimide (THPI) FM 756 0.015 ^ NT

Thiabendazole F 725 0.001 - 0.004 NT

Thiacloprid I 756 0.001 - 0.004 NT

Thiamethoxam I 756 0.005 - 0.018 0.02

Thiobencarb H 742 0.004 ^ NT

Triadimefon F 756 0.004 ^ NT

Trifluralin H 756 0.001 ^ NT

Vinclozolin F 756 0.001 ^ NT

NOTES

^ = Only one distinct detected concentration or LOD value was reported for the pair.

NT = No tolerance level was set for that pesticide/commodity pair.

SU = Safe for use in spot and/or crevice treatments in food handling establishments.

AL = Number shown is an Action Level established by FDA. Under the Food Quality Protection Act, responsibility for

 establishing tolerances in lieu of action levels has been transferred to EPA. In the interim, action levels are used.

(V) = Residue was found where no tolerance was established by EPA. Following "V" are the number of occurrences. 

 Refer to pages 2 and 3 in Appendix M to see the number of occurrences broken down by sample origin

 (domestic, imported, or unknown) for a commodity/pesticide pair.

* = Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one

 of the spatial isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable 

 via multiresidue methods.

Pesticide Types:

A = Acaricide L = Plant Activator

F = Fungicide, FM = Fungicide Metabolite P = Plant Growth Regulator

H = Herbicide R = Insect Growth Regulator

I = Insecticide, IM = Insecticide Metabolite S = Herbicide Safener

Many of the listed tolerances are the sum of a parent compound and metabolite(s)/isomer(s). The reader is 

advised to refer to EPA for the complete listing of compounds in tolerance expressions. The cited tolerances apply 

to 2013 and not to the current year. There may be instances where a tolerance was recently set or revoked that 

Appendix D. Page 4 of 4
Appendix E

Distribution of Residues by Pesticide

in Salmon

Appendix E shows residue detections for all compounds tested in salmon, including range 

of values detected, range of Limits of Detection (LODs), and U.S. Environmental Protection 

Agency (EPA) tolerance references for each pair. The EPA tolerances cited in this appendix 

apply to 2013 and not to the current year. There may be instances where tolerances have 

been recently set or revoked that would have an effect on whether a residue is violative or not. 

In 2013, the Pesticide Data Program (PDP) analyzed 352 salmon samples. PDP detected 

three different residues (including metabolites), representing three pesticides, in the salmon 

samples. 

Results for environmental contaminants across all commodities, including salmon, have 

been consolidated in a separate appendix because they have no registered uses and are not 

applied to crops (see Appendix H). PDP detected one environmental contaminant, DDT p,p’, 

in the salmon samples.
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of Values 

Detected, ppm

Range of 

LODs, ppm

EPA 

Tolerance 

Level, ppm

Acetamiprid I 293 0.002 ^ 0.01

Acetochlor H 352 0.005 ^ NA

Acibenzolar S methyl L 58 0.020 ^ NA

Acrinathrin I 352 0.010 ^ NA

Aldicarb sulfone IM 88 0.005 ^ NA

Aldicarb sulfoxide IM 29 0.005 ^ NA

Allethrin I 59 0.025 ^ EX

Atrazine H 352 0.002 ^ NA

Azinphos methyl I 294 0.010 ^ NA

Azinphos methyl oxygen analog IM 352 1 0.3 0.045 ^ 0.010 ^ NA

Azoxystrobin F 235 0.002 ^ NA

Bendiocarb I 235 0.003 ^ SU

Benfluralin H 352 0.010 ^ NA

Benoxacor S 235 0.010 ^ NA

Bensulide H 235 0.004 ^ NA

Bensulide oxygen analog HM 235 0.002 ^ NA

Bifenthrin I 352 0.005 ^ 0.05

Boscalid F 235 0.003 ^ NA

Bromacil H 206 0.003 ^ NA

Bupirimate F 59 0.001 ^ NA

Buprofezin I 117 0.001 ^ NA

Carbaryl I 352 0.003 ^ NA

Carbendazim (MBC) F 264 1 0.4 0.001 ^ 0.001 ^ NA

Carbofuran I 352 0.002 ^ NA

Carfentrazone ethyl H 293 0.005 ^ 0.30

Chlorantraniliprole I 323 0.010 ^ NA

Chlorfenapyr I 352 0.015 ^ 0.01

Chlorpropham H 352 0.020 ^ NA

Chlorpyrifos I 352 0.005 ^ 0.1

Chlorpyrifos oxygen analog IM 264 0.002 ^ 0.1

Clomazone H 352 0.005 ^ NA

Clothianidin I 293 0.010 ^ NA

Coumaphos I 352 0.010 ^ NA

Coumaphos oxygen analog IM 294 0.010 ^ NA

Cyfluthrin I 352 0.004 ^ 0.05

Cyhalothrin, Total (Cyhalothrin-L + R157836 epimer) I 352 0.005 ^ 0.01

Cymoxanil F 206 0.005 ^ NA

Cypermethrin I 352 1 0.3 0.018 ^ 0.010 ^ 0.05

Cyphenothrin I 352 0.015 ^ NA

Cyproconazole F 88 0.010 ^ NA

Cyprodinil F 88 0.005 ^ NA

DCPA H 352 0.002 ^ NA

APPENDIX E. DISTRIBUTION OF RESIDUES BY PESTICIDE IN SALMON

Appendix E. Page 1 of 5
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of Values 

Detected, ppm

Range of 

LODs, ppm

EPA 

Tolerance 

Level, ppm

DEF (Tribufos) H 352 0.002 ^ NA

Deltamethrin (includes parent Tralomethrin) I 352 0.015 ^ 0.05

Diazinon I 323 0.005 ^ NA

Dichlobenil H 352 0.010 ^ NA

Dichlorvos (DDVP) I 323 0.020 ^ 0.5

Diclofop methyl H 352 0.001 ^ NA

Dicloran F 322 0.016 ^ NA

Dicofol p,p' I 352 0.010 ^ NA

Difenoconazole F 88 0.010 ^ NA

Diflubenzuron I 264 0.002 ^ NA

Dimethenamid H 323 0.002 ^ NA

Dimethoate I 88 0.005 ^ NA

Dimethomorph F 88 0.003 ^ NA

Dinotefuran I 113 0.003 ^ 0.01

Diphenylamine (DPA) F 352 0.002 ^ NA

Disulfoton oxon IM 352 0.001 ^ NA

Disulfoton sulfone IM 352 0.020 ^ NA

Disulfoton sulfoxide IM 352 0.005 ^ NA

Diuron H 323 0.002 ^ 2.0 1

Endosulfan I I 352 0.010 ^ NA

Endosulfan II IM 352 0.015 ^ NA

Endosulfan sulfate IM 322 0.005 ^ NA

Esfenvalerate+Fenvalerate Total I 322 0.005 ^ 0.05

Ethalfluralin H 352 0.005 ^ NA

Ethion I 206 0.001 ^ NA

Ethion mono oxon IM 206 0.001 ^ NA

Ethoprop I 176 0.002 ^ NA

Etoxazole A 88 0.005 ^ NA

Famoxadone F 323 0.025 ^ NA

Fenamidone F 323 0.005 ^ NA

Fenazaquin I 59 0.005 ^ NA

Fenbuconazole F 264 0.005 ^ NA

Fenhexamid F 352 0.013 ^ NA

Fenpropathrin I 352 0.020 ^ NA

Fenpyroximate A 294 0.005 ^ NA

Fipronil sulfone (MB46136) IM 352 0.050 ^ NA

Flonicamid I 293 0.006 ^ NA

Flubendiamide I 352 0.035 ^ NA

Fludioxonil F 352 0.025 ^ NA

Flufenoxuron I 235 0.001 ^ NA

Flumioxazin H 177 0.010 ^ 1.5 2

Fluopicolide F 352 0.015 ^ NA

Fluquinconazole F 206 0.010 ^ NA

Fluridone H 234 0.001 ^ 0.5

Appendix E. Page 2 of 5
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of Values 

Detected, ppm

Range of 

LODs, ppm

EPA 

Tolerance 

Level, ppm

Flusilazole F 177 0.010 ^ NA

Flutolanil F 323 0.002 ^ NA

Flutriafol F 146 0.010 ^ NA

Fluvalinate I 352 0.050 ^ NA

Folpet F 59 0.030 ^ NA

Hexythiazox I 352 0.002 ^ NA

Hydroprene R 264 0.10 ^ 0.2

3-Hydroxycarbofuran IM 323 0.003 ^ NA

Imidacloprid I 323 0.003 ^ 0.05

Imiprothrin I 352 0.010 ^ NA

Indaziflam H 176 0.001 ^ NA

Indoxacarb I 352 0.020 ^ NA

Iprodione F 352 0.040 ^ NA

Kresoxim-methyl F 206 0.010 ^ NA

Lindane (BHC gamma) I 352 0.013 ^ NA

Linuron H 235 0.003 ^ NA

Lufenuron I 206 0.020 ^ NA

Malathion I 323 0.002 ^ NA

Malathion oxygen analog IM 293 0.002 ^ NA

Mandipropamid F 265 0.002 ^ NA

Metalaxyl/Mefenoxam * F 352 0.001 ^ NA

Methidathion I 352 0.010 ^ NA

Methiocarb sulfone IM 206 0.001 ^ NA

Methiocarb sulfoxide IM 206 0.001 ^ NA

Methomyl I 323 0.030 ^ NA

Methoxyfenozide I 294 0.003 ^ NA

Metolachlor H 293 0.001 ^ NA

Metribuzin H 264 0.005 ^ NA

Mevinphos I 293 0.002 ^ NA

MGK-264 I 352 0.10 ^ 5

Mirex I 323 0.001 ^ NA

Myclobutanil F 323 0.003 ^ NA

Napropamide H 352 0.005 ^ NA

Norflurazon H 265 0.002 ^ NA

Norflurazon desmethyl HM 352 0.005 ^ NA

Oryzalin H 177 0.020 ^ NA

Oxadiazon H 352 0.010 ^ NA

Oxamyl I 88 0.003 ^ NA

Oxamyl oxime IM 83 0.003 ^ NA

Oxydemeton methyl sulfone IM 352 0.002 ^ NA

Oxyfluorfen H 352 0.050 ^ NA

Paclobutrazol P 147 0.010 ^ NA

Parathion I 352 0.005 ^ NA

Parathion methyl I 352 0.010 ^ NA

Appendix E. Page 3 of 5
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of Values 

Detected, ppm

Range of 

LODs, ppm

EPA 

Tolerance 

Level, ppm

Parathion methyl oxygen analog IM 323 0.020 ^ NA

Pendimethalin H 352 0.050 ^ NA

Pentachloroaniline (PCA) FM 352 0.004 ^ NA

Pentachlorobenzene (PCB) FM 352 0.005 ^ NA

Pentachlorophenyl methyl sulfide FM 352 0.005 ^ NA

Permethrin cis IM 352 0.010 ^ NA

Permethrin trans IM 352 0.010 ^ NA

Phenothrin I 352 0.050 ^ 0.01

o-Phenylphenol F 352 0.005 ^ NA

Phorate I 352 0.010 ^ NA

Phorate oxygen analog IM 323 0.010 ^ NA

Phorate sulfone IM 322 0.010 ^ NA

Phorate sulfoxide IM 352 0.010 ^ NA

Phosalone I 206 0.001 ^ NA

Phosmet I 352 0.010 ^ NA

Piperonyl butoxide I 352 0.005 ^ EX

Pirimiphos methyl I 263 0.001 ^ NA

Pronamide H 352 0.002 ^ NA

Propargite I 352 0.050 ^ NA

Propetamphos I 322 0.010 ^ 0.1

Propiconazole F 293 0.010 ^ NA

Prothiofos I 146 0.010 ^ NA

Pyraclostrobin F 293 0.003 ^ NA

Pyraflufen ethyl H 206 0.010 ^ NA

Pyridaben I 352 0.005 ^ NA

Pyrimethanil F 234 0.050 ^ NA

Pyriproxyfen I 235 0.001 ^ 0.10

Quinoxyfen F 352 0.020 ^ NA

Quintozene (PCNB) F 352 0.004 ^ NA

Resmethrin cis IM 352 0.050 ^ 3.0

Resmethrin trans IM 352 0.050 ^ 3.0

Saflufenacil H 323 0.010 ^ NA

Sethoxydim H 322 0.003 ^ NA

Simazine H 323 0.005 ^ NA

Spirodiclofen A 323 0.010 ^ NA

Spiromesifen I 352 0.010 ^ NA

Spirotetramat I 88 0.002 ^ NA

Tebuconazole F 88 0.010 ^ NA

Tebufenozide I 323 0.002 ^ NA

Tebufenpyrad I 206 0.010 ^ NA

Tefluthrin I 352 0.002 ^ NA

Terbacil H 352 0.010 ^ NA

Terbutryn H 352 0.025 ^ NA

Tetraconazole F 206 0.010 ^ NA

Appendix E. Page 4 of 5
Pesticide

Pest. 

Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples 

with Detects

Range of Values 

Detected, ppm

Range of 

LODs, ppm

EPA 

Tolerance 

Level, ppm

Tetradifon I 352 0.010 ^ NA

Tetrahydrophthalimide (THPI) FM 352 0.010 ^ NA

Tetramethrin I 352 0.005 ^ NA

Thiacloprid I 206 0.001 ^ NA

Thiamethoxam I 323 0.003 ^ 0.02

Thiazopyr H 294 0.008 ^ NA

Thiobencarb H 352 0.010 ^ NA

Triazophos I 206 0.001 ^ NA

Trichlorfon I 323 0.010 ^ NA

Trifloxystrobin F 235 0.002 ^ NA

Trifloxysulfuron H 147 0.020 ^ NA

Triflumizole F 88 0.010 ^ NA

Trifluralin H 352 0.001 ^ NA

Triforine F 206 0.010 ^ NA

Vinclozolin F 352 0.010 ^ NA

NOTES

^ = Only one distinct detected concentration or LOD value was reported for the pair.

NA = Findings in salmon are covered by tolerances established for fish, by tolerances set for pesticide uses in food 

 handling establishments, and by action levels set for persistent chemicals commonly found in the enviroment.

 In addition, there are other findings that may arise from a number of attributable sources including runoff from

 agricultural uses to water sources or ponds. For the latter group, where no specific tolerance has been

 established, “NA” has been entered as the tolerance value.

EX = Exempt from the requirement of a tolerance in or on all food commodities.

SU = Safe for use in spot and/or crevice treatments in food handling establishments.

1 = Specific tolerance for Diuron in freshwater, farm-raised finfish.

2 = Specific tolerance for Flumioxazin in freshwater fish.

* = Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one

 of the spatial isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable 

 via multiresidue methods.

Pesticide Types:

A = Acaricide

F = Fungicide, FM = Fungicide Metabolite

H = Herbicide, HM = Herbicide Metabolite

I = Insecticide, IM = Insecticide Metabolite

L = Plant Activator

P = Plant Growth Regulator

R = Insect Growth Regulator

S = Herbicide Safener

Many of the listed tolerances are the sum of a parent compound and metabolite(s)/isomer(s). The reader is advised to refer to EPA for the complete listing of compounds in tolerance expressions. The cited tolerances apply to 2013 and not to the current year. There may be instances where a tolerance was recently set or revoked that would have an effect on whether a residue is violative or not. 

Appendix E. Page 5 of 5
Appendix F

Distribution of Residues by Pesticide

in Groundwater

Appendix F shows residue detections for all compounds tested in groundwater, including range 

of values detected and range of Limits of Detection (LODs) for each pair in parts per trillion (ppt). 

The U.S. Environmental Protection Agency (EPA) Human Health Benchmarks for Pesticides 

(HHBPs) are also shown.

In 2013, the Pesticide Data Program (PDP) analyzed 14 groundwater samples from 14 different 

collection sites, including 3 from school/childcare wells and 11 from private residential wells. 

PDP detected 25 different residues (including metabolites), representing 17 pesticides, in the 

groundwater samples. Most of the detections were for herbicides. The samples with detectable 

residues came from seven different sites.

The HHBP values were developed for compounds with no established EPA Maximum Contaminant 

Levels (MCLs) or Health Advisory (HA) values for drinking water, enabling citizens to better 

determine whether the detection of a pesticide in drinking water or source waters for drinking 

water may indicate a potential health risk. The HHBP values can be referenced at http://www.

epa.gov/pesticides/hhbp/. 

Results for environmental contaminants across all commodities, including groundwater, have 

been consolidated in a separate appendix because they have no registered uses and are not 

applied to crops (see Appendix H).
Pesticide (Type) / Commodity - Well Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples w/ 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA HHBP, 

ppt 1

2,4,5-T (H)

 Groundwater - Private Residence Wells 11 15 ^

 Groundwater - School/Daycare Wells 3 0.84 - 15

2,4,5-TP (H)

 Groundwater - Private Residence Wells 11 15 ^

 Groundwater - School/Daycare Wells 3 0.68 - 15

2,4-D (H)

 Groundwater - Private Residence Wells 11 1 9.1 4.2 ^ 2.5 ^

 Groundwater - School/Daycare Wells 3 1 33.3 9.5 ^ 0.65 - 2.5

2,4-DB (H)

 Groundwater - Private Residence Wells 11 6.0 ^

 Groundwater - School/Daycare Wells 3 6.0 - 39

Acetamiprid (I)

 Groundwater - Private Residence Wells 11 7.5 ^ 497,000

 Groundwater - School/Daycare Wells 3 1.7 - 7.5 497,000

Acetochlor (H)

 Groundwater - Private Residence Wells 11 10 ^ 140,000

 Groundwater - School/Daycare Wells 3 9.2 - 10 140,000

Acetochlor ethanesulfonic acid (HM)

 Groundwater - Private Residence Wells 11 1 9.1 39 ^ 9.0 ^

 Groundwater - School/Daycare Wells 3 1 33.3 2.7 ^ 1.6 - 9.0

Acetochlor oxanilic acid (HM)

 Groundwater - Private Residence Wells 11 10 ^

 Groundwater - School/Daycare Wells 3 1.4 - 10

Alachlor (H)

 Groundwater - Private Residence Wells 11 10 ^

 Groundwater - School/Daycare Wells 3 7.8 - 10

Alachlor ethanesulfonic acid (HM)

 Groundwater - Private Residence Wells 11 1 9.1 778 ^ 12.5 ^

 Groundwater - School/Daycare Wells 3 1 33.3 14 ^ 1.7 - 12.5

Alachlor oxanilic acid (HM)

 Groundwater - Private Residence Wells 11 10 ^

 Groundwater - School/Daycare Wells 3 1 33.3 2.9 ^ 0.61 - 10

Aldicarb sulfone (IM)

 Groundwater - Private Residence Wells 11 4.5 ^

 Groundwater - School/Daycare Wells 3 4.5 - 7.6

Aldicarb sulfoxide (IM)

 Groundwater - Private Residence Wells 11 15 ^

 Groundwater - School/Daycare Wells 3 15 ^

Aminopyralid (H)

 Groundwater - School/Daycare Wells 2 4.5 ^ 3,500,000

Atrazine (H)

 Groundwater - Private Residence Wells 11 1 9.1 86 ^ 10 ^

 Groundwater - School/Daycare Wells 3 1 33.3 41 ^ 0.66 - 10

Azinphos methyl (I)

 Groundwater - School/Daycare Wells 2 10 ^ 11,000

Azinphos methyl oxygen analog (IM)

 Groundwater - Private Residence Wells 11 7.5 ^

 Groundwater - School/Daycare Wells 3 4.5 - 7.5

Azoxystrobin (F)

 Groundwater - Private Residence Wells 11 1 9.1 11.8 ^ 3.0 ^ 1,260,000

 Groundwater - School/Daycare Wells 3 0.80 - 3.0 1,260,000

APPENDIX F. DISTRIBUTION OF RESIDUES BY PESTICIDE IN GROUNDWATER

Appendix F. Page 1 of 11
Pesticide (Type) / Commodity - Well Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples w/ 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA HHBP, 

ppt 1

Benfluralin (H)

 Groundwater - Private Residence Wells 11 50 ^ 35,000

 Groundwater - School/Daycare Wells 3 3.6 - 50 35,000

Bensulfuron methyl (H)

 Groundwater - Private Residence Wells 11 5.0 ^ 1,400,000

 Groundwater - School/Daycare Wells 3 1.5 - 5.0 1,400,000

Bentazon (H)

 Groundwater - Private Residence Wells 11 1.5 ^

 Groundwater - School/Daycare Wells 3 1 33.3 0.73 ^ 0.18 - 1.5

Bifenthrin (I)

 Groundwater - Private Residence Wells 11 10 ^

 Groundwater - School/Daycare Wells 3 3.2 - 10

Boscalid (F)

 Groundwater - Private Residence Wells 11 60 ^ 1,526,000

 Groundwater - School/Daycare Wells 1 60 ^ 1,526,000

Bromacil (H)

 Groundwater - Private Residence Wells 11 9.0 ^

 Groundwater - School/Daycare Wells 3 1.2 - 9.0

Bromuconazole 46 (trans) (FM)

 Groundwater - Private Residence Wells 11 3.0 ^

 Groundwater - School/Daycare Wells 3 3.0 - 3.2

Bromuconazole 47 (cis) (FM)

 Groundwater - Private Residence Wells 11 3.0 ^

 Groundwater - School/Daycare Wells 3 3.0 - 5.4

Butachlor (H)

 Groundwater - School/Daycare Wells 2 1.9 ^

Butylate (H)

 Groundwater - School/Daycare Wells 2 1.8 ^

Carbaryl (I)

 Groundwater - Private Residence Wells 11 7.5 ^

 Groundwater - School/Daycare Wells 3 1.2 - 7.5

Carbendazim (MBC) (F)

 Groundwater - Private Residence Wells 11 3.0 ^ 175,000

 Groundwater - School/Daycare Wells 1 3.0 ^ 175,000

Carbofuran (I)

 Groundwater - Private Residence Wells 11 4.0 ^

 Groundwater - School/Daycare Wells 3 0.41 - 4.0

Chlorantraniliprole (I)

 Groundwater - Private Residence Wells 11 15 ^ 11,060,000

 Groundwater - School/Daycare Wells 3 3.0 - 15 11,060,000

Chlorfenvinphos (I)

 Groundwater - School/Daycare Wells 2 9.6 ^

Chlorimuron ethyl (H)

 Groundwater - Private Residence Wells 11 6.0 ^ 630,000

 Groundwater - School/Daycare Wells 3 5.7 - 6.0 630,000

Chlorothalonil (F)

 Groundwater - Private Residence Wells 11 30 ^

 Groundwater - School/Daycare Wells 3 5.2 - 30

Chlorpyrifos (I)

 Groundwater - Private Residence Wells 11 30 ^

 Groundwater - School/Daycare Wells 3 3.0 - 30

Chlorpyrifos oxygen analog (IM)

 Groundwater - Private Residence Wells 11 12 ^

 Groundwater - School/Daycare Wells 3 12 - 21

Appendix F. Page 2 of 11
Pesticide (Type) / Commodity - Well Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples w/ 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA HHBP, 

ppt 1

Chlorsulfuron (H)

 Groundwater - School/Daycare Wells 2 1.7 ^ 140,000

Clomazone (H)

 Groundwater - Private Residence Wells 11 30 ^ 5,880,000

 Groundwater - School/Daycare Wells 1 30 ^ 5,880,000

Clopyralid (H)

 Groundwater - Private Residence Wells 11 12.5 ^ 1,050,000

 Groundwater - School/Daycare Wells 3 8.1 - 12.5 1,050,000

Clothianidin (I)

 Groundwater - Private Residence Wells 11 7.5 ^ 686,000

 Groundwater - School/Daycare Wells 3 4.8 - 7.5 686,000

Coumaphos (I)

 Groundwater - Private Residence Wells 11 15 ^ 2,000

 Groundwater - School/Daycare Wells 3 1.7 - 15 2,000

Coumaphos oxygen analog (IM)

 Groundwater - Private Residence Wells 11 9.0 ^

 Groundwater - School/Daycare Wells 3 1.6 - 9.0

Cyanazine (H)

 Groundwater - Private Residence Wells 11 50 ^

 Groundwater - School/Daycare Wells 3 0.78 - 50

Cycloate (H)

 Groundwater - School/Daycare Wells 2 3.3 ^ 35,000

Cyfluthrin (I)

 Groundwater - Private Residence Wells 11 100 ^ 168,000

 Groundwater - School/Daycare Wells 3 40 - 100 168,000

Cyhalothrin, Lambda (I)

 Groundwater - Private Residence Wells 11 50 ^ 7,000

 Groundwater - School/Daycare Wells 1 50 ^ 7,000

Cyhalothrin, Total (Cyhalothrin-L + R157836 epimer) (I)

 Groundwater - School/Daycare Wells 2 42 ^ 7,000

Cypermethrin (I)

 Groundwater - School/Daycare Wells 2 74 ^ 420,000

Cyphenothrin (I)

 Groundwater - School/Daycare Wells 2 14 ^

Cyproconazole (F)

 Groundwater - School/Daycare Wells 2 0.72 ^ 70,000

DCPA (H)

 Groundwater - Private Residence Wells 11 30 ^

 Groundwater - School/Daycare Wells 3 3.6 - 30

Deltamethrin (includes parent Tralomethrin) (I)

 Groundwater - School/Daycare Wells 2 84 ^

Desethyl atrazine (HM)

 Groundwater - Private Residence Wells 11 1 9.1 265 ^ 10 ^

 Groundwater - School/Daycare Wells 3 1 33.3 41 ^ 0.43 - 10

Desethyl-desisopropyl atrazine (HM)

 Groundwater - Private Residence Wells 11 2 18.2 28.3 - 194 15 ^

 Groundwater - School/Daycare Wells 3 15 - 30

Desisopropyl atrazine (HM)

 Groundwater - Private Residence Wells 11 1 9.1 83 ^ 50 ^

 Groundwater - School/Daycare Wells 3 1 33.3 15 ^ 3.1 - 50

Diazinon (I)

 Groundwater - Private Residence Wells 11 30 ^

 Groundwater - School/Daycare Wells 3 1 33.3 81 ^ 3.3 - 30

Appendix F. Page 3 of 11
Pesticide (Type) / Commodity - Well Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples w/ 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA HHBP, 

ppt 1

Diazinon oxygen analog (IM)

 Groundwater - Private Residence Wells 11 50 ^

 Groundwater - School/Daycare Wells 1 50 ^

Dibromochloropropane (DBCP) (T)

 Groundwater - School/Daycare Wells 2 8.1 ^

Dicamba (H)

 Groundwater - Private Residence Wells 11 15 ^

 Groundwater - School/Daycare Wells 3 15 - 67

Dichlobenil (H)

 Groundwater - Private Residence Wells 11 5.0 ^ 70,000

 Groundwater - School/Daycare Wells 1 5.0 ^ 70,000

Dichlorprop (H)

 Groundwater - Private Residence Wells 11 15 ^

 Groundwater - School/Daycare Wells 3 0.73 - 15

Dichlorvos (DDVP) (I)

 Groundwater - Private Residence Wells 11 30 ^ 4,000

 Groundwater - School/Daycare Wells 1 30 ^ 4,000

Dicofol p,p' (I)

 Groundwater - School/Daycare Wells 2 23 ^

Dicrotophos (I)

 Groundwater - Private Residence Wells 11 7.5 ^ 500

 Groundwater - School/Daycare Wells 3 0.90 - 7.5 500

Difenoconazole (F)

 Groundwater - Private Residence Wells 11 7.5 ^ 70,000

 Groundwater - School/Daycare Wells 3 3.2 - 7.5 70,000

Dimethenamid/Dimethenamid P (H)

 Groundwater - Private Residence Wells 11 10 ^ 350,000

 Groundwater - School/Daycare Wells 3 0.91 - 10 350,000

Dimethenamid ethanesulfonic acid (HM)

 Groundwater - Private Residence Wells 11 1 9.1 3.0 ^ 2.0 ^

 Groundwater - School/Daycare Wells 1 2.0 ^

Dimethenamid oxanilic acid (HM)

 Groundwater - Private Residence Wells 11 3.0 ^

 Groundwater - School/Daycare Wells 3 1 33.3 1.0 ^ 0.63 - 3.0

Dimethoate (I)

 Groundwater - Private Residence Wells 11 50 ^ 15,000

 Groundwater - School/Daycare Wells 3 1.3 - 50 15,000

Dinoseb (H)

 Groundwater - School/Daycare Wells 2 0.35 ^

Dinotefuran (I)

 Groundwater - Private Residence Wells 11 7.5 ^ 140,000

 Groundwater - School/Daycare Wells 1 7.5 ^ 140,000

Disulfoton (I)

 Groundwater - Private Residence Wells 11 50 ^

 Groundwater - School/Daycare Wells 3 8.6 - 50

Disulfoton sulfone (IM)

 Groundwater - Private Residence Wells 11 6.0 ^

 Groundwater - School/Daycare Wells 3 2.0 - 6.0

Diuron (H)

 Groundwater - Private Residence Wells 11 4.0 ^

 Groundwater - School/Daycare Wells 3 1.6 - 4.0

Epoxiconazole (F)

 Groundwater - Private Residence Wells 11 3.0 ^ 140,000

 Groundwater - School/Daycare Wells 3 2.2 - 3.0 140,000

Appendix F. Page 4 of 11
Pesticide (Type) / Commodity - Well Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples w/ 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA HHBP, 

ppt 1

EPTC (H)

 Groundwater - Private Residence Wells 11 30 ^ 350,000

 Groundwater - School/Daycare Wells 3 5.0 - 30 350,000

Esfenvalerate (I)

 Groundwater - Private Residence Wells 11 100 ^ 13,000

 Groundwater - School/Daycare Wells 1 100 ^ 13,000

Esfenvalerate+Fenvalerate Total (I)

 Groundwater - School/Daycare Wells 2 38 ^

Ethalfluralin (H)

 Groundwater - Private Residence Wells 11 30 ^ 280,000

 Groundwater - School/Daycare Wells 1 30 ^ 280,000

Ethion (I)

 Groundwater - School/Daycare Wells 2 25 ^

Ethion mono oxon (IM)

 Groundwater - School/Daycare Wells 2 18 ^

Ethofumesate (H)

 Groundwater - Private Residence Wells 11 30 ^ 1,980,000

 Groundwater - School/Daycare Wells 3 3.3 - 30 1,980,000

Ethoprop (I)

 Groundwater - School/Daycare Wells 2 5.3 ^ 10,000

Fenamiphos (I)

 Groundwater - Private Residence Wells 11 100 ^

 Groundwater - School/Daycare Wells 1 100 ^

Fenamiphos sulfone (IM)

 Groundwater - Private Residence Wells 11 7.5 ^

 Groundwater - School/Daycare Wells 3 0.79 - 7.5

Fenamiphos sulfoxide (IM)

 Groundwater - Private Residence Wells 11 7.5 ^

 Groundwater - School/Daycare Wells 3 1.4 - 7.5

Fenbuconazole (F)

 Groundwater - School/Daycare Wells 2 2.4 ^ 210,000

Fenitrothion (I)

 Groundwater - School/Daycare Wells 2 13 ^ 9,000

Fenitrothion oxygen analog (IM)

 Groundwater - Private Residence Wells 11 200 ^

 Groundwater - School/Daycare Wells 3 1.8 - 200

Fenpropathrin (I)

 Groundwater - School/Daycare Wells 2 14 ^ 175,000

Fenthion (I)

 Groundwater - School/Daycare Wells 2 22 ^ 500

Fenthion oxygen analog (IM)

 Groundwater - Private Residence Wells 8 50 ^

Fipronil (I)

 Groundwater - School/Daycare Wells 2 0.35 ^ 1,000

Flufenacet oxanilic acid (HM)

 Groundwater - Private Residence Wells 11 2.5 ^

 Groundwater - School/Daycare Wells 3 0.75 - 2.5

Flumetsulam (H)

 Groundwater - Private Residence Wells 11 15 ^ 7,000,000

 Groundwater - School/Daycare Wells 3 8.6 - 15 7,000,000

Fluometuron (H)

 Groundwater - Private Residence Wells 11 50 ^

 Groundwater - School/Daycare Wells 3 1.6 - 50

Appendix F. Page 5 of 11
Pesticide (Type) / Commodity - Well Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples w/ 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA HHBP, 

ppt 1

Fluroxypyr-meptyl (H)

 Groundwater - School/Daycare Wells 2 4.9 ^

Fluvalinate (as Tau-Fluvalinate) (I)

 Groundwater - School/Daycare Wells 2 130 ^ 35,000

Fonofos (I)

 Groundwater - Private Residence Wells 11 30 ^

 Groundwater - School/Daycare Wells 1 30 ^

Halosulfuron methyl (H)

 Groundwater - Private Residence Wells 11 9.0 ^ 700,000

 Groundwater - School/Daycare Wells 3 1.8 - 9.0 700,000

Hexaconazole (F)

 Groundwater - Private Residence Wells 11 3.0 ^ 140,000

 Groundwater - School/Daycare Wells 3 3.0 - 3.3 140,000

Hexazinone (H)

 Groundwater - Private Residence Wells 11 2 18.2 5.0 - 11.1 3.0 ^

 Groundwater - School/Daycare Wells 3 0.50 - 3.0

Hydroxy atrazine (HM)

 Groundwater - Private Residence Wells 11 1 9.1 3.0 ^ 2.0 ^ 70,000

 Groundwater - School/Daycare Wells 3 1 33.3 25 ^ 1.2 - 2.0 70,000

3-Hydroxycarbofuran (IM)

 Groundwater - Private Residence Wells 11 15 ^

 Groundwater - School/Daycare Wells 3 3.0 - 15

Imazamethabenz acid (H)

 Groundwater - Private Residence Wells 11 3.0 ^

 Groundwater - School/Daycare Wells 3 0.60 - 3.0

Imazamethabenz methyl (H)

 Groundwater - Private Residence Wells 11 1.5 ^ 1,750,000

 Groundwater - School/Daycare Wells 3 0.31 - 1.5 1,750,000

Imazamox (H)

 Groundwater - Private Residence Wells 11 4.0 ^

 Groundwater - School/Daycare Wells 3 1.7 - 4.0

Imazapic (H)

 Groundwater - Private Residence Wells 11 3.0 ^ 3,500,000

 Groundwater - School/Daycare Wells 3 0.90 - 3.0 3,500,000

Imazapyr (H)

 Groundwater - Private Residence Wells 11 2.5 ^ 17,500,000

 Groundwater - School/Daycare Wells 3 1 33.3 2.0 ^ 1.0 - 2.5 17,500,000

Imazaquin (H)

 Groundwater - Private Residence Wells 11 5.0 ^ 1,750,000

 Groundwater - School/Daycare Wells 3 1.1 - 5.0 1,750,000

Imazethapyr (H)

 Groundwater - Private Residence Wells 11 2.0 ^ 17,500,000

 Groundwater - School/Daycare Wells 3 1.0 - 2.0 17,500,000

Imidacloprid (H)

 Groundwater - Private Residence Wells 11 6.0 ^ 399,000

 Groundwater - School/Daycare Wells 3 3.6 - 6.0 399,000

Isoxaflutole (H)

 Groundwater - Private Residence Wells 11 12 ^ 140,000

 Groundwater - School/Daycare Wells 1 12 ^ 140,000

Isoxaflutole degradate (HM)

 Groundwater - Private Residence Wells 11 15 ^

 Groundwater - School/Daycare Wells 1 15 ^

Lindane (BHC gamma) (I)

 Groundwater - School/Daycare Wells 2 20 ^

Appendix F. Page 6 of 11
Pesticide (Type) / Commodity - Well Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples w/ 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA HHBP, 

ppt 1

Linuron (H)

 Groundwater - Private Residence Wells 11 6.0 ^ 54,000

 Groundwater - School/Daycare Wells 3 1.6 - 6.0 54,000

Malathion (I)

 Groundwater - Private Residence Wells 11 30 ^

 Groundwater - School/Daycare Wells 3 10 - 30

Malathion oxygen analog (IM)

 Groundwater - Private Residence Wells 11 600 ^

 Groundwater - School/Daycare Wells 3 0.37 - 600

MCPA (H)

 Groundwater - Private Residence Wells 11 1.5 ^

 Groundwater - School/Daycare Wells 3 0.39 - 1.5

MCPB (H)

 Groundwater - Private Residence Wells 11 6.0 ^

 Groundwater - School/Daycare Wells 3 6.0 - 12

Mecoprop (MCPP) (H)

 Groundwater - Private Residence Wells 11 15 ^ 280,000

 Groundwater - School/Daycare Wells 3 1 33.3 2.0 ^ 0.31 - 15 280,000

Mesotrione (H)

 Groundwater - Private Residence Wells 11 15 ^ 49,000

 Groundwater - School/Daycare Wells 1 15 ^ 49,000

Metalaxyl/Mefenoxam * (F)

 Groundwater - Private Residence Wells 11 2.5 ^

 Groundwater - School/Daycare Wells 3 1.0 - 2.5

Methidathion (I)

 Groundwater - Private Residence Wells 11 100 ^ 11,000

 Groundwater - School/Daycare Wells 1 100 ^ 11,000

Methomyl (I)

 Groundwater - Private Residence Wells 11 7.5 ^

 Groundwater - School/Daycare Wells 3 7.3 - 7.5

Methoxychlor Total (I)

 Groundwater - Private Residence Wells 11 50 ^

 Groundwater - School/Daycare Wells 1 50 ^

Methoxychlor olefin (IM)

 Groundwater - School/Daycare Wells 2 3.6 ^

Methoxychlor p,p' (IM)

 Groundwater - School/Daycare Wells 2 19 ^

Metolachlor (H)

 Groundwater - Private Residence Wells 11 15 ^

 Groundwater - School/Daycare Wells 3 1 33.3 9.3 ^ 1.5 - 15

Metolachlor ethanesulfonic acid (HM)

 Groundwater - Private Residence Wells 11 3 27.3 5.0 - 1308 3.0 ^

 Groundwater - School/Daycare Wells 3 1 33.3 340 ^ 0.36 - 3.0

Metolachlor oxanilic acid (HM)

 Groundwater - Private Residence Wells 11 1 9.1 75.1 ^ 3.0 ^

 Groundwater - School/Daycare Wells 3 1 33.3 58 ^ 1.8 - 3.0

Metribuzin (H)

 Groundwater - Private Residence Wells 11 30 ^

 Groundwater - School/Daycare Wells 1 30 ^

Metribuzin DA (HM)

 Groundwater - Private Residence Wells 11 6.0 ^

 Groundwater - School/Daycare Wells 1 6.0 ^

Appendix F. Page 7 of 11
Pesticide (Type) / Commodity - Well Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples w/ 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA HHBP, 

ppt 1

Metsulfuron methyl (H)

 Groundwater - Private Residence Wells 11 7.0 ^

 Groundwater - School/Daycare Wells 3 1.5 - 7.0

Myclobutanil (F)

 Groundwater - Private Residence Wells 11 50 ^ 175,000

 Groundwater - School/Daycare Wells 3 1.6 - 50 175,000

1-Naphthol (IM)

 Groundwater - Private Residence Wells 11 30 ^

 Groundwater - School/Daycare Wells 1 30 ^

Neburon (H)

 Groundwater - Private Residence Wells 11 3.0 ^

 Groundwater - School/Daycare Wells 3 3.0 - 4.8

Nicosulfuron (H)

 Groundwater - Private Residence Wells 11 8.0 ^ 8,750,000

 Groundwater - School/Daycare Wells 3 1.7 - 8.0 8,750,000

Norflurazon (H)

 Groundwater - Private Residence Wells 11 6.0 ^ 105,000

 Groundwater - School/Daycare Wells 3 4.8 - 6.0 105,000

Norflurazon desmethyl (HM)

 Groundwater - Private Residence Wells 11 15 ^

 Groundwater - School/Daycare Wells 3 1.8 - 15

Omethoate (IM)

 Groundwater - Private Residence Wells 11 7.5 ^

 Groundwater - School/Daycare Wells 3 0.30 - 7.5

Oxadiazon (H)

 Groundwater - Private Residence Wells 11 30 ^

 Groundwater - School/Daycare Wells 1 30 ^

Oxadixyl (F)

 Groundwater - Private Residence Wells 11 15 ^

 Groundwater - School/Daycare Wells 3 1.8 - 15

Oxamyl (I)

 Groundwater - Private Residence Wells 11 7.5 ^

 Groundwater - School/Daycare Wells 3 3.0 - 7.5

Oxydemeton methyl (I)

 Groundwater - Private Residence Wells 11 6.0 ^ 700

 Groundwater - School/Daycare Wells 3 0.97 - 6.0 700

Oxydemeton methyl sulfone (IM)

 Groundwater - School/Daycare Wells 2 2.0 ^

Parathion (I)

 Groundwater - School/Daycare Wells 2 15 ^ 200

Parathion methyl (I)

 Groundwater - Private Residence Wells 11 30 ^

 Groundwater - School/Daycare Wells 3 30 - 53

Parathion methyl oxygen analog (IM)

 Groundwater - Private Residence Wells 11 7.5 ^

 Groundwater - School/Daycare Wells 3 3.6 - 7.5

Pendimethalin (H)

 Groundwater - Private Residence Wells 11 30 ^ 210,000

 Groundwater - School/Daycare Wells 1 30 ^ 210,000

Permethrin cis (IM)

 Groundwater - Private Residence Wells 11 50 ^ 1,750,000

 Groundwater - School/Daycare Wells 3 9.0 - 50 1,750,000

Appendix F. Page 8 of 11
Pesticide (Type) / Commodity - Well Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples w/ 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA HHBP, 

ppt 1

Permethrin trans (IM)

 Groundwater - Private Residence Wells 11 50 ^ 1,750,000

 Groundwater - School/Daycare Wells 3 7.5 - 50 1,750,000

Phenothrin (I)

 Groundwater - School/Daycare Wells 2 27 ^

Phorate (I)

 Groundwater - Private Residence Wells 11 30 ^ 4,000

 Groundwater - School/Daycare Wells 3 12 - 30 4,000

Phorate oxygen analog (IM)

 Groundwater - Private Residence Wells 11 50 ^

 Groundwater - School/Daycare Wells 1 50 ^

Phorate sulfone (IM)

 Groundwater - Private Residence Wells 11 100 ^

 Groundwater - School/Daycare Wells 3 1.8 - 100

Phorate sulfoxide (IM)

 Groundwater - Private Residence Wells 11 100 ^

 Groundwater - School/Daycare Wells 3 0.44 - 100

Phosmet (I)

 Groundwater - Private Residence Wells 11 100 ^ 40,000

 Groundwater - School/Daycare Wells 1 100 ^ 40,000

Picloram (H)

 Groundwater - Private Residence Wells 11 12.5 ^

 Groundwater - School/Daycare Wells 3 10 - 12.5

Prallethrin (I)

 Groundwater - School/Daycare Wells 2 25 ^ 350,000

Prometon (H)

 Groundwater - Private Residence Wells 11 30 ^

 Groundwater - School/Daycare Wells 3 1 33.3 1.5 ^ 0.17 - 30

Prometryn (H)

 Groundwater - Private Residence Wells 11 1.0 ^ 280,000

 Groundwater - School/Daycare Wells 3 0.17 - 1.0 280,000

Propachlor (H)

 Groundwater - Private Residence Wells 11 30 ^

 Groundwater - School/Daycare Wells 3 0.64 - 30

Propachlor ESA (HM)

 Groundwater - Private Residence Wells 11 9.0 ^

 Groundwater - School/Daycare Wells 1 9.0 ^

Propachlor oxanilic acid (HM)

 Groundwater - Private Residence Wells 11 3.0 ^

 Groundwater - School/Daycare Wells 3 1.4 - 3.0

Propanil (H)

 Groundwater - Private Residence Wells 11 30 ^ 63,000

 Groundwater - School/Daycare Wells 3 2.2 - 30 63,000

Propazine (H)

 Groundwater - Private Residence Wells 11 30 ^

 Groundwater - School/Daycare Wells 3 1 33.3 0.70 ^ 0.42 - 30

Propiconazole (F)

 Groundwater - Private Residence Wells 11 50 ^ 700,000

 Groundwater - School/Daycare Wells 3 3.4 - 50 700,000

Propoxur (I)

 Groundwater - Private Residence Wells 11 6.0 ^

 Groundwater - School/Daycare Wells 1 6.0 ^

Appendix F. Page 9 of 11
Pesticide (Type) / Commodity - Well Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples w/ 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA HHBP, 

ppt 1

Prosulfuron (H)

 Groundwater - School/Daycare Wells 2 1.5 ^ 371,000

Pyrasulfotole (H)

 Groundwater - School/Daycare Wells 2 2.8 ^ 70,000

Pyroxsulam (H)

 Groundwater - School/Daycare Wells 2 3.9 ^ 7,000,000

Resmethrin (I)

 Groundwater - School/Daycare Wells 2 7.8 ^ 245,000

Saflufenacil (H)

 Groundwater - Private Residence Wells 11 4.5 ^ 322,000

 Groundwater - School/Daycare Wells 1 4.5 ^ 322,000

Siduron (H)

 Groundwater - Private Residence Wells 11 2.0 ^ 1,050,000

 Groundwater - School/Daycare Wells 3 1.0 - 2.0 1,050,000

Simazine (H)

 Groundwater - Private Residence Wells 11 30 ^

 Groundwater - School/Daycare Wells 3 1 33.3 5.4 ^ 0.71 - 30

Sulfometuron methyl (H)

 Groundwater - Private Residence Wells 11 2.5 ^ 1,925,000

 Groundwater - School/Daycare Wells 3 0.76 - 2.5 1,925,000

Tebuconazole (F)

 Groundwater - Private Residence Wells 11 50 ^ 203,000

 Groundwater - School/Daycare Wells 3 2.1 - 50 203,000

Tebupirimfos (I)

 Groundwater - Private Residence Wells 11 30 ^ 100

 Groundwater - School/Daycare Wells 1 30 ^ 100

Tebuthiuron (H)

 Groundwater - Private Residence Wells 11 30 ^

 Groundwater - School/Daycare Wells 3 1 33.3 0.35 ^ 0.21 - 30

Tefluthrin (I)

 Groundwater - School/Daycare Wells 2 2.1 ^

Tembotrione (H)

 Groundwater - Private Residence Wells 11 15 ^ 3,000

 Groundwater - School/Daycare Wells 3 5.5 - 15 3,000

Terbacil (H)

 Groundwater - School/Daycare Wells 2 0.71 ^

Terbufos (I)

 Groundwater - Private Residence Wells 11 30 ^

 Groundwater - School/Daycare Wells 3 6.3 - 30

Terbufos sulfone (IM)

 Groundwater - School/Daycare Wells 2 1.6 ^

Tetrachlorvinphos (I)

 Groundwater - School/Daycare Wells 2 7.5 ^ 296,000

Tetraconazole (F)

 Groundwater - Private Residence Wells 11 30 ^ 51,000

 Groundwater - School/Daycare Wells 3 1.2 - 30 51,000

Tetradifon (I)

 Groundwater - School/Daycare Wells 2 7.2 ^

Tetramethrin (I)

 Groundwater - School/Daycare Wells 2 28 ^

Thiamethoxam (I)

 Groundwater - Private Residence Wells 11 7.5 ^ 84,000

 Groundwater - School/Daycare Wells 3 6.1 - 7.5 84,000

Appendix F. Page 10 of 11
Pesticide (Type) / Commodity - Well Type

Number 

of 

Samples

Samples 

with 

Detections

% of 

Samples w/ 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA HHBP, 

ppt 1

Thifensulfuron (H)

 Groundwater - School/Daycare Wells 2 3.4 ^

Thifensulfuron methyl (H)

 Groundwater - Private Residence Wells 11 5.0 ^ 301,000

 Groundwater - School/Daycare Wells 1 5.0 ^ 301,000

Thiobencarb (H)

 Groundwater - Private Residence Wells 11 2.5 ^ 70,000

 Groundwater - School/Daycare Wells 3 2.5 - 3.9 70,000

Tri Allate (H)

 Groundwater - Private Residence Wells 11 30 ^ 175,000

 Groundwater - School/Daycare Wells 3 12 - 30 175,000

Triadimefon (F)

 Groundwater - School/Daycare Wells 2 1.3 ^ 238,000

Triadimenol (F)

 Groundwater - Private Residence Wells 11 6.0 ^ 24,000

 Groundwater - School/Daycare Wells 3 6.0 - 11 24,000

Triasulfuron (H)

 Groundwater - Private Residence Wells 11 7.0 ^ 70,000

 Groundwater - School/Daycare Wells 3 1.7 - 7.0 70,000

Triclopyr (H)

 Groundwater - Private Residence Wells 11 1 9.1 25 ^ 15 ^ 350,000

 Groundwater - School/Daycare Wells 3 1.6 - 15 350,000

Trifluralin (H)

 Groundwater - Private Residence Wells 11 30 ^

 Groundwater - School/Daycare Wells 1 30 ^

Triticonazole (F)

 Groundwater - Private Residence Wells 11 500 ^ 1,190,000

 Groundwater - School/Daycare Wells 3 4.7 - 500 1,190,000

NOTES

1

 = EPA HHBP values have been multiplied by a factor of 1,000,000 as a basis for comparison using a single scale.

 There is no intention to imply any more exactness in the value than that originally expressed by EPA.

^ = Only one distinct detected concentration or LOD value was reported for the pair.

* = Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one

 of the spatial isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable 

 via multiresidue methods.

Pesticide Types:

F = Fungicide, FM = Fungicide Metabolite

H = Herbicide, HM = Herbicide Metabolite

I = Insecticide, IM = Insecticide Metabolite

T = Nematicide

Appendix F. Page 11 of 11
Appendix G

Distribution of Residues by Pesticide

in Drinking Water

Appendix G shows residue detections for all compounds tested in drinking water, including range 

of values detected and range of Limits of Detection (LODs). The U.S. Environmental Protection 

Agency (EPA) National Primary Drinking Water Regulation (NPDWR) Maximum Contaminant 

Levels (MCLs) for drinking water, Health Advisory (HA) values for drinking water, Freshwater 

Aquatic Organism (FAOs) Criteria for ambient water, and Human Health Benchmarks for Pesticides 

(HHBPs) are also shown. Units for LODs, MCLs, HAs, FAOs, and HHBPs are shown in parts per 

trillion (ppt).

In 2013, the Pesticide Data Program (PDP) analyzed 100 drinking water samples, including 50 

fi nished drinking water samples and 50 untreated (raw intake) drinking water samples. PDP 

detected 36 different residues (including metabolites), representing 27 pesticides, in fi nished 

drinking water and 40 different residues (including metabolites), representing 31 pesticides, in the 

untreated intake water; most of the detections were herbicides. None of the fi nished drinking water 

samples exceeded EPA MCLs, HAs, FAO criteria, or HHBP levels for any pesticide detected. 

The MCLs are legally enforceable standards that apply to public water systems. EPA’s regulations 

for MCLs can be referenced at http://water.epa.gov/drink/contaminants/index.cfm. The HAs 

are an estimate of acceptable drinking water levels for a chemical substance based on health 

effects information. The values published are for lifetime HA, which is the concentration of a 

chemical in drinking water that is not expected to cause any adverse non-carcinogenic effects 

for a lifetime of exposure. The MCL and HA values can be referenced at http://water.epa.gov/

drink/standardsriskmanagement.cfm. FAO criteria are set by EPA and are the concentration of 

a chemical in water at or below which aquatic life are protected from acute and chronic adverse 

effects of the chemical. The FAO values can be referenced at http://water.epa.gov/drink/standards/

hascience.cfm. Health Advisories and FAO criteria are not legally enforceable Federal standards, 

but serve as technical guidance to assist Federal, State, and local offi cials. The HHBP values 

were developed for compounds with no established MCLs or HAs, enabling citizens to better 

determine whether the detection of a pesticide in drinking water or source waters for drinking water 

may indicate a potential health risk. The HHBP values can be referenced at http://www.epa.gov/

pesticides/hhbp/.

EPA MCL, HA, FAO, and HHBP values are expressed in parts per million (ppm). Because drinking 

water residues are expressed in parts per trillion (ppt), EPA MCL, HA, FAO, and HHBP values have 

been multiplied by a factor of 1,000,000 as a basis for comparison using a single scale. There is no 

intention to imply any more exactness in the value than that originally expressed by EPA.

Results for environmental contaminants across all commodities, including drinking water, have 

been consolidated in a separate appendix because they have no registered uses and are not 

applied to crops (see Appendix H). 
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detects

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA MCL, 

ppt 1

EPA HA 2, 

ppt 1

EPA 

FAO 3

, 

ppt 1

EPA HHBP, 

ppt 1

2,4,5-T (H)

 Water, Finished 50 0.84 - 15 70,000

 Water, Untreated 50 0.84 - 15

2,4,5-TP (H)

 Water, Finished 50 0.68 - 15 50,000 50,000

 Water, Untreated 50 0.68 - 15

2,4-D (H)

 Water, Finished 50 49 98 1.1 - 84 0.65 - 2.5 70,000

 Water, Untreated 50 49 98 1.1 - 99 0.65 - 2.5

2,4-DB (H)

 Water, Finished 50 6.0 - 39

 Water, Untreated 50 6.0 - 39

Acetamiprid (I)

 Water, Finished 50 1.7 - 7.5 497,000

 Water, Untreated 50 1.7 - 7.5

Acetochlor (H)

 Water, Finished 50 9.2 - 10 140,000

 Water, Untreated 50 9.2 - 10

Acetochlor ethanesulfonic acid (HM)

 Water, Finished 50 36 72 2.7 - 350 1.6 - 9.0

 Water, Untreated 50 38 76 2.7 - 400 1.6 - 9.0

Acetochlor oxanilic acid (HM)

 Water, Finished 50 26 52 2.3 - 890 1.4 - 10

 Water, Untreated 50 24 48 2.3 - 890 1.4 - 10

Alachlor (H)

 Water, Finished 50 7.8 - 10 2,000

 Water, Untreated 50 7.8 - 10

Alachlor ethanesulfonic acid (HM)

 Water, Finished 50 40 80 2.8 - 25 1.7 - 12.5

 Water, Untreated 50 40 80 2.8 - 30 1.7 - 12.5

Alachlor oxanilic acid (HM)

 Water, Finished 50 32 64 1.0 - 12 0.61 - 10

 Water, Untreated 50 31 62 1.0 - 20 0.61 - 10

Aldicarb sulfone (IM)

 Water, Finished 50 4.5 - 7.6 2,000 7,000

 Water, Untreated 50 4.5 - 7.6

Aldicarb sulfoxide (IM)

 Water, Finished 50 15 ^ 4,000 7,000

 Water, Untreated 50 15 ^

Aminopyralid (H)

 Water, Finished 43 4.5 ^ 3,500,000

 Water, Untreated 43 4.5 ^

Atrazine (H)

 Water, Finished 50 50 100 2.4 - 290 0.66 - 10 3,000

 Water, Untreated 50 50 100 2.7 - 580 0.66 - 10

Azinphos methyl (I)

 Water, Finished 43 10 ^ 11,000

 Water, Untreated 43 10 ^

Azinphos methyl oxygen analog (IM)

 Water, Finished 50 4.5 - 7.5

 Water, Untreated 50 4.5 - 7.5

Azoxystrobin (F)

 Water, Finished 50 30 60 1.3 - 7.1 0.80 - 3.0 1,260,000

 Water, Untreated 50 38 76 1.3 - 10 0.80 - 3.0

APPENDIX G. DISTRIBUTION OF RESIDUES BY PESTICIDE IN DRINKING WATER

Appendix G. Page 1 of 11
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detects

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA MCL, 

ppt 1

EPA HA 2, 

ppt 1

EPA 

FAO 3

, 

ppt 1

EPA HHBP, 

ppt 1

Benfluralin (H)

 Water, Finished 50 3.6 - 50 35,000

 Water, Untreated 50 3.6 - 50

Bensulfuron methyl (H)

 Water, Finished 50 1.5 - 5.0 1,400,000

 Water, Untreated 50 1.5 - 5.0

Bentazon (H)

 Water, Finished 50 35 70 0.30 - 14 0.18 - 1.5 200,000

 Water, Untreated 50 42 84 0.30 - 15 0.18 - 1.5

Bifenthrin (I)

 Water, Finished 50 3.2 - 10

 Water, Untreated 50 3.2 - 10

Boscalid (F)

 Water, Finished 7 60 ^ 1,526,000

 Water, Untreated 7 60 ^

Bromacil (H)

 Water, Finished 50 1.2 - 9.0 70,000

 Water, Untreated 50 1.2 - 9.0

Bromuconazole 46 (trans) (FM)

 Water, Finished 50 3.0 - 3.2

 Water, Untreated 50 3.0 - 3.2

Bromuconazole 47 (cis) (FM)

 Water, Finished 50 3.0 - 5.4

 Water, Untreated 50 3.0 - 5.4

Butachlor (H)

 Water, Finished 43 1.9 ^

 Water, Untreated 43 1.9 ^

Butylate (H)

 Water, Finished 43 1.8 ^ 400,000

 Water, Untreated 43 1.8 ^

Carbaryl (I)

 Water, Finished 50 1.2 - 7.5

 Water, Untreated 50 1.2 - 7.5

Carbendazim - MBC (F)

 Water, Finished 7 3.0 ^ 175,000

 Water, Untreated 7 3.0 ^

Carbofuran (I)

 Water, Finished 50 0.41 - 4.0 40,000

 Water, Untreated 50 0.41 - 4.0

Chlorantraniliprole (I)

 Water, Finished 50 3.0 - 15 11,060,000

 Water, Untreated 50 3 6 5.0 ^ 3.0 - 15

Chlorfenvinphos (I)

 Water, Finished 43 9.6 ^

 Water, Untreated 43 9.6 ^

Chlorimuron ethyl (H)

 Water, Finished 50 1 2 9.5 ^ 5.7 - 6.0 630,000

 Water, Untreated 50 7 14 9.5 - 35 5.7 - 6.0

Chlorothalonil (F)

 Water, Finished 50 5.2 - 30

 Water, Untreated 50 5.2 - 30

Chlorpyrifos (I)

 Water, Finished 50 3.0 - 30 2,000

 Water, Untreated 50 3.0 - 30 83

Chlorpyrifos oxygen analog (IM)

 Water, Finished 50 12 - 21

 Water, Untreated 50 12 - 21

Appendix G. Page 2 of 11
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detects

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA MCL, 

ppt 1

EPA HA 2, 

ppt 1

EPA 

FAO 3

, 

ppt 1

EPA HHBP, 

ppt 1

Chlorsulfuron (H)

 Water, Finished 43 1.7 ^ 140,000

 Water, Untreated 43 1 2.3 2.8 ^ 1.7 ^

Clomazone (H)

 Water, Finished 7 30 ^ 5,880,000

 Water, Untreated 7 30 ^

Clopyralid (H)

 Water, Finished 50 8.1 - 12.5 1,050,000

 Water, Untreated 50 8.1 - 12.5

Clothianidin (I)

 Water, Finished 50 3 6 8.0 - 18 4.8 - 7.5 686,000

 Water, Untreated 50 4 8 8.0 - 45 4.8 - 7.5

Coumaphos (I)

 Water, Finished 50 1.7 - 15 2,000

 Water, Untreated 50 1.7 - 15

Coumaphos oxygen analog (IM)

 Water, Finished 50 1.6 - 9.0

 Water, Untreated 50 1.6 - 9.0

Cyanazine (H)

 Water, Finished 50 0.78 - 50 1,000

 Water, Untreated 50 0.78 - 50

Cycloate (H)

 Water, Finished 43 3.3 ^ 35,000

 Water, Untreated 43 3.3 ^

Cyfluthrin (I)

 Water, Finished 50 40 - 100 168,000

 Water, Untreated 50 40 - 100

Cyhalothrin, Lambda (I)

 Water, Finished 7 50 ^ 7,000

 Water, Untreated 7 50 ^

Cyhalothrin, Total (Cyhalothrin-L + R157836 epimer) (I)

 Water, Finished 43 42 ^ 7,000

 Water, Untreated 43 42 ^

Cypermethrin (I)

 Water, Finished 43 74 ^ 420,000

 Water, Untreated 43 74 ^

Cyphenothrin (I)

 Water, Finished 43 14 ^

 Water, Untreated 43 14 ^

Cyproconazole (F)

 Water, Finished 43 0.72 ^ 70,000

 Water, Untreated 43 0.72 ^

DCPA (H)

 Water, Finished 50 3.6 - 30 70,000

 Water, Untreated 50 3.6 - 30

Deltamethrin (includes parent Tralomethrin) (I)

 Water, Finished 43 84 ^

 Water, Untreated 43 84 ^

Desethyl atrazine (HM)

 Water, Finished 50 50 100 2.1 - 330 0.43 - 10

 Water, Untreated 50 50 100 2.5 - 920 0.43 - 10

Desethyl-desisopropyl atrazine (HM)

 Water, Finished 50 2 4 25 ^ 15 - 30

 Water, Untreated 50 8 16 25 - 50 15 - 30

Desisopropyl atrazine (HM)

 Water, Finished 50 28 56 5.2 - 110 3.1 - 50

 Water, Untreated 50 33 66 5.2 - 370 3.1 - 50

Appendix G. Page 3 of 11
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detects

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA MCL, 

ppt 1

EPA HA 2, 

ppt 1

EPA 

FAO 3

, 

ppt 1

EPA HHBP, 

ppt 1

Diazinon (I)

 Water, Finished 50 3.3 - 30 1,000

 Water, Untreated 50 3.3 - 30 170

Diazinon oxygen analog (IM)

 Water, Finished 7 50 ^

 Water, Untreated 7 50 ^

Dibromochloropropane - DBCP (T)

 Water, Finished 43 8.1 ^

 Water, Untreated 43 8.1 ^

Dicamba (H)

 Water, Finished 50 15 - 67 4,000,000

 Water, Untreated 50 15 - 67

Dichlobenil (H)

 Water, Finished 7 5.0 ^ 70,000

 Water, Untreated 7 5.0 ^

Dichlorprop (H)

 Water, Finished 50 1 2 1.2 ^ 0.73 - 15

 Water, Untreated 50 1 2 1.2 ^ 0.73 - 15

Dichlorvos - DDVP (I)

 Water, Finished 7 30 ^ 4,000

 Water, Untreated 7 30 ^

Dicofol p,p' (I)

 Water, Finished 43 23 ^

 Water, Untreated 43 23 ^

Dicrotophos (I)

 Water, Finished 50 0.90 - 7.5 500

 Water, Untreated 50 0.90 - 7.5

Difenoconazole (F)

 Water, Finished 50 3.2 - 7.5 70,000

 Water, Untreated 50 3.2 - 7.5

Dimethenamid/Dimethenamid P (H)

 Water, Finished 50 12 24 1.5 - 4.3 0.91 - 10 350,000

 Water, Untreated 50 14 28 1.5 - 9.9 0.91 - 10

Dimethenamid ethanesulfonic acid (HM)

 Water, Finished 7 2.0 ^

 Water, Untreated 7 2.0 ^

Dimethenamid oxanilic acid (HM)

 Water, Finished 50 8 16 1.0 - 5.9 0.63 - 3.0

 Water, Untreated 50 8 16 1.0 - 37 0.63 - 3.0

Dimethoate (I)

 Water, Finished 50 1.3 - 50 15,000

 Water, Untreated 50 1.3 - 50

Dinoseb (H)

 Water, Finished 43 0.35 ^ 7,000 7,000

 Water, Untreated 43 0.35 ^

Dinotefuran (I)

 Water, Finished 7 7.5 ^ 140,000

 Water, Untreated 7 7.5 ^

Disulfoton (I)

 Water, Finished 50 8.6 - 50 700

 Water, Untreated 50 8.6 - 50

Disulfoton sulfone (IM)

 Water, Finished 50 2.0 - 6.0

 Water, Untreated 50 2.0 - 6.0

Diuron (H)

 Water, Finished 50 6 12 2.7 - 8.5 1.6 - 4.0

 Water, Untreated 50 9 18 2.7 - 7.0 1.6 - 4.0

Appendix G. Page 4 of 11
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detects

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA MCL, 

ppt 1

EPA HA 2, 

ppt 1

EPA 

FAO 3

, 

ppt 1

EPA HHBP, 

ppt 1

Epoxiconazole (F)

 Water, Finished 50 2.2 - 3.0 140,000

 Water, Untreated 50 2.2 - 3.0

EPTC (H)

 Water, Finished 50 5.0 - 30 350,000

 Water, Untreated 50 5.0 - 30

Esfenvalerate (I)

 Water, Finished 7 100 ^ 13,000

 Water, Untreated 7 100 ^

Esfenvalerate+Fenvalerate Total (I)

 Water, Finished 43 38 ^

 Water, Untreated 43 38 ^

Ethalfluralin (H)

 Water, Finished 7 30 ^ 280,000

 Water, Untreated 7 30 ^

Ethion (I)

 Water, Finished 43 25 ^

 Water, Untreated 43 25 ^

Ethion mono oxon (IM)

 Water, Finished 43 18 ^

 Water, Untreated 43 18 ^

Ethofumesate (H)

 Water, Finished 50 3.3 - 30 1,980,000

 Water, Untreated 50 3.3 - 30

Ethoprop (I)

 Water, Finished 43 5.3 ^ 10,000

 Water, Untreated 43 5.3 ^

Fenamiphos (I)

 Water, Finished 7 100 ^ 700

 Water, Untreated 7 100 ^

Fenamiphos sulfone (IM)

 Water, Finished 50 0.79 - 7.5

 Water, Untreated 50 0.79 - 7.5

Fenamiphos sulfoxide (IM)

 Water, Finished 50 1.4 - 7.5

 Water, Untreated 50 1.4 - 7.5

Fenbuconazole (F)

 Water, Finished 43 2.4 ^ 210,000

 Water, Untreated 43 2.4 ^

Fenitrothion (I)

 Water, Finished 43 13 ^ 9,000

 Water, Untreated 43 13 ^

Fenitrothion oxygen analog (IM)

 Water, Finished 50 1.8 - 200

 Water, Untreated 50 1.8 - 200

Fenpropathrin (I)

 Water, Finished 43 14 ^ 175,000

 Water, Untreated 43 14 ^

Fenthion (I)

 Water, Finished 43 22 ^ 500

 Water, Untreated 43 22 ^

Fenthion-O analog (IM)

 Water, Finished 2 50 ^

 Water, Untreated 2 50 ^

Fipronil (I)

 Water, Finished 43 0.35 ^ 1,000

 Water, Untreated 43 0.35 ^

Appendix G. Page 5 of 11
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detects

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA MCL, 

ppt 1

EPA HA 2, 

ppt 1

EPA 

FAO 3

, 

ppt 1

EPA HHBP, 

ppt 1

Flufenacet oxanilic acid (HM)

 Water, Finished 50 0.75 - 2.5

 Water, Untreated 50 0.75 - 2.5

Flumetsulam (H)

 Water, Finished 50 8.6 - 15 7,000,000

 Water, Untreated 50 8.6 - 15

Fluometuron (H)

 Water, Finished 50 1 2 2.7 ^ 1.6 - 50 90,000

 Water, Untreated 50 1 2 2.7 ^ 1.6 - 50

Fluroxypyr-meptyl (H)

 Water, Finished 43 4.9 ^

 Water, Untreated 43 4.9 ^

Fluvalinate (as Tau-Fluvalinate) (I)

 Water, Finished 43 130 ^ 35,000

 Water, Untreated 43 130 ^

Fonofos (I)

 Water, Finished 7 30 ^ 10,000

 Water, Untreated 7 30 ^

Halosulfuron methyl (H)

 Water, Finished 50 1.8 - 9.0 700,000

 Water, Untreated 50 1.8 - 9.0

Hexaconazole (F)

 Water, Finished 50 3.0 - 3.3 140,000

 Water, Untreated 50 3.0 - 3.3

Hexazinone (H)

 Water, Finished 50 0.50 - 3.0 400,000

 Water, Untreated 50 0.50 - 3.0

Hydroxy atrazine (HM)

 Water, Finished 50 50 100 2.0 - 550 1.2 - 2.0 70,000

 Water, Untreated 50 50 100 2.0 - 950 1.2 - 2.0

3-Hydroxycarbofuran (IM)

 Water, Finished 50 3.0 - 15

 Water, Untreated 50 3.0 - 15

Imazamethabenz acid (H)

 Water, Finished 50 8 16 1.0 - 3.2 0.60 - 3.0

 Water, Untreated 50 7 14 1.0 - 3.3 0.60 - 3.0

Imazamethabenz methyl (H)

 Water, Finished 50 0.31 - 1.5 1,750,000

 Water, Untreated 50 0.31 - 1.5

Imazamox (H)

 Water, Finished 50 1.7 - 4.0

 Water, Untreated 50 1.7 - 4.0

Imazapic (H)

 Water, Finished 50 0.90 - 3.0 3,500,000

 Water, Untreated 50 0.90 - 3.0

Imazapyr (H)

 Water, Finished 50 22 44 2.0 - 8.3 1.0 - 2.5 17,500,000

 Water, Untreated 50 19 38 2.0 - 5.8 1.0 - 2.5

Imazaquin (H)

 Water, Finished 50 1.1 - 5.0 1,750,000

 Water, Untreated 50 1.1 - 5.0

Imazethapyr (H)

 Water, Finished 50 1.0 - 2.0 17,500,000

 Water, Untreated 50 1.0 - 2.0

Imidacloprid (I)

 Water, Finished 50 3.6 - 6.0 399,000

 Water, Untreated 50 3.6 - 6.0

Appendix G. Page 6 of 11
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detects

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA MCL, 

ppt 1

EPA HA 2, 

ppt 1

EPA 

FAO 3

, 

ppt 1

EPA HHBP, 

ppt 1

Isoxaflutole (H)

 Water, Finished 7 12 ^ 140,000

 Water, Untreated 7 12 ^

Isoxaflutole degradate (HM)

 Water, Finished 7 15 ^

 Water, Untreated 7 15 ^

Lindane - BHC gamma (I)

 Water, Finished 43 20 ^ 200

 Water, Untreated 43 20 ^ 950

Linuron (H)

 Water, Finished 50 1.6 - 6.0 54,000

 Water, Untreated 50 1.6 - 6.0

Malathion (I)

 Water, Finished 50 10 - 30 500,000

 Water, Untreated 50 10 - 30

Malathion oxygen analog (IM)

 Water, Finished 50 0.37 - 600

 Water, Untreated 50 0.37 - 600

MCPA (H)

 Water, Finished 50 15 30 0.65 - 2.7 0.39 - 1.5 30,000

 Water, Untreated 50 10 20 0.65 - 3.5 0.39 - 1.5

MCPB (H)

 Water, Finished 50 6.0 - 12

 Water, Untreated 50 6.0 - 12

Mecoprop - MCPP (H)

 Water, Finished 50 30 60 0.52 - 2.8 0.31 - 15 280,000

 Water, Untreated 50 31 62 0.52 - 8.6 0.31 - 15

Mesotrione (H)

 Water, Finished 7 15 ^ 49,000

 Water, Untreated 7 15 ^

Metalaxyl/Mefenoxam * (F)

 Water, Finished 50 25 50 2.0 - 17 1.0 - 2.5

 Water, Untreated 50 25 50 2.0 - 21 1.0 - 2.5

Methidathion (I)

 Water, Finished 7 100 ^ 11,000

 Water, Untreated 7 100 ^

Methomyl (I)

 Water, Finished 50 7.3 - 7.5 200,000

 Water, Untreated 50 7.3 - 7.5

Methoxychlor olefin (IM)

 Water, Finished 43 3.6 ^ 40,000 40,000

 Water, Untreated 43 3.6 ^

Methoxychlor p,p' (IM)

 Water, Finished 43 19 ^ 40,000 40,000

 Water, Untreated 43 19 ^

Methoxychlor Total (I)

 Water, Finished 7 50 ^ 40,000 40,000

 Water, Untreated 7 50 ^

Metolachlor (H)

 Water, Finished 50 30 60 2.5 - 73 1.5 - 15 700,000

 Water, Untreated 50 30 60 2.5 - 170 1.5 - 15

Metolachlor ethanesulfonic acid (HM)

 Water, Finished 50 50 100 1.3 - 740 0.36 - 3.0

 Water, Untreated 50 50 100 0.60 - 720 0.36 - 3.0

Metolachlor oxanilic acid (HM)

 Water, Finished 50 42 84 3.0 - 1100 1.8 - 3.0

 Water, Untreated 50 43 86 3.0 - 1200 1.8 - 3.0

Appendix G. Page 7 of 11
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detects

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA MCL, 

ppt 1

EPA HA 2, 

ppt 1

EPA 

FAO 3

, 

ppt 1

EPA HHBP, 

ppt 1

Metribuzin (H)

 Water, Finished 7 30 ^ 70,000

 Water, Untreated 7 30 ^

Metribuzin DA (HM)

 Water, Finished 7 6.0 ^

 Water, Untreated 7 6.0 ^

Metsulfuron methyl (H)

 Water, Finished 50 1.5 - 7.0

 Water, Untreated 50 4 8 2.5 ^ 1.5 - 7.0

Myclobutanil (F)

 Water, Finished 50 1.6 - 50 175,000

 Water, Untreated 50 1.6 - 50

1-Naphthol (IM)

 Water, Finished 7 30 ^

 Water, Untreated 7 30 ^

Neburon (H)

 Water, Finished 50 3.0 - 4.8

 Water, Untreated 50 3.0 - 4.8

Nicosulfuron (H)

 Water, Finished 50 1.7 - 8.0 8,750,000

 Water, Untreated 50 1.7 - 8.0

Norflurazon (H)

 Water, Finished 50 4.8 - 6.0 105,000

 Water, Untreated 50 4.8 - 6.0

Norflurazon desmethyl (HM)

 Water, Finished 50 1 2 3.0 ^ 1.8 - 15

 Water, Untreated 50 1 2 3.0 ^ 1.8 - 15

Omethoate (IM)

 Water, Finished 50 0.30 - 7.5

 Water, Untreated 50 0.30 - 7.5

Oxadiazon (H)

 Water, Finished 7 30 ^

 Water, Untreated 7 30 ^

Oxadixyl (F)

 Water, Finished 50 1.8 - 15

 Water, Untreated 50 1.8 - 15

Oxamyl (I)

 Water, Finished 50 3.0 - 7.5 200,000

 Water, Untreated 50 3.0 - 7.5

Oxydemeton methyl (I)

 Water, Finished 50 0.97 - 6.0 700

 Water, Untreated 50 0.97 - 6.0

Oxydemeton methyl sulfone (IM)

 Water, Finished 43 2.0 ^

 Water, Untreated 43 2.0 ^

Parathion (I)

 Water, Finished 43 15 ^ 200

 Water, Untreated 43 15 ^ 65

Parathion methyl (I)

 Water, Finished 50 30 - 53

 Water, Untreated 50 30 - 53

Parathion methyl oxygen analog (IM)

 Water, Finished 50 3.6 - 7.5

 Water, Untreated 50 3.6 - 7.5

Pendimethalin (H)

 Water, Finished 7 30 ^ 210,000

 Water, Untreated 7 30 ^

Appendix G. Page 8 of 11
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detects

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA MCL, 

ppt 1

EPA HA 2, 

ppt 1

EPA 

FAO 3

, 

ppt 1

EPA HHBP, 

ppt 1

Permethrin cis (IM)

 Water, Finished 50 9.0 - 50 1,750,000

 Water, Untreated 50 9.0 - 50

Permethrin trans (IM)

 Water, Finished 50 7.5 - 50 1,750,000

 Water, Untreated 50 7.5 - 50

Phenothrin (I)

 Water, Finished 43 27 ^

 Water, Untreated 43 27 ^

Phorate (I)

 Water, Finished 50 12 - 30 4,000

 Water, Untreated 50 12 - 30

Phorate oxygen analog (IM)

 Water, Finished 7 50 ^

 Water, Untreated 7 50 ^

Phorate sulfone (IM)

 Water, Finished 50 1.8 - 100

 Water, Untreated 50 1.8 - 100

Phorate sulfoxide (IM)

 Water, Finished 50 0.44 - 100

 Water, Untreated 50 0.44 - 100

Phosmet (I)

 Water, Finished 7 100 ^ 40,000

 Water, Untreated 7 100 ^

Picloram (H)

 Water, Finished 50 10 - 12.5 500,000

 Water, Untreated 50 10 - 12.5

Prallethrin (I)

 Water, Finished 43 25 ^ 350,000

 Water, Untreated 43 25 ^

Prometon (H)

 Water, Finished 50 41 82 0.28 - 5.7 0.17 - 30 400,000

 Water, Untreated 50 40 80 0.28 - 12 0.17 - 30

Prometryn (H)

 Water, Finished 50 0.17 - 1.0 280,000

 Water, Untreated 50 15 30 0.28 - 2.4 0.17 - 1.0

Propachlor (H)

 Water, Finished 50 0.64 - 30

 Water, Untreated 50 0.64 - 30

Propachlor ESA (HM)

 Water, Finished 7 9.0 ^

 Water, Untreated 7 9.0 ^

Propachlor oxanilic acid (HM)

 Water, Finished 50 1.4 - 3.0

 Water, Untreated 50 1.4 - 3.0

Propanil (H)

 Water, Finished 50 2.2 - 30 63,000

 Water, Untreated 50 2.2 - 30

Propazine (H)

 Water, Finished 50 15 30 0.70 - 2.9 0.42 - 30 10,000

 Water, Untreated 50 16 32 0.70 - 5.6 0.42 - 30

Propiconazole (F)

 Water, Finished 50 3.4 - 50 700,000

 Water, Untreated 50 3.4 - 50

Propoxur (I)

 Water, Finished 7 6.0 ^

 Water, Untreated 7 6.0 ^

Appendix G. Page 9 of 11
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detects

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA MCL, 

ppt 1

EPA HA 2, 

ppt 1

EPA 

FAO 3

, 

ppt 1

EPA HHBP, 

ppt 1

Prosulfuron (H)

 Water, Finished 43 1.5 ^ 371,000

 Water, Untreated 43 1.5 ^

Pyrasulfotole (H)

 Water, Finished 43 2.8 ^ 70,000

 Water, Untreated 43 2.8 ^

Pyroxsulam (H)

 Water, Finished 43 3.9 ^ 7,000,000

 Water, Untreated 43 3.9 ^

Resmethrin (I)

 Water, Finished 43 7.8 ^ 245,000

 Water, Untreated 43 7.8 ^

Saflufenacil (H)

 Water, Finished 7 4.5 ^ 322,000

 Water, Untreated 7 4.5 ^

Siduron (H)

 Water, Finished 50 1.0 - 2.0 1,050,000

 Water, Untreated 50 1.0 - 2.0

Simazine (H)

 Water, Finished 50 24 48 1.2 - 34 0.71 - 30 4,000

 Water, Untreated 50 25 50 1.2 - 59 0.71 - 30

Sulfometuron methyl (H)

 Water, Finished 50 0.76 - 2.5 1,925,000

 Water, Untreated 50 1 2 3.1 ^ 0.76 - 2.5

Tebuconazole (F)

 Water, Finished 50 5 10 3.5 ^ 2.1 - 50 203,000

 Water, Untreated 50 2 4 3.5 ^ 2.1 - 50

Tebupirimfos (I)

 Water, Finished 7 30 ^ 100

 Water, Untreated 7 30 ^

Tebuthiuron (H)

 Water, Finished 50 27 54 0.35 - 0.82 0.21 - 30 500,000

 Water, Untreated 50 22 44 0.35 - 1.7 0.21 - 30

Tefluthrin (I)

 Water, Finished 43 2.1 ^

 Water, Untreated 43 2.1 ^

Tembotrione (H)

 Water, Finished 50 5.5 - 15 3,000

 Water, Untreated 50 5.5 - 15

Terbacil (H)

 Water, Finished 43 0.71 ^ 90,000

 Water, Untreated 43 0.71 ^

Terbufos (I)

 Water, Finished 50 6.3 - 30 400

 Water, Untreated 50 6.3 - 30

Terbufos sulfone (IM)

 Water, Finished 43 1.6 ^

 Water, Untreated 43 1.6 ^

Tetrachlorvinphos (I)

 Water, Finished 43 7.5 ^ 296,000

 Water, Untreated 43 7.5 ^

Tetraconazole (F)

 Water, Finished 50 5 10 2.0 ^ 1.2 - 30 51,000

 Water, Untreated 50 3 6 2.0 ^ 1.2 - 30

Tetradifon (I)

 Water, Finished 43 7.2 ^

 Water, Untreated 43 7.2 ^

Appendix G. Page 10 of 11
Pesticide (Type) / Commodity

Number 

of 

Samples

Samples 

with 

Detects

% of 

Samples 

with 

Detects

Range of 

Values 

Detected, ppt

Range of 

LODs, ppt

EPA MCL, 

ppt 1

EPA HA 2, 

ppt 1

EPA 

FAO 3

, 

ppt 1

EPA HHBP, 

ppt 1

Tetramethrin (I)

 Water, Finished 43 28 ^

 Water, Untreated 43 28 ^

Thiamethoxam (I)

 Water, Finished 50 1 2 10.2 ^ 6.1 - 7.5 84,000

 Water, Untreated 50 6.1 - 7.5

Thifensulfuron (H)

 Water, Finished 43 3.4 ^

 Water, Untreated 43 3.4 ^

Thifensulfuron methyl (H)

 Water, Finished 7 5.0 ^ 301,000

 Water, Untreated 7 5.0 ^

Thiobencarb (H)

 Water, Finished 50 2.5 - 3.9 70,000

 Water, Untreated 50 2.5 - 3.9

Tri Allate (H)

 Water, Finished 50 12 - 30 175,000

 Water, Untreated 50 12 - 30

Triadimefon (F)

 Water, Finished 43 1.3 ^ 238,000

 Water, Untreated 43 1.3 ^

Triadimenol (F)

 Water, Finished 50 6.0 - 11 24,000

 Water, Untreated 50 6.0 - 11

Triasulfuron (H)

 Water, Finished 50 1.7 - 7.0 70,000

 Water, Untreated 50 1.7 - 7.0

Triclopyr (H)

 Water, Finished 50 12 24 2.7 - 30 1.6 - 15 350,000

 Water, Untreated 50 11 22 2.7 - 16 1.6 - 15

Trifluralin (H)

 Water, Finished 7 30 ^ 10,000

 Water, Untreated 7 30 ^

Triticonazole (F)

 Water, Finished 50 4.7 - 500 1,190,000

 Water, Untreated 50 4.7 - 500

NOTES

1

 = EPA MCL, HA, FAO, and HHBP values have been multiplied by a factor of 1,000,000 as a basis for comparison using a single scale.

 There is no intention to imply any more exactness in the value than that originally expressed by EPA.

2 = EPA Health Advisory values shown are for lifetime exposure.

3

 = The FAO value applies to ambient water rather than drinking water.

^

 = Only one distinct detected concentration or LOD value was reported for the pair.

* = Metalaxyl and mefenoxam have separate registrations. Mefenoxam is also known as Metalaxyl-M, which is one of the spatial

 isomers comprising metalaxyl. The spatial isomers of metalaxyl are analytically indistinguishable via multiresidue methods.

Pesticide Types:

F = Fungicide, FM = Fungicide Metabolite

H = Herbicide, HM = Herbicide Metabolite

I = Insecticide, IM = Insecticide Metabolite

T = Nematicide

Appendix G. Page 11 of 11
Appendix H

Distribution of Residues 

for Environmental Contaminants

Appendix H shows residue detections across all commodities for 22 compounds identifi ed as 

environmental contaminants, including range of values detected, range of Limits of Detection 

(LODs), and U.S. Environmental Protection Agency (EPA) tolerances or Action Levels for 

each pair. Results for environmental contaminants have been consolidated in this appendix 

because they have no registered uses and are not applied to crops.

The EPA tolerances cited in this appendix apply to 2013 and not to the current year. There 

may be instances where tolerances have been recently set or revoked that would have an 

effect on whether a residue is violative or not.

Action Levels (ALs) are shown in this appendix, where applicable, and denote Action 

Level values established by FDA. Under the Food Quality Protection Act, responsibility for 

establishing tolerances in lieu of ALs has been transferred to EPA. In the interim, ALs are 

used.

The Pesticide Data Program reports tolerance violations to the U.S. Food and Drug 

Administration (FDA) as part of an interagency Memorandum of Understanding between 

the U.S. Department of Agriculture and FDA. Residues reported to FDA are shown in the 

“Pesticide/Commodity” column to the right of the commodity and are annotated as “X” (if the 

residue exceeded the established tolerance) or “V” (if the residue did not have a tolerance 

listed in the Code of Federal Regulations, Title 40, Part 180). In both cases, these annotations 

are followed by a number indicating the number of samples reported to FDA.
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Aldrin (insecticide) (parent of Dieldrin)

Apple Juice 379 0 0.010 ^ 0.03 AL

Baby Food - Applesauce 379 0 0.001 ^ 0.03 AL

Baby Food - Peas 378 0 0.020 ^ 0.03 AL

Bananas 708 0 0.040 ^ 0.02 AL

Broccoli 707 0 0.005 ^ 0.03 AL

Butter 756 0 0.001 ^ 0.3 AL

Carrots 712 0 0.002 ^ 0.1 AL

Cauliflower 532 0 0.001 ^ 0.03 AL

Celery 708 0 0.001 - 0.005 0.03 AL

Fish, Salmon 352 0 0.003 - 0.010 0.3 AL

Grape Juice 176 0 0.003 ^ 0.05 AL

Green Beans 378 0 0.010 ^ 0.05 AL

Infant Formula, Soy-based 179 0 0.005 ^ 0.05 AL

Mushrooms 532 0 0.010 ^ NT

Nectarines 543 0 0.002 ^ 0.3 AL

Peaches 285 0 0.005 ^ 0.02 AL

Plums 507 0 0.005 ^ 0.3 AL

Raspberries 652 0 0.005 - 0.040 0.05 AL

Raspberries, Frozen 53 0 0.005 - 0.040 0.05 AL

Summer Squash 709 0 0.005 - 0.020 0.1 AL

Water, Finished 43 0 9.6 ^ (ppt)

Water, Groundwater 2 0 9.6 ^ (ppt)

Water, Untreated 43 0 9.6 ^ (ppt)

Winter Squash 187 0 0.003 ^ 0.1 AL

TOTAL 9,900 0

BHC alpha (insecticide) (isomer of BHC)

Apple Juice 379 0 0.012 ^ 0.05 AL

Baby Food - Applesauce 379 0 0.001 ^ 0.05 AL

Baby Food - Peas 378 0 0.20 ^ 0.05 AL

Bananas 708 0 0.007 ^ NT

Broccoli 707 0 0.005 ^ NT

Butter 756 0 0.001 ^ 0.3 AL

Carrots 712 0 0.001 ^ 0.3 AL

Cauliflower 532 0 0.001 ^ 0.05 AL

Celery 708 0 0.001 - 0.003 0.05 AL

Fish, Salmon 352 0 0.012 ^ NA

Grape Juice 176 0 0.012 ^ 0.05 AL

Green Beans 378 0 0.20 ^ 0.05 AL

Infant Formula, Dairy-based 177 0 0.001 ^ NT

Infant Formula, Soy-based 179 0 0.003 ^ 0.05 AL

Mushrooms 532 0 0.012 ^ NT

Nectarines 543 0 0.001 ^ 0.05 AL

Peaches 285 0 0.005 ^ 0.05 AL

Plums 507 0 0.003 ^ 0.05 AL

Raspberries 652 0 0.003 - 0.007 0.05 AL

Raspberries, Frozen 53 0 0.003 - 0.007 0.05 AL

Summer Squash 709 0 0.003 - 0.20 0.05 AL

Winter Squash 187 0 0.002 ^ 0.05 AL

TOTAL 9,989 0

BHC beta (isomer of BHC)

Apple Juice 379 0 0.014 ^ 0.05 AL

Baby Food - Applesauce 379 0 0.001 ^ 0.05 AL

Baby Food - Peas 378 0 0.30 ^ 0.05 AL

APPENDIX H. DISTRIBUTION OF RESIDUES FOR ENVIRONMENTAL CONTAMINANTS

Appendix H. Page 1 of 8
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Carrots 712 2 0.3 0.012 - 0.018 0.001 ^ 0.3 AL

Celery 346 0 0.003 ^ 0.05 AL

Fish, Salmon 352 0 0.014 ^ NA

Grape Juice 176 0 0.014 ^ 0.05 AL

Green Beans 378 0 0.20 ^ 0.05 AL

Infant Formula, Soy-based 179 0 0.003 ^ 0.05 AL

Mushrooms 532 0 0.014 ^ NT

Nectarines 543 0 0.001 ^ 0.05 AL

Peaches 285 0 0.005 ^ 0.05 AL

Plums 507 0 0.003 ^ 0.05 AL

Raspberries 351 0 0.003 ^ 0.05 AL

Raspberries, Frozen 10 0 0.003 ^ 0.05 AL

Summer Squash 709 0 0.003 - 0.20 0.05 AL

TOTAL 6,216 2

BHC delta (isomer of BHC)

Celery 346 0 0.005 ^ 0.05 AL

Infant Formula, Soy-based 179 0 0.005 ^ 0.05 AL

Plums 507 0 0.005 ^ 0.05 AL

Raspberries 351 0 0.005 ^ 0.05 AL

Raspberries, Frozen 10 0 0.005 ^ 0.05 AL

Summer Squash 363 0 0.005 ^ 0.05 AL

TOTAL 1,756 0

BHC epsilon (isomer of BHC)

Celery 346 0 0.005 ^ 0.05 AL

Infant Formula, Soy-based 179 0 0.005 ^ 0.05 AL

Plums 507 0 0.005 ^ 0.05 AL

Raspberries 351 0 0.005 ^ 0.05 AL

Raspberries, Frozen 10 0 0.005 ^ 0.05 AL

Summer Squash 363 0 0.005 ^ 0.05 AL

TOTAL 1,756 0

Chlordane Total (insecticide) 

Carrots 712 4 0.6 0.017 ^ 0.010 ^ 0.1 AL

Nectarines 543 0 0.010 ^ 0.1 AL

TOTAL 1,255 4

Chlordane cis (isomer of Chlordane)

Apple Juice 379 0 0.010 ^ 0.1 AL

Baby Food - Applesauce 379 0 0.001 ^ 0.1 AL

Baby Food - Peas 378 0 0.005 ^ 0.1 AL

Bananas 708 0 0.005 ^ 0.1 AL

Broccoli 707 0 0.005 ^ 0.1 AL

Butter 756 0 0.001 ^ NT

Cauliflower 532 0 0.001 ^ 0.1 AL

Celery 708 0 0.001 - 0.005 0.1 AL

Fish, Salmon 352 0 0.010 ^ 0.3 AL

Grape Juice 176 0 0.010 ^ 0.1 AL

Green Beans 378 0 0.025 ^ 0.1 AL

Infant Formula, Dairy-based 177 0 0.001 ^ NT

Infant Formula, Soy-based 179 0 0.005 ^ 0.1 AL

Mushrooms 532 0 0.010 ^ NT

Peaches 285 0 0.005 ^ 0.1 AL

Plums 507 0 0.005 ^ 0.1 AL

Raspberries 652 0 0.005 ^ 0.1 AL

Raspberries, Frozen 53 0 0.005 ^ 0.1 AL

Summer Squash 709 3 0.4 0.008 - 0.012 0.005 - 0.050 0.1 AL

Appendix H. Page 2 of 8
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Water, Finished 43 0 4.2 ^ (ppt)

Water, Groundwater 2 0 4.2 ^ (ppt)

Water, Untreated 43 0 4.2 ^ (ppt)

Winter Squash 187 1 0.5 0.003 ^ 0.002 ^ 0.1 AL

TOTAL 8,822 4

Chlordane trans (isomer of Chlordane)

Apple Juice 379 0 0.010 ^ 0.1 AL

Baby Food - Applesauce 357 0 0.001 ^ 0.1 AL

Baby Food - Peas 378 0 0.025 ^ 0.1 AL

Bananas 708 0 0.005 ^ 0.1 AL

Broccoli 707 0 0.005 ^ 0.1 AL

Butter 756 0 0.001 ^ NT

Cauliflower 532 0 0.001 ^ 0.1 AL

Celery 708 0 0.001 - 0.005 0.1 AL

Fish, Salmon 352 0 0.010 ^ 0.3 AL

Grape Juice 176 0 0.010 ^ 0.1 AL

Green Beans 378 0 0.010 ^ 0.1 AL

Infant Formula, Dairy-based 177 0 0.001 ^ NT

Infant Formula, Soy-based 179 0 0.005 ^ 0.1 AL

Mushrooms 532 0 0.010 ^ NT

Peaches 285 0 0.005 ^ 0.1 AL

Plums 507 0 0.005 ^ 0.1 AL

Raspberries 652 0 0.005 ^ 0.1 AL

Raspberries, Frozen 53 0 0.005 ^ 0.1 AL

Summer Squash 709 2 0.3 0.006 - 0.007 0.005 - 0.025 0.1 AL

Water, Finished 43 0 4.8 ^ (ppt)

Water, Groundwater 2 0 4.8 ^ (ppt)

Water, Untreated 43 0 4.8 ^ (ppt)

Winter Squash 187 1 0.5 0.003 ^ 0.002 ^ 0.1 AL

TOTAL 8,800 3

DDD o,p' (metabolite of DDT)

Butter 722 0 0.001 ^ 1.25 AL

Cauliflower 532 0 0.001 ^ 0.5 AL

Celery 708 0 0.001 - 0.003 0.5 AL

Fish, Salmon 352 0 0.001 ^ 5 AL

Grape Juice 176 0 0.001 ^ 0.05 AL

Infant Formula, Dairy-based 177 0 0.001 ^ NT

Infant Formula, Soy-based 179 0 0.003 ^ 0.2 AL

Plums 507 0 0.003 ^ 0.2 AL

Raspberries 351 0 0.003 ^ 0.1 AL

Raspberries, Frozen 10 0 0.003 ^ 0.1 AL

Summer Squash 363 1 0.3 0.003 ^ 0.003 ^ 0.1 AL

TOTAL 4,077 1

DDD p,p' (metabolite of DDT)

Apple Juice 379 0 0.005 ^ 0.1 AL

Baby Food - Applesauce 379 0 0.001 ^ 0.1 AL

Baby Food - Peas 378 0 0.005 ^ 0.2 AL

Bananas 708 0 0.005 ^ NT

Broccoli 707 0 0.005 ^ NT

Butter 739 0 0.001 ^ 1.25 AL

Cauliflower 532 0 0.001 ^ 0.5 AL

Celery 708 1 0.1 0.002 ^ 0.001 - 0.003 0.5 AL

Fish, Salmon 352 0 0.005 ^ 5 AL

Grape Juice 146 0 0.005 ^ 0.05 AL

Green Beans 378 0 0.025 ^ 0.2 AL

Appendix H. Page 3 of 8
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Infant Formula, Dairy-based 177 0 0.001 ^ NT

Infant Formula, Soy-based 179 0 0.003 ^ 0.2 AL

Mushrooms 532 0 0.005 ^ 0.5 AL

Peaches 285 0 0.005 ^ 0.2 AL

Plums 507 0 0.003 ^ 0.2 AL

Raspberries 652 0 0.003 - 0.010 0.1 AL

Raspberries, Frozen 53 0 0.003 - 0.010 0.1 AL

Summer Squash 709 1 0.1 0.003 ^ 0.003 - 0.050 0.1 AL

Winter Squash 187 0 0.002 ^ 0.1 AL

TOTAL 8,687 2

DDE o,p' (metabolite of DDT)

Carrots 712 2 0.3 0.003 ^ 0.002 ^ 3 AL

Celery 346 0 0.005 ^ 0.5 AL

Fish, Salmon 352 0 0.001 ^ 5 AL

Grape Juice 176 0 0.001 ^ 0.05 AL

Infant Formula, Soy-based 179 0 0.005 ^ 0.2 AL

Nectarines 543 0 0.002 ^ 0.2 AL

Plums 507 0 0.005 ^ 0.2 AL

Raspberries 351 0 0.005 ^ 0.1 AL

Raspberries, Frozen 10 0 0.005 ^ 0.1 AL

Summer Squash 363 0 0.005 ^ 0.1 AL

TOTAL 3,539 2

DDE p,p' (metabolite of DDT)

Apple Juice 379 0 0.010 ^ 0.1 AL

Baby Food - Applesauce 379 0 0.001 ^ 0.1 AL

Baby Food - Peas 378 0 0.005 ^ 0.2 AL

Bananas 708 0 0.005 ^ NT

Broccoli 707 0 0.005 ^ NT

Butter 756 503 66.5 0.002 - 0.016 0.001 ^ 1.25 AL

Carrots 712 167 23.5 0.003 - 0.084 0.002 - 0.008 3 AL

Cauliflower 532 0 0.001 ^ 0.5 AL

Celery 708 122 17.2 0.002 - 0.012 0.001 - 0.003 0.5 AL

Fish, Salmon 352 0 0.010 ^ 5 AL

Grape Juice 176 0 0.010 ^ 0.05 AL

Green Beans 378 1 0.3 0.007 ^ 0.005 ^ 0.2 AL

Infant Formula, Dairy-based 177 0 0.001 ^ NT

Infant Formula, Soy-based 179 0 0.003 ^ 0.2 AL

Mushrooms 532 0 0.010 ^ 0.5 AL

Nectarines 543 1 0.2 0.003 ^ 0.002 - 0.008 0.2 AL

Peaches 285 0 0.005 ^ 0.2 AL

Plums 507 0 0.003 ^ 0.2 AL

Raspberries 652 0 0.003 - 0.005 0.1 AL

Raspberries, Frozen 53 0 0.003 - 0.005 0.1 AL

Summer Squash 709 19 2.7 0.003 - 0.008 0.003 - 0.005 0.1 AL

Winter Squash 187 4 2.1 0.003 ^ 0.002 ^ 0.1 AL

TOTAL 9,989 817

DDT o,p' (insecticide) 

Butter 755 0 0.001 - 0.004 1.25 AL

Carrots 712 44 6.2 0.002 - 0.004 0.001 ^ 3 AL

Cauliflower 532 0 0.001 - 0.003 0.5 AL

Celery 708 0 0.001 - 0.007 0.5 AL

Infant Formula, Dairy-based 177 0 0.001 ^ NT

Infant Formula, Soy-based 150 0 0.003 ^ 0.2 AL

Nectarines 543 0 0.001 ^ 0.2 AL

Plums 507 0 0.003 ^ 0.2 AL

Appendix H. Page 4 of 8
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Raspberries 351 0 0.003 ^ 0.1 AL

Raspberries, Frozen 10 0 0.003 ^ 0.1 AL

Summer Squash 362 9 2.5 0.003 - 0.013 0.003 ^ 0.1 AL

TOTAL 4,807 53

DDT p,p' (insecticide) 

Baby Food - Applesauce 357 0 0.001 ^ 0.1 AL

Bananas 708 0 0.076 ^ NT

Broccoli 665 0 0.005 ^ NT

Carrots 712 64 9 0.002 - 0.010 0.001 ^ 3 AL

Cauliflower 532 0 0.001 ^ 0.5 AL

Celery 708 9 1.3 0.002 ^ 0.001 - 0.003 0.5 AL

Fish, Salmon 352 2 0.6 0.002 - 0.003 0.001 ^ 5 AL

Grape Juice 146 0 0.001 ^ 0.05 AL

Infant Formula, Dairy-based 177 0 0.001 ^ NT

Infant Formula, Soy-based 179 0 0.003 ^ 0.2 AL

Nectarines 543 0 0.001 ^ 0.2 AL

Peaches 285 0 0.005 ^ 0.2 AL

Plums 507 0 0.003 ^ 0.2 AL

Raspberries 652 0 0.003 - 0.076 0.1 AL

Raspberries, Frozen 53 0 0.003 - 0.076 0.1 AL

Summer Squash 363 8 2.2 0.003 - 0.013 0.003 ^ 0.1 AL

Winter Squash 187 0 0.003 ^ 0.1 AL

TOTAL 7,126 83

Dieldrin (insecticide) (also a metabolite of Aldrin)

Apple Juice 379 0 0.010 ^ 0.03 AL

Baby Food - Applesauce 379 0 0.005 ^ 0.03 AL

Baby Food - Peas 378 0 0.050 ^ 0.03 AL

Bananas 708 0 0.020 ^ 0.02 AL

Broccoli 707 0 0.005 ^ 0.03 AL

Butter 720 0 0.003 ^ 0.3 AL

Carrots 712 9 1.3 0.007 - 0.014 0.004 ^ 0.1 AL

Cauliflower 532 0 0.002 ^ 0.03 AL

Celery 708 0 0.002 - 0.010 0.03 AL

Fish, Salmon 352 0 0.010 ^ 0.3 AL

Grape Juice 176 0 0.010 ^ 0.05 AL

Green Beans 378 0 0.025 ^ 0.05 AL

Infant Formula, Dairy-based 177 0 0.002 ^ NT

Infant Formula, Soy-based 179 0 0.010 ^ 0.05 AL

Mushrooms 532 0 0.010 ^ NT

Nectarines 543 0 0.004 ^ 0.3 AL

Peaches 285 0 0.005 ^ 0.02 AL

Plums 507 0 0.010 ^ 0.3 AL

Raspberries 652 0 0.010 - 0.020 0.05 AL

Raspberries, Frozen 53 0 0.010 - 0.020 0.05 AL

Summer Squash 709 19 2.7 0.011 - 0.094 0.010 - 0.050 0.1 AL

Winter Squash 187 2 1.1 0.010 - 0.12 0.006 ^ 0.1 AL

TOTAL 9,953 30

Endrin (insecticide) 

Apple Juice 379 0 0.010 ^ 0.03 AL

Baby Food - Applesauce 379 0 0.001 ^ 0.03 AL

Baby Food - Peas 378 0 0.12 ^ 0.03 AL

Bananas 708 0 0.031 ^ 0.02 AL

Broccoli 707 0 0.005 ^ 0.03 AL

Butter 756 0 0.009 - 0.060 0.3 AL

Cauliflower 532 0 0.008 - 0.025 0.03 AL

Appendix H. Page 5 of 8
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Celery 708 0 0.008 - 0.010 0.03 AL

Fish, Salmon 352 0 0.010 ^ 0.3 AL

Grape Juice 176 0 0.010 ^ 0.05 AL

Green Beans 378 0 0.030 ^ 0.05 AL

Infant Formula, Dairy-based 177 0 0.008 ^ NT

Infant Formula, Soy-based 179 0 0.010 ^ 0.05 AL

Mushrooms 532 0 0.010 ^ NT

Peaches 285 0 0.005 ^ 0.02 AL

Plums 507 0 0.010 ^ 0.3 AL

Raspberries 652 0 0.010 - 0.031 0.05 AL

Raspberries, Frozen 53 0 0.010 - 0.031 0.05 AL

Summer Squash 709 0 0.010 - 0.062 0.1 AL

Water, Finished 43 0 22 ^ (ppt)

Water, Groundwater 2 0 22 ^ (ppt)

Water, Untreated 43 0 22 ^ (ppt)

Winter Squash 187 2 1.1 0.005 ^ 0.003 ^ 0.1 AL

TOTAL 8,822 2

Heptachlor (insecticide) 

Apple Juice 379 0 0.002 ^ NT

Baby Food - Applesauce 379 0 0.001 ^ NT

Baby Food - Peas 378 0 0.015 ^ NT

Bananas 708 0 0.049 ^ NT

Broccoli 707 0 0.005 ^ NT

Butter 756 0 0.001 ^ NT

Carrots 712 0 0.001 ^ NT

Cauliflower 532 0 0.001 ^ NT

Celery 708 0 0.001 - 0.003 0.05 AL

Fish, Salmon 352 0 0.002 ^ 0.3 AL

Grape Juice 176 0 0.002 ^ 0.05 AL

Green Beans 378 0 0.005 ^ NT

Infant Formula, Dairy-based 177 0 0.001 ^ NT

Infant Formula, Soy-based 179 0 0.003 ^ 0.05 AL

Mushrooms 532 0 0.002 ^ NT

Nectarines 543 0 0.001 ^ 0.05 AL

Peaches 285 0 0.005 ^ 0.05 AL

Plums 507 0 0.003 ^ 0.05 AL

Raspberries 652 0 0.003 - 0.049 0.05 AL

Raspberries, Frozen 53 0 0.003 - 0.049 0.05 AL

Summer Squash 709 0 0.003 - 0.015 0.05 AL

Water, Finished 50 0 9.0 - 50

Water, Groundwater 14 0 9.0 - 50

Water, Untreated 50 0 9.0 - 50

Winter Squash 187 0 0.003 ^ 0.05 AL

TOTAL 10,103 0

Heptachlor epoxide (metabolite of Heptachlor)

Apple Juice 379 0 0.005 ^ NT

Baby Food - Applesauce 379 0 0.001 ^ NT

Baby Food - Peas 378 0 0.010 ^ NT

Bananas 708 0 0.041 ^ NT

Broccoli 707 0 0.005 ^ NT

Butter 756 0 0.005 ^ NT

Cauliflower 532 0 0.004 ^ NT

Celery 708 0 0.004 - 0.005 0.05 AL

Fish, Salmon 323 0 0.005 ^ 0.3 AL

Grape Juice 176 0 0.005 ^ 0.05 AL

Green Beans 378 0 0.010 ^ NT

Appendix H. Page 6 of 8
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

Infant Formula, Dairy-based 177 0 0.004 ^ NT

Infant Formula, Soy-based 179 0 0.005 ^ 0.05 AL

Mushrooms 532 0 0.005 ^ NT

Peaches 285 0 0.005 ^ 0.05 AL

Plums 507 0 0.005 ^ 0.05 AL

Raspberries 652 0 0.005 - 0.041 0.05 AL

Raspberries, Frozen 53 0 0.005 - 0.041 0.05 AL

Summer Squash 709 2 0.3 0.006 - 0.010 0.005 - 0.010 0.05 AL

Winter Squash 187 1 0.5 0.005 ^ 0.003 ^ 0.05 AL

TOTAL 8,705 3

Heptachlor epoxide cis (metabolite of Heptachlor)

Carrots (V-4) 712 4 0.6 0.007 - 0.016 0.004 ^ NT

Nectarines 543 0 0.004 ^ 0.05 AL

Water, Finished 50 0 9.0 - 100 (ppt)

Water, Groundwater 14 0 9.0 - 100 (ppt)

Water, Untreated 50 0 9.0 - 100 (ppt)

TOTAL 1,369 4

Heptachlor epoxide trans (metabolite of Heptachlor)

Water, Finished 50 0 9.0 - 100 (ppt)

Water, Groundwater 14 0 9.0 - 100 (ppt)

Water, Untreated 50 0 9.0 - 100 (ppt)

TOTAL 114 0

Hexachlorobenzene - HCB (metabolite and impurity of Quintozene)

Apple Juice 33 0 0.003 ^ NT

Baby Food - Applesauce 357 0 0.001 ^ NT

Broccoli 707 0 0.005 ^ 0.1

Butter 741 0 0.004 ^ NT

Carrots 712 0 0.002 ^ NT

Celery 678 0 0.001 - 0.003 NT

Green Beans 378 0 0.050 ^ 0.1

Infant Formula, Soy-based 179 0 0.003 ^ 0.1

Mushrooms 31 0 0.003 ^ NT

Peaches 285 0 0.005 ^ NT

Plums 507 0 0.003 ^ NT

Raspberries 351 0 0.003 ^ NT

Raspberries, Frozen 10 0 0.003 ^ NT

Summer Squash 709 0 0.003 - 0.10 NT

Winter Squash 187 0 0.002 ^ NT

TOTAL 5,865 0

Oxychlordane (metabolite of Chlordane)

Apple Juice 379 0 0.010 ^ 0.1 AL

Butter 756 0 0.003 ^ NT

Cauliflower 532 0 0.002 ^ 0.1 AL

Celery 332 0 0.002 ^ 0.1 AL

Fish, Salmon 146 0 0.010 ^ 0.3 AL

Mushrooms 532 0 0.010 ^ NT

Water, Finished 43 0 8.4 ^ (ppt)

Water, Groundwater 2 0 8.4 ^ (ppt)

Water, Untreated 43 0 8.4 ^ (ppt)

TOTAL 2,765 0

Appendix H. Page 7 of 8
 Pesticide / Commodity

Number of 

Samples

Samples 

with 

Detections

% of Samples 

with 

Detections

Range of Values 

Detected, ppm

Range of LODs, 

ppm

EPA 

Tolerance 

Level, ppm

NOTES

^ Only one distinct detected concentration or LOD value was reported for the pair.

AL = Numbers shown are Action Levels established by FDA for some pesticides. Under the Food Quality Protection Act, responsibility

for establishing tolerances in lieu of action levels has been transferred to EPA. In the interim, action levels are used.

NT = No tolerance level was set for that pesticide/commodity pair.

(V) = Residue was found where no tolerance was established by EPA. Following "V" are the number of occurrences. Refer to

pages 2 and 3 in Appendix M to see the number of occurrences broken down by sample origin (domestic, imported, or

unknown) for a commodity/pesticide pair.

(ppt) = Findings in water are expressed in parts-per-trillion (ppt). All other findings are expressed in parts-per-million (ppm).

Appendix H. Page 8 of 8
Appendix I

Sample Origin by State or Country

(Determined by Grower, Packer, or Distributor)

Appendix I gives the number of fruit and vegetable, infant formula, butter, and salmon samples 

per State or country of origin and the number of samples of unknown origin. Where available, 

the origin of fresh commodities is taken from the grower or packer information. For processed 

commodities, origin is determined primarily by packer or distributor.

As shown in Appendix I, fruit and vegetable, infant formula, butter, and salmon samples 

originated from 36 States and 34 foreign countries. There were 186 samples from mixed 

national origins (multiple countries). There were 345 domestic samples from unknown states. 

There were an additional 68 samples from unknown origins. Overall, for all samples excluding 

groundwater and drinking water, 70.8 percent were from U.S. sources, 26.6 percent were 

imports, 1.9 percent were of mixed national origin, and 0.7 percent were of unknown origin.
Part 1. Domestic Samples

Dairy Fish # of % of

BN BR CE CF CR GB MU NE PC PU RS SS WS AJ GJ IA IE RZ DF YF BU FS Samples Total

Alaska 18 18 0.2

Arizona 1 18 1 6 11 7 1 8 53 0.5

Arkansas 7 4 7 1 1 2 1 42 5 70 0.7

California 522 510 486 446 88 138 278 178 223 433 76 11 25 2 11 8 3 5 109 25 3577 35.8

Colorado 7 6 2 1 2 1 1 6 26 0.3

Florida 28 59 13 4 38 11 1 88 3 15 7 1 20 3 291 2.9

Georgia 13 15 5 28 1 1 63 0.6

Idaho 1 1 7 1 2 2 2 16 0.2

Illinois 10 1 1 3 3 1 4 3 31 7 64 0.6

Indiana 1 69 54 124 1.2

Iowa 1 1 <0.1

Kansas 2 46 0.1

Kentucky 1 1 <0.1

Maine 3 1 1 1 6 0.1

Maryland 8 10 6 12 20 3 1 10 19 5 94 0.9

Massachusetts 1 3 109 2 1 116 1.2

Michigan 2 22 35 9 3 14 2 19 25 272 301 7 5 47 1 764 7.6

Minnesota 2 1 2 1 1 1 3 144 1 156 1.6

Missouri 33 33 0.3

Nevada 3 1 4 0.0

New Jersey 1 3 1 18 10 1 2 14 22 9 81 0.8

New York 5 1 10 2 1 1 12 2 6 2 63 53 5 3 32 1 199 2.0

North Carolina 7 3 9 2 3 2 2 40 68 0.7

Ohio 2 3 1 11 19 13 1 2 18 9 7 1 64 72 62 3 288 2.9

Oklahoma 12 12 0.1

Oregon 31 1 32 0.3

Pennsylvania 6 3 135 2 2 2 1 10 1 162 1.6

Rhode Island 1 1 <0.1

South Carolina 17 17 0.2

Texas 16 22 3 7 15 36 2 39 19 1 1 1 19 2 183 1.8

Vermont 3 10 13 0.1

Virginia 1 9 8 18 0.2

Washington 5 3 2 1 6 5 21 14 1 10 27 18 15 128 1.3

West Virginia 4 4 0.0

Wisconsin 1 41 42 0.4

Wyoming 1 1 <0.1

Unknown State 15 20 9 19 61 92 7 11 5 6 61 1 3 10 10 2 1 9 3 345 3.5

No. of Domestic 0 623 652 515 576 310 474 313 268 235 439 394 28 151 161 362 376 7 174 173 751 95 7,077

% of Total 0 88 92 97 81 82 89 58 94 46 67 56 15 40 91 96 99 13 98 97 99 27 70.8

APPENDIX I. SAMPLE ORIGIN BY STATE OR COUNTRY 1 

Fresh F&V Processed F&V Formula

(Determined by Grower, Packer, or Distributor)

Appendix I. Page 1 of 3
Part 2. Imported Samples

Dairy Fish # of % of

BN BR CE CF CR GB MU NE PC PU RS SS WS AJ GJ IA IE RZ DF YF BU FS Samples Total

Argentina 28 28 0.3

Brazil 4 4 <0.1

Canada 5 12 5 84 2 51 3 1 10 18 191 1.9

Chile 227 16 269 1 1 3 4 40 86 647 6.5

China 34 1 104 139 1.4

Colombia 56 56 0.6

Costa Rica 154 1 155 1.6

Denmark 5 5 0.1

Republic 52 7 0.1

Ecuador 145 1 146 1.5

Guatemala 209 10 10 229 2.3

Honduras 95 1 16 112 1.1

Hong Kong 1 1 <0.1

Iceland 1 1 <0.1

Ireland 1 1 <0.1

Israel 6 6 0.1

Mexico 28 75 37 10 41 42 6 211 294 131 2 877 8.8

New Zealand 4 4 <0.1

Nicaragua 5 5 0.1

Norway 11 11 0.1

Panama 2 2 <0.1

Peru 1 1 <0.1

Russia 1 1 <0.1

Serbia 3 3 <0.1

Switzerland 2 2 <0.1

Turkey 8 8 0.1

United Kingdom 3 3 <0.1

Yugoslavia 1 1 <0.1

Unknown Country 13 13 0.1

No. of Imports 708 82 49 15 131 54 57 227 16 271 212 303 159 78 0 15 0 46 0 2 1 233 2,659

% of Total 100 12 7 3 18 14 11 42 6 53 33 43 85 21 0 4 0 87 0 1 <1 66 26.6

Dairy Fish # of % of

BN BR CE CF CR GB MU NE PC PU RS SS WS AJ GJ IA IE RZ DF YF BU FS Samples Total

Argentina / Austria / Brazil / Chile / China / Germany / Hungary 1 1 <0.1

Argentina / Austria / Brazil / Chile / China / Germany / Hungary / Turkey 1 1 <0.1

Argentina / Austria / Brazil / Chile / China / Germany / Hungary / Italy / Turkey / USA 2 2 <0.1

Argentina / Brazil 1 1 <0.1

Argentina / Brazil / Chile / China / Germany / Hungary / Italy / Turkey 1 1 <0.1

Argentina / Brazil / Chile / China / USA 4 4 <0.1

Argentina / Chile / China / Germany / Poland 1 1 <0.1

Argentina / Chile / China / USA 1 1 <0.1

Argentina / Chile / USA 1 1 <0.1

Argentina / China 36 36 0.4

Argentina / China / USA 8 8 0.1

Argentina / Mexico / USA 6 6 0.1

Argentina / Taiwan / USA 2 2 <0.1

Argentina / USA 5 6 11 0.1

Austria / Brazil / Chile / China / Germany / Italy / Turkey 1 1 <0.1

Brazil / Chile 4 4 <0.1

Brazil / China 1 1 <0.1

Brazil / USA 2 2 <0.1

Canada / USA 23 23 0.2

Chile / China 9 9 0.1

Chile / China / USA 14 14 0.1

China / Germany 1 1 <0.1

China / Germany / USA 3 3 <0.1

China / Russia 4 4 <0.1

China / USA 28 19 47 0.5

Mexico / USA 1 1 <0.1

No. of Mixed National Origin Samples 149 14 23 186

% of Total 39 8 7 1.9

Part 3. Mixed National Origin Samples

Fresh F&V

Fresh F&V Processed F&V Formula

Processed F&V Formula

Appendix I. Page 2 of 3
Part 4. Unknown Origin Samples

Dairy Fish # of % of

BN BR CE CF CR GB MU NE PC PU RS SS WS AJ GJ IA IE RZ DF YF BU FS Samples Total

Unknown Origin 3 7 2 5 14 1 3 1 1 1 12 1 1 2 2 3 4 4 1 68

% of Total <1 1 <1 1 4 <1 1 <1 <1 <1 2 <1 1 1 1 2 2 1 <1 0.7

Sample Totals: 708 708 708 532 712 378 532 543 285 507 652 709 187 379 176 379 378 53 177 179 756 352 9,990

NOTE

1

 Excludes groundwater and untreated/finished drinking water samples.

Commodity Legend

AJ = Apple Juice FS = Fish, Salmon PC = Peaches

BN = Bananas GB = Green Beans PU = Plums

BR = Broccoli GJ = Grape Juice RS = Raspberries, Fresh

BU = Butter IA = Baby Food - Applesauce RZ = Raspberries, Frozen

CE = Celery IE = Baby Food - Peas SS = Summer Squash

CF = Cauliflower MU = Mushrooms WS = Winter Squash

CR = Carrots NE = Nectarines YF = Soy-based Infant Formula

DF = Diary-based Infant Formula

Fresh F&V Processed F&V Formula

Appendix I. Page 3 of 3
Appendix J

Import vs. Domestic Pesticide Residue Comparisons

PDP is designed to provide a comprehensive statistical picture of pesticide residues in the 

U.S. food supply, representing all sources, including imports. Most commodities consumed 

are generally produced in the United States with import components that vary by commodity. 

However, several commodities tested over the past several years were cyclical; that is, part 

of the year the commodity was produced domestically and part of the year it was imported. 

Appendix J compares residue data reported for samples originating in the United States with 

those of the same commodity from major exporting countries in 2013. Residue data for 

domestic nectarines are compared with data for samples originating in Chile. Residue data 

for domestic raspberries and summer squash are compared with data for samples originating 

in Mexico. Only residues detected in more than 10 percent of all samples are included in each 

comparison. All pesticides detected, except thiabendazole in nectarines, were registered in 

the United States. However, the profi les of residue fi ndings were markedly different in the 

United States samples versus samples from these exporting countries. The differences in 

residue detections between countries were likely due to the pesticides used in response to 

pest pressures based on differing environmental, climatic, and growing conditions. 
Pesticide Origin

# of Samples 

Analyzed

# of Samples 

w/ Detections

% of Samples 

w/ Detections

Acetamiprid United States 313 6 1.9

Chile 227 67 29.5

Boscalid United States 313 73 23.3

Chile 227 8 3.5

Cyhalothrin, Lambda United States 313 11 3.5

Chile 227 115 50.7

Fenhexamid United States 313 14 4.5

Chile 227 49 21.6

Fludioxonil United States 257 210 81.7

Chile 12 1 8.3

Indoxacarb United States 313 70 22.4

Chile 225 28 12.4

Iprodione United States 313 2 0.6

Chile 227 218 96.0

Methoxyfenozide United States 313 65 20.8

Chile 227 48 21.1

Propiconazole United States 313 114 36.4

Chile 227 28 12.3

Pyraclostrobin United States 312 53 17.0

Chile 227 2 0.9

Pyrimethanil United States 313 14 4.5

Chile 226 54 23.9

Spinosad United States 313 59 18.8

Chile 227 114 50.2

Tebuconazole United States 313 23 7.3

Chile 227 177 78.0

Thiabendazole United States 313 23 7.3

Chile 227 50 22.0

NOTE: The Limits of Detection (LODs) for pesticide detections in nectarines are listed in Appendix B.

Appendix J. Import vs. Domestic Pesticide Residue Comparisons

2013 Distribution of Residues for Nectarine Samples

Originating in Chile vs. United States

(Only Pesticides with Residue Detections in at least 10 Percent of all Samples)

Appendix J. Page 1 of 3
Pesticide Origin

# of Samples 

Analyzed

# of Samples 

w/ Detections

% of Samples 

w/ Detections

Bifenazate United States 253 78 30.8

Mexico 96 26 27.1

Boscalid United States 439 121 27.6

Mexico 211 38 18.0

Cypermethrin United States 439 65 14.8

Mexico 211 27 12.8

Cyprodinil United States 439 48 10.9

Mexico 211 27 12.8

Myclobutanil United States 439 79 18.0

Mexico 211 18 8.5

Pyraclostrobin United States 439 101 23.0

Mexico 211 39 18.5

Spinetoram United States 439 80 18.2

Mexico 211 6 2.8

Spinosad United States 253 26 10.3

Mexico 96 15 15.6

NOTE: The Limits of Detection (LODs) for pesticide detections in raspberries are listed in Appendix B.

(Only Pesticides with Residue Detections in at least 10 Percent of all Samples)

2013 Distribution of Residues for Raspberry Samples

Originating in Mexico vs. United States

Appendix J. Page 2 of 3
Pesticide Origin

# of Samples 

Analyzed

# of Samples 

w/ Detections

% of Samples 

w/ Detections

Endosulfan sulfate United States 394 47 11.9

Mexico 294 75 25.5

Imidacloprid United States 394 33 8.4

Mexico 294 74 25.2

Propamocarb hydrochloride United States 394 68 17.3

Mexico 294 8 2.7

NOTE: The Limits of Detection (LODs) for pesticide detections in summer squash are listed in Appendix B.

2013 Distribution of Residues for Summer Squash Samples

Originating in Mexico vs. United States

(Only Pesticides with Residue Detections in at least 10 Percent of all Samples)

Appendix J. Page 3 of 3
Appendix K

Pesticide Residues by Commodity

(Pairs with Residue Detections in at Least 5 Percent of Samples)

Appendix K shows 149 commodity/pesticide pairs (including metabolites, isomers, and 

degradates) with detections in at least 5 percent of the samples tested. The data shown 

include the range and mean of values detected and U.S. Environmental Protection Agency 

(EPA) tolerance references for each pair. The EPA tolerances cited in this appendix apply 

to 2013 and not to the current year. There may be instances where tolerances have been 

recently set or revoked that would have an effect on whether a residue is violative or not. 
APPENDIX K. PESTICIDE RESIDUES A

 BY COMMODITY B

(Pairs With Residue Detections in at Least 5 Percent of Samples)

% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

1 Apple Juice (6 pesticides)

Acetamiprid * I 15 379 57 0.003 - 0.019 0.007 1.0

Carbendazim (MBC) 1 F 28 379 106 0.001 - 0.035 0.006 2.0

Diphenylamine (DPA) F 17.7 379 67 0.002 - 0.066 0.019 10.0

Pyrimethanil F 5.5 379 21 0.11 - 0.23 0.155 14

Tetrahydrophthalimide (THPI) 2 FM 25.9 379 98 0.010 - 0.56 0.075 25.0

Thiabendazole F 25.1 379 95 0.003 - 0.27 0.051 5.0

2 Baby Food - Applesauce (7 pesticides)

Acetamiprid * I 23.5 379 89 0.011 - 0.053 0.021 1.0

Carbendazim (MBC) 1 F 10 379 38 0.010 - 0.058 0.026 2.0

Fenpropathrin I 6.6 379 25 0.002 ^ 0.002 5.0

Myclobutanil F 9.5 379 36 0.002 ^ 0.002 0.5

Pyridaben I 5.5 379 21 0.002 ^ 0.002 0.5

Pyrimethanil F 8.4 379 32 0.003 - 0.13 0.02 14

Thiabendazole F 6.9 379 26 0.019 - 0.12 0.055 5.0

3 Bananas (5 pesticides)

Azoxystrobin F 21.3 708 151 0.005 - 0.077 0.012 2.0

Buprofezin I 6.5 708 46 0.001 - 0.097 0.007 0.20

Imazalil F 36.3 708 257 0.005 - 0.10 0.018 3.0

Myclobutanil F 16.4 708 116 0.002 - 0.11 0.026 4.0

Thiabendazole F 54.9 708 389 0.006 - 0.16 0.043 3.0

4 Broccoli (3 pesticides)

Azoxystrobin F 10.6 708 75 0.002 - 0.46 0.037 3.0

DCPA H 9.9 707 70 0.005 - 0.063 0.02 5.0

Imidacloprid I 9.7 708 69 0.010 - 1.5 0.041 3.5

5 Butter (4 pesticides)

Bifenthrin * I 14.8 756 112 0.003 - 0.006 0.003 1.0

Cyhalothrin, Total 3 * I 20.4 756 154 0.006 - 0.036 0.012 10.0

Novaluron I 37.2 723 269 0.002 - 0.013 0.004 20

Permethrin

 Permethrin cis 4 IM 27.2 756 206 0.002 - 0.008 0.002 3.0

 Permethrin trans 4 IM 28.3 756 214 0.002 - 0.010 0.003 3.0

6 Carrots (8 pesticides)

Azoxystrobin F 7.7 712 55 0.010 - 0.031 0.011 0.5

Boscalid F 23 712 164 0.025 - 0.17 0.037 1.0

Diazinon I 5.3 712 38 0.002 - 0.038 0.009 0.75

Iprodione F 8.1 712 58 0.033 - 1.4 0.072 5.0

Linuron H 21.3 712 152 0.033 - 0.52 0.055 1.0

Metalaxyl/Mefenoxam 5 F 10.8 711 77 0.008 - 0.035 0.012 0.5

Pyraclostrobin F 15.5 711 110 0.008 - 0.035 0.01 0.4

Trifluralin H 24 712 171 0.003 - 0.18 0.017 1.0

7 Cauliflower (1 pesticide)

Imidacloprid I 39.8 532 212 0.002 - 0.36 0.007 3.5

8 Celery (19 pesticides)

Acephate

 Acephate (parent) * I 22 708 156 0.003 - 0.45 0.077 10

 Methamidophos 6

 * I 9.2 708 65 0.002 - 0.031 0.009 1

Acetamiprid * I 10.9 708 77 0.002 - 0.061 0.007 3.00

Appendix K. Page 1 of 4
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

Azoxystrobin F 17.4 708 123 0.002 - 0.42 0.038 30.0

Boscalid F 8.9 693 62 0.006 - 0.10 0.022 45

Chlorantraniliprole I 28.7 708 203 0.003 - 0.29 0.017 13

Cyromazine R 14 648 91 0.005 - 0.32 0.023 7.0

Deltamethrin 7 I 11 708 78 0.020 ^ 0.02 0.05

Dicloran F 37.6 708 266 0.004 - 2.5 0.126 15

Flonicamid I 9.7 708 69 0.002 - 0.10 0.027 4.0

Imidacloprid I 5.4 708 38 0.002 - 0.046 0.007 6.0

Linuron H 15.1 708 107 0.005 - 0.090 0.015 0.5

Malathion I 10.6 708 75 0.002 - 0.17 0.031 8

Methoxyfenozide I 15.7 708 111 0.002 - 0.096 0.013 25

Omethoate IM 7.3 708 52 0.004 - 0.049 0.01 2.0

Oxamyl I 5.6 708 40 0.003 - 0.071 0.019 10.0

Permethrin

 Permethrin cis IM 42.8 708 303 0.002 - 0.24 0.022 5.0

 Permethrin trans IM 40 708 283 0.002 - 0.27 0.023 5.0

Propiconazole F 27.4 708 194 0.010 - 0.15 0.024 5.0

Pyraclostrobin F 17.5 708 124 0.003 - 0.47 0.039 29.0

Thiamethoxam I 12.1 708 86 0.003 - 0.16 0.011 4.0

9 Grape Juice (6 pesticides)

Boscalid F 8 176 14 0.006 - 0.079 0.045 3.5

Carbaryl I 25.6 176 45 0.003 - 0.026 0.006 10

Fenhexamid F 6.2 176 11 0.020 - 0.082 0.062 4.0

Imidacloprid I 9.7 176 17 0.004 - 0.041 0.027 1.5

Methoxyfenozide I 9.7 176 17 0.003 - 0.008 0.005 1.0

Phosmet I 8 176 14 0.011 - 0.015 0.012 10

10 Green Beans (11 pesticides)

Acephate

 Acephate (parent) * I 25.9 378 98 0.030 - 2.6 0.399 3.0

 Methamidophos 6 * IM 26.5 378 100 0.020 - 0.86 0.159 1

Azoxystrobin F 30.7 378 116 0.001 - 0.076 0.016 3.0

Bifenthrin * I 10.6 378 40 0.040 - 0.13 0.067 0.6

Boscalid F 9.3 378 35 0.006 - 0.87 0.064 1.6

Chlorantraniliprole I 12.2 378 46 0.001 - 0.020 0.004 2.0

Dicloran F 5.3 378 20 0.11 - 1.5 0.493 20

Dimethoate I 5.3 378 20 0.001 - 0.63 0.117 2.0

Metalaxyl/Mefenoxam 5 F 5 378 19 0.001 - 0.018 0.004 0.2

Myclobutanil F 5.3 378 20 0.006 - 0.089 0.025 1.0

Pyraclostrobin F 7.7 378 29 0.001 - 0.52 0.024 0.5

Tebuconazole F 6.3 378 24 0.001 - 0.20 0.026 0.1

11 Mushrooms (1 pesticide)

Thiabendazole F 47.7 532 254 0.003 - 2.0 0.295 40.0

12 Nectarines (17 pesticides)

Acetamiprid * I 13.4 543 73 0.017 - 0.23 0.038 1.20

Boscalid F 15.1 543 82 0.002 - 0.19 0.036 3.5

Cyhalothrin, Lambda * I 23.2 543 126 0.003 - 0.055 0.009 0.50

Cyprodinil F 6.6 543 36 0.003 - 0.22 0.065 2.0

Fenhexamid F 11.6 543 63 0.008 - 0.98 0.15 10.0

Fludioxonil F 78.6 271 213 0.033 - 3.4 0.446 5.0

Indoxacarb I 18.1 541 98 0.003 - 0.083 0.014 0.90

Iprodione F 40.7 543 221 0.008 - 7.2 1.588 20.0

Methoxyfenozide I 20.8 543 113 0.003 - 0.18 0.027 3.0

Myclobutanil F 6.3 539 34 0.003 - 0.078 0.012 2.0

Propiconazole F 26.3 543 143 0.007 - 0.64 0.079 4.0

Pyraclostrobin F 10.3 542 56 0.002 - 0.10 0.026 2.5

Appendix K. Page 2 of 4
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

Pyrimethanil F 12.5 542 68 0.002 - 1.0 0.051 10

Spinetoram I 9 543 49 0.013 - 0.16 0.027 0.20

Spinosad I 32 543 174 0.010 - 0.11 0.017 0.20

Tebuconazole F 37 543 201 0.002 - 3.4 0.255 1.0

Thiabendazole F 13.6 543 74 0.003 - 1.8 0.036 NT

13 Peaches (25 pesticides)

Acetamiprid * I 5.3 285 15 0.011 - 0.14 0.041 1.20

Azoxystrobin F 6 285 17 0.002 - 0.13 0.033 1.5

Boscalid F 36.8 285 105 0.010 - 0.35 0.069 3.5

Buprofezin I 5.6 285 16 0.011 - 0.030 0.02 9.0

Captan F 13.7 285 39 0.027 - 1.2 0.234 15.0

Chlorantraniliprole I 25.3 285 72 0.021 - 0.15 0.043 4.0

Clothianidin * I 9.1 285 26 0.010 - 0.13 0.039 0.80

Cyfluthrin * I 13.3 285 38 0.006 - 0.12 0.03 0.3

Cyhalothrin, Total 3 * I 9.8 285 28 0.008 - 0.14 0.031 0.50

Cyprodinil F 7.7 285 22 0.011 - 1.0 0.218 2.0

Esfenvalerate+Fenvalerate Total * I 11.6 285 33 0.005 - 0.13 0.032 3.0

Fenbuconazole F 22.8 285 65 0.005 - 0.19 0.022 1.0

Fenpropathrin I 9.1 285 26 0.006 - 1.0 0.213 1.4

Fludioxonil F 76.5 285 218 0.006 - 2.4 0.638 5.0

Hexythiazox I 5.3 285 15 0.011 - 0.15 0.042 1.0

Indoxacarb I 6.7 285 19 0.010 - 0.035 0.02 0.90

Iprodione F 6.7 285 19 0.005 - 1.8 0.999 20.0

Methoxyfenozide I 18.6 285 53 0.010 - 0.11 0.026 3.0

Permethrin Total I 7.7 285 22 0.015 - 0.68 0.166 1.0

Phosmet I 14.7 285 42 0.005 - 0.45 0.078 10

Propiconazole F 45.6 285 130 0.011 - 0.91 0.18 4.0

Pyraclostrobin F 37.9 285 108 0.003 - 0.23 0.04 2.5

Pyrimethanil F 12.3 285 35 0.10 - 0.58 0.314 10

Spirodiclofen A 30.9 285 88 0.010 - 0.29 0.052 1.0

Tebuconazole F 11.2 285 32 0.005 - 0.28 0.038 1.0

14 Plums (6 pesticides)

Fludioxonil F 44.4 507 225 0.012 - 1.7 0.386 5.0

Iprodione F 51.7 507 262 0.005 - 6.4 0.904 20.0

Methoxyfenozide I 5.9 507 30 0.005 - 0.059 0.011 0.30

Propiconazole F 5.9 507 30 0.011 - 0.39 0.112 0.60

Pyrimethanil F 7.3 507 37 0.005 - 1.4 0.181 10

Tebuconazole F 16.6 507 84 0.010 - 2.5 0.12 1.0

15 Raspberries (13 pesticides)

Acetamiprid * I 5.5 652 36 0.003 - 1.5 0.115 1.6

Azoxystrobin F 8 652 52 0.003 - 0.34 0.062 5.0

Bifenazate A 29.9 351 105 0.005 - 1.5 0.151 5.0

Boscalid F 24.5 652 160 0.005 - 3.0 0.13 6.0

Cypermethrin * I 14.1 652 92 0.010 - 0.47 0.083 0.8

Cyprodinil F 11.5 652 75 0.003 - 1.7 0.146 10

Fludioxonil F 6.4 652 42 0.011 - 0.56 0.127 5.0

Hexythiazox I 9 652 59 0.005 - 0.38 0.066 1.0

Malathion I 6.4 652 42 0.005 - 0.16 0.029 8

Myclobutanil F 14.9 652 97 0.001 - 0.21 0.033 2.0

Pyraclostrobin F 21.6 652 141 0.001 - 0.40 0.035 4.0

Spinetoram I 13.2 652 86 0.005 - 0.37 0.037 0.70

Spinosad (parent) 8 I 11.7 351 41 0.003 - 0.21 0.026 0.7

 Spinosad A IM 8 301 24 0.008 - 0.44 0.065 0.7

 Spinosad D IM 5.6 301 17 0.005 - 0.10 0.022 0.7

Appendix K. Page 3 of 4
% of Number of Number of Range of Mean of EPA

Pest. Samples with Samples Samples with Detections, Detections, Tolerance,

Commodity / Pesticide Type Detections Analyzed Detections ppm ppm ppm

16 Summer Squash (5 pesticides)

Endosulfan sulfate 9 IM 17.5 709 124 0.005 - 0.12 0.029 1.0

Imidacloprid I 15.5 709 110 0.010 - 0.19 0.044 0.5

Propamocarb hydrochloride 10 F 10.7 709 76 0.006 - 0.56 0.119 1.5

Pyraclostrobin F 7.1 709 50 0.003 - 0.029 0.011 0.5

Thiamethoxam * I 15 709 106 0.003 - 0.36 0.031 0.2

17 Winter Squash (6 pesticides)

Bifenthrin * I 11.8 187 22 0.005 - 0.072 0.01 0.4

Endosulfan sulfate 9 IM 17.6 187 33 0.005 - 0.070 0.017 1.0

Imidacloprid I 22.5 187 42 0.010 - 0.13 0.024 0.5

Metalaxyl/Mefenoxam 5 F 9.1 187 17 0.003 - 0.057 0.01 1.0

Propamocarb hydrochloride 10 F 20.3 187 38 0.010 - 0.61 0.138 1.5

Thiamethoxam * I 15.5 187 29 0.003 - 0.011 0.003 0.2

NOTES

A Excludes environmental contaminants, which are listed in Appendix H.

B Excludes groundwater and finished/untreated drinking water samples, which are listed in Appendix F and G.

NT No tolerance established.

* Residue may result from food handling establishment (FHE) application.

1 From parent, benomyl.

2 Metabolite of captafol and captan.

3 Includes cyhalothrin lambda plus R157836 epimer.

4 Isomer of parent, permethrin.

5 Metalaxyl/mefenoxam are spatial isomers which are analytically indistinguishable via multiresidue methods, but have

separate registrations.

6 Specific tolerance established for methamidophos in celery and green beans as a possible result of an acephate application.

7 Includes parent, tralomethrin.

8 Total of spinosyns A and D.

9 From parent, endosulfan.

10 Analytically determined as the salt (hydrochloride).

Pesticide Types:

A = Acaricide I = Insecticide, IM = Insecticide Metabolite

F = Fungicide, FM = Fungicide Metabolite R = Insect Growth Regulator

H = Herbicide

Appendix K. Page 4 of 4
Appendix L

Number of Pesticides Detected per Sample

Appendix L shows the percentage of samples versus the number of pesticides detected per 

sample, excluding groundwater and drinking water samples. The graph and data on page 1 

show the overall number of samples and percentages (of total number of samples analyzed) 

for each detection group across all commodities. The table on page 2 shows the number of 

pesticides detected by individual commodity. For the 9,990 samples analyzed, 40.5 percent 

of the samples had no detectable pesticides, 23.5 percent had 1 pesticide, and 36 percent of 

the samples had more than 1 pesticide. 

This appendix reports the number of distinct pesticides rather than residues. A parent 

compound and its metabolites are reported as a single pesticide.
0 1 2 3 4 5 6 7 8 9 10 11 12 13

0 1 2 3 4 5 6 7 8 9 10 11 12 13

Number of

Samples 4,050 2,350 1,472 845 504 314 211 117 56 35 29 5 0 2

Percent of

Total Samples 40.5 23.5 14.7 8.5 5.0 3.1 2.1 1.2 0.6 0.4 0.3 0.05 0 0.02

TOTAL NUMBER OF SAMPLES = 9,990

NOTES

1

 Environmental contaminants, listed in Appendix H, have been excluded from the count of pesticides detected in this appendix. Parent

 compounds and their metabolites are combined to report the number of "pesticides" rather than the number of "residues."

2

 Excludes groundwater and finished/untreated drinking water samples.

Number of Pesticides Detected per Sample

Number of Pesticides Detected per Sample

APPENDIX L. SAMPLES vs. NUMBER OF PESTICIDES 1 DETECTED PER SAMPLE 2

50

40

30

20

10

Percent of Samples

40.5

14.7

23.5

3.1

5.0

8.5

0.6 0.4 1.2

2.1

Multiple pesticide detections may result from the application of more than one pesticide, spray drift, crop rotation, 

and/or cross-contamination.

0.3 0.05 0.02

Appendix L. Page 1 of 2
Commodity (# of samples) 0 1 2 3 4 5 6 7 8 9 10 11 12 13

Fresh Fruit and Vegetables:

Bananas (708) 15.1 37.3 38.8 7.8 1.0 -- -- -- -- -- -- -- -- --

Broccoli (708) 63.7 23.4 8.5 3.1 0.8 0.4 -- -- -- -- -- -- -- --

Carrots (712) 34.8 26.8 17.6 11.1 4.1 2.7 1.7 1.1 0.1 -- -- -- -- --

Cauliflower (532) 48.3 44.2 6.8 0.8 -- -- -- -- -- -- -- -- -- --

Celery (708) 4.5 10.3 16.1 20.3 16.7 12.3 10.2 5.5 2.3 1.4 0.4 -- -- --

Green Beans (378) 29.6 28.6 18.8 12.4 6.9 2.6 0.5 0.3 0.3 -- -- -- -- --

Mushrooms (532) 50.0 45.9 2.3 1.7 0.2 -- -- -- -- -- -- -- -- --

Nectarines (543) 2.8 10.1 15.8 15.8 16.6 15.8 11.6 6.3 3.5 0.7 0.6 0.2 -- 0.2

Peaches (285) 2.1 7.7 15.8 12.6 16.8 7.4 9.8 7.7 4.6 6.0 7.7 1.4 -- 0.4

Plums (507) 7.1 45.8 33.9 10.1 1.2 0.8 0.6 0.4 0.2 -- -- -- -- --

Raspberries (652) 29.3 23.8 14.7 12.9 10.4 6.0 2.0 0.5 0.3 0.2 -- -- -- --

Summer Squash (709) 47.1 23.0 14.2 7.9 4.4 2.0 1.1 0.3 -- -- -- -- -- --

Winter Squash (187) 27.8 34.2 20.3 10.7 3.2 1.6 1.1 1.1 -- -- -- -- -- --

Processed Fruit and Vegetables:

Apple Juice (379) 54.1 13.7 10.6 6.3 6.3 6.3 1.6 0.8 0.3 -- -- -- -- --

Baby Food - Applesauce (379) 48.8 23.5 17.4 7.7 2.1 0.5 -- -- -- -- -- -- -- --

Baby Food - Peas (378) 100 -- -- -- -- -- -- -- -- -- -- -- -- --

Grape Juice (176) 63.1 17.0 6.3 11.9 1.7 -- -- -- -- -- -- -- -- --

Raspberries, Frozen (53) 54.7 13.2 11.3 1.9 -- 1.9 3.8 1.9 3.8 5.7 1.9 -- -- --

Percent of Total Samples 35.4 25.2 15.9 9.0 5.5 3.7 2.5 1.4 0.7 0.4 0.3 0.06 -- 0.02

Actual Number of Samples 3,015 2,150 1,354 768 471 313 211 117 56 35 29 5 -- 2

Infant Formula Products: 

Infant Formula, Dairy-based (177) 100 -- -- -- -- -- -- -- -- -- -- -- -- --

Infant Formula, Soy-based (179) 99.4 0.6 -- -- -- -- -- -- -- -- -- -- -- --

Actual Number of Samples 355 1 -- -- -- -- -- -- -- -- -- -- -- --

Dairy Product: 

Butter (756) 43.8 25.9 15.6 10.2 4.4 0.1 -- -- -- -- -- -- -- --

Actual Number of Samples 331 196 118 77 33 1 -- -- -- -- -- -- -- --

Fish Product: 

Salmon (352) 99.1 0.9 -- -- -- -- -- -- -- -- -- -- -- --

Actual Number of Samples 349 3 -- -- -- -- -- -- -- -- -- -- -- --

NOTES

1 Environmental contaminants, listed in Appendix H, have been excluded from the count of pesticides detected in this appendix. Parent

compounds and their metabolites are combined to report the number of "pesticides" rather than the number of "residues." 

2 Excludes the 14 groundwater and 100 drinking water samples.

Percent

TOTAL NUMBER OF FRUIT & VEGETABLE SAMPLES = 8,526

APPENDIX L. SAMPLES vs. NUMBER OF PESTICIDES DETECTED PER SAMPLE

Number of Pesticides 1 Detected per Sample 2

Appendix L. Page 2 of 2
Appendix M

Fruit and Vegetable Samples Reported to the

U.S. Food and Drug Administration as

Exceeding the Tolerance

or Without Established Tolerance

(per Code of Federal Regulations, Title 40, Part 180)

Appendix M shows pesticide residues reported to the U.S. Food and Drug Administration 

(FDA) as exceeding the tolerance or residues for which no established tolerance was listed 

under the Code of Federal Regulations, Title 40, Part 180. In 2013, a total of 317 samples 

with 350 pesticides were reported to the FDA as Presumptive Tolerance Violations.

Pesticides exceeding the tolerance were detected in 23 samples including 1 sample of 

broccoli, 1 sample of celery, 4 samples of green beans, 11 nectarine samples, 1 sample 

of plums, 1 sample of fresh raspberries, and 4 samples of summer squash. Of those 23 

samples, 17 were reported as imported produce.

In addition, 301 samples were found to have pesticides for which no tolerance was established, 

including 286 fresh fruit and vegetable samples, 13 processed fruit/vegetable samples, and 

2 butter samples.

o 276 samples contained 1 pesticide for which no tolerance was established.

o 24 samples contained 2 pesticides for which no tolerance was established.

o 1 sample of green beans contained 3 pesticides for which no tolerance was established.

Seven of the 301 samples also contained 1 pesticide each that exceeded an established 

tolerance.

The columns under the Sample Origin heading provide the number of samples that were of 

domestic, imported, or unknown origin for each pesticide/commodity pair listed.

Appendix M also notes if metabolites (or isomers) were detected as part of the same sample. 

In instances where both parent and metabolite (or isomer) were detected, the Pesticide Data 

Program accounted for both as part of the same tolerance expression.

A number of the fi ndings shown in this appendix are less than 0.01 ppm. Levels below 0.01 

ppm are deemed by the U.S. FDA to be “not of regulatory signifi cance”.

The EPA tolerances cited in this appendix apply to 2013 and not to the current year. There 

may be instances where tolerances have been recently set or revoked that would have an 

effect on whether a residue is violative or not.
Residues Exceeding Established Tolerance

Commodity / Pesticide

Limit of 

Detection, 

ppm

Concentration 

Detected, 

ppm

EPA 

Tolerance 

Level, ppm

Country of 

Origin

1 Broccoli / Cypermethrin 0.010 6.6 2.0 Mexico

2 Celery / Myclobutanil 0.001 0.083 0.03 Mexico

3 Green Beans / Cyfluthrin 0.10 0.11 0.05 U.S.

4 Green Beans / Dinotefuran 0.040 0.17 0.01 U.S.

5 Green Beans / Dinotefuran 0.040 0.17 0.01 U.S.

6 Green Beans / Tebuconazole 0.001 0.2 0.1 U.S.

7 Nectarines / Tebuconazole 0.001 3.4 1.0 Chile

8 Nectarines / Tebuconazole 0.001 2.9 1.0 Chile

9 Nectarines / Tebuconazole 0.001 2.4 1.0 Chile

10 Nectarines / Tebuconazole 0.001 2.1 1.0 Chile

11 Nectarines / Tebuconazole 0.001 2.1 1.0 Chile

12 Nectarines / Tebuconazole 0.001 1.5 1.0 Chile

13 Nectarines / Tebuconazole 0.001 1.5 1.0 Chile

14 Nectarines / Tebuconazole 0.001 1.3 1.0 Chile

15 Nectarines / Tebuconazole 0.001 1.3 1.0 Chile

16 Nectarines / Tebuconazole 0.001 1.2 1.0 Chile

17 Nectarines / Tebuconazole 0.001 1.2 1.0 Chile

18 Plums / Tebuconazole 0.010 2.5 1.0 Chile

19 Raspberries / Abamectin 0.020 0.095 0.01 Mexico

20 Summer Squash / Acephate 0.030 0.039 0.02 U.S.

21 Summer Squash / Tetrahydrophthalimide (THPI) 1 0.010 0.11 0.05 Mexico

22 Summer Squash / Tetrahydrophthalimide (THPI) 1 0.010 0.092 0.05 Mexico

23 Summer Squash / Thiamethoxam 0.060 0.36 0.2 U.S.

APPENDIX M. SAMPLES REPORTED TO FDA AS EXCEEDING THE TOLERANCE

OR WITHOUT ESTABLISHED TOLERANCE

(per Code of Federal Regulations, Title 40, Part 180)

Appendix M. Page 1 of 3
Commodity / Pesticide U.S. Import Unk.

1 Baby Food - Applesauce (1 pesticide)

Iprodione 357 1 0.3 0.002 ^ 0.001 ^ 1 0 0

2 Broccoli (7 pesticides)

Carbendazim (MBC) 708 1 0.1 0.049 ^ 0.010 ^ 0 1 0

Carbofuran (parent) 708 1 0.1 0.026 ^ 0.010 ^ 0 1 0

 3-Hydroxycarbofuran 2 708 1 0.1 0.017 ^ 0.010 ^ 0 1 0

Chlorpropham 707 3 0.4 0.008 - 0.013 0.005 ^ 2 1 0

Dicloran 707 1 0.1 0.035 ^ 0.005 ^ 1 0 0

Pronamide 707 1 0.1 0.007 ^ 0.005 ^ 1 0 0

Propamocarb hydrochloride 708 3 0.4 0.011 - 0.041 0.010 ^ 3 0 0

Tebuconazole 707 1 0.1 0.037 ^ 0.005 ^ 1 0 0

3 Butter (1 pesticide)

Chlorpropham 756 2 0.3 0.002 - 0.004 0.001 - 0.004 2 0 0

4 Carrots (3 pesticides)

Heptachlor epoxide cis 712 4 0.6 0.007 - 0.016 0.004 ^ 0 4 0

Quintozene - PCNB (parent)

 Pentachloroaniline (PCA) 712 35 4.9 0.003 - 0.010 0.002 ^ 20 15 0

 Pentachlorobenzene (PCB) 3 712 1 0.1 0.008 ^ 0.001 ^ 1 0 0

Phosmet 711 4 0.6 0.005 - 0.017 0.003 - 0.010 0 4 0

5 Cauliflower (3 pesticides)

Chlorpropham 532 9 1.7 0.002 - 0.007 0.001 ^ 9 0 0

Fenbuconazole 532 1 0.2 0.002 ^ 0.001 ^ 0 1 0

Pronamide 532 1 0.2 0.002 ^ 0.001 ^ 1 0 0

6 Celery (11 pesticides)

Carbendazim (MBC) 708 1 0.1 0.002 ^ 0.001 - 0.005 0 1 0

Chlorpropham 708 4 0.6 0.002 - 0.009 0.001 - 0.005 4 0 0

DCPA 708 16 2.3 0.002 - 0.011 0.001 - 0.003 16 0 0

Difenoconazole 708 2 0.3 0.004 - 0.006 0.003 - 0.005 2 0 0

Iprodione 376 1 0.3 0.006 ^ 0.005 - 0.009 1 0 0

Pendimethalin 708 5 0.7 0.002 - 0.007 0.001 - 0.005 1 4 0

Pentachloroaniline (PCA) 708 1 0.1 0.002 ^ 0.001 - 0.003 0 1 0

Pronamide 708 2 0.3 0.004 - 0.007 0.001 - 0.003 2 0 0

Propamocarb hydrochloride 4 346 3 0.9 0.011 - 0.035 0.010 ^ 3 0 0

Pyrimethanil 708 1 0.1 0.002 ^ 0.001 - 0.005 1 0 0

Tebuconazole 708 1 0.1 0.010 ^ 0.002 - 0.010 0 1 0

7 Grape Juice (1 pesticide)

Thiabendazole 176 1 0.6 0.003 ^ 0.003 ^ 1 0 0

8 Green Beans (9 pesticides)

Carbofuran (parent) 378 2 0.5 0.002 ^ 0.001 ^ 1 1 0

 3-Hydroxycarbofuran 2 378 1 0.3 0.004 ^ 0.002 ^ 0 1 0

Dimethomorph 378 1 0.3 0.036 ^ 0.001 ^ 0 1 0

Fenamidone 378 1 0.3 0.001 ^ 0.001 ^ 0 1 0

Fenpropathrin 378 1 0.3 0.067 ^ 0.050 ^ 0 1 0

Fluopicolide 378 1 0.3 0.007 ^ 0.002 ^ 1 0 0

Oxamyl 378 1 0.3 0.002 ^ 0.002 ^ 0 1 0

Propamocarb hydrochloride 4 378 6 1.6 0.001 - 0.14 0.001 ^ 2 3 1

Pyrimethanil 378 2 0.5 0.003 - 0.006 0.001 ^ 2 0 0

Trifloxystrobin 378 6 1.6 0.001 - 0.023 0.001 ^ 1 5 0

9 Mushrooms (2 pesticides)

Carbendazim (MBC) 532 5 0.9 0.011 - 0.56 0.001 ^ 3 2 0

o-Phenylphenol 5 532 7 1.3 0.005 - 0.035 0.005 ^ 7 0 0

Sample Origin

Distribution of Residues with No Tolerance Listed in 40 CFR, Part 180, 

Range of 

LODs, ppm

Number of 

Samples

Samples 

Reported

% of 

Samples 

Range of Values 

Detected, ppm

by Commodity/Pesticide

Appendix M. Page 2 of 3
Commodity / Pesticide U.S. Import Unk.

Range of Sample Origin

LODs, ppm

Number of 

Samples

Samples 

Reported

% of 

Samples 

Range of Values 

Detected, ppm

10 Nectarines (7 pesticides)

Azinphos methyl 543 3 0.6 0.008 - 0.080 0.005 ^ 0 3 0

Carbendazim (MBC) 543 2 0.4 0.005 - 0.026 0.003 ^ 1 1 0

Dimethoate 543 1 0.2 0.005 ^ 0.003 ^ 1 0 0

Imazalil 543 22 4.1 0.007 - 0.29 0.004 ^ 11 11 0

Penconazole 543 1 0.2 0.026 ^ 0.003 ^ 1 0 0

Permethrin Total 6 543 1 0.2 0.21 ^ 0.004 ^ 1 0 0

Thiabendazole 543 74 13.6 0.003 - 1.8 0.002 ^ 23 50 1

11 Peaches (2 pesticides)

Chlorpropham 285 3 1.1 0.011 - 0.013 0.005 ^ 3 0 0

Diphenylamine (DPA) 285 1 0.4 0.007 ^ 0.005 ^ 1 0 0

12 Plums (3 pesticides)

Chlorpropham 507 1 0.2 0.006 ^ 0.005 ^ 1 0 0

Imazalil 507 1 0.2 0.013 ^ 0.005 ^ 1 0 0

Thiabendazole 507 9 1.8 0.005 - 0.091 0.005 ^ 3 6 0

13 Raspberries, Fresh (9 pesticides)

Buprofezin 652 1 0.2 0.002 ^ 0.001 - 0.005 1 0 0

Carbendazim (MBC) 652 3 0.5 0.007 - 0.015 0.005 ^ 1 2 0

Chlorpropham 652 7 1.1 0.006 - 0.13 0.005 - 0.020 4 3 0

DCPA 652 3 0.5 0.003 - 0.005 0.003 - 0.010 2 1 0

Difenoconazole 652 1 0.2 0.098 ^ 0.005 ^ 0 1 0

Forchlorfenuron 351 3 0.9 0.003 - 0.004 0.003 ^ 1 2 0

Methoxyfenozide 652 1 0.2 0.026 ^ 0.005 - 0.006 0 1 0

Pyrimethanil 652 14 2.1 0.002 - 0.041 0.002 - 0.005 10 4 0

Spiromesifen 351 1 0.3 0.008 ^ 0.005 ^ 0 1 0

14 Raspberries, Frozen (4 pesticides)

Carbendazim (MBC) 53 8 15.1 0.006 - 0.22 0.005 ^ 0 8 0

Pyridaben 53 1 1.9 0.004 ^ 0.001 - 0.003 0 1 0

Pyrimethanil 53 4 7.5 0.007 - 0.14 0.002 - 0.005 0 4 0

Trifloxystrobin 53 1 1.9 0.011 ^ 0.003 - 0.005 0 1 0

15 Summer Squash (3 pesticides)

Pentachloroaniline (PCA) 709 11 1.6 0.003 - 0.018 0.003 - 0.12 5 6 0

Pronamide 363 1 0.3 0.003 ^ 0.003 ^ 1 0 0

Quinoxyfen 363 4 1.1 0.004 - 0.010 0.003 ^ 1 3 0

16 Winter Squash (3 pesticides)

Chlorpropham 187 2 1.1 0.010 ^ 0.006 ^ 1 1 0

Dimethoate 187 1 0.5 0.021 ^ 0.002 ^ 0 1 0

 Omethoate 7 187 1 0.5 0.052 ^ 0.003 ^ 0 1 0

Fenbuconazole 187 2 1.1 0.010 ^ 0.006 ^ 0 2 0

NOTES

1 Tetrahydrophthalimide (THPI) is a metabolite of captafol and captan.

2 One broccoli sample and one green bean sample contained both the parent, Carbofuran, and its metabolite, 3-Hydroxycarbofuran.

3 One carrot sample contained both the PCA and PCB metabolites.

4 Propamocarb analytically determined as the salt (hydrochloride).

5 o-Phenylphenol is a fungicide with a number of crop tolerances. It is also an ingredient in many cleaning products and is

used in the paper manufacturing process. Residues of o-Phenylphenol may be the result of direct use, transfer across

commodities, or may originate from various paper and cleaning products.

6 Permethrin Total includes the cis permethrin isomer plus the trans permethrin isomer.

7 Omethoate is a metabolite of the parent, Dimethoate. One winter squash sample contained both Dimethoate and Omethoate.

Note:

For those pesticide/commodity pairs where the minimum detected value is less than the limit of quantitation (three times

the limit of detection), the reported values are estimates. In a few cases, this may apply to the maximum detected value.

Appendix M. Page 3 of 3
PESTICIDE DATA PROGRAM

 Annual Summary, Calendar Year 2013

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